# Supplementary Information (SI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2025

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_xjj_2bd_auto
_database_code_depnum_ccdc_archive 'CCDC 2429793'
loop_
_audit_author_name
_audit_author_address
'Yaoguo Shen'
;Minjiang University
China
;
_audit_update_record             
;
2025-03-09 deposited with the CCDC.	2025-05-06 downloaded from the CCDC.
;
_audit_creation_date             2024-10-29
_audit_creation_method           
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         '2(C7 H5 F N O5 Sb)'
_chemical_formula_sum            'C14 H10 F2 N2 O10 Sb2'
_chemical_formula_weight         647.74
_chemical_melting_point          ?
_chemical_oxdiff_formula         'C H N O Sb F'
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   8.6106(5)
_cell_length_b                   22.0552(11)
_cell_length_c                   10.2958(5)
_cell_angle_alpha                90
_cell_angle_beta                 108.674(6)
_cell_angle_gamma                90
_cell_volume                     1852.33(18)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    5666
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      26.7960
_cell_measurement_theta_min      1.8430
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    2.996
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.76208
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
CrysAlisPro 1.171.42.93a (Rigaku Oxford Diffraction, 2023)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            ?
_exptl_crystal_density_diffrn    2.323
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             1232
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0203
_diffrn_reflns_av_unetI/netI     0.0311
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.948
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -27
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -9
_diffrn_reflns_number            9033
_diffrn_reflns_point_group_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.948
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         26.879
_diffrn_reflns_theta_min         1.847
_diffrn_ambient_temperature      293(2)
_diffrn_detector                 'Hybrid Pixel Array Detector'
_diffrn_detector_area_resol_mean 10.0000
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.948
_diffrn_measurement_details      
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
#--------------------------------------------------------------------------
  1  ω     58.00  93.00   0.50    3.02    --   16.00  82.00  30.00   70
  2  ω    -15.00  48.00   0.50    3.02    --   16.00  61.00-120.00  126
  3  ω     -9.00 105.00   0.50    3.02    --   16.00  77.00 120.00  228
  4  ω    -63.00  47.00   0.50    3.02    --   16.00 -61.00-120.00  220
  5  ω    -16.00  45.00   0.50    3.02    --   16.00  82.00  30.00  122
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  
'XtaLAB Pro II AFC12 (RINC): Kappa dual home/near'
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_type       
'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11      0.0128907000
_diffrn_orient_matrix_UB_12      -0.0305873000
_diffrn_orient_matrix_UB_13      -0.0151412000
_diffrn_orient_matrix_UB_21      -0.0029439000
_diffrn_orient_matrix_UB_22      0.0085799000
_diffrn_orient_matrix_UB_23      -0.0671616000
_diffrn_orient_matrix_UB_31      0.0859287000
_diffrn_orient_matrix_UB_32      0.0049271000
_diffrn_orient_matrix_UB_33      0.0234791000
_diffrn_oxdiff_digest_frames     
;
01e50f9dc481a8eea70cd71cb82640c61f000250965
;
_diffrn_oxdiff_digest_hkl        
;
01614f1a4fb0e02a593e4f831665105e4a3709
;
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'micro-focus sealed X-ray tube'
_diffrn_source_type              'Rigaku (Mo) X-ray Source'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                3343
_reflns_number_total             3774
_reflns_odcompleteness_completeness 98.28
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     26.32
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'CrysAlisPro 1.171.42.93a (Rigaku OD, 2023)'
_computing_data_collection       'CrysAlisPro 1.171.42.93a (Rigaku OD, 2023)'
_computing_data_reduction        'CrysAlisPro 1.171.42.93a (Rigaku OD, 2023)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'olex2.solve (Bourhis et al., 2015)'
_refine_diff_density_max         0.406
_refine_diff_density_min         -0.765
_refine_diff_density_rms         0.092
_refine_ls_extinction_coef       0.00224(10)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
_refine_ls_goodness_of_fit_ref   1.047
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     284
_refine_ls_number_reflns         3774
_refine_ls_number_restraints     6
_refine_ls_R_factor_all          0.0279
_refine_ls_R_factor_gt           0.0237
_refine_ls_restrained_S_all      1.047
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0226P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0511
_refine_ls_wR_factor_ref         0.0533
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
 At 1.5 times of:
  All O(H,H) groups
2. Restrained distances
 O5-H5A = O5-H5B
 0.85 with sigma of 0.02
 O8-H8A = O8-H8B
 0.85 with sigma of 0.02
 H5A-H5B
 1.34 with sigma of 0.04
 H8A-H8B
 1.34 with sigma of 0.04
3.a Aromatic/amide H refined with riding coordinates:
 C2(H2), C3(H3), C4(H4), C10(H10), C11(H11), C12(H12)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     iterative
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Sb1 Sb 0.67634(2) 0.58004(2) 0.48610(2) 0.02303(7) Uani 1 1 d . . . . .
F2 F 0.85607(19) 0.56457(8) 0.41723(17) 0.0342(4) Uani 1 1 d . . . . .
O1 O 0.5880(3) 0.75227(10) 0.3059(3) 0.0665(9) Uani 1 1 d . . . . .
O2 O 0.6997(3) 0.67396(9) 0.4405(2) 0.0367(6) Uani 1 1 d . . . . .
O3 O 0.5881(2) 0.48778(9) 0.37363(19) 0.0322(5) Uani 1 1 d . . . . .
O4 O 0.4311(3) 0.44366(10) 0.1811(2) 0.0522(7) Uani 1 1 d . . . . .
O5 O 0.9206(3) 0.61992(10) 0.6729(2) 0.0463(7) Uani 1 1 d D . . . .
H5A H 0.951(5) 0.5928(12) 0.734(3) 0.070 Uiso 1 1 d DR . . . .
H5B H 0.942(5) 0.6514(10) 0.721(3) 0.070 Uiso 1 1 d DR . . . .
N1 N 0.5312(3) 0.59552(10) 0.2669(2) 0.0248(6) Uani 1 1 d . . . . .
C1 C 0.5062(4) 0.65320(13) 0.2240(3) 0.0309(7) Uani 1 1 d . . . . .
C2 C 0.3994(4) 0.66747(15) 0.0971(3) 0.0403(9) Uani 1 1 d . . . . .
H2 H 0.382615 0.707604 0.068294 0.048 Uiso 1 1 calc R . . . .
C3 C 0.3172(4) 0.62097(17) 0.0129(3) 0.0455(10) Uani 1 1 d . . . . .
H3 H 0.243612 0.629680 -0.073252 0.055 Uiso 1 1 calc R . . . .
C4 C 0.3445(4) 0.56184(15) 0.0565(3) 0.0373(8) Uani 1 1 d . . . . .
H4 H 0.291354 0.530170 0.000020 0.045 Uiso 1 1 calc R . . . .
C5 C 0.4524(4) 0.55041(14) 0.1859(3) 0.0275(7) Uani 1 1 d . . . . .
C6 C 0.4926(4) 0.48803(14) 0.2495(3) 0.0327(8) Uani 1 1 d . . . . .
C7 C 0.6025(4) 0.69803(14) 0.3299(3) 0.0369(8) Uani 1 1 d . . . . .
Sb2 Sb 0.81676(2) 0.38964(2) 0.49456(2) 0.02302(7) Uani 1 1 d . . . . .
F1 F 0.63145(19) 0.37153(8) 0.55584(17) 0.0372(4) Uani 1 1 d . . . . .
O6 O 0.9979(3) 0.52070(9) 0.8275(2) 0.0457(6) Uani 1 1 d . . . . .
O7 O 0.8324(2) 0.47721(9) 0.63642(19) 0.0319(5) Uani 1 1 d . . . . .
O8 O 0.6240(3) 0.34839(10) 0.2862(2) 0.0477(7) Uani 1 1 d D . . . .
H8A H 0.556(4) 0.3761(12) 0.244(3) 0.072 Uiso 1 1 d DR . . . .
H8B H 0.567(4) 0.3156(11) 0.280(4) 0.072 Uiso 1 1 d DR . . . .
O9 O 0.8637(2) 0.29501(9) 0.50920(18) 0.0334(5) Uani 1 1 d . . . . .
O10 O 0.9756(3) 0.21560(9) 0.6407(2) 0.0454(6) Uani 1 1 d . . . . .
N2 N 0.9610(3) 0.37043(10) 0.7118(2) 0.0227(5) Uani 1 1 d . . . . .
C8 C 0.9416(4) 0.47697(14) 0.7539(3) 0.0297(7) Uani 1 1 d . . . . .
C9 C 1.0081(4) 0.41417(13) 0.8059(3) 0.0255(7) Uani 1 1 d . . . . .
C10 C 1.1117(4) 0.40256(14) 0.9359(3) 0.0335(8) Uani 1 1 d . . . . .
H10 H 1.143409 0.433455 1.000478 0.040 Uiso 1 1 calc R . . . .
C11 C 1.1681(4) 0.34375(15) 0.9688(3) 0.0372(8) Uani 1 1 d . . . . .
H11 H 1.239304 0.334810 1.055753 0.045 Uiso 1 1 calc R . . . .
C12 C 1.1176(4) 0.29874(14) 0.8715(3) 0.0346(8) Uani 1 1 d . . . . .
H12 H 1.152763 0.258979 0.892268 0.042 Uiso 1 1 calc R . . . .
C13 C 1.0138(4) 0.31363(13) 0.7425(3) 0.0268(7) Uani 1 1 d . . . . .
C14 C 0.9495(4) 0.27002(14) 0.6254(3) 0.0299(7) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sb1 F2 1.9279(16) . ?
Sb1 O2 2.147(2) . ?
Sb1 O3 2.3442(19) . ?
Sb1 O5 2.511(2) . ?
Sb1 N1 2.228(2) . ?
O1 C7 1.220(3) . ?
O2 C7 1.292(3) . ?
O3 C6 1.279(3) . ?
O4 C6 1.223(3) . ?
O5 H5A 0.850(17) . ?
O5 H5B 0.837(17) . ?
N1 C1 1.341(3) . ?
N1 C5 1.336(3) . ?
C1 C2 1.372(4) . ?
C1 C7 1.508(4) . ?
C2 H2 0.9300 . ?
C2 C3 1.383(4) . ?
C3 H3 0.9300 . ?
C3 C4 1.375(5) . ?
C4 H4 0.9300 . ?
C4 C5 1.382(4) . ?
C5 C6 1.515(4) . ?
Sb2 F1 1.9361(16) . ?
Sb2 O7 2.3991(19) . ?
Sb2 O8 2.430(2) . ?
Sb2 O9 2.122(2) . ?
Sb2 N2 2.224(2) . ?
O6 C8 1.226(3) . ?
O7 C8 1.273(3) . ?
O8 H8A 0.863(17) . ?
O8 H8B 0.867(17) . ?
O9 C14 1.310(3) . ?
O10 C14 1.222(3) . ?
N2 C9 1.335(3) . ?
N2 C13 1.336(3) . ?
C8 C9 1.528(4) . ?
C9 C10 1.374(4) . ?
C10 H10 0.9300 . ?
C10 C11 1.388(4) . ?
C11 H11 0.9300 . ?
C11 C12 1.378(4) . ?
C12 H12 0.9300 . ?
C12 C13 1.382(4) . ?
C13 C14 1.502(4) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
F2 Sb1 O2 87.02(8) . . ?
F2 Sb1 O3 80.57(7) . . ?
F2 Sb1 O5 76.66(8) . . ?
F2 Sb1 N1 84.87(8) . . ?
O2 Sb1 O3 140.13(7) . . ?
O2 Sb1 O5 73.46(7) . . ?
O2 Sb1 N1 72.08(8) . . ?
O3 Sb1 O5 137.89(7) . . ?
N1 Sb1 O3 69.19(7) . . ?
N1 Sb1 O5 141.49(8) . . ?
C7 O2 Sb1 120.63(19) . . ?
C6 O3 Sb1 119.52(19) . . ?
Sb1 O5 H5A 108(3) . . ?
Sb1 O5 H5B 136(3) . . ?
H5A O5 H5B 101(3) . . ?
C1 N1 Sb1 117.24(19) . . ?
C5 N1 Sb1 121.78(19) . . ?
C5 N1 C1 120.3(3) . . ?
N1 C1 C2 121.3(3) . . ?
N1 C1 C7 113.0(3) . . ?
C2 C1 C7 125.7(3) . . ?
C1 C2 H2 120.7 . . ?
C1 C2 C3 118.7(3) . . ?
C3 C2 H2 120.7 . . ?
C2 C3 H3 120.0 . . ?
C4 C3 C2 119.9(3) . . ?
C4 C3 H3 120.0 . . ?
C3 C4 H4 120.7 . . ?
C3 C4 C5 118.7(3) . . ?
C5 C4 H4 120.7 . . ?
N1 C5 C4 121.1(3) . . ?
N1 C5 C6 114.0(3) . . ?
C4 C5 C6 124.9(3) . . ?
O3 C6 C5 114.9(3) . . ?
O4 C6 O3 126.4(3) . . ?
O4 C6 C5 118.7(3) . . ?
O1 C7 O2 125.3(3) . . ?
O1 C7 C1 120.0(3) . . ?
O2 C7 C1 114.8(3) . . ?
F1 Sb2 O7 81.90(7) . . ?
F1 Sb2 O8 79.00(8) . . ?
F1 Sb2 O9 86.10(8) . . ?
F1 Sb2 N2 83.47(8) . . ?
O7 Sb2 O8 136.74(7) . . ?
O9 Sb2 O7 140.92(6) . . ?
O9 Sb2 O8 75.83(7) . . ?
O9 Sb2 N2 73.08(8) . . ?
N2 Sb2 O7 68.69(7) . . ?
N2 Sb2 O8 145.11(8) . . ?
C8 O7 Sb2 117.11(18) . . ?
Sb2 O8 H8A 110(2) . . ?
Sb2 O8 H8B 126(2) . . ?
H8A O8 H8B 106(3) . . ?
C14 O9 Sb2 121.17(18) . . ?
C9 N2 Sb2 122.28(19) . . ?
C9 N2 C13 120.3(2) . . ?
C13 N2 Sb2 117.03(19) . . ?
O6 C8 O7 127.6(3) . . ?
O6 C8 C9 117.8(3) . . ?
O7 C8 C9 114.6(3) . . ?
N2 C9 C8 114.1(3) . . ?
N2 C9 C10 121.6(3) . . ?
C10 C9 C8 124.3(3) . . ?
C9 C10 H10 120.7 . . ?
C9 C10 C11 118.6(3) . . ?
C11 C10 H10 120.7 . . ?
C10 C11 H11 120.3 . . ?
C12 C11 C10 119.4(3) . . ?
C12 C11 H11 120.3 . . ?
C11 C12 H12 120.5 . . ?
C11 C12 C13 118.9(3) . . ?
C13 C12 H12 120.5 . . ?
N2 C13 C12 121.1(3) . . ?
N2 C13 C14 113.6(2) . . ?
C12 C13 C14 125.3(3) . . ?
O9 C14 C13 114.8(3) . . ?
O10 C14 O9 123.9(3) . . ?
O10 C14 C13 121.4(3) . . ?

loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
_geom_hbond_publ_flag
O5 H5A O6 0.850(17) 1.833(18) 2.663(3) 165(3) . yes
O5 H5B O10 0.837(17) 1.973(19) 2.800(3) 169(4) 2_756 yes
O8 H8A O4 0.863(17) 1.829(18) 2.682(3) 170(4) . yes
O8 H8B O1 0.867(17) 1.94(2) 2.760(3) 158(3) 2_645 yes

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Sb1 O2 C7 O1 167.3(3) . . . . ?
Sb1 O2 C7 C1 -14.6(4) . . . . ?
Sb1 O3 C6 O4 -176.2(3) . . . . ?
Sb1 O3 C6 C5 2.5(4) . . . . ?
Sb1 N1 C1 C2 -170.6(2) . . . . ?
Sb1 N1 C1 C7 8.0(4) . . . . ?
Sb1 N1 C5 C4 170.7(2) . . . . ?
Sb1 N1 C5 C6 -9.1(4) . . . . ?
N1 C1 C2 C3 -0.1(5) . . . . ?
N1 C1 C7 O1 -178.1(3) . . . . ?
N1 C1 C7 O2 3.7(4) . . . . ?
N1 C5 C6 O3 3.9(4) . . . . ?
N1 C5 C6 O4 -177.3(3) . . . . ?
C1 N1 C5 C4 0.3(5) . . . . ?
C1 N1 C5 C6 -179.5(3) . . . . ?
C1 C2 C3 C4 -0.6(5) . . . . ?
C2 C1 C7 O1 0.4(6) . . . . ?
C2 C1 C7 O2 -177.8(3) . . . . ?
C2 C3 C4 C5 1.1(5) . . . . ?
C3 C4 C5 N1 -1.0(5) . . . . ?
C3 C4 C5 C6 178.7(3) . . . . ?
C4 C5 C6 O3 -175.9(3) . . . . ?
C4 C5 C6 O4 2.9(5) . . . . ?
C5 N1 C1 C2 0.3(5) . . . . ?
C5 N1 C1 C7 178.8(3) . . . . ?
C7 C1 C2 C3 -178.5(3) . . . . ?
Sb2 O7 C8 O6 160.6(3) . . . . ?
Sb2 O7 C8 C9 -19.1(3) . . . . ?
Sb2 O9 C14 O10 177.5(2) . . . . ?
Sb2 O9 C14 C13 -1.8(4) . . . . ?
Sb2 N2 C9 C8 5.1(4) . . . . ?
Sb2 N2 C9 C10 -172.9(2) . . . . ?
Sb2 N2 C13 C12 173.6(2) . . . . ?
Sb2 N2 C13 C14 -6.5(3) . . . . ?
O6 C8 C9 N2 -169.7(3) . . . . ?
O6 C8 C9 C10 8.2(5) . . . . ?
O7 C8 C9 N2 10.1(4) . . . . ?
O7 C8 C9 C10 -172.0(3) . . . . ?
N2 C9 C10 C11 0.1(5) . . . . ?
N2 C13 C14 O9 5.5(4) . . . . ?
N2 C13 C14 O10 -173.8(3) . . . . ?
C8 C9 C10 C11 -177.7(3) . . . . ?
C9 N2 C13 C12 0.1(5) . . . . ?
C9 N2 C13 C14 180.0(3) . . . . ?
C9 C10 C11 C12 -0.7(5) . . . . ?
C10 C11 C12 C13 1.0(5) . . . . ?
C11 C12 C13 N2 -0.7(5) . . . . ?
C11 C12 C13 C14 179.4(3) . . . . ?
C12 C13 C14 O9 -174.7(3) . . . . ?
C12 C13 C14 O10 6.1(5) . . . . ?
C13 N2 C9 C8 178.2(3) . . . . ?
C13 N2 C9 C10 0.2(5) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details 
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_oxdiff_exptl_absorpt_empirical_full_max 1.226
_oxdiff_exptl_absorpt_empirical_full_min 0.832
