# Supplementary Information (SI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2025

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_2
_database_code_depnum_ccdc_archive 'CCDC 2246126'
loop_
_audit_author_name
_audit_author_address
'Huang Hongyu'
;Xinjiang University
China
;
_audit_update_record             
;
2023-03-03 deposited with the CCDC.	2025-05-06 downloaded from the CCDC.
;
_audit_creation_date             2022-08-16
_audit_creation_method           
;
Olex2 1.3
(compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6226)
;
_shelx_SHELXL_version_number     2014/7
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'Cd4 Na3 O18 P5'
_chemical_formula_sum            'Cd4 Na3 O18 P5'
_chemical_formula_weight         961.42
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Cd Cd -0.8075 1.2024 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   6.7307(3)
_cell_length_b                   9.6642(5)
_cell_length_c                   11.5063(6)
_cell_angle_alpha                98.2750(10)
_cell_angle_beta                 92.1390(10)
_cell_angle_gamma                90.6220(10)
_cell_volume                     740.04(6)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    5813
_cell_measurement_temperature    296.15
_cell_measurement_theta_max      25.02
_cell_measurement_theta_min      2.97
_shelx_estimated_absorpt_T_max   0.567
_shelx_estimated_absorpt_T_min   0.567
_exptl_absorpt_coefficient_mu    6.406
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_type   none
_exptl_absorpt_process_details   ?
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    4.315
_exptl_crystal_density_meas      .
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             888
_exptl_crystal_size_max          0.1
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.1
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0531
_diffrn_reflns_av_unetI/netI     0.0448
_diffrn_reflns_Laue_measured_fraction_full 0.994
_diffrn_reflns_Laue_measured_fraction_max 0.994
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            14860
_diffrn_reflns_point_group_measured_fraction_full 0.994
_diffrn_reflns_point_group_measured_fraction_max 0.994
_diffrn_reflns_theta_full        25.050
_diffrn_reflns_theta_max         25.050
_diffrn_reflns_theta_min         2.130
_diffrn_ambient_temperature      296.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_source_current           30.0
_diffrn_source_power             1.5
_diffrn_source_voltage           50.0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                2186
_reflns_number_total             2599
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2014/7 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_refine_diff_density_max         1.399
_refine_diff_density_min         -1.284
_refine_diff_density_rms         0.210
_refine_ls_extinction_coef       0.0024(2)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2014/7 (Sheldrick 2014'
_refine_ls_goodness_of_fit_ref   1.050
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     262
_refine_ls_number_reflns         2599
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0456
_refine_ls_R_factor_gt           0.0328
_refine_ls_restrained_S_all      1.050
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0071P)²+6.4634P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0543
_refine_ls_wR_factor_ref         0.0591
_refine_special_details          ?
_olex2_refinement_description    
;
1. Shared sites
{Cd2, Na2}
{Cd3, Na3}
{Cd1, Na5}
{Cd5, Na1}
2. Uiso/Uaniso restraints and constraints
: with sigma of 0.005 and sigma for terminal atoms of 0.001
Uanis(Cd2) = Uanis(Na2)
Uanis(Cd3) = Uanis(Na3)
Uiso(Cd1) = Uiso(Na5)
Uiso(Cd5) = Uiso(Na1)
3. Others
 Fixed Sof: Cd1(0.85) Cd2(0.75) Cd3(0.6) Cd5(0.8) Na2(0.25) Na3(0.4) Na5(0.15)
 Na1(0.2)
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Cd1 Cd 0.83014(9) 0.40992(6) -0.11735(5) 0.01319(17) Uiso 0.85 1 d . . P A 19
Cd2 Cd 0.15171(10) 0.22210(7) 0.07116(6) 0.01598(18) Uani 0.75 1 d . . P B 5
Cd3 Cd 0.50344(12) 0.07208(8) 0.87237(7) 0.0188(2) Uani 0.6 1 d . . P C 12
Cd4 Cd 0.73417(7) 0.37236(5) 0.38695(4) 0.01393(16) Uani 1 1 d . . . D 16
Cd5 Cd 0.01576(9) 0.27824(6) 0.59376(5) 0.01210(17) Uiso 0.8 1 d . . P E 21
Na4 Na 0.4636(5) 0.7583(3) 0.3699(3) 0.0324(8) Uani 1 1 d . . . F 17
P1 P 0.6734(3) 0.56767(18) 0.15952(15) 0.0102(4) Uani 1 1 d . . . . .
P2 P 0.6697(3) 0.26165(18) 0.10625(15) 0.0102(4) Uani 1 1 d . . . . .
P3 P 0.2264(3) 0.42467(18) 0.35287(15) 0.0099(4) Uani 1 1 d . . . . .
P4 P 0.2598(3) -0.01139(18) 0.60491(15) 0.0099(4) Uani 1 1 d . . . . .
P5 P -0.0102(3) 0.07162(18) 0.80080(15) 0.0099(4) Uani 1 1 d . . . . .
O1 O 0.8247(7) 0.5830(5) 0.0673(4) 0.0134(11) Uani 1 1 d . . . . .
O2 O 0.8250(7) 0.2596(5) 0.0139(4) 0.0147(11) Uani 1 1 d . . . . .
O3 O 0.5721(7) 0.4158(4) 0.1212(4) 0.0127(11) Uani 1 1 d . . . . .
O4 O 0.4944(7) 0.1646(5) 0.0627(4) 0.0169(11) Uani 1 1 d . . . . .
O5 O 0.7640(7) 0.5697(5) 0.2831(4) 0.0140(11) Uani 1 1 d . . . . .
O6 O 0.5014(7) 0.6668(5) 0.1596(4) 0.0132(11) Uani 1 1 d . . . . .
O7 O 0.4139(7) 0.3474(5) 0.3793(5) 0.0200(12) Uani 1 1 d . . . . .
O8 O 0.1745(7) 0.4106(5) 0.2200(4) 0.0173(11) Uani 1 1 d . . . . .
O9 O 0.2500(7) 0.5806(4) 0.4026(4) 0.0141(11) Uani 1 1 d . . . . .
O10 O 0.0610(7) 0.3592(5) 0.4164(4) 0.0127(10) Uani 1 1 d . . . . .
O11 O 0.2337(7) 0.1153(5) 0.5425(4) 0.0165(11) Uani 1 1 d . . . . .
O12 O -0.0965(7) 0.2021(5) 0.7605(4) 0.0147(11) Uani 1 1 d . . . . .
O13 O 0.0662(6) -0.0181(4) 0.6822(4) 0.0113(10) Uani 1 1 d . . . . .
O14 O -0.1760(7) -0.0228(5) 0.8343(4) 0.0135(11) Uani 1 1 d . . . . .
O15 O 0.1611(7) 0.0959(5) 0.8884(4) 0.0149(11) Uani 1 1 d . . . . .
O16 O 0.4464(7) 0.0104(5) 0.6830(4) 0.0149(11) Uani 1 1 d . . . . .
O17 O 0.2544(7) -0.1482(4) 0.5225(4) 0.0130(11) Uani 1 1 d . . . . .
O18 O 0.7595(7) 0.2357(5) 0.2206(4) 0.0190(12) Uani 1 1 d . . . . .
Na2 Na 0.15171(10) 0.22210(7) 0.07116(6) 0.01598(18) Uani 0.25 1 d . . P B 6
Na6 Na 0.2848(4) 0.1261(2) 0.3550(2) 0.0080(6) Uani 1 1 d . . . G 11
Na3 Na 0.50344(12) 0.07208(8) 0.87237(7) 0.0188(2) Uani 0.4 1 d . . P C 13
Na5 Na 0.83014(9) 0.40992(6) -0.11735(5) 0.01319(17) Uiso 0.15 1 d . . P A 20
Na1 Na 0.01576(9) 0.27824(6) 0.59376(5) 0.01210(17) Uiso 0.2 1 d . . P E 22


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Cd1 O1 2.510(4) . ?
Cd1 O1 2.370(4) 2_765 ?
Cd1 O2 2.241(4) . ?
Cd1 O6 2.355(5) 2_665 ?
Cd1 O8 2.234(5) 2_665 ?
Cd1 O12 2.348(4) 1_654 ?
Cd2 O1 2.643(5) 2_665 ?
Cd2 O2 2.320(5) 1_455 ?
Cd2 O4 2.381(5) . ?
Cd2 O8 2.313(5) . ?
Cd2 O14 2.349(4) 2_556 ?
Cd2 O15 2.277(4) 1_554 ?
Cd3 Cd3 3.4287(16) 2_657 ?
Cd3 O4 2.247(5) 1_556 ?
Cd3 O4 2.506(5) 2_656 ?
Cd3 O6 2.603(4) 2_666 ?
Cd3 O14 2.384(5) 1_655 ?
Cd3 O15 2.329(5) . ?
Cd3 O16 2.193(5) . ?
Cd4 O5 2.403(4) . ?
Cd4 O7 2.163(5) . ?
Cd4 O9 2.396(5) 2_666 ?
Cd4 O10 2.221(4) 1_655 ?
Cd4 O17 2.536(4) 2_656 ?
Cd4 O18 2.176(5) . ?
Cd5 O5 2.358(4) 2_666 ?
Cd5 O9 2.259(4) 2_566 ?
Cd5 O10 2.317(4) . ?
Cd5 O11 2.197(4) . ?
Cd5 O12 2.301(5) . ?
Cd5 O17 2.441(4) 2_556 ?
Na4 P1 3.205(3) . ?
Na4 P4 3.031(3) 2_666 ?
Na4 O5 2.848(6) . ?
Na4 O6 2.477(5) . ?
Na4 O9 2.309(5) . ?
Na4 O11 2.469(6) 2_666 ?
Na4 O12 2.900(6) 2_566 ?
Na4 O16 2.475(5) 2_666 ?
Na4 O17 2.375(5) 1_565 ?
P1 O1 1.519(5) . ?
P1 O3 1.607(5) . ?
P1 O5 1.523(5) . ?
P1 O6 1.510(5) . ?
P1 Na5 3.4035(18) 2_765 ?
P1 Na5 3.4194(18) 2_665 ?
P2 O2 1.517(5) . ?
P2 O3 1.623(5) . ?
P2 O4 1.523(5) . ?
P2 O18 1.483(5) . ?
P2 Na2 3.3040(19) 1_655 ?
P2 Na3 3.1877(19) 1_554 ?
P3 O7 1.517(5) . ?
P3 O8 1.542(5) . ?
P3 O9 1.538(5) . ?
P3 O10 1.534(5) . ?
P3 Na6 2.920(3) . ?
P3 Na5 3.3508(18) 2_665 ?
P3 Na1 3.3085(18) 2_566 ?
P4 Na4 3.031(3) 2_666 ?
P4 O11 1.514(5) . ?
P4 O13 1.611(5) . ?
P4 O16 1.512(5) . ?
P4 O17 1.511(4) . ?
P4 Na6 3.309(3) 2_656 ?
P4 Na6 3.345(3) . ?
P4 Na3 3.4191(19) . ?
P4 Na1 3.2768(18) . ?
P5 O12 1.519(5) . ?
P5 O13 1.612(5) . ?
P5 O14 1.529(5) . ?
P5 O15 1.497(5) . ?
P5 Na2 3.3751(18) 1_556 ?
P5 Na6 2.995(3) 2_556 ?
P5 Na3 3.4049(19) 1_455 ?
P5 Na1 3.3295(18) . ?
O1 Cd1 2.370(4) 2_765 ?
O1 Cd2 2.643(5) 2_665 ?
O1 Na2 2.643(5) 2_665 ?
O1 Na5 2.370(4) 2_765 ?
O1 Na5 2.510(4) . ?
O2 Cd2 2.320(5) 1_655 ?
O2 Na2 2.320(5) 1_655 ?
O2 Na5 2.241(4) . ?
O4 Cd3 2.247(5) 1_554 ?
O4 Cd3 2.506(5) 2_656 ?
O4 Na2 2.381(5) . ?
O4 Na3 2.506(5) 2_656 ?
O4 Na3 2.247(5) 1_554 ?
O5 Cd5 2.358(4) 2_666 ?
O5 Na1 2.358(4) 2_666 ?
O6 Cd1 2.355(5) 2_665 ?
O6 Cd3 2.603(4) 2_666 ?
O6 Na3 2.603(4) 2_666 ?
O6 Na5 2.355(5) 2_665 ?
O7 Na6 2.275(5) . ?
O8 Cd1 2.234(5) 2_665 ?
O8 Na2 2.313(5) . ?
O8 Na5 2.234(5) 2_665 ?
O9 Cd4 2.396(5) 2_666 ?
O9 Cd5 2.259(4) 2_566 ?
O9 Na1 2.259(4) 2_566 ?
O10 Cd4 2.221(4) 1_455 ?
O10 Na6 2.746(5) . ?
O10 Na1 2.317(4) . ?
O11 Na4 2.469(6) 2_666 ?
O11 Na6 2.214(5) . ?
O11 Na1 2.197(4) . ?
O12 Cd1 2.348(4) 1_456 ?
O12 Na4 2.900(6) 2_566 ?
O12 Na5 2.348(4) 1_456 ?
O12 Na1 2.301(5) . ?
O13 Na6 2.569(5) 2_556 ?
O14 Cd2 2.349(4) 2_556 ?
O14 Cd3 2.384(5) 1_455 ?
O14 Na2 2.349(4) 2_556 ?
O14 Na6 2.349(5) 2_556 ?
O14 Na3 2.384(5) 1_455 ?
O15 Cd2 2.277(4) 1_556 ?
O15 Na2 2.277(4) 1_556 ?
O15 Na3 2.329(5) . ?
O16 Na4 2.475(5) 2_666 ?
O16 Na6 2.269(5) 2_656 ?
O16 Na3 2.193(5) . ?
O17 Cd4 2.536(4) 2_656 ?
O17 Cd5 2.441(4) 2_556 ?
O17 Na4 2.375(5) 1_545 ?
O17 Na1 2.441(4) 2_556 ?
Na2 P2 3.3040(19) 1_455 ?
Na2 P5 3.3751(18) 1_554 ?
Na2 O1 2.643(5) 2_665 ?
Na2 O2 2.320(5) 1_455 ?
Na2 O14 2.349(4) 2_556 ?
Na2 O15 2.277(4) 1_554 ?
Na6 P4 3.309(3) 2_656 ?
Na6 P5 2.995(3) 2_556 ?
Na6 O13 2.569(5) 2_556 ?
Na6 O14 2.349(5) 2_556 ?
Na6 O16 2.269(5) 2_656 ?
Na3 P2 3.1877(19) 1_556 ?
Na3 P5 3.4049(19) 1_655 ?
Na3 O4 2.506(5) 2_656 ?
Na3 O4 2.247(5) 1_556 ?
Na3 O6 2.603(4) 2_666 ?
Na3 O14 2.384(5) 1_655 ?
Na3 Na3 3.4287(16) 2_657 ?
Na5 P1 3.4035(18) 2_765 ?
Na5 P1 3.4194(18) 2_665 ?
Na5 P3 3.3507(18) 2_665 ?
Na5 O1 2.370(4) 2_765 ?
Na5 O6 2.355(5) 2_665 ?
Na5 O8 2.234(5) 2_665 ?
Na5 O12 2.348(4) 1_654 ?
Na5 Na5 3.6949(11) 2_765 ?
Na1 P3 3.3085(18) 2_566 ?
Na1 O5 2.358(4) 2_666 ?
Na1 O9 2.259(4) 2_566 ?
Na1 O17 2.441(4) 2_556 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Cd1 O1 81.62(15) 2_765 . ?
O2 Cd1 O1 81.15(15) . . ?
O2 Cd1 O1 82.41(16) . 2_765 ?
O2 Cd1 O6 83.81(16) . 2_665 ?
O2 Cd1 O12 80.18(16) . 1_654 ?
O6 Cd1 O1 106.03(14) 2_665 . ?
O6 Cd1 O1 163.01(15) 2_665 2_765 ?
O8 Cd1 O1 88.47(16) 2_665 . ?
O8 Cd1 O1 97.66(16) 2_665 2_765 ?
O8 Cd1 O2 169.51(16) 2_665 . ?
O8 Cd1 O6 97.69(16) 2_665 2_665 ?
O8 Cd1 O12 110.29(16) 2_665 1_654 ?
O12 Cd1 O1 157.96(15) 1_654 . ?
O12 Cd1 O1 84.40(15) 1_654 2_765 ?
O12 Cd1 O6 83.49(15) 1_654 2_665 ?
O2 Cd2 O1 75.22(15) 1_455 2_665 ?
O2 Cd2 O4 161.32(16) 1_455 . ?
O2 Cd2 O14 111.18(16) 1_455 2_556 ?
O4 Cd2 O1 94.88(15) . 2_665 ?
O8 Cd2 O1 83.67(15) . 2_665 ?
O8 Cd2 O2 95.71(16) . 1_455 ?
O8 Cd2 O4 98.93(16) . . ?
O8 Cd2 O14 105.49(16) . 2_556 ?
O14 Cd2 O1 167.78(15) 2_556 2_665 ?
O14 Cd2 O4 75.94(16) 2_556 . ?
O15 Cd2 O1 76.84(15) 1_554 2_665 ?
O15 Cd2 O2 83.50(16) 1_554 1_455 ?
O15 Cd2 O4 78.78(16) 1_554 . ?
O15 Cd2 O8 160.05(17) 1_554 . ?
O15 Cd2 O14 93.26(16) 1_554 2_556 ?
O4 Cd3 Cd3 46.92(12) 1_556 2_657 ?
O4 Cd3 Cd3 40.90(11) 2_656 2_657 ?
O4 Cd3 O4 87.83(16) 1_556 2_656 ?
O4 Cd3 O6 83.05(15) 1_556 2_666 ?
O4 Cd3 O6 170.87(15) 2_656 2_666 ?
O4 Cd3 O14 109.21(16) 1_556 1_655 ?
O4 Cd3 O15 80.48(16) 1_556 . ?
O6 Cd3 Cd3 129.97(10) 2_666 2_657 ?
O14 Cd3 Cd3 90.10(11) 1_655 2_657 ?
O14 Cd3 O4 72.98(15) 1_655 2_656 ?
O14 Cd3 O6 110.20(15) 1_655 2_666 ?
O15 Cd3 Cd3 86.51(12) . 2_657 ?
O15 Cd3 O4 93.72(16) . 2_656 ?
O15 Cd3 O6 84.65(15) . 2_666 ?
O15 Cd3 O14 162.77(16) . 1_655 ?
O16 Cd3 Cd3 139.33(13) . 2_657 ?
O16 Cd3 O4 166.17(17) . 1_556 ?
O16 Cd3 O4 99.62(16) . 2_656 ?
O16 Cd3 O6 89.28(16) . 2_666 ?
O16 Cd3 O14 84.22(16) . 1_655 ?
O16 Cd3 O15 87.38(16) . . ?
O5 Cd4 O17 171.21(15) . 2_656 ?
O7 Cd4 O5 99.48(17) . . ?
O7 Cd4 O9 92.83(18) . 2_666 ?
O7 Cd4 O10 167.62(17) . 1_655 ?
O7 Cd4 O17 86.79(16) . 2_656 ?
O7 Cd4 O18 91.81(19) . . ?
O9 Cd4 O5 116.94(15) 2_666 . ?
O9 Cd4 O17 68.53(14) 2_666 2_656 ?
O10 Cd4 O5 92.90(16) 1_655 . ?
O10 Cd4 O9 81.26(16) 1_655 2_666 ?
O10 Cd4 O17 80.93(15) 1_655 2_656 ?
O18 Cd4 O5 88.66(16) . . ?
O18 Cd4 O9 152.76(16) . 2_666 ?
O18 Cd4 O10 88.69(17) . 1_655 ?
O18 Cd4 O17 84.96(16) . 2_656 ?
O5 Cd5 O17 170.55(15) 2_666 2_556 ?
O9 Cd5 O5 98.39(16) 2_566 2_666 ?
O9 Cd5 O10 82.23(16) 2_566 . ?
O9 Cd5 O12 87.99(16) 2_566 . ?
O9 Cd5 O17 72.38(15) 2_566 2_556 ?
O10 Cd5 O5 99.90(16) . 2_666 ?
O10 Cd5 O17 81.15(15) . 2_556 ?
O11 Cd5 O5 96.34(17) . 2_666 ?
O11 Cd5 O9 163.75(17) . 2_566 ?
O11 Cd5 O10 88.51(16) . . ?
O11 Cd5 O12 99.47(16) . . ?
O11 Cd5 O17 93.07(16) . 2_556 ?
O12 Cd5 O5 87.67(16) . 2_666 ?
O12 Cd5 O10 168.39(16) . . ?
O12 Cd5 O17 89.95(16) . 2_556 ?
P4 Na4 P1 98.88(9) 2_666 . ?
O5 Na4 P1 28.38(10) . . ?
O5 Na4 P4 93.49(13) . 2_666 ?
O5 Na4 O12 123.59(16) . 2_566 ?
O6 Na4 P1 27.16(11) . . ?
O6 Na4 P4 100.18(14) . 2_666 ?
O6 Na4 O5 55.50(15) . . ?
O6 Na4 O12 70.73(16) . 2_566 ?
O9 Na4 P1 93.34(14) . . ?
O9 Na4 P4 165.16(18) . 2_666 ?
O9 Na4 O5 93.28(17) . . ?
O9 Na4 O6 94.54(18) . . ?
O9 Na4 O11 140.2(2) . 2_666 ?
O9 Na4 O12 73.93(17) . 2_566 ?
O9 Na4 O16 155.6(2) . 2_666 ?
O9 Na4 O17 72.79(17) . 1_565 ?
O11 Na4 P1 97.02(14) 2_666 . ?
O11 Na4 P4 29.79(12) 2_666 2_666 ?
O11 Na4 O5 79.01(16) 2_666 . ?
O11 Na4 O6 111.65(19) 2_666 . ?
O11 Na4 O12 141.95(19) 2_666 2_566 ?
O11 Na4 O16 59.52(16) 2_666 2_666 ?
O12 Na4 P1 96.34(13) 2_566 . ?
O12 Na4 P4 112.74(14) 2_566 2_666 ?
O16 Na4 P1 98.04(14) 2_666 . ?
O16 Na4 P4 29.74(11) 2_666 2_666 ?
O16 Na4 O5 106.90(17) 2_666 . ?
O16 Na4 O6 86.16(18) 2_666 . ?
O16 Na4 O12 83.41(17) 2_666 2_566 ?
O17 Na4 P1 165.99(16) 1_565 . ?
O17 Na4 P4 95.13(14) 1_565 2_666 ?
O17 Na4 O5 150.5(2) 1_565 . ?
O17 Na4 O6 148.7(2) 1_565 . ?
O17 Na4 O11 95.05(18) 1_565 2_666 ?
O17 Na4 O12 78.25(17) 1_565 2_566 ?
O17 Na4 O16 94.19(18) 1_565 2_666 ?
O1 P1 Na4 138.9(2) . . ?
O1 P1 O3 105.5(2) . . ?
O1 P1 O5 114.0(3) . . ?
O1 P1 Na5 124.93(19) . 2_665 ?
O1 P1 Na5 36.86(18) . 2_765 ?
O3 P1 Na4 114.67(18) . . ?
O3 P1 Na5 68.68(17) . 2_665 ?
O3 P1 Na5 115.72(17) . 2_765 ?
O5 P1 Na4 62.68(19) . . ?
O5 P1 O3 107.0(3) . . ?
O5 P1 Na5 77.29(18) . 2_765 ?
O5 P1 Na5 120.01(19) . 2_665 ?
O6 P1 Na4 48.46(19) . . ?
O6 P1 O1 114.4(3) . . ?
O6 P1 O3 104.0(3) . . ?
O6 P1 O5 111.0(3) . . ?
O6 P1 Na5 135.20(19) . 2_765 ?
O6 P1 Na5 35.32(18) . 2_665 ?
Na5 P1 Na5 161.14(6) 2_765 2_665 ?
O2 P2 O3 107.0(3) . . ?
O2 P2 O4 111.4(3) . . ?
O2 P2 Na2 38.57(18) . 1_655 ?
O2 P2 Na3 71.68(19) . 1_554 ?
O3 P2 Na2 120.97(17) . 1_655 ?
O3 P2 Na3 111.40(18) . 1_554 ?
O4 P2 O3 103.3(3) . . ?
O4 P2 Na2 130.65(19) . 1_655 ?
O4 P2 Na3 40.04(18) . 1_554 ?
O18 P2 O2 111.4(3) . . ?
O18 P2 O3 109.5(3) . . ?
O18 P2 O4 113.7(3) . . ?
O18 P2 Na2 72.8(2) . 1_655 ?
O18 P2 Na3 135.7(2) . 1_554 ?
O7 P3 O8 112.3(3) . . ?
O7 P3 O9 110.1(3) . . ?
O7 P3 O10 105.6(3) . . ?
O7 P3 Na6 50.38(19) . . ?
O7 P3 Na5 122.8(2) . 2_665 ?
O7 P3 Na1 145.5(2) . 2_566 ?
O8 P3 Na6 95.18(19) . . ?
O8 P3 Na5 33.52(17) . 2_665 ?
O8 P3 Na1 92.14(19) . 2_566 ?
O9 P3 O8 108.9(3) . . ?
O9 P3 Na6 154.4(2) . . ?
O9 P3 Na5 75.60(18) . 2_665 ?
O9 P3 Na1 36.24(18) . 2_566 ?
O10 P3 O8 110.4(3) . . ?
O10 P3 O9 109.3(3) . . ?
O10 P3 Na6 68.11(18) . . ?
O10 P3 Na5 126.67(18) . 2_665 ?
O10 P3 Na1 86.67(18) . 2_566 ?
O11 P4 Na4 54.1(2) . 2_666 ?
O11 P4 O13 105.8(3) . . ?
O11 P4 Na6 32.12(18) . . ?
O11 P4 Na6 118.4(2) . 2_656 ?
O11 P4 Na3 111.83(19) . . ?
O11 P4 Na1 34.23(18) . . ?
O13 P4 Na4 122.84(18) . 2_666 ?
O13 P4 Na6 130.46(18) . 2_656 ?
O13 P4 Na6 126.24(18) . . ?
O13 P4 Na3 83.94(17) . . ?
O13 P4 Na1 72.66(16) . . ?
O16 P4 Na4 54.3(2) . 2_666 ?
O16 P4 O11 108.4(3) . . ?
O16 P4 O13 110.8(3) . . ?
O16 P4 Na6 114.2(2) . . ?
O16 P4 Na6 36.06(18) . 2_656 ?
O16 P4 Na3 27.52(17) . . ?
O16 P4 Na1 112.83(19) . . ?
O17 P4 Na4 132.5(2) . 2_666 ?
O17 P4 O11 113.4(3) . . ?
O17 P4 O13 104.6(3) . . ?
O17 P4 O16 113.5(3) . . ?
O17 P4 Na6 78.40(19) . 2_656 ?
O17 P4 Na6 83.16(19) . . ?
O17 P4 Na3 129.16(19) . . ?
O17 P4 Na1 130.90(19) . . ?
Na6 P4 Na6 103.30(7) 2_656 . ?
O12 P5 O13 104.3(2) . . ?
O12 P5 O14 110.5(3) . . ?
O12 P5 Na2 97.03(18) . 1_556 ?
O12 P5 Na6 94.61(19) . 2_556 ?
O12 P5 Na3 74.51(19) . 1_455 ?
O12 P5 Na1 36.82(18) . . ?
O13 P5 Na2 141.74(18) . 1_556 ?
O13 P5 Na6 59.01(17) . 2_556 ?
O13 P5 Na3 122.16(17) . 1_455 ?
O13 P5 Na1 70.98(16) . . ?
O14 P5 O13 102.0(2) . . ?
O14 P5 Na2 99.73(18) . 1_556 ?
O14 P5 Na6 50.80(18) . 2_556 ?
O14 P5 Na3 37.61(18) . 1_455 ?
O14 P5 Na1 132.44(19) . . ?
O15 P5 O12 115.5(3) . . ?
O15 P5 O13 108.5(3) . . ?
O15 P5 O14 114.6(3) . . ?
O15 P5 Na2 33.30(18) . 1_556 ?
O15 P5 Na6 149.8(2) . 2_556 ?
O15 P5 Na3 124.3(2) . 1_455 ?
O15 P5 Na1 112.0(2) . . ?
Cd1 O1 Cd1 98.38(15) 2_765 . ?
P1 O1 Cd1 120.5(3) . 2_765 ?
P1 O1 Cd1 120.5(2) . . ?
P1 O1 Cd2 128.5(2) . 2_665 ?
P1 O1 Na2 128.5(2) . 2_665 ?
P1 O1 Na5 120.5(3) . 2_765 ?
P1 O1 Na5 120.5(2) . . ?
Na5 O1 Na5 98.38(15) 2_765 . ?
P2 O2 Cd1 123.5(3) . . ?
P2 O2 Cd2 117.4(3) . 1_655 ?
P2 O2 Na2 117.4(3) . 1_655 ?
P2 O2 Na5 123.5(3) . . ?
P1 O3 P2 130.3(3) . . ?
Cd3 O4 Cd3 92.17(16) 1_554 2_656 ?
P2 O4 Cd2 126.4(3) . . ?
P2 O4 Cd3 116.4(3) . 2_656 ?
P2 O4 Cd3 114.1(3) . 1_554 ?
P2 O4 Na2 126.4(3) . . ?
P2 O4 Na3 116.4(3) . 2_656 ?
P2 O4 Na3 114.1(3) . 1_554 ?
Na3 O4 Na3 92.17(16) 1_554 2_656 ?
P1 O5 Cd4 121.7(2) . . ?
P1 O5 Cd5 134.6(3) . 2_666 ?
P1 O5 Na4 88.9(2) . . ?
P1 O5 Na1 134.6(3) . 2_666 ?
P1 O6 Cd1 122.9(3) . 2_665 ?
P1 O6 Cd3 129.9(3) . 2_666 ?
P1 O6 Na4 104.4(2) . . ?
P1 O6 Na3 129.9(3) . 2_666 ?
P1 O6 Na5 122.9(3) . 2_665 ?
P3 O7 Cd4 141.1(3) . . ?
P3 O7 Na6 98.7(2) . . ?
P3 O8 Cd1 124.1(3) . 2_665 ?
P3 O8 Cd2 133.3(3) . . ?
P3 O8 Na2 133.3(3) . . ?
P3 O8 Na5 124.1(3) . 2_665 ?
P3 O9 Cd4 114.1(2) . 2_666 ?
P3 O9 Cd5 120.0(3) . 2_566 ?
P3 O9 Na4 134.4(3) . . ?
P3 O9 Na1 120.0(3) . 2_566 ?
P3 O10 Cd4 128.2(3) . 1_455 ?
P3 O10 Cd5 138.8(3) . . ?
P3 O10 Na6 80.67(19) . . ?
P3 O10 Na1 138.8(3) . . ?
P4 O11 Cd5 123.0(3) . . ?
P4 O11 Na4 96.1(2) . 2_666 ?
P4 O11 Na6 126.5(3) . . ?
P4 O11 Na1 123.0(3) . . ?
P5 O12 Cd1 125.8(3) . 1_456 ?
P5 O12 Cd5 119.9(3) . . ?
P5 O12 Na4 130.7(3) . 2_566 ?
P5 O12 Na5 125.8(3) . 1_456 ?
P5 O12 Na1 119.9(3) . . ?
P4 O13 P5 134.7(3) . . ?
P4 O13 Na6 135.2(2) . 2_556 ?
P5 O13 Na6 88.43(19) . 2_556 ?
P5 O14 Cd2 129.1(3) . 2_556 ?
P5 O14 Cd3 119.3(3) . 1_455 ?
P5 O14 Na2 129.1(3) . 2_556 ?
P5 O14 Na6 98.9(2) . 2_556 ?
P5 O14 Na3 119.3(3) . 1_455 ?
P5 O15 Cd2 125.5(3) . 1_556 ?
P5 O15 Cd3 132.9(3) . . ?
P5 O15 Na2 125.5(3) . 1_556 ?
P5 O15 Na3 132.9(3) . . ?
P4 O16 Cd3 133.9(3) . . ?
P4 O16 Na4 96.0(2) . 2_666 ?
P4 O16 Na6 120.8(3) . 2_656 ?
P4 O16 Na3 133.9(3) . . ?
P4 O17 Cd4 117.7(2) . 2_656 ?
P4 O17 Cd5 132.2(3) . 2_556 ?
P4 O17 Na4 132.4(3) . 1_545 ?
P4 O17 Na1 132.2(3) . 2_556 ?
P2 O18 Cd4 125.2(3) . . ?
P2 Na2 P5 81.89(4) 1_455 1_554 ?
O1 Na2 P2 93.87(10) 2_665 1_455 ?
O1 Na2 P5 73.50(10) 2_665 1_554 ?
O2 Na2 P2 24.06(11) 1_455 1_455 ?
O2 Na2 P5 62.36(11) 1_455 1_554 ?
O2 Na2 O1 75.22(15) 1_455 2_665 ?
O2 Na2 O4 161.32(16) 1_455 . ?
O2 Na2 O14 111.18(16) 1_455 2_556 ?
O4 Na2 P2 171.21(12) . 1_455 ?
O4 Na2 P5 99.88(11) . 1_554 ?
O4 Na2 O1 94.88(15) . 2_665 ?
O8 Na2 P2 82.79(12) . 1_455 ?
O8 Na2 P5 151.44(12) . 1_554 ?
O8 Na2 O1 83.67(15) . 2_665 ?
O8 Na2 O2 95.71(16) . 1_455 ?
O8 Na2 O4 98.93(16) . . ?
O8 Na2 O14 105.49(16) . 2_556 ?
O14 Na2 P2 95.29(11) 2_556 1_455 ?
O14 Na2 P5 99.81(11) 2_556 1_554 ?
O14 Na2 O1 167.78(15) 2_556 2_665 ?
O14 Na2 O4 75.94(16) 2_556 . ?
O15 Na2 P2 102.54(12) 1_554 1_455 ?
O15 Na2 P5 21.16(12) 1_554 1_554 ?
O15 Na2 O1 76.84(15) 1_554 2_665 ?
O15 Na2 O2 83.50(16) 1_554 1_455 ?
O15 Na2 O4 78.78(16) 1_554 . ?
O15 Na2 O8 160.05(17) 1_554 . ?
O15 Na2 O14 93.26(16) 1_554 2_556 ?
P3 Na6 P4 119.12(9) . 2_656 ?
P3 Na6 P4 120.77(9) . . ?
P3 Na6 P5 117.10(9) . 2_556 ?
P4 Na6 P4 76.70(7) 2_656 . ?
P5 Na6 P4 99.77(8) 2_556 . ?
P5 Na6 P4 115.41(8) 2_556 2_656 ?
O7 Na6 P3 30.90(12) . . ?
O7 Na6 P4 88.35(14) . 2_656 ?
O7 Na6 P4 113.96(15) . . ?
O7 Na6 P5 142.78(16) . 2_556 ?
O7 Na6 O10 56.97(16) . . ?
O7 Na6 O13 134.95(18) . 2_556 ?
O7 Na6 O14 118.7(2) . 2_556 ?
O10 Na6 P3 31.22(10) . . ?
O10 Na6 P4 140.13(13) . 2_656 ?
O10 Na6 P4 98.51(12) . . ?
O10 Na6 P5 104.44(12) . 2_556 ?
O11 Na6 P3 99.56(14) . . ?
O11 Na6 P4 88.71(15) . 2_656 ?
O11 Na6 P4 21.33(12) . . ?
O11 Na6 P5 110.75(15) . 2_556 ?
O11 Na6 O7 97.26(19) . . ?
O11 Na6 O10 78.09(16) . . ?
O11 Na6 O13 85.02(18) . 2_556 ?
O11 Na6 O14 140.96(19) . 2_556 ?
O11 Na6 O16 103.60(19) . 2_656 ?
O13 Na6 P3 104.18(13) 2_556 . ?
O13 Na6 P4 136.69(13) 2_556 2_656 ?
O13 Na6 P4 82.53(12) 2_556 . ?
O13 Na6 P5 32.56(10) 2_556 2_556 ?
O13 Na6 O10 79.97(15) 2_556 . ?
O14 Na6 P3 103.94(14) 2_556 . ?
O14 Na6 P4 127.32(14) 2_556 . ?
O14 Na6 P4 105.94(14) 2_556 2_656 ?
O14 Na6 P5 30.28(12) 2_556 2_556 ?
O14 Na6 O10 107.88(17) 2_556 . ?
O14 Na6 O13 59.32(15) 2_556 2_556 ?
O16 Na6 P3 131.56(16) 2_656 . ?
O16 Na6 P4 86.39(14) 2_656 . ?
O16 Na6 P4 23.09(12) 2_656 2_656 ?
O16 Na6 P5 93.34(14) 2_656 2_556 ?
O16 Na6 O7 103.63(19) 2_656 . ?
O16 Na6 O10 160.36(18) 2_656 . ?
O16 Na6 O13 119.61(17) 2_656 2_556 ?
O16 Na6 O14 83.37(17) 2_656 2_556 ?
P2 Na3 P4 158.41(5) 1_556 . ?
P2 Na3 P5 83.14(5) 1_556 1_655 ?
P2 Na3 Na3 62.99(4) 1_556 2_657 ?
P4 Na3 Na3 132.81(5) . 2_657 ?
P5 Na3 P4 102.76(5) 1_655 . ?
P5 Na3 Na3 105.09(4) 1_655 2_657 ?
O4 Na3 P2 100.68(11) 2_656 1_556 ?
O4 Na3 P2 25.85(12) 1_556 1_556 ?
O4 Na3 P4 148.78(13) 1_556 . ?
O4 Na3 P4 99.38(11) 2_656 . ?
O4 Na3 P5 106.72(12) 1_556 1_655 ?
O4 Na3 P5 95.64(11) 2_656 1_655 ?
O4 Na3 O4 87.83(16) 1_556 2_656 ?
O4 Na3 O6 170.87(15) 2_656 2_666 ?
O4 Na3 O6 83.05(15) 1_556 2_666 ?
O4 Na3 O14 109.21(16) 1_556 1_655 ?
O4 Na3 O15 80.48(16) 1_556 . ?
O4 Na3 Na3 46.92(12) 1_556 2_657 ?
O4 Na3 Na3 40.90(11) 2_656 2_657 ?
O6 Na3 P2 70.97(10) 2_666 1_556 ?
O6 Na3 P4 88.43(10) 2_666 . ?
O6 Na3 P5 87.17(10) 2_666 1_655 ?
O6 Na3 Na3 129.97(10) 2_666 2_657 ?
O14 Na3 P2 91.53(11) 1_655 1_556 ?
O14 Na3 P4 101.92(11) 1_655 . ?
O14 Na3 P5 23.04(11) 1_655 1_655 ?
O14 Na3 O4 72.98(15) 1_655 2_656 ?
O14 Na3 O6 110.20(15) 1_655 2_666 ?
O14 Na3 Na3 90.10(11) 1_655 2_657 ?
O15 Na3 P2 101.89(12) . 1_556 ?
O15 Na3 P4 68.83(11) . . ?
O15 Na3 P5 168.38(12) . 1_655 ?
O15 Na3 O4 93.72(16) . 2_656 ?
O15 Na3 O6 84.65(15) . 2_666 ?
O15 Na3 O14 162.77(16) . 1_655 ?
O15 Na3 Na3 86.51(12) . 2_657 ?
O16 Na3 P2 157.02(13) . 1_556 ?
O16 Na3 P4 18.58(12) . . ?
O16 Na3 P5 84.28(12) . 1_655 ?
O16 Na3 O4 99.62(16) . 2_656 ?
O16 Na3 O4 166.17(17) . 1_556 ?
O16 Na3 O6 89.28(16) . 2_666 ?
O16 Na3 O14 84.22(16) . 1_655 ?
O16 Na3 O15 87.38(16) . . ?
O16 Na3 Na3 139.33(13) . 2_657 ?
P1 Na5 P1 161.14(6) 2_765 2_665 ?
P1 Na5 Na5 130.49(4) 2_665 2_765 ?
P1 Na5 Na5 59.51(3) 2_765 2_765 ?
P3 Na5 P1 85.68(4) 2_665 2_765 ?
P3 Na5 P1 75.56(4) 2_665 2_665 ?
P3 Na5 Na5 114.38(4) 2_665 2_765 ?
O1 Na5 P1 91.10(11) . 2_665 ?
O1 Na5 P1 22.61(11) 2_765 2_765 ?
O1 Na5 P1 97.17(11) . 2_765 ?
O1 Na5 P1 172.70(11) 2_765 2_665 ?
O1 Na5 P3 109.97(11) . 2_665 ?
O1 Na5 P3 106.37(11) 2_765 2_665 ?
O1 Na5 O1 81.62(15) 2_765 . ?
O1 Na5 Na5 39.39(10) . 2_765 ?
O1 Na5 Na5 42.22(11) 2_765 2_765 ?
O2 Na5 P1 97.05(12) . 2_665 ?
O2 Na5 P1 100.94(12) . 2_765 ?
O2 Na5 P3 166.45(12) . 2_665 ?
O2 Na5 O1 82.41(16) . 2_765 ?
O2 Na5 O1 81.15(15) . . ?
O2 Na5 O6 83.81(16) . 2_665 ?
O2 Na5 O12 80.18(16) . 1_654 ?
O2 Na5 Na5 79.10(12) . 2_765 ?
O6 Na5 P1 21.76(11) 2_665 2_665 ?
O6 Na5 P1 156.78(11) 2_665 2_765 ?
O6 Na5 P3 85.58(11) 2_665 2_665 ?
O6 Na5 O1 106.03(14) 2_665 . ?
O6 Na5 O1 163.01(15) 2_665 2_765 ?
O6 Na5 Na5 143.23(11) 2_665 2_765 ?
O8 Na5 P1 81.53(13) 2_665 2_665 ?
O8 Na5 P1 81.78(13) 2_665 2_765 ?
O8 Na5 P3 22.42(12) 2_665 2_665 ?
O8 Na5 O1 88.47(16) 2_665 . ?
O8 Na5 O1 97.66(16) 2_665 2_765 ?
O8 Na5 O2 169.51(16) 2_665 . ?
O8 Na5 O6 97.69(16) 2_665 2_665 ?
O8 Na5 O12 110.29(16) 2_665 1_654 ?
O8 Na5 Na5 93.87(12) 2_665 2_765 ?
O12 Na5 P1 102.72(12) 1_654 2_665 ?
O12 Na5 P1 75.08(12) 1_654 2_765 ?
O12 Na5 P3 90.27(11) 1_654 2_665 ?
O12 Na5 O1 84.40(15) 1_654 2_765 ?
O12 Na5 O1 157.96(15) 1_654 . ?
O12 Na5 O6 83.49(15) 1_654 2_665 ?
O12 Na5 Na5 124.54(11) 1_654 2_765 ?
P3 Na1 P5 115.11(5) 2_566 . ?
P4 Na1 P3 167.19(5) . 2_566 ?
P4 Na1 P5 53.50(4) . . ?
O5 Na1 P3 75.23(11) 2_666 2_566 ?
O5 Na1 P4 97.64(11) 2_666 . ?
O5 Na1 P5 90.01(11) 2_666 . ?
O5 Na1 O17 170.55(15) 2_666 2_556 ?
O9 Na1 P3 23.73(12) 2_566 2_566 ?
O9 Na1 P4 157.35(12) 2_566 . ?
O9 Na1 P5 110.58(12) 2_566 . ?
O9 Na1 O5 98.39(16) 2_566 2_666 ?
O9 Na1 O10 82.23(16) 2_566 . ?
O9 Na1 O12 87.99(16) 2_566 . ?
O9 Na1 O17 72.38(15) 2_566 2_556 ?
O10 Na1 P3 81.41(11) . 2_566 ?
O10 Na1 P4 110.58(12) . . ?
O10 Na1 P5 162.64(12) . . ?
O10 Na1 O5 99.90(16) . 2_666 ?
O10 Na1 O17 81.15(15) . 2_556 ?
O11 Na1 P3 165.42(13) . 2_566 ?
O11 Na1 P4 22.82(12) . . ?
O11 Na1 P5 76.17(12) . . ?
O11 Na1 O5 96.34(17) . 2_666 ?
O11 Na1 O9 163.75(17) . 2_566 ?
O11 Na1 O10 88.51(16) . . ?
O11 Na1 O12 99.47(16) . . ?
O11 Na1 O17 93.07(16) . 2_556 ?
O12 Na1 P3 92.15(11) . 2_566 ?
O12 Na1 P4 76.77(11) . . ?
O12 Na1 P5 23.30(11) . . ?
O12 Na1 O5 87.67(16) . 2_666 ?
O12 Na1 O10 168.39(16) . . ?
O12 Na1 O17 89.95(16) . 2_556 ?
O17 Na1 P3 95.74(11) 2_556 2_566 ?
O17 Na1 P4 90.71(11) 2_556 . ?
O17 Na1 P5 91.42(11) 2_556 . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Na4 P1 O3 P2 -128.1(3) . . . . ?
Na4 P4 O13 P5 -15.8(5) 2_666 . . . ?
Na4 P4 O17 Na4 1.4(5) 2_666 . . 1_545 ?
O1 P1 O3 P2 60.9(4) . . . . ?
O1 P1 O5 Cd4 -117.8(3) . . . . ?
O1 P1 O5 Cd5 52.1(4) . . . 2_666 ?
O1 P1 O5 Na4 134.3(2) . . . . ?
O1 P1 O5 Na1 52.1(4) . . . 2_666 ?
O1 P1 O6 Cd1 116.6(3) . . . 2_665 ?
O1 P1 O6 Cd3 -38.7(4) . . . 2_666 ?
O1 P1 O6 Na4 -134.7(2) . . . . ?
O1 P1 O6 Na3 -38.7(4) . . . 2_666 ?
O1 P1 O6 Na5 116.6(3) . . . 2_665 ?
O2 P2 O3 P1 -59.7(4) . . . . ?
O2 P2 O4 Cd2 -130.5(3) . . . . ?
O2 P2 O4 Cd3 -7.1(4) . . . 1_554 ?
O2 P2 O4 Cd3 98.5(3) . . . 2_656 ?
O2 P2 O4 Na2 -130.5(3) . . . . ?
O2 P2 O4 Na3 98.5(3) . . . 2_656 ?
O2 P2 O4 Na3 -7.1(4) . . . 1_554 ?
O2 P2 O18 Cd4 124.8(3) . . . . ?
O3 P1 O1 Cd1 -112.4(3) . . . 2_765 ?
O3 P1 O1 Cd1 10.5(3) . . . . ?
O3 P1 O1 Cd2 122.1(3) . . . 2_665 ?
O3 P1 O1 Na2 122.1(3) . . . 2_665 ?
O3 P1 O1 Na5 10.5(3) . . . . ?
O3 P1 O1 Na5 -112.4(3) . . . 2_765 ?
O3 P1 O5 Cd4 -1.6(4) . . . . ?
O3 P1 O5 Cd5 168.4(3) . . . 2_666 ?
O3 P1 O5 Na4 -109.5(2) . . . . ?
O3 P1 O5 Na1 168.4(3) . . . 2_666 ?
O3 P1 O6 Cd1 2.1(3) . . . 2_665 ?
O3 P1 O6 Cd3 -153.2(3) . . . 2_666 ?
O3 P1 O6 Na4 110.7(2) . . . . ?
O3 P1 O6 Na3 -153.2(3) . . . 2_666 ?
O3 P1 O6 Na5 2.1(3) . . . 2_665 ?
O3 P2 O2 Cd1 -20.0(4) . . . . ?
O3 P2 O2 Cd2 118.7(3) . . . 1_655 ?
O3 P2 O2 Na2 118.7(3) . . . 1_655 ?
O3 P2 O2 Na5 -20.0(4) . . . . ?
O3 P2 O4 Cd2 -16.0(4) . . . . ?
O3 P2 O4 Cd3 107.5(3) . . . 1_554 ?
O3 P2 O4 Cd3 -146.9(2) . . . 2_656 ?
O3 P2 O4 Na2 -16.0(4) . . . . ?
O3 P2 O4 Na3 -146.9(2) . . . 2_656 ?
O3 P2 O4 Na3 107.5(3) . . . 1_554 ?
O3 P2 O18 Cd4 6.7(4) . . . . ?
O4 P2 O2 Cd1 92.3(3) . . . . ?
O4 P2 O2 Cd2 -129.1(3) . . . 1_655 ?
O4 P2 O2 Na2 -129.1(3) . . . 1_655 ?
O4 P2 O2 Na5 92.3(3) . . . . ?
O4 P2 O3 P1 -177.4(4) . . . . ?
O4 P2 O18 Cd4 -108.3(3) . . . . ?
O5 P1 O1 Cd1 127.6(3) . . . . ?
O5 P1 O1 Cd1 4.7(4) . . . 2_765 ?
O5 P1 O1 Cd2 -120.8(3) . . . 2_665 ?
O5 P1 O1 Na2 -120.8(3) . . . 2_665 ?
O5 P1 O1 Na5 4.7(4) . . . 2_765 ?
O5 P1 O1 Na5 127.6(3) . . . . ?
O5 P1 O3 P2 -60.9(4) . . . . ?
O5 P1 O6 Cd1 -112.6(3) . . . 2_665 ?
O5 P1 O6 Cd3 92.1(3) . . . 2_666 ?
O5 P1 O6 Na4 -4.0(3) . . . . ?
O5 P1 O6 Na3 92.1(3) . . . 2_666 ?
O5 P1 O6 Na5 -112.6(3) . . . 2_665 ?
O6 P1 O1 Cd1 134.0(3) . . . 2_765 ?
O6 P1 O1 Cd1 -103.1(3) . . . . ?
O6 P1 O1 Cd2 8.5(4) . . . 2_665 ?
O6 P1 O1 Na2 8.5(4) . . . 2_665 ?
O6 P1 O1 Na5 -103.1(3) . . . . ?
O6 P1 O1 Na5 134.0(3) . . . 2_765 ?
O6 P1 O3 P2 -178.4(4) . . . . ?
O6 P1 O5 Cd4 111.2(3) . . . . ?
O6 P1 O5 Cd5 -78.8(4) . . . 2_666 ?
O6 P1 O5 Na4 3.3(3) . . . . ?
O6 P1 O5 Na1 -78.8(4) . . . 2_666 ?
O7 P3 O8 Cd1 -116.1(3) . . . 2_665 ?
O7 P3 O8 Cd2 48.6(4) . . . . ?
O7 P3 O8 Na2 48.6(4) . . . . ?
O7 P3 O8 Na5 -116.1(3) . . . 2_665 ?
O7 P3 O9 Cd4 -68.1(3) . . . 2_666 ?
O7 P3 O9 Cd5 -170.0(3) . . . 2_566 ?
O7 P3 O9 Na4 61.0(5) . . . . ?
O7 P3 O9 Na1 -170.0(3) . . . 2_566 ?
O7 P3 O10 Cd4 -162.8(3) . . . 1_455 ?
O7 P3 O10 Cd5 40.2(5) . . . . ?
O7 P3 O10 Na6 -34.3(2) . . . . ?
O7 P3 O10 Na1 40.2(5) . . . . ?
O8 P3 O7 Cd4 82.6(5) . . . . ?
O8 P3 O7 Na6 -77.7(3) . . . . ?
O8 P3 O9 Cd4 168.3(2) . . . 2_666 ?
O8 P3 O9 Cd5 66.3(3) . . . 2_566 ?
O8 P3 O9 Na4 -62.6(4) . . . . ?
O8 P3 O9 Na1 66.3(3) . . . 2_566 ?
O8 P3 O10 Cd4 -41.1(4) . . . 1_455 ?
O8 P3 O10 Cd5 161.9(4) . . . . ?
O8 P3 O10 Na6 87.4(2) . . . . ?
O8 P3 O10 Na1 161.9(4) . . . . ?
O9 P3 O7 Cd4 -39.0(6) . . . . ?
O9 P3 O7 Na6 160.7(2) . . . . ?
O9 P3 O8 Cd1 6.2(4) . . . 2_665 ?
O9 P3 O8 Cd2 170.9(3) . . . . ?
O9 P3 O8 Na2 170.9(3) . . . . ?
O9 P3 O8 Na5 6.2(4) . . . 2_665 ?
O9 P3 O10 Cd4 78.7(4) . . . 1_455 ?
O9 P3 O10 Cd5 -78.3(4) . . . . ?
O9 P3 O10 Na6 -152.8(2) . . . . ?
O9 P3 O10 Na1 -78.3(4) . . . . ?
O10 P3 O7 Cd4 -156.9(4) . . . . ?
O10 P3 O7 Na6 42.8(3) . . . . ?
O10 P3 O8 Cd1 126.3(3) . . . 2_665 ?
O10 P3 O8 Cd2 -69.0(4) . . . . ?
O10 P3 O8 Na2 -69.0(4) . . . . ?
O10 P3 O8 Na5 126.3(3) . . . 2_665 ?
O10 P3 O9 Cd4 47.5(3) . . . 2_666 ?
O10 P3 O9 Cd5 -54.4(3) . . . 2_566 ?
O10 P3 O9 Na4 176.7(3) . . . . ?
O10 P3 O9 Na1 -54.4(3) . . . 2_566 ?
O11 P4 O13 P5 -72.9(5) . . . . ?
O11 P4 O13 Na6 87.2(4) . . . 2_556 ?
O11 P4 O16 Cd3 102.1(4) . . . . ?
O11 P4 O16 Na4 -0.6(3) . . . 2_666 ?
O11 P4 O16 Na6 -113.2(3) . . . 2_656 ?
O11 P4 O16 Na3 102.1(4) . . . . ?
O11 P4 O17 Cd4 -174.8(2) . . . 2_656 ?
O11 P4 O17 Cd5 -71.4(4) . . . 2_556 ?
O11 P4 O17 Na4 63.4(4) . . . 1_545 ?
O11 P4 O17 Na1 -71.4(4) . . . 2_556 ?
O12 P5 O13 P4 79.3(4) . . . . ?
O12 P5 O13 Na6 -86.8(2) . . . 2_556 ?
O12 P5 O14 Cd2 -170.1(3) . . . 2_556 ?
O12 P5 O14 Cd3 -17.7(3) . . . 1_455 ?
O12 P5 O14 Na2 -170.1(3) . . . 2_556 ?
O12 P5 O14 Na6 78.8(3) . . . 2_556 ?
O12 P5 O14 Na3 -17.7(3) . . . 1_455 ?
O12 P5 O15 Cd2 61.3(4) . . . 1_556 ?
O12 P5 O15 Cd3 -101.9(4) . . . . ?
O12 P5 O15 Na2 61.3(4) . . . 1_556 ?
O12 P5 O15 Na3 -101.9(4) . . . . ?
O13 P4 O11 Cd5 15.1(4) . . . . ?
O13 P4 O11 Na4 119.4(2) . . . 2_666 ?
O13 P4 O11 Na6 -134.9(3) . . . . ?
O13 P4 O11 Na1 15.1(4) . . . . ?
O13 P4 O16 Cd3 -13.5(5) . . . . ?
O13 P4 O16 Na4 -116.2(2) . . . 2_666 ?
O13 P4 O16 Na6 131.2(3) . . . 2_656 ?
O13 P4 O16 Na3 -13.5(5) . . . . ?
O13 P4 O17 Cd4 -60.0(3) . . . 2_656 ?
O13 P4 O17 Cd5 43.3(4) . . . 2_556 ?
O13 P4 O17 Na4 178.2(3) . . . 1_545 ?
O13 P4 O17 Na1 43.3(4) . . . 2_556 ?
O13 P5 O12 Cd1 -164.4(3) . . . 1_456 ?
O13 P5 O12 Cd5 -25.8(3) . . . . ?
O13 P5 O12 Na4 73.8(3) . . . 2_566 ?
O13 P5 O12 Na5 -164.4(3) . . . 1_456 ?
O13 P5 O12 Na1 -25.8(3) . . . . ?
O13 P5 O14 Cd2 79.5(3) . . . 2_556 ?
O13 P5 O14 Cd3 -128.1(3) . . . 1_455 ?
O13 P5 O14 Na2 79.5(3) . . . 2_556 ?
O13 P5 O14 Na6 -31.6(3) . . . 2_556 ?
O13 P5 O14 Na3 -128.1(3) . . . 1_455 ?
O13 P5 O15 Cd2 177.9(3) . . . 1_556 ?
O13 P5 O15 Cd3 14.7(4) . . . . ?
O13 P5 O15 Na2 177.9(3) . . . 1_556 ?
O13 P5 O15 Na3 14.7(4) . . . . ?
O14 P5 O12 Cd1 86.7(3) . . . 1_456 ?
O14 P5 O12 Cd5 -134.6(3) . . . . ?
O14 P5 O12 Na4 -35.1(4) . . . 2_566 ?
O14 P5 O12 Na5 86.7(3) . . . 1_456 ?
O14 P5 O12 Na1 -134.6(3) . . . . ?
O14 P5 O13 P4 -165.6(4) . . . . ?
O14 P5 O13 Na6 28.2(2) . . . 2_556 ?
O14 P5 O15 Cd2 -69.0(4) . . . 1_556 ?
O14 P5 O15 Cd3 127.8(3) . . . . ?
O14 P5 O15 Na2 -69.0(4) . . . 1_556 ?
O14 P5 O15 Na3 127.8(3) . . . . ?
O15 P5 O12 Cd1 -45.5(4) . . . 1_456 ?
O15 P5 O12 Cd5 93.2(3) . . . . ?
O15 P5 O12 Na4 -167.3(3) . . . 2_566 ?
O15 P5 O12 Na5 -45.5(4) . . . 1_456 ?
O15 P5 O12 Na1 93.2(3) . . . . ?
O15 P5 O13 P4 -44.3(5) . . . . ?
O15 P5 O13 Na6 149.6(2) . . . 2_556 ?
O15 P5 O14 Cd2 -37.4(4) . . . 2_556 ?
O15 P5 O14 Cd3 115.0(3) . . . 1_455 ?
O15 P5 O14 Na2 -37.4(4) . . . 2_556 ?
O15 P5 O14 Na6 -148.5(2) . . . 2_556 ?
O15 P5 O14 Na3 115.0(3) . . . 1_455 ?
O16 P4 O11 Cd5 -103.8(3) . . . . ?
O16 P4 O11 Na4 0.6(3) . . . 2_666 ?
O16 P4 O11 Na6 106.3(3) . . . . ?
O16 P4 O11 Na1 -103.8(3) . . . . ?
O16 P4 O13 P5 44.4(5) . . . . ?
O16 P4 O13 Na6 -155.5(3) . . . 2_556 ?
O16 P4 O17 Cd4 60.8(3) . . . 2_656 ?
O16 P4 O17 Cd5 164.2(3) . . . 2_556 ?
O16 P4 O17 Na4 -61.0(4) . . . 1_545 ?
O16 P4 O17 Na1 164.2(3) . . . 2_556 ?
O17 P4 O11 Cd5 129.1(3) . . . . ?
O17 P4 O11 Na4 -126.5(2) . . . 2_666 ?
O17 P4 O11 Na6 -20.8(4) . . . . ?
O17 P4 O11 Na1 129.1(3) . . . . ?
O17 P4 O13 P5 167.1(4) . . . . ?
O17 P4 O13 Na6 -32.8(4) . . . 2_556 ?
O17 P4 O16 Cd3 -130.9(4) . . . . ?
O17 P4 O16 Na4 126.5(2) . . . 2_666 ?
O17 P4 O16 Na6 13.8(4) . . . 2_656 ?
O17 P4 O16 Na3 -130.9(4) . . . . ?
O18 P2 O2 Cd1 -139.6(3) . . . . ?
O18 P2 O2 Cd2 -1.0(4) . . . 1_655 ?
O18 P2 O2 Na2 -1.0(4) . . . 1_655 ?
O18 P2 O2 Na5 -139.6(3) . . . . ?
O18 P2 O3 P1 61.1(5) . . . . ?
O18 P2 O4 Cd2 102.6(3) . . . . ?
O18 P2 O4 Cd3 -28.4(4) . . . 2_656 ?
O18 P2 O4 Cd3 -133.9(3) . . . 1_554 ?
O18 P2 O4 Na2 102.6(3) . . . . ?
O18 P2 O4 Na3 -133.9(3) . . . 1_554 ?
O18 P2 O4 Na3 -28.4(4) . . . 2_656 ?
Na2 P2 O3 P1 -20.1(5) 1_655 . . . ?
Na2 P2 O4 Na2 -170.20(14) 1_655 . . . ?
Na2 P5 O13 P4 -42.4(6) 1_556 . . . ?
Na2 P5 O14 Na2 -68.8(3) 1_556 . . 2_556 ?
Na6 P4 O11 Na6 68.4(4) 2_656 . . . ?
Na6 P4 O13 P5 -100.7(4) . . . . ?
Na6 P4 O13 P5 80.0(4) 2_656 . . . ?
Na6 P4 O13 Na6 -119.9(3) 2_656 . . 2_556 ?
Na6 P4 O13 Na6 59.4(4) . . . 2_556 ?
Na6 P4 O16 Na6 -79.2(3) . . . 2_656 ?
Na6 P5 O13 P4 166.1(5) 2_556 . . . ?
Na3 P2 O3 P1 -136.2(3) 1_554 . . . ?
Na3 P2 O4 Na3 105.6(3) 1_554 . . 2_656 ?
Na3 P4 O13 P5 38.1(4) . . . . ?
Na3 P5 O13 P4 159.8(3) 1_455 . . . ?
Na3 P5 O15 Na3 169.9(2) 1_455 . . . ?
Na5 P1 O1 Na5 122.9(4) 2_765 . . . ?
Na5 P1 O1 Na5 173.07(12) 2_665 . . 2_765 ?
Na5 P1 O1 Na5 -64.0(3) 2_665 . . . ?
Na5 P1 O3 P2 22.9(4) 2_765 . . . ?
Na5 P1 O3 P2 -177.1(4) 2_665 . . . ?
Na5 P1 O6 Na5 154.39(14) 2_765 . . 2_665 ?
Na1 P3 O10 Na1 -107.1(4) 2_566 . . . ?
Na1 P4 O13 P5 -64.1(4) . . . . ?
Na1 P4 O17 Na1 -36.2(5) . . . 2_556 ?
Na1 P5 O13 P4 63.3(4) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_1
_database_code_depnum_ccdc_archive 'CCDC 2431244'
loop_
_audit_author_name
_audit_author_address
'Lei Wu'
;Xinjiang University
China
;
_audit_update_record             
;
2025-03-14 deposited with the CCDC.	2025-05-06 downloaded from the CCDC.
;
_audit_creation_date             2023-05-26
_audit_creation_method           
;
Olex2 1.3
(compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408)
;
_shelx_SHELXL_version_number     2014/7
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'Mg6 Na8 O30 P8'
_chemical_formula_sum            'Mg6 Na8 O30 P8'
_chemical_formula_weight         1057.54
_chemical_absolute_configuration ?
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Mg Mg 0.0486 0.0363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      orthorhombic
_space_group_IT_number           33
_space_group_name_H-M_alt        'P n a 21'
_space_group_name_Hall           'P 2c -2n'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z+1/2'
'x+1/2, -y+1/2, z'
'-x+1/2, y+1/2, z+1/2'

_cell_length_a                   17.9576(12)
_cell_length_b                   10.4987(7)
_cell_length_c                   6.5119(4)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     1227.70(14)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    4528
_cell_measurement_temperature    296(2)
_cell_measurement_theta_max      27.31
_cell_measurement_theta_min      2.99
_shelx_estimated_absorpt_T_max   0.906
_shelx_estimated_absorpt_T_min   0.889
_exptl_absorpt_coefficient_mu    1.006
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_type   none
_exptl_absorpt_process_details   sadabs
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.861
_exptl_crystal_density_meas      .
_exptl_crystal_density_method    ?
_exptl_crystal_description       Block
_exptl_crystal_F_000             1040
_exptl_crystal_size_max          0.12
_exptl_crystal_size_mid          0.11
_exptl_crystal_size_min          0.1
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0605
_diffrn_reflns_av_unetI/netI     0.0585
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.930
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       8
_diffrn_reflns_limit_l_min       -8
_diffrn_reflns_number            11176
_diffrn_reflns_point_group_measured_fraction_full 0.994
_diffrn_reflns_point_group_measured_fraction_max 0.892
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.962
_diffrn_reflns_theta_min         2.247
_diffrn_ambient_temperature      296.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.930
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_source_current           30.0
_diffrn_source_power             1.5
_diffrn_source_voltage           50.0
_reflns_Friedel_coverage         0.765
_reflns_Friedel_fraction_full    0.989
_reflns_Friedel_fraction_max     0.846
_reflns_number_gt                2276
_reflns_number_total             2638
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2014/7 (Sheldrick, 2015)'
_computing_structure_solution    ?
_refine_diff_density_max         0.464
_refine_diff_density_min         -0.441
_refine_diff_density_rms         0.113
_refine_ls_abs_structure_details 
;
 Flack x determined using 865 quotients [(I+)-(I-)]/[(I+)+(I-)]
 (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259).
;
_refine_ls_abs_structure_Flack   -0.08(9)
_refine_ls_extinction_coef       0.0322(16)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2014/7 (Sheldrick 2014'
_refine_ls_goodness_of_fit_ref   1.039
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     236
_refine_ls_number_reflns         2638
_refine_ls_number_restraints     1
_refine_ls_R_factor_all          0.0483
_refine_ls_R_factor_gt           0.0360
_refine_ls_restrained_S_all      1.038
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0293P)²+0.3301P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0668
_refine_ls_wR_factor_ref         0.0716
_refine_special_details          ?
_olex2_refinement_description    
;
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
P1 P 0.43089(7) 0.26411(13) 0.3191(2) 0.0084(3) Uani 1 1 d . . . . .
P2 P 0.29192(7) 0.50308(13) 0.9624(2) 0.0075(3) Uani 1 1 d . . . . .
P4 P 0.55126(8) 0.27056(13) 0.0099(2) 0.0098(3) Uani 1 1 d . . . . .
P3 P 0.31994(7) -0.01203(13) 0.9521(2) 0.0079(3) Uani 1 1 d . . . . .
Mg2 Mg 0.33391(9) 0.50544(17) 0.4692(3) 0.0094(4) Uani 1 1 d . . . . .
Mg1 Mg 0.36073(9) -0.00615(16) 0.4592(3) 0.0097(4) Uani 1 1 d . . . . .
Mg3 Mg 0.25952(10) 0.24427(17) 1.1909(3) 0.0112(4) Uani 1 1 d . . . . .
Na2 Na 0.49256(13) -0.0257(2) 0.1772(4) 0.0181(6) Uani 1 1 d . . . . .
Na4 Na 0.29346(13) 0.74829(19) 1.2110(4) 0.0186(6) Uani 1 1 d . . . . .
Na3 Na 0.46097(13) 0.5410(2) 1.0339(4) 0.0228(6) Uani 1 1 d . . . . .
Na1 Na 0.39230(12) 0.2629(2) -0.2113(4) 0.0182(5) Uani 1 1 d . . . . .
O14 O 0.3382(2) 0.5356(3) 1.1520(6) 0.0108(9) Uani 1 1 d . . . . .
O12 O 0.23930(18) 0.3874(3) 0.9914(6) 0.0096(8) Uani 1 1 d . . . . .
O11 O 0.26809(18) 0.1043(3) 0.9774(6) 0.0102(8) Uani 1 1 d . . . . .
O15 O 0.3422(2) 0.4768(3) 0.7816(6) 0.0143(9) Uani 1 1 d . . . . .
O10 O 0.3636(2) -0.0432(3) 1.1472(6) 0.0106(9) Uani 1 1 d . . . . .
O4 O 0.43872(19) 0.1387(3) 0.4319(6) 0.0140(9) Uani 1 1 d . . . . .
O3 O 0.41598(19) 0.3729(3) 0.4656(6) 0.0130(8) Uani 1 1 d . . . . .
O6 O 0.6315(2) 0.3114(3) 0.0338(6) 0.0139(9) Uani 1 1 d . . . . .
O7 O 0.54528(18) 0.1289(3) -0.0274(6) 0.0121(8) Uani 1 1 d . . . . .
O1 O 0.5128(2) 0.2986(3) 0.2327(6) 0.0128(9) Uani 1 1 d . . . . .
O8 O 0.3721(2) 0.0119(3) 0.7723(6) 0.0121(9) Uani 1 1 d . . . . .
O2 O 0.3762(2) 0.2587(3) 0.1449(6) 0.0131(9) Uani 1 1 d . . . . .
O13 O 0.23659(19) 0.6143(3) 0.9232(6) 0.0115(9) Uani 1 1 d . . . . .
O9 O 0.26394(19) -0.1230(3) 0.9165(6) 0.0113(9) Uani 1 1 d . . . . .
O5 O 0.5090(2) 0.3508(4) -0.1403(6) 0.0168(9) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
P1 Mg3 3.196(2) 1_554 ?
P1 Na2 3.367(3) . ?
P1 Na3 3.149(3) 2_664 ?
P1 Na1 3.135(3) 1_556 ?
P1 O4 1.514(4) . ?
P1 O3 1.512(4) . ?
P1 O1 1.616(4) . ?
P1 O2 1.502(4) . ?
P2 Mg1 2.743(2) 4 ?
P2 Mg3 3.152(2) . ?
P2 Na4 3.041(3) . ?
P2 Na3 3.097(3) . ?
P2 Na1 3.299(3) 1_556 ?
P2 O14 1.527(4) . ?
P2 O12 1.550(3) . ?
P2 O15 1.509(4) . ?
P2 O13 1.554(4) . ?
P4 Mg2 3.139(2) 2_664 ?
P4 Na2 3.453(3) 2_654 ?
P4 Na4 3.406(3) 2_663 ?
P4 Na3 3.273(3) 1_554 ?
P4 Na1 3.198(3) . ?
P4 O6 1.512(4) . ?
P4 O7 1.511(4) . ?
P4 O1 1.634(4) . ?
P4 O5 1.498(4) . ?
P3 Mg2 2.771(2) 4_545 ?
P3 Na2 3.432(3) 1_556 ?
P3 Na4 3.066(3) 1_545 ?
P3 Na1 3.340(2) 1_556 ?
P3 O11 1.545(3) . ?
P3 O10 1.528(4) . ?
P3 O8 1.520(4) . ?
P3 O9 1.556(4) . ?
Mg2 P4 3.139(2) 2_665 ?
Mg2 P3 2.771(2) 4_554 ?
Mg2 Mg3 3.548(3) 1_554 ?
Mg2 Mg3 3.345(3) 4_554 ?
Mg2 Na4 3.139(3) 1_554 ?
Mg2 Na1 3.451(3) 1_556 ?
Mg2 O14 2.091(4) 1_554 ?
Mg2 O11 2.106(4) 4_554 ?
Mg2 O15 2.062(5) . ?
Mg2 O3 2.027(4) . ?
Mg2 O6 2.064(4) 2_665 ?
Mg2 O9 2.241(4) 4_554 ?
Mg1 P2 2.743(2) 4_544 ?
Mg1 Mg3 3.642(3) 1_554 ?
Mg1 Na2 3.011(3) 2_655 ?
Mg1 Na2 3.003(3) . ?
Mg1 Na4 3.274(3) 1_544 ?
Mg1 Na1 3.592(3) 1_556 ?
Mg1 O12 2.126(4) 4_544 ?
Mg1 O10 2.069(4) 1_554 ?
Mg1 O4 2.075(4) . ?
Mg1 O7 2.125(4) 2_655 ?
Mg1 O8 2.058(5) . ?
Mg1 O13 2.170(4) 4_544 ?
Mg3 P1 3.196(2) 1_556 ?
Mg3 Mg2 3.345(3) 4_545 ?
Mg3 Na4 3.267(3) 4_544 ?
Mg3 Na4 3.518(3) 4_545 ?
Mg3 Na1 3.547(3) 1_556 ?
Mg3 O12 2.020(4) . ?
Mg3 O11 2.029(4) . ?
Mg3 O6 2.583(4) 3_456 ?
Mg3 O2 2.122(4) 1_556 ?
Mg3 O13 2.038(4) 4_545 ?
Mg3 O9 2.068(4) 4 ?
Na2 Mg1 3.011(3) 2_654 ?
Na2 Na2 3.3112(8) 2_655 ?
Na2 Na2 3.3111(8) 2_654 ?
Na2 Na1 3.317(3) 2_655 ?
Na2 O10 2.332(4) 1_554 ?
Na2 O4 2.342(5) 2_654 ?
Na2 O4 2.581(5) . ?
Na2 O7 2.303(4) . ?
Na2 O7 2.310(5) 2_655 ?
Na2 O8 2.513(5) 2_654 ?
Na4 P3 3.066(3) 1_565 ?
Na4 Mg2 3.139(3) 1_556 ?
Na4 Mg1 3.274(3) 1_566 ?
Na4 Mg3 3.267(3) 4 ?
Na4 O14 2.404(4) . ?
Na4 O12 2.411(4) 4 ?
Na4 O11 2.553(4) 4 ?
Na4 O10 2.559(4) 1_565 ?
Na4 O6 2.574(5) 2_666 ?
Na4 O13 2.556(4) . ?
Na4 O9 2.406(5) 1_565 ?
Na3 P1 3.149(3) 2_665 ?
Na3 P4 3.273(3) 1_556 ?
Na3 Na3 3.648(2) 2_664 ?
Na3 Na1 3.548(3) 1_556 ?
Na3 O14 2.336(4) . ?
Na3 O15 2.775(5) . ?
Na3 O3 2.429(4) 2_665 ?
Na3 O1 3.003(4) 1_556 ?
Na3 O1 2.628(4) 2_665 ?
Na3 O5 2.453(5) 1_556 ?
Na3 O5 2.466(4) 2_666 ?
Na1 P1 3.135(3) 1_554 ?
Na1 P2 3.299(3) 1_554 ?
Na1 P3 3.340(2) 1_554 ?
Na1 Na2 3.317(3) 2_654 ?
Na1 Na4 3.378(3) 4_543 ?
Na1 O15 2.420(4) 1_554 ?
Na1 O4 2.792(5) 1_554 ?
Na1 O3 2.438(5) 1_554 ?
Na1 O8 2.662(4) 1_554 ?
Na1 O2 2.338(5) . ?
Na1 O5 2.335(4) . ?
O14 Mg2 2.091(4) 1_556 ?
O12 Mg1 2.126(4) 4 ?
O12 Na4 2.411(4) 4_544 ?
O11 Mg2 2.106(4) 4_545 ?
O11 Na4 2.553(4) 4_544 ?
O15 Na1 2.420(4) 1_556 ?
O10 Mg1 2.069(4) 1_556 ?
O10 Na2 2.332(4) 1_556 ?
O10 Na4 2.559(4) 1_545 ?
O4 Na2 2.342(5) 2_655 ?
O4 Na1 2.792(5) 1_556 ?
O3 Na3 2.429(4) 2_664 ?
O3 Na1 2.438(5) 1_556 ?
O6 Mg2 2.064(4) 2_664 ?
O6 Mg3 2.583(4) 3_554 ?
O6 Na4 2.574(5) 2_663 ?
O7 Mg1 2.125(4) 2_654 ?
O7 Na2 2.310(5) 2_654 ?
O1 Na3 2.628(4) 2_664 ?
O1 Na3 3.003(4) 1_554 ?
O8 Na2 2.513(5) 2_655 ?
O8 Na1 2.662(4) 1_556 ?
O2 Mg3 2.122(4) 1_554 ?
O13 Mg1 2.170(4) 4 ?
O13 Mg3 2.039(4) 4_554 ?
O9 Mg2 2.241(4) 4_545 ?
O9 Mg3 2.068(4) 4_544 ?
O9 Na4 2.406(5) 1_545 ?
O5 Na3 2.466(4) 2_663 ?
O5 Na3 2.453(5) 1_554 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Mg3 P1 Na2 100.73(6) 1_554 . ?
Na3 P1 Mg3 138.79(7) 2_664 1_554 ?
Na3 P1 Na2 120.42(7) 2_664 . ?
Na1 P1 Mg3 92.39(6) 1_556 1_554 ?
Na1 P1 Na2 109.67(7) 1_556 . ?
Na1 P1 Na3 72.89(7) 1_556 2_664 ?
O4 P1 Mg3 99.17(14) . 1_554 ?
O4 P1 Na2 46.90(16) . . ?
O4 P1 Na3 107.01(15) . 2_664 ?
O4 P1 Na1 62.88(16) . 1_556 ?
O4 P1 O1 106.2(2) . . ?
O3 P1 Mg3 92.49(14) . 1_554 ?
O3 P1 Na2 156.08(17) . . ?
O3 P1 Na3 48.55(14) . 2_664 ?
O3 P1 Na1 49.37(16) . 1_556 ?
O3 P1 O4 111.6(2) . . ?
O3 P1 O1 102.2(2) . . ?
O1 P1 Mg3 143.14(16) . 1_554 ?
O1 P1 Na2 78.91(14) . . ?
O1 P1 Na3 56.48(14) . 2_664 ?
O1 P1 Na1 122.81(16) . 1_556 ?
O2 P1 Mg3 33.91(15) . 1_554 ?
O2 P1 Na2 88.49(15) . . ?
O2 P1 Na3 139.78(16) . 2_664 ?
O2 P1 Na1 126.29(16) . 1_556 ?
O2 P1 O4 113.2(2) . . ?
O2 P1 O3 112.9(2) . . ?
O2 P1 O1 109.9(2) . . ?
Mg1 P2 Mg3 77.80(6) 4 . ?
Mg1 P2 Na4 92.47(7) 4 . ?
Mg1 P2 Na3 170.16(9) 4 . ?
Mg1 P2 Na1 121.09(7) 4 1_556 ?
Mg3 P2 Na1 66.67(6) . 1_556 ?
Na4 P2 Mg3 118.68(8) . . ?
Na4 P2 Na3 78.60(7) . . ?
Na4 P2 Na1 145.52(7) . 1_556 ?
Na3 P2 Mg3 102.75(7) . . ?
Na3 P2 Na1 67.30(6) . 1_556 ?
O14 P2 Mg1 123.90(16) . 4 ?
O14 P2 Mg3 84.92(15) . . ?
O14 P2 Na4 51.33(15) . . ?
O14 P2 Na3 46.88(16) . . ?
O14 P2 Na1 98.68(15) . 1_556 ?
O14 P2 O12 114.1(2) . . ?
O14 P2 O13 108.2(2) . . ?
O12 P2 Mg1 50.51(13) . 4 ?
O12 P2 Mg3 32.30(13) . . ?
O12 P2 Na4 127.13(15) . . ?
O12 P2 Na3 132.83(14) . . ?
O12 P2 Na1 77.07(14) . 1_556 ?
O12 P2 O13 102.64(18) . . ?
O15 P2 Mg1 125.84(18) . 4 ?
O15 P2 Mg3 108.75(16) . . ?
O15 P2 Na4 124.36(16) . . ?
O15 P2 Na3 63.53(16) . . ?
O15 P2 Na1 42.79(15) . 1_556 ?
O15 P2 O14 110.3(2) . . ?
O15 P2 O12 108.5(2) . . ?
O15 P2 O13 113.1(2) . . ?
O13 P2 Mg1 52.15(14) . 4 ?
O13 P2 Mg3 127.38(14) . . ?
O13 P2 Na4 57.13(15) . . ?
O13 P2 Na3 123.70(15) . . ?
O13 P2 Na1 150.14(16) . 1_556 ?
Mg2 P4 Na2 130.88(7) 2_664 2_654 ?
Mg2 P4 Na4 57.14(5) 2_664 2_663 ?
Mg2 P4 Na3 71.31(6) 2_664 1_554 ?
Mg2 P4 Na1 124.55(7) 2_664 . ?
Na4 P4 Na2 77.57(6) 2_663 2_654 ?
Na3 P4 Na2 124.25(8) 1_554 2_654 ?
Na3 P4 Na4 118.89(7) 1_554 2_663 ?
Na1 P4 Na2 59.69(7) . 2_654 ?
Na1 P4 Na4 118.15(8) . 2_663 ?
Na1 P4 Na3 66.50(6) . 1_554 ?
O6 P4 Mg2 33.89(14) . 2_664 ?
O6 P4 Na2 119.53(16) . 2_654 ?
O6 P4 Na4 45.15(16) . 2_663 ?
O6 P4 Na3 102.79(15) . 1_554 ?
O6 P4 Na1 154.73(17) . . ?
O6 P4 O1 105.1(2) . . ?
O7 P4 Mg2 140.41(15) . 2_664 ?
O7 P4 Na2 31.79(16) . 2_654 ?
O7 P4 Na4 84.79(15) . 2_663 ?
O7 P4 Na3 145.73(15) . 1_554 ?
O7 P4 Na1 80.77(15) . . ?
O7 P4 O6 111.31(19) . . ?
O7 P4 O1 106.9(2) . . ?
O1 P4 Mg2 102.58(14) . 2_664 ?
O1 P4 Na2 126.51(15) . 2_654 ?
O1 P4 Na4 149.78(15) . 2_663 ?
O1 P4 Na3 65.91(14) . 1_554 ?
O1 P4 Na1 91.55(14) . . ?
O5 P4 Mg2 81.75(16) . 2_664 ?
O5 P4 Na2 83.88(17) . 2_654 ?
O5 P4 Na4 94.28(16) . 2_663 ?
O5 P4 Na3 44.94(16) . 1_554 ?
O5 P4 Na1 42.90(16) . . ?
O5 P4 O6 113.0(2) . . ?
O5 P4 O7 114.4(2) . . ?
O5 P4 O1 105.3(2) . . ?
Mg2 P3 Na2 152.40(8) 4_545 1_556 ?
Mg2 P3 Na4 82.98(7) 4_545 1_545 ?
Mg2 P3 Na1 110.09(7) 4_545 1_556 ?
Na4 P3 Na2 82.58(7) 1_545 1_556 ?
Na4 P3 Na1 160.90(8) 1_545 1_556 ?
Na1 P3 Na2 79.68(6) 1_556 1_556 ?
O11 P3 Mg2 48.89(13) . 4_545 ?
O11 P3 Na2 122.14(15) . 1_556 ?
O11 P3 Na4 119.80(16) . 1_545 ?
O11 P3 Na1 65.48(14) . 1_556 ?
O11 P3 O9 102.60(19) . . ?
O10 P3 Mg2 119.48(16) . 4_545 ?
O10 P3 Na2 34.18(15) . 1_556 ?
O10 P3 Na4 56.41(15) . 1_545 ?
O10 P3 Na1 104.50(16) . 1_556 ?
O10 P3 O11 112.9(2) . . ?
O10 P3 O9 107.2(2) . . ?
O8 P3 Mg2 129.33(17) . 4_545 ?
O8 P3 Na2 77.29(16) . 1_556 ?
O8 P3 Na4 130.90(15) . 1_545 ?
O8 P3 Na1 51.10(14) . 1_556 ?
O8 P3 O11 108.8(2) . . ?
O8 P3 O10 111.1(2) . . ?
O8 P3 O9 114.0(2) . . ?
O9 P3 Mg2 53.93(14) . 4_545 ?
O9 P3 Na2 128.04(15) . 1_556 ?
O9 P3 Na4 50.78(15) . 1_545 ?
O9 P3 Na1 148.29(16) . 1_556 ?
P4 Mg2 Mg3 150.41(8) 2_665 1_554 ?
P4 Mg2 Mg3 74.42(6) 2_665 4_554 ?
P4 Mg2 Na4 65.72(6) 2_665 1_554 ?
P4 Mg2 Na1 107.59(7) 2_665 1_556 ?
P3 Mg2 P4 135.07(7) 4_554 2_665 ?
P3 Mg2 Mg3 63.44(5) 4_554 1_554 ?
P3 Mg2 Mg3 64.33(5) 4_554 4_554 ?
P3 Mg2 Na4 78.56(7) 4_554 1_554 ?
P3 Mg2 Na1 106.15(7) 4_554 1_556 ?
Mg3 Mg2 Mg3 127.66(5) 4_554 1_554 ?
Mg3 Mg2 Na1 116.43(8) 4_554 1_556 ?
Na4 Mg2 Mg3 105.49(7) 1_554 1_554 ?
Na4 Mg2 Mg3 60.41(6) 1_554 4_554 ?
Na4 Mg2 Na1 172.90(8) 1_554 1_556 ?
Na1 Mg2 Mg3 81.50(6) 1_556 1_554 ?
O14 Mg2 P4 86.90(12) 1_554 2_665 ?
O14 Mg2 P3 90.39(13) 1_554 4_554 ?
O14 Mg2 Mg3 68.06(11) 1_554 1_554 ?
O14 Mg2 Mg3 109.34(13) 1_554 4_554 ?
O14 Mg2 Na4 49.94(12) 1_554 1_554 ?
O14 Mg2 Na1 134.12(13) 1_554 1_556 ?
O14 Mg2 O11 88.99(17) 1_554 4_554 ?
O14 Mg2 O9 88.19(16) 1_554 4_554 ?
O11 Mg2 P4 101.53(11) 4_554 2_665 ?
O11 Mg2 P3 33.54(10) 4_554 4_554 ?
O11 Mg2 Mg3 93.81(11) 4_554 1_554 ?
O11 Mg2 Mg3 35.24(10) 4_554 4_554 ?
O11 Mg2 Na4 53.99(12) 4_554 1_554 ?
O11 Mg2 Na1 127.77(13) 4_554 1_556 ?
O11 Mg2 O9 67.57(13) 4_554 4_554 ?
O15 Mg2 P4 88.76(12) . 2_665 ?
O15 Mg2 P3 95.84(13) . 4_554 ?
O15 Mg2 Mg3 73.70(12) . 4_554 ?
O15 Mg2 Mg3 114.74(13) . 1_554 ?
O15 Mg2 Na4 131.55(13) . 1_554 ?
O15 Mg2 Na1 43.60(11) . 1_556 ?
O15 Mg2 O14 173.77(17) . 1_554 ?
O15 Mg2 O11 96.27(17) . 4_554 ?
O15 Mg2 O6 85.00(17) . 2_665 ?
O15 Mg2 O9 96.89(17) . 4_554 ?
O3 Mg2 P4 92.15(12) . 2_665 ?
O3 Mg2 P3 132.77(13) . 4_554 ?
O3 Mg2 Mg3 152.17(14) . 4_554 ?
O3 Mg2 Mg3 74.78(12) . 1_554 ?
O3 Mg2 Na4 136.02(14) . 1_554 ?
O3 Mg2 Na1 43.92(13) . 1_556 ?
O3 Mg2 O14 93.78(18) . 1_554 ?
O3 Mg2 O11 166.17(16) . 4_554 ?
O3 Mg2 O15 81.90(16) . . ?
O3 Mg2 O6 115.04(16) . 2_665 ?
O3 Mg2 O9 98.95(15) . 4_554 ?
O6 Mg2 P4 24.11(11) 2_665 2_665 ?
O6 Mg2 P3 111.69(12) 2_665 4_554 ?
O6 Mg2 Mg3 50.53(12) 2_665 4_554 ?
O6 Mg2 Mg3 159.62(14) 2_665 1_554 ?
O6 Mg2 Na4 54.69(12) 2_665 1_554 ?
O6 Mg2 Na1 118.24(14) 2_665 1_556 ?
O6 Mg2 O14 92.82(17) 2_665 1_554 ?
O6 Mg2 O11 78.29(15) 2_665 4_554 ?
O6 Mg2 O9 145.82(16) 2_665 4_554 ?
O9 Mg2 P4 168.14(12) 4_554 2_665 ?
O9 Mg2 P3 34.14(9) 4_554 4_554 ?
O9 Mg2 Mg3 97.11(11) 4_554 4_554 ?
O9 Mg2 Mg3 33.03(10) 4_554 1_554 ?
O9 Mg2 Na4 103.01(12) 4_554 1_554 ?
O9 Mg2 Na1 83.50(11) 4_554 1_556 ?
P2 Mg1 Mg3 58.63(5) 4_544 1_554 ?
P2 Mg1 Na2 150.08(10) 4_544 2_655 ?
P2 Mg1 Na2 142.65(10) 4_544 . ?
P2 Mg1 Na4 70.29(6) 4_544 1_544 ?
P2 Mg1 Na1 97.20(7) 4_544 1_556 ?
Na2 Mg1 Mg3 98.60(8) . 1_554 ?
Na2 Mg1 Mg3 125.63(7) 2_655 1_554 ?
Na2 Mg1 Na2 66.81(4) . 2_655 ?
Na2 Mg1 Na4 130.02(8) 2_655 1_544 ?
Na2 Mg1 Na4 86.29(8) . 1_544 ?
Na2 Mg1 Na1 59.53(6) 2_655 1_556 ?
Na2 Mg1 Na1 107.13(7) . 1_556 ?
Na4 Mg1 Mg3 98.49(7) 1_544 1_554 ?
Na4 Mg1 Na1 166.48(8) 1_544 1_556 ?
Na1 Mg1 Mg3 78.33(6) 1_556 1_554 ?
O12 Mg1 P2 34.25(9) 4_544 4_544 ?
O12 Mg1 Mg3 90.29(11) 4_544 1_554 ?
O12 Mg1 Na2 138.68(14) 4_544 2_655 ?
O12 Mg1 Na2 133.68(14) 4_544 . ?
O12 Mg1 Na4 47.39(11) 4_544 1_544 ?
O12 Mg1 Na1 119.18(13) 4_544 1_556 ?
O12 Mg1 O13 68.67(13) 4_544 4_544 ?
O10 Mg1 P2 92.23(13) 1_554 4_544 ?
O10 Mg1 Mg3 71.17(12) 1_554 1_554 ?
O10 Mg1 Na2 117.53(15) 1_554 2_655 ?
O10 Mg1 Na2 50.75(13) 1_554 . ?
O10 Mg1 Na4 51.43(12) 1_554 1_544 ?
O10 Mg1 Na1 136.92(13) 1_554 1_556 ?
O10 Mg1 O12 91.09(16) 1_554 4_544 ?
O10 Mg1 O4 92.12(17) 1_554 . ?
O10 Mg1 O7 84.66(17) 1_554 2_655 ?
O10 Mg1 O13 91.35(16) 1_554 4_544 ?
O4 Mg1 P2 130.48(13) . 4_544 ?
O4 Mg1 Mg3 76.50(12) . 1_554 ?
O4 Mg1 Na2 57.70(12) . . ?
O4 Mg1 Na2 50.85(12) . 2_655 ?
O4 Mg1 Na4 141.63(15) . 1_544 ?
O4 Mg1 Na1 50.83(12) . 1_556 ?
O4 Mg1 O12 164.56(16) . 4_544 ?
O4 Mg1 O7 84.95(14) . 2_655 ?
O4 Mg1 O13 96.15(15) . 4_544 ?
O7 Mg1 P2 144.57(12) 2_655 4_544 ?
O7 Mg1 Mg3 148.62(14) 2_655 1_554 ?
O7 Mg1 Na2 50.03(12) 2_655 . ?
O7 Mg1 Na2 49.69(11) 2_655 2_655 ?
O7 Mg1 Na4 80.56(12) 2_655 1_544 ?
O7 Mg1 Na1 109.07(12) 2_655 1_556 ?
O7 Mg1 O12 110.39(15) 2_655 4_544 ?
O7 Mg1 O13 175.90(19) 2_655 4_544 ?
O8 Mg1 P2 95.04(13) . 4_544 ?
O8 Mg1 Mg3 117.26(12) . 1_554 ?
O8 Mg1 Na2 122.29(14) . . ?
O8 Mg1 Na2 55.68(13) . 2_655 ?
O8 Mg1 Na4 126.73(13) . 1_544 ?
O8 Mg1 Na1 47.17(10) . 1_556 ?
O8 Mg1 O12 91.95(17) . 4_544 ?
O8 Mg1 O10 171.02(17) . 1_554 ?
O8 Mg1 O4 87.18(17) . . ?
O8 Mg1 O7 86.36(17) . 2_655 ?
O8 Mg1 O13 97.63(17) . 4_544 ?
O13 Mg1 P2 34.44(10) 4_544 4_544 ?
O13 Mg1 Mg3 29.04(11) 4_544 1_554 ?
O13 Mg1 Na2 127.51(14) 4_544 . ?
O13 Mg1 Na2 133.69(13) 4_544 2_655 ?
O13 Mg1 Na4 96.23(12) 4_544 1_544 ?
O13 Mg1 Na1 74.53(12) 4_544 1_556 ?
P1 Mg3 Mg2 130.15(7) 1_556 4_545 ?
P1 Mg3 Na4 121.98(8) 1_556 4_544 ?
P1 Mg3 Na4 90.47(6) 1_556 4_545 ?
P1 Mg3 Na1 62.74(6) 1_556 1_556 ?
P2 Mg3 P1 83.65(5) . 1_556 ?
P2 Mg3 Mg2 122.34(8) . 4_545 ?
P2 Mg3 Na4 119.61(7) . 4_545 ?
P2 Mg3 Na4 65.86(6) . 4_544 ?
P2 Mg3 Na1 58.65(5) . 1_556 ?
Mg2 Mg3 Na4 106.79(7) 4_545 4_545 ?
Mg2 Mg3 Na1 93.43(7) 4_545 1_556 ?
Na4 Mg3 Mg2 56.67(6) 4_544 4_545 ?
Na4 Mg3 Na4 147.34(9) 4_544 4_545 ?
Na4 Mg3 Na1 59.26(7) 4_544 1_556 ?
Na4 Mg3 Na1 153.11(8) 4_545 1_556 ?
O12 Mg3 P1 107.02(12) . 1_556 ?
O12 Mg3 P2 24.21(10) . . ?
O12 Mg3 Mg2 100.95(13) . 4_545 ?
O12 Mg3 Na4 47.36(12) . 4_544 ?
O12 Mg3 Na4 124.18(13) . 4_545 ?
O12 Mg3 Na1 66.72(12) . 1_556 ?
O12 Mg3 O11 96.41(18) . . ?
O12 Mg3 O6 75.73(14) . 3_456 ?
O12 Mg3 O2 91.92(16) . 1_556 ?
O12 Mg3 O13 169.03(18) . 4_545 ?
O12 Mg3 O9 85.33(16) . 4 ?
O11 Mg3 P1 98.81(11) . 1_556 ?
O11 Mg3 P2 106.66(13) . . ?
O11 Mg3 Mg2 36.80(10) . 4_545 ?
O11 Mg3 Na4 51.38(12) . 4_544 ?
O11 Mg3 Na4 133.55(13) . 4_545 ?
O11 Mg3 Na1 58.87(11) . 1_556 ?
O11 Mg3 O6 68.41(14) . 3_456 ?
O11 Mg3 O2 83.11(15) . 1_556 ?
O11 Mg3 O13 91.21(16) . 4_545 ?
O11 Mg3 O9 172.00(17) . 4 ?
O6 Mg3 P1 167.22(11) 3_456 1_556 ?
O6 Mg3 P2 99.92(10) 3_456 . ?
O6 Mg3 Mg2 38.08(8) 3_456 4_545 ?
O6 Mg3 Na4 50.56(10) 3_456 4_544 ?
O6 Mg3 Na4 98.25(11) 3_456 4_545 ?
O6 Mg3 Na1 108.54(12) 3_456 1_556 ?
O2 Mg3 P1 23.26(11) 1_556 1_556 ?
O2 Mg3 P2 71.91(11) 1_556 . ?
O2 Mg3 Mg2 119.20(12) 1_556 4_545 ?
O2 Mg3 Na4 98.72(13) 1_556 4_544 ?
O2 Mg3 Na4 113.71(13) 1_556 4_545 ?
O2 Mg3 Na1 39.48(12) 1_556 1_556 ?
O2 Mg3 O6 147.02(17) 1_556 3_456 ?
O13 Mg3 P1 79.44(11) 4_545 1_556 ?
O13 Mg3 P2 157.08(14) 4_545 . ?
O13 Mg3 Mg2 80.55(12) 4_545 4_545 ?
O13 Mg3 Na4 45.81(12) 4_545 4_545 ?
O13 Mg3 Na4 136.76(14) 4_545 4_544 ?
O13 Mg3 Na1 124.18(12) 4_545 1_556 ?
O13 Mg3 O6 99.96(14) 4_545 3_456 ?
O13 Mg3 O2 96.82(16) 4_545 1_556 ?
O13 Mg3 O9 86.05(18) 4_545 4 ?
O9 Mg3 P1 88.09(12) 4 1_556 ?
O9 Mg3 P2 77.99(11) 4 . ?
O9 Mg3 Mg2 135.21(13) 4 4_545 ?
O9 Mg3 Na4 127.68(13) 4 4_544 ?
O9 Mg3 Na4 41.69(11) 4 4_545 ?
O9 Mg3 Na1 128.61(13) 4 1_556 ?
O9 Mg3 O6 104.64(15) 4 3_456 ?
O9 Mg3 O2 104.67(16) 4 1_556 ?
Mg1 Na2 P1 60.74(6) . . ?
Mg1 Na2 P1 108.47(7) 2_654 . ?
Mg1 Na2 Mg1 166.03(10) . 2_654 ?
Mg1 Na2 Na2 112.02(12) 2_654 2_655 ?
Mg1 Na2 Na2 130.82(12) . 2_654 ?
Mg1 Na2 Na2 56.72(8) . 2_655 ?
Mg1 Na2 Na2 56.47(9) 2_654 2_654 ?
Mg1 Na2 Na1 68.98(7) 2_654 2_655 ?
Mg1 Na2 Na1 114.14(9) . 2_655 ?
Na2 Na2 P1 98.58(10) 2_654 . ?
Na2 Na2 P1 67.01(9) 2_655 . ?
Na2 Na2 Na2 159.05(14) 2_654 2_655 ?
Na2 Na2 Na1 106.69(11) 2_654 2_655 ?
Na2 Na2 Na1 81.77(9) 2_655 2_655 ?
Na1 Na2 P1 145.42(10) 2_655 . ?
O10 Na2 P1 76.56(11) 1_554 . ?
O10 Na2 Mg1 43.40(11) 1_554 . ?
O10 Na2 Mg1 146.96(16) 1_554 2_654 ?
O10 Na2 Na2 100.10(15) 1_554 2_655 ?
O10 Na2 Na2 90.61(14) 1_554 2_654 ?
O10 Na2 Na1 125.33(12) 1_554 2_655 ?
O10 Na2 O4 115.24(16) 1_554 2_654 ?
O10 Na2 O4 74.60(14) 1_554 . ?
O10 Na2 O8 170.48(19) 1_554 2_654 ?
O4 Na2 P1 144.93(14) 2_654 . ?
O4 Na2 P1 25.35(9) . . ?
O4 Na2 Mg1 123.80(11) . 2_654 ?
O4 Na2 Mg1 42.81(9) . . ?
O4 Na2 Mg1 150.14(13) 2_654 . ?
O4 Na2 Mg1 43.41(10) 2_654 2_654 ?
O4 Na2 Na2 50.88(11) 2_654 2_654 ?
O4 Na2 Na2 135.31(16) 2_654 2_655 ?
O4 Na2 Na2 44.74(11) . 2_655 ?
O4 Na2 Na2 123.56(14) . 2_654 ?
O4 Na2 Na1 55.97(11) 2_654 2_655 ?
O4 Na2 Na1 126.51(13) . 2_655 ?
O4 Na2 O4 167.02(11) 2_654 . ?
O4 Na2 O8 71.79(15) 2_654 2_654 ?
O7 Na2 P1 95.65(12) 2_655 . ?
O7 Na2 P1 69.96(11) . . ?
O7 Na2 Mg1 134.60(13) 2_655 2_654 ?
O7 Na2 Mg1 44.84(10) 2_655 . ?
O7 Na2 Mg1 44.71(10) . 2_654 ?
O7 Na2 Mg1 129.02(13) . . ?
O7 Na2 Na2 44.20(12) . 2_654 ?
O7 Na2 Na2 114.89(15) . 2_655 ?
O7 Na2 Na2 44.05(10) 2_655 2_655 ?
O7 Na2 Na2 156.79(15) 2_655 2_654 ?
O7 Na2 Na1 113.53(13) . 2_655 ?
O7 Na2 Na1 69.46(11) 2_655 2_655 ?
O7 Na2 O10 74.96(14) 2_655 1_554 ?
O7 Na2 O10 114.54(16) . 1_554 ?
O7 Na2 O4 119.05(15) 2_655 2_654 ?
O7 Na2 O4 75.26(15) . 2_654 ?
O7 Na2 O4 70.64(14) 2_655 . ?
O7 Na2 O4 93.12(14) . . ?
O7 Na2 O7 158.92(19) . 2_655 ?
O7 Na2 O8 96.12(15) 2_655 2_654 ?
O7 Na2 O8 72.79(14) . 2_654 ?
O8 Na2 P1 101.45(11) 2_654 . ?
O8 Na2 Mg1 42.55(11) 2_654 2_654 ?
O8 Na2 Mg1 127.46(14) 2_654 . ?
O8 Na2 Na2 70.75(13) 2_654 2_655 ?
O8 Na2 Na2 98.90(15) 2_654 2_654 ?
O8 Na2 Na1 52.15(9) 2_654 2_655 ?
O8 Na2 O4 99.53(14) 2_654 . ?
P2 Na4 P3 113.79(9) . 1_565 ?
P2 Na4 Mg2 66.40(6) . 1_556 ?
P2 Na4 Mg1 158.87(9) . 1_566 ?
P2 Na4 Mg3 119.72(8) . 4 ?
P3 Na4 Mg2 157.70(9) 1_565 1_556 ?
P3 Na4 Mg1 64.40(6) 1_565 1_566 ?
P3 Na4 Mg3 125.57(8) 1_565 4 ?
Mg2 Na4 Mg1 106.86(8) 1_556 1_566 ?
Mg2 Na4 Mg3 62.92(7) 1_556 4 ?
Mg3 Na4 Mg1 69.24(7) 4 1_566 ?
O14 Na4 P2 29.73(10) . . ?
O14 Na4 P3 128.51(14) . 1_565 ?
O14 Na4 Mg2 41.75(10) . 1_556 ?
O14 Na4 Mg1 133.41(13) . 1_566 ?
O14 Na4 Mg3 103.79(12) . 4 ?
O14 Na4 O12 139.94(16) . 4 ?
O14 Na4 O11 72.74(13) . 4 ?
O14 Na4 O10 127.18(16) . 1_565 ?
O14 Na4 O6 74.31(14) . 2_666 ?
O14 Na4 O13 60.33(13) . . ?
O14 Na4 O9 117.90(17) . 1_565 ?
O12 Na4 P2 156.03(13) 4 . ?
O12 Na4 P3 87.53(10) 4 1_565 ?
O12 Na4 Mg2 98.23(12) 4 1_556 ?
O12 Na4 Mg1 40.46(9) 4 1_566 ?
O12 Na4 Mg3 38.04(9) 4 4 ?
O12 Na4 O11 74.84(14) 4 4 ?
O12 Na4 O10 74.02(13) 4 1_565 ?
O12 Na4 O6 69.93(13) 4 2_666 ?
O12 Na4 O13 142.29(15) 4 . ?
O11 Na4 P2 81.76(10) 4 . ?
O11 Na4 P3 157.94(12) 4 1_565 ?
O11 Na4 Mg2 41.87(9) 4 1_556 ?
O11 Na4 Mg1 106.90(12) 4 1_566 ?
O11 Na4 Mg3 38.39(9) 4 4 ?
O11 Na4 O10 146.08(16) 4 1_565 ?
O11 Na4 O6 61.80(13) 4 2_666 ?
O11 Na4 O13 89.96(13) 4 . ?
O10 Na4 P2 129.95(13) 1_565 . ?
O10 Na4 P3 29.83(9) 1_565 1_565 ?
O10 Na4 Mg2 131.90(12) 1_565 1_556 ?
O10 Na4 Mg1 39.19(9) 1_565 1_566 ?
O10 Na4 Mg3 108.03(12) 1_565 4 ?
O10 Na4 O6 94.78(14) 1_565 2_666 ?
O6 Na4 P2 103.50(11) 2_666 . ?
O6 Na4 P3 124.60(12) 2_666 1_565 ?
O6 Na4 Mg2 40.87(9) 2_666 1_556 ?
O6 Na4 Mg1 66.15(10) 2_666 1_566 ?
O6 Na4 Mg3 50.81(10) 2_666 4 ?
O13 Na4 P2 30.71(8) . . ?
O13 Na4 P3 96.34(11) . 1_565 ?
O13 Na4 Mg2 92.18(10) . 1_556 ?
O13 Na4 Mg1 160.51(12) . 1_566 ?
O13 Na4 Mg3 125.30(12) . 4 ?
O13 Na4 O10 123.25(15) . 1_565 ?
O13 Na4 O6 132.36(14) . 2_666 ?
O9 Na4 P2 92.81(12) 1_565 . ?
O9 Na4 P3 30.07(9) 1_565 1_565 ?
O9 Na4 Mg2 159.12(13) 1_565 1_556 ?
O9 Na4 Mg1 91.85(11) 1_565 1_566 ?
O9 Na4 Mg3 134.89(12) 1_565 4 ?
O9 Na4 O12 102.10(14) 1_565 4 ?
O9 Na4 O11 141.18(15) 1_565 4 ?
O9 Na4 O10 59.89(13) 1_565 1_565 ?
O9 Na4 O6 154.59(16) 1_565 2_666 ?
O9 Na4 O13 68.69(14) 1_565 . ?
P1 Na3 P4 103.71(7) 2_665 1_556 ?
P1 Na3 Na3 61.30(7) 2_665 2_664 ?
P1 Na3 Na1 123.31(10) 2_665 1_556 ?
P2 Na3 P1 128.41(9) . 2_665 ?
P2 Na3 P4 111.53(8) . 1_556 ?
P2 Na3 Na3 102.25(9) . 2_664 ?
P2 Na3 Na1 59.07(6) . 1_556 ?
P4 Na3 Na3 64.06(8) 1_556 2_664 ?
P4 Na3 Na1 55.75(6) 1_556 1_556 ?
Na1 Na3 Na3 62.48(8) 1_556 2_664 ?
O14 Na3 P1 138.07(13) . 2_665 ?
O14 Na3 P2 28.49(10) . . ?
O14 Na3 P4 117.55(12) . 1_556 ?
O14 Na3 Na3 130.61(15) . 2_664 ?
O14 Na3 Na1 78.48(11) . 1_556 ?
O14 Na3 O15 57.56(13) . . ?
O14 Na3 O3 158.15(16) . 2_665 ?
O14 Na3 O1 97.48(14) . 1_556 ?
O14 Na3 O1 115.50(16) . 2_665 ?
O14 Na3 O5 117.67(15) . 1_556 ?
O14 Na3 O5 86.25(15) . 2_666 ?
O15 Na3 P1 111.64(12) . 2_665 ?
O15 Na3 P2 29.12(9) . . ?
O15 Na3 P4 98.17(10) . 1_556 ?
O15 Na3 Na3 73.13(10) . 2_664 ?
O15 Na3 Na1 42.86(9) . 1_556 ?
O15 Na3 O1 106.73(12) . 1_556 ?
O3 Na3 P1 27.82(9) 2_665 2_665 ?
O3 Na3 P2 155.81(14) 2_665 . ?
O3 Na3 P4 82.14(10) 2_665 1_556 ?
O3 Na3 Na3 64.82(12) 2_665 2_664 ?
O3 Na3 Na1 122.68(13) 2_665 1_556 ?
O3 Na3 O15 132.94(16) 2_665 . ?
O3 Na3 O1 96.46(13) 2_665 1_556 ?
O3 Na3 O1 57.42(13) 2_665 2_665 ?
O3 Na3 O5 84.17(14) 2_665 1_556 ?
O3 Na3 O5 77.69(14) 2_665 2_666 ?
O1 Na3 P1 30.83(9) 2_665 2_665 ?
O1 Na3 P1 123.44(10) 1_556 2_665 ?
O1 Na3 P2 98.39(12) 2_665 . ?
O1 Na3 P2 105.06(10) 1_556 . ?
O1 Na3 P4 115.56(12) 2_665 1_556 ?
O1 Na3 P4 29.78(8) 1_556 1_556 ?
O1 Na3 Na3 93.78(12) 1_556 2_664 ?
O1 Na3 Na3 54.27(9) 2_665 2_664 ?
O1 Na3 Na1 104.70(12) 2_665 1_556 ?
O1 Na3 Na1 66.70(9) 1_556 1_556 ?
O1 Na3 O15 81.46(13) 2_665 . ?
O1 Na3 O1 144.03(12) 2_665 1_556 ?
O5 Na3 P1 86.99(12) 2_666 2_665 ?
O5 Na3 P1 96.14(12) 1_556 2_665 ?
O5 Na3 P2 99.81(12) 1_556 . ?
O5 Na3 P2 113.77(12) 2_666 . ?
O5 Na3 P4 25.56(10) 1_556 1_556 ?
O5 Na3 P4 109.40(13) 2_666 1_556 ?
O5 Na3 Na3 142.39(15) 2_666 2_664 ?
O5 Na3 Na3 42.28(11) 1_556 2_664 ?
O5 Na3 Na1 147.36(14) 2_666 1_556 ?
O5 Na3 Na1 40.92(10) 1_556 1_556 ?
O5 Na3 O15 142.11(15) 2_666 . ?
O5 Na3 O15 78.40(13) 1_556 . ?
O5 Na3 O1 96.51(14) 1_556 2_665 ?
O5 Na3 O1 87.23(14) 2_666 1_556 ?
O5 Na3 O1 107.90(15) 2_666 2_665 ?
O5 Na3 O1 53.19(12) 1_556 1_556 ?
O5 Na3 O5 134.10(14) 1_556 2_666 ?
P1 Na1 P2 116.87(8) 1_554 1_554 ?
P1 Na1 P4 104.00(7) 1_554 . ?
P1 Na1 P3 113.59(8) 1_554 1_554 ?
P1 Na1 Na2 69.63(7) 1_554 2_654 ?
P1 Na1 Na4 94.15(8) 1_554 4_543 ?
P2 Na1 P3 109.80(7) 1_554 1_554 ?
P2 Na1 Na2 171.60(10) 1_554 2_654 ?
P2 Na1 Na4 63.03(6) 1_554 4_543 ?
P4 Na1 P2 108.30(8) . 1_554 ?
P4 Na1 P3 103.03(7) . 1_554 ?
P4 Na1 Na2 63.97(6) . 2_654 ?
P4 Na1 Na4 161.82(10) . 4_543 ?
P3 Na1 Na4 67.92(6) 1_554 4_543 ?
Na2 Na1 P3 70.33(6) 2_654 1_554 ?
Na2 Na1 Na4 123.28(9) 2_654 4_543 ?
O15 Na1 P1 93.43(13) 1_554 1_554 ?
O15 Na1 P2 25.06(10) 1_554 1_554 ?
O15 Na1 P4 108.49(12) 1_554 . ?
O15 Na1 P3 131.57(12) 1_554 1_554 ?
O15 Na1 Na2 157.57(14) 1_554 2_654 ?
O15 Na1 Na4 70.86(11) 1_554 4_543 ?
O15 Na1 O4 121.90(16) 1_554 1_554 ?
O15 Na1 O3 66.96(14) 1_554 1_554 ?
O15 Na1 O8 150.12(16) 1_554 1_554 ?
O4 Na1 P1 28.85(8) 1_554 1_554 ?
O4 Na1 P2 143.63(12) 1_554 1_554 ?
O4 Na1 P4 96.90(10) 1_554 . ?
O4 Na1 P3 88.73(10) 1_554 1_554 ?
O4 Na1 Na2 44.04(9) 1_554 2_654 ?
O4 Na1 Na4 98.57(11) 1_554 4_543 ?
O3 Na1 P1 28.08(9) 1_554 1_554 ?
O3 Na1 P2 91.66(10) 1_554 1_554 ?
O3 Na1 P4 102.78(11) 1_554 . ?
O3 Na1 P3 138.81(13) 1_554 1_554 ?
O3 Na1 Na2 93.33(12) 1_554 2_654 ?
O3 Na1 Na4 93.70(12) 1_554 4_543 ?
O3 Na1 O4 56.68(13) 1_554 1_554 ?
O3 Na1 O8 117.27(15) 1_554 1_554 ?
O8 Na1 P1 89.71(11) 1_554 1_554 ?
O8 Na1 P2 134.07(12) 1_554 1_554 ?
O8 Na1 P4 99.49(11) 1_554 . ?
O8 Na1 P3 26.38(9) 1_554 1_554 ?
O8 Na1 Na2 48.18(10) 1_554 2_654 ?
O8 Na1 Na4 79.28(11) 1_554 4_543 ?
O8 Na1 O4 62.94(12) 1_554 1_554 ?
O2 Na1 P1 174.28(13) . 1_554 ?
O2 Na1 P2 66.84(11) . 1_554 ?
O2 Na1 P4 70.38(11) . . ?
O2 Na1 P3 67.63(11) . 1_554 ?
O2 Na1 Na2 106.27(13) . 2_654 ?
O2 Na1 Na4 91.45(12) . 4_543 ?
O2 Na1 O15 89.45(15) . 1_554 ?
O2 Na1 O4 148.64(15) . 1_554 ?
O2 Na1 O3 152.49(17) . 1_554 ?
O2 Na1 O8 90.24(15) . 1_554 ?
O5 Na1 P1 89.61(12) . 1_554 ?
O5 Na1 P2 96.91(12) . 1_554 ?
O5 Na1 P4 25.89(10) . . ?
O5 Na1 P3 128.87(13) . 1_554 ?
O5 Na1 Na2 77.34(12) . 2_654 ?
O5 Na1 Na4 159.00(13) . 4_543 ?
O5 Na1 O15 88.31(15) . 1_554 ?
O5 Na1 O4 94.67(14) . 1_554 ?
O5 Na1 O3 80.04(15) . 1_554 ?
O5 Na1 O8 121.45(15) . 1_554 ?
O5 Na1 O2 85.54(16) . . ?
P2 O14 Mg2 138.2(2) . 1_556 ?
P2 O14 Na4 98.94(19) . . ?
P2 O14 Na3 104.6(2) . . ?
Mg2 O14 Na4 88.31(16) 1_556 . ?
Mg2 O14 Na3 111.30(19) 1_556 . ?
Na3 O14 Na4 110.22(15) . . ?
P2 O12 Mg1 95.24(17) . 4 ?
P2 O12 Mg3 123.5(2) . . ?
P2 O12 Na4 122.1(2) . 4_544 ?
Mg1 O12 Na4 92.15(15) 4 4_544 ?
Mg3 O12 Mg1 127.34(18) . 4 ?
Mg3 O12 Na4 94.60(14) . 4_544 ?
P3 O11 Mg2 97.57(17) . 4_545 ?
P3 O11 Mg3 133.7(2) . . ?
P3 O11 Na4 131.1(2) . 4_544 ?
Mg2 O11 Na4 84.14(14) 4_545 4_544 ?
Mg3 O11 Mg2 107.97(17) . 4_545 ?
Mg3 O11 Na4 90.23(14) . 4_544 ?
P2 O15 Mg2 134.4(2) . . ?
P2 O15 Na3 87.35(18) . . ?
P2 O15 Na1 112.1(2) . 1_556 ?
Mg2 O15 Na3 127.17(18) . . ?
Mg2 O15 Na1 100.42(17) . 1_556 ?
Na1 O15 Na3 85.87(14) 1_556 . ?
P3 O10 Mg1 139.8(2) . 1_556 ?
P3 O10 Na2 124.2(2) . 1_556 ?
P3 O10 Na4 93.77(18) . 1_545 ?
Mg1 O10 Na2 85.84(17) 1_556 1_556 ?
Mg1 O10 Na4 89.38(15) 1_556 1_545 ?
Na2 O10 Na4 122.85(17) 1_556 1_545 ?
P1 O4 Mg1 128.0(2) . . ?
P1 O4 Na2 107.7(2) . . ?
P1 O4 Na2 145.1(2) . 2_655 ?
P1 O4 Na1 88.27(17) . 1_556 ?
Mg1 O4 Na2 79.49(14) . . ?
Mg1 O4 Na2 85.74(15) . 2_655 ?
Mg1 O4 Na1 93.98(15) . 1_556 ?
Na2 O4 Na2 84.38(11) 2_655 . ?
Na2 O4 Na1 79.98(14) 2_655 1_556 ?
Na2 O4 Na1 163.48(17) . 1_556 ?
P1 O3 Mg2 130.9(2) . . ?
P1 O3 Na3 103.63(18) . 2_664 ?
P1 O3 Na1 102.54(19) . 1_556 ?
Mg2 O3 Na3 113.83(17) . 2_664 ?
Mg2 O3 Na1 100.86(17) . 1_556 ?
Na3 O3 Na1 100.19(16) 2_664 1_556 ?
P4 O6 Mg2 122.0(2) . 2_664 ?
P4 O6 Mg3 145.6(2) . 3_554 ?
P4 O6 Na4 110.2(2) . 2_663 ?
Mg2 O6 Mg3 91.39(14) 2_664 3_554 ?
Mg2 O6 Na4 84.44(15) 2_664 2_663 ?
Na4 O6 Mg3 78.63(12) 2_663 3_554 ?
P4 O7 Mg1 123.2(2) . 2_654 ?
P4 O7 Na2 128.0(2) . 2_654 ?
P4 O7 Na2 129.0(2) . . ?
Mg1 O7 Na2 85.13(15) 2_654 2_654 ?
Mg1 O7 Na2 85.60(15) 2_654 . ?
Na2 O7 Na2 91.75(12) . 2_654 ?
P1 O1 P4 130.8(2) . . ?
P1 O1 Na3 92.68(18) . 2_664 ?
P1 O1 Na3 93.33(16) . 1_554 ?
P4 O1 Na3 134.6(2) . 2_664 ?
P4 O1 Na3 84.31(16) . 1_554 ?
Na3 O1 Na3 80.46(10) 2_664 1_554 ?
P3 O8 Mg1 133.4(2) . . ?
P3 O8 Na2 142.6(2) . 2_655 ?
P3 O8 Na1 102.52(18) . 1_556 ?
Mg1 O8 Na2 81.77(15) . 2_655 ?
Mg1 O8 Na1 98.30(15) . 1_556 ?
Na2 O8 Na1 79.67(12) 2_655 1_556 ?
P1 O2 Mg3 122.8(2) . 1_554 ?
P1 O2 Na1 131.9(2) . . ?
Mg3 O2 Na1 105.29(18) 1_554 . ?
P2 O13 Mg1 93.40(17) . 4 ?
P2 O13 Mg3 127.1(2) . 4_554 ?
P2 O13 Na4 92.17(17) . . ?
Mg1 O13 Na4 124.29(18) 4 . ?
Mg3 O13 Mg1 119.85(19) 4_554 4 ?
Mg3 O13 Na4 99.32(15) 4_554 . ?
P3 O9 Mg2 91.93(18) . 4_545 ?
P3 O9 Mg3 137.9(2) . 4_544 ?
P3 O9 Na4 99.15(19) . 1_545 ?
Mg2 O9 Na4 112.87(18) 4_545 1_545 ?
Mg3 O9 Mg2 110.75(17) 4_544 4_545 ?
Mg3 O9 Na4 103.44(16) 4_544 1_545 ?
P4 O5 Na3 135.2(2) . 2_663 ?
P4 O5 Na3 109.5(2) . 1_554 ?
P4 O5 Na1 111.2(2) . . ?
Na3 O5 Na3 95.73(13) 1_554 2_663 ?
Na1 O5 Na3 95.63(15) . 1_554 ?
Na1 O5 Na3 102.02(17) . 2_663 ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Mg2 P4 O6 Mg3 164.2(6) 2_664 . . 3_554 ?
Mg2 P4 O6 Na4 -96.2(3) 2_664 . . 2_663 ?
Mg2 P4 O7 Mg1 22.6(4) 2_664 . . 2_654 ?
Mg2 P4 O7 Na2 136.89(19) 2_664 . . . ?
Mg2 P4 O7 Na2 -89.9(3) 2_664 . . 2_654 ?
Mg2 P4 O1 P1 152.1(3) 2_664 . . . ?
Mg2 P4 O1 Na3 62.65(10) 2_664 . . 1_554 ?
Mg2 P4 O1 Na3 -7.9(3) 2_664 . . 2_664 ?
Mg2 P4 O5 Na3 -71.76(16) 2_664 . . 1_554 ?
Mg2 P4 O5 Na3 48.7(3) 2_664 . . 2_663 ?
Mg2 P4 O5 Na1 -176.2(2) 2_664 . . . ?
Mg2 P3 O11 Mg3 123.9(4) 4_545 . . . ?
Mg2 P3 O11 Na4 -88.8(3) 4_545 . . 4_544 ?
Mg2 P3 O10 Mg1 -36.5(4) 4_545 . . 1_556 ?
Mg2 P3 O10 Na2 -168.37(15) 4_545 . . 1_556 ?
Mg2 P3 O10 Na4 57.03(16) 4_545 . . 1_545 ?
Mg2 P3 O8 Mg1 -29.6(4) 4_545 . . . ?
Mg2 P3 O8 Na2 174.1(2) 4_545 . . 2_655 ?
Mg2 P3 O8 Na1 84.8(2) 4_545 . . 1_556 ?
Mg2 P3 O9 Mg3 124.5(4) 4_545 . . 4_544 ?
Mg2 P3 O9 Na4 -113.5(2) 4_545 . . 1_545 ?
Mg1 P2 O14 Mg2 35.7(4) 4 . . 1_556 ?
Mg1 P2 O14 Na4 -61.9(2) 4 . . . ?
Mg1 P2 O14 Na3 -175.63(9) 4 . . . ?
Mg1 P2 O12 Mg3 -142.3(3) 4 . . . ?
Mg1 P2 O12 Na4 95.8(2) 4 . . 4_544 ?
Mg1 P2 O15 Mg2 33.2(4) 4 . . . ?
Mg1 P2 O15 Na3 176.49(10) 4 . . . ?
Mg1 P2 O15 Na1 -99.1(2) 4 . . 1_556 ?
Mg1 P2 O13 Mg3 -132.1(3) 4 . . 4_554 ?
Mg1 P2 O13 Na4 124.55(19) 4 . . . ?
Mg3 P1 O4 Mg1 5.7(3) 1_554 . . . ?
Mg3 P1 O4 Na2 96.15(14) 1_554 . . . ?
Mg3 P1 O4 Na2 -157.6(4) 1_554 . . 2_655 ?
Mg3 P1 O4 Na1 -87.98(10) 1_554 . . 1_556 ?
Mg3 P1 O3 Mg2 -25.6(3) 1_554 . . . ?
Mg3 P1 O3 Na3 -165.07(14) 1_554 . . 2_664 ?
Mg3 P1 O3 Na1 91.01(13) 1_554 . . 1_556 ?
Mg3 P1 O1 P4 -37.6(5) 1_554 . . . ?
Mg3 P1 O1 Na3 47.8(3) 1_554 . . 1_554 ?
Mg3 P1 O1 Na3 128.38(18) 1_554 . . 2_664 ?
Mg3 P1 O2 Na1 -179.9(5) 1_554 . . . ?
Mg3 P2 O14 Mg2 -36.0(3) . . . 1_556 ?
Mg3 P2 O14 Na4 -133.50(14) . . . . ?
Mg3 P2 O14 Na3 112.76(14) . . . . ?
Mg3 P2 O12 Mg1 142.3(3) . . . 4 ?
Mg3 P2 O12 Na4 -121.9(3) . . . 4_544 ?
Mg3 P2 O15 Mg2 121.5(3) . . . . ?
Mg3 P2 O15 Na3 -95.24(10) . . . . ?
Mg3 P2 O15 Na1 -10.8(2) . . . 1_556 ?
Mg3 P2 O13 Mg1 -21.5(2) . . . 4 ?
Mg3 P2 O13 Mg3 -153.57(18) . . . 4_554 ?
Mg3 P2 O13 Na4 103.03(15) . . . . ?
Na2 P1 O4 Mg1 -90.4(3) . . . . ?
Na2 P1 O4 Na2 106.2(4) . . . 2_655 ?
Na2 P1 O4 Na1 175.9(2) . . . 1_556 ?
Na2 P1 O3 Mg2 -149.5(2) . . . . ?
Na2 P1 O3 Na3 71.0(4) . . . 2_664 ?
Na2 P1 O3 Na1 -32.9(5) . . . 1_556 ?
Na2 P1 O1 P4 55.6(3) . . . . ?
Na2 P1 O1 Na3 -138.49(13) . . . 2_664 ?
Na2 P1 O1 Na3 140.92(12) . . . 1_554 ?
Na2 P1 O2 Mg3 111.9(2) . . . 1_554 ?
Na2 P1 O2 Na1 -68.0(3) . . . . ?
Na2 P4 O6 Mg2 120.4(2) 2_654 . . 2_664 ?
Na2 P4 O6 Mg3 -75.4(4) 2_654 . . 3_554 ?
Na2 P4 O6 Na4 24.1(2) 2_654 . . 2_663 ?
Na2 P4 O7 Mg1 112.5(4) 2_654 . . 2_654 ?
Na2 P4 O7 Na2 -133.2(4) 2_654 . . . ?
Na2 P4 O1 P1 -26.4(4) 2_654 . . . ?
Na2 P4 O1 Na3 -115.86(13) 2_654 . . 1_554 ?
Na2 P4 O1 Na3 173.55(17) 2_654 . . 2_664 ?
Na2 P4 O5 Na3 -84.2(3) 2_654 . . 2_663 ?
Na2 P4 O5 Na3 155.34(17) 2_654 . . 1_554 ?
Na2 P4 O5 Na1 50.92(18) 2_654 . . . ?
Na2 P3 O11 Mg2 -147.22(11) 1_556 . . 4_545 ?
Na2 P3 O11 Mg3 -23.3(4) 1_556 . . . ?
Na2 P3 O11 Na4 124.0(2) 1_556 . . 4_544 ?
Na2 P3 O10 Mg1 131.9(5) 1_556 . . 1_556 ?
Na2 P3 O10 Na4 -134.6(3) 1_556 . . 1_545 ?
Na2 P3 O8 Mg1 158.7(3) 1_556 . . . ?
Na2 P3 O8 Na2 2.4(3) 1_556 . . 2_655 ?
Na2 P3 O8 Na1 -86.90(14) 1_556 . . 1_556 ?
Na2 P3 O9 Mg2 145.30(12) 1_556 . . 4_545 ?
Na2 P3 O9 Mg3 -90.2(4) 1_556 . . 4_544 ?
Na2 P3 O9 Na4 31.8(2) 1_556 . . 1_545 ?
Na4 P2 O14 Mg2 97.5(4) . . . 1_556 ?
Na4 P2 O14 Na3 -113.7(2) . . . . ?
Na4 P2 O12 Mg1 56.4(2) . . . 4 ?
Na4 P2 O12 Mg3 -85.9(3) . . . . ?
Na4 P2 O12 Na4 152.21(13) . . . 4_544 ?
Na4 P2 O15 Mg2 -90.7(3) . . . . ?
Na4 P2 O15 Na3 52.55(19) . . . . ?
Na4 P2 O15 Na1 137.00(14) . . . 1_556 ?
Na4 P2 O13 Mg1 -124.5(2) . . . 4 ?
Na4 P2 O13 Mg3 103.4(3) . . . 4_554 ?
Na4 P4 O6 Mg2 96.2(3) 2_663 . . 2_664 ?
Na4 P4 O6 Mg3 -99.6(4) 2_663 . . 3_554 ?
Na4 P4 O7 Mg1 37.7(2) 2_663 . . 2_654 ?
Na4 P4 O7 Na2 152.1(2) 2_663 . . . ?
Na4 P4 O7 Na2 -74.8(2) 2_663 . . 2_654 ?
Na4 P4 O1 P1 -164.01(16) 2_663 . . . ?
Na4 P4 O1 Na3 106.5(3) 2_663 . . 1_554 ?
Na4 P4 O1 Na3 35.9(5) 2_663 . . 2_664 ?
Na4 P4 O5 Na3 -7.2(3) 2_663 . . 2_663 ?
Na4 P4 O5 Na3 -127.66(15) 2_663 . . 1_554 ?
Na4 P4 O5 Na1 127.92(17) 2_663 . . . ?
Na4 P3 O11 Mg2 -46.6(2) 1_545 . . 4_545 ?
Na4 P3 O11 Mg3 77.3(3) 1_545 . . . ?
Na4 P3 O11 Na4 -135.43(18) 1_545 . . 4_544 ?
Na4 P3 O10 Mg1 -93.5(4) 1_545 . . 1_556 ?
Na4 P3 O10 Na2 134.6(3) 1_545 . . 1_556 ?
Na4 P3 O8 Mg1 90.4(3) 1_545 . . . ?
Na4 P3 O8 Na2 -65.8(4) 1_545 . . 2_655 ?
Na4 P3 O8 Na1 -155.15(11) 1_545 . . 1_556 ?
Na4 P3 O9 Mg2 113.5(2) 1_545 . . 4_545 ?
Na4 P3 O9 Mg3 -122.0(4) 1_545 . . 4_544 ?
Na3 P1 O4 Mg1 153.5(2) 2_664 . . . ?
Na3 P1 O4 Na2 -116.03(14) 2_664 . . . ?
Na3 P1 O4 Na2 -9.8(4) 2_664 . . 2_655 ?
Na3 P1 O4 Na1 59.84(12) 2_664 . . 1_556 ?
Na3 P1 O3 Mg2 139.5(4) 2_664 . . . ?
Na3 P1 O3 Na1 -103.9(2) 2_664 . . 1_556 ?
Na3 P1 O1 P4 -166.0(4) 2_664 . . . ?
Na3 P1 O1 Na3 -80.59(11) 2_664 . . 1_554 ?
Na3 P1 O2 Mg3 -109.2(2) 2_664 . . 1_554 ?
Na3 P1 O2 Na1 70.8(4) 2_664 . . . ?
Na3 P2 O14 Mg2 -148.7(4) . . . 1_556 ?
Na3 P2 O14 Na4 113.7(2) . . . . ?
Na3 P2 O12 Mg1 167.69(13) . . . 4 ?
Na3 P2 O12 Mg3 25.4(4) . . . . ?
Na3 P2 O12 Na4 -96.5(2) . . . 4_544 ?
Na3 P2 O15 Mg2 -143.3(3) . . . . ?
Na3 P2 O15 Na1 84.45(19) . . . 1_556 ?
Na3 P2 O13 Mg1 -168.99(11) . . . 4 ?
Na3 P2 O13 Mg3 59.0(3) . . . 4_554 ?
Na3 P2 O13 Na4 -44.4(2) . . . . ?
Na3 P4 O6 Mg2 -22.0(3) 1_554 . . 2_664 ?
Na3 P4 O6 Mg3 142.2(4) 1_554 . . 3_554 ?
Na3 P4 O6 Na4 -118.23(14) 1_554 . . 2_663 ?
Na3 P4 O7 Mg1 174.43(14) 1_554 . . 2_654 ?
Na3 P4 O7 Na2 -71.2(4) 1_554 . . . ?
Na3 P4 O7 Na2 61.9(4) 1_554 . . 2_654 ?
Na3 P4 O1 P1 89.5(3) 1_554 . . . ?
Na3 P4 O1 Na3 -70.6(2) 1_554 . . 2_664 ?
Na3 P4 O5 Na3 120.5(4) 1_554 . . 2_663 ?
Na3 P4 O5 Na1 -104.4(3) 1_554 . . . ?
Na1 P1 O4 Mg1 93.7(3) 1_556 . . . ?
Na1 P1 O4 Na2 -69.6(4) 1_556 . . 2_655 ?
Na1 P1 O4 Na2 -175.9(2) 1_556 . . . ?
Na1 P1 O3 Mg2 -116.6(3) 1_556 . . . ?
Na1 P1 O3 Na3 103.9(2) 1_556 . . 2_664 ?
Na1 P1 O1 P4 161.9(2) 1_556 . . . ?
Na1 P1 O1 Na3 -112.71(13) 1_556 . . 1_554 ?
Na1 P1 O1 Na3 -32.12(19) 1_556 . . 2_664 ?
Na1 P1 O2 Mg3 -1.6(3) 1_556 . . 1_554 ?
Na1 P1 O2 Na1 178.48(19) 1_556 . . . ?
Na1 P2 O14 Mg2 -101.4(3) 1_556 . . 1_556 ?
Na1 P2 O14 Na4 161.07(12) 1_556 . . . ?
Na1 P2 O14 Na3 47.33(16) 1_556 . . . ?
Na1 P2 O12 Mg1 -151.13(16) 1_556 . . 4 ?
Na1 P2 O12 Mg3 66.6(2) 1_556 . . . ?
Na1 P2 O12 Na4 -55.28(17) 1_556 . . 4_544 ?
Na1 P2 O15 Mg2 132.3(4) 1_556 . . . ?
Na1 P2 O15 Na3 -84.45(19) 1_556 . . . ?
Na1 P2 O13 Mg1 87.7(3) 1_556 . . 4 ?
Na1 P2 O13 Mg3 -44.3(4) 1_556 . . 4_554 ?
Na1 P2 O13 Na4 -147.7(2) 1_556 . . . ?
Na1 P4 O6 Mg2 39.5(6) . . . 2_664 ?
Na1 P4 O6 Mg3 -156.3(2) . . . 3_554 ?
Na1 P4 O6 Na4 -56.7(4) . . . 2_663 ?
Na1 P4 O7 Mg1 157.4(3) . . . 2_654 ?
Na1 P4 O7 Na2 -88.3(2) . . . . ?
Na1 P4 O7 Na2 44.9(2) . . . 2_654 ?
Na1 P4 O1 P1 26.2(3) . . . . ?
Na1 P4 O1 Na3 -63.31(8) . . . 1_554 ?
Na1 P4 O1 Na3 -133.9(3) . . . 2_664 ?
Na1 P4 O5 Na3 -135.1(4) . . . 2_663 ?
Na1 P4 O5 Na3 104.4(3) . . . 1_554 ?
Na1 P3 O11 Mg2 154.1(2) 1_556 . . 4_545 ?
Na1 P3 O11 Mg3 -82.0(3) 1_556 . . . ?
Na1 P3 O11 Na4 65.2(2) 1_556 . . 4_544 ?
Na1 P3 O10 Mg1 87.1(4) 1_556 . . 1_556 ?
Na1 P3 O10 Na2 -44.7(2) 1_556 . . 1_556 ?
Na1 P3 O10 Na4 -179.34(9) 1_556 . . 1_545 ?
Na1 P3 O8 Mg1 -114.4(3) 1_556 . . . ?
Na1 P3 O8 Na2 89.3(3) 1_556 . . 2_655 ?
Na1 P3 O9 Mg2 -68.3(3) 1_556 . . 4_545 ?
Na1 P3 O9 Mg3 56.2(5) 1_556 . . 4_544 ?
Na1 P3 O9 Na4 178.22(18) 1_556 . . 1_545 ?
O14 P2 O12 Mg1 115.0(2) . . . 4 ?
O14 P2 O12 Mg3 -27.3(3) . . . . ?
O14 P2 O12 Na4 -149.1(2) . . . 4_544 ?
O14 P2 O15 Mg2 -147.1(3) . . . . ?
O14 P2 O15 Na3 -3.8(2) . . . . ?
O14 P2 O15 Na1 80.7(3) . . . 1_556 ?
O14 P2 O13 Mg1 -119.2(2) . . . 4 ?
O14 P2 O13 Mg3 108.7(3) . . . 4_554 ?
O14 P2 O13 Na4 5.3(2) . . . . ?
O12 P2 O14 Mg2 -21.7(4) . . . 1_556 ?
O12 P2 O14 Na4 -119.28(19) . . . . ?
O12 P2 O14 Na3 126.97(19) . . . . ?
O12 P2 O15 Mg2 87.3(3) . . . . ?
O12 P2 O15 Na3 -129.37(16) . . . . ?
O12 P2 O15 Na1 -44.9(3) . . . 1_556 ?
O12 P2 O13 Mg1 1.7(2) . . . 4 ?
O12 P2 O13 Mg3 -130.3(3) . . . 4_554 ?
O12 P2 O13 Na4 126.27(17) . . . . ?
O11 P3 O10 Mg1 18.0(4) . . . 1_556 ?
O11 P3 O10 Na2 -113.9(2) . . . 1_556 ?
O11 P3 O10 Na4 111.51(18) . . . 1_545 ?
O11 P3 O8 Mg1 -81.4(3) . . . . ?
O11 P3 O8 Na2 122.4(3) . . . 2_655 ?
O11 P3 O8 Na1 33.0(2) . . . 1_556 ?
O11 P3 O9 Mg2 -4.8(2) . . . 4_545 ?
O11 P3 O9 Mg3 119.7(3) . . . 4_544 ?
O11 P3 O9 Na4 -118.34(19) . . . 1_545 ?
O15 P2 O14 Mg2 -144.1(3) . . . 1_556 ?
O15 P2 O14 Na4 118.4(2) . . . . ?
O15 P2 O14 Na3 4.6(3) . . . . ?
O15 P2 O12 Mg1 -121.6(2) . . . 4 ?
O15 P2 O12 Mg3 96.1(3) . . . . ?
O15 P2 O12 Na4 -25.8(3) . . . 4_544 ?
O15 P2 O13 Mg1 118.4(2) . . . 4 ?
O15 P2 O13 Mg3 -13.7(3) . . . 4_554 ?
O15 P2 O13 Na4 -117.1(2) . . . . ?
O10 P3 O11 Mg2 -109.9(2) . . . 4_545 ?
O10 P3 O11 Mg3 14.0(4) . . . . ?
O10 P3 O11 Na4 161.3(2) . . . 4_544 ?
O10 P3 O8 Mg1 153.6(3) . . . . ?
O10 P3 O8 Na2 -2.6(4) . . . 2_655 ?
O10 P3 O8 Na1 -91.9(2) . . . 1_556 ?
O10 P3 O9 Mg2 114.34(19) . . . 4_545 ?
O10 P3 O9 Mg3 -121.2(3) . . . 4_544 ?
O10 P3 O9 Na4 0.8(2) . . . 1_545 ?
O4 P1 O3 Mg2 -126.5(3) . . . . ?
O4 P1 O3 Na3 94.0(2) . . . 2_664 ?
O4 P1 O3 Na1 -9.9(2) . . . 1_556 ?
O4 P1 O1 P4 94.1(3) . . . . ?
O4 P1 O1 Na3 179.46(17) . . . 1_554 ?
O4 P1 O1 Na3 -99.95(19) . . . 2_664 ?
O4 P1 O2 Mg3 70.9(3) . . . 1_554 ?
O4 P1 O2 Na1 -109.0(3) . . . . ?
O3 P1 O4 Mg1 102.1(3) . . . . ?
O3 P1 O4 Na2 -167.47(17) . . . . ?
O3 P1 O4 Na2 -61.2(4) . . . 2_655 ?
O3 P1 O4 Na1 8.4(2) . . . 1_556 ?
O3 P1 O1 P4 -148.8(3) . . . . ?
O3 P1 O1 Na3 17.1(2) . . . 2_664 ?
O3 P1 O1 Na3 -63.48(19) . . . 1_554 ?
O3 P1 O2 Mg3 -57.1(3) . . . 1_554 ?
O3 P1 O2 Na1 123.0(3) . . . . ?
O6 P4 O7 Mg1 0.5(4) . . . 2_654 ?
O6 P4 O7 Na2 -112.0(3) . . . 2_654 ?
O6 P4 O7 Na2 114.8(3) . . . . ?
O6 P4 O1 P1 -173.0(3) . . . . ?
O6 P4 O1 Na3 26.9(3) . . . 2_664 ?
O6 P4 O1 Na3 97.49(17) . . . 1_554 ?
O6 P4 O5 Na3 -85.1(2) . . . 1_554 ?
O6 P4 O5 Na3 35.4(4) . . . 2_663 ?
O6 P4 O5 Na1 170.5(2) . . . . ?
O7 P4 O6 Mg2 154.5(3) . . . 2_664 ?
O7 P4 O6 Mg3 -41.3(5) . . . 3_554 ?
O7 P4 O6 Na4 58.3(3) . . . 2_663 ?
O7 P4 O1 P1 -54.6(4) . . . . ?
O7 P4 O1 Na3 145.3(3) . . . 2_664 ?
O7 P4 O1 Na3 -144.13(17) . . . 1_554 ?
O7 P4 O5 Na3 146.1(2) . . . 1_554 ?
O7 P4 O5 Na3 -93.4(3) . . . 2_663 ?
O7 P4 O5 Na1 41.7(3) . . . . ?
O1 P1 O4 Mg1 -147.3(3) . . . . ?
O1 P1 O4 Na2 49.4(4) . . . 2_655 ?
O1 P1 O4 Na2 -56.9(2) . . . . ?
O1 P1 O4 Na1 119.02(17) . . . 1_556 ?
O1 P1 O3 Mg2 120.4(3) . . . . ?
O1 P1 O3 Na3 -19.1(2) . . . 2_664 ?
O1 P1 O3 Na1 -123.01(19) . . . 1_556 ?
O1 P1 O2 Mg3 -170.5(2) . . . 1_554 ?
O1 P1 O2 Na1 9.6(3) . . . . ?
O1 P4 O6 Mg2 -90.1(3) . . . 2_664 ?
O1 P4 O6 Mg3 74.1(4) . . . 3_554 ?
O1 P4 O6 Na4 173.62(19) . . . 2_663 ?
O1 P4 O7 Mg1 -113.8(3) . . . 2_654 ?
O1 P4 O7 Na2 133.7(2) . . . 2_654 ?
O1 P4 O7 Na2 0.5(3) . . . . ?
O1 P4 O5 Na3 29.1(2) . . . 1_554 ?
O1 P4 O5 Na3 149.6(3) . . . 2_663 ?
O1 P4 O5 Na1 -75.3(3) . . . . ?
O8 P3 O11 Mg2 126.2(2) . . . 4_545 ?
O8 P3 O11 Mg3 -109.8(3) . . . . ?
O8 P3 O11 Na4 37.4(3) . . . 4_544 ?
O8 P3 O10 Mg1 140.6(3) . . . 1_556 ?
O8 P3 O10 Na2 8.7(3) . . . 1_556 ?
O8 P3 O10 Na4 -125.88(18) . . . 1_545 ?
O8 P3 O9 Mg2 -122.3(2) . . . 4_545 ?
O8 P3 O9 Mg3 2.2(4) . . . 4_544 ?
O8 P3 O9 Na4 124.2(2) . . . 1_545 ?
O2 P1 O4 Mg1 -26.6(4) . . . . ?
O2 P1 O4 Na2 63.9(2) . . . . ?
O2 P1 O4 Na2 170.1(4) . . . 2_655 ?
O2 P1 O4 Na1 -120.26(19) . . . 1_556 ?
O2 P1 O3 Mg2 2.3(4) . . . . ?
O2 P1 O3 Na3 -137.1(2) . . . 2_664 ?
O2 P1 O3 Na1 119.0(2) . . . 1_556 ?
O2 P1 O1 P4 -28.7(4) . . . . ?
O2 P1 O1 Na3 137.23(17) . . . 2_664 ?
O2 P1 O1 Na3 56.6(2) . . . 1_554 ?
O13 P2 O14 Mg2 91.8(4) . . . 1_556 ?
O13 P2 O14 Na4 -5.7(2) . . . . ?
O13 P2 O14 Na3 -119.49(19) . . . . ?
O13 P2 O12 Mg1 -1.8(2) . . . 4 ?
O13 P2 O12 Mg3 -144.1(2) . . . . ?
O13 P2 O12 Na4 94.1(2) . . . 4_544 ?
O13 P2 O15 Mg2 -25.8(4) . . . . ?
O13 P2 O15 Na3 117.49(18) . . . . ?
O13 P2 O15 Na1 -158.05(19) . . . 1_556 ?
O9 P3 O11 Mg2 5.2(3) . . . 4_545 ?
O9 P3 O11 Mg3 129.1(3) . . . . ?
O9 P3 O11 Na4 -83.6(3) . . . 4_544 ?
O9 P3 O10 Mg1 -94.3(4) . . . 1_556 ?
O9 P3 O10 Na2 133.8(2) . . . 1_556 ?
O9 P3 O10 Na4 -0.8(2) . . . 1_545 ?
O9 P3 O8 Mg1 32.4(4) . . . . ?
O9 P3 O8 Na2 -123.8(3) . . . 2_655 ?
O9 P3 O8 Na1 146.87(18) . . . 1_556 ?
O5 P4 O6 Mg2 24.2(4) . . . 2_664 ?
O5 P4 O6 Mg3 -171.6(4) . . . 3_554 ?
O5 P4 O6 Na4 -72.0(2) . . . 2_663 ?
O5 P4 O7 Mg1 130.1(3) . . . 2_654 ?
O5 P4 O7 Na2 17.6(3) . . . 2_654 ?
O5 P4 O7 Na2 -115.6(3) . . . . ?
O5 P4 O1 P1 67.4(4) . . . . ?
O5 P4 O1 Na3 -22.11(19) . . . 1_554 ?
O5 P4 O1 Na3 -92.7(3) . . . 2_664 ?

_olex2_submission_special_instructions 'No special instructions were received'
