# Supplementary Information (SI) for Journal of Materials Chemistry C.
# This journal is © The Royal Society of Chemistry 2026

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_211227yhb_0m
_database_code_depnum_ccdc_archive 'CCDC 2168854'
loop_
_audit_author_name
_audit_author_address
'Haibo Yao'
;Guangxi minzu university
China
;
_audit_update_record             
;
2022-04-26 deposited with the CCDC.	2026-02-11 downloaded from the CCDC.
;
_audit_creation_date             2021-12-27
_audit_creation_method           
;
Olex2 1.5
(compiled 2021.12.09 svn.r5202d8cf for OlexSys, GUI svn.r6439)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C45 H88 B22 N6 Pt, 3(C3 H6 O)'
_chemical_formula_sum            'C54 H106 B22 N6 O3 Pt'
_chemical_formula_weight         1320.35
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0137 0.0067 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0070 0.0029 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0241 0.0134 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0389 0.0241 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -5.3886 5.5592 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   12.0464(5)
_cell_length_b                   18.6936(8)
_cell_length_c                   31.5101(13)
_cell_angle_alpha                90
_cell_angle_beta                 96.965(3)
_cell_angle_gamma                90
_cell_volume                     7043.4(5)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9690
_cell_measurement_temperature    213.00
_cell_measurement_theta_max      54.884
_cell_measurement_theta_min      3.207
_shelx_estimated_absorpt_T_max   0.874
_shelx_estimated_absorpt_T_min   0.830
_exptl_absorpt_coefficient_mu    2.764
_exptl_absorpt_correction_T_max  0.7508
_exptl_absorpt_correction_T_min  0.5429
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1918 before and 0.0682 after correction.
The Ratio of minimum to maximum transmission is 0.7231.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.245
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             2736
_exptl_crystal_size_max          0.07
_exptl_crystal_size_mid          0.07
_exptl_crystal_size_min          0.05
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0632
_diffrn_reflns_av_unetI/netI     0.0510
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.995
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       38
_diffrn_reflns_limit_l_min       -38
_diffrn_reflns_number            70386
_diffrn_reflns_point_group_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.995
_diffrn_reflns_theta_full        53.594
_diffrn_reflns_theta_max         55.078
_diffrn_reflns_theta_min         3.205
_diffrn_ambient_temperature      213.00
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'Bruker D8 Venture'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           GaK\a
_diffrn_radiation_wavelength     1.34139
_diffrn_source                   ?
_diffrn_source_current           2.86
_diffrn_source_power             0.1995708
_diffrn_source_voltage           69.78
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                10331
_reflns_number_total             13411
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v8.37A (Bruker, 2015)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT v8.37A (Bruker, 2015)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         1.664
_refine_diff_density_min         -1.509
_refine_diff_density_rms         0.106
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.023
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     783
_refine_ls_number_reflns         13411
_refine_ls_number_restraints     78
_refine_ls_R_factor_all          0.0720
_refine_ls_R_factor_gt           0.0495
_refine_ls_restrained_S_all      1.057
_refine_ls_shift/su_max          0.005
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0517P)²+23.5063P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1144
_refine_ls_wR_factor_ref         0.1260
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Restrained distances
 C33-C32
 1.53 with sigma of 0.01
 C30-C31 = C29-C30 = C29-C28 = C28-C27 = C27-C26 = C25-C26 = C25-C24 = C23-C24
 = C23-C22
 1.53 with sigma of 0.01
 C32-C31
 1.53 with sigma of 0.01
 C30-C32
 2.44 with sigma of 0.01
3. Uiso/Uaniso restraints and constraints
C22 \\sim C23 \\sim C24 \\sim C25 \\sim C26 \\sim C27 \\sim C28 \\sim C29 \\sim
C30 \\sim C31 \\sim C32 \\sim C33: within 2A with sigma of 0.01 and sigma for
terminal atoms of 0.02 within 2A
C22 \\sim C23 \\sim C24 \\sim C25 \\sim C26 \\sim C27 \\sim C28 \\sim C29 \\sim
C30 \\sim C31 \\sim C32 \\sim C33: within 2A with sigma of 0.005 and sigma for
terminal atoms of 0.01 within 2A
4.a Secondary CH2 refined with riding coordinates:
 C5(H5A,H5B), C6(H6A,H6B), C7(H7A,H7B), C10(H10A,H10B), C11(H11A,H11B),
 C12(H12A,H12B), C13(H13A,H13B), C14(H14A,H14B), C15(H15A,H15B), C16(H16A,H16B),
  C17(H17A,H17B), C18(H18A,H18B), C19(H19A,H19B), C20(H20A,H20B), C22(H22A,
 H22B), C23(H23A,H23B), C24(H24A,H24B), C25(H25A,H25B), C26(H26A,H26B),
 C27(H27A,H27B), C28(H28A,H28B), C29(H29A,H29B), C30(H30A,H30B), C31(H31A,H31B),
  C32(H32A,H32B)
4.b Aromatic/amide H refined with riding coordinates:
 C3(H3), C4(H4), C8(H8), C9(H9), C34(H34), C35(H35), C37(H37), C40(H40),
 C42(H42), C43(H43)
4.c Idealised Me refined as rotating group:
 C21(H21A,H21B,H21C), C33(H33A,H33B,H33C), C46(H46A,H46B,H46C), C48(H48A,H48B,
 H48C), C49(H49A,H49B,H49C), C51(H51A,H51B,H51C), C52(H52A,H52B,H52C), C54(H54A,
 H54B,H54C)
4.d Boron cage BH refined with riding coordinates:
 B1(H1), B2(H2), B3(H3A), B4(H4A), B5(H5), B6(H6), B7(H7), B8(H8A), B9(H9A),
 B10(H10), B11(H11), B12(H12), B13(H13), B14(H14), B15(H15), B16(H16), B17(H17),
  B18(H18), B19(H19), B20(H20), B21(H21), B22(H22)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.80385(2) 0.46009(2) 0.65927(2) 0.02906(8) Uani 1 1 d . . . . .
O1 O 0.8973(5) 0.7103(3) 0.73528(19) 0.0957(18) Uani 1 1 d . . . . .
N1 N 0.6892(3) 0.5417(2) 0.66247(11) 0.0289(8) Uani 1 1 d . . . . .
N2 N 0.6740(3) 0.4248(2) 0.61516(12) 0.0295(9) Uani 1 1 d . . . . .
N3 N 0.9491(3) 0.4946(2) 0.74269(12) 0.0359(10) Uani 1 1 d . . . . .
N4 N 1.0106(3) 0.5413(2) 0.68763(13) 0.0355(9) Uani 1 1 d . . . . .
N5 N 0.9308(4) 0.3198(2) 0.67266(14) 0.0398(10) Uani 1 1 d . . . . .
N6 N 0.9974(3) 0.3889(2) 0.62764(13) 0.0363(10) Uani 1 1 d . . . . .
C1 C 0.9262(4) 0.5021(3) 0.69981(15) 0.0324(11) Uani 1 1 d . . . . .
C2 C 0.9132(4) 0.3828(3) 0.65247(15) 0.0344(11) Uani 1 1 d . . . . .
C3 C 1.0471(5) 0.5300(3) 0.75684(17) 0.0452(14) Uani 1 1 d . . . . .
H3 H 1.081080 0.532903 0.785266 0.054 Uiso 1 1 calc R U . . .
C4 C 1.0845(5) 0.5592(3) 0.72297(18) 0.0460(14) Uani 1 1 d . . . . .
H4 H 1.149559 0.587050 0.723009 0.055 Uiso 1 1 calc R U . . .
C5 C 1.0206(5) 0.5637(3) 0.64386(16) 0.0405(13) Uani 1 1 d . . . . .
H5A H 1.060173 0.609566 0.644806 0.049 Uiso 1 1 calc R U . . .
H5B H 0.945333 0.571600 0.628982 0.049 Uiso 1 1 calc R U . . .
C6 C 1.0820(5) 0.5106(3) 0.61761(18) 0.0451(14) Uani 1 1 d . . . . .
H6A H 1.110894 0.536827 0.594366 0.054 Uiso 1 1 calc R U . . .
H6B H 1.146301 0.491225 0.636054 0.054 Uiso 1 1 calc R U . . .
C7 C 1.0110(5) 0.4480(3) 0.59827(16) 0.0400(13) Uani 1 1 d . . . . .
H7A H 0.936733 0.466179 0.587311 0.048 Uiso 1 1 calc R U . . .
H7B H 1.045272 0.429304 0.573872 0.048 Uiso 1 1 calc R U . . .
C8 C 1.0665(5) 0.3303(3) 0.63293(18) 0.0458(14) Uani 1 1 d . . . . .
H8 H 1.130480 0.322060 0.619299 0.055 Uiso 1 1 calc R U . . .
C9 C 1.0255(5) 0.2873(3) 0.66110(19) 0.0505(15) Uani 1 1 d . . . . .
H9 H 1.055529 0.243166 0.671161 0.061 Uiso 1 1 calc R U . . .
C10 C 0.8804(5) 0.4559(3) 0.77058(17) 0.0431(13) Uani 1 1 d . . . . .
H10A H 0.926647 0.444271 0.797443 0.052 Uiso 1 1 calc R U . . .
H10B H 0.855306 0.410807 0.756769 0.052 Uiso 1 1 calc R U . . .
C11 C 0.7794(7) 0.4975(4) 0.7806(3) 0.078(2) Uani 1 1 d . . . . .
H11A H 0.727333 0.500152 0.754172 0.094 Uiso 1 1 calc R U . . .
H11B H 0.742667 0.469218 0.801006 0.094 Uiso 1 1 calc R U . . .
C12 C 0.7933(6) 0.5702(4) 0.7977(2) 0.0676(19) Uani 1 1 d . . . . .
H12A H 0.826293 0.599989 0.776903 0.081 Uiso 1 1 calc R U . . .
H12B H 0.846324 0.568766 0.823835 0.081 Uiso 1 1 calc R U . . .
C13 C 0.6875(8) 0.6053(4) 0.8078(3) 0.095(3) Uani 1 1 d . . . . .
H13A H 0.630751 0.598532 0.783078 0.113 Uiso 1 1 calc R U . . .
H13B H 0.661708 0.579266 0.831771 0.113 Uiso 1 1 calc R U . . .
C14 C 0.6899(7) 0.6814(4) 0.8186(3) 0.079(2) Uani 1 1 d . . . . .
H14A H 0.714241 0.707673 0.794467 0.094 Uiso 1 1 calc R U . . .
H14B H 0.747096 0.688437 0.843114 0.094 Uiso 1 1 calc R U . . .
C15 C 0.5832(9) 0.7149(5) 0.8292(3) 0.107(3) Uani 1 1 d . . . . .
H15A H 0.524652 0.703204 0.805829 0.129 Uiso 1 1 calc R U . . .
H15B H 0.563019 0.690987 0.854848 0.129 Uiso 1 1 calc R U . . .
C16 C 0.5775(9) 0.7935(6) 0.8367(3) 0.106(3) Uani 1 1 d . . . . .
H16A H 0.500070 0.805147 0.840590 0.127 Uiso 1 1 calc R U . . .
H16B H 0.623392 0.803799 0.863902 0.127 Uiso 1 1 calc R U . . .
C17 C 0.6113(8) 0.8415(5) 0.8055(3) 0.099(3) Uani 1 1 d . . . . .
H17A H 0.575609 0.825807 0.777447 0.118 Uiso 1 1 calc R U . . .
H17B H 0.692182 0.836014 0.805399 0.118 Uiso 1 1 calc R U . . .
C18 C 0.5882(12) 0.9178(6) 0.8095(4) 0.141(5) Uani 1 1 d . . . . .
H18A H 0.615708 0.932169 0.838802 0.170 Uiso 1 1 calc R U . . .
H18B H 0.506782 0.923894 0.806013 0.170 Uiso 1 1 calc R U . . .
C19 C 0.6350(12) 0.9690(7) 0.7798(4) 0.139(5) Uani 1 1 d . . . . .
H19A H 0.638123 1.016687 0.792788 0.166 Uiso 1 1 calc R U . . .
H19B H 0.711792 0.954596 0.776670 0.166 Uiso 1 1 calc R U . . .
C20 C 0.5750(13) 0.9730(8) 0.7400(5) 0.171(6) Uani 1 1 d . . . . .
H20A H 0.498387 0.986748 0.743824 0.206 Uiso 1 1 calc R U . . .
H20B H 0.571356 0.924662 0.727837 0.206 Uiso 1 1 calc R U . . .
C21 C 0.6121(11) 1.0205(7) 0.7082(4) 0.138(4) Uani 1 1 d . . . . .
H21A H 0.559196 1.018966 0.682423 0.207 Uiso 1 1 calc R U . . .
H21B H 0.685153 1.005448 0.701606 0.207 Uiso 1 1 calc R U . . .
H21C H 0.616832 1.068983 0.719274 0.207 Uiso 1 1 calc R U . . .
C22 C 0.8571(8) 0.2878(4) 0.7016(2) 0.088(2) Uani 1 1 d D U . . .
H22A H 0.792404 0.319294 0.702651 0.106 Uiso 1 1 calc R U . . .
H22B H 0.897752 0.285783 0.730447 0.106 Uiso 1 1 calc R U . . .
C23 C 0.8161(10) 0.2149(5) 0.6893(3) 0.125(2) Uani 1 1 d D U . . .
H23A H 0.877041 0.181386 0.698143 0.150 Uiso 1 1 calc R U . . .
H23B H 0.755388 0.203789 0.706310 0.150 Uiso 1 1 calc R U . . .
C24 C 0.7752(12) 0.1994(6) 0.6444(3) 0.152(3) Uani 1 1 d D U . . .
H24A H 0.724628 0.238670 0.634524 0.182 Uiso 1 1 calc R U . . .
H24B H 0.840051 0.203579 0.628534 0.182 Uiso 1 1 calc R U . . .
C25 C 0.7177(15) 0.1332(7) 0.6295(4) 0.194(3) Uani 1 1 d D U . . .
H25A H 0.652836 0.127400 0.645219 0.233 Uiso 1 1 calc R U . . .
H25B H 0.768411 0.093146 0.637531 0.233 Uiso 1 1 calc R U . . .
C26 C 0.6776(16) 0.1268(10) 0.5824(4) 0.224(3) Uani 1 1 d D U . . .
H26A H 0.734255 0.094062 0.573753 0.269 Uiso 1 1 calc R U . . .
H26B H 0.700116 0.173827 0.572575 0.269 Uiso 1 1 calc R U . . .
C27 C 0.5815(16) 0.1105(11) 0.5478(6) 0.253(4) Uani 1 1 d D U . . .
H27A H 0.543612 0.153784 0.536090 0.304 Uiso 1 1 calc R U . . .
H27B H 0.604831 0.081180 0.524690 0.304 Uiso 1 1 calc R U . . .
C28 C 0.5122(18) 0.0689(12) 0.5762(6) 0.274(4) Uani 1 1 d D U . . .
H28A H 0.498834 0.094693 0.602234 0.329 Uiso 1 1 calc R U . . .
H28B H 0.540510 0.020626 0.583085 0.329 Uiso 1 1 calc R U . . .
C29 C 0.412(2) 0.0709(13) 0.5406(7) 0.292(4) Uani 1 1 d D U . . .
H29A H 0.379938 0.119033 0.537199 0.351 Uiso 1 1 calc R U . . .
H29B H 0.433571 0.054687 0.513235 0.351 Uiso 1 1 calc R U . . .
C30 C 0.3307(18) 0.0191(12) 0.5575(8) 0.306(5) Uani 1 1 d D U . . .
H30A H 0.340637 0.025873 0.588561 0.367 Uiso 1 1 calc R U . . .
H30B H 0.360315 -0.028579 0.552510 0.367 Uiso 1 1 calc R U . . .
C31 C 0.204(2) 0.0131(12) 0.5451(8) 0.318(5) Uani 1 1 d D U . . .
H31A H 0.186678 0.006671 0.514102 0.382 Uiso 1 1 calc R U . . .
H31B H 0.174028 -0.027549 0.559577 0.382 Uiso 1 1 calc R U . . .
C32 C 0.1558(18) 0.0830(13) 0.5592(9) 0.326(6) Uani 1 1 d D U . . .
H32A H 0.152665 0.115931 0.534840 0.391 Uiso 1 1 calc R U . . .
H32B H 0.210401 0.102930 0.581681 0.391 Uiso 1 1 calc R U . . .
C33 C 0.042(2) 0.0863(15) 0.5756(8) 0.341(7) Uani 1 1 d D U . . .
H33A H -0.015676 0.094065 0.551861 0.511 Uiso 1 1 calc R U . . .
H33B H 0.041463 0.125320 0.595899 0.511 Uiso 1 1 calc R U . . .
H33C H 0.028156 0.041547 0.589665 0.511 Uiso 1 1 calc R U . . .
C34 C 0.6747(4) 0.3678(3) 0.59011(15) 0.0344(11) Uani 1 1 d . . . . .
H34 H 0.738618 0.338573 0.592776 0.041 Uiso 1 1 calc R U . . .
C35 C 0.5861(4) 0.3497(3) 0.56048(16) 0.0371(12) Uani 1 1 d . . . . .
H35 H 0.589933 0.308454 0.543627 0.045 Uiso 1 1 calc R U . . .
C36 C 0.4905(4) 0.3922(3) 0.55533(14) 0.0299(11) Uani 1 1 d . . . . .
C37 C 0.4925(4) 0.4527(3) 0.58097(14) 0.0297(10) Uani 1 1 d . . . . .
H37 H 0.430280 0.483463 0.578246 0.036 Uiso 1 1 calc R U . . .
C38 C 0.5821(4) 0.4685(3) 0.60989(14) 0.0286(10) Uani 1 1 d . . . . .
C39 C 0.5908(4) 0.5341(3) 0.63666(14) 0.0279(10) Uani 1 1 d . . . . .
C40 C 0.5090(4) 0.5852(3) 0.63523(14) 0.0302(11) Uani 1 1 d . . . . .
H40 H 0.441966 0.578682 0.617060 0.036 Uiso 1 1 calc R U . . .
C41 C 0.5233(4) 0.6461(3) 0.65992(14) 0.0310(11) Uani 1 1 d . . . . .
C42 C 0.6247(4) 0.6530(3) 0.68581(16) 0.0387(12) Uani 1 1 d . . . . .
H42 H 0.638411 0.693623 0.703285 0.046 Uiso 1 1 calc R U . . .
C43 C 0.7053(4) 0.6006(3) 0.68596(16) 0.0378(12) Uani 1 1 d . . . . .
H43 H 0.773821 0.606713 0.703276 0.045 Uiso 1 1 calc R U . . .
C44 C 0.4334(4) 0.7018(3) 0.65880(14) 0.0314(11) Uani 1 1 d . . . . .
C45 C 0.3900(4) 0.3749(3) 0.52406(14) 0.0304(10) Uani 1 1 d . . . . .
C46 C 0.8501(10) 0.8304(5) 0.7245(3) 0.114(3) Uani 1 1 d . . . . .
H46A H 0.772017 0.839197 0.714309 0.172 Uiso 1 1 calc R U . . .
H46B H 0.896064 0.866445 0.713001 0.172 Uiso 1 1 calc R U . . .
H46C H 0.860940 0.832587 0.755485 0.172 Uiso 1 1 calc R U . . .
C47 C 0.8825(6) 0.7584(4) 0.7103(2) 0.0648(18) Uani 1 1 d . . . . .
C48 C 0.8954(7) 0.7489(5) 0.6643(3) 0.088(2) Uani 1 1 d . . . . .
H48A H 0.925791 0.701822 0.659925 0.132 Uiso 1 1 calc R U . . .
H48B H 0.945742 0.785135 0.655672 0.132 Uiso 1 1 calc R U . . .
H48C H 0.822977 0.753609 0.647355 0.132 Uiso 1 1 calc R U . . .
B1 B 0.3673(5) 0.7134(4) 0.70381(19) 0.0420(15) Uani 1 1 d . . . . .
H1 H 0.388463 0.683215 0.734058 0.050 Uiso 1 1 calc R U . . .
B2 B 0.4585(5) 0.7801(3) 0.6871(2) 0.0410(15) Uani 1 1 d . . . . .
H2 H 0.538925 0.793728 0.706495 0.049 Uiso 1 1 calc R U . . .
B3 B 0.4459(6) 0.7793(3) 0.6304(2) 0.0426(15) Uani 1 1 d . . . . .
H3A H 0.517701 0.792138 0.612799 0.051 Uiso 1 1 calc R U . . .
B4 B 0.3463(5) 0.7132(3) 0.61189(18) 0.0364(14) Uani 1 1 d . . . . .
H4A H 0.353378 0.682804 0.582061 0.044 Uiso 1 1 calc R U . . .
B5 B 0.2980(5) 0.6723(3) 0.65727(18) 0.0354(13) Uani 1 1 d . . . . .
H5 H 0.273422 0.615044 0.657066 0.042 Uiso 1 1 calc R U . . .
B6 B 0.3269(6) 0.8042(4) 0.7033(2) 0.0464(16) Uani 1 1 d . . . . .
H6 H 0.320222 0.834258 0.733312 0.056 Uiso 1 1 calc R U . . .
B7 B 0.3761(6) 0.8454(4) 0.6580(2) 0.0488(17) Uani 1 1 d . . . . .
H7 H 0.401743 0.902473 0.658339 0.059 Uiso 1 1 calc R U . . .
B8 B 0.3060(6) 0.8039(4) 0.6113(2) 0.0446(16) Uani 1 1 d . . . . .
H8A H 0.285625 0.833941 0.580992 0.054 Uiso 1 1 calc R U . . .
B9 B 0.2150(6) 0.7378(3) 0.6276(2) 0.0421(15) Uani 1 1 d . . . . .
H9A H 0.135111 0.724201 0.607877 0.051 Uiso 1 1 calc R U . . .
B10 B 0.2287(6) 0.7373(4) 0.6846(2) 0.0442(15) Uani 1 1 d . . . . .
H10 H 0.157669 0.723208 0.702361 0.053 Uiso 1 1 calc R U . . .
B11 B 0.2332(6) 0.8188(4) 0.6563(2) 0.0479(17) Uani 1 1 d . . . . .
H11 H 0.164711 0.858663 0.655560 0.058 Uiso 1 1 calc R U . . .
B12 B 0.3120(5) 0.4447(3) 0.50156(19) 0.0383(14) Uani 1 1 d . . . . .
H12 H 0.332671 0.501973 0.507549 0.046 Uiso 1 1 calc R U . . .
B13 B 0.3927(5) 0.3904(4) 0.47095(17) 0.0393(14) Uani 1 1 d . . . . .
H13 H 0.466102 0.412037 0.457036 0.047 Uiso 1 1 calc R U . . .
B14 B 0.3916(5) 0.3018(4) 0.49079(19) 0.0421(15) Uani 1 1 d . . . . .
H14 H 0.464157 0.265574 0.489632 0.051 Uiso 1 1 calc R U . . .
B15 B 0.3119(6) 0.3015(4) 0.53481(19) 0.0432(15) Uani 1 1 d . . . . .
H15 H 0.332767 0.265210 0.562512 0.052 Uiso 1 1 calc R U . . .
B16 B 0.2625(5) 0.3901(4) 0.54092(18) 0.0397(15) Uani 1 1 d . . . . .
H16 H 0.250567 0.411826 0.572849 0.048 Uiso 1 1 calc R U . . .
B17 B 0.2528(5) 0.4135(4) 0.45109(19) 0.0424(15) Uani 1 1 d . . . . .
H17 H 0.233583 0.450138 0.423463 0.051 Uiso 1 1 calc R U . . .
B18 B 0.3019(6) 0.3249(4) 0.44446(19) 0.0464(17) Uani 1 1 d . . . . .
H18 H 0.314870 0.303500 0.412565 0.056 Uiso 1 1 calc R U . . .
B19 B 0.2514(6) 0.2698(4) 0.4841(2) 0.0486(17) Uani 1 1 d . . . . .
H19 H 0.231089 0.212448 0.478363 0.058 Uiso 1 1 calc R U . . .
B20 B 0.1728(6) 0.3245(4) 0.5155(2) 0.0475(17) Uani 1 1 d . . . . .
H20 H 0.101251 0.302714 0.530546 0.057 Uiso 1 1 calc R U . . .
B21 B 0.1718(5) 0.4139(4) 0.49463(19) 0.0425(15) Uani 1 1 d . . . . .
H21 H 0.099712 0.450560 0.495723 0.051 Uiso 1 1 calc R U . . .
B22 B 0.1651(6) 0.3391(4) 0.45924(19) 0.0465(16) Uani 1 1 d . . . . .
H22 H 0.088436 0.327041 0.437157 0.056 Uiso 1 1 calc R U . . .
O2 O 0.8865(7) 0.9521(4) 0.6458(2) 0.135(3) Uani 1 1 d . . . . .
C49 C 0.7304(10) 0.9062(7) 0.6013(4) 0.143(5) Uani 1 1 d . . . . .
H49A H 0.716613 0.855860 0.605957 0.214 Uiso 1 1 calc R U . . .
H49B H 0.708821 0.917863 0.571460 0.214 Uiso 1 1 calc R U . . .
H49C H 0.686982 0.934792 0.619002 0.214 Uiso 1 1 calc R U . . .
C50 C 0.8516(11) 0.9217(5) 0.6129(3) 0.110(4) Uani 1 1 d . . . . .
C51 C 0.9317(11) 0.8957(8) 0.5823(3) 0.156(5) Uani 1 1 d . . . . .
H51A H 0.914893 0.919729 0.554997 0.234 Uiso 1 1 calc R U . . .
H51B H 0.923159 0.844473 0.578270 0.234 Uiso 1 1 calc R U . . .
H51C H 1.007974 0.906348 0.594188 0.234 Uiso 1 1 calc R U . . .
O3 O 0.8688(5) 0.2856(4) 0.55582(18) 0.107(2) Uani 1 1 d . . . . .
C52 C 0.8503(7) 0.3532(5) 0.4923(3) 0.093(3) Uani 1 1 d . . . . .
H52A H 0.827163 0.390574 0.510701 0.139 Uiso 1 1 calc R U . . .
H52B H 0.792203 0.345555 0.468612 0.139 Uiso 1 1 calc R U . . .
H52C H 0.918866 0.367496 0.481358 0.139 Uiso 1 1 calc R U . . .
C53 C 0.8695(6) 0.2871(5) 0.5167(3) 0.076(2) Uani 1 1 d . . . . .
C54 C 0.8979(9) 0.2220(5) 0.4938(3) 0.110(3) Uani 1 1 d . . . . .
H54A H 0.930362 0.186756 0.514269 0.166 Uiso 1 1 calc R U . . .
H54B H 0.951248 0.233834 0.474199 0.166 Uiso 1 1 calc R U . . .
H54C H 0.830635 0.202492 0.477902 0.166 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 N1 2.068(4) . ?
Pt1 N2 2.070(4) . ?
Pt1 C1 1.991(5) . ?
Pt1 C2 1.985(5) . ?
O1 C47 1.195(8) . ?
N1 C39 1.361(6) . ?
N1 C43 1.328(6) . ?
N2 C34 1.326(6) . ?
N2 C38 1.369(6) . ?
N3 C1 1.353(6) . ?
N3 C3 1.380(7) . ?
N3 C10 1.469(7) . ?
N4 C1 1.346(6) . ?
N4 C4 1.380(6) . ?
N4 C5 1.460(6) . ?
N5 C2 1.343(7) . ?
N5 C9 1.380(7) . ?
N5 C22 1.474(8) . ?
N6 C2 1.358(6) . ?
N6 C7 1.464(7) . ?
N6 C8 1.373(7) . ?
C3 H3 0.9400 . ?
C3 C4 1.326(8) . ?
C4 H4 0.9400 . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C5 C6 1.537(8) . ?
C6 H6A 0.9800 . ?
C6 H6B 0.9800 . ?
C6 C7 1.531(8) . ?
C7 H7A 0.9800 . ?
C7 H7B 0.9800 . ?
C8 H8 0.9400 . ?
C8 C9 1.336(8) . ?
C9 H9 0.9400 . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 C11 1.508(9) . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 C12 1.464(10) . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 C13 1.501(10) . ?
C13 H13A 0.9800 . ?
C13 H13B 0.9800 . ?
C13 C14 1.461(11) . ?
C14 H14A 0.9800 . ?
C14 H14B 0.9800 . ?
C14 C15 1.504(11) . ?
C15 H15A 0.9800 . ?
C15 H15B 0.9800 . ?
C15 C16 1.491(12) . ?
C16 H16A 0.9800 . ?
C16 H16B 0.9800 . ?
C16 C17 1.427(12) . ?
C17 H17A 0.9800 . ?
C17 H17B 0.9800 . ?
C17 C18 1.461(13) . ?
C18 H18A 0.9800 . ?
C18 H18B 0.9800 . ?
C18 C19 1.495(15) . ?
C19 H19A 0.9800 . ?
C19 H19B 0.9800 . ?
C19 C20 1.373(16) . ?
C20 H20A 0.9800 . ?
C20 H20B 0.9800 . ?
C20 C21 1.449(16) . ?
C21 H21A 0.9700 . ?
C21 H21B 0.9700 . ?
C21 H21C 0.9700 . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 C23 1.485(8) . ?
C23 H23A 0.9800 . ?
C23 H23B 0.9800 . ?
C23 C24 1.470(8) . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 C25 1.466(9) . ?
C25 H25A 0.9800 . ?
C25 H25B 0.9800 . ?
C25 C26 1.511(9) . ?
C26 H26A 0.9800 . ?
C26 H26B 0.9800 . ?
C26 C27 1.520(9) . ?
C27 H27A 0.9800 . ?
C27 H27B 0.9800 . ?
C27 C28 1.510(10) . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 C29 1.547(10) . ?
C29 H29A 0.9800 . ?
C29 H29B 0.9800 . ?
C29 C30 1.516(10) . ?
C30 H30A 0.9800 . ?
C30 H30B 0.9800 . ?
C30 C31 1.530(10) . ?
C31 H31A 0.9800 . ?
C31 H31B 0.9800 . ?
C31 C32 1.520(10) . ?
C32 H32A 0.9800 . ?
C32 H32B 0.9800 . ?
C32 C33 1.524(10) . ?
C33 H33A 0.9700 . ?
C33 H33B 0.9700 . ?
C33 H33C 0.9700 . ?
C34 H34 0.9400 . ?
C34 C35 1.373(7) . ?
C35 H35 0.9400 . ?
C35 C36 1.392(7) . ?
C36 C37 1.389(6) . ?
C36 C45 1.501(6) . ?
C37 H37 0.9400 . ?
C37 C38 1.358(6) . ?
C38 C39 1.485(6) . ?
C39 C40 1.370(7) . ?
C40 H40 0.9400 . ?
C40 C41 1.378(7) . ?
C41 C42 1.390(7) . ?
C41 C44 1.499(7) . ?
C42 H42 0.9400 . ?
C42 C43 1.380(7) . ?
C43 H43 0.9400 . ?
C44 B1 1.722(8) . ?
C44 B2 1.723(7) . ?
C44 B3 1.719(8) . ?
C44 B4 1.719(7) . ?
C44 B5 1.717(8) . ?
C45 B12 1.711(8) . ?
C45 B13 1.703(7) . ?
C45 B14 1.723(8) . ?
C45 B15 1.720(8) . ?
C45 B16 1.709(8) . ?
C46 H46A 0.9700 . ?
C46 H46B 0.9700 . ?
C46 H46C 0.9700 . ?
C46 C47 1.486(11) . ?
C47 C48 1.485(10) . ?
C48 H48A 0.9700 . ?
C48 H48B 0.9700 . ?
C48 H48C 0.9700 . ?
B1 H1 1.1100 . ?
B1 B2 1.783(10) . ?
B1 B5 1.772(8) . ?
B1 B6 1.767(9) . ?
B1 B10 1.763(9) . ?
B2 H2 1.1100 . ?
B2 B3 1.775(9) . ?
B2 B6 1.781(9) . ?
B2 B7 1.759(9) . ?
B3 H3A 1.1100 . ?
B3 B4 1.772(9) . ?
B3 B7 1.779(9) . ?
B3 B8 1.779(9) . ?
B4 H4A 1.1100 . ?
B4 B5 1.780(8) . ?
B4 B8 1.764(9) . ?
B4 B9 1.774(9) . ?
B5 H5 1.1100 . ?
B5 B9 1.773(9) . ?
B5 B10 1.758(9) . ?
B6 H6 1.1100 . ?
B6 B7 1.785(10) . ?
B6 B10 1.773(10) . ?
B6 B11 1.771(9) . ?
B7 H7 1.1100 . ?
B7 B8 1.783(9) . ?
B7 B11 1.786(10) . ?
B8 H8A 1.1100 . ?
B8 B9 1.769(10) . ?
B8 B11 1.778(10) . ?
B9 H9A 1.1100 . ?
B9 B10 1.784(9) . ?
B9 B11 1.765(9) . ?
B10 H10 1.1100 . ?
B10 B11 1.768(10) . ?
B11 H11 1.1100 . ?
B12 H12 1.1100 . ?
B12 B13 1.770(9) . ?
B12 B16 1.765(9) . ?
B12 B17 1.762(8) . ?
B12 B21 1.773(9) . ?
B13 H13 1.1100 . ?
B13 B14 1.771(9) . ?
B13 B17 1.779(9) . ?
B13 B18 1.781(9) . ?
B14 H14 1.1100 . ?
B14 B15 1.780(9) . ?
B14 B18 1.761(8) . ?
B14 B19 1.780(9) . ?
B15 H15 1.1100 . ?
B15 B16 1.779(10) . ?
B15 B19 1.774(9) . ?
B15 B20 1.764(10) . ?
B16 H16 1.1100 . ?
B16 B20 1.762(9) . ?
B16 B21 1.770(8) . ?
B17 H17 1.1100 . ?
B17 B18 1.780(10) . ?
B17 B21 1.777(9) . ?
B17 B22 1.783(10) . ?
B18 H18 1.1100 . ?
B18 B19 1.782(10) . ?
B18 B22 1.786(10) . ?
B19 H19 1.1100 . ?
B19 B20 1.774(10) . ?
B19 B22 1.782(10) . ?
B20 H20 1.1100 . ?
B20 B21 1.796(10) . ?
B20 B22 1.786(9) . ?
B21 H21 1.1100 . ?
B21 B22 1.784(9) . ?
B22 H22 1.1100 . ?
O2 C50 1.213(10) . ?
C49 H49A 0.9700 . ?
C49 H49B 0.9700 . ?
C49 H49C 0.9700 . ?
C49 C50 1.490(15) . ?
C50 C51 1.523(15) . ?
C51 H51A 0.9700 . ?
C51 H51B 0.9700 . ?
C51 H51C 0.9700 . ?
O3 C53 1.234(9) . ?
C52 H52A 0.9700 . ?
C52 H52B 0.9700 . ?
C52 H52C 0.9700 . ?
C52 C53 1.459(12) . ?
C53 C54 1.476(12) . ?
C54 H54A 0.9700 . ?
C54 H54B 0.9700 . ?
C54 H54C 0.9700 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 Pt1 N2 79.22(15) . . ?
C1 Pt1 N1 97.16(18) . . ?
C1 Pt1 N2 175.27(18) . . ?
C2 Pt1 N1 176.58(16) . . ?
C2 Pt1 N2 98.80(18) . . ?
C2 Pt1 C1 84.7(2) . . ?
C39 N1 Pt1 115.6(3) . . ?
C43 N1 Pt1 125.8(3) . . ?
C43 N1 C39 118.5(4) . . ?
C34 N2 Pt1 126.6(3) . . ?
C34 N2 C38 118.0(4) . . ?
C38 N2 Pt1 115.2(3) . . ?
C1 N3 C3 109.6(4) . . ?
C1 N3 C10 126.0(4) . . ?
C3 N3 C10 124.4(4) . . ?
C1 N4 C4 109.8(4) . . ?
C1 N4 C5 125.2(4) . . ?
C4 N4 C5 125.0(4) . . ?
C2 N5 C9 110.4(5) . . ?
C2 N5 C22 125.2(5) . . ?
C9 N5 C22 124.3(6) . . ?
C2 N6 C7 125.2(4) . . ?
C2 N6 C8 110.3(5) . . ?
C8 N6 C7 124.5(4) . . ?
N3 C1 Pt1 130.2(4) . . ?
N4 C1 Pt1 123.9(3) . . ?
N4 C1 N3 105.8(4) . . ?
N5 C2 Pt1 131.0(4) . . ?
N5 C2 N6 105.1(4) . . ?
N6 C2 Pt1 123.6(4) . . ?
N3 C3 H3 126.3 . . ?
C4 C3 N3 107.4(5) . . ?
C4 C3 H3 126.3 . . ?
N4 C4 H4 126.3 . . ?
C3 C4 N4 107.5(5) . . ?
C3 C4 H4 126.3 . . ?
N4 C5 H5A 108.5 . . ?
N4 C5 H5B 108.5 . . ?
N4 C5 C6 115.1(5) . . ?
H5A C5 H5B 107.5 . . ?
C6 C5 H5A 108.5 . . ?
C6 C5 H5B 108.5 . . ?
C5 C6 H6A 108.5 . . ?
C5 C6 H6B 108.5 . . ?
H6A C6 H6B 107.5 . . ?
C7 C6 C5 115.2(5) . . ?
C7 C6 H6A 108.5 . . ?
C7 C6 H6B 108.5 . . ?
N6 C7 C6 115.2(4) . . ?
N6 C7 H7A 108.5 . . ?
N6 C7 H7B 108.5 . . ?
C6 C7 H7A 108.5 . . ?
C6 C7 H7B 108.5 . . ?
H7A C7 H7B 107.5 . . ?
N6 C8 H8 126.5 . . ?
C9 C8 N6 107.1(5) . . ?
C9 C8 H8 126.5 . . ?
N5 C9 H9 126.5 . . ?
C8 C9 N5 107.1(5) . . ?
C8 C9 H9 126.5 . . ?
N3 C10 H10A 108.9 . . ?
N3 C10 H10B 108.9 . . ?
N3 C10 C11 113.5(5) . . ?
H10A C10 H10B 107.7 . . ?
C11 C10 H10A 108.9 . . ?
C11 C10 H10B 108.9 . . ?
C10 C11 H11A 107.4 . . ?
C10 C11 H11B 107.4 . . ?
H11A C11 H11B 106.9 . . ?
C12 C11 C10 119.8(7) . . ?
C12 C11 H11A 107.4 . . ?
C12 C11 H11B 107.4 . . ?
C11 C12 H12A 108.5 . . ?
C11 C12 H12B 108.5 . . ?
C11 C12 C13 115.0(7) . . ?
H12A C12 H12B 107.5 . . ?
C13 C12 H12A 108.5 . . ?
C13 C12 H12B 108.5 . . ?
C12 C13 H13A 107.6 . . ?
C12 C13 H13B 107.6 . . ?
H13A C13 H13B 107.1 . . ?
C14 C13 C12 118.7(8) . . ?
C14 C13 H13A 107.6 . . ?
C14 C13 H13B 107.6 . . ?
C13 C14 H14A 107.9 . . ?
C13 C14 H14B 107.9 . . ?
C13 C14 C15 117.6(8) . . ?
H14A C14 H14B 107.2 . . ?
C15 C14 H14A 107.9 . . ?
C15 C14 H14B 107.9 . . ?
C14 C15 H15A 107.3 . . ?
C14 C15 H15B 107.3 . . ?
H15A C15 H15B 106.9 . . ?
C16 C15 C14 120.2(9) . . ?
C16 C15 H15A 107.3 . . ?
C16 C15 H15B 107.3 . . ?
C15 C16 H16A 107.5 . . ?
C15 C16 H16B 107.5 . . ?
H16A C16 H16B 107.0 . . ?
C17 C16 C15 119.2(8) . . ?
C17 C16 H16A 107.5 . . ?
C17 C16 H16B 107.5 . . ?
C16 C17 H17A 107.6 . . ?
C16 C17 H17B 107.6 . . ?
C16 C17 C18 118.7(9) . . ?
H17A C17 H17B 107.1 . . ?
C18 C17 H17A 107.6 . . ?
C18 C17 H17B 107.6 . . ?
C17 C18 H18A 107.6 . . ?
C17 C18 H18B 107.6 . . ?
C17 C18 C19 118.7(10) . . ?
H18A C18 H18B 107.1 . . ?
C19 C18 H18A 107.6 . . ?
C19 C18 H18B 107.6 . . ?
C18 C19 H19A 108.7 . . ?
C18 C19 H19B 108.7 . . ?
H19A C19 H19B 107.6 . . ?
C20 C19 C18 114.3(13) . . ?
C20 C19 H19A 108.7 . . ?
C20 C19 H19B 108.7 . . ?
C19 C20 H20A 107.4 . . ?
C19 C20 H20B 107.4 . . ?
C19 C20 C21 119.6(13) . . ?
H20A C20 H20B 107.0 . . ?
C21 C20 H20A 107.4 . . ?
C21 C20 H20B 107.4 . . ?
C20 C21 H21A 109.5 . . ?
C20 C21 H21B 109.5 . . ?
C20 C21 H21C 109.5 . . ?
H21A C21 H21B 109.5 . . ?
H21A C21 H21C 109.5 . . ?
H21B C21 H21C 109.5 . . ?
N5 C22 H22A 108.6 . . ?
N5 C22 H22B 108.6 . . ?
N5 C22 C23 114.7(6) . . ?
H22A C22 H22B 107.6 . . ?
C23 C22 H22A 108.6 . . ?
C23 C22 H22B 108.6 . . ?
C22 C23 H23A 107.4 . . ?
C22 C23 H23B 107.4 . . ?
H23A C23 H23B 106.9 . . ?
C24 C23 C22 119.6(8) . . ?
C24 C23 H23A 107.4 . . ?
C24 C23 H23B 107.4 . . ?
C23 C24 H24A 106.2 . . ?
C23 C24 H24B 106.2 . . ?
H24A C24 H24B 106.4 . . ?
C25 C24 C23 124.3(10) . . ?
C25 C24 H24A 106.3 . . ?
C25 C24 H24B 106.2 . . ?
C24 C25 H25A 107.9 . . ?
C24 C25 H25B 107.9 . . ?
C24 C25 C26 117.6(12) . . ?
H25A C25 H25B 107.2 . . ?
C26 C25 H25A 107.9 . . ?
C26 C25 H25B 107.9 . . ?
C25 C26 H26A 99.9 . . ?
C25 C26 H26B 99.9 . . ?
C25 C26 C27 147.6(17) . . ?
H26A C26 H26B 104.1 . . ?
C27 C26 H26A 99.9 . . ?
C27 C26 H26B 99.9 . . ?
C26 C27 H27A 112.5 . . ?
C26 C27 H27B 112.5 . . ?
H27A C27 H27B 110.0 . . ?
C28 C27 C26 96.1(15) . . ?
C28 C27 H27A 112.5 . . ?
C28 C27 H27B 112.5 . . ?
C27 C28 H28A 113.7 . . ?
C27 C28 H28B 113.7 . . ?
C27 C28 C29 89.9(15) . . ?
H28A C28 H28B 110.9 . . ?
C29 C28 H28A 113.7 . . ?
C29 C28 H28B 113.7 . . ?
C28 C29 H29A 111.3 . . ?
C28 C29 H29B 111.3 . . ?
H29A C29 H29B 109.2 . . ?
C30 C29 C28 102.2(17) . . ?
C30 C29 H29A 111.3 . . ?
C30 C29 H29B 111.3 . . ?
C29 C30 H30A 105.2 . . ?
C29 C30 H30B 105.2 . . ?
C29 C30 C31 128(2) . . ?
H30A C30 H30B 105.9 . . ?
C31 C30 H30A 105.2 . . ?
C31 C30 H30B 105.2 . . ?
C30 C31 H31A 110.6 . . ?
C30 C31 H31B 110.6 . . ?
H31A C31 H31B 108.8 . . ?
C32 C31 C30 105.5(9) . . ?
C32 C31 H31A 110.6 . . ?
C32 C31 H31B 110.6 . . ?
C31 C32 H32A 106.9 . . ?
C31 C32 H32B 106.9 . . ?
C31 C32 C33 122(3) . . ?
H32A C32 H32B 106.7 . . ?
C33 C32 H32A 106.9 . . ?
C33 C32 H32B 106.9 . . ?
C32 C33 H33A 109.5 . . ?
C32 C33 H33B 109.5 . . ?
C32 C33 H33C 109.5 . . ?
H33A C33 H33B 109.5 . . ?
H33A C33 H33C 109.5 . . ?
H33B C33 H33C 109.5 . . ?
N2 C34 H34 118.6 . . ?
N2 C34 C35 122.9(5) . . ?
C35 C34 H34 118.6 . . ?
C34 C35 H35 119.9 . . ?
C34 C35 C36 120.1(5) . . ?
C36 C35 H35 119.9 . . ?
C35 C36 C45 122.9(4) . . ?
C37 C36 C35 116.2(4) . . ?
C37 C36 C45 120.9(4) . . ?
C36 C37 H37 119.2 . . ?
C38 C37 C36 121.5(4) . . ?
C38 C37 H37 119.2 . . ?
N2 C38 C39 115.0(4) . . ?
C37 C38 N2 121.1(4) . . ?
C37 C38 C39 123.8(4) . . ?
N1 C39 C38 115.0(4) . . ?
N1 C39 C40 121.1(4) . . ?
C40 C39 C38 123.9(4) . . ?
C39 C40 H40 119.4 . . ?
C39 C40 C41 121.2(4) . . ?
C41 C40 H40 119.4 . . ?
C40 C41 C42 116.6(5) . . ?
C40 C41 C44 121.3(4) . . ?
C42 C41 C44 122.0(4) . . ?
C41 C42 H42 119.9 . . ?
C43 C42 C41 120.2(5) . . ?
C43 C42 H42 119.9 . . ?
N1 C43 C42 122.2(4) . . ?
N1 C43 H43 118.9 . . ?
C42 C43 H43 118.9 . . ?
C41 C44 B1 118.2(4) . . ?
C41 C44 B2 119.8(4) . . ?
C41 C44 B3 119.3(4) . . ?
C41 C44 B4 118.0(4) . . ?
C41 C44 B5 117.3(4) . . ?
B1 C44 B2 62.4(4) . . ?
B3 C44 B1 113.6(4) . . ?
B3 C44 B2 62.1(3) . . ?
B3 C44 B4 62.0(3) . . ?
B4 C44 B1 113.4(4) . . ?
B4 C44 B2 113.0(4) . . ?
B5 C44 B1 62.0(3) . . ?
B5 C44 B2 113.2(4) . . ?
B5 C44 B3 113.5(4) . . ?
B5 C44 B4 62.4(3) . . ?
C36 C45 B12 117.8(4) . . ?
C36 C45 B13 119.9(4) . . ?
C36 C45 B14 120.2(4) . . ?
C36 C45 B15 117.4(4) . . ?
C36 C45 B16 116.4(4) . . ?
B12 C45 B14 113.5(4) . . ?
B12 C45 B15 113.9(4) . . ?
B13 C45 B12 62.5(3) . . ?
B13 C45 B14 62.2(3) . . ?
B13 C45 B15 113.9(4) . . ?
B13 C45 B16 113.7(4) . . ?
B15 C45 B14 62.3(4) . . ?
B16 C45 B12 62.1(3) . . ?
B16 C45 B14 113.5(4) . . ?
B16 C45 B15 62.5(4) . . ?
H46A C46 H46B 109.5 . . ?
H46A C46 H46C 109.5 . . ?
H46B C46 H46C 109.5 . . ?
C47 C46 H46A 109.5 . . ?
C47 C46 H46B 109.5 . . ?
C47 C46 H46C 109.5 . . ?
O1 C47 C46 120.4(8) . . ?
O1 C47 C48 121.9(8) . . ?
C46 C47 C48 117.7(7) . . ?
C47 C48 H48A 109.5 . . ?
C47 C48 H48B 109.5 . . ?
C47 C48 H48C 109.5 . . ?
H48A C48 H48B 109.5 . . ?
H48A C48 H48C 109.5 . . ?
H48B C48 H48C 109.5 . . ?
C44 B1 H1 124.2 . . ?
C44 B1 B2 58.8(3) . . ?
C44 B1 B5 58.9(3) . . ?
C44 B1 B6 105.5(5) . . ?
C44 B1 B10 105.2(4) . . ?
B2 B1 H1 121.5 . . ?
B5 B1 H1 121.8 . . ?
B5 B1 B2 107.8(4) . . ?
B6 B1 H1 122.0 . . ?
B6 B1 B2 60.2(4) . . ?
B6 B1 B5 107.9(4) . . ?
B10 B1 H1 122.2 . . ?
B10 B1 B2 108.2(5) . . ?
B10 B1 B5 59.7(3) . . ?
B10 B1 B6 60.3(4) . . ?
C44 B2 B1 58.8(3) . . ?
C44 B2 H2 124.5 . . ?
C44 B2 B3 58.8(3) . . ?
C44 B2 B6 104.9(4) . . ?
C44 B2 B7 105.5(4) . . ?
B1 B2 H2 121.8 . . ?
B3 B2 B1 108.0(4) . . ?
B3 B2 H2 121.1 . . ?
B3 B2 B6 108.7(5) . . ?
B6 B2 B1 59.4(4) . . ?
B6 B2 H2 122.2 . . ?
B7 B2 B1 108.1(5) . . ?
B7 B2 H2 121.8 . . ?
B7 B2 B3 60.4(4) . . ?
B7 B2 B6 60.6(4) . . ?
C44 B3 B2 59.1(3) . . ?
C44 B3 H3A 124.4 . . ?
C44 B3 B4 59.0(3) . . ?
C44 B3 B7 104.8(4) . . ?
C44 B3 B8 104.8(5) . . ?
B2 B3 H3A 121.7 . . ?
B2 B3 B7 59.3(4) . . ?
B2 B3 B8 107.5(5) . . ?
B4 B3 B2 108.1(4) . . ?
B4 B3 H3A 121.5 . . ?
B4 B3 B7 107.8(5) . . ?
B4 B3 B8 59.6(4) . . ?
B7 B3 H3A 122.6 . . ?
B8 B3 H3A 122.6 . . ?
B8 B3 B7 60.2(4) . . ?
C44 B4 B3 59.0(3) . . ?
C44 B4 H4A 124.3 . . ?
C44 B4 B5 58.7(3) . . ?
C44 B4 B8 105.4(4) . . ?
C44 B4 B9 105.3(4) . . ?
B3 B4 H4A 121.2 . . ?
B3 B4 B5 108.0(4) . . ?
B3 B4 B9 108.5(4) . . ?
B5 B4 H4A 121.8 . . ?
B8 B4 B3 60.4(4) . . ?
B8 B4 H4A 122.2 . . ?
B8 B4 B5 107.7(4) . . ?
B8 B4 B9 60.0(4) . . ?
B9 B4 H4A 122.1 . . ?
B9 B4 B5 59.9(3) . . ?
C44 B5 B1 59.1(3) . . ?
C44 B5 B4 58.9(3) . . ?
C44 B5 H5 124.2 . . ?
C44 B5 B9 105.4(4) . . ?
C44 B5 B10 105.6(4) . . ?
B1 B5 B4 108.2(4) . . ?
B1 B5 H5 121.4 . . ?
B1 B5 B9 108.4(4) . . ?
B4 B5 H5 121.5 . . ?
B9 B5 B4 59.9(3) . . ?
B9 B5 H5 122.0 . . ?
B10 B5 B1 59.9(4) . . ?
B10 B5 B4 108.5(5) . . ?
B10 B5 H5 121.8 . . ?
B10 B5 B9 60.7(4) . . ?
B1 B6 B2 60.4(4) . . ?
B1 B6 H6 121.8 . . ?
B1 B6 B7 107.7(4) . . ?
B1 B6 B10 59.7(4) . . ?
B1 B6 B11 107.6(5) . . ?
B2 B6 H6 122.1 . . ?
B2 B6 B7 59.1(4) . . ?
B7 B6 H6 121.9 . . ?
B10 B6 B2 107.9(4) . . ?
B10 B6 H6 121.7 . . ?
B10 B6 B7 108.1(5) . . ?
B11 B6 B2 107.4(4) . . ?
B11 B6 H6 121.9 . . ?
B11 B6 B7 60.3(4) . . ?
B11 B6 B10 59.9(4) . . ?
B2 B7 B3 60.2(4) . . ?
B2 B7 B6 60.3(4) . . ?
B2 B7 H7 121.6 . . ?
B2 B7 B8 108.0(5) . . ?
B2 B7 B11 107.6(5) . . ?
B3 B7 B6 108.3(5) . . ?
B3 B7 H7 121.6 . . ?
B3 B7 B8 59.9(4) . . ?
B3 B7 B11 107.6(5) . . ?
B6 B7 H7 121.8 . . ?
B6 B7 B11 59.4(4) . . ?
B8 B7 B6 107.6(5) . . ?
B8 B7 H7 121.9 . . ?
B8 B7 B11 59.7(4) . . ?
B11 B7 H7 122.3 . . ?
B3 B8 B7 59.9(4) . . ?
B3 B8 H8A 121.6 . . ?
B4 B8 B3 60.0(3) . . ?
B4 B8 B7 108.0(4) . . ?
B4 B8 H8A 121.8 . . ?
B4 B8 B9 60.3(4) . . ?
B4 B8 B11 107.7(5) . . ?
B7 B8 H8A 121.6 . . ?
B9 B8 B3 108.4(4) . . ?
B9 B8 B7 108.2(5) . . ?
B9 B8 H8A 121.5 . . ?
B9 B8 B11 59.7(4) . . ?
B11 B8 B3 108.0(5) . . ?
B11 B8 B7 60.2(4) . . ?
B11 B8 H8A 121.9 . . ?
B4 B9 H9A 121.8 . . ?
B4 B9 B10 107.6(4) . . ?
B5 B9 B4 60.2(3) . . ?
B5 B9 H9A 122.2 . . ?
B5 B9 B10 59.2(3) . . ?
B8 B9 B4 59.7(4) . . ?
B8 B9 B5 107.8(4) . . ?
B8 B9 H9A 121.6 . . ?
B8 B9 B10 108.0(5) . . ?
B10 B9 H9A 122.1 . . ?
B11 B9 B4 107.8(5) . . ?
B11 B9 B5 107.1(4) . . ?
B11 B9 B8 60.4(4) . . ?
B11 B9 H9A 121.9 . . ?
B11 B9 B10 59.8(4) . . ?
B1 B10 B6 60.0(4) . . ?
B1 B10 B9 108.4(5) . . ?
B1 B10 H10 121.5 . . ?
B1 B10 B11 107.8(5) . . ?
B5 B10 B1 60.4(3) . . ?
B5 B10 B6 108.3(5) . . ?
B5 B10 B9 60.1(3) . . ?
B5 B10 H10 121.5 . . ?
B5 B10 B11 107.7(5) . . ?
B6 B10 B9 108.0(5) . . ?
B6 B10 H10 121.6 . . ?
B9 B10 H10 121.7 . . ?
B11 B10 B6 60.0(4) . . ?
B11 B10 B9 59.6(4) . . ?
B11 B10 H10 122.1 . . ?
B6 B11 B7 60.2(4) . . ?
B6 B11 B8 108.5(5) . . ?
B6 B11 H11 121.3 . . ?
B7 B11 H11 121.7 . . ?
B8 B11 B7 60.0(4) . . ?
B8 B11 H11 121.6 . . ?
B9 B11 B6 108.9(5) . . ?
B9 B11 B7 108.3(5) . . ?
B9 B11 B8 59.9(4) . . ?
B9 B11 B10 60.6(4) . . ?
B9 B11 H11 121.3 . . ?
B10 B11 B6 60.1(4) . . ?
B10 B11 B7 108.2(5) . . ?
B10 B11 B8 108.4(5) . . ?
B10 B11 H11 121.4 . . ?
C45 B12 H12 124.4 . . ?
C45 B12 B13 58.5(3) . . ?
C45 B12 B16 58.9(3) . . ?
C45 B12 B17 105.3(4) . . ?
C45 B12 B21 105.7(4) . . ?
B13 B12 H12 121.3 . . ?
B13 B12 B21 108.9(4) . . ?
B16 B12 H12 121.7 . . ?
B16 B12 B13 107.8(5) . . ?
B16 B12 B21 60.0(3) . . ?
B17 B12 H12 122.1 . . ?
B17 B12 B13 60.5(4) . . ?
B17 B12 B16 108.0(4) . . ?
B17 B12 B21 60.4(3) . . ?
B21 B12 H12 121.7 . . ?
C45 B13 B12 59.0(3) . . ?
C45 B13 H13 124.2 . . ?
C45 B13 B14 59.4(3) . . ?
C45 B13 B17 104.9(4) . . ?
C45 B13 B18 105.0(4) . . ?
B12 B13 H13 121.5 . . ?
B12 B13 B17 59.5(3) . . ?
B12 B13 B18 107.7(4) . . ?
B14 B13 B12 108.4(4) . . ?
B14 B13 H13 121.4 . . ?
B14 B13 B17 107.7(5) . . ?
B14 B13 B18 59.5(4) . . ?
B17 B13 H13 122.6 . . ?
B17 B13 B18 60.0(4) . . ?
B18 B13 H13 122.6 . . ?
C45 B14 B13 58.3(3) . . ?
C45 B14 H14 124.8 . . ?
C45 B14 B15 58.8(3) . . ?
C45 B14 B18 105.0(4) . . ?
C45 B14 B19 104.9(4) . . ?
B13 B14 H14 121.3 . . ?
B13 B14 B15 107.8(4) . . ?
B13 B14 B19 108.7(5) . . ?
B15 B14 H14 121.7 . . ?
B18 B14 B13 60.6(4) . . ?
B18 B14 H14 121.9 . . ?
B18 B14 B15 108.2(5) . . ?
B18 B14 B19 60.4(4) . . ?
B19 B14 H14 122.0 . . ?
B19 B14 B15 59.8(4) . . ?
C45 B15 B14 59.0(3) . . ?
C45 B15 H15 124.4 . . ?
C45 B15 B16 58.4(3) . . ?
C45 B15 B19 105.3(4) . . ?
C45 B15 B20 104.9(5) . . ?
B14 B15 H15 121.5 . . ?
B16 B15 B14 107.5(4) . . ?
B16 B15 H15 122.1 . . ?
B19 B15 B14 60.1(4) . . ?
B19 B15 H15 122.2 . . ?
B19 B15 B16 107.6(5) . . ?
B20 B15 B14 108.1(4) . . ?
B20 B15 H15 122.3 . . ?
B20 B15 B16 59.6(4) . . ?
B20 B15 B19 60.2(4) . . ?
C45 B16 B12 59.0(3) . . ?
C45 B16 B15 59.0(3) . . ?
C45 B16 H16 124.2 . . ?
C45 B16 B20 105.5(4) . . ?
C45 B16 B21 105.9(4) . . ?
B12 B16 B15 108.4(4) . . ?
B12 B16 H16 121.2 . . ?
B12 B16 B21 60.2(3) . . ?
B15 B16 H16 121.3 . . ?
B20 B16 B12 108.9(4) . . ?
B20 B16 B15 59.8(4) . . ?
B20 B16 H16 121.8 . . ?
B20 B16 B21 61.1(4) . . ?
B21 B16 B15 109.0(4) . . ?
B21 B16 H16 121.4 . . ?
B12 B17 B13 60.0(3) . . ?
B12 B17 H17 121.7 . . ?
B12 B17 B18 108.1(4) . . ?
B12 B17 B21 60.1(3) . . ?
B12 B17 B22 108.1(4) . . ?
B13 B17 H17 121.6 . . ?
B13 B17 B18 60.1(4) . . ?
B13 B17 B22 108.2(5) . . ?
B18 B17 H17 121.6 . . ?
B18 B17 B22 60.2(4) . . ?
B21 B17 B13 108.4(4) . . ?
B21 B17 H17 121.4 . . ?
B21 B17 B18 108.4(5) . . ?
B21 B17 B22 60.1(4) . . ?
B22 B17 H17 121.6 . . ?
B13 B18 H18 121.8 . . ?
B13 B18 B19 108.1(4) . . ?
B13 B18 B22 108.0(5) . . ?
B14 B18 B13 60.0(3) . . ?
B14 B18 B17 108.1(4) . . ?
B14 B18 H18 121.5 . . ?
B14 B18 B19 60.3(4) . . ?
B14 B18 B22 108.2(4) . . ?
B17 B18 B13 59.9(4) . . ?
B17 B18 H18 121.8 . . ?
B17 B18 B19 108.0(5) . . ?
B17 B18 B22 60.0(4) . . ?
B19 B18 H18 121.6 . . ?
B19 B18 B22 59.9(4) . . ?
B22 B18 H18 121.7 . . ?
B14 B19 B18 59.3(4) . . ?
B14 B19 H19 122.1 . . ?
B14 B19 B22 107.6(5) . . ?
B15 B19 B14 60.1(4) . . ?
B15 B19 B18 107.5(4) . . ?
B15 B19 H19 121.9 . . ?
B15 B19 B22 107.9(5) . . ?
B18 B19 H19 122.0 . . ?
B20 B19 B14 107.7(4) . . ?
B20 B19 B15 59.6(4) . . ?
B20 B19 B18 108.0(5) . . ?
B20 B19 H19 121.7 . . ?
B20 B19 B22 60.3(4) . . ?
B22 B19 B18 60.1(4) . . ?
B22 B19 H19 121.6 . . ?
B15 B20 B19 60.2(4) . . ?
B15 B20 H20 121.2 . . ?
B15 B20 B21 108.5(5) . . ?
B15 B20 B22 108.2(5) . . ?
B16 B20 B15 60.6(4) . . ?
B16 B20 B19 108.4(5) . . ?
B16 B20 H20 121.8 . . ?
B16 B20 B21 59.7(4) . . ?
B16 B20 B22 107.4(5) . . ?
B19 B20 H20 121.4 . . ?
B19 B20 B21 108.2(5) . . ?
B19 B20 B22 60.1(4) . . ?
B21 B20 H20 121.7 . . ?
B22 B20 H20 122.0 . . ?
B22 B20 B21 59.8(4) . . ?
B12 B21 B17 59.5(3) . . ?
B12 B21 B20 107.0(5) . . ?
B12 B21 H21 122.2 . . ?
B12 B21 B22 107.6(5) . . ?
B16 B21 B12 59.8(3) . . ?
B16 B21 B17 107.1(4) . . ?
B16 B21 B20 59.2(4) . . ?
B16 B21 H21 122.4 . . ?
B16 B21 B22 107.2(5) . . ?
B17 B21 B20 107.4(5) . . ?
B17 B21 H21 122.1 . . ?
B17 B21 B22 60.1(4) . . ?
B20 B21 H21 122.3 . . ?
B22 B21 B20 59.8(4) . . ?
B22 B21 H21 121.8 . . ?
B17 B22 B18 59.8(4) . . ?
B17 B22 B20 107.6(4) . . ?
B17 B22 B21 59.8(4) . . ?
B17 B22 H22 122.0 . . ?
B18 B22 H22 122.0 . . ?
B19 B22 B17 107.8(5) . . ?
B19 B22 B18 59.9(4) . . ?
B19 B22 B20 59.6(4) . . ?
B19 B22 B21 108.3(4) . . ?
B19 B22 H22 121.7 . . ?
B20 B22 B18 107.3(5) . . ?
B20 B22 H22 122.1 . . ?
B21 B22 B18 107.9(4) . . ?
B21 B22 B20 60.4(4) . . ?
B21 B22 H22 121.4 . . ?
H49A C49 H49B 109.5 . . ?
H49A C49 H49C 109.5 . . ?
H49B C49 H49C 109.5 . . ?
C50 C49 H49A 109.5 . . ?
C50 C49 H49B 109.5 . . ?
C50 C49 H49C 109.5 . . ?
O2 C50 C49 121.9(12) . . ?
O2 C50 C51 120.7(12) . . ?
C49 C50 C51 117.4(9) . . ?
C50 C51 H51A 109.5 . . ?
C50 C51 H51B 109.5 . . ?
C50 C51 H51C 109.5 . . ?
H51A C51 H51B 109.5 . . ?
H51A C51 H51C 109.5 . . ?
H51B C51 H51C 109.5 . . ?
H52A C52 H52B 109.5 . . ?
H52A C52 H52C 109.5 . . ?
H52B C52 H52C 109.5 . . ?
C53 C52 H52A 109.5 . . ?
C53 C52 H52B 109.5 . . ?
C53 C52 H52C 109.5 . . ?
O3 C53 C52 121.7(8) . . ?
O3 C53 C54 120.0(9) . . ?
C52 C53 C54 118.2(8) . . ?
C53 C54 H54A 109.5 . . ?
C53 C54 H54B 109.5 . . ?
C53 C54 H54C 109.5 . . ?
H54A C54 H54B 109.5 . . ?
H54A C54 H54C 109.5 . . ?
H54B C54 H54C 109.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Pt1 N1 C39 C38 -0.7(5) . . . . ?
Pt1 N1 C39 C40 -178.6(3) . . . . ?
Pt1 N1 C43 C42 179.1(4) . . . . ?
Pt1 N2 C34 C35 -177.5(4) . . . . ?
Pt1 N2 C38 C37 177.9(4) . . . . ?
Pt1 N2 C38 C39 0.1(5) . . . . ?
N1 C39 C40 C41 -0.2(7) . . . . ?
N2 C34 C35 C36 0.7(8) . . . . ?
N2 C38 C39 N1 0.4(6) . . . . ?
N2 C38 C39 C40 178.3(4) . . . . ?
N3 C3 C4 N4 -0.7(7) . . . . ?
N3 C10 C11 C12 -52.8(8) . . . . ?
N4 C5 C6 C7 80.9(6) . . . . ?
N5 C22 C23 C24 -44.4(16) . . . . ?
N6 C8 C9 N5 0.4(7) . . . . ?
C1 N3 C3 C4 0.0(7) . . . . ?
C1 N3 C10 C11 -78.3(7) . . . . ?
C1 N4 C4 C3 1.1(7) . . . . ?
C1 N4 C5 C6 -88.9(6) . . . . ?
C2 N5 C9 C8 -0.8(7) . . . . ?
C2 N5 C22 C23 123.8(8) . . . . ?
C2 N6 C7 C6 90.7(6) . . . . ?
C2 N6 C8 C9 0.1(6) . . . . ?
C3 N3 C1 Pt1 175.9(4) . . . . ?
C3 N3 C1 N4 0.6(6) . . . . ?
C3 N3 C10 C11 100.7(7) . . . . ?
C4 N4 C1 Pt1 -176.7(4) . . . . ?
C4 N4 C1 N3 -1.1(6) . . . . ?
C4 N4 C5 C6 93.3(6) . . . . ?
C5 N4 C1 Pt1 5.2(7) . . . . ?
C5 N4 C1 N3 -179.2(5) . . . . ?
C5 N4 C4 C3 179.2(5) . . . . ?
C5 C6 C7 N6 -80.7(6) . . . . ?
C7 N6 C2 Pt1 -8.6(7) . . . . ?
C7 N6 C2 N5 177.5(4) . . . . ?
C7 N6 C8 C9 -178.0(5) . . . . ?
C8 N6 C2 Pt1 173.3(4) . . . . ?
C8 N6 C2 N5 -0.6(6) . . . . ?
C8 N6 C7 C6 -91.5(6) . . . . ?
C9 N5 C2 Pt1 -172.4(4) . . . . ?
C9 N5 C2 N6 0.8(6) . . . . ?
C9 N5 C22 C23 -53.3(11) . . . . ?
C10 N3 C1 Pt1 -4.9(8) . . . . ?
C10 N3 C1 N4 179.8(5) . . . . ?
C10 N3 C3 C4 -179.1(5) . . . . ?
C10 C11 C12 C13 -178.0(7) . . . . ?
C11 C12 C13 C14 -170.5(8) . . . . ?
C12 C13 C14 C15 -179.2(8) . . . . ?
C13 C14 C15 C16 -174.7(9) . . . . ?
C14 C15 C16 C17 52.6(15) . . . . ?
C15 C16 C17 C18 169.9(11) . . . . ?
C16 C17 C18 C19 173.1(11) . . . . ?
C17 C18 C19 C20 80.1(18) . . . . ?
C18 C19 C20 C21 -179.7(13) . . . . ?
C22 N5 C2 Pt1 10.2(8) . . . . ?
C22 N5 C2 N6 -176.6(5) . . . . ?
C22 N5 C9 C8 176.6(6) . . . . ?
C22 C23 C24 C25 -170.5(14) . . . . ?
C23 C24 C25 C26 178.0(15) . . . . ?
C24 C25 C26 C27 -129(3) . . . . ?
C25 C26 C27 C28 -20(4) . . . . ?
C26 C27 C28 C29 168.6(18) . . . . ?
C27 C28 C29 C30 170(2) . . . . ?
C28 C29 C30 C31 160(2) . . . . ?
C29 C30 C31 C32 -64(4) . . . . ?
C30 C31 C32 C33 -146(3) . . . . ?
C34 N2 C38 C37 2.3(7) . . . . ?
C34 N2 C38 C39 -175.5(4) . . . . ?
C34 C35 C36 C37 1.1(7) . . . . ?
C34 C35 C36 C45 -179.0(5) . . . . ?
C35 C36 C37 C38 -1.1(7) . . . . ?
C35 C36 C45 B12 -148.8(5) . . . . ?
C35 C36 C45 B13 -76.2(6) . . . . ?
C35 C36 C45 B14 -3.0(7) . . . . ?
C35 C36 C45 B15 69.3(6) . . . . ?
C35 C36 C45 B16 140.4(5) . . . . ?
C36 C37 C38 N2 -0.6(7) . . . . ?
C36 C37 C38 C39 177.1(4) . . . . ?
C36 C45 B12 B13 111.1(5) . . . . ?
C36 C45 B12 B16 -106.8(5) . . . . ?
C36 C45 B12 B17 151.1(4) . . . . ?
C36 C45 B12 B21 -146.0(4) . . . . ?
C36 C45 B13 B12 -107.9(5) . . . . ?
C36 C45 B13 B14 110.6(5) . . . . ?
C36 C45 B13 B17 -147.4(5) . . . . ?
C36 C45 B13 B18 150.3(5) . . . . ?
C36 C45 B14 B13 -110.2(5) . . . . ?
C36 C45 B14 B15 107.2(5) . . . . ?
C36 C45 B14 B18 -150.4(5) . . . . ?
C36 C45 B14 B19 146.8(5) . . . . ?
C36 C45 B15 B14 -111.5(5) . . . . ?
C36 C45 B15 B16 107.1(5) . . . . ?
C36 C45 B15 B19 -151.4(5) . . . . ?
C36 C45 B15 B20 146.1(4) . . . . ?
C36 C45 B16 B12 109.0(5) . . . . ?
C36 C45 B16 B15 -108.7(5) . . . . ?
C36 C45 B16 B20 -147.9(4) . . . . ?
C36 C45 B16 B21 148.4(5) . . . . ?
C37 C36 C45 B12 31.2(6) . . . . ?
C37 C36 C45 B13 103.7(5) . . . . ?
C37 C36 C45 B14 177.0(4) . . . . ?
C37 C36 C45 B15 -110.8(5) . . . . ?
C37 C36 C45 B16 -39.6(7) . . . . ?
C37 C38 C39 N1 -177.4(4) . . . . ?
C37 C38 C39 C40 0.5(7) . . . . ?
C38 N2 C34 C35 -2.4(7) . . . . ?
C38 C39 C40 C41 -178.0(4) . . . . ?
C39 N1 C43 C42 1.7(7) . . . . ?
C39 C40 C41 C42 0.6(7) . . . . ?
C39 C40 C41 C44 -179.3(4) . . . . ?
C40 C41 C42 C43 0.1(8) . . . . ?
C40 C41 C44 B1 112.2(5) . . . . ?
C40 C41 C44 B2 -175.2(5) . . . . ?
C40 C41 C44 B3 -102.5(6) . . . . ?
C40 C41 C44 B4 -30.6(7) . . . . ?
C40 C41 C44 B5 41.0(6) . . . . ?
C41 C42 C43 N1 -1.2(8) . . . . ?
C41 C44 B1 B2 110.9(5) . . . . ?
C41 C44 B1 B5 -107.7(5) . . . . ?
C41 C44 B1 B6 150.4(4) . . . . ?
C41 C44 B1 B10 -146.8(5) . . . . ?
C41 C44 B2 B1 -108.3(5) . . . . ?
C41 C44 B2 B3 109.6(5) . . . . ?
C41 C44 B2 B6 -147.4(5) . . . . ?
C41 C44 B2 B7 149.6(5) . . . . ?
C41 C44 B3 B2 -110.4(5) . . . . ?
C41 C44 B3 B4 108.2(5) . . . . ?
C41 C44 B3 B7 -149.7(4) . . . . ?
C41 C44 B3 B8 147.8(4) . . . . ?
C41 C44 B4 B3 -110.2(5) . . . . ?
C41 C44 B4 B5 107.9(5) . . . . ?
C41 C44 B4 B8 -150.4(5) . . . . ?
C41 C44 B4 B9 147.1(5) . . . . ?
C41 C44 B5 B1 109.2(5) . . . . ?
C41 C44 B5 B4 -109.1(5) . . . . ?
C41 C44 B5 B9 -148.3(4) . . . . ?
C41 C44 B5 B10 148.5(4) . . . . ?
C42 C41 C44 B1 -67.7(6) . . . . ?
C42 C41 C44 B2 4.9(7) . . . . ?
C42 C41 C44 B3 77.6(6) . . . . ?
C42 C41 C44 B4 149.6(5) . . . . ?
C42 C41 C44 B5 -138.8(5) . . . . ?
C43 N1 C39 C38 177.0(4) . . . . ?
C43 N1 C39 C40 -1.0(7) . . . . ?
C44 C41 C42 C43 179.9(5) . . . . ?
C44 B1 B2 B3 33.6(4) . . . . ?
C44 B1 B2 B6 135.0(4) . . . . ?
C44 B1 B2 B7 97.5(4) . . . . ?
C44 B1 B5 B4 -33.9(4) . . . . ?
C44 B1 B5 B9 -97.3(5) . . . . ?
C44 B1 B5 B10 -135.2(5) . . . . ?
C44 B1 B6 B2 -38.9(4) . . . . ?
C44 B1 B6 B7 -2.1(6) . . . . ?
C44 B1 B6 B10 98.9(5) . . . . ?
C44 B1 B6 B11 61.5(6) . . . . ?
C44 B1 B10 B5 38.7(4) . . . . ?
C44 B1 B10 B6 -99.5(5) . . . . ?
C44 B1 B10 B9 1.1(6) . . . . ?
C44 B1 B10 B11 -61.9(5) . . . . ?
C44 B2 B3 B4 34.2(4) . . . . ?
C44 B2 B3 B7 134.6(5) . . . . ?
C44 B2 B3 B8 97.1(5) . . . . ?
C44 B2 B6 B1 38.8(4) . . . . ?
C44 B2 B6 B7 -99.6(5) . . . . ?
C44 B2 B6 B10 1.2(6) . . . . ?
C44 B2 B6 B11 -62.0(6) . . . . ?
C44 B2 B7 B3 -39.3(4) . . . . ?
C44 B2 B7 B6 98.7(5) . . . . ?
C44 B2 B7 B8 -1.8(6) . . . . ?
C44 B2 B7 B11 61.3(6) . . . . ?
C44 B3 B4 B5 33.7(4) . . . . ?
C44 B3 B4 B8 134.3(4) . . . . ?
C44 B3 B4 B9 97.1(4) . . . . ?
C44 B3 B7 B2 39.2(4) . . . . ?
C44 B3 B7 B6 1.4(6) . . . . ?
C44 B3 B7 B8 -98.8(5) . . . . ?
C44 B3 B7 B11 -61.4(6) . . . . ?
C44 B3 B8 B4 -39.4(4) . . . . ?
C44 B3 B8 B7 98.8(5) . . . . ?
C44 B3 B8 B9 -2.1(6) . . . . ?
C44 B3 B8 B11 61.1(5) . . . . ?
C44 B4 B5 B1 34.0(4) . . . . ?
C44 B4 B5 B9 135.2(4) . . . . ?
C44 B4 B5 B10 97.5(4) . . . . ?
C44 B4 B8 B3 39.5(4) . . . . ?
C44 B4 B8 B7 2.1(6) . . . . ?
C44 B4 B8 B9 -99.0(4) . . . . ?
C44 B4 B8 B11 -61.5(5) . . . . ?
C44 B4 B9 B5 -38.7(4) . . . . ?
C44 B4 B9 B8 99.2(4) . . . . ?
C44 B4 B9 B10 -1.8(6) . . . . ?
C44 B4 B9 B11 61.3(5) . . . . ?
C44 B5 B9 B4 38.7(4) . . . . ?
C44 B5 B9 B8 1.3(5) . . . . ?
C44 B5 B9 B10 -99.5(4) . . . . ?
C44 B5 B9 B11 -62.4(5) . . . . ?
C44 B5 B10 B1 -38.9(4) . . . . ?
C44 B5 B10 B6 -1.5(6) . . . . ?
C44 B5 B10 B9 99.2(5) . . . . ?
C44 B5 B10 B11 62.0(5) . . . . ?
C45 C36 C37 C38 178.9(4) . . . . ?
C45 B12 B13 B14 34.4(4) . . . . ?
C45 B12 B13 B17 134.5(5) . . . . ?
C45 B12 B13 B18 97.3(5) . . . . ?
C45 B12 B16 B15 -33.6(4) . . . . ?
C45 B12 B16 B20 -97.1(5) . . . . ?
C45 B12 B16 B21 -135.4(4) . . . . ?
C45 B12 B17 B13 -39.1(4) . . . . ?
C45 B12 B17 B18 -1.7(6) . . . . ?
C45 B12 B17 B21 99.6(5) . . . . ?
C45 B12 B17 B22 61.9(5) . . . . ?
C45 B12 B21 B16 38.6(4) . . . . ?
C45 B12 B21 B17 -98.9(5) . . . . ?
C45 B12 B21 B20 1.6(5) . . . . ?
C45 B12 B21 B22 -61.4(5) . . . . ?
C45 B13 B14 B15 33.0(4) . . . . ?
C45 B13 B14 B18 134.3(5) . . . . ?
C45 B13 B14 B19 96.3(5) . . . . ?
C45 B13 B17 B12 39.2(4) . . . . ?
C45 B13 B17 B18 -99.0(5) . . . . ?
C45 B13 B17 B21 2.1(6) . . . . ?
C45 B13 B17 B22 -61.6(5) . . . . ?
C45 B13 B18 B14 -39.7(4) . . . . ?
C45 B13 B18 B17 98.7(4) . . . . ?
C45 B13 B18 B19 -2.0(6) . . . . ?
C45 B13 B18 B22 61.4(5) . . . . ?
C45 B14 B15 B16 33.9(4) . . . . ?
C45 B14 B15 B19 134.5(5) . . . . ?
C45 B14 B15 B20 96.9(5) . . . . ?
C45 B14 B18 B13 39.1(4) . . . . ?
C45 B14 B18 B17 1.9(6) . . . . ?
C45 B14 B18 B19 -98.9(5) . . . . ?
C45 B14 B18 B22 -61.6(6) . . . . ?
C45 B14 B19 B15 -39.1(4) . . . . ?
C45 B14 B19 B18 99.1(5) . . . . ?
C45 B14 B19 B20 -1.8(6) . . . . ?
C45 B14 B19 B22 61.8(5) . . . . ?
C45 B15 B16 B12 33.6(4) . . . . ?
C45 B15 B16 B20 135.2(4) . . . . ?
C45 B15 B16 B21 97.5(4) . . . . ?
C45 B15 B19 B14 39.3(4) . . . . ?
C45 B15 B19 B18 2.3(6) . . . . ?
C45 B15 B19 B20 -98.6(5) . . . . ?
C45 B15 B19 B22 -61.1(6) . . . . ?
C45 B15 B20 B16 -38.4(4) . . . . ?
C45 B15 B20 B19 99.3(5) . . . . ?
C45 B15 B20 B21 -1.5(5) . . . . ?
C45 B15 B20 B22 61.8(6) . . . . ?
C45 B16 B20 B15 38.8(4) . . . . ?
C45 B16 B20 B19 0.9(6) . . . . ?
C45 B16 B20 B21 -99.9(4) . . . . ?
C45 B16 B20 B22 -62.6(6) . . . . ?
C45 B16 B21 B12 -38.7(4) . . . . ?
C45 B16 B21 B17 -1.2(6) . . . . ?
C45 B16 B21 B20 99.2(5) . . . . ?
C45 B16 B21 B22 61.9(5) . . . . ?
B1 C44 B2 B3 -142.1(5) . . . . ?
B1 C44 B2 B6 -39.1(4) . . . . ?
B1 C44 B2 B7 -102.1(5) . . . . ?
B1 C44 B3 B2 36.4(4) . . . . ?
B1 C44 B3 B4 -105.0(5) . . . . ?
B1 C44 B3 B7 -2.9(6) . . . . ?
B1 C44 B3 B8 -65.4(5) . . . . ?
B1 C44 B4 B3 105.3(5) . . . . ?
B1 C44 B4 B5 -36.5(4) . . . . ?
B1 C44 B4 B8 65.1(5) . . . . ?
B1 C44 B4 B9 2.7(6) . . . . ?
B1 C44 B5 B4 141.8(4) . . . . ?
B1 C44 B5 B9 102.5(5) . . . . ?
B1 C44 B5 B10 39.3(4) . . . . ?
B1 B2 B3 C44 -33.6(4) . . . . ?
B1 B2 B3 B4 0.6(6) . . . . ?
B1 B2 B3 B7 101.0(5) . . . . ?
B1 B2 B3 B8 63.5(5) . . . . ?
B1 B2 B6 B7 -138.4(5) . . . . ?
B1 B2 B6 B10 -37.6(4) . . . . ?
B1 B2 B6 B11 -100.7(5) . . . . ?
B1 B2 B7 B3 -100.9(5) . . . . ?
B1 B2 B7 B6 37.0(4) . . . . ?
B1 B2 B7 B8 -63.4(6) . . . . ?
B1 B2 B7 B11 -0.3(6) . . . . ?
B1 B5 B9 B4 100.8(5) . . . . ?
B1 B5 B9 B8 63.3(5) . . . . ?
B1 B5 B9 B10 -37.5(4) . . . . ?
B1 B5 B9 B11 -0.4(6) . . . . ?
B1 B5 B10 B6 37.4(4) . . . . ?
B1 B5 B10 B9 138.1(5) . . . . ?
B1 B5 B10 B11 100.9(5) . . . . ?
B1 B6 B7 B2 -37.3(4) . . . . ?
B1 B6 B7 B3 0.5(6) . . . . ?
B1 B6 B7 B8 63.8(6) . . . . ?
B1 B6 B7 B11 100.5(5) . . . . ?
B1 B6 B10 B5 -37.7(4) . . . . ?
B1 B6 B10 B9 -101.2(5) . . . . ?
B1 B6 B10 B11 -137.9(5) . . . . ?
B1 B6 B11 B7 -100.7(5) . . . . ?
B1 B6 B11 B8 -63.7(6) . . . . ?
B1 B6 B11 B9 0.0(7) . . . . ?
B1 B6 B11 B10 37.4(4) . . . . ?
B1 B10 B11 B6 -37.5(4) . . . . ?
B1 B10 B11 B7 0.1(6) . . . . ?
B1 B10 B11 B8 63.7(6) . . . . ?
B1 B10 B11 B9 101.2(5) . . . . ?
B2 C44 B1 B5 141.4(4) . . . . ?
B2 C44 B1 B6 39.6(4) . . . . ?
B2 C44 B1 B10 102.3(5) . . . . ?
B2 C44 B3 B4 -141.4(5) . . . . ?
B2 C44 B3 B7 -39.3(4) . . . . ?
B2 C44 B3 B8 -101.8(5) . . . . ?
B2 C44 B4 B3 36.8(4) . . . . ?
B2 C44 B4 B5 -105.1(5) . . . . ?
B2 C44 B4 B8 -3.4(6) . . . . ?
B2 C44 B4 B9 -65.9(5) . . . . ?
B2 C44 B5 B1 -36.9(4) . . . . ?
B2 C44 B5 B4 104.8(5) . . . . ?
B2 C44 B5 B9 65.6(5) . . . . ?
B2 C44 B5 B10 2.4(6) . . . . ?
B2 B1 B5 C44 34.1(4) . . . . ?
B2 B1 B5 B4 0.2(6) . . . . ?
B2 B1 B5 B9 -63.2(5) . . . . ?
B2 B1 B5 B10 -101.1(5) . . . . ?
B2 B1 B6 B7 36.8(4) . . . . ?
B2 B1 B6 B10 137.8(5) . . . . ?
B2 B1 B6 B11 100.4(5) . . . . ?
B2 B1 B10 B5 100.3(5) . . . . ?
B2 B1 B10 B6 -37.8(4) . . . . ?
B2 B1 B10 B9 62.8(5) . . . . ?
B2 B1 B10 B11 -0.3(6) . . . . ?
B2 B3 B4 C44 -34.2(4) . . . . ?
B2 B3 B4 B5 -0.5(6) . . . . ?
B2 B3 B4 B8 100.1(5) . . . . ?
B2 B3 B4 B9 62.9(5) . . . . ?
B2 B3 B7 B6 -37.8(4) . . . . ?
B2 B3 B7 B8 -138.0(5) . . . . ?
B2 B3 B7 B11 -100.6(5) . . . . ?
B2 B3 B8 B4 -101.1(5) . . . . ?
B2 B3 B8 B7 37.1(4) . . . . ?
B2 B3 B8 B9 -63.7(5) . . . . ?
B2 B3 B8 B11 -0.6(6) . . . . ?
B2 B6 B7 B3 37.8(4) . . . . ?
B2 B6 B7 B8 101.1(5) . . . . ?
B2 B6 B7 B11 137.8(5) . . . . ?
B2 B6 B10 B1 37.8(4) . . . . ?
B2 B6 B10 B5 0.2(6) . . . . ?
B2 B6 B10 B9 -63.4(6) . . . . ?
B2 B6 B10 B11 -100.1(5) . . . . ?
B2 B6 B11 B7 -37.1(4) . . . . ?
B2 B6 B11 B8 0.0(6) . . . . ?
B2 B6 B11 B9 63.6(6) . . . . ?
B2 B6 B11 B10 101.0(5) . . . . ?
B2 B7 B8 B3 -37.6(5) . . . . ?
B2 B7 B8 B4 -0.2(6) . . . . ?
B2 B7 B8 B9 63.5(6) . . . . ?
B2 B7 B8 B11 100.3(5) . . . . ?
B2 B7 B11 B6 37.7(4) . . . . ?
B2 B7 B11 B8 -101.0(5) . . . . ?
B2 B7 B11 B9 -64.1(6) . . . . ?
B2 B7 B11 B10 0.2(6) . . . . ?
B3 C44 B1 B2 -36.3(4) . . . . ?
B3 C44 B1 B5 105.1(5) . . . . ?
B3 C44 B1 B6 3.2(6) . . . . ?
B3 C44 B1 B10 66.0(6) . . . . ?
B3 C44 B2 B1 142.1(5) . . . . ?
B3 C44 B2 B6 103.0(5) . . . . ?
B3 C44 B2 B7 40.0(4) . . . . ?
B3 C44 B4 B5 -141.9(4) . . . . ?
B3 C44 B4 B8 -40.2(4) . . . . ?
B3 C44 B4 B9 -102.7(5) . . . . ?
B3 C44 B5 B1 -105.3(5) . . . . ?
B3 C44 B5 B4 36.5(4) . . . . ?
B3 C44 B5 B9 -2.7(5) . . . . ?
B3 C44 B5 B10 -66.0(5) . . . . ?
B3 B2 B6 B1 100.4(5) . . . . ?
B3 B2 B6 B7 -38.0(4) . . . . ?
B3 B2 B6 B10 62.8(6) . . . . ?
B3 B2 B6 B11 -0.3(6) . . . . ?
B3 B2 B7 B6 137.9(5) . . . . ?
B3 B2 B7 B8 37.5(5) . . . . ?
B3 B2 B7 B11 100.6(5) . . . . ?
B3 B4 B5 C44 -33.8(4) . . . . ?
B3 B4 B5 B1 0.2(6) . . . . ?
B3 B4 B5 B9 101.4(5) . . . . ?
B3 B4 B5 B10 63.7(5) . . . . ?
B3 B4 B8 B7 -37.4(4) . . . . ?
B3 B4 B8 B9 -138.5(4) . . . . ?
B3 B4 B8 B11 -101.0(5) . . . . ?
B3 B4 B9 B5 -100.5(4) . . . . ?
B3 B4 B9 B8 37.4(4) . . . . ?
B3 B4 B9 B10 -63.6(6) . . . . ?
B3 B4 B9 B11 -0.5(6) . . . . ?
B3 B7 B8 B4 37.4(4) . . . . ?
B3 B7 B8 B9 101.2(5) . . . . ?
B3 B7 B8 B11 137.9(5) . . . . ?
B3 B7 B11 B6 101.2(5) . . . . ?
B3 B7 B11 B8 -37.5(4) . . . . ?
B3 B7 B11 B9 -0.6(6) . . . . ?
B3 B7 B11 B10 63.7(6) . . . . ?
B3 B8 B9 B4 -37.2(4) . . . . ?
B3 B8 B9 B5 0.5(6) . . . . ?
B3 B8 B9 B10 63.1(6) . . . . ?
B3 B8 B9 B11 100.5(5) . . . . ?
B3 B8 B11 B6 0.4(6) . . . . ?
B3 B8 B11 B7 37.6(4) . . . . ?
B3 B8 B11 B9 -101.2(5) . . . . ?
B3 B8 B11 B10 -63.4(6) . . . . ?
B4 C44 B1 B2 -104.7(5) . . . . ?
B4 C44 B1 B5 36.7(4) . . . . ?
B4 C44 B1 B6 -65.2(5) . . . . ?
B4 C44 B1 B10 -2.4(6) . . . . ?
B4 C44 B2 B1 105.3(5) . . . . ?
B4 C44 B2 B3 -36.7(4) . . . . ?
B4 C44 B2 B6 66.3(5) . . . . ?
B4 C44 B2 B7 3.3(6) . . . . ?
B4 C44 B3 B2 141.4(5) . . . . ?
B4 C44 B3 B7 102.1(5) . . . . ?
B4 C44 B3 B8 39.7(4) . . . . ?
B4 C44 B5 B1 -141.8(4) . . . . ?
B4 C44 B5 B9 -39.2(4) . . . . ?
B4 C44 B5 B10 -102.5(5) . . . . ?
B4 B3 B7 B2 100.9(5) . . . . ?
B4 B3 B7 B6 63.0(6) . . . . ?
B4 B3 B7 B8 -37.1(4) . . . . ?
B4 B3 B7 B11 0.2(6) . . . . ?
B4 B3 B8 B7 138.2(5) . . . . ?
B4 B3 B8 B9 37.3(4) . . . . ?
B4 B3 B8 B11 100.5(5) . . . . ?
B4 B5 B9 B8 -37.5(4) . . . . ?
B4 B5 B9 B10 -138.3(5) . . . . ?
B4 B5 B9 B11 -101.1(5) . . . . ?
B4 B5 B10 B1 -100.7(5) . . . . ?
B4 B5 B10 B6 -63.3(5) . . . . ?
B4 B5 B10 B9 37.4(4) . . . . ?
B4 B5 B10 B11 0.2(6) . . . . ?
B4 B8 B9 B5 37.7(4) . . . . ?
B4 B8 B9 B10 100.3(5) . . . . ?
B4 B8 B9 B11 137.7(5) . . . . ?
B4 B8 B11 B6 63.8(6) . . . . ?
B4 B8 B11 B7 101.0(5) . . . . ?
B4 B8 B11 B9 -37.8(4) . . . . ?
B4 B8 B11 B10 0.0(6) . . . . ?
B4 B9 B10 B1 0.4(6) . . . . ?
B4 B9 B10 B5 -37.3(4) . . . . ?
B4 B9 B10 B6 63.9(6) . . . . ?
B4 B9 B10 B11 100.8(5) . . . . ?
B4 B9 B11 B6 -63.3(6) . . . . ?
B4 B9 B11 B7 0.7(6) . . . . ?
B4 B9 B11 B8 37.6(4) . . . . ?
B4 B9 B11 B10 -100.4(5) . . . . ?
B5 C44 B1 B2 -141.4(4) . . . . ?
B5 C44 B1 B6 -101.9(5) . . . . ?
B5 C44 B1 B10 -39.1(4) . . . . ?
B5 C44 B2 B1 36.8(4) . . . . ?
B5 C44 B2 B3 -105.3(5) . . . . ?
B5 C44 B2 B6 -2.3(6) . . . . ?
B5 C44 B2 B7 -65.3(5) . . . . ?
B5 C44 B3 B2 104.8(4) . . . . ?
B5 C44 B3 B4 -36.6(4) . . . . ?
B5 C44 B3 B7 65.5(5) . . . . ?
B5 C44 B3 B8 3.0(5) . . . . ?
B5 C44 B4 B3 141.9(4) . . . . ?
B5 C44 B4 B8 101.7(5) . . . . ?
B5 C44 B4 B9 39.2(4) . . . . ?
B5 B1 B2 C44 -34.1(4) . . . . ?
B5 B1 B2 B3 -0.5(6) . . . . ?
B5 B1 B2 B6 100.9(5) . . . . ?
B5 B1 B2 B7 63.4(5) . . . . ?
B5 B1 B6 B2 -100.6(5) . . . . ?
B5 B1 B6 B7 -63.8(6) . . . . ?
B5 B1 B6 B10 37.2(4) . . . . ?
B5 B1 B6 B11 -0.2(6) . . . . ?
B5 B1 B10 B6 -138.2(5) . . . . ?
B5 B1 B10 B9 -37.6(4) . . . . ?
B5 B1 B10 B11 -100.6(5) . . . . ?
B5 B4 B8 B3 101.0(4) . . . . ?
B5 B4 B8 B7 63.7(6) . . . . ?
B5 B4 B8 B9 -37.5(4) . . . . ?
B5 B4 B8 B11 0.1(6) . . . . ?
B5 B4 B9 B8 137.9(4) . . . . ?
B5 B4 B9 B10 36.9(4) . . . . ?
B5 B4 B9 B11 100.0(5) . . . . ?
B5 B9 B10 B1 37.7(4) . . . . ?
B5 B9 B10 B6 101.2(5) . . . . ?
B5 B9 B10 B11 138.1(5) . . . . ?
B5 B9 B11 B6 0.2(6) . . . . ?
B5 B9 B11 B7 64.2(6) . . . . ?
B5 B9 B11 B8 101.1(5) . . . . ?
B5 B9 B11 B10 -36.9(4) . . . . ?
B5 B10 B11 B6 -101.3(5) . . . . ?
B5 B10 B11 B7 -63.7(6) . . . . ?
B5 B10 B11 B8 -0.1(6) . . . . ?
B5 B10 B11 B9 37.4(4) . . . . ?
B6 B1 B2 C44 -135.0(4) . . . . ?
B6 B1 B2 B3 -101.4(5) . . . . ?
B6 B1 B2 B7 -37.5(4) . . . . ?
B6 B1 B5 C44 97.7(5) . . . . ?
B6 B1 B5 B4 63.8(5) . . . . ?
B6 B1 B5 B9 0.4(6) . . . . ?
B6 B1 B5 B10 -37.5(5) . . . . ?
B6 B1 B10 B5 138.2(5) . . . . ?
B6 B1 B10 B9 100.6(5) . . . . ?
B6 B1 B10 B11 37.6(4) . . . . ?
B6 B2 B3 C44 -96.5(5) . . . . ?
B6 B2 B3 B4 -62.3(6) . . . . ?
B6 B2 B3 B7 38.0(5) . . . . ?
B6 B2 B3 B8 0.6(6) . . . . ?
B6 B2 B7 B3 -137.9(5) . . . . ?
B6 B2 B7 B8 -100.4(5) . . . . ?
B6 B2 B7 B11 -37.3(4) . . . . ?
B6 B7 B8 B3 -101.3(5) . . . . ?
B6 B7 B8 B4 -63.9(6) . . . . ?
B6 B7 B8 B9 -0.2(6) . . . . ?
B6 B7 B8 B11 36.6(4) . . . . ?
B6 B7 B11 B8 -138.7(5) . . . . ?
B6 B7 B11 B9 -101.8(5) . . . . ?
B6 B7 B11 B10 -37.6(4) . . . . ?
B6 B10 B11 B7 37.6(4) . . . . ?
B6 B10 B11 B8 101.2(5) . . . . ?
B6 B10 B11 B9 138.8(5) . . . . ?
B7 B2 B3 C44 -134.6(5) . . . . ?
B7 B2 B3 B4 -100.4(5) . . . . ?
B7 B2 B3 B8 -37.5(4) . . . . ?
B7 B2 B6 B1 138.4(5) . . . . ?
B7 B2 B6 B10 100.8(5) . . . . ?
B7 B2 B6 B11 37.7(5) . . . . ?
B7 B3 B4 C44 -96.9(5) . . . . ?
B7 B3 B4 B5 -63.2(5) . . . . ?
B7 B3 B4 B8 37.4(4) . . . . ?
B7 B3 B4 B9 0.2(6) . . . . ?
B7 B3 B8 B4 -138.2(5) . . . . ?
B7 B3 B8 B9 -100.9(5) . . . . ?
B7 B3 B8 B11 -37.7(5) . . . . ?
B7 B6 B10 B1 100.3(5) . . . . ?
B7 B6 B10 B5 62.7(6) . . . . ?
B7 B6 B10 B9 -0.9(6) . . . . ?
B7 B6 B10 B11 -37.6(4) . . . . ?
B7 B6 B11 B8 37.1(5) . . . . ?
B7 B6 B11 B9 100.7(5) . . . . ?
B7 B6 B11 B10 138.1(5) . . . . ?
B7 B8 B9 B4 -100.7(5) . . . . ?
B7 B8 B9 B5 -63.0(5) . . . . ?
B7 B8 B9 B10 -0.4(6) . . . . ?
B7 B8 B9 B11 37.0(4) . . . . ?
B7 B8 B11 B6 -37.2(5) . . . . ?
B7 B8 B11 B9 -138.8(5) . . . . ?
B7 B8 B11 B10 -100.9(5) . . . . ?
B8 B3 B4 C44 -134.3(4) . . . . ?
B8 B3 B4 B5 -100.6(5) . . . . ?
B8 B3 B4 B9 -37.2(4) . . . . ?
B8 B3 B7 B2 138.0(5) . . . . ?
B8 B3 B7 B6 100.2(5) . . . . ?
B8 B3 B7 B11 37.4(5) . . . . ?
B8 B4 B5 C44 -97.6(4) . . . . ?
B8 B4 B5 B1 -63.6(5) . . . . ?
B8 B4 B5 B9 37.6(4) . . . . ?
B8 B4 B5 B10 -0.1(6) . . . . ?
B8 B4 B9 B5 -137.9(4) . . . . ?
B8 B4 B9 B10 -101.0(5) . . . . ?
B8 B4 B9 B11 -37.9(4) . . . . ?
B8 B7 B11 B6 138.7(5) . . . . ?
B8 B7 B11 B9 36.9(4) . . . . ?
B8 B7 B11 B10 101.1(5) . . . . ?
B8 B9 B10 B1 -62.7(6) . . . . ?
B8 B9 B10 B5 -100.4(5) . . . . ?
B8 B9 B10 B6 0.8(6) . . . . ?
B8 B9 B10 B11 37.7(4) . . . . ?
B8 B9 B11 B6 -100.9(5) . . . . ?
B8 B9 B11 B7 -36.9(4) . . . . ?
B8 B9 B11 B10 -138.0(5) . . . . ?
B9 B4 B5 C44 -135.2(4) . . . . ?
B9 B4 B5 B1 -101.2(5) . . . . ?
B9 B4 B5 B10 -37.7(4) . . . . ?
B9 B4 B8 B3 138.5(4) . . . . ?
B9 B4 B8 B7 101.2(5) . . . . ?
B9 B4 B8 B11 37.6(4) . . . . ?
B9 B5 B10 B1 -138.1(5) . . . . ?
B9 B5 B10 B6 -100.7(5) . . . . ?
B9 B5 B10 B11 -37.2(4) . . . . ?
B9 B8 B11 B6 101.6(5) . . . . ?
B9 B8 B11 B7 138.8(5) . . . . ?
B9 B8 B11 B10 37.9(4) . . . . ?
B9 B10 B11 B6 -138.8(5) . . . . ?
B9 B10 B11 B7 -101.2(5) . . . . ?
B9 B10 B11 B8 -37.6(4) . . . . ?
B10 B1 B2 C44 -97.1(4) . . . . ?
B10 B1 B2 B3 -63.6(5) . . . . ?
B10 B1 B2 B6 37.9(4) . . . . ?
B10 B1 B2 B7 0.4(6) . . . . ?
B10 B1 B5 C44 135.2(5) . . . . ?
B10 B1 B5 B4 101.3(5) . . . . ?
B10 B1 B5 B9 37.9(4) . . . . ?
B10 B1 B6 B2 -137.8(5) . . . . ?
B10 B1 B6 B7 -101.1(5) . . . . ?
B10 B1 B6 B11 -37.4(5) . . . . ?
B10 B5 B9 B4 138.3(5) . . . . ?
B10 B5 B9 B8 100.8(5) . . . . ?
B10 B5 B9 B11 37.2(5) . . . . ?
B10 B6 B7 B2 -100.4(5) . . . . ?
B10 B6 B7 B3 -62.7(6) . . . . ?
B10 B6 B7 B8 0.7(6) . . . . ?
B10 B6 B7 B11 37.4(4) . . . . ?
B10 B6 B11 B7 -138.1(5) . . . . ?
B10 B6 B11 B8 -101.0(5) . . . . ?
B10 B6 B11 B9 -37.4(5) . . . . ?
B10 B9 B11 B6 37.2(5) . . . . ?
B10 B9 B11 B7 101.1(5) . . . . ?
B10 B9 B11 B8 138.0(5) . . . . ?
B11 B6 B7 B2 -137.8(5) . . . . ?
B11 B6 B7 B3 -100.1(5) . . . . ?
B11 B6 B7 B8 -36.7(4) . . . . ?
B11 B6 B10 B1 137.9(5) . . . . ?
B11 B6 B10 B5 100.3(5) . . . . ?
B11 B6 B10 B9 36.7(4) . . . . ?
B11 B7 B8 B3 -137.9(5) . . . . ?
B11 B7 B8 B4 -100.5(5) . . . . ?
B11 B7 B8 B9 -36.8(4) . . . . ?
B11 B8 B9 B4 -137.7(5) . . . . ?
B11 B8 B9 B5 -100.0(5) . . . . ?
B11 B8 B9 B10 -37.4(4) . . . . ?
B11 B9 B10 B1 -100.3(5) . . . . ?
B11 B9 B10 B5 -138.1(5) . . . . ?
B11 B9 B10 B6 -36.9(4) . . . . ?
B12 C45 B13 B14 -141.5(4) . . . . ?
B12 C45 B13 B17 -39.5(4) . . . . ?
B12 C45 B13 B18 -101.8(5) . . . . ?
B12 C45 B14 B13 37.0(4) . . . . ?
B12 C45 B14 B15 -105.6(5) . . . . ?
B12 C45 B14 B18 -3.2(6) . . . . ?
B12 C45 B14 B19 -66.0(5) . . . . ?
B12 C45 B15 B14 105.1(4) . . . . ?
B12 C45 B15 B16 -36.3(4) . . . . ?
B12 C45 B15 B19 65.2(6) . . . . ?
B12 C45 B15 B20 2.7(6) . . . . ?
B12 C45 B16 B15 142.3(4) . . . . ?
B12 C45 B16 B20 103.1(5) . . . . ?
B12 C45 B16 B21 39.3(4) . . . . ?
B12 B13 B14 C45 -34.2(4) . . . . ?
B12 B13 B14 B15 -1.2(5) . . . . ?
B12 B13 B14 B18 100.1(5) . . . . ?
B12 B13 B14 B19 62.1(5) . . . . ?
B12 B13 B17 B18 -138.2(5) . . . . ?
B12 B13 B17 B21 -37.1(4) . . . . ?
B12 B13 B17 B22 -100.8(5) . . . . ?
B12 B13 B18 B14 -101.4(5) . . . . ?
B12 B13 B18 B17 37.0(4) . . . . ?
B12 B13 B18 B19 -63.7(6) . . . . ?
B12 B13 B18 B22 -0.3(6) . . . . ?
B12 B16 B20 B15 100.8(5) . . . . ?
B12 B16 B20 B19 62.8(6) . . . . ?
B12 B16 B20 B21 -38.0(4) . . . . ?
B12 B16 B20 B22 -0.7(6) . . . . ?
B12 B16 B21 B17 37.5(4) . . . . ?
B12 B16 B21 B20 137.9(5) . . . . ?
B12 B16 B21 B22 100.7(5) . . . . ?
B12 B17 B18 B13 -37.3(4) . . . . ?
B12 B17 B18 B14 -0.2(6) . . . . ?
B12 B17 B18 B19 63.6(5) . . . . ?
B12 B17 B18 B22 100.9(5) . . . . ?
B12 B17 B21 B16 -37.6(4) . . . . ?
B12 B17 B21 B20 -99.9(5) . . . . ?
B12 B17 B21 B22 -138.0(5) . . . . ?
B12 B17 B22 B18 -100.9(5) . . . . ?
B12 B17 B22 B19 -63.6(6) . . . . ?
B12 B17 B22 B20 -0.7(6) . . . . ?
B12 B17 B22 B21 37.7(4) . . . . ?
B12 B21 B22 B17 -37.3(4) . . . . ?
B12 B21 B22 B18 -0.3(6) . . . . ?
B12 B21 B22 B19 63.1(6) . . . . ?
B12 B21 B22 B20 99.9(5) . . . . ?
B13 C45 B12 B16 142.1(4) . . . . ?
B13 C45 B12 B17 40.0(4) . . . . ?
B13 C45 B12 B21 102.9(5) . . . . ?
B13 C45 B14 B15 -142.6(4) . . . . ?
B13 C45 B14 B18 -40.2(4) . . . . ?
B13 C45 B14 B19 -103.0(5) . . . . ?
B13 C45 B15 B14 36.0(4) . . . . ?
B13 C45 B15 B16 -105.4(4) . . . . ?
B13 C45 B15 B19 -3.9(6) . . . . ?
B13 C45 B15 B20 -66.4(5) . . . . ?
B13 C45 B16 B12 -36.5(4) . . . . ?
B13 C45 B16 B15 105.7(5) . . . . ?
B13 C45 B16 B20 66.6(6) . . . . ?
B13 C45 B16 B21 2.8(6) . . . . ?
B13 B12 B16 C45 33.4(4) . . . . ?
B13 B12 B16 B15 -0.2(5) . . . . ?
B13 B12 B16 B20 -63.6(5) . . . . ?
B13 B12 B16 B21 -102.0(5) . . . . ?
B13 B12 B17 B18 37.4(4) . . . . ?
B13 B12 B17 B21 138.7(5) . . . . ?
B13 B12 B17 B22 101.0(5) . . . . ?
B13 B12 B21 B16 100.1(5) . . . . ?
B13 B12 B21 B17 -37.4(4) . . . . ?
B13 B12 B21 B20 63.1(5) . . . . ?
B13 B12 B21 B22 0.1(6) . . . . ?
B13 B14 B15 C45 -32.9(4) . . . . ?
B13 B14 B15 B16 1.1(5) . . . . ?
B13 B14 B15 B19 101.7(5) . . . . ?
B13 B14 B15 B20 64.0(5) . . . . ?
B13 B14 B18 B17 -37.2(4) . . . . ?
B13 B14 B18 B19 -138.0(5) . . . . ?
B13 B14 B18 B22 -100.7(5) . . . . ?
B13 B14 B19 B15 -100.2(5) . . . . ?
B13 B14 B19 B18 38.0(4) . . . . ?
B13 B14 B19 B20 -62.8(6) . . . . ?
B13 B14 B19 B22 0.8(6) . . . . ?
B13 B17 B18 B14 37.2(4) . . . . ?
B13 B17 B18 B19 100.9(4) . . . . ?
B13 B17 B18 B22 138.3(4) . . . . ?
B13 B17 B21 B12 37.0(4) . . . . ?
B13 B17 B21 B16 -0.6(6) . . . . ?
B13 B17 B21 B20 -62.9(6) . . . . ?
B13 B17 B21 B22 -100.9(5) . . . . ?
B13 B17 B22 B18 -37.4(4) . . . . ?
B13 B17 B22 B19 -0.1(6) . . . . ?
B13 B17 B22 B20 62.8(6) . . . . ?
B13 B17 B22 B21 101.1(5) . . . . ?
B13 B18 B19 B14 -37.6(4) . . . . ?
B13 B18 B19 B15 -0.3(7) . . . . ?
B13 B18 B19 B20 62.7(6) . . . . ?
B13 B18 B19 B22 100.7(5) . . . . ?
B13 B18 B22 B17 37.3(4) . . . . ?
B13 B18 B22 B19 -100.9(5) . . . . ?
B13 B18 B22 B20 -63.3(6) . . . . ?
B13 B18 B22 B21 0.4(6) . . . . ?
B14 C45 B12 B13 -36.9(4) . . . . ?
B14 C45 B12 B16 105.2(5) . . . . ?
B14 C45 B12 B17 3.1(6) . . . . ?
B14 C45 B12 B21 66.0(5) . . . . ?
B14 C45 B13 B12 141.5(4) . . . . ?
B14 C45 B13 B17 102.0(5) . . . . ?
B14 C45 B13 B18 39.7(4) . . . . ?
B14 C45 B15 B16 -141.4(4) . . . . ?
B14 C45 B15 B19 -39.8(4) . . . . ?
B14 C45 B15 B20 -102.4(5) . . . . ?
B14 C45 B16 B12 -105.2(5) . . . . ?
B14 C45 B16 B15 37.1(4) . . . . ?
B14 C45 B16 B20 -2.1(6) . . . . ?
B14 C45 B16 B21 -65.9(6) . . . . ?
B14 B13 B17 B12 101.4(5) . . . . ?
B14 B13 B17 B18 -36.9(4) . . . . ?
B14 B13 B17 B21 64.3(6) . . . . ?
B14 B13 B17 B22 0.6(5) . . . . ?
B14 B13 B18 B17 138.4(5) . . . . ?
B14 B13 B18 B19 37.7(5) . . . . ?
B14 B13 B18 B22 101.1(5) . . . . ?
B14 B15 B16 C45 -34.1(4) . . . . ?
B14 B15 B16 B12 -0.6(5) . . . . ?
B14 B15 B16 B20 101.1(5) . . . . ?
B14 B15 B16 B21 63.4(5) . . . . ?
B14 B15 B19 B18 -36.9(5) . . . . ?
B14 B15 B19 B20 -137.9(5) . . . . ?
B14 B15 B19 B22 -100.4(5) . . . . ?
B14 B15 B20 B16 -100.1(5) . . . . ?
B14 B15 B20 B19 37.6(5) . . . . ?
B14 B15 B20 B21 -63.2(6) . . . . ?
B14 B15 B20 B22 0.1(6) . . . . ?
B14 B18 B19 B15 37.3(5) . . . . ?
B14 B18 B19 B20 100.3(5) . . . . ?
B14 B18 B19 B22 138.3(5) . . . . ?
B14 B18 B22 B17 100.7(5) . . . . ?
B14 B18 B22 B19 -37.5(4) . . . . ?
B14 B18 B22 B20 0.1(7) . . . . ?
B14 B18 B22 B21 63.8(6) . . . . ?
B14 B19 B20 B15 -37.6(4) . . . . ?
B14 B19 B20 B16 0.6(6) . . . . ?
B14 B19 B20 B21 63.8(6) . . . . ?
B14 B19 B20 B22 100.6(5) . . . . ?
B14 B19 B22 B17 -0.4(6) . . . . ?
B14 B19 B22 B18 36.8(4) . . . . ?
B14 B19 B22 B20 -100.7(5) . . . . ?
B14 B19 B22 B21 -63.6(6) . . . . ?
B15 C45 B12 B13 -105.7(4) . . . . ?
B15 C45 B12 B16 36.4(4) . . . . ?
B15 C45 B12 B17 -65.6(5) . . . . ?
B15 C45 B12 B21 -2.7(6) . . . . ?
B15 C45 B13 B12 105.5(5) . . . . ?
B15 C45 B13 B14 -36.0(4) . . . . ?
B15 C45 B13 B17 66.0(6) . . . . ?
B15 C45 B13 B18 3.7(6) . . . . ?
B15 C45 B14 B13 142.6(4) . . . . ?
B15 C45 B14 B18 102.4(5) . . . . ?
B15 C45 B14 B19 39.6(4) . . . . ?
B15 C45 B16 B12 -142.3(4) . . . . ?
B15 C45 B16 B20 -39.2(4) . . . . ?
B15 C45 B16 B21 -102.9(5) . . . . ?
B15 B14 B18 B13 100.6(5) . . . . ?
B15 B14 B18 B17 63.5(6) . . . . ?
B15 B14 B18 B19 -37.3(5) . . . . ?
B15 B14 B18 B22 0.0(6) . . . . ?
B15 B14 B19 B18 138.2(5) . . . . ?
B15 B14 B19 B20 37.4(5) . . . . ?
B15 B14 B19 B22 100.9(5) . . . . ?
B15 B16 B20 B19 -38.0(4) . . . . ?
B15 B16 B20 B21 -138.7(5) . . . . ?
B15 B16 B20 B22 -101.5(5) . . . . ?
B15 B16 B21 B12 -100.8(5) . . . . ?
B15 B16 B21 B17 -63.4(6) . . . . ?
B15 B16 B21 B20 37.1(4) . . . . ?
B15 B16 B21 B22 -0.2(6) . . . . ?
B15 B19 B20 B16 38.1(4) . . . . ?
B15 B19 B20 B21 101.3(5) . . . . ?
B15 B19 B20 B22 138.1(5) . . . . ?
B15 B19 B22 B17 63.1(6) . . . . ?
B15 B19 B22 B18 100.3(5) . . . . ?
B15 B19 B22 B20 -37.3(4) . . . . ?
B15 B19 B22 B21 -0.2(6) . . . . ?
B15 B20 B21 B12 0.0(6) . . . . ?
B15 B20 B21 B16 -37.3(4) . . . . ?
B15 B20 B21 B17 62.6(5) . . . . ?
B15 B20 B21 B22 100.7(5) . . . . ?
B15 B20 B22 B17 -63.2(6) . . . . ?
B15 B20 B22 B18 -0.1(7) . . . . ?
B15 B20 B22 B19 37.6(5) . . . . ?
B15 B20 B22 B21 -101.2(5) . . . . ?
B16 C45 B12 B13 -142.1(4) . . . . ?
B16 C45 B12 B17 -102.0(5) . . . . ?
B16 C45 B12 B21 -39.2(4) . . . . ?
B16 C45 B13 B12 36.4(4) . . . . ?
B16 C45 B13 B14 -105.1(5) . . . . ?
B16 C45 B13 B17 -3.1(6) . . . . ?
B16 C45 B13 B18 -65.4(6) . . . . ?
B16 C45 B14 B13 105.5(5) . . . . ?
B16 C45 B14 B15 -37.2(4) . . . . ?
B16 C45 B14 B18 65.2(5) . . . . ?
B16 C45 B14 B19 2.4(6) . . . . ?
B16 C45 B15 B14 141.4(4) . . . . ?
B16 C45 B15 B19 101.5(5) . . . . ?
B16 C45 B15 B20 39.0(4) . . . . ?
B16 B12 B13 C45 -33.6(4) . . . . ?
B16 B12 B13 B14 0.8(5) . . . . ?
B16 B12 B13 B17 100.9(5) . . . . ?
B16 B12 B13 B18 63.7(5) . . . . ?
B16 B12 B17 B13 -100.7(5) . . . . ?
B16 B12 B17 B18 -63.4(6) . . . . ?
B16 B12 B17 B21 37.9(4) . . . . ?
B16 B12 B17 B22 0.3(6) . . . . ?
B16 B12 B21 B17 -137.5(5) . . . . ?
B16 B12 B21 B20 -37.0(4) . . . . ?
B16 B12 B21 B22 -100.0(5) . . . . ?
B16 B15 B19 B14 100.4(5) . . . . ?
B16 B15 B19 B18 63.5(6) . . . . ?
B16 B15 B19 B20 -37.5(4) . . . . ?
B16 B15 B19 B22 0.0(6) . . . . ?
B16 B15 B20 B19 137.7(5) . . . . ?
B16 B15 B20 B21 36.9(4) . . . . ?
B16 B15 B20 B22 100.2(5) . . . . ?
B16 B20 B21 B12 37.3(4) . . . . ?
B16 B20 B21 B17 99.9(5) . . . . ?
B16 B20 B21 B22 138.0(5) . . . . ?
B16 B20 B22 B17 0.8(7) . . . . ?
B16 B20 B22 B18 63.9(6) . . . . ?
B16 B20 B22 B19 101.6(5) . . . . ?
B16 B20 B22 B21 -37.2(4) . . . . ?
B16 B21 B22 B17 -100.2(5) . . . . ?
B16 B21 B22 B18 -63.2(6) . . . . ?
B16 B21 B22 B19 0.2(6) . . . . ?
B16 B21 B22 B20 37.0(4) . . . . ?
B17 B12 B13 C45 -134.5(5) . . . . ?
B17 B12 B13 B14 -100.1(5) . . . . ?
B17 B12 B13 B18 -37.2(4) . . . . ?
B17 B12 B16 C45 97.3(5) . . . . ?
B17 B12 B16 B15 63.7(5) . . . . ?
B17 B12 B16 B20 0.3(6) . . . . ?
B17 B12 B16 B21 -38.1(4) . . . . ?
B17 B12 B21 B16 137.5(5) . . . . ?
B17 B12 B21 B20 100.5(5) . . . . ?
B17 B12 B21 B22 37.5(4) . . . . ?
B17 B13 B14 C45 -97.2(4) . . . . ?
B17 B13 B14 B15 -64.1(5) . . . . ?
B17 B13 B14 B18 37.1(4) . . . . ?
B17 B13 B14 B19 -0.8(6) . . . . ?
B17 B13 B18 B14 -138.4(5) . . . . ?
B17 B13 B18 B19 -100.7(5) . . . . ?
B17 B13 B18 B22 -37.3(4) . . . . ?
B17 B18 B19 B14 -101.0(5) . . . . ?
B17 B18 B19 B15 -63.6(6) . . . . ?
B17 B18 B19 B20 -0.7(6) . . . . ?
B17 B18 B19 B22 37.4(4) . . . . ?
B17 B18 B22 B19 -138.2(4) . . . . ?
B17 B18 B22 B20 -100.6(5) . . . . ?
B17 B18 B22 B21 -36.9(4) . . . . ?
B17 B21 B22 B18 37.0(4) . . . . ?
B17 B21 B22 B19 100.4(5) . . . . ?
B17 B21 B22 B20 137.1(5) . . . . ?
B18 B13 B14 C45 -134.3(5) . . . . ?
B18 B13 B14 B15 -101.2(5) . . . . ?
B18 B13 B14 B19 -37.9(4) . . . . ?
B18 B13 B17 B12 138.2(5) . . . . ?
B18 B13 B17 B21 101.1(5) . . . . ?
B18 B13 B17 B22 37.4(4) . . . . ?
B18 B14 B15 C45 -96.9(5) . . . . ?
B18 B14 B15 B16 -63.0(5) . . . . ?
B18 B14 B15 B19 37.6(5) . . . . ?
B18 B14 B15 B20 0.0(6) . . . . ?
B18 B14 B19 B15 -138.2(5) . . . . ?
B18 B14 B19 B20 -100.8(5) . . . . ?
B18 B14 B19 B22 -37.2(4) . . . . ?
B18 B17 B21 B12 100.7(5) . . . . ?
B18 B17 B21 B16 63.1(5) . . . . ?
B18 B17 B21 B20 0.8(5) . . . . ?
B18 B17 B21 B22 -37.3(4) . . . . ?
B18 B17 B22 B19 37.3(4) . . . . ?
B18 B17 B22 B20 100.2(5) . . . . ?
B18 B17 B22 B21 138.5(4) . . . . ?
B18 B19 B20 B15 -100.1(5) . . . . ?
B18 B19 B20 B16 -62.0(6) . . . . ?
B18 B19 B20 B21 1.2(6) . . . . ?
B18 B19 B20 B22 38.0(4) . . . . ?
B18 B19 B22 B17 -37.2(4) . . . . ?
B18 B19 B22 B20 -137.6(5) . . . . ?
B18 B19 B22 B21 -100.4(5) . . . . ?
B19 B14 B15 C45 -134.5(5) . . . . ?
B19 B14 B15 B16 -100.6(5) . . . . ?
B19 B14 B15 B20 -37.7(5) . . . . ?
B19 B14 B18 B13 138.0(5) . . . . ?
B19 B14 B18 B17 100.8(5) . . . . ?
B19 B14 B18 B22 37.3(5) . . . . ?
B19 B15 B16 C45 -97.5(5) . . . . ?
B19 B15 B16 B12 -63.9(5) . . . . ?
B19 B15 B16 B20 37.7(4) . . . . ?
B19 B15 B16 B21 0.1(6) . . . . ?
B19 B15 B20 B16 -137.7(5) . . . . ?
B19 B15 B20 B21 -100.8(5) . . . . ?
B19 B15 B20 B22 -37.5(5) . . . . ?
B19 B18 B22 B17 138.2(4) . . . . ?
B19 B18 B22 B20 37.6(4) . . . . ?
B19 B18 B22 B21 101.3(5) . . . . ?
B19 B20 B21 B12 -63.8(5) . . . . ?
B19 B20 B21 B16 -101.1(5) . . . . ?
B19 B20 B21 B17 -1.2(6) . . . . ?
B19 B20 B21 B22 36.9(4) . . . . ?
B19 B20 B22 B17 -100.7(5) . . . . ?
B19 B20 B22 B18 -37.7(5) . . . . ?
B19 B20 B22 B21 -138.8(5) . . . . ?
B20 B15 B16 C45 -135.2(4) . . . . ?
B20 B15 B16 B12 -101.6(4) . . . . ?
B20 B15 B16 B21 -37.7(4) . . . . ?
B20 B15 B19 B14 137.9(5) . . . . ?
B20 B15 B19 B18 101.0(5) . . . . ?
B20 B15 B19 B22 37.5(5) . . . . ?
B20 B16 B21 B12 -137.9(5) . . . . ?
B20 B16 B21 B17 -100.4(5) . . . . ?
B20 B16 B21 B22 -37.2(4) . . . . ?
B20 B19 B22 B17 100.3(5) . . . . ?
B20 B19 B22 B18 137.6(5) . . . . ?
B20 B19 B22 B21 37.1(4) . . . . ?
B20 B21 B22 B17 -137.1(5) . . . . ?
B20 B21 B22 B18 -100.2(5) . . . . ?
B20 B21 B22 B19 -36.8(4) . . . . ?
B21 B12 B13 C45 -97.2(5) . . . . ?
B21 B12 B13 B14 -62.8(5) . . . . ?
B21 B12 B13 B17 37.3(4) . . . . ?
B21 B12 B13 B18 0.1(6) . . . . ?
B21 B12 B16 C45 135.4(4) . . . . ?
B21 B12 B16 B15 101.8(5) . . . . ?
B21 B12 B16 B20 38.3(5) . . . . ?
B21 B12 B17 B13 -138.7(5) . . . . ?
B21 B12 B17 B18 -101.3(5) . . . . ?
B21 B12 B17 B22 -37.7(5) . . . . ?
B21 B16 B20 B15 138.7(5) . . . . ?
B21 B16 B20 B19 100.8(5) . . . . ?
B21 B16 B20 B22 37.3(4) . . . . ?
B21 B17 B18 B13 -101.0(4) . . . . ?
B21 B17 B18 B14 -63.8(6) . . . . ?
B21 B17 B18 B19 -0.1(6) . . . . ?
B21 B17 B18 B22 37.2(4) . . . . ?
B21 B17 B22 B18 -138.5(4) . . . . ?
B21 B17 B22 B19 -101.3(5) . . . . ?
B21 B17 B22 B20 -38.4(5) . . . . ?
B21 B20 B22 B17 38.1(4) . . . . ?
B21 B20 B22 B18 101.1(5) . . . . ?
B21 B20 B22 B19 138.8(5) . . . . ?
B22 B17 B18 B13 -138.3(4) . . . . ?
B22 B17 B18 B14 -101.1(5) . . . . ?
B22 B17 B18 B19 -37.3(4) . . . . ?
B22 B17 B21 B12 138.0(5) . . . . ?
B22 B17 B21 B16 100.4(5) . . . . ?
B22 B17 B21 B20 38.1(4) . . . . ?
B22 B18 B19 B14 -138.3(5) . . . . ?
B22 B18 B19 B15 -101.0(5) . . . . ?
B22 B18 B19 B20 -38.0(4) . . . . ?
B22 B19 B20 B15 -138.1(5) . . . . ?
B22 B19 B20 B16 -100.0(5) . . . . ?
B22 B19 B20 B21 -36.8(4) . . . . ?
B22 B20 B21 B12 -100.8(5) . . . . ?
B22 B20 B21 B16 -138.0(5) . . . . ?
B22 B20 B21 B17 -38.2(4) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_211115yhb_0m
_database_code_depnum_ccdc_archive 'CCDC 2168889'
loop_
_audit_author_name
_audit_author_address
'Haibo Yao' 'Guangxi minzu university'
_audit_update_record             
;
2022-04-26 deposited with the CCDC.	2026-02-11 downloaded from the CCDC.
;
_audit_creation_date             2021-11-16
_audit_creation_method           
;
Olex2 1.5
(compiled 2021.10.07 svn.r9718050b for OlexSys, GUI svn.r6410)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C53 H92 B22 N6 Pt'
_chemical_formula_sum            'C53 H92 B22 N6 Pt'
_chemical_formula_weight         1246.23
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0137 0.0067 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0070 0.0029 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0241 0.0134 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -5.3886 5.5592 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   12.9019(13)
_cell_length_b                   15.2663(13)
_cell_length_c                   19.9007(17)
_cell_angle_alpha                82.301(5)
_cell_angle_beta                 84.738(6)
_cell_angle_gamma                86.187(6)
_cell_volume                     3862.2(6)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    9790
_cell_measurement_temperature    213.01
_cell_measurement_theta_max      54.745
_cell_measurement_theta_min      3.826
_shelx_estimated_absorpt_T_max   0.886
_shelx_estimated_absorpt_T_min   0.865
_exptl_absorpt_coefficient_mu    2.487
_exptl_absorpt_correction_T_max  0.7508
_exptl_absorpt_correction_T_min  0.5423
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1245 before and 0.0810 after correction.
The Ratio of minimum to maximum transmission is 0.7223.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.072
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             1280
_exptl_crystal_size_max          0.06
_exptl_crystal_size_mid          0.05
_exptl_crystal_size_min          0.05
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0673
_diffrn_reflns_av_unetI/netI     0.0590
_diffrn_reflns_Laue_measured_fraction_full 0.994
_diffrn_reflns_Laue_measured_fraction_max 0.991
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_number            54436
_diffrn_reflns_point_group_measured_fraction_full 0.994
_diffrn_reflns_point_group_measured_fraction_max 0.991
_diffrn_reflns_theta_full        53.594
_diffrn_reflns_theta_max         55.033
_diffrn_reflns_theta_min         2.997
_diffrn_ambient_temperature      213.01
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.991
_diffrn_measurement_device_type  'Bruker D8 Venture'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           GaK\a
_diffrn_radiation_wavelength     1.34139
_diffrn_source                   ?
_diffrn_source_current           2.86
_diffrn_source_power             0.1995708
_diffrn_source_voltage           69.78
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                11344
_reflns_number_total             14633
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v8.37A (Bruker, 2015)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT v8.37A (Bruker, 2015)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         1.210
_refine_diff_density_min         -2.088
_refine_diff_density_rms         0.140
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.011
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           fullcycle
_refine_ls_number_parameters     741
_refine_ls_number_reflns         14633
_refine_ls_number_restraints     172
_refine_ls_R_factor_all          0.0924
_refine_ls_R_factor_gt           0.0743
_refine_ls_restrained_S_all      1.400
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1480P)²+5.5690P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2042
_refine_ls_wR_factor_ref         0.2236
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Restrained distances
 C44-C43 = C45-C44 = C46-C45 = C47-C46
 1.53 with sigma of 0.01
 C47-C48 = C48-C49
 1.53 with sigma of 0.01
 C47-C49
 2.44 with sigma of 0.02
 C46-C49
 4.5 with sigma of 0.02
 C45-C47
 2.44 with sigma of 0.02
 C50-C49
 1.53 with sigma of 0.01
 C51-C52
 1.53 with sigma of 0.01
 C47-C48 = C48-C49 = C49-C50 = C51-C50
 1.53 with sigma of 0.01
 C53-C52
 1.53 with sigma of 0.01
 C51-C53
 2.44 with sigma of 0.02
 C46-C44
 2.44 with sigma of 0.01
 C50-C52
 2.44 with sigma of 0.02
 C39-C38
 1.53 with sigma of 0.01
 H32A-H51B_$1 = H50A-H53C
 2.05 with sigma of 0.01
 C38-C37
 1.53 with sigma of 0.01
 H51B-H32B_$1
 2.05 with sigma of 0.02
 C46-C48
 2.44 with sigma of 0.02
 C51_$1-C52_$1
 3 with sigma of 0.02
3. Rigid bond restraints
 C39, C40
 with sigma for 1-2 distances of 0.005 and sigma for 1-3 distances of 0.005
 C27, C28
 with sigma for 1-2 distances of 0.005 and sigma for 1-3 distances of 0.005
4. Uiso/Uaniso restraints and constraints
C43 \\sim C44 \\sim C45 \\sim C47: within 2A with sigma of 0.01 and sigma for
terminal atoms of 0.02 within 2A
C44 \\sim C45 \\sim C46 \\sim C47: within 2A with sigma of 0.01 and sigma for
terminal atoms of 0.02 within 2A
C44: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
C47 \\sim C48 \\sim C49: within 2A with sigma of 0.01 and sigma for terminal
atoms of 0.02 within 2A
C47 \\sim C48 \\sim C49 \\sim C50 \\sim C51 \\sim C52: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
N4 \\sim C42 \\sim C43 \\sim C44 \\sim C45 \\sim C46 \\sim C47 \\sim C48 \\sim
C49 \\sim C50 \\sim C51 \\sim C52: within 2A with sigma of 0.01 and sigma for
terminal atoms of 0.02 within 2A
C52 \\sim C53: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
C42 \\sim C43 \\sim C44 \\sim C45 \\sim C46 \\sim C47 \\sim C48 \\sim C49 \\sim
C50 \\sim C51 \\sim C52 \\sim C53: within 2A with sigma of 0.005 and sigma for
terminal atoms of 0.01 within 2A
C32 \\sim C33 \\sim C34 \\sim C35 \\sim C36 \\sim C37 \\sim C38 \\sim C39 \\sim
C40 \\sim C41: within 2A with sigma of 0.005 and sigma for terminal atoms of
0.01 within 2A
C28 \\sim C24 \\sim C29 \\sim C27: within 2A with sigma of 0.005 and sigma for
terminal atoms of 0.01 within 2A
5.a Secondary CH2 refined with riding coordinates:
 C13(H13A,H13B), C14(H14A,H14B), C15(H15A,H15B), C30(H30A,H30B), C31(H31A,
 H31B), C32(H32A,H32B), C33(H33A,H33B), C34(H34A,H34B), C35(H35A,H35B),
 C36(H36A,H36B), C37(H37A,H37B), C38(H38A,H38B), C39(H39A,H39B), C40(H40A,H40B),
  C42(H42A,H42B), C43(H43A,H43B), C44(H44A,H44B), C45(H45A,H45B), C46(H46A,
 H46B), C47(H47A,H47B), C48(H48A,H48B), C49(H49A,H49B), C50(H50A,H50B),
 C51(H51A,H51B), C52(H52A,H52B)
5.b Aromatic/amide H refined with riding coordinates:
 C1(H1), C2(H2), C4(H4), C7(H7), C9(H9), C10(H10), C19(H19), C20(H20),
 C21(H21), C22(H22), C26(H26), C27(H27), C28(H28), C29(H29)
5.c Idealised Me refined as rotating group:
 C41(H41A,H41B,H41C), C53(H53A,H53B,H53C)
5.d Boron cage BH refined with riding coordinates:
 B1(H1A), B2(H2A), B3(H3), B4(H4A), B5(H5), B6(H6), B7(H7A), B8(H8), B9(H9A),
 B10(H10A), B11(H11), B12(H12), B13(H13), B14(H14), B15(H15), B16(H16),
 B17(H17), B18(H18), B19(H19A), B20(H20A), B21(H21A), B22(H22A)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.238580 0.745420 0.327380 0.05712(14) Uani 1 1 d . . . . .
N1 N 0.313260 0.700750 0.414110 0.0558(13) Uani 1 1 d . . . . .
N2 N 0.166440 0.626950 0.357270 0.0527(12) Uani 1 1 d . . . . .
N3 N 0.270430 0.936350 0.320220 0.0641(15) Uani 1 1 d . . . . .
N4 N 0.406290 0.870040 0.274170 0.0635(14) Uani 1 1 d . U . . .
N5 N 0.084030 0.843430 0.242590 0.0697(16) Uani 1 1 d . . . . .
N6 N 0.180880 0.756590 0.185580 0.0731(17) Uani 1 1 d . . . . .
C1 C 0.375820 0.742550 0.445930 0.0635(17) Uani 1 1 d . . . . .
H1 H 0.396488 0.798498 0.425470 0.076 Uiso 1 1 calc R U . . .
C2 C 0.412200 0.709600 0.506520 0.0634(17) Uani 1 1 d . . . . .
H2 H 0.458651 0.742029 0.525779 0.076 Uiso 1 1 calc R U . . .
C3 C 0.383030 0.631570 0.539400 0.0536(14) Uani 1 1 d . . . . .
C4 C 0.319100 0.585050 0.507410 0.0552(15) Uani 1 1 d . . . . .
H4 H 0.298674 0.529183 0.528221 0.066 Uiso 1 1 calc R U . . .
C5 C 0.284320 0.619210 0.445000 0.0551(15) Uani 1 1 d . . . . .
C6 C 0.207700 0.575580 0.411330 0.0550(15) Uani 1 1 d . . . . .
C7 C 0.178050 0.492640 0.430550 0.0554(15) Uani 1 1 d . . . . .
H7 H 0.207122 0.458646 0.467872 0.066 Uiso 1 1 calc R U . . .
C8 C 0.105980 0.455900 0.396970 0.0546(15) Uani 1 1 d . . . . .
C9 C 0.057310 0.511580 0.347010 0.0633(17) Uani 1 1 d . . . . .
H9 H 0.002270 0.492356 0.325841 0.076 Uiso 1 1 calc R U . . .
C10 C 0.091720 0.596100 0.329080 0.0624(17) Uani 1 1 d . . . . .
H10 H 0.059383 0.633341 0.294638 0.075 Uiso 1 1 calc R U . . .
C11 C 0.416100 0.594480 0.609200 0.0563(15) Uani 1 1 d . . . . .
C12 C 0.076830 0.360670 0.416180 0.0556(15) Uani 1 1 d . . . . .
C13 C 0.171610 0.954090 0.359890 0.0696(19) Uani 1 1 d . . . . .
H13A H 0.177826 1.007009 0.381881 0.084 Uiso 1 1 calc R U . . .
H13B H 0.160973 0.904422 0.396019 0.084 Uiso 1 1 calc R U . . .
C14 C 0.069450 0.968810 0.317890 0.076(2) Uani 1 1 d . . . . .
H14A H 0.014306 1.000011 0.344189 0.091 Uiso 1 1 calc R U . . .
H14B H 0.086093 1.006794 0.275028 0.091 Uiso 1 1 calc R U . . .
C15 C 0.028540 0.883920 0.302120 0.072(2) Uani 1 1 d . . . . .
H15A H 0.031584 0.840052 0.342727 0.086 Uiso 1 1 calc R U . . .
H15B H -0.045045 0.895373 0.293573 0.086 Uiso 1 1 calc R U . . .
C16 C 0.310700 0.857730 0.306160 0.0551(15) Uani 1 1 d . . . . .
C17 C 0.161830 0.782120 0.246080 0.0606(17) Uani 1 1 d . . . . .
C18 C 0.425050 0.961310 0.268370 0.0662(19) Uani 1 1 d . . . . .
C19 C 0.516970 1.005160 0.239960 0.078(2) Uani 1 1 d . . . . .
H19 H 0.577279 0.975709 0.221801 0.093 Uiso 1 1 calc R U . . .
C20 C 0.506990 1.097790 0.242240 0.088(3) Uani 1 1 d . . . . .
H20 H 0.563738 1.131668 0.224339 0.105 Uiso 1 1 calc R U . . .
C21 C 0.417280 1.141770 0.269680 0.086(3) Uani 1 1 d . . . . .
H21 H 0.414398 1.203586 0.268873 0.103 Uiso 1 1 calc R U . . .
C22 C 0.334260 1.094610 0.297530 0.077(2) Uani 1 1 d . . . . .
H22 H 0.274392 1.122551 0.317617 0.093 Uiso 1 1 calc R U . . .
C23 C 0.341370 1.001750 0.295140 0.0663(18) Uani 1 1 d . . . . .
C24 C 0.052840 0.862090 0.174960 0.095(2) Uani 1 1 d . U . . .
C25 C 0.115830 0.803520 0.138780 0.084(2) Uani 1 1 d . . . . .
C26 C 0.110990 0.805530 0.068780 0.106(3) Uani 1 1 d . . . . .
H26 H 0.154375 0.767158 0.043963 0.127 Uiso 1 1 calc R U . . .
C27 C 0.041710 0.864600 0.037750 0.123(3) Uani 1 1 d . U . . .
H27 H 0.042156 0.871078 -0.009917 0.148 Uiso 1 1 calc R U . . .
C28 C -0.032930 0.917980 0.075920 0.120(2) Uani 1 1 d . U . . .
H28 H -0.086385 0.952408 0.054242 0.144 Uiso 1 1 calc R U . . .
C29 C -0.023890 0.917570 0.149370 0.110(2) Uani 1 1 d . U . . .
H29 H -0.068025 0.953094 0.176173 0.131 Uiso 1 1 calc R U . . .
C30 C 0.253650 0.681940 0.167950 0.081(2) Uani 1 1 d . . . . .
H30A H 0.300791 0.665046 0.203989 0.097 Uiso 1 1 calc R U . . .
H30B H 0.295745 0.699930 0.125407 0.097 Uiso 1 1 calc R U . . .
C31 C 0.189470 0.602470 0.159790 0.111(4) Uani 1 1 d . . . . .
H31A H 0.139351 0.591779 0.199690 0.133 Uiso 1 1 calc R U . . .
H31B H 0.149783 0.617841 0.119767 0.133 Uiso 1 1 calc R U . . .
C32 C 0.255540 0.517760 0.151960 0.115(3) Uani 1 1 d . U . . .
H32A H 0.297545 0.526533 0.108246 0.138 Uiso 1 1 calc DR U . . .
H32B H 0.303978 0.509108 0.187738 0.138 Uiso 1 1 calc R U . . .
C33 C 0.203420 0.439130 0.154650 0.120(2) Uani 1 1 d . U . . .
H33A H 0.146892 0.451984 0.124488 0.145 Uiso 1 1 calc R U . . .
H33B H 0.170510 0.426320 0.201005 0.145 Uiso 1 1 calc R U . . .
C34 C 0.258920 0.357480 0.137600 0.126(2) Uani 1 1 d . U . . .
H34A H 0.319492 0.346725 0.164500 0.151 Uiso 1 1 calc R U . . .
H34B H 0.285502 0.367392 0.089619 0.151 Uiso 1 1 calc R U . . .
C35 C 0.198320 0.272650 0.148440 0.130(2) Uani 1 1 d . U . . .
H35A H 0.182386 0.255260 0.197321 0.157 Uiso 1 1 calc R U . . .
H35B H 0.132122 0.284629 0.127512 0.157 Uiso 1 1 calc R U . . .
C36 C 0.259260 0.196950 0.118050 0.134(3) Uani 1 1 d . U . . .
H36A H 0.328872 0.190390 0.134713 0.161 Uiso 1 1 calc R U . . .
H36B H 0.267905 0.212047 0.068496 0.161 Uiso 1 1 calc R U . . .
C37 C 0.207870 0.108130 0.134820 0.141(3) Uani 1 1 d D U . . .
H37A H 0.143565 0.111993 0.111669 0.169 Uiso 1 1 calc R U . . .
H37B H 0.188373 0.098144 0.183893 0.169 Uiso 1 1 calc R U . . .
C38 C 0.276920 0.026640 0.114350 0.147(3) Uani 1 1 d D U . . .
H38A H 0.343827 0.024084 0.134399 0.177 Uiso 1 1 calc R U . . .
H38B H 0.242062 -0.027974 0.131639 0.177 Uiso 1 1 calc R U . . .
C39 C 0.295030 0.034510 0.038180 0.157(3) Uani 1 1 d D U . . .
H39A H 0.339420 0.083878 0.021685 0.189 Uiso 1 1 calc R U . . .
H39B H 0.228288 0.046905 0.017976 0.189 Uiso 1 1 calc R U . . .
C40 C 0.353050 -0.060480 0.013970 0.164(3) Uani 1 1 d . U . . .
H40A H 0.426432 -0.068196 0.023699 0.197 Uiso 1 1 calc R U . . .
H40B H 0.315956 -0.112767 0.034473 0.197 Uiso 1 1 calc R U . . .
C41 C 0.339970 -0.037980 -0.063730 0.185(5) Uani 1 1 d . U . . .
H41A H 0.379251 -0.082032 -0.088081 0.278 Uiso 1 1 calc R U . . .
H41B H 0.365713 0.020000 -0.079954 0.278 Uiso 1 1 calc R U . . .
H41C H 0.266815 -0.037923 -0.071451 0.278 Uiso 1 1 calc R U . . .
C42 C 0.474530 0.801770 0.243190 0.0810(19) Uani 1 1 d . U . . .
H42A H 0.449051 0.743104 0.259945 0.097 Uiso 1 1 calc R U . . .
H42B H 0.545385 0.803256 0.256871 0.097 Uiso 1 1 calc R U . . .
C43 C 0.476900 0.816650 0.167400 0.103(2) Uani 1 1 d D U . . .
H43A H 0.502330 0.875448 0.151075 0.124 Uiso 1 1 calc R U . . .
H43B H 0.405669 0.815964 0.154172 0.124 Uiso 1 1 calc R U . . .
C44 C 0.545970 0.747390 0.132540 0.139(3) Uani 1 1 d D U . . .
H44A H 0.524610 0.688076 0.151454 0.167 Uiso 1 1 calc R U . . .
H44B H 0.536094 0.755728 0.083808 0.167 Uiso 1 1 calc R U . . .
C45 C 0.660660 0.754080 0.142060 0.185(3) Uani 1 1 d D U . . .
H45A H 0.671800 0.811561 0.156211 0.222 Uiso 1 1 calc R U . . .
H45B H 0.682932 0.707447 0.177427 0.222 Uiso 1 1 calc R U . . .
C46 C 0.722590 0.744110 0.075850 0.226(4) Uani 1 1 d D U . . .
H46A H 0.771975 0.791058 0.064968 0.271 Uiso 1 1 calc R U . . .
H46B H 0.675987 0.748757 0.039168 0.271 Uiso 1 1 calc R U . . .
C47 C 0.783360 0.650630 0.082590 0.254(4) Uani 1 1 d D U . . .
H47A H 0.820478 0.655994 0.122534 0.305 Uiso 1 1 calc R U . . .
H47B H 0.725155 0.614044 0.100976 0.305 Uiso 1 1 calc R U . . .
C48 C 0.855750 0.579410 0.052370 0.272(5) Uani 1 1 d D U . . .
H48A H 0.927043 0.592222 0.059563 0.327 Uiso 1 1 calc R U . . .
H48B H 0.850371 0.588988 0.003098 0.327 Uiso 1 1 calc R U . . .
C49 C 0.845290 0.479270 0.075170 0.292(5) Uani 1 1 d D U . . .
H49A H 0.858952 0.474690 0.123186 0.350 Uiso 1 1 calc R U . . .
H49B H 0.909286 0.454379 0.052805 0.350 Uiso 1 1 calc R U . . .
C50 C 0.770850 0.402960 0.076950 0.304(5) Uani 1 1 d D U . . .
H50A H 0.802943 0.356800 0.050729 0.364 Uiso 1 1 calc DR U . . .
H50B H 0.752713 0.376432 0.123828 0.364 Uiso 1 1 calc R U . . .
C51 C 0.673390 0.448190 0.044260 0.310(6) Uani 1 1 d D U . . .
H51A H 0.651418 0.502216 0.064529 0.372 Uiso 1 1 calc R U . . .
H51B H 0.689734 0.464472 -0.004711 0.372 Uiso 1 1 calc DR U . . .
C52 C 0.586320 0.384040 0.056470 0.313(6) Uani 1 1 d D U . . .
H52A H 0.555563 0.379975 0.103599 0.376 Uiso 1 1 calc R U . . .
H52B H 0.531452 0.402368 0.025749 0.376 Uiso 1 1 calc R U . . .
C53 C 0.640450 0.296510 0.041630 0.317(8) Uani 1 1 d D U . . .
H53A H 0.683730 0.305482 -0.000950 0.476 Uiso 1 1 calc R U . . .
H53B H 0.588585 0.254498 0.038208 0.476 Uiso 1 1 calc R U . . .
H53C H 0.683624 0.273619 0.078149 0.476 Uiso 1 1 calc DR U . . .
B1 B 0.540960 0.566980 0.616500 0.072(2) Uani 1 1 d . . . . .
H1A H 0.602317 0.575560 0.573615 0.086 Uiso 1 1 calc R U . . .
B2 B 0.479260 0.658100 0.651970 0.079(3) Uani 1 1 d . . . . .
H2A H 0.501533 0.726307 0.632069 0.094 Uiso 1 1 calc R U . . .
B3 B 0.355880 0.637810 0.678890 0.082(3) Uani 1 1 d . . . . .
H3 H 0.296283 0.693784 0.676730 0.098 Uiso 1 1 calc R U . . .
B4 B 0.329900 0.526150 0.660970 0.068(2) Uani 1 1 d . . . . .
H4A H 0.253663 0.508281 0.646586 0.082 Uiso 1 1 calc R U . . .
B5 B 0.445440 0.481860 0.626610 0.0602(19) Uani 1 1 d . . . . .
H5 H 0.444662 0.433313 0.589852 0.072 Uiso 1 1 calc R U . . .
B6 B 0.539210 0.474880 0.686010 0.074(2) Uani 1 1 d . . . . .
H6 H 0.603224 0.422528 0.687660 0.089 Uiso 1 1 calc R U . . .
B7 B 0.559630 0.579140 0.704550 0.089(3) Uani 1 1 d . . . . .
H7A H 0.636321 0.594380 0.719932 0.107 Uiso 1 1 calc R U . . .
B8 B 0.441700 0.623730 0.738060 0.093(3) Uani 1 1 d . . . . .
H8 H 0.439874 0.670213 0.776584 0.112 Uiso 1 1 calc R U . . .
B9 B 0.349710 0.547020 0.742120 0.082(3) Uani 1 1 d . . . . .
H9A H 0.283313 0.542181 0.781819 0.098 Uiso 1 1 calc R U . . .
B10 B 0.411810 0.451850 0.711880 0.068(2) Uani 1 1 d . . . . .
H10A H 0.390876 0.383403 0.732144 0.082 Uiso 1 1 calc R U . . .
B11 B 0.476330 0.512910 0.760550 0.074(2) Uani 1 1 d . . . . .
H11 H 0.495805 0.485989 0.812779 0.089 Uiso 1 1 calc R U . . .
B12 B -0.051910 0.342240 0.439150 0.076(2) Uani 1 1 d . . . . .
H12 H -0.116252 0.394148 0.440571 0.091 Uiso 1 1 calc R U . . .
B13 B 0.011780 0.312680 0.360450 0.076(3) Uani 1 1 d . . . . .
H13 H -0.011555 0.345214 0.310396 0.091 Uiso 1 1 calc R U . . .
B14 B 0.152270 0.282890 0.373810 0.071(2) Uani 1 1 d . . . . .
H14 H 0.218271 0.296389 0.334702 0.085 Uiso 1 1 calc R U . . .
B15 B 0.160560 0.288780 0.461750 0.063(2) Uani 1 1 d . . . . .
H15 H 0.234852 0.307352 0.478597 0.075 Uiso 1 1 calc R U . . .
B16 B 0.044120 0.325800 0.498930 0.067(2) Uani 1 1 d . . . . .
H16 H 0.041942 0.368797 0.539870 0.080 Uiso 1 1 calc R U . . .
B17 B -0.068260 0.236490 0.414050 0.082(3) Uani 1 1 d . . . . .
H17 H -0.144815 0.218959 0.399946 0.099 Uiso 1 1 calc R U . . .
B18 B 0.053610 0.198580 0.372920 0.086(3) Uani 1 1 d . . . . .
H18 H 0.056553 0.157245 0.330878 0.103 Uiso 1 1 calc R U . . .
B19 B 0.144970 0.185110 0.437090 0.070(2) Uani 1 1 d . . . . .
H19A H 0.209019 0.132831 0.437096 0.084 Uiso 1 1 calc R U . . .
B20 B 0.085080 0.212430 0.511100 0.070(2) Uani 1 1 d . . . . .
H20A H 0.108832 0.178490 0.560649 0.084 Uiso 1 1 calc R U . . .
B21 B -0.044980 0.245980 0.499600 0.083(3) Uani 1 1 d . . . . .
H21A H -0.106919 0.234704 0.541871 0.100 Uiso 1 1 calc R U . . .
B22 B 0.019420 0.156440 0.458400 0.076(2) Uani 1 1 d . . . . .
H22A H -0.000091 0.086211 0.472088 0.091 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 N1 2.0675 . ?
Pt1 N2 2.0797 . ?
Pt1 C16 1.9824 . ?
Pt1 C17 1.9721 . ?
N1 C1 1.3154 . ?
N1 C5 1.3717 . ?
N2 C6 1.3709 . ?
N2 C10 1.3024 . ?
N3 C13 1.4659 . ?
N3 C16 1.3301 . ?
N3 C23 1.4099 . ?
N4 C16 1.3477 . ?
N4 C18 1.4177 . ?
N4 C42 1.4806 . ?
N5 C15 1.5099 . ?
N5 C17 1.3262 . ?
N5 C24 1.4268 . ?
N6 C17 1.3117 . ?
N6 C25 1.4035 . ?
N6 C30 1.4858 . ?
C1 H1 0.9400 . ?
C1 C2 1.3554 . ?
C2 H2 0.9400 . ?
C2 C3 1.3396 . ?
C3 C4 1.3731 . ?
C3 C11 1.5159 . ?
C4 H4 0.9400 . ?
C4 C5 1.3833 . ?
C5 C6 1.4827 . ?
C6 C7 1.3430 . ?
C7 H7 0.9400 . ?
C7 C8 1.3819 . ?
C8 C9 1.3865 . ?
C8 C12 1.5161 . ?
C9 H9 0.9400 . ?
C9 C10 1.3831 . ?
C10 H10 0.9400 . ?
C11 B1 1.6520 . ?
C11 B2 1.6691 . ?
C11 B3 1.7159 . ?
C11 B4 1.7443 . ?
C11 B5 1.7312 . ?
C12 B12 1.7133 . ?
C12 B13 1.7150 . ?
C12 B14 1.7413 . ?
C12 B15 1.7173 . ?
C12 B16 1.6855 . ?
C13 H13A 0.9800 . ?
C13 H13B 0.9800 . ?
C13 C14 1.6121 . ?
C14 H14A 0.9800 . ?
C14 H14B 0.9800 . ?
C14 C15 1.5123 . ?
C15 H15A 0.9800 . ?
C15 H15B 0.9800 . ?
C18 C19 1.4337 . ?
C18 C23 1.3132 . ?
C19 H19 0.9400 . ?
C19 C20 1.4178 . ?
C20 H20 0.9400 . ?
C20 C21 1.4027 . ?
C21 H21 0.9400 . ?
C21 C22 1.3637 . ?
C22 H22 0.9400 . ?
C22 C23 1.4214 . ?
C24 C25 1.3953 . ?
C24 C29 1.3499 . ?
C25 C26 1.3963 . ?
C26 H26 0.9400 . ?
C26 C27 1.3558 . ?
C27 H27 0.9400 . ?
C27 C28 1.4477 . ?
C28 H28 0.9400 . ?
C28 C29 1.4761 . ?
C29 H29 0.9400 . ?
C30 H30A 0.9800 . ?
C30 H30B 0.9800 . ?
C30 C31 1.5476 . ?
C31 H31A 0.9800 . ?
C31 H31B 0.9800 . ?
C31 C32 1.5187 . ?
C32 H32A 0.9800 . ?
C32 H32B 0.9800 . ?
C32 C33 1.4070 . ?
C33 H33A 0.9800 . ?
C33 H33B 0.9800 . ?
C33 C34 1.4600 . ?
C34 H34A 0.9800 . ?
C34 H34B 0.9800 . ?
C34 C35 1.5375 . ?
C35 H35A 0.9800 . ?
C35 H35B 0.9800 . ?
C35 C36 1.5161 . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 C37 1.5321 . ?
C37 H37A 0.9800 . ?
C37 H37B 0.9800 . ?
C37 C38 1.5586 . ?
C38 H38A 0.9800 . ?
C38 H38B 0.9800 . ?
C38 C39 1.5023 . ?
C39 H39A 0.9800 . ?
C39 H39B 0.9800 . ?
C39 C40 1.6947 . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 C41 1.5605 . ?
C41 H41A 0.9700 . ?
C41 H41B 0.9700 . ?
C41 H41C 0.9700 . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 C43 1.4927 . ?
C43 H43A 0.9800 . ?
C43 H43B 0.9800 . ?
C43 C44 1.5334 . ?
C44 H44A 0.9800 . ?
C44 H44B 0.9800 . ?
C44 C45 1.5207 . ?
C45 H45A 0.9800 . ?
C45 H45B 0.9800 . ?
C45 C46 1.4974 . ?
C46 H46A 0.9800 . ?
C46 H46B 0.9800 . ?
C46 C47 1.5775 . ?
C47 H47A 0.9800 . ?
C47 H47B 0.9800 . ?
C47 C48 1.5340 . ?
C48 H48A 0.9800 . ?
C48 H48B 0.9800 . ?
C48 C49 1.5465 . ?
C49 H49A 0.9800 . ?
C49 H49B 0.9800 . ?
C49 C50 1.5532 . ?
C50 H50A 0.9800 . ?
C50 H50B 0.9800 . ?
C50 C51 1.5477 . ?
C51 H51A 0.9800 . ?
C51 H51B 0.9800 . ?
C51 C52 1.5207 . ?
C52 H52A 0.9800 . ?
C52 H52B 0.9800 . ?
C52 C53 1.5180 . ?
C53 H53A 0.9700 . ?
C53 H53B 0.9700 . ?
C53 H53C 0.9700 . ?
B1 H1A 1.1100 . ?
B1 B2 1.7549 . ?
B1 B5 1.8290 . ?
B1 B6 1.8353 . ?
B1 B7 1.8258 . ?
B2 H2A 1.1100 . ?
B2 B3 1.6678 . ?
B2 B7 1.8215 . ?
B2 B8 1.7567 . ?
B3 H3 1.1100 . ?
B3 B4 1.8456 . ?
B3 B8 1.6728 . ?
B3 B9 1.7435 . ?
B4 H4A 1.1100 . ?
B4 B5 1.7175 . ?
B4 B9 1.7318 . ?
B4 B10 1.7773 . ?
B5 H5 1.1100 . ?
B5 B6 1.7561 . ?
B5 B10 1.7207 . ?
B6 H6 1.1100 . ?
B6 B7 1.7233 . ?
B6 B10 1.7215 . ?
B6 B11 1.7729 . ?
B7 H7A 1.1100 . ?
B7 B8 1.7381 . ?
B7 B11 1.7442 . ?
B8 H8 1.1100 . ?
B8 B9 1.7113 . ?
B8 B11 1.7307 . ?
B9 H9A 1.1100 . ?
B9 B10 1.7624 . ?
B9 B11 1.7378 . ?
B10 H10A 1.1100 . ?
B10 B11 1.7300 . ?
B11 H11 1.1100 . ?
B12 H12 1.1100 . ?
B12 B13 1.7988 . ?
B12 B16 1.7783 . ?
B12 B17 1.7835 . ?
B12 B21 1.7729 . ?
B13 H13 1.1100 . ?
B13 B14 1.8733 . ?
B13 B17 1.7839 . ?
B13 B18 1.7807 . ?
B14 H14 1.1100 . ?
B14 B15 1.7776 . ?
B14 B18 1.8723 . ?
B14 B19 1.8211 . ?
B15 H15 1.1100 . ?
B15 B16 1.7085 . ?
B15 B19 1.7478 . ?
B15 B20 1.7147 . ?
B16 H16 1.1100 . ?
B16 B20 1.7672 . ?
B16 B21 1.7279 . ?
B17 H17 1.1100 . ?
B17 B18 1.8020 . ?
B17 B21 1.7820 . ?
B17 B22 1.8062 . ?
B18 H18 1.1100 . ?
B18 B19 1.7989 . ?
B18 B22 1.7633 . ?
B19 H19A 1.1100 . ?
B19 B20 1.6892 . ?
B19 B22 1.7070 . ?
B20 H20A 1.1100 . ?
B20 B21 1.7479 . ?
B20 B22 1.7457 . ?
B21 H21A 1.1100 . ?
B21 B22 1.8043 . ?
B22 H22A 1.1100 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 Pt1 N2 80.3 . . ?
C16 Pt1 N1 95.4 . . ?
C16 Pt1 N2 175.6 . . ?
C17 Pt1 N1 176.6 . . ?
C17 Pt1 N2 96.3 . . ?
C17 Pt1 C16 87.9 . . ?
C1 N1 Pt1 129.0 . . ?
C1 N1 C5 117.0 . . ?
C5 N1 Pt1 113.7 . . ?
C6 N2 Pt1 114.0 . . ?
C10 N2 Pt1 127.6 . . ?
C10 N2 C6 118.3 . . ?
C16 N3 C13 126.7 . . ?
C16 N3 C23 109.5 . . ?
C23 N3 C13 123.7 . . ?
C16 N4 C18 108.4 . . ?
C16 N4 C42 125.6 . . ?
C18 N4 C42 125.7 . . ?
C17 N5 C15 125.7 . . ?
C17 N5 C24 110.9 . . ?
C24 N5 C15 123.3 . . ?
C17 N6 C25 111.5 . . ?
C17 N6 C30 126.0 . . ?
C25 N6 C30 122.3 . . ?
N1 C1 H1 118.1 . . ?
N1 C1 C2 123.8 . . ?
C2 C1 H1 118.1 . . ?
C1 C2 H2 119.5 . . ?
C3 C2 C1 121.1 . . ?
C3 C2 H2 119.5 . . ?
C2 C3 C4 117.0 . . ?
C2 C3 C11 123.1 . . ?
C4 C3 C11 119.9 . . ?
C3 C4 H4 119.5 . . ?
C3 C4 C5 121.0 . . ?
C5 C4 H4 119.5 . . ?
N1 C5 C4 120.2 . . ?
N1 C5 C6 116.5 . . ?
C4 C5 C6 123.0 . . ?
N2 C6 C5 114.8 . . ?
C7 C6 N2 120.5 . . ?
C7 C6 C5 124.7 . . ?
C6 C7 H7 119.1 . . ?
C6 C7 C8 121.8 . . ?
C8 C7 H7 119.1 . . ?
C7 C8 C9 116.8 . . ?
C7 C8 C12 121.8 . . ?
C9 C8 C12 121.3 . . ?
C8 C9 H9 120.8 . . ?
C10 C9 C8 118.4 . . ?
C10 C9 H9 120.8 . . ?
N2 C10 C9 123.6 . . ?
N2 C10 H10 118.2 . . ?
C9 C10 H10 118.2 . . ?
C3 C11 B1 118.0 . . ?
C3 C11 B2 119.1 . . ?
C3 C11 B3 118.5 . . ?
C3 C11 B4 116.6 . . ?
C3 C11 B5 118.9 . . ?
B1 C11 B2 63.8 . . ?
B1 C11 B3 113.0 . . ?
B1 C11 B4 115.2 . . ?
B1 C11 B5 65.4 . . ?
B2 C11 B3 59.0 . . ?
B2 C11 B4 113.6 . . ?
B2 C11 B5 115.2 . . ?
B3 C11 B4 64.5 . . ?
B3 C11 B5 112.0 . . ?
B5 C11 B4 59.2 . . ?
C8 C12 B12 117.5 . . ?
C8 C12 B13 118.6 . . ?
C8 C12 B14 115.6 . . ?
C8 C12 B15 118.3 . . ?
C8 C12 B16 117.9 . . ?
B12 C12 B13 63.3 . . ?
B12 C12 B14 118.6 . . ?
B12 C12 B15 113.3 . . ?
B13 C12 B14 65.6 . . ?
B13 C12 B15 114.2 . . ?
B15 C12 B14 61.9 . . ?
B16 C12 B12 63.1 . . ?
B16 C12 B13 114.5 . . ?
B16 C12 B14 113.9 . . ?
B16 C12 B15 60.3 . . ?
N3 C13 H13A 108.3 . . ?
N3 C13 H13B 108.3 . . ?
N3 C13 C14 116.0 . . ?
H13A C13 H13B 107.4 . . ?
C14 C13 H13A 108.3 . . ?
C14 C13 H13B 108.3 . . ?
C13 C14 H14A 108.8 . . ?
C13 C14 H14B 108.8 . . ?
H14A C14 H14B 107.7 . . ?
C15 C14 C13 113.9 . . ?
C15 C14 H14A 108.8 . . ?
C15 C14 H14B 108.8 . . ?
N5 C15 C14 116.6 . . ?
N5 C15 H15A 108.1 . . ?
N5 C15 H15B 108.1 . . ?
C14 C15 H15A 108.1 . . ?
C14 C15 H15B 108.1 . . ?
H15A C15 H15B 107.3 . . ?
N3 C16 Pt1 125.0 . . ?
N3 C16 N4 107.4 . . ?
N4 C16 Pt1 127.6 . . ?
N5 C17 Pt1 124.4 . . ?
N6 C17 Pt1 127.9 . . ?
N6 C17 N5 107.6 . . ?
N4 C18 C19 128.5 . . ?
C23 C18 N4 107.5 . . ?
C23 C18 C19 124.0 . . ?
C18 C19 H19 123.7 . . ?
C20 C19 C18 112.6 . . ?
C20 C19 H19 123.7 . . ?
C19 C20 H20 118.1 . . ?
C21 C20 C19 123.8 . . ?
C21 C20 H20 118.1 . . ?
C20 C21 H21 120.1 . . ?
C22 C21 C20 119.8 . . ?
C22 C21 H21 120.1 . . ?
C21 C22 H22 121.1 . . ?
C21 C22 C23 117.7 . . ?
C23 C22 H22 121.1 . . ?
N3 C23 C22 130.7 . . ?
C18 C23 N3 107.2 . . ?
C18 C23 C22 122.0 . . ?
C25 C24 N5 104.1 . . ?
C29 C24 N5 130.6 . . ?
C29 C24 C25 125.1 . . ?
C24 C25 N6 105.9 . . ?
C24 C25 C26 120.7 . . ?
C26 C25 N6 133.2 . . ?
C25 C26 H26 121.1 . . ?
C27 C26 C25 117.9 . . ?
C27 C26 H26 121.1 . . ?
C26 C27 H27 119.1 . . ?
C26 C27 C28 121.9 . . ?
C28 C27 H27 119.1 . . ?
C27 C28 H28 120.5 . . ?
C27 C28 C29 119.0 . . ?
C29 C28 H28 120.5 . . ?
C24 C29 C28 114.6 . . ?
C24 C29 H29 122.7 . . ?
C28 C29 H29 122.7 . . ?
N6 C30 H30A 109.9 . . ?
N6 C30 H30B 109.9 . . ?
N6 C30 C31 108.9 . . ?
H30A C30 H30B 108.3 . . ?
C31 C30 H30A 109.9 . . ?
C31 C30 H30B 109.9 . . ?
C30 C31 H31A 108.8 . . ?
C30 C31 H31B 108.8 . . ?
H31A C31 H31B 107.7 . . ?
C32 C31 C30 113.7 . . ?
C32 C31 H31A 108.8 . . ?
C32 C31 H31B 108.8 . . ?
C31 C32 H32A 107.9 . . ?
C31 C32 H32B 107.9 . . ?
H32A C32 H32B 107.2 . . ?
C33 C32 C31 117.6 . . ?
C33 C32 H32A 107.9 . . ?
C33 C32 H32B 107.9 . . ?
C32 C33 H33A 107.0 . . ?
C32 C33 H33B 107.0 . . ?
C32 C33 C34 121.2 . . ?
H33A C33 H33B 106.8 . . ?
C34 C33 H33A 107.0 . . ?
C34 C33 H33B 107.0 . . ?
C33 C34 H34A 107.9 . . ?
C33 C34 H34B 107.9 . . ?
C33 C34 C35 117.8 . . ?
H34A C34 H34B 107.2 . . ?
C35 C34 H34A 107.9 . . ?
C35 C34 H34B 107.9 . . ?
C34 C35 H35A 109.2 . . ?
C34 C35 H35B 109.2 . . ?
H35A C35 H35B 107.9 . . ?
C36 C35 C34 112.0 . . ?
C36 C35 H35A 109.2 . . ?
C36 C35 H35B 109.2 . . ?
C35 C36 H36A 108.8 . . ?
C35 C36 H36B 108.8 . . ?
C35 C36 C37 114.0 . . ?
H36A C36 H36B 107.7 . . ?
C37 C36 H36A 108.8 . . ?
C37 C36 H36B 108.8 . . ?
C36 C37 H37A 108.5 . . ?
C36 C37 H37B 108.5 . . ?
C36 C37 C38 114.9 . . ?
H37A C37 H37B 107.5 . . ?
C38 C37 H37A 108.5 . . ?
C38 C37 H37B 108.5 . . ?
C37 C38 H38A 109.8 . . ?
C37 C38 H38B 109.8 . . ?
H38A C38 H38B 108.2 . . ?
C39 C38 C37 109.4 . . ?
C39 C38 H38A 109.8 . . ?
C39 C38 H38B 109.8 . . ?
C38 C39 H39A 109.6 . . ?
C38 C39 H39B 109.6 . . ?
C38 C39 C40 110.4 . . ?
H39A C39 H39B 108.1 . . ?
C40 C39 H39A 109.6 . . ?
C40 C39 H39B 109.6 . . ?
C39 C40 H40A 112.3 . . ?
C39 C40 H40B 112.3 . . ?
H40A C40 H40B 109.9 . . ?
C41 C40 C39 97.2 . . ?
C41 C40 H40A 112.3 . . ?
C41 C40 H40B 112.3 . . ?
C40 C41 H41A 109.5 . . ?
C40 C41 H41B 109.5 . . ?
C40 C41 H41C 109.5 . . ?
H41A C41 H41B 109.5 . . ?
H41A C41 H41C 109.5 . . ?
H41B C41 H41C 109.5 . . ?
N4 C42 H42A 109.4 . . ?
N4 C42 H42B 109.4 . . ?
N4 C42 C43 111.2 . . ?
H42A C42 H42B 108.0 . . ?
C43 C42 H42A 109.4 . . ?
C43 C42 H42B 109.4 . . ?
C42 C43 H43A 108.9 . . ?
C42 C43 H43B 108.9 . . ?
C42 C43 C44 113.5 . . ?
H43A C43 H43B 107.7 . . ?
C44 C43 H43A 108.9 . . ?
C44 C43 H43B 108.9 . . ?
C43 C44 H44A 109.3 . . ?
C43 C44 H44B 109.3 . . ?
H44A C44 H44B 107.9 . . ?
C45 C44 C43 111.8 . . ?
C45 C44 H44A 109.3 . . ?
C45 C44 H44B 109.3 . . ?
C44 C45 H45A 110.0 . . ?
C44 C45 H45B 110.0 . . ?
H45A C45 H45B 108.4 . . ?
C46 C45 C44 108.5 . . ?
C46 C45 H45A 110.0 . . ?
C46 C45 H45B 110.0 . . ?
C45 C46 H46A 110.0 . . ?
C45 C46 H46B 110.0 . . ?
C45 C46 C47 108.4 . . ?
H46A C46 H46B 108.4 . . ?
C47 C46 H46A 110.0 . . ?
C47 C46 H46B 110.0 . . ?
C46 C47 H47A 98.8 . . ?
C46 C47 H47B 98.8 . . ?
H47A C47 H47B 103.9 . . ?
C48 C47 C46 151.2 . . ?
C48 C47 H47A 98.8 . . ?
C48 C47 H47B 98.8 . . ?
C47 C48 H48A 106.7 . . ?
C47 C48 H48B 106.7 . . ?
C47 C48 C49 122.7 . . ?
H48A C48 H48B 106.6 . . ?
C49 C48 H48A 106.7 . . ?
C49 C48 H48B 106.7 . . ?
C48 C49 H49A 101.2 . . ?
C48 C49 H49B 101.2 . . ?
C48 C49 C50 142.9 . . ?
H49A C49 H49B 104.5 . . ?
C50 C49 H49A 101.2 . . ?
C50 C49 H49B 101.2 . . ?
C49 C50 H50A 110.9 . . ?
C49 C50 H50B 110.9 . . ?
H50A C50 H50B 108.9 . . ?
C51 C50 C49 104.2 . . ?
C51 C50 H50A 110.9 . . ?
C51 C50 H50B 110.9 . . ?
C50 C51 H51A 109.9 . . ?
C50 C51 H51B 109.9 . . ?
H51A C51 H51B 108.3 . . ?
C52 C51 C50 108.7 . . ?
C52 C51 H51A 109.9 . . ?
C52 C51 H51B 109.9 . . ?
C51 C52 H52A 111.0 . . ?
C51 C52 H52B 111.0 . . ?
H52A C52 H52B 109.0 . . ?
C53 C52 C51 103.7 . . ?
C53 C52 H52A 111.0 . . ?
C53 C52 H52B 111.0 . . ?
C52 C53 H53A 109.5 . . ?
C52 C53 H53B 109.5 . . ?
C52 C53 H53C 109.5 . . ?
H53A C53 H53B 109.5 . . ?
H53A C53 H53C 109.5 . . ?
H53B C53 H53C 109.5 . . ?
C11 B1 H1A 123.9 . . ?
C11 B1 B2 58.6 . . ?
C11 B1 B5 59.4 . . ?
C11 B1 B6 103.4 . . ?
C11 B1 B7 104.3 . . ?
B2 B1 H1A 121.5 . . ?
B2 B1 B5 106.5 . . ?
B2 B1 B6 105.6 . . ?
B2 B1 B7 61.1 . . ?
B5 B1 H1A 123.9 . . ?
B5 B1 B6 57.3 . . ?
B6 B1 H1A 125.0 . . ?
B7 B1 H1A 124.6 . . ?
B7 B1 B5 102.4 . . ?
B7 B1 B6 56.2 . . ?
C11 B2 B1 57.6 . . ?
C11 B2 H2A 124.3 . . ?
C11 B2 B7 103.8 . . ?
C11 B2 B8 104.8 . . ?
B1 B2 H2A 120.3 . . ?
B1 B2 B7 61.4 . . ?
B1 B2 B8 108.2 . . ?
B3 B2 C11 61.9 . . ?
B3 B2 B1 110.2 . . ?
B3 B2 H2A 120.7 . . ?
B3 B2 B7 106.1 . . ?
B3 B2 B8 58.4 . . ?
B7 B2 H2A 123.7 . . ?
B8 B2 H2A 123.6 . . ?
B8 B2 B7 58.1 . . ?
C11 B3 H3 124.7 . . ?
C11 B3 B4 58.5 . . ?
C11 B3 B9 103.8 . . ?
B2 B3 C11 59.1 . . ?
B2 B3 H3 118.8 . . ?
B2 B3 B4 108.7 . . ?
B2 B3 B8 63.5 . . ?
B2 B3 B9 110.9 . . ?
B4 B3 H3 123.1 . . ?
B8 B3 C11 106.4 . . ?
B8 B3 H3 121.2 . . ?
B8 B3 B4 106.5 . . ?
B8 B3 B9 60.1 . . ?
B9 B3 H3 122.8 . . ?
B9 B3 B4 57.6 . . ?
C11 B4 B3 57.0 . . ?
C11 B4 H4A 125.0 . . ?
C11 B4 B10 104.2 . . ?
B3 B4 H4A 123.6 . . ?
B5 B4 C11 60.0 . . ?
B5 B4 B3 106.6 . . ?
B5 B4 H4A 121.5 . . ?
B5 B4 B9 107.4 . . ?
B5 B4 B10 59.0 . . ?
B9 B4 C11 103.1 . . ?
B9 B4 B3 58.2 . . ?
B9 B4 H4A 123.1 . . ?
B9 B4 B10 60.3 . . ?
B10 B4 B3 105.6 . . ?
B10 B4 H4A 123.1 . . ?
C11 B5 B1 55.2 . . ?
C11 B5 H5 125.2 . . ?
C11 B5 B6 103.5 . . ?
B1 B5 H5 122.1 . . ?
B4 B5 C11 60.8 . . ?
B4 B5 B1 107.9 . . ?
B4 B5 H5 119.8 . . ?
B4 B5 B6 109.2 . . ?
B4 B5 B10 62.3 . . ?
B6 B5 B1 61.5 . . ?
B6 B5 H5 122.5 . . ?
B10 B5 C11 107.2 . . ?
B10 B5 B1 109.3 . . ?
B10 B5 H5 120.6 . . ?
B10 B5 B6 59.3 . . ?
B1 B6 H6 120.2 . . ?
B5 B6 B1 61.2 . . ?
B5 B6 H6 121.5 . . ?
B5 B6 B11 107.0 . . ?
B7 B6 B1 61.6 . . ?
B7 B6 B5 109.9 . . ?
B7 B6 H6 120.6 . . ?
B7 B6 B11 59.8 . . ?
B10 B6 B1 109.0 . . ?
B10 B6 B5 59.3 . . ?
B10 B6 H6 122.1 . . ?
B10 B6 B7 108.3 . . ?
B10 B6 B11 59.3 . . ?
B11 B6 B1 108.8 . . ?
B11 B6 H6 122.5 . . ?
B1 B7 H7A 121.6 . . ?
B2 B7 B1 57.5 . . ?
B2 B7 H7A 123.3 . . ?
B6 B7 B1 62.2 . . ?
B6 B7 B2 107.6 . . ?
B6 B7 H7A 120.5 . . ?
B6 B7 B8 107.9 . . ?
B6 B7 B11 61.5 . . ?
B8 B7 B1 105.9 . . ?
B8 B7 B2 59.1 . . ?
B8 B7 H7A 123.2 . . ?
B8 B7 B11 59.6 . . ?
B11 B7 B1 110.6 . . ?
B11 B7 B2 107.7 . . ?
B11 B7 H7A 120.3 . . ?
B2 B8 H8 120.9 . . ?
B3 B8 B2 58.1 . . ?
B3 B8 B7 109.7 . . ?
B3 B8 H8 120.5 . . ?
B3 B8 B9 62.0 . . ?
B3 B8 B11 111.7 . . ?
B7 B8 B2 62.8 . . ?
B7 B8 H8 120.6 . . ?
B9 B8 B2 108.3 . . ?
B9 B8 B7 108.5 . . ?
B9 B8 H8 121.5 . . ?
B9 B8 B11 60.6 . . ?
B11 B8 B2 111.4 . . ?
B11 B8 B7 60.4 . . ?
B11 B8 H8 119.5 . . ?
B3 B9 H9A 120.4 . . ?
B3 B9 B10 110.8 . . ?
B4 B9 B3 64.2 . . ?
B4 B9 H9A 118.7 . . ?
B4 B9 B10 61.1 . . ?
B4 B9 B11 109.9 . . ?
B8 B9 B3 57.9 . . ?
B8 B9 B4 110.0 . . ?
B8 B9 H9A 122.6 . . ?
B8 B9 B10 107.4 . . ?
B8 B9 B11 60.2 . . ?
B10 B9 H9A 121.4 . . ?
B11 B9 B3 108.0 . . ?
B11 B9 H9A 121.9 . . ?
B11 B9 B10 59.2 . . ?
B4 B10 H10A 122.7 . . ?
B5 B10 B4 58.8 . . ?
B5 B10 B6 61.3 . . ?
B5 B10 B9 105.9 . . ?
B5 B10 H10A 121.5 . . ?
B5 B10 B11 110.6 . . ?
B6 B10 B4 108.0 . . ?
B6 B10 B9 107.6 . . ?
B6 B10 H10A 120.7 . . ?
B6 B10 B11 61.8 . . ?
B9 B10 B4 58.6 . . ?
B9 B10 H10A 123.5 . . ?
B11 B10 B4 108.1 . . ?
B11 B10 B9 59.7 . . ?
B11 B10 H10A 120.0 . . ?
B6 B11 H11 123.5 . . ?
B7 B11 B6 58.7 . . ?
B7 B11 H11 122.4 . . ?
B8 B11 B6 106.0 . . ?
B8 B11 B7 60.0 . . ?
B8 B11 B9 59.1 . . ?
B8 B11 H11 122.2 . . ?
B9 B11 B6 106.4 . . ?
B9 B11 B7 107.1 . . ?
B9 B11 H11 122.1 . . ?
B10 B11 B6 58.9 . . ?
B10 B11 B7 107.0 . . ?
B10 B11 B8 108.0 . . ?
B10 B11 B9 61.1 . . ?
B10 B11 H11 121.5 . . ?
C12 B12 H12 125.5 . . ?
C12 B12 B13 58.4 . . ?
C12 B12 B16 57.7 . . ?
C12 B12 B17 104.1 . . ?
C12 B12 B21 102.6 . . ?
B13 B12 H12 122.1 . . ?
B16 B12 H12 123.1 . . ?
B16 B12 B13 106.2 . . ?
B16 B12 B17 106.5 . . ?
B17 B12 H12 122.4 . . ?
B17 B12 B13 59.7 . . ?
B21 B12 H12 123.6 . . ?
B21 B12 B13 106.7 . . ?
B21 B12 B16 58.2 . . ?
B21 B12 B17 60.1 . . ?
C12 B13 B12 58.3 . . ?
C12 B13 H13 125.7 . . ?
C12 B13 B14 57.9 . . ?
C12 B13 B17 104.0 . . ?
C12 B13 B18 104.8 . . ?
B12 B13 H13 121.7 . . ?
B12 B13 B14 107.9 . . ?
B14 B13 H13 120.7 . . ?
B17 B13 B12 59.7 . . ?
B17 B13 H13 122.0 . . ?
B17 B13 B14 109.6 . . ?
B18 B13 B12 108.6 . . ?
B18 B13 H13 121.4 . . ?
B18 B13 B14 61.6 . . ?
B18 B13 B17 60.7 . . ?
C12 B14 B13 56.5 . . ?
C12 B14 H14 126.6 . . ?
C12 B14 B15 58.4 . . ?
C12 B14 B18 100.0 . . ?
C12 B14 B19 101.2 . . ?
B13 B14 H14 124.8 . . ?
B15 B14 B13 104.2 . . ?
B15 B14 H14 123.1 . . ?
B15 B14 B18 104.0 . . ?
B15 B14 B19 58.1 . . ?
B18 B14 B13 56.8 . . ?
B18 B14 H14 125.4 . . ?
B19 B14 B13 102.6 . . ?
B19 B14 H14 125.0 . . ?
B19 B14 B18 58.3 . . ?
C12 B15 B14 59.7 . . ?
C12 B15 H15 124.4 . . ?
C12 B15 B19 105.3 . . ?
B14 B15 H15 118.8 . . ?
B16 B15 C12 58.9 . . ?
B16 B15 B14 111.0 . . ?
B16 B15 H15 120.1 . . ?
B16 B15 B19 108.4 . . ?
B16 B15 B20 62.2 . . ?
B19 B15 B14 62.2 . . ?
B19 B15 H15 122.8 . . ?
B20 B15 C12 106.5 . . ?
B20 B15 B14 110.9 . . ?
B20 B15 H15 121.2 . . ?
B20 B15 B19 58.4 . . ?
C12 B16 B12 59.2 . . ?
C12 B16 B15 60.8 . . ?
C12 B16 H16 123.7 . . ?
C12 B16 B20 105.5 . . ?
C12 B16 B21 105.7 . . ?
B12 B16 H16 120.1 . . ?
B15 B16 B12 110.5 . . ?
B15 B16 H16 120.5 . . ?
B15 B16 B20 59.1 . . ?
B15 B16 B21 108.3 . . ?
B20 B16 B12 109.1 . . ?
B20 B16 H16 122.6 . . ?
B21 B16 B12 60.7 . . ?
B21 B16 H16 122.2 . . ?
B21 B16 B20 60.0 . . ?
B12 B17 B13 60.6 . . ?
B12 B17 H17 121.0 . . ?
B12 B17 B18 108.3 . . ?
B12 B17 B22 108.3 . . ?
B13 B17 H17 122.4 . . ?
B13 B17 B18 59.5 . . ?
B13 B17 B22 106.3 . . ?
B18 B17 H17 122.5 . . ?
B18 B17 B22 58.5 . . ?
B21 B17 B12 59.6 . . ?
B21 B17 B13 107.0 . . ?
B21 B17 H17 122.3 . . ?
B21 B17 B18 106.8 . . ?
B21 B17 B22 60.4 . . ?
B22 B17 H17 122.3 . . ?
B13 B18 B14 61.6 . . ?
B13 B18 B17 59.7 . . ?
B13 B18 H18 121.0 . . ?
B13 B18 B19 107.3 . . ?
B14 B18 H18 121.1 . . ?
B17 B18 B14 108.9 . . ?
B17 B18 H18 121.8 . . ?
B19 B18 B14 59.4 . . ?
B19 B18 B17 105.7 . . ?
B19 B18 H18 123.9 . . ?
B22 B18 B13 108.4 . . ?
B22 B18 B14 106.9 . . ?
B22 B18 B17 60.9 . . ?
B22 B18 H18 122.4 . . ?
B22 B18 B19 57.3 . . ?
B14 B19 H19A 119.6 . . ?
B15 B19 B14 59.7 . . ?
B15 B19 B18 108.4 . . ?
B15 B19 H19A 122.3 . . ?
B18 B19 B14 62.3 . . ?
B18 B19 H19A 120.9 . . ?
B20 B19 B14 110.0 . . ?
B20 B19 B15 59.8 . . ?
B20 B19 B18 109.8 . . ?
B20 B19 H19A 120.6 . . ?
B20 B19 B22 61.9 . . ?
B22 B19 B14 111.8 . . ?
B22 B19 B15 109.4 . . ?
B22 B19 B18 60.3 . . ?
B22 B19 H19A 119.8 . . ?
B15 B20 B16 58.7 . . ?
B15 B20 H20A 121.7 . . ?
B15 B20 B21 107.1 . . ?
B15 B20 B22 109.1 . . ?
B16 B20 H20A 122.5 . . ?
B19 B20 B15 61.8 . . ?
B19 B20 B16 108.4 . . ?
B19 B20 H20A 120.8 . . ?
B19 B20 B21 109.3 . . ?
B19 B20 B22 59.6 . . ?
B21 B20 B16 58.9 . . ?
B21 B20 H20A 121.4 . . ?
B22 B20 B16 108.7 . . ?
B22 B20 H20A 120.6 . . ?
B22 B20 B21 62.2 . . ?
B12 B21 B17 60.2 . . ?
B12 B21 H21A 120.4 . . ?
B12 B21 B22 108.8 . . ?
B16 B21 B12 61.0 . . ?
B16 B21 B17 108.8 . . ?
B16 B21 B20 61.1 . . ?
B16 B21 H21A 121.1 . . ?
B16 B21 B22 107.9 . . ?
B17 B21 H21A 121.4 . . ?
B17 B21 B22 60.5 . . ?
B20 B21 B12 110.2 . . ?
B20 B21 B17 108.4 . . ?
B20 B21 H21A 121.1 . . ?
B20 B21 B22 58.8 . . ?
B22 B21 H21A 122.2 . . ?
B17 B22 H22A 121.3 . . ?
B18 B22 B17 60.6 . . ?
B18 B22 B21 107.5 . . ?
B18 B22 H22A 120.3 . . ?
B19 B22 B17 109.6 . . ?
B19 B22 B18 62.4 . . ?
B19 B22 B20 58.6 . . ?
B19 B22 B21 106.0 . . ?
B19 B22 H22A 121.4 . . ?
B20 B22 B17 107.4 . . ?
B20 B22 B18 108.8 . . ?
B20 B22 B21 59.0 . . ?
B20 B22 H22A 122.5 . . ?
B21 B22 B17 59.1 . . ?
B21 B22 H22A 123.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Pt1 N1 C1 C2 173.1 . . . . ?
Pt1 N1 C5 C4 -173.0 . . . . ?
Pt1 N1 C5 C6 1.5 . . . . ?
Pt1 N2 C6 C5 8.9 . . . . ?
Pt1 N2 C6 C7 -171.4 . . . . ?
Pt1 N2 C10 C9 171.4 . . . . ?
N1 C1 C2 C3 -2.2 . . . . ?
N1 C5 C6 N2 -7.0 . . . . ?
N1 C5 C6 C7 173.4 . . . . ?
N2 C6 C7 C8 0.2 . . . . ?
N3 C13 C14 C15 78.3 . . . . ?
N4 C18 C19 C20 179.4 . . . . ?
N4 C18 C23 N3 2.0 . . . . ?
N4 C18 C23 C22 -179.9 . . . . ?
N4 C42 C43 C44 -179.6 . . . . ?
N5 C24 C25 N6 -1.5 . . . . ?
N5 C24 C25 C26 -176.8 . . . . ?
N5 C24 C29 C28 -179.3 . . . . ?
N6 C25 C26 C27 -175.1 . . . . ?
N6 C30 C31 C32 -171.5 . . . . ?
C1 N1 C5 C4 1.2 . . . . ?
C1 N1 C5 C6 175.6 . . . . ?
C1 C2 C3 C4 3.1 . . . . ?
C1 C2 C3 C11 -176.1 . . . . ?
C2 C3 C4 C5 -1.9 . . . . ?
C2 C3 C11 B1 -66.0 . . . . ?
C2 C3 C11 B2 7.9 . . . . ?
C2 C3 C11 B3 76.3 . . . . ?
C2 C3 C11 B4 150.3 . . . . ?
C2 C3 C11 B5 -141.9 . . . . ?
C3 C4 C5 N1 -0.2 . . . . ?
C3 C4 C5 C6 -174.2 . . . . ?
C3 C11 B1 B2 110.6 . . . . ?
C3 C11 B1 B5 -111.0 . . . . ?
C3 C11 B1 B6 -149.1 . . . . ?
C3 C11 B1 B7 152.9 . . . . ?
C3 C11 B2 B1 -109.0 . . . . ?
C3 C11 B2 B3 107.6 . . . . ?
C3 C11 B2 B7 -151.3 . . . . ?
C3 C11 B2 B8 148.6 . . . . ?
C3 C11 B3 B2 -108.6 . . . . ?
C3 C11 B3 B4 107.8 . . . . ?
C3 C11 B3 B8 -152.6 . . . . ?
C3 C11 B3 B9 145.0 . . . . ?
C3 C11 B4 B3 -110.6 . . . . ?
C3 C11 B4 B5 109.3 . . . . ?
C3 C11 B4 B9 -148.0 . . . . ?
C3 C11 B4 B10 149.8 . . . . ?
C3 C11 B5 B1 109.7 . . . . ?
C3 C11 B5 B4 -105.5 . . . . ?
C3 C11 B5 B6 149.9 . . . . ?
C3 C11 B5 B10 -148.4 . . . . ?
C4 C3 C11 B1 114.8 . . . . ?
C4 C3 C11 B2 -171.2 . . . . ?
C4 C3 C11 B3 -102.8 . . . . ?
C4 C3 C11 B4 -28.9 . . . . ?
C4 C3 C11 B5 39.0 . . . . ?
C4 C5 C6 N2 167.3 . . . . ?
C4 C5 C6 C7 -12.4 . . . . ?
C5 N1 C1 C2 0.0 . . . . ?
C5 C6 C7 C8 179.9 . . . . ?
C6 N2 C10 C9 -5.4 . . . . ?
C6 C7 C8 C9 -6.6 . . . . ?
C6 C7 C8 C12 176.6 . . . . ?
C7 C8 C9 C10 7.0 . . . . ?
C7 C8 C12 B12 122.3 . . . . ?
C7 C8 C12 B13 -164.8 . . . . ?
C7 C8 C12 B14 -89.9 . . . . ?
C7 C8 C12 B15 -19.5 . . . . ?
C7 C8 C12 B16 49.9 . . . . ?
C8 C9 C10 N2 -1.1 . . . . ?
C8 C12 B12 B13 110.0 . . . . ?
C8 C12 B12 B16 -109.1 . . . . ?
C8 C12 B12 B17 150.1 . . . . ?
C8 C12 B12 B21 -148.0 . . . . ?
C8 C12 B13 B12 -108.3 . . . . ?
C8 C12 B13 B14 107.0 . . . . ?
C8 C12 B13 B17 -148.4 . . . . ?
C8 C12 B13 B18 148.7 . . . . ?
C8 C12 B14 B13 -111.4 . . . . ?
C8 C12 B14 B15 109.8 . . . . ?
C8 C12 B14 B18 -149.8 . . . . ?
C8 C12 B14 B19 150.8 . . . . ?
C8 C12 B15 B14 -105.6 . . . . ?
C8 C12 B15 B16 107.8 . . . . ?
C8 C12 B15 B19 -149.6 . . . . ?
C8 C12 B15 B20 149.5 . . . . ?
C8 C12 B16 B12 108.5 . . . . ?
C8 C12 B16 B15 -108.3 . . . . ?
C8 C12 B16 B20 -148.3 . . . . ?
C8 C12 B16 B21 149.2 . . . . ?
C9 C8 C12 B12 -54.3 . . . . ?
C9 C8 C12 B13 18.6 . . . . ?
C9 C8 C12 B14 93.5 . . . . ?
C9 C8 C12 B15 163.9 . . . . ?
C9 C8 C12 B16 -126.8 . . . . ?
C10 N2 C6 C5 -173.8 . . . . ?
C10 N2 C6 C7 5.8 . . . . ?
C11 C3 C4 C5 177.3 . . . . ?
C11 B1 B2 B3 34.1 . . . . ?
C11 B1 B2 B7 131.9 . . . . ?
C11 B1 B2 B8 96.3 . . . . ?
C11 B1 B5 B4 -31.9 . . . . ?
C11 B1 B5 B6 -134.5 . . . . ?
C11 B1 B5 B10 -98.0 . . . . ?
C11 B1 B6 B5 39.1 . . . . ?
C11 B1 B6 B7 -98.4 . . . . ?
C11 B1 B6 B10 2.7 . . . . ?
C11 B1 B6 B11 -60.4 . . . . ?
C11 B1 B7 B2 -41.0 . . . . ?
C11 B1 B7 B6 96.7 . . . . ?
C11 B1 B7 B8 -5.4 . . . . ?
C11 B1 B7 B11 57.5 . . . . ?
C11 B2 B3 B4 32.3 . . . . ?
C11 B2 B3 B8 131.9 . . . . ?
C11 B2 B3 B9 93.9 . . . . ?
C11 B2 B7 B1 40.4 . . . . ?
C11 B2 B7 B6 1.7 . . . . ?
C11 B2 B7 B8 -99.0 . . . . ?
C11 B2 B7 B11 -63.2 . . . . ?
C11 B2 B8 B3 -42.8 . . . . ?
C11 B2 B8 B7 97.2 . . . . ?
C11 B2 B8 B9 -4.7 . . . . ?
C11 B2 B8 B11 60.1 . . . . ?
C11 B3 B4 B5 35.4 . . . . ?
C11 B3 B4 B9 136.0 . . . . ?
C11 B3 B4 B10 97.1 . . . . ?
C11 B3 B8 B2 41.8 . . . . ?
C11 B3 B8 B7 4.4 . . . . ?
C11 B3 B8 B9 -96.7 . . . . ?
C11 B3 B8 B11 -60.6 . . . . ?
C11 B3 B9 B4 -37.6 . . . . ?
C11 B3 B9 B8 101.2 . . . . ?
C11 B3 B9 B10 3.2 . . . . ?
C11 B3 B9 B11 66.3 . . . . ?
C11 B4 B5 B1 29.8 . . . . ?
C11 B4 B5 B6 95.1 . . . . ?
C11 B4 B5 B10 132.7 . . . . ?
C11 B4 B9 B3 36.8 . . . . ?
C11 B4 B9 B8 0.4 . . . . ?
C11 B4 B9 B10 -99.1 . . . . ?
C11 B4 B9 B11 -64.2 . . . . ?
C11 B4 B10 B5 -41.1 . . . . ?
C11 B4 B10 B6 -2.9 . . . . ?
C11 B4 B10 B9 97.1 . . . . ?
C11 B4 B10 B11 62.5 . . . . ?
C11 B5 B6 B1 -37.1 . . . . ?
C11 B5 B6 B7 2.1 . . . . ?
C11 B5 B6 B10 102.2 . . . . ?
C11 B5 B6 B11 65.5 . . . . ?
C11 B5 B10 B4 42.2 . . . . ?
C11 B5 B10 B6 -95.8 . . . . ?
C11 B5 B10 B9 5.9 . . . . ?
C11 B5 B10 B11 -57.1 . . . . ?
C12 C8 C9 C10 -176.3 . . . . ?
C12 B12 B13 B14 31.0 . . . . ?
C12 B12 B13 B17 133.7 . . . . ?
C12 B12 B13 B18 96.2 . . . . ?
C12 B12 B16 B15 -33.9 . . . . ?
C12 B12 B16 B20 -97.1 . . . . ?
C12 B12 B16 B21 -134.0 . . . . ?
C12 B12 B17 B13 -39.4 . . . . ?
C12 B12 B17 B18 -2.6 . . . . ?
C12 B12 B17 B21 96.6 . . . . ?
C12 B12 B17 B22 59.4 . . . . ?
C12 B12 B21 B16 38.5 . . . . ?
C12 B12 B21 B17 -99.2 . . . . ?
C12 B12 B21 B20 0.9 . . . . ?
C12 B12 B21 B22 -61.9 . . . . ?
C12 B13 B14 B15 35.4 . . . . ?
C12 B13 B14 B18 133.0 . . . . ?
C12 B13 B14 B19 95.3 . . . . ?
C12 B13 B17 B12 39.4 . . . . ?
C12 B13 B17 B18 -99.3 . . . . ?
C12 B13 B17 B21 0.5 . . . . ?
C12 B13 B17 B22 -62.8 . . . . ?
C12 B13 B18 B14 -39.8 . . . . ?
C12 B13 B18 B17 98.0 . . . . ?
C12 B13 B18 B19 -0.4 . . . . ?
C12 B13 B18 B22 60.0 . . . . ?
C12 B14 B15 B16 30.3 . . . . ?
C12 B14 B15 B19 130.7 . . . . ?
C12 B14 B15 B20 97.4 . . . . ?
C12 B14 B18 B13 38.2 . . . . ?
C12 B14 B18 B17 0.4 . . . . ?
C12 B14 B18 B19 -97.1 . . . . ?
C12 B14 B18 B22 -63.9 . . . . ?
C12 B14 B19 B15 -41.2 . . . . ?
C12 B14 B19 B18 94.9 . . . . ?
C12 B14 B19 B20 -7.5 . . . . ?
C12 B14 B19 B22 59.2 . . . . ?
C12 B15 B16 B12 33.3 . . . . ?
C12 B15 B16 B20 133.8 . . . . ?
C12 B15 B16 B21 98.1 . . . . ?
C12 B15 B19 B14 42.7 . . . . ?
C12 B15 B19 B18 2.4 . . . . ?
C12 B15 B19 B20 -100.2 . . . . ?
C12 B15 B19 B22 -61.8 . . . . ?
C12 B15 B20 B16 -40.1 . . . . ?
C12 B15 B20 B19 98.1 . . . . ?
C12 B15 B20 B21 -5.1 . . . . ?
C12 B15 B20 B22 60.7 . . . . ?
C12 B16 B20 B15 40.8 . . . . ?
C12 B16 B20 B19 2.5 . . . . ?
C12 B16 B20 B21 -99.4 . . . . ?
C12 B16 B20 B22 -60.7 . . . . ?
C12 B16 B21 B12 -40.0 . . . . ?
C12 B16 B21 B17 -1.9 . . . . ?
C12 B16 B21 B20 99.2 . . . . ?
C12 B16 B21 B22 62.2 . . . . ?
C13 N3 C16 Pt1 7.0 . . . . ?
C13 N3 C16 N4 -174.4 . . . . ?
C13 N3 C23 C18 173.7 . . . . ?
C13 N3 C23 C22 -4.1 . . . . ?
C13 C14 C15 N5 -80.0 . . . . ?
C15 N5 C17 Pt1 -11.3 . . . . ?
C15 N5 C17 N6 172.8 . . . . ?
C15 N5 C24 C25 -172.9 . . . . ?
C15 N5 C24 C29 2.6 . . . . ?
C16 N3 C13 C14 -87.3 . . . . ?
C16 N3 C23 C18 -2.2 . . . . ?
C16 N3 C23 C22 -180.0 . . . . ?
C16 N4 C18 C19 178.0 . . . . ?
C16 N4 C18 C23 -1.2 . . . . ?
C16 N4 C42 C43 105.5 . . . . ?
C17 N5 C15 C14 93.1 . . . . ?
C17 N5 C24 C25 2.6 . . . . ?
C17 N5 C24 C29 178.1 . . . . ?
C17 N6 C25 C24 0.1 . . . . ?
C17 N6 C25 C26 174.4 . . . . ?
C17 N6 C30 C31 103.9 . . . . ?
C18 N4 C16 Pt1 178.4 . . . . ?
C18 N4 C16 N3 -0.1 . . . . ?
C18 N4 C42 C43 -66.7 . . . . ?
C18 C19 C20 C21 0.4 . . . . ?
C19 C18 C23 N3 -177.3 . . . . ?
C19 C18 C23 C22 0.8 . . . . ?
C19 C20 C21 C22 1.5 . . . . ?
C20 C21 C22 C23 -2.3 . . . . ?
C21 C22 C23 N3 178.8 . . . . ?
C21 C22 C23 C18 1.2 . . . . ?
C23 N3 C13 C14 97.5 . . . . ?
C23 N3 C16 Pt1 -177.2 . . . . ?
C23 N3 C16 N4 1.3 . . . . ?
C23 C18 C19 C20 -1.5 . . . . ?
C24 N5 C15 C14 -92.1 . . . . ?
C24 N5 C17 Pt1 173.3 . . . . ?
C24 N5 C17 N6 -2.6 . . . . ?
C24 C25 C26 C27 -1.5 . . . . ?
C25 N6 C17 Pt1 -174.2 . . . . ?
C25 N6 C17 N5 1.6 . . . . ?
C25 N6 C30 C31 -69.8 . . . . ?
C25 C24 C29 C28 -4.7 . . . . ?
C25 C26 C27 C28 -6.3 . . . . ?
C26 C27 C28 C29 8.8 . . . . ?
C27 C28 C29 C24 -3.2 . . . . ?
C29 C24 C25 N6 -177.4 . . . . ?
C29 C24 C25 C26 7.4 . . . . ?
C30 N6 C17 Pt1 11.6 . . . . ?
C30 N6 C17 N5 -172.7 . . . . ?
C30 N6 C25 C24 174.6 . . . . ?
C30 N6 C25 C26 -11.1 . . . . ?
C30 C31 C32 C33 170.5 . . . . ?
C31 C32 C33 C34 170.8 . . . . ?
C32 C33 C34 C35 174.3 . . . . ?
C33 C34 C35 C36 170.5 . . . . ?
C34 C35 C36 C37 173.1 . . . . ?
C35 C36 C37 C38 -170.5 . . . . ?
C36 C37 C38 C39 -66.3 . . . . ?
C37 C38 C39 C40 -170.9 . . . . ?
C38 C39 C40 C41 169.4 . . . . ?
C42 N4 C16 Pt1 5.1 . . . . ?
C42 N4 C16 N3 -173.4 . . . . ?
C42 N4 C18 C19 -8.7 . . . . ?
C42 N4 C18 C23 172.1 . . . . ?
C42 C43 C44 C45 -67.2 . . . . ?
C43 C44 C45 C46 -137.6 . . . . ?
C44 C45 C46 C47 -107.9 . . . . ?
C45 C46 C47 C48 177.3 . . . . ?
C46 C47 C48 C49 -147.3 . . . . ?
C47 C48 C49 C50 63.6 . . . . ?
C48 C49 C50 C51 -1.1 . . . . ?
C49 C50 C51 C52 -168.4 . . . . ?
C50 C51 C52 C53 -43.7 . . . . ?
B1 C11 B2 B3 -143.4 . . . . ?
B1 C11 B2 B7 -42.3 . . . . ?
B1 C11 B2 B8 -102.4 . . . . ?
B1 C11 B3 B2 35.5 . . . . ?
B1 C11 B3 B4 -108.0 . . . . ?
B1 C11 B3 B8 -8.4 . . . . ?
B1 C11 B3 B9 -70.9 . . . . ?
B1 C11 B4 B3 104.7 . . . . ?
B1 C11 B4 B5 -35.4 . . . . ?
B1 C11 B4 B9 67.3 . . . . ?
B1 C11 B4 B10 5.1 . . . . ?
B1 C11 B5 B4 144.8 . . . . ?
B1 C11 B5 B6 40.2 . . . . ?
B1 C11 B5 B10 101.9 . . . . ?
B1 B2 B3 C11 -32.5 . . . . ?
B1 B2 B3 B4 -0.1 . . . . ?
B1 B2 B3 B8 99.4 . . . . ?
B1 B2 B3 B9 61.4 . . . . ?
B1 B2 B7 B6 -38.6 . . . . ?
B1 B2 B7 B8 -139.3 . . . . ?
B1 B2 B7 B11 -103.5 . . . . ?
B1 B2 B8 B3 -103.0 . . . . ?
B1 B2 B8 B7 37.0 . . . . ?
B1 B2 B8 B9 -65.0 . . . . ?
B1 B2 B8 B11 -0.1 . . . . ?
B1 B5 B6 B7 39.2 . . . . ?
B1 B5 B6 B10 139.3 . . . . ?
B1 B5 B6 B11 102.6 . . . . ?
B1 B5 B10 B4 100.6 . . . . ?
B1 B5 B10 B6 -37.4 . . . . ?
B1 B5 B10 B9 64.3 . . . . ?
B1 B5 B10 B11 1.3 . . . . ?
B1 B6 B7 B2 36.5 . . . . ?
B1 B6 B7 B8 98.9 . . . . ?
B1 B6 B7 B11 137.6 . . . . ?
B1 B6 B10 B4 0.2 . . . . ?
B1 B6 B10 B5 37.2 . . . . ?
B1 B6 B10 B9 -61.6 . . . . ?
B1 B6 B10 B11 -101.2 . . . . ?
B1 B6 B11 B7 -38.8 . . . . ?
B1 B6 B11 B8 -0.4 . . . . ?
B1 B6 B11 B9 61.5 . . . . ?
B1 B6 B11 B10 101.3 . . . . ?
B1 B7 B8 B2 -34.8 . . . . ?
B1 B7 B8 B3 0.6 . . . . ?
B1 B7 B8 B9 66.7 . . . . ?
B1 B7 B8 B11 104.9 . . . . ?
B1 B7 B11 B6 39.6 . . . . ?
B1 B7 B11 B8 -96.8 . . . . ?
B1 B7 B11 B9 -59.6 . . . . ?
B1 B7 B11 B10 4.6 . . . . ?
B2 C11 B1 B5 138.4 . . . . ?
B2 C11 B1 B6 100.3 . . . . ?
B2 C11 B1 B7 42.3 . . . . ?
B2 C11 B3 B4 -143.6 . . . . ?
B2 C11 B3 B8 -44.0 . . . . ?
B2 C11 B3 B9 -106.4 . . . . ?
B2 C11 B4 B3 33.8 . . . . ?
B2 C11 B4 B5 -106.3 . . . . ?
B2 C11 B4 B9 -3.6 . . . . ?
B2 C11 B4 B10 -65.8 . . . . ?
B2 C11 B5 B1 -41.2 . . . . ?
B2 C11 B5 B4 103.6 . . . . ?
B2 C11 B5 B6 -1.0 . . . . ?
B2 C11 B5 B10 60.6 . . . . ?
B2 B1 B5 C11 36.2 . . . . ?
B2 B1 B5 B4 4.3 . . . . ?
B2 B1 B5 B6 -98.3 . . . . ?
B2 B1 B5 B10 -61.8 . . . . ?
B2 B1 B6 B5 99.8 . . . . ?
B2 B1 B6 B7 -37.7 . . . . ?
B2 B1 B6 B10 63.4 . . . . ?
B2 B1 B6 B11 0.3 . . . . ?
B2 B1 B7 B6 137.7 . . . . ?
B2 B1 B7 B8 35.5 . . . . ?
B2 B1 B7 B11 98.4 . . . . ?
B2 B3 B4 C11 -32.5 . . . . ?
B2 B3 B4 B5 2.9 . . . . ?
B2 B3 B4 B9 103.4 . . . . ?
B2 B3 B4 B10 64.5 . . . . ?
B2 B3 B8 B7 -37.4 . . . . ?
B2 B3 B8 B9 -138.5 . . . . ?
B2 B3 B8 B11 -102.4 . . . . ?
B2 B3 B9 B4 -99.4 . . . . ?
B2 B3 B9 B8 39.4 . . . . ?
B2 B3 B9 B10 -58.7 . . . . ?
B2 B3 B9 B11 4.5 . . . . ?
B2 B7 B8 B3 35.4 . . . . ?
B2 B7 B8 B9 101.5 . . . . ?
B2 B7 B8 B11 139.7 . . . . ?
B2 B7 B11 B6 100.8 . . . . ?
B2 B7 B11 B8 -35.6 . . . . ?
B2 B7 B11 B9 1.6 . . . . ?
B2 B7 B11 B10 65.8 . . . . ?
B2 B8 B9 B3 -36.4 . . . . ?
B2 B8 B9 B4 2.7 . . . . ?
B2 B8 B9 B10 67.6 . . . . ?
B2 B8 B9 B11 104.7 . . . . ?
B2 B8 B11 B6 0.3 . . . . ?
B2 B8 B11 B7 38.1 . . . . ?
B2 B8 B11 B9 -99.6 . . . . ?
B2 B8 B11 B10 -61.5 . . . . ?
B3 C11 B1 B2 -33.7 . . . . ?
B3 C11 B1 B5 104.6 . . . . ?
B3 C11 B1 B6 66.5 . . . . ?
B3 C11 B1 B7 8.5 . . . . ?
B3 C11 B2 B1 143.4 . . . . ?
B3 C11 B2 B7 101.1 . . . . ?
B3 C11 B2 B8 41.0 . . . . ?
B3 C11 B4 B5 -140.1 . . . . ?
B3 C11 B4 B9 -37.3 . . . . ?
B3 C11 B4 B10 -99.5 . . . . ?
B3 C11 B5 B1 -106.1 . . . . ?
B3 C11 B5 B4 38.6 . . . . ?
B3 C11 B5 B6 -66.0 . . . . ?
B3 C11 B5 B10 -4.3 . . . . ?
B3 B2 B7 B1 104.6 . . . . ?
B3 B2 B7 B6 66.0 . . . . ?
B3 B2 B7 B8 -34.7 . . . . ?
B3 B2 B7 B11 1.1 . . . . ?
B3 B2 B8 B7 140.0 . . . . ?
B3 B2 B8 B9 38.1 . . . . ?
B3 B2 B8 B11 102.9 . . . . ?
B3 B4 B5 C11 -34.2 . . . . ?
B3 B4 B5 B1 -4.3 . . . . ?
B3 B4 B5 B6 61.0 . . . . ?
B3 B4 B5 B10 98.5 . . . . ?
B3 B4 B9 B8 -36.4 . . . . ?
B3 B4 B9 B10 -135.8 . . . . ?
B3 B4 B9 B11 -100.9 . . . . ?
B3 B4 B10 B5 -100.2 . . . . ?
B3 B4 B10 B6 -62.1 . . . . ?
B3 B4 B10 B9 38.0 . . . . ?
B3 B4 B10 B11 3.3 . . . . ?
B3 B8 B9 B4 39.1 . . . . ?
B3 B8 B9 B10 104.0 . . . . ?
B3 B8 B9 B11 141.1 . . . . ?
B3 B8 B11 B6 63.3 . . . . ?
B3 B8 B11 B7 101.1 . . . . ?
B3 B8 B11 B9 -36.6 . . . . ?
B3 B8 B11 B10 1.5 . . . . ?
B3 B9 B10 B4 -42.1 . . . . ?
B3 B9 B10 B5 -5.8 . . . . ?
B3 B9 B10 B6 58.6 . . . . ?
B3 B9 B10 B11 99.1 . . . . ?
B3 B9 B11 B6 -65.1 . . . . ?
B3 B9 B11 B7 -3.6 . . . . ?
B3 B9 B11 B8 34.0 . . . . ?
B3 B9 B11 B10 -103.9 . . . . ?
B4 C11 B1 B2 -105.2 . . . . ?
B4 C11 B1 B5 33.2 . . . . ?
B4 C11 B1 B6 -4.9 . . . . ?
B4 C11 B1 B7 -62.9 . . . . ?
B4 C11 B2 B1 107.6 . . . . ?
B4 C11 B2 B3 -35.8 . . . . ?
B4 C11 B2 B7 65.3 . . . . ?
B4 C11 B2 B8 5.2 . . . . ?
B4 C11 B3 B2 143.6 . . . . ?
B4 C11 B3 B8 99.6 . . . . ?
B4 C11 B3 B9 37.2 . . . . ?
B4 C11 B5 B1 -144.8 . . . . ?
B4 C11 B5 B6 -104.6 . . . . ?
B4 C11 B5 B10 -42.9 . . . . ?
B4 B3 B8 B2 103.0 . . . . ?
B4 B3 B8 B7 65.6 . . . . ?
B4 B3 B8 B9 -35.4 . . . . ?
B4 B3 B8 B11 0.6 . . . . ?
B4 B3 B9 B8 138.8 . . . . ?
B4 B3 B9 B10 40.8 . . . . ?
B4 B3 B9 B11 103.9 . . . . ?
B4 B5 B6 B1 -100.4 . . . . ?
B4 B5 B6 B7 -61.2 . . . . ?
B4 B5 B6 B10 38.8 . . . . ?
B4 B5 B6 B11 2.1 . . . . ?
B4 B5 B10 B6 -138.0 . . . . ?
B4 B5 B10 B9 -36.3 . . . . ?
B4 B5 B10 B11 -99.3 . . . . ?
B4 B9 B10 B5 36.4 . . . . ?
B4 B9 B10 B6 100.7 . . . . ?
B4 B9 B10 B11 141.2 . . . . ?
B4 B9 B11 B6 3.2 . . . . ?
B4 B9 B11 B7 64.7 . . . . ?
B4 B9 B11 B8 102.3 . . . . ?
B4 B9 B11 B10 -35.7 . . . . ?
B4 B10 B11 B6 -101.2 . . . . ?
B4 B10 B11 B7 -66.3 . . . . ?
B4 B10 B11 B8 -3.0 . . . . ?
B4 B10 B11 B9 34.2 . . . . ?
B5 C11 B1 B2 -138.4 . . . . ?
B5 C11 B1 B6 -38.1 . . . . ?
B5 C11 B1 B7 -96.1 . . . . ?
B5 C11 B2 B1 41.9 . . . . ?
B5 C11 B2 B3 -101.5 . . . . ?
B5 C11 B2 B7 -0.4 . . . . ?
B5 C11 B2 B8 -60.5 . . . . ?
B5 C11 B3 B2 107.1 . . . . ?
B5 C11 B3 B4 -36.5 . . . . ?
B5 C11 B3 B8 63.1 . . . . ?
B5 C11 B3 B9 0.7 . . . . ?
B5 C11 B4 B3 140.1 . . . . ?
B5 C11 B4 B9 102.7 . . . . ?
B5 C11 B4 B10 40.5 . . . . ?
B5 B1 B2 C11 -36.6 . . . . ?
B5 B1 B2 B3 -2.5 . . . . ?
B5 B1 B2 B7 95.3 . . . . ?
B5 B1 B2 B8 59.7 . . . . ?
B5 B1 B6 B7 -137.5 . . . . ?
B5 B1 B6 B10 -36.4 . . . . ?
B5 B1 B6 B11 -99.5 . . . . ?
B5 B1 B7 B2 -102.1 . . . . ?
B5 B1 B7 B6 35.6 . . . . ?
B5 B1 B7 B8 -66.6 . . . . ?
B5 B1 B7 B11 -3.7 . . . . ?
B5 B4 B9 B3 99.1 . . . . ?
B5 B4 B9 B8 62.6 . . . . ?
B5 B4 B9 B10 -36.8 . . . . ?
B5 B4 B9 B11 -1.9 . . . . ?
B5 B4 B10 B6 38.1 . . . . ?
B5 B4 B10 B9 138.2 . . . . ?
B5 B4 B10 B11 103.5 . . . . ?
B5 B6 B7 B1 -39.0 . . . . ?
B5 B6 B7 B2 -2.5 . . . . ?
B5 B6 B7 B8 59.9 . . . . ?
B5 B6 B7 B11 98.6 . . . . ?
B5 B6 B10 B4 -37.0 . . . . ?
B5 B6 B10 B9 -98.8 . . . . ?
B5 B6 B10 B11 -138.4 . . . . ?
B5 B6 B11 B7 -103.5 . . . . ?
B5 B6 B11 B8 -65.0 . . . . ?
B5 B6 B11 B9 -3.2 . . . . ?
B5 B6 B11 B10 36.7 . . . . ?
B5 B10 B11 B6 -38.5 . . . . ?
B5 B10 B11 B7 -3.6 . . . . ?
B5 B10 B11 B8 59.6 . . . . ?
B5 B10 B11 B9 96.8 . . . . ?
B6 B1 B2 C11 -96.4 . . . . ?
B6 B1 B2 B3 -62.3 . . . . ?
B6 B1 B2 B7 35.5 . . . . ?
B6 B1 B2 B8 -0.1 . . . . ?
B6 B1 B5 C11 134.5 . . . . ?
B6 B1 B5 B4 102.6 . . . . ?
B6 B1 B5 B10 36.5 . . . . ?
B6 B1 B7 B2 -137.7 . . . . ?
B6 B1 B7 B8 -102.2 . . . . ?
B6 B1 B7 B11 -39.3 . . . . ?
B6 B5 B10 B4 138.0 . . . . ?
B6 B5 B10 B9 101.7 . . . . ?
B6 B5 B10 B11 38.7 . . . . ?
B6 B7 B8 B2 -100.1 . . . . ?
B6 B7 B8 B3 -64.7 . . . . ?
B6 B7 B8 B9 1.4 . . . . ?
B6 B7 B8 B11 39.6 . . . . ?
B6 B7 B11 B8 -136.4 . . . . ?
B6 B7 B11 B9 -99.2 . . . . ?
B6 B7 B11 B10 -35.0 . . . . ?
B6 B10 B11 B7 34.9 . . . . ?
B6 B10 B11 B8 98.2 . . . . ?
B6 B10 B11 B9 135.4 . . . . ?
B7 B1 B2 C11 -131.9 . . . . ?
B7 B1 B2 B3 -97.8 . . . . ?
B7 B1 B2 B8 -35.6 . . . . ?
B7 B1 B5 C11 99.4 . . . . ?
B7 B1 B5 B4 67.5 . . . . ?
B7 B1 B5 B6 -35.1 . . . . ?
B7 B1 B5 B10 1.4 . . . . ?
B7 B1 B6 B5 137.5 . . . . ?
B7 B1 B6 B10 101.1 . . . . ?
B7 B1 B6 B11 38.0 . . . . ?
B7 B2 B3 C11 -97.3 . . . . ?
B7 B2 B3 B4 -65.0 . . . . ?
B7 B2 B3 B8 34.6 . . . . ?
B7 B2 B3 B9 -3.4 . . . . ?
B7 B2 B8 B3 -140.0 . . . . ?
B7 B2 B8 B9 -101.9 . . . . ?
B7 B2 B8 B11 -37.1 . . . . ?
B7 B6 B10 B4 65.7 . . . . ?
B7 B6 B10 B5 102.7 . . . . ?
B7 B6 B10 B9 3.8 . . . . ?
B7 B6 B10 B11 -35.7 . . . . ?
B7 B6 B11 B8 38.4 . . . . ?
B7 B6 B11 B9 100.3 . . . . ?
B7 B6 B11 B10 140.2 . . . . ?
B7 B8 B9 B3 -103.0 . . . . ?
B7 B8 B9 B4 -63.9 . . . . ?
B7 B8 B9 B10 1.0 . . . . ?
B7 B8 B9 B11 38.1 . . . . ?
B7 B8 B11 B6 -37.8 . . . . ?
B7 B8 B11 B9 -137.7 . . . . ?
B7 B8 B11 B10 -99.6 . . . . ?
B8 B2 B3 C11 -131.9 . . . . ?
B8 B2 B3 B4 -99.6 . . . . ?
B8 B2 B3 B9 -38.0 . . . . ?
B8 B2 B7 B1 139.3 . . . . ?
B8 B2 B7 B6 100.7 . . . . ?
B8 B2 B7 B11 35.8 . . . . ?
B8 B3 B4 C11 -99.5 . . . . ?
B8 B3 B4 B5 -64.0 . . . . ?
B8 B3 B4 B9 36.5 . . . . ?
B8 B3 B4 B10 -2.4 . . . . ?
B8 B3 B9 B4 -138.8 . . . . ?
B8 B3 B9 B10 -98.1 . . . . ?
B8 B3 B9 B11 -35.0 . . . . ?
B8 B7 B11 B6 136.4 . . . . ?
B8 B7 B11 B9 37.2 . . . . ?
B8 B7 B11 B10 101.4 . . . . ?
B8 B9 B10 B4 -103.7 . . . . ?
B8 B9 B10 B5 -67.3 . . . . ?
B8 B9 B10 B6 -3.0 . . . . ?
B8 B9 B10 B11 37.6 . . . . ?
B8 B9 B11 B6 -99.1 . . . . ?
B8 B9 B11 B7 -37.6 . . . . ?
B8 B9 B11 B10 -137.9 . . . . ?
B9 B3 B4 C11 -136.0 . . . . ?
B9 B3 B4 B5 -100.5 . . . . ?
B9 B3 B4 B10 -38.9 . . . . ?
B9 B3 B8 B2 138.5 . . . . ?
B9 B3 B8 B7 101.1 . . . . ?
B9 B3 B8 B11 36.1 . . . . ?
B9 B4 B5 C11 -95.3 . . . . ?
B9 B4 B5 B1 -65.5 . . . . ?
B9 B4 B5 B6 -0.2 . . . . ?
B9 B4 B5 B10 37.4 . . . . ?
B9 B4 B10 B5 -138.2 . . . . ?
B9 B4 B10 B6 -100.1 . . . . ?
B9 B4 B10 B11 -34.7 . . . . ?
B9 B8 B11 B6 99.9 . . . . ?
B9 B8 B11 B7 137.7 . . . . ?
B9 B8 B11 B10 38.1 . . . . ?
B9 B10 B11 B6 -135.4 . . . . ?
B9 B10 B11 B7 -100.5 . . . . ?
B9 B10 B11 B8 -37.2 . . . . ?
B10 B4 B5 C11 -132.7 . . . . ?
B10 B4 B5 B1 -102.8 . . . . ?
B10 B4 B5 B6 -37.5 . . . . ?
B10 B4 B9 B3 135.8 . . . . ?
B10 B4 B9 B8 99.4 . . . . ?
B10 B4 B9 B11 34.9 . . . . ?
B10 B5 B6 B1 -139.3 . . . . ?
B10 B5 B6 B7 -100.1 . . . . ?
B10 B5 B6 B11 -36.7 . . . . ?
B10 B6 B7 B1 -102.1 . . . . ?
B10 B6 B7 B2 -65.6 . . . . ?
B10 B6 B7 B8 -3.2 . . . . ?
B10 B6 B7 B11 35.5 . . . . ?
B10 B6 B11 B7 -140.2 . . . . ?
B10 B6 B11 B8 -101.7 . . . . ?
B10 B6 B11 B9 -39.9 . . . . ?
B10 B9 B11 B6 38.8 . . . . ?
B10 B9 B11 B7 100.4 . . . . ?
B10 B9 B11 B8 137.9 . . . . ?
B11 B6 B7 B1 -137.6 . . . . ?
B11 B6 B7 B2 -101.1 . . . . ?
B11 B6 B7 B8 -38.7 . . . . ?
B11 B6 B10 B4 101.4 . . . . ?
B11 B6 B10 B5 138.4 . . . . ?
B11 B6 B10 B9 39.5 . . . . ?
B11 B7 B8 B2 -139.7 . . . . ?
B11 B7 B8 B3 -104.3 . . . . ?
B11 B7 B8 B9 -38.2 . . . . ?
B11 B8 B9 B3 -141.1 . . . . ?
B11 B8 B9 B4 -102.0 . . . . ?
B11 B8 B9 B10 -37.1 . . . . ?
B11 B9 B10 B4 -141.2 . . . . ?
B11 B9 B10 B5 -104.9 . . . . ?
B11 B9 B10 B6 -40.5 . . . . ?
B12 C12 B13 B14 -144.6 . . . . ?
B12 C12 B13 B17 -40.1 . . . . ?
B12 C12 B13 B18 -103.0 . . . . ?
B12 C12 B14 B13 36.1 . . . . ?
B12 C12 B14 B15 -102.7 . . . . ?
B12 C12 B14 B18 -2.3 . . . . ?
B12 C12 B14 B19 -61.7 . . . . ?
B12 C12 B15 B14 111.1 . . . . ?
B12 C12 B15 B16 -35.6 . . . . ?
B12 C12 B15 B19 67.1 . . . . ?
B12 C12 B15 B20 6.1 . . . . ?
B12 C12 B16 B15 143.2 . . . . ?
B12 C12 B16 B20 103.2 . . . . ?
B12 C12 B16 B21 40.7 . . . . ?
B12 B13 B14 C12 -31.2 . . . . ?
B12 B13 B14 B15 4.2 . . . . ?
B12 B13 B14 B18 101.9 . . . . ?
B12 B13 B14 B19 64.1 . . . . ?
B12 B13 B17 B18 -138.6 . . . . ?
B12 B13 B17 B21 -38.8 . . . . ?
B12 B13 B17 B22 -102.1 . . . . ?
B12 B13 B18 B14 -100.8 . . . . ?
B12 B13 B18 B17 37.0 . . . . ?
B12 B13 B18 B19 -61.5 . . . . ?
B12 B13 B18 B22 -1.0 . . . . ?
B12 B16 B20 B15 103.0 . . . . ?
B12 B16 B20 B19 64.8 . . . . ?
B12 B16 B20 B21 -37.2 . . . . ?
B12 B16 B20 B22 1.6 . . . . ?
B12 B16 B21 B17 38.0 . . . . ?
B12 B16 B21 B20 139.1 . . . . ?
B12 B16 B21 B22 102.1 . . . . ?
B12 B17 B18 B13 -37.3 . . . . ?
B12 B17 B18 B14 1.3 . . . . ?
B12 B17 B18 B19 63.8 . . . . ?
B12 B17 B18 B22 100.7 . . . . ?
B12 B17 B21 B16 -38.4 . . . . ?
B12 B17 B21 B20 -103.3 . . . . ?
B12 B17 B21 B22 -138.7 . . . . ?
B12 B17 B22 B18 -100.7 . . . . ?
B12 B17 B22 B19 -60.5 . . . . ?
B12 B17 B22 B20 1.5 . . . . ?
B12 B17 B22 B21 36.8 . . . . ?
B12 B21 B22 B17 -37.2 . . . . ?
B12 B21 B22 B18 0.9 . . . . ?
B12 B21 B22 B19 66.4 . . . . ?
B12 B21 B22 B20 102.7 . . . . ?
B13 C12 B12 B16 140.9 . . . . ?
B13 C12 B12 B17 40.1 . . . . ?
B13 C12 B12 B21 102.1 . . . . ?
B13 C12 B14 B15 -138.8 . . . . ?
B13 C12 B14 B18 -38.4 . . . . ?
B13 C12 B14 B19 -97.7 . . . . ?
B13 C12 B15 B14 41.2 . . . . ?
B13 C12 B15 B16 -105.5 . . . . ?
B13 C12 B15 B19 -2.9 . . . . ?
B13 C12 B15 B20 -63.8 . . . . ?
B13 C12 B16 B12 -38.3 . . . . ?
B13 C12 B16 B15 104.9 . . . . ?
B13 C12 B16 B20 65.0 . . . . ?
B13 C12 B16 B21 2.4 . . . . ?
B13 B12 B16 C12 34.0 . . . . ?
B13 B12 B16 B15 0.1 . . . . ?
B13 B12 B16 B20 -63.1 . . . . ?
B13 B12 B16 B21 -99.9 . . . . ?
B13 B12 B17 B18 36.9 . . . . ?
B13 B12 B17 B21 136.0 . . . . ?
B13 B12 B17 B22 98.8 . . . . ?
B13 B12 B21 B16 99.0 . . . . ?
B13 B12 B21 B17 -38.8 . . . . ?
B13 B12 B21 B20 61.3 . . . . ?
B13 B12 B21 B22 -1.5 . . . . ?
B13 B14 B15 C12 -34.6 . . . . ?
B13 B14 B15 B16 -4.3 . . . . ?
B13 B14 B15 B19 96.2 . . . . ?
B13 B14 B15 B20 62.8 . . . . ?
B13 B14 B18 B17 -37.8 . . . . ?
B13 B14 B18 B19 -135.3 . . . . ?
B13 B14 B18 B22 -102.1 . . . . ?
B13 B14 B19 B15 -99.0 . . . . ?
B13 B14 B19 B18 37.1 . . . . ?
B13 B14 B19 B20 -65.4 . . . . ?
B13 B14 B19 B22 1.4 . . . . ?
B13 B17 B18 B14 38.6 . . . . ?
B13 B17 B18 B19 101.1 . . . . ?
B13 B17 B18 B22 138.0 . . . . ?
B13 B17 B21 B12 39.3 . . . . ?
B13 B17 B21 B16 0.9 . . . . ?
B13 B17 B21 B20 -64.0 . . . . ?
B13 B17 B21 B22 -99.5 . . . . ?
B13 B17 B22 B18 -37.0 . . . . ?
B13 B17 B22 B19 3.2 . . . . ?
B13 B17 B22 B20 65.3 . . . . ?
B13 B17 B22 B21 100.6 . . . . ?
B13 B18 B19 B14 -40.4 . . . . ?
B13 B18 B19 B15 -1.2 . . . . ?
B13 B18 B19 B20 62.4 . . . . ?
B13 B18 B19 B22 101.1 . . . . ?
B13 B18 B22 B17 37.5 . . . . ?
B13 B18 B22 B19 -99.2 . . . . ?
B13 B18 B22 B20 -62.3 . . . . ?
B13 B18 B22 B21 0.1 . . . . ?
B14 C12 B12 B13 -36.9 . . . . ?
B14 C12 B12 B16 104.0 . . . . ?
B14 C12 B12 B17 3.2 . . . . ?
B14 C12 B12 B21 65.2 . . . . ?
B14 C12 B13 B12 144.6 . . . . ?
B14 C12 B13 B17 104.6 . . . . ?
B14 C12 B13 B18 41.7 . . . . ?
B14 C12 B15 B16 -146.7 . . . . ?
B14 C12 B15 B19 -44.0 . . . . ?
B14 C12 B15 B20 -105.0 . . . . ?
B14 C12 B16 B12 -111.2 . . . . ?
B14 C12 B16 B15 32.0 . . . . ?
B14 C12 B16 B20 -7.9 . . . . ?
B14 C12 B16 B21 -70.5 . . . . ?
B14 B13 B17 B12 99.8 . . . . ?
B14 B13 B17 B18 -38.8 . . . . ?
B14 B13 B17 B21 61.0 . . . . ?
B14 B13 B17 B22 -2.3 . . . . ?
B14 B13 B18 B17 137.8 . . . . ?
B14 B13 B18 B19 39.4 . . . . ?
B14 B13 B18 B22 99.8 . . . . ?
B14 B15 B16 C12 -30.6 . . . . ?
B14 B15 B16 B12 2.8 . . . . ?
B14 B15 B16 B20 103.3 . . . . ?
B14 B15 B16 B21 67.5 . . . . ?
B14 B15 B19 B18 -40.3 . . . . ?
B14 B15 B19 B20 -143.0 . . . . ?
B14 B15 B19 B22 -104.5 . . . . ?
B14 B15 B20 B16 -103.4 . . . . ?
B14 B15 B20 B19 34.8 . . . . ?
B14 B15 B20 B21 -68.4 . . . . ?
B14 B15 B20 B22 -2.6 . . . . ?
B14 B18 B19 B15 39.1 . . . . ?
B14 B18 B19 B20 102.8 . . . . ?
B14 B18 B19 B22 141.4 . . . . ?
B14 B18 B22 B17 102.6 . . . . ?
B14 B18 B22 B19 -34.1 . . . . ?
B14 B18 B22 B20 2.8 . . . . ?
B14 B18 B22 B21 65.1 . . . . ?
B14 B19 B20 B15 -33.6 . . . . ?
B14 B19 B20 B16 3.3 . . . . ?
B14 B19 B20 B21 65.9 . . . . ?
B14 B19 B20 B22 104.7 . . . . ?
B14 B19 B22 B17 -2.9 . . . . ?
B14 B19 B22 B18 36.5 . . . . ?
B14 B19 B22 B20 -101.8 . . . . ?
B14 B19 B22 B21 -65.2 . . . . ?
B15 C12 B12 B13 -106.4 . . . . ?
B15 C12 B12 B16 34.5 . . . . ?
B15 C12 B12 B17 -66.3 . . . . ?
B15 C12 B12 B21 -4.3 . . . . ?
B15 C12 B13 B12 105.1 . . . . ?
B15 C12 B13 B14 -39.6 . . . . ?
B15 C12 B13 B17 65.0 . . . . ?
B15 C12 B13 B18 2.1 . . . . ?
B15 C12 B14 B13 138.8 . . . . ?
B15 C12 B14 B18 100.4 . . . . ?
B15 C12 B14 B19 41.0 . . . . ?
B15 C12 B16 B12 -143.2 . . . . ?
B15 C12 B16 B20 -40.0 . . . . ?
B15 C12 B16 B21 -102.5 . . . . ?
B15 B14 B18 B13 98.0 . . . . ?
B15 B14 B18 B17 60.2 . . . . ?
B15 B14 B18 B19 -37.4 . . . . ?
B15 B14 B18 B22 -4.1 . . . . ?
B15 B14 B19 B18 136.1 . . . . ?
B15 B14 B19 B20 33.7 . . . . ?
B15 B14 B19 B22 100.4 . . . . ?
B15 B16 B20 B19 -38.3 . . . . ?
B15 B16 B20 B21 -140.2 . . . . ?
B15 B16 B20 B22 -101.5 . . . . ?
B15 B16 B21 B12 -103.8 . . . . ?
B15 B16 B21 B17 -65.7 . . . . ?
B15 B16 B21 B20 35.3 . . . . ?
B15 B16 B21 B22 -1.7 . . . . ?
B15 B19 B20 B16 36.9 . . . . ?
B15 B19 B20 B21 99.5 . . . . ?
B15 B19 B20 B22 138.3 . . . . ?
B15 B19 B22 B17 61.3 . . . . ?
B15 B19 B22 B18 100.7 . . . . ?
B15 B19 B22 B20 -37.6 . . . . ?
B15 B19 B22 B21 -1.0 . . . . ?
B15 B20 B21 B12 2.7 . . . . ?
B15 B20 B21 B16 -34.9 . . . . ?
B15 B20 B21 B17 66.9 . . . . ?
B15 B20 B21 B22 103.0 . . . . ?
B15 B20 B22 B17 -64.4 . . . . ?
B15 B20 B22 B18 -0.2 . . . . ?
B15 B20 B22 B19 38.4 . . . . ?
B15 B20 B22 B21 -99.7 . . . . ?
B16 C12 B12 B13 -140.9 . . . . ?
B16 C12 B12 B17 -100.8 . . . . ?
B16 C12 B12 B21 -38.8 . . . . ?
B16 C12 B13 B12 38.2 . . . . ?
B16 C12 B13 B14 -106.4 . . . . ?
B16 C12 B13 B17 -1.9 . . . . ?
B16 C12 B13 B18 -64.8 . . . . ?
B16 C12 B14 B13 107.3 . . . . ?
B16 C12 B14 B15 -31.5 . . . . ?
B16 C12 B14 B18 68.9 . . . . ?
B16 C12 B14 B19 9.5 . . . . ?
B16 C12 B15 B14 146.7 . . . . ?
B16 C12 B15 B19 102.6 . . . . ?
B16 C12 B15 B20 41.7 . . . . ?
B16 B12 B13 C12 -33.7 . . . . ?
B16 B12 B13 B14 -2.7 . . . . ?
B16 B12 B13 B17 100.0 . . . . ?
B16 B12 B13 B18 62.5 . . . . ?
B16 B12 B17 B13 -99.4 . . . . ?
B16 B12 B17 B18 -62.5 . . . . ?
B16 B12 B17 B21 36.6 . . . . ?
B16 B12 B17 B22 -0.6 . . . . ?
B16 B12 B21 B17 -137.8 . . . . ?
B16 B12 B21 B20 -37.6 . . . . ?
B16 B12 B21 B22 -100.4 . . . . ?
B16 B15 B19 B14 104.5 . . . . ?
B16 B15 B19 B18 64.2 . . . . ?
B16 B15 B19 B20 -38.4 . . . . ?
B16 B15 B19 B22 0.0 . . . . ?
B16 B15 B20 B19 138.2 . . . . ?
B16 B15 B20 B21 35.0 . . . . ?
B16 B15 B20 B22 100.8 . . . . ?
B16 B20 B21 B12 37.6 . . . . ?
B16 B20 B21 B17 101.8 . . . . ?
B16 B20 B21 B22 138.0 . . . . ?
B16 B20 B22 B17 -1.9 . . . . ?
B16 B20 B22 B18 62.2 . . . . ?
B16 B20 B22 B19 100.8 . . . . ?
B16 B20 B22 B21 -37.3 . . . . ?
B16 B21 B22 B17 -101.9 . . . . ?
B16 B21 B22 B18 -63.8 . . . . ?
B16 B21 B22 B19 1.7 . . . . ?
B16 B21 B22 B20 38.0 . . . . ?
B17 B12 B13 C12 -133.7 . . . . ?
B17 B12 B13 B14 -102.7 . . . . ?
B17 B12 B13 B18 -37.5 . . . . ?
B17 B12 B16 C12 96.5 . . . . ?
B17 B12 B16 B15 62.6 . . . . ?
B17 B12 B16 B20 -0.6 . . . . ?
B17 B12 B16 B21 -37.4 . . . . ?
B17 B12 B21 B16 137.8 . . . . ?
B17 B12 B21 B20 100.1 . . . . ?
B17 B12 B21 B22 37.3 . . . . ?
B17 B13 B14 C12 -94.6 . . . . ?
B17 B13 B14 B15 -59.2 . . . . ?
B17 B13 B14 B18 38.5 . . . . ?
B17 B13 B14 B19 0.7 . . . . ?
B17 B13 B18 B14 -137.8 . . . . ?
B17 B13 B18 B19 -98.5 . . . . ?
B17 B13 B18 B22 -38.0 . . . . ?
B17 B18 B19 B14 -103.0 . . . . ?
B17 B18 B19 B15 -63.8 . . . . ?
B17 B18 B19 B20 -0.1 . . . . ?
B17 B18 B19 B22 38.5 . . . . ?
B17 B18 B22 B19 -136.7 . . . . ?
B17 B18 B22 B20 -99.8 . . . . ?
B17 B18 B22 B21 -37.4 . . . . ?
B17 B21 B22 B18 38.1 . . . . ?
B17 B21 B22 B19 103.6 . . . . ?
B17 B21 B22 B20 139.9 . . . . ?
B18 B13 B14 C12 -133.0 . . . . ?
B18 B13 B14 B15 -97.6 . . . . ?
B18 B13 B14 B19 -37.8 . . . . ?
B18 B13 B17 B12 138.6 . . . . ?
B18 B13 B17 B21 99.8 . . . . ?
B18 B13 B17 B22 36.5 . . . . ?
B18 B14 B15 C12 -93.3 . . . . ?
B18 B14 B15 B16 -63.0 . . . . ?
B18 B14 B15 B19 37.5 . . . . ?
B18 B14 B15 B20 4.1 . . . . ?
B18 B14 B19 B15 -136.1 . . . . ?
B18 B14 B19 B20 -102.4 . . . . ?
B18 B14 B19 B22 -35.7 . . . . ?
B18 B17 B21 B12 101.8 . . . . ?
B18 B17 B21 B16 63.4 . . . . ?
B18 B17 B21 B20 -1.5 . . . . ?
B18 B17 B21 B22 -37.0 . . . . ?
B18 B17 B22 B19 40.2 . . . . ?
B18 B17 B22 B20 102.2 . . . . ?
B18 B17 B22 B21 137.5 . . . . ?
B18 B19 B20 B15 -100.3 . . . . ?
B18 B19 B20 B16 -63.4 . . . . ?
B18 B19 B20 B21 -0.8 . . . . ?
B18 B19 B20 B22 37.9 . . . . ?
B18 B19 B22 B17 -39.4 . . . . ?
B18 B19 B22 B20 -138.2 . . . . ?
B18 B19 B22 B21 -101.7 . . . . ?
B19 B14 B15 C12 -130.7 . . . . ?
B19 B14 B15 B16 -100.4 . . . . ?
B19 B14 B15 B20 -33.3 . . . . ?
B19 B14 B18 B13 135.3 . . . . ?
B19 B14 B18 B17 97.5 . . . . ?
B19 B14 B18 B22 33.2 . . . . ?
B19 B15 B16 C12 -97.1 . . . . ?
B19 B15 B16 B12 -63.7 . . . . ?
B19 B15 B16 B20 36.8 . . . . ?
B19 B15 B16 B21 1.0 . . . . ?
B19 B15 B20 B16 -138.2 . . . . ?
B19 B15 B20 B21 -103.2 . . . . ?
B19 B15 B20 B22 -37.4 . . . . ?
B19 B18 B22 B17 136.7 . . . . ?
B19 B18 B22 B20 36.9 . . . . ?
B19 B18 B22 B21 99.3 . . . . ?
B19 B20 B21 B12 -62.7 . . . . ?
B19 B20 B21 B16 -100.3 . . . . ?
B19 B20 B21 B17 1.5 . . . . ?
B19 B20 B21 B22 37.6 . . . . ?
B19 B20 B22 B17 -102.7 . . . . ?
B19 B20 B22 B18 -38.6 . . . . ?
B19 B20 B22 B21 -138.1 . . . . ?
B20 B15 B16 C12 -133.8 . . . . ?
B20 B15 B16 B12 -100.5 . . . . ?
B20 B15 B16 B21 -35.7 . . . . ?
B20 B15 B19 B14 143.0 . . . . ?
B20 B15 B19 B18 102.6 . . . . ?
B20 B15 B19 B22 38.5 . . . . ?
B20 B16 B21 B12 -139.1 . . . . ?
B20 B16 B21 B17 -101.1 . . . . ?
B20 B16 B21 B22 -37.0 . . . . ?
B20 B19 B22 B17 98.9 . . . . ?
B20 B19 B22 B18 138.2 . . . . ?
B20 B19 B22 B21 36.5 . . . . ?
B20 B21 B22 B17 -139.9 . . . . ?
B20 B21 B22 B18 -101.9 . . . . ?
B20 B21 B22 B19 -36.4 . . . . ?
B21 B12 B13 C12 -94.7 . . . . ?
B21 B12 B13 B14 -63.7 . . . . ?
B21 B12 B13 B17 39.0 . . . . ?
B21 B12 B13 B18 1.5 . . . . ?
B21 B12 B16 C12 134.0 . . . . ?
B21 B12 B16 B15 100.0 . . . . ?
B21 B12 B16 B20 36.8 . . . . ?
B21 B12 B17 B13 -136.0 . . . . ?
B21 B12 B17 B18 -99.1 . . . . ?
B21 B12 B17 B22 -37.1 . . . . ?
B21 B16 B20 B15 140.2 . . . . ?
B21 B16 B20 B19 101.9 . . . . ?
B21 B16 B20 B22 38.7 . . . . ?
B21 B17 B18 B13 -100.2 . . . . ?
B21 B17 B18 B14 -61.5 . . . . ?
B21 B17 B18 B19 1.0 . . . . ?
B21 B17 B18 B22 37.8 . . . . ?
B21 B17 B22 B18 -137.5 . . . . ?
B21 B17 B22 B19 -97.3 . . . . ?
B21 B17 B22 B20 -35.3 . . . . ?
B21 B20 B22 B17 35.4 . . . . ?
B21 B20 B22 B18 99.5 . . . . ?
B21 B20 B22 B19 138.1 . . . . ?
B22 B17 B18 B13 -138.0 . . . . ?
B22 B17 B18 B14 -99.3 . . . . ?
B22 B17 B18 B19 -36.8 . . . . ?
B22 B17 B21 B12 138.7 . . . . ?
B22 B17 B21 B16 100.3 . . . . ?
B22 B17 B21 B20 35.5 . . . . ?
B22 B18 B19 B14 -141.4 . . . . ?
B22 B18 B19 B15 -102.3 . . . . ?
B22 B18 B19 B20 -38.6 . . . . ?
B22 B19 B20 B15 -138.3 . . . . ?
B22 B19 B20 B16 -101.4 . . . . ?
B22 B19 B20 B21 -38.8 . . . . ?
B22 B20 B21 B12 -100.4 . . . . ?
B22 B20 B21 B16 -138.0 . . . . ?
B22 B20 B21 B17 -36.2 . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 -0.500 -0.363 0.500 904.4 249.5 ?
2 0.461 0.593 0.080 8.4 0.9 ?
3 0.539 0.407 0.920 8.4 0.8 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_210914yhb_0m
_database_code_depnum_ccdc_archive 'CCDC 2168883'
loop_
_audit_author_name
_audit_author_address
'Haibo Yao'
;Guangxi minzu university
China
;
_audit_update_record             
;
2022-04-26 deposited with the CCDC.	2026-02-11 downloaded from the CCDC.
;
_audit_creation_date             2021-09-14
_audit_creation_method           
;
Olex2 1.5
(compiled 2021.08.20 svn.r13c46975 for OlexSys, GUI svn.r6396)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C53 H92 B22 N6 Pt, C3 H6 O'
_chemical_formula_sum            'C56 H98 B22 N6 O Pt'
_chemical_formula_weight         1304.31
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0137 0.0067 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0070 0.0029 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0241 0.0134 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0389 0.0241 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -5.3886 5.5592 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   14.3504(2)
_cell_length_b                   14.5641(2)
_cell_length_c                   18.6103(2)
_cell_angle_alpha                76.6580(10)
_cell_angle_beta                 67.4670(10)
_cell_angle_gamma                73.8900(10)
_cell_volume                     3417.45(8)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    9786
_cell_measurement_temperature    213.01
_cell_measurement_theta_max      54.901
_cell_measurement_theta_min      3.438
_shelx_estimated_absorpt_T_max   0.871
_shelx_estimated_absorpt_T_min   0.805
_exptl_absorpt_coefficient_mu    2.832
_exptl_absorpt_correction_T_max  0.7508
_exptl_absorpt_correction_T_min  0.4806
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1146 before and 0.0507 after correction.
The Ratio of minimum to maximum transmission is 0.6401.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.268
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             1344
_exptl_crystal_size_max          0.08
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.05
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0349
_diffrn_reflns_av_unetI/netI     0.0295
_diffrn_reflns_Laue_measured_fraction_full 0.994
_diffrn_reflns_Laue_measured_fraction_max 0.992
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            47187
_diffrn_reflns_point_group_measured_fraction_full 0.994
_diffrn_reflns_point_group_measured_fraction_max 0.992
_diffrn_reflns_theta_full        53.594
_diffrn_reflns_theta_max         54.931
_diffrn_reflns_theta_min         3.437
_diffrn_ambient_temperature      213.01
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           GaK\a
_diffrn_radiation_wavelength     1.34139
_diffrn_source                   ?
_diffrn_source_current           2.86
_diffrn_source_power             0.1995708
_diffrn_source_voltage           69.78
_diffrn_standards_number         0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                12363
_reflns_number_total             12925
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT v8.37A (Bruker, 2015)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT v8.37A (Bruker, 2015)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         1.459
_refine_diff_density_min         -1.325
_refine_diff_density_rms         0.101
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.112
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     779
_refine_ls_number_reflns         12925
_refine_ls_number_restraints     126
_refine_ls_R_factor_all          0.0420
_refine_ls_R_factor_gt           0.0403
_refine_ls_restrained_S_all      1.155
_refine_ls_shift/su_max          0.006
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1000P)²] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1230
_refine_ls_wR_factor_ref         0.1260
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Restrained distances
 C48-C47 = C49-C48 = C49-C50 = C51-C50 = C52-C51 = C52-C53
 1.53 with sigma of 0.01
 C40-C39 = C40-C41 = C38-C39 = C38-C37 = C36-C35 = C34-C35
 1.53 with sigma of 0.01
 C56-C55 = C55-C54
 1.52 with sigma of 0.01
 C51-C49
 2.45 with sigma of 0.01
 C51-C50 = C50-C49 = C52-C51
 1.53 with sigma of 0.01
 H15B-H54B_$1
 2.1 with sigma of 0.01
 H38B-H54C = H38B-H54B
 2.1 with sigma of 0.01
3. Rigid bond restraints
 C31, C32, C49, C50, C52, C53
 with sigma for 1-2 distances of 0.005 and sigma for 1-3 distances of 0.005
4. Uiso/Uaniso restraints and constraints
C47 \\sim C48 \\sim C49 \\sim C50 \\sim C51 \\sim C52 \\sim C53: within 2A with
sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
C36 \\sim C37 \\sim C38 \\sim C39 \\sim C40 \\sim C41: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
C55 \\sim C56 \\sim C54 \\sim O029: within 2A with sigma of 0.01 and sigma for
terminal atoms of 0.02 within 2A
C44 \\sim C45 \\sim C46 \\sim C47 \\sim C48 \\sim C49 \\sim C50 \\sim C51 \\sim
C52 \\sim C53: within 2A with sigma of 0.005 and sigma for terminal atoms of
0.01 within 2A
5.a Secondary CH2 refined with riding coordinates:
 C15(H15A,H15B), C16(H16A,H16B), C17(H17A,H17B), C30(H30A,H30B), C31(H31A,
 H31B), C32(H32A,H32B), C33(H33A,H33B), C34(H34A,H34B), C35(H35A,H35B),
 C36(H36A,H36B), C37(H37A,H37B), C38(H38A,H38B), C39(H39A,H39B), C40(H40A,H40B),
  C42(H42A,H42B), C43(H43A,H43B), C44(H44A,H44B), C45(H45A,H45B), C46(H46A,
 H46B), C47(H47A,H47B), C48(H48A,H48B), C49(H49A,H49B), C50(H50A,H50B),
 C51(H51A,H51B), C52(H52A,H52B)
5.b Aromatic/amide H refined with riding coordinates:
 C3(H3), C5(H5), C6(H6), C9(H9), C10(H10), C12(H12), C20(H20), C21(H21),
 C22(H22), C23(H23), C25(H25), C26(H26), C27(H27), C28(H28)
5.c Idealised Me refined as rotating group:
 C41(H41A,H41B,H41C), C53(H53A,H53B,H53C), C54(H54A,H54B,H54C), C56(H56A,H56B,
 H56C)
5.d Boron cage BH refined with riding coordinates:
 B1(H1), B2(H2), B3(H3A), B4(H4), B5(H5A), B6(H6A), B7(H7), B8(H8), B9(H9A),
 B10(H10A), B11(H11), B12(H12A), B13(H13), B14(H14), B15(H15), B16(H16),
 B17(H17), B18(H18), B19(H19), B20(H20A), B21(H21A), B22(H22A)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.35234(2) 0.14719(2) 0.76578(2) 0.03270(8) Uani 1 1 d . . . . .
N1 N 0.4859(2) 0.0966(2) 0.67661(18) 0.0367(6) Uani 1 1 d . . . . .
N2 N 0.4167(2) 0.0260(2) 0.82756(18) 0.0380(6) Uani 1 1 d . . . . .
N3 N 0.3106(2) 0.35313(19) 0.69076(17) 0.0404(6) Uani 1 1 d . . . . .
N4 N 0.2118(2) 0.26945(19) 0.68296(16) 0.0378(6) Uani 1 1 d . . . . .
N5 N 0.1369(2) 0.1522(3) 0.87373(19) 0.0445(7) Uani 1 1 d . . . . .
N6 N 0.2148(2) 0.2236(2) 0.91775(16) 0.0431(6) Uani 1 1 d . . . . .
C1 C 0.2919(3) 0.2638(3) 0.7060(2) 0.0377(7) Uani 1 1 d . . . . .
C2 C 0.2262(3) 0.1792(3) 0.8573(2) 0.0404(8) Uani 1 1 d . . . . .
C3 C 0.5126(3) 0.1327(2) 0.60028(18) 0.0348(6) Uani 1 1 d . . . . .
H3 H 0.466768 0.185745 0.583997 0.042 Uiso 1 1 calc R U . . .
C4 C 0.6034(3) 0.0966(2) 0.5444(2) 0.0382(7) Uani 1 1 d . . . . .
C5 C 0.6694(3) 0.0192(3) 0.5706(2) 0.0482(8) Uani 1 1 d . . . . .
H5 H 0.733092 -0.006866 0.534660 0.058 Uiso 1 1 calc R U . . .
C6 C 0.6432(3) -0.0204(3) 0.6491(2) 0.0520(9) Uani 1 1 d . . . . .
H6 H 0.688379 -0.072796 0.666677 0.062 Uiso 1 1 calc R U . . .
C7 C 0.5492(3) 0.0186(2) 0.70068(19) 0.0400(7) Uani 1 1 d . . . . .
C8 C 0.5106(3) -0.0218(2) 0.78469(19) 0.0402(7) Uani 1 1 d . . . . .
C9 C 0.5617(3) -0.1023(3) 0.8205(2) 0.0515(9) Uani 1 1 d . . . . .
H9 H 0.627150 -0.135018 0.791347 0.062 Uiso 1 1 calc R U . . .
C10 C 0.5174(3) -0.1354(3) 0.8991(2) 0.0500(8) Uani 1 1 d . . . . .
H10 H 0.552421 -0.190572 0.923359 0.060 Uiso 1 1 calc R U . . .
C11 C 0.4208(3) -0.0866(2) 0.9422(2) 0.0404(7) Uani 1 1 d . . . . .
C12 C 0.3744(3) -0.0062(2) 0.90279(18) 0.0390(7) Uani 1 1 d . . . . .
H12 H 0.309016 0.027668 0.930901 0.047 Uiso 1 1 calc R U . . .
C13 C 0.6288(3) 0.1363(2) 0.45857(18) 0.0383(7) Uani 1 1 d . . . . .
C14 C 0.3678(3) -0.1166(3) 1.02835(19) 0.0421(7) Uani 1 1 d . . . . .
C15 C 0.1714(3) 0.1875(3) 0.6831(2) 0.0442(7) Uani 1 1 d . . . . .
H15A H 0.228086 0.130600 0.675113 0.053 Uiso 1 1 calc R U . . .
H15B H 0.147133 0.201355 0.638371 0.053 Uiso 1 1 calc DR U . . .
C16 C 0.0833(3) 0.1626(3) 0.7578(2) 0.0482(8) Uani 1 1 d . . . . .
H16A H 0.042400 0.129536 0.744544 0.058 Uiso 1 1 calc R U . . .
H16B H 0.038299 0.222915 0.776184 0.058 Uiso 1 1 calc R U . . .
C17 C 0.1169(3) 0.0989(3) 0.8256(2) 0.0478(8) Uani 1 1 d . . . . .
H17A H 0.062901 0.063533 0.859299 0.057 Uiso 1 1 calc R U . . .
H17B H 0.179686 0.051316 0.803627 0.057 Uiso 1 1 calc R U . . .
C18 C 0.1762(3) 0.3649(3) 0.6539(2) 0.0454(8) Uani 1 1 d . . . . .
C19 C 0.2398(3) 0.4179(2) 0.6589(2) 0.0438(7) Uani 1 1 d . . . . .
C20 C 0.2249(4) 0.5176(3) 0.6372(3) 0.0612(10) Uani 1 1 d . . . . .
H20 H 0.268306 0.553675 0.639916 0.073 Uiso 1 1 calc R U . . .
C21 C 0.1425(5) 0.5600(4) 0.6116(4) 0.0845(18) Uani 1 1 d . . . . .
H21 H 0.127705 0.627439 0.598116 0.101 Uiso 1 1 calc R U . . .
C22 C 0.0802(5) 0.5061(4) 0.6048(4) 0.0797(16) Uani 1 1 d . . . . .
H22 H 0.026688 0.537864 0.584851 0.096 Uiso 1 1 calc R U . . .
C23 C 0.0951(3) 0.4084(3) 0.6266(3) 0.0640(11) Uani 1 1 d . . . . .
H23 H 0.052181 0.372369 0.623204 0.077 Uiso 1 1 calc R U . . .
C24 C 0.0659(3) 0.1797(3) 0.9453(2) 0.0544(9) Uani 1 1 d . . . . .
C25 C -0.0329(4) 0.1656(5) 0.9880(3) 0.0804(16) Uani 1 1 d . . . . .
H25 H -0.065266 0.132237 0.970016 0.097 Uiso 1 1 calc R U . . .
C26 C -0.0814(4) 0.2024(7) 1.0575(3) 0.120(3) Uani 1 1 d . . . . .
H26 H -0.149677 0.196329 1.087142 0.145 Uiso 1 1 calc R U . . .
C27 C -0.0315(5) 0.2491(7) 1.0856(3) 0.106(3) Uani 1 1 d . . . . .
H27 H -0.067837 0.274737 1.133052 0.127 Uiso 1 1 calc R U . . .
C28 C 0.0674(4) 0.2582(5) 1.0463(3) 0.0812(16) Uani 1 1 d . . . . .
H28 H 0.101712 0.286116 1.066929 0.097 Uiso 1 1 calc R U . . .
C29 C 0.1166(3) 0.2238(4) 0.9731(2) 0.0538(10) Uani 1 1 d . . . . .
C30 C 0.3948(3) 0.3801(3) 0.7017(3) 0.0531(9) Uani 1 1 d . . . . .
H30A H 0.415420 0.333338 0.742912 0.064 Uiso 1 1 calc R U . . .
H30B H 0.369626 0.443529 0.719701 0.064 Uiso 1 1 calc R U . . .
C31 C 0.4874(4) 0.3840(4) 0.6285(4) 0.0902(17) Uani 1 1 d . U . . .
H31A H 0.468864 0.429936 0.586079 0.108 Uiso 1 1 calc R U . . .
H31B H 0.517119 0.320236 0.611196 0.108 Uiso 1 1 calc R U . . .
C32 C 0.5699(5) 0.4195(4) 0.6529(3) 0.0833(15) Uani 1 1 d . U . . .
H32A H 0.544760 0.487954 0.659420 0.100 Uiso 1 1 calc R U . . .
H32B H 0.573277 0.382898 0.703420 0.100 Uiso 1 1 calc R U . . .
C33 C 0.6688(6) 0.4067(7) 0.5965(6) 0.125(3) Uani 1 1 d . . . . .
H33A H 0.663830 0.433687 0.544461 0.150 Uiso 1 1 calc R U . . .
H33B H 0.698632 0.337475 0.596570 0.150 Uiso 1 1 calc R U . . .
C34 C 0.7389(5) 0.4537(4) 0.6110(5) 0.104(2) Uani 1 1 d D . . . .
H34A H 0.809993 0.429452 0.578234 0.125 Uiso 1 1 calc R U . . .
H34B H 0.734674 0.434510 0.666037 0.125 Uiso 1 1 calc R U . . .
C35 C 0.7152(5) 0.5628(4) 0.5942(5) 0.096(2) Uani 1 1 d D . . . .
H35A H 0.650801 0.588203 0.634478 0.115 Uiso 1 1 calc R U . . .
H35B H 0.704945 0.582625 0.543245 0.115 Uiso 1 1 calc R U . . .
C36 C 0.8009(4) 0.6057(4) 0.5929(4) 0.0882(16) Uani 1 1 d D U . . .
H36A H 0.865838 0.577024 0.554761 0.106 Uiso 1 1 calc R U . . .
H36B H 0.808570 0.588028 0.644778 0.106 Uiso 1 1 calc R U . . .
C37 C 0.7829(6) 0.7147(5) 0.5721(5) 0.1067(18) Uani 1 1 d D U . . .
H37A H 0.713657 0.742729 0.605559 0.128 Uiso 1 1 calc R U . . .
H37B H 0.784776 0.731611 0.517548 0.128 Uiso 1 1 calc R U . . .
C38 C 0.8603(7) 0.7603(6) 0.5812(5) 0.130(2) Uani 1 1 d D U . . .
H38A H 0.848976 0.828676 0.559079 0.156 Uiso 1 1 calc R U . . .
H38B H 0.930057 0.729325 0.550499 0.156 Uiso 1 1 calc DR U . . .
C39 C 0.8541(8) 0.7520(7) 0.6692(6) 0.141(3) Uani 1 1 d D U . . .
H39A H 0.781608 0.762975 0.703355 0.169 Uiso 1 1 calc R U . . .
H39B H 0.887800 0.686550 0.685925 0.169 Uiso 1 1 calc R U . . .
C40 C 0.9070(9) 0.8263(7) 0.6786(7) 0.165(3) Uani 1 1 d D U . . .
H40A H 0.977090 0.820166 0.640052 0.198 Uiso 1 1 calc R U . . .
H40B H 0.868445 0.891701 0.667603 0.198 Uiso 1 1 calc R U . . .
C41 C 0.9121(9) 0.8114(8) 0.7600(7) 0.171(4) Uani 1 1 d D U . . .
H41A H 0.939994 0.862271 0.764921 0.256 Uiso 1 1 calc R U . . .
H41B H 0.956290 0.749315 0.769028 0.256 Uiso 1 1 calc R U . . .
H41C H 0.843328 0.813061 0.798530 0.256 Uiso 1 1 calc R U . . .
C42 C 0.2904(3) 0.2694(3) 0.9227(2) 0.0470(8) Uani 1 1 d . . . . .
H42A H 0.358306 0.246019 0.884927 0.056 Uiso 1 1 calc R U . . .
H42B H 0.295265 0.250636 0.975426 0.056 Uiso 1 1 calc R U . . .
C43 C 0.2623(3) 0.3789(3) 0.9059(3) 0.0550(9) Uani 1 1 d . . . . .
H43A H 0.252432 0.397403 0.854755 0.066 Uiso 1 1 calc R U . . .
H43B H 0.196690 0.402496 0.945915 0.066 Uiso 1 1 calc R U . . .
C44 C 0.3432(4) 0.4263(3) 0.9052(3) 0.0625(10) Uani 1 1 d . U . . .
H44A H 0.408431 0.402853 0.864776 0.075 Uiso 1 1 calc R U . . .
H44B H 0.353534 0.406749 0.956051 0.075 Uiso 1 1 calc R U . . .
C45 C 0.3168(5) 0.5354(4) 0.8895(4) 0.0789(12) Uani 1 1 d . U . . .
H45A H 0.318776 0.555085 0.834977 0.095 Uiso 1 1 calc R U . . .
H45B H 0.246118 0.558218 0.923650 0.095 Uiso 1 1 calc R U . . .
C46 C 0.3859(6) 0.5827(4) 0.9022(5) 0.0940(14) Uani 1 1 d . U . . .
H46A H 0.362612 0.652473 0.889806 0.113 Uiso 1 1 calc R U . . .
H46B H 0.375776 0.569328 0.958513 0.113 Uiso 1 1 calc R U . . .
C47 C 0.4933(7) 0.5596(5) 0.8612(6) 0.1201(19) Uani 1 1 d D U . . .
H47A H 0.501925 0.564754 0.805634 0.144 Uiso 1 1 calc R U . . .
H47B H 0.517053 0.491241 0.878722 0.144 Uiso 1 1 calc R U . . .
C48 C 0.5673(7) 0.6125(7) 0.8642(7) 0.156(2) Uani 1 1 d D U . . .
H48A H 0.545970 0.625149 0.918345 0.187 Uiso 1 1 calc R U . . .
H48B H 0.559574 0.675210 0.831283 0.187 Uiso 1 1 calc R U . . .
C49 C 0.6801(7) 0.5655(9) 0.8392(8) 0.193(3) Uani 1 1 d D U . . .
H49A H 0.705763 0.564828 0.782325 0.232 Uiso 1 1 calc R U . . .
H49B H 0.687580 0.498311 0.864561 0.232 Uiso 1 1 calc R U . . .
C50 C 0.7474(9) 0.6138(9) 0.8583(9) 0.206(3) Uani 1 1 d D U . . .
H50A H 0.749238 0.678420 0.828152 0.247 Uiso 1 1 calc R U . . .
H50B H 0.721452 0.619236 0.914411 0.247 Uiso 1 1 calc R U . . .
C51 C 0.8537(8) 0.5485(10) 0.8352(9) 0.210(3) Uani 1 1 d D U . . .
H51A H 0.864512 0.531477 0.784254 0.252 Uiso 1 1 calc R U . . .
H51B H 0.901712 0.590489 0.824583 0.252 Uiso 1 1 calc R U . . .
C52 C 0.8945(9) 0.4567(10) 0.8799(8) 0.209(4) Uani 1 1 d D U . . .
H52A H 0.878163 0.401638 0.868710 0.250 Uiso 1 1 calc R U . . .
H52B H 0.863262 0.459485 0.936501 0.250 Uiso 1 1 calc R U . . .
C53 C 1.0102(8) 0.4460(9) 0.8537(7) 0.185(4) Uani 1 1 d D U . . .
H53A H 1.031342 0.497738 0.811901 0.278 Uiso 1 1 calc R U . . .
H53B H 1.044456 0.384331 0.834784 0.278 Uiso 1 1 calc R U . . .
H53C H 1.029111 0.449056 0.897791 0.278 Uiso 1 1 calc R U . . .
B1 B 0.4117(4) -0.0990(4) 1.0962(3) 0.0580(12) Uani 1 1 d . . . . .
H1 H 0.479470 -0.066445 1.080825 0.070 Uiso 1 1 calc R U . . .
B2 B 0.4273(4) -0.2170(4) 1.0765(3) 0.0648(13) Uani 1 1 d . . . . .
H2 H 0.504483 -0.261855 1.049182 0.078 Uiso 1 1 calc R U . . .
B3 B 0.3182(4) -0.2193(3) 1.0531(3) 0.0568(11) Uani 1 1 d . . . . .
H3A H 0.323805 -0.264519 1.010497 0.068 Uiso 1 1 calc R U . . .
B4 B 0.2358(4) -0.1021(3) 1.0601(3) 0.0519(10) Uani 1 1 d . . . . .
H4 H 0.188257 -0.071089 1.021713 0.062 Uiso 1 1 calc R U . . .
B5 B 0.2925(4) -0.0286(3) 1.0871(2) 0.0488(9) Uani 1 1 d . . . . .
H5A H 0.282014 0.050162 1.066389 0.059 Uiso 1 1 calc R U . . .
B6 B 0.3838(5) -0.1919(5) 1.1749(3) 0.0737(16) Uani 1 1 d . . . . .
H6A H 0.431997 -0.219623 1.213010 0.088 Uiso 1 1 calc R U . . .
B7 B 0.3005(4) -0.0774(4) 1.1813(3) 0.0633(12) Uani 1 1 d . . . . .
H7 H 0.294382 -0.030950 1.223289 0.076 Uiso 1 1 calc R U . . .
B8 B 0.1906(4) -0.0798(4) 1.1591(3) 0.0548(10) Uani 1 1 d . . . . .
H8 H 0.113072 -0.035508 1.186487 0.066 Uiso 1 1 calc R U . . .
B9 B 0.2082(4) -0.1993(4) 1.1378(3) 0.0621(12) Uani 1 1 d . . . . .
H9A H 0.141546 -0.232770 1.151384 0.074 Uiso 1 1 calc R U . . .
B10 B 0.3274(5) -0.2689(4) 1.1475(3) 0.0673(15) Uani 1 1 d . . . . .
H10A H 0.339450 -0.347885 1.167396 0.081 Uiso 1 1 calc R U . . .
B11 B 0.2480(4) -0.1838(4) 1.2125(3) 0.0632(12) Uani 1 1 d . . . . .
H11 H 0.207054 -0.207763 1.275274 0.076 Uiso 1 1 calc R U . . .
B12 B 0.6914(3) 0.0541(3) 0.3940(2) 0.0435(8) Uani 1 1 d . . . . .
H12A H 0.711906 -0.024932 0.411940 0.052 Uiso 1 1 calc R U . . .
B13 B 0.7573(3) 0.1341(3) 0.4039(2) 0.0446(8) Uani 1 1 d . . . . .
H13 H 0.820952 0.107774 0.428334 0.054 Uiso 1 1 calc R U . . .
B14 B 0.6667(4) 0.2452(3) 0.4250(2) 0.0487(10) Uani 1 1 d . . . . .
H14 H 0.670827 0.291312 0.463116 0.058 Uiso 1 1 calc R U . . .
B15 B 0.5464(3) 0.2319(3) 0.4263(2) 0.0471(9) Uani 1 1 d . . . . .
H15 H 0.472142 0.270025 0.465150 0.056 Uiso 1 1 calc R U . . .
B16 B 0.5608(3) 0.1141(3) 0.4084(2) 0.0474(9) Uani 1 1 d . . . . .
H16 H 0.496219 0.075430 0.435606 0.057 Uiso 1 1 calc R U . . .
B17 B 0.7733(4) 0.1152(3) 0.3095(2) 0.0500(10) Uani 1 1 d . . . . .
H17 H 0.847808 0.076941 0.271053 0.060 Uiso 1 1 calc R U . . .
B18 B 0.7584(4) 0.2330(3) 0.3278(3) 0.0547(11) Uani 1 1 d . . . . .
H18 H 0.822877 0.271839 0.301567 0.066 Uiso 1 1 calc R U . . .
B19 B 0.6274(4) 0.2943(3) 0.3415(3) 0.0557(11) Uani 1 1 d . . . . .
H19 H 0.606318 0.373386 0.324143 0.067 Uiso 1 1 calc R U . . .
B20 B 0.5626(4) 0.2119(4) 0.3317(2) 0.0551(11) Uani 1 1 d . . . . .
H20A H 0.498765 0.237141 0.307433 0.066 Uiso 1 1 calc R U . . .
B21 B 0.6523(4) 0.1012(3) 0.3118(2) 0.0505(10) Uani 1 1 d . . . . .
H21A H 0.647844 0.053786 0.274837 0.061 Uiso 1 1 calc R U . . .
B22 B 0.6925(4) 0.2134(3) 0.2713(2) 0.0524(10) Uani 1 1 d . . . . .
H22A H 0.713602 0.240047 0.207420 0.063 Uiso 1 1 calc R U . . .
O029 O 1.1268(12) 0.8124(11) 0.4454(8) 0.277(5) Uani 1 1 d . U . . .
C54 C 1.0048(8) 0.7677(9) 0.4114(5) 0.177(4) Uani 1 1 d D U . . .
H54A H 1.020749 0.766702 0.355952 0.266 Uiso 1 1 calc R U . . .
H54B H 0.930632 0.784478 0.436879 0.266 Uiso 1 1 calc DR U . . .
H54C H 1.031721 0.704432 0.435307 0.266 Uiso 1 1 calc DR U . . .
C55 C 1.0520(13) 0.8389(10) 0.4204(12) 0.207(5) Uani 1 1 d D U . . .
C56 C 1.0329(12) 0.9419(9) 0.3847(9) 0.244(8) Uani 1 1 d D U . . .
H56A H 0.960058 0.970711 0.406143 0.366 Uiso 1 1 calc R U . . .
H56B H 1.053116 0.945715 0.328204 0.366 Uiso 1 1 calc R U . . .
H56C H 1.072923 0.976509 0.396517 0.366 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 N1 2.077(3) . ?
Pt1 N2 2.064(3) . ?
Pt1 C1 1.982(4) . ?
Pt1 C2 1.983(4) . ?
N1 C3 1.338(4) . ?
N1 C7 1.349(4) . ?
N2 C8 1.360(5) . ?
N2 C12 1.324(4) . ?
N3 C1 1.345(4) . ?
N3 C19 1.395(4) . ?
N3 C30 1.464(5) . ?
N4 C1 1.349(5) . ?
N4 C15 1.464(4) . ?
N4 C18 1.399(4) . ?
N5 C2 1.346(5) . ?
N5 C17 1.460(5) . ?
N5 C24 1.397(5) . ?
N6 C2 1.358(5) . ?
N6 C29 1.390(5) . ?
N6 C42 1.462(5) . ?
C3 H3 0.9400 . ?
C3 C4 1.375(5) . ?
C4 C5 1.384(5) . ?
C4 C13 1.504(5) . ?
C5 H5 0.9400 . ?
C5 C6 1.384(5) . ?
C6 H6 0.9400 . ?
C6 C7 1.377(5) . ?
C7 C8 1.480(4) . ?
C8 C9 1.377(5) . ?
C9 H9 0.9400 . ?
C9 C10 1.381(5) . ?
C10 H10 0.9400 . ?
C10 C11 1.391(5) . ?
C11 C12 1.378(5) . ?
C11 C14 1.505(5) . ?
C12 H12 0.9400 . ?
C13 B12 1.711(5) . ?
C13 B13 1.727(5) . ?
C13 B14 1.721(5) . ?
C13 B15 1.715(5) . ?
C13 B16 1.714(6) . ?
C14 B1 1.704(6) . ?
C14 B2 1.720(5) . ?
C14 B3 1.726(6) . ?
C14 B4 1.721(6) . ?
C14 B5 1.726(6) . ?
C15 H15A 0.9800 . ?
C15 H15B 0.9800 . ?
C15 C16 1.528(5) . ?
C16 H16A 0.9800 . ?
C16 H16B 0.9800 . ?
C16 C17 1.537(5) . ?
C17 H17A 0.9800 . ?
C17 H17B 0.9800 . ?
C18 C19 1.388(5) . ?
C18 C23 1.381(5) . ?
C19 C20 1.393(5) . ?
C20 H20 0.9400 . ?
C20 C21 1.379(7) . ?
C21 H21 0.9400 . ?
C21 C22 1.397(9) . ?
C22 H22 0.9400 . ?
C22 C23 1.367(7) . ?
C23 H23 0.9400 . ?
C24 C25 1.381(6) . ?
C24 C29 1.382(6) . ?
C25 H25 0.9400 . ?
C25 C26 1.367(8) . ?
C26 H26 0.9400 . ?
C26 C27 1.403(9) . ?
C27 H27 0.9400 . ?
C27 C28 1.353(8) . ?
C28 H28 0.9400 . ?
C28 C29 1.409(6) . ?
C30 H30A 0.9800 . ?
C30 H30B 0.9800 . ?
C30 C31 1.498(7) . ?
C31 H31A 0.9800 . ?
C31 H31B 0.9800 . ?
C31 C32 1.654(8) . ?
C32 H32A 0.9800 . ?
C32 H32B 0.9800 . ?
C32 C33 1.398(10) . ?
C33 H33A 0.9800 . ?
C33 H33B 0.9800 . ?
C33 C34 1.492(9) . ?
C34 H34A 0.9800 . ?
C34 H34B 0.9800 . ?
C34 C35 1.513(7) . ?
C35 H35A 0.9800 . ?
C35 H35B 0.9800 . ?
C35 C36 1.517(6) . ?
C36 H36A 0.9800 . ?
C36 H36B 0.9800 . ?
C36 C37 1.518(8) . ?
C37 H37A 0.9800 . ?
C37 H37B 0.9800 . ?
C37 C38 1.519(7) . ?
C38 H38A 0.9800 . ?
C38 H38B 0.9800 . ?
C38 C39 1.584(8) . ?
C39 H39A 0.9800 . ?
C39 H39B 0.9800 . ?
C39 C40 1.556(8) . ?
C40 H40A 0.9800 . ?
C40 H40B 0.9800 . ?
C40 C41 1.509(8) . ?
C41 H41A 0.9700 . ?
C41 H41B 0.9700 . ?
C41 H41C 0.9700 . ?
C42 H42A 0.9800 . ?
C42 H42B 0.9800 . ?
C42 C43 1.521(5) . ?
C43 H43A 0.9800 . ?
C43 H43B 0.9800 . ?
C43 C44 1.501(6) . ?
C44 H44A 0.9800 . ?
C44 H44B 0.9800 . ?
C44 C45 1.513(7) . ?
C45 H45A 0.9800 . ?
C45 H45B 0.9800 . ?
C45 C46 1.465(9) . ?
C46 H46A 0.9800 . ?
C46 H46B 0.9800 . ?
C46 C47 1.414(11) . ?
C47 H47A 0.9800 . ?
C47 H47B 0.9800 . ?
C47 C48 1.499(8) . ?
C48 H48A 0.9800 . ?
C48 H48B 0.9800 . ?
C48 C49 1.503(8) . ?
C49 H49A 0.9800 . ?
C49 H49B 0.9800 . ?
C49 C50 1.519(7) . ?
C50 H50A 0.9800 . ?
C50 H50B 0.9800 . ?
C50 C51 1.515(7) . ?
C51 H51A 0.9800 . ?
C51 H51B 0.9800 . ?
C51 C52 1.499(7) . ?
C52 H52A 0.9800 . ?
C52 H52B 0.9800 . ?
C52 C53 1.514(9) . ?
C53 H53A 0.9700 . ?
C53 H53B 0.9700 . ?
C53 H53C 0.9700 . ?
B1 H1 1.1100 . ?
B1 B2 1.775(8) . ?
B1 B5 1.781(7) . ?
B1 B6 1.753(7) . ?
B1 B7 1.781(7) . ?
B2 H2 1.1100 . ?
B2 B3 1.788(8) . ?
B2 B6 1.785(8) . ?
B2 B10 1.749(7) . ?
B3 H3A 1.1100 . ?
B3 B4 1.788(7) . ?
B3 B9 1.764(7) . ?
B3 B10 1.778(7) . ?
B4 H4 1.1100 . ?
B4 B5 1.763(7) . ?
B4 B8 1.778(7) . ?
B4 B9 1.783(6) . ?
B5 H5A 1.1100 . ?
B5 B7 1.768(6) . ?
B5 B8 1.771(6) . ?
B6 H6A 1.1100 . ?
B6 B7 1.762(9) . ?
B6 B10 1.805(10) . ?
B6 B11 1.780(8) . ?
B7 H7 1.1100 . ?
B7 B8 1.789(7) . ?
B7 B11 1.790(7) . ?
B8 H8 1.1100 . ?
B8 B9 1.801(7) . ?
B8 B11 1.788(7) . ?
B9 H9A 1.1100 . ?
B9 B10 1.783(8) . ?
B9 B11 1.770(8) . ?
B10 H10A 1.1100 . ?
B10 B11 1.776(8) . ?
B11 H11 1.1100 . ?
B12 H12A 1.1100 . ?
B12 B13 1.770(6) . ?
B12 B16 1.778(6) . ?
B12 B17 1.779(6) . ?
B12 B21 1.756(6) . ?
B13 H13 1.1100 . ?
B13 B14 1.788(6) . ?
B13 B17 1.759(6) . ?
B13 B18 1.770(6) . ?
B14 H14 1.1100 . ?
B14 B15 1.780(7) . ?
B14 B18 1.797(6) . ?
B14 B19 1.783(7) . ?
B15 H15 1.1100 . ?
B15 B16 1.764(6) . ?
B15 B19 1.785(6) . ?
B15 B20 1.768(6) . ?
B16 H16 1.1100 . ?
B16 B20 1.766(6) . ?
B16 B21 1.790(6) . ?
B17 H17 1.1100 . ?
B17 B18 1.765(6) . ?
B17 B21 1.786(7) . ?
B17 B22 1.772(7) . ?
B18 H18 1.1100 . ?
B18 B19 1.789(7) . ?
B18 B22 1.769(7) . ?
B19 H19 1.1100 . ?
B19 B20 1.786(8) . ?
B19 B22 1.770(6) . ?
B20 H20A 1.1100 . ?
B20 B21 1.775(7) . ?
B20 B22 1.773(6) . ?
B21 H21A 1.1100 . ?
B21 B22 1.786(6) . ?
B22 H22A 1.1100 . ?
O029 C55 1.260(16) . ?
C54 H54A 0.9700 . ?
C54 H54B 0.9700 . ?
C54 H54C 0.9700 . ?
C54 C55 1.456(9) . ?
C55 C56 1.490(9) . ?
C56 H56A 0.9700 . ?
C56 H56B 0.9700 . ?
C56 H56C 0.9700 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N2 Pt1 N1 79.63(12) . . ?
C1 Pt1 N1 99.98(13) . . ?
C1 Pt1 N2 179.45(10) . . ?
C1 Pt1 C2 86.29(16) . . ?
C2 Pt1 N1 173.10(12) . . ?
C2 Pt1 N2 94.13(15) . . ?
C3 N1 Pt1 126.6(2) . . ?
C3 N1 C7 119.0(3) . . ?
C7 N1 Pt1 114.3(2) . . ?
C8 N2 Pt1 114.6(2) . . ?
C12 N2 Pt1 125.5(3) . . ?
C12 N2 C8 119.8(3) . . ?
C1 N3 C19 109.8(3) . . ?
C1 N3 C30 126.4(3) . . ?
C19 N3 C30 123.8(3) . . ?
C1 N4 C15 125.5(3) . . ?
C1 N4 C18 110.2(3) . . ?
C18 N4 C15 124.2(3) . . ?
C2 N5 C17 125.4(3) . . ?
C2 N5 C24 110.4(3) . . ?
C24 N5 C17 124.1(3) . . ?
C2 N6 C29 109.2(3) . . ?
C2 N6 C42 126.1(3) . . ?
C29 N6 C42 124.6(3) . . ?
N3 C1 Pt1 127.9(3) . . ?
N3 C1 N4 107.4(3) . . ?
N4 C1 Pt1 124.0(3) . . ?
N5 C2 Pt1 124.6(3) . . ?
N5 C2 N6 107.2(3) . . ?
N6 C2 Pt1 127.9(3) . . ?
N1 C3 H3 118.2 . . ?
N1 C3 C4 123.6(3) . . ?
C4 C3 H3 118.2 . . ?
C3 C4 C5 116.5(3) . . ?
C3 C4 C13 122.1(3) . . ?
C5 C4 C13 121.3(3) . . ?
C4 C5 H5 119.5 . . ?
C4 C5 C6 121.1(3) . . ?
C6 C5 H5 119.5 . . ?
C5 C6 H6 120.8 . . ?
C7 C6 C5 118.5(3) . . ?
C7 C6 H6 120.8 . . ?
N1 C7 C6 121.2(3) . . ?
N1 C7 C8 115.8(3) . . ?
C6 C7 C8 123.0(3) . . ?
N2 C8 C7 115.4(3) . . ?
N2 C8 C9 119.5(3) . . ?
C9 C8 C7 125.1(3) . . ?
C8 C9 H9 119.8 . . ?
C8 C9 C10 120.4(3) . . ?
C10 C9 H9 119.8 . . ?
C9 C10 H10 120.2 . . ?
C9 C10 C11 119.7(3) . . ?
C11 C10 H10 120.2 . . ?
C10 C11 C14 123.2(3) . . ?
C12 C11 C10 116.9(3) . . ?
C12 C11 C14 120.0(3) . . ?
N2 C12 C11 123.7(3) . . ?
N2 C12 H12 118.1 . . ?
C11 C12 H12 118.1 . . ?
C4 C13 B12 116.3(3) . . ?
C4 C13 B13 116.9(3) . . ?
C4 C13 B14 119.5(3) . . ?
C4 C13 B15 121.0(3) . . ?
C4 C13 B16 118.2(3) . . ?
B12 C13 B13 62.0(2) . . ?
B12 C13 B14 113.6(2) . . ?
B12 C13 B15 113.1(3) . . ?
B12 C13 B16 62.5(2) . . ?
B14 C13 B13 62.4(2) . . ?
B15 C13 B13 113.4(3) . . ?
B15 C13 B14 62.4(3) . . ?
B16 C13 B13 113.7(3) . . ?
B16 C13 B14 113.9(3) . . ?
B16 C13 B15 61.9(2) . . ?
C11 C14 B1 120.2(3) . . ?
C11 C14 B2 119.2(3) . . ?
C11 C14 B3 116.6(3) . . ?
C11 C14 B4 116.7(3) . . ?
C11 C14 B5 118.9(3) . . ?
B1 C14 B2 62.5(3) . . ?
B1 C14 B3 114.2(3) . . ?
B1 C14 B4 113.5(3) . . ?
B1 C14 B5 62.6(3) . . ?
B2 C14 B3 62.5(3) . . ?
B2 C14 B4 113.7(3) . . ?
B2 C14 B5 113.7(3) . . ?
B3 C14 B5 113.3(3) . . ?
B4 C14 B3 62.5(3) . . ?
B4 C14 B5 61.5(3) . . ?
N4 C15 H15A 108.5 . . ?
N4 C15 H15B 108.5 . . ?
N4 C15 C16 115.2(3) . . ?
H15A C15 H15B 107.5 . . ?
C16 C15 H15A 108.5 . . ?
C16 C15 H15B 108.5 . . ?
C15 C16 H16A 108.5 . . ?
C15 C16 H16B 108.5 . . ?
C15 C16 C17 115.2(3) . . ?
H16A C16 H16B 107.5 . . ?
C17 C16 H16A 108.5 . . ?
C17 C16 H16B 108.5 . . ?
N5 C17 C16 114.1(3) . . ?
N5 C17 H17A 108.7 . . ?
N5 C17 H17B 108.7 . . ?
C16 C17 H17A 108.7 . . ?
C16 C17 H17B 108.7 . . ?
H17A C17 H17B 107.6 . . ?
C19 C18 N4 105.7(3) . . ?
C23 C18 N4 132.6(4) . . ?
C23 C18 C19 121.6(4) . . ?
C18 C19 N3 106.9(3) . . ?
C18 C19 C20 121.9(4) . . ?
C20 C19 N3 131.2(4) . . ?
C19 C20 H20 122.1 . . ?
C21 C20 C19 115.7(4) . . ?
C21 C20 H20 122.1 . . ?
C20 C21 H21 118.9 . . ?
C20 C21 C22 122.2(5) . . ?
C22 C21 H21 118.9 . . ?
C21 C22 H22 119.2 . . ?
C23 C22 C21 121.6(5) . . ?
C23 C22 H22 119.2 . . ?
C18 C23 H23 121.5 . . ?
C22 C23 C18 117.0(5) . . ?
C22 C23 H23 121.5 . . ?
C25 C24 N5 132.3(4) . . ?
C25 C24 C29 122.0(4) . . ?
C29 C24 N5 105.6(3) . . ?
C24 C25 H25 121.5 . . ?
C26 C25 C24 117.0(5) . . ?
C26 C25 H25 121.5 . . ?
C25 C26 H26 119.3 . . ?
C25 C26 C27 121.4(5) . . ?
C27 C26 H26 119.3 . . ?
C26 C27 H27 119.0 . . ?
C28 C27 C26 121.9(5) . . ?
C28 C27 H27 119.0 . . ?
C27 C28 H28 121.5 . . ?
C27 C28 C29 116.9(5) . . ?
C29 C28 H28 121.5 . . ?
N6 C29 C28 131.9(4) . . ?
C24 C29 N6 107.5(3) . . ?
C24 C29 C28 120.5(4) . . ?
N3 C30 H30A 108.9 . . ?
N3 C30 H30B 108.9 . . ?
N3 C30 C31 113.2(4) . . ?
H30A C30 H30B 107.7 . . ?
C31 C30 H30A 108.9 . . ?
C31 C30 H30B 108.9 . . ?
C30 C31 H31A 110.7 . . ?
C30 C31 H31B 110.7 . . ?
C30 C31 C32 105.2(5) . . ?
H31A C31 H31B 108.8 . . ?
C32 C31 H31A 110.7 . . ?
C32 C31 H31B 110.7 . . ?
C31 C32 H32A 109.1 . . ?
C31 C32 H32B 109.1 . . ?
H32A C32 H32B 107.9 . . ?
C33 C32 C31 112.3(5) . . ?
C33 C32 H32A 109.1 . . ?
C33 C32 H32B 109.1 . . ?
C32 C33 H33A 109.1 . . ?
C32 C33 H33B 109.1 . . ?
C32 C33 C34 112.6(7) . . ?
H33A C33 H33B 107.8 . . ?
C34 C33 H33A 109.1 . . ?
C34 C33 H33B 109.1 . . ?
C33 C34 H34A 108.7 . . ?
C33 C34 H34B 108.7 . . ?
C33 C34 C35 114.4(6) . . ?
H34A C34 H34B 107.6 . . ?
C35 C34 H34A 108.7 . . ?
C35 C34 H34B 108.7 . . ?
C34 C35 H35A 109.2 . . ?
C34 C35 H35B 109.2 . . ?
C34 C35 C36 112.2(5) . . ?
H35A C35 H35B 107.9 . . ?
C36 C35 H35A 109.2 . . ?
C36 C35 H35B 109.2 . . ?
C35 C36 H36A 108.8 . . ?
C35 C36 H36B 108.8 . . ?
C35 C36 C37 114.0(5) . . ?
H36A C36 H36B 107.6 . . ?
C37 C36 H36A 108.8 . . ?
C37 C36 H36B 108.8 . . ?
C36 C37 H37A 108.6 . . ?
C36 C37 H37B 108.6 . . ?
C36 C37 C38 114.8(6) . . ?
H37A C37 H37B 107.6 . . ?
C38 C37 H37A 108.6 . . ?
C38 C37 H37B 108.6 . . ?
C37 C38 H38A 108.7 . . ?
C37 C38 H38B 108.7 . . ?
C37 C38 C39 114.1(6) . . ?
H38A C38 H38B 107.6 . . ?
C39 C38 H38A 108.7 . . ?
C39 C38 H38B 108.7 . . ?
C38 C39 H39A 109.3 . . ?
C38 C39 H39B 109.3 . . ?
H39A C39 H39B 108.0 . . ?
C40 C39 C38 111.6(7) . . ?
C40 C39 H39A 109.3 . . ?
C40 C39 H39B 109.3 . . ?
C39 C40 H40A 109.2 . . ?
C39 C40 H40B 109.2 . . ?
H40A C40 H40B 107.9 . . ?
C41 C40 C39 111.9(8) . . ?
C41 C40 H40A 109.2 . . ?
C41 C40 H40B 109.2 . . ?
C40 C41 H41A 109.5 . . ?
C40 C41 H41B 109.5 . . ?
C40 C41 H41C 109.5 . . ?
H41A C41 H41B 109.5 . . ?
H41A C41 H41C 109.5 . . ?
H41B C41 H41C 109.5 . . ?
N6 C42 H42A 109.2 . . ?
N6 C42 H42B 109.2 . . ?
N6 C42 C43 112.3(3) . . ?
H42A C42 H42B 107.9 . . ?
C43 C42 H42A 109.2 . . ?
C43 C42 H42B 109.2 . . ?
C42 C43 H43A 109.1 . . ?
C42 C43 H43B 109.1 . . ?
H43A C43 H43B 107.8 . . ?
C44 C43 C42 112.7(3) . . ?
C44 C43 H43A 109.1 . . ?
C44 C43 H43B 109.1 . . ?
C43 C44 H44A 108.8 . . ?
C43 C44 H44B 108.8 . . ?
C43 C44 C45 114.0(4) . . ?
H44A C44 H44B 107.7 . . ?
C45 C44 H44A 108.8 . . ?
C45 C44 H44B 108.8 . . ?
C44 C45 H45A 108.7 . . ?
C44 C45 H45B 108.7 . . ?
H45A C45 H45B 107.6 . . ?
C46 C45 C44 114.3(5) . . ?
C46 C45 H45A 108.7 . . ?
C46 C45 H45B 108.7 . . ?
C45 C46 H46A 107.4 . . ?
C45 C46 H46B 107.4 . . ?
H46A C46 H46B 106.9 . . ?
C47 C46 C45 119.7(6) . . ?
C47 C46 H46A 107.4 . . ?
C47 C46 H46B 107.4 . . ?
C46 C47 H47A 106.6 . . ?
C46 C47 H47B 106.6 . . ?
C46 C47 C48 122.7(7) . . ?
H47A C47 H47B 106.6 . . ?
C48 C47 H47A 106.6 . . ?
C48 C47 H47B 106.6 . . ?
C47 C48 H48A 107.8 . . ?
C47 C48 H48B 107.8 . . ?
C47 C48 C49 118.2(8) . . ?
H48A C48 H48B 107.1 . . ?
C49 C48 H48A 107.8 . . ?
C49 C48 H48B 107.8 . . ?
C48 C49 H49A 108.5 . . ?
C48 C49 H49B 108.5 . . ?
C48 C49 C50 115.1(9) . . ?
H49A C49 H49B 107.5 . . ?
C50 C49 H49A 108.5 . . ?
C50 C49 H49B 108.5 . . ?
C49 C50 H50A 110.7 . . ?
C49 C50 H50B 110.7 . . ?
H50A C50 H50B 108.8 . . ?
C51 C50 C49 105.1(7) . . ?
C51 C50 H50A 110.7 . . ?
C51 C50 H50B 110.7 . . ?
C50 C51 H51A 105.1 . . ?
C50 C51 H51B 105.1 . . ?
H51A C51 H51B 105.9 . . ?
C52 C51 C50 128.9(13) . . ?
C52 C51 H51A 105.1 . . ?
C52 C51 H51B 105.1 . . ?
C51 C52 H52A 110.3 . . ?
C51 C52 H52B 110.2 . . ?
C51 C52 C53 107.3(10) . . ?
H52A C52 H52B 108.5 . . ?
C53 C52 H52A 110.3 . . ?
C53 C52 H52B 110.3 . . ?
C52 C53 H53A 109.5 . . ?
C52 C53 H53B 109.5 . . ?
C52 C53 H53C 109.5 . . ?
H53A C53 H53B 109.5 . . ?
H53A C53 H53C 109.5 . . ?
H53B C53 H53C 109.5 . . ?
C14 B1 H1 123.6 . . ?
C14 B1 B2 59.2(3) . . ?
C14 B1 B5 59.3(2) . . ?
C14 B1 B6 106.3(4) . . ?
C14 B1 B7 105.5(3) . . ?
B2 B1 H1 121.0 . . ?
B2 B1 B5 108.4(3) . . ?
B2 B1 B7 108.3(3) . . ?
B5 B1 H1 121.7 . . ?
B6 B1 H1 121.9 . . ?
B6 B1 B2 60.8(3) . . ?
B6 B1 B5 107.8(4) . . ?
B6 B1 B7 59.8(3) . . ?
B7 B1 H1 122.5 . . ?
B7 B1 B5 59.5(3) . . ?
C14 B2 B1 58.3(2) . . ?
C14 B2 H2 124.9 . . ?
C14 B2 B3 58.9(2) . . ?
C14 B2 B6 104.3(4) . . ?
C14 B2 B10 105.5(3) . . ?
B1 B2 H2 122.0 . . ?
B1 B2 B3 107.8(3) . . ?
B1 B2 B6 59.0(3) . . ?
B3 B2 H2 121.2 . . ?
B6 B2 H2 122.2 . . ?
B6 B2 B3 108.8(4) . . ?
B10 B2 B1 108.5(4) . . ?
B10 B2 H2 121.3 . . ?
B10 B2 B3 60.3(3) . . ?
B10 B2 B6 61.4(4) . . ?
C14 B3 B2 58.6(3) . . ?
C14 B3 H3A 124.8 . . ?
C14 B3 B4 58.6(2) . . ?
C14 B3 B9 105.0(3) . . ?
C14 B3 B10 104.1(4) . . ?
B2 B3 H3A 122.3 . . ?
B4 B3 B2 107.4(4) . . ?
B4 B3 H3A 121.5 . . ?
B9 B3 B2 107.4(4) . . ?
B9 B3 H3A 122.0 . . ?
B9 B3 B4 60.3(3) . . ?
B9 B3 B10 60.5(3) . . ?
B10 B3 B2 58.7(3) . . ?
B10 B3 H3A 122.8 . . ?
B10 B3 B4 108.0(4) . . ?
C14 B4 B3 58.9(2) . . ?
C14 B4 H4 124.4 . . ?
C14 B4 B5 59.4(2) . . ?
C14 B4 B8 105.7(3) . . ?
C14 B4 B9 104.4(3) . . ?
B3 B4 H4 121.4 . . ?
B5 B4 B3 108.6(3) . . ?
B5 B4 H4 121.1 . . ?
B5 B4 B8 60.0(3) . . ?
B5 B4 B9 108.2(4) . . ?
B8 B4 B3 108.6(3) . . ?
B8 B4 H4 121.6 . . ?
B8 B4 B9 60.8(3) . . ?
B9 B4 B3 59.2(3) . . ?
B9 B4 H4 122.7 . . ?
C14 B5 B1 58.1(2) . . ?
C14 B5 B4 59.1(2) . . ?
C14 B5 H5A 124.5 . . ?
C14 B5 B7 105.2(3) . . ?
C14 B5 B8 105.8(3) . . ?
B1 B5 H5A 121.7 . . ?
B4 B5 B1 107.8(3) . . ?
B4 B5 H5A 121.2 . . ?
B4 B5 B7 108.9(3) . . ?
B4 B5 B8 60.4(3) . . ?
B7 B5 B1 60.2(3) . . ?
B7 B5 H5A 121.8 . . ?
B7 B5 B8 60.7(3) . . ?
B8 B5 B1 108.7(3) . . ?
B8 B5 H5A 121.5 . . ?
B1 B6 B2 60.2(3) . . ?
B1 B6 H6A 121.4 . . ?
B1 B6 B7 60.9(3) . . ?
B1 B6 B10 107.0(4) . . ?
B1 B6 B11 108.4(4) . . ?
B2 B6 H6A 122.5 . . ?
B2 B6 B10 58.3(3) . . ?
B7 B6 B2 108.8(3) . . ?
B7 B6 H6A 120.5 . . ?
B7 B6 B10 108.3(4) . . ?
B7 B6 B11 60.7(3) . . ?
B10 B6 H6A 122.8 . . ?
B11 B6 B2 106.4(4) . . ?
B11 B6 H6A 122.1 . . ?
B11 B6 B10 59.4(3) . . ?
B1 B7 H7 122.3 . . ?
B1 B7 B8 107.9(3) . . ?
B1 B7 B11 106.7(4) . . ?
B5 B7 B1 60.3(3) . . ?
B5 B7 H7 121.9 . . ?
B5 B7 B8 59.7(3) . . ?
B5 B7 B11 107.0(3) . . ?
B6 B7 B1 59.3(3) . . ?
B6 B7 B5 108.1(4) . . ?
B6 B7 H7 121.4 . . ?
B6 B7 B8 108.8(4) . . ?
B6 B7 B11 60.2(3) . . ?
B8 B7 H7 121.4 . . ?
B8 B7 B11 60.0(3) . . ?
B11 B7 H7 122.5 . . ?
B4 B8 B7 107.3(3) . . ?
B4 B8 H8 122.3 . . ?
B4 B8 B9 59.8(3) . . ?
B4 B8 B11 106.8(3) . . ?
B5 B8 B4 59.6(2) . . ?
B5 B8 B7 59.6(3) . . ?
B5 B8 H8 122.3 . . ?
B5 B8 B9 107.0(3) . . ?
B5 B8 B11 107.0(3) . . ?
B7 B8 H8 121.9 . . ?
B7 B8 B9 107.3(4) . . ?
B9 B8 H8 122.3 . . ?
B11 B8 B7 60.1(3) . . ?
B11 B8 H8 122.4 . . ?
B11 B8 B9 59.1(3) . . ?
B3 B9 B4 60.5(3) . . ?
B3 B9 B8 108.6(3) . . ?
B3 B9 H9A 121.1 . . ?
B3 B9 B10 60.2(3) . . ?
B3 B9 B11 108.3(4) . . ?
B4 B9 B8 59.5(3) . . ?
B4 B9 H9A 122.1 . . ?
B8 B9 H9A 121.6 . . ?
B10 B9 B4 108.0(3) . . ?
B10 B9 B8 108.2(4) . . ?
B10 B9 H9A 121.6 . . ?
B11 B9 B4 107.3(4) . . ?
B11 B9 B8 60.1(3) . . ?
B11 B9 H9A 121.9 . . ?
B11 B9 B10 60.0(3) . . ?
B2 B10 B3 60.9(3) . . ?
B2 B10 B6 60.3(3) . . ?
B2 B10 B9 108.3(3) . . ?
B2 B10 H10A 121.1 . . ?
B2 B10 B11 108.1(4) . . ?
B3 B10 B6 108.4(3) . . ?
B3 B10 B9 59.4(3) . . ?
B3 B10 H10A 121.6 . . ?
B6 B10 H10A 121.8 . . ?
B9 B10 B6 107.4(4) . . ?
B9 B10 H10A 122.2 . . ?
B11 B10 B3 107.4(4) . . ?
B11 B10 B6 59.6(3) . . ?
B11 B10 B9 59.7(3) . . ?
B11 B10 H10A 122.1 . . ?
B6 B11 B7 59.1(3) . . ?
B6 B11 B8 108.0(3) . . ?
B6 B11 H11 121.6 . . ?
B7 B11 H11 122.0 . . ?
B8 B11 B7 60.0(3) . . ?
B8 B11 H11 121.3 . . ?
B9 B11 B6 109.1(4) . . ?
B9 B11 B7 108.6(3) . . ?
B9 B11 B8 60.8(3) . . ?
B9 B11 B10 60.4(3) . . ?
B9 B11 H11 120.9 . . ?
B10 B11 B6 61.0(4) . . ?
B10 B11 B7 108.3(3) . . ?
B10 B11 B8 109.2(3) . . ?
B10 B11 H11 120.9 . . ?
C13 B12 H12A 124.0 . . ?
C13 B12 B13 59.5(2) . . ?
C13 B12 B16 58.8(2) . . ?
C13 B12 B17 105.6(3) . . ?
C13 B12 B21 106.1(3) . . ?
B13 B12 H12A 121.4 . . ?
B13 B12 B16 108.6(3) . . ?
B13 B12 B17 59.4(2) . . ?
B16 B12 H12A 120.9 . . ?
B16 B12 B17 109.1(3) . . ?
B17 B12 H12A 122.0 . . ?
B21 B12 H12A 121.5 . . ?
B21 B12 B13 108.5(3) . . ?
B21 B12 B16 60.9(2) . . ?
B21 B12 B17 60.7(3) . . ?
C13 B13 B12 58.5(2) . . ?
C13 B13 H13 124.3 . . ?
C13 B13 B14 58.6(2) . . ?
C13 B13 B17 105.7(3) . . ?
C13 B13 B18 105.7(3) . . ?
B12 B13 H13 121.6 . . ?
B12 B13 B14 107.6(3) . . ?
B14 B13 H13 121.4 . . ?
B17 B13 B12 60.5(2) . . ?
B17 B13 H13 121.7 . . ?
B17 B13 B14 108.6(3) . . ?
B17 B13 B18 60.0(2) . . ?
B18 B13 B12 108.3(3) . . ?
B18 B13 H13 121.8 . . ?
B18 B13 B14 60.7(2) . . ?
C13 B14 B13 59.0(2) . . ?
C13 B14 H14 124.4 . . ?
C13 B14 B15 58.6(2) . . ?
C13 B14 B18 104.8(3) . . ?
C13 B14 B19 105.1(3) . . ?
B13 B14 H14 122.1 . . ?
B13 B14 B18 59.2(2) . . ?
B15 B14 B13 107.5(3) . . ?
B15 B14 H14 121.6 . . ?
B15 B14 B18 107.8(3) . . ?
B15 B14 B19 60.1(3) . . ?
B18 B14 H14 122.6 . . ?
B19 B14 B13 107.2(3) . . ?
B19 B14 H14 122.4 . . ?
B19 B14 B18 60.0(3) . . ?
C13 B15 B14 59.0(2) . . ?
C13 B15 H15 124.5 . . ?
C13 B15 B16 59.0(2) . . ?
C13 B15 B19 105.2(3) . . ?
C13 B15 B20 104.9(3) . . ?
B14 B15 H15 121.3 . . ?
B14 B15 B19 60.0(3) . . ?
B16 B15 B14 108.7(3) . . ?
B16 B15 H15 121.0 . . ?
B16 B15 B19 108.7(3) . . ?
B16 B15 B20 60.0(3) . . ?
B19 B15 H15 122.0 . . ?
B20 B15 B14 108.2(3) . . ?
B20 B15 H15 122.3 . . ?
B20 B15 B19 60.4(3) . . ?
C13 B16 B12 58.6(2) . . ?
C13 B16 B15 59.1(2) . . ?
C13 B16 H16 124.4 . . ?
C13 B16 B20 105.0(3) . . ?
C13 B16 B21 104.5(3) . . ?
B12 B16 H16 122.4 . . ?
B12 B16 B21 59.0(2) . . ?
B15 B16 B12 107.6(3) . . ?
B15 B16 H16 121.3 . . ?
B15 B16 B20 60.1(2) . . ?
B15 B16 B21 108.0(3) . . ?
B20 B16 B12 106.8(3) . . ?
B20 B16 H16 122.5 . . ?
B20 B16 B21 59.9(3) . . ?
B21 B16 H16 122.7 . . ?
B12 B17 H17 122.4 . . ?
B12 B17 B21 59.0(2) . . ?
B13 B17 B12 60.1(2) . . ?
B13 B17 H17 121.7 . . ?
B13 B17 B18 60.3(2) . . ?
B13 B17 B21 107.7(3) . . ?
B13 B17 B22 107.8(3) . . ?
B18 B17 B12 108.1(3) . . ?
B18 B17 H17 121.2 . . ?
B18 B17 B21 108.6(3) . . ?
B18 B17 B22 60.0(3) . . ?
B21 B17 H17 121.8 . . ?
B22 B17 B12 107.0(3) . . ?
B22 B17 H17 122.0 . . ?
B22 B17 B21 60.3(3) . . ?
B13 B18 B14 60.1(2) . . ?
B13 B18 H18 122.0 . . ?
B13 B18 B19 107.7(3) . . ?
B14 B18 H18 122.0 . . ?
B17 B18 B13 59.7(2) . . ?
B17 B18 B14 107.9(3) . . ?
B17 B18 H18 121.6 . . ?
B17 B18 B19 108.1(3) . . ?
B17 B18 B22 60.2(3) . . ?
B19 B18 B14 59.6(3) . . ?
B19 B18 H18 121.9 . . ?
B22 B18 B13 107.4(3) . . ?
B22 B18 B14 107.2(3) . . ?
B22 B18 H18 122.2 . . ?
B22 B18 B19 59.6(3) . . ?
B14 B19 B15 59.8(2) . . ?
B14 B19 B18 60.4(3) . . ?
B14 B19 H19 121.8 . . ?
B14 B19 B20 107.3(3) . . ?
B15 B19 B18 107.9(3) . . ?
B15 B19 H19 122.1 . . ?
B15 B19 B20 59.3(3) . . ?
B18 B19 H19 121.7 . . ?
B20 B19 B18 107.4(3) . . ?
B20 B19 H19 122.3 . . ?
B22 B19 B14 107.8(3) . . ?
B22 B19 B15 107.3(3) . . ?
B22 B19 B18 59.6(3) . . ?
B22 B19 H19 122.0 . . ?
B22 B19 B20 59.8(3) . . ?
B15 B20 B19 60.3(3) . . ?
B15 B20 H20A 121.8 . . ?
B15 B20 B21 108.4(3) . . ?
B15 B20 B22 107.9(3) . . ?
B16 B20 B15 59.9(2) . . ?
B16 B20 B19 108.6(3) . . ?
B16 B20 H20A 121.1 . . ?
B16 B20 B21 60.7(3) . . ?
B16 B20 B22 108.9(3) . . ?
B19 B20 H20A 121.6 . . ?
B21 B20 B19 108.5(3) . . ?
B21 B20 H20A 121.2 . . ?
B22 B20 B19 59.6(3) . . ?
B22 B20 H20A 121.6 . . ?
B22 B20 B21 60.4(3) . . ?
B12 B21 B16 60.2(2) . . ?
B12 B21 B17 60.3(2) . . ?
B12 B21 B20 107.3(3) . . ?
B12 B21 H21A 121.8 . . ?
B12 B21 B22 107.4(3) . . ?
B16 B21 H21A 121.8 . . ?
B17 B21 B16 108.2(3) . . ?
B17 B21 H21A 121.7 . . ?
B20 B21 B16 59.4(2) . . ?
B20 B21 B17 107.5(3) . . ?
B20 B21 H21A 122.3 . . ?
B20 B21 B22 59.7(3) . . ?
B22 B21 B16 107.2(3) . . ?
B22 B21 B17 59.5(3) . . ?
B22 B21 H21A 122.4 . . ?
B17 B22 B20 108.2(3) . . ?
B17 B22 B21 60.3(3) . . ?
B17 B22 H22A 121.7 . . ?
B18 B22 B17 59.8(3) . . ?
B18 B22 B19 60.7(3) . . ?
B18 B22 B20 108.9(3) . . ?
B18 B22 B21 108.4(3) . . ?
B18 B22 H22A 121.3 . . ?
B19 B22 B17 108.6(3) . . ?
B19 B22 B20 60.6(3) . . ?
B19 B22 B21 108.7(3) . . ?
B19 B22 H22A 121.0 . . ?
B20 B22 B21 59.8(3) . . ?
B20 B22 H22A 121.4 . . ?
B21 B22 H22A 121.5 . . ?
H54A C54 H54B 109.5 . . ?
H54A C54 H54C 109.5 . . ?
H54B C54 H54C 109.5 . . ?
C55 C54 H54A 109.5 . . ?
C55 C54 H54B 109.5 . . ?
C55 C54 H54C 109.5 . . ?
O029 C55 C54 120.3(13) . . ?
O029 C55 C56 115.5(14) . . ?
C54 C55 C56 122.7(15) . . ?
C55 C56 H56A 109.5 . . ?
C55 C56 H56B 109.5 . . ?
C55 C56 H56C 109.5 . . ?
H56A C56 H56B 109.5 . . ?
H56A C56 H56C 109.5 . . ?
H56B C56 H56C 109.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Pt1 N1 C3 C4 178.8(3) . . . . ?
Pt1 N1 C7 C6 -176.8(3) . . . . ?
Pt1 N1 C7 C8 3.9(4) . . . . ?
Pt1 N2 C8 C7 -2.1(4) . . . . ?
Pt1 N2 C8 C9 178.4(3) . . . . ?
Pt1 N2 C12 C11 -178.8(3) . . . . ?
N1 C3 C4 C5 -0.7(5) . . . . ?
N1 C3 C4 C13 177.3(3) . . . . ?
N1 C7 C8 N2 -1.2(5) . . . . ?
N1 C7 C8 C9 178.2(4) . . . . ?
N2 C8 C9 C10 1.0(6) . . . . ?
N3 C19 C20 C21 -176.3(5) . . . . ?
N3 C30 C31 C32 177.8(3) . . . . ?
N4 C15 C16 C17 -83.3(4) . . . . ?
N4 C18 C19 N3 -0.1(4) . . . . ?
N4 C18 C19 C20 -177.9(3) . . . . ?
N4 C18 C23 C22 177.6(5) . . . . ?
N5 C24 C25 C26 179.5(6) . . . . ?
N5 C24 C29 N6 1.2(5) . . . . ?
N5 C24 C29 C28 -178.1(5) . . . . ?
N6 C42 C43 C44 -175.9(3) . . . . ?
C1 N3 C19 C18 -0.8(4) . . . . ?
C1 N3 C19 C20 176.8(4) . . . . ?
C1 N3 C30 C31 95.0(5) . . . . ?
C1 N4 C15 C16 92.4(4) . . . . ?
C1 N4 C18 C19 0.9(4) . . . . ?
C1 N4 C18 C23 -177.0(4) . . . . ?
C2 N5 C17 C16 -84.1(5) . . . . ?
C2 N5 C24 C25 -177.3(6) . . . . ?
C2 N5 C24 C29 -1.0(5) . . . . ?
C2 N6 C29 C24 -1.0(5) . . . . ?
C2 N6 C29 C28 178.3(6) . . . . ?
C2 N6 C42 C43 103.2(4) . . . . ?
C3 N1 C7 C6 4.0(5) . . . . ?
C3 N1 C7 C8 -175.3(3) . . . . ?
C3 C4 C5 C6 1.5(6) . . . . ?
C3 C4 C13 B12 -142.1(3) . . . . ?
C3 C4 C13 B13 147.6(3) . . . . ?
C3 C4 C13 B14 75.6(4) . . . . ?
C3 C4 C13 B15 1.9(5) . . . . ?
C3 C4 C13 B16 -70.6(4) . . . . ?
C4 C5 C6 C7 0.3(6) . . . . ?
C4 C13 B12 B13 -108.0(3) . . . . ?
C4 C13 B12 B16 109.8(3) . . . . ?
C4 C13 B12 B17 -147.0(3) . . . . ?
C4 C13 B12 B21 149.6(3) . . . . ?
C4 C13 B13 B12 107.0(3) . . . . ?
C4 C13 B13 B14 -110.9(3) . . . . ?
C4 C13 B13 B17 146.6(3) . . . . ?
C4 C13 B13 B18 -150.8(3) . . . . ?
C4 C13 B14 B13 107.0(3) . . . . ?
C4 C13 B14 B15 -111.9(3) . . . . ?
C4 C13 B14 B18 146.0(3) . . . . ?
C4 C13 B14 B19 -151.7(3) . . . . ?
C4 C13 B15 B14 109.4(3) . . . . ?
C4 C13 B15 B16 -107.8(3) . . . . ?
C4 C13 B15 B19 149.2(3) . . . . ?
C4 C13 B15 B20 -148.0(3) . . . . ?
C4 C13 B16 B12 -106.7(3) . . . . ?
C4 C13 B16 B15 112.1(3) . . . . ?
C4 C13 B16 B20 152.5(3) . . . . ?
C4 C13 B16 B21 -145.4(3) . . . . ?
C5 C4 C13 B12 35.8(5) . . . . ?
C5 C4 C13 B13 -34.6(5) . . . . ?
C5 C4 C13 B14 -106.6(4) . . . . ?
C5 C4 C13 B15 179.8(3) . . . . ?
C5 C4 C13 B16 107.2(4) . . . . ?
C5 C6 C7 N1 -3.1(6) . . . . ?
C5 C6 C7 C8 176.1(4) . . . . ?
C6 C7 C8 N2 179.5(4) . . . . ?
C6 C7 C8 C9 -1.0(6) . . . . ?
C7 N1 C3 C4 -2.1(5) . . . . ?
C7 C8 C9 C10 -178.4(4) . . . . ?
C8 N2 C12 C11 0.9(5) . . . . ?
C8 C9 C10 C11 -0.3(6) . . . . ?
C9 C10 C11 C12 -0.2(6) . . . . ?
C9 C10 C11 C14 -178.9(4) . . . . ?
C10 C11 C12 N2 -0.1(5) . . . . ?
C10 C11 C14 B1 72.1(5) . . . . ?
C10 C11 C14 B2 -1.2(5) . . . . ?
C10 C11 C14 B3 -73.1(5) . . . . ?
C10 C11 C14 B4 -144.0(4) . . . . ?
C10 C11 C14 B5 145.4(4) . . . . ?
C11 C14 B1 B2 -109.5(4) . . . . ?
C11 C14 B1 B5 109.2(4) . . . . ?
C11 C14 B1 B6 -149.4(4) . . . . ?
C11 C14 B1 B7 148.2(3) . . . . ?
C11 C14 B2 B1 111.0(4) . . . . ?
C11 C14 B2 B3 -106.7(4) . . . . ?
C11 C14 B2 B6 149.6(4) . . . . ?
C11 C14 B2 B10 -146.6(4) . . . . ?
C11 C14 B3 B2 110.8(4) . . . . ?
C11 C14 B3 B4 -107.8(3) . . . . ?
C11 C14 B3 B9 -147.8(3) . . . . ?
C11 C14 B3 B10 149.5(3) . . . . ?
C11 C14 B4 B3 107.7(4) . . . . ?
C11 C14 B4 B5 -110.1(3) . . . . ?
C11 C14 B4 B8 -149.8(3) . . . . ?
C11 C14 B4 B9 147.1(3) . . . . ?
C11 C14 B5 B1 -111.1(3) . . . . ?
C11 C14 B5 B4 106.5(3) . . . . ?
C11 C14 B5 B7 -150.3(3) . . . . ?
C11 C14 B5 B8 146.4(3) . . . . ?
C12 N2 C8 C7 178.2(3) . . . . ?
C12 N2 C8 C9 -1.3(5) . . . . ?
C12 C11 C14 B1 -106.5(4) . . . . ?
C12 C11 C14 B2 -179.8(4) . . . . ?
C12 C11 C14 B3 108.3(4) . . . . ?
C12 C11 C14 B4 37.3(5) . . . . ?
C12 C11 C14 B5 -33.2(5) . . . . ?
C13 C4 C5 C6 -176.5(4) . . . . ?
C13 B12 B13 B14 -33.4(3) . . . . ?
C13 B12 B13 B17 -135.3(3) . . . . ?
C13 B12 B13 B18 -97.6(3) . . . . ?
C13 B12 B16 B15 34.4(2) . . . . ?
C13 B12 B16 B20 97.6(3) . . . . ?
C13 B12 B16 B21 135.2(3) . . . . ?
C13 B12 B17 B13 39.0(3) . . . . ?
C13 B12 B17 B18 1.2(4) . . . . ?
C13 B12 B17 B21 -100.0(3) . . . . ?
C13 B12 B17 B22 -62.1(4) . . . . ?
C13 B12 B21 B16 -38.9(3) . . . . ?
C13 B12 B21 B17 99.1(3) . . . . ?
C13 B12 B21 B20 -1.5(4) . . . . ?
C13 B12 B21 B22 61.4(4) . . . . ?
C13 B13 B14 B15 -34.2(3) . . . . ?
C13 B13 B14 B18 -134.9(3) . . . . ?
C13 B13 B14 B19 -97.5(3) . . . . ?
C13 B13 B17 B12 -38.6(3) . . . . ?
C13 B13 B17 B18 99.3(3) . . . . ?
C13 B13 B17 B21 -2.4(4) . . . . ?
C13 B13 B17 B22 61.2(4) . . . . ?
C13 B13 B18 B14 38.9(3) . . . . ?
C13 B13 B18 B17 -99.4(3) . . . . ?
C13 B13 B18 B19 1.6(4) . . . . ?
C13 B13 B18 B22 -61.3(4) . . . . ?
C13 B14 B15 B16 -33.2(2) . . . . ?
C13 B14 B15 B19 -134.5(3) . . . . ?
C13 B14 B15 B20 -96.8(3) . . . . ?
C13 B14 B18 B13 -38.9(3) . . . . ?
C13 B14 B18 B17 -1.8(4) . . . . ?
C13 B14 B18 B19 99.1(3) . . . . ?
C13 B14 B18 B22 61.7(4) . . . . ?
C13 B14 B19 B15 39.1(3) . . . . ?
C13 B14 B19 B18 -98.6(3) . . . . ?
C13 B14 B19 B20 2.0(4) . . . . ?
C13 B14 B19 B22 -61.0(4) . . . . ?
C13 B15 B16 B12 -34.2(2) . . . . ?
C13 B15 B16 B20 -133.9(3) . . . . ?
C13 B15 B16 B21 -96.5(3) . . . . ?
C13 B15 B19 B14 -39.3(3) . . . . ?
C13 B15 B19 B18 -1.3(4) . . . . ?
C13 B15 B19 B20 98.7(3) . . . . ?
C13 B15 B19 B22 61.6(4) . . . . ?
C13 B15 B20 B16 39.8(3) . . . . ?
C13 B15 B20 B19 -99.3(3) . . . . ?
C13 B15 B20 B21 1.9(4) . . . . ?
C13 B15 B20 B22 -62.1(4) . . . . ?
C13 B16 B20 B15 -39.8(3) . . . . ?
C13 B16 B20 B19 -2.9(4) . . . . ?
C13 B16 B20 B21 98.3(3) . . . . ?
C13 B16 B20 B22 60.4(4) . . . . ?
C13 B16 B21 B12 38.5(3) . . . . ?
C13 B16 B21 B17 0.7(4) . . . . ?
C13 B16 B21 B20 -99.2(3) . . . . ?
C13 B16 B21 B22 -62.0(4) . . . . ?
C14 C11 C12 N2 178.6(3) . . . . ?
C14 B1 B2 B3 -33.4(3) . . . . ?
C14 B1 B2 B6 -135.1(4) . . . . ?
C14 B1 B2 B10 -97.2(4) . . . . ?
C14 B1 B5 B4 33.3(3) . . . . ?
C14 B1 B5 B7 135.3(3) . . . . ?
C14 B1 B5 B8 97.4(3) . . . . ?
C14 B1 B6 B2 39.2(3) . . . . ?
C14 B1 B6 B7 -98.8(4) . . . . ?
C14 B1 B6 B10 3.1(5) . . . . ?
C14 B1 B6 B11 -59.6(5) . . . . ?
C14 B1 B7 B5 -38.9(3) . . . . ?
C14 B1 B7 B6 100.1(4) . . . . ?
C14 B1 B7 B8 -1.6(5) . . . . ?
C14 B1 B7 B11 61.5(4) . . . . ?
C14 B2 B3 B4 -33.9(3) . . . . ?
C14 B2 B3 B9 -97.3(3) . . . . ?
C14 B2 B3 B10 -134.7(4) . . . . ?
C14 B2 B6 B1 -38.3(3) . . . . ?
C14 B2 B6 B7 -0.2(5) . . . . ?
C14 B2 B6 B10 100.2(4) . . . . ?
C14 B2 B6 B11 63.8(5) . . . . ?
C14 B2 B10 B3 39.2(3) . . . . ?
C14 B2 B10 B6 -98.0(4) . . . . ?
C14 B2 B10 B9 2.0(6) . . . . ?
C14 B2 B10 B11 -61.2(5) . . . . ?
C14 B3 B4 B5 -33.8(3) . . . . ?
C14 B3 B4 B8 -97.5(3) . . . . ?
C14 B3 B4 B9 -134.3(4) . . . . ?
C14 B3 B9 B4 39.3(3) . . . . ?
C14 B3 B9 B8 3.0(5) . . . . ?
C14 B3 B9 B10 -97.9(4) . . . . ?
C14 B3 B9 B11 -60.8(4) . . . . ?
C14 B3 B10 B2 -38.7(3) . . . . ?
C14 B3 B10 B6 -0.2(5) . . . . ?
C14 B3 B10 B9 99.5(4) . . . . ?
C14 B3 B10 B11 62.8(4) . . . . ?
C14 B4 B5 B1 -32.9(3) . . . . ?
C14 B4 B5 B7 -96.8(4) . . . . ?
C14 B4 B5 B8 -134.8(3) . . . . ?
C14 B4 B8 B5 39.4(3) . . . . ?
C14 B4 B8 B7 2.3(4) . . . . ?
C14 B4 B8 B9 -98.0(3) . . . . ?
C14 B4 B8 B11 -60.8(4) . . . . ?
C14 B4 B9 B3 -39.2(3) . . . . ?
C14 B4 B9 B8 100.1(4) . . . . ?
C14 B4 B9 B10 -0.9(5) . . . . ?
C14 B4 B9 B11 62.4(4) . . . . ?
C14 B5 B7 B1 38.2(3) . . . . ?
C14 B5 B7 B6 1.8(4) . . . . ?
C14 B5 B7 B8 -99.9(3) . . . . ?
C14 B5 B7 B11 -61.6(4) . . . . ?
C14 B5 B8 B4 -39.3(3) . . . . ?
C14 B5 B8 B7 98.8(4) . . . . ?
C14 B5 B8 B9 -1.6(4) . . . . ?
C14 B5 B8 B11 60.5(4) . . . . ?
C15 N4 C1 Pt1 -13.7(5) . . . . ?
C15 N4 C1 N3 174.8(3) . . . . ?
C15 N4 C18 C19 -175.4(3) . . . . ?
C15 N4 C18 C23 6.8(6) . . . . ?
C15 C16 C17 N5 84.0(4) . . . . ?
C17 N5 C2 Pt1 -2.7(6) . . . . ?
C17 N5 C2 N6 -177.7(3) . . . . ?
C17 N5 C24 C25 0.9(8) . . . . ?
C17 N5 C24 C29 177.1(4) . . . . ?
C18 N4 C1 Pt1 170.1(2) . . . . ?
C18 N4 C1 N3 -1.4(4) . . . . ?
C18 N4 C15 C16 -92.0(4) . . . . ?
C18 C19 C20 C21 0.9(7) . . . . ?
C19 N3 C1 Pt1 -169.7(3) . . . . ?
C19 N3 C1 N4 1.3(4) . . . . ?
C19 N3 C30 C31 -81.9(5) . . . . ?
C19 C18 C23 C22 0.0(7) . . . . ?
C19 C20 C21 C22 -2.4(9) . . . . ?
C20 C21 C22 C23 2.8(11) . . . . ?
C21 C22 C23 C18 -1.5(9) . . . . ?
C23 C18 C19 N3 178.1(4) . . . . ?
C23 C18 C19 C20 0.3(6) . . . . ?
C24 N5 C2 Pt1 175.4(3) . . . . ?
C24 N5 C2 N6 0.5(5) . . . . ?
C24 N5 C17 C16 98.0(4) . . . . ?
C24 C25 C26 C27 -2.4(12) . . . . ?
C25 C24 C29 N6 177.9(5) . . . . ?
C25 C24 C29 C28 -1.4(8) . . . . ?
C25 C26 C27 C28 -1.4(15) . . . . ?
C26 C27 C28 C29 3.8(12) . . . . ?
C27 C28 C29 N6 178.4(6) . . . . ?
C27 C28 C29 C24 -2.4(9) . . . . ?
C29 N6 C2 Pt1 -174.4(3) . . . . ?
C29 N6 C2 N5 0.3(5) . . . . ?
C29 N6 C42 C43 -73.0(5) . . . . ?
C29 C24 C25 C26 3.8(9) . . . . ?
C30 N3 C1 Pt1 12.9(5) . . . . ?
C30 N3 C1 N4 -176.0(3) . . . . ?
C30 N3 C19 C18 176.6(3) . . . . ?
C30 N3 C19 C20 -5.8(6) . . . . ?
C30 C31 C32 C33 166.9(6) . . . . ?
C31 C32 C33 C34 170.2(6) . . . . ?
C32 C33 C34 C35 -72.1(11) . . . . ?
C33 C34 C35 C36 -167.8(7) . . . . ?
C34 C35 C36 C37 177.0(7) . . . . ?
C35 C36 C37 C38 172.2(7) . . . . ?
C36 C37 C38 C39 -66.9(10) . . . . ?
C37 C38 C39 C40 -161.3(8) . . . . ?
C38 C39 C40 C41 -173.5(9) . . . . ?
C42 N6 C2 Pt1 8.9(6) . . . . ?
C42 N6 C2 N5 -176.3(3) . . . . ?
C42 N6 C29 C24 175.7(4) . . . . ?
C42 N6 C29 C28 -5.0(8) . . . . ?
C42 C43 C44 C45 -179.3(4) . . . . ?
C43 C44 C45 C46 169.8(5) . . . . ?
C44 C45 C46 C47 56.6(9) . . . . ?
C45 C46 C47 C48 173.1(8) . . . . ?
C46 C47 C48 C49 162.3(10) . . . . ?
C47 C48 C49 C50 -168.9(11) . . . . ?
C48 C49 C50 C51 174.5(12) . . . . ?
C49 C50 C51 C52 -80.5(19) . . . . ?
C50 C51 C52 C53 -153.3(13) . . . . ?
B1 C14 B2 B3 142.3(4) . . . . ?
B1 C14 B2 B6 38.7(4) . . . . ?
B1 C14 B2 B10 102.5(4) . . . . ?
B1 C14 B3 B2 -36.5(4) . . . . ?
B1 C14 B3 B4 105.0(4) . . . . ?
B1 C14 B3 B9 65.0(4) . . . . ?
B1 C14 B3 B10 2.3(5) . . . . ?
B1 C14 B4 B3 -106.1(4) . . . . ?
B1 C14 B4 B5 36.2(3) . . . . ?
B1 C14 B4 B8 -3.5(4) . . . . ?
B1 C14 B4 B9 -66.7(4) . . . . ?
B1 C14 B5 B4 -142.4(3) . . . . ?
B1 C14 B5 B7 -39.2(3) . . . . ?
B1 C14 B5 B8 -102.5(3) . . . . ?
B1 B2 B3 C14 33.1(3) . . . . ?
B1 B2 B3 B4 -0.7(4) . . . . ?
B1 B2 B3 B9 -64.2(4) . . . . ?
B1 B2 B3 B10 -101.6(4) . . . . ?
B1 B2 B6 B7 38.1(4) . . . . ?
B1 B2 B6 B10 138.5(4) . . . . ?
B1 B2 B6 B11 102.1(4) . . . . ?
B1 B2 B10 B3 100.4(4) . . . . ?
B1 B2 B10 B6 -36.8(4) . . . . ?
B1 B2 B10 B9 63.2(5) . . . . ?
B1 B2 B10 B11 0.1(5) . . . . ?
B1 B5 B7 B6 -36.4(4) . . . . ?
B1 B5 B7 B8 -138.1(4) . . . . ?
B1 B5 B7 B11 -99.9(4) . . . . ?
B1 B5 B8 B4 -100.4(4) . . . . ?
B1 B5 B8 B7 37.7(3) . . . . ?
B1 B5 B8 B9 -62.6(4) . . . . ?
B1 B5 B8 B11 -0.5(4) . . . . ?
B1 B6 B7 B5 36.8(3) . . . . ?
B1 B6 B7 B8 100.1(4) . . . . ?
B1 B6 B7 B11 136.5(4) . . . . ?
B1 B6 B10 B2 37.0(4) . . . . ?
B1 B6 B10 B3 -1.8(5) . . . . ?
B1 B6 B10 B9 -64.5(5) . . . . ?
B1 B6 B10 B11 -101.6(4) . . . . ?
B1 B6 B11 B7 -39.3(4) . . . . ?
B1 B6 B11 B8 -3.1(6) . . . . ?
B1 B6 B11 B9 61.4(5) . . . . ?
B1 B6 B11 B10 99.3(4) . . . . ?
B1 B7 B8 B4 -0.5(5) . . . . ?
B1 B7 B8 B5 -37.5(3) . . . . ?
B1 B7 B8 B9 62.4(4) . . . . ?
B1 B7 B8 B11 99.3(4) . . . . ?
B1 B7 B11 B6 38.2(3) . . . . ?
B1 B7 B11 B8 -101.4(3) . . . . ?
B1 B7 B11 B9 -63.4(4) . . . . ?
B1 B7 B11 B10 0.6(5) . . . . ?
B2 C14 B1 B5 -141.3(3) . . . . ?
B2 C14 B1 B6 -39.9(4) . . . . ?
B2 C14 B1 B7 -102.4(4) . . . . ?
B2 C14 B3 B4 141.5(4) . . . . ?
B2 C14 B3 B9 101.4(4) . . . . ?
B2 C14 B3 B10 38.8(3) . . . . ?
B2 C14 B4 B3 -37.1(4) . . . . ?
B2 C14 B4 B5 105.1(4) . . . . ?
B2 C14 B4 B8 65.4(4) . . . . ?
B2 C14 B4 B9 2.3(5) . . . . ?
B2 C14 B5 B1 37.2(3) . . . . ?
B2 C14 B5 B4 -105.2(3) . . . . ?
B2 C14 B5 B7 -2.0(4) . . . . ?
B2 C14 B5 B8 -65.3(4) . . . . ?
B2 B1 B5 C14 -34.5(3) . . . . ?
B2 B1 B5 B4 -1.1(4) . . . . ?
B2 B1 B5 B7 100.9(4) . . . . ?
B2 B1 B5 B8 62.9(4) . . . . ?
B2 B1 B6 B7 -138.0(4) . . . . ?
B2 B1 B6 B10 -36.1(4) . . . . ?
B2 B1 B6 B11 -98.8(5) . . . . ?
B2 B1 B7 B5 -101.0(3) . . . . ?
B2 B1 B7 B6 38.0(4) . . . . ?
B2 B1 B7 B8 -63.7(4) . . . . ?
B2 B1 B7 B11 -0.6(4) . . . . ?
B2 B3 B4 C14 33.8(3) . . . . ?
B2 B3 B4 B5 0.0(4) . . . . ?
B2 B3 B4 B8 -63.6(4) . . . . ?
B2 B3 B4 B9 -100.5(4) . . . . ?
B2 B3 B9 B4 100.5(4) . . . . ?
B2 B3 B9 B8 64.2(4) . . . . ?
B2 B3 B9 B10 -36.6(4) . . . . ?
B2 B3 B9 B11 0.5(4) . . . . ?
B2 B3 B10 B6 38.5(4) . . . . ?
B2 B3 B10 B9 138.2(4) . . . . ?
B2 B3 B10 B11 101.4(4) . . . . ?
B2 B6 B7 B1 -37.9(3) . . . . ?
B2 B6 B7 B5 -1.0(5) . . . . ?
B2 B6 B7 B8 62.3(5) . . . . ?
B2 B6 B7 B11 98.7(4) . . . . ?
B2 B6 B10 B3 -38.8(4) . . . . ?
B2 B6 B10 B9 -101.5(4) . . . . ?
B2 B6 B10 B11 -138.6(4) . . . . ?
B2 B6 B11 B7 -102.7(4) . . . . ?
B2 B6 B11 B8 -66.5(5) . . . . ?
B2 B6 B11 B9 -2.0(5) . . . . ?
B2 B6 B11 B10 35.9(4) . . . . ?
B2 B10 B11 B6 -37.2(4) . . . . ?
B2 B10 B11 B7 -0.4(5) . . . . ?
B2 B10 B11 B8 63.3(5) . . . . ?
B2 B10 B11 B9 101.0(4) . . . . ?
B3 C14 B1 B2 36.5(3) . . . . ?
B3 C14 B1 B5 -104.8(3) . . . . ?
B3 C14 B1 B6 -3.5(5) . . . . ?
B3 C14 B1 B7 -65.9(4) . . . . ?
B3 C14 B2 B1 -142.3(4) . . . . ?
B3 C14 B2 B6 -103.6(4) . . . . ?
B3 C14 B2 B10 -39.8(4) . . . . ?
B3 C14 B4 B5 142.2(3) . . . . ?
B3 C14 B4 B8 102.5(4) . . . . ?
B3 C14 B4 B9 39.4(3) . . . . ?
B3 C14 B5 B1 106.2(3) . . . . ?
B3 C14 B5 B4 -36.3(3) . . . . ?
B3 C14 B5 B7 66.9(4) . . . . ?
B3 C14 B5 B8 3.6(4) . . . . ?
B3 B2 B6 B1 -99.9(4) . . . . ?
B3 B2 B6 B7 -61.7(5) . . . . ?
B3 B2 B6 B10 38.6(4) . . . . ?
B3 B2 B6 B11 2.3(5) . . . . ?
B3 B2 B10 B6 -137.2(4) . . . . ?
B3 B2 B10 B9 -37.2(4) . . . . ?
B3 B2 B10 B11 -100.3(4) . . . . ?
B3 B4 B5 C14 33.6(3) . . . . ?
B3 B4 B5 B1 0.7(4) . . . . ?
B3 B4 B5 B7 -63.2(4) . . . . ?
B3 B4 B5 B8 -101.2(4) . . . . ?
B3 B4 B8 B5 101.2(4) . . . . ?
B3 B4 B8 B7 64.1(4) . . . . ?
B3 B4 B8 B9 -36.2(3) . . . . ?
B3 B4 B8 B11 1.0(4) . . . . ?
B3 B4 B9 B8 139.4(4) . . . . ?
B3 B4 B9 B10 38.4(4) . . . . ?
B3 B4 B9 B11 101.6(4) . . . . ?
B3 B9 B10 B2 37.8(4) . . . . ?
B3 B9 B10 B6 101.5(4) . . . . ?
B3 B9 B10 B11 138.6(4) . . . . ?
B3 B9 B11 B6 1.0(5) . . . . ?
B3 B9 B11 B7 63.8(5) . . . . ?
B3 B9 B11 B8 101.4(3) . . . . ?
B3 B9 B11 B10 -37.2(3) . . . . ?
B3 B10 B11 B6 -101.5(4) . . . . ?
B3 B10 B11 B7 -64.8(5) . . . . ?
B3 B10 B11 B8 -1.0(5) . . . . ?
B3 B10 B11 B9 36.6(3) . . . . ?
B4 C14 B1 B2 105.6(3) . . . . ?
B4 C14 B1 B5 -35.7(3) . . . . ?
B4 C14 B1 B6 65.6(5) . . . . ?
B4 C14 B1 B7 3.2(4) . . . . ?
B4 C14 B2 B1 -105.2(4) . . . . ?
B4 C14 B2 B3 37.1(4) . . . . ?
B4 C14 B2 B6 -66.5(5) . . . . ?
B4 C14 B2 B10 -2.7(5) . . . . ?
B4 C14 B3 B2 -141.5(4) . . . . ?
B4 C14 B3 B9 -40.1(3) . . . . ?
B4 C14 B3 B10 -102.7(4) . . . . ?
B4 C14 B5 B1 142.4(3) . . . . ?
B4 C14 B5 B7 103.2(3) . . . . ?
B4 C14 B5 B8 39.9(3) . . . . ?
B4 B3 B9 B8 -36.3(3) . . . . ?
B4 B3 B9 B10 -137.1(4) . . . . ?
B4 B3 B9 B11 -100.0(4) . . . . ?
B4 B3 B10 B2 -99.8(4) . . . . ?
B4 B3 B10 B6 -61.3(5) . . . . ?
B4 B3 B10 B9 38.4(3) . . . . ?
B4 B3 B10 B11 1.7(5) . . . . ?
B4 B5 B7 B1 100.2(4) . . . . ?
B4 B5 B7 B6 63.8(4) . . . . ?
B4 B5 B7 B8 -37.9(3) . . . . ?
B4 B5 B7 B11 0.4(5) . . . . ?
B4 B5 B8 B7 138.1(4) . . . . ?
B4 B5 B8 B9 37.7(3) . . . . ?
B4 B5 B8 B11 99.8(4) . . . . ?
B4 B8 B9 B3 36.7(3) . . . . ?
B4 B8 B9 B10 100.5(4) . . . . ?
B4 B8 B9 B11 137.6(3) . . . . ?
B4 B8 B11 B6 64.8(5) . . . . ?
B4 B8 B11 B7 100.6(4) . . . . ?
B4 B8 B11 B9 -37.5(3) . . . . ?
B4 B8 B11 B10 0.0(5) . . . . ?
B4 B9 B10 B2 -0.7(6) . . . . ?
B4 B9 B10 B3 -38.5(4) . . . . ?
B4 B9 B10 B6 62.9(5) . . . . ?
B4 B9 B10 B11 100.0(4) . . . . ?
B4 B9 B11 B6 -63.0(5) . . . . ?
B4 B9 B11 B7 -0.1(5) . . . . ?
B4 B9 B11 B8 37.5(3) . . . . ?
B4 B9 B11 B10 -101.1(4) . . . . ?
B5 C14 B1 B2 141.3(3) . . . . ?
B5 C14 B1 B6 101.4(4) . . . . ?
B5 C14 B1 B7 39.0(3) . . . . ?
B5 C14 B2 B1 -37.3(3) . . . . ?
B5 C14 B2 B3 105.0(3) . . . . ?
B5 C14 B2 B6 1.4(5) . . . . ?
B5 C14 B2 B10 65.2(5) . . . . ?
B5 C14 B3 B2 -105.6(3) . . . . ?
B5 C14 B3 B4 35.9(3) . . . . ?
B5 C14 B3 B9 -4.2(4) . . . . ?
B5 C14 B3 B10 -66.8(4) . . . . ?
B5 C14 B4 B3 -142.2(3) . . . . ?
B5 C14 B4 B8 -39.7(3) . . . . ?
B5 C14 B4 B9 -102.8(4) . . . . ?
B5 B1 B2 C14 34.5(3) . . . . ?
B5 B1 B2 B3 1.1(4) . . . . ?
B5 B1 B2 B6 -100.6(4) . . . . ?
B5 B1 B2 B10 -62.7(4) . . . . ?
B5 B1 B6 B2 101.5(4) . . . . ?
B5 B1 B6 B7 -36.5(4) . . . . ?
B5 B1 B6 B10 65.4(5) . . . . ?
B5 B1 B6 B11 2.8(6) . . . . ?
B5 B1 B7 B6 139.0(4) . . . . ?
B5 B1 B7 B8 37.3(3) . . . . ?
B5 B1 B7 B11 100.4(4) . . . . ?
B5 B4 B8 B7 -37.1(3) . . . . ?
B5 B4 B8 B9 -137.4(4) . . . . ?
B5 B4 B8 B11 -100.2(4) . . . . ?
B5 B4 B9 B3 -101.3(4) . . . . ?
B5 B4 B9 B8 38.1(3) . . . . ?
B5 B4 B9 B10 -62.9(5) . . . . ?
B5 B4 B9 B11 0.4(5) . . . . ?
B5 B7 B8 B4 37.1(3) . . . . ?
B5 B7 B8 B9 100.0(3) . . . . ?
B5 B7 B8 B11 136.9(4) . . . . ?
B5 B7 B11 B6 101.4(4) . . . . ?
B5 B7 B11 B8 -38.1(3) . . . . ?
B5 B7 B11 B9 -0.1(5) . . . . ?
B5 B7 B11 B10 63.9(5) . . . . ?
B5 B8 B9 B3 -0.9(5) . . . . ?
B5 B8 B9 B4 -37.6(3) . . . . ?
B5 B8 B9 B10 62.9(4) . . . . ?
B5 B8 B9 B11 100.0(4) . . . . ?
B5 B8 B11 B6 2.2(5) . . . . ?
B5 B8 B11 B7 38.1(3) . . . . ?
B5 B8 B11 B9 -100.0(4) . . . . ?
B5 B8 B11 B10 -62.5(4) . . . . ?
B6 B1 B2 C14 135.1(4) . . . . ?
B6 B1 B2 B3 101.7(4) . . . . ?
B6 B1 B2 B10 37.9(4) . . . . ?
B6 B1 B5 C14 -98.7(4) . . . . ?
B6 B1 B5 B4 -65.4(5) . . . . ?
B6 B1 B5 B7 36.6(4) . . . . ?
B6 B1 B5 B8 -1.4(5) . . . . ?
B6 B1 B7 B5 -139.0(4) . . . . ?
B6 B1 B7 B8 -101.7(4) . . . . ?
B6 B1 B7 B11 -38.5(4) . . . . ?
B6 B2 B3 C14 95.6(4) . . . . ?
B6 B2 B3 B4 61.8(4) . . . . ?
B6 B2 B3 B9 -1.7(5) . . . . ?
B6 B2 B3 B10 -39.1(4) . . . . ?
B6 B2 B10 B3 137.2(4) . . . . ?
B6 B2 B10 B9 100.0(5) . . . . ?
B6 B2 B10 B11 36.9(4) . . . . ?
B6 B7 B8 B4 -63.3(4) . . . . ?
B6 B7 B8 B5 -100.4(4) . . . . ?
B6 B7 B8 B9 -0.4(4) . . . . ?
B6 B7 B8 B11 36.5(3) . . . . ?
B6 B7 B11 B8 -139.6(4) . . . . ?
B6 B7 B11 B9 -101.6(4) . . . . ?
B6 B7 B11 B10 -37.5(4) . . . . ?
B6 B10 B11 B7 36.7(3) . . . . ?
B6 B10 B11 B8 100.5(4) . . . . ?
B6 B10 B11 B9 138.1(3) . . . . ?
B7 B1 B2 C14 97.5(3) . . . . ?
B7 B1 B2 B3 64.2(4) . . . . ?
B7 B1 B2 B6 -37.5(3) . . . . ?
B7 B1 B2 B10 0.3(5) . . . . ?
B7 B1 B5 C14 -135.3(3) . . . . ?
B7 B1 B5 B4 -102.0(4) . . . . ?
B7 B1 B5 B8 -38.0(3) . . . . ?
B7 B1 B6 B2 138.0(4) . . . . ?
B7 B1 B6 B10 101.8(4) . . . . ?
B7 B1 B6 B11 39.2(4) . . . . ?
B7 B5 B8 B4 -138.1(4) . . . . ?
B7 B5 B8 B9 -100.4(4) . . . . ?
B7 B5 B8 B11 -38.3(3) . . . . ?
B7 B6 B10 B2 101.2(4) . . . . ?
B7 B6 B10 B3 62.5(5) . . . . ?
B7 B6 B10 B9 -0.3(5) . . . . ?
B7 B6 B10 B11 -37.4(3) . . . . ?
B7 B6 B11 B8 36.2(3) . . . . ?
B7 B6 B11 B9 100.7(4) . . . . ?
B7 B6 B11 B10 138.6(3) . . . . ?
B7 B8 B9 B3 -63.5(4) . . . . ?
B7 B8 B9 B4 -100.3(3) . . . . ?
B7 B8 B9 B10 0.3(4) . . . . ?
B7 B8 B9 B11 37.3(3) . . . . ?
B7 B8 B11 B6 -35.8(4) . . . . ?
B7 B8 B11 B9 -138.1(4) . . . . ?
B7 B8 B11 B10 -100.6(4) . . . . ?
B8 B4 B5 C14 134.8(3) . . . . ?
B8 B4 B5 B1 101.8(3) . . . . ?
B8 B4 B5 B7 38.0(3) . . . . ?
B8 B4 B9 B3 -139.4(4) . . . . ?
B8 B4 B9 B10 -101.0(4) . . . . ?
B8 B4 B9 B11 -37.8(3) . . . . ?
B8 B5 B7 B1 138.1(4) . . . . ?
B8 B5 B7 B6 101.7(4) . . . . ?
B8 B5 B7 B11 38.2(3) . . . . ?
B8 B7 B11 B6 139.6(4) . . . . ?
B8 B7 B11 B9 38.0(3) . . . . ?
B8 B7 B11 B10 102.0(4) . . . . ?
B8 B9 B10 B2 -63.6(5) . . . . ?
B8 B9 B10 B3 -101.5(4) . . . . ?
B8 B9 B10 B6 0.0(4) . . . . ?
B8 B9 B10 B11 37.1(3) . . . . ?
B8 B9 B11 B6 -100.5(4) . . . . ?
B8 B9 B11 B7 -37.6(3) . . . . ?
B8 B9 B11 B10 -138.6(3) . . . . ?
B9 B3 B4 C14 134.3(4) . . . . ?
B9 B3 B4 B5 100.5(4) . . . . ?
B9 B3 B4 B8 36.8(3) . . . . ?
B9 B3 B10 B2 -138.2(4) . . . . ?
B9 B3 B10 B6 -99.8(4) . . . . ?
B9 B3 B10 B11 -36.8(3) . . . . ?
B9 B4 B5 C14 96.3(3) . . . . ?
B9 B4 B5 B1 63.4(4) . . . . ?
B9 B4 B5 B7 -0.5(5) . . . . ?
B9 B4 B5 B8 -38.5(3) . . . . ?
B9 B4 B8 B5 137.4(4) . . . . ?
B9 B4 B8 B7 100.3(4) . . . . ?
B9 B4 B8 B11 37.2(3) . . . . ?
B9 B8 B11 B6 102.2(4) . . . . ?
B9 B8 B11 B7 138.1(4) . . . . ?
B9 B8 B11 B10 37.5(4) . . . . ?
B9 B10 B11 B6 -138.1(3) . . . . ?
B9 B10 B11 B7 -101.4(4) . . . . ?
B9 B10 B11 B8 -37.7(3) . . . . ?
B10 B2 B3 C14 134.7(4) . . . . ?
B10 B2 B3 B4 100.9(4) . . . . ?
B10 B2 B3 B9 37.4(4) . . . . ?
B10 B2 B6 B1 -138.5(4) . . . . ?
B10 B2 B6 B7 -100.3(4) . . . . ?
B10 B2 B6 B11 -36.4(4) . . . . ?
B10 B3 B4 C14 95.8(4) . . . . ?
B10 B3 B4 B5 62.0(4) . . . . ?
B10 B3 B4 B8 -1.7(5) . . . . ?
B10 B3 B4 B9 -38.5(4) . . . . ?
B10 B3 B9 B4 137.1(4) . . . . ?
B10 B3 B9 B8 100.8(4) . . . . ?
B10 B3 B9 B11 37.1(4) . . . . ?
B10 B6 B7 B1 -99.7(4) . . . . ?
B10 B6 B7 B5 -62.9(4) . . . . ?
B10 B6 B7 B8 0.4(4) . . . . ?
B10 B6 B7 B11 36.8(3) . . . . ?
B10 B6 B11 B7 -138.6(3) . . . . ?
B10 B6 B11 B8 -102.4(4) . . . . ?
B10 B6 B11 B9 -37.9(3) . . . . ?
B10 B9 B11 B6 38.2(4) . . . . ?
B10 B9 B11 B7 101.0(4) . . . . ?
B10 B9 B11 B8 138.6(3) . . . . ?
B11 B6 B7 B1 -136.5(4) . . . . ?
B11 B6 B7 B5 -99.7(4) . . . . ?
B11 B6 B7 B8 -36.4(3) . . . . ?
B11 B6 B10 B2 138.6(4) . . . . ?
B11 B6 B10 B3 99.9(4) . . . . ?
B11 B6 B10 B9 37.1(3) . . . . ?
B11 B7 B8 B4 -99.8(4) . . . . ?
B11 B7 B8 B5 -136.9(4) . . . . ?
B11 B7 B8 B9 -36.9(3) . . . . ?
B11 B8 B9 B3 -100.8(4) . . . . ?
B11 B8 B9 B4 -137.6(3) . . . . ?
B11 B8 B9 B10 -37.1(3) . . . . ?
B11 B9 B10 B2 -100.7(5) . . . . ?
B11 B9 B10 B3 -138.6(4) . . . . ?
B11 B9 B10 B6 -37.1(3) . . . . ?
B12 C13 B13 B14 142.1(3) . . . . ?
B12 C13 B13 B17 39.5(3) . . . . ?
B12 C13 B13 B18 102.2(3) . . . . ?
B12 C13 B14 B13 -36.3(3) . . . . ?
B12 C13 B14 B15 104.8(3) . . . . ?
B12 C13 B14 B18 2.7(4) . . . . ?
B12 C13 B14 B19 65.0(4) . . . . ?
B12 C13 B15 B14 -105.5(3) . . . . ?
B12 C13 B15 B16 37.3(3) . . . . ?
B12 C13 B15 B19 -65.7(4) . . . . ?
B12 C13 B15 B20 -3.0(4) . . . . ?
B12 C13 B16 B15 -141.1(3) . . . . ?
B12 C13 B16 B20 -100.8(3) . . . . ?
B12 C13 B16 B21 -38.6(3) . . . . ?
B12 B13 B14 C13 33.4(3) . . . . ?
B12 B13 B14 B15 -0.8(4) . . . . ?
B12 B13 B14 B18 -101.5(3) . . . . ?
B12 B13 B14 B19 -64.2(4) . . . . ?
B12 B13 B17 B18 137.9(3) . . . . ?
B12 B13 B17 B21 36.2(3) . . . . ?
B12 B13 B17 B22 99.8(3) . . . . ?
B12 B13 B18 B14 100.4(3) . . . . ?
B12 B13 B18 B17 -37.9(3) . . . . ?
B12 B13 B18 B19 63.0(4) . . . . ?
B12 B13 B18 B22 0.2(4) . . . . ?
B12 B16 B20 B15 -101.0(3) . . . . ?
B12 B16 B20 B19 -64.1(4) . . . . ?
B12 B16 B20 B21 37.1(3) . . . . ?
B12 B16 B20 B22 -0.8(4) . . . . ?
B12 B16 B21 B17 -37.7(3) . . . . ?
B12 B16 B21 B20 -137.6(3) . . . . ?
B12 B16 B21 B22 -100.5(3) . . . . ?
B12 B17 B18 B13 37.7(3) . . . . ?
B12 B17 B18 B14 0.3(5) . . . . ?
B12 B17 B18 B19 -62.7(4) . . . . ?
B12 B17 B18 B22 -99.6(3) . . . . ?
B12 B17 B21 B16 37.7(3) . . . . ?
B12 B17 B21 B20 100.4(3) . . . . ?
B12 B17 B21 B22 137.3(3) . . . . ?
B12 B17 B22 B18 101.5(3) . . . . ?
B12 B17 B22 B19 64.0(4) . . . . ?
B12 B17 B22 B20 -0.2(4) . . . . ?
B12 B17 B22 B21 -37.4(3) . . . . ?
B12 B21 B22 B17 38.1(3) . . . . ?
B12 B21 B22 B18 1.3(4) . . . . ?
B12 B21 B22 B19 -63.2(4) . . . . ?
B12 B21 B22 B20 -100.3(3) . . . . ?
B13 C13 B12 B16 -142.2(3) . . . . ?
B13 C13 B12 B17 -39.0(3) . . . . ?
B13 C13 B12 B21 -102.3(3) . . . . ?
B13 C13 B14 B15 141.1(3) . . . . ?
B13 C13 B14 B18 39.0(3) . . . . ?
B13 C13 B14 B19 101.3(3) . . . . ?
B13 C13 B15 B14 -37.4(3) . . . . ?
B13 C13 B15 B16 105.4(3) . . . . ?
B13 C13 B15 B19 2.4(4) . . . . ?
B13 C13 B15 B20 65.2(4) . . . . ?
B13 C13 B16 B12 36.2(3) . . . . ?
B13 C13 B16 B15 -104.9(3) . . . . ?
B13 C13 B16 B20 -64.6(4) . . . . ?
B13 C13 B16 B21 -2.4(4) . . . . ?
B13 B12 B16 C13 -33.8(3) . . . . ?
B13 B12 B16 B15 0.5(4) . . . . ?
B13 B12 B16 B20 63.8(4) . . . . ?
B13 B12 B16 B21 101.3(3) . . . . ?
B13 B12 B17 B18 -37.8(3) . . . . ?
B13 B12 B17 B21 -139.0(3) . . . . ?
B13 B12 B17 B22 -101.1(3) . . . . ?
B13 B12 B21 B16 -101.5(3) . . . . ?
B13 B12 B21 B17 36.5(3) . . . . ?
B13 B12 B21 B20 -64.0(4) . . . . ?
B13 B12 B21 B22 -1.2(4) . . . . ?
B13 B14 B15 C13 34.3(3) . . . . ?
B13 B14 B15 B16 1.2(4) . . . . ?
B13 B14 B15 B19 -100.2(3) . . . . ?
B13 B14 B15 B20 -62.4(4) . . . . ?
B13 B14 B18 B17 37.1(3) . . . . ?
B13 B14 B18 B19 138.0(3) . . . . ?
B13 B14 B18 B22 100.6(3) . . . . ?
B13 B14 B19 B15 100.7(3) . . . . ?
B13 B14 B19 B18 -37.0(3) . . . . ?
B13 B14 B19 B20 63.6(4) . . . . ?
B13 B14 B19 B22 0.6(4) . . . . ?
B13 B17 B18 B14 -37.3(3) . . . . ?
B13 B17 B18 B19 -100.3(3) . . . . ?
B13 B17 B18 B22 -137.2(3) . . . . ?
B13 B17 B21 B12 -36.6(3) . . . . ?
B13 B17 B21 B16 1.1(4) . . . . ?
B13 B17 B21 B20 63.8(4) . . . . ?
B13 B17 B21 B22 100.7(3) . . . . ?
B13 B17 B22 B18 38.3(3) . . . . ?
B13 B17 B22 B19 0.7(4) . . . . ?
B13 B17 B22 B20 -63.5(4) . . . . ?
B13 B17 B22 B21 -100.6(3) . . . . ?
B13 B18 B19 B14 37.5(3) . . . . ?
B13 B18 B19 B15 -0.2(4) . . . . ?
B13 B18 B19 B20 -62.8(4) . . . . ?
B13 B18 B19 B22 -100.2(3) . . . . ?
B13 B18 B22 B17 -37.9(3) . . . . ?
B13 B18 B22 B19 100.7(3) . . . . ?
B13 B18 B22 B20 62.6(4) . . . . ?
B13 B18 B22 B21 -0.9(4) . . . . ?
B14 C13 B12 B13 36.5(3) . . . . ?
B14 C13 B12 B16 -105.7(3) . . . . ?
B14 C13 B12 B17 -2.5(4) . . . . ?
B14 C13 B12 B21 -65.8(4) . . . . ?
B14 C13 B13 B12 -142.1(3) . . . . ?
B14 C13 B13 B17 -102.5(3) . . . . ?
B14 C13 B13 B18 -39.9(3) . . . . ?
B14 C13 B15 B16 142.8(3) . . . . ?
B14 C13 B15 B19 39.8(3) . . . . ?
B14 C13 B15 B20 102.5(3) . . . . ?
B14 C13 B16 B12 105.3(3) . . . . ?
B14 C13 B16 B15 -35.9(3) . . . . ?
B14 C13 B16 B20 4.5(4) . . . . ?
B14 C13 B16 B21 66.6(4) . . . . ?
B14 B13 B17 B12 -100.1(3) . . . . ?
B14 B13 B17 B18 37.7(3) . . . . ?
B14 B13 B17 B21 -64.0(4) . . . . ?
B14 B13 B17 B22 -0.4(4) . . . . ?
B14 B13 B18 B17 -138.3(3) . . . . ?
B14 B13 B18 B19 -37.3(3) . . . . ?
B14 B13 B18 B22 -100.2(3) . . . . ?
B14 B15 B16 C13 33.2(3) . . . . ?
B14 B15 B16 B12 -1.1(4) . . . . ?
B14 B15 B16 B20 -100.7(3) . . . . ?
B14 B15 B16 B21 -63.3(4) . . . . ?
B14 B15 B19 B18 38.0(3) . . . . ?
B14 B15 B19 B20 138.0(3) . . . . ?
B14 B15 B19 B22 100.9(4) . . . . ?
B14 B15 B20 B16 101.5(3) . . . . ?
B14 B15 B20 B19 -37.6(3) . . . . ?
B14 B15 B20 B21 63.6(4) . . . . ?
B14 B15 B20 B22 -0.4(4) . . . . ?
B14 B18 B19 B15 -37.7(3) . . . . ?
B14 B18 B19 B20 -100.4(3) . . . . ?
B14 B18 B19 B22 -137.7(3) . . . . ?
B14 B18 B22 B17 -101.2(3) . . . . ?
B14 B18 B22 B19 37.4(3) . . . . ?
B14 B18 B22 B20 -0.7(4) . . . . ?
B14 B18 B22 B21 -64.2(4) . . . . ?
B14 B19 B20 B15 37.3(3) . . . . ?
B14 B19 B20 B16 0.5(4) . . . . ?
B14 B19 B20 B21 -63.9(4) . . . . ?
B14 B19 B20 B22 -100.9(3) . . . . ?
B14 B19 B22 B17 -0.8(4) . . . . ?
B14 B19 B22 B18 -37.9(3) . . . . ?
B14 B19 B22 B20 100.0(3) . . . . ?
B14 B19 B22 B21 63.2(4) . . . . ?
B15 C13 B12 B13 105.2(3) . . . . ?
B15 C13 B12 B16 -37.0(3) . . . . ?
B15 C13 B12 B17 66.2(4) . . . . ?
B15 C13 B12 B21 2.9(4) . . . . ?
B15 C13 B13 B12 -104.7(3) . . . . ?
B15 C13 B13 B14 37.3(3) . . . . ?
B15 C13 B13 B17 -65.2(4) . . . . ?
B15 C13 B13 B18 -2.6(4) . . . . ?
B15 C13 B14 B13 -141.1(3) . . . . ?
B15 C13 B14 B18 -102.1(3) . . . . ?
B15 C13 B14 B19 -39.8(3) . . . . ?
B15 C13 B16 B12 141.1(3) . . . . ?
B15 C13 B16 B20 40.3(3) . . . . ?
B15 C13 B16 B21 102.5(3) . . . . ?
B15 B14 B18 B13 -100.1(3) . . . . ?
B15 B14 B18 B17 -63.0(4) . . . . ?
B15 B14 B18 B19 37.8(3) . . . . ?
B15 B14 B18 B22 0.4(4) . . . . ?
B15 B14 B19 B18 -137.7(3) . . . . ?
B15 B14 B19 B20 -37.1(3) . . . . ?
B15 B14 B19 B22 -100.1(4) . . . . ?
B15 B16 B20 B19 36.9(3) . . . . ?
B15 B16 B20 B21 138.1(3) . . . . ?
B15 B16 B20 B22 100.2(4) . . . . ?
B15 B16 B21 B12 100.1(3) . . . . ?
B15 B16 B21 B17 62.4(4) . . . . ?
B15 B16 B21 B20 -37.5(3) . . . . ?
B15 B16 B21 B22 -0.3(4) . . . . ?
B15 B19 B20 B16 -36.7(3) . . . . ?
B15 B19 B20 B21 -101.2(3) . . . . ?
B15 B19 B20 B22 -138.2(3) . . . . ?
B15 B19 B22 B17 -63.9(4) . . . . ?
B15 B19 B22 B18 -101.0(4) . . . . ?
B15 B19 B22 B20 36.9(3) . . . . ?
B15 B19 B22 B21 0.1(5) . . . . ?
B15 B20 B21 B12 -0.3(4) . . . . ?
B15 B20 B21 B16 37.5(3) . . . . ?
B15 B20 B21 B17 -63.8(4) . . . . ?
B15 B20 B21 B22 -100.6(4) . . . . ?
B15 B20 B22 B17 64.1(4) . . . . ?
B15 B20 B22 B18 0.7(4) . . . . ?
B15 B20 B22 B19 -37.5(3) . . . . ?
B15 B20 B22 B21 101.5(3) . . . . ?
B16 C13 B12 B13 142.2(3) . . . . ?
B16 C13 B12 B17 103.2(3) . . . . ?
B16 C13 B12 B21 39.9(3) . . . . ?
B16 C13 B13 B12 -36.4(3) . . . . ?
B16 C13 B13 B14 105.6(3) . . . . ?
B16 C13 B13 B17 3.1(4) . . . . ?
B16 C13 B13 B18 65.7(4) . . . . ?
B16 C13 B14 B13 -105.4(3) . . . . ?
B16 C13 B14 B15 35.7(3) . . . . ?
B16 C13 B14 B18 -66.4(4) . . . . ?
B16 C13 B14 B19 -4.1(4) . . . . ?
B16 C13 B15 B14 -142.8(3) . . . . ?
B16 C13 B15 B19 -103.0(3) . . . . ?
B16 C13 B15 B20 -40.2(3) . . . . ?
B16 B12 B13 C13 33.6(3) . . . . ?
B16 B12 B13 B14 0.2(4) . . . . ?
B16 B12 B13 B17 -101.7(3) . . . . ?
B16 B12 B13 B18 -64.0(3) . . . . ?
B16 B12 B17 B13 100.8(3) . . . . ?
B16 B12 B17 B18 63.0(4) . . . . ?
B16 B12 B17 B21 -38.2(3) . . . . ?
B16 B12 B17 B22 -0.2(4) . . . . ?
B16 B12 B21 B17 138.0(3) . . . . ?
B16 B12 B21 B20 37.4(3) . . . . ?
B16 B12 B21 B22 100.3(3) . . . . ?
B16 B15 B19 B14 -101.2(3) . . . . ?
B16 B15 B19 B18 -63.2(4) . . . . ?
B16 B15 B19 B20 36.8(3) . . . . ?
B16 B15 B19 B22 -0.3(5) . . . . ?
B16 B15 B20 B19 -139.1(3) . . . . ?
B16 B15 B20 B21 -37.9(3) . . . . ?
B16 B15 B20 B22 -101.9(4) . . . . ?
B16 B20 B21 B12 -37.8(3) . . . . ?
B16 B20 B21 B17 -101.3(3) . . . . ?
B16 B20 B21 B22 -138.1(3) . . . . ?
B16 B20 B22 B17 0.6(4) . . . . ?
B16 B20 B22 B18 -62.8(4) . . . . ?
B16 B20 B22 B19 -101.0(4) . . . . ?
B16 B20 B22 B21 38.0(3) . . . . ?
B16 B21 B22 B17 101.4(3) . . . . ?
B16 B21 B22 B18 64.6(4) . . . . ?
B16 B21 B22 B19 0.1(5) . . . . ?
B16 B21 B22 B20 -37.0(3) . . . . ?
B17 B12 B13 C13 135.3(3) . . . . ?
B17 B12 B13 B14 101.9(3) . . . . ?
B17 B12 B13 B18 37.7(3) . . . . ?
B17 B12 B16 C13 -97.0(3) . . . . ?
B17 B12 B16 B15 -62.6(4) . . . . ?
B17 B12 B16 B20 0.6(4) . . . . ?
B17 B12 B16 B21 38.1(3) . . . . ?
B17 B12 B21 B16 -138.0(3) . . . . ?
B17 B12 B21 B20 -100.6(3) . . . . ?
B17 B12 B21 B22 -37.7(3) . . . . ?
B17 B13 B14 C13 97.4(3) . . . . ?
B17 B13 B14 B15 63.2(4) . . . . ?
B17 B13 B14 B18 -37.5(3) . . . . ?
B17 B13 B14 B19 -0.1(4) . . . . ?
B17 B13 B18 B14 138.3(3) . . . . ?
B17 B13 B18 B19 101.0(4) . . . . ?
B17 B13 B18 B22 38.1(3) . . . . ?
B17 B18 B19 B14 100.6(3) . . . . ?
B17 B18 B19 B15 62.9(4) . . . . ?
B17 B18 B19 B20 0.2(4) . . . . ?
B17 B18 B19 B22 -37.1(3) . . . . ?
B17 B18 B22 B19 138.6(3) . . . . ?
B17 B18 B22 B20 100.5(3) . . . . ?
B17 B18 B22 B21 37.0(3) . . . . ?
B17 B21 B22 B18 -36.8(3) . . . . ?
B17 B21 B22 B19 -101.3(4) . . . . ?
B17 B21 B22 B20 -138.4(3) . . . . ?
B18 B13 B14 C13 134.9(3) . . . . ?
B18 B13 B14 B15 100.7(3) . . . . ?
B18 B13 B14 B19 37.3(3) . . . . ?
B18 B13 B17 B12 -137.9(3) . . . . ?
B18 B13 B17 B21 -101.7(4) . . . . ?
B18 B13 B17 B22 -38.1(3) . . . . ?
B18 B14 B15 C13 96.8(3) . . . . ?
B18 B14 B15 B16 63.6(4) . . . . ?
B18 B14 B15 B19 -37.8(3) . . . . ?
B18 B14 B15 B20 0.0(4) . . . . ?
B18 B14 B19 B15 137.7(3) . . . . ?
B18 B14 B19 B20 100.6(3) . . . . ?
B18 B14 B19 B22 37.5(3) . . . . ?
B18 B17 B21 B12 -100.4(3) . . . . ?
B18 B17 B21 B16 -62.7(4) . . . . ?
B18 B17 B21 B20 0.0(4) . . . . ?
B18 B17 B21 B22 36.9(3) . . . . ?
B18 B17 B22 B19 -37.5(3) . . . . ?
B18 B17 B22 B20 -101.7(3) . . . . ?
B18 B17 B22 B21 -138.9(3) . . . . ?
B18 B19 B20 B15 100.9(3) . . . . ?
B18 B19 B20 B16 64.2(4) . . . . ?
B18 B19 B20 B21 -0.3(4) . . . . ?
B18 B19 B20 B22 -37.3(3) . . . . ?
B18 B19 B22 B17 37.1(3) . . . . ?
B18 B19 B22 B20 137.9(3) . . . . ?
B18 B19 B22 B21 101.1(4) . . . . ?
B19 B14 B15 C13 134.5(3) . . . . ?
B19 B14 B15 B16 101.3(3) . . . . ?
B19 B14 B15 B20 37.7(3) . . . . ?
B19 B14 B18 B13 -138.0(3) . . . . ?
B19 B14 B18 B17 -100.9(4) . . . . ?
B19 B14 B18 B22 -37.4(3) . . . . ?
B19 B15 B16 C13 96.9(3) . . . . ?
B19 B15 B16 B12 62.7(4) . . . . ?
B19 B15 B16 B20 -37.0(3) . . . . ?
B19 B15 B16 B21 0.4(4) . . . . ?
B19 B15 B20 B16 139.1(3) . . . . ?
B19 B15 B20 B21 101.2(4) . . . . ?
B19 B15 B20 B22 37.2(3) . . . . ?
B19 B18 B22 B17 -138.6(3) . . . . ?
B19 B18 B22 B20 -38.1(3) . . . . ?
B19 B18 B22 B21 -101.6(3) . . . . ?
B19 B20 B21 B12 63.7(4) . . . . ?
B19 B20 B21 B16 101.4(3) . . . . ?
B19 B20 B21 B17 0.2(4) . . . . ?
B19 B20 B21 B22 -36.7(3) . . . . ?
B19 B20 B22 B17 101.6(3) . . . . ?
B19 B20 B22 B18 38.2(3) . . . . ?
B19 B20 B22 B21 139.0(3) . . . . ?
B20 B15 B16 C13 133.9(3) . . . . ?
B20 B15 B16 B12 99.6(3) . . . . ?
B20 B15 B16 B21 37.4(3) . . . . ?
B20 B15 B19 B14 -138.0(3) . . . . ?
B20 B15 B19 B18 -100.0(4) . . . . ?
B20 B15 B19 B22 -37.1(3) . . . . ?
B20 B16 B21 B12 137.6(3) . . . . ?
B20 B16 B21 B17 99.9(4) . . . . ?
B20 B16 B21 B22 37.1(3) . . . . ?
B20 B19 B22 B17 -100.8(3) . . . . ?
B20 B19 B22 B18 -137.9(3) . . . . ?
B20 B19 B22 B21 -36.8(3) . . . . ?
B20 B21 B22 B17 138.4(3) . . . . ?
B20 B21 B22 B18 101.6(3) . . . . ?
B20 B21 B22 B19 37.1(3) . . . . ?
B21 B12 B13 C13 98.2(3) . . . . ?
B21 B12 B13 B14 64.8(4) . . . . ?
B21 B12 B13 B17 -37.1(3) . . . . ?
B21 B12 B13 B18 0.6(4) . . . . ?
B21 B12 B16 C13 -135.2(3) . . . . ?
B21 B12 B16 B15 -100.8(3) . . . . ?
B21 B12 B16 B20 -37.5(3) . . . . ?
B21 B12 B17 B13 139.0(3) . . . . ?
B21 B12 B17 B18 101.2(4) . . . . ?
B21 B12 B17 B22 38.0(3) . . . . ?
B21 B16 B20 B15 -138.1(3) . . . . ?
B21 B16 B20 B19 -101.2(3) . . . . ?
B21 B16 B20 B22 -37.9(3) . . . . ?
B21 B17 B18 B13 100.2(3) . . . . ?
B21 B17 B18 B14 62.9(4) . . . . ?
B21 B17 B18 B19 -0.1(4) . . . . ?
B21 B17 B18 B22 -37.0(3) . . . . ?
B21 B17 B22 B18 138.9(3) . . . . ?
B21 B17 B22 B19 101.4(3) . . . . ?
B21 B17 B22 B20 37.2(3) . . . . ?
B21 B20 B22 B17 -37.4(3) . . . . ?
B21 B20 B22 B18 -100.8(3) . . . . ?
B21 B20 B22 B19 -139.0(3) . . . . ?
B22 B17 B18 B13 137.2(3) . . . . ?
B22 B17 B18 B14 99.9(4) . . . . ?
B22 B17 B18 B19 36.9(3) . . . . ?
B22 B17 B21 B12 -137.3(3) . . . . ?
B22 B17 B21 B16 -99.7(3) . . . . ?
B22 B17 B21 B20 -37.0(3) . . . . ?
B22 B18 B19 B14 137.7(3) . . . . ?
B22 B18 B19 B15 100.0(4) . . . . ?
B22 B18 B19 B20 37.4(3) . . . . ?
B22 B19 B20 B15 138.2(3) . . . . ?
B22 B19 B20 B16 101.5(4) . . . . ?
B22 B19 B20 B21 37.0(3) . . . . ?
B22 B20 B21 B12 100.3(3) . . . . ?
B22 B20 B21 B16 138.1(3) . . . . ?
B22 B20 B21 B17 36.8(3) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
