# Supplementary Information (SI) for Industrial Chemistry & Materials.
# This journal is © Institute of Process Engineering of CAS 2026

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_12-16-b1_auto
_database_code_depnum_ccdc_archive 'CCDC 2523489'
loop_
_audit_author_name
_audit_author_address
'Qiao-Fei Xu'
;Xiamen University
China
;
_audit_update_record             
;
2026-01-16 deposited with the CCDC.	2026-04-16 downloaded from the CCDC.
;
_audit_creation_date             2025-03-31
_audit_creation_method           
;
Olex2 1.5
(compiled 2025.03.04 svn.red2d20d0 for OlexSys, GUI svn.r7188)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'F10 Gd0.3 K Yb2.7'
_chemical_formula_sum            'F10 Gd0.30 K Yb2.70'
_chemical_formula_weight         743.48
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Gd Gd -0.1653 3.9035 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Yb Yb -0.3850 5.5486 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      cubic
_space_group_IT_number           225
_space_group_name_H-M_alt        'F m -3 m'
_space_group_name_Hall           '-F 4 2 3'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x, z'
'-x, -y, z'
'y, -x, z'
'x, -z, y'
'x, -y, -z'
'x, z, -y'
'z, y, -x'
'-x, y, -z'
'-z, y, x'
'z, x, y'
'y, z, x'
'-y, -z, x'
'z, -x, -y'
'-y, z, -x'
'-z, -x, y'
'-z, x, -y'
'y, -z, -x'
'y, x, -z'
'-y, -x, -z'
'-x, z, y'
'-x, -z, -y'
'z, -y, x'
'-z, -y, -x'
'x, y+1/2, z+1/2'
'-y, x+1/2, z+1/2'
'-x, -y+1/2, z+1/2'
'y, -x+1/2, z+1/2'
'x, -z+1/2, y+1/2'
'x, -y+1/2, -z+1/2'
'x, z+1/2, -y+1/2'
'z, y+1/2, -x+1/2'
'-x, y+1/2, -z+1/2'
'-z, y+1/2, x+1/2'
'z, x+1/2, y+1/2'
'y, z+1/2, x+1/2'
'-y, -z+1/2, x+1/2'
'z, -x+1/2, -y+1/2'
'-y, z+1/2, -x+1/2'
'-z, -x+1/2, y+1/2'
'-z, x+1/2, -y+1/2'
'y, -z+1/2, -x+1/2'
'y, x+1/2, -z+1/2'
'-y, -x+1/2, -z+1/2'
'-x, z+1/2, y+1/2'
'-x, -z+1/2, -y+1/2'
'z, -y+1/2, x+1/2'
'-z, -y+1/2, -x+1/2'
'x+1/2, y, z+1/2'
'-y+1/2, x, z+1/2'
'-x+1/2, -y, z+1/2'
'y+1/2, -x, z+1/2'
'x+1/2, -z, y+1/2'
'x+1/2, -y, -z+1/2'
'x+1/2, z, -y+1/2'
'z+1/2, y, -x+1/2'
'-x+1/2, y, -z+1/2'
'-z+1/2, y, x+1/2'
'z+1/2, x, y+1/2'
'y+1/2, z, x+1/2'
'-y+1/2, -z, x+1/2'
'z+1/2, -x, -y+1/2'
'-y+1/2, z, -x+1/2'
'-z+1/2, -x, y+1/2'
'-z+1/2, x, -y+1/2'
'y+1/2, -z, -x+1/2'
'y+1/2, x, -z+1/2'
'-y+1/2, -x, -z+1/2'
'-x+1/2, z, y+1/2'
'-x+1/2, -z, -y+1/2'
'z+1/2, -y, x+1/2'
'-z+1/2, -y, -x+1/2'
'x+1/2, y+1/2, z'
'-y+1/2, x+1/2, z'
'-x+1/2, -y+1/2, z'
'y+1/2, -x+1/2, z'
'x+1/2, -z+1/2, y'
'x+1/2, -y+1/2, -z'
'x+1/2, z+1/2, -y'
'z+1/2, y+1/2, -x'
'-x+1/2, y+1/2, -z'
'-z+1/2, y+1/2, x'
'z+1/2, x+1/2, y'
'y+1/2, z+1/2, x'
'-y+1/2, -z+1/2, x'
'z+1/2, -x+1/2, -y'
'-y+1/2, z+1/2, -x'
'-z+1/2, -x+1/2, y'
'-z+1/2, x+1/2, -y'
'y+1/2, -z+1/2, -x'
'y+1/2, x+1/2, -z'
'-y+1/2, -x+1/2, -z'
'-x+1/2, z+1/2, y'
'-x+1/2, -z+1/2, -y'
'z+1/2, -y+1/2, x'
'-z+1/2, -y+1/2, -x'
'-x, -y, -z'
'y, -x, -z'
'x, y, -z'
'-y, x, -z'
'-x, z, -y'
'-x, y, z'
'-x, -z, y'
'-z, -y, x'
'x, -y, z'
'z, -y, -x'
'-z, -x, -y'
'-y, -z, -x'
'y, z, -x'
'-z, x, y'
'y, -z, x'
'z, x, -y'
'z, -x, y'
'-y, z, x'
'-y, -x, z'
'y, x, z'
'x, -z, -y'
'x, z, y'
'-z, y, -x'
'z, y, x'
'-x, -y+1/2, -z+1/2'
'y, -x+1/2, -z+1/2'
'x, y+1/2, -z+1/2'
'-y, x+1/2, -z+1/2'
'-x, z+1/2, -y+1/2'
'-x, y+1/2, z+1/2'
'-x, -z+1/2, y+1/2'
'-z, -y+1/2, x+1/2'
'x, -y+1/2, z+1/2'
'z, -y+1/2, -x+1/2'
'-z, -x+1/2, -y+1/2'
'-y, -z+1/2, -x+1/2'
'y, z+1/2, -x+1/2'
'-z, x+1/2, y+1/2'
'y, -z+1/2, x+1/2'
'z, x+1/2, -y+1/2'
'z, -x+1/2, y+1/2'
'-y, z+1/2, x+1/2'
'-y, -x+1/2, z+1/2'
'y, x+1/2, z+1/2'
'x, -z+1/2, -y+1/2'
'x, z+1/2, y+1/2'
'-z, y+1/2, -x+1/2'
'z, y+1/2, x+1/2'
'-x+1/2, -y, -z+1/2'
'y+1/2, -x, -z+1/2'
'x+1/2, y, -z+1/2'
'-y+1/2, x, -z+1/2'
'-x+1/2, z, -y+1/2'
'-x+1/2, y, z+1/2'
'-x+1/2, -z, y+1/2'
'-z+1/2, -y, x+1/2'
'x+1/2, -y, z+1/2'
'z+1/2, -y, -x+1/2'
'-z+1/2, -x, -y+1/2'
'-y+1/2, -z, -x+1/2'
'y+1/2, z, -x+1/2'
'-z+1/2, x, y+1/2'
'y+1/2, -z, x+1/2'
'z+1/2, x, -y+1/2'
'z+1/2, -x, y+1/2'
'-y+1/2, z, x+1/2'
'-y+1/2, -x, z+1/2'
'y+1/2, x, z+1/2'
'x+1/2, -z, -y+1/2'
'x+1/2, z, y+1/2'
'-z+1/2, y, -x+1/2'
'z+1/2, y, x+1/2'
'-x+1/2, -y+1/2, -z'
'y+1/2, -x+1/2, -z'
'x+1/2, y+1/2, -z'
'-y+1/2, x+1/2, -z'
'-x+1/2, z+1/2, -y'
'-x+1/2, y+1/2, z'
'-x+1/2, -z+1/2, y'
'-z+1/2, -y+1/2, x'
'x+1/2, -y+1/2, z'
'z+1/2, -y+1/2, -x'
'-z+1/2, -x+1/2, -y'
'-y+1/2, -z+1/2, -x'
'y+1/2, z+1/2, -x'
'-z+1/2, x+1/2, y'
'y+1/2, -z+1/2, x'
'z+1/2, x+1/2, -y'
'z+1/2, -x+1/2, y'
'-y+1/2, z+1/2, x'
'-y+1/2, -x+1/2, z'
'y+1/2, x+1/2, z'
'x+1/2, -z+1/2, -y'
'x+1/2, z+1/2, y'
'-z+1/2, y+1/2, -x'
'z+1/2, y+1/2, x'

_cell_length_a                   11.4254(3)
_cell_length_b                   11.4254(3)
_cell_length_c                   11.4254(3)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     1491.47(10)
_cell_formula_units_Z            8
_cell_measurement_reflns_used    2039
_cell_measurement_temperature    100.00(10)
_cell_measurement_theta_max      29.2210
_cell_measurement_theta_min      3.0700
_shelx_estimated_absorpt_T_max   0.404
_shelx_estimated_absorpt_T_min   0.156
_exptl_absorpt_coefficient_mu    36.917
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.70426
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
CrysAlisPro 1.171.42.94a (Rigaku Oxford Diffraction, 2023)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    6.622
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             2538
_exptl_crystal_size_max          0.08
_exptl_crystal_size_mid          0.05
_exptl_crystal_size_min          0.03
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0395
_diffrn_reflns_av_unetI/netI     0.0167
_diffrn_reflns_Laue_measured_fraction_full 0.990
_diffrn_reflns_Laue_measured_fraction_max 0.933
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            2589
_diffrn_reflns_point_group_measured_fraction_full 0.990
_diffrn_reflns_point_group_measured_fraction_max 0.933
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         29.003
_diffrn_reflns_theta_min         3.566
_diffrn_ambient_temperature      100.15
_diffrn_detector_area_resol_mean 10.0000
_diffrn_detector_type            HyPix
_diffrn_measured_fraction_theta_full 0.990
_diffrn_measured_fraction_theta_max 0.933
_diffrn_measurement_details      
;
List of Runs (angles in degrees, time in seconds):

  # Type    Start    End  Width  tₑₓₚ   ω     θ     κ     φ   Frames
#--------------------------------------------------------------------------
  1  ω    -37.00  35.00   0.50    2.64    --    8.33 -87.00  15.00  144
  2  ω    -23.00  50.00   0.50    2.64    --   -7.55  77.00-180.00  146
  3  ω    -43.00  18.00   0.50    2.64    --   -7.55  87.00 132.00  122
  4  ω    -26.00  23.00   0.50    2.64    --    8.33  87.00 132.00   98
;
_diffrn_measurement_device       'four-circle diffractometer'
_diffrn_measurement_device_type  'XtaLAB Synergy, Dualflex, HyPix'
_diffrn_measurement_method       'ω scans'
_diffrn_oxdiff_digest_hkl        
;
011c39010fa9b066141c19f7e3d851d5819418
;
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                124
_reflns_number_total             126
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'CrysAlisPro 1.171.42.94a (Rigaku OD, 2023)'
_computing_data_collection       'CrysAlisPro 1.171.42.94a (Rigaku OD, 2023)'
_computing_data_reduction        'CrysAlisPro 1.171.42.94a (Rigaku OD, 2023)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXS  (Sheldrick, 2008)'
_refine_diff_density_max         1.284
_refine_diff_density_min         -1.757
_refine_diff_density_rms         0.321
_refine_ls_extinction_coef       0.00029(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
_refine_ls_goodness_of_fit_ref   1.202
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_parameters     13
_refine_ls_number_reflns         126
_refine_ls_number_restraints     6
_refine_ls_R_factor_all          0.0181
_refine_ls_R_factor_gt           0.0133
_refine_ls_restrained_S_all      1.180
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0307P)²+22.1853P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0487
_refine_ls_wR_factor_ref         0.0493
_refine_special_details          ?
_olex2_refinement_description    
;
1. Shared sites
{Yb2, Gd2}
2. Uiso/Uaniso restraints and constraints
Uanis(F2) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002
Uanis(Yb2) = Uanis(Gd2)
3. Others
 Fixed Sof: Yb2(0.1125) Gd2(0.0125)
;
_atom_sites_solution_hydrogens   .
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
K1 K 0.750000 0.250000 0.250000 0.0069(11) Uani 1 24 d S T P . .
F2 F 0.6122(3) 0.1122(3) 0.1122(3) 0.0052(8) Uani 1 6 d S TU P . .
F1 F 0.3339(3) 0.3339(3) 0.000000 0.0062(9) Uani 1 4 d S T P . .
Yb2 Yb 0.500000 0.24010(5) 0.000000 0.0018(3) Uani 0.9 8 d S T P . 1
Gd2 Gd 0.500000 0.24010(5) 0.000000 0.0018(3) Uani 0.1 8 d S T P . 2


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
K1 F2 2.728(5) . ?
K1 F2 2.728(5) 75_655 ?
K1 F2 2.728(5) 124_645 ?
K1 F2 2.728(5) 146_565 ?
K1 F1 3.1616(18) 103_655 ?
K1 F1 3.1616(18) 49 ?
K1 F1 3.1616(18) 176 ?
K1 F1 3.1616(18) 170 ?
K1 F1 3.1616(18) 56 ?
K1 F1 3.1616(18) 10_655 ?
K1 F1 3.1616(18) 77 ?
K1 F1 3.1616(18) 2_655 ?
F2 Yb2 2.3283(15) . ?
F2 Yb2 2.3283(15) 5 ?
F2 Yb2 2.3283(14) 170 ?
F2 Gd2 2.3283(15) . ?
F1 Yb2 2.1796(12) 98_565 ?
F1 Yb2 2.1796(12) . ?
F1 Gd2 2.1796(12) . ?
Yb2 Yb2 3.8794(8) 170 ?
Yb2 Yb2 3.8794(8) 5 ?
Yb2 Yb2 3.8794(8) 101_655 ?
Yb2 Yb2 3.8794(8) 74_545 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
F2 K1 F2 109.5 . 124_645 ?
F2 K1 F2 109.5 124_645 146_565 ?
F2 K1 F2 109.5 . 146_565 ?
F2 K1 F2 109.5 . 75_655 ?
F2 K1 F2 109.471(1) 124_645 75_655 ?
F2 K1 F2 109.5 75_655 146_565 ?
F2 K1 F1 150.65(7) 75_655 103_655 ?
F2 K1 F1 150.65(7) 75_655 176 ?
F2 K1 F1 99.88(7) 146_565 2_655 ?
F2 K1 F1 58.56(2) 146_565 56 ?
F2 K1 F1 58.56(2) . 103_655 ?
F2 K1 F1 150.65(7) 146_565 170 ?
F2 K1 F1 150.65(7) 124_645 56 ?
F2 K1 F1 150.65(7) . 10_655 ?
F2 K1 F1 99.88(7) 124_645 170 ?
F2 K1 F1 58.56(2) 124_645 10_655 ?
F2 K1 F1 150.65(7) 124_645 2_655 ?
F2 K1 F1 58.56(2) 75_655 10_655 ?
F2 K1 F1 99.88(7) 124_645 176 ?
F2 K1 F1 99.88(7) 146_565 10_655 ?
F2 K1 F1 58.56(2) 146_565 176 ?
F2 K1 F1 150.65(7) . 77 ?
F2 K1 F1 58.56(2) 124_645 103_655 ?
F2 K1 F1 99.88(7) 124_645 77 ?
F2 K1 F1 58.56(2) . 56 ?
F2 K1 F1 58.56(2) 75_655 77 ?
F2 K1 F1 99.88(7) 75_655 56 ?
F2 K1 F1 58.56(2) 146_565 77 ?
F2 K1 F1 58.56(2) . 170 ?
F2 K1 F1 150.65(7) . 49 ?
F2 K1 F1 58.56(2) 75_655 170 ?
F2 K1 F1 58.56(2) 124_645 49 ?
F2 K1 F1 58.56(2) . 2_655 ?
F2 K1 F1 99.88(7) 75_655 49 ?
F2 K1 F1 58.56(2) 75_655 2_655 ?
F2 K1 F1 58.56(2) 146_565 49 ?
F2 K1 F1 58.56(2) . 176 ?
F2 K1 F1 99.88(7) 146_565 103_655 ?
F1 K1 F1 95.27(3) 49 176 ?
F1 K1 F1 144.71(9) 77 103_655 ?
F1 K1 F1 117.12(4) 103_655 2_655 ?
F1 K1 F1 50.24(11) 10_655 49 ?
F1 K1 F1 117.12(4) 10_655 2_655 ?
F1 K1 F1 144.71(9) 10_655 56 ?
F1 K1 F1 95.27(3) 103_655 170 ?
F1 K1 F1 95.27(3) 77 56 ?
F1 K1 F1 50.24(11) 176 103_655 ?
F1 K1 F1 50.77(14) 176 56 ?
F1 K1 F1 144.71(9) 49 2_655 ?
F1 K1 F1 95.27(3) 103_655 56 ?
F1 K1 F1 117.12(4) 176 170 ?
F1 K1 F1 50.24(11) 77 49 ?
F1 K1 F1 95.27(3) 56 170 ?
F1 K1 F1 50.24(11) 10_655 77 ?
F1 K1 F1 95.27(3) 49 103_655 ?
F1 K1 F1 50.24(11) 56 2_655 ?
F1 K1 F1 144.71(9) 10_655 176 ?
F1 K1 F1 50.77(14) 170 2_655 ?
F1 K1 F1 95.27(3) 77 2_655 ?
F1 K1 F1 95.27(3) 10_655 170 ?
F1 K1 F1 95.27(3) 176 2_655 ?
F1 K1 F1 117.12(4) 77 170 ?
F1 K1 F1 117.12(4) 77 176 ?
F1 K1 F1 144.71(9) 49 170 ?
F1 K1 F1 117.12(4) 10_655 103_655 ?
F1 K1 F1 117.12(4) 49 56 ?
Yb2 F2 K1 105.85(12) 170 . ?
Yb2 F2 K1 105.85(12) 5 . ?
Yb2 F2 K1 105.85(12) . . ?
Yb2 F2 Yb2 112.84(10) . 5 ?
Yb2 F2 Yb2 112.84(10) 170 5 ?
Yb2 F2 Yb2 112.84(10) . 170 ?
Gd2 F2 K1 105.85(12) . . ?
Gd2 F2 Yb2 112.84(10) . 170 ?
Gd2 F2 Yb2 112.84(10) . 5 ?
K1 F1 K1 129.23(14) 49_454 121_655 ?
Yb2 F1 K1 96.60(3) 98_565 121_655 ?
Yb2 F1 K1 96.60(3) . 121_655 ?
Yb2 F1 K1 96.60(3) . 49_454 ?
Yb2 F1 K1 96.60(3) 98_565 49_454 ?
Yb2 F1 Yb2 148.9(2) 98_565 . ?
F2 Yb2 F2 66.79(13) 172_545 99 ?
F2 Yb2 F2 66.79(13) 74_545 . ?
F2 Yb2 F2 66.79(13) 99 . ?
F2 Yb2 F2 66.79(13) 172_545 74_545 ?
F2 Yb2 F2 102.2(2) 99 74_545 ?
F2 Yb2 F2 102.2(2) 172_545 . ?
F2 Yb2 Yb2 86.86(11) 74_545 170 ?
F2 Yb2 Yb2 86.86(11) . 74_545 ?
F2 Yb2 Yb2 33.58(5) . 5 ?
F2 Yb2 Yb2 33.58(5) 172_545 101_655 ?
F2 Yb2 Yb2 86.86(11) 99 5 ?
F2 Yb2 Yb2 33.58(5) 99 101_655 ?
F2 Yb2 Yb2 33.58(5) 99 170 ?
F2 Yb2 Yb2 86.86(11) 74_545 101_655 ?
F2 Yb2 Yb2 86.86(11) 172_545 5 ?
F2 Yb2 Yb2 86.86(11) . 101_655 ?
F2 Yb2 Yb2 33.58(5) 74_545 5 ?
F2 Yb2 Yb2 33.58(5) 172_545 74_545 ?
F2 Yb2 Yb2 86.86(11) 172_545 170 ?
F2 Yb2 Yb2 86.86(11) 99 74_545 ?
F2 Yb2 Yb2 33.58(5) 74_545 74_545 ?
F2 Yb2 Yb2 33.58(5) . 170 ?
F1 Yb2 F2 141.99(5) 2_655 172_545 ?
F1 Yb2 F2 141.99(5) 2_655 74_545 ?
F1 Yb2 F2 80.17(13) 2_655 . ?
F1 Yb2 F2 80.17(13) 58_554 172_545 ?
F1 Yb2 F2 80.17(13) . 74_545 ?
F1 Yb2 F2 80.17(13) . 172_545 ?
F1 Yb2 F2 141.99(5) 56 172_545 ?
F1 Yb2 F2 141.99(5) 56 99 ?
F1 Yb2 F2 141.99(5) 58_554 74_545 ?
F1 Yb2 F2 80.17(13) 2_655 99 ?
F1 Yb2 F2 80.17(13) 56 . ?
F1 Yb2 F2 80.17(13) 58_554 99 ?
F1 Yb2 F2 141.99(5) 58_554 . ?
F1 Yb2 F2 141.99(5) . 99 ?
F1 Yb2 F2 80.17(13) 56 74_545 ?
F1 Yb2 F2 141.99(5) . . ?
F1 Yb2 F1 76.01(9) 2_655 58_554 ?
F1 Yb2 F1 121.1(2) 56 58_554 ?
F1 Yb2 F1 121.1(2) 2_655 . ?
F1 Yb2 F1 76.01(9) 56 2_655 ?
F1 Yb2 F1 76.01(9) 56 . ?
F1 Yb2 F1 76.01(9) 58_554 . ?
F1 Yb2 Yb2 74.45(11) 56 5 ?
F1 Yb2 Yb2 110.34(7) 2_655 101_655 ?
F1 Yb2 Yb2 74.45(11) . 74_545 ?
F1 Yb2 Yb2 110.34(7) 2_655 5 ?
F1 Yb2 Yb2 74.45(11) 2_655 170 ?
F1 Yb2 Yb2 164.45(11) 58_554 5 ?
F1 Yb2 Yb2 164.45(11) 56 101_655 ?
F1 Yb2 Yb2 110.34(7) . 5 ?
F1 Yb2 Yb2 110.34(7) 56 170 ?
F1 Yb2 Yb2 74.45(11) 58_554 101_655 ?
F1 Yb2 Yb2 164.45(11) . 170 ?
F1 Yb2 Yb2 110.34(7) 56 74_545 ?
F1 Yb2 Yb2 110.34(7) . 101_655 ?
F1 Yb2 Yb2 164.45(11) 2_655 74_545 ?
F1 Yb2 Yb2 110.34(7) 58_554 74_545 ?
F1 Yb2 Yb2 110.34(7) 58_554 170 ?
Yb2 Yb2 Yb2 90.0 74_545 170 ?
Yb2 Yb2 Yb2 60.0 101_655 170 ?
Yb2 Yb2 Yb2 60.0 101_655 74_545 ?
Yb2 Yb2 Yb2 90.0 101_655 5 ?
Yb2 Yb2 Yb2 60.0 74_545 5 ?
Yb2 Yb2 Yb2 60.0 5 170 ?
K1 Gd2 K1 90.0 49_454 169_655 ?
K1 Gd2 K1 176.791(17) 121_655 169_655 ?
K1 Gd2 K1 176.791(17) 49_454 . ?
K1 Gd2 K1 90.0 . 169_655 ?
K1 Gd2 K1 90.0 49_454 121_655 ?
K1 Gd2 K1 90.0 . 121_655 ?
F2 Gd2 K1 91.007(6) 99 . ?
F2 Gd2 K1 142.72(12) 74_545 169_655 ?
F2 Gd2 K1 40.49(12) 74_545 121_655 ?
F2 Gd2 K1 40.49(12) 172_545 49_454 ?
F2 Gd2 K1 142.72(12) 99 121_655 ?
F2 Gd2 K1 91.007(6) 172_545 169_655 ?
F2 Gd2 K1 91.007(6) . 121_655 ?
F2 Gd2 K1 91.007(6) 74_545 49_454 ?
F2 Gd2 K1 142.72(12) . 49_454 ?
F2 Gd2 K1 91.007(6) 74_545 . ?
F2 Gd2 K1 40.49(12) 99 169_655 ?
F2 Gd2 K1 40.49(12) . . ?
F2 Gd2 K1 91.007(6) . 169_655 ?
F2 Gd2 K1 142.72(12) 172_545 . ?
F2 Gd2 K1 91.007(6) 172_545 121_655 ?
F2 Gd2 K1 91.007(6) 99 49_454 ?
F2 Gd2 F2 102.2(2) 172_545 . ?
F2 Gd2 F2 102.2(2) 99 74_545 ?
F2 Gd2 F2 66.79(13) 172_545 74_545 ?
F2 Gd2 F2 66.79(13) 99 . ?
F2 Gd2 F2 66.79(13) 74_545 . ?
F2 Gd2 F2 66.79(13) 172_545 99 ?
F1 Gd2 K1 51.00(4) . 49_454 ?
F1 Gd2 K1 51.00(4) 58_554 49_454 ?
F1 Gd2 K1 127.00(5) 2_655 121_655 ?
F1 Gd2 K1 51.00(4) . 121_655 ?
F1 Gd2 K1 127.00(5) 2_655 49_454 ?
F1 Gd2 K1 127.00(5) 56 169_655 ?
F1 Gd2 K1 127.00(5) 58_554 121_655 ?
F1 Gd2 K1 51.00(4) 58_554 169_655 ?
F1 Gd2 K1 127.00(5) 56 49_454 ?
F1 Gd2 K1 51.00(4) 56 . ?
F1 Gd2 K1 51.00(4) 2_655 169_655 ?
F1 Gd2 K1 51.00(4) 2_655 . ?
F1 Gd2 K1 127.00(5) . 169_655 ?
F1 Gd2 K1 127.00(5) 58_554 . ?
F1 Gd2 K1 127.00(5) . . ?
F1 Gd2 K1 51.00(4) 56 121_655 ?
F1 Gd2 F2 141.99(5) 56 99 ?
F1 Gd2 F2 141.99(5) . . ?
F1 Gd2 F2 80.17(13) . 74_545 ?
F1 Gd2 F2 80.17(13) 2_655 99 ?
F1 Gd2 F2 141.99(5) 2_655 74_545 ?
F1 Gd2 F2 80.17(13) 58_554 99 ?
F1 Gd2 F2 141.99(5) 56 172_545 ?
F1 Gd2 F2 141.99(5) . 99 ?
F1 Gd2 F2 80.17(13) 2_655 . ?
F1 Gd2 F2 141.99(5) 2_655 172_545 ?
F1 Gd2 F2 141.99(5) 58_554 74_545 ?
F1 Gd2 F2 80.17(13) 56 74_545 ?
F1 Gd2 F2 141.99(5) 58_554 . ?
F1 Gd2 F2 80.17(13) 56 . ?
F1 Gd2 F2 80.17(13) . 172_545 ?
F1 Gd2 F2 80.17(13) 58_554 172_545 ?
F1 Gd2 F1 76.01(9) 58_554 . ?
F1 Gd2 F1 121.1(2) 2_655 . ?
F1 Gd2 F1 76.01(9) 56 . ?
F1 Gd2 F1 121.1(2) 56 58_554 ?
F1 Gd2 F1 76.01(9) 56 2_655 ?
F1 Gd2 F1 76.01(9) 2_655 58_554 ?

_olex2_submission_special_instructions 'No special instructions were received'
_oxdiff_exptl_absorpt_empirical_details 
;
Empirical correction (ABSPACK) includes:
- Absorption correction using spherical harmonics
- Frame scaling
;
_oxdiff_exptl_absorpt_empirical_full_max 1.243
_oxdiff_exptl_absorpt_empirical_full_min 0.855
