# Supplementary Information (SI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2026

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_DyCA
_database_code_depnum_ccdc_archive 'CCDC 2502518'
loop_
_audit_author_name
_audit_author_address
'Yue Yang'
;Nankai University
China
;
_audit_update_record             
;
2025-11-13 deposited with the CCDC.	2026-03-27 downloaded from the CCDC.
;
_audit_creation_date             2025-11-12
_audit_creation_method           
;
Olex2 1.3
(compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C41 H72 Dy O10 P2, C18 H33 O P, Cl, 3(H2 O)'
_chemical_formula_sum            'C59 H111 Cl Dy O14 P3'
_chemical_formula_weight         1335.33
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -9.8046 9.8477 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   15.2125(4)
_cell_length_b                   15.5239(4)
_cell_length_c                   16.9589(5)
_cell_angle_alpha                107.052(2)
_cell_angle_beta                 94.261(2)
_cell_angle_gamma                117.435(3)
_cell_volume                     3293.17(18)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    25209
_cell_measurement_temperature    100.00(10)
_cell_measurement_theta_max      74.4380
_cell_measurement_theta_min      2.8100
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    7.604
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.65377
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
CrysAlisPro 1.171.41.122a (Rigaku Oxford Diffraction, 2021)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            'clear light yellow'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   light
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    1.347
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             1410
_exptl_crystal_size_max          0.14
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.11
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0456
_diffrn_reflns_av_unetI/netI     0.0464
_diffrn_reflns_Laue_measured_fraction_full 0.992
_diffrn_reflns_Laue_measured_fraction_max 0.944
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            40438
_diffrn_reflns_point_group_measured_fraction_full 0.992
_diffrn_reflns_point_group_measured_fraction_max 0.944
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         74.696
_diffrn_reflns_theta_min         2.812
_diffrn_ambient_environment      N~2~
_diffrn_ambient_temperature      100.00(10)
_diffrn_detector                 'Hybrid Pixel Array Detector'
_diffrn_detector_area_resol_mean 10.0000
_diffrn_detector_type            'HyPix-Arc 150'
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.944
_diffrn_measurement_details      
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
#--------------------------------------------------------------------------
  1  ω     64.00 106.00   0.50    0.05    --   55.73  30.00 -90.00   84
  2  ω     64.00  90.00   0.50    0.05    --   55.73  45.00 -30.00   52
  3  ω     96.00 121.00   0.50    0.05    --   87.28  30.00   0.00   50
  4  ω     85.00 111.00   0.50    0.05    --   55.73  30.00  30.00   52
  5  ω     66.00 100.00   0.50    0.05    --   55.73  45.00 150.00   68
  6  ω     42.00  93.00   0.50    0.05    --   87.28 -95.00 -30.00  102
  7  ω     50.00  93.00   0.50    0.05    --   87.28 -95.00  30.00   86
  8  ω     38.00  93.00   0.50    0.05    --   83.67 -98.00 103.76  110
  9  ω     59.00  93.00   0.50    0.05    --   87.28 -95.00   0.00   68
 10  ω     39.00  96.00   0.50    0.05    --   87.28-112.00 -60.00  114
 11  ω     57.00  93.00   0.50    0.05    --   87.28 -95.00 -60.00   72
 12  ω     43.00  68.00   0.50    0.05    --   87.28 -95.00-150.00   50
 13  ω     20.00  61.00   0.50    0.05    --   66.80 -95.00 -60.00   82
 14  ω     44.00  69.00   0.50    0.05    --   87.28 -95.00 150.00   50
 15  ω     95.00 134.00   0.50    0.05    --   87.28 112.00  30.00   78
 16  ω     95.00 140.00   0.50    0.05    --   87.28 112.00 -30.00   90
 17  ω    107.00 140.00   0.50    0.05    --   87.28 112.00 -60.00   66
 18  ω     95.00 120.00   0.50    0.05    --   87.28 112.00-120.00   50
 19  ω     97.00 139.00   0.50    0.05    --   87.28 112.00-180.00   84
 20  ω     96.00 121.00   0.50    0.05    --   87.28 112.00 -90.00   50
 21  ω    100.00 131.00   0.50    0.05    --   87.28 112.00 120.00   62
 22  ω    -32.00  -3.00   0.50    0.05    --  -56.42  45.00 120.00   58
 23  ω    -32.00  -7.00   0.50    0.05    --  -56.42  45.00 150.00   50
 24  ω    -32.00  -4.00   0.50    0.05    --  -56.42  45.00  90.00   56
 25  ω    -29.00  -3.00   0.50    0.05    --  -56.42  45.00  30.00   52
 26  ω    -70.00 -26.00   0.50    0.05    --  -77.48 112.00 -30.00   88
 27  ω    -96.00 -28.00   0.50    0.05    --  -77.48 112.00-150.00  136
 28  ω    -97.00 -71.00   0.50    0.05    --  -82.00 112.00 -90.00   52
 29  ω    -97.00 -54.00   0.50    0.05    --  -82.00 112.00-180.00   86
 30  ω    -69.00 -25.00   0.50    0.05    --  -77.48 112.00  30.00   88
 31  ω    -94.00 -46.00   0.50    0.05    --  -82.00 103.00 -31.79   96
 32  ω    -96.00 -28.00   0.50    0.05    --  -77.48 112.00  90.00  136
 33  ω    -97.00 -69.00   0.50    0.05    --  -82.00 112.00  60.00   56
 34  ω    -97.00 -72.00   0.50    0.05    --  -82.00 112.00 120.00   50
 35  ω    -94.00 -34.00   0.50    0.05    --  -82.00 101.00 159.85  120
 36  ω   -134.00-102.00   0.50    0.05    --  -82.00 -30.00  90.00   64
 37  ω   -135.00 -92.00   0.50    0.05    --  -82.00 -45.00 150.00   86
 38  ω   -124.00 -90.00   0.50    0.05    --  -82.00 -45.00  30.00   68
 39  ω   -129.00 -87.00   0.50    0.05    --  -77.48 -45.00 -60.00   84
 40  ω   -110.00 -65.00   0.50    0.05    --  -56.42 -45.00 -60.00   90
 41  ω   -130.00 -81.00   0.50    0.05    --  -77.48 -30.00-120.00   98
 42  ω   -133.00 -81.00   0.50    0.05    --  -77.48 -30.00-180.00  104
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'ROD, Synergy Custom system, HyPix-Arc 150'
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_type       
'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11      -0.0559735000
_diffrn_orient_matrix_UB_12      0.0002519000
_diffrn_orient_matrix_UB_13      0.0720583000
_diffrn_orient_matrix_UB_21      -0.0658324000
_diffrn_orient_matrix_UB_22      -0.1200221000
_diffrn_orient_matrix_UB_23      -0.0401752000
_diffrn_orient_matrix_UB_31      0.0799797000
_diffrn_orient_matrix_UB_32      -0.0089393000
_diffrn_orient_matrix_UB_33      0.0529869000
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.54184
_diffrn_source                   'Rotating-anode X-ray tube'
_diffrn_source_type              'Rigaku (Cu) X-ray Source'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                11354
_reflns_number_total             12738
_reflns_odcompleteness_completeness 99.32
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     66.97
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'CrysAlisPro 1.171.41.122a (Rigaku OD, 2021)'
_computing_data_collection       'CrysAlisPro 1.171.41.122a (Rigaku OD, 2021)'
_computing_data_reduction        'CrysAlisPro 1.171.41.122a (Rigaku OD, 2021)'
_computing_molecular_graphics    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         1.863
_refine_diff_density_min         -1.831
_refine_diff_density_rms         0.089
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.029
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     738
_refine_ls_number_reflns         12738
_refine_ls_number_restraints     2
_refine_ls_R_factor_all          0.0522
_refine_ls_R_factor_gt           0.0458
_refine_ls_restrained_S_all      1.029
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0662P)²+4.6017P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1187
_refine_ls_wR_factor_ref         0.1227
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All O(H,H) groups
2. Restrained distances
 Dy1-H2a \\sim Dy1-H2b
 with sigma of 0.02
3. Others
 1*[Sof(O14A)+Sof(H14e)+Sof(H14f)]+1*[Sof(O14B)+Sof(H14c)+Sof(H14d)]+1*
 [Sof(O13)+Sof(H13c)+Sof(H13d)]=1 with esd of 0.0001
 Sof(O14A)=Sof(H14e)=Sof(H14f)=FVAR(1)
 Sof(O14B)=Sof(H14c)=Sof(H14d)=FVAR(2)
 Sof(O13)=Sof(H13c)=Sof(H13d)=FVAR(3)
4.a Riding coordinates:
 O12(H12c,H12d), O14B(H14c,H14d)
4.b Free rotating group:
 O2(H2a,H2b), O11(H11c,H11d), O14A(H14e,H14f), O13(H13c,H13d)
4.c Rotating group:
 O3(H3a,H3b), O1(H1a,H1b)
4.d Ternary CH refined with riding coordinates:
 C42(H42), C17(H17), C48(H48), C36(H36), C54(H54), C6(H6), C18(H18), C24(H24),
 C30(H30)
4.e Secondary CH2 refined with riding coordinates:
 C43(H43a,H43b), C55(H55a,H55b), C7(H7a,H7b), C59(H59a,H59b), C47(H47a,H47b),
 C56(H56a,H56b), C19(H19a,H19b), C25(H25a,H25b), C57(H57a,H57b), C41(H41a,H41b),
  C49(H49a,H49b), C12(H12a,H12b), C29(H29a,H29b), C23(H23a,H23b), C44(H44a,
 H44b), C16(H16a,H16b), C15(H15a,H15b), C11(H11a,H11b), C46(H46a,H46b),
 C58(H58a,H58b), C8(H8a,H8b), C39(H39a,H39b), C27(H27a,H27b), C40(H40a,H40b),
 C31(H31a,H31b), C22(H22a,H22b), C28(H28a,H28b), C10(H10a,H10b), C9(H9a,H9b),
 C14(H14a,H14b), C13(H13a,H13b), C26(H26a,H26b), C20(H20a,H20b), C53(H53a,H53b),
  C52(H52a,H52b), C21(H21a,H21b), C32(H32a,H32b), C45(H45a,H45b), C50(H50a,
 H50b), C37(H37a,H37b), C34(H34a,H34b), C51(H51a,H51b), C38(H38a,H38b),
 C35(H35a,H35b), C33(H33a,H33b)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.53867(2) 0.52927(2) 0.25879(2) 0.02216(8) Uani 1 1 d D . . . .
P1 P 0.66571(7) 0.81976(6) 0.36311(5) 0.02210(19) Uani 1 1 d . . . . .
P2 P 0.41382(7) 0.24003(6) 0.15866(5) 0.02150(18) Uani 1 1 d . . . . .
P3 P 0.92076(7) 0.56333(7) 0.24716(6) 0.0259(2) Uani 1 1 d . . . . .
Cl1 Cl 0.58494(9) 0.68149(8) 0.55869(6) 0.0434(3) Uani 1 1 d . . . . .
O3 O 0.6557(2) 0.54733(19) 0.17350(16) 0.0294(6) Uani 1 1 d . . . . .
H3A H 0.714713 0.559756 0.199013 0.044 Uiso 1 1 d R U . . .
H3B H 0.672444 0.581058 0.138734 0.044 Uiso 1 1 d R U . . .
O2 O 0.6736(2) 0.5266(2) 0.33228(16) 0.0282(6) Uani 1 1 d G . . . .
H2A H 0.728096 0.531959 0.315316 0.042 Uiso 1 1 d DG U . . .
H2B H 0.691506 0.545691 0.388766 0.042 Uiso 1 1 d DG U . . .
O9 O 0.6204(2) 0.70248(18) 0.32689(16) 0.0254(5) Uani 1 1 d . . . . .
O5 O 0.3785(2) 0.5205(2) 0.26673(16) 0.0307(6) Uani 1 1 d . . . . .
O10 O 0.46016(19) 0.35700(18) 0.19383(15) 0.0240(5) Uani 1 1 d . . . . .
O4 O 0.4611(2) 0.5279(2) 0.12956(17) 0.0309(6) Uani 1 1 d . . . . .
O15 O 0.8143(2) 0.5465(2) 0.24572(18) 0.0335(6) Uani 1 1 d . . . . .
O1 O 0.4979(2) 0.5066(2) 0.38482(18) 0.0355(6) Uani 1 1 d . . . . .
H1A H 0.543404 0.561224 0.428741 0.053 Uiso 1 1 d R U . . .
H1B H 0.503970 0.455034 0.389600 0.053 Uiso 1 1 d R U . . .
O8 O 0.3031(3) 0.4868(3) -0.01615(19) 0.0516(9) Uani 1 1 d . . . . .
O6 O 0.1644(2) 0.4808(3) 0.2250(2) 0.0421(7) Uani 1 1 d . . . . .
O7 O 0.1220(3) 0.4643(3) 0.0471(2) 0.0504(8) Uani 1 1 d . . . . .
O12 O 0.7325(3) 0.5888(3) 0.50336(19) 0.0482(8) Uani 1 1 d . . . . .
H12C H 0.702633 0.620557 0.526106 0.072 Uiso 1 1 d R U . . .
H12D H 0.718963 0.539327 0.522956 0.072 Uiso 1 1 d R U . . .
C42 C 0.4567(3) 0.2032(3) 0.2396(2) 0.0252(7) Uani 1 1 d . . . . .
H42 H 0.448051 0.243306 0.293537 0.030 Uiso 1 1 calc R U . . .
C43 C 0.5712(3) 0.2407(3) 0.2567(2) 0.0291(8) Uani 1 1 d . . . . .
H43A H 0.584999 0.200004 0.207379 0.035 Uiso 1 1 calc R U . . .
H43B H 0.610176 0.315200 0.263606 0.035 Uiso 1 1 calc R U . . .
C17 C 0.7350(3) 0.8713(3) 0.4730(2) 0.0245(7) Uani 1 1 d . . . . .
H17 H 0.684195 0.835786 0.503384 0.029 Uiso 1 1 calc R U . . .
C48 C 0.2758(3) 0.1776(3) 0.1375(2) 0.0274(8) Uani 1 1 d . . . . .
H48 H 0.246766 0.100277 0.116882 0.033 Uiso 1 1 calc R U . . .
C36 C 0.9182(3) 0.4396(3) 0.2128(2) 0.0274(8) Uani 1 1 d . . . . .
H36 H 0.989769 0.453681 0.226297 0.033 Uiso 1 1 calc R U . . .
C54 C 0.4481(3) 0.2028(3) 0.0587(2) 0.0251(8) Uani 1 1 d . . . . .
H54 H 0.408529 0.214283 0.017103 0.030 Uiso 1 1 calc R U . . .
C6 C 0.5643(3) 0.8501(3) 0.3586(2) 0.0286(8) Uani 1 1 d . . . . .
H6 H 0.595824 0.926314 0.369463 0.034 Uiso 1 1 calc R U . . .
C55 C 0.5620(3) 0.2739(3) 0.0635(2) 0.0282(8) Uani 1 1 d . . . . .
H55A H 0.579844 0.347892 0.085709 0.034 Uiso 1 1 calc R U . . .
H55B H 0.605267 0.264721 0.103074 0.034 Uiso 1 1 calc R U . . .
O11 O 0.5746(3) 0.6419(3) 0.0289(3) 0.0625(10) Uani 1 1 d G . . . .
H11C H 0.553151 0.618786 0.068638 0.094 Uiso 1 1 d G U . . .
H11D H 0.550386 0.585842 -0.016663 0.094 Uiso 1 1 d G U . . .
C7 C 0.4923(3) 0.7886(3) 0.2689(3) 0.0315(9) Uani 1 1 d . . . . .
H7A H 0.531248 0.809724 0.227142 0.038 Uiso 1 1 calc R U . . .
H7B H 0.466145 0.713092 0.254747 0.038 Uiso 1 1 calc R U . . .
C18 C 0.7554(3) 0.8815(3) 0.3037(2) 0.0274(8) Uani 1 1 d . . . . .
H18 H 0.823613 0.897859 0.333365 0.033 Uiso 1 1 calc R U . . .
C59 C 0.4160(3) 0.0864(3) 0.0199(2) 0.0289(8) Uani 1 1 d . . . . .
H59A H 0.452859 0.070200 0.058594 0.035 Uiso 1 1 calc R U . . .
H59B H 0.341818 0.042592 0.013603 0.035 Uiso 1 1 calc R U . . .
C47 C 0.3939(3) 0.0879(3) 0.2305(3) 0.0312(8) Uani 1 1 d . . . . .
H47A H 0.320387 0.065527 0.221619 0.037 Uiso 1 1 calc R U . . .
H47B H 0.402975 0.043016 0.180637 0.037 Uiso 1 1 calc R U . . .
C56 C 0.5831(3) 0.2466(3) -0.0248(2) 0.0289(8) Uani 1 1 d . . . . .
H56A H 0.543920 0.261123 -0.063154 0.035 Uiso 1 1 calc R U . . .
H56B H 0.656676 0.290992 -0.020386 0.035 Uiso 1 1 calc R U . . .
C19 C 0.7694(3) 0.9859(3) 0.3036(3) 0.0323(9) Uani 1 1 d . . . . .
H19A H 0.704519 0.974306 0.273001 0.039 Uiso 1 1 calc R U . . .
H19B H 0.786890 1.034392 0.362881 0.039 Uiso 1 1 calc R U . . .
C1 C 0.3692(3) 0.5117(3) 0.1261(2) 0.0294(8) Uani 1 1 d . . . . .
C25 C 0.9638(3) 0.7263(3) 0.1913(3) 0.0327(9) Uani 1 1 d . . . . .
H25A H 0.890171 0.703576 0.180251 0.039 Uiso 1 1 calc R U . . .
H25B H 0.996321 0.774690 0.251359 0.039 Uiso 1 1 calc R U . . .
C57 C 0.5527(3) 0.1317(3) -0.0621(2) 0.0327(9) Uani 1 1 d . . . . .
H57A H 0.595788 0.118556 -0.026186 0.039 Uiso 1 1 calc R U . . .
H57B H 0.564531 0.115112 -0.119869 0.039 Uiso 1 1 calc R U . . .
C5 C 0.2951(3) 0.4926(3) 0.0543(3) 0.0358(9) Uani 1 1 d . . . . .
C41 C 0.8556(4) 0.3731(3) 0.2613(3) 0.0353(9) Uani 1 1 d . . . . .
H41A H 0.887403 0.410879 0.323137 0.042 Uiso 1 1 calc R U . . .
H41B H 0.785627 0.362071 0.250888 0.042 Uiso 1 1 calc R U . . .
C49 C 0.2322(3) 0.2027(4) 0.0681(3) 0.0364(9) Uani 1 1 d . . . . .
H49A H 0.263906 0.279383 0.085645 0.044 Uiso 1 1 calc R U . . .
H49B H 0.249777 0.176547 0.014528 0.044 Uiso 1 1 calc R U . . .
C12 C 0.7781(3) 0.9894(3) 0.5187(2) 0.0328(9) Uani 1 1 d . . . . .
H12A H 0.830943 1.028874 0.492435 0.039 Uiso 1 1 calc R U . . .
H12B H 0.722655 1.005564 0.512824 0.039 Uiso 1 1 calc R U . . .
C3 C 0.2231(3) 0.4887(3) 0.1777(3) 0.0323(9) Uani 1 1 d . . . . .
C29 C 1.0872(3) 0.6574(3) 0.1813(3) 0.0342(9) Uani 1 1 d . . . . .
H29A H 1.090413 0.592464 0.165908 0.041 Uiso 1 1 calc R U . . .
H29B H 1.128909 0.702855 0.240281 0.041 Uiso 1 1 calc R U . . .
C23 C 0.7325(4) 0.8067(3) 0.2135(3) 0.0358(9) Uani 1 1 d . . . . .
H23A H 0.666506 0.789410 0.180031 0.043 Uiso 1 1 calc R U . . .
H23B H 0.726819 0.741100 0.215019 0.043 Uiso 1 1 calc R U . . .
C44 C 0.6066(3) 0.2277(3) 0.3369(3) 0.0346(9) Uani 1 1 d . . . . .
H44A H 0.598214 0.272937 0.387009 0.042 Uiso 1 1 calc R U . . .
H44B H 0.679926 0.249376 0.345589 0.042 Uiso 1 1 calc R U . . .
C16 C 0.8182(3) 0.8438(3) 0.4835(3) 0.0341(9) Uani 1 1 d . . . . .
H16A H 0.871481 0.878310 0.455273 0.041 Uiso 1 1 calc R U . . .
H16B H 0.788414 0.767353 0.455853 0.041 Uiso 1 1 calc R U . . .
C2 C 0.3278(3) 0.5081(3) 0.1975(2) 0.0282(8) Uani 1 1 d . . . . .
C24 C 0.9766(3) 0.6307(3) 0.1767(2) 0.0284(8) Uani 1 1 d . . . . .
H24 H 0.936642 0.580941 0.117360 0.034 Uiso 1 1 calc R U . . .
C15 C 0.8664(4) 0.8794(4) 0.5780(3) 0.0400(10) Uani 1 1 d . . . . .
H15A H 0.814549 0.839102 0.604610 0.048 Uiso 1 1 calc R U . . .
H15B H 0.922859 0.864652 0.583718 0.048 Uiso 1 1 calc R U . . .
C11 C 0.5054(3) 0.8276(4) 0.4261(3) 0.0389(10) Uani 1 1 d . . . . .
H11A H 0.552342 0.871432 0.483482 0.047 Uiso 1 1 calc R U . . .
H11B H 0.477220 0.753378 0.418993 0.047 Uiso 1 1 calc R U . . .
C46 C 0.4304(3) 0.0765(3) 0.3117(3) 0.0362(9) Uani 1 1 d . . . . .
H46A H 0.416960 0.118019 0.360667 0.043 Uiso 1 1 calc R U . . .
H46B H 0.391453 0.002370 0.305664 0.043 Uiso 1 1 calc R U . . .
C58 C 0.4401(3) 0.0610(3) -0.0668(2) 0.0343(9) Uani 1 1 d . . . . .
H58A H 0.396962 0.069294 -0.107222 0.041 Uiso 1 1 calc R U . . .
H58B H 0.423205 -0.012777 -0.088824 0.041 Uiso 1 1 calc R U . . .
C8 C 0.4025(3) 0.8068(3) 0.2616(3) 0.0372(10) Uani 1 1 d . . . . .
H8A H 0.427814 0.879943 0.266602 0.045 Uiso 1 1 calc R U . . .
H8B H 0.354902 0.760414 0.204757 0.045 Uiso 1 1 calc R U . . .
C39 C 0.8062(4) 0.2080(3) 0.1388(3) 0.0406(10) Uani 1 1 d . . . . .
H39A H 0.733509 0.188093 0.123882 0.049 Uiso 1 1 calc R U . . .
H39B H 0.809621 0.143160 0.122688 0.049 Uiso 1 1 calc R U . . .
C27 C 1.1229(4) 0.8109(3) 0.1402(3) 0.0396(10) Uani 1 1 d . . . . .
H27A H 1.150628 0.845351 0.099922 0.047 Uiso 1 1 calc R U . . .
H27B H 1.164033 0.860387 0.198548 0.047 Uiso 1 1 calc R U . . .
C40 C 0.8497(4) 0.2679(3) 0.2337(3) 0.0381(10) Uani 1 1 d . . . . .
H40A H 0.919024 0.278745 0.249635 0.046 Uiso 1 1 calc R U . . .
H40B H 0.806263 0.225954 0.264271 0.046 Uiso 1 1 calc R U . . .
C4 C 0.2015(3) 0.4803(3) 0.0868(3) 0.0358(9) Uani 1 1 d . . . . .
C31 C 1.0878(3) 0.6198(3) 0.3789(2) 0.0339(9) Uani 1 1 d . . . . .
H31A H 1.055003 0.548142 0.379284 0.041 Uiso 1 1 calc R U . . .
H31B H 1.128036 0.622593 0.335437 0.041 Uiso 1 1 calc R U . . .
C22 C 0.8175(3) 0.8564(3) 0.1710(3) 0.0346(9) Uani 1 1 d . . . . .
H22A H 0.881960 0.867187 0.201546 0.042 Uiso 1 1 calc R U . . .
H22B H 0.800074 0.808045 0.111661 0.042 Uiso 1 1 calc R U . . .
C30 C 1.0047(3) 0.6447(3) 0.3552(2) 0.0317(9) Uani 1 1 d . . . . .
H30 H 1.041935 0.717826 0.356616 0.038 Uiso 1 1 calc R U . . .
C28 C 1.1308(3) 0.7134(4) 0.1206(3) 0.0364(9) Uani 1 1 d . . . . .
H28A H 1.203392 0.732655 0.126269 0.044 Uiso 1 1 calc R U . . .
H28B H 1.092832 0.665669 0.061180 0.044 Uiso 1 1 calc R U . . .
C10 C 0.4181(4) 0.8505(4) 0.4183(3) 0.0461(12) Uani 1 1 d . . . . .
H10A H 0.446803 0.925796 0.429530 0.055 Uiso 1 1 calc R U . . .
H10B H 0.379657 0.833773 0.461414 0.055 Uiso 1 1 calc R U . . .
C9 C 0.3455(3) 0.7861(4) 0.3294(3) 0.0419(10) Uani 1 1 d . . . . .
H9A H 0.312344 0.710897 0.319960 0.050 Uiso 1 1 calc R U . . .
H9B H 0.291312 0.804283 0.325239 0.050 Uiso 1 1 calc R U . . .
C14 C 0.9076(3) 0.9954(3) 0.6245(3) 0.0387(10) Uani 1 1 d . . . . .
H14A H 0.933884 1.014758 0.685961 0.046 Uiso 1 1 calc R U . . .
H14B H 0.964950 1.036186 0.602499 0.046 Uiso 1 1 calc R U . . .
C13 C 0.8244(3) 1.0220(3) 0.6124(3) 0.0379(10) Uani 1 1 d . . . . .
H13A H 0.853623 1.098258 0.641169 0.046 Uiso 1 1 calc R U . . .
H13B H 0.770098 0.986226 0.639245 0.046 Uiso 1 1 calc R U . . .
C26 C 1.0123(4) 0.7831(3) 0.1328(3) 0.0402(10) Uani 1 1 d . . . . .
H26A H 0.972793 0.738209 0.073218 0.048 Uiso 1 1 calc R U . . .
H26B H 1.008821 0.847892 0.147322 0.048 Uiso 1 1 calc R U . . .
C20 C 0.8539(4) 1.0345(3) 0.2606(3) 0.0382(10) Uani 1 1 d . . . . .
H20A H 0.920041 1.053049 0.294869 0.046 Uiso 1 1 calc R U . . .
H20B H 0.859026 1.099520 0.258153 0.046 Uiso 1 1 calc R U . . .
C53 C 0.2428(3) 0.2109(3) 0.2198(3) 0.0349(9) Uani 1 1 d . . . . .
H53A H 0.267660 0.190435 0.262797 0.042 Uiso 1 1 calc R U . . .
H53B H 0.274240 0.287789 0.243136 0.042 Uiso 1 1 calc R U . . .
C52 C 0.1266(3) 0.1599(4) 0.2027(3) 0.0449(11) Uani 1 1 d . . . . .
H52A H 0.107899 0.185306 0.255816 0.054 Uiso 1 1 calc R U . . .
H52B H 0.095522 0.083229 0.184903 0.054 Uiso 1 1 calc R U . . .
C21 C 0.8338(3) 0.9599(3) 0.1705(3) 0.0365(9) Uani 1 1 d . . . . .
H21A H 0.772477 0.948373 0.133999 0.044 Uiso 1 1 calc R U . . .
H21B H 0.892671 0.991571 0.146216 0.044 Uiso 1 1 calc R U . . .
C32 C 1.1592(4) 0.6975(4) 0.4664(3) 0.0437(11) Uani 1 1 d . . . . .
H32A H 1.209390 0.677507 0.481465 0.052 Uiso 1 1 calc R U . . .
H32B H 1.197421 0.768208 0.464348 0.052 Uiso 1 1 calc R U . . .
C45 C 0.5439(4) 0.1134(4) 0.3287(3) 0.0389(10) Uani 1 1 d . . . . .
H45A H 0.556896 0.068949 0.281551 0.047 Uiso 1 1 calc R U . . .
H45B H 0.565612 0.106424 0.381923 0.047 Uiso 1 1 calc R U . . .
C50 C 0.1163(4) 0.1529(4) 0.0524(3) 0.0468(12) Uani 1 1 d . . . . .
H50A H 0.091435 0.173895 0.009870 0.056 Uiso 1 1 calc R U . . .
H50B H 0.084337 0.075931 0.028635 0.056 Uiso 1 1 calc R U . . .
C37 C 0.8717(4) 0.3795(3) 0.1166(2) 0.0373(10) Uani 1 1 d . . . . .
H37A H 0.802552 0.369338 0.101994 0.045 Uiso 1 1 calc R U . . .
H37B H 0.914526 0.420719 0.085392 0.045 Uiso 1 1 calc R U . . .
C34 C 1.0157(4) 0.7229(4) 0.5112(3) 0.0447(11) Uani 1 1 d . . . . .
H34A H 1.047701 0.794948 0.511742 0.054 Uiso 1 1 calc R U . . .
H34B H 0.975350 0.718632 0.554550 0.054 Uiso 1 1 calc R U . . .
C51 C 0.0843(4) 0.1851(4) 0.1332(3) 0.0469(12) Uani 1 1 d . . . . .
H51A H 0.008737 0.147856 0.121104 0.056 Uiso 1 1 calc R U . . .
H51B H 0.109623 0.260992 0.153504 0.056 Uiso 1 1 calc R U . . .
C38 C 0.8650(4) 0.2733(3) 0.0894(3) 0.0477(12) Uani 1 1 d . . . . .
H38A H 0.831127 0.234638 0.027947 0.057 Uiso 1 1 calc R U . . .
H38B H 0.934963 0.284137 0.097857 0.057 Uiso 1 1 calc R U . . .
C35 C 0.9440(3) 0.6462(3) 0.4232(3) 0.0379(10) Uani 1 1 d . . . . .
H35A H 0.905193 0.575231 0.424493 0.046 Uiso 1 1 calc R U . . .
H35B H 0.894380 0.667105 0.408636 0.046 Uiso 1 1 calc R U . . .
C33 C 1.0989(4) 0.6995(4) 0.5341(3) 0.0489(12) Uani 1 1 d . . . . .
H33A H 1.067377 0.631038 0.540600 0.059 Uiso 1 1 calc R U . . .
H33B H 1.146155 0.753462 0.589273 0.059 Uiso 1 1 calc R U . . .
O14B O 0.7297(6) 0.4762(8) 0.6038(5) 0.0414(16) Uani 0.487(3) 1 d . . P A 2
H14C H 0.753389 0.487164 0.656244 0.062 Uiso 0.487(3) 1 d R U P A 2
H14D H 0.675029 0.472964 0.618654 0.062 Uiso 0.487(3) 1 d R U P A 2
O14A O 0.6541(9) 0.4163(8) 0.5605(6) 0.035(2) Uani 0.316(3) 1 d G . P B 1
H14E H 0.711312 0.466195 0.596756 0.052 Uiso 0.316(3) 1 d G U P B 1
H14F H 0.611334 0.438578 0.569303 0.052 Uiso 0.316(3) 1 d G U P B 1
O13 O 0.8971(11) 0.6288(13) 0.6576(10) 0.040(4) Uani 0.197(3) 1 d G . P C 3
H13C H 0.859039 0.590037 0.605950 0.060 Uiso 0.197(3) 1 d G U P C 3
H13D H 0.871058 0.590161 0.687218 0.060 Uiso 0.197(3) 1 d G U P C 3


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy1 O3 2.345(3) . ?
Dy1 O2 2.345(3) . ?
Dy1 O9 2.235(2) . ?
Dy1 O5 2.393(3) . ?
Dy1 O10 2.219(2) . ?
Dy1 O4 2.400(3) . ?
Dy1 O1 2.348(3) . ?
P1 O9 1.514(2) . ?
P1 C17 1.810(4) . ?
P1 C6 1.812(4) . ?
P1 C18 1.832(4) . ?
P2 O10 1.508(2) . ?
P2 C42 1.819(4) . ?
P2 C48 1.813(4) . ?
P2 C54 1.821(4) . ?
P3 O15 1.514(3) . ?
P3 C36 1.817(4) . ?
P3 C24 1.819(4) . ?
P3 C30 1.841(4) . ?
O3 H3A 0.8742 . ?
O3 H3B 0.8759 . ?
O2 H2A 0.8729 . ?
O2 H2B 0.8945 . ?
O5 C2 1.267(5) . ?
O4 C1 1.294(5) . ?
O1 H1A 0.8749 . ?
O1 H1B 0.8723 . ?
O8 C5 1.191(5) . ?
O6 C3 1.232(5) . ?
O7 C4 1.218(5) . ?
O12 H12C 0.8487 . ?
O12 H12D 0.8694 . ?
C42 H42 1.0000 . ?
C42 C43 1.533(5) . ?
C42 C47 1.543(5) . ?
C43 H43A 0.9900 . ?
C43 H43B 0.9900 . ?
C43 C44 1.529(5) . ?
C17 H17 1.0000 . ?
C17 C12 1.542(5) . ?
C17 C16 1.525(5) . ?
C48 H48 1.0000 . ?
C48 C49 1.539(5) . ?
C48 C53 1.545(6) . ?
C36 H36 1.0000 . ?
C36 C41 1.535(5) . ?
C36 C37 1.536(5) . ?
C54 H54 1.0000 . ?
C54 C55 1.547(5) . ?
C54 C59 1.542(5) . ?
C6 H6 1.0000 . ?
C6 C7 1.537(5) . ?
C6 C11 1.527(6) . ?
C55 H55A 0.9900 . ?
C55 H55B 0.9900 . ?
C55 C56 1.532(5) . ?
O11 H11C 0.8697 . ?
O11 H11D 0.8709 . ?
C7 H7A 0.9900 . ?
C7 H7B 0.9900 . ?
C7 C8 1.521(6) . ?
C18 H18 1.0000 . ?
C18 C19 1.535(5) . ?
C18 C23 1.523(5) . ?
C59 H59A 0.9900 . ?
C59 H59B 0.9900 . ?
C59 C58 1.526(5) . ?
C47 H47A 0.9900 . ?
C47 H47B 0.9900 . ?
C47 C46 1.534(6) . ?
C56 H56A 0.9900 . ?
C56 H56B 0.9900 . ?
C56 C57 1.527(5) . ?
C19 H19A 0.9900 . ?
C19 H19B 0.9900 . ?
C19 C20 1.525(6) . ?
C1 C5 1.455(6) . ?
C1 C2 1.410(5) . ?
C25 H25A 0.9900 . ?
C25 H25B 0.9900 . ?
C25 C24 1.536(5) . ?
C25 C26 1.525(6) . ?
C57 H57A 0.9900 . ?
C57 H57B 0.9900 . ?
C57 C58 1.529(6) . ?
C5 C4 1.515(6) . ?
C41 H41A 0.9900 . ?
C41 H41B 0.9900 . ?
C41 C40 1.518(6) . ?
C49 H49A 0.9900 . ?
C49 H49B 0.9900 . ?
C49 C50 1.527(6) . ?
C12 H12A 0.9900 . ?
C12 H12B 0.9900 . ?
C12 C13 1.520(5) . ?
C3 C2 1.470(6) . ?
C3 C4 1.506(6) . ?
C29 H29A 0.9900 . ?
C29 H29B 0.9900 . ?
C29 C24 1.525(6) . ?
C29 C28 1.534(6) . ?
C23 H23A 0.9900 . ?
C23 H23B 0.9900 . ?
C23 C22 1.527(6) . ?
C44 H44A 0.9900 . ?
C44 H44B 0.9900 . ?
C44 C45 1.534(6) . ?
C16 H16A 0.9900 . ?
C16 H16B 0.9900 . ?
C16 C15 1.532(6) . ?
C24 H24 1.0000 . ?
C15 H15A 0.9900 . ?
C15 H15B 0.9900 . ?
C15 C14 1.521(6) . ?
C11 H11A 0.9900 . ?
C11 H11B 0.9900 . ?
C11 C10 1.531(6) . ?
C46 H46A 0.9900 . ?
C46 H46B 0.9900 . ?
C46 C45 1.520(6) . ?
C58 H58A 0.9900 . ?
C58 H58B 0.9900 . ?
C8 H8A 0.9900 . ?
C8 H8B 0.9900 . ?
C8 C9 1.512(6) . ?
C39 H39A 0.9900 . ?
C39 H39B 0.9900 . ?
C39 C40 1.514(6) . ?
C39 C38 1.518(6) . ?
C27 H27A 0.9900 . ?
C27 H27B 0.9900 . ?
C27 C28 1.514(6) . ?
C27 C26 1.517(7) . ?
C40 H40A 0.9900 . ?
C40 H40B 0.9900 . ?
C31 H31A 0.9900 . ?
C31 H31B 0.9900 . ?
C31 C30 1.541(6) . ?
C31 C32 1.530(6) . ?
C22 H22A 0.9900 . ?
C22 H22B 0.9900 . ?
C22 C21 1.511(6) . ?
C30 H30 1.0000 . ?
C30 C35 1.532(6) . ?
C28 H28A 0.9900 . ?
C28 H28B 0.9900 . ?
C10 H10A 0.9900 . ?
C10 H10B 0.9900 . ?
C10 C9 1.531(6) . ?
C9 H9A 0.9900 . ?
C9 H9B 0.9900 . ?
C14 H14A 0.9900 . ?
C14 H14B 0.9900 . ?
C14 C13 1.518(6) . ?
C13 H13A 0.9900 . ?
C13 H13B 0.9900 . ?
C26 H26A 0.9900 . ?
C26 H26B 0.9900 . ?
C20 H20A 0.9900 . ?
C20 H20B 0.9900 . ?
C20 C21 1.528(6) . ?
C53 H53A 0.9900 . ?
C53 H53B 0.9900 . ?
C53 C52 1.528(6) . ?
C52 H52A 0.9900 . ?
C52 H52B 0.9900 . ?
C52 C51 1.533(6) . ?
C21 H21A 0.9900 . ?
C21 H21B 0.9900 . ?
C32 H32A 0.9900 . ?
C32 H32B 0.9900 . ?
C32 C33 1.524(6) . ?
C45 H45A 0.9900 . ?
C45 H45B 0.9900 . ?
C50 H50A 0.9900 . ?
C50 H50B 0.9900 . ?
C50 C51 1.512(7) . ?
C37 H37A 0.9900 . ?
C37 H37B 0.9900 . ?
C37 C38 1.526(6) . ?
C34 H34A 0.9900 . ?
C34 H34B 0.9900 . ?
C34 C35 1.533(6) . ?
C34 C33 1.523(7) . ?
C51 H51A 0.9900 . ?
C51 H51B 0.9900 . ?
C38 H38A 0.9900 . ?
C38 H38B 0.9900 . ?
C35 H35A 0.9900 . ?
C35 H35B 0.9900 . ?
C33 H33A 0.9900 . ?
C33 H33B 0.9900 . ?
O14B H14C 0.8698 . ?
O14B H14D 0.8709 . ?
O14A H14E 0.8692 . ?
O14A H14F 0.8700 . ?
O13 H13C 0.8704 . ?
O13 H13D 0.8698 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O3 Dy1 O5 143.17(9) . . ?
O3 Dy1 O4 73.85(9) . . ?
O3 Dy1 O1 146.65(10) . . ?
O2 Dy1 O3 73.68(9) . . ?
O2 Dy1 O5 143.15(9) . . ?
O2 Dy1 O4 147.21(9) . . ?
O2 Dy1 O1 72.99(10) . . ?
O9 Dy1 O3 90.47(9) . . ?
O9 Dy1 O2 88.90(9) . . ?
O9 Dy1 O5 90.06(9) . . ?
O9 Dy1 O4 95.80(9) . . ?
O9 Dy1 O1 89.89(9) . . ?
O5 Dy1 O4 69.47(9) . . ?
O10 Dy1 O3 89.57(9) . . ?
O10 Dy1 O2 89.61(9) . . ?
O10 Dy1 O9 178.44(9) . . ?
O10 Dy1 O5 90.84(10) . . ?
O10 Dy1 O4 85.71(9) . . ?
O10 Dy1 O1 89.22(9) . . ?
O1 Dy1 O5 70.18(10) . . ?
O1 Dy1 O4 139.21(10) . . ?
O9 P1 C17 109.33(15) . . ?
O9 P1 C6 109.63(16) . . ?
O9 P1 C18 110.53(16) . . ?
C17 P1 C6 109.03(17) . . ?
C17 P1 C18 108.23(18) . . ?
C6 P1 C18 110.05(18) . . ?
O10 P2 C42 108.09(15) . . ?
O10 P2 C48 109.47(16) . . ?
O10 P2 C54 108.53(16) . . ?
C42 P2 C54 114.43(17) . . ?
C48 P2 C42 107.78(17) . . ?
C48 P2 C54 108.47(18) . . ?
O15 P3 C36 111.05(17) . . ?
O15 P3 C24 110.45(17) . . ?
O15 P3 C30 110.47(17) . . ?
C36 P3 C24 108.30(17) . . ?
C36 P3 C30 108.85(19) . . ?
C24 P3 C30 107.62(18) . . ?
Dy1 O3 H3A 114.1 . . ?
Dy1 O3 H3B 131.7 . . ?
H3A O3 H3B 102.6 . . ?
Dy1 O2 H2A 126.2 . . ?
Dy1 O2 H2B 124.8 . . ?
H2A O2 H2B 104.9 . . ?
P1 O9 Dy1 171.75(16) . . ?
C2 O5 Dy1 114.1(2) . . ?
P2 O10 Dy1 173.22(16) . . ?
C1 O4 Dy1 113.5(2) . . ?
Dy1 O1 H1A 109.6 . . ?
Dy1 O1 H1B 109.5 . . ?
H1A O1 H1B 104.4 . . ?
H12C O12 H12D 106.9 . . ?
P2 C42 H42 104.8 . . ?
C43 C42 P2 113.4(3) . . ?
C43 C42 H42 104.8 . . ?
C43 C42 C47 110.8(3) . . ?
C47 C42 P2 117.0(3) . . ?
C47 C42 H42 104.8 . . ?
C42 C43 H43A 109.5 . . ?
C42 C43 H43B 109.5 . . ?
H43A C43 H43B 108.1 . . ?
C44 C43 C42 110.7(3) . . ?
C44 C43 H43A 109.5 . . ?
C44 C43 H43B 109.5 . . ?
P1 C17 H17 106.2 . . ?
C12 C17 P1 114.0(3) . . ?
C12 C17 H17 106.2 . . ?
C16 C17 P1 112.7(3) . . ?
C16 C17 H17 106.2 . . ?
C16 C17 C12 110.8(3) . . ?
P2 C48 H48 108.2 . . ?
C49 C48 P2 111.5(3) . . ?
C49 C48 H48 108.2 . . ?
C49 C48 C53 110.1(3) . . ?
C53 C48 P2 110.6(3) . . ?
C53 C48 H48 108.2 . . ?
P3 C36 H36 108.8 . . ?
C41 C36 P3 109.5(3) . . ?
C41 C36 H36 108.8 . . ?
C41 C36 C37 109.6(3) . . ?
C37 C36 P3 111.3(3) . . ?
C37 C36 H36 108.8 . . ?
P2 C54 H54 105.8 . . ?
C55 C54 P2 113.0(2) . . ?
C55 C54 H54 105.8 . . ?
C59 C54 P2 114.5(3) . . ?
C59 C54 H54 105.8 . . ?
C59 C54 C55 111.1(3) . . ?
P1 C6 H6 108.1 . . ?
C7 C6 P1 109.3(3) . . ?
C7 C6 H6 108.1 . . ?
C11 C6 P1 112.0(3) . . ?
C11 C6 H6 108.1 . . ?
C11 C6 C7 111.0(3) . . ?
C54 C55 H55A 109.6 . . ?
C54 C55 H55B 109.6 . . ?
H55A C55 H55B 108.1 . . ?
C56 C55 C54 110.4(3) . . ?
C56 C55 H55A 109.6 . . ?
C56 C55 H55B 109.6 . . ?
H11C O11 H11D 104.5 . . ?
C6 C7 H7A 109.2 . . ?
C6 C7 H7B 109.2 . . ?
H7A C7 H7B 107.9 . . ?
C8 C7 C6 112.2(3) . . ?
C8 C7 H7A 109.2 . . ?
C8 C7 H7B 109.2 . . ?
P1 C18 H18 105.7 . . ?
C19 C18 P1 115.9(3) . . ?
C19 C18 H18 105.7 . . ?
C23 C18 P1 112.2(3) . . ?
C23 C18 H18 105.7 . . ?
C23 C18 C19 110.7(3) . . ?
C54 C59 H59A 109.5 . . ?
C54 C59 H59B 109.5 . . ?
H59A C59 H59B 108.1 . . ?
C58 C59 C54 110.6(3) . . ?
C58 C59 H59A 109.5 . . ?
C58 C59 H59B 109.5 . . ?
C42 C47 H47A 109.9 . . ?
C42 C47 H47B 109.9 . . ?
H47A C47 H47B 108.3 . . ?
C46 C47 C42 109.0(3) . . ?
C46 C47 H47A 109.9 . . ?
C46 C47 H47B 109.9 . . ?
C55 C56 H56A 109.5 . . ?
C55 C56 H56B 109.5 . . ?
H56A C56 H56B 108.1 . . ?
C57 C56 C55 110.7(3) . . ?
C57 C56 H56A 109.5 . . ?
C57 C56 H56B 109.5 . . ?
C18 C19 H19A 109.5 . . ?
C18 C19 H19B 109.5 . . ?
H19A C19 H19B 108.1 . . ?
C20 C19 C18 110.6(3) . . ?
C20 C19 H19A 109.5 . . ?
C20 C19 H19B 109.5 . . ?
O4 C1 C5 128.5(4) . . ?
O4 C1 C2 120.5(3) . . ?
C2 C1 C5 111.0(4) . . ?
H25A C25 H25B 108.1 . . ?
C24 C25 H25A 109.5 . . ?
C24 C25 H25B 109.5 . . ?
C26 C25 H25A 109.5 . . ?
C26 C25 H25B 109.5 . . ?
C26 C25 C24 110.9(3) . . ?
C56 C57 H57A 109.5 . . ?
C56 C57 H57B 109.5 . . ?
C56 C57 C58 110.9(3) . . ?
H57A C57 H57B 108.1 . . ?
C58 C57 H57A 109.5 . . ?
C58 C57 H57B 109.5 . . ?
O8 C5 C1 129.0(4) . . ?
O8 C5 C4 125.4(4) . . ?
C1 C5 C4 105.6(4) . . ?
C36 C41 H41A 109.3 . . ?
C36 C41 H41B 109.3 . . ?
H41A C41 H41B 108.0 . . ?
C40 C41 C36 111.5(3) . . ?
C40 C41 H41A 109.3 . . ?
C40 C41 H41B 109.3 . . ?
C48 C49 H49A 109.3 . . ?
C48 C49 H49B 109.3 . . ?
H49A C49 H49B 108.0 . . ?
C50 C49 C48 111.4(3) . . ?
C50 C49 H49A 109.3 . . ?
C50 C49 H49B 109.3 . . ?
C17 C12 H12A 109.7 . . ?
C17 C12 H12B 109.7 . . ?
H12A C12 H12B 108.2 . . ?
C13 C12 C17 109.6(3) . . ?
C13 C12 H12A 109.7 . . ?
C13 C12 H12B 109.7 . . ?
O6 C3 C2 127.6(4) . . ?
O6 C3 C4 126.6(4) . . ?
C2 C3 C4 105.7(3) . . ?
H29A C29 H29B 108.1 . . ?
C24 C29 H29A 109.5 . . ?
C24 C29 H29B 109.5 . . ?
C24 C29 C28 110.7(3) . . ?
C28 C29 H29A 109.5 . . ?
C28 C29 H29B 109.5 . . ?
C18 C23 H23A 109.6 . . ?
C18 C23 H23B 109.6 . . ?
C18 C23 C22 110.2(3) . . ?
H23A C23 H23B 108.1 . . ?
C22 C23 H23A 109.6 . . ?
C22 C23 H23B 109.6 . . ?
C43 C44 H44A 109.6 . . ?
C43 C44 H44B 109.6 . . ?
C43 C44 C45 110.2(3) . . ?
H44A C44 H44B 108.1 . . ?
C45 C44 H44A 109.6 . . ?
C45 C44 H44B 109.6 . . ?
C17 C16 H16A 109.6 . . ?
C17 C16 H16B 109.6 . . ?
C17 C16 C15 110.3(3) . . ?
H16A C16 H16B 108.1 . . ?
C15 C16 H16A 109.6 . . ?
C15 C16 H16B 109.6 . . ?
O5 C2 C1 121.6(4) . . ?
O5 C2 C3 128.2(4) . . ?
C1 C2 C3 110.1(3) . . ?
P3 C24 H24 106.6 . . ?
C25 C24 P3 111.3(3) . . ?
C25 C24 H24 106.6 . . ?
C29 C24 P3 112.5(3) . . ?
C29 C24 C25 112.6(3) . . ?
C29 C24 H24 106.6 . . ?
C16 C15 H15A 109.3 . . ?
C16 C15 H15B 109.3 . . ?
H15A C15 H15B 108.0 . . ?
C14 C15 C16 111.6(4) . . ?
C14 C15 H15A 109.3 . . ?
C14 C15 H15B 109.3 . . ?
C6 C11 H11A 109.6 . . ?
C6 C11 H11B 109.6 . . ?
C6 C11 C10 110.4(4) . . ?
H11A C11 H11B 108.1 . . ?
C10 C11 H11A 109.6 . . ?
C10 C11 H11B 109.6 . . ?
C47 C46 H46A 109.4 . . ?
C47 C46 H46B 109.4 . . ?
H46A C46 H46B 108.0 . . ?
C45 C46 C47 111.3(3) . . ?
C45 C46 H46A 109.4 . . ?
C45 C46 H46B 109.4 . . ?
C59 C58 C57 111.9(3) . . ?
C59 C58 H58A 109.2 . . ?
C59 C58 H58B 109.2 . . ?
C57 C58 H58A 109.2 . . ?
C57 C58 H58B 109.2 . . ?
H58A C58 H58B 107.9 . . ?
C7 C8 H8A 109.2 . . ?
C7 C8 H8B 109.2 . . ?
H8A C8 H8B 107.9 . . ?
C9 C8 C7 112.1(4) . . ?
C9 C8 H8A 109.2 . . ?
C9 C8 H8B 109.2 . . ?
H39A C39 H39B 108.0 . . ?
C40 C39 H39A 109.4 . . ?
C40 C39 H39B 109.4 . . ?
C40 C39 C38 111.0(4) . . ?
C38 C39 H39A 109.4 . . ?
C38 C39 H39B 109.4 . . ?
H27A C27 H27B 108.1 . . ?
C28 C27 H27A 109.6 . . ?
C28 C27 H27B 109.6 . . ?
C28 C27 C26 110.3(4) . . ?
C26 C27 H27A 109.6 . . ?
C26 C27 H27B 109.6 . . ?
C41 C40 H40A 109.2 . . ?
C41 C40 H40B 109.2 . . ?
C39 C40 C41 112.0(4) . . ?
C39 C40 H40A 109.2 . . ?
C39 C40 H40B 109.2 . . ?
H40A C40 H40B 107.9 . . ?
O7 C4 C5 127.0(4) . . ?
O7 C4 C3 125.5(4) . . ?
C3 C4 C5 107.5(3) . . ?
H31A C31 H31B 108.0 . . ?
C30 C31 H31A 109.4 . . ?
C30 C31 H31B 109.4 . . ?
C32 C31 H31A 109.4 . . ?
C32 C31 H31B 109.4 . . ?
C32 C31 C30 111.1(3) . . ?
C23 C22 H22A 109.1 . . ?
C23 C22 H22B 109.1 . . ?
H22A C22 H22B 107.9 . . ?
C21 C22 C23 112.3(4) . . ?
C21 C22 H22A 109.1 . . ?
C21 C22 H22B 109.1 . . ?
P3 C30 H30 106.0 . . ?
C31 C30 P3 115.1(3) . . ?
C31 C30 H30 106.0 . . ?
C35 C30 P3 112.1(3) . . ?
C35 C30 C31 111.0(3) . . ?
C35 C30 H30 106.0 . . ?
C29 C28 H28A 109.5 . . ?
C29 C28 H28B 109.5 . . ?
C27 C28 C29 110.8(4) . . ?
C27 C28 H28A 109.5 . . ?
C27 C28 H28B 109.5 . . ?
H28A C28 H28B 108.1 . . ?
C11 C10 H10A 109.4 . . ?
C11 C10 H10B 109.4 . . ?
C11 C10 C9 111.0(4) . . ?
H10A C10 H10B 108.0 . . ?
C9 C10 H10A 109.4 . . ?
C9 C10 H10B 109.4 . . ?
C8 C9 C10 110.9(4) . . ?
C8 C9 H9A 109.5 . . ?
C8 C9 H9B 109.5 . . ?
C10 C9 H9A 109.5 . . ?
C10 C9 H9B 109.5 . . ?
H9A C9 H9B 108.1 . . ?
C15 C14 H14A 109.5 . . ?
C15 C14 H14B 109.5 . . ?
H14A C14 H14B 108.1 . . ?
C13 C14 C15 110.8(3) . . ?
C13 C14 H14A 109.5 . . ?
C13 C14 H14B 109.5 . . ?
C12 C13 H13A 109.3 . . ?
C12 C13 H13B 109.3 . . ?
C14 C13 C12 111.6(4) . . ?
C14 C13 H13A 109.3 . . ?
C14 C13 H13B 109.3 . . ?
H13A C13 H13B 108.0 . . ?
C25 C26 H26A 109.1 . . ?
C25 C26 H26B 109.1 . . ?
C27 C26 C25 112.3(4) . . ?
C27 C26 H26A 109.1 . . ?
C27 C26 H26B 109.1 . . ?
H26A C26 H26B 107.9 . . ?
C19 C20 H20A 109.3 . . ?
C19 C20 H20B 109.3 . . ?
C19 C20 C21 111.7(3) . . ?
H20A C20 H20B 107.9 . . ?
C21 C20 H20A 109.3 . . ?
C21 C20 H20B 109.3 . . ?
C48 C53 H53A 109.4 . . ?
C48 C53 H53B 109.4 . . ?
H53A C53 H53B 108.0 . . ?
C52 C53 C48 111.2(4) . . ?
C52 C53 H53A 109.4 . . ?
C52 C53 H53B 109.4 . . ?
C53 C52 H52A 109.4 . . ?
C53 C52 H52B 109.4 . . ?
C53 C52 C51 111.1(4) . . ?
H52A C52 H52B 108.0 . . ?
C51 C52 H52A 109.4 . . ?
C51 C52 H52B 109.4 . . ?
C22 C21 C20 110.7(3) . . ?
C22 C21 H21A 109.5 . . ?
C22 C21 H21B 109.5 . . ?
C20 C21 H21A 109.5 . . ?
C20 C21 H21B 109.5 . . ?
H21A C21 H21B 108.1 . . ?
C31 C32 H32A 109.5 . . ?
C31 C32 H32B 109.5 . . ?
H32A C32 H32B 108.1 . . ?
C33 C32 C31 110.8(4) . . ?
C33 C32 H32A 109.5 . . ?
C33 C32 H32B 109.5 . . ?
C44 C45 H45A 109.5 . . ?
C44 C45 H45B 109.5 . . ?
C46 C45 C44 110.8(3) . . ?
C46 C45 H45A 109.5 . . ?
C46 C45 H45B 109.5 . . ?
H45A C45 H45B 108.1 . . ?
C49 C50 H50A 109.2 . . ?
C49 C50 H50B 109.2 . . ?
H50A C50 H50B 107.9 . . ?
C51 C50 C49 111.9(4) . . ?
C51 C50 H50A 109.2 . . ?
C51 C50 H50B 109.2 . . ?
C36 C37 H37A 109.5 . . ?
C36 C37 H37B 109.5 . . ?
H37A C37 H37B 108.1 . . ?
C38 C37 C36 110.8(3) . . ?
C38 C37 H37A 109.5 . . ?
C38 C37 H37B 109.5 . . ?
H34A C34 H34B 107.9 . . ?
C35 C34 H34A 109.3 . . ?
C35 C34 H34B 109.3 . . ?
C33 C34 H34A 109.3 . . ?
C33 C34 H34B 109.3 . . ?
C33 C34 C35 111.8(4) . . ?
C52 C51 H51A 109.4 . . ?
C52 C51 H51B 109.4 . . ?
C50 C51 C52 111.1(4) . . ?
C50 C51 H51A 109.4 . . ?
C50 C51 H51B 109.4 . . ?
H51A C51 H51B 108.0 . . ?
C39 C38 C37 112.6(4) . . ?
C39 C38 H38A 109.1 . . ?
C39 C38 H38B 109.1 . . ?
C37 C38 H38A 109.1 . . ?
C37 C38 H38B 109.1 . . ?
H38A C38 H38B 107.8 . . ?
C30 C35 C34 110.8(4) . . ?
C30 C35 H35A 109.5 . . ?
C30 C35 H35B 109.5 . . ?
C34 C35 H35A 109.5 . . ?
C34 C35 H35B 109.5 . . ?
H35A C35 H35B 108.1 . . ?
C32 C33 H33A 109.3 . . ?
C32 C33 H33B 109.3 . . ?
C34 C33 C32 111.8(4) . . ?
C34 C33 H33A 109.3 . . ?
C34 C33 H33B 109.3 . . ?
H33A C33 H33B 107.9 . . ?
H14C O14B H14D 87.1 . . ?
H14E O14A H14F 104.5 . . ?
H13C O13 H13D 104.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Dy1 O5 C2 C1 -6.9(4) . . . . ?
Dy1 O5 C2 C3 173.0(3) . . . . ?
Dy1 O4 C1 C5 -171.4(3) . . . . ?
Dy1 O4 C1 C2 6.9(4) . . . . ?
P1 C17 C12 C13 173.9(3) . . . . ?
P1 C17 C16 C15 -174.1(3) . . . . ?
P1 C6 C7 C8 177.6(3) . . . . ?
P1 C6 C11 C10 -178.0(3) . . . . ?
P1 C18 C19 C20 173.8(3) . . . . ?
P1 C18 C23 C22 -172.0(3) . . . . ?
P2 C42 C43 C44 168.2(3) . . . . ?
P2 C42 C47 C46 -170.5(3) . . . . ?
P2 C48 C49 C50 -178.2(3) . . . . ?
P2 C48 C53 C52 179.3(3) . . . . ?
P2 C54 C55 C56 -173.4(3) . . . . ?
P2 C54 C59 C58 175.4(3) . . . . ?
P3 C36 C41 C40 179.1(3) . . . . ?
P3 C36 C37 C38 -177.1(3) . . . . ?
P3 C30 C35 C34 -174.5(3) . . . . ?
O9 P1 C17 C12 -175.8(3) . . . . ?
O9 P1 C17 C16 56.8(3) . . . . ?
O9 P1 C6 C7 -49.1(3) . . . . ?
O9 P1 C6 C11 74.3(3) . . . . ?
O9 P1 C18 C19 153.1(3) . . . . ?
O9 P1 C18 C23 24.5(3) . . . . ?
O10 P2 C42 C43 -68.2(3) . . . . ?
O10 P2 C42 C47 160.9(3) . . . . ?
O10 P2 C48 C49 63.8(3) . . . . ?
O10 P2 C48 C53 -59.1(3) . . . . ?
O10 P2 C54 C55 45.0(3) . . . . ?
O10 P2 C54 C59 173.6(3) . . . . ?
O4 C1 C5 O8 0.9(7) . . . . ?
O4 C1 C5 C4 -179.4(4) . . . . ?
O4 C1 C2 O5 0.0(6) . . . . ?
O4 C1 C2 C3 -180.0(3) . . . . ?
O15 P3 C36 C41 -49.2(3) . . . . ?
O15 P3 C36 C37 72.1(3) . . . . ?
O15 P3 C24 C25 47.9(3) . . . . ?
O15 P3 C24 C29 175.4(3) . . . . ?
O15 P3 C30 C31 147.4(3) . . . . ?
O15 P3 C30 C35 19.3(4) . . . . ?
O8 C5 C4 O7 -1.0(7) . . . . ?
O8 C5 C4 C3 177.6(4) . . . . ?
O6 C3 C2 O5 0.0(7) . . . . ?
O6 C3 C2 C1 179.9(4) . . . . ?
O6 C3 C4 O7 0.1(7) . . . . ?
O6 C3 C4 C5 -178.5(4) . . . . ?
C42 P2 C48 C49 -178.9(3) . . . . ?
C42 P2 C48 C53 58.3(3) . . . . ?
C42 P2 C54 C55 -75.7(3) . . . . ?
C42 P2 C54 C59 52.8(3) . . . . ?
C42 C43 C44 C45 56.9(4) . . . . ?
C42 C47 C46 C45 -57.8(4) . . . . ?
C43 C42 C47 C46 57.5(4) . . . . ?
C43 C44 C45 C46 -56.9(5) . . . . ?
C17 P1 C6 C7 -168.8(3) . . . . ?
C17 P1 C6 C11 -45.3(3) . . . . ?
C17 P1 C18 C19 -87.2(3) . . . . ?
C17 P1 C18 C23 144.2(3) . . . . ?
C17 C12 C13 C14 57.5(5) . . . . ?
C17 C16 C15 C14 -55.8(5) . . . . ?
C48 P2 C42 C43 173.5(3) . . . . ?
C48 P2 C42 C47 42.7(3) . . . . ?
C48 P2 C54 C55 163.9(3) . . . . ?
C48 P2 C54 C59 -67.6(3) . . . . ?
C48 C49 C50 C51 55.7(5) . . . . ?
C48 C53 C52 C51 -56.2(5) . . . . ?
C36 P3 C24 C25 169.7(3) . . . . ?
C36 P3 C24 C29 -62.8(3) . . . . ?
C36 P3 C30 C31 25.3(4) . . . . ?
C36 P3 C30 C35 -102.8(3) . . . . ?
C36 C41 C40 C39 -56.3(5) . . . . ?
C36 C37 C38 C39 55.4(6) . . . . ?
C54 P2 C42 C43 52.8(3) . . . . ?
C54 P2 C42 C47 -78.0(3) . . . . ?
C54 P2 C48 C49 -54.5(3) . . . . ?
C54 P2 C48 C53 -177.3(3) . . . . ?
C54 C55 C56 C57 -57.2(4) . . . . ?
C54 C59 C58 C57 55.2(4) . . . . ?
C6 P1 C17 C12 -55.9(3) . . . . ?
C6 P1 C17 C16 176.6(3) . . . . ?
C6 P1 C18 C19 31.9(3) . . . . ?
C6 P1 C18 C23 -96.7(3) . . . . ?
C6 C7 C8 C9 -53.3(5) . . . . ?
C6 C11 C10 C9 57.6(5) . . . . ?
C55 C54 C59 C58 -55.1(4) . . . . ?
C55 C56 C57 C58 57.1(4) . . . . ?
C7 C6 C11 C10 -55.5(5) . . . . ?
C7 C8 C9 C10 54.6(5) . . . . ?
C18 P1 C17 C12 63.8(3) . . . . ?
C18 P1 C17 C16 -63.7(3) . . . . ?
C18 P1 C6 C7 72.6(3) . . . . ?
C18 P1 C6 C11 -163.9(3) . . . . ?
C18 C19 C20 C21 55.7(5) . . . . ?
C18 C23 C22 C21 -56.5(5) . . . . ?
C59 C54 C55 C56 56.3(4) . . . . ?
C47 C42 C43 C44 -57.9(4) . . . . ?
C47 C46 C45 C44 58.1(5) . . . . ?
C56 C57 C58 C59 -56.5(4) . . . . ?
C19 C18 C23 C22 56.7(5) . . . . ?
C19 C20 C21 C22 -54.6(5) . . . . ?
C1 C5 C4 O7 179.2(4) . . . . ?
C1 C5 C4 C3 -2.2(4) . . . . ?
C5 C1 C2 O5 178.5(3) . . . . ?
C5 C1 C2 C3 -1.4(4) . . . . ?
C41 C36 C37 C38 -55.9(5) . . . . ?
C49 C48 C53 C52 55.6(4) . . . . ?
C49 C50 C51 C52 -55.6(5) . . . . ?
C12 C17 C16 C15 56.8(4) . . . . ?
C23 C18 C19 C20 -56.9(5) . . . . ?
C23 C22 C21 C20 55.1(5) . . . . ?
C16 C17 C12 C13 -57.6(4) . . . . ?
C16 C15 C14 C13 55.4(5) . . . . ?
C2 C1 C5 O8 -177.5(4) . . . . ?
C2 C1 C5 C4 2.2(4) . . . . ?
C2 C3 C4 O7 180.0(4) . . . . ?
C2 C3 C4 C5 1.4(4) . . . . ?
C24 P3 C36 C41 -170.6(3) . . . . ?
C24 P3 C36 C37 -49.3(3) . . . . ?
C24 P3 C30 C31 -91.9(3) . . . . ?
C24 P3 C30 C35 140.0(3) . . . . ?
C24 C25 C26 C27 -53.5(5) . . . . ?
C24 C29 C28 C27 56.8(5) . . . . ?
C15 C14 C13 C12 -56.7(5) . . . . ?
C11 C6 C7 C8 53.6(5) . . . . ?
C11 C10 C9 C8 -57.0(5) . . . . ?
C40 C39 C38 C37 -53.8(6) . . . . ?
C4 C3 C2 O5 -179.9(4) . . . . ?
C4 C3 C2 C1 0.0(4) . . . . ?
C31 C30 C35 C34 55.3(5) . . . . ?
C31 C32 C33 C34 -55.4(6) . . . . ?
C30 P3 C36 C41 72.6(3) . . . . ?
C30 P3 C36 C37 -166.0(3) . . . . ?
C30 P3 C24 C25 -72.8(3) . . . . ?
C30 P3 C24 C29 54.7(3) . . . . ?
C30 C31 C32 C33 56.0(5) . . . . ?
C28 C29 C24 P3 179.7(3) . . . . ?
C28 C29 C24 C25 -53.6(4) . . . . ?
C28 C27 C26 C25 57.4(5) . . . . ?
C26 C25 C24 P3 179.1(3) . . . . ?
C26 C25 C24 C29 51.7(5) . . . . ?
C26 C27 C28 C29 -58.5(5) . . . . ?
C53 C48 C49 C50 -55.1(5) . . . . ?
C53 C52 C51 C50 55.9(6) . . . . ?
C32 C31 C30 P3 174.9(3) . . . . ?
C32 C31 C30 C35 -56.4(5) . . . . ?
C37 C36 C41 C40 56.7(5) . . . . ?
C38 C39 C40 C41 53.9(6) . . . . ?
C35 C34 C33 C32 55.1(6) . . . . ?
C33 C34 C35 C30 -54.8(5) . . . . ?


_olex2_submission_special_instructions 'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details 
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_oxdiff_exptl_absorpt_empirical_full_max 1.440
_oxdiff_exptl_absorpt_empirical_full_min 0.621
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_Dy2CA2n
_database_code_depnum_ccdc_archive 'CCDC 2502521'
loop_
_audit_author_name
_audit_author_address
'Yue Yang'
;Nankai University
China
;
_audit_update_record             
;
2025-11-13 deposited with the CCDC.	2026-03-27 downloaded from the CCDC.
;
_audit_creation_date             2025-01-04
_audit_creation_method           
;
Olex2 1.3
(compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C82 H136 Cl2 Dy2 O16 P4, 2(C H4 O)'
_chemical_formula_sum            'C84 H144 Cl2 Dy2 O18 P4'
_chemical_formula_weight         1961.76
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -9.8046 9.8477 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'I 1 2/a 1'
_space_group_name_Hall           '-I 2ya'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y, z'
'-x+1/2, -y+1/2, -z+1/2'
'x, -y+1/2, z+1/2'

_cell_length_a                   33.7159(4)
_cell_length_b                   10.76120(10)
_cell_length_c                   51.6078(8)
_cell_angle_alpha                90
_cell_angle_beta                 106.692(2)
_cell_angle_gamma                90
_cell_volume                     17935.5(4)
_cell_formula_units_Z            8
_cell_measurement_reflns_used    29408
_cell_measurement_temperature    120.00(10)
_cell_measurement_theta_max      76.3630
_cell_measurement_theta_min      3.5690
_shelx_estimated_absorpt_T_max   0.390
_shelx_estimated_absorpt_T_min   0.183
_exptl_absorpt_coefficient_mu    10.550
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.70009
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
CrysAlisPro 1.171.42.99a (Rigaku Oxford Diffraction, 2023)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            'clear light yellow'
_exptl_crystal_colour_lustre     clear
_exptl_crystal_colour_modifier   light
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    1.453
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       needle
_exptl_crystal_F_000             8144
_exptl_crystal_size_max          0.244
_exptl_crystal_size_mid          0.13
_exptl_crystal_size_min          0.11
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0373
_diffrn_reflns_av_unetI/netI     0.0361
_diffrn_reflns_Laue_measured_fraction_full 0.992
_diffrn_reflns_Laue_measured_fraction_max 0.949
_diffrn_reflns_limit_h_max       42
_diffrn_reflns_limit_h_min       -42
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       61
_diffrn_reflns_limit_l_min       -65
_diffrn_reflns_number            61447
_diffrn_reflns_point_group_measured_fraction_full 0.992
_diffrn_reflns_point_group_measured_fraction_max 0.949
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         76.709
_diffrn_reflns_theta_min         3.576
_diffrn_ambient_environment      N~2~
_diffrn_ambient_temperature      120.00(10)
_diffrn_detector                 'Hybrid Pixel Array Detector'
_diffrn_detector_area_resol_mean 10.0000
_diffrn_detector_type            HyPix
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.949
_diffrn_measurement_details      
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
#--------------------------------------------------------------------------
  1  ω     44.00 103.00   0.50    0.05    --   47.15  76.00 -65.00  118
  2  ω    111.00 177.00   0.50    0.05    --  105.91  61.00   0.00  132
  3  ω     84.00 178.00   0.50    0.05    --  105.91  76.00 -65.00  188
  4  ω    152.00 177.00   0.50    0.05    --  105.91  30.00-150.00   50
  5  ω     97.00 136.00   0.50    0.05    --  105.91  30.00-150.00   78
  6  ω     37.00  95.00   0.50    0.05    --  105.91 -77.00 -30.00  116
  7  ω     35.00  75.00   0.50    0.05    --  105.91 -61.00 -30.00   80
  8  ω     50.00 105.00   0.50    0.05    --  105.91 -76.00 168.00  110
  9  ω    -24.00  61.00   0.50    0.05    --   47.15 -76.00 168.00  170
 10  ω    -22.00  28.00   0.50    0.05    --  -47.15  19.00  90.00  100
 11  ω    -45.00  26.00   0.50    0.05    --  -47.15  76.00 -65.00  142
 12  ω    -86.00 -61.00   0.50    0.05    -- -104.50  77.00  30.00   50
 13  ω    -68.00 -43.00   0.50    0.05    -- -104.50  61.00  90.00   50
 14  ω    -81.00 -46.00   0.50    0.05    -- -104.50  76.00 -65.00   70
 15  ω    -64.00 -35.00   0.50    0.05    -- -104.50  61.00 -60.00   58
 16  ω    -62.00 -33.00   0.50    0.05    -- -104.50  61.00 -90.00   58
 17  ω    -60.00 -32.00   0.50    0.05    -- -104.50  61.00-120.00   56
 18  ω     -1.00  27.00   0.50    0.05    --  -47.15  19.00 -90.00   56
 19  ω    -62.00 -35.00   0.50    0.05    -- -104.50  61.00   0.00   54
 20  ω    -65.00 -38.00   0.50    0.05    -- -104.50  61.00 150.00   54
 21  ω    -97.00 -72.00   0.50    0.05    --  -47.15 -76.00 168.00   50
 22  ω   -173.00-145.00   0.50    0.05    -- -104.50 -76.00 168.00   56
 23  ω   -121.00 -95.00   0.50    0.05    -- -104.50 -45.00-120.00   52
 24  ω   -165.00-134.00   0.50    0.05    -- -104.50 -45.00-120.00   62
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'XtaLAB Synergy R, HyPix'
_diffrn_measurement_method       'ω scans'
_diffrn_orient_matrix_type       
'CrysAlisPro convention (1999,Acta A55,543-557)'
_diffrn_orient_matrix_UB_11      0.0200115000
_diffrn_orient_matrix_UB_12      -0.0744453000
_diffrn_orient_matrix_UB_13      0.0259688000
_diffrn_orient_matrix_UB_21      -0.0362345000
_diffrn_orient_matrix_UB_22      -0.0931223000
_diffrn_orient_matrix_UB_23      -0.0075769000
_diffrn_orient_matrix_UB_31      0.0236913000
_diffrn_orient_matrix_UB_32      -0.0792476000
_diffrn_orient_matrix_UB_33      -0.0154905000
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.54184
_diffrn_source                   'Rotating-anode X-ray tube'
_diffrn_source_type              'PhotonJet R (Cu) X-ray Source'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                15208
_reflns_number_total             17941
_reflns_odcompleteness_completeness 99.24
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta     66.97
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'CrysAlisPro 1.171.42.99a (Rigaku OD, 2023)'
_computing_data_collection       'CrysAlisPro 1.171.42.99a (Rigaku OD, 2023)'
_computing_data_reduction        'CrysAlisPro 1.171.42.99a (Rigaku OD, 2023)'
_computing_molecular_graphics    'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         0.786
_refine_diff_density_min         -1.105
_refine_diff_density_rms         0.092
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.044
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1047
_refine_ls_number_reflns         17941
_refine_ls_number_restraints     67
_refine_ls_R_factor_all          0.0551
_refine_ls_R_factor_gt           0.0454
_refine_ls_restrained_S_all      1.049
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0555P)²+74.9274P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1097
_refine_ls_wR_factor_ref         0.1153
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups, All C(H,H,H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups, All O(H) groups, All O(H,H) groups
2. Restrained distances
 Dy1-H1A \\sim Dy1-H1B
 with sigma of 0.02
3. Uiso/Uaniso restraints and constraints
O18A \\sim C83A \\sim C83 \\sim O18: within 2A with sigma of 0.001 and sigma
for terminal atoms of 0.002 within 2A
Uanis(C77) \\sim Ueq, Uanis(O18) \\sim Ueq, Uanis(C83) \\sim Ueq: with sigma of
0.002 and sigma for terminal atoms of 0.004
Uanis(C80A) \\sim Ueq, Uanis(C82A) \\sim Ueq: with sigma of 0.02 and sigma for
terminal atoms of 0.04
Uanis(C79A) \\sim Ueq: with sigma of 0.02 and sigma for terminal atoms of 0.04
4. Others
 Sof(O18A)=Sof(H18C)=Sof(C83A)=Sof(H83D)=Sof(H83E)=Sof(H83F)=1-FVAR(1)
 Sof(C83)=Sof(H83A)=Sof(H83B)=Sof(H83C)=Sof(O18)=Sof(H18)=FVAR(1)
 Sof(H78A)=Sof(H78B)=Sof(C79A)=Sof(H79C)=Sof(H79D)=1-FVAR(2)
 Sof(H78C)=Sof(H78D)=Sof(C79)=Sof(H79A)=Sof(H79B)=FVAR(2)
 Fixed Sof: H81C(0.66667) H81D(0.66667) H81A(0.33333) H81B(0.33333)
 H77(0.33333) H77A(0.66667) C80(0.5) H80A(0.5) H80B(0.5) C82A(0.33333)
 H82A(0.33333) H82B(0.33333) C82(0.66667) H82C(0.66667) H82D(0.66667) C80A(0.5)
 H80C(0.5) H80D(0.5)
5.a Riding coordinates:
 C83(H83A,H83B,H83C)
5.b Free rotating group:
 O1(H1A,H1B)
5.c Rotating group:
 O7(H7A,H7B)
5.d Ternary CH refined with riding coordinates:
 C11(H11), C17(H17), C23(H23), C71(H71), C35(H35), C65(H65), C41(H41),
 C29(H29), C47(H47), C53(H53), C59(H59), C77(H77), C77(H77A)
5.e Secondary CH2 refined with riding coordinates:
 C12(H12A,H12B), C13(H13A,H13B), C16(H16A,H16B), C73(H73A,H73B), C24(H24A,
 H24B), C36(H36A,H36B), C18(H18A,H18B), C15(H15A,H15B), C14(H14A,H14B),
 C22(H22A,H22B), C72(H72A,H72B), C21(H21A,H21B), C40(H40A,H40B), C66(H66A,H66B),
  C30(H30A,H30B), C20(H20A,H20B), C25(H25A,H25B), C19(H19A,H19B), C34(H34A,
 H34B), C74(H74A,H74B), C42(H42A,H42B), C26(H26A,H26B), C76(H76A,H76B),
 C28(H28A,H28B), C75(H75A,H75B), C37(H37A,H37B), C70(H70A,H70B), C68(H68A,H68B),
  C39(H39A,H39B), C49(H49A,H49B), C31(H31A,H31B), C27(H27A,H27B), C54(H54A,
 H54B), C38(H38A,H38B), C46(H46A,H46B), C33(H33A,H33B), C64(H64A,H64B),
 C69(H69A,H69B), C57(H57A,H57B), C48(H48A,H48B), C60(H60A,H60B), C62(H62A,H62B),
  C32(H32A,H32B), C67(H67A,H67B), C63(H63A,H63B), C58(H58A,H58B), C52(H52A,
 H52B), C61(H61A,H61B), C78(H78C,H78D), C78(H78A,H78B), C45(H45A,H45B),
 C81(H81C,H81D), C81(H81A,H81B), C43(H43A,H43B), C44(H44A,H44B), C55(H55A,H55B),
  C56(H56A,H56B), C50(H50A,H50B), C51(H51A,H51B), C80(H80A,H80B), C79(H79A,
 H79B), C82A(H82A,H82B), C82(H82C,H82D), C80A(H80C,H80D), C79A(H79C,H79D)
5.f Idealised Me refined as rotating group:
 C84(H84A,H84B,H84C), C83A(H83D,H83E,H83F)
5.g Idealised tetrahedral OH refined as rotating group:
 O17(H17A), O18(H18), O18A(H18C)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.44908(2) 0.20192(2) 0.34894(2) 0.02053(6) Uani 1 1 d D . . . .
Dy2 Dy 0.56400(2) 0.70371(2) 0.39487(2) 0.02089(6) Uani 1 1 d . . . . .
Cl2 Cl 0.53448(3) 0.68514(10) 0.43665(2) 0.0339(2) Uani 1 1 d . . . . .
P3 P 0.34656(3) 0.07300(9) 0.30693(2) 0.0246(2) Uani 1 1 d . . . . .
P2 P 0.42085(3) 0.18124(9) 0.41367(2) 0.0249(2) Uani 1 1 d . . . . .
P1 P 0.59024(3) 0.76143(11) 0.33008(2) 0.0333(2) Uani 1 1 d . . . . .
P4 P 0.66958(3) 0.61063(11) 0.43617(2) 0.0335(2) Uani 1 1 d . . . . .
Cl1 Cl 0.46173(4) 0.23661(14) 0.30239(2) 0.0518(3) Uani 1 1 d . . . . .
O1 O 0.46492(8) -0.0067(2) 0.35010(6) 0.0283(6) Uani 1 1 d G . . . .
H1A H 0.487929 -0.040036 0.359759 0.042 Uiso 1 1 d DG U . . .
H1B H 0.447868 -0.068917 0.345470 0.042 Uiso 1 1 d DG U . . .
O16 O 0.43211(8) 0.1896(2) 0.38744(5) 0.0251(6) Uani 1 1 d . . . . .
O7 O 0.55555(8) 0.4958(2) 0.38382(6) 0.0305(6) Uani 1 1 d . . . . .
H7A H 0.565543 0.451082 0.398322 0.046 Uiso 1 1 d R U . . .
H7B H 0.529174 0.477970 0.378712 0.046 Uiso 1 1 d R U . . .
O10 O 0.35103(8) 0.6089(3) 0.32680(6) 0.0350(7) Uani 1 1 d . . . . .
O5 O 0.51944(8) 0.1854(2) 0.37620(5) 0.0255(6) Uani 1 1 d . . . . .
O3 O 0.39709(8) 0.3644(2) 0.33858(6) 0.0280(6) Uani 1 1 d . . . . .
O11 O 0.53366(8) -0.0908(2) 0.38420(5) 0.0251(6) Uani 1 1 d . . . . .
O15 O 0.58468(9) 0.7467(3) 0.35797(6) 0.0340(6) Uani 1 1 d . . . . .
O2 O 0.38712(7) 0.1096(2) 0.32692(5) 0.0247(5) Uani 1 1 d . . . . .
O6 O 0.49475(8) 0.6860(2) 0.36690(6) 0.0270(6) Uani 1 1 d . . . . .
O12 O 0.60935(8) -0.1346(2) 0.41959(6) 0.0277(6) Uani 1 1 d . . . . .
O9 O 0.41348(9) 0.8016(3) 0.34089(7) 0.0354(7) Uani 1 1 d . . . . .
O4 O 0.47922(8) 0.4083(2) 0.36138(6) 0.0272(6) Uani 1 1 d . . . . .
O8 O 0.62738(8) 0.6160(3) 0.41568(6) 0.0325(6) Uani 1 1 d . . . . .
O13 O 0.65191(9) 0.1098(3) 0.43869(7) 0.0397(7) Uani 1 1 d . . . . .
O14 O 0.59462(10) 0.3026(3) 0.41235(7) 0.0443(8) Uani 1 1 d . . . . .
O17 O 0.53926(13) 0.9722(4) 0.45461(9) 0.0636(11) Uani 1 1 d . . . . .
H17A H 0.534309 0.898330 0.449435 0.095 Uiso 1 1 calc R U . . .
C5 C 0.38801(11) 0.5914(3) 0.33643(8) 0.0230(8) Uani 1 1 d . . . . .
C1 C 0.41061(11) 0.4730(3) 0.34257(8) 0.0223(7) Uani 1 1 d . . . . .
C4 C 0.42051(11) 0.6893(3) 0.34452(8) 0.0224(7) Uani 1 1 d . . . . .
C11 C 0.46519(12) 0.2201(4) 0.44210(8) 0.0279(8) Uani 1 1 d . . . . .
H11 H 0.481412 0.141643 0.447286 0.033 Uiso 1 1 calc R U . . .
C3 C 0.46100(11) 0.6294(3) 0.35684(7) 0.0216(7) Uani 1 1 d . . . . .
C9 C 0.61732(12) 0.0929(4) 0.42312(8) 0.0271(8) Uani 1 1 d . . . . .
C6 C 0.55033(11) 0.1302(3) 0.39137(7) 0.0216(7) Uani 1 1 d . . . . .
C7 C 0.55687(11) -0.0001(4) 0.39510(7) 0.0236(8) Uani 1 1 d . . . . .
C17 C 0.37729(12) 0.2840(4) 0.41187(8) 0.0300(9) Uani 1 1 d . . . . .
H17 H 0.370006 0.278575 0.429301 0.036 Uiso 1 1 calc R U . . .
C12 C 0.49463(12) 0.3147(4) 0.43450(9) 0.0301(9) Uani 1 1 d . . . . .
H12A H 0.502241 0.284879 0.418418 0.036 Uiso 1 1 calc R U . . .
H12B H 0.480514 0.395866 0.430025 0.036 Uiso 1 1 calc R U . . .
C23 C 0.40508(12) 0.0218(4) 0.41785(8) 0.0293(9) Uani 1 1 d . . . . .
H23 H 0.378919 0.006865 0.403054 0.035 Uiso 1 1 calc R U . . .
C2 C 0.45395(11) 0.4981(4) 0.35454(8) 0.0246(8) Uani 1 1 d . . . . .
C8 C 0.59659(11) -0.0257(3) 0.41379(8) 0.0223(7) Uani 1 1 d . . . . .
C13 C 0.53367(13) 0.3298(4) 0.45836(9) 0.0371(10) Uani 1 1 d . . . . .
H13A H 0.549010 0.250159 0.461603 0.045 Uiso 1 1 calc R U . . .
H13B H 0.551850 0.393297 0.453823 0.045 Uiso 1 1 calc R U . . .
C16 C 0.45399(13) 0.2641(4) 0.46743(8) 0.0336(9) Uani 1 1 d . . . . .
H16A H 0.439430 0.344905 0.463745 0.040 Uiso 1 1 calc R U . . .
H16B H 0.435156 0.203144 0.472132 0.040 Uiso 1 1 calc R U . . .
C71 C 0.66601(12) 0.5879(4) 0.47022(9) 0.0342(10) Uani 1 1 d . . . . .
H71 H 0.694639 0.572956 0.482282 0.041 Uiso 1 1 calc R U . . .
C35 C 0.32178(13) 0.2011(4) 0.28527(9) 0.0308(9) Uani 1 1 d . . . . .
H35 H 0.297522 0.165853 0.271179 0.037 Uiso 1 1 calc R U . . .
C65 C 0.69750(12) 0.7536(5) 0.43587(9) 0.0356(10) Uani 1 1 d . . . . .
H65 H 0.681461 0.820086 0.441940 0.043 Uiso 1 1 calc R U . . .
C73 C 0.64474(14) 0.6748(5) 0.50964(9) 0.0400(11) Uani 1 1 d . . . . .
H73A H 0.672816 0.663843 0.522264 0.048 Uiso 1 1 calc R U . . .
H73B H 0.631776 0.747025 0.515886 0.048 Uiso 1 1 calc R U . . .
C24 C 0.43708(13) -0.0708(4) 0.41329(11) 0.0402(11) Uani 1 1 d . . . . .
H24A H 0.441426 -0.055504 0.395382 0.048 Uiso 1 1 calc R U . . .
H24B H 0.463852 -0.058451 0.427291 0.048 Uiso 1 1 calc R U . . .
C36 C 0.30510(13) 0.3017(4) 0.30036(9) 0.0326(9) Uani 1 1 d . . . . .
H36A H 0.328202 0.336410 0.315011 0.039 Uiso 1 1 calc R U . . .
H36B H 0.284934 0.264142 0.308717 0.039 Uiso 1 1 calc R U . . .
C18 C 0.38823(12) 0.4202(4) 0.40734(9) 0.0315(9) Uani 1 1 d . . . . .
H18A H 0.410304 0.449257 0.423335 0.038 Uiso 1 1 calc R U . . .
H18B H 0.399115 0.424277 0.391470 0.038 Uiso 1 1 calc R U . . .
C15 C 0.49322(15) 0.2778(4) 0.49113(9) 0.0383(10) Uani 1 1 d . . . . .
H15A H 0.485831 0.308314 0.507237 0.046 Uiso 1 1 calc R U . . .
H15B H 0.506747 0.195729 0.495593 0.046 Uiso 1 1 calc R U . . .
C14 C 0.52313(15) 0.3685(5) 0.48395(9) 0.0433(11) Uani 1 1 d . . . . .
H14A H 0.510560 0.452392 0.481353 0.052 Uiso 1 1 calc R U . . .
H14B H 0.548898 0.372891 0.499138 0.052 Uiso 1 1 calc R U . . .
C41 C 0.35323(14) -0.0563(4) 0.28572(9) 0.0355(10) Uani 1 1 d . . . . .
H41 H 0.351426 -0.133423 0.296136 0.043 Uiso 1 1 calc R U . . .
C22 C 0.33939(13) 0.2426(4) 0.38853(10) 0.0370(10) Uani 1 1 d . . . . .
H22A H 0.347431 0.238270 0.371551 0.044 Uiso 1 1 calc R U . . .
H22B H 0.330865 0.158329 0.392449 0.044 Uiso 1 1 calc R U . . .
C72 C 0.64828(14) 0.7011(4) 0.48130(9) 0.0360(10) Uani 1 1 d . . . . .
H72A H 0.666554 0.773803 0.481944 0.043 Uiso 1 1 calc R U . . .
H72B H 0.620597 0.721507 0.469052 0.043 Uiso 1 1 calc R U . . .
C10 C 0.58797(12) 0.1905(4) 0.40936(8) 0.0279(8) Uani 1 1 d . . . . .
C21 C 0.30282(13) 0.3309(5) 0.38457(11) 0.0429(11) Uani 1 1 d . . . . .
H21A H 0.279873 0.302506 0.369005 0.051 Uiso 1 1 calc R U . . .
H21B H 0.292952 0.329112 0.400872 0.051 Uiso 1 1 calc R U . . .
C29 C 0.31061(11) 0.0232(4) 0.32526(9) 0.0299(9) Uani 1 1 d . . . . .
H29 H 0.306109 0.096796 0.335901 0.036 Uiso 1 1 calc R U . . .
C40 C 0.35066(14) 0.2588(4) 0.27041(9) 0.0358(10) Uani 1 1 d . . . . .
H40A H 0.375516 0.292487 0.283837 0.043 Uiso 1 1 calc R U . . .
H40B H 0.359861 0.193478 0.259916 0.043 Uiso 1 1 calc R U . . .
C66 C 0.69923(14) 0.7922(5) 0.40751(10) 0.0443(12) Uani 1 1 d . . . . .
H66A H 0.714710 0.728649 0.400503 0.053 Uiso 1 1 calc R U . . .
H66B H 0.670725 0.795809 0.395147 0.053 Uiso 1 1 calc R U . . .
C47 C 0.54537(16) 0.7001(5) 0.30479(10) 0.0483(13) Uani 1 1 d . . . . .
H47 H 0.522873 0.762485 0.303407 0.058 Uiso 1 1 calc R U . . .
C30 C 0.32896(12) -0.0792(4) 0.34596(9) 0.0325(9) Uani 1 1 d . . . . .
H30A H 0.334125 -0.154404 0.336355 0.039 Uiso 1 1 calc R U . . .
H30B H 0.355813 -0.050851 0.358115 0.039 Uiso 1 1 calc R U . . .
C20 C 0.31444(14) 0.4628(5) 0.37954(10) 0.0415(11) Uani 1 1 d . . . . .
H20A H 0.290416 0.518361 0.377832 0.050 Uiso 1 1 calc R U . . .
H20B H 0.322009 0.466428 0.362382 0.050 Uiso 1 1 calc R U . . .
C25 C 0.42231(15) -0.2037(4) 0.41458(10) 0.0423(11) Uani 1 1 d . . . . .
H25A H 0.396913 -0.218017 0.399491 0.051 Uiso 1 1 calc R U . . .
H25B H 0.443828 -0.262063 0.412402 0.051 Uiso 1 1 calc R U . . .
C53 C 0.63868(15) 0.6861(5) 0.33046(11) 0.0428(11) Uani 1 1 d . . . . .
H53 H 0.658913 0.717099 0.347422 0.051 Uiso 1 1 calc R U . . .
C19 C 0.35065(14) 0.5065(4) 0.40267(10) 0.0393(10) Uani 1 1 d . . . . .
H19A H 0.341968 0.510644 0.419420 0.047 Uiso 1 1 calc R U . . .
H19B H 0.358674 0.591294 0.398684 0.047 Uiso 1 1 calc R U . . .
C34 C 0.26753(13) -0.0162(5) 0.30740(10) 0.0438(12) Uani 1 1 d . . . . .
H34A H 0.255402 0.051764 0.294668 0.053 Uiso 1 1 calc R U . . .
H34B H 0.270285 -0.090213 0.296653 0.053 Uiso 1 1 calc R U . . .
C74 C 0.61929(15) 0.5597(5) 0.51034(11) 0.0455(11) Uani 1 1 d . . . . .
H74A H 0.590326 0.573421 0.499312 0.055 Uiso 1 1 calc R U . . .
H74B H 0.619212 0.542627 0.529177 0.055 Uiso 1 1 calc R U . . .
C42 C 0.39612(17) -0.0592(5) 0.28104(11) 0.0520(14) Uani 1 1 d . . . . .
H42A H 0.398800 0.010985 0.269256 0.062 Uiso 1 1 calc R U . . .
H42B H 0.417821 -0.050321 0.298537 0.062 Uiso 1 1 calc R U . . .
C26 C 0.4133(2) -0.2295(5) 0.44113(11) 0.0579(16) Uani 1 1 d . . . . .
H26A H 0.439153 -0.221843 0.456174 0.070 Uiso 1 1 calc R U . . .
H26B H 0.402878 -0.315505 0.441124 0.070 Uiso 1 1 calc R U . . .
C76 C 0.64015(14) 0.4710(5) 0.47106(11) 0.0444(12) Uani 1 1 d . . . . .
H76A H 0.611966 0.481454 0.458554 0.053 Uiso 1 1 calc R U . . .
H76B H 0.653061 0.398157 0.465000 0.053 Uiso 1 1 calc R U . . .
C28 C 0.39510(18) -0.0043(5) 0.44450(10) 0.0483(12) Uani 1 1 d . . . . .
H28A H 0.420007 0.011204 0.459880 0.058 Uiso 1 1 calc R U . . .
H28B H 0.372973 0.052764 0.446258 0.058 Uiso 1 1 calc R U . . .
C75 C 0.63741(15) 0.4488(5) 0.49928(12) 0.0502(13) Uani 1 1 d . . . . .
H75A H 0.665436 0.431028 0.511372 0.060 Uiso 1 1 calc R U . . .
H75B H 0.619915 0.374837 0.499235 0.060 Uiso 1 1 calc R U . . .
C37 C 0.28394(13) 0.4069(4) 0.28111(10) 0.0413(11) Uani 1 1 d . . . . .
H37A H 0.258829 0.373941 0.267803 0.050 Uiso 1 1 calc R U . . .
H37B H 0.275200 0.472946 0.291644 0.050 Uiso 1 1 calc R U . . .
C70 C 0.74151(14) 0.7571(5) 0.45580(11) 0.0469(12) Uani 1 1 d . . . . .
H70A H 0.740070 0.737439 0.474250 0.056 Uiso 1 1 calc R U . . .
H70B H 0.758888 0.693133 0.450585 0.056 Uiso 1 1 calc R U . . .
C68 C 0.76318(14) 0.9195(5) 0.42790(12) 0.0520(14) Uani 1 1 d . . . . .
H68A H 0.781319 0.860522 0.421927 0.062 Uiso 1 1 calc R U . . .
H68B H 0.775226 1.003702 0.428440 0.062 Uiso 1 1 calc R U . . .
C39 C 0.32944(16) 0.3627(4) 0.25132(9) 0.0423(11) Uani 1 1 d . . . . .
H39A H 0.349543 0.400829 0.242987 0.051 Uiso 1 1 calc R U . . .
H39B H 0.306492 0.327383 0.236638 0.051 Uiso 1 1 calc R U . . .
C49 C 0.48555(18) 0.5564(6) 0.29275(11) 0.0608(16) Uani 1 1 d . . . . .
H49A H 0.474197 0.478244 0.297818 0.073 Uiso 1 1 calc R U . . .
H49B H 0.466600 0.625099 0.293921 0.073 Uiso 1 1 calc R U . . .
C31 C 0.29974(14) -0.1119(5) 0.36281(10) 0.0426(11) Uani 1 1 d . . . . .
H31A H 0.311581 -0.181550 0.375131 0.051 Uiso 1 1 calc R U . . .
H31B H 0.297095 -0.039394 0.374021 0.051 Uiso 1 1 calc R U . . .
C59 C 0.59626(14) 0.9249(5) 0.32227(10) 0.0415(11) Uani 1 1 d . . . . .
H59 H 0.603282 0.927688 0.304722 0.050 Uiso 1 1 calc R U . . .
C27 C 0.3810(2) -0.1380(5) 0.44545(11) 0.0606(16) Uani 1 1 d . . . . .
H27A H 0.354511 -0.150754 0.431243 0.073 Uiso 1 1 calc R U . . .
H27B H 0.376300 -0.154201 0.463204 0.073 Uiso 1 1 calc R U . . .
C54 C 0.63760(17) 0.5462(5) 0.33458(12) 0.0508(13) Uani 1 1 d . . . . .
H54A H 0.619048 0.507105 0.318179 0.061 Uiso 1 1 calc R U . . .
H54B H 0.626479 0.528183 0.349970 0.061 Uiso 1 1 calc R U . . .
C38 C 0.31246(14) 0.4621(4) 0.26621(10) 0.0411(11) Uani 1 1 d . . . . .
H38A H 0.335773 0.504775 0.279307 0.049 Uiso 1 1 calc R U . . .
H38B H 0.297097 0.524678 0.253074 0.049 Uiso 1 1 calc R U . . .
C46 C 0.31923(17) -0.0689(4) 0.25842(9) 0.0444(12) Uani 1 1 d . . . . .
H46A H 0.291566 -0.067855 0.261487 0.053 Uiso 1 1 calc R U . . .
H46B H 0.320870 0.001828 0.246511 0.053 Uiso 1 1 calc R U . . .
C33 C 0.23894(15) -0.0462(6) 0.32450(13) 0.0630(17) Uani 1 1 d . . . . .
H33A H 0.211705 -0.073085 0.312603 0.076 Uiso 1 1 calc R U . . .
H33B H 0.234589 0.029501 0.334252 0.076 Uiso 1 1 calc R U . . .
C64 C 0.55796(15) 1.0036(5) 0.31900(12) 0.0517(13) Uani 1 1 d . . . . .
H64A H 0.549341 0.999123 0.335764 0.062 Uiso 1 1 calc R U . . .
H64B H 0.535118 0.970068 0.303990 0.062 Uiso 1 1 calc R U . . .
C69 C 0.76126(15) 0.8839(5) 0.45587(12) 0.0542(14) Uani 1 1 d . . . . .
H69A H 0.745007 0.946937 0.462412 0.065 Uiso 1 1 calc R U . . .
H69B H 0.789619 0.882858 0.468470 0.065 Uiso 1 1 calc R U . . .
C57 C 0.70148(17) 0.6625(6) 0.31436(12) 0.0584(15) Uani 1 1 d . . . . .
H57A H 0.712415 0.678341 0.298795 0.070 Uiso 1 1 calc R U . . .
H57B H 0.720070 0.704205 0.330387 0.070 Uiso 1 1 calc R U . . .
C48 C 0.52904(18) 0.5811(5) 0.31239(12) 0.0567(14) Uani 1 1 d . . . . .
H48A H 0.527304 0.586309 0.331182 0.068 Uiso 1 1 calc R U . . .
H48B H 0.547932 0.512039 0.311381 0.068 Uiso 1 1 calc R U . . .
C60 C 0.63316(16) 0.9824(5) 0.34415(11) 0.0520(13) Uani 1 1 d . . . . .
H60A H 0.627621 0.977940 0.361954 0.062 Uiso 1 1 calc R U . . .
H60B H 0.658519 0.933666 0.345299 0.062 Uiso 1 1 calc R U . . .
C62 C 0.60157(17) 1.1938(5) 0.33438(13) 0.0578(15) Uani 1 1 d . . . . .
H62A H 0.594788 1.196488 0.351807 0.069 Uiso 1 1 calc R U . . .
H62B H 0.606537 1.280027 0.329396 0.069 Uiso 1 1 calc R U . . .
C32 C 0.25705(15) -0.1484(6) 0.34483(12) 0.0575(15) Uani 1 1 d . . . . .
H32A H 0.259219 -0.226165 0.335066 0.069 Uiso 1 1 calc R U . . .
H32B H 0.238377 -0.164094 0.356186 0.069 Uiso 1 1 calc R U . . .
C67 C 0.71989(14) 0.9177(5) 0.40774(11) 0.0487(12) Uani 1 1 d . . . . .
H67A H 0.702668 0.983004 0.412668 0.058 Uiso 1 1 calc R U . . .
H67B H 0.721966 0.936412 0.389396 0.058 Uiso 1 1 calc R U . . .
C63 C 0.56578(17) 1.1400(5) 0.31304(14) 0.0613(16) Uani 1 1 d . . . . .
H63A H 0.571426 1.145388 0.295279 0.074 Uiso 1 1 calc R U . . .
H63B H 0.540603 1.189447 0.311995 0.074 Uiso 1 1 calc R U . . .
C58 C 0.65826(17) 0.7186(6) 0.30845(12) 0.0554(14) Uani 1 1 d . . . . .
H58A H 0.660070 0.810126 0.307096 0.066 Uiso 1 1 calc R U . . .
H58B H 0.640691 0.687028 0.290888 0.066 Uiso 1 1 calc R U . . .
C84 C 0.5722(2) 0.9750(6) 0.47773(11) 0.0658(17) Uani 1 1 d . . . . .
H84A H 0.597797 0.955760 0.473145 0.099 Uiso 1 1 calc R U . . .
H84B H 0.567895 0.913236 0.490616 0.099 Uiso 1 1 calc R U . . .
H84C H 0.574367 1.057878 0.485871 0.099 Uiso 1 1 calc R U . . .
C52 C 0.55015(19) 0.6897(8) 0.27584(11) 0.080(2) Uani 1 1 d . . . . .
H52A H 0.561106 0.768594 0.270779 0.095 Uiso 1 1 calc R U . . .
H52B H 0.569799 0.622286 0.275164 0.095 Uiso 1 1 calc R U . . .
C61 C 0.64025(17) 1.1179(5) 0.33768(13) 0.0575(14) Uani 1 1 d . . . . .
H61A H 0.663016 1.153308 0.352470 0.069 Uiso 1 1 calc R U . . .
H61B H 0.648572 1.121772 0.320793 0.069 Uiso 1 1 calc R U . . .
C78 C 0.73573(15) 0.4361(5) 0.45215(12) 0.0552(14) Uani 1 1 d . . . . .
H78C H 0.750825 0.508003 0.462328 0.066 Uiso 0.597(18) 1 calc R U P A 2
H78D H 0.724149 0.387705 0.464601 0.066 Uiso 0.597(18) 1 calc R U P A 2
H78A H 0.727569 0.439934 0.469098 0.066 Uiso 0.403(18) 1 calc R U P A 1
H78B H 0.760270 0.489976 0.454340 0.066 Uiso 0.403(18) 1 calc R U P A 1
C45 C 0.3253(3) -0.1907(5) 0.24494(13) 0.078(2) Uani 1 1 d . . . . .
H45A H 0.320855 -0.260934 0.256172 0.093 Uiso 1 1 calc R U . . .
H45B H 0.304240 -0.196698 0.227099 0.093 Uiso 1 1 calc R U . . .
C81 C 0.7102(2) 0.3073(6) 0.40068(14) 0.074(2) Uani 1 1 d . . . . .
H81C H 0.724799 0.354294 0.389656 0.088 Uiso 0.6667 1 calc R U P B 2
H81D H 0.694507 0.238945 0.389502 0.088 Uiso 0.6667 1 calc R U P B 2
H81A H 0.690222 0.255061 0.406522 0.088 Uiso 0.3333 1 calc R U P C 1
H81B H 0.708367 0.287204 0.381645 0.088 Uiso 0.3333 1 calc R U P C 1
C43 C 0.4018(2) -0.1813(7) 0.26781(13) 0.083(2) Uani 1 1 d . . . . .
H43A H 0.401254 -0.250577 0.280327 0.100 Uiso 1 1 calc R U . . .
H43B H 0.429146 -0.181696 0.264306 0.100 Uiso 1 1 calc R U . . .
C44 C 0.3678(3) -0.2017(7) 0.24107(14) 0.105(3) Uani 1 1 d . . . . .
H44A H 0.370776 -0.139423 0.227645 0.126 Uiso 1 1 calc R U . . .
H44B H 0.370990 -0.285259 0.233904 0.126 Uiso 1 1 calc R U . . .
C55 C 0.6812(2) 0.4913(6) 0.34024(16) 0.076(2) Uani 1 1 d . . . . .
H55A H 0.698410 0.521364 0.358069 0.091 Uiso 1 1 calc R U . . .
H55B H 0.679461 0.399674 0.341259 0.091 Uiso 1 1 calc R U . . .
C56 C 0.7018(2) 0.5239(6) 0.31956(15) 0.0712(18) Uani 1 1 d . . . . .
H56A H 0.687702 0.480682 0.302467 0.085 Uiso 1 1 calc R U . . .
H56B H 0.730858 0.494418 0.325533 0.085 Uiso 1 1 calc R U . . .
C50 C 0.4887(3) 0.5466(8) 0.26422(13) 0.092(3) Uani 1 1 d . . . . .
H50A H 0.505811 0.473572 0.262839 0.111 Uiso 1 1 calc R U . . .
H50B H 0.460697 0.533926 0.251592 0.111 Uiso 1 1 calc R U . . .
C77 C 0.7003(2) 0.4835(6) 0.42874(13) 0.0648(15) Uani 1 1 d . U . . .
H77 H 0.680381 0.416172 0.429784 0.078 Uiso 0.3333 1 calc R U P D 1
H77A H 0.716242 0.528720 0.418051 0.078 Uiso 0.6667 1 calc R U P E 2
C51 C 0.5076(3) 0.6619(11) 0.25615(13) 0.124(4) Uani 1 1 d . . . . .
H51A H 0.489008 0.733511 0.255697 0.149 Uiso 1 1 calc R U . . .
H51B H 0.510495 0.650697 0.237732 0.149 Uiso 1 1 calc R U . . .
C80 C 0.7429(3) 0.2523(11) 0.4270(2) 0.037(2) Uani 0.5 1 d . . P A 2
H80A H 0.728264 0.204835 0.437850 0.044 Uiso 0.5 1 calc R U P A 2
H80B H 0.762182 0.195360 0.421574 0.044 Uiso 0.5 1 calc R U P A 2
C79 C 0.7660(3) 0.3550(9) 0.44297(18) 0.043(3) Uani 0.597(18) 1 d . . P A 2
H79A H 0.779864 0.404349 0.431916 0.052 Uiso 0.597(18) 1 calc R U P A 2
H79B H 0.787430 0.322159 0.458870 0.052 Uiso 0.597(18) 1 calc R U P A 2
C83 C 0.6945(7) 0.128(2) 0.5011(5) 0.140(3) Uani 0.613(10) 1 d . U P F 1
H83A H 0.679146 0.194216 0.489509 0.210 Uiso 0.613(10) 1 d R U P F 1
H83B H 0.723746 0.150656 0.507869 0.210 Uiso 0.613(10) 1 d R U P F 1
H83C H 0.683126 0.115086 0.516399 0.210 Uiso 0.613(10) 1 d R U P F 1
O18 O 0.6918(5) 0.0215(12) 0.4868(3) 0.141(3) Uani 0.613(10) 1 d . U P F 1
H18 H 0.690669 0.038376 0.470746 0.211 Uiso 0.613(10) 1 calc R U P F 1
C82A C 0.7009(6) 0.4584(15) 0.4040(4) 0.054(4) Uani 0.3333 1 d . U P A 1
H82A H 0.722571 0.508758 0.399543 0.064 Uiso 0.3333 1 calc R U P A 1
H82B H 0.673849 0.480884 0.391203 0.064 Uiso 0.3333 1 calc R U P A 1
C82 C 0.6806(2) 0.3939(7) 0.40996(17) 0.0463(18) Uani 0.6667 1 d . . P A 2
H82C H 0.662368 0.436426 0.393903 0.056 Uiso 0.6667 1 calc R U P A 2
H82D H 0.662715 0.342737 0.417989 0.056 Uiso 0.6667 1 calc R U P A 2
C80A C 0.7515(6) 0.2878(17) 0.4178(5) 0.096(6) Uani 0.5 1 d . U P A 1
H80C H 0.770285 0.353871 0.415040 0.115 Uiso 0.5 1 calc R U P A 1
H80D H 0.762218 0.206226 0.414061 0.115 Uiso 0.5 1 calc R U P A 1
C79A C 0.7477(4) 0.2922(13) 0.4467(4) 0.056(5) Uani 0.403(18) 1 d . U P A 1
H79C H 0.774177 0.267906 0.459892 0.067 Uiso 0.403(18) 1 calc R U P A 1
H79D H 0.725780 0.234470 0.448592 0.067 Uiso 0.403(18) 1 calc R U P A 1
O18A O 0.7075(7) 0.203(2) 0.4897(5) 0.141(3) Uani 0.387(10) 1 d . U P F 2
H18C H 0.693636 0.258082 0.479467 0.211 Uiso 0.387(10) 1 calc R U P F 2
C83A C 0.6736(10) 0.108(3) 0.5026(7) 0.140(3) Uani 0.387(10) 1 d . U P F 2
H83D H 0.667953 0.030363 0.492428 0.211 Uiso 0.387(10) 1 calc R U P F 2
H83E H 0.647517 0.152832 0.500672 0.211 Uiso 0.387(10) 1 calc R U P F 2
H83F H 0.686780 0.090406 0.521768 0.211 Uiso 0.387(10) 1 calc R U P F 2


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy1 Cl1 2.5848(11) . ?
Dy1 O1 2.305(3) . ?
Dy1 O16 2.224(3) . ?
Dy1 O5 2.392(3) . ?
Dy1 O3 2.425(3) . ?
Dy1 O2 2.298(2) . ?
Dy1 O4 2.450(3) . ?
Dy2 Cl2 2.6292(10) . ?
Dy2 O7 2.306(3) . ?
Dy2 O11 2.432(2) 1_565 ?
Dy2 O15 2.256(3) . ?
Dy2 O6 2.374(3) . ?
Dy2 O12 2.423(3) 1_565 ?
Dy2 O8 2.301(3) . ?
P3 O2 1.510(3) . ?
P3 C35 1.820(4) . ?
P3 C41 1.824(4) . ?
P3 C29 1.819(4) . ?
P2 O16 1.510(3) . ?
P2 C11 1.817(4) . ?
P2 C17 1.819(4) . ?
P2 C23 1.828(4) . ?
P1 O15 1.512(3) . ?
P1 C47 1.815(5) . ?
P1 C53 1.819(5) . ?
P1 C59 1.829(5) . ?
P4 O8 1.511(3) . ?
P4 C71 1.812(5) . ?
P4 C65 1.806(5) . ?
P4 C77 1.822(6) . ?
O1 H1A 0.8699 . ?
O1 H1B 0.8699 . ?
O7 H7A 0.8720 . ?
O7 H7B 0.8733 . ?
O10 C5 1.217(4) . ?
O5 C6 1.258(4) . ?
O3 C1 1.250(4) . ?
O11 C7 1.277(4) . ?
O6 C3 1.264(4) . ?
O12 C8 1.255(4) . ?
O9 C4 1.235(4) . ?
O4 C2 1.269(5) . ?
O13 C9 1.225(5) . ?
O14 C10 1.228(5) . ?
O17 H17A 0.8400 . ?
O17 C84 1.377(7) . ?
C5 C1 1.471(5) . ?
C5 C4 1.491(5) . ?
C1 C2 1.439(5) . ?
C4 C3 1.478(5) . ?
C11 H11 1.0000 . ?
C11 C12 1.549(5) . ?
C11 C16 1.536(6) . ?
C3 C2 1.432(5) . ?
C9 C8 1.468(5) . ?
C9 C10 1.478(5) . ?
C6 C7 1.424(5) . ?
C6 C10 1.489(5) . ?
C7 C8 1.434(5) . ?
C17 H17 1.0000 . ?
C17 C18 1.545(6) . ?
C17 C22 1.548(6) . ?
C12 H12A 0.9900 . ?
C12 H12B 0.9900 . ?
C12 C13 1.531(6) . ?
C23 H23 1.0000 . ?
C23 C24 1.535(6) . ?
C23 C28 1.533(6) . ?
C13 H13A 0.9900 . ?
C13 H13B 0.9900 . ?
C13 C14 1.521(6) . ?
C16 H16A 0.9900 . ?
C16 H16B 0.9900 . ?
C16 C15 1.529(6) . ?
C71 H71 1.0000 . ?
C71 C72 1.538(6) . ?
C71 C76 1.538(6) . ?
C35 H35 1.0000 . ?
C35 C36 1.531(6) . ?
C35 C40 1.533(6) . ?
C65 H65 1.0000 . ?
C65 C66 1.538(7) . ?
C65 C70 1.544(6) . ?
C73 H73A 0.9900 . ?
C73 H73B 0.9900 . ?
C73 C72 1.528(6) . ?
C73 C74 1.513(7) . ?
C24 H24A 0.9900 . ?
C24 H24B 0.9900 . ?
C24 C25 1.523(6) . ?
C36 H36A 0.9900 . ?
C36 H36B 0.9900 . ?
C36 C37 1.540(6) . ?
C18 H18A 0.9900 . ?
C18 H18B 0.9900 . ?
C18 C19 1.533(6) . ?
C15 H15A 0.9900 . ?
C15 H15B 0.9900 . ?
C15 C14 1.524(6) . ?
C14 H14A 0.9900 . ?
C14 H14B 0.9900 . ?
C41 H41 1.0000 . ?
C41 C42 1.533(7) . ?
C41 C46 1.546(6) . ?
C22 H22A 0.9900 . ?
C22 H22B 0.9900 . ?
C22 C21 1.523(6) . ?
C72 H72A 0.9900 . ?
C72 H72B 0.9900 . ?
C21 H21A 0.9900 . ?
C21 H21B 0.9900 . ?
C21 C20 1.515(7) . ?
C29 H29 1.0000 . ?
C29 C30 1.536(6) . ?
C29 C34 1.539(5) . ?
C40 H40A 0.9900 . ?
C40 H40B 0.9900 . ?
C40 C39 1.526(6) . ?
C66 H66A 0.9900 . ?
C66 H66B 0.9900 . ?
C66 C67 1.518(7) . ?
C47 H47 1.0000 . ?
C47 C48 1.490(7) . ?
C47 C52 1.552(7) . ?
C30 H30A 0.9900 . ?
C30 H30B 0.9900 . ?
C30 C31 1.531(6) . ?
C20 H20A 0.9900 . ?
C20 H20B 0.9900 . ?
C20 C19 1.517(6) . ?
C25 H25A 0.9900 . ?
C25 H25B 0.9900 . ?
C25 C26 1.512(8) . ?
C53 H53 1.0000 . ?
C53 C54 1.523(7) . ?
C53 C58 1.510(7) . ?
C19 H19A 0.9900 . ?
C19 H19B 0.9900 . ?
C34 H34A 0.9900 . ?
C34 H34B 0.9900 . ?
C34 C33 1.517(7) . ?
C74 H74A 0.9900 . ?
C74 H74B 0.9900 . ?
C74 C75 1.524(7) . ?
C42 H42A 0.9900 . ?
C42 H42B 0.9900 . ?
C42 C43 1.518(8) . ?
C26 H26A 0.9900 . ?
C26 H26B 0.9900 . ?
C26 C27 1.530(9) . ?
C76 H76A 0.9900 . ?
C76 H76B 0.9900 . ?
C76 C75 1.505(7) . ?
C28 H28A 0.9900 . ?
C28 H28B 0.9900 . ?
C28 C27 1.520(7) . ?
C75 H75A 0.9900 . ?
C75 H75B 0.9900 . ?
C37 H37A 0.9900 . ?
C37 H37B 0.9900 . ?
C37 C38 1.514(7) . ?
C70 H70A 0.9900 . ?
C70 H70B 0.9900 . ?
C70 C69 1.518(8) . ?
C68 H68A 0.9900 . ?
C68 H68B 0.9900 . ?
C68 C69 1.513(8) . ?
C68 C67 1.530(7) . ?
C39 H39A 0.9900 . ?
C39 H39B 0.9900 . ?
C39 C38 1.522(7) . ?
C49 H49A 0.9900 . ?
C49 H49B 0.9900 . ?
C49 C48 1.547(8) . ?
C49 C50 1.510(8) . ?
C31 H31A 0.9900 . ?
C31 H31B 0.9900 . ?
C31 C32 1.523(7) . ?
C59 H59 1.0000 . ?
C59 C64 1.512(7) . ?
C59 C60 1.549(7) . ?
C27 H27A 0.9900 . ?
C27 H27B 0.9900 . ?
C54 H54A 0.9900 . ?
C54 H54B 0.9900 . ?
C54 C55 1.534(8) . ?
C38 H38A 0.9900 . ?
C38 H38B 0.9900 . ?
C46 H46A 0.9900 . ?
C46 H46B 0.9900 . ?
C46 C45 1.524(7) . ?
C33 H33A 0.9900 . ?
C33 H33B 0.9900 . ?
C33 C32 1.522(8) . ?
C64 H64A 0.9900 . ?
C64 H64B 0.9900 . ?
C64 C63 1.539(8) . ?
C69 H69A 0.9900 . ?
C69 H69B 0.9900 . ?
C57 H57A 0.9900 . ?
C57 H57B 0.9900 . ?
C57 C58 1.525(7) . ?
C57 C56 1.515(9) . ?
C48 H48A 0.9900 . ?
C48 H48B 0.9900 . ?
C60 H60A 0.9900 . ?
C60 H60B 0.9900 . ?
C60 C61 1.531(8) . ?
C62 H62A 0.9900 . ?
C62 H62B 0.9900 . ?
C62 C63 1.497(8) . ?
C62 C61 1.506(8) . ?
C32 H32A 0.9900 . ?
C32 H32B 0.9900 . ?
C67 H67A 0.9900 . ?
C67 H67B 0.9900 . ?
C63 H63A 0.9900 . ?
C63 H63B 0.9900 . ?
C58 H58A 0.9900 . ?
C58 H58B 0.9900 . ?
C84 H84A 0.9800 . ?
C84 H84B 0.9800 . ?
C84 H84C 0.9800 . ?
C52 H52A 0.9900 . ?
C52 H52B 0.9900 . ?
C52 C51 1.530(9) . ?
C61 H61A 0.9900 . ?
C61 H61B 0.9900 . ?
C78 H78C 0.9900 . ?
C78 H78D 0.9900 . ?
C78 H78A 0.9900 . ?
C78 H78B 0.9900 . ?
C78 C77 1.522(8) . ?
C78 C79 1.518(9) . ?
C78 C79A 1.644(14) . ?
C45 H45A 0.9900 . ?
C45 H45B 0.9900 . ?
C45 C44 1.506(12) . ?
C81 H81C 0.9900 . ?
C81 H81D 0.9900 . ?
C81 H81A 0.9900 . ?
C81 H81B 0.9900 . ?
C81 C80 1.594(12) . ?
C81 C82A 1.674(16) . ?
C81 C82 1.541(9) . ?
C81 C80A 1.43(2) . ?
C43 H43A 0.9900 . ?
C43 H43B 0.9900 . ?
C43 C44 1.536(10) . ?
C44 H44A 0.9900 . ?
C44 H44B 0.9900 . ?
C55 H55A 0.9900 . ?
C55 H55B 0.9900 . ?
C55 C56 1.473(9) . ?
C56 H56A 0.9900 . ?
C56 H56B 0.9900 . ?
C50 H50A 0.9900 . ?
C50 H50B 0.9900 . ?
C50 C51 1.508(11) . ?
C77 H77 1.0000 . ?
C77 H77A 1.0000 . ?
C77 C82A 1.309(16) . ?
C77 C82 1.393(9) . ?
C51 H51A 0.9900 . ?
C51 H51B 0.9900 . ?
C80 H80A 0.9900 . ?
C80 H80B 0.9900 . ?
C80 C79 1.463(17) . ?
C79 H79A 0.9900 . ?
C79 H79B 0.9900 . ?
C83 H83A 0.9797 . ?
C83 H83B 0.9801 . ?
C83 H83C 0.9807 . ?
C83 O18 1.35(2) . ?
O18 H18 0.8400 . ?
C82A H82A 0.9900 . ?
C82A H82B 0.9900 . ?
C82 H82C 0.9900 . ?
C82 H82D 0.9900 . ?
C80A H80C 0.9900 . ?
C80A H80D 0.9900 . ?
C80A C79A 1.53(3) . ?
C79A H79C 0.9900 . ?
C79A H79D 0.9900 . ?
O18A H18C 0.8400 . ?
O18A C83A 1.80(4) . ?
C83A H83D 0.9800 . ?
C83A H83E 0.9800 . ?
C83A H83F 0.9800 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Dy1 Cl1 93.78(8) . . ?
O1 Dy1 O5 74.28(9) . . ?
O1 Dy1 O3 148.85(9) . . ?
O1 Dy1 O4 143.21(9) . . ?
O16 Dy1 Cl1 172.96(7) . . ?
O16 Dy1 O1 92.06(10) . . ?
O16 Dy1 O5 86.35(9) . . ?
O16 Dy1 O3 83.39(10) . . ?
O16 Dy1 O2 89.17(9) . . ?
O16 Dy1 O4 90.78(10) . . ?
O5 Dy1 Cl1 99.02(7) . . ?
O5 Dy1 O3 135.68(9) . . ?
O5 Dy1 O4 69.31(9) . . ?
O3 Dy1 Cl1 89.58(7) . . ?
O3 Dy1 O4 67.86(8) . . ?
O2 Dy1 Cl1 88.40(7) . . ?
O2 Dy1 O1 76.27(9) . . ?
O2 Dy1 O5 150.01(9) . . ?
O2 Dy1 O3 72.88(9) . . ?
O2 Dy1 O4 140.47(9) . . ?
O4 Dy1 Cl1 86.90(7) . . ?
O7 Dy2 Cl2 94.60(8) . . ?
O7 Dy2 O11 144.30(9) . 1_565 ?
O7 Dy2 O6 75.04(9) . . ?
O7 Dy2 O12 147.26(9) . 1_565 ?
O11 Dy2 Cl2 91.21(7) 1_565 . ?
O15 Dy2 Cl2 171.68(9) . . ?
O15 Dy2 O7 92.07(11) . . ?
O15 Dy2 O11 80.47(10) . 1_565 ?
O15 Dy2 O6 89.51(10) . . ?
O15 Dy2 O12 89.76(10) . 1_565 ?
O15 Dy2 O8 90.41(11) . . ?
O6 Dy2 Cl2 87.41(7) . . ?
O6 Dy2 O11 70.06(9) . 1_565 ?
O6 Dy2 O12 137.68(9) . 1_565 ?
O12 Dy2 Cl2 87.32(7) 1_565 . ?
O12 Dy2 O11 68.10(8) 1_565 1_565 ?
O8 Dy2 Cl2 96.07(8) . . ?
O8 Dy2 O7 75.49(10) . . ?
O8 Dy2 O11 138.81(9) . 1_565 ?
O8 Dy2 O6 150.51(9) . . ?
O8 Dy2 O12 71.81(9) . 1_565 ?
O2 P3 C35 112.83(17) . . ?
O2 P3 C41 111.45(18) . . ?
O2 P3 C29 109.23(17) . . ?
C35 P3 C41 108.9(2) . . ?
C29 P3 C35 106.61(19) . . ?
C29 P3 C41 107.6(2) . . ?
O16 P2 C11 110.47(17) . . ?
O16 P2 C17 108.97(17) . . ?
O16 P2 C23 108.56(17) . . ?
C11 P2 C17 111.49(19) . . ?
C11 P2 C23 108.71(19) . . ?
C17 P2 C23 108.57(19) . . ?
O15 P1 C47 109.9(2) . . ?
O15 P1 C53 107.4(2) . . ?
O15 P1 C59 111.3(2) . . ?
C47 P1 C53 114.0(3) . . ?
C47 P1 C59 108.3(2) . . ?
C53 P1 C59 106.0(2) . . ?
O8 P4 C71 111.86(18) . . ?
O8 P4 C65 110.48(19) . . ?
O8 P4 C77 111.1(2) . . ?
C71 P4 C77 107.6(3) . . ?
C65 P4 C71 107.7(2) . . ?
C65 P4 C77 108.0(3) . . ?
Dy1 O1 H1A 125.3 . . ?
Dy1 O1 H1B 127.8 . . ?
H1A O1 H1B 104.5 . . ?
P2 O16 Dy1 179.67(17) . . ?
Dy2 O7 H7A 109.5 . . ?
Dy2 O7 H7B 109.3 . . ?
H7A O7 H7B 104.3 . . ?
C6 O5 Dy1 154.9(2) . . ?
C1 O3 Dy1 115.6(2) . . ?
C7 O11 Dy2 115.5(2) . 1_545 ?
P1 O15 Dy2 167.92(19) . . ?
P3 O2 Dy1 165.30(17) . . ?
C3 O6 Dy2 154.3(2) . . ?
C8 O12 Dy2 115.1(2) . 1_545 ?
C2 O4 Dy1 115.0(2) . . ?
P4 O8 Dy2 154.73(17) . . ?
C84 O17 H17A 109.5 . . ?
O10 C5 C1 128.9(3) . . ?
O10 C5 C4 126.1(3) . . ?
C1 C5 C4 104.9(3) . . ?
O3 C1 C5 129.2(3) . . ?
O3 C1 C2 121.6(3) . . ?
C2 C1 C5 109.2(3) . . ?
O9 C4 C5 123.7(3) . . ?
O9 C4 C3 127.2(3) . . ?
C3 C4 C5 109.0(3) . . ?
P2 C11 H11 106.4 . . ?
C12 C11 P2 112.7(3) . . ?
C12 C11 H11 106.4 . . ?
C16 C11 P2 114.3(3) . . ?
C16 C11 H11 106.4 . . ?
C16 C11 C12 110.2(3) . . ?
O6 C3 C4 125.3(3) . . ?
O6 C3 C2 128.2(3) . . ?
C2 C3 C4 106.5(3) . . ?
O13 C9 C8 128.2(4) . . ?
O13 C9 C10 126.1(4) . . ?
C8 C9 C10 105.7(3) . . ?
O5 C6 C7 128.1(3) . . ?
O5 C6 C10 126.0(3) . . ?
C7 C6 C10 105.9(3) . . ?
O11 C7 C6 129.9(3) . . ?
O11 C7 C8 119.0(3) . . ?
C6 C7 C8 111.0(3) . . ?
P2 C17 H17 108.8 . . ?
C18 C17 P2 111.1(3) . . ?
C18 C17 H17 108.8 . . ?
C18 C17 C22 109.5(4) . . ?
C22 C17 P2 109.8(3) . . ?
C22 C17 H17 108.8 . . ?
C11 C12 H12A 109.8 . . ?
C11 C12 H12B 109.8 . . ?
H12A C12 H12B 108.2 . . ?
C13 C12 C11 109.4(3) . . ?
C13 C12 H12A 109.8 . . ?
C13 C12 H12B 109.8 . . ?
P2 C23 H23 106.5 . . ?
C24 C23 P2 110.5(3) . . ?
C24 C23 H23 106.5 . . ?
C28 C23 P2 115.1(3) . . ?
C28 C23 H23 106.5 . . ?
C28 C23 C24 111.4(4) . . ?
O4 C2 C1 119.6(3) . . ?
O4 C2 C3 130.2(3) . . ?
C3 C2 C1 110.1(3) . . ?
O12 C8 C9 129.4(3) . . ?
O12 C8 C7 122.0(3) . . ?
C7 C8 C9 108.5(3) . . ?
C12 C13 H13A 109.3 . . ?
C12 C13 H13B 109.3 . . ?
H13A C13 H13B 108.0 . . ?
C14 C13 C12 111.5(4) . . ?
C14 C13 H13A 109.3 . . ?
C14 C13 H13B 109.3 . . ?
C11 C16 H16A 109.7 . . ?
C11 C16 H16B 109.7 . . ?
H16A C16 H16B 108.2 . . ?
C15 C16 C11 110.0(3) . . ?
C15 C16 H16A 109.7 . . ?
C15 C16 H16B 109.7 . . ?
P4 C71 H71 107.7 . . ?
C72 C71 P4 113.3(3) . . ?
C72 C71 H71 107.7 . . ?
C76 C71 P4 109.5(3) . . ?
C76 C71 H71 107.7 . . ?
C76 C71 C72 110.7(4) . . ?
P3 C35 H35 107.1 . . ?
C36 C35 P3 113.2(3) . . ?
C36 C35 H35 107.1 . . ?
C36 C35 C40 110.3(3) . . ?
C40 C35 P3 111.6(3) . . ?
C40 C35 H35 107.1 . . ?
P4 C65 H65 106.1 . . ?
C66 C65 P4 113.6(3) . . ?
C66 C65 H65 106.1 . . ?
C66 C65 C70 109.6(4) . . ?
C70 C65 P4 114.7(4) . . ?
C70 C65 H65 106.1 . . ?
H73A C73 H73B 107.9 . . ?
C72 C73 H73A 109.2 . . ?
C72 C73 H73B 109.2 . . ?
C74 C73 H73A 109.2 . . ?
C74 C73 H73B 109.2 . . ?
C74 C73 C72 112.1(4) . . ?
C23 C24 H24A 109.6 . . ?
C23 C24 H24B 109.6 . . ?
H24A C24 H24B 108.1 . . ?
C25 C24 C23 110.5(4) . . ?
C25 C24 H24A 109.6 . . ?
C25 C24 H24B 109.6 . . ?
C35 C36 H36A 109.4 . . ?
C35 C36 H36B 109.4 . . ?
C35 C36 C37 111.2(4) . . ?
H36A C36 H36B 108.0 . . ?
C37 C36 H36A 109.4 . . ?
C37 C36 H36B 109.4 . . ?
C17 C18 H18A 109.2 . . ?
C17 C18 H18B 109.2 . . ?
H18A C18 H18B 107.9 . . ?
C19 C18 C17 112.1(3) . . ?
C19 C18 H18A 109.2 . . ?
C19 C18 H18B 109.2 . . ?
C16 C15 H15A 109.6 . . ?
C16 C15 H15B 109.6 . . ?
H15A C15 H15B 108.1 . . ?
C14 C15 C16 110.4(4) . . ?
C14 C15 H15A 109.6 . . ?
C14 C15 H15B 109.6 . . ?
C13 C14 C15 111.8(4) . . ?
C13 C14 H14A 109.3 . . ?
C13 C14 H14B 109.3 . . ?
C15 C14 H14A 109.3 . . ?
C15 C14 H14B 109.3 . . ?
H14A C14 H14B 107.9 . . ?
P3 C41 H41 105.9 . . ?
C42 C41 P3 113.2(3) . . ?
C42 C41 H41 105.9 . . ?
C42 C41 C46 109.9(4) . . ?
C46 C41 P3 115.3(3) . . ?
C46 C41 H41 105.9 . . ?
C17 C22 H22A 109.1 . . ?
C17 C22 H22B 109.1 . . ?
H22A C22 H22B 107.9 . . ?
C21 C22 C17 112.4(4) . . ?
C21 C22 H22A 109.1 . . ?
C21 C22 H22B 109.1 . . ?
C71 C72 H72A 109.5 . . ?
C71 C72 H72B 109.5 . . ?
C73 C72 C71 110.8(4) . . ?
C73 C72 H72A 109.5 . . ?
C73 C72 H72B 109.5 . . ?
H72A C72 H72B 108.1 . . ?
O14 C10 C9 124.4(4) . . ?
O14 C10 C6 126.7(4) . . ?
C9 C10 C6 108.8(3) . . ?
C22 C21 H21A 109.3 . . ?
C22 C21 H21B 109.3 . . ?
H21A C21 H21B 108.0 . . ?
C20 C21 C22 111.6(4) . . ?
C20 C21 H21A 109.3 . . ?
C20 C21 H21B 109.3 . . ?
P3 C29 H29 106.3 . . ?
C30 C29 P3 112.2(3) . . ?
C30 C29 H29 106.3 . . ?
C30 C29 C34 109.9(3) . . ?
C34 C29 P3 115.1(3) . . ?
C34 C29 H29 106.3 . . ?
C35 C40 H40A 109.2 . . ?
C35 C40 H40B 109.2 . . ?
H40A C40 H40B 107.9 . . ?
C39 C40 C35 111.9(4) . . ?
C39 C40 H40A 109.2 . . ?
C39 C40 H40B 109.2 . . ?
C65 C66 H66A 109.2 . . ?
C65 C66 H66B 109.2 . . ?
H66A C66 H66B 107.9 . . ?
C67 C66 C65 112.1(4) . . ?
C67 C66 H66A 109.2 . . ?
C67 C66 H66B 109.2 . . ?
P1 C47 H47 105.4 . . ?
C48 C47 P1 114.7(4) . . ?
C48 C47 H47 105.4 . . ?
C48 C47 C52 109.9(5) . . ?
C52 C47 P1 115.0(4) . . ?
C52 C47 H47 105.4 . . ?
C29 C30 H30A 109.4 . . ?
C29 C30 H30B 109.4 . . ?
H30A C30 H30B 108.0 . . ?
C31 C30 C29 111.3(3) . . ?
C31 C30 H30A 109.4 . . ?
C31 C30 H30B 109.4 . . ?
C21 C20 H20A 109.6 . . ?
C21 C20 H20B 109.6 . . ?
C21 C20 C19 110.2(4) . . ?
H20A C20 H20B 108.1 . . ?
C19 C20 H20A 109.6 . . ?
C19 C20 H20B 109.6 . . ?
C24 C25 H25A 109.3 . . ?
C24 C25 H25B 109.3 . . ?
H25A C25 H25B 108.0 . . ?
C26 C25 C24 111.4(4) . . ?
C26 C25 H25A 109.3 . . ?
C26 C25 H25B 109.3 . . ?
P1 C53 H53 104.2 . . ?
C54 C53 P1 112.6(3) . . ?
C54 C53 H53 104.2 . . ?
C58 C53 P1 118.3(4) . . ?
C58 C53 H53 104.2 . . ?
C58 C53 C54 111.6(4) . . ?
C18 C19 H19A 109.2 . . ?
C18 C19 H19B 109.2 . . ?
C20 C19 C18 112.2(4) . . ?
C20 C19 H19A 109.2 . . ?
C20 C19 H19B 109.2 . . ?
H19A C19 H19B 107.9 . . ?
C29 C34 H34A 109.4 . . ?
C29 C34 H34B 109.4 . . ?
H34A C34 H34B 108.0 . . ?
C33 C34 C29 111.0(4) . . ?
C33 C34 H34A 109.4 . . ?
C33 C34 H34B 109.4 . . ?
C73 C74 H74A 109.7 . . ?
C73 C74 H74B 109.7 . . ?
C73 C74 C75 109.9(4) . . ?
H74A C74 H74B 108.2 . . ?
C75 C74 H74A 109.7 . . ?
C75 C74 H74B 109.7 . . ?
C41 C42 H42A 109.8 . . ?
C41 C42 H42B 109.8 . . ?
H42A C42 H42B 108.2 . . ?
C43 C42 C41 109.5(5) . . ?
C43 C42 H42A 109.8 . . ?
C43 C42 H42B 109.8 . . ?
C25 C26 H26A 109.6 . . ?
C25 C26 H26B 109.6 . . ?
C25 C26 C27 110.5(4) . . ?
H26A C26 H26B 108.1 . . ?
C27 C26 H26A 109.6 . . ?
C27 C26 H26B 109.6 . . ?
C71 C76 H76A 109.5 . . ?
C71 C76 H76B 109.5 . . ?
H76A C76 H76B 108.1 . . ?
C75 C76 C71 110.5(4) . . ?
C75 C76 H76A 109.5 . . ?
C75 C76 H76B 109.5 . . ?
C23 C28 H28A 109.5 . . ?
C23 C28 H28B 109.5 . . ?
H28A C28 H28B 108.1 . . ?
C27 C28 C23 110.7(4) . . ?
C27 C28 H28A 109.5 . . ?
C27 C28 H28B 109.5 . . ?
C74 C75 H75A 109.1 . . ?
C74 C75 H75B 109.1 . . ?
C76 C75 C74 112.4(4) . . ?
C76 C75 H75A 109.1 . . ?
C76 C75 H75B 109.1 . . ?
H75A C75 H75B 107.9 . . ?
C36 C37 H37A 109.2 . . ?
C36 C37 H37B 109.2 . . ?
H37A C37 H37B 107.9 . . ?
C38 C37 C36 111.8(4) . . ?
C38 C37 H37A 109.2 . . ?
C38 C37 H37B 109.2 . . ?
C65 C70 H70A 109.4 . . ?
C65 C70 H70B 109.4 . . ?
H70A C70 H70B 108.0 . . ?
C69 C70 C65 111.1(4) . . ?
C69 C70 H70A 109.4 . . ?
C69 C70 H70B 109.4 . . ?
H68A C68 H68B 108.1 . . ?
C69 C68 H68A 109.5 . . ?
C69 C68 H68B 109.5 . . ?
C69 C68 C67 110.6(4) . . ?
C67 C68 H68A 109.5 . . ?
C67 C68 H68B 109.5 . . ?
C40 C39 H39A 109.4 . . ?
C40 C39 H39B 109.4 . . ?
H39A C39 H39B 108.0 . . ?
C38 C39 C40 111.3(4) . . ?
C38 C39 H39A 109.4 . . ?
C38 C39 H39B 109.4 . . ?
H49A C49 H49B 108.2 . . ?
C48 C49 H49A 109.8 . . ?
C48 C49 H49B 109.8 . . ?
C50 C49 H49A 109.8 . . ?
C50 C49 H49B 109.8 . . ?
C50 C49 C48 109.4(5) . . ?
C30 C31 H31A 109.4 . . ?
C30 C31 H31B 109.4 . . ?
H31A C31 H31B 108.0 . . ?
C32 C31 C30 111.3(4) . . ?
C32 C31 H31A 109.4 . . ?
C32 C31 H31B 109.4 . . ?
P1 C59 H59 107.4 . . ?
C64 C59 P1 114.7(3) . . ?
C64 C59 H59 107.4 . . ?
C64 C59 C60 109.8(4) . . ?
C60 C59 P1 109.9(3) . . ?
C60 C59 H59 107.4 . . ?
C26 C27 H27A 109.4 . . ?
C26 C27 H27B 109.4 . . ?
C28 C27 C26 111.3(5) . . ?
C28 C27 H27A 109.4 . . ?
C28 C27 H27B 109.4 . . ?
H27A C27 H27B 108.0 . . ?
C53 C54 H54A 109.6 . . ?
C53 C54 H54B 109.6 . . ?
C53 C54 C55 110.3(5) . . ?
H54A C54 H54B 108.1 . . ?
C55 C54 H54A 109.6 . . ?
C55 C54 H54B 109.6 . . ?
C37 C38 C39 111.5(4) . . ?
C37 C38 H38A 109.3 . . ?
C37 C38 H38B 109.3 . . ?
C39 C38 H38A 109.3 . . ?
C39 C38 H38B 109.3 . . ?
H38A C38 H38B 108.0 . . ?
C41 C46 H46A 109.8 . . ?
C41 C46 H46B 109.8 . . ?
H46A C46 H46B 108.3 . . ?
C45 C46 C41 109.3(4) . . ?
C45 C46 H46A 109.8 . . ?
C45 C46 H46B 109.8 . . ?
C34 C33 H33A 109.4 . . ?
C34 C33 H33B 109.4 . . ?
C34 C33 C32 111.0(5) . . ?
H33A C33 H33B 108.0 . . ?
C32 C33 H33A 109.4 . . ?
C32 C33 H33B 109.4 . . ?
C59 C64 H64A 109.3 . . ?
C59 C64 H64B 109.3 . . ?
C59 C64 C63 111.5(4) . . ?
H64A C64 H64B 108.0 . . ?
C63 C64 H64A 109.3 . . ?
C63 C64 H64B 109.3 . . ?
C70 C69 H69A 109.4 . . ?
C70 C69 H69B 109.4 . . ?
C68 C69 C70 111.4(4) . . ?
C68 C69 H69A 109.4 . . ?
C68 C69 H69B 109.4 . . ?
H69A C69 H69B 108.0 . . ?
H57A C57 H57B 107.8 . . ?
C58 C57 H57A 109.1 . . ?
C58 C57 H57B 109.1 . . ?
C56 C57 H57A 109.1 . . ?
C56 C57 H57B 109.1 . . ?
C56 C57 C58 112.6(5) . . ?
C47 C48 C49 109.1(5) . . ?
C47 C48 H48A 109.9 . . ?
C47 C48 H48B 109.9 . . ?
C49 C48 H48A 109.9 . . ?
C49 C48 H48B 109.9 . . ?
H48A C48 H48B 108.3 . . ?
C59 C60 H60A 109.4 . . ?
C59 C60 H60B 109.4 . . ?
H60A C60 H60B 108.0 . . ?
C61 C60 C59 111.4(4) . . ?
C61 C60 H60A 109.4 . . ?
C61 C60 H60B 109.4 . . ?
H62A C62 H62B 108.0 . . ?
C63 C62 H62A 109.4 . . ?
C63 C62 H62B 109.4 . . ?
C63 C62 C61 111.3(5) . . ?
C61 C62 H62A 109.4 . . ?
C61 C62 H62B 109.4 . . ?
C31 C32 H32A 109.5 . . ?
C31 C32 H32B 109.5 . . ?
C33 C32 C31 110.8(4) . . ?
C33 C32 H32A 109.5 . . ?
C33 C32 H32B 109.5 . . ?
H32A C32 H32B 108.1 . . ?
C66 C67 C68 111.3(4) . . ?
C66 C67 H67A 109.4 . . ?
C66 C67 H67B 109.4 . . ?
C68 C67 H67A 109.4 . . ?
C68 C67 H67B 109.4 . . ?
H67A C67 H67B 108.0 . . ?
C64 C63 H63A 109.3 . . ?
C64 C63 H63B 109.3 . . ?
C62 C63 C64 111.7(5) . . ?
C62 C63 H63A 109.3 . . ?
C62 C63 H63B 109.3 . . ?
H63A C63 H63B 107.9 . . ?
C53 C58 C57 110.9(5) . . ?
C53 C58 H58A 109.5 . . ?
C53 C58 H58B 109.5 . . ?
C57 C58 H58A 109.5 . . ?
C57 C58 H58B 109.5 . . ?
H58A C58 H58B 108.0 . . ?
O17 C84 H84A 109.5 . . ?
O17 C84 H84B 109.5 . . ?
O17 C84 H84C 109.5 . . ?
H84A C84 H84B 109.5 . . ?
H84A C84 H84C 109.5 . . ?
H84B C84 H84C 109.5 . . ?
C47 C52 H52A 110.0 . . ?
C47 C52 H52B 110.0 . . ?
H52A C52 H52B 108.4 . . ?
C51 C52 C47 108.5(5) . . ?
C51 C52 H52A 110.0 . . ?
C51 C52 H52B 110.0 . . ?
C60 C61 H61A 109.5 . . ?
C60 C61 H61B 109.5 . . ?
C62 C61 C60 110.9(5) . . ?
C62 C61 H61A 109.5 . . ?
C62 C61 H61B 109.5 . . ?
H61A C61 H61B 108.0 . . ?
H78C C78 H78D 107.8 . . ?
H78A C78 H78B 108.1 . . ?
C77 C78 H78C 109.0 . . ?
C77 C78 H78D 109.0 . . ?
C77 C78 H78A 109.5 . . ?
C77 C78 H78B 109.5 . . ?
C77 C78 C79A 110.8(7) . . ?
C79 C78 H78C 109.0 . . ?
C79 C78 H78D 109.0 . . ?
C79 C78 C77 112.9(6) . . ?
C79A C78 H78A 109.5 . . ?
C79A C78 H78B 109.5 . . ?
C46 C45 H45A 109.1 . . ?
C46 C45 H45B 109.1 . . ?
H45A C45 H45B 107.8 . . ?
C44 C45 C46 112.7(6) . . ?
C44 C45 H45A 109.1 . . ?
C44 C45 H45B 109.1 . . ?
H81C C81 H81D 108.4 . . ?
H81A C81 H81B 108.8 . . ?
C80 C81 H81C 110.1 . . ?
C80 C81 H81D 110.1 . . ?
C82A C81 H81A 110.8 . . ?
C82A C81 H81B 110.8 . . ?
C82 C81 H81C 110.1 . . ?
C82 C81 H81D 110.1 . . ?
C82 C81 C80 108.1(6) . . ?
C80A C81 H81A 110.8 . . ?
C80A C81 H81B 110.8 . . ?
C80A C81 C82A 104.9(11) . . ?
C42 C43 H43A 109.3 . . ?
C42 C43 H43B 109.3 . . ?
C42 C43 C44 111.7(5) . . ?
H43A C43 H43B 107.9 . . ?
C44 C43 H43A 109.3 . . ?
C44 C43 H43B 109.3 . . ?
C45 C44 C43 111.3(6) . . ?
C45 C44 H44A 109.4 . . ?
C45 C44 H44B 109.4 . . ?
C43 C44 H44A 109.4 . . ?
C43 C44 H44B 109.4 . . ?
H44A C44 H44B 108.0 . . ?
C54 C55 H55A 108.9 . . ?
C54 C55 H55B 108.9 . . ?
H55A C55 H55B 107.7 . . ?
C56 C55 C54 113.3(5) . . ?
C56 C55 H55A 108.9 . . ?
C56 C55 H55B 108.9 . . ?
C57 C56 H56A 109.1 . . ?
C57 C56 H56B 109.1 . . ?
C55 C56 C57 112.4(5) . . ?
C55 C56 H56A 109.1 . . ?
C55 C56 H56B 109.1 . . ?
H56A C56 H56B 107.8 . . ?
C49 C50 H50A 109.3 . . ?
C49 C50 H50B 109.3 . . ?
H50A C50 H50B 108.0 . . ?
C51 C50 C49 111.4(6) . . ?
C51 C50 H50A 109.3 . . ?
C51 C50 H50B 109.3 . . ?
P4 C77 H77 95.8 . . ?
P4 C77 H77A 100.3 . . ?
C78 C77 P4 116.6(4) . . ?
C78 C77 H77 95.8 . . ?
C78 C77 H77A 100.3 . . ?
C82A C77 P4 121.8(9) . . ?
C82A C77 C78 118.5(9) . . ?
C82A C77 H77 95.8 . . ?
C82 C77 P4 118.6(5) . . ?
C82 C77 C78 115.5(6) . . ?
C82 C77 H77A 100.3 . . ?
C52 C51 H51A 109.3 . . ?
C52 C51 H51B 109.3 . . ?
C50 C51 C52 111.6(7) . . ?
C50 C51 H51A 109.3 . . ?
C50 C51 H51B 109.3 . . ?
H51A C51 H51B 108.0 . . ?
C81 C80 H80A 109.9 . . ?
C81 C80 H80B 109.9 . . ?
H80A C80 H80B 108.3 . . ?
C79 C80 C81 109.0(8) . . ?
C79 C80 H80A 109.9 . . ?
C79 C80 H80B 109.9 . . ?
C78 C79 H79A 110.0 . . ?
C78 C79 H79B 110.0 . . ?
C80 C79 C78 108.3(8) . . ?
C80 C79 H79A 110.0 . . ?
C80 C79 H79B 110.0 . . ?
H79A C79 H79B 108.4 . . ?
H83A C83 H83B 109.5 . . ?
H83A C83 H83C 109.5 . . ?
H83B C83 H83C 109.4 . . ?
O18 C83 H83A 110.2 . . ?
O18 C83 H83B 108.2 . . ?
O18 C83 H83C 110.0 . . ?
C83 O18 H18 109.5 . . ?
C81 C82A H82A 109.5 . . ?
C81 C82A H82B 109.5 . . ?
C77 C82A C81 110.9(11) . . ?
C77 C82A H82A 109.5 . . ?
C77 C82A H82B 109.5 . . ?
H82A C82A H82B 108.0 . . ?
C81 C82 H82C 108.7 . . ?
C81 C82 H82D 108.7 . . ?
C77 C82 C81 114.3(6) . . ?
C77 C82 H82C 108.7 . . ?
C77 C82 H82D 108.7 . . ?
H82C C82 H82D 107.6 . . ?
C81 C80A H80C 110.8 . . ?
C81 C80A H80D 110.8 . . ?
C81 C80A C79A 105.0(11) . . ?
H80C C80A H80D 108.8 . . ?
C79A C80A H80C 110.8 . . ?
C79A C80A H80D 110.8 . . ?
C78 C79A H79C 110.4 . . ?
C78 C79A H79D 110.4 . . ?
C80A C79A C78 106.7(12) . . ?
C80A C79A H79C 110.4 . . ?
C80A C79A H79D 110.4 . . ?
H79C C79A H79D 108.6 . . ?
C83A O18A H18C 109.5 . . ?
O18A C83A H83D 109.5 . . ?
O18A C83A H83E 109.5 . . ?
O18A C83A H83F 109.5 . . ?
H83D C83A H83E 109.5 . . ?
H83D C83A H83F 109.5 . . ?
H83E C83A H83F 109.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Dy1 O5 C6 C7 18.2(8) . . . . ?
Dy1 O5 C6 C10 -161.6(4) . . . . ?
Dy1 O3 C1 C5 174.7(3) . . . . ?
Dy1 O3 C1 C2 -4.7(5) . . . . ?
Dy1 O4 C2 C1 5.1(4) . . . . ?
Dy1 O4 C2 C3 -175.4(3) . . . . ?
Dy2 O11 C7 C6 174.0(3) 1_545 . . . ?
Dy2 O11 C7 C8 -4.5(4) 1_545 . . . ?
Dy2 O6 C3 C4 159.4(4) . . . . ?
Dy2 O6 C3 C2 -21.8(8) . . . . ?
Dy2 O12 C8 C9 -174.7(3) 1_545 . . . ?
Dy2 O12 C8 C7 3.7(5) 1_545 . . . ?
P3 C35 C36 C37 -179.2(3) . . . . ?
P3 C35 C40 C39 177.6(3) . . . . ?
P3 C41 C42 C43 169.5(4) . . . . ?
P3 C41 C46 C45 -171.6(4) . . . . ?
P3 C29 C30 C31 175.1(3) . . . . ?
P3 C29 C34 C33 -175.5(4) . . . . ?
P2 C11 C12 C13 -172.8(3) . . . . ?
P2 C11 C16 C15 172.6(3) . . . . ?
P2 C17 C18 C19 173.8(3) . . . . ?
P2 C17 C22 C21 -175.6(3) . . . . ?
P2 C23 C24 C25 -175.6(3) . . . . ?
P2 C23 C28 C27 178.2(4) . . . . ?
P1 C47 C48 C49 166.3(4) . . . . ?
P1 C47 C52 C51 -168.9(6) . . . . ?
P1 C53 C54 C55 -169.0(4) . . . . ?
P1 C53 C58 C57 171.3(4) . . . . ?
P1 C59 C64 C63 178.8(4) . . . . ?
P1 C59 C60 C61 177.7(4) . . . . ?
P4 C71 C72 C73 178.2(3) . . . . ?
P4 C71 C76 C75 178.9(3) . . . . ?
P4 C65 C66 C67 175.4(3) . . . . ?
P4 C65 C70 C69 -175.3(4) . . . . ?
P4 C77 C82A C81 -151.6(8) . . . . ?
P4 C77 C82 C81 167.7(5) . . . . ?
O16 P2 C11 C12 30.4(3) . . . . ?
O16 P2 C11 C16 157.3(3) . . . . ?
O16 P2 C17 C18 -60.0(3) . . . . ?
O16 P2 C17 C22 61.3(3) . . . . ?
O16 P2 C23 C24 49.3(3) . . . . ?
O16 P2 C23 C28 176.5(3) . . . . ?
O10 C5 C1 O3 2.3(7) . . . . ?
O10 C5 C1 C2 -178.3(4) . . . . ?
O10 C5 C4 O9 -4.1(7) . . . . ?
O10 C5 C4 C3 176.5(4) . . . . ?
O5 C6 C7 O11 0.2(7) . . . . ?
O5 C6 C7 C8 178.8(4) . . . . ?
O5 C6 C10 O14 0.6(7) . . . . ?
O5 C6 C10 C9 -178.4(4) . . . . ?
O3 C1 C2 O4 -0.4(6) . . . . ?
O3 C1 C2 C3 -179.9(3) . . . . ?
O11 C7 C8 O12 0.6(6) . . . . ?
O11 C7 C8 C9 179.2(3) . . . . ?
O15 P1 C47 C48 -41.5(5) . . . . ?
O15 P1 C47 C52 -170.4(5) . . . . ?
O15 P1 C53 C54 65.4(4) . . . . ?
O15 P1 C53 C58 -162.0(4) . . . . ?
O15 P1 C59 C64 -67.7(4) . . . . ?
O15 P1 C59 C60 56.6(4) . . . . ?
O2 P3 C35 C36 -69.9(3) . . . . ?
O2 P3 C35 C40 55.3(3) . . . . ?
O2 P3 C41 C42 -29.9(4) . . . . ?
O2 P3 C41 C46 -157.7(3) . . . . ?
O2 P3 C29 C30 -53.7(3) . . . . ?
O2 P3 C29 C34 179.5(3) . . . . ?
O6 C3 C2 O4 -1.4(7) . . . . ?
O6 C3 C2 C1 178.1(4) . . . . ?
O9 C4 C3 O6 3.8(6) . . . . ?
O9 C4 C3 C2 -175.3(4) . . . . ?
O8 P4 C71 C72 -69.0(3) . . . . ?
O8 P4 C71 C76 55.1(3) . . . . ?
O8 P4 C65 C66 -51.8(3) . . . . ?
O8 P4 C65 C70 -179.0(3) . . . . ?
O8 P4 C77 C78 -158.1(5) . . . . ?
O8 P4 C77 C82A 41.9(12) . . . . ?
O8 P4 C77 C82 -12.9(7) . . . . ?
O13 C9 C8 O12 0.1(7) . . . . ?
O13 C9 C8 C7 -178.4(4) . . . . ?
O13 C9 C10 O14 -1.4(7) . . . . ?
O13 C9 C10 C6 177.6(4) . . . . ?
C5 C1 C2 O4 -179.8(3) . . . . ?
C5 C1 C2 C3 0.6(4) . . . . ?
C5 C4 C3 O6 -176.9(4) . . . . ?
C5 C4 C3 C2 4.0(4) . . . . ?
C1 C5 C4 O9 175.7(4) . . . . ?
C1 C5 C4 C3 -3.6(4) . . . . ?
C4 C5 C1 O3 -177.5(4) . . . . ?
C4 C5 C1 C2 1.9(4) . . . . ?
C4 C3 C2 O4 177.6(4) . . . . ?
C4 C3 C2 C1 -2.8(4) . . . . ?
C11 P2 C17 C18 62.2(3) . . . . ?
C11 P2 C17 C22 -176.5(3) . . . . ?
C11 P2 C23 C24 -70.9(3) . . . . ?
C11 P2 C23 C28 56.3(4) . . . . ?
C11 C12 C13 C14 -56.2(5) . . . . ?
C11 C16 C15 C14 57.7(5) . . . . ?
C6 C7 C8 O12 -178.2(3) . . . . ?
C6 C7 C8 C9 0.5(4) . . . . ?
C7 C6 C10 O14 -179.3(4) . . . . ?
C7 C6 C10 C9 1.7(4) . . . . ?
C17 P2 C11 C12 -90.9(3) . . . . ?
C17 P2 C11 C16 35.9(4) . . . . ?
C17 P2 C23 C24 167.6(3) . . . . ?
C17 P2 C23 C28 -65.2(4) . . . . ?
C17 C18 C19 C20 -55.1(5) . . . . ?
C17 C22 C21 C20 56.7(5) . . . . ?
C12 C11 C16 C15 -59.3(5) . . . . ?
C12 C13 C14 C15 55.9(5) . . . . ?
C23 P2 C11 C12 149.5(3) . . . . ?
C23 P2 C11 C16 -83.7(3) . . . . ?
C23 P2 C17 C18 -178.1(3) . . . . ?
C23 P2 C17 C22 -56.7(3) . . . . ?
C23 C24 C25 C26 -56.5(6) . . . . ?
C23 C28 C27 C26 55.8(6) . . . . ?
C8 C9 C10 O14 179.6(4) . . . . ?
C8 C9 C10 C6 -1.4(4) . . . . ?
C16 C11 C12 C13 58.2(5) . . . . ?
C16 C15 C14 C13 -56.0(5) . . . . ?
C71 P4 O8 Dy2 69.3(5) . . . . ?
C71 P4 C65 C66 -174.2(3) . . . . ?
C71 P4 C65 C70 58.6(4) . . . . ?
C71 P4 C77 C78 -35.3(6) . . . . ?
C71 P4 C77 C82A 164.7(11) . . . . ?
C71 P4 C77 C82 109.9(6) . . . . ?
C71 C76 C75 C74 57.0(5) . . . . ?
C35 P3 O2 Dy1 -27.6(7) . . . . ?
C35 P3 C41 C42 95.2(4) . . . . ?
C35 P3 C41 C46 -32.6(4) . . . . ?
C35 P3 C29 C30 -175.9(3) . . . . ?
C35 P3 C29 C34 57.3(4) . . . . ?
C35 C36 C37 C38 -55.1(5) . . . . ?
C35 C40 C39 C38 55.6(5) . . . . ?
C65 P4 O8 Dy2 -50.7(5) . . . . ?
C65 P4 C71 C72 52.6(3) . . . . ?
C65 P4 C71 C76 176.6(3) . . . . ?
C65 P4 C77 C78 80.7(6) . . . . ?
C65 P4 C77 C82A -79.4(11) . . . . ?
C65 P4 C77 C82 -134.2(6) . . . . ?
C65 C66 C67 C68 55.4(5) . . . . ?
C65 C70 C69 C68 -57.7(5) . . . . ?
C73 C74 C75 C76 -56.8(5) . . . . ?
C24 C23 C28 C27 -55.1(6) . . . . ?
C24 C25 C26 C27 57.3(6) . . . . ?
C36 C35 C40 C39 -55.7(5) . . . . ?
C36 C37 C38 C39 54.7(5) . . . . ?
C18 C17 C22 C21 -53.4(5) . . . . ?
C41 P3 O2 Dy1 95.3(7) . . . . ?
C41 P3 C35 C36 165.9(3) . . . . ?
C41 P3 C35 C40 -69.0(3) . . . . ?
C41 P3 C29 C30 67.4(3) . . . . ?
C41 P3 C29 C34 -59.3(4) . . . . ?
C41 C42 C43 C44 57.2(8) . . . . ?
C41 C46 C45 C44 -56.3(7) . . . . ?
C22 C17 C18 C19 52.3(5) . . . . ?
C22 C21 C20 C19 -56.9(5) . . . . ?
C72 C71 C76 C75 -55.5(5) . . . . ?
C72 C73 C74 C75 55.7(5) . . . . ?
C10 C9 C8 O12 179.1(4) . . . . ?
C10 C9 C8 C7 0.6(4) . . . . ?
C10 C6 C7 O11 -179.9(4) . . . . ?
C10 C6 C7 C8 -1.4(4) . . . . ?
C21 C20 C19 C18 56.3(5) . . . . ?
C29 P3 O2 Dy1 -145.9(6) . . . . ?
C29 P3 C35 C36 50.1(3) . . . . ?
C29 P3 C35 C40 175.2(3) . . . . ?
C29 P3 C41 C42 -149.6(3) . . . . ?
C29 P3 C41 C46 82.6(4) . . . . ?
C29 C30 C31 C32 55.5(5) . . . . ?
C29 C34 C33 C32 -57.8(6) . . . . ?
C40 C35 C36 C37 54.9(4) . . . . ?
C40 C39 C38 C37 -54.8(5) . . . . ?
C66 C65 C70 C69 55.5(5) . . . . ?
C47 P1 O15 Dy2 4.0(11) . . . . ?
C47 P1 C53 C54 -56.6(5) . . . . ?
C47 P1 C53 C58 76.0(5) . . . . ?
C47 P1 C59 C64 53.2(4) . . . . ?
C47 P1 C59 C60 177.5(4) . . . . ?
C47 C52 C51 C50 -56.0(10) . . . . ?
C30 C29 C34 C33 56.6(5) . . . . ?
C30 C31 C32 C33 -55.8(7) . . . . ?
C25 C26 C27 C28 -57.0(6) . . . . ?
C53 P1 O15 Dy2 -120.5(10) . . . . ?
C53 P1 C47 C48 79.1(5) . . . . ?
C53 P1 C47 C52 -49.8(6) . . . . ?
C53 P1 C59 C64 175.9(4) . . . . ?
C53 P1 C59 C60 -59.8(4) . . . . ?
C53 C54 C55 C56 -53.7(8) . . . . ?
C34 C29 C30 C31 -55.4(5) . . . . ?
C34 C33 C32 C31 57.0(7) . . . . ?
C74 C73 C72 C71 -55.6(5) . . . . ?
C42 C41 C46 C45 59.0(6) . . . . ?
C42 C43 C44 C45 -54.0(9) . . . . ?
C76 C71 C72 C73 54.7(5) . . . . ?
C28 C23 C24 C25 55.2(5) . . . . ?
C70 C65 C66 C67 -54.8(5) . . . . ?
C49 C50 C51 C52 56.2(11) . . . . ?
C59 P1 O15 Dy2 124.0(10) . . . . ?
C59 P1 C47 C48 -163.3(4) . . . . ?
C59 P1 C47 C52 67.8(5) . . . . ?
C59 P1 C53 C54 -175.6(4) . . . . ?
C59 P1 C53 C58 -43.0(5) . . . . ?
C59 C64 C63 C62 -56.0(7) . . . . ?
C59 C60 C61 C62 56.2(7) . . . . ?
C54 C53 C58 C57 -55.6(7) . . . . ?
C54 C55 C56 C57 52.0(8) . . . . ?
C46 C41 C42 C43 -59.9(5) . . . . ?
C46 C45 C44 C43 53.7(8) . . . . ?
C64 C59 C60 C61 -55.2(6) . . . . ?
C69 C68 C67 C66 -55.8(6) . . . . ?
C48 C47 C52 C51 59.9(8) . . . . ?
C48 C49 C50 C51 -56.9(9) . . . . ?
C60 C59 C64 C63 54.5(6) . . . . ?
C67 C68 C69 C70 57.1(6) . . . . ?
C63 C62 C61 C60 -56.5(7) . . . . ?
C58 C53 C54 C55 55.2(7) . . . . ?
C58 C57 C56 C55 -51.7(8) . . . . ?
C52 C47 C48 C49 -62.3(6) . . . . ?
C61 C62 C63 C64 56.2(7) . . . . ?
C78 C77 C82A C81 48.7(15) . . . . ?
C78 C77 C82 C81 -46.8(10) . . . . ?
C81 C80 C79 C78 62.7(10) . . . . ?
C81 C80A C79A C78 -67.9(14) . . . . ?
C56 C57 C58 C53 53.3(7) . . . . ?
C50 C49 C48 C47 60.4(7) . . . . ?
C77 P4 O8 Dy2 -170.5(5) . . . . ?
C77 P4 C71 C72 168.7(3) . . . . ?
C77 P4 C71 C76 -67.2(4) . . . . ?
C77 P4 C65 C66 69.9(4) . . . . ?
C77 P4 C65 C70 -57.3(4) . . . . ?
C77 C78 C79 C80 -56.2(9) . . . . ?
C77 C78 C79A C80A 48.1(13) . . . . ?
C80 C81 C82 C77 51.6(10) . . . . ?
C79 C78 C77 P4 -165.3(6) . . . . ?
C79 C78 C77 C82 48.4(9) . . . . ?
C82A C81 C80A C79A 73.4(14) . . . . ?
C82 C81 C80 C79 -60.3(10) . . . . ?
C80A C81 C82A C77 -65.1(16) . . . . ?
C79A C78 C77 P4 156.4(8) . . . . ?
C79A C78 C77 C82A -42.9(14) . . . . ?


_olex2_submission_special_instructions 'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details 
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_oxdiff_exptl_absorpt_empirical_full_max 1.358
_oxdiff_exptl_absorpt_empirical_full_min 0.764
