# Supplementary Information (SI) for Chemical Science.
# This journal is © The Royal Society of Chemistry 2026

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
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data_cu_20250517b_0m_pl
_database_code_depnum_ccdc_archive 'CCDC 2454644'
loop_
_audit_author_name
_audit_author_address
'Hao-Hui Xie'
;NanJing University of Science and Technology
China
;
_audit_update_record             
;
2025-09-02 deposited with the CCDC.	2026-03-06 downloaded from the CCDC.
;
_audit_creation_date             2025-05-19
_audit_creation_method           
;
Olex2 1.5
(compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C26 H30 Au2 B10 Cl2 P2'
_chemical_formula_sum            'C26 H30 Au2 B10 Cl2 P2'
_chemical_formula_weight         977.37
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -4.4197 7.2980 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   10.1696(3)
_cell_length_b                   23.2022(6)
_cell_length_c                   13.7961(4)
_cell_angle_alpha                90
_cell_angle_beta                 100.2800(10)
_cell_angle_gamma                90
_cell_volume                     3203.03(16)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9671
_cell_measurement_temperature    174.15
_cell_measurement_theta_max      68.207
_cell_measurement_theta_min      3.772
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    19.583
_exptl_absorpt_correction_T_max  0.7531
_exptl_absorpt_correction_T_min  0.3874
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
 SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D.,
 J. Appl. Cryst. 48 (2015) 3-10
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            white
_exptl_crystal_colour_lustre     ?
_exptl_crystal_colour_modifier   ?
_exptl_crystal_colour_primary    white
_exptl_crystal_density_diffrn    2.027
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             1832
_exptl_crystal_preparation       ?
_exptl_crystal_size_max          0.16
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.12
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0429
_diffrn_reflns_av_unetI/netI     0.0350
_diffrn_reflns_Laue_measured_fraction_full 0.995
_diffrn_reflns_Laue_measured_fraction_max 0.995
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_k_min       -27
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            26860
_diffrn_reflns_point_group_measured_fraction_full 0.995
_diffrn_reflns_point_group_measured_fraction_max 0.995
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         68.233
_diffrn_reflns_theta_min         3.773
_diffrn_ambient_temperature      174.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  multi-scan
_diffrn_measurement_method       ?
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_source                   ?
_diffrn_source_current           1.1
_diffrn_source_power             0.05500000000000001
_diffrn_source_voltage           50.0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                5577
_reflns_number_total             5837
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.41 (?, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.41 (?, 2016)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         1.042
_refine_diff_density_min         -1.968
_refine_diff_density_rms         0.181
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.139
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     379
_refine_ls_number_reflns         5837
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0378
_refine_ls_R_factor_gt           0.0341
_refine_ls_restrained_S_all      1.139
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0365P)²+12.6189P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0869
_refine_ls_wR_factor_ref         0.0879
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups
2.a Aromatic/amide H refined with riding coordinates:
 C22(H22), C2(H2), C3(H3), C16(H16), C8(H8), C6(H6), C18(H18), C12(H12),
 C20(H20), C19(H19), C17(H17), C23(H23), C11(H11), C5(H5), C24(H24), C9(H9),
 C4(H4A), C26(H26), C10(H10), C25(H25)
2.b Boron cage BH refined with riding coordinates:
 B1(H1), B2(H2A), B3(H3A), B7(H7), B6(H6A), B4(H4), B8(H8A), B5(H5A), B9(H9A),
 B10(H10A)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au2 Au 0.73780(2) 0.88981(2) 0.36772(2) 0.03526(9) Uani 1 1 d . . . . .
Au1 Au 0.76303(2) 0.57455(2) 0.53749(2) 0.03551(9) Uani 1 1 d . . . . .
P2 P 0.52491(13) 0.87174(5) 0.37847(10) 0.0256(3) Uani 1 1 d . . . . .
P1 P 0.78826(14) 0.64879(6) 0.43947(10) 0.0287(3) Uani 1 1 d . . . . .
Cl1 Cl 0.74129(18) 0.49829(7) 0.63650(12) 0.0514(4) Uani 1 1 d . . . . .
Cl2 Cl 0.95550(18) 0.90666(11) 0.3579(2) 0.0837(8) Uani 1 1 d . . . . .
C13 C 0.6308(5) 0.6913(2) 0.4121(4) 0.0240(10) Uani 1 1 d . . . . .
C14 C 0.5013(5) 0.79242(19) 0.3893(3) 0.0216(9) Uani 1 1 d . . . . .
C22 C 0.5763(7) 0.9313(2) 0.5530(4) 0.0372(13) Uani 1 1 d . . . . .
H22 H 0.664945 0.932174 0.539992 0.045 Uiso 1 1 calc R U . . .
C15 C 0.4093(6) 0.8949(2) 0.2706(4) 0.0317(12) Uani 1 1 d . . . . .
C2 C 0.9664(6) 0.7422(3) 0.4480(5) 0.0412(14) Uani 1 1 d . . . . .
H2 H 0.937028 0.745889 0.378927 0.049 Uiso 1 1 calc R U . . .
C1 C 0.9145(6) 0.6990(2) 0.4992(4) 0.0346(12) Uani 1 1 d . . . . .
B1 B 0.6246(6) 0.7576(2) 0.4681(4) 0.0257(11) Uani 1 1 d . . . . .
H1 H 0.712118 0.779670 0.513990 0.031 Uiso 1 1 calc R U . . .
C21 C 0.4770(6) 0.9040(2) 0.4872(4) 0.0332(12) Uani 1 1 d . . . . .
C7 C 0.8370(6) 0.6262(2) 0.3248(4) 0.0313(11) Uani 1 1 d . . . . .
C3 C 1.0605(6) 0.7800(3) 0.4966(6) 0.0474(16) Uani 1 1 d . . . . .
H3 H 1.092864 0.810358 0.461104 0.057 Uiso 1 1 calc R U . . .
B2 B 0.6104(6) 0.7505(2) 0.3368(4) 0.0238(11) Uani 1 1 d . . . . .
H2A H 0.688647 0.767737 0.296826 0.029 Uiso 1 1 calc R U . . .
C16 C 0.4647(6) 0.9173(2) 0.1933(4) 0.0361(13) Uani 1 1 d . . . . .
H16 H 0.558991 0.918689 0.198371 0.043 Uiso 1 1 calc R U . . .
B3 B 0.4392(6) 0.7527(2) 0.2850(4) 0.0262(12) Uani 1 1 d . . . . .
H3A H 0.403380 0.771911 0.210534 0.031 Uiso 1 1 calc R U . . .
B7 B 0.4640(6) 0.7631(3) 0.4966(4) 0.0285(12) Uani 1 1 d . . . . .
H7 H 0.444228 0.788989 0.561002 0.034 Uiso 1 1 calc R U . . .
C8 C 0.8919(7) 0.5710(3) 0.3245(5) 0.0440(15) Uani 1 1 d . . . . .
H8 H 0.896529 0.546956 0.380829 0.053 Uiso 1 1 calc R U . . .
C6 C 0.9579(8) 0.6937(3) 0.5997(5) 0.0514(18) Uani 1 1 d . . . . .
H6 H 0.921271 0.664769 0.635743 0.062 Uiso 1 1 calc R U . . .
C18 C 0.2463(8) 0.9350(3) 0.1007(6) 0.054(2) Uani 1 1 d . . . . .
H18 H 0.190476 0.947352 0.041662 0.065 Uiso 1 1 calc R U . . .
B6 B 0.5488(7) 0.6966(3) 0.5115(4) 0.0299(13) Uani 1 1 d . . . . .
H6A H 0.586734 0.677623 0.585892 0.036 Uiso 1 1 calc R U . . .
C12 C 0.8304(6) 0.6599(3) 0.2410(4) 0.0365(12) Uani 1 1 d . . . . .
H12 H 0.794633 0.697764 0.239697 0.044 Uiso 1 1 calc R U . . .
C20 C 0.2714(7) 0.8941(3) 0.2623(7) 0.058(2) Uani 1 1 d . . . . .
H20 H 0.232415 0.879481 0.314878 0.070 Uiso 1 1 calc R U . . .
C19 C 0.1898(8) 0.9145(3) 0.1776(7) 0.067(3) Uani 1 1 d . . . . .
H19 H 0.095450 0.914306 0.172780 0.080 Uiso 1 1 calc R U . . .
C17 C 0.3822(8) 0.9375(3) 0.1087(5) 0.0485(17) Uani 1 1 d . . . . .
H17 H 0.420349 0.953198 0.056400 0.058 Uiso 1 1 calc R U . . .
C23 C 0.5486(9) 0.9573(3) 0.6375(5) 0.0532(18) Uani 1 1 d . . . . .
H23 H 0.618126 0.975825 0.681654 0.064 Uiso 1 1 calc R U . . .
C11 C 0.8759(6) 0.6384(3) 0.1591(4) 0.0389(13) Uani 1 1 d . . . . .
H11 H 0.869643 0.661517 0.101597 0.047 Uiso 1 1 calc R U . . .
B4 B 0.5231(6) 0.6858(2) 0.3000(4) 0.0267(12) Uani 1 1 d . . . . .
H4 H 0.543398 0.659956 0.235692 0.032 Uiso 1 1 calc R U . . .
C5 C 1.0552(8) 0.7309(3) 0.6474(6) 0.065(2) Uani 1 1 d . . . . .
H5 H 1.086213 0.726886 0.716216 0.078 Uiso 1 1 calc R U . . .
C24 C 0.4227(9) 0.9566(3) 0.6574(6) 0.056(2) Uani 1 1 d . . . . .
H24 H 0.404205 0.974896 0.715098 0.067 Uiso 1 1 calc R U . . .
C9 C 0.9396(8) 0.5511(3) 0.2430(6) 0.0528(17) Uani 1 1 d . . . . .
H9 H 0.979540 0.513996 0.244953 0.063 Uiso 1 1 calc R U . . .
B8 B 0.3482(6) 0.7604(2) 0.3835(4) 0.0269(12) Uani 1 1 d . . . . .
H8A H 0.251843 0.784875 0.373261 0.032 Uiso 1 1 calc R U . . .
C4 C 1.1078(7) 0.7740(3) 0.5953(6) 0.059(2) Uani 1 1 d . . . . .
H4A H 1.175503 0.799001 0.627980 0.070 Uiso 1 1 calc R U . . .
C26 C 0.3508(8) 0.9028(3) 0.5097(7) 0.071(3) Uani 1 1 d . . . . .
H26 H 0.281066 0.883605 0.466828 0.085 Uiso 1 1 calc R U . . .
C10 C 0.9303(7) 0.5835(3) 0.1601(5) 0.0462(16) Uani 1 1 d . . . . .
H10 H 0.960733 0.568866 0.103676 0.055 Uiso 1 1 calc R U . . .
C25 C 0.3234(10) 0.9297(3) 0.5952(8) 0.074(3) Uani 1 1 d . . . . .
H25 H 0.235342 0.929046 0.609301 0.089 Uiso 1 1 calc R U . . .
B5 B 0.4856(6) 0.6523(2) 0.4081(4) 0.0288(12) Uani 1 1 d . . . . .
H5A H 0.482128 0.604265 0.414658 0.035 Uiso 1 1 calc R U . . .
B9 B 0.3602(6) 0.6915(2) 0.3292(5) 0.0293(12) Uani 1 1 d . . . . .
H9A H 0.271626 0.669851 0.283899 0.035 Uiso 1 1 calc R U . . .
B10 B 0.3764(6) 0.6980(3) 0.4598(5) 0.0303(13) Uani 1 1 d . . . . .
H10A H 0.298755 0.680454 0.500125 0.036 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au2 P2 2.2361(13) . ?
Au2 Cl2 2.2758(17) . ?
Au1 P1 2.2327(13) . ?
Au1 Cl1 2.2701(15) . ?
P2 C14 1.865(5) . ?
P2 C15 1.806(6) . ?
P2 C21 1.819(6) . ?
P1 C13 1.861(5) . ?
P1 C1 1.818(6) . ?
P1 C7 1.818(6) . ?
C13 B1 1.728(7) . ?
C13 B2 1.713(7) . ?
C13 B6 1.732(8) . ?
C13 B4 1.733(7) . ?
C13 B5 1.723(8) . ?
C14 B1 1.709(7) . ?
C14 B2 1.728(7) . ?
C14 B3 1.731(7) . ?
C14 B7 1.732(7) . ?
C14 B8 1.714(7) . ?
C22 H22 0.9500 . ?
C22 C21 1.385(9) . ?
C22 C23 1.386(9) . ?
C15 C16 1.392(8) . ?
C15 C20 1.386(9) . ?
C2 H2 0.9500 . ?
C2 C1 1.384(9) . ?
C2 C3 1.380(9) . ?
C1 C6 1.383(9) . ?
B1 H1 1.1200 . ?
B1 B2 1.798(8) . ?
B1 B7 1.752(8) . ?
B1 B6 1.767(8) . ?
C21 C26 1.373(9) . ?
C7 C8 1.397(8) . ?
C7 C12 1.387(8) . ?
C3 H3 0.9500 . ?
C3 C4 1.369(11) . ?
B2 H2A 1.1200 . ?
B2 B3 1.761(8) . ?
B2 B4 1.772(8) . ?
C16 H16 0.9500 . ?
C16 C17 1.393(9) . ?
B3 H3A 1.1200 . ?
B3 B4 1.765(8) . ?
B3 B8 1.783(8) . ?
B3 B9 1.790(8) . ?
B7 H7 1.1200 . ?
B7 B6 1.762(8) . ?
B7 B8 1.781(8) . ?
B7 B10 1.781(9) . ?
C8 H8 0.9500 . ?
C8 C9 1.381(10) . ?
C6 H6 0.9500 . ?
C6 C5 1.387(10) . ?
C18 H18 0.9500 . ?
C18 C19 1.379(12) . ?
C18 C17 1.368(11) . ?
B6 H6A 1.1200 . ?
B6 B5 1.781(8) . ?
B6 B10 1.771(9) . ?
C12 H12 0.9500 . ?
C12 C11 1.388(8) . ?
C20 H20 0.9500 . ?
C20 C19 1.389(11) . ?
C19 H19 0.9500 . ?
C17 H17 0.9500 . ?
C23 H23 0.9500 . ?
C23 C24 1.356(12) . ?
C11 H11 0.9500 . ?
C11 C10 1.387(9) . ?
B4 H4 1.1200 . ?
B4 B5 1.782(8) . ?
B4 B9 1.779(9) . ?
C5 H5 0.9500 . ?
C5 C4 1.393(12) . ?
C24 H24 0.9500 . ?
C24 C25 1.355(13) . ?
C9 H9 0.9500 . ?
C9 C10 1.359(10) . ?
B8 H8A 1.1200 . ?
B8 B9 1.777(8) . ?
B8 B10 1.783(8) . ?
C4 H4A 0.9500 . ?
C26 H26 0.9500 . ?
C26 C25 1.405(10) . ?
C10 H10 0.9500 . ?
C25 H25 0.9500 . ?
B5 H5A 1.1200 . ?
B5 B9 1.773(8) . ?
B5 B10 1.775(9) . ?
B9 H9A 1.1200 . ?
B9 B10 1.786(9) . ?
B10 H10A 1.1200 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P2 Au2 Cl2 179.00(7) . . ?
P1 Au1 Cl1 178.84(6) . . ?
C14 P2 Au2 109.28(16) . . ?
C15 P2 Au2 112.66(19) . . ?
C15 P2 C14 106.6(2) . . ?
C15 P2 C21 109.0(3) . . ?
C21 P2 Au2 112.5(2) . . ?
C21 P2 C14 106.4(2) . . ?
C13 P1 Au1 110.11(17) . . ?
C1 P1 Au1 111.6(2) . . ?
C1 P1 C13 105.4(2) . . ?
C1 P1 C7 107.4(3) . . ?
C7 P1 Au1 112.52(19) . . ?
C7 P1 C13 109.5(2) . . ?
B1 C13 P1 118.6(3) . . ?
B1 C13 B6 61.4(3) . . ?
B1 C13 B4 113.4(4) . . ?
B2 C13 P1 123.7(4) . . ?
B2 C13 B1 63.0(3) . . ?
B2 C13 B6 113.5(4) . . ?
B2 C13 B4 61.9(3) . . ?
B2 C13 B5 113.0(4) . . ?
B6 C13 P1 113.3(3) . . ?
B6 C13 B4 113.3(4) . . ?
B4 C13 P1 121.8(3) . . ?
B5 C13 P1 115.5(3) . . ?
B5 C13 B1 112.4(4) . . ?
B5 C13 B6 62.1(3) . . ?
B5 C13 B4 62.1(3) . . ?
B1 C14 P2 115.3(3) . . ?
B1 C14 B2 63.1(3) . . ?
B1 C14 B3 113.2(4) . . ?
B1 C14 B7 61.2(3) . . ?
B1 C14 B8 112.5(4) . . ?
B2 C14 P2 114.8(3) . . ?
B2 C14 B3 61.2(3) . . ?
B2 C14 B7 113.1(4) . . ?
B3 C14 P2 119.5(3) . . ?
B3 C14 B7 113.4(4) . . ?
B7 C14 P2 120.5(3) . . ?
B8 C14 P2 123.6(3) . . ?
B8 C14 B2 112.5(4) . . ?
B8 C14 B3 62.3(3) . . ?
B8 C14 B7 62.2(3) . . ?
C21 C22 H22 119.5 . . ?
C21 C22 C23 121.1(7) . . ?
C23 C22 H22 119.5 . . ?
C16 C15 P2 116.7(5) . . ?
C20 C15 P2 124.4(5) . . ?
C20 C15 C16 118.9(6) . . ?
C1 C2 H2 119.8 . . ?
C3 C2 H2 119.8 . . ?
C3 C2 C1 120.4(6) . . ?
C2 C1 P1 122.4(4) . . ?
C6 C1 P1 118.0(5) . . ?
C6 C1 C2 119.6(6) . . ?
C13 B1 H1 124.9 . . ?
C13 B1 B2 58.1(3) . . ?
C13 B1 B7 106.0(4) . . ?
C13 B1 B6 59.4(3) . . ?
C14 B1 C13 102.6(4) . . ?
C14 B1 H1 124.2 . . ?
C14 B1 B2 59.0(3) . . ?
C14 B1 B7 60.0(3) . . ?
C14 B1 B6 106.2(4) . . ?
B2 B1 H1 121.6 . . ?
B7 B1 H1 121.2 . . ?
B7 B1 B2 108.8(4) . . ?
B7 B1 B6 60.1(3) . . ?
B6 B1 H1 121.7 . . ?
B6 B1 B2 107.9(4) . . ?
C22 C21 P2 117.2(5) . . ?
C26 C21 P2 125.2(5) . . ?
C26 C21 C22 117.6(6) . . ?
C8 C7 P1 116.0(5) . . ?
C12 C7 P1 125.6(4) . . ?
C12 C7 C8 118.4(5) . . ?
C2 C3 H3 119.7 . . ?
C4 C3 C2 120.6(7) . . ?
C4 C3 H3 119.7 . . ?
C13 B2 C14 102.4(4) . . ?
C13 B2 B1 58.9(3) . . ?
C13 B2 H2A 124.4 . . ?
C13 B2 B3 105.8(4) . . ?
C13 B2 B4 59.6(3) . . ?
C14 B2 B1 57.9(3) . . ?
C14 B2 H2A 124.9 . . ?
C14 B2 B3 59.5(3) . . ?
C14 B2 B4 105.7(4) . . ?
B1 B2 H2A 121.8 . . ?
B3 B2 B1 107.6(4) . . ?
B3 B2 H2A 121.9 . . ?
B3 B2 B4 59.9(3) . . ?
B4 B2 B1 108.2(4) . . ?
B4 B2 H2A 121.6 . . ?
C15 C16 H16 119.9 . . ?
C15 C16 C17 120.2(6) . . ?
C17 C16 H16 119.9 . . ?
C14 B3 B2 59.3(3) . . ?
C14 B3 H3A 124.1 . . ?
C14 B3 B4 105.9(4) . . ?
C14 B3 B8 58.4(3) . . ?
C14 B3 B9 105.0(4) . . ?
B2 B3 H3A 121.3 . . ?
B2 B3 B4 60.3(3) . . ?
B2 B3 B8 107.7(4) . . ?
B2 B3 B9 108.1(4) . . ?
B4 B3 H3A 121.9 . . ?
B4 B3 B8 107.8(4) . . ?
B4 B3 B9 60.0(3) . . ?
B8 B3 H3A 122.1 . . ?
B8 B3 B9 59.6(3) . . ?
B9 B3 H3A 122.4 . . ?
C14 B7 B1 58.7(3) . . ?
C14 B7 H7 124.4 . . ?
C14 B7 B6 105.4(4) . . ?
C14 B7 B8 58.4(3) . . ?
C14 B7 B10 105.3(4) . . ?
B1 B7 H7 121.6 . . ?
B1 B7 B6 60.4(3) . . ?
B1 B7 B8 107.3(4) . . ?
B1 B7 B10 108.3(4) . . ?
B6 B7 H7 122.1 . . ?
B6 B7 B8 107.7(4) . . ?
B6 B7 B10 60.0(4) . . ?
B8 B7 H7 122.0 . . ?
B10 B7 H7 122.0 . . ?
B10 B7 B8 60.1(3) . . ?
C7 C8 H8 119.8 . . ?
C9 C8 C7 120.4(6) . . ?
C9 C8 H8 119.8 . . ?
C1 C6 H6 120.2 . . ?
C1 C6 C5 119.6(7) . . ?
C5 C6 H6 120.2 . . ?
C19 C18 H18 119.8 . . ?
C17 C18 H18 119.8 . . ?
C17 C18 C19 120.4(7) . . ?
C13 B6 B1 59.2(3) . . ?
C13 B6 B7 105.4(4) . . ?
C13 B6 H6A 124.2 . . ?
C13 B6 B5 58.7(3) . . ?
C13 B6 B10 105.3(4) . . ?
B1 B6 H6A 121.7 . . ?
B1 B6 B5 107.9(4) . . ?
B1 B6 B10 108.0(4) . . ?
B7 B6 B1 59.5(3) . . ?
B7 B6 H6A 122.1 . . ?
B7 B6 B5 108.2(4) . . ?
B7 B6 B10 60.5(3) . . ?
B5 B6 H6A 121.6 . . ?
B10 B6 H6A 122.1 . . ?
B10 B6 B5 59.9(4) . . ?
C7 C12 H12 119.9 . . ?
C7 C12 C11 120.1(5) . . ?
C11 C12 H12 119.9 . . ?
C15 C20 H20 119.7 . . ?
C15 C20 C19 120.6(7) . . ?
C19 C20 H20 119.7 . . ?
C18 C19 C20 119.7(7) . . ?
C18 C19 H19 120.1 . . ?
C20 C19 H19 120.1 . . ?
C16 C17 H17 120.0 . . ?
C18 C17 C16 120.1(7) . . ?
C18 C17 H17 120.0 . . ?
C22 C23 H23 119.8 . . ?
C24 C23 C22 120.4(7) . . ?
C24 C23 H23 119.8 . . ?
C12 C11 H11 119.6 . . ?
C10 C11 C12 120.8(6) . . ?
C10 C11 H11 119.6 . . ?
C13 B4 B2 58.5(3) . . ?
C13 B4 B3 104.8(4) . . ?
C13 B4 H4 124.7 . . ?
C13 B4 B5 58.7(3) . . ?
C13 B4 B9 104.9(4) . . ?
B2 B4 H4 121.8 . . ?
B2 B4 B5 107.5(4) . . ?
B2 B4 B9 108.1(4) . . ?
B3 B4 B2 59.7(3) . . ?
B3 B4 H4 122.1 . . ?
B3 B4 B5 108.1(4) . . ?
B3 B4 B9 60.7(3) . . ?
B5 B4 H4 121.8 . . ?
B9 B4 H4 122.1 . . ?
B9 B4 B5 59.7(3) . . ?
C6 C5 H5 119.7 . . ?
C6 C5 C4 120.6(7) . . ?
C4 C5 H5 119.7 . . ?
C23 C24 H24 120.0 . . ?
C25 C24 C23 120.0(7) . . ?
C25 C24 H24 120.0 . . ?
C8 C9 H9 119.4 . . ?
C10 C9 C8 121.3(6) . . ?
C10 C9 H9 119.4 . . ?
C14 B8 B3 59.3(3) . . ?
C14 B8 B7 59.4(3) . . ?
C14 B8 H8A 123.6 . . ?
C14 B8 B9 106.3(4) . . ?
C14 B8 B10 106.0(4) . . ?
B3 B8 H8A 121.1 . . ?
B3 B8 B10 108.5(4) . . ?
B7 B8 B3 108.7(4) . . ?
B7 B8 H8A 121.3 . . ?
B7 B8 B10 60.0(3) . . ?
B9 B8 B3 60.4(3) . . ?
B9 B8 B7 108.4(4) . . ?
B9 B8 H8A 121.8 . . ?
B9 B8 B10 60.2(3) . . ?
B10 B8 H8A 122.0 . . ?
C3 C4 C5 119.1(7) . . ?
C3 C4 H4A 120.4 . . ?
C5 C4 H4A 120.4 . . ?
C21 C26 H26 119.5 . . ?
C21 C26 C25 121.0(8) . . ?
C25 C26 H26 119.5 . . ?
C11 C10 H10 120.5 . . ?
C9 C10 C11 119.0(6) . . ?
C9 C10 H10 120.5 . . ?
C24 C25 C26 119.9(8) . . ?
C24 C25 H25 120.0 . . ?
C26 C25 H25 120.0 . . ?
C13 B5 B6 59.2(3) . . ?
C13 B5 B4 59.2(3) . . ?
C13 B5 H5A 124.0 . . ?
C13 B5 B9 105.6(4) . . ?
C13 B5 B10 105.6(4) . . ?
B6 B5 B4 108.6(4) . . ?
B6 B5 H5A 121.4 . . ?
B4 B5 H5A 121.1 . . ?
B9 B5 B6 108.2(4) . . ?
B9 B5 B4 60.1(3) . . ?
B9 B5 H5A 122.1 . . ?
B9 B5 B10 60.4(4) . . ?
B10 B5 B6 59.7(4) . . ?
B10 B5 B4 108.6(4) . . ?
B10 B5 H5A 122.0 . . ?
B3 B9 H9A 122.1 . . ?
B4 B9 B3 59.3(3) . . ?
B4 B9 H9A 121.9 . . ?
B4 B9 B10 108.3(4) . . ?
B8 B9 B3 60.0(3) . . ?
B8 B9 B4 107.4(4) . . ?
B8 B9 H9A 122.0 . . ?
B8 B9 B10 60.1(3) . . ?
B5 B9 B3 107.3(4) . . ?
B5 B9 B4 60.2(3) . . ?
B5 B9 B8 107.4(4) . . ?
B5 B9 H9A 122.1 . . ?
B5 B9 B10 59.8(3) . . ?
B10 B9 B3 108.1(4) . . ?
B10 B9 H9A 121.4 . . ?
B7 B10 B8 59.9(3) . . ?
B7 B10 B9 108.1(4) . . ?
B7 B10 H10A 121.8 . . ?
B6 B10 B7 59.5(3) . . ?
B6 B10 B8 107.2(4) . . ?
B6 B10 B5 60.3(3) . . ?
B6 B10 B9 108.1(4) . . ?
B6 B10 H10A 121.9 . . ?
B8 B10 B9 59.7(3) . . ?
B8 B10 H10A 122.4 . . ?
B5 B10 B7 107.7(4) . . ?
B5 B10 B8 107.0(4) . . ?
B5 B10 B9 59.7(3) . . ?
B5 B10 H10A 122.0 . . ?
B9 B10 H10A 121.6 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Au2 P2 C14 B1 43.5(4) . . . . ?
Au2 P2 C14 B2 -27.1(4) . . . . ?
Au2 P2 C14 B3 -96.7(4) . . . . ?
Au2 P2 C14 B7 113.6(4) . . . . ?
Au2 P2 C14 B8 -171.4(3) . . . . ?
Au2 P2 C15 C16 3.8(5) . . . . ?
Au2 P2 C15 C20 -173.3(5) . . . . ?
Au2 P2 C21 C22 -4.7(5) . . . . ?
Au2 P2 C21 C26 176.0(6) . . . . ?
Au1 P1 C13 B1 106.5(3) . . . . ?
Au1 P1 C13 B2 -178.4(3) . . . . ?
Au1 P1 C13 B6 37.5(4) . . . . ?
Au1 P1 C13 B4 -103.1(4) . . . . ?
Au1 P1 C13 B5 -31.4(4) . . . . ?
Au1 P1 C1 C2 167.4(4) . . . . ?
Au1 P1 C1 C6 -13.4(5) . . . . ?
Au1 P1 C7 C8 -19.2(5) . . . . ?
Au1 P1 C7 C12 164.2(5) . . . . ?
P2 C14 B1 C13 -146.3(3) . . . . ?
P2 C14 B1 B2 -106.3(4) . . . . ?
P2 C14 B1 B7 112.4(4) . . . . ?
P2 C14 B1 B6 152.3(3) . . . . ?
P2 C14 B2 C13 147.4(3) . . . . ?
P2 C14 B2 B1 107.1(4) . . . . ?
P2 C14 B2 B3 -111.4(4) . . . . ?
P2 C14 B2 B4 -151.0(3) . . . . ?
P2 C14 B3 B2 103.9(4) . . . . ?
P2 C14 B3 B4 143.8(4) . . . . ?
P2 C14 B3 B8 -114.9(4) . . . . ?
P2 C14 B3 B9 -153.7(3) . . . . ?
P2 C14 B7 B1 -104.0(4) . . . . ?
P2 C14 B7 B6 -143.9(4) . . . . ?
P2 C14 B7 B8 114.5(4) . . . . ?
P2 C14 B7 B10 153.6(4) . . . . ?
P2 C14 B8 B3 108.6(4) . . . . ?
P2 C14 B8 B7 -109.8(4) . . . . ?
P2 C14 B8 B9 148.1(4) . . . . ?
P2 C14 B8 B10 -149.0(4) . . . . ?
P2 C15 C16 C17 -178.3(4) . . . . ?
P2 C15 C20 C19 177.9(6) . . . . ?
P2 C21 C26 C25 -179.2(7) . . . . ?
P1 C13 B1 C14 156.0(3) . . . . ?
P1 C13 B1 B2 115.6(4) . . . . ?
P1 C13 B1 B7 -141.9(4) . . . . ?
P1 C13 B1 B6 -102.4(4) . . . . ?
P1 C13 B2 C14 -147.7(3) . . . . ?
P1 C13 B2 B1 -107.9(4) . . . . ?
P1 C13 B2 B3 150.8(3) . . . . ?
P1 C13 B2 B4 111.2(4) . . . . ?
P1 C13 B6 B1 111.1(4) . . . . ?
P1 C13 B6 B7 150.2(4) . . . . ?
P1 C13 B6 B5 -107.6(4) . . . . ?
P1 C13 B6 B10 -146.8(3) . . . . ?
P1 C13 B4 B2 -114.2(4) . . . . ?
P1 C13 B4 B3 -153.5(4) . . . . ?
P1 C13 B4 B5 104.1(4) . . . . ?
P1 C13 B4 B9 143.5(4) . . . . ?
P1 C13 B5 B6 104.1(4) . . . . ?
P1 C13 B5 B4 -114.1(4) . . . . ?
P1 C13 B5 B9 -153.7(3) . . . . ?
P1 C13 B5 B10 143.3(4) . . . . ?
P1 C1 C6 C5 179.3(6) . . . . ?
P1 C7 C8 C9 -176.1(6) . . . . ?
P1 C7 C12 C11 177.3(5) . . . . ?
C13 P1 C1 C2 -73.1(5) . . . . ?
C13 P1 C1 C6 106.1(5) . . . . ?
C13 P1 C7 C8 -142.1(5) . . . . ?
C13 P1 C7 C12 41.4(6) . . . . ?
C13 B1 B2 C14 132.4(4) . . . . ?
C13 B1 B2 B3 98.2(4) . . . . ?
C13 B1 B2 B4 34.9(4) . . . . ?
C13 B1 B7 C14 -95.5(4) . . . . ?
C13 B1 B7 B6 39.2(4) . . . . ?
C13 B1 B7 B8 -61.8(5) . . . . ?
C13 B1 B7 B10 1.7(5) . . . . ?
C13 B1 B6 B7 -135.1(4) . . . . ?
C13 B1 B6 B5 -34.1(4) . . . . ?
C13 B1 B6 B10 -97.5(4) . . . . ?
C13 B2 B3 C14 95.3(4) . . . . ?
C13 B2 B3 B4 -39.5(4) . . . . ?
C13 B2 B3 B8 61.3(5) . . . . ?
C13 B2 B3 B9 -1.7(5) . . . . ?
C13 B2 B4 B3 134.8(4) . . . . ?
C13 B2 B4 B5 33.7(4) . . . . ?
C13 B2 B4 B9 96.8(4) . . . . ?
C13 B6 B5 B4 -34.0(4) . . . . ?
C13 B6 B5 B9 -97.7(4) . . . . ?
C13 B6 B5 B10 -135.2(4) . . . . ?
C13 B6 B10 B7 -99.2(4) . . . . ?
C13 B6 B10 B8 -61.5(5) . . . . ?
C13 B6 B10 B5 38.6(4) . . . . ?
C13 B6 B10 B9 1.5(5) . . . . ?
C13 B4 B5 B6 34.0(4) . . . . ?
C13 B4 B5 B9 134.8(4) . . . . ?
C13 B4 B5 B10 97.4(4) . . . . ?
C13 B4 B9 B3 98.8(4) . . . . ?
C13 B4 B9 B8 61.6(5) . . . . ?
C13 B4 B9 B5 -38.9(3) . . . . ?
C13 B4 B9 B10 -1.9(5) . . . . ?
C13 B5 B9 B3 2.0(5) . . . . ?
C13 B5 B9 B4 39.3(4) . . . . ?
C13 B5 B9 B8 -61.2(5) . . . . ?
C13 B5 B9 B10 -99.3(4) . . . . ?
C13 B5 B10 B7 -1.6(5) . . . . ?
C13 B5 B10 B6 -38.9(4) . . . . ?
C13 B5 B10 B8 61.5(5) . . . . ?
C13 B5 B10 B9 99.4(4) . . . . ?
C14 P2 C15 C16 -116.0(4) . . . . ?
C14 P2 C15 C20 66.8(6) . . . . ?
C14 P2 C21 C22 114.9(4) . . . . ?
C14 P2 C21 C26 -64.4(7) . . . . ?
C14 B1 B2 C13 -132.4(4) . . . . ?
C14 B1 B2 B3 -34.2(3) . . . . ?
C14 B1 B2 B4 -97.5(4) . . . . ?
C14 B1 B7 B6 134.7(4) . . . . ?
C14 B1 B7 B8 33.8(4) . . . . ?
C14 B1 B7 B10 97.2(4) . . . . ?
C14 B1 B6 C13 95.3(4) . . . . ?
C14 B1 B6 B7 -39.9(4) . . . . ?
C14 B1 B6 B5 61.1(5) . . . . ?
C14 B1 B6 B10 -2.2(5) . . . . ?
C14 B2 B3 B4 -134.8(4) . . . . ?
C14 B2 B3 B8 -34.0(3) . . . . ?
C14 B2 B3 B9 -97.0(4) . . . . ?
C14 B2 B4 C13 -95.4(4) . . . . ?
C14 B2 B4 B3 39.4(4) . . . . ?
C14 B2 B4 B5 -61.7(5) . . . . ?
C14 B2 B4 B9 1.4(5) . . . . ?
C14 B3 B4 C13 -0.7(5) . . . . ?
C14 B3 B4 B2 -39.4(4) . . . . ?
C14 B3 B4 B5 60.7(5) . . . . ?
C14 B3 B4 B9 98.4(4) . . . . ?
C14 B3 B8 B7 -34.4(4) . . . . ?
C14 B3 B8 B9 -135.4(4) . . . . ?
C14 B3 B8 B10 -98.0(4) . . . . ?
C14 B3 B9 B4 -100.0(4) . . . . ?
C14 B3 B9 B8 38.2(4) . . . . ?
C14 B3 B9 B5 -62.2(5) . . . . ?
C14 B3 B9 B10 0.9(5) . . . . ?
C14 B7 B6 C13 0.2(5) . . . . ?
C14 B7 B6 B1 39.1(4) . . . . ?
C14 B7 B6 B5 -61.4(5) . . . . ?
C14 B7 B6 B10 -99.1(4) . . . . ?
C14 B7 B8 B3 34.3(4) . . . . ?
C14 B7 B8 B9 98.4(4) . . . . ?
C14 B7 B8 B10 135.4(4) . . . . ?
C14 B7 B10 B6 99.2(4) . . . . ?
C14 B7 B10 B8 -38.3(4) . . . . ?
C14 B7 B10 B5 61.5(5) . . . . ?
C14 B7 B10 B9 -1.6(5) . . . . ?
C14 B8 B9 B3 -38.9(4) . . . . ?
C14 B8 B9 B4 -2.0(5) . . . . ?
C14 B8 B9 B5 61.4(5) . . . . ?
C14 B8 B9 B10 99.4(4) . . . . ?
C14 B8 B10 B7 38.9(4) . . . . ?
C14 B8 B10 B6 1.4(5) . . . . ?
C14 B8 B10 B5 -62.0(5) . . . . ?
C14 B8 B10 B9 -99.9(4) . . . . ?
C22 C21 C26 C25 1.5(12) . . . . ?
C22 C23 C24 C25 0.7(11) . . . . ?
C15 P2 C14 B1 165.5(4) . . . . ?
C15 P2 C14 B2 94.9(4) . . . . ?
C15 P2 C14 B3 25.3(4) . . . . ?
C15 P2 C14 B7 -124.4(4) . . . . ?
C15 P2 C14 B8 -49.4(4) . . . . ?
C15 P2 C21 C22 -130.5(4) . . . . ?
C15 P2 C21 C26 50.2(7) . . . . ?
C15 C16 C17 C18 -0.8(9) . . . . ?
C15 C20 C19 C18 0.9(12) . . . . ?
C2 C1 C6 C5 -1.5(10) . . . . ?
C2 C3 C4 C5 -2.9(11) . . . . ?
C1 P1 C13 B1 -14.0(4) . . . . ?
C1 P1 C13 B2 61.1(4) . . . . ?
C1 P1 C13 B6 -83.0(4) . . . . ?
C1 P1 C13 B4 136.5(4) . . . . ?
C1 P1 C13 B5 -151.9(4) . . . . ?
C1 P1 C7 C8 104.0(5) . . . . ?
C1 P1 C7 C12 -72.5(6) . . . . ?
C1 C2 C3 C4 2.5(10) . . . . ?
C1 C6 C5 C4 1.1(12) . . . . ?
B1 C13 B2 C14 -39.9(4) . . . . ?
B1 C13 B2 B3 -101.3(4) . . . . ?
B1 C13 B2 B4 -140.9(4) . . . . ?
B1 C13 B6 B7 39.1(4) . . . . ?
B1 C13 B6 B5 141.3(4) . . . . ?
B1 C13 B6 B10 102.1(4) . . . . ?
B1 C13 B4 B2 37.7(4) . . . . ?
B1 C13 B4 B3 -1.6(6) . . . . ?
B1 C13 B4 B5 -104.0(4) . . . . ?
B1 C13 B4 B9 -64.6(5) . . . . ?
B1 C13 B5 B6 -36.4(4) . . . . ?
B1 C13 B5 B4 105.5(4) . . . . ?
B1 C13 B5 B9 65.8(5) . . . . ?
B1 C13 B5 B10 2.8(5) . . . . ?
B1 C14 B2 C13 40.4(3) . . . . ?
B1 C14 B2 B3 141.6(4) . . . . ?
B1 C14 B2 B4 101.9(4) . . . . ?
B1 C14 B3 B2 -37.1(4) . . . . ?
B1 C14 B3 B4 2.8(5) . . . . ?
B1 C14 B3 B8 104.2(4) . . . . ?
B1 C14 B3 B9 65.3(5) . . . . ?
B1 C14 B7 B6 -39.9(4) . . . . ?
B1 C14 B7 B8 -141.5(4) . . . . ?
B1 C14 B7 B10 -102.3(4) . . . . ?
B1 C14 B8 B3 -105.4(4) . . . . ?
B1 C14 B8 B7 36.2(4) . . . . ?
B1 C14 B8 B9 -65.9(5) . . . . ?
B1 C14 B8 B10 -3.0(5) . . . . ?
B1 B2 B3 C14 33.5(3) . . . . ?
B1 B2 B3 B4 -101.2(4) . . . . ?
B1 B2 B3 B8 -0.5(5) . . . . ?
B1 B2 B3 B9 -63.5(5) . . . . ?
B1 B2 B4 C13 -34.6(4) . . . . ?
B1 B2 B4 B3 100.2(4) . . . . ?
B1 B2 B4 B5 -0.9(5) . . . . ?
B1 B2 B4 B9 62.2(5) . . . . ?
B1 B7 B6 C13 -38.9(4) . . . . ?
B1 B7 B6 B5 -100.5(5) . . . . ?
B1 B7 B6 B10 -138.1(4) . . . . ?
B1 B7 B8 C14 -33.9(4) . . . . ?
B1 B7 B8 B3 0.4(5) . . . . ?
B1 B7 B8 B9 64.5(5) . . . . ?
B1 B7 B8 B10 101.5(5) . . . . ?
B1 B7 B10 B6 37.7(4) . . . . ?
B1 B7 B10 B8 -99.9(4) . . . . ?
B1 B7 B10 B5 0.0(6) . . . . ?
B1 B7 B10 B9 -63.1(5) . . . . ?
B1 B6 B5 C13 34.3(4) . . . . ?
B1 B6 B5 B4 0.3(6) . . . . ?
B1 B6 B5 B9 -63.4(5) . . . . ?
B1 B6 B5 B10 -100.9(5) . . . . ?
B1 B6 B10 B7 -37.2(4) . . . . ?
B1 B6 B10 B8 0.5(6) . . . . ?
B1 B6 B10 B5 100.6(4) . . . . ?
B1 B6 B10 B9 63.5(5) . . . . ?
C21 P2 C14 B1 -78.2(4) . . . . ?
C21 P2 C14 B2 -148.8(4) . . . . ?
C21 P2 C14 B3 141.5(4) . . . . ?
C21 P2 C14 B7 -8.1(5) . . . . ?
C21 P2 C14 B8 66.9(4) . . . . ?
C21 P2 C15 C16 129.5(4) . . . . ?
C21 P2 C15 C20 -47.6(6) . . . . ?
C21 C22 C23 C24 0.0(9) . . . . ?
C21 C26 C25 C24 -0.9(15) . . . . ?
C7 P1 C13 B1 -129.3(4) . . . . ?
C7 P1 C13 B2 -54.2(4) . . . . ?
C7 P1 C13 B6 161.7(4) . . . . ?
C7 P1 C13 B4 21.2(5) . . . . ?
C7 P1 C13 B5 92.8(4) . . . . ?
C7 P1 C1 C2 43.6(5) . . . . ?
C7 P1 C1 C6 -137.2(5) . . . . ?
C7 C8 C9 C10 -2.3(11) . . . . ?
C7 C12 C11 C10 -1.0(9) . . . . ?
C3 C2 C1 P1 179.0(5) . . . . ?
C3 C2 C1 C6 -0.2(9) . . . . ?
B2 C13 B1 C14 40.4(4) . . . . ?
B2 C13 B1 B7 102.5(4) . . . . ?
B2 C13 B1 B6 142.0(4) . . . . ?
B2 C13 B6 B1 -36.8(4) . . . . ?
B2 C13 B6 B7 2.3(6) . . . . ?
B2 C13 B6 B5 104.6(4) . . . . ?
B2 C13 B6 B10 65.3(5) . . . . ?
B2 C13 B4 B3 -39.3(4) . . . . ?
B2 C13 B4 B5 -141.7(4) . . . . ?
B2 C13 B4 B9 -102.3(4) . . . . ?
B2 C13 B5 B6 -105.4(4) . . . . ?
B2 C13 B5 B4 36.4(4) . . . . ?
B2 C13 B5 B9 -3.2(5) . . . . ?
B2 C13 B5 B10 -66.2(5) . . . . ?
B2 C14 B1 C13 -40.0(3) . . . . ?
B2 C14 B1 B7 -141.3(4) . . . . ?
B2 C14 B1 B6 -101.4(4) . . . . ?
B2 C14 B3 B4 39.9(4) . . . . ?
B2 C14 B3 B8 141.2(4) . . . . ?
B2 C14 B3 B9 102.4(4) . . . . ?
B2 C14 B7 B1 37.3(4) . . . . ?
B2 C14 B7 B6 -2.6(5) . . . . ?
B2 C14 B7 B8 -104.2(4) . . . . ?
B2 C14 B7 B10 -65.0(5) . . . . ?
B2 C14 B8 B3 -36.4(4) . . . . ?
B2 C14 B8 B7 105.2(4) . . . . ?
B2 C14 B8 B9 3.0(5) . . . . ?
B2 C14 B8 B10 66.0(5) . . . . ?
B2 B1 B7 C14 -34.5(4) . . . . ?
B2 B1 B7 B6 100.3(4) . . . . ?
B2 B1 B7 B8 -0.7(5) . . . . ?
B2 B1 B7 B10 62.8(5) . . . . ?
B2 B1 B6 C13 33.3(4) . . . . ?
B2 B1 B6 B7 -101.8(4) . . . . ?
B2 B1 B6 B5 -0.8(5) . . . . ?
B2 B1 B6 B10 -64.2(5) . . . . ?
B2 B3 B4 C13 38.7(4) . . . . ?
B2 B3 B4 B5 100.1(4) . . . . ?
B2 B3 B4 B9 137.8(4) . . . . ?
B2 B3 B8 C14 34.4(4) . . . . ?
B2 B3 B8 B7 0.0(5) . . . . ?
B2 B3 B8 B9 -101.0(4) . . . . ?
B2 B3 B8 B10 -63.6(5) . . . . ?
B2 B3 B9 B4 -37.9(4) . . . . ?
B2 B3 B9 B8 100.3(4) . . . . ?
B2 B3 B9 B5 -0.2(5) . . . . ?
B2 B3 B9 B10 63.0(5) . . . . ?
B2 B4 B5 C13 -33.6(4) . . . . ?
B2 B4 B5 B6 0.4(6) . . . . ?
B2 B4 B5 B9 101.2(4) . . . . ?
B2 B4 B5 B10 63.8(5) . . . . ?
B2 B4 B9 B3 37.6(4) . . . . ?
B2 B4 B9 B8 0.4(5) . . . . ?
B2 B4 B9 B5 -100.1(4) . . . . ?
B2 B4 B9 B10 -63.1(5) . . . . ?
C16 C15 C20 C19 0.9(10) . . . . ?
B3 C14 B1 C13 -3.6(5) . . . . ?
B3 C14 B1 B2 36.4(4) . . . . ?
B3 C14 B1 B7 -105.0(4) . . . . ?
B3 C14 B1 B6 -65.1(5) . . . . ?
B3 C14 B2 C13 -101.2(4) . . . . ?
B3 C14 B2 B1 -141.6(4) . . . . ?
B3 C14 B2 B4 -39.6(4) . . . . ?
B3 C14 B7 B1 104.6(4) . . . . ?
B3 C14 B7 B6 64.7(5) . . . . ?
B3 C14 B7 B8 -36.9(4) . . . . ?
B3 C14 B7 B10 2.3(6) . . . . ?
B3 C14 B8 B7 141.6(4) . . . . ?
B3 C14 B8 B9 39.5(4) . . . . ?
B3 C14 B8 B10 102.4(4) . . . . ?
B3 B2 B4 C13 -134.8(4) . . . . ?
B3 B2 B4 B5 -101.1(5) . . . . ?
B3 B2 B4 B9 -38.0(4) . . . . ?
B3 B4 B5 C13 -96.7(4) . . . . ?
B3 B4 B5 B6 -62.6(5) . . . . ?
B3 B4 B5 B9 38.1(4) . . . . ?
B3 B4 B5 B10 0.8(6) . . . . ?
B3 B4 B9 B8 -37.2(4) . . . . ?
B3 B4 B9 B5 -137.7(4) . . . . ?
B3 B4 B9 B10 -100.7(4) . . . . ?
B3 B8 B9 B4 36.9(4) . . . . ?
B3 B8 B9 B5 100.4(5) . . . . ?
B3 B8 B9 B10 138.4(4) . . . . ?
B3 B8 B10 B7 101.3(4) . . . . ?
B3 B8 B10 B6 63.8(5) . . . . ?
B3 B8 B10 B5 0.4(6) . . . . ?
B3 B8 B10 B9 -37.5(4) . . . . ?
B3 B9 B10 B7 0.4(6) . . . . ?
B3 B9 B10 B6 -62.5(5) . . . . ?
B3 B9 B10 B8 37.2(4) . . . . ?
B3 B9 B10 B5 -99.9(5) . . . . ?
B7 C14 B1 C13 101.3(4) . . . . ?
B7 C14 B1 B2 141.3(4) . . . . ?
B7 C14 B1 B6 39.9(4) . . . . ?
B7 C14 B2 C13 3.8(5) . . . . ?
B7 C14 B2 B1 -36.5(4) . . . . ?
B7 C14 B2 B3 105.0(4) . . . . ?
B7 C14 B2 B4 65.4(5) . . . . ?
B7 C14 B3 B2 -104.4(4) . . . . ?
B7 C14 B3 B4 -64.5(5) . . . . ?
B7 C14 B3 B8 36.8(4) . . . . ?
B7 C14 B3 B9 -2.0(5) . . . . ?
B7 C14 B8 B3 -141.6(4) . . . . ?
B7 C14 B8 B9 -102.1(4) . . . . ?
B7 C14 B8 B10 -39.2(4) . . . . ?
B7 B1 B2 C13 -97.5(4) . . . . ?
B7 B1 B2 C14 34.9(4) . . . . ?
B7 B1 B2 B3 0.7(5) . . . . ?
B7 B1 B2 B4 -62.6(5) . . . . ?
B7 B1 B6 C13 135.1(4) . . . . ?
B7 B1 B6 B5 101.0(5) . . . . ?
B7 B1 B6 B10 37.7(4) . . . . ?
B7 B6 B5 C13 97.3(4) . . . . ?
B7 B6 B5 B4 63.2(5) . . . . ?
B7 B6 B5 B9 -0.4(6) . . . . ?
B7 B6 B5 B10 -37.9(4) . . . . ?
B7 B6 B10 B8 37.7(4) . . . . ?
B7 B6 B10 B5 137.9(4) . . . . ?
B7 B6 B10 B9 100.7(4) . . . . ?
B7 B8 B9 B3 -101.4(4) . . . . ?
B7 B8 B9 B4 -64.5(5) . . . . ?
B7 B8 B9 B5 -1.1(6) . . . . ?
B7 B8 B9 B10 36.9(4) . . . . ?
B7 B8 B10 B6 -37.5(4) . . . . ?
B7 B8 B10 B5 -100.9(5) . . . . ?
B7 B8 B10 B9 -138.8(4) . . . . ?
C8 C7 C12 C11 0.9(9) . . . . ?
C8 C9 C10 C11 2.1(11) . . . . ?
C6 C5 C4 C3 1.1(12) . . . . ?
B6 C13 B1 C14 -101.6(4) . . . . ?
B6 C13 B1 B2 -142.0(4) . . . . ?
B6 C13 B1 B7 -39.5(4) . . . . ?
B6 C13 B2 C14 -3.7(5) . . . . ?
B6 C13 B2 B1 36.1(4) . . . . ?
B6 C13 B2 B3 -65.2(5) . . . . ?
B6 C13 B2 B4 -104.8(5) . . . . ?
B6 C13 B4 B2 105.3(4) . . . . ?
B6 C13 B4 B3 66.0(5) . . . . ?
B6 C13 B4 B5 -36.4(4) . . . . ?
B6 C13 B4 B9 2.9(5) . . . . ?
B6 C13 B5 B4 141.9(4) . . . . ?
B6 C13 B5 B9 102.2(4) . . . . ?
B6 C13 B5 B10 39.2(4) . . . . ?
B6 B1 B2 C13 -33.8(4) . . . . ?
B6 B1 B2 C14 98.5(4) . . . . ?
B6 B1 B2 B3 64.4(5) . . . . ?
B6 B1 B2 B4 1.1(5) . . . . ?
B6 B1 B7 C14 -134.7(4) . . . . ?
B6 B1 B7 B8 -100.9(4) . . . . ?
B6 B1 B7 B10 -37.5(4) . . . . ?
B6 B7 B8 C14 -97.6(4) . . . . ?
B6 B7 B8 B3 -63.2(5) . . . . ?
B6 B7 B8 B9 0.8(5) . . . . ?
B6 B7 B8 B10 37.9(4) . . . . ?
B6 B7 B10 B8 -137.5(4) . . . . ?
B6 B7 B10 B5 -37.7(4) . . . . ?
B6 B7 B10 B9 -100.8(5) . . . . ?
B6 B5 B9 B3 64.1(5) . . . . ?
B6 B5 B9 B4 101.4(4) . . . . ?
B6 B5 B9 B8 0.9(6) . . . . ?
B6 B5 B9 B10 -37.2(4) . . . . ?
B6 B5 B10 B7 37.3(4) . . . . ?
B6 B5 B10 B8 100.5(4) . . . . ?
B6 B5 B10 B9 138.3(4) . . . . ?
C12 C7 C8 C9 0.7(10) . . . . ?
C12 C11 C10 C9 -0.5(10) . . . . ?
C20 C15 C16 C17 -1.0(9) . . . . ?
C19 C18 C17 C16 2.6(10) . . . . ?
C17 C18 C19 C20 -2.7(11) . . . . ?
C23 C22 C21 P2 179.6(5) . . . . ?
C23 C22 C21 C26 -1.1(9) . . . . ?
C23 C24 C25 C26 -0.3(13) . . . . ?
B4 C13 B1 C14 3.2(5) . . . . ?
B4 C13 B1 B2 -37.3(4) . . . . ?
B4 C13 B1 B7 65.2(5) . . . . ?
B4 C13 B1 B6 104.7(5) . . . . ?
B4 C13 B2 C14 101.1(4) . . . . ?
B4 C13 B2 B1 140.9(4) . . . . ?
B4 C13 B2 B3 39.6(4) . . . . ?
B4 C13 B6 B1 -104.9(4) . . . . ?
B4 C13 B6 B7 -65.8(5) . . . . ?
B4 C13 B6 B5 36.4(4) . . . . ?
B4 C13 B6 B10 -2.8(5) . . . . ?
B4 C13 B5 B6 -141.9(4) . . . . ?
B4 C13 B5 B9 -39.7(4) . . . . ?
B4 C13 B5 B10 -102.7(4) . . . . ?
B4 B2 B3 C14 134.8(4) . . . . ?
B4 B2 B3 B8 100.8(4) . . . . ?
B4 B2 B3 B9 37.8(4) . . . . ?
B4 B3 B8 C14 98.1(4) . . . . ?
B4 B3 B8 B7 63.7(5) . . . . ?
B4 B3 B8 B9 -37.3(4) . . . . ?
B4 B3 B8 B10 0.1(5) . . . . ?
B4 B3 B9 B8 138.2(4) . . . . ?
B4 B3 B9 B5 37.7(4) . . . . ?
B4 B3 B9 B10 100.9(4) . . . . ?
B4 B5 B9 B3 -37.3(4) . . . . ?
B4 B5 B9 B8 -100.5(4) . . . . ?
B4 B5 B9 B10 -138.6(4) . . . . ?
B4 B5 B10 B7 -63.8(5) . . . . ?
B4 B5 B10 B6 -101.1(4) . . . . ?
B4 B5 B10 B8 -0.7(6) . . . . ?
B4 B5 B10 B9 37.2(4) . . . . ?
B4 B9 B10 B7 63.1(5) . . . . ?
B4 B9 B10 B6 0.2(5) . . . . ?
B4 B9 B10 B8 100.0(4) . . . . ?
B4 B9 B10 B5 -37.2(4) . . . . ?
B8 C14 B1 C13 64.7(5) . . . . ?
B8 C14 B1 B2 104.7(4) . . . . ?
B8 C14 B1 B7 -36.6(4) . . . . ?
B8 C14 B1 B6 3.3(5) . . . . ?
B8 C14 B2 C13 -64.3(5) . . . . ?
B8 C14 B2 B1 -104.7(4) . . . . ?
B8 C14 B2 B3 36.9(4) . . . . ?
B8 C14 B2 B4 -2.8(5) . . . . ?
B8 C14 B3 B2 -141.2(4) . . . . ?
B8 C14 B3 B4 -101.4(4) . . . . ?
B8 C14 B3 B9 -38.8(4) . . . . ?
B8 C14 B7 B1 141.5(4) . . . . ?
B8 C14 B7 B6 101.6(4) . . . . ?
B8 C14 B7 B10 39.1(4) . . . . ?
B8 B3 B4 C13 -61.9(5) . . . . ?
B8 B3 B4 B2 -100.6(4) . . . . ?
B8 B3 B4 B5 -0.5(5) . . . . ?
B8 B3 B4 B9 37.2(4) . . . . ?
B8 B3 B9 B4 -138.2(4) . . . . ?
B8 B3 B9 B5 -100.4(5) . . . . ?
B8 B3 B9 B10 -37.3(4) . . . . ?
B8 B7 B6 C13 61.3(5) . . . . ?
B8 B7 B6 B1 100.2(4) . . . . ?
B8 B7 B6 B5 -0.2(5) . . . . ?
B8 B7 B6 B10 -37.9(4) . . . . ?
B8 B7 B10 B6 137.5(4) . . . . ?
B8 B7 B10 B5 99.8(5) . . . . ?
B8 B7 B10 B9 36.7(4) . . . . ?
B8 B9 B10 B7 -36.8(4) . . . . ?
B8 B9 B10 B6 -99.8(4) . . . . ?
B8 B9 B10 B5 -137.2(4) . . . . ?
B5 C13 B1 C14 -64.9(5) . . . . ?
B5 C13 B1 B2 -105.3(4) . . . . ?
B5 C13 B1 B7 -2.8(5) . . . . ?
B5 C13 B1 B6 36.7(4) . . . . ?
B5 C13 B2 C14 64.6(5) . . . . ?
B5 C13 B2 B1 104.4(4) . . . . ?
B5 C13 B2 B3 3.1(5) . . . . ?
B5 C13 B2 B4 -36.5(4) . . . . ?
B5 C13 B6 B1 -141.3(4) . . . . ?
B5 C13 B6 B7 -102.3(4) . . . . ?
B5 C13 B6 B10 -39.2(4) . . . . ?
B5 C13 B4 B2 141.7(4) . . . . ?
B5 C13 B4 B3 102.4(4) . . . . ?
B5 C13 B4 B9 39.4(4) . . . . ?
B5 B6 B10 B7 -137.9(4) . . . . ?
B5 B6 B10 B8 -100.2(5) . . . . ?
B5 B6 B10 B9 -37.2(4) . . . . ?
B5 B4 B9 B3 137.7(4) . . . . ?
B5 B4 B9 B8 100.5(4) . . . . ?
B5 B4 B9 B10 37.0(4) . . . . ?
B5 B9 B10 B7 100.3(5) . . . . ?
B5 B9 B10 B6 37.4(4) . . . . ?
B5 B9 B10 B8 137.2(4) . . . . ?
B9 B3 B4 C13 -99.1(4) . . . . ?
B9 B3 B4 B2 -137.8(4) . . . . ?
B9 B3 B4 B5 -37.7(4) . . . . ?
B9 B3 B8 C14 135.4(4) . . . . ?
B9 B3 B8 B7 101.1(4) . . . . ?
B9 B3 B8 B10 37.5(4) . . . . ?
B9 B4 B5 C13 -134.8(4) . . . . ?
B9 B4 B5 B6 -100.8(4) . . . . ?
B9 B4 B5 B10 -37.4(4) . . . . ?
B9 B8 B10 B7 138.8(4) . . . . ?
B9 B8 B10 B6 101.3(5) . . . . ?
B9 B8 B10 B5 37.9(4) . . . . ?
B9 B5 B10 B7 -101.0(4) . . . . ?
B9 B5 B10 B6 -138.3(4) . . . . ?
B9 B5 B10 B8 -37.9(4) . . . . ?
B10 B7 B6 C13 99.2(4) . . . . ?
B10 B7 B6 B1 138.1(4) . . . . ?
B10 B7 B6 B5 37.7(4) . . . . ?
B10 B7 B8 C14 -135.4(4) . . . . ?
B10 B7 B8 B3 -101.1(4) . . . . ?
B10 B7 B8 B9 -37.0(4) . . . . ?
B10 B6 B5 C13 135.2(4) . . . . ?
B10 B6 B5 B4 101.2(4) . . . . ?
B10 B6 B5 B9 37.5(4) . . . . ?
B10 B8 B9 B3 -138.4(4) . . . . ?
B10 B8 B9 B4 -101.4(4) . . . . ?
B10 B8 B9 B5 -38.0(4) . . . . ?
B10 B5 B9 B3 101.3(4) . . . . ?
B10 B5 B9 B4 138.6(4) . . . . ?
B10 B5 B9 B8 38.1(4) . . . . ?

_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
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# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
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data_mo_xhh25041
_database_code_depnum_ccdc_archive 'CCDC 2454647'
loop_
_audit_author_name
_audit_author_address
'Haohui Xie'
;NanJing University of Science and Technology
China
;
_audit_update_record             
;
2025-05-28 deposited with the CCDC.	2026-03-06 downloaded from the CCDC.
;
# start Validation Reply Form
_vrf_THETM01_mo_xhh25041         
;
PROBLEM: The value of sine(theta_max)/wavelength is less than 0.550
RESPONSE: poor quantities of crystals.
;
_vrf_PLAT971_mo_xhh25041         
;
PROBLEM: Check Calcd Resid. Dens.  0.25Ang From Au2             5.01 eA-3
RESPONSE: The relatively large residual density is close to heavy gold atoms.
;
_vrf_PLAT972_mo_xhh25041         
;
PROBLEM: Check Calcd Resid. Dens.  0.94Ang From Au3            -4.69 eA-3
RESPONSE: The relatively large residual density is close to heavy gold atoms.
;
_vrf_PLAT973_mo_xhh25041         
;
PROBLEM: Check Calcd Positive Resid. Density on       Au7       6.27 eA-3
RESPONSE: The relatively large residual density is close to heavy gold atoms.
;
_vrf_RINTA01_mo_xhh25041         
;
PROBLEM: The value of Rint is greater than 0.18
RESPONSE: poor quantities of crystals.
;
_vrf_PLAT020_mo_xhh25041         
;
PROBLEM: The Value of Rint is Greater Than 0.12 .........      0.226 Report
RESPONSE: poor quantities of crystals.
;
_vrf_PLAT342_mo_xhh25041         
;
PROBLEM: Low Bond Precision on  C-C Bonds ...............    0.05486 Ang.
RESPONSE: Because of heavy gold atoms.
;
_vrf_PLAT971_mo_xhh25041_2       
;
PROBLEM: Check Calcd Resid. Dens.  0.96Ang From Au7             3.31 eA-3
RESPONSE: The relatively large residual density is close to heavy gold atoms.
;
_vrf_PLAT972_mo_xhh25041_2       
;
PROBLEM: Check Calcd Resid. Dens.  1.14Ang From Au3            -3.49 eA-3
RESPONSE: The relatively large residual density is close to heavy gold atoms.
;
# Added during the CSD deposition process: Wednesday 28 May 2025 04:04 AM
# end Validation Reply Form

_audit_creation_date             2025-05-28
_audit_creation_method           
;
Olex2 1.5
(compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C156 H180 Au18 B60 P12 S8, 2(Cl)'
_chemical_formula_sum            'C156 H180 Au18 B60 Cl2 P12 S8'
_chemical_formula_weight         6948.01
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   17.012(5)
_cell_length_b                   18.535(5)
_cell_length_c                   19.375(5)
_cell_angle_alpha                101.561(6)
_cell_angle_beta                 109.044(6)
_cell_angle_gamma                104.722(6)
_cell_volume                     5310(2)
_cell_formula_units_Z            1
_cell_measurement_reflns_used    5959
_cell_measurement_temperature    296.00
_cell_measurement_theta_max      21.221
_cell_measurement_theta_min      2.478
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    12.614
_exptl_absorpt_correction_T_max  0.7446
_exptl_absorpt_correction_T_min  0.2767
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1658 before and 0.1102 after correction.
The Ratio of minimum to maximum transmission is 0.3716.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.173
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       blcok
_exptl_crystal_F_000             3180
_exptl_crystal_size_max          0.075
_exptl_crystal_size_mid          0.068
_exptl_crystal_size_min          0.056
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.2264
_diffrn_reflns_av_unetI/netI     0.1486
_diffrn_reflns_Laue_measured_fraction_full 0.980
_diffrn_reflns_Laue_measured_fraction_max 0.980
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            82652
_diffrn_reflns_point_group_measured_fraction_full 0.980
_diffrn_reflns_point_group_measured_fraction_max 0.980
_diffrn_reflns_theta_full        21.373
_diffrn_reflns_theta_max         21.373
_diffrn_reflns_theta_min         1.899
_diffrn_ambient_temperature      296.00
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.980
_diffrn_measured_fraction_theta_max 0.980
_diffrn_measurement_device_type  multi-scan
_diffrn_measurement_method       ?
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_source_current           1.6
_diffrn_source_power             0.08
_diffrn_source_voltage           50.0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                6951
_reflns_number_total             11765
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.40B (?, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.40B (?, 2016)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'olex2.solve 1.5 (Bourhis et al., 2015)'
_refine_diff_density_max         4.479
_refine_diff_density_min         -4.566
_refine_diff_density_rms         0.484
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.066
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1009
_refine_ls_number_reflns         11765
_refine_ls_number_restraints     1022
_refine_ls_R_factor_all          0.1793
_refine_ls_R_factor_gt           0.1129
_refine_ls_restrained_S_all      1.022
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1791P)²+272.9688P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2631
_refine_ls_wR_factor_ref         0.3393
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups
2. Restrained distances
 P2-C78
 2.7 with sigma of 0.02
 P2-C74
 2.7 with sigma of 0.02
3. Uiso/Uaniso restraints and constraints
C55 \\sim C55 \\sim C28 \\sim C27 \\sim C32 \\sim P6 \\sim C31 \\sim C30 \\sim
C29: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A
P6 \\sim C10 \\sim C20 \\sim C19 \\sim C18 \\sim C17 \\sim C7: within 2A with
sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A
C21 \\sim C22 \\sim C23 \\sim C24 \\sim C25 \\sim C26 \\sim P6: within 2A with
sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A
C1 \\sim C6 \\sim C5 \\sim C4 \\sim C3 \\sim C2 \\sim P1: within 2A with sigma
of 0.04 and sigma for terminal atoms of 0.08 within 2A
C71 \\sim C70 \\sim C69 \\sim C68 \\sim C67 \\sim C72 \\sim P2: within 2A with
sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A
C67 \\sim C68 \\sim P2: within 2A with sigma of 0.04 and sigma for terminal
atoms of 0.08 within 2A
C45 \\sim C44 \\sim C43 \\sim C42 \\sim C41 \\sim C46 \\sim P4: within 2A with
sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A
C42 \\sim C41 \\sim C43: within 2A with sigma of 0.001 and sigma for terminal
atoms of 0.002 within 2A
C37 \\sim C36 \\sim C35 \\sim C34 \\sim C33 \\sim P5 \\sim C38: within 2A with
sigma of 0.001 and sigma for terminal atoms of 0.002 within 2A
C38 \\sim C33 \\sim C34: within 2A with sigma of 0.001 and sigma for terminal
atoms of 0.002 within 2A
C8 \\sim C9 \\sim B2 \\sim B10 \\sim B1 \\sim B9 \\sim B6 \\sim B3 \\sim B4
\\sim B5 \\sim B7 \\sim B8: within 2A with sigma of 0.001 and sigma for
terminal atoms of 0.002 within 2A
B7 \\sim C8 \\sim B8 \\sim B5: within 2A with sigma of 0.001 and sigma for
terminal atoms of 0.002 within 2A
B29 \\sim B28 \\sim B27 \\sim C65 \\sim B30 \\sim B31 \\sim B32 \\sim C66 \\sim
B33 \\sim B34 \\sim B36 \\sim B35 \\sim P2 \\sim P3: within 2A with sigma of
0.001 and sigma for terminal atoms of 0.002 within 2A
C59 \\sim P3 \\sim C53 \\sim C54 \\sim C55 \\sim C56 \\sim C57 \\sim C58:
within 2A with sigma of 0.001 and sigma for terminal atoms of 0.002 within 2A
C58 \\sim C53 \\sim C57: within 2A with sigma of 0.001 and sigma for terminal
atoms of 0.002 within 2A
C16 \\sim C14 \\sim C15 \\sim C11 \\sim C12 \\sim C13 \\sim P1: within 2A with
sigma of 0.001 and sigma for terminal atoms of 0.002 within 2A
C16 \\sim C11 \\sim C15 \\sim C14 \\sim C13 \\sim C12 \\sim P1: within 2A with
sigma of 0.001 and sigma for terminal atoms of 0.002 within 2A
C78 \\sim C77 \\sim C76 \\sim C75 \\sim C74 \\sim C73 \\sim P2: within 2A with
sigma of 0.001 and sigma for terminal atoms of 0.002 within 2A
C75 \\sim C74 \\sim C76 \\sim C77 \\sim C78 \\sim C73 \\sim P2: within 2A with
sigma of 0.001 and sigma for terminal atoms of 0.002 within 2A
B7 \\sim B3 \\sim C8 \\sim B9 \\sim B6 \\sim B8: within 2A with sigma of 0.001
and sigma for terminal atoms of 0.002 within 2A
B7 \\sim C8 \\sim B9 \\sim B1 \\sim P1: within 2A with sigma of 0.001 and sigma
for terminal atoms of 0.002 within 2A
B21 \\sim B23 \\sim B22 \\sim B19 \\sim B20 \\sim B26: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
B24 \\sim B22 \\sim B23 \\sim B25 \\sim B26 \\sim B21 \\sim B19 \\sim B20 \\sim
B18 \\sim C40 \\sim C39: within 2A with sigma of 0.01 and sigma for terminal
atoms of 0.02 within 2A
C67 \\sim C68 \\sim C72 \\sim C71 \\sim C70 \\sim C69: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
C49 \\sim C48 \\sim C47 \\sim C52 \\sim C51 \\sim C50: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
C62 \\sim C63 \\sim C64 \\sim C59 \\sim C60 \\sim C61: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
4.a Aromatic/amide H refined with riding coordinates:
 C42(H42), C43(H43), C44(H44), C45(H45), C46(H46), C22(H22A), C26(H26A),
 C25(H25A), C24(H24A), C23(H23A), C7(H7), C17(H17A), C18(H18A), C19(H19A),
 C20(H20A), C60(H60), C61(H61), C62(H62), C63(H63), C64(H64), C54(H54),
 C55(H55), C56(H56), C57(H57), C58(H58), C68(H68), C69(H69), C70(H70), C71(H71),
  C72(H72), C49(H49), C48(H48), C52(H52), C51(H51), C50(H50), C74(H74),
 C78(H78), C77(H77), C76(H76), C75(H75), C2(H2A), C6(H6A), C5(H5A), C4(H4A),
 C3(H3A), C15(H15), C14(H14), C13(H13), C11(H11), C16(H16), C28(H28A),
 C29(H29A), C30(H30A), C31(H31A), C32(H32), C37(H37), C36(H36), C35(H35),
 C34(H34), C38(H38)
4.b Fitted hexagon refined as free rotating group:
 C42(C43,C44,C45,C46,C41), C22(C21,C26,C25,C24,C23), C7(C17,C18,C19,C20,C10),
 C59(C60,C61,C62,C63,C64), C54(C55,C56,C57,C58,C53), C67(C68,C69,C70,C71,C72),
 C49(C48,C47,C52,C51,C50), C74(C73,C78,C77,C76,C75), C2(C1,C6,C5,C4,C3),
 C15(C14,C13,C12,C11,C16), C28(C29,C30,C31,C32,C27), C37(C36,C35,C34,C33,C38)
4.c Boron cage BH refined with riding coordinates:
 B2(H2), B29(H29), B28(H28), B18(H18), B17(H17), B24(H24), B19(H19), B27(H27),
 B10(H10), B26(H26), B1(H1), B25(H25), B9(H9), B30(H30), B31(H31), B20(H20),
 B22(H22), B21(H21), B6(H6), B3(H3), B4(H4), B23(H23), B5(H5), B32(H32A),
 B33(H33), B34(H34A), B36(H36A), B35(H35A), B7(H7A), B8(H8)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     iterative
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au1 Au 0.57464(12) 0.46014(10) 0.26280(10) 0.0560(5) Uani 1 1 d . . . . .
Au7 Au 0.61933(12) 0.57676(10) 0.60746(10) 0.0572(5) Uani 1 1 d . . . . .
Au3 Au 0.58317(13) 0.52436(10) 0.42433(10) 0.0596(6) Uani 1 1 d . . . . .
Au4 Au 0.53519(13) 0.38365(10) 0.51144(10) 0.0620(6) Uani 1 1 d . . . . .
Au2 Au 0.67185(13) 0.64065(10) 0.35212(11) 0.0603(6) Uani 1 1 d . . . . .
Au8 Au 0.68696(13) 0.62701(11) 0.78609(11) 0.0611(6) Uani 1 1 d . . . . .
Au9 Au 0.74291(13) 0.74155(10) 0.69790(11) 0.0621(6) Uani 1 1 d . . . . .
Au5 Au 0.48714(15) 0.19955(10) 0.42625(11) 0.0675(6) Uani 1 1 d . . . . .
Au6 Au 0.54315(13) 0.27085(10) 0.60565(11) 0.0638(6) Uani 1 1 d . . . . .
S4 S 0.6050(7) 0.6725(7) 0.6947(7) 0.057(3) Uani 1 1 d . . . . .
S3 S 0.4289(8) 0.2667(6) 0.4992(7) 0.062(3) Uani 1 1 d . . . . .
S2 S 0.6550(9) 0.4919(7) 0.5295(7) 0.068(3) Uani 1 1 d . . . . .
P2 P 0.6154(10) 0.3656(7) 0.2047(8) 0.0744(16) Uani 1 1 d D U . . .
P4 P 0.6378(9) 0.2629(7) 0.7132(7) 0.064(3) Uani 1 1 d . U . . .
P1 P 0.8152(9) 0.7148(8) 0.3869(8) 0.074(2) Uani 1 1 d . U . . .
S1 S 0.5277(8) 0.5593(6) 0.3122(8) 0.065(3) Uani 1 1 d . . . . .
P6 P 0.8817(9) 0.8015(8) 0.7105(8) 0.071(4) Uani 1 1 d . U . . .
P5 P 0.7662(11) 0.5901(10) 0.8821(9) 0.087(3) Uani 1 1 d . U . . .
P3 P 0.5372(10) 0.1325(8) 0.3490(8) 0.0757(16) Uani 1 1 d . U . . .
C8 C 0.856(3) 0.794(3) 0.481(3) 0.074(2) Uani 1 1 d . U . . .
C39 C 0.798(3) 0.505(3) 0.848(3) 0.063(6) Uani 1 1 d . U . . .
C9 C 0.885(3) 0.835(3) 0.625(3) 0.074(2) Uani 1 1 d . U . . .
B2 B 0.924(4) 0.784(3) 0.564(3) 0.074(2) Uani 1 1 d . U . . .
H2 H 0.948885 0.735905 0.570045 0.089 Uiso 1 1 calc R U . . .
C40 C 0.732(3) 0.353(3) 0.769(3) 0.061(6) Uani 1 1 d . U . . .
B29 B 0.596(5) 0.205(3) 0.241(4) 0.0750(16) Uani 1 1 d . U . . .
H29 H 0.535340 0.167793 0.190765 0.090 Uiso 1 1 calc R U . . .
B28 B 0.604(5) 0.281(3) 0.322(3) 0.0750(16) Uani 1 1 d . U . . .
H28 H 0.540291 0.288069 0.315468 0.090 Uiso 1 1 calc R U . . .
B18 B 0.744(3) 0.415(3) 0.849(3) 0.060(6) Uani 1 1 d . U . . .
H18 H 0.695678 0.404475 0.875710 0.073 Uiso 1 1 calc R U . . .
B17 B 0.716(4) 0.436(3) 0.758(3) 0.063(15) Uani 1 1 d . . . . .
H17 H 0.651659 0.438727 0.724099 0.076 Uiso 1 1 calc R U . . .
B24 B 0.822(3) 0.502(3) 0.764(3) 0.064(6) Uani 1 1 d . U . . .
H24 H 0.824378 0.547652 0.734854 0.077 Uiso 1 1 calc R U . . .
B19 B 0.861(3) 0.463(3) 0.912(3) 0.062(5) Uani 1 1 d . U . . .
H19 H 0.888217 0.480900 0.974680 0.074 Uiso 1 1 calc R U . . .
B27 B 0.688(4) 0.292(3) 0.412(4) 0.0750(16) Uani 1 1 d . U . . .
H27 H 0.680148 0.307564 0.466332 0.090 Uiso 1 1 calc R U . . .
C65 C 0.630(4) 0.209(3) 0.342(3) 0.0751(16) Uani 1 1 d . U . . .
B10 B 0.799(4) 0.871(3) 0.581(3) 0.074(2) Uani 1 1 d . U . . .
H10 H 0.748514 0.878859 0.602740 0.089 Uiso 1 1 calc R U . . .
B26 B 0.835(3) 0.351(3) 0.767(3) 0.062(5) Uani 1 1 d . U . . .
H26 H 0.845712 0.298403 0.740335 0.074 Uiso 1 1 calc R U . . .
B1 B 0.803(4) 0.774(4) 0.537(3) 0.074(2) Uani 1 1 d . U . . .
H1 H 0.753077 0.717627 0.527569 0.089 Uiso 1 1 calc R U . . .
B25 B 0.777(3) 0.400(3) 0.711(3) 0.063(6) Uani 1 1 d . U . . .
H25 H 0.750770 0.376872 0.648418 0.075 Uiso 1 1 calc R U . . .
C42 C 0.495(3) 0.248(2) 0.7541(19) 0.106(8) Uani 1 1 d G U . . .
H42 H 0.469945 0.255680 0.707003 0.127 Uiso 1 1 calc R U . . .
C43 C 0.4460(19) 0.236(2) 0.798(2) 0.106(8) Uani 1 1 d G U . . .
H43 H 0.387976 0.234973 0.780765 0.127 Uiso 1 1 calc R U . . .
C44 C 0.484(3) 0.224(3) 0.869(2) 0.126(17) Uani 1 1 d G U . . .
H44 H 0.450820 0.215723 0.898245 0.151 Uiso 1 1 calc R U . . .
C45 C 0.570(3) 0.225(3) 0.8949(18) 0.121(17) Uani 1 1 d G U . . .
H45 H 0.595634 0.217181 0.941964 0.145 Uiso 1 1 calc R U . . .
C46 C 0.620(2) 0.237(2) 0.851(2) 0.096(14) Uani 1 1 d G U . . .
H46 H 0.677604 0.237887 0.868203 0.115 Uiso 1 1 calc R U . . .
C41 C 0.582(2) 0.249(3) 0.780(2) 0.106(8) Uani 1 1 d G U . . .
B9 B 0.767(4) 0.838(3) 0.481(3) 0.074(2) Uani 1 1 d . U . . .
H9 H 0.700225 0.821398 0.436502 0.089 Uiso 1 1 calc R U . . .
B30 B 0.684(4) 0.173(3) 0.283(3) 0.0751(16) Uani 1 1 d . U . . .
H30 H 0.672804 0.111398 0.255315 0.090 Uiso 1 1 calc R U . . .
B31 B 0.713(4) 0.247(3) 0.239(4) 0.0750(16) Uani 1 1 d . U . . .
H31 H 0.723737 0.237568 0.185347 0.090 Uiso 1 1 calc R U . . .
B20 B 0.818(3) 0.365(3) 0.854(3) 0.061(5) Uani 1 1 d . U . . .
H20 H 0.818253 0.318640 0.881301 0.073 Uiso 1 1 calc R U . . .
B22 B 0.902(4) 0.523(4) 0.857(3) 0.065(5) Uani 1 1 d . U . . .
H22 H 0.953772 0.581278 0.886945 0.078 Uiso 1 1 calc R U . . .
B21 B 0.920(4) 0.429(3) 0.860(3) 0.062(5) Uani 1 1 d . U . . .
H21 H 0.986023 0.426516 0.890086 0.074 Uiso 1 1 calc R U . . .
B6 B 0.839(4) 0.938(3) 0.542(3) 0.074(2) Uani 1 1 d . U . . .
H6 H 0.814040 0.986322 0.534864 0.089 Uiso 1 1 calc R U . . .
B3 B 0.969(4) 0.855(3) 0.523(3) 0.074(2) Uani 1 1 d . U . . .
H3 H 1.021426 0.851701 0.503157 0.089 Uiso 1 1 calc R U . . .
B4 B 0.990(4) 0.885(3) 0.628(4) 0.074(2) Uani 1 1 d . U . . .
H4 H 1.055231 0.899318 0.674011 0.089 Uiso 1 1 calc R U . . .
B23 B 0.892(3) 0.454(3) 0.768(3) 0.064(6) Uani 1 1 d . U . . .
H23 H 0.940576 0.467308 0.742247 0.077 Uiso 1 1 calc R U . . .
B5 B 0.913(4) 0.934(3) 0.632(4) 0.074(2) Uani 1 1 d . U . . .
H5 H 0.936045 0.981824 0.686096 0.089 Uiso 1 1 calc R U . . .
C22 C 1.026(2) 0.7466(18) 0.7729(18) 0.102(15) Uani 1 1 d G U . . .
H22A H 1.058864 0.795652 0.809315 0.122 Uiso 1 1 calc R U . . .
C21 C 0.942(2) 0.7331(15) 0.720(2) 0.072(11) Uani 1 1 d G U . . .
C26 C 0.8930(16) 0.6597(17) 0.6651(17) 0.065(10) Uani 1 1 d G U . . .
H26A H 0.836588 0.650704 0.629414 0.078 Uiso 1 1 calc R U . . .
C25 C 0.928(2) 0.5999(14) 0.6639(19) 0.091(13) Uani 1 1 d G U . . .
H25A H 0.895624 0.550782 0.627388 0.110 Uiso 1 1 calc R U . . .
C24 C 1.013(2) 0.613(2) 0.717(2) 0.098(14) Uani 1 1 d G U . . .
H24A H 1.036280 0.573293 0.716325 0.117 Uiso 1 1 calc R U . . .
C23 C 1.0615(17) 0.687(3) 0.772(2) 0.103(15) Uani 1 1 d G U . . .
H23A H 1.117900 0.695728 0.807289 0.124 Uiso 1 1 calc R U . . .
C7 C 0.891(2) 0.918(2) 0.823(3) 0.15(2) Uani 1 1 d G U . . .
H7 H 0.830519 0.892125 0.802462 0.180 Uiso 1 1 calc R U . . .
C17 C 0.930(3) 0.986(3) 0.885(3) 0.15(2) Uani 1 1 d G U . . .
H17A H 0.895463 1.005717 0.906552 0.174 Uiso 1 1 calc R U . . .
C18 C 1.021(3) 1.025(2) 0.916(2) 0.14(2) Uani 1 1 d G U . . .
H18A H 1.047498 1.070249 0.957588 0.172 Uiso 1 1 calc R U . . .
C19 C 1.074(2) 0.995(3) 0.884(3) 0.15(2) Uani 1 1 d G U . . .
H19A H 1.134591 1.021191 0.904537 0.178 Uiso 1 1 calc R U . . .
C20 C 1.035(3) 0.927(3) 0.822(3) 0.137(19) Uani 1 1 d G U . . .
H20A H 1.069649 0.907600 0.800448 0.164 Uiso 1 1 calc R U . . .
C10 C 0.944(3) 0.889(2) 0.791(2) 0.109(15) Uani 1 1 d G U . . .
C59 C 0.454(2) 0.0835(18) 0.2538(15) 0.0757(18) Uani 1 1 d G U . . .
C60 C 0.454(2) 0.0172(18) 0.2053(19) 0.086(6) Uani 1 1 d G U . . .
H60 H 0.496276 -0.005529 0.222932 0.104 Uiso 1 1 calc R U . . .
C61 C 0.391(3) -0.0152(16) 0.1303(18) 0.096(7) Uani 1 1 d G U . . .
H61 H 0.390490 -0.059582 0.097806 0.115 Uiso 1 1 calc R U . . .
C62 C 0.327(2) 0.0187(19) 0.1039(15) 0.100(8) Uani 1 1 d G U . . .
H62 H 0.284780 -0.002934 0.053740 0.120 Uiso 1 1 calc R U . . .
C63 C 0.327(2) 0.085(2) 0.152(2) 0.096(7) Uani 1 1 d G U . . .
H63 H 0.284854 0.107767 0.134798 0.116 Uiso 1 1 calc R U . . .
C64 C 0.391(2) 0.1174(16) 0.2274(18) 0.087(6) Uani 1 1 d G U . . .
H64 H 0.390640 0.161822 0.259924 0.104 Uiso 1 1 calc R U . . .
C54 C 0.5194(19) 0.0129(17) 0.4120(18) 0.0765(19) Uani 1 1 d G U . . .
H54 H 0.472762 0.027369 0.417553 0.092 Uiso 1 1 calc R U . . .
C55 C 0.537(2) -0.0493(16) 0.4357(18) 0.077(2) Uani 1 1 d G U . . .
H55 H 0.502714 -0.076393 0.457173 0.092 Uiso 1 1 calc R U . . .
C56 C 0.607(2) -0.0710(15) 0.4273(18) 0.077(2) Uani 1 1 d G U . . .
H56 H 0.618956 -0.112556 0.443228 0.092 Uiso 1 1 calc R U . . .
C57 C 0.6586(18) -0.0305(17) 0.3953(18) 0.077(2) Uani 1 1 d G U . . .
H57 H 0.705246 -0.044956 0.389663 0.092 Uiso 1 1 calc R U . . .
C58 C 0.641(2) 0.0317(16) 0.3715(18) 0.0765(19) Uani 1 1 d G U . . .
H58 H 0.675295 0.058806 0.350043 0.092 Uiso 1 1 calc R U . . .
C53 C 0.571(2) 0.0534(15) 0.3799(18) 0.0762(18) Uani 1 1 d G U . . .
C67 C 0.521(2) 0.2921(17) 0.1232(16) 0.080(8) Uani 1 1 d G U . . .
C68 C 0.5240(19) 0.224(2) 0.079(2) 0.085(8) Uani 1 1 d G U . . .
H68 H 0.577298 0.215038 0.090451 0.102 Uiso 1 1 calc R U . . .
C69 C 0.447(3) 0.1704(16) 0.0194(19) 0.089(9) Uani 1 1 d G U . . .
H69 H 0.449474 0.125106 -0.009772 0.107 Uiso 1 1 calc R U . . .
C70 C 0.368(2) 0.1843(19) 0.0031(17) 0.096(9) Uani 1 1 d G U . . .
H70 H 0.316536 0.148275 -0.037120 0.116 Uiso 1 1 calc R U . . .
C71 C 0.365(2) 0.252(2) 0.047(2) 0.100(9) Uani 1 1 d G U . . .
H71 H 0.311421 0.261377 0.035755 0.120 Uiso 1 1 calc R U . . .
C72 C 0.441(3) 0.3060(16) 0.1068(19) 0.093(9) Uani 1 1 d G U . . .
H72 H 0.439243 0.351310 0.135978 0.111 Uiso 1 1 calc R U . . .
C49 C 0.728(3) 0.111(2) 0.6111(18) 0.109(10) Uani 1 1 d G U . . .
H49 H 0.736578 0.100614 0.565787 0.131 Uiso 1 1 calc R U . . .
C48 C 0.693(3) 0.169(2) 0.628(2) 0.104(9) Uani 1 1 d G U . . .
H48 H 0.678409 0.197554 0.594645 0.124 Uiso 1 1 calc R U . . .
C47 C 0.680(3) 0.1848(19) 0.696(2) 0.096(9) Uani 1 1 d G U . . .
C52 C 0.701(3) 0.142(2) 0.7467(18) 0.101(9) Uani 1 1 d G U . . .
H52 H 0.692595 0.152875 0.792092 0.122 Uiso 1 1 calc R U . . .
C51 C 0.736(3) 0.084(2) 0.729(2) 0.106(9) Uani 1 1 d G U . . .
H51 H 0.750764 0.055936 0.763235 0.127 Uiso 1 1 calc R U . . .
C50 C 0.749(3) 0.069(2) 0.662(2) 0.110(10) Uani 1 1 d G U . . .
H50 H 0.772756 0.029804 0.650083 0.131 Uiso 1 1 calc R U . . .
C74 C 0.7609(17) 0.4811(12) 0.2171(14) 0.0752(19) Uani 1 1 d DG U . . .
H74 H 0.755389 0.510610 0.259017 0.090 Uiso 1 1 calc R U . . .
C73 C 0.6993(15) 0.4065(12) 0.1746(14) 0.0749(18) Uani 1 1 d G U . . .
C78 C 0.7075(16) 0.3624(12) 0.1120(13) 0.0752(19) Uani 1 1 d DG U . . .
H78 H 0.666281 0.312488 0.083515 0.090 Uiso 1 1 calc R U . . .
C77 C 0.7775(18) 0.3928(15) 0.0919(14) 0.075(2) Uani 1 1 d G U . . .
H77 H 0.782981 0.363270 0.050053 0.091 Uiso 1 1 calc R U . . .
C76 C 0.8391(16) 0.4674(15) 0.1345(17) 0.076(2) Uani 1 1 d G U . . .
H76 H 0.885887 0.487722 0.121072 0.091 Uiso 1 1 calc R U . . .
C75 C 0.8308(15) 0.5115(12) 0.1971(16) 0.075(2) Uani 1 1 d G U . . .
H75 H 0.872092 0.561393 0.225554 0.091 Uiso 1 1 calc R U . . .
C2 C 0.766(2) 0.731(2) 0.245(2) 0.107(15) Uani 1 1 d G U . . .
H2A H 0.711595 0.695912 0.238367 0.129 Uiso 1 1 calc R U . . .
C1 C 0.838(3) 0.757(2) 0.315(2) 0.083(12) Uani 1 1 d G U . . .
C6 C 0.918(2) 0.808(2) 0.3247(19) 0.126(17) Uani 1 1 d G U . . .
H6A H 0.966341 0.825741 0.371715 0.151 Uiso 1 1 calc R U . . .
C5 C 0.927(3) 0.834(2) 0.264(2) 0.15(2) Uani 1 1 d G U . . .
H5A H 0.980982 0.868854 0.270611 0.181 Uiso 1 1 calc R U . . .
C4 C 0.855(3) 0.808(3) 0.194(2) 0.15(2) Uani 1 1 d G U . . .
H4A H 0.860931 0.825496 0.153384 0.182 Uiso 1 1 calc R U . . .
C3 C 0.774(3) 0.756(3) 0.1843(19) 0.140(19) Uani 1 1 d G U . . .
H3A H 0.726237 0.739025 0.137261 0.168 Uiso 1 1 calc R U . . .
C15 C 0.9681(19) 0.5492(16) 0.4248(18) 0.075(2) Uani 1 1 d G U . . .
H15 H 0.995902 0.512187 0.430019 0.090 Uiso 1 1 calc R U . . .
C14 C 1.0007(17) 0.6109(18) 0.3995(17) 0.075(2) Uani 1 1 d G U . . .
H14 H 1.050262 0.615118 0.387873 0.090 Uiso 1 1 calc R U . . .
C13 C 0.959(2) 0.6662(15) 0.3917(17) 0.075(2) Uani 1 1 d G U . . .
H13 H 0.981030 0.707430 0.374777 0.090 Uiso 1 1 calc R U . . .
C12 C 0.885(2) 0.6598(16) 0.4091(18) 0.075(2) Uani 1 1 d G U . . .
C11 C 0.8526(17) 0.5981(18) 0.4343(18) 0.075(2) Uani 1 1 d G U . . .
H11 H 0.803077 0.593882 0.445974 0.090 Uiso 1 1 calc R U . . .
C16 C 0.894(2) 0.5428(15) 0.4422(17) 0.075(2) Uani 1 1 d G U . . .
H16 H 0.872308 0.501568 0.459070 0.090 Uiso 1 1 calc R U . . .
C28 C 0.896(3) 0.727(3) 0.917(2) 0.15(2) Uani 1 1 d G U . . .
H28A H 0.861135 0.727444 0.869232 0.185 Uiso 1 1 calc R U . . .
C29 C 0.978(3) 0.785(2) 0.960(3) 0.17(2) Uani 1 1 d G U . . .
H29A H 0.997605 0.825891 0.941594 0.209 Uiso 1 1 calc R U . . .
C30 C 1.031(2) 0.784(2) 1.032(3) 0.18(2) Uani 1 1 d G U . . .
H30A H 1.085272 0.823575 1.060769 0.215 Uiso 1 1 calc R U . . .
C31 C 1.001(3) 0.724(3) 1.060(2) 0.15(2) Uani 1 1 d G U . . .
H31A H 1.036470 0.722812 1.107582 0.184 Uiso 1 1 calc R U . . .
C32 C 0.920(3) 0.665(2) 1.016(3) 0.114(17) Uani 1 1 d G U . . .
H32 H 0.900000 0.624364 1.035221 0.136 Uiso 1 1 calc R U . . .
C27 C 0.867(2) 0.666(2) 0.945(3) 0.120(18) Uani 1 1 d G U . . .
C37 C 0.5562(19) 0.4672(19) 0.9154(18) 0.088(3) Uani 1 1 d G U . . .
H37 H 0.499857 0.431890 0.882917 0.105 Uiso 1 1 calc R U . . .
C36 C 0.584(2) 0.484(2) 0.9945(19) 0.088(3) Uani 1 1 d G U . . .
H36 H 0.545546 0.460093 1.014965 0.105 Uiso 1 1 calc R U . . .
C35 C 0.668(2) 0.537(2) 1.0430(14) 0.088(3) Uani 1 1 d G U . . .
H35 H 0.686085 0.548087 1.095956 0.105 Uiso 1 1 calc R U . . .
C34 C 0.7246(19) 0.5726(19) 1.0124(18) 0.088(3) Uani 1 1 d G U . . .
H34 H 0.780935 0.607879 1.044901 0.105 Uiso 1 1 calc R U . . .
C33 C 0.697(2) 0.556(2) 0.9333(19) 0.087(3) Uani 1 1 d G U . . .
C38 C 0.613(2) 0.503(2) 0.8848(14) 0.087(3) Uani 1 1 d G U . . .
H38 H 0.594709 0.491682 0.831861 0.105 Uiso 1 1 calc R U . . .
B32 B 0.773(4) 0.340(3) 0.321(3) 0.0750(16) Uani 1 1 d . U . . .
H32A H 0.822611 0.389361 0.317877 0.090 Uiso 1 1 calc R U . . .
C66 C 0.665(4) 0.313(3) 0.272(3) 0.0749(16) Uani 1 1 d . U . . .
B33 B 0.793(5) 0.322(3) 0.410(4) 0.0750(16) Uani 1 1 d . U . . .
H33 H 0.854599 0.355508 0.462116 0.090 Uiso 1 1 calc R U . . .
B34 B 0.708(4) 0.364(3) 0.368(3) 0.0750(16) Uani 1 1 d . U . . .
H34A H 0.712328 0.424604 0.392055 0.090 Uiso 1 1 calc R U . . .
B36 B 0.792(4) 0.248(3) 0.327(3) 0.0750(16) Uani 1 1 d . U . . .
H36A H 0.850323 0.233386 0.326172 0.090 Uiso 1 1 calc R U . . .
B35 B 0.739(4) 0.223(3) 0.393(3) 0.0751(16) Uani 1 1 d . U . . .
H35A H 0.763560 0.191970 0.433341 0.090 Uiso 1 1 calc R U . . .
B7 B 0.877(4) 0.893(3) 0.475(3) 0.074(2) Uani 1 1 d . U . . .
H7A H 0.875838 0.912447 0.425037 0.089 Uiso 1 1 calc R U . . .
B8 B 0.948(4) 0.944(4) 0.566(3) 0.074(2) Uani 1 1 d . U . . .
H8 H 0.993953 1.002252 0.574733 0.089 Uiso 1 1 calc R U . . .
Cl1 Cl 0.746(3) 0.1885(18) 1.032(2) 0.28(2) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au1 Au3 3.059(3) . ?
Au1 Au2 3.150(2) . ?
Au1 P2 2.271(12) . ?
Au1 S1 2.339(11) . ?
Au7 Au3 3.287(3) . ?
Au7 Au3 3.260(3) 2_666 ?
Au7 Au4 3.234(3) 2_666 ?
Au7 Au4 3.363(3) . ?
Au7 Au8 3.120(3) . ?
Au7 Au9 3.001(3) . ?
Au7 S4 2.314(12) . ?
Au7 S2 2.292(12) . ?
Au3 Au4 3.323(3) 2_666 ?
Au3 Au4 3.449(2) . ?
Au3 Au2 3.133(2) . ?
Au3 S2 2.291(13) . ?
Au3 S1 2.358(13) . ?
Au4 Au5 3.237(3) . ?
Au4 Au6 3.039(2) . ?
Au4 S3 2.355(12) . ?
Au4 S2 2.340(13) . ?
Au2 P1 2.268(14) . ?
Au2 S1 2.302(12) . ?
Au8 Au9 3.134(2) . ?
Au8 S4 2.319(11) . ?
Au8 P5 2.256(14) . ?
Au9 S4 2.343(11) . ?
Au9 P6 2.246(13) . ?
Au5 Au6 3.177(3) . ?
Au5 S3 2.316(12) . ?
Au5 P3 2.266(13) . ?
Au6 S3 2.298(12) . ?
Au6 P4 2.239(12) . ?
P2 C67 1.82(3) . ?
P2 C73 1.767(14) . ?
P2 C66 1.89(5) . ?
P4 C40 1.82(5) . ?
P4 C41 1.86(3) . ?
P4 C47 1.79(2) . ?
P1 C8 1.88(5) . ?
P1 C1 1.82(3) . ?
P1 C12 1.76(3) . ?
P6 C9 1.90(5) . ?
P6 C21 1.82(3) . ?
P6 C10 1.79(3) . ?
P5 C39 1.86(5) . ?
P5 C27 1.77(3) . ?
P5 C33 1.85(3) . ?
P3 C65 1.89(5) . ?
P3 C59 1.79(3) . ?
P3 C53 1.84(2) . ?
C8 B2 1.72(8) . ?
C8 B1 1.68(7) . ?
C8 B9 1.89(8) . ?
C8 B3 1.77(7) . ?
C8 B7 1.81(7) . ?
C39 B18 1.69(7) . ?
C39 B17 1.80(8) . ?
C39 B24 1.81(7) . ?
C39 B19 1.79(6) . ?
C39 B22 1.67(7) . ?
C9 B2 1.76(8) . ?
C9 B10 1.79(8) . ?
C9 B1 1.73(7) . ?
C9 B4 1.77(7) . ?
C9 B5 1.74(7) . ?
B2 H2 1.1000 . ?
B2 B1 1.90(8) . ?
B2 B3 1.80(8) . ?
B2 B4 1.83(8) . ?
C40 B18 1.64(7) . ?
C40 B17 1.66(6) . ?
C40 B26 1.78(6) . ?
C40 B25 1.79(7) . ?
C40 B20 1.73(7) . ?
B29 H29 1.1000 . ?
B29 B28 1.82(8) . ?
B29 C65 1.83(7) . ?
B29 B30 1.76(8) . ?
B29 B31 1.96(9) . ?
B29 C66 1.90(7) . ?
B28 H28 1.1000 . ?
B28 B27 1.79(8) . ?
B28 C65 1.59(7) . ?
B28 C66 1.70(7) . ?
B28 B34 1.82(9) . ?
B18 H18 1.1000 . ?
B18 B17 1.83(7) . ?
B18 B19 1.82(7) . ?
B18 B20 1.73(7) . ?
B17 H17 1.1000 . ?
B17 B24 1.85(8) . ?
B17 B25 1.74(7) . ?
B24 H24 1.1000 . ?
B24 B25 1.79(8) . ?
B24 B22 1.76(8) . ?
B24 B23 1.66(7) . ?
B19 H19 1.1000 . ?
B19 B20 1.75(8) . ?
B19 B22 1.85(7) . ?
B19 B21 1.77(7) . ?
B27 H27 1.1000 . ?
B27 C65 1.64(8) . ?
B27 B33 1.75(9) . ?
B27 B34 1.74(7) . ?
B27 B35 1.77(7) . ?
C65 B30 1.81(7) . ?
C65 B35 1.71(8) . ?
B10 H10 1.1000 . ?
B10 B1 1.86(8) . ?
B10 B9 1.77(8) . ?
B10 B6 1.69(8) . ?
B10 B5 1.79(8) . ?
B26 H26 1.1000 . ?
B26 B25 1.76(7) . ?
B26 B20 1.77(7) . ?
B26 B21 1.90(8) . ?
B26 B23 1.90(8) . ?
B1 H1 1.1000 . ?
B1 B9 1.85(8) . ?
B25 H25 1.1000 . ?
B25 B23 1.79(8) . ?
C42 H42 0.9300 . ?
C42 C43 1.3900 . ?
C42 C41 1.3900 . ?
C43 H43 0.9300 . ?
C43 C44 1.3900 . ?
C44 H44 0.9300 . ?
C44 C45 1.3900 . ?
C45 H45 0.9300 . ?
C45 C46 1.3900 . ?
C46 H46 0.9300 . ?
C46 C41 1.3900 . ?
B9 H9 1.1000 . ?
B9 B6 1.83(8) . ?
B9 B7 1.92(8) . ?
B30 H30 1.1000 . ?
B30 B31 1.81(7) . ?
B30 B36 1.80(9) . ?
B30 B35 1.93(8) . ?
B31 H31 1.1000 . ?
B31 B32 1.87(8) . ?
B31 C66 1.77(7) . ?
B31 B36 1.79(8) . ?
B20 H20 1.1000 . ?
B20 B21 1.79(7) . ?
B22 H22 1.1000 . ?
B22 B21 1.85(7) . ?
B22 B23 1.85(8) . ?
B21 H21 1.1000 . ?
B21 B23 1.87(7) . ?
B6 H6 1.1000 . ?
B6 B5 1.82(9) . ?
B6 B7 1.77(8) . ?
B6 B8 1.72(8) . ?
B3 H3 1.1000 . ?
B3 B4 1.87(8) . ?
B3 B7 1.92(9) . ?
B3 B8 1.86(8) . ?
B4 H4 1.1000 . ?
B4 B5 1.80(9) . ?
B4 B8 1.88(8) . ?
B23 H23 1.1000 . ?
B5 H5 1.1000 . ?
B5 B8 1.60(8) . ?
C22 H22A 0.9300 . ?
C22 C21 1.3900 . ?
C22 C23 1.3900 . ?
C21 C26 1.3900 . ?
C26 H26A 0.9300 . ?
C26 C25 1.3900 . ?
C25 H25A 0.9300 . ?
C25 C24 1.3900 . ?
C24 H24A 0.9300 . ?
C24 C23 1.3900 . ?
C23 H23A 0.9300 . ?
C7 H7 0.9300 . ?
C7 C17 1.3900 . ?
C7 C10 1.3900 . ?
C17 H17A 0.9300 . ?
C17 C18 1.3900 . ?
C18 H18A 0.9300 . ?
C18 C19 1.3900 . ?
C19 H19A 0.9300 . ?
C19 C20 1.3900 . ?
C20 H20A 0.9300 . ?
C20 C10 1.3900 . ?
C59 C60 1.3900 . ?
C59 C64 1.3900 . ?
C60 H60 0.9300 . ?
C60 C61 1.3900 . ?
C61 H61 0.9300 . ?
C61 C62 1.3900 . ?
C62 H62 0.9300 . ?
C62 C63 1.3900 . ?
C63 H63 0.9300 . ?
C63 C64 1.3900 . ?
C64 H64 0.9300 . ?
C54 H54 0.9300 . ?
C54 C55 1.3900 . ?
C54 C53 1.3900 . ?
C55 H55 0.9300 . ?
C55 C56 1.3900 . ?
C56 H56 0.9300 . ?
C56 C57 1.3900 . ?
C57 H57 0.9300 . ?
C57 C58 1.3900 . ?
C58 H58 0.9300 . ?
C58 C53 1.3900 . ?
C67 C68 1.3900 . ?
C67 C72 1.3900 . ?
C68 H68 0.9300 . ?
C68 C69 1.3900 . ?
C69 H69 0.9300 . ?
C69 C70 1.3900 . ?
C70 H70 0.9300 . ?
C70 C71 1.3900 . ?
C71 H71 0.9300 . ?
C71 C72 1.3900 . ?
C72 H72 0.9300 . ?
C49 H49 0.9300 . ?
C49 C48 1.3900 . ?
C49 C50 1.3900 . ?
C48 H48 0.9300 . ?
C48 C47 1.3900 . ?
C47 C52 1.3900 . ?
C52 H52 0.9300 . ?
C52 C51 1.3900 . ?
C51 H51 0.9300 . ?
C51 C50 1.3900 . ?
C50 H50 0.9300 . ?
C74 H74 0.9300 . ?
C74 C73 1.3900 . ?
C74 C75 1.3900 . ?
C73 C78 1.3900 . ?
C78 H78 0.9300 . ?
C78 C77 1.3900 . ?
C77 H77 0.9300 . ?
C77 C76 1.3900 . ?
C76 H76 0.9300 . ?
C76 C75 1.3900 . ?
C75 H75 0.9300 . ?
C2 H2A 0.9300 . ?
C2 C1 1.3900 . ?
C2 C3 1.3900 . ?
C1 C6 1.3900 . ?
C6 H6A 0.9300 . ?
C6 C5 1.3900 . ?
C5 H5A 0.9300 . ?
C5 C4 1.3900 . ?
C4 H4A 0.9300 . ?
C4 C3 1.3900 . ?
C3 H3A 0.9300 . ?
C15 H15 0.9300 . ?
C15 C14 1.3900 . ?
C15 C16 1.3900 . ?
C14 H14 0.9300 . ?
C14 C13 1.3900 . ?
C13 H13 0.9300 . ?
C13 C12 1.3900 . ?
C12 C11 1.3900 . ?
C11 H11 0.9300 . ?
C11 C16 1.3900 . ?
C16 H16 0.9300 . ?
C28 H28A 0.9300 . ?
C28 C29 1.3900(12) . ?
C28 C27 1.3900 . ?
C29 H29A 0.9300 . ?
C29 C30 1.3900 . ?
C30 H30A 0.9300 . ?
C30 C31 1.3900 . ?
C31 H31A 0.9300 . ?
C31 C32 1.3900 . ?
C32 H32 0.9300 . ?
C32 C27 1.3900 . ?
C37 H37 0.9300 . ?
C37 C36 1.3900 . ?
C37 C38 1.3900 . ?
C36 H36 0.9300 . ?
C36 C35 1.3900 . ?
C35 H35 0.9300 . ?
C35 C34 1.3900 . ?
C34 H34 0.9300 . ?
C34 C33 1.3900 . ?
C33 C38 1.3900 . ?
C38 H38 0.9300 . ?
B32 H32A 1.1000 . ?
B32 C66 1.66(8) . ?
B32 B33 1.77(8) . ?
B32 B34 1.73(8) . ?
B32 B36 1.84(7) . ?
C66 B34 1.71(8) . ?
B33 H33 1.1000 . ?
B33 B34 1.85(8) . ?
B33 B36 1.89(8) . ?
B33 B35 1.75(8) . ?
B34 H34A 1.1000 . ?
B36 H36A 1.1000 . ?
B36 B35 1.84(8) . ?
B35 H35A 1.1000 . ?
B7 H7A 1.1000 . ?
B7 B8 1.68(8) . ?
B8 H8 1.1000 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Au3 Au1 Au2 60.58(6) . . ?
P2 Au1 Au3 135.3(3) . . ?
P2 Au1 Au2 133.7(4) . . ?
P2 Au1 S1 175.0(5) . . ?
S1 Au1 Au3 49.6(3) . . ?
S1 Au1 Au2 46.8(3) . . ?
Au3 Au7 Au3 93.12(6) 2_666 . ?
Au3 Au7 Au4 60.19(5) 2_666 . ?
Au3 Au7 Au4 62.48(5) . . ?
Au4 Au7 Au3 61.26(6) 2_666 . ?
Au4 Au7 Au3 64.16(6) 2_666 2_666 ?
Au4 Au7 Au4 93.97(6) 2_666 . ?
Au8 Au7 Au3 170.06(8) . . ?
Au8 Au7 Au3 95.31(7) . 2_666 ?
Au8 Au7 Au4 117.77(7) . . ?
Au8 Au7 Au4 127.56(8) . 2_666 ?
Au9 Au7 Au3 135.20(8) . 2_666 ?
Au9 Au7 Au3 115.09(7) . . ?
Au9 Au7 Au4 98.51(7) . 2_666 ?
Au9 Au7 Au4 163.72(8) . . ?
Au9 Au7 Au8 61.56(6) . . ?
S4 Au7 Au3 85.3(3) . 2_666 ?
S4 Au7 Au3 138.6(3) . . ?
S4 Au7 Au4 81.4(3) . 2_666 ?
S4 Au7 Au4 142.9(3) . . ?
S4 Au7 Au8 47.7(3) . . ?
S4 Au7 Au9 50.3(3) . . ?
S2 Au7 Au3 44.2(3) . . ?
S2 Au7 Au3 102.6(3) . 2_666 ?
S2 Au7 Au4 44.0(3) . . ?
S2 Au7 Au4 103.9(3) . 2_666 ?
S2 Au7 Au8 128.2(3) . . ?
S2 Au7 Au9 122.0(3) . . ?
S2 Au7 S4 171.7(4) . . ?
Au1 Au3 Au7 97.62(7) . 2_666 ?
Au1 Au3 Au7 169.25(8) . . ?
Au1 Au3 Au4 114.58(7) . . ?
Au1 Au3 Au4 132.07(8) . 2_666 ?
Au1 Au3 Au2 61.16(6) . . ?
Au7 Au3 Au7 86.88(6) 2_666 . ?
Au7 Au3 Au4 57.56(5) 2_666 . ?
Au7 Au3 Au4 59.84(5) . . ?
Au7 Au3 Au4 58.60(5) . 2_666 ?
Au7 Au3 Au4 61.43(6) 2_666 2_666 ?
Au4 Au3 Au4 90.85(6) 2_666 . ?
Au2 Au3 Au7 121.49(7) . . ?
Au2 Au3 Au7 135.61(8) . 2_666 ?
Au2 Au3 Au4 102.46(7) . 2_666 ?
Au2 Au3 Au4 164.88(8) . . ?
S2 Au3 Au1 125.2(3) . . ?
S2 Au3 Au7 98.1(3) . 2_666 ?
S2 Au3 Au7 44.2(3) . . ?
S2 Au3 Au4 101.3(3) . 2_666 ?
S2 Au3 Au4 42.4(3) . . ?
S2 Au3 Au2 126.2(3) . . ?
S2 Au3 S1 171.7(4) . . ?
S1 Au3 Au1 49.1(3) . . ?
S1 Au3 Au7 89.1(3) . 2_666 ?
S1 Au3 Au7 141.1(3) . . ?
S1 Au3 Au4 142.9(3) . . ?
S1 Au3 Au4 85.8(3) . 2_666 ?
S1 Au3 Au2 47.0(3) . . ?
Au7 Au4 Au7 86.03(6) 2_666 . ?
Au7 Au4 Au3 57.67(5) . . ?
Au7 Au4 Au3 58.29(5) 2_666 . ?
Au7 Au4 Au3 60.15(6) 2_666 2_666 ?
Au7 Au4 Au5 101.25(7) 2_666 . ?
Au3 Au4 Au7 58.37(5) 2_666 . ?
Au3 Au4 Au3 89.15(6) 2_666 . ?
Au5 Au4 Au7 170.75(8) . . ?
Au5 Au4 Au3 121.49(7) . . ?
Au5 Au4 Au3 130.29(8) . 2_666 ?
Au6 Au4 Au7 117.52(7) . . ?
Au6 Au4 Au7 136.11(9) . 2_666 ?
Au6 Au4 Au3 99.42(7) . 2_666 ?
Au6 Au4 Au3 165.59(9) . . ?
Au6 Au4 Au5 60.73(6) . . ?
S3 Au4 Au7 141.2(3) . . ?
S3 Au4 Au7 89.5(3) . 2_666 ?
S3 Au4 Au3 86.2(3) . 2_666 ?
S3 Au4 Au3 144.6(3) . . ?
S3 Au4 Au5 45.6(3) . . ?
S3 Au4 Au6 48.4(3) . . ?
S2 Au4 Au7 42.9(3) . . ?
S2 Au4 Au7 97.8(3) . 2_666 ?
S2 Au4 Au3 99.8(3) . 2_666 ?
S2 Au4 Au3 41.3(3) . . ?
S2 Au4 Au5 129.4(3) . . ?
S2 Au4 Au6 125.0(3) . . ?
S2 Au4 S3 172.2(4) . . ?
Au3 Au2 Au1 58.27(6) . . ?
P1 Au2 Au1 128.8(4) . . ?
P1 Au2 Au3 131.5(4) . . ?
P1 Au2 S1 176.5(5) . . ?
S1 Au2 Au1 47.7(3) . . ?
S1 Au2 Au3 48.5(3) . . ?
Au7 Au8 Au9 57.36(6) . . ?
S4 Au8 Au7 47.6(3) . . ?
S4 Au8 Au9 48.1(3) . . ?
P5 Au8 Au7 136.9(4) . . ?
P5 Au8 Au9 132.3(4) . . ?
P5 Au8 S4 175.5(5) . . ?
Au7 Au9 Au8 61.09(6) . . ?
S4 Au9 Au7 49.4(3) . . ?
S4 Au9 Au8 47.4(3) . . ?
P6 Au9 Au7 129.6(4) . . ?
P6 Au9 Au8 126.2(4) . . ?
P6 Au9 S4 173.6(5) . . ?
Au6 Au5 Au4 56.54(5) . . ?
S3 Au5 Au4 46.6(3) . . ?
S3 Au5 Au6 46.3(3) . . ?
P3 Au5 Au4 134.3(4) . . ?
P3 Au5 Au6 136.9(4) . . ?
P3 Au5 S3 176.8(5) . . ?
Au4 Au6 Au5 62.73(6) . . ?
S3 Au6 Au4 50.1(3) . . ?
S3 Au6 Au5 46.7(3) . . ?
P4 Au6 Au4 138.2(4) . . ?
P4 Au6 Au5 136.5(3) . . ?
P4 Au6 S3 171.0(5) . . ?
Au7 S4 Au8 84.7(4) . . ?
Au7 S4 Au9 80.2(3) . . ?
Au8 S4 Au9 84.5(4) . . ?
Au5 S3 Au4 87.7(4) . . ?
Au6 S3 Au4 81.5(4) . . ?
Au6 S3 Au5 87.0(4) . . ?
Au7 S2 Au4 93.1(5) . . ?
Au3 S2 Au7 91.6(4) . . ?
Au3 S2 Au4 96.3(5) . . ?
C67 P2 Au1 111.0(14) . . ?
C67 P2 C66 108(2) . . ?
C73 P2 Au1 111.0(8) . . ?
C73 P2 C67 109.8(14) . . ?
C73 P2 C66 105(2) . . ?
C66 P2 Au1 111.9(15) . . ?
C40 P4 Au6 113.7(15) . . ?
C40 P4 C41 103(2) . . ?
C41 P4 Au6 109.6(13) . . ?
C47 P4 Au6 113.2(14) . . ?
C47 P4 C40 108(2) . . ?
C47 P4 C41 108.8(19) . . ?
C8 P1 Au2 110.5(16) . . ?
C1 P1 Au2 115.0(15) . . ?
C1 P1 C8 110(2) . . ?
C12 P1 Au2 110.9(12) . . ?
C12 P1 C8 102(2) . . ?
C12 P1 C1 106.9(18) . . ?
Au1 S1 Au3 81.3(4) . . ?
Au2 S1 Au1 85.5(4) . . ?
Au2 S1 Au3 84.5(4) . . ?
C9 P6 Au9 112.5(16) . . ?
C21 P6 Au9 109.0(11) . . ?
C21 P6 C9 108(2) . . ?
C10 P6 Au9 114.8(17) . . ?
C10 P6 C9 104(2) . . ?
C10 P6 C21 108(2) . . ?
C39 P5 Au8 113.7(15) . . ?
C27 P5 Au8 112.0(16) . . ?
C27 P5 C39 106(2) . . ?
C27 P5 C33 112(2) . . ?
C33 P5 Au8 109.1(13) . . ?
C33 P5 C39 104.3(19) . . ?
C65 P3 Au5 105.9(15) . . ?
C59 P3 Au5 112.0(13) . . ?
C59 P3 C65 107(2) . . ?
C59 P3 C53 103.9(16) . . ?
C53 P3 Au5 114.7(11) . . ?
C53 P3 C65 112.9(19) . . ?
P1 C8 B9 109(3) . . ?
B2 C8 P1 120(3) . . ?
B2 C8 B9 121(4) . . ?
B2 C8 B3 62(3) . . ?
B2 C8 B7 116(4) . . ?
B1 C8 P1 115(3) . . ?
B1 C8 B2 68(3) . . ?
B1 C8 B9 62(3) . . ?
B1 C8 B3 119(4) . . ?
B1 C8 B7 114(4) . . ?
B3 C8 P1 119(3) . . ?
B3 C8 B9 120(4) . . ?
B3 C8 B7 65(3) . . ?
B7 C8 P1 116(3) . . ?
B7 C8 B9 63(3) . . ?
B18 C39 P5 120(3) . . ?
B18 C39 B17 63(3) . . ?
B18 C39 B24 113(4) . . ?
B18 C39 B19 63(3) . . ?
B17 C39 P5 113(3) . . ?
B17 C39 B24 62(3) . . ?
B24 C39 P5 114(3) . . ?
B19 C39 P5 124(3) . . ?
B19 C39 B17 115(4) . . ?
B19 C39 B24 113(3) . . ?
B22 C39 P5 117(3) . . ?
B22 C39 B18 116(4) . . ?
B22 C39 B17 114(4) . . ?
B22 C39 B24 61(3) . . ?
B22 C39 B19 64(3) . . ?
B2 C9 P6 117(3) . . ?
B2 C9 B10 117(4) . . ?
B2 C9 B4 62(3) . . ?
B10 C9 P6 117(3) . . ?
B1 C9 P6 115(3) . . ?
B1 C9 B2 66(3) . . ?
B1 C9 B10 64(3) . . ?
B1 C9 B4 118(4) . . ?
B1 C9 B5 114(4) . . ?
B4 C9 P6 117(3) . . ?
B4 C9 B10 115(4) . . ?
B5 C9 P6 120(3) . . ?
B5 C9 B2 112(4) . . ?
B5 C9 B10 61(3) . . ?
B5 C9 B4 62(3) . . ?
C8 B2 C9 96(4) . . ?
C8 B2 H2 127.5 . . ?
C8 B2 B1 55(3) . . ?
C8 B2 B3 60(3) . . ?
C8 B2 B4 106(4) . . ?
C9 B2 H2 128.0 . . ?
C9 B2 B1 56(3) . . ?
C9 B2 B3 104(4) . . ?
C9 B2 B4 59(3) . . ?
B1 B2 H2 123.6 . . ?
B3 B2 H2 120.7 . . ?
B3 B2 B1 107(4) . . ?
B3 B2 B4 62(3) . . ?
B4 B2 H2 120.5 . . ?
B4 B2 B1 107(4) . . ?
B18 C40 P4 125(3) . . ?
B18 C40 B17 67(3) . . ?
B18 C40 B26 112(4) . . ?
B18 C40 B25 114(4) . . ?
B18 C40 B20 62(3) . . ?
B17 C40 P4 116(3) . . ?
B17 C40 B26 111(4) . . ?
B17 C40 B25 60(3) . . ?
B17 C40 B20 115(4) . . ?
B26 C40 P4 115(3) . . ?
B26 C40 B25 59(3) . . ?
B25 C40 P4 113(3) . . ?
B20 C40 P4 125(3) . . ?
B20 C40 B26 61(3) . . ?
B20 C40 B25 109(3) . . ?
B28 B29 H29 126.2 . . ?
B28 B29 C65 52(3) . . ?
B28 B29 B31 101(4) . . ?
B28 B29 C66 54(3) . . ?
C65 B29 H29 129.9 . . ?
C65 B29 B31 100(4) . . ?
C65 B29 C66 90(4) . . ?
B30 B29 H29 123.6 . . ?
B30 B29 B28 103(4) . . ?
B30 B29 C65 60(3) . . ?
B30 B29 B31 58(3) . . ?
B30 B29 C66 97(4) . . ?
B31 B29 H29 125.2 . . ?
C66 B29 H29 132.4 . . ?
C66 B29 B31 55(3) . . ?
B29 B28 H28 112.9 . . ?
B29 B28 B34 116(4) . . ?
B27 B28 B29 114(4) . . ?
B27 B28 H28 123.8 . . ?
B27 B28 B34 58(3) . . ?
C65 B28 B29 65(3) . . ?
C65 B28 H28 123.4 . . ?
C65 B28 B27 58(3) . . ?
C65 B28 C66 106(4) . . ?
C65 B28 B34 105(4) . . ?
C66 B28 B29 65(3) . . ?
C66 B28 H28 124.2 . . ?
C66 B28 B27 103(4) . . ?
C66 B28 B34 58(3) . . ?
B34 B28 H28 122.0 . . ?
C39 B18 H18 123.1 . . ?
C39 B18 B17 61(3) . . ?
C39 B18 B19 61(3) . . ?
C39 B18 B20 105(4) . . ?
C40 B18 C39 105(4) . . ?
C40 B18 H18 122.6 . . ?
C40 B18 B17 57(3) . . ?
C40 B18 B19 110(4) . . ?
C40 B18 B20 62(3) . . ?
B17 B18 H18 121.0 . . ?
B19 B18 H18 118.9 . . ?
B19 B18 B17 112(4) . . ?
B20 B18 H18 123.0 . . ?
B20 B18 B17 107(4) . . ?
B20 B18 B19 59(3) . . ?
C39 B17 B18 56(3) . . ?
C39 B17 H17 126.6 . . ?
C39 B17 B24 59(3) . . ?
C40 B17 C39 100(4) . . ?
C40 B17 B18 56(3) . . ?
C40 B17 H17 123.9 . . ?
C40 B17 B24 108(4) . . ?
C40 B17 B25 63(3) . . ?
B18 B17 H17 124.7 . . ?
B18 B17 B24 105(4) . . ?
B24 B17 H17 121.9 . . ?
B25 B17 C39 105(4) . . ?
B25 B17 B18 107(4) . . ?
B25 B17 H17 120.3 . . ?
B25 B17 B24 60(3) . . ?
C39 B24 B17 59(3) . . ?
C39 B24 H24 126.5 . . ?
B17 B24 H24 122.8 . . ?
B25 B24 C39 103(4) . . ?
B25 B24 B17 57(3) . . ?
B25 B24 H24 122.1 . . ?
B22 B24 C39 56(3) . . ?
B22 B24 B17 108(4) . . ?
B22 B24 H24 119.5 . . ?
B22 B24 B25 112(4) . . ?
B23 B24 C39 106(4) . . ?
B23 B24 B17 109(4) . . ?
B23 B24 H24 118.9 . . ?
B23 B24 B25 63(3) . . ?
B23 B24 B22 65(3) . . ?
C39 B19 B18 56(3) . . ?
C39 B19 H19 128.6 . . ?
C39 B19 B22 55(3) . . ?
B18 B19 H19 124.6 . . ?
B18 B19 B22 102(4) . . ?
B20 B19 C39 100(4) . . ?
B20 B19 B18 58(3) . . ?
B20 B19 H19 123.3 . . ?
B20 B19 B22 107(4) . . ?
B20 B19 B21 61(3) . . ?
B22 B19 H19 123.5 . . ?
B21 B19 C39 102(4) . . ?
B21 B19 B18 106(4) . . ?
B21 B19 H19 121.4 . . ?
B21 B19 B22 61(3) . . ?
B28 B27 H27 122.4 . . ?
C65 B27 B28 55(3) . . ?
C65 B27 H27 124.9 . . ?
C65 B27 B33 107(4) . . ?
C65 B27 B34 107(4) . . ?
C65 B27 B35 60(3) . . ?
B33 B27 B28 111(4) . . ?
B33 B27 H27 119.7 . . ?
B33 B27 B35 60(3) . . ?
B34 B27 B28 62(3) . . ?
B34 B27 H27 118.8 . . ?
B34 B27 B33 64(3) . . ?
B34 B27 B35 111(4) . . ?
B35 B27 B28 106(4) . . ?
B35 B27 H27 121.3 . . ?
B29 C65 P3 108(3) . . ?
B28 C65 P3 114(4) . . ?
B28 C65 B29 64(3) . . ?
B28 C65 B27 67(3) . . ?
B28 C65 B30 110(4) . . ?
B28 C65 B35 119(4) . . ?
B27 C65 P3 121(3) . . ?
B27 C65 B29 121(4) . . ?
B27 C65 B30 117(4) . . ?
B27 C65 B35 63(3) . . ?
B30 C65 P3 117(3) . . ?
B30 C65 B29 58(3) . . ?
B35 C65 P3 122(3) . . ?
B35 C65 B29 117(4) . . ?
B35 C65 B30 66(3) . . ?
C9 B10 H10 124.5 . . ?
C9 B10 B1 56(3) . . ?
B1 B10 H10 123.3 . . ?
B9 B10 C9 108(4) . . ?
B9 B10 H10 118.3 . . ?
B9 B10 B1 61(3) . . ?
B9 B10 B5 113(4) . . ?
B6 B10 C9 108(4) . . ?
B6 B10 H10 118.4 . . ?
B6 B10 B1 111(4) . . ?
B6 B10 B9 64(3) . . ?
B6 B10 B5 63(3) . . ?
B5 B10 C9 58(3) . . ?
B5 B10 H10 120.9 . . ?
B5 B10 B1 105(4) . . ?
C40 B26 H26 124.3 . . ?
C40 B26 B21 104(4) . . ?
C40 B26 B23 104(3) . . ?
B25 B26 C40 61(3) . . ?
B25 B26 H26 121.1 . . ?
B25 B26 B20 108(4) . . ?
B25 B26 B21 107(4) . . ?
B25 B26 B23 58(3) . . ?
B20 B26 C40 58(3) . . ?
B20 B26 H26 122.8 . . ?
B20 B26 B21 58(3) . . ?
B20 B26 B23 105(4) . . ?
B21 B26 H26 123.6 . . ?
B21 B26 B23 59(3) . . ?
B23 B26 H26 124.4 . . ?
C8 B1 C9 99(4) . . ?
C8 B1 B2 57(3) . . ?
C8 B1 B10 102(4) . . ?
C8 B1 H1 126.3 . . ?
C8 B1 B9 65(3) . . ?
C9 B1 B2 58(3) . . ?
C9 B1 B10 60(3) . . ?
C9 B1 H1 125.9 . . ?
C9 B1 B9 107(4) . . ?
B2 B1 H1 120.4 . . ?
B10 B1 B2 107(4) . . ?
B10 B1 H1 124.3 . . ?
B9 B1 B2 114(4) . . ?
B9 B1 B10 57(3) . . ?
B9 B1 H1 118.2 . . ?
C40 B25 B24 105(4) . . ?
C40 B25 H25 124.2 . . ?
C40 B25 B23 108(4) . . ?
B17 B25 C40 56(3) . . ?
B17 B25 B24 63(3) . . ?
B17 B25 B26 108(4) . . ?
B17 B25 H25 121.5 . . ?
B17 B25 B23 108(4) . . ?
B24 B25 H25 123.3 . . ?
B24 B25 B23 55(3) . . ?
B26 B25 C40 60(3) . . ?
B26 B25 B24 108(4) . . ?
B26 B25 H25 119.4 . . ?
B26 B25 B23 65(3) . . ?
B23 B25 H25 121.5 . . ?
C43 C42 H42 120.0 . . ?
C43 C42 C41 120.0 . . ?
C41 C42 H42 120.0 . . ?
C42 C43 H43 120.0 . . ?
C44 C43 C42 120.0 . . ?
C44 C43 H43 120.0 . . ?
C43 C44 H44 120.0 . . ?
C43 C44 C45 120.0 . . ?
C45 C44 H44 120.0 . . ?
C44 C45 H45 120.0 . . ?
C44 C45 C46 120.0 . . ?
C46 C45 H45 120.0 . . ?
C45 C46 H46 120.0 . . ?
C41 C46 C45 120.0 . . ?
C41 C46 H46 120.0 . . ?
C42 C41 P4 115(2) . . ?
C46 C41 P4 125(2) . . ?
C46 C41 C42 120.0 . . ?
C8 B9 H9 129.3 . . ?
C8 B9 B7 57(3) . . ?
B10 B9 C8 98(4) . . ?
B10 B9 B1 62(3) . . ?
B10 B9 H9 126.1 . . ?
B10 B9 B6 56(3) . . ?
B10 B9 B7 99(4) . . ?
B1 B9 C8 53(3) . . ?
B1 B9 H9 123.2 . . ?
B1 B9 B7 101(4) . . ?
B6 B9 C8 98(4) . . ?
B6 B9 B1 105(4) . . ?
B6 B9 H9 125.6 . . ?
B6 B9 B7 56(3) . . ?
B7 B9 H9 126.5 . . ?
B29 B30 C65 62(3) . . ?
B29 B30 H30 114.7 . . ?
B29 B30 B31 67(3) . . ?
B29 B30 B36 115(4) . . ?
B29 B30 B35 111(4) . . ?
C65 B30 H30 126.9 . . ?
C65 B30 B31 107(4) . . ?
C65 B30 B35 55(3) . . ?
B31 B30 H30 120.4 . . ?
B31 B30 B35 107(4) . . ?
B36 B30 C65 101(4) . . ?
B36 B30 H30 122.4 . . ?
B36 B30 B31 60(3) . . ?
B36 B30 B35 59(3) . . ?
B35 B30 H30 123.5 . . ?
B29 B31 H31 122.4 . . ?
B30 B31 B29 55(3) . . ?
B30 B31 H31 125.9 . . ?
B30 B31 B32 104(4) . . ?
B32 B31 B29 106(4) . . ?
B32 B31 H31 123.8 . . ?
C66 B31 B29 61(3) . . ?
C66 B31 B30 100(4) . . ?
C66 B31 H31 127.1 . . ?
C66 B31 B32 54(3) . . ?
C66 B31 B36 102(4) . . ?
B36 B31 B29 106(4) . . ?
B36 B31 B30 60(3) . . ?
B36 B31 H31 122.5 . . ?
B36 B31 B32 60(3) . . ?
C40 B20 B19 110(4) . . ?
C40 B20 B26 61(3) . . ?
C40 B20 H20 122.3 . . ?
C40 B20 B21 110(4) . . ?
B18 B20 C40 57(3) . . ?
B18 B20 B19 63(3) . . ?
B18 B20 B26 109(4) . . ?
B18 B20 H20 122.2 . . ?
B18 B20 B21 109(4) . . ?
B19 B20 B26 114(4) . . ?
B19 B20 H20 118.9 . . ?
B19 B20 B21 60(3) . . ?
B26 B20 H20 118.2 . . ?
B26 B20 B21 64(3) . . ?
B21 B20 H20 119.8 . . ?
C39 B22 B24 63(3) . . ?
C39 B22 B19 61(3) . . ?
C39 B22 H22 122.7 . . ?
C39 B22 B21 104(4) . . ?
C39 B22 B23 104(4) . . ?
B24 B22 B19 112(4) . . ?
B24 B22 H22 120.9 . . ?
B24 B22 B21 105(4) . . ?
B24 B22 B23 55(3) . . ?
B19 B22 H22 120.1 . . ?
B19 B22 B21 57(3) . . ?
B19 B22 B23 107(4) . . ?
B21 B22 H22 124.7 . . ?
B21 B22 B23 61(3) . . ?
B23 B22 H22 124.8 . . ?
B19 B21 B26 107(4) . . ?
B19 B21 B20 59(3) . . ?
B19 B21 B22 61(3) . . ?
B19 B21 H21 120.7 . . ?
B19 B21 B23 110(4) . . ?
B26 B21 H21 122.6 . . ?
B20 B21 B26 57(3) . . ?
B20 B21 B22 105(4) . . ?
B20 B21 H21 124.9 . . ?
B20 B21 B23 105(4) . . ?
B22 B21 B26 107(4) . . ?
B22 B21 H21 122.2 . . ?
B22 B21 B23 60(3) . . ?
B23 B21 B26 61(3) . . ?
B23 B21 H21 121.4 . . ?
B10 B6 B9 60(3) . . ?
B10 B6 H6 121.8 . . ?
B10 B6 B5 61(3) . . ?
B10 B6 B7 109(4) . . ?
B10 B6 B8 104(5) . . ?
B9 B6 H6 118.4 . . ?
B5 B6 B9 109(4) . . ?
B5 B6 H6 124.7 . . ?
B7 B6 B9 65(3) . . ?
B7 B6 H6 122.0 . . ?
B7 B6 B5 103(4) . . ?
B8 B6 B9 109(4) . . ?
B8 B6 H6 125.5 . . ?
B8 B6 B5 54(3) . . ?
B8 B6 B7 58(3) . . ?
C8 B3 B2 58(3) . . ?
C8 B3 H3 128.0 . . ?
C8 B3 B4 102(4) . . ?
C8 B3 B7 59(3) . . ?
C8 B3 B8 95(4) . . ?
B2 B3 H3 121.8 . . ?
B2 B3 B4 60(3) . . ?
B2 B3 B7 107(4) . . ?
B2 B3 B8 104(4) . . ?
B4 B3 H3 122.2 . . ?
B4 B3 B7 105(4) . . ?
B7 B3 H3 123.3 . . ?
B8 B3 H3 128.5 . . ?
B8 B3 B4 60(3) . . ?
B8 B3 B7 53(3) . . ?
C9 B4 B2 58(3) . . ?
C9 B4 B3 101(4) . . ?
C9 B4 H4 127.8 . . ?
C9 B4 B5 58(3) . . ?
C9 B4 B8 94(4) . . ?
B2 B4 B3 58(3) . . ?
B2 B4 H4 122.7 . . ?
B2 B4 B8 102(4) . . ?
B3 B4 H4 123.7 . . ?
B3 B4 B8 60(3) . . ?
B5 B4 B2 106(4) . . ?
B5 B4 B3 103(4) . . ?
B5 B4 H4 124.2 . . ?
B5 B4 B8 52(3) . . ?
B8 B4 H4 129.5 . . ?
B24 B23 B26 108(4) . . ?
B24 B23 B25 62(3) . . ?
B24 B23 B22 60(3) . . ?
B24 B23 B21 109(4) . . ?
B24 B23 H23 120.3 . . ?
B26 B23 H23 123.1 . . ?
B25 B23 B26 57(3) . . ?
B25 B23 B22 108(4) . . ?
B25 B23 B21 107(4) . . ?
B25 B23 H23 122.2 . . ?
B22 B23 B26 107(4) . . ?
B22 B23 B21 60(3) . . ?
B22 B23 H23 121.9 . . ?
B21 B23 B26 60(3) . . ?
B21 B23 H23 121.6 . . ?
C9 B5 B10 61(3) . . ?
C9 B5 B6 105(4) . . ?
C9 B5 B4 60(3) . . ?
C9 B5 H5 124.2 . . ?
B10 B5 B6 56(3) . . ?
B10 B5 B4 113(4) . . ?
B10 B5 H5 123.0 . . ?
B6 B5 H5 121.6 . . ?
B4 B5 B6 117(4) . . ?
B4 B5 H5 114.1 . . ?
B8 B5 C9 106(4) . . ?
B8 B5 B10 104(4) . . ?
B8 B5 B6 60(4) . . ?
B8 B5 B4 67(4) . . ?
B8 B5 H5 122.2 . . ?
C21 C22 H22A 120.0 . . ?
C21 C22 C23 120.0 . . ?
C23 C22 H22A 120.0 . . ?
C22 C21 P6 128(2) . . ?
C22 C21 C26 120.0 . . ?
C26 C21 P6 112(2) . . ?
C21 C26 H26A 120.0 . . ?
C25 C26 C21 120.0 . . ?
C25 C26 H26A 120.0 . . ?
C26 C25 H25A 120.0 . . ?
C24 C25 C26 120.0 . . ?
C24 C25 H25A 120.0 . . ?
C25 C24 H24A 120.0 . . ?
C25 C24 C23 120.0 . . ?
C23 C24 H24A 120.0 . . ?
C22 C23 H23A 120.0 . . ?
C24 C23 C22 120.0 . . ?
C24 C23 H23A 120.0 . . ?
C17 C7 H7 120.0 . . ?
C17 C7 C10 120.00(7) . . ?
C10 C7 H7 120.0 . . ?
C7 C17 H17A 120.0 . . ?
C7 C17 C18 120.0 . . ?
C18 C17 H17A 120.0 . . ?
C17 C18 H18A 120.0 . . ?
C17 C18 C19 120.0 . . ?
C19 C18 H18A 120.0 . . ?
C18 C19 H19A 120.0 . . ?
C20 C19 C18 120.00(7) . . ?
C20 C19 H19A 120.0 . . ?
C19 C20 H20A 120.0 . . ?
C10 C20 C19 120.0 . . ?
C10 C20 H20A 120.0 . . ?
C7 C10 P6 114(3) . . ?
C20 C10 P6 126(3) . . ?
C20 C10 C7 120.0 . . ?
C60 C59 P3 122.8(19) . . ?
C60 C59 C64 120.0 . . ?
C64 C59 P3 117.0(19) . . ?
C59 C60 H60 120.0 . . ?
C59 C60 C61 120.0 . . ?
C61 C60 H60 120.0 . . ?
C60 C61 H61 120.0 . . ?
C62 C61 C60 120.0 . . ?
C62 C61 H61 120.0 . . ?
C61 C62 H62 120.0 . . ?
C61 C62 C63 120.0 . . ?
C63 C62 H62 120.0 . . ?
C62 C63 H63 120.0 . . ?
C64 C63 C62 120.0 . . ?
C64 C63 H63 120.0 . . ?
C59 C64 H64 120.0 . . ?
C63 C64 C59 120.0 . . ?
C63 C64 H64 120.0 . . ?
C55 C54 H54 120.0 . . ?
C55 C54 C53 120.0 . . ?
C53 C54 H54 120.0 . . ?
C54 C55 H55 120.0 . . ?
C54 C55 C56 120.0 . . ?
C56 C55 H55 120.0 . . ?
C55 C56 H56 120.0 . . ?
C57 C56 C55 120.0 . . ?
C57 C56 H56 120.0 . . ?
C56 C57 H57 120.0 . . ?
C58 C57 C56 120.0 . . ?
C58 C57 H57 120.0 . . ?
C57 C58 H58 120.0 . . ?
C57 C58 C53 120.0 . . ?
C53 C58 H58 120.0 . . ?
C54 C53 P3 114.8(17) . . ?
C58 C53 P3 125.2(17) . . ?
C58 C53 C54 120.0 . . ?
C68 C67 P2 124(2) . . ?
C68 C67 C72 120.0 . . ?
C72 C67 P2 116(2) . . ?
C67 C68 H68 120.0 . . ?
C67 C68 C69 120.0 . . ?
C69 C68 H68 120.0 . . ?
C68 C69 H69 120.0 . . ?
C70 C69 C68 120.0 . . ?
C70 C69 H69 120.0 . . ?
C69 C70 H70 120.0 . . ?
C69 C70 C71 120.0 . . ?
C71 C70 H70 120.0 . . ?
C70 C71 H71 120.0 . . ?
C72 C71 C70 120.0 . . ?
C72 C71 H71 120.0 . . ?
C67 C72 H72 120.0 . . ?
C71 C72 C67 120.0 . . ?
C71 C72 H72 120.0 . . ?
C48 C49 H49 120.0 . . ?
C48 C49 C50 120.0 . . ?
C50 C49 H49 120.0 . . ?
C49 C48 H48 120.0 . . ?
C49 C48 C47 120.0 . . ?
C47 C48 H48 120.0 . . ?
C48 C47 P4 116(2) . . ?
C52 C47 P4 124(2) . . ?
C52 C47 C48 120.0 . . ?
C47 C52 H52 120.0 . . ?
C51 C52 C47 120.0 . . ?
C51 C52 H52 120.0 . . ?
C52 C51 H51 120.0 . . ?
C52 C51 C50 120.0 . . ?
C50 C51 H51 120.0 . . ?
C49 C50 H50 120.0 . . ?
C51 C50 C49 120.0 . . ?
C51 C50 H50 120.0 . . ?
C73 C74 H74 120.0 . . ?
C73 C74 C75 120.0 . . ?
C75 C74 H74 120.0 . . ?
C74 C73 P2 119.6(9) . . ?
C78 C73 P2 120.2(9) . . ?
C78 C73 C74 120.0 . . ?
C73 C78 H78 120.0 . . ?
C73 C78 C77 120.0 . . ?
C77 C78 H78 120.0 . . ?
C78 C77 H77 120.0 . . ?
C76 C77 C78 120.0 . . ?
C76 C77 H77 120.0 . . ?
C77 C76 H76 120.0 . . ?
C77 C76 C75 120.0 . . ?
C75 C76 H76 120.0 . . ?
C74 C75 H75 120.0 . . ?
C76 C75 C74 120.0 . . ?
C76 C75 H75 120.0 . . ?
C1 C2 H2A 120.0 . . ?
C1 C2 C3 120.0 . . ?
C3 C2 H2A 120.0 . . ?
C2 C1 P1 114(2) . . ?
C2 C1 C6 120.0 . . ?
C6 C1 P1 126(2) . . ?
C1 C6 H6A 120.0 . . ?
C5 C6 C1 120.0 . . ?
C5 C6 H6A 120.0 . . ?
C6 C5 H5A 120.0 . . ?
C4 C5 C6 120.0 . . ?
C4 C5 H5A 120.0 . . ?
C5 C4 H4A 120.0 . . ?
C5 C4 C3 120.0 . . ?
C3 C4 H4A 120.0 . . ?
C2 C3 H3A 120.0 . . ?
C4 C3 C2 120.0 . . ?
C4 C3 H3A 120.0 . . ?
C14 C15 H15 120.0 . . ?
C14 C15 C16 120.0 . . ?
C16 C15 H15 120.0 . . ?
C15 C14 H14 120.0 . . ?
C15 C14 C13 120.0 . . ?
C13 C14 H14 120.0 . . ?
C14 C13 H13 120.0 . . ?
C12 C13 C14 120.0 . . ?
C12 C13 H13 120.0 . . ?
C13 C12 P1 124.9(18) . . ?
C13 C12 C11 120.0 . . ?
C11 C12 P1 114.2(18) . . ?
C12 C11 H11 120.0 . . ?
C16 C11 C12 120.0 . . ?
C16 C11 H11 120.0 . . ?
C15 C16 H16 120.0 . . ?
C11 C16 C15 120.0 . . ?
C11 C16 H16 120.0 . . ?
C29 C28 H28A 120.0 . . ?
C29 C28 C27 120.0 . . ?
C27 C28 H28A 120.0 . . ?
C28 C29 H29A 120.0 . . ?
C28 C29 C30 120.0 . . ?
C30 C29 H29A 120.0 . . ?
C29 C30 H30A 120.0 . . ?
C29 C30 C31 120.00(8) . . ?
C31 C30 H30A 120.0 . . ?
C30 C31 H31A 120.0 . . ?
C32 C31 C30 120.0 . . ?
C32 C31 H31A 120.0 . . ?
C31 C32 H32 120.0 . . ?
C31 C32 C27 120.0 . . ?
C27 C32 H32 120.0 . . ?
C28 C27 P5 116(3) . . ?
C32 C27 P5 124(3) . . ?
C32 C27 C28 120.00(8) . . ?
C36 C37 H37 120.0 . . ?
C36 C37 C38 120.00(6) . . ?
C38 C37 H37 120.0 . . ?
C37 C36 H36 120.0 . . ?
C35 C36 C37 120.0 . . ?
C35 C36 H36 120.0 . . ?
C36 C35 H35 120.0 . . ?
C34 C35 C36 120.0 . . ?
C34 C35 H35 120.0 . . ?
C35 C34 H34 120.0 . . ?
C35 C34 C33 120.0 . . ?
C33 C34 H34 120.0 . . ?
C34 C33 P5 126(2) . . ?
C34 C33 C38 120.0 . . ?
C38 C33 P5 114(2) . . ?
C37 C38 H38 120.0 . . ?
C33 C38 C37 120.0 . . ?
C33 C38 H38 120.0 . . ?
B31 B32 H32A 120.3 . . ?
C66 B32 B31 60(3) . . ?
C66 B32 H32A 124.3 . . ?
C66 B32 B33 109(4) . . ?
C66 B32 B34 61(3) . . ?
C66 B32 B36 104(4) . . ?
B33 B32 B31 112(4) . . ?
B33 B32 H32A 118.2 . . ?
B33 B32 B36 63(3) . . ?
B34 B32 B31 113(5) . . ?
B34 B32 H32A 116.9 . . ?
B34 B32 B33 64(3) . . ?
B34 B32 B36 113(4) . . ?
B36 B32 B31 58(3) . . ?
B36 B32 H32A 122.2 . . ?
B29 C66 P2 113(3) . . ?
B28 C66 P2 115(3) . . ?
B28 C66 B29 61(3) . . ?
B28 C66 B31 115(4) . . ?
B28 C66 B34 65(3) . . ?
B31 C66 P2 117(3) . . ?
B31 C66 B29 64(3) . . ?
B32 C66 P2 122(3) . . ?
B32 C66 B29 118(4) . . ?
B32 C66 B28 114(4) . . ?
B32 C66 B31 66(3) . . ?
B32 C66 B34 62(3) . . ?
B34 C66 P2 116(3) . . ?
B34 C66 B29 118(4) . . ?
B34 C66 B31 119(4) . . ?
B27 B33 B32 103(5) . . ?
B27 B33 H33 123.8 . . ?
B27 B33 B34 58(3) . . ?
B27 B33 B36 107(5) . . ?
B27 B33 B35 61(3) . . ?
B32 B33 H33 123.6 . . ?
B32 B33 B34 57(3) . . ?
B32 B33 B36 60(3) . . ?
B34 B33 H33 123.9 . . ?
B34 B33 B36 106(4) . . ?
B36 B33 H33 121.7 . . ?
B35 B33 B32 108(5) . . ?
B35 B33 H33 120.6 . . ?
B35 B33 B34 107(5) . . ?
B35 B33 B36 61(3) . . ?
B28 B34 B33 105(4) . . ?
B28 B34 H34A 123.3 . . ?
B27 B34 B28 60(3) . . ?
B27 B34 B33 58(3) . . ?
B27 B34 H34A 123.0 . . ?
B32 B34 B28 104(4) . . ?
B32 B34 B27 105(4) . . ?
B32 B34 B33 59(3) . . ?
B32 B34 H34A 123.5 . . ?
C66 B34 B28 57(3) . . ?
C66 B34 B27 104(4) . . ?
C66 B34 B32 58(3) . . ?
C66 B34 B33 103(4) . . ?
C66 B34 H34A 125.2 . . ?
B33 B34 H34A 123.9 . . ?
B30 B36 B32 106(4) . . ?
B30 B36 B33 108(4) . . ?
B30 B36 H36A 120.7 . . ?
B30 B36 B35 64(3) . . ?
B31 B36 B30 61(3) . . ?
B31 B36 B32 62(3) . . ?
B31 B36 B33 110(4) . . ?
B31 B36 H36A 118.1 . . ?
B31 B36 B35 112(5) . . ?
B32 B36 B33 56(3) . . ?
B32 B36 H36A 125.9 . . ?
B33 B36 H36A 123.6 . . ?
B35 B36 B32 101(4) . . ?
B35 B36 B33 56(3) . . ?
B35 B36 H36A 122.7 . . ?
B27 B35 B30 106(4) . . ?
B27 B35 B36 108(4) . . ?
B27 B35 H35A 122.8 . . ?
C65 B35 B27 56(3) . . ?
C65 B35 B30 59(3) . . ?
C65 B35 B33 104(4) . . ?
C65 B35 B36 103(4) . . ?
C65 B35 H35A 125.9 . . ?
B30 B35 H35A 122.8 . . ?
B33 B35 B27 60(3) . . ?
B33 B35 B30 108(4) . . ?
B33 B35 B36 63(3) . . ?
B33 B35 H35A 121.0 . . ?
B36 B35 B30 57(3) . . ?
B36 B35 H35A 122.2 . . ?
C8 B7 B9 61(3) . . ?
C8 B7 B3 56(3) . . ?
C8 B7 H7A 127.3 . . ?
B9 B7 H7A 120.5 . . ?
B6 B7 C8 104(4) . . ?
B6 B7 B9 59(3) . . ?
B6 B7 B3 112(4) . . ?
B6 B7 H7A 121.4 . . ?
B3 B7 B9 111(4) . . ?
B3 B7 H7A 119.0 . . ?
B8 B7 C8 100(4) . . ?
B8 B7 B9 106(4) . . ?
B8 B7 B6 60(3) . . ?
B8 B7 B3 62(3) . . ?
B8 B7 H7A 124.4 . . ?
B6 B8 B3 117(4) . . ?
B6 B8 B4 118(4) . . ?
B6 B8 H8 114.6 . . ?
B3 B8 B4 60(3) . . ?
B3 B8 H8 118.6 . . ?
B4 B8 H8 118.2 . . ?
B5 B8 B6 66(4) . . ?
B5 B8 B3 112(4) . . ?
B5 B8 B4 62(4) . . ?
B5 B8 B7 117(5) . . ?
B5 B8 H8 117.7 . . ?
B7 B8 B6 62(3) . . ?
B7 B8 B3 65(3) . . ?
B7 B8 B4 116(4) . . ?
B7 B8 H8 116.1 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Au1 P2 C67 C68 -175.5(15) . . . . ?
Au1 P2 C67 C72 2.7(19) . . . . ?
Au1 P2 C73 C74 32.6(19) . . . . ?
Au1 P2 C73 C78 -152.0(14) . . . . ?
Au1 P2 C66 B29 117(3) . . . . ?
Au1 P2 C66 B28 49(4) . . . . ?
Au1 P2 C66 B31 -172(3) . . . . ?
Au1 P2 C66 B32 -95(4) . . . . ?
Au1 P2 C66 B34 -23(4) . . . . ?
Au2 P1 C8 B2 103(3) . . . . ?
Au2 P1 C8 B1 25(4) . . . . ?
Au2 P1 C8 B9 -42(3) . . . . ?
Au2 P1 C8 B3 175(3) . . . . ?
Au2 P1 C8 B7 -110(3) . . . . ?
Au2 P1 C1 C2 -7(3) . . . . ?
Au2 P1 C1 C6 175(2) . . . . ?
Au2 P1 C12 C13 142.6(15) . . . . ?
Au2 P1 C12 C11 -26.7(18) . . . . ?
Au8 P5 C39 B18 -105(3) . . . . ?
Au8 P5 C39 B17 -33(3) . . . . ?
Au8 P5 C39 B24 35(3) . . . . ?
Au8 P5 C39 B19 180(3) . . . . ?
Au8 P5 C39 B22 103(3) . . . . ?
Au8 P5 C27 C28 -18(3) . . . . ?
Au8 P5 C27 C32 167(2) . . . . ?
Au8 P5 C33 C34 -137.7(17) . . . . ?
Au8 P5 C33 C38 48.0(19) . . . . ?
Au9 P6 C21 C22 -132.8(16) . . . . ?
Au9 P6 C21 C26 46.5(18) . . . . ?
Au9 P6 C10 C7 -15(3) . . . . ?
Au9 P6 C10 C20 165(2) . . . . ?
Au5 P3 C65 B29 -118(3) . . . . ?
Au5 P3 C65 B28 -49(4) . . . . ?
Au5 P3 C65 B27 27(4) . . . . ?
Au5 P3 C65 B30 -180(3) . . . . ?
Au5 P3 C65 B35 103(3) . . . . ?
Au5 P3 C59 C60 -154.8(17) . . . . ?
Au5 P3 C59 C64 29(2) . . . . ?
Au5 P3 C53 C54 37(2) . . . . ?
Au5 P3 C53 C58 -145.0(16) . . . . ?
Au6 P4 C40 B18 105(3) . . . . ?
Au6 P4 C40 B17 25(4) . . . . ?
Au6 P4 C40 B26 -108(3) . . . . ?
Au6 P4 C40 B25 -42(3) . . . . ?
Au6 P4 C40 B20 -178(3) . . . . ?
Au6 P4 C41 C42 -2(2) . . . . ?
Au6 P4 C41 C46 176(2) . . . . ?
Au6 P4 C47 C48 35(2) . . . . ?
Au6 P4 C47 C52 -147(2) . . . . ?
P2 C67 C68 C69 178(2) . . . . ?
P2 C67 C72 C71 -178(2) . . . . ?
P2 C73 C78 C77 -175(2) . . . . ?
P2 C66 B34 B28 107(4) . . . . ?
P2 C66 B34 B27 147(4) . . . . ?
P2 C66 B34 B32 -114(4) . . . . ?
P2 C66 B34 B33 -153(3) . . . . ?
P4 C40 B18 C39 -146(3) . . . . ?
P4 C40 B18 B17 -107(4) . . . . ?
P4 C40 B18 B19 149(3) . . . . ?
P4 C40 B18 B20 114(4) . . . . ?
P4 C40 B17 C39 155(3) . . . . ?
P4 C40 B17 B18 119(4) . . . . ?
P4 C40 B17 B24 -144(3) . . . . ?
P4 C40 B17 B25 -103(4) . . . . ?
P4 C40 B26 B25 103(4) . . . . ?
P4 C40 B26 B20 -117(4) . . . . ?
P4 C40 B26 B21 -156(3) . . . . ?
P4 C40 B26 B23 144(3) . . . . ?
P4 C40 B25 B17 108(4) . . . . ?
P4 C40 B25 B24 151(3) . . . . ?
P4 C40 B25 B26 -107(4) . . . . ?
P4 C40 B25 B23 -152(3) . . . . ?
P4 C40 B20 B18 -115(4) . . . . ?
P4 C40 B20 B19 -151(3) . . . . ?
P4 C40 B20 B26 102(4) . . . . ?
P4 C40 B20 B21 145(3) . . . . ?
P4 C47 C52 C51 -178(3) . . . . ?
P1 C8 B2 C9 -148(3) . . . . ?
P1 C8 B2 B1 -107(4) . . . . ?
P1 C8 B2 B3 109(4) . . . . ?
P1 C8 B2 B4 153(3) . . . . ?
P1 C8 B1 C9 156(3) . . . . ?
P1 C8 B1 B2 114(4) . . . . ?
P1 C8 B1 B10 -143(3) . . . . ?
P1 C8 B1 B9 -99(4) . . . . ?
P1 C8 B9 B10 154(3) . . . . ?
P1 C8 B9 B1 108(4) . . . . ?
P1 C8 B9 B6 -149(3) . . . . ?
P1 C8 B9 B7 -110(4) . . . . ?
P1 C8 B3 B2 -110(4) . . . . ?
P1 C8 B3 B4 -152(3) . . . . ?
P1 C8 B3 B7 107(4) . . . . ?
P1 C8 B3 B8 147(3) . . . . ?
P1 C8 B7 B9 99(4) . . . . ?
P1 C8 B7 B6 141(4) . . . . ?
P1 C8 B7 B3 -112(4) . . . . ?
P1 C8 B7 B8 -158(3) . . . . ?
P1 C1 C6 C5 178(3) . . . . ?
P1 C12 C11 C16 170(2) . . . . ?
P6 C9 B2 C8 147(3) . . . . ?
P6 C9 B2 B1 107(4) . . . . ?
P6 C9 B2 B3 -152(3) . . . . ?
P6 C9 B2 B4 -108(4) . . . . ?
P6 C9 B10 B1 -106(4) . . . . ?
P6 C9 B10 B9 -141(3) . . . . ?
P6 C9 B10 B6 151(3) . . . . ?
P6 C9 B10 B5 112(4) . . . . ?
P6 C9 B1 C8 -152(3) . . . . ?
P6 C9 B1 B2 -110(4) . . . . ?
P6 C9 B1 B10 109(4) . . . . ?
P6 C9 B1 B9 142(3) . . . . ?
P6 C9 B4 B2 108(4) . . . . ?
P6 C9 B4 B3 149(3) . . . . ?
P6 C9 B4 B5 -112(4) . . . . ?
P6 C9 B4 B8 -151(3) . . . . ?
P6 C9 B5 B10 -106(4) . . . . ?
P6 C9 B5 B6 -141(4) . . . . ?
P6 C9 B5 B4 107(4) . . . . ?
P6 C9 B5 B8 157(4) . . . . ?
P6 C21 C26 C25 -179(2) . . . . ?
P5 C39 B18 C40 140(3) . . . . ?
P5 C39 B18 B17 103(4) . . . . ?
P5 C39 B18 B19 -115(4) . . . . ?
P5 C39 B18 B20 -156(3) . . . . ?
P5 C39 B17 C40 -149(3) . . . . ?
P5 C39 B17 B18 -113(3) . . . . ?
P5 C39 B17 B24 106(3) . . . . ?
P5 C39 B17 B25 146(3) . . . . ?
P5 C39 B24 B17 -105(3) . . . . ?
P5 C39 B24 B25 -143(3) . . . . ?
P5 C39 B24 B22 109(4) . . . . ?
P5 C39 B24 B23 153(3) . . . . ?
P5 C39 B19 B18 110(4) . . . . ?
P5 C39 B19 B20 149(3) . . . . ?
P5 C39 B19 B22 -107(4) . . . . ?
P5 C39 B19 B21 -148(3) . . . . ?
P5 C39 B22 B24 -104(4) . . . . ?
P5 C39 B22 B19 116(4) . . . . ?
P5 C39 B22 B21 156(3) . . . . ?
P5 C39 B22 B23 -142(3) . . . . ?
P5 C33 C38 C37 175(2) . . . . ?
P3 C65 B30 B29 95(4) . . . . ?
P3 C65 B30 B31 146(4) . . . . ?
P3 C65 B30 B36 -153(3) . . . . ?
P3 C65 B30 B35 -115(4) . . . . ?
P3 C65 B35 B27 -111(4) . . . . ?
P3 C65 B35 B30 108(4) . . . . ?
P3 C65 B35 B33 -149(3) . . . . ?
P3 C65 B35 B36 145(3) . . . . ?
P3 C59 C60 C61 -176(3) . . . . ?
P3 C59 C64 C63 176(3) . . . . ?
C8 P1 C1 C2 -132(3) . . . . ?
C8 P1 C1 C6 49(3) . . . . ?
C8 P1 C12 C13 -99(2) . . . . ?
C8 P1 C12 C11 91(2) . . . . ?
C8 B2 B3 B4 131(4) . . . . ?
C8 B2 B3 B7 33(4) . . . . ?
C8 B2 B3 B8 87(4) . . . . ?
C8 B2 B4 C9 87(4) . . . . ?
C8 B2 B4 B3 -43(4) . . . . ?
C8 B2 B4 B5 53(5) . . . . ?
C8 B2 B4 B8 0(5) . . . . ?
C8 B1 B9 B10 -126(4) . . . . ?
C8 B1 B9 B6 -89(4) . . . . ?
C8 B1 B9 B7 -32(3) . . . . ?
C8 B9 B6 B10 -94(4) . . . . ?
C8 B9 B6 B5 -56(4) . . . . ?
C8 B9 B6 B7 40(4) . . . . ?
C8 B9 B6 B8 2(5) . . . . ?
C8 B3 B4 C9 0(5) . . . . ?
C8 B3 B4 B2 41(4) . . . . ?
C8 B3 B4 B5 -60(4) . . . . ?
C8 B3 B4 B8 -89(4) . . . . ?
C8 B3 B8 B6 -7(5) . . . . ?
C8 B3 B8 B4 101(4) . . . . ?
C8 B3 B8 B5 67(5) . . . . ?
C8 B3 B8 B7 -44(4) . . . . ?
C8 B7 B8 B6 -100(4) . . . . ?
C8 B7 B8 B3 43(3) . . . . ?
C8 B7 B8 B4 9(5) . . . . ?
C8 B7 B8 B5 -61(6) . . . . ?
C39 P5 C27 C28 106(3) . . . . ?
C39 P5 C27 C32 -69(4) . . . . ?
C39 P5 C33 C34 100(2) . . . . ?
C39 P5 C33 C38 -74(2) . . . . ?
C39 B18 B17 C40 136(4) . . . . ?
C39 B18 B17 B24 34(3) . . . . ?
C39 B18 B17 B25 97(4) . . . . ?
C39 B18 B19 B20 -133(4) . . . . ?
C39 B18 B19 B22 -30(3) . . . . ?
C39 B18 B19 B21 -94(4) . . . . ?
C39 B18 B20 C40 -99(4) . . . . ?
C39 B18 B20 B19 42(3) . . . . ?
C39 B18 B20 B26 -66(5) . . . . ?
C39 B18 B20 B21 3(5) . . . . ?
C39 B17 B24 B25 134(4) . . . . ?
C39 B17 B24 B22 29(3) . . . . ?
C39 B17 B24 B23 98(4) . . . . ?
C39 B17 B25 C40 94(4) . . . . ?
C39 B17 B25 B24 -39(3) . . . . ?
C39 B17 B25 B26 62(4) . . . . ?
C39 B17 B25 B23 -6(4) . . . . ?
C39 B24 B25 C40 0(4) . . . . ?
C39 B24 B25 B17 39(3) . . . . ?
C39 B24 B25 B26 -63(4) . . . . ?
C39 B24 B25 B23 -102(4) . . . . ?
C39 B24 B22 B19 38(3) . . . . ?
C39 B24 B22 B21 98(4) . . . . ?
C39 B24 B22 B23 133(4) . . . . ?
C39 B24 B23 B26 61(5) . . . . ?
C39 B24 B23 B25 96(4) . . . . ?
C39 B24 B23 B22 -39(3) . . . . ?
C39 B24 B23 B21 -3(5) . . . . ?
C39 B19 B20 C40 -4(4) . . . . ?
C39 B19 B20 B18 -38(3) . . . . ?
C39 B19 B20 B26 62(4) . . . . ?
C39 B19 B20 B21 98(4) . . . . ?
C39 B19 B22 B24 -39(4) . . . . ?
C39 B19 B22 B21 -133(4) . . . . ?
C39 B19 B22 B23 -97(4) . . . . ?
C39 B19 B21 B26 -63(4) . . . . ?
C39 B19 B21 B20 -95(4) . . . . ?
C39 B19 B21 B22 38(3) . . . . ?
C39 B19 B21 B23 1(5) . . . . ?
C39 B22 B21 B19 -41(3) . . . . ?
C39 B22 B21 B26 59(4) . . . . ?
C39 B22 B21 B20 -1(5) . . . . ?
C39 B22 B21 B23 98(4) . . . . ?
C39 B22 B23 B24 42(4) . . . . ?
C39 B22 B23 B26 -59(4) . . . . ?
C39 B22 B23 B25 1(5) . . . . ?
C39 B22 B23 B21 -98(4) . . . . ?
C9 P6 C21 C22 105(2) . . . . ?
C9 P6 C21 C26 -76(2) . . . . ?
C9 P6 C10 C7 108(3) . . . . ?
C9 P6 C10 C20 -71(3) . . . . ?
C9 B2 B3 C8 -88(4) . . . . ?
C9 B2 B3 B4 42(4) . . . . ?
C9 B2 B3 B7 -56(5) . . . . ?
C9 B2 B3 B8 -1(5) . . . . ?
C9 B2 B4 B3 -130(4) . . . . ?
C9 B2 B4 B5 -35(4) . . . . ?
C9 B2 B4 B8 -88(4) . . . . ?
C9 B10 B1 C8 -93(4) . . . . ?
C9 B10 B1 B2 -34(3) . . . . ?
C9 B10 B1 B9 -141(4) . . . . ?
C9 B10 B9 C8 -8(4) . . . . ?
C9 B10 B9 B1 33(4) . . . . ?
C9 B10 B9 B6 -102(4) . . . . ?
C9 B10 B9 B7 -65(4) . . . . ?
C9 B10 B6 B9 101(4) . . . . ?
C9 B10 B6 B5 -37(4) . . . . ?
C9 B10 B6 B7 57(5) . . . . ?
C9 B10 B6 B8 -3(5) . . . . ?
C9 B10 B5 B6 138(4) . . . . ?
C9 B10 B5 B4 30(4) . . . . ?
C9 B10 B5 B8 101(5) . . . . ?
C9 B1 B9 C8 92(4) . . . . ?
C9 B1 B9 B10 -35(4) . . . . ?
C9 B1 B9 B6 2(5) . . . . ?
C9 B1 B9 B7 60(4) . . . . ?
C9 B4 B5 B10 -31(4) . . . . ?
C9 B4 B5 B6 -93(5) . . . . ?
C9 B4 B5 B8 -127(4) . . . . ?
C9 B4 B8 B6 6(5) . . . . ?
C9 B4 B8 B3 -100(4) . . . . ?
C9 B4 B8 B5 43(4) . . . . ?
C9 B4 B8 B7 -65(5) . . . . ?
C9 B5 B8 B6 99(4) . . . . ?
C9 B5 B8 B3 -12(6) . . . . ?
C9 B5 B8 B4 -46(4) . . . . ?
C9 B5 B8 B7 60(6) . . . . ?
B2 C8 B1 C9 42(4) . . . . ?
B2 C8 B1 B10 103(4) . . . . ?
B2 C8 B1 B9 147(4) . . . . ?
B2 C8 B9 B10 10(5) . . . . ?
B2 C8 B9 B1 -36(4) . . . . ?
B2 C8 B9 B6 66(5) . . . . ?
B2 C8 B9 B7 106(5) . . . . ?
B2 C8 B3 B4 -42(4) . . . . ?
B2 C8 B3 B7 -143(4) . . . . ?
B2 C8 B3 B8 -103(4) . . . . ?
B2 C8 B7 B9 -113(4) . . . . ?
B2 C8 B7 B6 -71(5) . . . . ?
B2 C8 B7 B3 36(4) . . . . ?
B2 C8 B7 B8 -10(5) . . . . ?
B2 C9 B10 B1 40(4) . . . . ?
B2 C9 B10 B9 5(5) . . . . ?
B2 C9 B10 B6 -62(5) . . . . ?
B2 C9 B10 B5 -102(4) . . . . ?
B2 C9 B1 C8 -42(4) . . . . ?
B2 C9 B1 B10 -141(4) . . . . ?
B2 C9 B1 B9 -108(4) . . . . ?
B2 C9 B4 B3 41(4) . . . . ?
B2 C9 B4 B5 140(4) . . . . ?
B2 C9 B4 B8 101(4) . . . . ?
B2 C9 B5 B10 110(4) . . . . ?
B2 C9 B5 B6 74(5) . . . . ?
B2 C9 B5 B4 -38(4) . . . . ?
B2 C9 B5 B8 12(6) . . . . ?
B2 B1 B9 C8 30(3) . . . . ?
B2 B1 B9 B10 -96(4) . . . . ?
B2 B1 B9 B6 -59(5) . . . . ?
B2 B1 B9 B7 -2(5) . . . . ?
B2 B3 B4 C9 -41(4) . . . . ?
B2 B3 B4 B5 -101(4) . . . . ?
B2 B3 B4 B8 -130(4) . . . . ?
B2 B3 B8 B6 -65(5) . . . . ?
B2 B3 B8 B4 43(4) . . . . ?
B2 B3 B8 B5 9(6) . . . . ?
B2 B3 B8 B7 -102(4) . . . . ?
B2 B4 B5 C9 35(4) . . . . ?
B2 B4 B5 B10 4(6) . . . . ?
B2 B4 B5 B6 -58(5) . . . . ?
B2 B4 B5 B8 -92(4) . . . . ?
B2 B4 B8 B6 65(5) . . . . ?
B2 B4 B8 B3 -42(3) . . . . ?
B2 B4 B8 B5 102(4) . . . . ?
B2 B4 B8 B7 -6(5) . . . . ?
C40 P4 C41 C42 120(2) . . . . ?
C40 P4 C41 C46 -62(3) . . . . ?
C40 P4 C47 C48 -92(3) . . . . ?
C40 P4 C47 C52 86(3) . . . . ?
C40 B18 B17 C39 -136(4) . . . . ?
C40 B18 B17 B24 -101(4) . . . . ?
C40 B18 B17 B25 -39(4) . . . . ?
C40 B18 B19 C39 97(4) . . . . ?
C40 B18 B19 B20 -36(4) . . . . ?
C40 B18 B19 B22 67(4) . . . . ?
C40 B18 B19 B21 3(5) . . . . ?
C40 B18 B20 B19 141(4) . . . . ?
C40 B18 B20 B26 34(4) . . . . ?
C40 B18 B20 B21 102(4) . . . . ?
C40 B17 B24 C39 -91(4) . . . . ?
C40 B17 B24 B25 43(4) . . . . ?
C40 B17 B24 B22 -62(5) . . . . ?
C40 B17 B24 B23 7(5) . . . . ?
C40 B17 B25 B24 -133(4) . . . . ?
C40 B17 B25 B26 -31(4) . . . . ?
C40 B17 B25 B23 -100(4) . . . . ?
C40 B26 B25 B17 30(4) . . . . ?
C40 B26 B25 B24 97(4) . . . . ?
C40 B26 B25 B23 132(4) . . . . ?
C40 B26 B20 B18 -32(3) . . . . ?
C40 B26 B20 B19 -100(4) . . . . ?
C40 B26 B20 B21 -135(4) . . . . ?
C40 B26 B21 B19 5(4) . . . . ?
C40 B26 B21 B20 38(3) . . . . ?
C40 B26 B21 B22 -59(4) . . . . ?
C40 B26 B21 B23 -98(4) . . . . ?
C40 B25 B23 B24 -96(4) . . . . ?
C40 B25 B23 B26 43(3) . . . . ?
C40 B25 B23 B22 -56(5) . . . . ?
C40 B25 B23 B21 7(5) . . . . ?
C40 B20 B21 B19 101(4) . . . . ?
C40 B20 B21 B26 -41(3) . . . . ?
C40 B20 B21 B22 59(5) . . . . ?
C40 B20 B21 B23 -3(5) . . . . ?
B29 B28 B27 C65 -33(4) . . . . ?
B29 B28 B27 B33 64(5) . . . . ?
B29 B28 B27 B34 106(5) . . . . ?
B29 B28 B27 B35 0(6) . . . . ?
B29 B28 C65 P3 -99(4) . . . . ?
B29 B28 C65 B27 146(4) . . . . ?
B29 B28 C65 B30 35(4) . . . . ?
B29 B28 C65 B35 108(5) . . . . ?
B29 B28 C66 P2 103(4) . . . . ?
B29 B28 C66 B31 -37(4) . . . . ?
B29 B28 C66 B32 -110(4) . . . . ?
B29 B28 C66 B34 -149(4) . . . . ?
B29 B28 B34 B27 -103(5) . . . . ?
B29 B28 B34 B32 -4(5) . . . . ?
B29 B28 B34 C66 31(4) . . . . ?
B29 B28 B34 B33 -65(5) . . . . ?
B29 C65 B30 B31 51(4) . . . . ?
B29 C65 B30 B36 112(4) . . . . ?
B29 C65 B30 B35 151(4) . . . . ?
B29 C65 B35 B27 113(4) . . . . ?
B29 C65 B35 B30 -28(4) . . . . ?
B29 C65 B35 B33 75(5) . . . . ?
B29 C65 B35 B36 10(5) . . . . ?
B29 B30 B31 B32 99(4) . . . . ?
B29 B30 B31 C66 44(4) . . . . ?
B29 B30 B31 B36 142(4) . . . . ?
B29 B30 B36 B31 -39(4) . . . . ?
B29 B30 B36 B32 5(5) . . . . ?
B29 B30 B36 B33 64(5) . . . . ?
B29 B30 B36 B35 100(4) . . . . ?
B29 B31 B32 C66 -34(3) . . . . ?
B29 B31 B32 B33 66(5) . . . . ?
B29 B31 B32 B34 -4(5) . . . . ?
B29 B31 B32 B36 100(4) . . . . ?
B29 B31 C66 P2 -104(4) . . . . ?
B29 B31 C66 B28 35(4) . . . . ?
B29 B31 C66 B32 141(4) . . . . ?
B29 B31 C66 B34 109(4) . . . . ?
B29 B31 B36 B30 32(3) . . . . ?
B29 B31 B36 B32 -99(4) . . . . ?
B29 B31 B36 B33 -68(5) . . . . ?
B29 B31 B36 B35 -8(5) . . . . ?
B29 C66 B34 B28 -31(4) . . . . ?
B29 C66 B34 B27 9(6) . . . . ?
B29 C66 B34 B32 108(4) . . . . ?
B29 C66 B34 B33 69(5) . . . . ?
B28 B29 C65 P3 108(4) . . . . ?
B28 B29 C65 B27 -36(5) . . . . ?
B28 B29 C65 B30 -141(5) . . . . ?
B28 B29 C65 B35 -110(5) . . . . ?
B28 B29 B30 C65 31(3) . . . . ?
B28 B29 B30 B31 -95(4) . . . . ?
B28 B29 B30 B36 -59(5) . . . . ?
B28 B29 B30 B35 5(5) . . . . ?
B28 B29 C66 P2 -107(4) . . . . ?
B28 B29 C66 B31 143(4) . . . . ?
B28 B29 C66 B32 103(5) . . . . ?
B28 B29 C66 B34 32(4) . . . . ?
B28 B27 C65 P3 -105(4) . . . . ?
B28 B27 C65 B29 35(4) . . . . ?
B28 B27 C65 B30 102(4) . . . . ?
B28 B27 C65 B35 143(4) . . . . ?
B28 B27 B33 B32 6(5) . . . . ?
B28 B27 B33 B34 42(4) . . . . ?
B28 B27 B33 B36 -56(5) . . . . ?
B28 B27 B33 B35 -97(4) . . . . ?
B28 B27 B34 B32 -98(5) . . . . ?
B28 B27 B34 C66 -38(4) . . . . ?
B28 B27 B34 B33 -135(4) . . . . ?
B28 B27 B35 C65 -31(4) . . . . ?
B28 B27 B35 B30 3(5) . . . . ?
B28 B27 B35 B33 105(4) . . . . ?
B28 B27 B35 B36 63(5) . . . . ?
B28 C65 B30 B29 -37(5) . . . . ?
B28 C65 B30 B31 14(6) . . . . ?
B28 C65 B30 B36 75(5) . . . . ?
B28 C65 B30 B35 113(5) . . . . ?
B28 C65 B35 B27 40(4) . . . . ?
B28 C65 B35 B30 -101(5) . . . . ?
B28 C65 B35 B33 2(6) . . . . ?
B28 C65 B35 B36 -64(5) . . . . ?
B28 C66 B34 B27 40(4) . . . . ?
B28 C66 B34 B32 139(4) . . . . ?
B28 C66 B34 B33 100(4) . . . . ?
B18 C39 B17 C40 -36(3) . . . . ?
B18 C39 B17 B24 -141(4) . . . . ?
B18 C39 B17 B25 -101(4) . . . . ?
B18 C39 B24 B17 38(3) . . . . ?
B18 C39 B24 B25 0(4) . . . . ?
B18 C39 B24 B22 -108(4) . . . . ?
B18 C39 B24 B23 -65(5) . . . . ?
B18 C39 B19 B20 39(3) . . . . ?
B18 C39 B19 B22 143(4) . . . . ?
B18 C39 B19 B21 102(4) . . . . ?
B18 C39 B22 B24 103(4) . . . . ?
B18 C39 B22 B19 -37(4) . . . . ?
B18 C39 B22 B21 3(5) . . . . ?
B18 C39 B22 B23 65(5) . . . . ?
B18 C40 B17 C39 36(3) . . . . ?
B18 C40 B17 B24 96(4) . . . . ?
B18 C40 B17 B25 138(4) . . . . ?
B18 C40 B26 B25 -105(4) . . . . ?
B18 C40 B26 B20 35(4) . . . . ?
B18 C40 B26 B21 -4(5) . . . . ?
B18 C40 B26 B23 -64(4) . . . . ?
B18 C40 B25 B17 -43(4) . . . . ?
B18 C40 B25 B24 0(5) . . . . ?
B18 C40 B25 B26 103(4) . . . . ?
B18 C40 B25 B23 57(5) . . . . ?
B18 C40 B20 B19 -36(4) . . . . ?
B18 C40 B20 B26 -143(4) . . . . ?
B18 C40 B20 B21 -100(4) . . . . ?
B18 B17 B24 C39 -33(3) . . . . ?
B18 B17 B24 B25 102(4) . . . . ?
B18 B17 B24 B22 -4(5) . . . . ?
B18 B17 B24 B23 65(5) . . . . ?
B18 B17 B25 C40 36(3) . . . . ?
B18 B17 B25 B24 -97(4) . . . . ?
B18 B17 B25 B26 4(5) . . . . ?
B18 B17 B25 B23 -64(5) . . . . ?
B18 B19 B20 C40 34(3) . . . . ?
B18 B19 B20 B26 100(4) . . . . ?
B18 B19 B20 B21 137(4) . . . . ?
B18 B19 B22 C39 31(3) . . . . ?
B18 B19 B22 B24 -8(5) . . . . ?
B18 B19 B22 B21 -102(4) . . . . ?
B18 B19 B22 B23 -66(4) . . . . ?
B18 B19 B21 B26 -5(4) . . . . ?
B18 B19 B21 B20 -37(3) . . . . ?
B18 B19 B21 B22 95(4) . . . . ?
B18 B19 B21 B23 59(5) . . . . ?
B18 B20 B21 B19 41(4) . . . . ?
B18 B20 B21 B26 -102(4) . . . . ?
B18 B20 B21 B22 -1(5) . . . . ?
B18 B20 B21 B23 -63(5) . . . . ?
B17 C39 B18 C40 37(3) . . . . ?
B17 C39 B18 B19 142(4) . . . . ?
B17 C39 B18 B20 101(4) . . . . ?
B17 C39 B24 B25 -38(3) . . . . ?
B17 C39 B24 B22 -146(4) . . . . ?
B17 C39 B24 B23 -103(4) . . . . ?
B17 C39 B19 B18 -37(3) . . . . ?
B17 C39 B19 B20 2(4) . . . . ?
B17 C39 B19 B22 106(4) . . . . ?
B17 C39 B19 B21 65(4) . . . . ?
B17 C39 B22 B24 32(4) . . . . ?
B17 C39 B22 B19 -107(4) . . . . ?
B17 C39 B22 B21 -68(4) . . . . ?
B17 C39 B22 B23 -5(5) . . . . ?
B17 C40 B18 C39 -40(3) . . . . ?
B17 C40 B18 B19 -104(4) . . . . ?
B17 C40 B18 B20 -139(4) . . . . ?
B17 C40 B26 B25 -32(4) . . . . ?
B17 C40 B26 B20 108(4) . . . . ?
B17 C40 B26 B21 69(4) . . . . ?
B17 C40 B26 B23 9(5) . . . . ?
B17 C40 B25 B24 42(4) . . . . ?
B17 C40 B25 B26 145(4) . . . . ?
B17 C40 B25 B23 100(4) . . . . ?
B17 C40 B20 B18 42(4) . . . . ?
B17 C40 B20 B19 6(5) . . . . ?
B17 C40 B20 B26 -101(4) . . . . ?
B17 C40 B20 B21 -58(5) . . . . ?
B17 B18 B19 C39 36(3) . . . . ?
B17 B18 B19 B20 -97(4) . . . . ?
B17 B18 B19 B22 5(5) . . . . ?
B17 B18 B19 B21 -58(5) . . . . ?
B17 B18 B20 C40 -35(3) . . . . ?
B17 B18 B20 B19 106(4) . . . . ?
B17 B18 B20 B26 -2(5) . . . . ?
B17 B18 B20 B21 67(5) . . . . ?
B17 B24 B25 C40 -39(3) . . . . ?
B17 B24 B25 B26 -102(4) . . . . ?
B17 B24 B25 B23 -141(4) . . . . ?
B17 B24 B22 C39 -30(4) . . . . ?
B17 B24 B22 B19 8(5) . . . . ?
B17 B24 B22 B21 68(4) . . . . ?
B17 B24 B22 B23 103(4) . . . . ?
B17 B24 B23 B26 -1(5) . . . . ?
B17 B24 B23 B25 34(4) . . . . ?
B17 B24 B23 B22 -101(4) . . . . ?
B17 B24 B23 B21 -65(5) . . . . ?
B17 B25 B23 B24 -36(4) . . . . ?
B17 B25 B23 B26 102(4) . . . . ?
B17 B25 B23 B22 4(5) . . . . ?
B17 B25 B23 B21 67(4) . . . . ?
B24 C39 B18 C40 0(5) . . . . ?
B24 C39 B18 B17 -37(3) . . . . ?
B24 C39 B18 B19 105(4) . . . . ?
B24 C39 B18 B20 64(4) . . . . ?
B24 C39 B17 C40 105(4) . . . . ?
B24 C39 B17 B18 141(4) . . . . ?
B24 C39 B17 B25 40(3) . . . . ?
B24 C39 B19 B18 -105(4) . . . . ?
B24 C39 B19 B20 -66(4) . . . . ?
B24 C39 B19 B22 38(4) . . . . ?
B24 C39 B19 B21 -3(5) . . . . ?
B24 C39 B22 B19 -140(4) . . . . ?
B24 C39 B22 B21 -100(4) . . . . ?
B24 C39 B22 B23 -38(3) . . . . ?
B24 B17 B25 C40 133(4) . . . . ?
B24 B17 B25 B26 102(4) . . . . ?
B24 B17 B25 B23 33(3) . . . . ?
B24 B25 B23 B26 139(4) . . . . ?
B24 B25 B23 B22 40(3) . . . . ?
B24 B25 B23 B21 103(4) . . . . ?
B24 B22 B21 B19 -107(4) . . . . ?
B24 B22 B21 B26 -7(4) . . . . ?
B24 B22 B21 B20 -66(4) . . . . ?
B24 B22 B21 B23 33(3) . . . . ?
B24 B22 B23 B26 -101(4) . . . . ?
B24 B22 B23 B25 -41(4) . . . . ?
B24 B22 B23 B21 -140(4) . . . . ?
B19 C39 B18 C40 -105(4) . . . . ?
B19 C39 B18 B17 -142(4) . . . . ?
B19 C39 B18 B20 -41(3) . . . . ?
B19 C39 B17 C40 1(4) . . . . ?
B19 C39 B17 B18 37(3) . . . . ?
B19 C39 B17 B24 -104(4) . . . . ?
B19 C39 B17 B25 -64(4) . . . . ?
B19 C39 B24 B17 107(4) . . . . ?
B19 C39 B24 B25 69(4) . . . . ?
B19 C39 B24 B22 -39(4) . . . . ?
B19 C39 B24 B23 4(5) . . . . ?
B19 C39 B22 B24 140(4) . . . . ?
B19 C39 B22 B21 39(3) . . . . ?
B19 C39 B22 B23 102(4) . . . . ?
B19 B18 B17 C39 -35(3) . . . . ?
B19 B18 B17 C40 100(4) . . . . ?
B19 B18 B17 B24 -1(5) . . . . ?
B19 B18 B17 B25 61(5) . . . . ?
B19 B18 B20 C40 -141(4) . . . . ?
B19 B18 B20 B26 -108(4) . . . . ?
B19 B18 B20 B21 -39(4) . . . . ?
B19 B20 B21 B26 -143(4) . . . . ?
B19 B20 B21 B22 -42(3) . . . . ?
B19 B20 B21 B23 -104(4) . . . . ?
B19 B22 B21 B26 100(4) . . . . ?
B19 B22 B21 B20 41(3) . . . . ?
B19 B22 B21 B23 140(4) . . . . ?
B19 B22 B23 B24 106(4) . . . . ?
B19 B22 B23 B26 5(4) . . . . ?
B19 B22 B23 B25 65(4) . . . . ?
B19 B22 B23 B21 -35(3) . . . . ?
B19 B21 B23 B24 1(5) . . . . ?
B19 B21 B23 B26 -99(4) . . . . ?
B19 B21 B23 B25 -65(5) . . . . ?
B19 B21 B23 B22 37(4) . . . . ?
B27 B28 C65 P3 115(4) . . . . ?
B27 B28 C65 B29 -146(4) . . . . ?
B27 B28 C65 B30 -112(5) . . . . ?
B27 B28 C65 B35 -38(4) . . . . ?
B27 B28 C66 P2 -146(3) . . . . ?
B27 B28 C66 B29 111(4) . . . . ?
B27 B28 C66 B31 74(5) . . . . ?
B27 B28 C66 B32 1(5) . . . . ?
B27 B28 C66 B34 -38(3) . . . . ?
B27 B28 B34 B32 100(4) . . . . ?
B27 B28 B34 C66 135(4) . . . . ?
B27 B28 B34 B33 38(4) . . . . ?
B27 C65 B30 B29 -111(4) . . . . ?
B27 C65 B30 B31 -60(5) . . . . ?
B27 C65 B30 B36 1(5) . . . . ?
B27 C65 B30 B35 39(4) . . . . ?
B27 C65 B35 B30 -141(4) . . . . ?
B27 C65 B35 B33 -38(4) . . . . ?
B27 C65 B35 B36 -103(4) . . . . ?
B27 B33 B34 B28 -39(4) . . . . ?
B27 B33 B34 B32 -137(5) . . . . ?
B27 B33 B34 C66 -99(4) . . . . ?
B27 B33 B36 B30 -1(5) . . . . ?
B27 B33 B36 B31 63(5) . . . . ?
B27 B33 B36 B32 96(5) . . . . ?
B27 B33 B36 B35 -41(4) . . . . ?
B27 B33 B35 C65 36(4) . . . . ?
B27 B33 B35 B30 98(4) . . . . ?
B27 B33 B35 B36 134(4) . . . . ?
C65 P3 C59 C60 89(2) . . . . ?
C65 P3 C59 C64 -87(2) . . . . ?
C65 P3 C53 C54 158(2) . . . . ?
C65 P3 C53 C58 -24(3) . . . . ?
C65 B29 B28 B27 31(4) . . . . ?
C65 B29 B28 C66 124(4) . . . . ?
C65 B29 B28 B34 95(5) . . . . ?
C65 B29 B30 B31 -126(4) . . . . ?
C65 B29 B30 B36 -90(4) . . . . ?
C65 B29 B30 B35 -25(3) . . . . ?
C65 B29 C66 P2 -148(3) . . . . ?
C65 B29 C66 B28 -41(3) . . . . ?
C65 B29 C66 B31 102(4) . . . . ?
C65 B29 C66 B32 62(4) . . . . ?
C65 B29 C66 B34 -9(5) . . . . ?
C65 B28 B27 B33 97(4) . . . . ?
C65 B28 B27 B34 139(4) . . . . ?
C65 B28 B27 B35 33(4) . . . . ?
C65 B28 C66 P2 154(4) . . . . ?
C65 B28 C66 B29 51(4) . . . . ?
C65 B28 C66 B31 14(6) . . . . ?
C65 B28 C66 B32 -59(5) . . . . ?
C65 B28 C66 B34 -98(5) . . . . ?
C65 B28 B34 B27 -35(4) . . . . ?
C65 B28 B34 B32 65(5) . . . . ?
C65 B28 B34 C66 100(4) . . . . ?
C65 B28 B34 B33 4(5) . . . . ?
C65 B27 B33 B32 65(4) . . . . ?
C65 B27 B33 B34 100(4) . . . . ?
C65 B27 B33 B36 2(5) . . . . ?
C65 B27 B33 B35 -39(4) . . . . ?
C65 B27 B34 B28 34(4) . . . . ?
C65 B27 B34 B32 -64(5) . . . . ?
C65 B27 B34 C66 -4(5) . . . . ?
C65 B27 B34 B33 -101(5) . . . . ?
C65 B27 B35 B30 34(3) . . . . ?
C65 B27 B35 B33 137(4) . . . . ?
C65 B27 B35 B36 94(4) . . . . ?
C65 B30 B31 B29 -48(4) . . . . ?
C65 B30 B31 B32 51(5) . . . . ?
C65 B30 B31 C66 -4(5) . . . . ?
C65 B30 B31 B36 94(4) . . . . ?
C65 B30 B36 B31 -103(4) . . . . ?
C65 B30 B36 B32 -59(4) . . . . ?
C65 B30 B36 B33 0(4) . . . . ?
C65 B30 B36 B35 36(3) . . . . ?
B10 C9 B2 C8 1(5) . . . . ?
B10 C9 B2 B1 -39(4) . . . . ?
B10 C9 B2 B3 61(5) . . . . ?
B10 C9 B2 B4 105(4) . . . . ?
B10 C9 B1 C8 99(4) . . . . ?
B10 C9 B1 B2 141(4) . . . . ?
B10 C9 B1 B9 33(4) . . . . ?
B10 C9 B4 B2 -109(4) . . . . ?
B10 C9 B4 B3 -68(5) . . . . ?
B10 C9 B4 B5 31(4) . . . . ?
B10 C9 B4 B8 -8(5) . . . . ?
B10 C9 B5 B6 -35(4) . . . . ?
B10 C9 B5 B4 -148(4) . . . . ?
B10 C9 B5 B8 -98(5) . . . . ?
B10 B1 B9 C8 126(4) . . . . ?
B10 B1 B9 B6 37(4) . . . . ?
B10 B1 B9 B7 94(4) . . . . ?
B10 B9 B6 B5 38(4) . . . . ?
B10 B9 B6 B7 133(5) . . . . ?
B10 B9 B6 B8 95(5) . . . . ?
B10 B6 B5 C9 38(4) . . . . ?
B10 B6 B5 B4 101(5) . . . . ?
B10 B6 B5 B8 138(5) . . . . ?
B10 B6 B7 C8 -1(5) . . . . ?
B10 B6 B7 B9 42(4) . . . . ?
B10 B6 B7 B3 -60(5) . . . . ?
B10 B6 B7 B8 -95(5) . . . . ?
B10 B6 B8 B3 66(5) . . . . ?
B10 B6 B8 B4 -2(6) . . . . ?
B10 B6 B8 B5 -37(4) . . . . ?
B10 B6 B8 B7 104(4) . . . . ?
B10 B5 B8 B6 35(4) . . . . ?
B10 B5 B8 B3 -76(5) . . . . ?
B10 B5 B8 B4 -110(4) . . . . ?
B10 B5 B8 B7 -3(6) . . . . ?
B26 C40 B18 C39 65(4) . . . . ?
B26 C40 B18 B17 105(4) . . . . ?
B26 C40 B18 B19 1(5) . . . . ?
B26 C40 B18 B20 -34(4) . . . . ?
B26 C40 B17 C39 -70(4) . . . . ?
B26 C40 B17 B18 -106(4) . . . . ?
B26 C40 B17 B24 -10(5) . . . . ?
B26 C40 B17 B25 32(4) . . . . ?
B26 C40 B25 B17 -145(4) . . . . ?
B26 C40 B25 B24 -103(4) . . . . ?
B26 C40 B25 B23 -45(4) . . . . ?
B26 C40 B20 B18 143(4) . . . . ?
B26 C40 B20 B19 107(4) . . . . ?
B26 C40 B20 B21 43(4) . . . . ?
B26 B25 B23 B24 -139(4) . . . . ?
B26 B25 B23 B22 -99(4) . . . . ?
B26 B25 B23 B21 -36(3) . . . . ?
B26 B20 B21 B19 143(4) . . . . ?
B26 B20 B21 B22 101(4) . . . . ?
B26 B20 B21 B23 39(3) . . . . ?
B26 B21 B23 B24 100(4) . . . . ?
B26 B21 B23 B25 34(3) . . . . ?
B26 B21 B23 B22 136(4) . . . . ?
B1 C8 B2 C9 -41(3) . . . . ?
B1 C8 B2 B3 -144(4) . . . . ?
B1 C8 B2 B4 -100(4) . . . . ?
B1 C8 B9 B10 46(4) . . . . ?
B1 C8 B9 B6 102(4) . . . . ?
B1 C8 B9 B7 142(4) . . . . ?
B1 C8 B3 B2 38(5) . . . . ?
B1 C8 B3 B4 -4(6) . . . . ?
B1 C8 B3 B7 -104(5) . . . . ?
B1 C8 B3 B8 -64(5) . . . . ?
B1 C8 B7 B9 -37(4) . . . . ?
B1 C8 B7 B6 5(6) . . . . ?
B1 C8 B7 B3 113(5) . . . . ?
B1 C8 B7 B8 67(5) . . . . ?
B1 C9 B2 C8 40(3) . . . . ?
B1 C9 B2 B3 101(4) . . . . ?
B1 C9 B2 B4 145(4) . . . . ?
B1 C9 B10 B9 -35(4) . . . . ?
B1 C9 B10 B6 -103(4) . . . . ?
B1 C9 B10 B5 -142(4) . . . . ?
B1 C9 B4 B2 -37(4) . . . . ?
B1 C9 B4 B3 4(6) . . . . ?
B1 C9 B4 B5 103(5) . . . . ?
B1 C9 B4 B8 64(5) . . . . ?
B1 C9 B5 B10 37(4) . . . . ?
B1 C9 B5 B6 2(5) . . . . ?
B1 C9 B5 B4 -111(4) . . . . ?
B1 C9 B5 B8 -61(5) . . . . ?
B1 B2 B3 C8 -30(3) . . . . ?
B1 B2 B3 B4 101(4) . . . . ?
B1 B2 B3 B7 3(5) . . . . ?
B1 B2 B3 B8 58(5) . . . . ?
B1 B2 B4 C9 30(4) . . . . ?
B1 B2 B4 B3 -100(4) . . . . ?
B1 B2 B4 B5 -5(5) . . . . ?
B1 B2 B4 B8 -58(4) . . . . ?
B1 B10 B9 C8 -41(3) . . . . ?
B1 B10 B9 B6 -136(4) . . . . ?
B1 B10 B9 B7 -98(4) . . . . ?
B1 B10 B6 B9 41(4) . . . . ?
B1 B10 B6 B5 -97(5) . . . . ?
B1 B10 B6 B7 -3(6) . . . . ?
B1 B10 B6 B8 -63(5) . . . . ?
B1 B10 B5 C9 -32(4) . . . . ?
B1 B10 B5 B6 106(4) . . . . ?
B1 B10 B5 B4 -2(6) . . . . ?
B1 B10 B5 B8 69(5) . . . . ?
B1 B9 B6 B10 -40(4) . . . . ?
B1 B9 B6 B5 -1(5) . . . . ?
B1 B9 B6 B7 94(4) . . . . ?
B1 B9 B6 B8 56(5) . . . . ?
B25 C40 B18 C39 0(5) . . . . ?
B25 C40 B18 B17 40(4) . . . . ?
B25 C40 B18 B19 -64(4) . . . . ?
B25 C40 B18 B20 -99(4) . . . . ?
B25 C40 B17 C39 -102(4) . . . . ?
B25 C40 B17 B18 -138(4) . . . . ?
B25 C40 B17 B24 -41(3) . . . . ?
B25 C40 B26 B20 140(4) . . . . ?
B25 C40 B26 B21 102(4) . . . . ?
B25 C40 B26 B23 41(3) . . . . ?
B25 C40 B20 B18 108(4) . . . . ?
B25 C40 B20 B19 71(4) . . . . ?
B25 C40 B20 B26 -36(4) . . . . ?
B25 C40 B20 B21 7(5) . . . . ?
B25 B17 B24 C39 -134(4) . . . . ?
B25 B17 B24 B22 -106(4) . . . . ?
B25 B17 B24 B23 -36(4) . . . . ?
B25 B24 B22 C39 -91(4) . . . . ?
B25 B24 B22 B19 -53(5) . . . . ?
B25 B24 B22 B21 7(5) . . . . ?
B25 B24 B22 B23 42(4) . . . . ?
B25 B24 B23 B26 -35(3) . . . . ?
B25 B24 B23 B22 -135(4) . . . . ?
B25 B24 B23 B21 -100(4) . . . . ?
B25 B26 B20 C40 36(4) . . . . ?
B25 B26 B20 B18 4(5) . . . . ?
B25 B26 B20 B19 -64(5) . . . . ?
B25 B26 B20 B21 -99(4) . . . . ?
B25 B26 B21 B19 68(4) . . . . ?
B25 B26 B21 B20 101(4) . . . . ?
B25 B26 B21 B22 4(4) . . . . ?
B25 B26 B21 B23 -35(3) . . . . ?
C42 C43 C44 C45 0.0 . . . . ?
C43 C42 C41 P4 178(3) . . . . ?
C43 C42 C41 C46 0.0 . . . . ?
C43 C44 C45 C46 0.0 . . . . ?
C44 C45 C46 C41 0.0 . . . . ?
C45 C46 C41 P4 -178(3) . . . . ?
C45 C46 C41 C42 0.0 . . . . ?
C41 P4 C40 B18 -14(4) . . . . ?
C41 P4 C40 B17 -93(3) . . . . ?
C41 P4 C40 B26 134(3) . . . . ?
C41 P4 C40 B25 -160(3) . . . . ?
C41 P4 C40 B20 64(4) . . . . ?
C41 P4 C47 C48 157(2) . . . . ?
C41 P4 C47 C52 -25(3) . . . . ?
C41 C42 C43 C44 0.0 . . . . ?
B9 C8 B2 C9 -7(5) . . . . ?
B9 C8 B2 B1 34(4) . . . . ?
B9 C8 B2 B3 -110(4) . . . . ?
B9 C8 B2 B4 -66(5) . . . . ?
B9 C8 B1 C9 -105(4) . . . . ?
B9 C8 B1 B2 -147(4) . . . . ?
B9 C8 B1 B10 -44(3) . . . . ?
B9 C8 B3 B2 111(5) . . . . ?
B9 C8 B3 B4 69(5) . . . . ?
B9 C8 B3 B7 -32(4) . . . . ?
B9 C8 B3 B8 8(5) . . . . ?
B9 C8 B7 B6 42(4) . . . . ?
B9 C8 B7 B3 149(4) . . . . ?
B9 C8 B7 B8 103(4) . . . . ?
B9 B10 B1 C8 48(4) . . . . ?
B9 B10 B1 C9 141(4) . . . . ?
B9 B10 B1 B2 107(4) . . . . ?
B9 B10 B6 B5 -138(4) . . . . ?
B9 B10 B6 B7 -44(4) . . . . ?
B9 B10 B6 B8 -104(4) . . . . ?
B9 B10 B5 C9 -97(5) . . . . ?
B9 B10 B5 B6 41(4) . . . . ?
B9 B10 B5 B4 -67(6) . . . . ?
B9 B10 B5 B8 4(6) . . . . ?
B9 B6 B5 C9 0(5) . . . . ?
B9 B6 B5 B10 -38(4) . . . . ?
B9 B6 B5 B4 64(5) . . . . ?
B9 B6 B5 B8 100(5) . . . . ?
B9 B6 B7 C8 -43(4) . . . . ?
B9 B6 B7 B3 -102(4) . . . . ?
B9 B6 B7 B8 -136(5) . . . . ?
B9 B6 B8 B3 3(6) . . . . ?
B9 B6 B8 B4 -65(5) . . . . ?
B9 B6 B8 B5 -100(5) . . . . ?
B9 B6 B8 B7 41(4) . . . . ?
B9 B7 B8 B6 -38(4) . . . . ?
B9 B7 B8 B3 105(4) . . . . ?
B9 B7 B8 B4 71(5) . . . . ?
B9 B7 B8 B5 2(6) . . . . ?
B30 B29 B28 B27 -4(5) . . . . ?
B30 B29 B28 C65 -35(4) . . . . ?
B30 B29 B28 C66 90(4) . . . . ?
B30 B29 B28 B34 61(5) . . . . ?
B30 B29 C65 P3 -111(3) . . . . ?
B30 B29 C65 B28 141(5) . . . . ?
B30 B29 C65 B27 104(5) . . . . ?
B30 B29 C65 B35 30(4) . . . . ?
B30 B29 C66 P2 152(3) . . . . ?
B30 B29 C66 B28 -101(4) . . . . ?
B30 B29 C66 B31 42(3) . . . . ?
B30 B29 C66 B32 2(5) . . . . ?
B30 B29 C66 B34 -69(5) . . . . ?
B30 C65 B35 B27 141(4) . . . . ?
B30 C65 B35 B33 103(4) . . . . ?
B30 C65 B35 B36 38(3) . . . . ?
B30 B31 B32 C66 -92(4) . . . . ?
B30 B31 B32 B33 8(6) . . . . ?
B30 B31 B32 B34 -62(5) . . . . ?
B30 B31 B32 B36 42(4) . . . . ?
B30 B31 C66 P2 -145(4) . . . . ?
B30 B31 C66 B29 -41(4) . . . . ?
B30 B31 C66 B28 -6(6) . . . . ?
B30 B31 C66 B32 101(4) . . . . ?
B30 B31 C66 B34 68(5) . . . . ?
B30 B31 B36 B32 -131(4) . . . . ?
B30 B31 B36 B33 -100(4) . . . . ?
B30 B31 B36 B35 -40(4) . . . . ?
B30 B36 B35 B27 -97(4) . . . . ?
B30 B36 B35 C65 -39(3) . . . . ?
B30 B36 B35 B33 -138(4) . . . . ?
B31 B29 B28 B27 -63(5) . . . . ?
B31 B29 B28 C65 -94(4) . . . . ?
B31 B29 B28 C66 30(3) . . . . ?
B31 B29 B28 B34 1(5) . . . . ?
B31 B29 C65 P3 -155(3) . . . . ?
B31 B29 C65 B28 96(4) . . . . ?
B31 B29 C65 B27 60(5) . . . . ?
B31 B29 C65 B30 -44(3) . . . . ?
B31 B29 C65 B35 -14(5) . . . . ?
B31 B29 B30 C65 126(4) . . . . ?
B31 B29 B30 B36 36(4) . . . . ?
B31 B29 B30 B35 101(4) . . . . ?
B31 B29 C66 P2 110(4) . . . . ?
B31 B29 C66 B28 -143(4) . . . . ?
B31 B29 C66 B32 -40(4) . . . . ?
B31 B29 C66 B34 -111(5) . . . . ?
B31 B30 B36 B32 44(4) . . . . ?
B31 B30 B36 B33 103(4) . . . . ?
B31 B30 B36 B35 139(4) . . . . ?
B31 B32 C66 P2 -108(4) . . . . ?
B31 B32 C66 B29 40(4) . . . . ?
B31 B32 C66 B28 108(4) . . . . ?
B31 B32 C66 B34 148(4) . . . . ?
B31 B32 B33 B27 -70(5) . . . . ?
B31 B32 B33 B34 -106(5) . . . . ?
B31 B32 B33 B36 32(4) . . . . ?
B31 B32 B33 B35 -7(6) . . . . ?
B31 B32 B34 B28 5(5) . . . . ?
B31 B32 B34 B27 67(5) . . . . ?
B31 B32 B34 C66 -30(3) . . . . ?
B31 B32 B34 B33 104(4) . . . . ?
B31 B32 B36 B30 -43(4) . . . . ?
B31 B32 B36 B33 -144(5) . . . . ?
B31 B32 B36 B35 -109(5) . . . . ?
B31 C66 B34 B28 -105(4) . . . . ?
B31 C66 B34 B27 -66(5) . . . . ?
B31 C66 B34 B32 34(4) . . . . ?
B31 C66 B34 B33 -6(5) . . . . ?
B31 B36 B35 B27 -59(5) . . . . ?
B31 B36 B35 C65 0(5) . . . . ?
B31 B36 B35 B30 38(4) . . . . ?
B31 B36 B35 B33 -100(4) . . . . ?
B20 C40 B18 C39 99(4) . . . . ?
B20 C40 B18 B17 139(4) . . . . ?
B20 C40 B18 B19 35(3) . . . . ?
B20 C40 B17 C39 -4(4) . . . . ?
B20 C40 B17 B18 -40(4) . . . . ?
B20 C40 B17 B24 57(5) . . . . ?
B20 C40 B17 B25 98(4) . . . . ?
B20 C40 B26 B25 -140(4) . . . . ?
B20 C40 B26 B21 -38(3) . . . . ?
B20 C40 B26 B23 -99(4) . . . . ?
B20 C40 B25 B17 -109(4) . . . . ?
B20 C40 B25 B24 -67(4) . . . . ?
B20 C40 B25 B26 36(4) . . . . ?
B20 C40 B25 B23 -9(5) . . . . ?
B20 B18 B17 C39 -98(4) . . . . ?
B20 B18 B17 C40 37(4) . . . . ?
B20 B18 B17 B24 -64(4) . . . . ?
B20 B18 B17 B25 -2(5) . . . . ?
B20 B18 B19 C39 133(4) . . . . ?
B20 B18 B19 B22 103(4) . . . . ?
B20 B18 B19 B21 39(3) . . . . ?
B20 B19 B22 C39 91(4) . . . . ?
B20 B19 B22 B24 52(5) . . . . ?
B20 B19 B22 B21 -42(3) . . . . ?
B20 B19 B22 B23 -6(4) . . . . ?
B20 B19 B21 B26 32(3) . . . . ?
B20 B19 B21 B22 133(4) . . . . ?
B20 B19 B21 B23 96(4) . . . . ?
B20 B26 B25 C40 -35(3) . . . . ?
B20 B26 B25 B17 -5(5) . . . . ?
B20 B26 B25 B24 62(5) . . . . ?
B20 B26 B25 B23 97(4) . . . . ?
B20 B26 B21 B19 -33(3) . . . . ?
B20 B26 B21 B22 -97(4) . . . . ?
B20 B26 B21 B23 -136(4) . . . . ?
B20 B21 B23 B24 63(5) . . . . ?
B20 B21 B23 B26 -37(3) . . . . ?
B20 B21 B23 B25 -3(5) . . . . ?
B20 B21 B23 B22 99(4) . . . . ?
B22 C39 B18 C40 -68(5) . . . . ?
B22 C39 B18 B17 -105(4) . . . . ?
B22 C39 B18 B19 37(4) . . . . ?
B22 C39 B18 B20 -4(5) . . . . ?
B22 C39 B17 C40 72(4) . . . . ?
B22 C39 B17 B18 108(4) . . . . ?
B22 C39 B17 B24 -32(4) . . . . ?
B22 C39 B17 B25 8(5) . . . . ?
B22 C39 B24 B17 146(4) . . . . ?
B22 C39 B24 B25 108(4) . . . . ?
B22 C39 B24 B23 44(4) . . . . ?
B22 C39 B19 B18 -143(4) . . . . ?
B22 C39 B19 B20 -104(4) . . . . ?
B22 C39 B19 B21 -41(4) . . . . ?
B22 B24 B25 C40 58(4) . . . . ?
B22 B24 B25 B17 97(4) . . . . ?
B22 B24 B25 B26 -5(5) . . . . ?
B22 B24 B25 B23 -44(4) . . . . ?
B22 B24 B23 B26 100(4) . . . . ?
B22 B24 B23 B25 135(4) . . . . ?
B22 B24 B23 B21 36(4) . . . . ?
B22 B19 B20 C40 -60(4) . . . . ?
B22 B19 B20 B18 -94(4) . . . . ?
B22 B19 B20 B26 6(5) . . . . ?
B22 B19 B20 B21 42(3) . . . . ?
B22 B19 B21 B26 -101(4) . . . . ?
B22 B19 B21 B20 -133(4) . . . . ?
B22 B19 B21 B23 -36(4) . . . . ?
B22 B21 B23 B24 -36(4) . . . . ?
B22 B21 B23 B26 -136(4) . . . . ?
B22 B21 B23 B25 -102(4) . . . . ?
B21 B19 B20 C40 -103(4) . . . . ?
B21 B19 B20 B18 -137(4) . . . . ?
B21 B19 B20 B26 -37(4) . . . . ?
B21 B19 B22 C39 133(4) . . . . ?
B21 B19 B22 B24 94(4) . . . . ?
B21 B19 B22 B23 36(3) . . . . ?
B21 B26 B25 C40 -97(4) . . . . ?
B21 B26 B25 B17 -67(5) . . . . ?
B21 B26 B25 B24 0(4) . . . . ?
B21 B26 B25 B23 35(3) . . . . ?
B21 B26 B20 C40 135(4) . . . . ?
B21 B26 B20 B18 103(4) . . . . ?
B21 B26 B20 B19 35(3) . . . . ?
B21 B22 B23 B24 140(4) . . . . ?
B21 B22 B23 B26 39(3) . . . . ?
B21 B22 B23 B25 99(4) . . . . ?
B6 B10 B1 C8 6(5) . . . . ?
B6 B10 B1 C9 99(5) . . . . ?
B6 B10 B1 B2 65(5) . . . . ?
B6 B10 B1 B9 -42(4) . . . . ?
B6 B10 B9 C8 95(4) . . . . ?
B6 B10 B9 B1 136(4) . . . . ?
B6 B10 B9 B7 38(4) . . . . ?
B6 B10 B5 C9 -138(4) . . . . ?
B6 B10 B5 B4 -107(5) . . . . ?
B6 B10 B5 B8 -37(4) . . . . ?
B6 B5 B8 B3 -111(5) . . . . ?
B6 B5 B8 B4 -145(4) . . . . ?
B6 B5 B8 B7 -38(5) . . . . ?
B6 B7 B8 B3 143(4) . . . . ?
B6 B7 B8 B4 109(5) . . . . ?
B6 B7 B8 B5 40(5) . . . . ?
B3 C8 B2 C9 103(4) . . . . ?
B3 C8 B2 B1 144(4) . . . . ?
B3 C8 B2 B4 44(4) . . . . ?
B3 C8 B1 C9 6(6) . . . . ?
B3 C8 B1 B2 -36(4) . . . . ?
B3 C8 B1 B10 67(5) . . . . ?
B3 C8 B1 B9 111(5) . . . . ?
B3 C8 B9 B10 -64(5) . . . . ?
B3 C8 B9 B1 -110(5) . . . . ?
B3 C8 B9 B6 -7(5) . . . . ?
B3 C8 B9 B7 32(4) . . . . ?
B3 C8 B7 B9 -149(4) . . . . ?
B3 C8 B7 B6 -107(4) . . . . ?
B3 C8 B7 B8 -46(4) . . . . ?
B3 B2 B4 C9 130(4) . . . . ?
B3 B2 B4 B5 96(4) . . . . ?
B3 B2 B4 B8 43(4) . . . . ?
B3 B4 B5 C9 95(4) . . . . ?
B3 B4 B5 B10 64(5) . . . . ?
B3 B4 B5 B6 2(5) . . . . ?
B3 B4 B5 B8 -32(4) . . . . ?
B3 B4 B8 B6 107(5) . . . . ?
B3 B4 B8 B5 143(4) . . . . ?
B3 B4 B8 B7 36(4) . . . . ?
B3 B7 B8 B6 -143(4) . . . . ?
B3 B7 B8 B4 -34(4) . . . . ?
B3 B7 B8 B5 -103(5) . . . . ?
B4 C9 B2 C8 -105(4) . . . . ?
B4 C9 B2 B1 -145(4) . . . . ?
B4 C9 B2 B3 -44(4) . . . . ?
B4 C9 B10 B1 111(4) . . . . ?
B4 C9 B10 B9 76(5) . . . . ?
B4 C9 B10 B6 8(6) . . . . ?
B4 C9 B10 B5 -31(4) . . . . ?
B4 C9 B1 C8 -6(6) . . . . ?
B4 C9 B1 B2 36(4) . . . . ?
B4 C9 B1 B10 -105(5) . . . . ?
B4 C9 B1 B9 -72(5) . . . . ?
B4 C9 B5 B10 148(4) . . . . ?
B4 C9 B5 B6 112(4) . . . . ?
B4 C9 B5 B8 50(4) . . . . ?
B4 B2 B3 C8 -131(4) . . . . ?
B4 B2 B3 B7 -98(4) . . . . ?
B4 B2 B3 B8 -43(4) . . . . ?
B4 B3 B8 B6 -108(5) . . . . ?
B4 B3 B8 B5 -35(4) . . . . ?
B4 B3 B8 B7 -145(4) . . . . ?
B4 B5 B8 B6 145(4) . . . . ?
B4 B5 B8 B3 34(4) . . . . ?
B4 B5 B8 B7 106(5) . . . . ?
B23 B24 B25 C40 102(4) . . . . ?
B23 B24 B25 B17 141(4) . . . . ?
B23 B24 B25 B26 39(4) . . . . ?
B23 B24 B22 C39 -133(4) . . . . ?
B23 B24 B22 B19 -96(4) . . . . ?
B23 B24 B22 B21 -35(4) . . . . ?
B23 B26 B25 C40 -132(4) . . . . ?
B23 B26 B25 B17 -102(4) . . . . ?
B23 B26 B25 B24 -35(3) . . . . ?
B23 B26 B20 C40 97(4) . . . . ?
B23 B26 B20 B18 65(4) . . . . ?
B23 B26 B20 B19 -3(5) . . . . ?
B23 B26 B20 B21 -38(3) . . . . ?
B23 B26 B21 B19 103(4) . . . . ?
B23 B26 B21 B20 136(4) . . . . ?
B23 B26 B21 B22 39(3) . . . . ?
B23 B22 B21 B19 -140(4) . . . . ?
B23 B22 B21 B26 -39(3) . . . . ?
B23 B22 B21 B20 -99(4) . . . . ?
B5 C9 B2 C8 -67(4) . . . . ?
B5 C9 B2 B1 -107(4) . . . . ?
B5 C9 B2 B3 -6(5) . . . . ?
B5 C9 B2 B4 38(4) . . . . ?
B5 C9 B10 B1 142(4) . . . . ?
B5 C9 B10 B9 107(4) . . . . ?
B5 C9 B10 B6 39(4) . . . . ?
B5 C9 B1 C8 63(5) . . . . ?
B5 C9 B1 B2 105(4) . . . . ?
B5 C9 B1 B10 -36(4) . . . . ?
B5 C9 B1 B9 -3(5) . . . . ?
B5 C9 B4 B2 -140(4) . . . . ?
B5 C9 B4 B3 -99(4) . . . . ?
B5 C9 B4 B8 -39(3) . . . . ?
B5 B10 B1 C8 -60(5) . . . . ?
B5 B10 B1 C9 33(4) . . . . ?
B5 B10 B1 B2 -1(5) . . . . ?
B5 B10 B1 B9 -108(4) . . . . ?
B5 B10 B9 C8 55(5) . . . . ?
B5 B10 B9 B1 95(5) . . . . ?
B5 B10 B9 B6 -40(4) . . . . ?
B5 B10 B9 B7 -3(5) . . . . ?
B5 B10 B6 B9 138(4) . . . . ?
B5 B10 B6 B7 94(5) . . . . ?
B5 B10 B6 B8 34(4) . . . . ?
B5 B6 B7 C8 63(4) . . . . ?
B5 B6 B7 B9 105(4) . . . . ?
B5 B6 B7 B3 4(5) . . . . ?
B5 B6 B7 B8 -31(4) . . . . ?
B5 B6 B8 B3 104(5) . . . . ?
B5 B6 B8 B4 35(4) . . . . ?
B5 B6 B8 B7 141(5) . . . . ?
B5 B4 B8 B6 -37(4) . . . . ?
B5 B4 B8 B3 -143(4) . . . . ?
B5 B4 B8 B7 -108(5) . . . . ?
C22 C21 C26 C25 0.0 . . . . ?
C21 P6 C10 C7 -137(2) . . . . ?
C21 P6 C10 C20 44(3) . . . . ?
C21 C22 C23 C24 0.0 . . . . ?
C21 C26 C25 C24 0.0 . . . . ?
C26 C25 C24 C23 0.0 . . . . ?
C25 C24 C23 C22 0.0 . . . . ?
C23 C22 C21 P6 179(2) . . . . ?
C23 C22 C21 C26 0.0 . . . . ?
C7 C17 C18 C19 0.0 . . . . ?
C17 C7 C10 P6 -179(3) . . . . ?
C17 C7 C10 C20 0.0 . . . . ?
C17 C18 C19 C20 0.0 . . . . ?
C18 C19 C20 C10 0.0 . . . . ?
C19 C20 C10 P6 179(4) . . . . ?
C19 C20 C10 C7 0.0 . . . . ?
C10 P6 C21 C22 -7(3) . . . . ?
C10 P6 C21 C26 172(2) . . . . ?
C10 C7 C17 C18 0.0 . . . . ?
C59 P3 C65 B29 2(3) . . . . ?
C59 P3 C65 B28 71(4) . . . . ?
C59 P3 C65 B27 147(4) . . . . ?
C59 P3 C65 B30 -60(4) . . . . ?
C59 P3 C65 B35 -137(3) . . . . ?
C59 P3 C53 C54 -86(2) . . . . ?
C59 P3 C53 C58 92(2) . . . . ?
C59 C60 C61 C62 0.0 . . . . ?
C60 C59 C64 C63 0.0 . . . . ?
C60 C61 C62 C63 0.0 . . . . ?
C61 C62 C63 C64 0.0 . . . . ?
C62 C63 C64 C59 0.0 . . . . ?
C64 C59 C60 C61 0.0 . . . . ?
C54 C55 C56 C57 0.0 . . . . ?
C55 C54 C53 P3 178(2) . . . . ?
C55 C54 C53 C58 0.0 . . . . ?
C55 C56 C57 C58 0.0 . . . . ?
C56 C57 C58 C53 0.0 . . . . ?
C57 C58 C53 P3 -178(3) . . . . ?
C57 C58 C53 C54 0.0 . . . . ?
C53 P3 C65 B29 116(3) . . . . ?
C53 P3 C65 B28 -175(3) . . . . ?
C53 P3 C65 B27 -99(4) . . . . ?
C53 P3 C65 B30 54(4) . . . . ?
C53 P3 C65 B35 -23(4) . . . . ?
C53 P3 C59 C60 -30(2) . . . . ?
C53 P3 C59 C64 153.5(18) . . . . ?
C53 C54 C55 C56 0.0 . . . . ?
C67 P2 C73 C74 155.8(18) . . . . ?
C67 P2 C73 C78 -29(2) . . . . ?
C67 P2 C66 B29 -6(4) . . . . ?
C67 P2 C66 B28 -73(4) . . . . ?
C67 P2 C66 B31 66(4) . . . . ?
C67 P2 C66 B32 143(4) . . . . ?
C67 P2 C66 B34 -146(4) . . . . ?
C67 C68 C69 C70 0.0 . . . . ?
C68 C67 C72 C71 0.0 . . . . ?
C68 C69 C70 C71 0.0 . . . . ?
C69 C70 C71 C72 0.0 . . . . ?
C70 C71 C72 C67 0.0 . . . . ?
C72 C67 C68 C69 0.0 . . . . ?
C49 C48 C47 P4 178(3) . . . . ?
C49 C48 C47 C52 0.0 . . . . ?
C48 C49 C50 C51 0.0 . . . . ?
C48 C47 C52 C51 0.0 . . . . ?
C47 P4 C40 B18 -129(4) . . . . ?
C47 P4 C40 B17 152(3) . . . . ?
C47 P4 C40 B26 19(4) . . . . ?
C47 P4 C40 B25 85(3) . . . . ?
C47 P4 C40 B20 -51(4) . . . . ?
C47 P4 C41 C42 -126(2) . . . . ?
C47 P4 C41 C46 52(3) . . . . ?
C47 C52 C51 C50 0.0 . . . . ?
C52 C51 C50 C49 0.0 . . . . ?
C50 C49 C48 C47 0.0 . . . . ?
C74 C73 C78 C77 0.0 . . . . ?
C73 P2 C67 C68 61(2) . . . . ?
C73 P2 C67 C72 -120.4(18) . . . . ?
C73 P2 C66 B29 -123(3) . . . . ?
C73 P2 C66 B28 170(3) . . . . ?
C73 P2 C66 B31 -51(4) . . . . ?
C73 P2 C66 B32 26(4) . . . . ?
C73 P2 C66 B34 97(4) . . . . ?
C73 C74 C75 C76 0.0 . . . . ?
C73 C78 C77 C76 0.0 . . . . ?
C78 C77 C76 C75 0.0 . . . . ?
C77 C76 C75 C74 0.0 . . . . ?
C75 C74 C73 P2 175(2) . . . . ?
C75 C74 C73 C78 0.0 . . . . ?
C2 C1 C6 C5 0.0 . . . . ?
C1 P1 C8 B2 -129(4) . . . . ?
C1 P1 C8 B1 153(4) . . . . ?
C1 P1 C8 B9 86(3) . . . . ?
C1 P1 C8 B3 -56(4) . . . . ?
C1 P1 C8 B7 18(4) . . . . ?
C1 P1 C12 C13 17(3) . . . . ?
C1 P1 C12 C11 -152.8(18) . . . . ?
C1 C2 C3 C4 0.0 . . . . ?
C1 C6 C5 C4 0.0 . . . . ?
C6 C5 C4 C3 0.0 . . . . ?
C5 C4 C3 C2 0.0 . . . . ?
C3 C2 C1 P1 -178(3) . . . . ?
C3 C2 C1 C6 0.0 . . . . ?
C15 C14 C13 C12 0.0 . . . . ?
C14 C15 C16 C11 0.0 . . . . ?
C14 C13 C12 P1 -169(3) . . . . ?
C14 C13 C12 C11 0.0 . . . . ?
C13 C12 C11 C16 0.0 . . . . ?
C12 P1 C8 B2 -15(4) . . . . ?
C12 P1 C8 B1 -93(4) . . . . ?
C12 P1 C8 B9 -160(3) . . . . ?
C12 P1 C8 B3 57(4) . . . . ?
C12 P1 C8 B7 132(3) . . . . ?
C12 P1 C1 C2 117(2) . . . . ?
C12 P1 C1 C6 -61(3) . . . . ?
C12 C11 C16 C15 0.0 . . . . ?
C16 C15 C14 C13 0.0 . . . . ?
C28 C29 C30 C31 0.0 . . . . ?
C29 C28 C27 P5 -175(4) . . . . ?
C29 C28 C27 C32 0.0 . . . . ?
C29 C30 C31 C32 0.0 . . . . ?
C30 C31 C32 C27 0.0 . . . . ?
C31 C32 C27 P5 175(4) . . . . ?
C31 C32 C27 C28 0.0 . . . . ?
C27 P5 C39 B18 132(4) . . . . ?
C27 P5 C39 B17 -156(3) . . . . ?
C27 P5 C39 B24 -88(3) . . . . ?
C27 P5 C39 B19 56(4) . . . . ?
C27 P5 C39 B22 -20(4) . . . . ?
C27 P5 C33 C34 -13(3) . . . . ?
C27 P5 C33 C38 172(2) . . . . ?
C27 C28 C29 C30 0.0 . . . . ?
C37 C36 C35 C34 0.0 . . . . ?
C36 C37 C38 C33 0.0 . . . . ?
C36 C35 C34 C33 0.0 . . . . ?
C35 C34 C33 P5 -174(3) . . . . ?
C35 C34 C33 C38 0.0 . . . . ?
C34 C33 C38 C37 0.0 . . . . ?
C33 P5 C39 B18 14(4) . . . . ?
C33 P5 C39 B17 86(3) . . . . ?
C33 P5 C39 B24 154(3) . . . . ?
C33 P5 C39 B19 -62(4) . . . . ?
C33 P5 C39 B22 -138(3) . . . . ?
C33 P5 C27 C28 -141(2) . . . . ?
C33 P5 C27 C32 44(4) . . . . ?
C38 C37 C36 C35 0.0 . . . . ?
B32 B31 C66 P2 115(4) . . . . ?
B32 B31 C66 B29 -141(4) . . . . ?
B32 B31 C66 B28 -106(5) . . . . ?
B32 B31 C66 B34 -32(4) . . . . ?
B32 B31 B36 B30 131(4) . . . . ?
B32 B31 B36 B33 31(4) . . . . ?
B32 B31 B36 B35 91(4) . . . . ?
B32 C66 B34 B28 -139(4) . . . . ?
B32 C66 B34 B27 -99(4) . . . . ?
B32 C66 B34 B33 -39(4) . . . . ?
B32 B33 B34 B28 98(4) . . . . ?
B32 B33 B34 B27 137(5) . . . . ?
B32 B33 B34 C66 39(4) . . . . ?
B32 B33 B36 B30 -97(4) . . . . ?
B32 B33 B36 B31 -33(4) . . . . ?
B32 B33 B36 B35 -137(5) . . . . ?
B32 B33 B35 B27 -95(5) . . . . ?
B32 B33 B35 C65 -59(5) . . . . ?
B32 B33 B35 B30 3(6) . . . . ?
B32 B33 B35 B36 39(4) . . . . ?
B32 B36 B35 B27 5(6) . . . . ?
B32 B36 B35 C65 64(5) . . . . ?
B32 B36 B35 B30 102(4) . . . . ?
B32 B36 B35 B33 -36(4) . . . . ?
C66 P2 C67 C68 -53(3) . . . . ?
C66 P2 C67 C72 125(2) . . . . ?
C66 P2 C73 C74 -89(2) . . . . ?
C66 P2 C73 C78 87(2) . . . . ?
C66 B29 B28 B27 -93(5) . . . . ?
C66 B29 B28 C65 -124(4) . . . . ?
C66 B29 B28 B34 -29(4) . . . . ?
C66 B29 C65 P3 151(3) . . . . ?
C66 B29 C65 B28 42(4) . . . . ?
C66 B29 C65 B27 6(5) . . . . ?
C66 B29 C65 B30 -98(4) . . . . ?
C66 B29 C65 B35 -68(4) . . . . ?
C66 B29 B30 C65 86(3) . . . . ?
C66 B29 B30 B31 -40(3) . . . . ?
C66 B29 B30 B36 -4(5) . . . . ?
C66 B29 B30 B35 60(4) . . . . ?
C66 B28 B27 C65 -101(4) . . . . ?
C66 B28 B27 B33 -5(5) . . . . ?
C66 B28 B27 B34 38(3) . . . . ?
C66 B28 B27 B35 -68(4) . . . . ?
C66 B28 C65 P3 -150(3) . . . . ?
C66 B28 C65 B29 -51(4) . . . . ?
C66 B28 C65 B27 95(5) . . . . ?
C66 B28 C65 B30 -17(6) . . . . ?
C66 B28 C65 B35 57(6) . . . . ?
C66 B28 B34 B27 -135(4) . . . . ?
C66 B28 B34 B32 -35(3) . . . . ?
C66 B28 B34 B33 -96(4) . . . . ?
C66 B31 B32 B33 100(5) . . . . ?
C66 B31 B32 B34 30(4) . . . . ?
C66 B31 B32 B36 134(4) . . . . ?
C66 B31 B36 B30 95(4) . . . . ?
C66 B31 B36 B32 -36(3) . . . . ?
C66 B31 B36 B33 -5(5) . . . . ?
C66 B31 B36 B35 55(5) . . . . ?
C66 B32 B33 B27 -5(5) . . . . ?
C66 B32 B33 B34 -42(4) . . . . ?
C66 B32 B33 B36 97(4) . . . . ?
C66 B32 B33 B35 58(5) . . . . ?
C66 B32 B34 B28 35(3) . . . . ?
C66 B32 B34 B27 97(4) . . . . ?
C66 B32 B34 B33 134(4) . . . . ?
C66 B32 B36 B30 -3(5) . . . . ?
C66 B32 B36 B31 40(4) . . . . ?
C66 B32 B36 B33 -105(4) . . . . ?
C66 B32 B36 B35 -69(5) . . . . ?
B33 B27 C65 P3 151(3) . . . . ?
B33 B27 C65 B29 -69(5) . . . . ?
B33 B27 C65 B28 -104(4) . . . . ?
B33 B27 C65 B30 -2(5) . . . . ?
B33 B27 C65 B35 38(4) . . . . ?
B33 B27 B34 B28 135(4) . . . . ?
B33 B27 B34 B32 37(4) . . . . ?
B33 B27 B34 C66 97(4) . . . . ?
B33 B27 B35 C65 -137(4) . . . . ?
B33 B27 B35 B30 -102(4) . . . . ?
B33 B27 B35 B36 -42(4) . . . . ?
B33 B32 C66 P2 148(3) . . . . ?
B33 B32 C66 B29 -65(5) . . . . ?
B33 B32 C66 B28 3(5) . . . . ?
B33 B32 C66 B31 -105(4) . . . . ?
B33 B32 C66 B34 43(4) . . . . ?
B33 B32 B34 B28 -99(4) . . . . ?
B33 B32 B34 B27 -37(4) . . . . ?
B33 B32 B34 C66 -134(4) . . . . ?
B33 B32 B36 B30 101(4) . . . . ?
B33 B32 B36 B31 144(5) . . . . ?
B33 B32 B36 B35 35(4) . . . . ?
B33 B36 B35 B27 41(4) . . . . ?
B33 B36 B35 C65 99(4) . . . . ?
B33 B36 B35 B30 138(4) . . . . ?
B34 B28 B27 C65 -139(4) . . . . ?
B34 B28 B27 B33 -43(4) . . . . ?
B34 B28 B27 B35 -106(4) . . . . ?
B34 B28 C65 P3 150(3) . . . . ?
B34 B28 C65 B29 -112(4) . . . . ?
B34 B28 C65 B27 35(4) . . . . ?
B34 B28 C65 B30 -77(5) . . . . ?
B34 B28 C65 B35 -4(6) . . . . ?
B34 B28 C66 P2 -108(4) . . . . ?
B34 B28 C66 B29 149(4) . . . . ?
B34 B28 C66 B31 112(5) . . . . ?
B34 B28 C66 B32 39(4) . . . . ?
B34 B27 C65 P3 -142(4) . . . . ?
B34 B27 C65 B29 -2(6) . . . . ?
B34 B27 C65 B28 -37(4) . . . . ?
B34 B27 C65 B30 65(5) . . . . ?
B34 B27 C65 B35 106(4) . . . . ?
B34 B27 B33 B32 -36(4) . . . . ?
B34 B27 B33 B36 -98(4) . . . . ?
B34 B27 B33 B35 -139(4) . . . . ?
B34 B27 B35 C65 -97(5) . . . . ?
B34 B27 B35 B30 -63(5) . . . . ?
B34 B27 B35 B33 39(4) . . . . ?
B34 B27 B35 B36 -3(6) . . . . ?
B34 B32 C66 P2 104(4) . . . . ?
B34 B32 C66 B29 -108(4) . . . . ?
B34 B32 C66 B28 -40(4) . . . . ?
B34 B32 C66 B31 -148(4) . . . . ?
B34 B32 B33 B27 36(4) . . . . ?
B34 B32 B33 B36 138(5) . . . . ?
B34 B32 B33 B35 99(5) . . . . ?
B34 B32 B36 B30 60(5) . . . . ?
B34 B32 B36 B31 103(5) . . . . ?
B34 B32 B36 B33 -41(4) . . . . ?
B34 B32 B36 B35 -6(6) . . . . ?
B34 B33 B36 B30 -62(4) . . . . ?
B34 B33 B36 B31 2(5) . . . . ?
B34 B33 B36 B32 36(4) . . . . ?
B34 B33 B36 B35 -101(5) . . . . ?
B34 B33 B35 B27 -35(4) . . . . ?
B34 B33 B35 C65 1(5) . . . . ?
B34 B33 B35 B30 63(5) . . . . ?
B34 B33 B35 B36 99(4) . . . . ?
B36 B30 B31 B29 -142(4) . . . . ?
B36 B30 B31 B32 -43(4) . . . . ?
B36 B30 B31 C66 -98(4) . . . . ?
B36 B31 B32 C66 -134(4) . . . . ?
B36 B31 B32 B33 -34(4) . . . . ?
B36 B31 B32 B34 -104(4) . . . . ?
B36 B31 C66 P2 154(3) . . . . ?
B36 B31 C66 B29 -102(4) . . . . ?
B36 B31 C66 B28 -67(5) . . . . ?
B36 B31 C66 B32 39(4) . . . . ?
B36 B31 C66 B34 7(5) . . . . ?
B36 B32 C66 P2 -146(3) . . . . ?
B36 B32 C66 B29 1(5) . . . . ?
B36 B32 C66 B28 69(5) . . . . ?
B36 B32 C66 B31 -39(3) . . . . ?
B36 B32 C66 B34 109(4) . . . . ?
B36 B32 B33 B27 -102(4) . . . . ?
B36 B32 B33 B34 -138(5) . . . . ?
B36 B32 B33 B35 -39(4) . . . . ?
B36 B32 B34 B28 -59(5) . . . . ?
B36 B32 B34 B27 4(6) . . . . ?
B36 B32 B34 C66 -93(5) . . . . ?
B36 B32 B34 B33 41(4) . . . . ?
B36 B33 B34 B28 61(5) . . . . ?
B36 B33 B34 B27 100(4) . . . . ?
B36 B33 B34 B32 -37(4) . . . . ?
B36 B33 B34 C66 2(5) . . . . ?
B36 B33 B35 B27 -134(4) . . . . ?
B36 B33 B35 C65 -98(4) . . . . ?
B36 B33 B35 B30 -36(4) . . . . ?
B35 B27 C65 P3 113(4) . . . . ?
B35 B27 C65 B29 -107(5) . . . . ?
B35 B27 C65 B28 -143(4) . . . . ?
B35 B27 C65 B30 -40(4) . . . . ?
B35 B27 B33 B32 103(4) . . . . ?
B35 B27 B33 B34 139(4) . . . . ?
B35 B27 B33 B36 41(4) . . . . ?
B35 B27 B34 B28 98(5) . . . . ?
B35 B27 B34 B32 0(6) . . . . ?
B35 B27 B34 C66 60(6) . . . . ?
B35 B27 B34 B33 -37(4) . . . . ?
B35 C65 B30 B29 -151(4) . . . . ?
B35 C65 B30 B31 -100(4) . . . . ?
B35 C65 B30 B36 -38(3) . . . . ?
B35 B30 B31 B29 -106(4) . . . . ?
B35 B30 B31 B32 -6(5) . . . . ?
B35 B30 B31 C66 -62(5) . . . . ?
B35 B30 B31 B36 36(4) . . . . ?
B35 B30 B36 B31 -139(4) . . . . ?
B35 B30 B36 B32 -95(4) . . . . ?
B35 B30 B36 B33 -36(3) . . . . ?
B35 B33 B34 B28 -3(5) . . . . ?
B35 B33 B34 B27 37(4) . . . . ?
B35 B33 B34 B32 -101(5) . . . . ?
B35 B33 B34 C66 -62(5) . . . . ?
B35 B33 B36 B30 39(4) . . . . ?
B35 B33 B36 B31 103(5) . . . . ?
B35 B33 B36 B32 137(5) . . . . ?
B7 C8 B2 C9 66(5) . . . . ?
B7 C8 B2 B1 107(5) . . . . ?
B7 C8 B2 B3 -38(4) . . . . ?
B7 C8 B2 B4 6(5) . . . . ?
B7 C8 B1 C9 -68(5) . . . . ?
B7 C8 B1 B2 -110(4) . . . . ?
B7 C8 B1 B10 -7(5) . . . . ?
B7 C8 B1 B9 37(4) . . . . ?
B7 C8 B9 B10 -96(4) . . . . ?
B7 C8 B9 B1 -142(4) . . . . ?
B7 C8 B9 B6 -39(3) . . . . ?
B7 C8 B3 B2 143(4) . . . . ?
B7 C8 B3 B4 101(4) . . . . ?
B7 C8 B3 B8 40(3) . . . . ?
B7 B9 B6 B10 -133(5) . . . . ?
B7 B9 B6 B5 -95(5) . . . . ?
B7 B9 B6 B8 -38(4) . . . . ?
B7 B6 B5 C9 -67(5) . . . . ?
B7 B6 B5 B10 -105(4) . . . . ?
B7 B6 B5 B4 -4(5) . . . . ?
B7 B6 B5 B8 33(4) . . . . ?
B7 B6 B8 B3 -38(4) . . . . ?
B7 B6 B8 B4 -106(5) . . . . ?
B7 B6 B8 B5 -141(5) . . . . ?
B7 B3 B4 C9 60(4) . . . . ?
B7 B3 B4 B2 101(4) . . . . ?
B7 B3 B4 B5 0(5) . . . . ?
B7 B3 B4 B8 -29(3) . . . . ?
B7 B3 B8 B6 37(4) . . . . ?
B7 B3 B8 B4 145(4) . . . . ?
B7 B3 B8 B5 110(5) . . . . ?
B8 B6 B5 C9 -100(5) . . . . ?
B8 B6 B5 B10 -138(5) . . . . ?
B8 B6 B5 B4 -36(4) . . . . ?
B8 B6 B7 C8 94(4) . . . . ?
B8 B6 B7 B9 136(5) . . . . ?
B8 B6 B7 B3 35(4) . . . . ?
B8 B3 B4 C9 89(4) . . . . ?
B8 B3 B4 B2 130(4) . . . . ?
B8 B3 B4 B5 29(3) . . . . ?
B8 B4 B5 C9 127(4) . . . . ?
B8 B4 B5 B10 96(5) . . . . ?
B8 B4 B5 B6 34(4) . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 -0.075 0.218 0.688 85.8 18.1 ?
2 0.075 0.782 0.312 85.8 12.3 ?
3 0.097 0.663 0.963 10.6 0.0 ?
4 0.500 0.000 1.000 304.0 49.5 ?
5 0.180 0.162 0.022 16.3 0.0 ?
6 0.417 0.338 0.950 7.3 0.0 ?
7 0.583 0.663 0.050 7.3 0.0 ?
8 0.820 0.838 0.978 16.3 0.0 ?
9 0.903 0.337 0.037 10.6 0.0 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_cu_20251114_zz_nlg_xhh_25313_0m_pl
_database_code_depnum_ccdc_archive 'CCDC 2504018'
loop_
_audit_author_name
_audit_author_address
'Hao-Hui Xie'
;NanJing University of Science and Technology
China
;
_audit_update_record             
;
2025-11-19 deposited with the CCDC.	2026-03-06 downloaded from the CCDC.
;
_audit_creation_date             2025-11-17
_audit_creation_method           
;
Olex2 1.5
(compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C104 H120 Au7 B38 P8'
_chemical_formula_sum            'C104 H120 Au7 B38 P8'
_chemical_formula_weight         3407.30
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -4.4197 7.2980 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'C 1 2/c 1'
_space_group_name_Hall           '-C 2yc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   20.7101(11)
_cell_length_b                   24.5585(12)
_cell_length_c                   30.2178(14)
_cell_angle_alpha                90
_cell_angle_beta                 108.257(3)
_cell_angle_gamma                90
_cell_volume                     14595.4(13)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9906
_cell_measurement_temperature    193.15
_cell_measurement_theta_max      68.365
_cell_measurement_theta_min      2.878
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    13.986
_exptl_absorpt_correction_T_max  0.7531
_exptl_absorpt_correction_T_min  0.5241
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1057 before and 0.0752 after correction.
The Ratio of minimum to maximum transmission is 0.6959.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.551
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             6428
_exptl_crystal_size_max          0.12
_exptl_crystal_size_mid          0.08
_exptl_crystal_size_min          0.07
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0791
_diffrn_reflns_av_unetI/netI     0.0479
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max       24
_diffrn_reflns_limit_h_min       -24
_diffrn_reflns_limit_k_max       29
_diffrn_reflns_limit_k_min       -29
_diffrn_reflns_limit_l_max       36
_diffrn_reflns_limit_l_min       -36
_diffrn_reflns_number            84544
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         68.623
_diffrn_reflns_theta_min         2.878
_diffrn_ambient_temperature      193.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  multi-scan
_diffrn_measurement_method       ?
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_source                   ?
_diffrn_source_current           1.11
_diffrn_source_power             0.05550000000000001
_diffrn_source_voltage           50.0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                10593
_reflns_number_total             13433
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.41 (?, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.41 (?, 2016)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    ?
_refine_diff_density_max         1.344
_refine_diff_density_min         -1.198
_refine_diff_density_rms         0.180
_refine_ls_extinction_coef       0.0000290(19)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
_refine_ls_goodness_of_fit_ref   1.033
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     713
_refine_ls_number_reflns         13433
_refine_ls_number_restraints     4
_refine_ls_R_factor_all          0.0521
_refine_ls_R_factor_gt           0.0407
_refine_ls_restrained_S_all      1.037
_refine_ls_shift/su_max          0.008
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0530P)²+30.4026P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0997
_refine_ls_wR_factor_ref         0.1051
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups
2. Restrained distances
 H1-H38
 2.1 with sigma of 0.01
 B2-H2A \\sim B2-H2B
 with sigma of 0.02
 B2-H2B \\sim B3-H2B
 with sigma of 0.02
3. Rigid body (RIGU) restrains
 H2A
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 H2B
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
4.a Aromatic/amide H refined with riding coordinates:
 C18(H18), C19(H19), C16(H16), C20(H20), C17(H17), C42(H42), C32(H32),
 C22(H22), C23(H23), C26(H26), C25(H25), C24(H24), C34(H34), C29(H29), C30(H30),
  C38(H38), C2(H2), C28(H28), C8(H8), C12(H12), C37(H37), C6(H6), C31(H31),
 C43(H43), C46(H46), C48(H48), C3(H3), C35(H35), C5(H5), C45(H45), C9(H9),
 C49(H49), C51(H51), C44(H44), C4(H4), C11(H11), C10(H10), C36(H36), C50(H50),
 C52(H52)
4.b Boron cage BH refined with riding coordinates:
 B13(H13), B12(H12A), B14(H14), B11(H11A), B15(H15), B16(H16A), B18(H18A),
 B19(H19A), B17(H17A), B2(H2A), B1(H1), B3(H3A), B6(H6A), B10(H10A), B4(H4A),
 B5(H5A), B7(H7), B8(H8A), B9(H9A)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au1 Au 0.49465(2) 0.30294(2) 0.33083(2) 0.04224(9) Uani 1 1 d . . . . .
Au2 Au 0.43874(2) 0.39976(2) 0.30863(2) 0.03659(9) Uani 1 1 d . . . . .
Au4 Au 0.63102(2) 0.33578(2) 0.25868(2) 0.04849(10) Uani 1 1 d . . . . .
Au3 Au 0.500000 0.35465(2) 0.250000 0.03599(10) Uani 1 2 d S T P . .
P55 P 0.47498(9) 0.43422(7) 0.38532(5) 0.0381(4) Uani 1 1 d . . . . .
P12 P 0.53492(11) 0.22651(8) 0.37546(6) 0.0470(4) Uani 1 1 d . . . . .
P37 P 0.36306(9) 0.47649(7) 0.29416(6) 0.0418(4) Uani 1 1 d . . . . .
P7 P 0.73052(11) 0.29013(8) 0.29284(7) 0.0509(5) Uani 1 1 d . . . . .
C15 C 0.5359(4) 0.2352(3) 0.4354(3) 0.055(2) Uani 1 1 d . . . . .
C13 C 0.7180(4) 0.2444(3) 0.3386(2) 0.0462(17) Uani 1 1 d . . . . .
C18 C 0.5333(7) 0.2552(4) 0.5251(3) 0.088(4) Uani 1 1 d . . . . .
H18 H 0.530170 0.261768 0.555379 0.105 Uiso 1 1 calc R U . . .
C19 C 0.5582(6) 0.2065(5) 0.5162(3) 0.082(3) Uani 1 1 d . . . . .
H19 H 0.573872 0.179991 0.540039 0.098 Uiso 1 1 calc R U . . .
C16 C 0.5147(6) 0.2834(4) 0.4469(3) 0.081(3) Uani 1 1 d . . . . .
H16 H 0.500339 0.310866 0.423743 0.097 Uiso 1 1 calc R U . . .
C20 C 0.5600(5) 0.1963(4) 0.4709(3) 0.073(3) Uani 1 1 d . . . . .
H20 H 0.577749 0.162747 0.464149 0.087 Uiso 1 1 calc R U . . .
C17 C 0.5132(7) 0.2940(4) 0.4928(3) 0.099(4) Uani 1 1 d . . . . .
H17 H 0.498098 0.328304 0.500317 0.119 Uiso 1 1 calc R U . . .
C39 C 0.4695(4) 0.5081(3) 0.3778(2) 0.0395(16) Uani 1 1 d . . . . .
C42 C 0.3478(4) 0.4913(3) 0.2008(2) 0.0451(17) Uani 1 1 d . . . . .
H42 H 0.385501 0.467332 0.205963 0.054 Uiso 1 1 calc R U . . .
C32 C 0.6099(4) 0.4098(3) 0.4025(3) 0.0474(17) Uani 1 1 d . . . . .
H32 H 0.597754 0.404867 0.369766 0.057 Uiso 1 1 calc R U . . .
C21 C 0.4917(5) 0.1641(3) 0.3517(3) 0.056(2) Uani 1 1 d . . . . .
C33 C 0.4157(4) 0.4145(3) 0.4152(2) 0.0501(18) Uani 1 1 d . . . . .
C22 C 0.4597(6) 0.1622(4) 0.3050(3) 0.088(4) Uani 1 1 d . . . . .
H22 H 0.456531 0.194293 0.286809 0.106 Uiso 1 1 calc R U . . .
C41 C 0.3241(4) 0.5049(3) 0.2370(2) 0.0475(18) Uani 1 1 d . . . . .
C23 C 0.4317(7) 0.1141(4) 0.2836(4) 0.097(4) Uani 1 1 d . . . . .
H23 H 0.412141 0.113034 0.250634 0.116 Uiso 1 1 calc R U . . .
C26 C 0.4894(8) 0.1191(4) 0.3776(4) 0.113(5) Uani 1 1 d . . . . .
H26 H 0.506404 0.120872 0.410681 0.136 Uiso 1 1 calc R U . . .
C25 C 0.4624(9) 0.0708(6) 0.3560(5) 0.150(7) Uani 1 1 d . . . . .
H25 H 0.465296 0.038909 0.374324 0.180 Uiso 1 1 calc R U . . .
C24 C 0.4317(7) 0.0679(5) 0.3091(5) 0.104(4) Uani 1 1 d . . . . .
H24 H 0.411055 0.035208 0.294603 0.125 Uiso 1 1 calc R U . . .
C14 C 0.6245(4) 0.2140(3) 0.3779(2) 0.0460(18) Uani 1 1 d . . . . .
C27 C 0.5607(4) 0.4217(2) 0.4233(2) 0.0404(16) Uani 1 1 d . . . . .
C34 C 0.3751(6) 0.3684(4) 0.3989(3) 0.079(3) Uani 1 1 d . . . . .
H34 H 0.378162 0.349874 0.372012 0.095 Uiso 1 1 calc R U . . .
C1 C 0.8015(4) 0.3331(4) 0.3238(3) 0.062(2) Uani 1 1 d . . . . .
C29 C 0.6450(5) 0.4192(4) 0.4979(3) 0.062(2) Uani 1 1 d . . . . .
H29 H 0.656741 0.421567 0.530904 0.074 Uiso 1 1 calc R U . . .
C30 C 0.6950(5) 0.4097(3) 0.4776(3) 0.062(2) Uani 1 1 d . . . . .
H30 H 0.741256 0.406289 0.496235 0.074 Uiso 1 1 calc R U . . .
C38 C 0.4019(4) 0.4401(3) 0.4525(3) 0.059(2) Uani 1 1 d . . . . .
H38 H 0.426171 0.472728 0.463735 0.070 Uiso 1 1 calc DR U . . .
C47 C 0.2918(4) 0.4627(3) 0.3144(3) 0.054(2) Uani 1 1 d . . . . .
C2 C 0.8685(5) 0.3161(5) 0.3343(4) 0.081(3) Uani 1 1 d . . . . .
H2 H 0.879113 0.281486 0.324332 0.098 Uiso 1 1 calc R U . . .
C40 C 0.4136(4) 0.5293(3) 0.3318(2) 0.0405(16) Uani 1 1 d . . . . .
C28 C 0.5787(4) 0.4253(3) 0.4710(2) 0.0499(19) Uani 1 1 d . . . . .
H28 H 0.544768 0.432163 0.485412 0.060 Uiso 1 1 calc R U . . .
C8 C 0.8074(5) 0.2127(4) 0.2606(3) 0.072(3) Uani 1 1 d . . . . .
H8 H 0.834282 0.206667 0.291999 0.087 Uiso 1 1 calc R U . . .
C12 C 0.7149(6) 0.2573(4) 0.2041(3) 0.091(4) Uani 1 1 d . . . . .
H12 H 0.677867 0.282067 0.196407 0.109 Uiso 1 1 calc R U . . .
C37 C 0.3583(5) 0.4236(4) 0.4737(3) 0.075(3) Uani 1 1 d . . . . .
H37 H 0.352508 0.443684 0.499110 0.090 Uiso 1 1 calc R U . . .
C6 C 0.7873(5) 0.3846(4) 0.3372(3) 0.077(3) Uani 1 1 d . . . . .
H6 H 0.741555 0.397057 0.327902 0.092 Uiso 1 1 calc R U . . .
C31 C 0.6771(4) 0.4051(3) 0.4301(3) 0.0524(19) Uani 1 1 d . . . . .
H31 H 0.711263 0.398619 0.415856 0.063 Uiso 1 1 calc R U . . .
C43 C 0.3167(5) 0.5126(4) 0.1569(3) 0.067(2) Uani 1 1 d . . . . .
H43 H 0.332492 0.502491 0.131743 0.080 Uiso 1 1 calc R U . . .
C46 C 0.2687(5) 0.5401(4) 0.2289(3) 0.071(3) Uani 1 1 d . . . . .
H46 H 0.251574 0.549375 0.253673 0.085 Uiso 1 1 calc R U . . .
C48 C 0.2766(5) 0.4885(4) 0.3503(3) 0.065(2) Uani 1 1 d . . . . .
H48 H 0.305370 0.517001 0.366415 0.077 Uiso 1 1 calc R U . . .
C3 C 0.9202(5) 0.3509(6) 0.3599(5) 0.102(4) Uani 1 1 d . . . . .
H3 H 0.966260 0.339603 0.367267 0.122 Uiso 1 1 calc R U . . .
C35 C 0.3304(8) 0.3496(6) 0.4216(5) 0.127(6) Uani 1 1 d . . . . .
H35 H 0.305382 0.317128 0.411135 0.152 Uiso 1 1 calc R U . . .
C5 C 0.8378(6) 0.4180(5) 0.3637(4) 0.098(4) Uani 1 1 d . . . . .
H5 H 0.827237 0.452097 0.374552 0.118 Uiso 1 1 calc R U . . .
C7 C 0.7534(5) 0.2492(4) 0.2506(3) 0.062(2) Uani 1 1 d . . . . .
C45 C 0.2387(5) 0.5616(4) 0.1848(3) 0.077(3) Uani 1 1 d . . . . .
H45 H 0.201079 0.585675 0.179322 0.092 Uiso 1 1 calc R U . . .
C9 C 0.8221(7) 0.1854(5) 0.2251(4) 0.097(4) Uani 1 1 d . . . . .
H9 H 0.859152 0.160528 0.232518 0.116 Uiso 1 1 calc R U . . .
C49 C 0.2215(6) 0.4746(5) 0.3635(4) 0.095(4) Uani 1 1 d . . . . .
H49 H 0.212841 0.493430 0.388525 0.114 Uiso 1 1 calc R U . . .
C51 C 0.1925(7) 0.4069(7) 0.3048(6) 0.144(7) Uani 1 1 d . . . . .
H51 H 0.164178 0.377859 0.289121 0.173 Uiso 1 1 calc R U . . .
C44 C 0.2631(5) 0.5482(4) 0.1493(3) 0.077(3) Uani 1 1 d . . . . .
H44 H 0.243064 0.563532 0.119288 0.092 Uiso 1 1 calc R U . . .
C4 C 0.9057(6) 0.4006(6) 0.3744(4) 0.098(4) Uani 1 1 d . . . . .
H4 H 0.941612 0.423600 0.391729 0.118 Uiso 1 1 calc R U . . .
C11 C 0.7308(7) 0.2291(5) 0.1689(4) 0.105(5) Uani 1 1 d . . . . .
H11 H 0.704204 0.234767 0.137402 0.126 Uiso 1 1 calc R U . . .
C10 C 0.7847(7) 0.1932(4) 0.1792(4) 0.099(4) Uani 1 1 d . . . . .
H10 H 0.795587 0.174208 0.155042 0.119 Uiso 1 1 calc R U . . .
C36 C 0.3219(7) 0.3771(5) 0.4584(4) 0.101(4) Uani 1 1 d . . . . .
H36 H 0.290880 0.364016 0.473443 0.122 Uiso 1 1 calc R U . . .
C50 C 0.1783(8) 0.4334(7) 0.3410(6) 0.146(7) Uani 1 1 d . . . . .
H50 H 0.139986 0.423561 0.350124 0.175 Uiso 1 1 calc R U . . .
C52 C 0.2477(6) 0.4222(5) 0.2912(4) 0.095(4) Uani 1 1 d . . . . .
H52 H 0.255565 0.404600 0.265399 0.114 Uiso 1 1 calc R U . . .
B13 B 0.7625(5) 0.1996(4) 0.4268(3) 0.055(2) Uani 1 1 d . . . . .
H13 H 0.804028 0.193483 0.460562 0.066 Uiso 1 1 calc R U . . .
B12 B 0.6812(5) 0.1700(4) 0.4155(3) 0.051(2) Uani 1 1 d . . . . .
H12A H 0.667780 0.144298 0.441974 0.061 Uiso 1 1 calc R U . . .
B14 B 0.6904(5) 0.2419(4) 0.4224(3) 0.050(2) Uani 1 1 d . . . . .
H14 H 0.682959 0.263751 0.452970 0.060 Uiso 1 1 calc R U . . .
B11 B 0.6488(5) 0.1548(3) 0.3553(3) 0.053(2) Uani 1 1 d . . . . .
H11A H 0.614301 0.119285 0.341928 0.063 Uiso 1 1 calc R U . . .
B15 B 0.6651(5) 0.2710(3) 0.3657(3) 0.045(2) Uani 1 1 d . . . . .
H15 H 0.641723 0.312515 0.358500 0.054 Uiso 1 1 calc R U . . .
B16 B 0.7522(5) 0.2617(4) 0.3969(3) 0.054(2) Uani 1 1 d . . . . .
H16A H 0.786794 0.297078 0.410667 0.064 Uiso 1 1 calc R U . . .
B18 B 0.7358(5) 0.1467(4) 0.3857(3) 0.056(2) Uani 1 1 d . . . . .
H18A H 0.759566 0.105323 0.392488 0.067 Uiso 1 1 calc R U . . .
B19 B 0.7096(5) 0.1758(3) 0.3292(3) 0.052(2) Uani 1 1 d . . . . .
H19A H 0.716252 0.154747 0.297999 0.062 Uiso 1 1 calc R U . . .
B17 B 0.7799(5) 0.2029(4) 0.3734(3) 0.054(2) Uani 1 1 d . . . . .
H17A H 0.832713 0.199473 0.371231 0.065 Uiso 1 1 calc R U . . .
B2 B 0.4300(5) 0.6094(3) 0.3984(3) 0.047(2) Uani 1 1 d D . . . .
H2A H 0.397928 0.622899 0.420137 0.057 Uiso 1 1 calc DR U . A 1
B1 B 0.4856(4) 0.5529(3) 0.4198(3) 0.046(2) Uani 1 1 d . . . . .
H1 H 0.480283 0.535819 0.452848 0.055 Uiso 1 1 calc DR U . . .
B3 B 0.3838(4) 0.5887(3) 0.3383(3) 0.0425(19) Uani 1 1 d D . . . .
H3A H 0.327086 0.589939 0.329566 0.051 Uiso 1 1 calc R U . . .
B6 B 0.5158(5) 0.6101(4) 0.4024(3) 0.055(2) Uani 1 1 d . . . . .
H6A H 0.551061 0.638250 0.428000 0.065 Uiso 1 1 calc R U . . .
B10 B 0.6388(5) 0.2162(4) 0.3246(3) 0.049(2) Uani 1 1 d . . . . .
H10A H 0.597634 0.221350 0.290464 0.059 Uiso 1 1 calc R U . . .
B4 B 0.4441(5) 0.5837(4) 0.3069(3) 0.050(2) Uani 1 1 d . . . . .
H4A H 0.431618 0.593386 0.268974 0.060 Uiso 1 1 calc R U . . .
B5 B 0.4522(5) 0.6337(3) 0.3502(3) 0.049(2) Uani 1 1 d . . . . .
H5A H 0.443921 0.677679 0.340445 0.058 Uiso 1 1 calc R U . . .
B7 B 0.5249(5) 0.5966(3) 0.3462(3) 0.049(2) Uani 1 1 d . . . . .
H7 H 0.565663 0.616216 0.334605 0.059 Uiso 1 1 calc R U . . .
B8 B 0.4979(4) 0.5294(3) 0.3320(3) 0.0423(18) Uani 1 1 d . . . . .
H8A H 0.519851 0.502389 0.310453 0.051 Uiso 1 1 calc R U . . .
B9 B 0.5436(4) 0.5458(3) 0.3896(3) 0.0452(19) Uani 1 1 d . . . . .
H9A H 0.596499 0.530102 0.405858 0.054 Uiso 1 1 calc R U . . .
H2B H 0.391(6) 0.581(5) 0.3762(6) 0.22(8) Uiso 1 1 d D . . B 2


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au1 Au2 2.6377(4) . ?
Au1 Au4 3.2139(5) 2_655 ?
Au1 Au3 2.7858(3) . ?
Au1 P12 2.3094(18) . ?
Au2 Au4 2.6177(4) 2_655 ?
Au2 Au3 2.7173(3) . ?
Au2 P55 2.3581(16) . ?
Au2 P37 2.4019(18) . ?
Au4 Au3 2.6834(4) . ?
Au4 P7 2.2881(19) . ?
P55 C39 1.827(7) . ?
P55 C33 1.804(8) . ?
P55 C27 1.813(7) . ?
P12 C15 1.818(8) . ?
P12 C21 1.806(9) . ?
P12 C14 1.860(8) . ?
P37 C41 1.803(7) . ?
P37 C47 1.799(9) . ?
P37 C40 1.822(7) . ?
P7 C13 1.861(7) . ?
P7 C1 1.812(10) . ?
P7 C7 1.801(9) . ?
C15 C16 1.343(12) . ?
C15 C20 1.407(11) . ?
C13 B15 1.692(11) . ?
C13 B16 1.734(11) . ?
C13 B19 1.709(11) . ?
C13 B17 1.717(11) . ?
C13 B10 1.707(13) . ?
C18 H18 0.9500 . ?
C18 C19 1.363(15) . ?
C18 C17 1.336(15) . ?
C19 H19 0.9500 . ?
C19 C20 1.402(13) . ?
C16 H16 0.9500 . ?
C16 C17 1.422(12) . ?
C20 H20 0.9500 . ?
C17 H17 0.9500 . ?
C39 C40 1.593(9) . ?
C39 B1 1.634(9) . ?
C39 B8 1.747(11) . ?
C39 B9 1.732(11) . ?
C42 H42 0.9500 . ?
C42 C41 1.372(10) . ?
C42 C43 1.384(10) . ?
C32 H32 0.9500 . ?
C32 C27 1.385(10) . ?
C32 C31 1.384(11) . ?
C21 C22 1.359(12) . ?
C21 C26 1.366(12) . ?
C33 C34 1.404(11) . ?
C33 C38 1.395(11) . ?
C22 H22 0.9500 . ?
C22 C23 1.385(14) . ?
C41 C46 1.396(11) . ?
C23 H23 0.9500 . ?
C23 C24 1.371(16) . ?
C26 H26 0.9500 . ?
C26 C25 1.385(16) . ?
C25 H25 0.9500 . ?
C25 C24 1.361(17) . ?
C24 H24 0.9500 . ?
C14 B12 1.732(11) . ?
C14 B14 1.730(12) . ?
C14 B11 1.745(10) . ?
C14 B15 1.731(12) . ?
C14 B10 1.726(10) . ?
C27 C28 1.375(9) . ?
C34 H34 0.9500 . ?
C34 C35 1.393(14) . ?
C1 C2 1.389(13) . ?
C1 C6 1.389(14) . ?
C29 H29 0.9500 . ?
C29 C30 1.381(13) . ?
C29 C28 1.368(11) . ?
C30 H30 0.9500 . ?
C30 C31 1.369(11) . ?
C38 H38 0.9500 . ?
C38 C37 1.324(12) . ?
C47 C48 1.374(11) . ?
C47 C52 1.382(12) . ?
C2 H2 0.9500 . ?
C2 C3 1.397(16) . ?
C40 B3 1.622(10) . ?
C40 B4 1.745(12) . ?
C40 B8 1.745(11) . ?
C28 H28 0.9500 . ?
C8 H8 0.9500 . ?
C8 C7 1.390(12) . ?
C8 C9 1.379(13) . ?
C12 H12 0.9500 . ?
C12 C7 1.395(12) . ?
C12 C11 1.390(13) . ?
C37 H37 0.9500 . ?
C37 C36 1.368(14) . ?
C6 H6 0.9500 . ?
C6 C5 1.372(15) . ?
C31 H31 0.9500 . ?
C43 H43 0.9500 . ?
C43 C44 1.375(13) . ?
C46 H46 0.9500 . ?
C46 C45 1.387(12) . ?
C48 H48 0.9500 . ?
C48 C49 1.364(13) . ?
C3 H3 0.9500 . ?
C3 C4 1.362(17) . ?
C35 H35 0.9500 . ?
C35 C36 1.359(15) . ?
C5 H5 0.9500 . ?
C5 C4 1.407(16) . ?
C45 H45 0.9500 . ?
C45 C44 1.360(14) . ?
C9 H9 0.9500 . ?
C9 C10 1.374(15) . ?
C49 H49 0.9500 . ?
C49 C50 1.380(17) . ?
C51 H51 0.9500 . ?
C51 C50 1.382(17) . ?
C51 C52 1.382(16) . ?
C44 H44 0.9500 . ?
C4 H4 0.9500 . ?
C11 H11 0.9500 . ?
C11 C10 1.380(15) . ?
C10 H10 0.9500 . ?
C36 H36 0.9500 . ?
C50 H50 0.9500 . ?
C52 H52 0.9500 . ?
B13 H13 1.1200 . ?
B13 B12 1.768(14) . ?
B13 B14 1.791(13) . ?
B13 B16 1.752(12) . ?
B13 B18 1.761(14) . ?
B13 B17 1.760(12) . ?
B12 H12A 1.1200 . ?
B12 B14 1.782(13) . ?
B12 B11 1.771(12) . ?
B12 B18 1.748(13) . ?
B14 H14 1.1200 . ?
B14 B15 1.776(11) . ?
B14 B16 1.756(14) . ?
B11 H11A 1.1200 . ?
B11 B18 1.758(14) . ?
B11 B19 1.758(14) . ?
B11 B10 1.747(11) . ?
B15 H15 1.1200 . ?
B15 B16 1.769(13) . ?
B15 B10 1.799(12) . ?
B16 H16A 1.1200 . ?
B16 B17 1.783(13) . ?
B18 H18A 1.1200 . ?
B18 B19 1.772(12) . ?
B18 B17 1.756(14) . ?
B19 H19A 1.1200 . ?
B19 B17 1.768(14) . ?
B19 B10 1.739(13) . ?
B17 H17A 1.1200 . ?
B2 H2A 1.1200 . ?
B2 B1 1.788(11) . ?
B2 B3 1.840(11) . ?
B2 B6 1.744(14) . ?
B2 B5 1.763(13) . ?
B2 H2B 1.12(2) . ?
B1 H1 1.1200 . ?
B1 B6 1.688(12) . ?
B1 B9 1.731(12) . ?
B3 H3A 1.1200 . ?
B3 B4 1.793(13) . ?
B3 B5 1.743(13) . ?
B3 H2B 1.12(2) . ?
B6 H6A 1.1200 . ?
B6 B5 1.803(12) . ?
B6 B7 1.795(13) . ?
B6 B9 1.764(12) . ?
B10 H10A 1.1200 . ?
B4 H4A 1.1200 . ?
B4 B5 1.762(12) . ?
B4 B7 1.751(13) . ?
B4 B8 1.751(12) . ?
B5 H5A 1.1200 . ?
B5 B7 1.794(13) . ?
B7 H7 1.1200 . ?
B7 B8 1.752(11) . ?
B7 B9 1.762(12) . ?
B8 H8A 1.1200 . ?
B8 B9 1.748(11) . ?
B9 H9A 1.1200 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Au2 Au1 Au4 52.017(9) . 2_655 ?
Au2 Au1 Au3 60.060(10) . . ?
Au3 Au1 Au4 52.547(8) . 2_655 ?
P12 Au1 Au2 158.55(5) . . ?
P12 Au1 Au4 138.11(5) . 2_655 ?
P12 Au1 Au3 140.92(5) . . ?
Au1 Au2 Au3 62.675(11) . . ?
Au4 Au2 Au1 75.403(12) 2_655 . ?
Au4 Au2 Au3 60.362(10) 2_655 . ?
P55 Au2 Au1 95.41(4) . . ?
P55 Au2 Au4 155.14(5) . 2_655 ?
P55 Au2 Au3 135.82(5) . . ?
P55 Au2 P37 83.45(6) . . ?
P37 Au2 Au1 164.35(5) . . ?
P37 Au2 Au4 99.19(4) . 2_655 ?
P37 Au2 Au3 127.77(4) . . ?
Au2 Au4 Au1 52.580(10) 2_655 2_655 ?
Au2 Au4 Au3 61.660(11) 2_655 . ?
Au3 Au4 Au1 55.503(9) . 2_655 ?
P7 Au4 Au1 129.36(6) . 2_655 ?
P7 Au4 Au2 147.61(5) . 2_655 ?
P7 Au4 Au3 150.33(5) . . ?
Au1 Au3 Au1 125.765(18) . 2_655 ?
Au2 Au3 Au1 155.844(9) . 2_655 ?
Au2 Au3 Au1 57.262(9) 2_655 2_655 ?
Au2 Au3 Au1 57.264(9) . . ?
Au2 Au3 Au1 155.844(9) 2_655 . ?
Au2 Au3 Au2 131.883(19) . 2_655 ?
Au4 Au3 Au1 98.761(11) 2_655 2_655 ?
Au4 Au3 Au1 71.951(11) . 2_655 ?
Au4 Au3 Au1 71.951(11) 2_655 . ?
Au4 Au3 Au1 98.763(11) . . ?
Au4 Au3 Au2 57.977(9) . 2_655 ?
Au4 Au3 Au2 132.151(10) 2_655 2_655 ?
Au4 Au3 Au2 132.151(10) . . ?
Au4 Au3 Au2 57.981(9) 2_655 . ?
Au4 Au3 Au4 160.10(2) 2_655 . ?
C39 P55 Au2 104.2(2) . . ?
C33 P55 Au2 109.8(2) . . ?
C33 P55 C39 107.6(4) . . ?
C33 P55 C27 108.8(3) . . ?
C27 P55 Au2 120.5(2) . . ?
C27 P55 C39 105.0(3) . . ?
C15 P12 Au1 112.0(3) . . ?
C15 P12 C14 106.4(4) . . ?
C21 P12 Au1 114.4(3) . . ?
C21 P12 C15 110.2(4) . . ?
C21 P12 C14 103.8(4) . . ?
C14 P12 Au1 109.3(2) . . ?
C41 P37 Au2 123.3(3) . . ?
C41 P37 C40 108.7(3) . . ?
C47 P37 Au2 110.4(3) . . ?
C47 P37 C41 103.3(4) . . ?
C47 P37 C40 107.1(3) . . ?
C40 P37 Au2 103.3(2) . . ?
C13 P7 Au4 108.4(3) . . ?
C1 P7 Au4 114.7(3) . . ?
C1 P7 C13 104.3(4) . . ?
C7 P7 Au4 110.7(3) . . ?
C7 P7 C13 108.6(4) . . ?
C7 P7 C1 109.9(4) . . ?
C16 C15 P12 117.2(6) . . ?
C16 C15 C20 118.0(8) . . ?
C20 C15 P12 124.7(7) . . ?
B15 C13 P7 113.0(5) . . ?
B15 C13 B16 62.2(5) . . ?
B15 C13 B19 114.4(6) . . ?
B15 C13 B17 113.9(6) . . ?
B15 C13 B10 63.9(5) . . ?
B16 C13 P7 120.0(6) . . ?
B19 C13 P7 120.1(5) . . ?
B19 C13 B16 113.5(6) . . ?
B19 C13 B17 62.1(5) . . ?
B17 C13 P7 124.3(6) . . ?
B17 C13 B16 62.2(5) . . ?
B10 C13 P7 114.1(5) . . ?
B10 C13 B16 114.0(6) . . ?
B10 C13 B19 61.2(5) . . ?
B10 C13 B17 112.6(6) . . ?
C19 C18 H18 118.9 . . ?
C17 C18 H18 118.9 . . ?
C17 C18 C19 122.1(9) . . ?
C18 C19 H19 120.7 . . ?
C18 C19 C20 118.5(9) . . ?
C20 C19 H19 120.7 . . ?
C15 C16 H16 119.3 . . ?
C15 C16 C17 121.5(9) . . ?
C17 C16 H16 119.3 . . ?
C15 C20 H20 119.7 . . ?
C19 C20 C15 120.7(9) . . ?
C19 C20 H20 119.7 . . ?
C18 C17 C16 119.1(10) . . ?
C18 C17 H17 120.5 . . ?
C16 C17 H17 120.5 . . ?
C40 C39 P55 115.6(4) . . ?
C40 C39 B1 112.0(5) . . ?
C40 C39 B8 62.8(4) . . ?
C40 C39 B9 111.1(5) . . ?
B1 C39 P55 125.7(5) . . ?
B1 C39 B8 112.1(6) . . ?
B1 C39 B9 61.8(5) . . ?
B8 C39 P55 111.9(4) . . ?
B9 C39 P55 119.3(5) . . ?
B9 C39 B8 60.3(5) . . ?
C41 C42 H42 120.1 . . ?
C41 C42 C43 119.7(8) . . ?
C43 C42 H42 120.1 . . ?
C27 C32 H32 120.4 . . ?
C31 C32 H32 120.4 . . ?
C31 C32 C27 119.2(7) . . ?
C22 C21 P12 117.5(7) . . ?
C22 C21 C26 118.4(9) . . ?
C26 C21 P12 124.1(7) . . ?
C34 C33 P55 117.8(6) . . ?
C38 C33 P55 128.8(6) . . ?
C38 C33 C34 113.4(8) . . ?
C21 C22 H22 119.6 . . ?
C21 C22 C23 120.7(10) . . ?
C23 C22 H22 119.6 . . ?
C42 C41 P37 120.3(6) . . ?
C42 C41 C46 119.5(7) . . ?
C46 C41 P37 120.2(6) . . ?
C22 C23 H23 119.4 . . ?
C24 C23 C22 121.1(11) . . ?
C24 C23 H23 119.4 . . ?
C21 C26 H26 119.9 . . ?
C21 C26 C25 120.3(11) . . ?
C25 C26 H26 119.9 . . ?
C26 C25 H25 119.2 . . ?
C24 C25 C26 121.6(12) . . ?
C24 C25 H25 119.2 . . ?
C23 C24 H24 121.3 . . ?
C25 C24 C23 117.4(11) . . ?
C25 C24 H24 121.3 . . ?
B12 C14 P12 126.2(5) . . ?
B12 C14 B11 61.2(5) . . ?
B14 C14 P12 119.9(5) . . ?
B14 C14 B12 62.0(5) . . ?
B14 C14 B11 112.4(6) . . ?
B14 C14 B15 61.7(5) . . ?
B11 C14 P12 122.0(6) . . ?
B15 C14 P12 113.7(5) . . ?
B15 C14 B12 111.7(6) . . ?
B15 C14 B11 111.9(6) . . ?
B10 C14 P12 114.7(5) . . ?
B10 C14 B12 110.7(6) . . ?
B10 C14 B14 112.9(6) . . ?
B10 C14 B11 60.4(5) . . ?
B10 C14 B15 62.7(5) . . ?
C32 C27 P55 117.6(5) . . ?
C28 C27 P55 122.9(6) . . ?
C28 C27 C32 119.5(7) . . ?
C33 C34 H34 119.7 . . ?
C35 C34 C33 120.7(9) . . ?
C35 C34 H34 119.7 . . ?
C2 C1 P7 122.3(8) . . ?
C6 C1 P7 118.0(7) . . ?
C6 C1 C2 119.7(10) . . ?
C30 C29 H29 119.8 . . ?
C28 C29 H29 119.8 . . ?
C28 C29 C30 120.5(8) . . ?
C29 C30 H30 120.5 . . ?
C31 C30 C29 119.0(8) . . ?
C31 C30 H30 120.5 . . ?
C33 C38 H38 116.7 . . ?
C37 C38 C33 126.6(8) . . ?
C37 C38 H38 116.7 . . ?
C48 C47 P37 126.7(7) . . ?
C48 C47 C52 117.0(9) . . ?
C52 C47 P37 116.4(7) . . ?
C1 C2 H2 120.6 . . ?
C1 C2 C3 118.7(11) . . ?
C3 C2 H2 120.6 . . ?
C39 C40 P37 115.5(4) . . ?
C39 C40 B3 112.8(5) . . ?
C39 C40 B4 111.3(6) . . ?
C39 C40 B8 62.9(5) . . ?
B3 C40 P37 123.4(5) . . ?
B3 C40 B4 64.2(5) . . ?
B3 C40 B8 114.6(6) . . ?
B4 C40 P37 119.4(5) . . ?
B8 C40 P37 112.5(5) . . ?
B8 C40 B4 60.2(5) . . ?
C27 C28 H28 119.7 . . ?
C29 C28 C27 120.6(8) . . ?
C29 C28 H28 119.7 . . ?
C7 C8 H8 119.9 . . ?
C9 C8 H8 119.9 . . ?
C9 C8 C7 120.3(9) . . ?
C7 C12 H12 120.0 . . ?
C11 C12 H12 120.0 . . ?
C11 C12 C7 120.1(9) . . ?
C38 C37 H37 120.7 . . ?
C38 C37 C36 118.6(9) . . ?
C36 C37 H37 120.7 . . ?
C1 C6 H6 119.3 . . ?
C5 C6 C1 121.5(10) . . ?
C5 C6 H6 119.3 . . ?
C32 C31 H31 119.5 . . ?
C30 C31 C32 121.0(8) . . ?
C30 C31 H31 119.5 . . ?
C42 C43 H43 119.7 . . ?
C44 C43 C42 120.6(9) . . ?
C44 C43 H43 119.7 . . ?
C41 C46 H46 120.0 . . ?
C45 C46 C41 120.0(9) . . ?
C45 C46 H46 120.0 . . ?
C47 C48 H48 118.8 . . ?
C49 C48 C47 122.3(9) . . ?
C49 C48 H48 118.8 . . ?
C2 C3 H3 119.4 . . ?
C4 C3 C2 121.2(11) . . ?
C4 C3 H3 119.4 . . ?
C34 C35 H35 119.5 . . ?
C36 C35 C34 121.1(10) . . ?
C36 C35 H35 119.5 . . ?
C6 C5 H5 120.7 . . ?
C6 C5 C4 118.5(12) . . ?
C4 C5 H5 120.7 . . ?
C8 C7 P7 125.3(7) . . ?
C8 C7 C12 118.5(8) . . ?
C12 C7 P7 116.2(7) . . ?
C46 C45 H45 120.0 . . ?
C44 C45 C46 120.0(9) . . ?
C44 C45 H45 120.0 . . ?
C8 C9 H9 119.2 . . ?
C10 C9 C8 121.7(10) . . ?
C10 C9 H9 119.2 . . ?
C48 C49 H49 119.7 . . ?
C48 C49 C50 120.7(10) . . ?
C50 C49 H49 119.7 . . ?
C50 C51 H51 119.8 . . ?
C50 C51 C52 120.5(12) . . ?
C52 C51 H51 119.8 . . ?
C43 C44 H44 119.9 . . ?
C45 C44 C43 120.2(8) . . ?
C45 C44 H44 119.9 . . ?
C3 C4 C5 120.2(13) . . ?
C3 C4 H4 119.9 . . ?
C5 C4 H4 119.9 . . ?
C12 C11 H11 119.5 . . ?
C10 C11 C12 121.0(10) . . ?
C10 C11 H11 119.5 . . ?
C9 C10 C11 118.4(10) . . ?
C9 C10 H10 120.8 . . ?
C11 C10 H10 120.8 . . ?
C37 C36 H36 120.3 . . ?
C35 C36 C37 119.5(10) . . ?
C35 C36 H36 120.3 . . ?
C49 C50 C51 118.1(12) . . ?
C49 C50 H50 121.0 . . ?
C51 C50 H50 121.0 . . ?
C47 C52 C51 121.4(10) . . ?
C47 C52 H52 119.3 . . ?
C51 C52 H52 119.3 . . ?
B12 B13 H13 122.3 . . ?
B12 B13 B14 60.1(5) . . ?
B14 B13 H13 121.9 . . ?
B16 B13 H13 121.4 . . ?
B16 B13 B12 107.7(7) . . ?
B16 B13 B14 59.4(5) . . ?
B16 B13 B18 108.6(6) . . ?
B16 B13 B17 61.0(5) . . ?
B18 B13 H13 121.8 . . ?
B18 B13 B12 59.4(6) . . ?
B18 B13 B14 107.8(7) . . ?
B17 B13 H13 121.6 . . ?
B17 B13 B12 107.3(7) . . ?
B17 B13 B14 108.1(6) . . ?
B17 B13 B18 59.8(6) . . ?
C14 B12 B13 106.2(6) . . ?
C14 B12 H12A 123.5 . . ?
C14 B12 B14 59.0(5) . . ?
C14 B12 B11 59.8(4) . . ?
C14 B12 B18 106.3(6) . . ?
B13 B12 H12A 121.9 . . ?
B13 B12 B14 60.6(5) . . ?
B13 B12 B11 108.4(7) . . ?
B14 B12 H12A 121.1 . . ?
B11 B12 H12A 121.2 . . ?
B11 B12 B14 108.7(6) . . ?
B18 B12 B13 60.1(6) . . ?
B18 B12 H12A 121.9 . . ?
B18 B12 B14 108.7(7) . . ?
B18 B12 B11 59.9(5) . . ?
C14 B14 B13 105.2(6) . . ?
C14 B14 B12 59.1(5) . . ?
C14 B14 H14 123.6 . . ?
C14 B14 B15 59.1(5) . . ?
C14 B14 B16 105.9(6) . . ?
B13 B14 H14 123.0 . . ?
B12 B14 B13 59.3(5) . . ?
B12 B14 H14 122.2 . . ?
B15 B14 B13 107.0(6) . . ?
B15 B14 B12 107.3(6) . . ?
B15 B14 H14 121.8 . . ?
B16 B14 B13 59.2(5) . . ?
B16 B14 B12 106.8(7) . . ?
B16 B14 H14 122.5 . . ?
B16 B14 B15 60.1(5) . . ?
C14 B11 B12 59.0(5) . . ?
C14 B11 H11A 124.0 . . ?
C14 B11 B18 105.3(6) . . ?
C14 B11 B19 105.4(6) . . ?
C14 B11 B10 59.3(4) . . ?
B12 B11 H11A 121.8 . . ?
B18 B11 B12 59.4(5) . . ?
B18 B11 H11A 122.3 . . ?
B18 B11 B19 60.5(5) . . ?
B19 B11 B12 107.8(7) . . ?
B19 B11 H11A 122.2 . . ?
B10 B11 B12 107.9(6) . . ?
B10 B11 H11A 121.6 . . ?
B10 B11 B18 107.9(7) . . ?
B10 B11 B19 59.5(5) . . ?
C13 B15 C14 102.8(6) . . ?
C13 B15 B14 105.8(6) . . ?
C13 B15 H15 124.2 . . ?
C13 B15 B16 60.1(5) . . ?
C13 B15 B10 58.5(5) . . ?
C14 B15 B14 59.1(5) . . ?
C14 B15 H15 124.7 . . ?
C14 B15 B16 105.3(6) . . ?
C14 B15 B10 58.5(4) . . ?
B14 B15 H15 122.2 . . ?
B14 B15 B10 107.4(6) . . ?
B16 B15 B14 59.4(5) . . ?
B16 B15 H15 121.8 . . ?
B16 B15 B10 108.0(6) . . ?
B10 B15 H15 121.9 . . ?
C13 B16 B13 104.8(7) . . ?
C13 B16 B14 104.9(7) . . ?
C13 B16 B15 57.8(5) . . ?
C13 B16 H16A 125.3 . . ?
C13 B16 B17 58.4(5) . . ?
B13 B16 B14 61.4(5) . . ?
B13 B16 B15 109.1(7) . . ?
B13 B16 H16A 121.6 . . ?
B13 B16 B17 59.7(5) . . ?
B14 B16 B15 60.5(5) . . ?
B14 B16 H16A 121.4 . . ?
B14 B16 B17 108.6(7) . . ?
B15 B16 H16A 121.7 . . ?
B15 B16 B17 107.1(7) . . ?
B17 B16 H16A 121.9 . . ?
B13 B18 H18A 121.1 . . ?
B13 B18 B19 108.4(6) . . ?
B12 B18 B13 60.5(5) . . ?
B12 B18 B11 60.7(5) . . ?
B12 B18 H18A 121.3 . . ?
B12 B18 B19 108.2(6) . . ?
B12 B18 B17 108.4(7) . . ?
B11 B18 B13 109.2(6) . . ?
B11 B18 H18A 121.2 . . ?
B11 B18 B19 59.8(5) . . ?
B19 B18 H18A 121.8 . . ?
B17 B18 B13 60.1(5) . . ?
B17 B18 B11 108.4(6) . . ?
B17 B18 H18A 121.6 . . ?
B17 B18 B19 60.2(5) . . ?
C13 B19 B11 105.3(6) . . ?
C13 B19 B18 104.6(6) . . ?
C13 B19 H19A 124.2 . . ?
C13 B19 B17 59.1(5) . . ?
C13 B19 B10 59.3(5) . . ?
B11 B19 B18 59.7(5) . . ?
B11 B19 H19A 122.4 . . ?
B11 B19 B17 107.8(6) . . ?
B18 B19 H19A 122.9 . . ?
B17 B19 B18 59.5(5) . . ?
B17 B19 H19A 121.4 . . ?
B10 B19 B11 59.9(5) . . ?
B10 B19 B18 107.6(6) . . ?
B10 B19 H19A 121.2 . . ?
B10 B19 B17 108.6(6) . . ?
C13 B17 B13 105.2(6) . . ?
C13 B17 B16 59.4(5) . . ?
C13 B17 B18 105.0(7) . . ?
C13 B17 B19 58.7(5) . . ?
C13 B17 H17A 124.3 . . ?
B13 B17 B16 59.3(5) . . ?
B13 B17 B19 108.6(7) . . ?
B13 B17 H17A 122.3 . . ?
B16 B17 H17A 121.7 . . ?
B18 B17 B13 60.1(6) . . ?
B18 B17 B16 107.4(7) . . ?
B18 B17 B19 60.4(5) . . ?
B18 B17 H17A 122.4 . . ?
B19 B17 B16 108.4(7) . . ?
B19 B17 H17A 121.0 . . ?
B1 B2 H2A 116.8 . . ?
B1 B2 B3 102.7(5) . . ?
B1 B2 H2B 90(8) . . ?
B3 B2 H2A 116.0 . . ?
B3 B2 H2B 34.8(15) . . ?
B6 B2 H2A 137.4 . . ?
B6 B2 B1 57.1(5) . . ?
B6 B2 B3 105.9(6) . . ?
B6 B2 B5 61.9(5) . . ?
B6 B2 H2B 125(8) . . ?
B5 B2 H2A 137.7 . . ?
B5 B2 B1 104.8(6) . . ?
B5 B2 B3 57.8(5) . . ?
B5 B2 H2B 92(2) . . ?
C39 B1 B2 106.9(5) . . ?
C39 B1 H1 112.7 . . ?
C39 B1 B6 108.9(6) . . ?
C39 B1 B9 61.9(5) . . ?
B2 B1 H1 112.4 . . ?
B6 B1 B2 60.2(5) . . ?
B6 B1 H1 137.7 . . ?
B6 B1 B9 62.1(5) . . ?
B9 B1 B2 111.3(6) . . ?
B9 B1 H1 135.3 . . ?
C40 B3 B2 105.6(5) . . ?
C40 B3 H3A 113.9 . . ?
C40 B3 B4 61.2(5) . . ?
C40 B3 B5 106.2(6) . . ?
C40 B3 H2B 92(8) . . ?
B2 B3 H3A 114.1 . . ?
B2 B3 H2B 34.6(14) . . ?
H3A B3 H2B 92.6 . . ?
B4 B3 B2 107.9(6) . . ?
B4 B3 H3A 136.8 . . ?
B4 B3 H2B 129(8) . . ?
B5 B3 B2 58.9(5) . . ?
B5 B3 H3A 139.2 . . ?
B5 B3 B4 59.8(5) . . ?
B5 B3 H2B 93(2) . . ?
B2 B6 H6A 118.9 . . ?
B2 B6 B5 59.6(5) . . ?
B2 B6 B7 109.8(6) . . ?
B2 B6 B9 111.7(7) . . ?
B1 B6 B2 62.8(5) . . ?
B1 B6 H6A 121.5 . . ?
B1 B6 B5 107.3(7) . . ?
B1 B6 B7 107.4(6) . . ?
B1 B6 B9 60.1(5) . . ?
B5 B6 H6A 123.1 . . ?
B7 B6 H6A 121.9 . . ?
B7 B6 B5 59.8(5) . . ?
B9 B6 H6A 121.2 . . ?
B9 B6 B5 107.1(6) . . ?
B9 B6 B7 59.3(5) . . ?
C13 B10 C14 102.3(6) . . ?
C13 B10 B11 105.9(6) . . ?
C13 B10 B15 57.6(5) . . ?
C13 B10 B19 59.5(5) . . ?
C13 B10 H10A 125.2 . . ?
C14 B10 B11 60.3(4) . . ?
C14 B10 B15 58.8(4) . . ?
C14 B10 B19 107.1(6) . . ?
C14 B10 H10A 123.9 . . ?
B11 B10 B15 108.6(6) . . ?
B11 B10 H10A 121.1 . . ?
B15 B10 H10A 122.0 . . ?
B19 B10 B11 60.6(5) . . ?
B19 B10 B15 107.9(7) . . ?
B19 B10 H10A 121.2 . . ?
C40 B4 B3 54.5(4) . . ?
C40 B4 H4A 127.2 . . ?
C40 B4 B5 100.2(6) . . ?
C40 B4 B7 104.2(6) . . ?
C40 B4 B8 59.9(5) . . ?
B3 B4 H4A 123.5 . . ?
B5 B4 B3 58.7(5) . . ?
B5 B4 H4A 123.4 . . ?
B7 B4 B3 107.8(6) . . ?
B7 B4 H4A 121.4 . . ?
B7 B4 B5 61.4(5) . . ?
B8 B4 B3 106.2(6) . . ?
B8 B4 H4A 121.0 . . ?
B8 B4 B5 108.0(6) . . ?
B8 B4 B7 60.0(5) . . ?
B2 B5 B6 58.5(5) . . ?
B2 B5 H5A 119.1 . . ?
B2 B5 B7 109.0(6) . . ?
B3 B5 B2 63.3(5) . . ?
B3 B5 B6 107.6(6) . . ?
B3 B5 B4 61.5(5) . . ?
B3 B5 H5A 120.6 . . ?
B3 B5 B7 108.1(6) . . ?
B6 B5 H5A 123.4 . . ?
B4 B5 B2 112.9(6) . . ?
B4 B5 B6 107.4(6) . . ?
B4 B5 H5A 120.3 . . ?
B4 B5 B7 59.0(5) . . ?
B7 B5 B6 59.9(5) . . ?
B7 B5 H5A 122.3 . . ?
B6 B7 H7 122.0 . . ?
B4 B7 B6 108.3(7) . . ?
B4 B7 B5 59.6(5) . . ?
B4 B7 H7 121.3 . . ?
B4 B7 B8 60.0(5) . . ?
B4 B7 B9 108.5(6) . . ?
B5 B7 B6 60.3(5) . . ?
B5 B7 H7 122.3 . . ?
B8 B7 B6 106.7(6) . . ?
B8 B7 B5 106.5(6) . . ?
B8 B7 H7 122.8 . . ?
B8 B7 B9 59.7(5) . . ?
B9 B7 B6 59.5(5) . . ?
B9 B7 B5 107.6(7) . . ?
B9 B7 H7 121.7 . . ?
C39 B8 B4 104.1(6) . . ?
C39 B8 B7 104.4(6) . . ?
C39 B8 H8A 125.6 . . ?
C39 B8 B9 59.4(4) . . ?
C40 B8 C39 54.3(4) . . ?
C40 B8 B4 59.9(5) . . ?
C40 B8 B7 104.1(6) . . ?
C40 B8 H8A 125.7 . . ?
C40 B8 B9 103.4(6) . . ?
B4 B8 B7 60.0(5) . . ?
B4 B8 H8A 121.3 . . ?
B7 B8 H8A 123.0 . . ?
B9 B8 B4 109.1(6) . . ?
B9 B8 B7 60.4(5) . . ?
B9 B8 H8A 121.6 . . ?
C39 B9 B6 101.3(6) . . ?
C39 B9 B7 104.6(6) . . ?
C39 B9 B8 60.3(4) . . ?
C39 B9 H9A 126.0 . . ?
B1 B9 C39 56.3(4) . . ?
B1 B9 B6 57.7(5) . . ?
B1 B9 B7 107.1(6) . . ?
B1 B9 B8 107.5(6) . . ?
B1 B9 H9A 123.3 . . ?
B6 B9 H9A 123.6 . . ?
B7 B9 B6 61.2(5) . . ?
B7 B9 H9A 121.8 . . ?
B8 B9 B6 108.3(6) . . ?
B8 B9 B7 59.9(5) . . ?
B8 B9 H9A 120.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Au1 P12 C15 C16 -0.7(9) . . . . ?
Au1 P12 C15 C20 -177.7(7) . . . . ?
Au1 P12 C21 C22 23.8(10) . . . . ?
Au1 P12 C21 C26 -156.4(10) . . . . ?
Au1 P12 C14 B12 166.8(5) . . . . ?
Au1 P12 C14 B14 91.3(5) . . . . ?
Au1 P12 C14 B11 -117.4(5) . . . . ?
Au1 P12 C14 B15 21.5(5) . . . . ?
Au1 P12 C14 B10 -48.1(5) . . . . ?
Au2 P55 C39 C40 28.5(6) . . . . ?
Au2 P55 C39 B1 177.3(6) . . . . ?
Au2 P55 C39 B8 -40.8(5) . . . . ?
Au2 P55 C39 B9 -108.1(5) . . . . ?
Au2 P55 C33 C34 23.2(8) . . . . ?
Au2 P55 C33 C38 -154.1(7) . . . . ?
Au2 P55 C27 C32 22.9(6) . . . . ?
Au2 P55 C27 C28 -159.3(5) . . . . ?
Au2 P37 C41 C42 -14.5(8) . . . . ?
Au2 P37 C41 C46 164.3(6) . . . . ?
Au2 P37 C47 C48 114.2(8) . . . . ?
Au2 P37 C47 C52 -66.3(9) . . . . ?
Au2 P37 C40 C39 -29.0(5) . . . . ?
Au2 P37 C40 B3 -175.0(5) . . . . ?
Au2 P37 C40 B4 108.1(5) . . . . ?
Au2 P37 C40 B8 40.7(5) . . . . ?
Au4 P7 C13 B15 -34.4(6) . . . . ?
Au4 P7 C13 B16 -104.4(5) . . . . ?
Au4 P7 C13 B19 105.6(6) . . . . ?
Au4 P7 C13 B17 -179.4(6) . . . . ?
Au4 P7 C13 B10 36.1(5) . . . . ?
Au4 P7 C1 C2 -160.1(7) . . . . ?
Au4 P7 C1 C6 19.9(8) . . . . ?
Au4 P7 C7 C8 -173.9(8) . . . . ?
Au4 P7 C7 C12 9.3(9) . . . . ?
P55 C39 C40 P37 0.8(7) . . . . ?
P55 C39 C40 B3 150.4(5) . . . . ?
P55 C39 C40 B4 -139.6(5) . . . . ?
P55 C39 C40 B8 -102.6(5) . . . . ?
P55 C39 B1 B2 -147.2(6) . . . . ?
P55 C39 B1 B6 149.3(6) . . . . ?
P55 C39 B1 B9 107.3(6) . . . . ?
P55 C39 B8 C40 108.5(5) . . . . ?
P55 C39 B8 B4 143.7(5) . . . . ?
P55 C39 B8 B7 -154.2(5) . . . . ?
P55 C39 B8 B9 -112.2(5) . . . . ?
P55 C39 B9 B1 -117.3(5) . . . . ?
P55 C39 B9 B6 -155.4(5) . . . . ?
P55 C39 B9 B7 141.7(5) . . . . ?
P55 C39 B9 B8 99.9(5) . . . . ?
P55 C33 C34 C35 177.3(11) . . . . ?
P55 C33 C38 C37 -179.1(8) . . . . ?
P55 C27 C28 C29 -175.4(6) . . . . ?
P12 C15 C16 C17 179.7(9) . . . . ?
P12 C15 C20 C19 -179.4(8) . . . . ?
P12 C21 C22 C23 173.1(10) . . . . ?
P12 C21 C26 C25 -172.0(13) . . . . ?
P12 C14 B12 B13 -147.6(6) . . . . ?
P12 C14 B12 B14 -108.1(7) . . . . ?
P12 C14 B12 B11 110.3(7) . . . . ?
P12 C14 B12 B18 149.5(6) . . . . ?
P12 C14 B14 B13 156.5(5) . . . . ?
P12 C14 B14 B12 117.8(6) . . . . ?
P12 C14 B14 B15 -102.6(6) . . . . ?
P12 C14 B14 B16 -141.8(5) . . . . ?
P12 C14 B11 B12 -116.9(6) . . . . ?
P12 C14 B11 B18 -155.7(5) . . . . ?
P12 C14 B11 B19 141.3(5) . . . . ?
P12 C14 B11 B10 102.3(6) . . . . ?
P12 C14 B15 C13 -146.6(5) . . . . ?
P12 C14 B15 B14 112.5(6) . . . . ?
P12 C14 B15 B16 151.3(5) . . . . ?
P12 C14 B15 B10 -106.7(5) . . . . ?
P12 C14 B10 C13 144.5(5) . . . . ?
P12 C14 B10 B11 -114.1(6) . . . . ?
P12 C14 B10 B15 105.1(5) . . . . ?
P12 C14 B10 B19 -154.0(5) . . . . ?
P37 C41 C46 C45 -179.7(8) . . . . ?
P37 C47 C48 C49 -179.1(9) . . . . ?
P37 C47 C52 C51 177.8(13) . . . . ?
P37 C40 B3 B2 148.2(6) . . . . ?
P37 C40 B3 B4 -109.6(6) . . . . ?
P37 C40 B3 B5 -150.3(5) . . . . ?
P37 C40 B4 B3 115.4(6) . . . . ?
P37 C40 B4 B5 154.5(5) . . . . ?
P37 C40 B4 B7 -142.6(5) . . . . ?
P37 C40 B4 B8 -100.5(6) . . . . ?
P37 C40 B8 C39 -108.2(5) . . . . ?
P37 C40 B8 B4 112.1(5) . . . . ?
P37 C40 B8 B7 154.1(5) . . . . ?
P37 C40 B8 B9 -143.4(5) . . . . ?
P7 C13 B15 C14 146.5(5) . . . . ?
P7 C13 B15 B14 -152.3(5) . . . . ?
P7 C13 B15 B16 -113.0(6) . . . . ?
P7 C13 B15 B10 106.6(6) . . . . ?
P7 C13 B16 B13 -154.7(6) . . . . ?
P7 C13 B16 B14 141.5(6) . . . . ?
P7 C13 B16 B15 101.8(6) . . . . ?
P7 C13 B16 B17 -115.5(7) . . . . ?
P7 C13 B19 B11 -142.7(6) . . . . ?
P7 C13 B19 B18 155.3(6) . . . . ?
P7 C13 B19 B17 115.4(7) . . . . ?
P7 C13 B19 B10 -102.7(6) . . . . ?
P7 C13 B17 B13 148.1(6) . . . . ?
P7 C13 B17 B16 108.9(7) . . . . ?
P7 C13 B17 B18 -149.4(6) . . . . ?
P7 C13 B17 B19 -109.1(7) . . . . ?
P7 C13 B10 C14 -144.8(5) . . . . ?
P7 C13 B10 B11 152.9(5) . . . . ?
P7 C13 B10 B15 -104.9(5) . . . . ?
P7 C13 B10 B19 112.4(6) . . . . ?
P7 C1 C2 C3 -177.5(8) . . . . ?
P7 C1 C6 C5 175.2(9) . . . . ?
C15 P12 C21 C22 151.1(9) . . . . ?
C15 P12 C21 C26 -29.0(12) . . . . ?
C15 P12 C14 B12 45.7(7) . . . . ?
C15 P12 C14 B14 -29.8(6) . . . . ?
C15 P12 C14 B11 121.4(6) . . . . ?
C15 P12 C14 B15 -99.7(5) . . . . ?
C15 P12 C14 B10 -169.2(5) . . . . ?
C15 C16 C17 C18 0(2) . . . . ?
C13 P7 C1 C2 81.5(8) . . . . ?
C13 P7 C1 C6 -98.4(7) . . . . ?
C13 P7 C7 C8 -55.0(10) . . . . ?
C13 P7 C7 C12 128.1(9) . . . . ?
C13 B15 B16 B13 -95.8(7) . . . . ?
C13 B15 B16 B14 -134.8(7) . . . . ?
C13 B15 B16 B17 -32.7(6) . . . . ?
C13 B15 B10 C14 132.8(6) . . . . ?
C13 B15 B10 B11 97.4(7) . . . . ?
C13 B15 B10 B19 33.3(5) . . . . ?
C13 B16 B17 B13 -134.9(7) . . . . ?
C13 B16 B17 B18 -97.5(7) . . . . ?
C13 B16 B17 B19 -33.7(6) . . . . ?
C13 B19 B17 B13 96.8(7) . . . . ?
C13 B19 B17 B16 33.9(6) . . . . ?
C13 B19 B17 B18 134.0(7) . . . . ?
C13 B19 B10 C14 -94.4(6) . . . . ?
C13 B19 B10 B11 -134.2(6) . . . . ?
C13 B19 B10 B15 -32.5(5) . . . . ?
C18 C19 C20 C15 -0.9(17) . . . . ?
C19 C18 C17 C16 3(2) . . . . ?
C16 C15 C20 C19 3.6(16) . . . . ?
C20 C15 C16 C17 -3.2(17) . . . . ?
C17 C18 C19 C20 -2.5(19) . . . . ?
C39 P55 C33 C34 136.1(7) . . . . ?
C39 P55 C33 C38 -41.3(8) . . . . ?
C39 P55 C27 C32 -94.0(6) . . . . ?
C39 P55 C27 C28 83.7(7) . . . . ?
C39 C40 B3 B2 1.4(8) . . . . ?
C39 C40 B3 B4 103.6(6) . . . . ?
C39 C40 B3 B5 62.9(8) . . . . ?
C39 C40 B4 B3 -105.9(6) . . . . ?
C39 C40 B4 B5 -66.8(7) . . . . ?
C39 C40 B4 B7 -3.9(8) . . . . ?
C39 C40 B4 B8 38.1(5) . . . . ?
C39 C40 B8 B4 -139.8(6) . . . . ?
C39 C40 B8 B7 -97.7(6) . . . . ?
C39 C40 B8 B9 -35.3(5) . . . . ?
C39 B1 B6 B2 99.0(6) . . . . ?
C39 B1 B6 B5 58.3(8) . . . . ?
C39 B1 B6 B7 -4.7(9) . . . . ?
C39 B1 B6 B9 -41.9(6) . . . . ?
C39 B1 B9 B6 134.3(6) . . . . ?
C39 B1 B9 B7 96.4(6) . . . . ?
C39 B1 B9 B8 33.4(5) . . . . ?
C39 B8 B9 B1 -31.8(5) . . . . ?
C39 B8 B9 B6 -92.8(7) . . . . ?
C39 B8 B9 B7 -131.8(6) . . . . ?
C42 C41 C46 C45 -0.8(14) . . . . ?
C42 C43 C44 C45 -2.1(16) . . . . ?
C32 C27 C28 C29 2.3(11) . . . . ?
C21 P12 C15 C16 -129.4(8) . . . . ?
C21 P12 C15 C20 53.7(9) . . . . ?
C21 P12 C14 B12 -70.7(6) . . . . ?
C21 P12 C14 B14 -146.1(5) . . . . ?
C21 P12 C14 B11 5.1(6) . . . . ?
C21 P12 C14 B15 144.0(5) . . . . ?
C21 P12 C14 B10 74.4(6) . . . . ?
C21 C22 C23 C24 4(2) . . . . ?
C21 C26 C25 C24 -6(3) . . . . ?
C33 P55 C39 C40 -88.1(6) . . . . ?
C33 P55 C39 B1 60.7(7) . . . . ?
C33 P55 C39 B8 -157.4(5) . . . . ?
C33 P55 C39 B9 135.3(5) . . . . ?
C33 P55 C27 C32 151.0(6) . . . . ?
C33 P55 C27 C28 -31.2(7) . . . . ?
C33 C34 C35 C36 4(2) . . . . ?
C33 C38 C37 C36 -0.5(17) . . . . ?
C22 C21 C26 C25 8(2) . . . . ?
C22 C23 C24 C25 -2(2) . . . . ?
C41 P37 C47 C48 -112.2(8) . . . . ?
C41 P37 C47 C52 67.3(9) . . . . ?
C41 P37 C40 C39 -161.4(5) . . . . ?
C41 P37 C40 B3 52.6(7) . . . . ?
C41 P37 C40 B4 -24.4(6) . . . . ?
C41 P37 C40 B8 -91.8(5) . . . . ?
C41 C42 C43 C44 1.5(13) . . . . ?
C41 C46 C45 C44 0.2(16) . . . . ?
C26 C21 C22 C23 -6.7(19) . . . . ?
C26 C25 C24 C23 3(3) . . . . ?
C14 P12 C15 C16 118.7(8) . . . . ?
C14 P12 C15 C20 -58.3(9) . . . . ?
C14 P12 C21 C22 -95.3(9) . . . . ?
C14 P12 C21 C26 84.5(11) . . . . ?
C14 B12 B14 B13 -135.4(6) . . . . ?
C14 B12 B14 B15 -35.6(6) . . . . ?
C14 B12 B14 B16 -98.8(6) . . . . ?
C14 B12 B11 B18 135.4(7) . . . . ?
C14 B12 B11 B19 97.6(6) . . . . ?
C14 B12 B11 B10 34.8(6) . . . . ?
C14 B12 B18 B13 99.6(7) . . . . ?
C14 B12 B18 B11 -39.2(6) . . . . ?
C14 B12 B18 B19 -1.7(9) . . . . ?
C14 B12 B18 B17 62.0(8) . . . . ?
C14 B14 B15 C13 -95.7(6) . . . . ?
C14 B14 B15 B16 -135.4(6) . . . . ?
C14 B14 B15 B10 -34.4(6) . . . . ?
C14 B14 B16 C13 0.5(7) . . . . ?
C14 B14 B16 B13 -98.5(7) . . . . ?
C14 B14 B16 B15 38.8(5) . . . . ?
C14 B14 B16 B17 -60.7(7) . . . . ?
C14 B11 B18 B13 1.2(8) . . . . ?
C14 B11 B18 B12 38.6(6) . . . . ?
C14 B11 B18 B19 -99.4(6) . . . . ?
C14 B11 B18 B17 -62.6(8) . . . . ?
C14 B11 B19 C13 0.8(8) . . . . ?
C14 B11 B19 B18 99.1(7) . . . . ?
C14 B11 B19 B17 62.7(7) . . . . ?
C14 B11 B19 B10 -38.9(5) . . . . ?
C14 B11 B10 C13 95.3(6) . . . . ?
C14 B11 B10 B15 34.7(6) . . . . ?
C14 B11 B10 B19 135.2(7) . . . . ?
C14 B15 B16 C13 96.1(6) . . . . ?
C14 B15 B16 B13 0.3(8) . . . . ?
C14 B15 B16 B14 -38.7(5) . . . . ?
C14 B15 B16 B17 63.4(7) . . . . ?
C14 B15 B10 C13 -132.8(6) . . . . ?
C14 B15 B10 B11 -35.4(6) . . . . ?
C14 B15 B10 B19 -99.5(6) . . . . ?
C27 P55 C39 C40 156.1(5) . . . . ?
C27 P55 C39 B1 -55.1(7) . . . . ?
C27 P55 C39 B8 86.8(5) . . . . ?
C27 P55 C39 B9 19.6(6) . . . . ?
C27 P55 C33 C34 -110.7(8) . . . . ?
C27 P55 C33 C38 71.9(8) . . . . ?
C27 C32 C31 C30 2.9(12) . . . . ?
C34 C33 C38 C37 3.5(14) . . . . ?
C34 C35 C36 C37 -1(2) . . . . ?
C1 P7 C13 B15 88.2(6) . . . . ?
C1 P7 C13 B16 18.2(7) . . . . ?
C1 P7 C13 B19 -131.9(6) . . . . ?
C1 P7 C13 B17 -56.8(7) . . . . ?
C1 P7 C13 B10 158.7(5) . . . . ?
C1 P7 C7 C8 58.5(10) . . . . ?
C1 P7 C7 C12 -118.4(9) . . . . ?
C1 C2 C3 C4 -0.1(18) . . . . ?
C1 C6 C5 C4 4.5(17) . . . . ?
C29 C30 C31 C32 -0.2(12) . . . . ?
C30 C29 C28 C27 0.5(13) . . . . ?
C38 C33 C34 C35 -5.0(16) . . . . ?
C38 C37 C36 C35 -1(2) . . . . ?
C47 P37 C41 C42 -140.3(6) . . . . ?
C47 P37 C41 C46 38.6(8) . . . . ?
C47 P37 C40 C39 87.6(6) . . . . ?
C47 P37 C40 B3 -58.4(7) . . . . ?
C47 P37 C40 B4 -135.4(6) . . . . ?
C47 P37 C40 B8 157.2(5) . . . . ?
C47 C48 C49 C50 0(2) . . . . ?
C2 C1 C6 C5 -4.7(15) . . . . ?
C2 C3 C4 C5 0(2) . . . . ?
C40 P37 C41 C42 106.3(7) . . . . ?
C40 P37 C41 C46 -74.9(8) . . . . ?
C40 P37 C47 C48 2.4(9) . . . . ?
C40 P37 C47 C52 -178.1(8) . . . . ?
C40 C39 B1 B2 2.6(8) . . . . ?
C40 C39 B1 B6 -60.9(8) . . . . ?
C40 C39 B1 B9 -102.9(6) . . . . ?
C40 C39 B8 B4 35.2(5) . . . . ?
C40 C39 B8 B7 97.3(6) . . . . ?
C40 C39 B8 B9 139.3(6) . . . . ?
C40 C39 B9 B1 104.4(6) . . . . ?
C40 C39 B9 B6 66.3(7) . . . . ?
C40 C39 B9 B7 3.4(7) . . . . ?
C40 C39 B9 B8 -38.4(5) . . . . ?
C40 B3 B4 B5 -133.5(6) . . . . ?
C40 B3 B4 B7 -95.0(6) . . . . ?
C40 B3 B4 B8 -32.0(5) . . . . ?
C40 B3 B5 B2 -98.7(6) . . . . ?
C40 B3 B5 B6 -59.2(7) . . . . ?
C40 B3 B5 B4 41.5(5) . . . . ?
C40 B3 B5 B7 4.0(8) . . . . ?
C40 B4 B5 B2 1.5(8) . . . . ?
C40 B4 B5 B3 -36.9(5) . . . . ?
C40 B4 B5 B6 64.0(8) . . . . ?
C40 B4 B5 B7 100.7(6) . . . . ?
C40 B4 B7 B6 -57.1(7) . . . . ?
C40 B4 B7 B5 -94.1(6) . . . . ?
C40 B4 B7 B8 42.0(5) . . . . ?
C40 B4 B7 B9 5.9(8) . . . . ?
C40 B4 B8 C39 -32.7(5) . . . . ?
C40 B4 B8 B7 -131.4(6) . . . . ?
C40 B4 B8 B9 -94.8(6) . . . . ?
C40 B8 B9 C39 33.0(5) . . . . ?
C40 B8 B9 B1 1.2(7) . . . . ?
C40 B8 B9 B6 -59.8(7) . . . . ?
C40 B8 B9 B7 -98.8(6) . . . . ?
C28 C29 C30 C31 -1.5(13) . . . . ?
C8 C9 C10 C11 0(2) . . . . ?
C12 C11 C10 C9 0(2) . . . . ?
C6 C1 C2 C3 2.4(14) . . . . ?
C6 C5 C4 C3 -2.1(19) . . . . ?
C31 C32 C27 P55 173.9(6) . . . . ?
C31 C32 C27 C28 -4.0(11) . . . . ?
C43 C42 C41 P37 178.9(6) . . . . ?
C43 C42 C41 C46 0.0(12) . . . . ?
C46 C45 C44 C43 1.2(17) . . . . ?
C48 C47 C52 C51 -2.7(19) . . . . ?
C48 C49 C50 C51 0(3) . . . . ?
C7 P7 C13 B15 -154.6(6) . . . . ?
C7 P7 C13 B16 135.3(6) . . . . ?
C7 P7 C13 B19 -14.7(7) . . . . ?
C7 P7 C13 B17 60.3(7) . . . . ?
C7 P7 C13 B10 -84.2(6) . . . . ?
C7 P7 C1 C2 -34.7(8) . . . . ?
C7 P7 C1 C6 145.4(7) . . . . ?
C7 C8 C9 C10 0.2(19) . . . . ?
C7 C12 C11 C10 0(2) . . . . ?
C9 C8 C7 P7 -176.9(9) . . . . ?
C9 C8 C7 C12 -0.1(17) . . . . ?
C11 C12 C7 P7 177.3(11) . . . . ?
C11 C12 C7 C8 0.2(18) . . . . ?
C50 C51 C52 C47 3(3) . . . . ?
C52 C47 C48 C49 1.4(16) . . . . ?
C52 C51 C50 C49 -1(3) . . . . ?
B13 B12 B14 C14 135.4(6) . . . . ?
B13 B12 B14 B15 99.9(7) . . . . ?
B13 B12 B14 B16 36.7(6) . . . . ?
B13 B12 B11 C14 -98.4(7) . . . . ?
B13 B12 B11 B18 37.0(6) . . . . ?
B13 B12 B11 B19 -0.8(8) . . . . ?
B13 B12 B11 B10 -63.6(8) . . . . ?
B13 B12 B18 B11 -138.8(6) . . . . ?
B13 B12 B18 B19 -101.3(7) . . . . ?
B13 B12 B18 B17 -37.6(6) . . . . ?
B13 B14 B15 C13 2.2(8) . . . . ?
B13 B14 B15 C14 97.9(7) . . . . ?
B13 B14 B15 B16 -37.5(6) . . . . ?
B13 B14 B15 B10 63.5(8) . . . . ?
B13 B14 B16 C13 99.0(7) . . . . ?
B13 B14 B16 B15 137.4(7) . . . . ?
B13 B14 B16 B17 37.8(6) . . . . ?
B13 B16 B17 C13 134.9(7) . . . . ?
B13 B16 B17 B18 37.4(6) . . . . ?
B13 B16 B17 B19 101.2(8) . . . . ?
B13 B18 B19 C13 -2.6(9) . . . . ?
B13 B18 B19 B11 -102.0(7) . . . . ?
B13 B18 B19 B17 37.1(7) . . . . ?
B13 B18 B19 B10 -64.6(9) . . . . ?
B13 B18 B17 C13 -99.1(7) . . . . ?
B13 B18 B17 B16 -37.1(6) . . . . ?
B13 B18 B17 B19 -138.7(7) . . . . ?
B12 C14 B14 B13 38.7(6) . . . . ?
B12 C14 B14 B15 139.7(6) . . . . ?
B12 C14 B14 B16 100.4(7) . . . . ?
B12 C14 B11 B18 -38.8(6) . . . . ?
B12 C14 B11 B19 -101.8(7) . . . . ?
B12 C14 B11 B10 -140.8(7) . . . . ?
B12 C14 B15 C13 62.9(7) . . . . ?
B12 C14 B15 B14 -38.0(6) . . . . ?
B12 C14 B15 B16 0.9(7) . . . . ?
B12 C14 B15 B10 102.9(6) . . . . ?
B12 C14 B10 C13 -65.1(7) . . . . ?
B12 C14 B10 B11 36.3(7) . . . . ?
B12 C14 B10 B15 -104.5(7) . . . . ?
B12 C14 B10 B19 -3.6(9) . . . . ?
B12 B13 B14 C14 -38.6(5) . . . . ?
B12 B13 B14 B15 -100.4(7) . . . . ?
B12 B13 B14 B16 -138.3(7) . . . . ?
B12 B13 B16 C13 -61.8(8) . . . . ?
B12 B13 B16 B14 37.3(6) . . . . ?
B12 B13 B16 B15 -1.3(8) . . . . ?
B12 B13 B16 B17 -100.5(7) . . . . ?
B12 B13 B18 B11 37.4(6) . . . . ?
B12 B13 B18 B19 100.9(7) . . . . ?
B12 B13 B18 B17 138.1(6) . . . . ?
B12 B13 B17 C13 61.8(8) . . . . ?
B12 B13 B17 B16 101.0(7) . . . . ?
B12 B13 B17 B18 -37.0(6) . . . . ?
B12 B13 B17 B19 0.2(8) . . . . ?
B12 B14 B15 C13 -60.1(8) . . . . ?
B12 B14 B15 C14 35.5(6) . . . . ?
B12 B14 B15 B16 -99.8(7) . . . . ?
B12 B14 B15 B10 1.2(9) . . . . ?
B12 B14 B16 C13 62.3(7) . . . . ?
B12 B14 B16 B13 -36.7(6) . . . . ?
B12 B14 B16 B15 100.6(6) . . . . ?
B12 B14 B16 B17 1.1(8) . . . . ?
B12 B11 B18 B13 -37.4(6) . . . . ?
B12 B11 B18 B19 -138.0(7) . . . . ?
B12 B11 B18 B17 -101.2(7) . . . . ?
B12 B11 B19 C13 -61.0(7) . . . . ?
B12 B11 B19 B18 37.3(6) . . . . ?
B12 B11 B19 B17 0.9(8) . . . . ?
B12 B11 B19 B10 -100.7(6) . . . . ?
B12 B11 B10 C13 60.6(8) . . . . ?
B12 B11 B10 C14 -34.7(6) . . . . ?
B12 B11 B10 B15 0.0(9) . . . . ?
B12 B11 B10 B19 100.5(8) . . . . ?
B12 B18 B19 C13 61.5(9) . . . . ?
B12 B18 B19 B11 -37.9(6) . . . . ?
B12 B18 B19 B17 101.2(8) . . . . ?
B12 B18 B19 B10 -0.5(9) . . . . ?
B12 B18 B17 C13 -61.3(8) . . . . ?
B12 B18 B17 B13 37.8(6) . . . . ?
B12 B18 B17 B16 0.7(8) . . . . ?
B12 B18 B17 B19 -100.9(7) . . . . ?
B14 C14 B12 B13 -39.5(6) . . . . ?
B14 C14 B12 B11 -141.7(7) . . . . ?
B14 C14 B12 B18 -102.4(7) . . . . ?
B14 C14 B11 B12 36.3(6) . . . . ?
B14 C14 B11 B18 -2.5(8) . . . . ?
B14 C14 B11 B19 -65.5(7) . . . . ?
B14 C14 B11 B10 -104.5(7) . . . . ?
B14 C14 B15 C13 100.9(6) . . . . ?
B14 C14 B15 B16 38.8(6) . . . . ?
B14 C14 B15 B10 140.8(6) . . . . ?
B14 C14 B10 C13 2.2(7) . . . . ?
B14 C14 B10 B11 103.6(7) . . . . ?
B14 C14 B10 B15 -37.2(6) . . . . ?
B14 C14 B10 B19 63.7(8) . . . . ?
B14 B13 B12 C14 38.8(5) . . . . ?
B14 B13 B12 B11 101.6(6) . . . . ?
B14 B13 B12 B18 138.5(6) . . . . ?
B14 B13 B16 C13 -99.1(7) . . . . ?
B14 B13 B16 B15 -38.6(6) . . . . ?
B14 B13 B16 B17 -137.7(7) . . . . ?
B14 B13 B18 B12 -37.1(6) . . . . ?
B14 B13 B18 B11 0.3(8) . . . . ?
B14 B13 B18 B19 63.9(8) . . . . ?
B14 B13 B18 B17 101.0(6) . . . . ?
B14 B13 B17 C13 -1.6(9) . . . . ?
B14 B13 B17 B16 37.5(7) . . . . ?
B14 B13 B17 B18 -100.5(8) . . . . ?
B14 B13 B17 B19 -63.2(8) . . . . ?
B14 B12 B11 C14 -34.1(6) . . . . ?
B14 B12 B11 B18 101.3(8) . . . . ?
B14 B12 B11 B19 63.5(8) . . . . ?
B14 B12 B11 B10 0.7(10) . . . . ?
B14 B12 B18 B13 37.5(6) . . . . ?
B14 B12 B18 B11 -101.3(7) . . . . ?
B14 B12 B18 B19 -63.8(8) . . . . ?
B14 B12 B18 B17 0.0(8) . . . . ?
B14 B15 B16 C13 134.8(7) . . . . ?
B14 B15 B16 B13 39.0(6) . . . . ?
B14 B15 B16 B17 102.1(7) . . . . ?
B14 B15 B10 C13 -98.1(6) . . . . ?
B14 B15 B10 C14 34.6(6) . . . . ?
B14 B15 B10 B11 -0.8(9) . . . . ?
B14 B15 B10 B19 -64.9(8) . . . . ?
B14 B16 B17 C13 96.3(7) . . . . ?
B14 B16 B17 B13 -38.6(6) . . . . ?
B14 B16 B17 B18 -1.1(8) . . . . ?
B14 B16 B17 B19 62.7(7) . . . . ?
B11 C14 B12 B13 102.1(7) . . . . ?
B11 C14 B12 B14 141.7(7) . . . . ?
B11 C14 B12 B18 39.3(7) . . . . ?
B11 C14 B14 B13 2.7(8) . . . . ?
B11 C14 B14 B12 -36.0(6) . . . . ?
B11 C14 B14 B15 103.7(7) . . . . ?
B11 C14 B14 B16 64.4(7) . . . . ?
B11 C14 B15 C13 -3.6(7) . . . . ?
B11 C14 B15 B14 -104.5(7) . . . . ?
B11 C14 B15 B16 -65.7(7) . . . . ?
B11 C14 B15 B10 36.3(6) . . . . ?
B11 C14 B10 C13 -101.4(7) . . . . ?
B11 C14 B10 B15 -140.8(7) . . . . ?
B11 C14 B10 B19 -39.9(6) . . . . ?
B11 B12 B14 C14 34.4(6) . . . . ?
B11 B12 B14 B13 -101.0(7) . . . . ?
B11 B12 B14 B15 -1.1(9) . . . . ?
B11 B12 B14 B16 -64.3(8) . . . . ?
B11 B12 B18 B13 138.8(6) . . . . ?
B11 B12 B18 B19 37.5(6) . . . . ?
B11 B12 B18 B17 101.2(7) . . . . ?
B11 B18 B19 C13 99.4(7) . . . . ?
B11 B18 B19 B17 139.1(7) . . . . ?
B11 B18 B19 B10 37.4(6) . . . . ?
B11 B18 B17 C13 3.0(8) . . . . ?
B11 B18 B17 B13 102.1(7) . . . . ?
B11 B18 B17 B16 65.0(8) . . . . ?
B11 B18 B17 B19 -36.6(6) . . . . ?
B11 B19 B17 C13 -97.5(6) . . . . ?
B11 B19 B17 B13 -0.7(8) . . . . ?
B11 B19 B17 B16 -63.6(7) . . . . ?
B11 B19 B17 B18 36.4(6) . . . . ?
B11 B19 B10 C13 134.2(6) . . . . ?
B11 B19 B10 C14 39.8(6) . . . . ?
B11 B19 B10 B15 101.7(6) . . . . ?
B15 C13 B16 B13 103.5(7) . . . . ?
B15 C13 B16 B14 39.7(6) . . . . ?
B15 C13 B16 B17 142.7(7) . . . . ?
B15 C13 B19 B11 -3.3(8) . . . . ?
B15 C13 B19 B18 -65.4(8) . . . . ?
B15 C13 B19 B17 -105.2(7) . . . . ?
B15 C13 B19 B10 36.7(6) . . . . ?
B15 C13 B17 B13 3.3(9) . . . . ?
B15 C13 B17 B16 -35.9(7) . . . . ?
B15 C13 B17 B18 65.8(8) . . . . ?
B15 C13 B17 B19 106.1(7) . . . . ?
B15 C13 B10 C14 -40.0(5) . . . . ?
B15 C13 B10 B11 -102.2(6) . . . . ?
B15 C13 B10 B19 -142.7(6) . . . . ?
B15 C14 B12 B13 -1.7(8) . . . . ?
B15 C14 B12 B14 37.9(6) . . . . ?
B15 C14 B12 B11 -103.8(7) . . . . ?
B15 C14 B12 B18 -64.5(8) . . . . ?
B15 C14 B14 B13 -101.0(6) . . . . ?
B15 C14 B14 B12 -139.7(6) . . . . ?
B15 C14 B14 B16 -39.3(6) . . . . ?
B15 C14 B11 B12 103.6(7) . . . . ?
B15 C14 B11 B18 64.8(7) . . . . ?
B15 C14 B11 B19 1.8(8) . . . . ?
B15 C14 B11 B10 -37.2(6) . . . . ?
B15 C14 B10 C13 39.4(5) . . . . ?
B15 C14 B10 B11 140.8(7) . . . . ?
B15 C14 B10 B19 100.9(7) . . . . ?
B15 B14 B16 C13 -38.4(5) . . . . ?
B15 B14 B16 B13 -137.4(7) . . . . ?
B15 B14 B16 B17 -99.6(6) . . . . ?
B15 B16 B17 C13 32.4(6) . . . . ?
B15 B16 B17 B13 -102.5(7) . . . . ?
B15 B16 B17 B18 -65.0(7) . . . . ?
B15 B16 B17 B19 -1.3(8) . . . . ?
B16 C13 B15 C14 -100.5(6) . . . . ?
B16 C13 B15 B14 -39.4(6) . . . . ?
B16 C13 B15 B10 -140.4(6) . . . . ?
B16 C13 B19 B11 65.5(8) . . . . ?
B16 C13 B19 B18 3.4(9) . . . . ?
B16 C13 B19 B17 -36.4(7) . . . . ?
B16 C13 B19 B10 105.5(7) . . . . ?
B16 C13 B17 B13 39.1(7) . . . . ?
B16 C13 B17 B18 101.6(7) . . . . ?
B16 C13 B17 B19 142.0(7) . . . . ?
B16 C13 B10 C14 -1.9(7) . . . . ?
B16 C13 B10 B11 -64.2(7) . . . . ?
B16 C13 B10 B15 38.1(6) . . . . ?
B16 C13 B10 B19 -104.6(6) . . . . ?
B16 B13 B12 C14 1.8(8) . . . . ?
B16 B13 B12 B14 -37.0(6) . . . . ?
B16 B13 B12 B11 64.7(8) . . . . ?
B16 B13 B12 B18 101.6(7) . . . . ?
B16 B13 B14 C14 99.7(6) . . . . ?
B16 B13 B14 B12 138.3(7) . . . . ?
B16 B13 B14 B15 37.9(6) . . . . ?
B16 B13 B18 B12 -100.0(7) . . . . ?
B16 B13 B18 B11 -62.5(9) . . . . ?
B16 B13 B18 B19 1.0(10) . . . . ?
B16 B13 B18 B17 38.1(7) . . . . ?
B16 B13 B17 C13 -39.2(6) . . . . ?
B16 B13 B17 B18 -138.0(7) . . . . ?
B16 B13 B17 B19 -100.7(7) . . . . ?
B16 B14 B15 C13 39.7(6) . . . . ?
B16 B14 B15 C14 135.4(6) . . . . ?
B16 B14 B15 B10 101.0(7) . . . . ?
B16 B15 B10 C13 -35.5(5) . . . . ?
B16 B15 B10 C14 97.3(6) . . . . ?
B16 B15 B10 B11 61.9(8) . . . . ?
B16 B15 B10 B19 -2.2(8) . . . . ?
B18 B13 B12 C14 -99.8(6) . . . . ?
B18 B13 B12 B14 -138.5(6) . . . . ?
B18 B13 B12 B11 -36.9(6) . . . . ?
B18 B13 B14 C14 -1.8(8) . . . . ?
B18 B13 B14 B12 36.8(6) . . . . ?
B18 B13 B14 B15 -63.6(8) . . . . ?
B18 B13 B14 B16 -101.5(7) . . . . ?
B18 B13 B16 C13 1.0(9) . . . . ?
B18 B13 B16 B14 100.1(8) . . . . ?
B18 B13 B16 B15 61.5(8) . . . . ?
B18 B13 B16 B17 -37.6(7) . . . . ?
B18 B13 B17 C13 98.8(7) . . . . ?
B18 B13 B17 B16 138.0(7) . . . . ?
B18 B13 B17 B19 37.3(6) . . . . ?
B18 B12 B14 C14 98.1(7) . . . . ?
B18 B12 B14 B13 -37.3(6) . . . . ?
B18 B12 B14 B15 62.5(8) . . . . ?
B18 B12 B14 B16 -0.6(8) . . . . ?
B18 B12 B11 C14 -135.4(7) . . . . ?
B18 B12 B11 B19 -37.7(6) . . . . ?
B18 B12 B11 B10 -100.6(8) . . . . ?
B18 B11 B19 C13 -98.3(6) . . . . ?
B18 B11 B19 B17 -36.3(6) . . . . ?
B18 B11 B19 B10 -138.0(7) . . . . ?
B18 B11 B10 C13 -2.1(8) . . . . ?
B18 B11 B10 C14 -97.5(7) . . . . ?
B18 B11 B10 B15 -62.7(8) . . . . ?
B18 B11 B10 B19 37.8(6) . . . . ?
B18 B19 B17 C13 -134.0(7) . . . . ?
B18 B19 B17 B13 -37.2(6) . . . . ?
B18 B19 B17 B16 -100.0(7) . . . . ?
B18 B19 B10 C13 96.9(7) . . . . ?
B18 B19 B10 C14 2.5(9) . . . . ?
B18 B19 B10 B11 -37.4(6) . . . . ?
B18 B19 B10 B15 64.4(8) . . . . ?
B19 C13 B15 C14 4.2(7) . . . . ?
B19 C13 B15 B14 65.4(8) . . . . ?
B19 C13 B15 B16 104.8(7) . . . . ?
B19 C13 B15 B10 -35.7(6) . . . . ?
B19 C13 B16 B13 -2.9(9) . . . . ?
B19 C13 B16 B14 -66.6(8) . . . . ?
B19 C13 B16 B15 -106.3(7) . . . . ?
B19 C13 B16 B17 36.4(7) . . . . ?
B19 C13 B17 B13 -102.9(8) . . . . ?
B19 C13 B17 B16 -142.0(7) . . . . ?
B19 C13 B17 B18 -40.4(6) . . . . ?
B19 C13 B10 C14 102.7(6) . . . . ?
B19 C13 B10 B11 40.5(6) . . . . ?
B19 C13 B10 B15 142.7(6) . . . . ?
B19 B11 B18 B13 100.6(7) . . . . ?
B19 B11 B18 B12 138.0(7) . . . . ?
B19 B11 B18 B17 36.8(6) . . . . ?
B19 B11 B10 C13 -39.9(6) . . . . ?
B19 B11 B10 C14 -135.2(7) . . . . ?
B19 B11 B10 B15 -100.5(7) . . . . ?
B19 B18 B17 C13 39.6(6) . . . . ?
B19 B18 B17 B13 138.7(7) . . . . ?
B19 B18 B17 B16 101.6(7) . . . . ?
B17 C13 B15 C14 -64.6(8) . . . . ?
B17 C13 B15 B14 -3.5(9) . . . . ?
B17 C13 B15 B16 35.9(7) . . . . ?
B17 C13 B15 B10 -104.6(7) . . . . ?
B17 C13 B16 B13 -39.3(6) . . . . ?
B17 C13 B16 B14 -103.0(7) . . . . ?
B17 C13 B16 B15 -142.7(7) . . . . ?
B17 C13 B19 B11 101.9(7) . . . . ?
B17 C13 B19 B18 39.9(6) . . . . ?
B17 C13 B19 B10 141.9(6) . . . . ?
B17 C13 B10 C14 66.5(7) . . . . ?
B17 C13 B10 B11 4.2(8) . . . . ?
B17 C13 B10 B15 106.5(6) . . . . ?
B17 C13 B10 B19 -36.2(6) . . . . ?
B17 B13 B12 C14 -62.5(7) . . . . ?
B17 B13 B12 B14 -101.3(6) . . . . ?
B17 B13 B12 B11 0.3(8) . . . . ?
B17 B13 B12 B18 37.2(6) . . . . ?
B17 B13 B14 C14 61.4(8) . . . . ?
B17 B13 B14 B12 100.0(7) . . . . ?
B17 B13 B14 B15 -0.4(9) . . . . ?
B17 B13 B14 B16 -38.2(7) . . . . ?
B17 B13 B16 C13 38.6(6) . . . . ?
B17 B13 B16 B14 137.7(7) . . . . ?
B17 B13 B16 B15 99.1(7) . . . . ?
B17 B13 B18 B12 -138.1(6) . . . . ?
B17 B13 B18 B11 -100.7(7) . . . . ?
B17 B13 B18 B19 -37.1(6) . . . . ?
B17 B18 B19 C13 -39.7(6) . . . . ?
B17 B18 B19 B11 -139.1(7) . . . . ?
B17 B18 B19 B10 -101.7(7) . . . . ?
B17 B19 B10 C13 34.0(6) . . . . ?
B17 B19 B10 C14 -60.5(8) . . . . ?
B17 B19 B10 B11 -100.3(7) . . . . ?
B17 B19 B10 B15 1.4(8) . . . . ?
B2 B1 B6 B5 -40.8(6) . . . . ?
B2 B1 B6 B7 -103.8(7) . . . . ?
B2 B1 B6 B9 -140.9(6) . . . . ?
B2 B1 B9 C39 -98.4(6) . . . . ?
B2 B1 B9 B6 35.9(6) . . . . ?
B2 B1 B9 B7 -1.9(7) . . . . ?
B2 B1 B9 B8 -65.0(7) . . . . ?
B2 B3 B4 C40 98.3(6) . . . . ?
B2 B3 B4 B5 -35.2(5) . . . . ?
B2 B3 B4 B7 3.3(7) . . . . ?
B2 B3 B4 B8 66.3(7) . . . . ?
B2 B3 B5 B6 39.4(5) . . . . ?
B2 B3 B5 B4 140.1(6) . . . . ?
B2 B3 B5 B7 102.7(6) . . . . ?
B2 B6 B5 B3 -41.7(6) . . . . ?
B2 B6 B5 B4 -106.6(7) . . . . ?
B2 B6 B5 B7 -142.8(6) . . . . ?
B2 B6 B7 B4 -3.0(8) . . . . ?
B2 B6 B7 B5 33.7(6) . . . . ?
B2 B6 B7 B8 -66.2(8) . . . . ?
B2 B6 B7 B9 -104.1(7) . . . . ?
B2 B6 B9 C39 0.3(8) . . . . ?
B2 B6 B9 B1 -37.1(6) . . . . ?
B2 B6 B9 B7 100.9(7) . . . . ?
B2 B6 B9 B8 62.4(8) . . . . ?
B2 B5 B7 B6 -33.1(6) . . . . ?
B2 B5 B7 B4 105.8(7) . . . . ?
B2 B5 B7 B8 67.0(7) . . . . ?
B2 B5 B7 B9 4.3(8) . . . . ?
B1 C39 C40 P37 -152.2(5) . . . . ?
B1 C39 C40 B3 -2.6(9) . . . . ?
B1 C39 C40 B4 67.4(7) . . . . ?
B1 C39 C40 B8 104.4(6) . . . . ?
B1 C39 B8 C40 -104.2(6) . . . . ?
B1 C39 B8 B4 -69.0(7) . . . . ?
B1 C39 B8 B7 -6.9(8) . . . . ?
B1 C39 B8 B9 35.1(6) . . . . ?
B1 C39 B9 B6 -38.1(5) . . . . ?
B1 C39 B9 B7 -101.0(6) . . . . ?
B1 C39 B9 B8 -142.8(6) . . . . ?
B1 B2 B3 C40 0.2(8) . . . . ?
B1 B2 B3 B4 -64.0(7) . . . . ?
B1 B2 B3 B5 -99.6(6) . . . . ?
B1 B2 B6 B5 133.7(6) . . . . ?
B1 B2 B6 B7 99.9(6) . . . . ?
B1 B2 B6 B9 36.1(6) . . . . ?
B1 B2 B5 B3 95.9(6) . . . . ?
B1 B2 B5 B6 -38.9(5) . . . . ?
B1 B2 B5 B4 58.2(8) . . . . ?
B1 B2 B5 B7 -5.3(7) . . . . ?
B1 B6 B5 B2 42.3(6) . . . . ?
B1 B6 B5 B3 0.6(8) . . . . ?
B1 B6 B5 B4 -64.2(8) . . . . ?
B1 B6 B5 B7 -100.5(7) . . . . ?
B1 B6 B7 B4 63.6(8) . . . . ?
B1 B6 B7 B5 100.3(7) . . . . ?
B1 B6 B7 B8 0.4(8) . . . . ?
B1 B6 B7 B9 -37.5(6) . . . . ?
B1 B6 B9 C39 37.4(5) . . . . ?
B1 B6 B9 B7 138.0(6) . . . . ?
B1 B6 B9 B8 99.6(6) . . . . ?
B3 C40 B4 B5 39.0(5) . . . . ?
B3 C40 B4 B7 101.9(6) . . . . ?
B3 C40 B4 B8 144.0(6) . . . . ?
B3 C40 B8 C39 104.2(6) . . . . ?
B3 C40 B8 B4 -35.6(6) . . . . ?
B3 C40 B8 B7 6.5(8) . . . . ?
B3 C40 B8 B9 68.9(7) . . . . ?
B3 B2 B1 C39 -1.6(8) . . . . ?
B3 B2 B1 B6 100.9(7) . . . . ?
B3 B2 B1 B9 64.2(7) . . . . ?
B3 B2 B6 B1 -95.0(6) . . . . ?
B3 B2 B6 B5 38.7(5) . . . . ?
B3 B2 B6 B7 4.9(8) . . . . ?
B3 B2 B6 B9 -59.0(8) . . . . ?
B3 B2 B5 B6 -134.8(6) . . . . ?
B3 B2 B5 B4 -37.7(6) . . . . ?
B3 B2 B5 B7 -101.2(6) . . . . ?
B3 B4 B5 B2 38.4(6) . . . . ?
B3 B4 B5 B6 100.9(7) . . . . ?
B3 B4 B5 B7 137.6(6) . . . . ?
B3 B4 B7 B6 -0.3(8) . . . . ?
B3 B4 B7 B5 -37.3(6) . . . . ?
B3 B4 B7 B8 98.8(7) . . . . ?
B3 B4 B7 B9 62.7(8) . . . . ?
B3 B4 B8 C39 -2.8(7) . . . . ?
B3 B4 B8 C40 29.9(5) . . . . ?
B3 B4 B8 B7 -101.5(7) . . . . ?
B3 B4 B8 B9 -64.9(8) . . . . ?
B3 B5 B7 B6 -100.3(7) . . . . ?
B3 B5 B7 B4 38.6(6) . . . . ?
B3 B5 B7 B8 -0.2(8) . . . . ?
B3 B5 B7 B9 -62.9(7) . . . . ?
B6 B2 B1 C39 -102.5(7) . . . . ?
B6 B2 B1 B9 -36.7(6) . . . . ?
B6 B2 B3 C40 59.2(8) . . . . ?
B6 B2 B3 B4 -5.0(7) . . . . ?
B6 B2 B3 B5 -40.6(6) . . . . ?
B6 B2 B5 B3 134.8(6) . . . . ?
B6 B2 B5 B4 97.1(7) . . . . ?
B6 B2 B5 B7 33.6(6) . . . . ?
B6 B1 B9 C39 -134.3(6) . . . . ?
B6 B1 B9 B7 -37.9(6) . . . . ?
B6 B1 B9 B8 -100.9(6) . . . . ?
B6 B5 B7 B4 138.9(7) . . . . ?
B6 B5 B7 B8 100.1(7) . . . . ?
B6 B5 B7 B9 37.4(6) . . . . ?
B6 B7 B8 C39 3.7(8) . . . . ?
B6 B7 B8 C40 59.8(7) . . . . ?
B6 B7 B8 B4 101.8(7) . . . . ?
B6 B7 B8 B9 -37.8(6) . . . . ?
B6 B7 B9 C39 95.0(7) . . . . ?
B6 B7 B9 B1 36.3(6) . . . . ?
B6 B7 B9 B8 137.0(7) . . . . ?
B10 C13 B15 C14 39.9(5) . . . . ?
B10 C13 B15 B14 101.1(6) . . . . ?
B10 C13 B15 B16 140.4(6) . . . . ?
B10 C13 B16 B13 64.7(8) . . . . ?
B10 C13 B16 B14 0.9(8) . . . . ?
B10 C13 B16 B15 -38.8(6) . . . . ?
B10 C13 B16 B17 104.0(7) . . . . ?
B10 C13 B19 B11 -40.0(6) . . . . ?
B10 C13 B19 B18 -102.1(7) . . . . ?
B10 C13 B19 B17 -141.9(6) . . . . ?
B10 C13 B17 B13 -67.0(8) . . . . ?
B10 C13 B17 B16 -106.2(7) . . . . ?
B10 C13 B17 B18 -4.5(8) . . . . ?
B10 C13 B17 B19 35.8(6) . . . . ?
B10 C14 B12 B13 66.2(8) . . . . ?
B10 C14 B12 B14 105.7(7) . . . . ?
B10 C14 B12 B11 -36.0(7) . . . . ?
B10 C14 B12 B18 3.3(9) . . . . ?
B10 C14 B14 B13 -63.4(7) . . . . ?
B10 C14 B14 B12 -102.1(6) . . . . ?
B10 C14 B14 B15 37.6(6) . . . . ?
B10 C14 B14 B16 -1.7(8) . . . . ?
B10 C14 B11 B12 140.8(7) . . . . ?
B10 C14 B11 B18 102.0(7) . . . . ?
B10 C14 B11 B19 39.0(6) . . . . ?
B10 C14 B15 C13 -39.9(5) . . . . ?
B10 C14 B15 B14 -140.8(6) . . . . ?
B10 C14 B15 B16 -102.0(6) . . . . ?
B10 B11 B18 B13 63.3(8) . . . . ?
B10 B11 B18 B12 100.7(7) . . . . ?
B10 B11 B18 B19 -37.3(6) . . . . ?
B10 B11 B18 B17 -0.5(8) . . . . ?
B10 B11 B19 C13 39.7(6) . . . . ?
B10 B11 B19 B18 138.0(7) . . . . ?
B10 B11 B19 B17 101.6(7) . . . . ?
B10 B15 B16 C13 34.8(6) . . . . ?
B10 B15 B16 B13 -61.0(7) . . . . ?
B10 B15 B16 B14 -100.0(6) . . . . ?
B10 B15 B16 B17 2.1(8) . . . . ?
B10 B19 B17 C13 -34.1(6) . . . . ?
B10 B19 B17 B13 62.7(8) . . . . ?
B10 B19 B17 B16 -0.1(8) . . . . ?
B10 B19 B17 B18 99.9(7) . . . . ?
B4 C40 B3 B2 -102.2(7) . . . . ?
B4 C40 B3 B5 -40.7(6) . . . . ?
B4 C40 B8 C39 139.8(6) . . . . ?
B4 C40 B8 B7 42.1(5) . . . . ?
B4 C40 B8 B9 104.5(6) . . . . ?
B4 B3 B5 B2 -140.1(6) . . . . ?
B4 B3 B5 B6 -100.7(6) . . . . ?
B4 B3 B5 B7 -37.5(6) . . . . ?
B4 B5 B7 B6 -138.9(7) . . . . ?
B4 B5 B7 B8 -38.8(6) . . . . ?
B4 B5 B7 B9 -101.5(6) . . . . ?
B4 B7 B8 C39 -98.2(6) . . . . ?
B4 B7 B8 C40 -42.0(5) . . . . ?
B4 B7 B8 B9 -139.6(7) . . . . ?
B4 B7 B9 C39 -5.8(8) . . . . ?
B4 B7 B9 B1 -64.5(7) . . . . ?
B4 B7 B9 B6 -100.8(7) . . . . ?
B4 B7 B9 B8 36.2(6) . . . . ?
B4 B8 B9 C39 95.4(6) . . . . ?
B4 B8 B9 B1 63.6(7) . . . . ?
B4 B8 B9 B6 2.6(9) . . . . ?
B4 B8 B9 B7 -36.4(6) . . . . ?
B5 B2 B1 C39 -61.3(7) . . . . ?
B5 B2 B1 B6 41.3(6) . . . . ?
B5 B2 B1 B9 4.5(7) . . . . ?
B5 B2 B3 C40 99.8(7) . . . . ?
B5 B2 B3 B4 35.6(6) . . . . ?
B5 B2 B6 B1 -133.7(6) . . . . ?
B5 B2 B6 B7 -33.8(6) . . . . ?
B5 B2 B6 B9 -97.6(7) . . . . ?
B5 B3 B4 C40 133.5(6) . . . . ?
B5 B3 B4 B7 38.5(6) . . . . ?
B5 B3 B4 B8 101.6(6) . . . . ?
B5 B6 B7 B4 -36.7(6) . . . . ?
B5 B6 B7 B8 -99.9(7) . . . . ?
B5 B6 B7 B9 -137.8(7) . . . . ?
B5 B6 B9 C39 -63.2(8) . . . . ?
B5 B6 B9 B1 -100.5(7) . . . . ?
B5 B6 B9 B7 37.4(6) . . . . ?
B5 B6 B9 B8 -1.0(9) . . . . ?
B5 B4 B7 B6 37.0(6) . . . . ?
B5 B4 B7 B8 136.1(7) . . . . ?
B5 B4 B7 B9 100.0(7) . . . . ?
B5 B4 B8 C39 58.9(8) . . . . ?
B5 B4 B8 C40 91.6(7) . . . . ?
B5 B4 B8 B7 -39.8(6) . . . . ?
B5 B4 B8 B9 -3.2(9) . . . . ?
B5 B7 B8 C39 -59.6(7) . . . . ?
B5 B7 B8 C40 -3.4(7) . . . . ?
B5 B7 B8 B4 38.6(6) . . . . ?
B5 B7 B8 B9 -101.1(7) . . . . ?
B5 B7 B9 C39 57.2(7) . . . . ?
B5 B7 B9 B1 -1.5(7) . . . . ?
B5 B7 B9 B6 -37.8(6) . . . . ?
B5 B7 B9 B8 99.2(6) . . . . ?
B7 B6 B5 B2 142.8(6) . . . . ?
B7 B6 B5 B3 101.1(6) . . . . ?
B7 B6 B5 B4 36.2(6) . . . . ?
B7 B6 B9 C39 -100.6(6) . . . . ?
B7 B6 B9 B1 -138.0(6) . . . . ?
B7 B6 B9 B8 -38.4(6) . . . . ?
B7 B4 B5 B2 -99.1(7) . . . . ?
B7 B4 B5 B3 -137.6(6) . . . . ?
B7 B4 B5 B6 -36.6(6) . . . . ?
B7 B4 B8 C39 98.7(6) . . . . ?
B7 B4 B8 C40 131.4(6) . . . . ?
B7 B4 B8 B9 36.6(6) . . . . ?
B7 B8 B9 C39 131.8(6) . . . . ?
B7 B8 B9 B1 100.0(6) . . . . ?
B7 B8 B9 B6 39.0(6) . . . . ?
B8 C39 C40 P37 103.4(5) . . . . ?
B8 C39 C40 B3 -107.0(7) . . . . ?
B8 C39 C40 B4 -37.0(5) . . . . ?
B8 C39 B1 B2 71.0(7) . . . . ?
B8 C39 B1 B6 7.5(8) . . . . ?
B8 C39 B1 B9 -34.5(6) . . . . ?
B8 C39 B9 B1 142.8(6) . . . . ?
B8 C39 B9 B6 104.7(6) . . . . ?
B8 C39 B9 B7 41.8(5) . . . . ?
B8 C40 B3 B2 -68.1(7) . . . . ?
B8 C40 B3 B4 34.1(6) . . . . ?
B8 C40 B3 B5 -6.6(8) . . . . ?
B8 C40 B4 B3 -144.0(6) . . . . ?
B8 C40 B4 B5 -105.0(6) . . . . ?
B8 C40 B4 B7 -42.1(5) . . . . ?
B8 B4 B5 B2 -60.0(9) . . . . ?
B8 B4 B5 B3 -98.4(7) . . . . ?
B8 B4 B5 B6 2.6(9) . . . . ?
B8 B4 B5 B7 39.2(6) . . . . ?
B8 B4 B7 B6 -99.1(7) . . . . ?
B8 B4 B7 B5 -136.1(7) . . . . ?
B8 B4 B7 B9 -36.1(6) . . . . ?
B8 B7 B9 C39 -42.0(5) . . . . ?
B8 B7 B9 B1 -100.7(6) . . . . ?
B8 B7 B9 B6 -137.0(7) . . . . ?
B9 C39 C40 P37 140.8(5) . . . . ?
B9 C39 C40 B3 -69.6(8) . . . . ?
B9 C39 C40 B4 0.4(7) . . . . ?
B9 C39 C40 B8 37.4(5) . . . . ?
B9 C39 B1 B2 105.5(6) . . . . ?
B9 C39 B1 B6 42.0(6) . . . . ?
B9 C39 B8 C40 -139.3(6) . . . . ?
B9 C39 B8 B4 -104.1(6) . . . . ?
B9 C39 B8 B7 -42.0(5) . . . . ?
B9 B1 B6 B2 140.9(6) . . . . ?
B9 B1 B6 B5 100.1(6) . . . . ?
B9 B1 B6 B7 37.1(6) . . . . ?
B9 B6 B5 B2 105.6(7) . . . . ?
B9 B6 B5 B3 63.9(8) . . . . ?
B9 B6 B5 B4 -1.0(9) . . . . ?
B9 B6 B5 B7 -37.2(6) . . . . ?
B9 B6 B7 B4 101.1(7) . . . . ?
B9 B6 B7 B5 137.8(7) . . . . ?
B9 B6 B7 B8 37.9(6) . . . . ?
B9 B7 B8 C39 41.5(5) . . . . ?
B9 B7 B8 C40 97.6(6) . . . . ?
B9 B7 B8 B4 139.6(7) . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 -0.299 -0.981 -0.852 4116.9 964.8 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_cu_20250504b_0m_pl
_database_code_depnum_ccdc_archive 'CCDC 2495511'
loop_
_audit_author_name
_audit_author_address
'Hao-Hui Xie'
;NanJing University of Science and Technology
China
;
_audit_update_record             
;
2025-10-15 deposited with the CCDC.	2026-03-06 downloaded from the CCDC.
;
_audit_creation_date             2025-10-07
_audit_creation_method           
;
Olex2 1.5
(compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C52 H60 Au8 B20 P4 S4'
_chemical_formula_sum            'C52 H60 Au8 B20 P4 S4'
_chemical_formula_weight         2729.05
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -4.4197 7.2980 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   13.2101(5)
_cell_length_b                   22.4739(8)
_cell_length_c                   26.7665(9)
_cell_angle_alpha                90
_cell_angle_beta                 93.683(2)
_cell_angle_gamma                90
_cell_volume                     7930.1(5)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9673
_cell_measurement_temperature    100.15
_cell_measurement_theta_max      74.653
_cell_measurement_theta_min      3.309
_shelx_estimated_absorpt_T_max   0.324
_shelx_estimated_absorpt_T_min   0.243
_exptl_absorpt_coefficient_mu    29.061
_exptl_absorpt_correction_T_max  0.7538
_exptl_absorpt_correction_T_min  0.4160
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1325 before and 0.0843 after correction.
The Ratio of minimum to maximum transmission is 0.5519.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            yellow
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    2.286
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             4912
_exptl_crystal_size_max          0.068
_exptl_crystal_size_mid          0.064
_exptl_crystal_size_min          0.05
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.1850
_diffrn_reflns_av_unetI/netI     0.1414
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.993
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       28
_diffrn_reflns_limit_k_min       -26
_diffrn_reflns_limit_l_max       33
_diffrn_reflns_limit_l_min       -33
_diffrn_reflns_number            121298
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.993
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         75.056
_diffrn_reflns_theta_min         2.569
_diffrn_ambient_temperature      100.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  multi-scan
_diffrn_measurement_method       ?
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_source                   ?
_diffrn_source_current           1.1
_diffrn_source_power             0.05500000000000001
_diffrn_source_voltage           50.0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                12424
_reflns_number_total             16249
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.41 (?, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.41 (?, 2016)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'olex2.solve 1.5 (Bourhis et al., 2015)'
_refine_diff_density_max         3.444
_refine_diff_density_min         -2.457
_refine_diff_density_rms         0.484
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.054
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     793
_refine_ls_number_reflns         16249
_refine_ls_number_restraints     66
_refine_ls_R_factor_all          0.1144
_refine_ls_R_factor_gt           0.0760
_refine_ls_restrained_S_all      1.053
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1090P)²+376.1726P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1978
_refine_ls_wR_factor_ref         0.2121
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups
2. Uiso/Uaniso restraints and constraints
B15 \\sim B11 \\sim B14 \\sim B13 \\sim B12: within 2A with sigma of 0.01 and
sigma for terminal atoms of 0.02 within 2A
C7 \\sim C12 \\sim C11 \\sim C10 \\sim C9 \\sim C8: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
3.a Aromatic/amide H refined with riding coordinates:
 C35(H35), C46(H46), C16(H16), C24(H24), C2(H2), C37(H37), C23(H23), C38(H38),
 C28(H28), C36(H36), C8(H8), C20(H20), C48(H48), C30(H30), C12(H12), C6(H6),
 C22(H22), C29(H29), C26(H26), C44(H44), C4(H4), C5(H5), C43(H43), C51(H51),
 C49(H49), C9(H9), C31(H31), C32(H32), C42(H42), C34(H34), C25(H25), C45(H45),
 C52(H52), C3(H3), C19(H19), C11(H11), C18(H18), C17(H17), C10(H10), C50(H50)
3.b Boron cage BH refined with riding coordinates:
 B2(H2a), B5(H5a), B6(H6a), B13(H13), B4(H4a), B12(H12a), B16(H16a), B11(H11a),
  B15(H15), B14(H14), B3(H3a), B17(H17a), B18(H18a), B20(H20a), B7(H7),
 B19(H19a), B1(H1), B8(H8a), B9(H9a), B10(H10a)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     iterative
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au5 Au 0.52747(6) 0.88872(3) 0.71122(3) 0.02138(16) Uani 1 1 d . . . . .
Au2 Au 0.25156(6) 0.97492(3) 0.57732(3) 0.02104(16) Uani 1 1 d . . . . .
Au3 Au 0.28482(6) 0.87192(3) 0.51385(3) 0.02023(16) Uani 1 1 d . . . . .
Au4 Au 0.42054(6) 0.87236(3) 0.61127(3) 0.02163(16) Uani 1 1 d . . . . .
Au7 Au 0.13391(6) 0.94892(3) 0.67828(3) 0.02185(16) Uani 1 1 d . . . . .
Au1 Au 0.20311(5) 1.07405(3) 0.64665(3) 0.02070(16) Uani 1 1 d . . . . .
Au6 Au 0.31047(6) 0.85313(3) 0.71513(3) 0.02411(17) Uani 1 1 d . . . . .
Au8 Au 0.09610(6) 0.81778(3) 0.70784(3) 0.02307(17) Uani 1 1 d . . . . .
S3 S 0.4434(4) 0.80611(17) 0.67793(17) 0.0249(8) Uani 1 1 d . . . . .
S1 S 0.0975(3) 1.00410(17) 0.60631(15) 0.0221(8) Uani 1 1 d . . . . .
S2 S 0.1737(4) 0.89715(19) 0.75160(18) 0.0299(9) Uani 1 1 d . . . . .
S4 S 0.4022(3) 0.94130(17) 0.54666(15) 0.0225(8) Uani 1 1 d . . . . .
P3 P 0.1683(4) 0.80730(17) 0.48059(15) 0.0202(8) Uani 1 1 d . . . . .
P2 P 0.6195(3) 0.96928(17) 0.73455(17) 0.0202(8) Uani 1 1 d . . . . .
P1 P 0.3101(3) 1.14436(17) 0.67904(17) 0.0207(8) Uani 1 1 d . . . . .
P4 P 0.0145(3) 0.74173(18) 0.66763(17) 0.0219(8) Uani 1 1 d . . . . .
C35 C -0.1367(17) 0.8279(8) 0.4509(7) 0.030(4) Uani 1 1 d . . . . .
H35 H -0.190500 0.808598 0.431964 0.036 Uiso 1 1 calc R U . . .
C46 C 0.0627(17) 0.6742(8) 0.7516(7) 0.029(4) Uani 1 1 d . . . . .
H46 H 0.105252 0.707015 0.760790 0.035 Uiso 1 1 calc R U . . .
C16 C 0.6872(19) 0.9102(8) 0.8187(8) 0.037(5) Uani 1 1 d . . . . .
H16 H 0.629112 0.886462 0.810144 0.044 Uiso 1 1 calc R U . . .
C1 C 0.2478(14) 1.2097(7) 0.7031(7) 0.023(3) Uani 1 1 d . . . . .
C14 C 0.5419(15) 1.0344(8) 0.7555(8) 0.029(4) Uani 1 1 d . . . . .
C24 C 0.7642(14) 1.0188(7) 0.5883(7) 0.023(3) Uani 1 1 d . . . . .
H24 H 0.793418 1.027116 0.557572 0.028 Uiso 1 1 calc R U . . .
C2 C 0.2951(15) 1.2538(8) 0.7325(8) 0.028(4) Uani 1 1 d . . . . .
H2 H 0.365141 1.250821 0.742613 0.034 Uiso 1 1 calc R U . . .
C7 C 0.3900(16) 1.1700(9) 0.6307(8) 0.033(3) Uani 1 1 d . U . . .
C37 C -0.0803(15) 0.9048(8) 0.5099(7) 0.029(4) Uani 1 1 d . . . . .
H37 H -0.094775 0.935832 0.532390 0.034 Uiso 1 1 calc R U . . .
C27 C 0.2009(13) 0.7798(8) 0.4196(7) 0.023(3) Uani 1 1 d . . . . .
C23 C 0.6604(14) 1.0125(8) 0.5893(8) 0.027(4) Uani 1 1 d . . . . .
H23 H 0.617501 1.016055 0.559626 0.032 Uiso 1 1 calc R U . . .
C38 C 0.0215(13) 0.8859(7) 0.5039(7) 0.023(3) Uani 1 1 d . . . . .
H38 H 0.076617 0.906899 0.520152 0.027 Uiso 1 1 calc R U . . .
C28 C 0.2614(19) 0.8152(9) 0.3947(7) 0.036(5) Uani 1 1 d . . . . .
H28 H 0.285207 0.850998 0.410231 0.043 Uiso 1 1 calc R U . . .
C36 C -0.1586(16) 0.8755(9) 0.4810(8) 0.033(4) Uani 1 1 d . . . . .
H36 H -0.226686 0.888604 0.482379 0.039 Uiso 1 1 calc R U . . .
C8 C 0.4253(19) 1.2298(10) 0.6311(9) 0.039(3) Uani 1 1 d . U . . .
H8 H 0.413532 1.256332 0.657793 0.047 Uiso 1 1 calc R U . . .
C39 C 0.1527(13) 0.7435(7) 0.5247(7) 0.020(3) Uani 1 1 d . . . . .
C20 C 0.7925(14) 0.9942(8) 0.7992(7) 0.027(4) Uani 1 1 d . . . . .
H20 H 0.805674 1.026962 0.778150 0.032 Uiso 1 1 calc R U . . .
C48 C -0.118(2) 0.8262(8) 0.6301(9) 0.039(5) Uani 1 1 d . . . . .
H48 H -0.060162 0.851184 0.634083 0.047 Uiso 1 1 calc R U . . .
C30 C 0.2594(16) 0.7461(8) 0.3268(8) 0.031(4) Uani 1 1 d . . . . .
H30 H 0.281228 0.733750 0.295250 0.037 Uiso 1 1 calc R U . . .
C21 C 0.6805(14) 0.9934(7) 0.6801(7) 0.024(3) Uani 1 1 d . . . . .
C12 C 0.4116(17) 1.1299(10) 0.5941(8) 0.035(3) Uani 1 1 d . U . . .
H12 H 0.391051 1.089630 0.596877 0.042 Uiso 1 1 calc R U . . .
C41 C 0.0041(15) 0.6762(8) 0.7065(8) 0.029(4) Uani 1 1 d . . . . .
C6 C 0.1469(14) 1.2177(7) 0.6846(7) 0.027(4) Uani 1 1 d . . . . .
H6 H 0.114764 1.188227 0.663662 0.032 Uiso 1 1 calc R U . . .
C22 C 0.6205(15) 1.0007(8) 0.6351(9) 0.033(4) Uani 1 1 d . . . . .
H22 H 0.548966 0.997365 0.636120 0.039 Uiso 1 1 calc R U . . .
C33 C 0.0394(14) 0.8375(8) 0.4747(7) 0.026(4) Uani 1 1 d . . . . .
C29 C 0.292(2) 0.8015(11) 0.3456(7) 0.048(7) Uani 1 1 d . . . . .
H29 H 0.331740 0.827947 0.327277 0.058 Uiso 1 1 calc R U . . .
C26 C 0.7844(15) 0.9993(8) 0.6771(7) 0.027(4) Uani 1 1 d . . . . .
H26 H 0.828268 0.994094 0.706344 0.033 Uiso 1 1 calc R U . . .
C44 C 0.0066(16) 0.5766(9) 0.7686(8) 0.034(4) Uani 1 1 d . . . . .
H44 H 0.007116 0.543032 0.790103 0.041 Uiso 1 1 calc R U . . .
C15 C 0.7129(15) 0.9566(7) 0.7883(7) 0.025(4) Uani 1 1 d . . . . .
C13 C 0.3983(14) 1.1142(7) 0.7305(7) 0.022(3) Uani 1 1 d . . . . .
C4 C 0.141(2) 1.3102(9) 0.7282(8) 0.040(5) Uani 1 1 d . . . . .
H4 H 0.104760 1.344856 0.736658 0.047 Uiso 1 1 calc R U . . .
C5 C 0.0937(14) 1.2685(8) 0.6967(8) 0.028(4) Uani 1 1 d . . . . .
H5 H 0.025926 1.274461 0.683615 0.033 Uiso 1 1 calc R U . . .
C43 C -0.0498(17) 0.5753(9) 0.7218(9) 0.037(5) Uani 1 1 d . . . . .
H43 H -0.086388 0.540536 0.711571 0.044 Uiso 1 1 calc R U . . .
C51 C -0.2875(18) 0.7535(11) 0.6195(10) 0.046(6) Uani 1 1 d . . . . .
H51 H -0.345091 0.728221 0.615275 0.055 Uiso 1 1 calc R U . . .
C49 C -0.2094(17) 0.8500(8) 0.6127(8) 0.033(4) Uani 1 1 d . . . . .
H49 H -0.213616 0.891068 0.604310 0.040 Uiso 1 1 calc R U . . .
C9 C 0.481(2) 1.2482(11) 0.5880(10) 0.046(4) Uani 1 1 d . U . . .
H9 H 0.506721 1.287535 0.586701 0.055 Uiso 1 1 calc R U . . .
C31 C 0.1982(17) 0.7093(8) 0.3512(8) 0.034(5) Uani 1 1 d . . . . .
H31 H 0.176714 0.672480 0.336647 0.041 Uiso 1 1 calc R U . . .
C32 C 0.1674(15) 0.7257(8) 0.3976(7) 0.026(4) Uani 1 1 d . . . . .
H32 H 0.123423 0.700517 0.414662 0.031 Uiso 1 1 calc R U . . .
C42 C -0.0517(16) 0.6240(9) 0.6914(9) 0.035(5) Uani 1 1 d . . . . .
H42 H -0.090077 0.623311 0.660133 0.042 Uiso 1 1 calc R U . . .
C34 C -0.0378(15) 0.8075(8) 0.4475(7) 0.028(4) Uani 1 1 d . . . . .
H34 H -0.023649 0.774163 0.427329 0.034 Uiso 1 1 calc R U . . .
C25 C 0.825(2) 1.0130(10) 0.6315(9) 0.045(5) Uani 1 1 d . . . . .
H25 H 0.896583 1.018395 0.630437 0.054 Uiso 1 1 calc R U . . .
C45 C 0.061(2) 0.6269(9) 0.7827(8) 0.040(5) Uani 1 1 d . . . . .
H45 H 0.097102 0.628263 0.814444 0.047 Uiso 1 1 calc R U . . .
C47 C -0.1092(16) 0.7656(7) 0.6420(7) 0.027(4) Uani 1 1 d . . . . .
C40 C 0.0797(14) 0.7153(8) 0.6132(7) 0.025(4) Uani 1 1 d . . . . .
C52 C -0.1966(17) 0.7304(8) 0.6374(9) 0.036(5) Uani 1 1 d . . . . .
H52 H -0.192609 0.689732 0.646898 0.043 Uiso 1 1 calc R U . . .
C3 C 0.2375(14) 1.3034(7) 0.7473(7) 0.022(3) Uani 1 1 d . . . . .
H3 H 0.266572 1.331592 0.770410 0.027 Uiso 1 1 calc R U . . .
C19 C 0.8542(17) 0.9824(9) 0.8430(9) 0.038(5) Uani 1 1 d . . . . .
H19 H 0.910454 1.007390 0.852124 0.046 Uiso 1 1 calc R U . . .
C11 C 0.4633(18) 1.1479(11) 0.5532(9) 0.042(4) Uani 1 1 d . U . . .
H11 H 0.477340 1.120031 0.527924 0.051 Uiso 1 1 calc R U . . .
C18 C 0.832(2) 0.9349(10) 0.8721(10) 0.046(6) Uani 1 1 d . . . . .
H18 H 0.877079 0.926043 0.900373 0.056 Uiso 1 1 calc R U . . .
C17 C 0.748(2) 0.8986(11) 0.8623(12) 0.053(7) Uani 1 1 d . . . . .
H17 H 0.732338 0.867283 0.884334 0.063 Uiso 1 1 calc R U . . .
C10 C 0.496(2) 1.2089(11) 0.5490(10) 0.046(4) Uani 1 1 d . U . . .
H10 H 0.526973 1.222033 0.519945 0.055 Uiso 1 1 calc R U . . .
C50 C -0.2966(19) 0.8143(11) 0.6072(9) 0.043(5) Uani 1 1 d . . . . .
H50 H -0.360043 0.830681 0.595513 0.051 Uiso 1 1 calc R U . . .
B2 B 0.517(2) 1.1290(11) 0.8205(9) 0.039(6) Uani 1 1 d . . . . .
H2A H 0.548693 1.158401 0.851313 0.046 Uiso 1 1 calc R U . . .
B5 B 0.4214(18) 1.0385(9) 0.7256(7) 0.026(4) Uani 1 1 d . . . . .
H5A H 0.390395 1.009021 0.694532 0.031 Uiso 1 1 calc R U . . .
B6 B 0.5181(17) 1.0933(8) 0.7166(8) 0.024(4) Uani 1 1 d . . . . .
H6A H 0.550294 1.099384 0.679250 0.028 Uiso 1 1 calc R U . . .
B13 B 0.0251(17) 0.6636(8) 0.5716(8) 0.025(3) Uani 1 1 d . U . . .
H13 H -0.051239 0.642973 0.575115 0.031 Uiso 1 1 calc R U . . .
B4 B 0.4380(19) 1.0121(9) 0.7864(10) 0.034(5) Uani 1 1 d . . . . .
H4A H 0.418990 0.964835 0.795071 0.041 Uiso 1 1 calc R U . . .
B12 B 0.0417(17) 0.7389(8) 0.5548(8) 0.026(3) Uani 1 1 d . U . . .
H12A H -0.026024 0.768118 0.546613 0.031 Uiso 1 1 calc R U . . .
B16 B 0.2588(17) 0.7253(9) 0.5653(8) 0.027(4) Uani 1 1 d . . . . .
H16A H 0.336040 0.745609 0.564194 0.033 Uiso 1 1 calc R U . . .
B11 B 0.1576(16) 0.7680(8) 0.5853(7) 0.021(3) Uani 1 1 d . U . . .
H11A H 0.166204 0.815766 0.596573 0.025 Uiso 1 1 calc R U . . .
B15 B 0.2157(16) 0.7073(8) 0.6215(7) 0.020(3) Uani 1 1 d . U . . .
H15 H 0.261462 0.715304 0.657516 0.024 Uiso 1 1 calc R U . . .
B14 B 0.1355(18) 0.6440(8) 0.6133(8) 0.027(3) Uani 1 1 d . U . . .
H14 H 0.129909 0.610794 0.644257 0.032 Uiso 1 1 calc R U . . .
B3 B 0.4175(15) 1.0739(9) 0.8292(9) 0.029(4) Uani 1 1 d . . . . .
H3A H 0.383887 1.067748 0.866178 0.035 Uiso 1 1 calc R U . . .
B17 B 0.2096(15) 0.6763(8) 0.5173(8) 0.023(4) Uani 1 1 d . . . . .
H17A H 0.252807 0.665031 0.483901 0.028 Uiso 1 1 calc R U . . .
B18 B 0.2473(17) 0.6499(8) 0.5788(7) 0.024(4) Uani 1 1 d . . . . .
H18A H 0.314051 0.619520 0.585664 0.029 Uiso 1 1 calc R U . . .
B20 B 0.0745(16) 0.6833(8) 0.5125(9) 0.027(4) Uani 1 1 d . . . . .
H20A H 0.029580 0.675575 0.476148 0.032 Uiso 1 1 calc R U . . .
B7 B 0.5948(19) 1.1005(9) 0.7729(10) 0.033(5) Uani 1 1 d . . . . .
H7 H 0.677624 1.110954 0.772294 0.039 Uiso 1 1 calc R U . . .
B19 B 0.1315(18) 0.6242(8) 0.5482(9) 0.029(5) Uani 1 1 d . . . . .
H19A H 0.123047 0.576823 0.535696 0.035 Uiso 1 1 calc R U . . .
B1 B 0.3905(18) 1.1366(10) 0.7913(8) 0.030(5) Uani 1 1 d . . . . .
H1 H 0.337135 1.171769 0.803342 0.036 Uiso 1 1 calc R U . . .
B8 B 0.545(2) 1.0501(10) 0.8186(8) 0.033(5) Uani 1 1 d . . . . .
H8A H 0.593804 1.027568 0.848542 0.040 Uiso 1 1 calc R U . . .
B9 B 0.4957(19) 1.1546(9) 0.7584(8) 0.029(5) Uani 1 1 d . . . . .
H9A H 0.511944 1.201981 0.748842 0.035 Uiso 1 1 calc R U . . .
B10 B 0.3462(19) 1.0665(10) 0.7711(9) 0.032(5) Uani 1 1 d . . . . .
H10A H 0.263358 1.055656 0.769865 0.039 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au5 Au4 2.9669(10) . ?
Au5 Au6 2.9844(11) . ?
Au5 S3 2.312(4) . ?
Au5 P2 2.247(4) . ?
Au2 Au3 2.9210(9) . ?
Au2 Au4 3.2955(9) . ?
Au2 Au7 3.2558(10) . ?
Au2 Au1 2.9950(9) . ?
Au2 S1 2.319(5) . ?
Au2 S4 2.327(5) . ?
Au3 Au4 3.0680(9) . ?
Au3 S4 2.331(4) . ?
Au3 P3 2.258(4) . ?
Au4 Au6 3.2479(11) . ?
Au4 S3 2.329(4) . ?
Au4 S4 2.323(4) . ?
Au7 Au1 3.0920(9) . ?
Au7 Au6 3.2790(10) . ?
Au7 Au8 3.1005(9) . ?
Au7 S1 2.316(4) . ?
Au7 S2 2.313(5) . ?
Au1 S1 2.322(4) . ?
Au1 P1 2.256(4) . ?
Au6 Au8 2.9356(11) . ?
Au6 S3 2.327(5) . ?
Au6 S2 2.328(5) . ?
Au8 S2 2.335(4) . ?
Au8 P4 2.257(4) . ?
P3 C27 1.823(17) . ?
P3 C39 1.877(18) . ?
P3 C33 1.83(2) . ?
P2 C14 1.89(2) . ?
P2 C21 1.792(18) . ?
P2 C15 1.855(17) . ?
P1 C1 1.821(17) . ?
P1 C7 1.82(2) . ?
P1 C13 1.874(18) . ?
P4 C41 1.813(19) . ?
P4 C47 1.81(2) . ?
P4 C40 1.84(2) . ?
C35 H35 0.9500 . ?
C35 C36 1.38(3) . ?
C35 C34 1.39(3) . ?
C46 H46 0.9500 . ?
C46 C41 1.39(3) . ?
C46 C45 1.35(3) . ?
C16 H16 0.9500 . ?
C16 C15 1.38(3) . ?
C16 C17 1.40(3) . ?
C1 C2 1.39(3) . ?
C1 C6 1.40(2) . ?
C14 B5 1.74(3) . ?
C14 B6 1.70(3) . ?
C14 B4 1.72(3) . ?
C14 B7 1.69(3) . ?
C14 B8 1.72(3) . ?
C24 H24 0.9500 . ?
C24 C23 1.38(3) . ?
C24 C25 1.37(3) . ?
C2 H2 0.9500 . ?
C2 C3 1.42(3) . ?
C7 C8 1.42(3) . ?
C7 C12 1.37(3) . ?
C37 H37 0.9500 . ?
C37 C38 1.43(3) . ?
C37 C36 1.41(3) . ?
C27 C28 1.33(3) . ?
C27 C32 1.41(2) . ?
C23 H23 0.9500 . ?
C23 C22 1.39(3) . ?
C38 H38 0.9500 . ?
C38 C33 1.37(3) . ?
C28 H28 0.9500 . ?
C28 C29 1.43(3) . ?
C36 H36 0.9500 . ?
C8 H8 0.9500 . ?
C8 C9 1.46(3) . ?
C39 B12 1.72(3) . ?
C39 B16 1.77(3) . ?
C39 B11 1.71(3) . ?
C39 B17 1.70(2) . ?
C39 B20 1.72(3) . ?
C20 H20 0.9500 . ?
C20 C15 1.37(3) . ?
C20 C19 1.41(3) . ?
C48 H48 0.9500 . ?
C48 C49 1.37(3) . ?
C48 C47 1.40(2) . ?
C30 H30 0.9500 . ?
C30 C29 1.40(3) . ?
C30 C31 1.35(3) . ?
C21 C22 1.41(3) . ?
C21 C26 1.39(3) . ?
C12 H12 0.9500 . ?
C12 C11 1.39(3) . ?
C41 C42 1.43(3) . ?
C6 H6 0.9500 . ?
C6 C5 1.39(3) . ?
C22 H22 0.9500 . ?
C33 C34 1.39(3) . ?
C29 H29 0.9500 . ?
C26 H26 0.9500 . ?
C26 C25 1.40(3) . ?
C44 H44 0.9500 . ?
C44 C43 1.42(3) . ?
C44 C45 1.38(3) . ?
C13 B5 1.73(3) . ?
C13 B6 1.71(3) . ?
C13 B1 1.71(3) . ?
C13 B9 1.71(3) . ?
C13 B10 1.70(3) . ?
C4 H4 0.9500 . ?
C4 C5 1.38(3) . ?
C4 C3 1.35(3) . ?
C5 H5 0.9500 . ?
C43 H43 0.9500 . ?
C43 C42 1.36(3) . ?
C51 H51 0.9500 . ?
C51 C52 1.37(3) . ?
C51 C50 1.41(3) . ?
C49 H49 0.9500 . ?
C49 C50 1.40(3) . ?
C9 H9 0.9500 . ?
C9 C10 1.39(4) . ?
C31 H31 0.9500 . ?
C31 C32 1.38(3) . ?
C32 H32 0.9500 . ?
C42 H42 0.9500 . ?
C34 H34 0.9500 . ?
C25 H25 0.9500 . ?
C45 H45 0.9500 . ?
C47 C52 1.40(3) . ?
C40 B13 1.73(2) . ?
C40 B12 1.70(3) . ?
C40 B11 1.77(3) . ?
C40 B15 1.80(3) . ?
C40 B14 1.76(3) . ?
C52 H52 0.9500 . ?
C3 H3 0.9500 . ?
C19 H19 0.9500 . ?
C19 C18 1.36(4) . ?
C11 H11 0.9500 . ?
C11 C10 1.44(4) . ?
C18 H18 0.9500 . ?
C18 C17 1.39(4) . ?
C17 H17 0.9500 . ?
C10 H10 0.9500 . ?
C50 H50 0.9500 . ?
B2 H2A 1.1200 . ?
B2 B3 1.83(4) . ?
B2 B7 1.81(4) . ?
B2 B1 1.80(3) . ?
B2 B8 1.81(3) . ?
B2 B9 1.76(3) . ?
B5 H5A 1.1200 . ?
B5 B6 1.80(3) . ?
B5 B4 1.73(3) . ?
B5 B10 1.74(3) . ?
B6 H6A 1.1200 . ?
B6 B7 1.77(3) . ?
B6 B9 1.81(3) . ?
B13 H13 1.1200 . ?
B13 B12 1.77(3) . ?
B13 B14 1.83(3) . ?
B13 B20 1.81(3) . ?
B13 B19 1.81(3) . ?
B4 H4A 1.1200 . ?
B4 B3 1.83(3) . ?
B4 B8 1.81(4) . ?
B4 B10 1.75(3) . ?
B12 H12A 1.1200 . ?
B12 B11 1.81(3) . ?
B12 B20 1.76(3) . ?
B16 H16A 1.1200 . ?
B16 B11 1.76(3) . ?
B16 B15 1.69(3) . ?
B16 B17 1.78(3) . ?
B16 B18 1.74(3) . ?
B11 H11A 1.1200 . ?
B11 B15 1.81(3) . ?
B15 H15 1.1200 . ?
B15 B14 1.78(3) . ?
B15 B18 1.79(3) . ?
B14 H14 1.1200 . ?
B14 B18 1.80(3) . ?
B14 B19 1.80(3) . ?
B3 H3A 1.1200 . ?
B3 B1 1.76(3) . ?
B3 B8 1.80(3) . ?
B3 B10 1.77(3) . ?
B17 H17A 1.1200 . ?
B17 B18 1.79(3) . ?
B17 B20 1.79(3) . ?
B17 B19 1.80(3) . ?
B18 H18A 1.1200 . ?
B18 B19 1.78(3) . ?
B20 H20A 1.1200 . ?
B20 B19 1.78(3) . ?
B7 H7 1.1200 . ?
B7 B8 1.82(3) . ?
B7 B9 1.81(3) . ?
B19 H19A 1.1200 . ?
B1 H1 1.1200 . ?
B1 B9 1.74(4) . ?
B1 B10 1.75(3) . ?
B8 H8A 1.1200 . ?
B9 H9A 1.1200 . ?
B10 H10A 1.1200 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Au4 Au5 Au6 66.15(2) . . ?
S3 Au5 Au4 50.51(10) . . ?
S3 Au5 Au6 50.19(12) . . ?
P2 Au5 Au4 124.63(11) . . ?
P2 Au5 Au6 135.25(12) . . ?
P2 Au5 S3 172.73(18) . . ?
Au3 Au2 Au4 58.78(2) . . ?
Au3 Au2 Au7 115.99(3) . . ?
Au3 Au2 Au1 174.83(3) . . ?
Au7 Au2 Au4 89.81(2) . . ?
Au1 Au2 Au4 121.16(3) . . ?
Au1 Au2 Au7 59.12(2) . . ?
S1 Au2 Au3 125.92(10) . . ?
S1 Au2 Au4 134.35(10) . . ?
S1 Au2 Au7 45.33(10) . . ?
S1 Au2 Au1 49.85(10) . . ?
S1 Au2 S4 177.12(14) . . ?
S4 Au2 Au3 51.22(10) . . ?
S4 Au2 Au4 44.82(10) . . ?
S4 Au2 Au7 134.36(10) . . ?
S4 Au2 Au1 132.97(10) . . ?
Au2 Au3 Au4 66.72(2) . . ?
S4 Au3 Au2 51.10(11) . . ?
S4 Au3 Au4 48.64(10) . . ?
P3 Au3 Au2 127.94(12) . . ?
P3 Au3 Au4 133.14(11) . . ?
P3 Au3 S4 178.01(15) . . ?
Au5 Au4 Au2 115.90(3) . . ?
Au5 Au4 Au3 170.11(3) . . ?
Au5 Au4 Au6 57.18(2) . . ?
Au3 Au4 Au2 54.51(2) . . ?
Au3 Au4 Au6 117.24(3) . . ?
Au6 Au4 Au2 89.80(3) . . ?
S3 Au4 Au5 50.02(10) . . ?
S3 Au4 Au2 135.29(12) . . ?
S3 Au4 Au3 133.56(11) . . ?
S3 Au4 Au6 45.75(12) . . ?
S4 Au4 Au5 127.55(10) . . ?
S4 Au4 Au2 44.92(11) . . ?
S4 Au4 Au3 48.87(10) . . ?
S4 Au4 Au6 134.03(11) . . ?
S4 Au4 S3 177.55(14) . . ?
Au2 Au7 Au6 89.95(3) . . ?
Au1 Au7 Au2 56.23(2) . . ?
Au1 Au7 Au6 117.54(3) . . ?
Au1 Au7 Au8 171.80(3) . . ?
Au8 Au7 Au2 118.40(3) . . ?
Au8 Au7 Au6 54.71(2) . . ?
S1 Au7 Au2 45.42(11) . . ?
S1 Au7 Au1 48.27(10) . . ?
S1 Au7 Au6 135.04(11) . . ?
S1 Au7 Au8 133.87(10) . . ?
S2 Au7 Au2 134.42(14) . . ?
S2 Au7 Au1 129.41(11) . . ?
S2 Au7 Au6 45.24(13) . . ?
S2 Au7 Au8 48.46(11) . . ?
S2 Au7 S1 177.66(15) . . ?
Au2 Au1 Au7 64.65(2) . . ?
S1 Au1 Au2 49.77(11) . . ?
S1 Au1 Au7 48.09(10) . . ?
P1 Au1 Au2 127.28(12) . . ?
P1 Au1 Au7 136.12(11) . . ?
P1 Au1 S1 174.89(16) . . ?
Au5 Au6 Au4 56.67(2) . . ?
Au5 Au6 Au7 118.67(3) . . ?
Au4 Au6 Au7 90.23(2) . . ?
Au8 Au6 Au5 174.19(3) . . ?
Au8 Au6 Au4 117.52(3) . . ?
Au8 Au6 Au7 59.55(2) . . ?
S3 Au6 Au5 49.75(10) . . ?
S3 Au6 Au4 45.79(10) . . ?
S3 Au6 Au7 135.33(11) . . ?
S3 Au6 Au8 126.86(10) . . ?
S3 Au6 S2 177.90(15) . . ?
S2 Au6 Au5 132.35(11) . . ?
S2 Au6 Au4 134.78(11) . . ?
S2 Au6 Au7 44.85(11) . . ?
S2 Au6 Au8 51.08(11) . . ?
Au6 Au8 Au7 65.74(2) . . ?
S2 Au8 Au7 47.85(11) . . ?
S2 Au8 Au6 50.88(13) . . ?
P4 Au8 Au7 132.69(11) . . ?
P4 Au8 Au6 131.76(13) . . ?
P4 Au8 S2 177.27(18) . . ?
Au5 S3 Au4 79.47(12) . . ?
Au5 S3 Au6 80.07(13) . . ?
Au6 S3 Au4 88.46(14) . . ?
Au2 S1 Au1 80.38(14) . . ?
Au7 S1 Au2 89.26(14) . . ?
Au7 S1 Au1 83.64(13) . . ?
Au7 S2 Au6 89.91(18) . . ?
Au7 S2 Au8 83.69(16) . . ?
Au6 S2 Au8 78.03(15) . . ?
Au2 S4 Au3 77.67(14) . . ?
Au4 S4 Au2 90.26(16) . . ?
Au4 S4 Au3 82.49(13) . . ?
C27 P3 Au3 112.1(6) . . ?
C27 P3 C39 110.3(8) . . ?
C27 P3 C33 108.7(8) . . ?
C39 P3 Au3 110.0(5) . . ?
C33 P3 Au3 113.7(6) . . ?
C33 P3 C39 101.4(8) . . ?
C14 P2 Au5 114.3(6) . . ?
C21 P2 Au5 106.3(6) . . ?
C21 P2 C14 106.7(9) . . ?
C21 P2 C15 111.4(10) . . ?
C15 P2 Au5 114.4(6) . . ?
C15 P2 C14 103.6(8) . . ?
C1 P1 Au1 114.5(6) . . ?
C1 P1 C13 107.8(8) . . ?
C7 P1 Au1 109.0(7) . . ?
C7 P1 C1 107.1(9) . . ?
C7 P1 C13 106.0(9) . . ?
C13 P1 Au1 112.0(5) . . ?
C41 P4 Au8 113.1(7) . . ?
C41 P4 C40 104.4(9) . . ?
C47 P4 Au8 110.3(6) . . ?
C47 P4 C41 111.0(9) . . ?
C47 P4 C40 104.7(8) . . ?
C40 P4 Au8 112.9(6) . . ?
C36 C35 H35 119.2 . . ?
C36 C35 C34 121.6(19) . . ?
C34 C35 H35 119.2 . . ?
C41 C46 H46 119.1 . . ?
C45 C46 H46 119.1 . . ?
C45 C46 C41 121.8(19) . . ?
C15 C16 H16 120.5 . . ?
C15 C16 C17 119(2) . . ?
C17 C16 H16 120.5 . . ?
C2 C1 P1 125.4(15) . . ?
C2 C1 C6 119.4(16) . . ?
C6 C1 P1 114.8(13) . . ?
B5 C14 P2 113.8(12) . . ?
B6 C14 P2 120.2(15) . . ?
B6 C14 B5 63.1(12) . . ?
B6 C14 B4 113.5(16) . . ?
B6 C14 B8 115.6(15) . . ?
B4 C14 P2 112.5(12) . . ?
B4 C14 B5 60.2(13) . . ?
B4 C14 B8 63.6(15) . . ?
B7 C14 P2 122.5(14) . . ?
B7 C14 B5 115.4(15) . . ?
B7 C14 B6 62.8(12) . . ?
B7 C14 B4 116.7(17) . . ?
B7 C14 B8 64.5(14) . . ?
B8 C14 P2 118.1(14) . . ?
B8 C14 B5 113.6(17) . . ?
C23 C24 H24 119.8 . . ?
C25 C24 H24 119.8 . . ?
C25 C24 C23 120(2) . . ?
C1 C2 H2 120.4 . . ?
C1 C2 C3 119.3(17) . . ?
C3 C2 H2 120.4 . . ?
C8 C7 P1 119.9(17) . . ?
C12 C7 P1 117.2(15) . . ?
C12 C7 C8 123(2) . . ?
C38 C37 H37 121.3 . . ?
C36 C37 H37 121.3 . . ?
C36 C37 C38 117.5(17) . . ?
C28 C27 P3 115.4(13) . . ?
C28 C27 C32 119.1(17) . . ?
C32 C27 P3 125.5(15) . . ?
C24 C23 H23 121.0 . . ?
C24 C23 C22 118.1(18) . . ?
C22 C23 H23 121.0 . . ?
C37 C38 H38 120.1 . . ?
C33 C38 C37 119.9(16) . . ?
C33 C38 H38 120.1 . . ?
C27 C28 H28 118.5 . . ?
C27 C28 C29 122.9(19) . . ?
C29 C28 H28 118.5 . . ?
C35 C36 C37 120.5(19) . . ?
C35 C36 H36 119.8 . . ?
C37 C36 H36 119.8 . . ?
C7 C8 H8 122.0 . . ?
C7 C8 C9 116(2) . . ?
C9 C8 H8 122.0 . . ?
B12 C39 P3 118.2(10) . . ?
B12 C39 B16 111.4(14) . . ?
B12 C39 B20 61.4(12) . . ?
B16 C39 P3 116.7(12) . . ?
B11 C39 P3 110.6(11) . . ?
B11 C39 B12 63.7(12) . . ?
B11 C39 B16 60.7(12) . . ?
B11 C39 B20 114.7(15) . . ?
B17 C39 P3 122.4(13) . . ?
B17 C39 B12 113.3(13) . . ?
B17 C39 B16 61.8(11) . . ?
B17 C39 B11 113.9(13) . . ?
B17 C39 B20 62.9(11) . . ?
B20 C39 P3 124.7(12) . . ?
B20 C39 B16 112.2(13) . . ?
C15 C20 H20 121.4 . . ?
C15 C20 C19 117.3(19) . . ?
C19 C20 H20 121.4 . . ?
C49 C48 H48 119.5 . . ?
C49 C48 C47 121(2) . . ?
C47 C48 H48 119.5 . . ?
C29 C30 H30 118.4 . . ?
C31 C30 H30 118.4 . . ?
C31 C30 C29 123(2) . . ?
C22 C21 P2 118.2(15) . . ?
C26 C21 P2 125.0(15) . . ?
C26 C21 C22 116.3(17) . . ?
C7 C12 H12 119.8 . . ?
C7 C12 C11 120(2) . . ?
C11 C12 H12 119.8 . . ?
C46 C41 P4 117.8(14) . . ?
C46 C41 C42 117.8(17) . . ?
C42 C41 P4 124.0(15) . . ?
C1 C6 H6 119.8 . . ?
C5 C6 C1 120.4(16) . . ?
C5 C6 H6 119.8 . . ?
C23 C22 C21 123.5(18) . . ?
C23 C22 H22 118.2 . . ?
C21 C22 H22 118.2 . . ?
C38 C33 P3 116.1(14) . . ?
C38 C33 C34 122.5(19) . . ?
C34 C33 P3 120.8(16) . . ?
C28 C29 H29 122.5 . . ?
C30 C29 C28 115(2) . . ?
C30 C29 H29 122.5 . . ?
C21 C26 H26 119.6 . . ?
C21 C26 C25 120.7(18) . . ?
C25 C26 H26 119.6 . . ?
C43 C44 H44 120.2 . . ?
C45 C44 H44 120.2 . . ?
C45 C44 C43 119.6(17) . . ?
C16 C15 P2 113.4(15) . . ?
C20 C15 P2 122.3(15) . . ?
C20 C15 C16 123.8(17) . . ?
B5 C13 P1 113.7(11) . . ?
B6 C13 P1 118.6(12) . . ?
B6 C13 B5 63.0(12) . . ?
B1 C13 P1 121.3(12) . . ?
B1 C13 B5 112.5(14) . . ?
B1 C13 B6 113.6(14) . . ?
B9 C13 P1 123.0(12) . . ?
B9 C13 B5 115.1(14) . . ?
B9 C13 B6 64.0(12) . . ?
B9 C13 B1 61.2(13) . . ?
B10 C13 P1 116.1(13) . . ?
B10 C13 B5 60.8(12) . . ?
B10 C13 B6 112.5(14) . . ?
B10 C13 B1 61.8(13) . . ?
B10 C13 B9 112.3(15) . . ?
C5 C4 H4 118.9 . . ?
C3 C4 H4 118.9 . . ?
C3 C4 C5 122.2(19) . . ?
C6 C5 H5 120.6 . . ?
C4 C5 C6 118.9(19) . . ?
C4 C5 H5 120.6 . . ?
C44 C43 H43 120.0 . . ?
C42 C43 C44 120.0(19) . . ?
C42 C43 H43 120.0 . . ?
C52 C51 H51 119.7 . . ?
C52 C51 C50 121(2) . . ?
C50 C51 H51 119.7 . . ?
C48 C49 H49 119.7 . . ?
C48 C49 C50 120.6(18) . . ?
C50 C49 H49 119.7 . . ?
C8 C9 H9 119.5 . . ?
C10 C9 C8 121(2) . . ?
C10 C9 H9 119.5 . . ?
C30 C31 H31 120.3 . . ?
C30 C31 C32 119.4(17) . . ?
C32 C31 H31 120.3 . . ?
C27 C32 H32 119.9 . . ?
C31 C32 C27 120.3(18) . . ?
C31 C32 H32 119.9 . . ?
C41 C42 H42 120.0 . . ?
C43 C42 C41 120(2) . . ?
C43 C42 H42 120.0 . . ?
C35 C34 H34 121.1 . . ?
C33 C34 C35 117.8(19) . . ?
C33 C34 H34 121.1 . . ?
C24 C25 C26 121(2) . . ?
C24 C25 H25 119.5 . . ?
C26 C25 H25 119.5 . . ?
C46 C45 C44 120(2) . . ?
C46 C45 H45 119.8 . . ?
C44 C45 H45 119.8 . . ?
C48 C47 P4 115.8(17) . . ?
C52 C47 P4 125.8(14) . . ?
C52 C47 C48 118(2) . . ?
B13 C40 P4 121.9(13) . . ?
B13 C40 B11 114.0(14) . . ?
B13 C40 B15 112.4(14) . . ?
B13 C40 B14 63.2(12) . . ?
B12 C40 P4 120.2(13) . . ?
B12 C40 B13 62.0(11) . . ?
B12 C40 B11 63.0(11) . . ?
B12 C40 B15 112.2(14) . . ?
B12 C40 B14 112.6(14) . . ?
B11 C40 P4 115.8(11) . . ?
B11 C40 B15 61.1(11) . . ?
B15 C40 P4 116.7(11) . . ?
B14 C40 P4 120.6(13) . . ?
B14 C40 B11 110.8(14) . . ?
B14 C40 B15 59.8(11) . . ?
C51 C52 C47 121.3(18) . . ?
C51 C52 H52 119.4 . . ?
C47 C52 H52 119.4 . . ?
C2 C3 H3 120.2 . . ?
C4 C3 C2 119.6(17) . . ?
C4 C3 H3 120.2 . . ?
C20 C19 H19 120.3 . . ?
C18 C19 C20 119.3(19) . . ?
C18 C19 H19 120.3 . . ?
C12 C11 H11 119.9 . . ?
C12 C11 C10 120(2) . . ?
C10 C11 H11 119.9 . . ?
C19 C18 H18 118.4 . . ?
C19 C18 C17 123(2) . . ?
C17 C18 H18 118.4 . . ?
C16 C17 H17 121.3 . . ?
C18 C17 C16 117(3) . . ?
C18 C17 H17 121.3 . . ?
C9 C10 C11 119(2) . . ?
C9 C10 H10 120.5 . . ?
C11 C10 H10 120.5 . . ?
C51 C50 H50 120.9 . . ?
C49 C50 C51 118(2) . . ?
C49 C50 H50 120.9 . . ?
B3 B2 H2A 123.2 . . ?
B7 B2 H2A 121.4 . . ?
B7 B2 B3 107.3(15) . . ?
B7 B2 B8 60.5(12) . . ?
B1 B2 H2A 124.0 . . ?
B1 B2 B3 58.0(13) . . ?
B1 B2 B7 106.4(16) . . ?
B1 B2 B8 105.4(16) . . ?
B8 B2 H2A 122.0 . . ?
B8 B2 B3 59.4(13) . . ?
B9 B2 H2A 122.0 . . ?
B9 B2 B3 105.8(16) . . ?
B9 B2 B7 60.9(14) . . ?
B9 B2 B1 58.4(14) . . ?
B9 B2 B8 108.2(15) . . ?
C14 B5 H5A 126.2 . . ?
C14 B5 B6 57.4(11) . . ?
C14 B5 B10 104.1(14) . . ?
C13 B5 C14 100.2(13) . . ?
C13 B5 H5A 125.4 . . ?
C13 B5 B6 58.0(11) . . ?
C13 B5 B4 106.0(14) . . ?
C13 B5 B10 58.7(12) . . ?
B6 B5 H5A 122.3 . . ?
B4 B5 C14 59.5(12) . . ?
B4 B5 H5A 120.9 . . ?
B4 B5 B6 108.1(15) . . ?
B4 B5 B10 60.6(12) . . ?
B10 B5 H5A 122.5 . . ?
B10 B5 B6 106.8(15) . . ?
C14 B6 C13 102.6(15) . . ?
C14 B6 B5 59.4(11) . . ?
C14 B6 H6A 125.1 . . ?
C14 B6 B7 58.5(11) . . ?
C14 B6 B9 104.2(14) . . ?
C13 B6 B5 59.1(11) . . ?
C13 B6 H6A 124.7 . . ?
C13 B6 B7 106.0(15) . . ?
C13 B6 B9 57.8(12) . . ?
B5 B6 H6A 121.1 . . ?
B5 B6 B9 107.0(16) . . ?
B7 B6 B5 108.8(14) . . ?
B7 B6 H6A 121.2 . . ?
B7 B6 B9 60.7(11) . . ?
B9 B6 H6A 123.0 . . ?
C40 B13 H13 124.4 . . ?
C40 B13 B12 58.0(11) . . ?
C40 B13 B14 59.2(11) . . ?
C40 B13 B20 103.9(13) . . ?
C40 B13 B19 104.5(15) . . ?
B12 B13 H13 123.0 . . ?
B12 B13 B14 106.3(13) . . ?
B12 B13 B20 58.9(11) . . ?
B12 B13 B19 105.6(15) . . ?
B14 B13 H13 122.3 . . ?
B20 B13 H13 123.5 . . ?
B20 B13 B14 106.0(15) . . ?
B20 B13 B19 58.9(12) . . ?
B19 B13 H13 123.4 . . ?
B19 B13 B14 59.1(13) . . ?
C14 B4 B5 60.4(13) . . ?
C14 B4 H4A 124.8 . . ?
C14 B4 B3 103.6(15) . . ?
C14 B4 B8 58.2(12) . . ?
C14 B4 B10 104.3(15) . . ?
B5 B4 H4A 120.1 . . ?
B5 B4 B3 108.2(15) . . ?
B5 B4 B8 109.4(16) . . ?
B5 B4 B10 59.8(14) . . ?
B3 B4 H4A 123.2 . . ?
B8 B4 H4A 121.7 . . ?
B8 B4 B3 59.3(13) . . ?
B10 B4 H4A 123.3 . . ?
B10 B4 B3 59.3(12) . . ?
B10 B4 B8 106.7(16) . . ?
C39 B12 B13 107.5(15) . . ?
C39 B12 H12A 124.5 . . ?
C39 B12 B11 57.8(11) . . ?
C39 B12 B20 59.3(12) . . ?
C40 B12 C39 103.9(15) . . ?
C40 B12 B13 60.0(11) . . ?
C40 B12 H12A 123.3 . . ?
C40 B12 B11 60.3(11) . . ?
C40 B12 B20 107.5(14) . . ?
B13 B12 H12A 120.1 . . ?
B13 B12 B11 110.2(14) . . ?
B11 B12 H12A 121.2 . . ?
B20 B12 B13 61.6(12) . . ?
B20 B12 H12A 121.2 . . ?
B20 B12 B11 108.1(15) . . ?
C39 B16 H16A 125.3 . . ?
C39 B16 B17 57.4(11) . . ?
B11 B16 C39 58.0(11) . . ?
B11 B16 H16A 119.8 . . ?
B11 B16 B17 107.9(15) . . ?
B15 B16 C39 107.6(16) . . ?
B15 B16 H16A 118.7 . . ?
B15 B16 B11 63.5(12) . . ?
B15 B16 B17 111.4(15) . . ?
B15 B16 B18 62.8(12) . . ?
B17 B16 H16A 121.6 . . ?
B18 B16 C39 106.1(14) . . ?
B18 B16 H16A 119.6 . . ?
B18 B16 B11 112.9(16) . . ?
B18 B16 B17 61.1(11) . . ?
C39 B11 C40 101.5(13) . . ?
C39 B11 B12 58.5(11) . . ?
C39 B11 B16 61.2(11) . . ?
C39 B11 H11A 124.2 . . ?
C39 B11 B15 104.7(13) . . ?
C40 B11 B12 56.7(10) . . ?
C40 B11 H11A 125.5 . . ?
C40 B11 B15 60.5(10) . . ?
B12 B11 H11A 122.5 . . ?
B12 B11 B15 106.6(12) . . ?
B16 B11 C40 103.8(13) . . ?
B16 B11 B12 107.7(14) . . ?
B16 B11 H11A 122.7 . . ?
B16 B11 B15 56.5(11) . . ?
B15 B11 H11A 123.0 . . ?
C40 B15 B11 58.4(11) . . ?
C40 B15 H15 124.5 . . ?
B16 B15 C40 104.9(14) . . ?
B16 B15 B11 60.1(11) . . ?
B16 B15 H15 122.3 . . ?
B16 B15 B14 108.3(15) . . ?
B16 B15 B18 60.0(11) . . ?
B11 B15 H15 121.7 . . ?
B14 B15 C40 59.0(11) . . ?
B14 B15 B11 107.9(15) . . ?
B14 B15 H15 121.2 . . ?
B14 B15 B18 60.5(12) . . ?
B18 B15 C40 105.4(13) . . ?
B18 B15 B11 108.1(13) . . ?
B18 B15 H15 122.0 . . ?
C40 B14 B13 57.6(11) . . ?
C40 B14 B15 61.2(11) . . ?
C40 B14 H14 124.0 . . ?
C40 B14 B18 106.8(13) . . ?
C40 B14 B19 103.7(14) . . ?
B13 B14 H14 121.6 . . ?
B15 B14 B13 109.0(14) . . ?
B15 B14 H14 120.6 . . ?
B15 B14 B18 60.1(11) . . ?
B15 B14 B19 107.3(14) . . ?
B18 B14 B13 108.5(15) . . ?
B18 B14 H14 121.6 . . ?
B19 B14 B13 59.8(12) . . ?
B19 B14 H14 123.6 . . ?
B19 B14 B18 59.6(12) . . ?
B2 B3 B4 107.4(15) . . ?
B2 B3 H3A 121.6 . . ?
B4 B3 H3A 122.8 . . ?
B1 B3 B2 60.3(13) . . ?
B1 B3 B4 106.3(17) . . ?
B1 B3 H3A 122.0 . . ?
B1 B3 B8 107.7(17) . . ?
B1 B3 B10 59.6(13) . . ?
B8 B3 B2 60.0(12) . . ?
B8 B3 B4 60.0(12) . . ?
B8 B3 H3A 122.0 . . ?
B10 B3 B2 107.3(17) . . ?
B10 B3 B4 58.2(13) . . ?
B10 B3 H3A 123.0 . . ?
B10 B3 B8 106.4(16) . . ?
C39 B17 B16 60.8(11) . . ?
C39 B17 H17A 123.0 . . ?
C39 B17 B18 106.6(15) . . ?
C39 B17 B20 59.0(11) . . ?
C39 B17 B19 104.7(15) . . ?
B16 B17 H17A 122.3 . . ?
B16 B17 B18 58.3(11) . . ?
B16 B17 B20 108.3(15) . . ?
B16 B17 B19 105.3(16) . . ?
B18 B17 H17A 122.2 . . ?
B18 B17 B19 59.6(12) . . ?
B20 B17 H17A 121.3 . . ?
B20 B17 B18 108.2(16) . . ?
B20 B17 B19 59.4(11) . . ?
B19 B17 H17A 123.9 . . ?
B16 B18 B15 57.2(11) . . ?
B16 B18 B14 105.3(15) . . ?
B16 B18 B17 60.6(11) . . ?
B16 B18 H18A 123.2 . . ?
B16 B18 B19 107.6(14) . . ?
B15 B18 B14 59.5(11) . . ?
B15 B18 B17 106.5(13) . . ?
B15 B18 H18A 123.3 . . ?
B14 B18 H18A 122.4 . . ?
B17 B18 B14 107.9(15) . . ?
B17 B18 H18A 121.4 . . ?
B19 B18 B15 107.3(15) . . ?
B19 B18 B14 60.2(12) . . ?
B19 B18 B17 60.4(11) . . ?
B19 B18 H18A 121.4 . . ?
C39 B20 B13 105.8(14) . . ?
C39 B20 B12 59.3(11) . . ?
C39 B20 B17 58.1(10) . . ?
C39 B20 H20A 124.4 . . ?
C39 B20 B19 104.9(15) . . ?
B13 B20 H20A 121.5 . . ?
B12 B20 B13 59.4(11) . . ?
B12 B20 B17 107.6(15) . . ?
B12 B20 H20A 122.1 . . ?
B12 B20 B19 107.3(16) . . ?
B17 B20 B13 109.3(15) . . ?
B17 B20 H20A 121.3 . . ?
B19 B20 B13 60.6(12) . . ?
B19 B20 B17 60.6(12) . . ?
B19 B20 H20A 122.3 . . ?
C14 B7 B2 105.0(18) . . ?
C14 B7 B6 58.8(12) . . ?
C14 B7 H7 124.5 . . ?
C14 B7 B8 58.5(12) . . ?
C14 B7 B9 104.5(16) . . ?
B2 B7 H7 122.6 . . ?
B2 B7 B8 59.9(14) . . ?
B2 B7 B9 58.3(13) . . ?
B6 B7 B2 108.1(16) . . ?
B6 B7 H7 121.0 . . ?
B6 B7 B8 107.5(16) . . ?
B6 B7 B9 60.8(12) . . ?
B8 B7 H7 122.4 . . ?
B9 B7 H7 123.4 . . ?
B9 B7 B8 105.7(18) . . ?
B13 B19 H19A 120.4 . . ?
B14 B19 B13 61.1(12) . . ?
B14 B19 B17 107.7(15) . . ?
B14 B19 H19A 121.5 . . ?
B17 B19 B13 108.8(13) . . ?
B17 B19 H19A 122.0 . . ?
B18 B19 B13 110.2(15) . . ?
B18 B19 B14 60.3(13) . . ?
B18 B19 B17 60.0(12) . . ?
B18 B19 H19A 120.7 . . ?
B20 B19 B13 60.5(12) . . ?
B20 B19 B14 108.8(14) . . ?
B20 B19 B17 60.0(11) . . ?
B20 B19 B18 109.1(14) . . ?
B20 B19 H19A 121.2 . . ?
C13 B1 B2 105.8(17) . . ?
C13 B1 B3 106.8(15) . . ?
C13 B1 H1 123.9 . . ?
C13 B1 B9 59.2(12) . . ?
C13 B1 B10 58.8(12) . . ?
B2 B1 H1 121.6 . . ?
B3 B1 B2 61.7(13) . . ?
B3 B1 H1 120.6 . . ?
B9 B1 B2 59.7(14) . . ?
B9 B1 B3 109.8(15) . . ?
B9 B1 H1 121.3 . . ?
B9 B1 B10 108.3(17) . . ?
B10 B1 B2 109.2(16) . . ?
B10 B1 B3 60.6(13) . . ?
B10 B1 H1 121.3 . . ?
C14 B8 B2 103.7(16) . . ?
C14 B8 B4 58.2(12) . . ?
C14 B8 B3 104.7(17) . . ?
C14 B8 B7 57.0(12) . . ?
C14 B8 H8A 125.7 . . ?
B2 B8 B4 108.6(18) . . ?
B2 B8 B7 59.7(14) . . ?
B2 B8 H8A 122.1 . . ?
B4 B8 B7 106.2(16) . . ?
B4 B8 H8A 121.6 . . ?
B3 B8 B2 60.7(14) . . ?
B3 B8 B4 60.8(13) . . ?
B3 B8 B7 107.7(17) . . ?
B3 B8 H8A 121.6 . . ?
B7 B8 H8A 122.8 . . ?
C13 B9 B2 107.8(17) . . ?
C13 B9 B6 58.2(11) . . ?
C13 B9 B7 104.5(14) . . ?
C13 B9 B1 59.6(12) . . ?
C13 B9 H9A 123.8 . . ?
B2 B9 B6 108.2(14) . . ?
B2 B9 B7 60.8(14) . . ?
B2 B9 H9A 120.4 . . ?
B6 B9 H9A 122.7 . . ?
B7 B9 B6 58.5(12) . . ?
B7 B9 H9A 122.7 . . ?
B1 B9 B2 61.9(14) . . ?
B1 B9 B6 107.7(15) . . ?
B1 B9 B7 109.1(16) . . ?
B1 B9 H9A 120.5 . . ?
C13 B10 B5 60.5(12) . . ?
C13 B10 B4 106.6(17) . . ?
C13 B10 B3 106.6(15) . . ?
C13 B10 B1 59.4(12) . . ?
C13 B10 H10A 123.5 . . ?
B5 B10 B4 59.6(13) . . ?
B5 B10 B3 110.7(17) . . ?
B5 B10 B1 110.3(17) . . ?
B5 B10 H10A 120.1 . . ?
B4 B10 B3 62.6(14) . . ?
B4 B10 B1 110.0(17) . . ?
B4 B10 H10A 121.1 . . ?
B3 B10 H10A 120.7 . . ?
B1 B10 B3 59.8(12) . . ?
B1 B10 H10A 120.7 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Au5 P2 C14 B5 -31.1(15) . . . . ?
Au5 P2 C14 B6 -102.8(12) . . . . ?
Au5 P2 C14 B4 34.9(15) . . . . ?
Au5 P2 C14 B7 -177.9(14) . . . . ?
Au5 P2 C14 B8 105.9(13) . . . . ?
Au5 P2 C21 C22 50.2(15) . . . . ?
Au5 P2 C21 C26 -122.4(14) . . . . ?
Au5 P2 C15 C16 -24.8(17) . . . . ?
Au5 P2 C15 C20 162.2(13) . . . . ?
Au3 P3 C27 C28 -24.3(17) . . . . ?
Au3 P3 C27 C32 156.0(15) . . . . ?
Au3 P3 C39 B12 109.3(12) . . . . ?
Au3 P3 C39 B16 -27.9(14) . . . . ?
Au3 P3 C39 B11 38.8(12) . . . . ?
Au3 P3 C39 B17 -100.0(12) . . . . ?
Au3 P3 C39 B20 -177.5(12) . . . . ?
Au3 P3 C33 C38 -19.5(16) . . . . ?
Au3 P3 C33 C34 169.1(12) . . . . ?
Au1 P1 C1 C2 167.9(15) . . . . ?
Au1 P1 C1 C6 -19.9(16) . . . . ?
Au1 P1 C7 C8 148.5(17) . . . . ?
Au1 P1 C7 C12 -29.9(19) . . . . ?
Au1 P1 C13 B5 26.7(15) . . . . ?
Au1 P1 C13 B6 97.7(11) . . . . ?
Au1 P1 C13 B1 -112.4(13) . . . . ?
Au1 P1 C13 B9 173.7(13) . . . . ?
Au1 P1 C13 B10 -41.0(14) . . . . ?
Au8 P4 C41 C46 -13(2) . . . . ?
Au8 P4 C41 C42 174.3(17) . . . . ?
Au8 P4 C47 C48 27.8(18) . . . . ?
Au8 P4 C47 C52 -146.5(17) . . . . ?
Au8 P4 C40 B13 -172.0(11) . . . . ?
Au8 P4 C40 B12 -98.1(12) . . . . ?
Au8 P4 C40 B11 -25.7(14) . . . . ?
Au8 P4 C40 B15 43.3(12) . . . . ?
Au8 P4 C40 B14 112.4(12) . . . . ?
P3 C27 C28 C29 -178(2) . . . . ?
P3 C27 C32 C31 -179.3(15) . . . . ?
P3 C39 B12 C40 -141.2(11) . . . . ?
P3 C39 B12 B13 156.3(12) . . . . ?
P3 C39 B12 B11 -100.5(13) . . . . ?
P3 C39 B12 B20 116.4(14) . . . . ?
P3 C39 B16 B11 99.8(13) . . . . ?
P3 C39 B16 B15 141.1(12) . . . . ?
P3 C39 B16 B17 -114.3(14) . . . . ?
P3 C39 B16 B18 -152.9(13) . . . . ?
P3 C39 B11 C40 150.6(11) . . . . ?
P3 C39 B11 B12 112.1(12) . . . . ?
P3 C39 B11 B16 -109.8(13) . . . . ?
P3 C39 B11 B15 -147.2(11) . . . . ?
P3 C39 B17 B16 105.3(15) . . . . ?
P3 C39 B17 B18 142.7(13) . . . . ?
P3 C39 B17 B20 -115.7(15) . . . . ?
P3 C39 B17 B19 -155.2(13) . . . . ?
P3 C39 B20 B13 -144.6(13) . . . . ?
P3 C39 B20 B12 -106.1(15) . . . . ?
P3 C39 B20 B17 112.2(16) . . . . ?
P3 C39 B20 B19 152.4(13) . . . . ?
P3 C33 C34 C35 170.3(13) . . . . ?
P2 C14 B5 C13 -154.1(12) . . . . ?
P2 C14 B5 B6 -113.2(16) . . . . ?
P2 C14 B5 B4 103.2(14) . . . . ?
P2 C14 B5 B10 145.8(13) . . . . ?
P2 C14 B6 C13 145.2(12) . . . . ?
P2 C14 B6 B5 103.2(14) . . . . ?
P2 C14 B6 B7 -113.6(16) . . . . ?
P2 C14 B6 B9 -155.3(13) . . . . ?
P2 C14 B4 B5 -105.4(14) . . . . ?
P2 C14 B4 B3 151.1(13) . . . . ?
P2 C14 B4 B8 111.3(15) . . . . ?
P2 C14 B4 B10 -147.6(14) . . . . ?
P2 C14 B7 B2 -147.6(14) . . . . ?
P2 C14 B7 B6 110.1(18) . . . . ?
P2 C14 B7 B8 -108.3(18) . . . . ?
P2 C14 B7 B9 151.9(15) . . . . ?
P2 C14 B8 B2 153.8(14) . . . . ?
P2 C14 B8 B4 -102.6(15) . . . . ?
P2 C14 B8 B3 -143.4(13) . . . . ?
P2 C14 B8 B7 114.9(16) . . . . ?
P2 C21 C22 C23 -172.4(15) . . . . ?
P2 C21 C26 C25 173.8(15) . . . . ?
P1 C1 C2 C3 177.9(14) . . . . ?
P1 C1 C6 C5 -174.5(16) . . . . ?
P1 C7 C8 C9 -174.1(18) . . . . ?
P1 C7 C12 C11 173.3(18) . . . . ?
P1 C13 B5 C14 151.9(12) . . . . ?
P1 C13 B5 B6 111.2(14) . . . . ?
P1 C13 B5 B4 -147.1(14) . . . . ?
P1 C13 B5 B10 -107.7(15) . . . . ?
P1 C13 B6 C14 -145.9(11) . . . . ?
P1 C13 B6 B5 -103.7(12) . . . . ?
P1 C13 B6 B7 153.7(12) . . . . ?
P1 C13 B6 B9 115.1(14) . . . . ?
P1 C13 B1 B2 -151.9(14) . . . . ?
P1 C13 B1 B3 143.5(13) . . . . ?
P1 C13 B1 B9 -113.2(15) . . . . ?
P1 C13 B1 B10 104.9(16) . . . . ?
P1 C13 B9 B2 150.7(14) . . . . ?
P1 C13 B9 B6 -108.5(16) . . . . ?
P1 C13 B9 B7 -145.7(15) . . . . ?
P1 C13 B9 B1 110.5(16) . . . . ?
P1 C13 B10 B5 103.9(14) . . . . ?
P1 C13 B10 B4 143.0(14) . . . . ?
P1 C13 B10 B3 -151.4(13) . . . . ?
P1 C13 B10 B1 -113.2(14) . . . . ?
P4 C41 C42 C43 175.7(19) . . . . ?
P4 C47 C52 C51 177(2) . . . . ?
P4 C40 B13 B12 109.9(16) . . . . ?
P4 C40 B13 B14 -111.0(15) . . . . ?
P4 C40 B13 B20 148.5(13) . . . . ?
P4 C40 B13 B19 -150.5(12) . . . . ?
P4 C40 B12 C39 145.0(12) . . . . ?
P4 C40 B12 B13 -112.5(15) . . . . ?
P4 C40 B12 B11 105.6(14) . . . . ?
P4 C40 B12 B20 -153.2(13) . . . . ?
P4 C40 B11 C39 -151.8(11) . . . . ?
P4 C40 B11 B12 -112.4(14) . . . . ?
P4 C40 B11 B16 145.3(12) . . . . ?
P4 C40 B11 B15 107.7(13) . . . . ?
P4 C40 B15 B16 -145.8(12) . . . . ?
P4 C40 B15 B11 -106.2(13) . . . . ?
P4 C40 B15 B14 111.5(14) . . . . ?
P4 C40 B15 B18 151.8(11) . . . . ?
P4 C40 B14 B13 112.9(15) . . . . ?
P4 C40 B14 B15 -105.1(13) . . . . ?
P4 C40 B14 B18 -145.5(12) . . . . ?
P4 C40 B14 B19 152.6(13) . . . . ?
C46 C41 C42 C43 3(3) . . . . ?
C1 P1 C7 C8 24(2) . . . . ?
C1 P1 C7 C12 -154.3(17) . . . . ?
C1 P1 C13 B5 153.5(13) . . . . ?
C1 P1 C13 B6 -135.5(12) . . . . ?
C1 P1 C13 B1 14.4(17) . . . . ?
C1 P1 C13 B9 -59.5(17) . . . . ?
C1 P1 C13 B10 85.8(14) . . . . ?
C1 C2 C3 C4 -7(3) . . . . ?
C1 C6 C5 C4 -1(3) . . . . ?
C14 P2 C21 C22 -72.2(15) . . . . ?
C14 P2 C21 C26 115.3(15) . . . . ?
C14 P2 C15 C16 100.2(15) . . . . ?
C14 P2 C15 C20 -72.8(18) . . . . ?
C14 B5 B6 C13 -130.4(15) . . . . ?
C14 B5 B6 B7 -32.6(14) . . . . ?
C14 B5 B6 B9 -96.7(15) . . . . ?
C14 B5 B4 B3 95.6(17) . . . . ?
C14 B5 B4 B8 32.6(14) . . . . ?
C14 B5 B4 B10 131.2(16) . . . . ?
C14 B5 B10 C13 93.5(14) . . . . ?
C14 B5 B10 B4 -42.0(14) . . . . ?
C14 B5 B10 B3 -4.4(19) . . . . ?
C14 B5 B10 B1 59.9(18) . . . . ?
C14 B6 B7 B2 -96.9(19) . . . . ?
C14 B6 B7 B8 -33.7(15) . . . . ?
C14 B6 B7 B9 -132.3(18) . . . . ?
C14 B6 B9 C13 -96.1(15) . . . . ?
C14 B6 B9 B2 4(2) . . . . ?
C14 B6 B9 B7 40.5(15) . . . . ?
C14 B6 B9 B1 -61.4(17) . . . . ?
C14 B4 B3 B2 -1(2) . . . . ?
C14 B4 B3 B1 62.1(19) . . . . ?
C14 B4 B3 B8 -39.3(15) . . . . ?
C14 B4 B3 B10 98.7(17) . . . . ?
C14 B4 B8 B2 94.9(17) . . . . ?
C14 B4 B8 B3 133.6(17) . . . . ?
C14 B4 B8 B7 32.1(13) . . . . ?
C14 B4 B10 C13 3(2) . . . . ?
C14 B4 B10 B5 42.5(15) . . . . ?
C14 B4 B10 B3 -97.5(17) . . . . ?
C14 B4 B10 B1 -60(2) . . . . ?
C14 B7 B8 B2 -135.0(17) . . . . ?
C14 B7 B8 B4 -32.6(14) . . . . ?
C14 B7 B8 B3 -96.4(16) . . . . ?
C14 B7 B9 C13 -4(2) . . . . ?
C14 B7 B9 B2 98.9(19) . . . . ?
C14 B7 B9 B6 -40.8(15) . . . . ?
C14 B7 B9 B1 59(2) . . . . ?
C24 C23 C22 C21 -2(3) . . . . ?
C2 C1 C6 C5 -2(3) . . . . ?
C7 P1 C1 C2 -71.1(19) . . . . ?
C7 P1 C1 C6 101.1(16) . . . . ?
C7 P1 C13 B5 -92.1(15) . . . . ?
C7 P1 C13 B6 -21.1(14) . . . . ?
C7 P1 C13 B1 128.8(15) . . . . ?
C7 P1 C13 B9 54.9(17) . . . . ?
C7 P1 C13 B10 -159.8(14) . . . . ?
C7 C8 C9 C10 1(4) . . . . ?
C7 C12 C11 C10 1(4) . . . . ?
C37 C38 C33 P3 -166.9(14) . . . . ?
C37 C38 C33 C34 4(3) . . . . ?
C27 P3 C39 B12 -126.5(13) . . . . ?
C27 P3 C39 B16 96.3(13) . . . . ?
C27 P3 C39 B11 163.0(11) . . . . ?
C27 P3 C39 B17 24.2(15) . . . . ?
C27 P3 C39 B20 -53.3(16) . . . . ?
C27 P3 C33 C38 -145.2(14) . . . . ?
C27 P3 C33 C34 43.5(17) . . . . ?
C27 C28 C29 C30 -4(4) . . . . ?
C23 C24 C25 C26 1(3) . . . . ?
C38 C37 C36 C35 4(3) . . . . ?
C38 C33 C34 C35 0(3) . . . . ?
C28 C27 C32 C31 1(3) . . . . ?
C36 C35 C34 C33 -1(3) . . . . ?
C36 C37 C38 C33 -6(3) . . . . ?
C8 C7 C12 C11 -5(4) . . . . ?
C8 C9 C10 C11 -5(4) . . . . ?
C39 P3 C27 C28 -147.3(15) . . . . ?
C39 P3 C27 C32 33.0(19) . . . . ?
C39 P3 C33 C38 98.6(14) . . . . ?
C39 P3 C33 C34 -72.8(16) . . . . ?
C39 B12 B11 C40 -133.1(14) . . . . ?
C39 B12 B11 B16 -38.0(12) . . . . ?
C39 B12 B11 B15 -97.3(14) . . . . ?
C39 B12 B20 B13 135.9(15) . . . . ?
C39 B12 B20 B17 33.5(12) . . . . ?
C39 B12 B20 B19 97.3(16) . . . . ?
C39 B16 B11 C40 95.7(14) . . . . ?
C39 B16 B11 B12 36.7(12) . . . . ?
C39 B16 B11 B15 135.3(14) . . . . ?
C39 B16 B15 C40 0.1(17) . . . . ?
C39 B16 B15 B11 -38.8(12) . . . . ?
C39 B16 B15 B14 61.8(17) . . . . ?
C39 B16 B15 B18 99.5(15) . . . . ?
C39 B16 B17 B18 -136.8(16) . . . . ?
C39 B16 B17 B20 -36.2(13) . . . . ?
C39 B16 B17 B19 -98.5(15) . . . . ?
C39 B16 B18 B15 -101.9(16) . . . . ?
C39 B16 B18 B14 -65.3(17) . . . . ?
C39 B16 B18 B17 36.9(14) . . . . ?
C39 B16 B18 B19 -2(2) . . . . ?
C39 B11 B15 C40 -95.1(14) . . . . ?
C39 B11 B15 B16 39.6(13) . . . . ?
C39 B11 B15 B14 -61.6(16) . . . . ?
C39 B11 B15 B18 2.3(17) . . . . ?
C39 B17 B18 B16 -38.6(14) . . . . ?
C39 B17 B18 B15 -3.3(17) . . . . ?
C39 B17 B18 B14 59.3(15) . . . . ?
C39 B17 B18 B19 97.5(15) . . . . ?
C39 B17 B20 B13 -97.0(15) . . . . ?
C39 B17 B20 B12 -34.0(13) . . . . ?
C39 B17 B20 B19 -134.3(16) . . . . ?
C39 B17 B19 B13 2.1(19) . . . . ?
C39 B17 B19 B14 -62.6(17) . . . . ?
C39 B17 B19 B18 -100.9(15) . . . . ?
C39 B17 B19 B20 39.3(13) . . . . ?
C39 B20 B19 B13 100.0(15) . . . . ?
C39 B20 B19 B14 61.1(19) . . . . ?
C39 B20 B19 B17 -38.9(14) . . . . ?
C39 B20 B19 B18 -3(2) . . . . ?
C20 C19 C18 C17 -4(4) . . . . ?
C48 C49 C50 C51 -1(4) . . . . ?
C48 C47 C52 C51 3(3) . . . . ?
C30 C31 C32 C27 -1(3) . . . . ?
C21 P2 C14 B5 86.1(14) . . . . ?
C21 P2 C14 B6 14.4(15) . . . . ?
C21 P2 C14 B4 152.1(14) . . . . ?
C21 P2 C14 B7 -60.7(18) . . . . ?
C21 P2 C14 B8 -136.9(14) . . . . ?
C21 P2 C15 C16 -145.4(15) . . . . ?
C21 P2 C15 C20 41.6(18) . . . . ?
C21 C26 C25 C24 -2(3) . . . . ?
C12 C7 C8 C9 4(3) . . . . ?
C12 C11 C10 C9 4(4) . . . . ?
C41 P4 C47 C48 154.0(17) . . . . ?
C41 P4 C47 C52 -20(2) . . . . ?
C41 P4 C40 B13 64.8(15) . . . . ?
C41 P4 C40 B12 138.7(13) . . . . ?
C41 P4 C40 B11 -148.9(13) . . . . ?
C41 P4 C40 B15 -79.9(13) . . . . ?
C41 P4 C40 B14 -10.8(15) . . . . ?
C41 C46 C45 C44 5(4) . . . . ?
C6 C1 C2 C3 6(3) . . . . ?
C22 C21 C26 C25 1(3) . . . . ?
C33 P3 C27 C28 102.3(16) . . . . ?
C33 P3 C27 C32 -77.4(18) . . . . ?
C33 P3 C39 B12 -11.4(14) . . . . ?
C33 P3 C39 B16 -148.6(13) . . . . ?
C33 P3 C39 B11 -81.9(13) . . . . ?
C33 P3 C39 B17 139.3(13) . . . . ?
C33 P3 C39 B20 61.8(16) . . . . ?
C29 C30 C31 C32 -1(3) . . . . ?
C26 C21 C22 C23 1(3) . . . . ?
C44 C43 C42 C41 1(4) . . . . ?
C15 P2 C14 B5 -156.2(13) . . . . ?
C15 P2 C14 B6 132.1(14) . . . . ?
C15 P2 C14 B4 -90.2(15) . . . . ?
C15 P2 C14 B7 57.0(19) . . . . ?
C15 P2 C14 B8 -19.2(16) . . . . ?
C15 P2 C21 C22 175.4(13) . . . . ?
C15 P2 C21 C26 2.8(17) . . . . ?
C15 C16 C17 C18 -1(4) . . . . ?
C15 C20 C19 C18 0(3) . . . . ?
C13 P1 C1 C2 42.6(19) . . . . ?
C13 P1 C1 C6 -145.2(14) . . . . ?
C13 P1 C7 C8 -90.7(19) . . . . ?
C13 P1 C7 C12 90.8(18) . . . . ?
C13 B5 B6 C14 130.4(15) . . . . ?
C13 B5 B6 B7 97.8(16) . . . . ?
C13 B5 B6 B9 33.7(12) . . . . ?
C13 B5 B4 C14 -92.6(15) . . . . ?
C13 B5 B4 B3 3(2) . . . . ?
C13 B5 B4 B8 -60.0(19) . . . . ?
C13 B5 B4 B10 38.6(15) . . . . ?
C13 B5 B10 B4 -135.5(16) . . . . ?
C13 B5 B10 B3 -97.9(16) . . . . ?
C13 B5 B10 B1 -33.6(14) . . . . ?
C13 B6 B7 C14 95.1(15) . . . . ?
C13 B6 B7 B2 -1.8(19) . . . . ?
C13 B6 B7 B8 61.4(17) . . . . ?
C13 B6 B7 B9 -37.2(14) . . . . ?
C13 B6 B9 B2 100.1(19) . . . . ?
C13 B6 B9 B7 136.6(16) . . . . ?
C13 B6 B9 B1 34.7(13) . . . . ?
C13 B1 B9 B2 -135.7(15) . . . . ?
C13 B1 B9 B6 -34.1(12) . . . . ?
C13 B1 B9 B7 -96.0(15) . . . . ?
C13 B1 B10 B5 34.0(14) . . . . ?
C13 B1 B10 B4 97.9(18) . . . . ?
C13 B1 B10 B3 136.8(16) . . . . ?
C5 C4 C3 C2 4(3) . . . . ?
C43 C44 C45 C46 -2(4) . . . . ?
C49 C48 C47 P4 -176.9(17) . . . . ?
C49 C48 C47 C52 -2(3) . . . . ?
C31 C30 C29 C28 4(4) . . . . ?
C32 C27 C28 C29 2(3) . . . . ?
C34 C35 C36 C37 0(3) . . . . ?
C25 C24 C23 C22 0(3) . . . . ?
C45 C46 C41 P4 -179.2(18) . . . . ?
C45 C46 C41 C42 -6(3) . . . . ?
C45 C44 C43 C42 -1(4) . . . . ?
C47 P4 C41 C46 -137.4(17) . . . . ?
C47 P4 C41 C42 50(2) . . . . ?
C47 P4 C40 B13 -52.0(15) . . . . ?
C47 P4 C40 B12 21.9(15) . . . . ?
C47 P4 C40 B11 94.4(13) . . . . ?
C47 P4 C40 B15 163.4(11) . . . . ?
C47 P4 C40 B14 -127.5(13) . . . . ?
C47 C48 C49 C50 1(4) . . . . ?
C40 P4 C41 C46 110.3(18) . . . . ?
C40 P4 C41 C42 -63(2) . . . . ?
C40 P4 C47 C48 -93.9(17) . . . . ?
C40 P4 C47 C52 92(2) . . . . ?
C40 B13 B12 C39 96.2(16) . . . . ?
C40 B13 B12 B11 34.8(14) . . . . ?
C40 B13 B12 B20 135.0(16) . . . . ?
C40 B13 B14 B15 -34.7(14) . . . . ?
C40 B13 B14 B18 -98.5(14) . . . . ?
C40 B13 B14 B19 -134.1(15) . . . . ?
C40 B13 B20 C39 0.3(18) . . . . ?
C40 B13 B20 B12 -38.1(13) . . . . ?
C40 B13 B20 B17 61.4(17) . . . . ?
C40 B13 B20 B19 98.7(16) . . . . ?
C40 B13 B19 B14 39.6(12) . . . . ?
C40 B13 B19 B17 -60.7(18) . . . . ?
C40 B13 B19 B18 3.4(18) . . . . ?
C40 B13 B19 B20 -97.7(14) . . . . ?
C40 B12 B11 C39 133.1(14) . . . . ?
C40 B12 B11 B16 95.2(15) . . . . ?
C40 B12 B11 B15 35.8(13) . . . . ?
C40 B12 B20 C39 -96.0(15) . . . . ?
C40 B12 B20 B13 39.9(14) . . . . ?
C40 B12 B20 B17 -62.5(17) . . . . ?
C40 B12 B20 B19 1.4(19) . . . . ?
C40 B11 B15 B16 134.7(15) . . . . ?
C40 B11 B15 B14 33.4(13) . . . . ?
C40 B11 B15 B18 97.3(14) . . . . ?
C40 B15 B14 B13 33.3(13) . . . . ?
C40 B15 B14 B18 134.2(14) . . . . ?
C40 B15 B14 B19 96.5(15) . . . . ?
C40 B15 B18 B16 98.6(15) . . . . ?
C40 B15 B18 B14 -39.6(12) . . . . ?
C40 B15 B18 B17 61.8(15) . . . . ?
C40 B15 B18 B19 -1.6(16) . . . . ?
C40 B14 B18 B16 5.5(18) . . . . ?
C40 B14 B18 B15 41.0(12) . . . . ?
C40 B14 B18 B17 -58.0(16) . . . . ?
C40 B14 B18 B19 -96.3(14) . . . . ?
C40 B14 B19 B13 -38.6(13) . . . . ?
C40 B14 B19 B17 63.5(17) . . . . ?
C40 B14 B19 B18 101.7(13) . . . . ?
C40 B14 B19 B20 -0.1(19) . . . . ?
C52 C51 C50 C49 2(4) . . . . ?
C3 C4 C5 C6 0(3) . . . . ?
C19 C20 C15 P2 175.5(15) . . . . ?
C19 C20 C15 C16 3(3) . . . . ?
C19 C18 C17 C16 4(4) . . . . ?
C17 C16 C15 P2 -175.9(19) . . . . ?
C17 C16 C15 C20 -3(3) . . . . ?
C50 C51 C52 C47 -3(4) . . . . ?
B2 B3 B1 C13 99.3(17) . . . . ?
B2 B3 B1 B9 36.6(14) . . . . ?
B2 B3 B1 B10 137.0(17) . . . . ?
B2 B3 B8 C14 -97.6(16) . . . . ?
B2 B3 B8 B4 -137.1(17) . . . . ?
B2 B3 B8 B7 -38.1(15) . . . . ?
B2 B3 B10 C13 0(2) . . . . ?
B2 B3 B10 B5 63.8(19) . . . . ?
B2 B3 B10 B4 100.1(16) . . . . ?
B2 B3 B10 B1 -38.3(16) . . . . ?
B2 B7 B8 C14 135.0(17) . . . . ?
B2 B7 B8 B4 102.4(18) . . . . ?
B2 B7 B8 B3 38.6(14) . . . . ?
B2 B7 B9 C13 -102.6(18) . . . . ?
B2 B7 B9 B6 -139.7(17) . . . . ?
B2 B7 B9 B1 -40.2(15) . . . . ?
B2 B1 B9 C13 135.7(15) . . . . ?
B2 B1 B9 B6 101.6(15) . . . . ?
B2 B1 B9 B7 39.7(15) . . . . ?
B2 B1 B10 C13 -97.3(19) . . . . ?
B2 B1 B10 B5 -63(2) . . . . ?
B2 B1 B10 B4 1(2) . . . . ?
B2 B1 B10 B3 39.5(17) . . . . ?
B5 C14 B6 C13 42.0(12) . . . . ?
B5 C14 B6 B7 143.2(17) . . . . ?
B5 C14 B6 B9 101.6(16) . . . . ?
B5 C14 B4 B3 -103.5(16) . . . . ?
B5 C14 B4 B8 -143.3(16) . . . . ?
B5 C14 B4 B10 -42.2(15) . . . . ?
B5 C14 B7 B2 66(2) . . . . ?
B5 C14 B7 B6 -36.2(17) . . . . ?
B5 C14 B7 B8 105(2) . . . . ?
B5 C14 B7 B9 6(2) . . . . ?
B5 C14 B8 B2 -69.1(19) . . . . ?
B5 C14 B8 B4 34.5(14) . . . . ?
B5 C14 B8 B3 -6.3(19) . . . . ?
B5 C14 B8 B7 -108.0(16) . . . . ?
B5 C13 B6 C14 -42.2(11) . . . . ?
B5 C13 B6 B7 -102.6(14) . . . . ?
B5 C13 B6 B9 -141.2(14) . . . . ?
B5 C13 B1 B2 68(2) . . . . ?
B5 C13 B1 B3 4(2) . . . . ?
B5 C13 B1 B9 107.2(16) . . . . ?
B5 C13 B1 B10 -34.7(16) . . . . ?
B5 C13 B9 B2 -63(2) . . . . ?
B5 C13 B9 B6 38.1(15) . . . . ?
B5 C13 B9 B7 1(2) . . . . ?
B5 C13 B9 B1 -103.0(17) . . . . ?
B5 C13 B10 B4 39.1(15) . . . . ?
B5 C13 B10 B3 104.8(17) . . . . ?
B5 C13 B10 B1 142.9(16) . . . . ?
B5 B6 B7 C14 33.0(15) . . . . ?
B5 B6 B7 B2 -64.0(19) . . . . ?
B5 B6 B7 B8 -1(2) . . . . ?
B5 B6 B7 B9 -99.4(17) . . . . ?
B5 B6 B9 C13 -34.2(13) . . . . ?
B5 B6 B9 B2 65.9(19) . . . . ?
B5 B6 B9 B7 102.4(16) . . . . ?
B5 B6 B9 B1 0.5(18) . . . . ?
B5 B4 B3 B2 -64(2) . . . . ?
B5 B4 B3 B1 -1(2) . . . . ?
B5 B4 B3 B8 -102.2(18) . . . . ?
B5 B4 B3 B10 35.8(16) . . . . ?
B5 B4 B8 C14 -33.4(15) . . . . ?
B5 B4 B8 B2 61(2) . . . . ?
B5 B4 B8 B3 100.2(17) . . . . ?
B5 B4 B8 B7 -1(2) . . . . ?
B5 B4 B10 C13 -39.6(15) . . . . ?
B5 B4 B10 B3 -140.0(17) . . . . ?
B5 B4 B10 B1 -102.4(19) . . . . ?
B6 C14 B5 C13 -41.0(13) . . . . ?
B6 C14 B5 B4 -143.6(16) . . . . ?
B6 C14 B5 B10 -101.1(16) . . . . ?
B6 C14 B4 B5 35.2(15) . . . . ?
B6 C14 B4 B3 -68(2) . . . . ?
B6 C14 B4 B8 -108.1(17) . . . . ?
B6 C14 B4 B10 -7(2) . . . . ?
B6 C14 B7 B2 102.3(17) . . . . ?
B6 C14 B7 B8 141.6(18) . . . . ?
B6 C14 B7 B9 41.8(16) . . . . ?
B6 C14 B8 B2 1(2) . . . . ?
B6 C14 B8 B4 104.8(17) . . . . ?
B6 C14 B8 B3 64.0(19) . . . . ?
B6 C14 B8 B7 -37.7(16) . . . . ?
B6 C13 B5 C14 40.7(13) . . . . ?
B6 C13 B5 B4 101.6(17) . . . . ?
B6 C13 B5 B10 141.1(15) . . . . ?
B6 C13 B1 B2 -1(2) . . . . ?
B6 C13 B1 B3 -65.3(18) . . . . ?
B6 C13 B1 B9 38.1(14) . . . . ?
B6 C13 B1 B10 -103.9(16) . . . . ?
B6 C13 B9 B2 -100.8(16) . . . . ?
B6 C13 B9 B7 -37.2(15) . . . . ?
B6 C13 B9 B1 -141.0(14) . . . . ?
B6 C13 B10 B5 -37.3(14) . . . . ?
B6 C13 B10 B4 2(2) . . . . ?
B6 C13 B10 B3 67.5(18) . . . . ?
B6 C13 B10 B1 105.7(15) . . . . ?
B6 B5 B4 C14 -31.7(14) . . . . ?
B6 B5 B4 B3 63.9(19) . . . . ?
B6 B5 B4 B8 1(2) . . . . ?
B6 B5 B4 B10 99.4(16) . . . . ?
B6 B5 B10 C13 33.8(13) . . . . ?
B6 B5 B10 B4 -101.7(16) . . . . ?
B6 B5 B10 B3 -64.1(18) . . . . ?
B6 B5 B10 B1 0(2) . . . . ?
B6 B7 B8 C14 33.8(15) . . . . ?
B6 B7 B8 B2 -101.1(16) . . . . ?
B6 B7 B8 B4 1(2) . . . . ?
B6 B7 B8 B3 -62.6(18) . . . . ?
B6 B7 B9 C13 37.1(14) . . . . ?
B6 B7 B9 B2 139.7(17) . . . . ?
B6 B7 B9 B1 99.5(16) . . . . ?
B13 C40 B12 C39 -102.4(15) . . . . ?
B13 C40 B12 B11 -141.9(15) . . . . ?
B13 C40 B12 B20 -40.7(14) . . . . ?
B13 C40 B11 C39 -2.8(18) . . . . ?
B13 C40 B11 B12 36.6(14) . . . . ?
B13 C40 B11 B16 -65.7(18) . . . . ?
B13 C40 B11 B15 -103.3(16) . . . . ?
B13 C40 B15 B16 66.3(17) . . . . ?
B13 C40 B15 B11 105.9(15) . . . . ?
B13 C40 B15 B14 -36.4(14) . . . . ?
B13 C40 B15 B18 3.9(17) . . . . ?
B13 C40 B14 B15 142.1(15) . . . . ?
B13 C40 B14 B18 101.6(15) . . . . ?
B13 C40 B14 B19 39.7(14) . . . . ?
B13 B12 B11 C39 98.5(16) . . . . ?
B13 B12 B11 C40 -34.7(14) . . . . ?
B13 B12 B11 B16 60.5(18) . . . . ?
B13 B12 B11 B15 1.1(19) . . . . ?
B13 B12 B20 C39 -135.9(15) . . . . ?
B13 B12 B20 B17 -102.4(16) . . . . ?
B13 B12 B20 B19 -38.6(15) . . . . ?
B13 B14 B18 B16 66.2(16) . . . . ?
B13 B14 B18 B15 101.7(14) . . . . ?
B13 B14 B18 B17 2.7(16) . . . . ?
B13 B14 B18 B19 -35.6(11) . . . . ?
B13 B14 B19 B17 102.1(14) . . . . ?
B13 B14 B19 B18 140.3(13) . . . . ?
B13 B14 B19 B20 38.6(14) . . . . ?
B13 B20 B19 B14 -38.8(14) . . . . ?
B13 B20 B19 B17 -138.9(15) . . . . ?
B13 B20 B19 B18 -102.9(16) . . . . ?
B4 C14 B5 C13 102.7(15) . . . . ?
B4 C14 B5 B6 143.6(16) . . . . ?
B4 C14 B5 B10 42.5(14) . . . . ?
B4 C14 B6 C13 7.9(19) . . . . ?
B4 C14 B6 B5 -34.1(15) . . . . ?
B4 C14 B6 B7 109.1(19) . . . . ?
B4 C14 B6 B9 67.5(19) . . . . ?
B4 C14 B7 B2 -2(2) . . . . ?
B4 C14 B7 B6 -104.0(19) . . . . ?
B4 C14 B7 B8 37.6(18) . . . . ?
B4 C14 B7 B9 -62(2) . . . . ?
B4 C14 B8 B2 -103.6(18) . . . . ?
B4 C14 B8 B3 -40.8(14) . . . . ?
B4 C14 B8 B7 -142.5(16) . . . . ?
B4 B5 B6 C14 32.5(15) . . . . ?
B4 B5 B6 C13 -97.9(16) . . . . ?
B4 B5 B6 B7 0(2) . . . . ?
B4 B5 B6 B9 -64.2(18) . . . . ?
B4 B5 B10 C13 135.5(16) . . . . ?
B4 B5 B10 B3 37.6(16) . . . . ?
B4 B5 B10 B1 101.9(18) . . . . ?
B4 B3 B1 C13 -2(2) . . . . ?
B4 B3 B1 B2 -101.0(16) . . . . ?
B4 B3 B1 B9 -64.4(18) . . . . ?
B4 B3 B1 B10 36.0(16) . . . . ?
B4 B3 B8 C14 39.5(13) . . . . ?
B4 B3 B8 B2 137.1(17) . . . . ?
B4 B3 B8 B7 99.0(16) . . . . ?
B4 B3 B10 C13 -100.4(17) . . . . ?
B4 B3 B10 B5 -36.3(15) . . . . ?
B4 B3 B10 B1 -138.4(17) . . . . ?
B12 C39 B16 B11 -40.1(13) . . . . ?
B12 C39 B16 B15 1.2(18) . . . . ?
B12 C39 B16 B17 105.8(15) . . . . ?
B12 C39 B16 B18 67.2(18) . . . . ?
B12 C39 B11 C40 38.5(12) . . . . ?
B12 C39 B11 B16 138.0(14) . . . . ?
B12 C39 B11 B15 100.7(13) . . . . ?
B12 C39 B17 B16 -102.7(16) . . . . ?
B12 C39 B17 B18 -65.3(17) . . . . ?
B12 C39 B17 B20 36.4(15) . . . . ?
B12 C39 B17 B19 -3.1(19) . . . . ?
B12 C39 B20 B13 -38.5(13) . . . . ?
B12 C39 B20 B17 -141.7(15) . . . . ?
B12 C39 B20 B19 -101.6(16) . . . . ?
B12 C40 B13 B14 139.1(16) . . . . ?
B12 C40 B13 B20 38.6(14) . . . . ?
B12 C40 B13 B19 99.6(15) . . . . ?
B12 C40 B11 C39 -39.4(13) . . . . ?
B12 C40 B11 B16 -102.3(15) . . . . ?
B12 C40 B11 B15 -139.9(14) . . . . ?
B12 C40 B15 B16 -1.3(17) . . . . ?
B12 C40 B15 B11 38.3(13) . . . . ?
B12 C40 B15 B14 -104.0(15) . . . . ?
B12 C40 B15 B18 -63.7(15) . . . . ?
B12 C40 B14 B13 -38.7(14) . . . . ?
B12 C40 B14 B15 103.3(16) . . . . ?
B12 C40 B14 B18 62.9(18) . . . . ?
B12 C40 B14 B19 1.0(19) . . . . ?
B12 B13 B14 C40 35.3(14) . . . . ?
B12 B13 B14 B15 1(2) . . . . ?
B12 B13 B14 B18 -63.2(17) . . . . ?
B12 B13 B14 B19 -98.7(16) . . . . ?
B12 B13 B20 C39 38.4(13) . . . . ?
B12 B13 B20 B17 99.5(15) . . . . ?
B12 B13 B20 B19 136.9(16) . . . . ?
B12 B13 B19 B14 99.9(14) . . . . ?
B12 B13 B19 B17 0(2) . . . . ?
B12 B13 B19 B18 63.6(18) . . . . ?
B12 B13 B19 B20 -37.4(14) . . . . ?
B12 B11 B15 C40 -34.2(12) . . . . ?
B12 B11 B15 B16 100.5(15) . . . . ?
B12 B11 B15 B14 -0.7(18) . . . . ?
B12 B11 B15 B18 63.2(17) . . . . ?
B12 B20 B19 B13 38.1(14) . . . . ?
B12 B20 B19 B14 -1(2) . . . . ?
B12 B20 B19 B17 -100.8(15) . . . . ?
B12 B20 B19 B18 -64.9(19) . . . . ?
B16 C39 B12 C40 -2.0(17) . . . . ?
B16 C39 B12 B13 -64.4(17) . . . . ?
B16 C39 B12 B11 38.8(12) . . . . ?
B16 C39 B12 B20 -104.4(15) . . . . ?
B16 C39 B11 C40 -99.6(14) . . . . ?
B16 C39 B11 B12 -138.0(14) . . . . ?
B16 C39 B11 B15 -37.3(13) . . . . ?
B16 C39 B17 B18 37.4(13) . . . . ?
B16 C39 B17 B20 139.1(16) . . . . ?
B16 C39 B17 B19 99.6(16) . . . . ?
B16 C39 B20 B13 64.6(18) . . . . ?
B16 C39 B20 B12 103.1(16) . . . . ?
B16 C39 B20 B17 -38.6(15) . . . . ?
B16 C39 B20 B19 2(2) . . . . ?
B16 B11 B15 C40 -134.7(15) . . . . ?
B16 B11 B15 B14 -101.3(16) . . . . ?
B16 B11 B15 B18 -37.3(14) . . . . ?
B16 B15 B14 C40 -96.7(15) . . . . ?
B16 B15 B14 B13 -63.4(19) . . . . ?
B16 B15 B14 B18 37.5(14) . . . . ?
B16 B15 B14 B19 0(2) . . . . ?
B16 B15 B18 B14 -138.1(16) . . . . ?
B16 B15 B18 B17 -36.8(14) . . . . ?
B16 B15 B18 B19 -100.1(15) . . . . ?
B16 B17 B18 B15 35.3(14) . . . . ?
B16 B17 B18 B14 97.9(15) . . . . ?
B16 B17 B18 B19 136.1(16) . . . . ?
B16 B17 B20 C39 37.0(13) . . . . ?
B16 B17 B20 B13 -59.9(16) . . . . ?
B16 B17 B20 B12 3.0(18) . . . . ?
B16 B17 B20 B19 -97.3(16) . . . . ?
B16 B17 B19 B13 65.3(18) . . . . ?
B16 B17 B19 B14 0.5(18) . . . . ?
B16 B17 B19 B18 -37.7(13) . . . . ?
B16 B17 B19 B20 102.5(16) . . . . ?
B16 B18 B19 B13 -61.3(19) . . . . ?
B16 B18 B19 B14 -97.9(17) . . . . ?
B16 B18 B19 B17 39.3(15) . . . . ?
B16 B18 B19 B20 3(2) . . . . ?
B11 C39 B12 C40 -40.8(12) . . . . ?
B11 C39 B12 B13 -103.2(15) . . . . ?
B11 C39 B12 B20 -143.2(14) . . . . ?
B11 C39 B16 B15 41.3(13) . . . . ?
B11 C39 B16 B17 145.9(15) . . . . ?
B11 C39 B16 B18 107.3(17) . . . . ?
B11 C39 B17 B16 -32.3(15) . . . . ?
B11 C39 B17 B18 5.1(18) . . . . ?
B11 C39 B17 B20 106.7(16) . . . . ?
B11 C39 B17 B19 67.2(17) . . . . ?
B11 C39 B20 B13 -2.2(19) . . . . ?
B11 C39 B20 B12 36.3(14) . . . . ?
B11 C39 B20 B17 -105.4(15) . . . . ?
B11 C39 B20 B19 -65.3(18) . . . . ?
B11 C40 B13 B12 -37.0(15) . . . . ?
B11 C40 B13 B14 102.2(16) . . . . ?
B11 C40 B13 B20 1.6(19) . . . . ?
B11 C40 B13 B19 62.6(17) . . . . ?
B11 C40 B12 C39 39.5(12) . . . . ?
B11 C40 B12 B13 141.9(16) . . . . ?
B11 C40 B12 B20 101.2(16) . . . . ?
B11 C40 B15 B16 -39.6(12) . . . . ?
B11 C40 B15 B14 -142.3(14) . . . . ?
B11 C40 B15 B18 -102.0(13) . . . . ?
B11 C40 B14 B13 -107.2(15) . . . . ?
B11 C40 B14 B15 34.9(13) . . . . ?
B11 C40 B14 B18 -5.5(18) . . . . ?
B11 C40 B14 B19 -67.4(17) . . . . ?
B11 B12 B20 C39 -32.3(12) . . . . ?
B11 B12 B20 B13 103.7(15) . . . . ?
B11 B12 B20 B17 1.3(18) . . . . ?
B11 B12 B20 B19 65.1(17) . . . . ?
B11 B16 B15 C40 38.8(12) . . . . ?
B11 B16 B15 B14 100.5(16) . . . . ?
B11 B16 B15 B18 138.2(15) . . . . ?
B11 B16 B17 C39 30.0(13) . . . . ?
B11 B16 B17 B18 -106.8(17) . . . . ?
B11 B16 B17 B20 -6.3(18) . . . . ?
B11 B16 B17 B19 -68.5(16) . . . . ?
B11 B16 B18 B15 -40.3(15) . . . . ?
B11 B16 B18 B14 -3.7(19) . . . . ?
B11 B16 B18 B17 98.5(17) . . . . ?
B11 B16 B18 B19 59(2) . . . . ?
B11 B15 B14 C40 -33.2(13) . . . . ?
B11 B15 B14 B13 0.1(19) . . . . ?
B11 B15 B14 B18 101.0(14) . . . . ?
B11 B15 B14 B19 63.3(17) . . . . ?
B11 B15 B18 B16 37.4(13) . . . . ?
B11 B15 B18 B14 -100.8(15) . . . . ?
B11 B15 B18 B17 0.6(18) . . . . ?
B11 B15 B18 B19 -62.8(16) . . . . ?
B15 C40 B13 B12 -104.0(16) . . . . ?
B15 C40 B13 B14 35.1(13) . . . . ?
B15 C40 B13 B20 -65.5(17) . . . . ?
B15 C40 B13 B19 -4.5(18) . . . . ?
B15 C40 B12 C39 2.0(16) . . . . ?
B15 C40 B12 B13 104.4(15) . . . . ?
B15 C40 B12 B11 -37.5(12) . . . . ?
B15 C40 B12 B20 63.7(17) . . . . ?
B15 C40 B11 C39 100.5(13) . . . . ?
B15 C40 B11 B12 139.9(14) . . . . ?
B15 C40 B11 B16 37.6(12) . . . . ?
B15 C40 B14 B13 -142.1(15) . . . . ?
B15 C40 B14 B18 -40.5(12) . . . . ?
B15 C40 B14 B19 -102.4(15) . . . . ?
B15 B16 B11 C39 -135.3(14) . . . . ?
B15 B16 B11 C40 -39.6(13) . . . . ?
B15 B16 B11 B12 -98.6(14) . . . . ?
B15 B16 B17 C39 97.8(16) . . . . ?
B15 B16 B17 B18 -39.0(15) . . . . ?
B15 B16 B17 B20 61.5(18) . . . . ?
B15 B16 B17 B19 -0.7(19) . . . . ?
B15 B16 B18 B14 36.6(14) . . . . ?
B15 B16 B18 B17 138.8(16) . . . . ?
B15 B16 B18 B19 99.6(17) . . . . ?
B15 B14 B18 B16 -35.6(13) . . . . ?
B15 B14 B18 B17 -99.0(14) . . . . ?
B15 B14 B18 B19 -137.3(14) . . . . ?
B15 B14 B19 B13 -102.3(15) . . . . ?
B15 B14 B19 B17 -0.2(19) . . . . ?
B15 B14 B19 B18 37.9(13) . . . . ?
B15 B14 B19 B20 -64(2) . . . . ?
B15 B18 B19 B13 -1.1(18) . . . . ?
B15 B18 B19 B14 -37.7(12) . . . . ?
B15 B18 B19 B17 99.5(14) . . . . ?
B15 B18 B19 B20 63.6(18) . . . . ?
B14 C40 B13 B12 -139.1(16) . . . . ?
B14 C40 B13 B20 -100.5(16) . . . . ?
B14 C40 B13 B19 -39.6(13) . . . . ?
B14 C40 B12 C39 -63.2(16) . . . . ?
B14 C40 B12 B13 39.2(15) . . . . ?
B14 C40 B12 B11 -102.7(16) . . . . ?
B14 C40 B12 B20 -1(2) . . . . ?
B14 C40 B11 C39 66.1(16) . . . . ?
B14 C40 B11 B12 105.5(15) . . . . ?
B14 C40 B11 B16 3.2(18) . . . . ?
B14 C40 B11 B15 -34.4(13) . . . . ?
B14 C40 B15 B16 102.7(15) . . . . ?
B14 C40 B15 B11 142.3(14) . . . . ?
B14 C40 B15 B18 40.3(13) . . . . ?
B14 B13 B12 C39 60.3(18) . . . . ?
B14 B13 B12 C40 -35.9(14) . . . . ?
B14 B13 B12 B11 -1(2) . . . . ?
B14 B13 B12 B20 99.1(16) . . . . ?
B14 B13 B20 C39 -61.2(15) . . . . ?
B14 B13 B20 B12 -99.6(14) . . . . ?
B14 B13 B20 B17 -0.1(16) . . . . ?
B14 B13 B20 B19 37.2(13) . . . . ?
B14 B13 B19 B17 -100.3(16) . . . . ?
B14 B13 B19 B18 -36.2(13) . . . . ?
B14 B13 B19 B20 -137.3(14) . . . . ?
B14 B15 B18 B16 138.1(16) . . . . ?
B14 B15 B18 B17 101.4(15) . . . . ?
B14 B15 B18 B19 38.0(14) . . . . ?
B14 B18 B19 B13 36.6(13) . . . . ?
B14 B18 B19 B17 137.2(14) . . . . ?
B14 B18 B19 B20 101.3(16) . . . . ?
B3 B2 B7 C14 1(2) . . . . ?
B3 B2 B7 B6 62.3(19) . . . . ?
B3 B2 B7 B8 -37.9(16) . . . . ?
B3 B2 B7 B9 98.8(17) . . . . ?
B3 B2 B1 C13 -100.9(16) . . . . ?
B3 B2 B1 B9 -139.4(16) . . . . ?
B3 B2 B1 B10 -39.0(16) . . . . ?
B3 B2 B8 C14 99.4(18) . . . . ?
B3 B2 B8 B4 38.8(16) . . . . ?
B3 B2 B8 B7 137.0(17) . . . . ?
B3 B2 B9 C13 -4(2) . . . . ?
B3 B2 B9 B6 -66(2) . . . . ?
B3 B2 B9 B7 -101.3(16) . . . . ?
B3 B2 B9 B1 35.0(14) . . . . ?
B3 B4 B8 C14 -133.6(17) . . . . ?
B3 B4 B8 B2 -38.7(16) . . . . ?
B3 B4 B8 B7 -101.5(18) . . . . ?
B3 B4 B10 C13 100.5(16) . . . . ?
B3 B4 B10 B5 140.0(17) . . . . ?
B3 B4 B10 B1 37.7(16) . . . . ?
B3 B1 B9 C13 98.3(16) . . . . ?
B3 B1 B9 B2 -37.5(14) . . . . ?
B3 B1 B9 B6 64.1(18) . . . . ?
B3 B1 B9 B7 2(2) . . . . ?
B3 B1 B10 C13 -136.8(16) . . . . ?
B3 B1 B10 B5 -102.8(18) . . . . ?
B3 B1 B10 B4 -38.8(16) . . . . ?
B17 C39 B12 C40 65.4(16) . . . . ?
B17 C39 B12 B13 3.0(19) . . . . ?
B17 C39 B12 B11 106.2(15) . . . . ?
B17 C39 B12 B20 -37.0(14) . . . . ?
B17 C39 B16 B11 -145.9(15) . . . . ?
B17 C39 B16 B15 -104.6(16) . . . . ?
B17 C39 B16 B18 -38.6(15) . . . . ?
B17 C39 B11 C40 -66.9(17) . . . . ?
B17 C39 B11 B12 -105.3(15) . . . . ?
B17 C39 B11 B16 32.7(14) . . . . ?
B17 C39 B11 B15 -4.6(18) . . . . ?
B17 C39 B20 B13 103.2(16) . . . . ?
B17 C39 B20 B12 141.7(15) . . . . ?
B17 C39 B20 B19 40.1(14) . . . . ?
B17 B16 B11 C39 -29.8(12) . . . . ?
B17 B16 B11 C40 65.9(16) . . . . ?
B17 B16 B11 B12 7.0(18) . . . . ?
B17 B16 B11 B15 105.5(16) . . . . ?
B17 B16 B15 C40 -61.1(17) . . . . ?
B17 B16 B15 B11 -99.9(16) . . . . ?
B17 B16 B15 B14 1(2) . . . . ?
B17 B16 B15 B18 38.3(14) . . . . ?
B17 B16 B18 B15 -138.8(16) . . . . ?
B17 B16 B18 B14 -102.2(15) . . . . ?
B17 B16 B18 B19 -39.2(15) . . . . ?
B17 B18 B19 B13 -100.6(15) . . . . ?
B17 B18 B19 B14 -137.2(14) . . . . ?
B17 B18 B19 B20 -36.0(15) . . . . ?
B17 B20 B19 B13 138.9(15) . . . . ?
B17 B20 B19 B14 100.1(17) . . . . ?
B17 B20 B19 B18 35.9(15) . . . . ?
B18 B16 B11 C39 -95.3(16) . . . . ?
B18 B16 B11 C40 0.4(19) . . . . ?
B18 B16 B11 B12 -58.5(18) . . . . ?
B18 B16 B11 B15 40.0(14) . . . . ?
B18 B16 B15 C40 -99.4(14) . . . . ?
B18 B16 B15 B11 -138.2(15) . . . . ?
B18 B16 B15 B14 -37.7(14) . . . . ?
B18 B16 B17 C39 136.8(16) . . . . ?
B18 B16 B17 B20 100.6(16) . . . . ?
B18 B16 B17 B19 38.3(14) . . . . ?
B18 B15 B14 C40 -134.2(14) . . . . ?
B18 B15 B14 B13 -100.9(16) . . . . ?
B18 B15 B14 B19 -37.7(13) . . . . ?
B18 B14 B19 B13 -140.3(13) . . . . ?
B18 B14 B19 B17 -38.1(13) . . . . ?
B18 B14 B19 B20 -101.7(16) . . . . ?
B18 B17 B20 C39 98.8(15) . . . . ?
B18 B17 B20 B13 1.8(17) . . . . ?
B18 B17 B20 B12 64.8(16) . . . . ?
B18 B17 B20 B19 -35.6(13) . . . . ?
B18 B17 B19 B13 103.0(17) . . . . ?
B18 B17 B19 B14 38.3(14) . . . . ?
B18 B17 B19 B20 140.2(16) . . . . ?
B20 C39 B12 C40 102.4(14) . . . . ?
B20 C39 B12 B13 39.9(14) . . . . ?
B20 C39 B12 B11 143.2(14) . . . . ?
B20 C39 B16 B11 -106.9(16) . . . . ?
B20 C39 B16 B15 -65.5(18) . . . . ?
B20 C39 B16 B17 39.1(15) . . . . ?
B20 C39 B16 B18 0(2) . . . . ?
B20 C39 B11 C40 3.0(17) . . . . ?
B20 C39 B11 B12 -35.4(13) . . . . ?
B20 C39 B11 B16 102.6(15) . . . . ?
B20 C39 B11 B15 65.3(17) . . . . ?
B20 C39 B17 B16 -139.1(16) . . . . ?
B20 C39 B17 B18 -101.6(15) . . . . ?
B20 C39 B17 B19 -39.5(14) . . . . ?
B20 B13 B12 C39 -38.8(13) . . . . ?
B20 B13 B12 C40 -135.0(16) . . . . ?
B20 B13 B12 B11 -100.2(16) . . . . ?
B20 B13 B14 C40 96.9(14) . . . . ?
B20 B13 B14 B15 62.2(17) . . . . ?
B20 B13 B14 B18 -1.6(16) . . . . ?
B20 B13 B14 B19 -37.1(13) . . . . ?
B20 B13 B19 B14 137.3(14) . . . . ?
B20 B13 B19 B17 37.0(13) . . . . ?
B20 B13 B19 B18 101.1(15) . . . . ?
B20 B12 B11 C39 32.8(12) . . . . ?
B20 B12 B11 C40 -100.3(15) . . . . ?
B20 B12 B11 B16 -5.1(18) . . . . ?
B20 B12 B11 B15 -64.5(16) . . . . ?
B20 B17 B18 B16 -100.7(16) . . . . ?
B20 B17 B18 B15 -65.4(16) . . . . ?
B20 B17 B18 B14 -2.8(16) . . . . ?
B20 B17 B18 B19 35.5(12) . . . . ?
B20 B17 B19 B13 -37.2(14) . . . . ?
B20 B17 B19 B14 -101.9(15) . . . . ?
B20 B17 B19 B18 -140.2(16) . . . . ?
B7 C14 B5 C13 -5(2) . . . . ?
B7 C14 B5 B6 36.1(17) . . . . ?
B7 C14 B5 B4 -108(2) . . . . ?
B7 C14 B5 B10 -65(2) . . . . ?
B7 C14 B6 C13 -101.2(15) . . . . ?
B7 C14 B6 B5 -143.2(17) . . . . ?
B7 C14 B6 B9 -41.7(15) . . . . ?
B7 C14 B4 B5 105.3(18) . . . . ?
B7 C14 B4 B3 2(2) . . . . ?
B7 C14 B4 B8 -37.9(17) . . . . ?
B7 C14 B4 B10 63(2) . . . . ?
B7 C14 B8 B2 38.9(16) . . . . ?
B7 C14 B8 B4 142.5(16) . . . . ?
B7 C14 B8 B3 101.7(16) . . . . ?
B7 B2 B3 B4 0(2) . . . . ?
B7 B2 B3 B1 -98.9(17) . . . . ?
B7 B2 B3 B8 38.4(15) . . . . ?
B7 B2 B3 B10 -61(2) . . . . ?
B7 B2 B1 C13 0(2) . . . . ?
B7 B2 B1 B3 100.4(17) . . . . ?
B7 B2 B1 B9 -39.0(15) . . . . ?
B7 B2 B1 B10 61(2) . . . . ?
B7 B2 B8 C14 -37.6(15) . . . . ?
B7 B2 B8 B4 -98.3(17) . . . . ?
B7 B2 B8 B3 -137.0(17) . . . . ?
B7 B2 B9 C13 97.0(16) . . . . ?
B7 B2 B9 B6 35.5(16) . . . . ?
B7 B2 B9 B1 136.2(16) . . . . ?
B7 B6 B9 C13 -136.6(16) . . . . ?
B7 B6 B9 B2 -36.5(17) . . . . ?
B7 B6 B9 B1 -101.9(17) . . . . ?
B19 B13 B12 C39 -1.4(19) . . . . ?
B19 B13 B12 C40 -97.6(16) . . . . ?
B19 B13 B12 B11 -62.8(18) . . . . ?
B19 B13 B12 B20 37.4(14) . . . . ?
B19 B13 B14 C40 134.1(15) . . . . ?
B19 B13 B14 B15 99.3(16) . . . . ?
B19 B13 B14 B18 35.5(12) . . . . ?
B19 B13 B20 C39 -98.5(15) . . . . ?
B19 B13 B20 B12 -136.9(16) . . . . ?
B19 B13 B20 B17 -37.3(13) . . . . ?
B19 B14 B18 B16 101.8(14) . . . . ?
B19 B14 B18 B15 137.3(14) . . . . ?
B19 B14 B18 B17 38.3(12) . . . . ?
B19 B17 B18 B16 -136.1(16) . . . . ?
B19 B17 B18 B15 -100.8(15) . . . . ?
B19 B17 B18 B14 -38.3(12) . . . . ?
B19 B17 B20 C39 134.3(16) . . . . ?
B19 B17 B20 B13 37.4(13) . . . . ?
B19 B17 B20 B12 100.4(16) . . . . ?
B1 C13 B5 C14 -65.3(18) . . . . ?
B1 C13 B5 B6 -106.0(16) . . . . ?
B1 C13 B5 B4 -4(2) . . . . ?
B1 C13 B5 B10 35.1(16) . . . . ?
B1 C13 B6 C14 62.0(17) . . . . ?
B1 C13 B6 B5 104.2(15) . . . . ?
B1 C13 B6 B7 1.6(18) . . . . ?
B1 C13 B6 B9 -37.0(14) . . . . ?
B1 C13 B9 B2 40.3(15) . . . . ?
B1 C13 B9 B6 141.0(14) . . . . ?
B1 C13 B9 B7 103.8(17) . . . . ?
B1 C13 B10 B5 -142.9(16) . . . . ?
B1 C13 B10 B4 -103.8(18) . . . . ?
B1 C13 B10 B3 -38.2(14) . . . . ?
B1 B2 B3 B4 99.2(18) . . . . ?
B1 B2 B3 B8 137.3(17) . . . . ?
B1 B2 B3 B10 38.0(15) . . . . ?
B1 B2 B7 C14 -60(2) . . . . ?
B1 B2 B7 B6 1(2) . . . . ?
B1 B2 B7 B8 -98.7(19) . . . . ?
B1 B2 B7 B9 37.9(15) . . . . ?
B1 B2 B8 C14 63(2) . . . . ?
B1 B2 B8 B4 2(2) . . . . ?
B1 B2 B8 B3 -36.6(16) . . . . ?
B1 B2 B8 B7 100.4(18) . . . . ?
B1 B2 B9 C13 -39.2(14) . . . . ?
B1 B2 B9 B6 -100.8(17) . . . . ?
B1 B2 B9 B7 -136.2(16) . . . . ?
B1 B3 B8 C14 -59.4(18) . . . . ?
B1 B3 B8 B2 38.2(14) . . . . ?
B1 B3 B8 B4 -98.9(17) . . . . ?
B1 B3 B8 B7 0.1(19) . . . . ?
B1 B3 B10 C13 38.0(15) . . . . ?
B1 B3 B10 B5 102.1(18) . . . . ?
B1 B3 B10 B4 138.4(17) . . . . ?
B8 C14 B5 C13 66.9(17) . . . . ?
B8 C14 B5 B6 107.9(16) . . . . ?
B8 C14 B5 B4 -35.8(15) . . . . ?
B8 C14 B5 B10 6.8(19) . . . . ?
B8 C14 B6 C13 -62.8(18) . . . . ?
B8 C14 B6 B5 -104.8(18) . . . . ?
B8 C14 B6 B7 38.4(17) . . . . ?
B8 C14 B6 B9 -3(2) . . . . ?
B8 C14 B4 B5 143.3(16) . . . . ?
B8 C14 B4 B3 39.8(16) . . . . ?
B8 C14 B4 B10 101.1(18) . . . . ?
B8 C14 B7 B2 -39.3(16) . . . . ?
B8 C14 B7 B6 -141.6(18) . . . . ?
B8 C14 B7 B9 -99.8(19) . . . . ?
B8 B2 B3 B4 -38.1(15) . . . . ?
B8 B2 B3 B1 -137.3(17) . . . . ?
B8 B2 B3 B10 -99.3(17) . . . . ?
B8 B2 B7 C14 38.7(15) . . . . ?
B8 B2 B7 B6 100.2(17) . . . . ?
B8 B2 B7 B9 136.6(17) . . . . ?
B8 B2 B1 C13 -64(2) . . . . ?
B8 B2 B1 B3 37.3(16) . . . . ?
B8 B2 B1 B9 -102.2(17) . . . . ?
B8 B2 B1 B10 -2(2) . . . . ?
B8 B2 B9 C13 58(2) . . . . ?
B8 B2 B9 B6 -3(2) . . . . ?
B8 B2 B9 B7 -39.0(16) . . . . ?
B8 B2 B9 B1 97.3(19) . . . . ?
B8 B4 B3 B2 38.1(15) . . . . ?
B8 B4 B3 B1 101.4(17) . . . . ?
B8 B4 B3 B10 138.0(17) . . . . ?
B8 B4 B10 C13 63.5(19) . . . . ?
B8 B4 B10 B5 103.1(17) . . . . ?
B8 B4 B10 B3 -36.9(15) . . . . ?
B8 B4 B10 B1 1(2) . . . . ?
B8 B3 B1 C13 61.2(18) . . . . ?
B8 B3 B1 B2 -38.0(14) . . . . ?
B8 B3 B1 B9 -1(2) . . . . ?
B8 B3 B1 B10 99.0(17) . . . . ?
B8 B3 B10 C13 -63.3(18) . . . . ?
B8 B3 B10 B5 1(2) . . . . ?
B8 B3 B10 B4 37.2(15) . . . . ?
B8 B3 B10 B1 -101.2(17) . . . . ?
B8 B7 B9 C13 -64.5(19) . . . . ?
B8 B7 B9 B2 38.1(15) . . . . ?
B8 B7 B9 B6 -101.6(16) . . . . ?
B8 B7 B9 B1 -2.1(19) . . . . ?
B9 C13 B5 C14 2(2) . . . . ?
B9 C13 B5 B6 -38.5(15) . . . . ?
B9 C13 B5 B4 63(2) . . . . ?
B9 C13 B5 B10 102.6(18) . . . . ?
B9 C13 B6 C14 99.0(14) . . . . ?
B9 C13 B6 B5 141.2(14) . . . . ?
B9 C13 B6 B7 38.6(14) . . . . ?
B9 C13 B1 B2 -38.8(15) . . . . ?
B9 C13 B1 B3 -103.4(16) . . . . ?
B9 C13 B1 B10 -141.9(16) . . . . ?
B9 C13 B10 B5 -107.2(16) . . . . ?
B9 C13 B10 B4 -68.1(19) . . . . ?
B9 C13 B10 B3 -2(2) . . . . ?
B9 C13 B10 B1 35.7(15) . . . . ?
B9 B2 B3 B4 64(2) . . . . ?
B9 B2 B3 B1 -35.2(15) . . . . ?
B9 B2 B3 B8 102.1(17) . . . . ?
B9 B2 B3 B10 3(2) . . . . ?
B9 B2 B7 C14 -98.0(17) . . . . ?
B9 B2 B7 B6 -36.5(15) . . . . ?
B9 B2 B7 B8 -136.6(17) . . . . ?
B9 B2 B1 C13 38.5(14) . . . . ?
B9 B2 B1 B3 139.4(16) . . . . ?
B9 B2 B1 B10 100.5(18) . . . . ?
B9 B2 B8 C14 2(2) . . . . ?
B9 B2 B8 B4 -59(2) . . . . ?
B9 B2 B8 B3 -97.9(19) . . . . ?
B9 B2 B8 B7 39.1(18) . . . . ?
B9 B6 B7 C14 132.3(18) . . . . ?
B9 B6 B7 B2 35.4(15) . . . . ?
B9 B6 B7 B8 98.6(17) . . . . ?
B9 B7 B8 C14 97.6(17) . . . . ?
B9 B7 B8 B2 -37.4(14) . . . . ?
B9 B7 B8 B4 65.0(18) . . . . ?
B9 B7 B8 B3 1.2(19) . . . . ?
B9 B1 B10 C13 -33.9(14) . . . . ?
B9 B1 B10 B5 0(2) . . . . ?
B9 B1 B10 B4 64(2) . . . . ?
B9 B1 B10 B3 102.9(16) . . . . ?
B10 C13 B5 C14 -100.4(15) . . . . ?
B10 C13 B5 B6 -141.1(15) . . . . ?
B10 C13 B5 B4 -39.4(16) . . . . ?
B10 C13 B6 C14 -5.8(17) . . . . ?
B10 C13 B6 B5 36.4(13) . . . . ?
B10 C13 B6 B7 -66.2(17) . . . . ?
B10 C13 B6 B9 -104.8(16) . . . . ?
B10 C13 B1 B2 103.2(18) . . . . ?
B10 C13 B1 B3 38.6(15) . . . . ?
B10 C13 B1 B9 141.9(16) . . . . ?
B10 C13 B9 B2 4(2) . . . . ?
B10 C13 B9 B6 105.1(16) . . . . ?
B10 C13 B9 B7 68(2) . . . . ?
B10 C13 B9 B1 -36.0(15) . . . . ?
B10 B5 B6 C14 96.3(16) . . . . ?
B10 B5 B6 C13 -34.1(14) . . . . ?
B10 B5 B6 B7 63.7(18) . . . . ?
B10 B5 B6 B9 -0.4(18) . . . . ?
B10 B5 B4 C14 -131.2(16) . . . . ?
B10 B5 B4 B3 -35.6(15) . . . . ?
B10 B5 B4 B8 -98.5(17) . . . . ?
B10 B4 B3 B2 -99.9(18) . . . . ?
B10 B4 B3 B1 -36.6(15) . . . . ?
B10 B4 B3 B8 -138.0(17) . . . . ?
B10 B4 B8 C14 -96.7(17) . . . . ?
B10 B4 B8 B2 -2(2) . . . . ?
B10 B4 B8 B3 36.9(16) . . . . ?
B10 B4 B8 B7 -64.6(19) . . . . ?
B10 B3 B1 C13 -37.7(14) . . . . ?
B10 B3 B1 B2 -137.0(17) . . . . ?
B10 B3 B1 B9 -100.4(17) . . . . ?
B10 B3 B8 C14 3.2(19) . . . . ?
B10 B3 B8 B2 100.8(17) . . . . ?
B10 B3 B8 B4 -36.4(14) . . . . ?
B10 B3 B8 B7 62.7(18) . . . . ?
B10 B1 B9 C13 33.8(14) . . . . ?
B10 B1 B9 B2 -102.0(16) . . . . ?
B10 B1 B9 B6 -0.4(19) . . . . ?
B10 B1 B9 B7 -62.3(19) . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 -0.252 0.000 0.000 843.9 97.6 ?
2 -0.389 0.500 0.500 843.9 97.6 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_mo_xhh_m_dcm_bf4_0m_pl
_database_code_depnum_ccdc_archive 'CCDC 2495512'
loop_
_audit_author_name
_audit_author_address
'Hao-Hui Xie'
;NanJing University of Science and Technology
China
;
_audit_update_record             
;
2025-10-15 deposited with the CCDC.	2026-03-06 downloaded from the CCDC.
;
_audit_creation_date             2025-10-07
_audit_creation_method           
;
Olex2 1.5
(compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C52 H60 Au8 B20 P4 S4, C H2 Cl2'
_chemical_formula_sum            'C53 H62 Au8 B20 Cl2 P4 S4'
_chemical_formula_weight         2824.78
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   13.3226(17)
_cell_length_b                   23.431(3)
_cell_length_c                   26.702(4)
_cell_angle_alpha                90
_cell_angle_beta                 93.581(5)
_cell_angle_gamma                90
_cell_volume                     8319(2)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    805
_cell_measurement_temperature    100.15
_cell_measurement_theta_max      55.168
_cell_measurement_theta_min      4.536
_shelx_estimated_absorpt_T_max   0.534
_shelx_estimated_absorpt_T_min   0.394
_exptl_absorpt_coefficient_mu    14.324
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_correction_T_min  0.2895
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1907 before and 0.1243 after correction.
The Ratio of minimum to maximum transmission is 0.3883.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            yellow
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    2.255
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             5100
_exptl_crystal_preparation       ?
_exptl_crystal_size_max          0.08
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.05
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.2642
_diffrn_reflns_av_unetI/netI     0.1298
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.992
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       30
_diffrn_reflns_limit_k_min       -30
_diffrn_reflns_limit_l_max       34
_diffrn_reflns_limit_l_min       -34
_diffrn_reflns_number            192735
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.992
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.584
_diffrn_reflns_theta_min         2.268
_diffrn_ambient_temperature      100.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  multi-scan
_diffrn_measurement_method       ?
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_source_current           1.6
_diffrn_source_power             0.08
_diffrn_source_voltage           50.0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                13420
_reflns_number_total             19124
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'olex2.solve 1.5 (Bourhis et al., 2015)'
_refine_diff_density_max         6.070
_refine_diff_density_min         -3.152
_refine_diff_density_rms         0.416
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.049
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     805
_refine_ls_number_reflns         19124
_refine_ls_number_restraints     199
_refine_ls_R_factor_all          0.0925
_refine_ls_R_factor_gt           0.0650
_refine_ls_restrained_S_all      1.049
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0762P)²+16.4983P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1688
_refine_ls_wR_factor_ref         0.1901
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups, All C(H,H) groups
2. Restrained distances
 Cl2-C4
 1.78 with sigma of 0.02
 Cl3-C4
 1.77 with sigma of 0.02
 Cl2-C4 = Cl3-C4
 1.771 with sigma of 0.01
 Cl2-Cl3
 2.916 with sigma of 0.03
 Cl2-Cl3
 2.92 with sigma of 0.04
3. Uiso/Uaniso restraints and constraints
Cl2 \\sim Cl3 \\sim C4: within 2A with sigma of 0.04 and sigma for terminal
atoms of 0.08 within 2A
B02F \\sim B023: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02 within 2A
C63 \\sim B023 \\sim C39 \\sim C162 \\sim C05F \\sim C17 \\sim C40: within 2A
with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
C01X \\sim C01A \\sim C02R \\sim C02E \\sim C03H \\sim C32: within 2A with
sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
C011 \\sim B036 \\sim B02K \\sim B02N \\sim B01B \\sim B012: within 2A with
sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
B026 \\sim B01P \\sim B02F \\sim B023 \\sim B01Z: within 2A with sigma of 0.01
and sigma for terminal atoms of 0.02 within 2A
B02F \\sim B01P \\sim B026 \\sim B02Y: within 2A with sigma of 0.01 and sigma
for terminal atoms of 0.02 within 2A
4. Rigid body (RIGU) restrains
 Cl2, Cl3, C4
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
5. Others
 Fixed X: Cl3(-0.72291)
 Fixed Y: Cl3(-0.30383)
 Fixed Z: Cl3(-0.02685)
6.a Secondary CH2 refined with riding coordinates:
 C4(H4a,H4b)
6.b Aromatic/amide H refined with riding coordinates:
 C00X(H00X), C01A(H01A), C01E(H01E), C01F(H01F), C01G(H01G), C01M(H01M),
 C01N(H01N), C01O(H01O), C01S(H01S), C020(H020), C024(H024), C029(H029),
 C19(H19), C02C(H02C), C02E(H02E), C02G(H02G), C23(H23), C02T(H02T), C040(H040),
  C02L(H02L), C03W(H03W), C02R(H02R), C02W(H02W), C039(H039), C32(H32),
 C03F(H03F), C03H(H03H), C03P(H03P), C03U(H03U), C03X(H03X), C041(H041),
 C048(H048), C04O(H04O), C059(H059), C39(H39), C162(H162), C63(H63), C40(H40),
 C17(H17), C(H)
6.c Fitted hexagon refined as free rotating group:
 C05F(C39,C162,C63,C40,C17)
6.d Boron cage BH refined with riding coordinates:
 B012(H012), B01B(H01B), B01P(H01P), B01V(H01V), B01Z(H01Z), B023(H023),
 B026(H026), B028(H028), B02F(H02F), B02H(H02H), B02K(H02K), B02N(H02N),
 B02Y(H02Y), B036(H036), B03B(H03B), B03O(H03O), B03Q(H03Q), B03R(H03R),
 B03S(H03S), B049(H049)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     iterative
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au3 Au -0.29377(4) 0.07318(2) 0.14935(2) 0.01887(13) Uani 1 1 d . . . . .
Au4 Au -0.25166(4) -0.02868(2) 0.08907(2) 0.02139(13) Uani 1 1 d . . . . .
Au5 Au -0.21692(4) -0.12618(2) 0.02342(2) 0.02069(13) Uani 1 1 d . . . . .
Au2 Au -0.35553(4) -0.04448(2) 0.19460(2) 0.02294(14) Uani 1 1 d . . . . .
Au7 Au 0.04539(4) -0.09250(2) 0.21817(2) 0.02407(14) Uani 1 1 d . . . . .
Au1 Au -0.39043(5) -0.16708(2) 0.22470(2) 0.02571(14) Uani 1 1 d . . . . .
Au6 Au -0.07497(4) -0.12072(2) 0.12443(2) 0.02493(14) Uani 1 1 d . . . . .
Au8 Au -0.17259(5) -0.13357(2) 0.23187(2) 0.02778(15) Uani 1 1 d . . . . .
S00J S -0.4023(3) 0.00113(14) 0.12037(15) 0.0229(8) Uani 1 1 d . . . . .
S00Q S -0.1030(3) -0.05949(16) 0.05662(15) 0.0263(8) Uani 1 1 d . . . . .
S00T S -0.3087(3) -0.09246(16) 0.26796(16) 0.0326(9) Uani 1 1 d . . . . .
S00V S -0.0388(3) -0.17624(15) 0.19565(17) 0.0308(9) Uani 1 1 d . . . . .
P00I P -0.4801(3) -0.23744(15) 0.18475(15) 0.0218(8) Uani 1 1 d . . . . .
P00L P -0.1839(2) 0.14381(15) 0.16944(14) 0.0176(7) Uani 1 1 d . . . . .
P00P P -0.3347(3) -0.18819(15) -0.00805(14) 0.0196(7) Uani 1 1 d . . . . .
P00W P 0.1346(3) -0.01170(15) 0.23052(16) 0.0247(8) Uani 1 1 d . . . . .
C00X C -0.6008(12) -0.1549(7) 0.1400(7) 0.035(4) Uani 1 1 d . . . . .
H00X H -0.538867 -0.135168 0.138388 0.042 Uiso 1 1 calc R U . . .
C010 C -0.0890(9) 0.1229(5) 0.2213(6) 0.019(3) Uani 1 1 d . . . . .
C011 C -0.4195(9) -0.2662(6) 0.1294(5) 0.020(2) Uani 1 1 d . U . . .
C019 C -0.3044(9) -0.2225(6) -0.0669(5) 0.019(3) Uani 1 1 d . . . . .
C01A C 0.1203(12) 0.0029(6) 0.1283(6) 0.031(3) Uani 1 1 d . U . . .
H01A H 0.051818 -0.006733 0.131768 0.038 Uiso 1 1 calc R U . . .
C01D C -0.3502(10) -0.2448(6) 0.0381(6) 0.024(3) Uani 1 1 d . . . . .
C01E C -0.4734(12) -0.1047(7) 0.0082(6) 0.031(4) Uani 1 1 d . . . . .
H01E H -0.417832 -0.086022 0.025131 0.037 Uiso 1 1 calc R U . . .
C01F C -0.5657(10) -0.0811(8) 0.0090(6) 0.032(4) Uani 1 1 d . . . . .
H01F H -0.574876 -0.046717 0.027027 0.038 Uiso 1 1 calc R U . . .
C01G C -0.1919(12) -0.2168(7) -0.1347(6) 0.031(4) Uani 1 1 d . . . . .
H01G H -0.138884 -0.198987 -0.151103 0.037 Uiso 1 1 calc R U . . .
C01I C 0.0571(10) 0.0495(6) 0.2498(5) 0.021(3) Uani 1 1 d . . . . .
C01M C -0.3481(11) -0.2686(6) -0.0888(5) 0.022(3) Uani 1 1 d . . . . .
H01M H -0.401733 -0.286037 -0.072712 0.026 Uiso 1 1 calc R U . . .
C01N C -0.0476(11) 0.1248(6) 0.0404(6) 0.030(4) Uani 1 1 d . . . . .
H01N H -0.036660 0.093749 0.018518 0.036 Uiso 1 1 calc R U . . .
C01O C -0.6497(12) -0.1079(8) -0.0175(6) 0.036(4) Uani 1 1 d . . . . .
H01O H -0.714024 -0.090329 -0.018379 0.044 Uiso 1 1 calc R U . . .
C01S C -0.2394(11) -0.2667(7) -0.1555(6) 0.032(4) Uani 1 1 d . . . . .
H01S H -0.216023 -0.283127 -0.185140 0.038 Uiso 1 1 calc R U . . .
C01X C 0.1848(12) 0.0078(7) 0.1703(7) 0.037(3) Uani 1 1 d . U . . .
C020 C -0.0915(13) 0.1152(6) 0.0841(6) 0.032(4) Uani 1 1 d . . . . .
H020 H -0.107112 0.077135 0.093029 0.038 Uiso 1 1 calc R U . . .
C024 C -0.1930(13) 0.2581(6) 0.2085(7) 0.038(4) Uani 1 1 d . . . . .
H024 H -0.123298 0.255689 0.218333 0.045 Uiso 1 1 calc R U . . .
C029 C -0.3206(13) -0.2918(7) -0.1324(6) 0.034(4) Uani 1 1 d . . . . .
H029 H -0.354932 -0.323931 -0.146825 0.041 Uiso 1 1 calc R U . . .
C19 C -0.2428(13) 0.3080(7) 0.2160(9) 0.052(6) Uani 1 1 d . . . . .
H19 H -0.207952 0.339181 0.231704 0.062 Uiso 1 1 calc R U . . .
C02B C -0.4573(10) -0.1559(6) -0.0168(5) 0.020(3) Uani 1 1 d . . . . .
C02C C -0.7797(13) -0.1563(9) 0.1271(8) 0.053(6) Uani 1 1 d . . . . .
H02C H -0.840634 -0.137789 0.116176 0.063 Uiso 1 1 calc R U . . .
C02E C 0.2577(12) 0.0273(7) 0.0774(8) 0.038(3) Uani 1 1 d . U . . .
H02E H 0.283504 0.033249 0.045440 0.046 Uiso 1 1 calc R U . . .
C02G C -0.4287(10) -0.3044(6) 0.2669(6) 0.026(3) Uani 1 1 d . . . . .
H02G H -0.384286 -0.273782 0.275692 0.031 Uiso 1 1 calc R U . . .
C23 C -0.0378(14) 0.2250(8) 0.0577(7) 0.045(5) Uani 1 1 d . . . . .
H23 H -0.019135 0.262480 0.048486 0.054 Uiso 1 1 calc R U . . .
C02D C -0.4934(10) -0.3012(6) 0.2237(5) 0.021(3) Uani 1 1 d . . . . .
C02T C -0.5570(13) -0.3474(7) 0.2115(6) 0.032(4) Uani 1 1 d . . . . .
H02T H -0.599945 -0.346291 0.181727 0.038 Uiso 1 1 calc R U . . .
C040 C -0.5577(11) -0.3934(6) 0.2418(6) 0.029(3) Uani 1 1 d . . . . .
H040 H -0.602867 -0.423985 0.234159 0.035 Uiso 1 1 calc R U . . .
C02L C -0.4930(12) -0.3958(7) 0.2837(6) 0.032(4) Uani 1 1 d . . . . .
H02L H -0.491631 -0.428657 0.304617 0.039 Uiso 1 1 calc R U . . .
C03W C -0.4299(12) -0.3506(8) 0.2954(7) 0.040(4) Uani 1 1 d . . . . .
H03W H -0.385940 -0.352573 0.324768 0.048 Uiso 1 1 calc R U . . .
C02I C -0.1140(9) 0.1590(6) 0.1159(6) 0.021(3) Uani 1 1 d . . . . .
C02R C 0.1545(12) 0.0118(6) 0.0807(7) 0.035(3) Uani 1 1 d . U . . .
H02R H 0.110725 0.007829 0.051415 0.041 Uiso 1 1 calc R U . . .
C02W C -0.2231(12) -0.1952(7) -0.0917(6) 0.032(4) Uani 1 1 d . . . . .
H02W H -0.191870 -0.161984 -0.077455 0.039 Uiso 1 1 calc R U . . .
C039 C -0.0185(12) 0.1797(7) 0.0273(7) 0.038(4) Uani 1 1 d . . . . .
H039 H 0.014841 0.185701 -0.002712 0.045 Uiso 1 1 calc R U . . .
C32 C 0.2844(13) 0.0199(8) 0.1678(8) 0.049(3) Uani 1 1 d . U . . .
H32 H 0.330048 0.019660 0.196558 0.059 Uiso 1 1 calc R U . . .
C03F C -0.5398(11) -0.1823(7) -0.0427(7) 0.034(4) Uani 1 1 d . . . . .
H03F H -0.529424 -0.216247 -0.061047 0.041 Uiso 1 1 calc R U . . .
C03H C 0.3161(14) 0.0332(9) 0.1176(8) 0.051(4) Uani 1 1 d . U . . .
H03H H 0.382565 0.046760 0.114369 0.061 Uiso 1 1 calc R U . . .
C03I C -0.2419(10) 0.2101(6) 0.1868(5) 0.022(3) Uani 1 1 d . . . . .
C03P C -0.6377(13) -0.1594(7) -0.0420(6) 0.034(4) Uani 1 1 d . . . . .
H03P H -0.693739 -0.178729 -0.057842 0.040 Uiso 1 1 calc R U . . .
C03U C -0.6941(14) -0.2346(8) 0.1677(8) 0.057(6) Uani 1 1 d . . . . .
H03U H -0.696343 -0.269999 0.184969 0.068 Uiso 1 1 calc R U . . .
C03X C -0.0854(13) 0.2158(7) 0.1024(7) 0.039(4) Uani 1 1 d . . . . .
H03X H -0.098567 0.247015 0.123642 0.047 Uiso 1 1 calc R U . . .
C041 C -0.3427(11) 0.2158(7) 0.1701(6) 0.031(4) Uani 1 1 d . . . . .
H041 H -0.377629 0.184335 0.154785 0.038 Uiso 1 1 calc R U . . .
C048 C -0.7792(13) -0.2106(10) 0.1496(10) 0.070(8) Uani 1 1 d . . . . .
H048 H -0.840859 -0.230507 0.151919 0.084 Uiso 1 1 calc R U . . .
C04O C -0.3405(14) 0.3133(7) 0.2013(9) 0.050(5) Uani 1 1 d . . . . .
H04O H -0.375410 0.347626 0.207794 0.060 Uiso 1 1 calc R U . . .
C059 C -0.3919(13) 0.2672(7) 0.1757(8) 0.045(5) Uani 1 1 d . . . . .
H059 H -0.459478 0.271840 0.162740 0.054 Uiso 1 1 calc R U . . .
C05F C 0.2248(12) -0.0155(6) 0.2847(6) 0.086(5) Uani 1 1 d G U . . .
C39 C 0.2066(11) -0.0572(6) 0.3201(7) 0.098(6) Uani 1 1 d G U . . .
H39 H 0.150117 -0.081735 0.315073 0.118 Uiso 1 1 calc R U . . .
C162 C 0.2709(14) -0.0629(7) 0.3628(6) 0.108(6) Uani 1 1 d G U . . .
H162 H 0.258462 -0.091333 0.386991 0.130 Uiso 1 1 calc R U . . .
C63 C 0.3535(13) -0.0269(7) 0.3702(6) 0.106(6) Uani 1 1 d G U . . .
H63 H 0.397517 -0.030814 0.399367 0.127 Uiso 1 1 calc R U . . .
C40 C 0.3718(11) 0.0147(6) 0.3348(6) 0.090(5) Uani 1 1 d G U . . .
H40 H 0.428229 0.039304 0.339825 0.109 Uiso 1 1 calc R U . . .
C17 C 0.3074(12) 0.0204(6) 0.2921(5) 0.079(5) Uani 1 1 d G U . . .
H17 H 0.319885 0.048902 0.267907 0.094 Uiso 1 1 calc R U . . .
C C -0.6852(14) -0.1305(7) 0.1216(7) 0.038(4) Uani 1 1 d . . . . .
H H -0.681855 -0.095153 0.104454 0.046 Uiso 1 1 calc R U . . .
B012 B -0.3437(11) -0.2181(6) 0.0997(6) 0.018(2) Uani 1 1 d . U . . .
H012 H -0.332739 -0.172105 0.109993 0.022 Uiso 1 1 calc R U . . .
C1 C -0.6016(10) -0.2086(7) 0.1616(6) 0.030(4) Uani 1 1 d . . . . .
B01B B -0.4603(11) -0.2447(7) 0.0715(6) 0.020(2) Uani 1 1 d . U . . .
H01B H -0.525227 -0.215008 0.063563 0.024 Uiso 1 1 calc R U . . .
B01P B -0.0410(12) 0.0321(7) 0.2868(7) 0.024(3) Uani 1 1 d . U . . .
H01P H -0.056075 -0.011699 0.301328 0.029 Uiso 1 1 calc R U . . .
B01V B -0.2662(14) -0.3348(8) 0.0954(6) 0.027(4) Uani 1 1 d . . . . .
H01V H -0.203150 -0.365939 0.102729 0.033 Uiso 1 1 calc R U . . .
B01Z B 0.1027(13) 0.1184(6) 0.2618(7) 0.024(3) Uani 1 1 d . U . . .
H01Z H 0.183376 0.131199 0.259914 0.029 Uiso 1 1 calc R U . . .
B023 B 0.0289(12) 0.1036(6) 0.2067(7) 0.020(3) Uani 1 1 d . U . . .
H023 H 0.058818 0.106269 0.168475 0.024 Uiso 1 1 calc R U . . .
B026 B -0.1358(12) 0.0795(7) 0.2657(7) 0.023(3) Uani 1 1 d . U . . .
H026 H -0.217000 0.067167 0.265343 0.028 Uiso 1 1 calc R U . . .
B028 B -0.3006(12) -0.3119(7) 0.0338(7) 0.025(4) Uani 1 1 d . . . . .
H028 H -0.260461 -0.325986 0.000283 0.030 Uiso 1 1 calc R U . . .
B02F B -0.0612(12) 0.0502(6) 0.2220(7) 0.021(3) Uani 1 1 d . U . . .
H02F H -0.090686 0.018181 0.193620 0.025 Uiso 1 1 calc R U . . .
B02H B -0.0931(14) 0.1508(8) 0.2803(7) 0.031(4) Uani 1 1 d . . . . .
H02H H -0.145091 0.185811 0.290739 0.037 Uiso 1 1 calc R U . . .
B02K B -0.3714(11) -0.3353(6) 0.1311(6) 0.019(2) Uani 1 1 d . U . . .
H02K H -0.377081 -0.365216 0.163564 0.022 Uiso 1 1 calc R U . . .
B02N B -0.2894(11) -0.2760(7) 0.1354(6) 0.021(2) Uani 1 1 d . U . . .
H02N H -0.241555 -0.266859 0.170457 0.025 Uiso 1 1 calc R U . . .
B02Y B -0.0636(12) 0.0938(7) 0.3229(7) 0.025(3) Uani 1 1 d . U . . .
H02Y H -0.095654 0.090967 0.360600 0.030 Uiso 1 1 calc R U . . .
B036 B -0.4789(12) -0.3156(6) 0.0908(6) 0.021(2) Uani 1 1 d . U . . .
H036 H -0.555990 -0.332859 0.095939 0.025 Uiso 1 1 calc R U . . .
B03B B -0.3812(13) -0.3587(8) 0.0696(7) 0.028(4) Uani 1 1 d . . . . .
H03B H -0.394058 -0.404867 0.060519 0.033 Uiso 1 1 calc R U . . .
B03O B 0.0614(12) 0.0729(7) 0.3119(6) 0.025(4) Uani 1 1 d . . . . .
H03O H 0.114127 0.055515 0.342485 0.030 Uiso 1 1 calc R U . . .
B03Q B 0.0285(14) 0.1469(8) 0.3081(7) 0.033(4) Uani 1 1 d . . . . .
H03Q H 0.058941 0.178423 0.336746 0.040 Uiso 1 1 calc R U . . .
B03R B -0.2435(12) -0.2636(7) 0.0775(7) 0.025(4) Uani 1 1 d . . . . .
H03R H -0.165375 -0.247082 0.073851 0.030 Uiso 1 1 calc R U . . .
B03S B 0.0065(11) 0.1644(7) 0.2425(7) 0.025(4) Uani 1 1 d . . . . .
H03S H 0.020694 0.208001 0.227251 0.030 Uiso 1 1 calc R U . . .
B049 B -0.4369(15) -0.3026(7) 0.0299(7) 0.031(4) Uani 1 1 d . . . . .
H049 H -0.484800 -0.311347 -0.005282 0.037 Uiso 1 1 calc R U . . .
Cl2 Cl -0.8548(18) -0.3169(11) 0.0555(9) 0.432(17) Uani 1 1 d D U . . .
Cl3 Cl -0.722911 -0.303830 -0.026851 0.352(13) Uani 1 1 d D U . . .
C4 C -0.7576(15) -0.2752(9) 0.0312(5) 0.096(10) Uani 1 1 d D U . . .
H4A H -0.698365 -0.274847 0.055531 0.116 Uiso 1 1 calc R U . . .
H4B H -0.781071 -0.235437 0.026264 0.116 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au3 Au4 2.9519(8) . ?
Au3 Au2 3.1402(8) . ?
Au3 S00J 2.323(3) . ?
Au3 P00L 2.252(3) . ?
Au4 Au5 2.9338(8) . ?
Au4 Au2 3.2371(9) . ?
Au4 Au6 3.2872(8) . ?
Au4 S00J 2.328(4) . ?
Au4 S00Q 2.326(4) . ?
Au5 Au6 3.1983(9) . ?
Au5 S00Q 2.316(4) . ?
Au5 P00P 2.261(3) . ?
Au2 Au1 3.0267(8) . ?
Au2 Au8 3.3144(8) . ?
Au2 S00J 2.303(4) . ?
Au2 S00T 2.311(4) . ?
Au7 Au6 2.9618(9) . ?
Au7 Au8 3.1025(9) . ?
Au7 S00V 2.321(4) . ?
Au7 P00W 2.249(4) . ?
Au1 Au8 3.0011(9) . ?
Au1 S00T 2.328(4) . ?
Au1 P00I 2.263(4) . ?
Au6 Au8 3.2371(10) . ?
Au6 S00Q 2.322(4) . ?
Au6 S00V 2.330(4) . ?
Au8 S00T 2.315(4) . ?
Au8 S00V 2.308(4) . ?
P00I C011 1.854(15) . ?
P00I C02D 1.836(14) . ?
P00I C1 1.826(14) . ?
P00L C010 1.882(14) . ?
P00L C02I 1.790(15) . ?
P00L C03I 1.808(15) . ?
P00P C019 1.832(14) . ?
P00P C01D 1.833(15) . ?
P00P C02B 1.803(14) . ?
P00W C01I 1.859(15) . ?
P00W C01X 1.839(19) . ?
P00W C05F 1.825(10) . ?
C00X H00X 0.9500 . ?
C00X C 1.33(2) . ?
C00X C1 1.38(2) . ?
C010 B023 1.70(2) . ?
C010 B026 1.71(2) . ?
C010 B02F 1.742(19) . ?
C010 B02H 1.71(2) . ?
C010 B03S 1.672(19) . ?
C011 B012 1.74(2) . ?
C011 B01B 1.68(2) . ?
C011 B02K 1.74(2) . ?
C011 B02N 1.747(19) . ?
C011 B036 1.71(2) . ?
C019 C01M 1.344(18) . ?
C019 C02W 1.45(2) . ?
C01A H01A 0.9500 . ?
C01A C01X 1.37(2) . ?
C01A C02R 1.39(2) . ?
C01D B012 1.76(2) . ?
C01D B01B 1.76(2) . ?
C01D B028 1.71(2) . ?
C01D B03R 1.77(2) . ?
C01D B049 1.78(2) . ?
C01E H01E 0.9500 . ?
C01E C01F 1.35(2) . ?
C01E C02B 1.39(2) . ?
C01F H01F 0.9500 . ?
C01F C01O 1.43(2) . ?
C01G H01G 0.9500 . ?
C01G C01S 1.42(2) . ?
C01G C02W 1.35(2) . ?
C01I B01P 1.73(2) . ?
C01I B01Z 1.746(19) . ?
C01I B023 1.74(2) . ?
C01I B02F 1.70(2) . ?
C01I B03O 1.74(2) . ?
C01M H01M 0.9500 . ?
C01M C029 1.36(2) . ?
C01N H01N 0.9500 . ?
C01N C020 1.35(2) . ?
C01N C039 1.40(2) . ?
C01O H01O 0.9500 . ?
C01O C03P 1.39(2) . ?
C01S H01S 0.9500 . ?
C01S C029 1.41(2) . ?
C01X C32 1.36(2) . ?
C020 H020 0.9500 . ?
C020 C02I 1.38(2) . ?
C024 H024 0.9500 . ?
C024 C19 1.36(2) . ?
C024 C03I 1.41(2) . ?
C029 H029 0.9500 . ?
C19 H19 0.9500 . ?
C19 C04O 1.34(2) . ?
C02B C03F 1.40(2) . ?
C02C H02C 0.9500 . ?
C02C C048 1.41(3) . ?
C02C C 1.41(3) . ?
C02E H02E 0.9500 . ?
C02E C02R 1.43(2) . ?
C02E C03H 1.29(2) . ?
C02G H02G 0.9500 . ?
C02G C02D 1.398(19) . ?
C02G C03W 1.32(2) . ?
C23 H23 0.9500 . ?
C23 C039 1.37(3) . ?
C23 C03X 1.40(2) . ?
C02D C02T 1.40(2) . ?
C02T H02T 0.9500 . ?
C02T C040 1.35(2) . ?
C040 H040 0.9500 . ?
C040 C02L 1.37(2) . ?
C02L H02L 0.9500 . ?
C02L C03W 1.38(2) . ?
C03W H03W 0.9500 . ?
C02I C03X 1.44(2) . ?
C02R H02R 0.9500 . ?
C02W H02W 0.9500 . ?
C039 H039 0.9500 . ?
C32 H32 0.9500 . ?
C32 C03H 1.46(3) . ?
C03F H03F 0.9500 . ?
C03F C03P 1.41(2) . ?
C03H H03H 0.9500 . ?
C03I C041 1.395(19) . ?
C03P H03P 0.9500 . ?
C03U H03U 0.9500 . ?
C03U C048 1.33(2) . ?
C03U C1 1.39(2) . ?
C03X H03X 0.9500 . ?
C041 H041 0.9500 . ?
C041 C059 1.39(2) . ?
C048 H048 0.9500 . ?
C04O H04O 0.9500 . ?
C04O C059 1.43(2) . ?
C059 H059 0.9500 . ?
C05F C39 1.3900 . ?
C05F C17 1.3900 . ?
C39 H39 0.9500 . ?
C39 C162 1.3900 . ?
C162 H162 0.9500 . ?
C162 C63 1.3900 . ?
C63 H63 0.9500 . ?
C63 C40 1.3900 . ?
C40 H40 0.9500 . ?
C40 C17 1.3900 . ?
C17 H17 0.9500 . ?
C H 0.9500 . ?
B012 H012 1.1200 . ?
B012 B01B 1.80(2) . ?
B012 B02N 1.78(2) . ?
B012 B03R 1.84(2) . ?
B01B H01B 1.1200 . ?
B01B B036 1.76(2) . ?
B01B B049 1.79(2) . ?
B01P H01P 1.1200 . ?
B01P B026 1.75(2) . ?
B01P B02F 1.78(2) . ?
B01P B02Y 1.77(2) . ?
B01P B03O 1.76(2) . ?
B01V H01V 1.1200 . ?
B01V B028 1.76(2) . ?
B01V B02K 1.74(2) . ?
B01V B02N 1.78(2) . ?
B01V B03B 1.73(2) . ?
B01V B03R 1.77(2) . ?
B01Z H01Z 1.1200 . ?
B01Z B023 1.75(2) . ?
B01Z B03O 1.82(3) . ?
B01Z B03Q 1.76(3) . ?
B01Z B03S 1.73(2) . ?
B023 H023 1.1200 . ?
B023 B02F 1.80(2) . ?
B023 B03S 1.75(2) . ?
B026 H026 1.1200 . ?
B026 B02F 1.72(2) . ?
B026 B02H 1.80(2) . ?
B026 B02Y 1.78(2) . ?
B028 H028 1.1200 . ?
B028 B03B 1.84(3) . ?
B028 B03R 1.77(2) . ?
B028 B049 1.83(3) . ?
B02F H02F 1.1200 . ?
B02H H02H 1.1200 . ?
B02H B02Y 1.78(2) . ?
B02H B03Q 1.74(2) . ?
B02H B03S 1.75(3) . ?
B02K H02K 1.1200 . ?
B02K B02N 1.77(2) . ?
B02K B036 1.80(2) . ?
B02K B03B 1.73(2) . ?
B02N H02N 1.1200 . ?
B02N B03R 1.72(2) . ?
B02Y H02Y 1.1200 . ?
B02Y B03O 1.78(2) . ?
B02Y B03Q 1.81(3) . ?
B036 H036 1.1200 . ?
B036 B03B 1.77(2) . ?
B036 B049 1.78(2) . ?
B03B H03B 1.1200 . ?
B03B B049 1.82(3) . ?
B03O H03O 1.1200 . ?
B03O B03Q 1.79(3) . ?
B03Q H03Q 1.1200 . ?
B03Q B03S 1.81(3) . ?
B03R H03R 1.1200 . ?
B03S H03S 1.1200 . ?
B049 H049 1.1200 . ?
Cl2 C4 1.775(9) . ?
Cl3 C4 1.777(9) . ?
C4 H4A 0.9900 . ?
C4 H4B 0.9900 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Au4 Au3 Au2 64.11(2) . . ?
S00J Au3 Au4 50.69(9) . . ?
S00J Au3 Au2 46.98(9) . . ?
P00L Au3 Au4 125.54(9) . . ?
P00L Au3 Au2 137.35(9) . . ?
P00L Au3 S00J 174.22(14) . . ?
Au3 Au4 Au2 60.773(19) . . ?
Au3 Au4 Au6 122.07(2) . . ?
Au5 Au4 Au3 176.18(3) . . ?
Au5 Au4 Au2 121.54(2) . . ?
Au5 Au4 Au6 61.566(19) . . ?
Au2 Au4 Au6 90.71(2) . . ?
S00J Au4 Au3 50.53(8) . . ?
S00J Au4 Au5 128.30(8) . . ?
S00J Au4 Au2 45.34(9) . . ?
S00J Au4 Au6 135.35(10) . . ?
S00Q Au4 Au3 130.49(9) . . ?
S00Q Au4 Au5 50.65(9) . . ?
S00Q Au4 Au2 135.16(10) . . ?
S00Q Au4 Au6 44.94(10) . . ?
S00Q Au4 S00J 178.89(13) . . ?
Au4 Au5 Au6 64.664(19) . . ?
S00Q Au5 Au4 50.96(9) . . ?
S00Q Au5 Au6 46.48(10) . . ?
P00P Au5 Au4 126.21(9) . . ?
P00P Au5 Au6 134.35(10) . . ?
P00P Au5 S00Q 177.04(13) . . ?
Au3 Au2 Au4 55.120(17) . . ?
Au3 Au2 Au8 117.58(2) . . ?
Au4 Au2 Au8 89.26(2) . . ?
Au1 Au2 Au3 169.63(3) . . ?
Au1 Au2 Au4 114.88(2) . . ?
Au1 Au2 Au8 56.275(19) . . ?
S00J Au2 Au3 47.52(8) . . ?
S00J Au2 Au4 45.98(9) . . ?
S00J Au2 Au1 129.14(8) . . ?
S00J Au2 Au8 134.82(9) . . ?
S00J Au2 S00T 178.51(13) . . ?
S00T Au2 Au3 133.63(10) . . ?
S00T Au2 Au4 133.32(11) . . ?
S00T Au2 Au1 49.53(10) . . ?
S00T Au2 Au8 44.29(11) . . ?
Au6 Au7 Au8 64.48(2) . . ?
S00V Au7 Au6 50.57(11) . . ?
S00V Au7 Au8 47.74(10) . . ?
P00W Au7 Au6 124.42(11) . . ?
P00W Au7 Au8 137.21(10) . . ?
P00W Au7 S00V 172.90(16) . . ?
Au8 Au1 Au2 66.711(19) . . ?
S00T Au1 Au2 49.02(10) . . ?
S00T Au1 Au8 49.55(11) . . ?
P00I Au1 Au2 130.65(10) . . ?
P00I Au1 Au8 134.46(10) . . ?
P00I Au1 S00T 175.99(15) . . ?
Au5 Au6 Au4 53.770(17) . . ?
Au5 Au6 Au8 119.64(2) . . ?
Au7 Au6 Au4 115.88(2) . . ?
Au7 Au6 Au5 169.10(2) . . ?
Au7 Au6 Au8 59.87(2) . . ?
Au8 Au6 Au4 89.74(2) . . ?
S00Q Au6 Au4 45.04(9) . . ?
S00Q Au6 Au5 46.32(9) . . ?
S00Q Au6 Au7 124.97(9) . . ?
S00Q Au6 Au8 134.00(9) . . ?
S00Q Au6 S00V 175.28(13) . . ?
S00V Au6 Au4 135.13(11) . . ?
S00V Au6 Au5 138.36(9) . . ?
S00V Au6 Au7 50.30(9) . . ?
S00V Au6 Au8 45.46(10) . . ?
Au7 Au8 Au2 116.45(2) . . ?
Au7 Au8 Au6 55.654(19) . . ?
Au1 Au8 Au2 57.014(19) . . ?
Au1 Au8 Au7 169.17(3) . . ?
Au1 Au8 Au6 114.09(2) . . ?
Au6 Au8 Au2 90.22(2) . . ?
S00T Au8 Au2 44.18(10) . . ?
S00T Au8 Au7 133.08(10) . . ?
S00T Au8 Au1 49.92(10) . . ?
S00T Au8 Au6 134.31(11) . . ?
S00V Au8 Au2 136.02(11) . . ?
S00V Au8 Au7 48.08(9) . . ?
S00V Au8 Au1 128.97(9) . . ?
S00V Au8 Au6 46.00(11) . . ?
S00V Au8 S00T 178.83(13) . . ?
Au3 S00J Au4 78.78(11) . . ?
Au2 S00J Au3 85.50(12) . . ?
Au2 S00J Au4 88.69(12) . . ?
Au5 S00Q Au4 78.40(11) . . ?
Au5 S00Q Au6 87.20(13) . . ?
Au6 S00Q Au4 90.02(14) . . ?
Au2 S00T Au1 81.46(13) . . ?
Au2 S00T Au8 91.53(15) . . ?
Au8 S00T Au1 80.52(13) . . ?
Au7 S00V Au6 79.13(12) . . ?
Au8 S00V Au7 84.18(13) . . ?
Au8 S00V Au6 88.53(13) . . ?
C011 P00I Au1 113.4(4) . . ?
C02D P00I Au1 113.1(5) . . ?
C02D P00I C011 102.6(6) . . ?
C1 P00I Au1 108.7(6) . . ?
C1 P00I C011 106.6(7) . . ?
C1 P00I C02D 112.2(6) . . ?
C010 P00L Au3 112.4(4) . . ?
C02I P00L Au3 108.6(5) . . ?
C02I P00L C010 106.3(6) . . ?
C02I P00L C03I 106.6(7) . . ?
C03I P00L Au3 114.3(4) . . ?
C03I P00L C010 108.3(6) . . ?
C019 P00P Au5 114.6(4) . . ?
C019 P00P C01D 107.5(7) . . ?
C01D P00P Au5 108.7(5) . . ?
C02B P00P Au5 112.3(5) . . ?
C02B P00P C019 108.6(6) . . ?
C02B P00P C01D 104.6(6) . . ?
C01I P00W Au7 113.1(4) . . ?
C01X P00W Au7 107.4(5) . . ?
C01X P00W C01I 106.8(7) . . ?
C05F P00W Au7 113.0(5) . . ?
C05F P00W C01I 99.6(7) . . ?
C05F P00W C01X 116.7(8) . . ?
C C00X H00X 119.4 . . ?
C C00X C1 121.2(17) . . ?
C1 C00X H00X 119.4 . . ?
B023 C010 P00L 119.1(10) . . ?
B023 C010 B026 112.6(11) . . ?
B023 C010 B02F 63.0(8) . . ?
B023 C010 B02H 113.4(11) . . ?
B026 C010 P00L 114.1(9) . . ?
B026 C010 B02F 59.9(9) . . ?
B026 C010 B02H 63.5(10) . . ?
B02F C010 P00L 113.3(9) . . ?
B02H C010 P00L 121.3(9) . . ?
B02H C010 B02F 112.6(12) . . ?
B03S C010 P00L 124.0(10) . . ?
B03S C010 B023 62.5(9) . . ?
B03S C010 B026 114.5(12) . . ?
B03S C010 B02F 114.1(11) . . ?
B03S C010 B02H 62.2(10) . . ?
B012 C011 P00I 115.0(9) . . ?
B012 C011 B02K 113.0(11) . . ?
B012 C011 B02N 61.6(8) . . ?
B01B C011 P00I 119.5(9) . . ?
B01B C011 B012 63.3(9) . . ?
B01B C011 B02K 113.5(11) . . ?
B01B C011 B02N 112.6(11) . . ?
B01B C011 B036 62.5(9) . . ?
B02K C011 P00I 119.7(10) . . ?
B02K C011 B02N 60.9(8) . . ?
B02N C011 P00I 117.0(9) . . ?
B036 C011 P00I 121.2(9) . . ?
B036 C011 B012 115.1(11) . . ?
B036 C011 B02K 62.7(9) . . ?
B036 C011 B02N 112.6(11) . . ?
C01M C019 P00P 127.8(11) . . ?
C01M C019 C02W 118.1(13) . . ?
C02W C019 P00P 114.1(10) . . ?
C01X C01A H01A 119.7 . . ?
C01X C01A C02R 120.6(15) . . ?
C02R C01A H01A 119.7 . . ?
B012 C01D P00P 111.7(9) . . ?
B012 C01D B01B 61.4(9) . . ?
B012 C01D B03R 62.7(9) . . ?
B012 C01D B049 112.4(11) . . ?
B01B C01D P00P 118.1(9) . . ?
B01B C01D B03R 111.3(12) . . ?
B01B C01D B049 60.8(9) . . ?
B028 C01D P00P 124.0(11) . . ?
B028 C01D B012 113.2(11) . . ?
B028 C01D B01B 111.9(12) . . ?
B028 C01D B03R 60.9(8) . . ?
B028 C01D B049 62.9(10) . . ?
B03R C01D P00P 117.3(10) . . ?
B03R C01D B049 112.0(11) . . ?
B049 C01D P00P 124.5(10) . . ?
C01F C01E H01E 119.1 . . ?
C01F C01E C02B 121.8(16) . . ?
C02B C01E H01E 119.1 . . ?
C01E C01F H01F 120.1 . . ?
C01E C01F C01O 119.8(17) . . ?
C01O C01F H01F 120.1 . . ?
C01S C01G H01G 120.4 . . ?
C02W C01G H01G 120.4 . . ?
C02W C01G C01S 119.2(14) . . ?
B01P C01I P00W 115.3(9) . . ?
B01P C01I B01Z 112.3(12) . . ?
B01P C01I B023 114.1(11) . . ?
B01P C01I B03O 60.9(10) . . ?
B01Z C01I P00W 124.8(10) . . ?
B023 C01I P00W 118.7(10) . . ?
B023 C01I B01Z 60.4(8) . . ?
B023 C01I B03O 113.2(11) . . ?
B02F C01I P00W 113.7(9) . . ?
B02F C01I B01P 62.6(9) . . ?
B02F C01I B01Z 111.9(10) . . ?
B02F C01I B023 63.1(8) . . ?
B02F C01I B03O 112.7(12) . . ?
B03O C01I P00W 121.4(9) . . ?
B03O C01I B01Z 63.0(10) . . ?
C019 C01M H01M 117.8 . . ?
C019 C01M C029 124.3(15) . . ?
C029 C01M H01M 117.8 . . ?
C020 C01N H01N 119.6 . . ?
C020 C01N C039 120.7(16) . . ?
C039 C01N H01N 119.6 . . ?
C01F C01O H01O 119.8 . . ?
C03P C01O C01F 120.4(16) . . ?
C03P C01O H01O 119.8 . . ?
C01G C01S H01S 119.8 . . ?
C029 C01S C01G 120.5(14) . . ?
C029 C01S H01S 119.8 . . ?
C01A C01X P00W 116.7(13) . . ?
C32 C01X P00W 120.2(15) . . ?
C32 C01X C01A 122.6(18) . . ?
C01N C020 H020 119.0 . . ?
C01N C020 C02I 122.0(15) . . ?
C02I C020 H020 119.0 . . ?
C19 C024 H024 119.1 . . ?
C19 C024 C03I 121.8(15) . . ?
C03I C024 H024 119.1 . . ?
C01M C029 C01S 117.7(15) . . ?
C01M C029 H029 121.2 . . ?
C01S C029 H029 121.2 . . ?
C024 C19 H19 119.7 . . ?
C04O C19 C024 120.6(17) . . ?
C04O C19 H19 119.7 . . ?
C01E C02B P00P 117.6(11) . . ?
C01E C02B C03F 118.4(14) . . ?
C03F C02B P00P 123.6(12) . . ?
C048 C02C H02C 121.6 . . ?
C048 C02C C 116.7(15) . . ?
C C02C H02C 121.6 . . ?
C02R C02E H02E 119.8 . . ?
C03H C02E H02E 119.8 . . ?
C03H C02E C02R 120.5(19) . . ?
C02D C02G H02G 120.4 . . ?
C03W C02G H02G 120.4 . . ?
C03W C02G C02D 119.3(15) . . ?
C039 C23 H23 120.1 . . ?
C039 C23 C03X 119.8(17) . . ?
C03X C23 H23 120.1 . . ?
C02G C02D P00I 115.7(11) . . ?
C02G C02D C02T 119.0(13) . . ?
C02T C02D P00I 125.1(11) . . ?
C02D C02T H02T 119.9 . . ?
C040 C02T C02D 120.3(15) . . ?
C040 C02T H02T 119.9 . . ?
C02T C040 H040 120.1 . . ?
C02T C040 C02L 119.7(16) . . ?
C02L C040 H040 120.1 . . ?
C040 C02L H02L 120.1 . . ?
C040 C02L C03W 119.8(16) . . ?
C03W C02L H02L 120.1 . . ?
C02G C03W C02L 121.9(17) . . ?
C02G C03W H03W 119.1 . . ?
C02L C03W H03W 119.1 . . ?
C020 C02I P00L 119.2(11) . . ?
C020 C02I C03X 117.6(15) . . ?
C03X C02I P00L 123.0(12) . . ?
C01A C02R C02E 117.7(16) . . ?
C01A C02R H02R 121.2 . . ?
C02E C02R H02R 121.2 . . ?
C019 C02W H02W 119.9 . . ?
C01G C02W C019 120.2(13) . . ?
C01G C02W H02W 119.9 . . ?
C01N C039 H039 120.0 . . ?
C23 C039 C01N 120.0(16) . . ?
C23 C039 H039 120.0 . . ?
C01X C32 H32 122.4 . . ?
C01X C32 C03H 115.2(18) . . ?
C03H C32 H32 122.4 . . ?
C02B C03F H03F 119.3 . . ?
C02B C03F C03P 121.4(16) . . ?
C03P C03F H03F 119.3 . . ?
C02E C03H C32 123.0(18) . . ?
C02E C03H H03H 118.5 . . ?
C32 C03H H03H 118.5 . . ?
C024 C03I P00L 126.7(11) . . ?
C041 C03I P00L 114.7(11) . . ?
C041 C03I C024 117.9(14) . . ?
C01O C03P C03F 118.1(16) . . ?
C01O C03P H03P 121.0 . . ?
C03F C03P H03P 121.0 . . ?
C048 C03U H03U 119.6 . . ?
C048 C03U C1 120.8(17) . . ?
C1 C03U H03U 119.6 . . ?
C23 C03X C02I 119.9(17) . . ?
C23 C03X H03X 120.1 . . ?
C02I C03X H03X 120.1 . . ?
C03I C041 H041 120.0 . . ?
C059 C041 C03I 120.1(15) . . ?
C059 C041 H041 120.0 . . ?
C02C C048 H048 119.4 . . ?
C03U C048 C02C 121.3(19) . . ?
C03U C048 H048 119.4 . . ?
C19 C04O H04O 120.1 . . ?
C19 C04O C059 119.7(16) . . ?
C059 C04O H04O 120.1 . . ?
C041 C059 C04O 119.6(15) . . ?
C041 C059 H059 120.2 . . ?
C04O C059 H059 120.2 . . ?
C39 C05F P00W 116.0(9) . . ?
C39 C05F C17 120.0 . . ?
C17 C05F P00W 124.0(9) . . ?
C05F C39 H39 120.0 . . ?
C05F C39 C162 120.0 . . ?
C162 C39 H39 120.0 . . ?
C39 C162 H162 120.0 . . ?
C39 C162 C63 120.0 . . ?
C63 C162 H162 120.0 . . ?
C162 C63 H63 120.0 . . ?
C162 C63 C40 120.0 . . ?
C40 C63 H63 120.0 . . ?
C63 C40 H40 120.0 . . ?
C17 C40 C63 120.0 . . ?
C17 C40 H40 120.0 . . ?
C05F C17 H17 120.0 . . ?
C40 C17 C05F 120.0 . . ?
C40 C17 H17 120.0 . . ?
C00X C C02C 121.2(17) . . ?
C00X C H 119.4 . . ?
C02C C H 119.4 . . ?
C011 B012 C01D 101.5(10) . . ?
C011 B012 H012 125.6 . . ?
C011 B012 B01B 56.9(8) . . ?
C011 B012 B02N 59.4(8) . . ?
C011 B012 B03R 103.1(10) . . ?
C01D B012 H012 124.8 . . ?
C01D B012 B01B 59.5(8) . . ?
C01D B012 B02N 102.9(11) . . ?
C01D B012 B03R 59.0(8) . . ?
B01B B012 H012 122.2 . . ?
B01B B012 B03R 106.9(11) . . ?
B02N B012 H012 123.9 . . ?
B02N B012 B01B 105.7(10) . . ?
B02N B012 B03R 56.8(9) . . ?
B03R B012 H012 123.5 . . ?
C00X C1 P00I 116.6(12) . . ?
C00X C1 C03U 118.4(14) . . ?
C03U C1 P00I 124.7(12) . . ?
C011 B01B C01D 103.5(10) . . ?
C011 B01B B012 59.8(8) . . ?
C011 B01B H01B 124.1 . . ?
C011 B01B B036 59.5(9) . . ?
C011 B01B B049 106.6(11) . . ?
C01D B01B B012 59.1(8) . . ?
C01D B01B H01B 124.2 . . ?
C01D B01B B049 60.2(9) . . ?
B012 B01B H01B 120.1 . . ?
B036 B01B C01D 106.4(11) . . ?
B036 B01B B012 109.8(11) . . ?
B036 B01B H01B 121.4 . . ?
B036 B01B B049 60.1(9) . . ?
B049 B01B B012 110.1(12) . . ?
B049 B01B H01B 121.0 . . ?
C01I B01P H01P 124.8 . . ?
C01I B01P B026 102.8(11) . . ?
C01I B01P B02F 57.8(9) . . ?
C01I B01P B02Y 106.1(11) . . ?
C01I B01P B03O 59.8(9) . . ?
B026 B01P H01P 123.5 . . ?
B026 B01P B02F 58.3(9) . . ?
B026 B01P B02Y 60.8(9) . . ?
B026 B01P B03O 107.7(11) . . ?
B02F B01P H01P 122.3 . . ?
B02Y B01P H01P 121.2 . . ?
B02Y B01P B02F 108.2(11) . . ?
B03O B01P H01P 121.0 . . ?
B03O B01P B02F 107.9(11) . . ?
B03O B01P B02Y 60.3(9) . . ?
B028 B01V H01V 120.6 . . ?
B028 B01V B02N 106.2(11) . . ?
B028 B01V B03R 60.0(9) . . ?
B02K B01V H01V 121.3 . . ?
B02K B01V B028 109.9(12) . . ?
B02K B01V B02N 60.1(9) . . ?
B02K B01V B03R 108.1(12) . . ?
B02N B01V H01V 123.7 . . ?
B03B B01V H01V 119.6 . . ?
B03B B01V B028 63.6(10) . . ?
B03B B01V B02K 59.6(10) . . ?
B03B B01V B02N 107.8(12) . . ?
B03B B01V B03R 111.0(12) . . ?
B03R B01V H01V 121.5 . . ?
B03R B01V B02N 58.0(10) . . ?
C01I B01Z H01Z 124.3 . . ?
C01I B01Z B023 59.6(8) . . ?
C01I B01Z B03O 58.4(8) . . ?
C01I B01Z B03Q 106.0(13) . . ?
B023 B01Z H01Z 120.4 . . ?
B023 B01Z B03O 108.8(11) . . ?
B023 B01Z B03Q 110.7(12) . . ?
B03O B01Z H01Z 121.6 . . ?
B03Q B01Z H01Z 120.7 . . ?
B03Q B01Z B03O 59.9(10) . . ?
B03S B01Z C01I 106.2(11) . . ?
B03S B01Z H01Z 121.0 . . ?
B03S B01Z B023 60.4(9) . . ?
B03S B01Z B03O 109.4(13) . . ?
B03S B01Z B03Q 62.3(10) . . ?
C010 B023 C01I 101.8(11) . . ?
C010 B023 B01Z 103.4(12) . . ?
C010 B023 H023 125.6 . . ?
C010 B023 B02F 59.6(9) . . ?
C010 B023 B03S 57.9(8) . . ?
C01I B023 B01Z 60.0(8) . . ?
C01I B023 H023 124.7 . . ?
C01I B023 B02F 57.4(8) . . ?
C01I B023 B03S 105.6(12) . . ?
B01Z B023 H023 122.7 . . ?
B01Z B023 B02F 107.1(12) . . ?
B02F B023 H023 121.7 . . ?
B03S B023 B01Z 59.1(9) . . ?
B03S B023 H023 122.3 . . ?
B03S B023 B02F 107.7(12) . . ?
C010 B026 B01P 108.3(12) . . ?
C010 B026 H026 122.8 . . ?
C010 B026 B02F 61.1(9) . . ?
C010 B026 B02H 58.3(9) . . ?
C010 B026 B02Y 106.4(11) . . ?
B01P B026 H026 121.1 . . ?
B01P B026 B02H 108.0(11) . . ?
B01P B026 B02Y 60.3(9) . . ?
B02F B026 B01P 61.9(10) . . ?
B02F B026 H026 119.2 . . ?
B02F B026 B02H 109.3(12) . . ?
B02F B026 B02Y 110.6(12) . . ?
B02H B026 H026 122.3 . . ?
B02Y B026 H026 121.6 . . ?
B02Y B026 B02H 59.6(9) . . ?
C01D B028 B01V 107.1(12) . . ?
C01D B028 H028 122.0 . . ?
C01D B028 B03B 105.7(12) . . ?
C01D B028 B03R 61.2(9) . . ?
C01D B028 B049 60.5(9) . . ?
B01V B028 H028 123.1 . . ?
B01V B028 B03B 57.4(10) . . ?
B01V B028 B03R 60.1(10) . . ?
B01V B028 B049 106.8(13) . . ?
B03B B028 H028 124.3 . . ?
B03R B028 H028 120.6 . . ?
B03R B028 B03B 106.2(13) . . ?
B03R B028 B049 110.3(11) . . ?
B049 B028 H028 120.9 . . ?
B049 B028 B03B 59.4(10) . . ?
C010 B02F B01P 105.1(11) . . ?
C010 B02F B023 57.4(8) . . ?
C010 B02F H02F 125.6 . . ?
C01I B02F C010 101.8(10) . . ?
C01I B02F B01P 59.6(9) . . ?
C01I B02F B023 59.5(8) . . ?
C01I B02F B026 105.4(12) . . ?
C01I B02F H02F 124.5 . . ?
B01P B02F B023 108.9(11) . . ?
B01P B02F H02F 121.5 . . ?
B023 B02F H02F 121.5 . . ?
B026 B02F C010 59.0(9) . . ?
B026 B02F B01P 59.8(9) . . ?
B026 B02F B023 107.3(11) . . ?
B026 B02F H02F 122.2 . . ?
C010 B02H B026 58.2(9) . . ?
C010 B02H H02H 124.4 . . ?
C010 B02H B02Y 106.4(12) . . ?
C010 B02H B03Q 106.9(13) . . ?
C010 B02H B03S 57.8(10) . . ?
B026 B02H H02H 122.9 . . ?
B02Y B02H B026 59.8(10) . . ?
B02Y B02H H02H 120.4 . . ?
B03Q B02H B026 108.5(12) . . ?
B03Q B02H H02H 120.3 . . ?
B03Q B02H B02Y 61.8(10) . . ?
B03Q B02H B03S 62.3(11) . . ?
B03S B02H B026 106.5(13) . . ?
B03S B02H H02H 120.9 . . ?
B03S B02H B02Y 111.1(12) . . ?
C011 B02K B01V 106.7(11) . . ?
C011 B02K H02K 124.0 . . ?
C011 B02K B02N 59.7(8) . . ?
C011 B02K B036 57.8(8) . . ?
B01V B02K H02K 121.5 . . ?
B01V B02K B02N 61.0(10) . . ?
B01V B02K B036 108.0(12) . . ?
B02N B02K H02K 120.9 . . ?
B02N B02K B036 107.6(10) . . ?
B036 B02K H02K 122.3 . . ?
B03B B02K C011 105.3(11) . . ?
B03B B02K B01V 59.9(9) . . ?
B03B B02K H02K 122.2 . . ?
B03B B02K B02N 108.7(12) . . ?
B03B B02K B036 60.1(9) . . ?
C011 B02N B012 59.0(8) . . ?
C011 B02N B01V 104.8(11) . . ?
C011 B02N B02K 59.4(8) . . ?
C011 B02N H02N 124.1 . . ?
B012 B02N H02N 119.5 . . ?
B01V B02N B012 110.3(12) . . ?
B01V B02N H02N 122.5 . . ?
B02K B02N B012 109.6(10) . . ?
B02K B02N B01V 58.8(9) . . ?
B02K B02N H02N 121.4 . . ?
B03R B02N C011 107.6(11) . . ?
B03R B02N B012 63.1(9) . . ?
B03R B02N B01V 60.5(10) . . ?
B03R B02N B02K 109.1(11) . . ?
B03R B02N H02N 120.2 . . ?
B01P B02Y B026 58.9(9) . . ?
B01P B02Y B02H 107.6(13) . . ?
B01P B02Y H02Y 121.9 . . ?
B01P B02Y B03O 59.5(9) . . ?
B01P B02Y B03Q 107.5(13) . . ?
B026 B02Y H02Y 122.9 . . ?
B026 B02Y B03Q 106.2(12) . . ?
B02H B02Y B026 60.6(9) . . ?
B02H B02Y H02Y 122.5 . . ?
B02H B02Y B03Q 58.0(10) . . ?
B03O B02Y B026 105.5(12) . . ?
B03O B02Y B02H 105.9(13) . . ?
B03O B02Y H02Y 123.1 . . ?
B03O B02Y B03Q 59.9(10) . . ?
B03Q B02Y H02Y 122.6 . . ?
C011 B036 B01B 58.0(8) . . ?
C011 B036 B02K 59.5(8) . . ?
C011 B036 H036 124.3 . . ?
C011 B036 B03B 104.9(11) . . ?
C011 B036 B049 106.0(11) . . ?
B01B B036 B02K 107.2(10) . . ?
B01B B036 H036 121.5 . . ?
B01B B036 B03B 109.0(12) . . ?
B01B B036 B049 60.9(9) . . ?
B02K B036 H036 122.5 . . ?
B03B B036 B02K 58.0(9) . . ?
B03B B036 H036 122.2 . . ?
B03B B036 B049 61.6(10) . . ?
B049 B036 B02K 107.9(12) . . ?
B049 B036 H036 121.1 . . ?
B01V B03B B028 59.0(9) . . ?
B01V B03B B036 109.8(13) . . ?
B01V B03B H03B 121.1 . . ?
B01V B03B B049 108.5(12) . . ?
B028 B03B H03B 123.2 . . ?
B02K B03B B01V 60.5(10) . . ?
B02K B03B B028 107.1(12) . . ?
B02K B03B B036 61.9(9) . . ?
B02K B03B H03B 120.9 . . ?
B02K B03B B049 109.3(12) . . ?
B036 B03B B028 107.0(12) . . ?
B036 B03B H03B 121.0 . . ?
B036 B03B B049 59.5(10) . . ?
B049 B03B B028 59.8(10) . . ?
B049 B03B H03B 121.4 . . ?
C01I B03O B01P 59.3(9) . . ?
C01I B03O B01Z 58.6(9) . . ?
C01I B03O B02Y 105.6(11) . . ?
C01I B03O H03O 124.1 . . ?
C01I B03O B03Q 104.9(12) . . ?
B01P B03O B01Z 107.4(11) . . ?
B01P B03O B02Y 60.1(9) . . ?
B01P B03O H03O 121.1 . . ?
B01P B03O B03Q 108.9(11) . . ?
B01Z B03O H03O 122.9 . . ?
B02Y B03O B01Z 106.8(11) . . ?
B02Y B03O H03O 122.1 . . ?
B02Y B03O B03Q 60.9(10) . . ?
B03Q B03O B01Z 58.4(10) . . ?
B03Q B03O H03O 122.2 . . ?
B01Z B03Q B02Y 108.0(13) . . ?
B01Z B03Q B03O 61.7(10) . . ?
B01Z B03Q H03Q 122.3 . . ?
B01Z B03Q B03S 57.9(10) . . ?
B02H B03Q B01Z 105.6(13) . . ?
B02H B03Q B02Y 60.2(10) . . ?
B02H B03Q B03O 106.9(13) . . ?
B02H B03Q H03Q 123.0 . . ?
B02H B03Q B03S 59.0(10) . . ?
B02Y B03Q H03Q 121.7 . . ?
B03O B03Q B02Y 59.2(10) . . ?
B03O B03Q H03Q 121.5 . . ?
B03O B03Q B03S 107.4(13) . . ?
B03S B03Q B02Y 107.2(12) . . ?
B03S B03Q H03Q 122.9 . . ?
C01D B03R B012 58.2(8) . . ?
C01D B03R H03R 125.3 . . ?
B012 B03R H03R 121.7 . . ?
B01V B03R C01D 104.5(10) . . ?
B01V B03R B012 108.7(12) . . ?
B01V B03R H03R 121.7 . . ?
B028 B03R C01D 57.9(8) . . ?
B028 B03R B012 107.1(10) . . ?
B028 B03R B01V 59.9(9) . . ?
B028 B03R H03R 121.9 . . ?
B02N B03R C01D 104.9(11) . . ?
B02N B03R B012 60.1(9) . . ?
B02N B03R B01V 61.4(10) . . ?
B02N B03R B028 108.8(12) . . ?
B02N B03R H03R 121.4 . . ?
C010 B03S B01Z 105.8(12) . . ?
C010 B03S B023 59.6(9) . . ?
C010 B03S B02H 59.9(9) . . ?
C010 B03S B03Q 105.6(12) . . ?
C010 B03S H03S 123.4 . . ?
B01Z B03S B023 60.5(9) . . ?
B01Z B03S B02H 106.8(12) . . ?
B01Z B03S B03Q 59.8(10) . . ?
B01Z B03S H03S 122.6 . . ?
B023 B03S B03Q 108.9(12) . . ?
B023 B03S H03S 120.4 . . ?
B02H B03S B023 109.2(12) . . ?
B02H B03S B03Q 58.7(10) . . ?
B02H B03S H03S 121.8 . . ?
B03Q B03S H03S 122.5 . . ?
C01D B049 B01B 59.0(9) . . ?
C01D B049 B028 56.6(9) . . ?
C01D B049 B03B 103.8(12) . . ?
C01D B049 H049 124.9 . . ?
B01B B049 B028 105.4(11) . . ?
B01B B049 B03B 105.4(12) . . ?
B01B B049 H049 123.1 . . ?
B028 B049 H049 122.6 . . ?
B036 B049 C01D 104.7(11) . . ?
B036 B049 B01B 59.1(9) . . ?
B036 B049 B028 107.2(12) . . ?
B036 B049 B03B 58.8(9) . . ?
B036 B049 H049 122.7 . . ?
B03B B049 B028 60.8(10) . . ?
B03B B049 H049 123.2 . . ?
Cl2 C4 Cl3 110.3(12) . . ?
Cl2 C4 H4A 109.6 . . ?
Cl2 C4 H4B 109.6 . . ?
Cl3 C4 H4A 109.6 . . ?
Cl3 C4 H4B 109.6 . . ?
H4A C4 H4B 108.1 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Au3 P00L C010 B023 101.5(9) . . . . ?
Au3 P00L C010 B026 -35.5(11) . . . . ?
Au3 P00L C010 B02F 30.6(10) . . . . ?
Au3 P00L C010 B02H -108.1(11) . . . . ?
Au3 P00L C010 B03S 176.2(10) . . . . ?
Au3 P00L C02I C020 -33.9(12) . . . . ?
Au3 P00L C02I C03X 142.0(11) . . . . ?
Au3 P00L C03I C024 169.1(13) . . . . ?
Au3 P00L C03I C041 -20.3(13) . . . . ?
Au5 P00P C019 C01M 165.3(11) . . . . ?
Au5 P00P C019 C02W -14.7(12) . . . . ?
Au5 P00P C01D B012 38.5(9) . . . . ?
Au5 P00P C01D B01B 106.7(9) . . . . ?
Au5 P00P C01D B028 -102.8(10) . . . . ?
Au5 P00P C01D B03R -31.0(11) . . . . ?
Au5 P00P C01D B049 178.9(10) . . . . ?
Au5 P00P C02B C01E -17.2(13) . . . . ?
Au5 P00P C02B C03F 170.0(12) . . . . ?
Au7 P00W C01I B01P 33.6(10) . . . . ?
Au7 P00W C01I B01Z -179.3(10) . . . . ?
Au7 P00W C01I B023 -107.1(9) . . . . ?
Au7 P00W C01I B02F -36.0(11) . . . . ?
Au7 P00W C01I B03O 103.6(10) . . . . ?
Au7 P00W C01X C01A 43.1(14) . . . . ?
Au7 P00W C01X C32 -129.5(14) . . . . ?
Au7 P00W C05F C39 -20.2(11) . . . . ?
Au7 P00W C05F C17 160.4(9) . . . . ?
Au1 P00I C011 B012 -28.7(10) . . . . ?
Au1 P00I C011 B01B -100.8(9) . . . . ?
Au1 P00I C011 B02K 111.0(9) . . . . ?
Au1 P00I C011 B02N 40.8(10) . . . . ?
Au1 P00I C011 B036 -174.7(9) . . . . ?
Au1 P00I C02D C02G -14.9(12) . . . . ?
Au1 P00I C02D C02T 169.9(11) . . . . ?
Au1 P00I C1 C00X 42.3(14) . . . . ?
Au1 P00I C1 C03U -132.5(17) . . . . ?
P00I C011 B012 C01D -153.2(8) . . . . ?
P00I C011 B012 B01B -111.9(11) . . . . ?
P00I C011 B012 B02N 108.5(10) . . . . ?
P00I C011 B012 B03R 146.3(9) . . . . ?
P00I C011 B01B C01D 146.5(9) . . . . ?
P00I C011 B01B B012 105.0(11) . . . . ?
P00I C011 B01B B036 -112.2(11) . . . . ?
P00I C011 B01B B049 -151.0(10) . . . . ?
P00I C011 B02K B01V -146.8(9) . . . . ?
P00I C011 B02K B02N -106.3(11) . . . . ?
P00I C011 B02K B036 112.2(11) . . . . ?
P00I C011 B02K B03B 150.7(9) . . . . ?
P00I C011 B02N B012 -105.3(11) . . . . ?
P00I C011 B02N B01V 149.6(10) . . . . ?
P00I C011 B02N B02K 110.6(11) . . . . ?
P00I C011 B02N B03R -147.1(10) . . . . ?
P00I C011 B036 B01B 109.5(11) . . . . ?
P00I C011 B036 B02K -109.8(12) . . . . ?
P00I C011 B036 B03B -147.3(10) . . . . ?
P00I C011 B036 B049 148.5(10) . . . . ?
P00I C02D C02T C040 177.0(12) . . . . ?
P00L C010 B023 C01I -143.4(9) . . . . ?
P00L C010 B023 B01Z 155.0(9) . . . . ?
P00L C010 B023 B02F -102.9(11) . . . . ?
P00L C010 B023 B03S 115.5(11) . . . . ?
P00L C010 B026 B01P 145.3(10) . . . . ?
P00L C010 B026 B02F 103.9(10) . . . . ?
P00L C010 B026 B02H -114.4(11) . . . . ?
P00L C010 B026 B02Y -151.2(9) . . . . ?
P00L C010 B02F C01I 153.6(9) . . . . ?
P00L C010 B02F B01P -145.0(9) . . . . ?
P00L C010 B02F B023 112.0(11) . . . . ?
P00L C010 B02F B026 -105.4(10) . . . . ?
P00L C010 B02H B026 103.4(11) . . . . ?
P00L C010 B02H B02Y 140.2(10) . . . . ?
P00L C010 B02H B03Q -154.9(11) . . . . ?
P00L C010 B02H B03S -114.8(12) . . . . ?
P00L C010 B03S B01Z -148.7(11) . . . . ?
P00L C010 B03S B023 -108.1(12) . . . . ?
P00L C010 B03S B02H 110.7(12) . . . . ?
P00L C010 B03S B03Q 148.9(10) . . . . ?
P00L C02I C03X C23 -174.8(13) . . . . ?
P00L C03I C041 C059 -172.3(14) . . . . ?
P00P C019 C01M C029 -179.3(12) . . . . ?
P00P C019 C02W C01G 178.6(13) . . . . ?
P00P C01D B012 C011 151.0(8) . . . . ?
P00P C01D B012 B01B 111.1(10) . . . . ?
P00P C01D B012 B02N -148.0(9) . . . . ?
P00P C01D B012 B03R -110.5(10) . . . . ?
P00P C01D B01B C011 -142.6(10) . . . . ?
P00P C01D B01B B012 -100.8(11) . . . . ?
P00P C01D B01B B036 155.7(9) . . . . ?
P00P C01D B01B B049 115.8(12) . . . . ?
P00P C01D B028 B01V 145.0(11) . . . . ?
P00P C01D B028 B03B -154.9(10) . . . . ?
P00P C01D B028 B03R 104.9(12) . . . . ?
P00P C01D B028 B049 -114.9(12) . . . . ?
P00P C01D B03R B012 101.7(11) . . . . ?
P00P C01D B03R B01V -155.0(10) . . . . ?
P00P C01D B03R B028 -115.6(13) . . . . ?
P00P C01D B03R B02N 141.3(10) . . . . ?
P00P C01D B049 B01B -105.8(12) . . . . ?
P00P C01D B049 B028 114.2(14) . . . . ?
P00P C01D B049 B036 -144.7(11) . . . . ?
P00P C01D B049 B03B 154.4(11) . . . . ?
P00P C02B C03F C03P 170.1(12) . . . . ?
P00W C01I B01P B026 -143.5(9) . . . . ?
P00W C01I B01P B02F -104.8(10) . . . . ?
P00W C01I B01P B02Y 153.5(9) . . . . ?
P00W C01I B01P B03O 113.3(10) . . . . ?
P00W C01I B01Z B023 106.1(13) . . . . ?
P00W C01I B01Z B03O -111.0(12) . . . . ?
P00W C01I B01Z B03Q -148.9(11) . . . . ?
P00W C01I B01Z B03S 145.9(11) . . . . ?
P00W C01I B023 C010 145.2(9) . . . . ?
P00W C01I B023 B01Z -115.9(11) . . . . ?
P00W C01I B023 B02F 103.6(11) . . . . ?
P00W C01I B023 B03S -155.1(9) . . . . ?
P00W C01I B02F C010 -151.9(9) . . . . ?
P00W C01I B02F B01P 107.3(11) . . . . ?
P00W C01I B02F B023 -111.4(11) . . . . ?
P00W C01I B02F B026 147.3(9) . . . . ?
P00W C01I B03O B01P -103.5(11) . . . . ?
P00W C01I B03O B01Z 116.1(12) . . . . ?
P00W C01I B03O B02Y -143.5(10) . . . . ?
P00W C01I B03O B03Q 153.1(10) . . . . ?
P00W C01X C32 C03H 178.3(13) . . . . ?
P00W C05F C39 C162 -179.5(13) . . . . ?
P00W C05F C17 C40 179.4(15) . . . . ?
C010 P00L C02I C020 87.3(12) . . . . ?
C010 P00L C02I C03X -96.9(12) . . . . ?
C010 P00L C03I C024 43.0(16) . . . . ?
C010 P00L C03I C041 -146.4(11) . . . . ?
C010 B023 B02F C01I -131.1(12) . . . . ?
C010 B023 B02F B01P -96.3(12) . . . . ?
C010 B023 B02F B026 -33.0(10) . . . . ?
C010 B023 B03S B01Z 134.0(12) . . . . ?
C010 B023 B03S B02H 35.0(10) . . . . ?
C010 B023 B03S B03Q 97.5(12) . . . . ?
C010 B026 B02F C01I 94.7(10) . . . . ?
C010 B026 B02F B01P 134.6(11) . . . . ?
C010 B026 B02F B023 32.4(10) . . . . ?
C010 B026 B02H B02Y -138.2(12) . . . . ?
C010 B026 B02H B03Q -98.7(15) . . . . ?
C010 B026 B02H B03S -33.0(10) . . . . ?
C010 B026 B02Y B01P -102.0(12) . . . . ?
C010 B026 B02Y B02H 36.2(11) . . . . ?
C010 B026 B02Y B03O -63.5(14) . . . . ?
C010 B026 B02Y B03Q -1.0(15) . . . . ?
C010 B02H B02Y B01P 0.6(15) . . . . ?
C010 B02H B02Y B026 -36.1(11) . . . . ?
C010 B02H B02Y B03O 63.0(14) . . . . ?
C010 B02H B02Y B03Q 100.7(14) . . . . ?
C010 B02H B03Q B01Z 2.2(17) . . . . ?
C010 B02H B03Q B02Y -99.9(13) . . . . ?
C010 B02H B03Q B03O -62.3(16) . . . . ?
C010 B02H B03Q B03S 38.1(12) . . . . ?
C010 B02H B03S B01Z -98.8(12) . . . . ?
C010 B02H B03S B023 -34.9(10) . . . . ?
C010 B02H B03S B03Q -135.8(13) . . . . ?
C011 P00I C02D C02G 107.6(12) . . . . ?
C011 P00I C02D C02T -67.6(13) . . . . ?
C011 P00I C1 C00X -80.3(15) . . . . ?
C011 P00I C1 C03U 104.9(18) . . . . ?
C011 B012 B01B C01D -131.4(11) . . . . ?
C011 B012 B01B B036 -33.6(11) . . . . ?
C011 B012 B01B B049 -98.0(12) . . . . ?
C011 B012 B02N B01V 95.5(12) . . . . ?
C011 B012 B02N B02K 32.4(11) . . . . ?
C011 B012 B02N B03R 134.5(11) . . . . ?
C011 B012 B03R C01D 95.7(10) . . . . ?
C011 B012 B03R B01V 0.0(13) . . . . ?
C011 B012 B03R B028 63.2(14) . . . . ?
C011 B012 B03R B02N -39.1(9) . . . . ?
C011 B01B B036 B02K -34.8(10) . . . . ?
C011 B01B B036 B03B -96.1(12) . . . . ?
C011 B01B B036 B049 -136.1(12) . . . . ?
C011 B01B B049 C01D -96.3(11) . . . . ?
C011 B01B B049 B028 -62.5(14) . . . . ?
C011 B01B B049 B036 38.6(10) . . . . ?
C011 B01B B049 B03B 0.8(15) . . . . ?
C011 B02K B02N B012 -32.2(11) . . . . ?
C011 B02K B02N B01V -134.7(12) . . . . ?
C011 B02K B02N B03R -99.6(12) . . . . ?
C011 B02K B036 B01B 34.2(10) . . . . ?
C011 B02K B036 B03B 136.1(12) . . . . ?
C011 B02K B036 B049 98.4(12) . . . . ?
C011 B02K B03B B01V 100.7(12) . . . . ?
C011 B02K B03B B028 63.1(13) . . . . ?
C011 B02K B03B B036 -37.4(10) . . . . ?
C011 B02K B03B B049 -0.2(15) . . . . ?
C011 B02N B03R C01D 1.2(14) . . . . ?
C011 B02N B03R B012 39.8(9) . . . . ?
C011 B02N B03R B01V -97.4(12) . . . . ?
C011 B02N B03R B028 -59.5(13) . . . . ?
C011 B036 B03B B01V 0.0(16) . . . . ?
C011 B036 B03B B028 -62.5(14) . . . . ?
C011 B036 B03B B02K 38.2(10) . . . . ?
C011 B036 B03B B049 -100.4(12) . . . . ?
C011 B036 B049 C01D 1.2(14) . . . . ?
C011 B036 B049 B01B -37.7(10) . . . . ?
C011 B036 B049 B028 60.3(13) . . . . ?
C011 B036 B049 B03B 98.6(12) . . . . ?
C019 P00P C01D B012 163.0(8) . . . . ?
C019 P00P C01D B01B -128.8(10) . . . . ?
C019 P00P C01D B028 21.7(12) . . . . ?
C019 P00P C01D B03R 93.5(11) . . . . ?
C019 P00P C01D B049 -56.6(13) . . . . ?
C019 P00P C02B C01E -145.0(12) . . . . ?
C019 P00P C02B C03F 42.2(15) . . . . ?
C019 C01M C029 C01S 2(2) . . . . ?
C01A C01X C32 C03H 6(3) . . . . ?
C01D P00P C019 C01M 44.5(14) . . . . ?
C01D P00P C019 C02W -135.6(11) . . . . ?
C01D P00P C02B C01E 100.5(12) . . . . ?
C01D P00P C02B C03F -72.3(14) . . . . ?
C01D B012 B01B C011 131.4(11) . . . . ?
C01D B012 B01B B036 97.8(12) . . . . ?
C01D B012 B01B B049 33.4(11) . . . . ?
C01D B012 B02N C011 -95.9(10) . . . . ?
C01D B012 B02N B01V -0.5(14) . . . . ?
C01D B012 B02N B02K -63.5(13) . . . . ?
C01D B012 B02N B03R 38.6(9) . . . . ?
C01D B012 B03R B01V -95.8(11) . . . . ?
C01D B012 B03R B028 -32.5(11) . . . . ?
C01D B012 B03R B02N -134.8(11) . . . . ?
C01D B01B B036 C011 96.2(11) . . . . ?
C01D B01B B036 B02K 61.4(14) . . . . ?
C01D B01B B036 B03B 0.1(15) . . . . ?
C01D B01B B036 B049 -39.9(11) . . . . ?
C01D B01B B049 B028 33.8(11) . . . . ?
C01D B01B B049 B036 134.9(11) . . . . ?
C01D B01B B049 B03B 97.1(12) . . . . ?
C01D B028 B03B B01V -100.6(12) . . . . ?
C01D B028 B03B B02K -62.3(14) . . . . ?
C01D B028 B03B B036 2.7(15) . . . . ?
C01D B028 B03B B049 40.5(11) . . . . ?
C01D B028 B03R B012 32.6(11) . . . . ?
C01D B028 B03R B01V 134.8(13) . . . . ?
C01D B028 B03R B02N 96.2(12) . . . . ?
C01D B028 B049 B01B -34.8(11) . . . . ?
C01D B028 B049 B036 -96.6(12) . . . . ?
C01D B028 B049 B03B -134.1(13) . . . . ?
C01E C01F C01O C03P 3(2) . . . . ?
C01E C02B C03F C03P -3(2) . . . . ?
C01F C01E C02B P00P -171.7(12) . . . . ?
C01F C01E C02B C03F 2(2) . . . . ?
C01F C01O C03P C03F -4(2) . . . . ?
C01G C01S C029 C01M -3(2) . . . . ?
C01I P00W C01X C01A -78.6(14) . . . . ?
C01I P00W C01X C32 108.8(15) . . . . ?
C01I P00W C05F C39 100.2(10) . . . . ?
C01I P00W C05F C17 -79.3(12) . . . . ?
C01I B01P B026 C010 -2.6(15) . . . . ?
C01I B01P B026 B02F 38.5(10) . . . . ?
C01I B01P B026 B02H -64.3(15) . . . . ?
C01I B01P B026 B02Y -101.4(12) . . . . ?
C01I B01P B02F C010 -95.0(10) . . . . ?
C01I B01P B02F B023 -34.7(10) . . . . ?
C01I B01P B02F B026 -134.2(11) . . . . ?
C01I B01P B02Y B026 96.0(12) . . . . ?
C01I B01P B02Y B02H 58.5(14) . . . . ?
C01I B01P B02Y B03O -39.9(10) . . . . ?
C01I B01P B02Y B03Q -2.7(14) . . . . ?
C01I B01P B03O B01Z 34.8(10) . . . . ?
C01I B01P B03O B02Y 134.5(12) . . . . ?
C01I B01P B03O B03Q 96.5(13) . . . . ?
C01I B01Z B023 C010 96.1(11) . . . . ?
C01I B01Z B023 B02F 34.2(10) . . . . ?
C01I B01Z B023 B03S 134.9(13) . . . . ?
C01I B01Z B03O B01P -35.1(10) . . . . ?
C01I B01Z B03O B02Y -98.3(11) . . . . ?
C01I B01Z B03O B03Q -136.9(12) . . . . ?
C01I B01Z B03Q B02H -63.9(15) . . . . ?
C01I B01Z B03Q B02Y -0.8(15) . . . . ?
C01I B01Z B03Q B03O 37.3(10) . . . . ?
C01I B01Z B03Q B03S -100.2(12) . . . . ?
C01I B01Z B03S C010 0.7(16) . . . . ?
C01I B01Z B03S B023 -39.5(11) . . . . ?
C01I B01Z B03S B02H 63.4(15) . . . . ?
C01I B01Z B03S B03Q 99.8(13) . . . . ?
C01I B023 B02F C010 131.1(12) . . . . ?
C01I B023 B02F B01P 34.8(11) . . . . ?
C01I B023 B02F B026 98.0(12) . . . . ?
C01I B023 B03S C010 -94.4(11) . . . . ?
C01I B023 B03S B01Z 39.6(10) . . . . ?
C01I B023 B03S B02H -59.4(13) . . . . ?
C01I B023 B03S B03Q 3.1(14) . . . . ?
C01I B03O B03Q B01Z -37.1(11) . . . . ?
C01I B03O B03Q B02H 61.8(16) . . . . ?
C01I B03O B03Q B02Y 99.8(12) . . . . ?
C01I B03O B03Q B03S -0.3(15) . . . . ?
C01M C019 C02W C01G -1(2) . . . . ?
C01N C020 C02I P00L 173.4(12) . . . . ?
C01N C020 C02I C03X -3(2) . . . . ?
C01S C01G C02W C019 0(2) . . . . ?
C01X P00W C01I B01P 151.5(10) . . . . ?
C01X P00W C01I B01Z -61.3(12) . . . . ?
C01X P00W C01I B023 10.8(11) . . . . ?
C01X P00W C01I B02F 81.9(11) . . . . ?
C01X P00W C01I B03O -138.5(11) . . . . ?
C01X P00W C05F C39 -145.4(10) . . . . ?
C01X P00W C05F C17 35.2(13) . . . . ?
C01X C01A C02R C02E -1(2) . . . . ?
C01X C32 C03H C02E -8(3) . . . . ?
C020 C01N C039 C23 -3(3) . . . . ?
C020 C02I C03X C23 1(2) . . . . ?
C024 C19 C04O C059 -3(3) . . . . ?
C024 C03I C041 C059 -1(2) . . . . ?
C19 C024 C03I P00L 174.0(16) . . . . ?
C19 C024 C03I C041 4(3) . . . . ?
C19 C04O C059 C041 5(3) . . . . ?
C02B P00P C019 C01M -68.2(14) . . . . ?
C02B P00P C019 C02W 111.8(11) . . . . ?
C02B P00P C01D B012 -81.7(10) . . . . ?
C02B P00P C01D B01B -13.5(12) . . . . ?
C02B P00P C01D B028 137.0(11) . . . . ?
C02B P00P C01D B03R -151.2(10) . . . . ?
C02B P00P C01D B049 58.7(13) . . . . ?
C02B C01E C01F C01O -2(2) . . . . ?
C02B C03F C03P C01O 4(2) . . . . ?
C02G C02D C02T C040 2(2) . . . . ?
C02D P00I C011 B012 -151.0(9) . . . . ?
C02D P00I C011 B01B 136.8(10) . . . . ?
C02D P00I C011 B02K -11.4(11) . . . . ?
C02D P00I C011 B02N -81.6(10) . . . . ?
C02D P00I C011 B036 62.9(11) . . . . ?
C02D P00I C1 C00X 168.1(13) . . . . ?
C02D P00I C1 C03U -7(2) . . . . ?
C02D C02G C03W C02L 0(3) . . . . ?
C02D C02T C040 C02L -3(2) . . . . ?
C02T C040 C02L C03W 2(2) . . . . ?
C040 C02L C03W C02G -1(3) . . . . ?
C03W C02G C02D P00I -176.3(13) . . . . ?
C03W C02G C02D C02T -1(2) . . . . ?
C02I P00L C010 B023 -17.2(11) . . . . ?
C02I P00L C010 B026 -154.2(10) . . . . ?
C02I P00L C010 B02F -88.1(10) . . . . ?
C02I P00L C010 B02H 133.3(11) . . . . ?
C02I P00L C010 B03S 57.6(13) . . . . ?
C02I P00L C03I C024 -71.0(15) . . . . ?
C02I P00L C03I C041 99.6(12) . . . . ?
C02R C01A C01X P00W -174.3(12) . . . . ?
C02R C01A C01X C32 -2(3) . . . . ?
C02R C02E C03H C32 6(3) . . . . ?
C02W C019 C01M C029 1(2) . . . . ?
C02W C01G C01S C029 3(2) . . . . ?
C039 C01N C020 C02I 4(3) . . . . ?
C039 C23 C03X C02I 0(3) . . . . ?
C03H C02E C02R C01A -1(2) . . . . ?
C03I P00L C010 B023 -131.4(10) . . . . ?
C03I P00L C010 B026 91.6(11) . . . . ?
C03I P00L C010 B02F 157.7(9) . . . . ?
C03I P00L C010 B02H 19.1(13) . . . . ?
C03I P00L C010 B03S -56.6(13) . . . . ?
C03I P00L C02I C020 -157.4(11) . . . . ?
C03I P00L C02I C03X 18.4(13) . . . . ?
C03I C024 C19 C04O -2(3) . . . . ?
C03I C041 C059 C04O -3(3) . . . . ?
C03X C23 C039 C01N 1(3) . . . . ?
C048 C02C C C00X -5(3) . . . . ?
C048 C03U C1 P00I 180(2) . . . . ?
C048 C03U C1 C00X 5(3) . . . . ?
C05F P00W C01I B01P -86.7(11) . . . . ?
C05F P00W C01I B01Z 60.5(13) . . . . ?
C05F P00W C01I B023 132.6(10) . . . . ?
C05F P00W C01I B02F -156.3(11) . . . . ?
C05F P00W C01I B03O -16.6(13) . . . . ?
C05F P00W C01X C01A 171.1(12) . . . . ?
C05F P00W C01X C32 -1.5(18) . . . . ?
C05F C39 C162 C63 0.0 . . . . ?
C39 C05F C17 C40 0.0 . . . . ?
C39 C162 C63 C40 0.0 . . . . ?
C162 C63 C40 C17 0.0 . . . . ?
C63 C40 C17 C05F 0.0 . . . . ?
C17 C05F C39 C162 0.0 . . . . ?
C C00X C1 P00I 179.3(14) . . . . ?
C C00X C1 C03U -6(3) . . . . ?
C C02C C048 C03U 4(4) . . . . ?
B012 C011 B01B C01D 41.5(10) . . . . ?
B012 C011 B01B B036 142.8(11) . . . . ?
B012 C011 B01B B049 104.0(12) . . . . ?
B012 C011 B02K B01V -6.3(14) . . . . ?
B012 C011 B02K B02N 34.1(11) . . . . ?
B012 C011 B02K B036 -107.4(12) . . . . ?
B012 C011 B02K B03B -68.9(13) . . . . ?
B012 C011 B02N B01V -105.1(12) . . . . ?
B012 C011 B02N B02K -144.1(12) . . . . ?
B012 C011 B02N B03R -41.8(10) . . . . ?
B012 C011 B036 B01B -36.6(11) . . . . ?
B012 C011 B036 B02K 104.1(12) . . . . ?
B012 C011 B036 B03B 66.7(14) . . . . ?
B012 C011 B036 B049 2.5(15) . . . . ?
B012 C01D B01B C011 -41.8(10) . . . . ?
B012 C01D B01B B036 -103.6(11) . . . . ?
B012 C01D B01B B049 -143.4(11) . . . . ?
B012 C01D B028 B01V 4.2(16) . . . . ?
B012 C01D B028 B03B 64.3(13) . . . . ?
B012 C01D B028 B03R -35.9(12) . . . . ?
B012 C01D B028 B049 104.2(12) . . . . ?
B012 C01D B03R B01V 103.3(12) . . . . ?
B012 C01D B03R B028 142.7(13) . . . . ?
B012 C01D B03R B02N 39.6(10) . . . . ?
B012 C01D B049 B01B 34.5(11) . . . . ?
B012 C01D B049 B028 -105.6(12) . . . . ?
B012 C01D B049 B036 -4.5(15) . . . . ?
B012 C01D B049 B03B -65.4(14) . . . . ?
B012 B01B B036 C011 33.8(11) . . . . ?
B012 B01B B036 B02K -1.0(15) . . . . ?
B012 B01B B036 B03B -62.4(15) . . . . ?
B012 B01B B036 B049 -102.3(13) . . . . ?
B012 B01B B049 C01D -33.0(10) . . . . ?
B012 B01B B049 B028 0.8(15) . . . . ?
B012 B01B B049 B036 101.9(12) . . . . ?
B012 B01B B049 B03B 64.1(14) . . . . ?
B012 B02N B03R C01D -38.6(9) . . . . ?
B012 B02N B03R B01V -137.2(11) . . . . ?
B012 B02N B03R B028 -99.3(11) . . . . ?
C1 P00I C011 B012 90.9(10) . . . . ?
C1 P00I C011 B01B 18.7(12) . . . . ?
C1 P00I C011 B02K -129.5(10) . . . . ?
C1 P00I C011 B02N 160.3(10) . . . . ?
C1 P00I C011 B036 -55.2(12) . . . . ?
C1 P00I C02D C02G -138.3(12) . . . . ?
C1 P00I C02D C02T 46.5(15) . . . . ?
C1 C00X C C02C 5(3) . . . . ?
C1 C03U C048 C02C -5(4) . . . . ?
B01B C011 B012 C01D -41.3(10) . . . . ?
B01B C011 B012 B02N -139.6(12) . . . . ?
B01B C011 B012 B03R -101.9(11) . . . . ?
B01B C011 B02K B01V 63.3(13) . . . . ?
B01B C011 B02K B02N 103.8(12) . . . . ?
B01B C011 B02K B036 -37.7(11) . . . . ?
B01B C011 B02K B03B 0.8(14) . . . . ?
B01B C011 B02N B012 38.8(11) . . . . ?
B01B C011 B02N B01V -66.3(14) . . . . ?
B01B C011 B02N B02K -105.2(12) . . . . ?
B01B C011 B02N B03R -3.0(15) . . . . ?
B01B C011 B036 B02K 140.8(12) . . . . ?
B01B C011 B036 B03B 103.3(12) . . . . ?
B01B C011 B036 B049 39.1(11) . . . . ?
B01B C01D B012 C011 39.9(9) . . . . ?
B01B C01D B012 B02N 100.8(10) . . . . ?
B01B C01D B012 B03R 138.4(11) . . . . ?
B01B C01D B028 B01V -62.8(14) . . . . ?
B01B C01D B028 B03B -2.8(15) . . . . ?
B01B C01D B028 B03R -102.9(13) . . . . ?
B01B C01D B028 B049 37.2(11) . . . . ?
B01B C01D B03R B012 -38.7(10) . . . . ?
B01B C01D B03R B01V 64.6(14) . . . . ?
B01B C01D B03R B028 103.9(13) . . . . ?
B01B C01D B03R B02N 0.8(14) . . . . ?
B01B C01D B049 B028 -140.0(12) . . . . ?
B01B C01D B049 B036 -38.9(10) . . . . ?
B01B C01D B049 B03B -99.8(12) . . . . ?
B01B B012 B02N C011 -34.3(10) . . . . ?
B01B B012 B02N B01V 61.1(14) . . . . ?
B01B B012 B02N B02K -1.9(15) . . . . ?
B01B B012 B02N B03R 100.2(12) . . . . ?
B01B B012 B03R C01D 36.8(10) . . . . ?
B01B B012 B03R B01V -59.0(14) . . . . ?
B01B B012 B03R B028 4.3(15) . . . . ?
B01B B012 B03R B02N -98.0(11) . . . . ?
B01B B036 B03B B01V 60.8(15) . . . . ?
B01B B036 B03B B028 -1.7(15) . . . . ?
B01B B036 B03B B02K 98.9(12) . . . . ?
B01B B036 B03B B049 -39.6(11) . . . . ?
B01B B036 B049 C01D 38.9(10) . . . . ?
B01B B036 B049 B028 98.0(12) . . . . ?
B01B B036 B049 B03B 136.3(12) . . . . ?
B01P C01I B01Z B023 -105.9(12) . . . . ?
B01P C01I B01Z B03O 37.0(10) . . . . ?
B01P C01I B01Z B03Q -0.9(14) . . . . ?
B01P C01I B01Z B03S -66.1(14) . . . . ?
B01P C01I B023 C010 4.1(14) . . . . ?
B01P C01I B023 B01Z 102.9(13) . . . . ?
B01P C01I B023 B02F -37.5(11) . . . . ?
B01P C01I B023 B03S 63.8(13) . . . . ?
B01P C01I B02F C010 100.8(12) . . . . ?
B01P C01I B02F B023 141.3(12) . . . . ?
B01P C01I B02F B026 40.0(10) . . . . ?
B01P C01I B03O B01Z -140.4(11) . . . . ?
B01P C01I B03O B02Y -40.0(10) . . . . ?
B01P C01I B03O B03Q -103.4(12) . . . . ?
B01P B026 B02F C010 -134.6(11) . . . . ?
B01P B026 B02F C01I -39.9(10) . . . . ?
B01P B026 B02F B023 -102.2(11) . . . . ?
B01P B026 B02H C010 100.8(13) . . . . ?
B01P B026 B02H B02Y -37.4(12) . . . . ?
B01P B026 B02H B03Q 2.1(18) . . . . ?
B01P B026 B02H B03S 67.7(15) . . . . ?
B01P B026 B02Y B02H 138.2(13) . . . . ?
B01P B026 B02Y B03O 38.5(11) . . . . ?
B01P B026 B02Y B03Q 101.0(13) . . . . ?
B01P B02Y B03O C01I 39.6(10) . . . . ?
B01P B02Y B03O B01Z 100.8(12) . . . . ?
B01P B02Y B03O B03Q 138.2(13) . . . . ?
B01P B02Y B03Q B01Z 2.2(15) . . . . ?
B01P B02Y B03Q B02H 100.2(13) . . . . ?
B01P B02Y B03Q B03O -37.0(11) . . . . ?
B01P B02Y B03Q B03S 63.3(14) . . . . ?
B01P B03O B03Q B01Z -99.3(13) . . . . ?
B01P B03O B03Q B02H -0.4(18) . . . . ?
B01P B03O B03Q B02Y 37.6(12) . . . . ?
B01P B03O B03Q B03S -62.4(16) . . . . ?
B01V B028 B03B B02K 38.3(11) . . . . ?
B01V B028 B03B B036 103.3(13) . . . . ?
B01V B028 B03B B049 141.1(13) . . . . ?
B01V B028 B03R C01D -134.8(13) . . . . ?
B01V B028 B03R B012 -102.1(13) . . . . ?
B01V B028 B03R B02N -38.6(11) . . . . ?
B01V B028 B049 C01D 100.5(12) . . . . ?
B01V B028 B049 B01B 65.7(14) . . . . ?
B01V B028 B049 B036 3.9(15) . . . . ?
B01V B028 B049 B03B -33.6(11) . . . . ?
B01V B02K B02N C011 134.7(12) . . . . ?
B01V B02K B02N B012 102.5(13) . . . . ?
B01V B02K B02N B03R 35.1(11) . . . . ?
B01V B02K B036 C011 -98.7(12) . . . . ?
B01V B02K B036 B01B -64.6(14) . . . . ?
B01V B02K B036 B03B 37.4(11) . . . . ?
B01V B02K B036 B049 -0.4(14) . . . . ?
B01V B02K B03B B028 -37.6(11) . . . . ?
B01V B02K B03B B036 -138.1(12) . . . . ?
B01V B02K B03B B049 -100.9(13) . . . . ?
B01V B02N B03R C01D 98.6(11) . . . . ?
B01V B02N B03R B012 137.2(11) . . . . ?
B01V B02N B03R B028 37.9(10) . . . . ?
B01V B03B B049 C01D -3.5(16) . . . . ?
B01V B03B B049 B01B -64.7(15) . . . . ?
B01V B03B B049 B028 34.6(11) . . . . ?
B01V B03B B049 B036 -102.6(14) . . . . ?
B01Z C01I B01P B026 65.3(13) . . . . ?
B01Z C01I B01P B02F 104.0(11) . . . . ?
B01Z C01I B01P B02Y 2.3(14) . . . . ?
B01Z C01I B01P B03O -37.9(11) . . . . ?
B01Z C01I B023 C010 -98.8(12) . . . . ?
B01Z C01I B023 B02F -140.4(13) . . . . ?
B01Z C01I B023 B03S -39.1(11) . . . . ?
B01Z C01I B02F C010 -3.8(15) . . . . ?
B01Z C01I B02F B01P -104.6(13) . . . . ?
B01Z C01I B02F B023 36.6(12) . . . . ?
B01Z C01I B02F B026 -64.6(14) . . . . ?
B01Z C01I B03O B01P 140.4(11) . . . . ?
B01Z C01I B03O B02Y 100.4(12) . . . . ?
B01Z C01I B03O B03Q 37.0(11) . . . . ?
B01Z B023 B02F C010 95.8(12) . . . . ?
B01Z B023 B02F C01I -35.2(11) . . . . ?
B01Z B023 B02F B01P -0.4(15) . . . . ?
B01Z B023 B02F B026 62.8(13) . . . . ?
B01Z B023 B03S C010 -134.0(12) . . . . ?
B01Z B023 B03S B02H -98.9(13) . . . . ?
B01Z B023 B03S B03Q -36.5(11) . . . . ?
B01Z B03O B03Q B02H 98.9(14) . . . . ?
B01Z B03O B03Q B02Y 136.9(12) . . . . ?
B01Z B03O B03Q B03S 36.8(11) . . . . ?
B01Z B03Q B03S C010 99.4(13) . . . . ?
B01Z B03Q B03S B023 36.8(11) . . . . ?
B01Z B03Q B03S B02H 138.3(13) . . . . ?
B023 C010 B026 B01P 5.6(16) . . . . ?
B023 C010 B026 B02F -35.9(11) . . . . ?
B023 C010 B026 B02H 105.8(12) . . . . ?
B023 C010 B026 B02Y 69.0(14) . . . . ?
B023 C010 B02F C01I 41.6(11) . . . . ?
B023 C010 B02F B01P 103.0(12) . . . . ?
B023 C010 B02F B026 142.6(12) . . . . ?
B023 C010 B02H B026 -104.6(12) . . . . ?
B023 C010 B02H B02Y -67.8(15) . . . . ?
B023 C010 B02H B03Q -3.0(17) . . . . ?
B023 C010 B02H B03S 37.2(11) . . . . ?
B023 C010 B03S B01Z -40.6(12) . . . . ?
B023 C010 B03S B02H -141.2(12) . . . . ?
B023 C010 B03S B03Q -103.0(13) . . . . ?
B023 C01I B01P B026 -1.0(15) . . . . ?
B023 C01I B01P B02F 37.7(10) . . . . ?
B023 C01I B01P B02Y -64.0(14) . . . . ?
B023 C01I B01P B03O -104.2(12) . . . . ?
B023 C01I B01Z B03O 143.0(12) . . . . ?
B023 C01I B01Z B03Q 105.0(13) . . . . ?
B023 C01I B01Z B03S 39.9(12) . . . . ?
B023 C01I B02F C010 -40.5(10) . . . . ?
B023 C01I B02F B01P -141.3(12) . . . . ?
B023 C01I B02F B026 -101.3(11) . . . . ?
B023 C01I B03O B01P 105.7(12) . . . . ?
B023 C01I B03O B01Z -34.7(11) . . . . ?
B023 C01I B03O B02Y 65.7(14) . . . . ?
B023 C01I B03O B03Q 2.3(15) . . . . ?
B023 B01Z B03O C01I 33.3(10) . . . . ?
B023 B01Z B03O B01P -1.8(15) . . . . ?
B023 B01Z B03O B02Y -65.0(14) . . . . ?
B023 B01Z B03O B03Q -103.6(13) . . . . ?
B023 B01Z B03Q B02H -0.9(16) . . . . ?
B023 B01Z B03Q B02Y 62.2(14) . . . . ?
B023 B01Z B03Q B03O 100.3(11) . . . . ?
B023 B01Z B03Q B03S -37.2(11) . . . . ?
B023 B01Z B03S C010 40.2(11) . . . . ?
B023 B01Z B03S B02H 102.9(13) . . . . ?
B023 B01Z B03S B03Q 139.4(12) . . . . ?
B026 C010 B023 C01I -5.8(14) . . . . ?
B026 C010 B023 B01Z -67.4(13) . . . . ?
B026 C010 B023 B02F 34.7(11) . . . . ?
B026 C010 B023 B03S -106.9(13) . . . . ?
B026 C010 B02F C01I -101.0(12) . . . . ?
B026 C010 B02F B01P -39.6(10) . . . . ?
B026 C010 B02F B023 -142.6(12) . . . . ?
B026 C010 B02H B02Y 36.9(11) . . . . ?
B026 C010 B02H B03Q 101.7(13) . . . . ?
B026 C010 B02H B03S 141.9(12) . . . . ?
B026 C010 B03S B01Z 63.2(15) . . . . ?
B026 C010 B03S B023 103.8(12) . . . . ?
B026 C010 B03S B02H -37.4(12) . . . . ?
B026 C010 B03S B03Q 0.8(16) . . . . ?
B026 B01P B02F C010 39.3(10) . . . . ?
B026 B01P B02F C01I 134.2(11) . . . . ?
B026 B01P B02F B023 99.5(12) . . . . ?
B026 B01P B02Y B02H -37.5(11) . . . . ?
B026 B01P B02Y B03O -135.9(12) . . . . ?
B026 B01P B02Y B03Q -98.7(12) . . . . ?
B026 B01P B03O C01I -94.8(12) . . . . ?
B026 B01P B03O B01Z -60.1(15) . . . . ?
B026 B01P B03O B02Y 39.6(12) . . . . ?
B026 B01P B03O B03Q 1.7(17) . . . . ?
B026 B02H B02Y B01P 36.7(11) . . . . ?
B026 B02H B02Y B03O 99.1(13) . . . . ?
B026 B02H B02Y B03Q 136.8(14) . . . . ?
B026 B02H B03Q B01Z 63.6(17) . . . . ?
B026 B02H B03Q B02Y -38.6(13) . . . . ?
B026 B02H B03Q B03O -1.0(18) . . . . ?
B026 B02H B03Q B03S 99.4(14) . . . . ?
B026 B02H B03S C010 33.2(10) . . . . ?
B026 B02H B03S B01Z -65.6(14) . . . . ?
B026 B02H B03S B023 -1.7(15) . . . . ?
B026 B02H B03S B03Q -102.6(13) . . . . ?
B026 B02Y B03O C01I 1.4(14) . . . . ?
B026 B02Y B03O B01P -38.2(11) . . . . ?
B026 B02Y B03O B01Z 62.6(13) . . . . ?
B026 B02Y B03O B03Q 100.0(12) . . . . ?
B026 B02Y B03Q B01Z -59.6(14) . . . . ?
B026 B02Y B03Q B02H 38.4(12) . . . . ?
B026 B02Y B03Q B03O -98.8(13) . . . . ?
B026 B02Y B03Q B03S 1.5(16) . . . . ?
B028 C01D B012 C011 -63.3(13) . . . . ?
B028 C01D B012 B01B -103.2(12) . . . . ?
B028 C01D B012 B02N -2.3(14) . . . . ?
B028 C01D B012 B03R 35.2(11) . . . . ?
B028 C01D B01B C011 63.5(13) . . . . ?
B028 C01D B01B B012 105.4(12) . . . . ?
B028 C01D B01B B036 1.8(15) . . . . ?
B028 C01D B01B B049 -38.0(11) . . . . ?
B028 C01D B03R B012 -142.7(13) . . . . ?
B028 C01D B03R B01V -39.4(12) . . . . ?
B028 C01D B03R B02N -103.1(13) . . . . ?
B028 C01D B049 B01B 140.0(12) . . . . ?
B028 C01D B049 B036 101.1(13) . . . . ?
B028 C01D B049 B03B 40.2(12) . . . . ?
B028 B01V B02K C011 -57.9(14) . . . . ?
B028 B01V B02K B02N -97.7(13) . . . . ?
B028 B01V B02K B036 2.9(15) . . . . ?
B028 B01V B02K B03B 40.4(12) . . . . ?
B028 B01V B02N C011 64.8(14) . . . . ?
B028 B01V B02N B012 2.9(15) . . . . ?
B028 B01V B02N B02K 104.1(13) . . . . ?
B028 B01V B02N B03R -37.3(11) . . . . ?
B028 B01V B03B B02K -137.1(12) . . . . ?
B028 B01V B03B B036 -98.4(13) . . . . ?
B028 B01V B03B B049 -35.0(11) . . . . ?
B028 B01V B03R C01D 38.4(11) . . . . ?
B028 B01V B03R B012 99.3(12) . . . . ?
B028 B01V B03R B02N 137.7(12) . . . . ?
B028 B03B B049 C01D -38.1(11) . . . . ?
B028 B03B B049 B01B -99.3(12) . . . . ?
B028 B03B B049 B036 -137.2(12) . . . . ?
B02F C010 B023 C01I -40.5(10) . . . . ?
B02F C010 B023 B01Z -102.1(11) . . . . ?
B02F C010 B023 B03S -141.5(12) . . . . ?
B02F C010 B026 B01P 41.4(11) . . . . ?
B02F C010 B026 B02H 141.7(12) . . . . ?
B02F C010 B026 B02Y 104.9(12) . . . . ?
B02F C010 B02H B026 -35.5(11) . . . . ?
B02F C010 B02H B02Y 1.3(15) . . . . ?
B02F C010 B02H B03Q 66.1(15) . . . . ?
B02F C010 B02H B03S 106.3(12) . . . . ?
B02F C010 B03S B01Z -3.3(17) . . . . ?
B02F C010 B03S B023 37.4(12) . . . . ?
B02F C010 B03S B02H -103.9(13) . . . . ?
B02F C010 B03S B03Q -65.6(15) . . . . ?
B02F C01I B01P B026 -38.7(10) . . . . ?
B02F C01I B01P B02Y -101.7(11) . . . . ?
B02F C01I B01P B03O -141.9(11) . . . . ?
B02F C01I B01Z B023 -37.7(12) . . . . ?
B02F C01I B01Z B03O 105.2(13) . . . . ?
B02F C01I B01Z B03Q 67.3(15) . . . . ?
B02F C01I B01Z B03S 2.1(17) . . . . ?
B02F C01I B023 C010 41.6(10) . . . . ?
B02F C01I B023 B01Z 140.4(13) . . . . ?
B02F C01I B023 B03S 101.3(12) . . . . ?
B02F C01I B03O B01P 36.4(11) . . . . ?
B02F C01I B03O B01Z -103.9(12) . . . . ?
B02F C01I B03O B02Y -3.5(15) . . . . ?
B02F C01I B03O B03Q -66.9(14) . . . . ?
B02F B01P B026 C010 -41.0(10) . . . . ?
B02F B01P B026 B02H -102.7(13) . . . . ?
B02F B01P B026 B02Y -139.9(12) . . . . ?
B02F B01P B02Y B026 35.3(11) . . . . ?
B02F B01P B02Y B02H -2.2(15) . . . . ?
B02F B01P B02Y B03O -100.6(12) . . . . ?
B02F B01P B02Y B03Q -63.4(14) . . . . ?
B02F B01P B03O C01I -33.3(10) . . . . ?
B02F B01P B03O B01Z 1.5(15) . . . . ?
B02F B01P B03O B02Y 101.2(12) . . . . ?
B02F B01P B03O B03Q 63.2(16) . . . . ?
B02F B023 B03S C010 -34.3(10) . . . . ?
B02F B023 B03S B01Z 99.7(12) . . . . ?
B02F B023 B03S B02H 0.8(15) . . . . ?
B02F B023 B03S B03Q 63.2(13) . . . . ?
B02F B026 B02H C010 35.1(11) . . . . ?
B02F B026 B02H B02Y -103.1(13) . . . . ?
B02F B026 B02H B03Q -63.6(16) . . . . ?
B02F B026 B02H B03S 2.1(15) . . . . ?
B02F B026 B02Y B01P -37.4(11) . . . . ?
B02F B026 B02Y B02H 100.9(13) . . . . ?
B02F B026 B02Y B03O 1.1(15) . . . . ?
B02F B026 B02Y B03Q 63.7(14) . . . . ?
B02H C010 B023 C01I 63.9(13) . . . . ?
B02H C010 B023 B01Z 2.3(14) . . . . ?
B02H C010 B023 B02F 104.4(13) . . . . ?
B02H C010 B023 B03S -37.1(12) . . . . ?
B02H C010 B026 B01P -100.2(13) . . . . ?
B02H C010 B026 B02F -141.7(12) . . . . ?
B02H C010 B026 B02Y -36.8(11) . . . . ?
B02H C010 B02F C01I -64.1(14) . . . . ?
B02H C010 B02F B01P -2.7(14) . . . . ?
B02H C010 B02F B023 -105.7(13) . . . . ?
B02H C010 B02F B026 37.0(12) . . . . ?
B02H C010 B03S B01Z 100.6(13) . . . . ?
B02H C010 B03S B023 141.2(12) . . . . ?
B02H C010 B03S B03Q 38.2(11) . . . . ?
B02H B026 B02F C010 -34.0(10) . . . . ?
B02H B026 B02F C01I 60.7(13) . . . . ?
B02H B026 B02F B01P 100.6(12) . . . . ?
B02H B026 B02F B023 -1.6(15) . . . . ?
B02H B026 B02Y B01P -138.2(13) . . . . ?
B02H B026 B02Y B03O -99.7(13) . . . . ?
B02H B026 B02Y B03Q -37.2(12) . . . . ?
B02H B02Y B03O C01I -61.8(14) . . . . ?
B02H B02Y B03O B01P -101.4(13) . . . . ?
B02H B02Y B03O B01Z -0.6(15) . . . . ?
B02H B02Y B03O B03Q 36.8(11) . . . . ?
B02H B02Y B03Q B01Z -98.0(14) . . . . ?
B02H B02Y B03Q B03O -137.2(14) . . . . ?
B02H B02Y B03Q B03S -36.9(12) . . . . ?
B02H B03Q B03S C010 -38.8(11) . . . . ?
B02H B03Q B03S B01Z -138.3(13) . . . . ?
B02H B03Q B03S B023 -101.5(12) . . . . ?
B02K C011 B012 C01D 64.5(12) . . . . ?
B02K C011 B012 B01B 105.8(12) . . . . ?
B02K C011 B012 B02N -33.8(11) . . . . ?
B02K C011 B012 B03R 3.9(14) . . . . ?
B02K C011 B01B C01D -63.5(13) . . . . ?
B02K C011 B01B B012 -105.0(12) . . . . ?
B02K C011 B01B B036 37.8(11) . . . . ?
B02K C011 B01B B049 -1.0(15) . . . . ?
B02K C011 B02N B012 144.1(12) . . . . ?
B02K C011 B02N B01V 39.0(11) . . . . ?
B02K C011 B02N B03R 102.3(12) . . . . ?
B02K C011 B036 B01B -140.8(12) . . . . ?
B02K C011 B036 B03B -37.5(11) . . . . ?
B02K C011 B036 B049 -101.7(12) . . . . ?
B02K B01V B028 C01D 59.3(15) . . . . ?
B02K B01V B028 B03B -38.6(11) . . . . ?
B02K B01V B028 B03R 99.9(13) . . . . ?
B02K B01V B028 B049 -4.2(15) . . . . ?
B02K B01V B02N C011 -39.3(10) . . . . ?
B02K B01V B02N B012 -101.2(11) . . . . ?
B02K B01V B02N B03R -141.4(11) . . . . ?
B02K B01V B03B B028 137.1(12) . . . . ?
B02K B01V B03B B036 38.8(11) . . . . ?
B02K B01V B03B B049 102.2(13) . . . . ?
B02K B01V B03R C01D -64.6(14) . . . . ?
B02K B01V B03R B012 -3.7(14) . . . . ?
B02K B01V B03R B028 -103.0(12) . . . . ?
B02K B01V B03R B02N 34.7(10) . . . . ?
B02K B02N B03R C01D 64.2(13) . . . . ?
B02K B02N B03R B012 102.8(11) . . . . ?
B02K B02N B03R B01V -34.4(10) . . . . ?
B02K B02N B03R B028 3.5(14) . . . . ?
B02K B036 B03B B01V -38.2(11) . . . . ?
B02K B036 B03B B028 -100.6(12) . . . . ?
B02K B036 B03B B049 -138.5(12) . . . . ?
B02K B036 B049 C01D -61.2(13) . . . . ?
B02K B036 B049 B01B -100.2(11) . . . . ?
B02K B036 B049 B028 -2.2(14) . . . . ?
B02K B036 B049 B03B 36.2(10) . . . . ?
B02K B03B B049 C01D 60.8(14) . . . . ?
B02K B03B B049 B01B -0.4(16) . . . . ?
B02K B03B B049 B028 99.0(12) . . . . ?
B02K B03B B049 B036 -38.2(11) . . . . ?
B02N C011 B012 C01D 98.3(11) . . . . ?
B02N C011 B012 B01B 139.6(12) . . . . ?
B02N C011 B012 B03R 37.8(10) . . . . ?
B02N C011 B01B C01D 3.3(14) . . . . ?
B02N C011 B01B B012 -38.1(11) . . . . ?
B02N C011 B01B B036 104.6(12) . . . . ?
B02N C011 B01B B049 65.8(14) . . . . ?
B02N C011 B02K B01V -40.4(11) . . . . ?
B02N C011 B02K B036 -141.5(12) . . . . ?
B02N C011 B02K B03B -103.0(12) . . . . ?
B02N C011 B036 B01B -104.7(12) . . . . ?
B02N C011 B036 B02K 36.1(11) . . . . ?
B02N C011 B036 B03B -1.4(15) . . . . ?
B02N C011 B036 B049 -65.6(14) . . . . ?
B02N B012 B01B C011 35.4(11) . . . . ?
B02N B012 B01B C01D -96.0(12) . . . . ?
B02N B012 B01B B036 1.8(15) . . . . ?
B02N B012 B01B B049 -62.5(14) . . . . ?
B02N B012 B03R C01D 134.8(11) . . . . ?
B02N B012 B03R B01V 39.0(10) . . . . ?
B02N B012 B03R B028 102.3(13) . . . . ?
B02N B01V B028 C01D -4.2(16) . . . . ?
B02N B01V B028 B03B -102.2(13) . . . . ?
B02N B01V B028 B03R 36.4(11) . . . . ?
B02N B01V B028 B049 -67.7(14) . . . . ?
B02N B01V B02K C011 39.8(10) . . . . ?
B02N B01V B02K B036 100.6(11) . . . . ?
B02N B01V B02K B03B 138.1(12) . . . . ?
B02N B01V B03B B028 99.7(13) . . . . ?
B02N B01V B03B B02K -37.5(11) . . . . ?
B02N B01V B03B B036 1.3(16) . . . . ?
B02N B01V B03B B049 64.7(15) . . . . ?
B02N B01V B03R C01D -99.3(12) . . . . ?
B02N B01V B03R B012 -38.4(10) . . . . ?
B02N B01V B03R B028 -137.7(12) . . . . ?
B02N B02K B036 C011 -34.3(11) . . . . ?
B02N B02K B036 B01B -0.2(15) . . . . ?
B02N B02K B036 B03B 101.8(13) . . . . ?
B02N B02K B036 B049 64.0(14) . . . . ?
B02N B02K B03B B01V 38.1(11) . . . . ?
B02N B02K B03B B028 0.5(14) . . . . ?
B02N B02K B03B B036 -100.0(11) . . . . ?
B02N B02K B03B B049 -62.8(14) . . . . ?
B02Y B01P B026 C010 98.8(12) . . . . ?
B02Y B01P B026 B02F 139.9(12) . . . . ?
B02Y B01P B026 B02H 37.2(12) . . . . ?
B02Y B01P B02F C010 2.9(14) . . . . ?
B02Y B01P B02F C01I 97.9(12) . . . . ?
B02Y B01P B02F B023 63.1(14) . . . . ?
B02Y B01P B02F B026 -36.3(11) . . . . ?
B02Y B01P B03O C01I -134.5(12) . . . . ?
B02Y B01P B03O B01Z -99.7(12) . . . . ?
B02Y B01P B03O B03Q -38.0(12) . . . . ?
B02Y B026 B02F C010 -97.9(12) . . . . ?
B02Y B026 B02F C01I -3.2(14) . . . . ?
B02Y B026 B02F B01P 36.7(10) . . . . ?
B02Y B026 B02F B023 -65.4(13) . . . . ?
B02Y B026 B02H C010 138.2(12) . . . . ?
B02Y B026 B02H B03Q 39.5(13) . . . . ?
B02Y B026 B02H B03S 105.2(13) . . . . ?
B02Y B02H B03Q B01Z 102.2(14) . . . . ?
B02Y B02H B03Q B03O 37.6(13) . . . . ?
B02Y B02H B03Q B03S 138.0(13) . . . . ?
B02Y B02H B03S C010 96.6(13) . . . . ?
B02Y B02H B03S B01Z -2.3(16) . . . . ?
B02Y B02H B03S B023 61.7(15) . . . . ?
B02Y B02H B03S B03Q -39.2(12) . . . . ?
B02Y B03O B03Q B01Z -136.9(12) . . . . ?
B02Y B03O B03Q B02H -38.0(13) . . . . ?
B02Y B03O B03Q B03S -100.1(13) . . . . ?
B02Y B03Q B03S C010 -1.4(16) . . . . ?
B02Y B03Q B03S B01Z -100.8(13) . . . . ?
B02Y B03Q B03S B023 -64.0(14) . . . . ?
B02Y B03Q B03S B02H 37.4(12) . . . . ?
B036 C011 B012 C01D -5.0(14) . . . . ?
B036 C011 B012 B01B 36.3(11) . . . . ?
B036 C011 B012 B02N -103.3(12) . . . . ?
B036 C011 B012 B03R -65.5(13) . . . . ?
B036 C011 B01B C01D -101.3(11) . . . . ?
B036 C011 B01B B012 -142.8(11) . . . . ?
B036 C011 B01B B049 -38.8(11) . . . . ?
B036 C011 B02K B01V 101.1(12) . . . . ?
B036 C011 B02K B02N 141.5(12) . . . . ?
B036 C011 B02K B03B 38.5(11) . . . . ?
B036 C011 B02N B012 107.2(12) . . . . ?
B036 C011 B02N B01V 2.1(15) . . . . ?
B036 C011 B02N B02K -36.8(11) . . . . ?
B036 C011 B02N B03R 65.4(14) . . . . ?
B036 B01B B049 C01D -134.9(11) . . . . ?
B036 B01B B049 B028 -101.1(13) . . . . ?
B036 B01B B049 B03B -37.8(10) . . . . ?
B036 B02K B02N C011 33.5(10) . . . . ?
B036 B02K B02N B012 1.3(16) . . . . ?
B036 B02K B02N B01V -101.2(12) . . . . ?
B036 B02K B02N B03R -66.1(14) . . . . ?
B036 B02K B03B B01V 138.1(12) . . . . ?
B036 B02K B03B B028 100.5(12) . . . . ?
B036 B02K B03B B049 37.2(11) . . . . ?
B036 B03B B049 C01D 99.1(12) . . . . ?
B036 B03B B049 B01B 37.9(10) . . . . ?
B036 B03B B049 B028 137.2(12) . . . . ?
B03B B01V B028 C01D 98.0(13) . . . . ?
B03B B01V B028 B03R 138.6(13) . . . . ?
B03B B01V B028 B049 34.4(11) . . . . ?
B03B B01V B02K C011 -98.3(12) . . . . ?
B03B B01V B02K B02N -138.1(12) . . . . ?
B03B B01V B02K B036 -37.5(11) . . . . ?
B03B B01V B02N C011 -2.0(15) . . . . ?
B03B B01V B02N B012 -63.9(15) . . . . ?
B03B B01V B02N B02K 37.2(11) . . . . ?
B03B B01V B02N B03R -104.2(13) . . . . ?
B03B B01V B03R C01D -1.0(16) . . . . ?
B03B B01V B03R B012 59.9(15) . . . . ?
B03B B01V B03R B028 -39.4(12) . . . . ?
B03B B01V B03R B02N 98.4(14) . . . . ?
B03B B028 B03R C01D -99.3(12) . . . . ?
B03B B028 B03R B012 -66.7(13) . . . . ?
B03B B028 B03R B01V 35.5(11) . . . . ?
B03B B028 B03R B02N -3.1(14) . . . . ?
B03B B028 B049 C01D 134.1(13) . . . . ?
B03B B028 B049 B01B 99.2(13) . . . . ?
B03B B028 B049 B036 37.5(11) . . . . ?
B03B B02K B02N C011 97.2(12) . . . . ?
B03B B02K B02N B012 64.9(14) . . . . ?
B03B B02K B02N B01V -37.6(11) . . . . ?
B03B B02K B02N B03R -2.5(15) . . . . ?
B03B B02K B036 C011 -136.1(12) . . . . ?
B03B B02K B036 B01B -102.0(13) . . . . ?
B03B B02K B036 B049 -37.8(11) . . . . ?
B03B B036 B049 C01D -97.4(12) . . . . ?
B03B B036 B049 B01B -136.3(12) . . . . ?
B03B B036 B049 B028 -38.4(11) . . . . ?
B03O C01I B01P B026 103.2(12) . . . . ?
B03O C01I B01P B02F 141.9(11) . . . . ?
B03O C01I B01P B02Y 40.2(10) . . . . ?
B03O C01I B01Z B023 -143.0(12) . . . . ?
B03O C01I B01Z B03Q -38.0(11) . . . . ?
B03O C01I B01Z B03S -103.1(13) . . . . ?
B03O C01I B023 C010 -63.1(13) . . . . ?
B03O C01I B023 B01Z 35.7(12) . . . . ?
B03O C01I B023 B02F -104.7(13) . . . . ?
B03O C01I B023 B03S -3.4(15) . . . . ?
B03O C01I B02F C010 65.0(14) . . . . ?
B03O C01I B02F B01P -35.8(11) . . . . ?
B03O C01I B02F B023 105.5(12) . . . . ?
B03O C01I B02F B026 4.2(14) . . . . ?
B03O B01P B026 C010 59.4(15) . . . . ?
B03O B01P B026 B02F 100.5(13) . . . . ?
B03O B01P B026 B02H -2.3(17) . . . . ?
B03O B01P B026 B02Y -39.4(12) . . . . ?
B03O B01P B02F C010 -60.9(13) . . . . ?
B03O B01P B02F C01I 34.1(10) . . . . ?
B03O B01P B02F B023 -0.7(15) . . . . ?
B03O B01P B02F B026 -100.1(12) . . . . ?
B03O B01P B02Y B026 135.9(12) . . . . ?
B03O B01P B02Y B02H 98.4(13) . . . . ?
B03O B01P B02Y B03Q 37.2(11) . . . . ?
B03O B01Z B023 C010 63.3(13) . . . . ?
B03O B01Z B023 C01I -32.8(10) . . . . ?
B03O B01Z B023 B02F 1.4(15) . . . . ?
B03O B01Z B023 B03S 102.1(13) . . . . ?
B03O B01Z B03Q B02H -101.2(14) . . . . ?
B03O B01Z B03Q B02Y -38.1(11) . . . . ?
B03O B01Z B03Q B03S -137.5(11) . . . . ?
B03O B01Z B03S C010 -60.9(15) . . . . ?
B03O B01Z B03S B023 -101.1(12) . . . . ?
B03O B01Z B03S B02H 1.8(15) . . . . ?
B03O B01Z B03S B03Q 38.3(11) . . . . ?
B03O B02Y B03Q B01Z 39.2(11) . . . . ?
B03O B02Y B03Q B02H 137.2(14) . . . . ?
B03O B02Y B03Q B03S 100.3(13) . . . . ?
B03O B03Q B03S C010 60.9(15) . . . . ?
B03O B03Q B03S B01Z -38.6(11) . . . . ?
B03O B03Q B03S B023 -1.8(15) . . . . ?
B03O B03Q B03S B02H 99.7(14) . . . . ?
B03Q B01Z B023 C010 -0.8(14) . . . . ?
B03Q B01Z B023 C01I -96.8(13) . . . . ?
B03Q B01Z B023 B02F -62.7(14) . . . . ?
B03Q B01Z B023 B03S 38.1(12) . . . . ?
B03Q B01Z B03O C01I 136.9(12) . . . . ?
B03Q B01Z B03O B01P 101.8(12) . . . . ?
B03Q B01Z B03O B02Y 38.6(11) . . . . ?
B03Q B01Z B03S C010 -99.2(13) . . . . ?
B03Q B01Z B03S B023 -139.4(12) . . . . ?
B03Q B01Z B03S B02H -36.5(12) . . . . ?
B03Q B02H B02Y B01P -100.1(13) . . . . ?
B03Q B02H B02Y B026 -136.8(14) . . . . ?
B03Q B02H B02Y B03O -37.7(12) . . . . ?
B03Q B02H B03S C010 135.8(13) . . . . ?
B03Q B02H B03S B01Z 37.0(11) . . . . ?
B03Q B02H B03S B023 100.9(13) . . . . ?
B03Q B02Y B03O C01I -98.6(13) . . . . ?
B03Q B02Y B03O B01P -138.2(13) . . . . ?
B03Q B02Y B03O B01Z -37.4(11) . . . . ?
B03R C01D B012 C011 -98.5(11) . . . . ?
B03R C01D B012 B01B -138.4(11) . . . . ?
B03R C01D B012 B02N -37.5(10) . . . . ?
B03R C01D B01B C011 -2.5(14) . . . . ?
B03R C01D B01B B012 39.3(10) . . . . ?
B03R C01D B01B B036 -64.3(13) . . . . ?
B03R C01D B01B B049 -104.1(12) . . . . ?
B03R C01D B028 B01V 40.1(11) . . . . ?
B03R C01D B028 B03B 100.2(13) . . . . ?
B03R C01D B028 B049 140.1(13) . . . . ?
B03R C01D B049 B01B 102.8(13) . . . . ?
B03R C01D B049 B028 -37.2(12) . . . . ?
B03R C01D B049 B036 63.9(15) . . . . ?
B03R C01D B049 B03B 3.0(16) . . . . ?
B03R B012 B01B C011 94.8(12) . . . . ?
B03R B012 B01B C01D -36.6(10) . . . . ?
B03R B012 B01B B036 61.2(14) . . . . ?
B03R B012 B01B B049 -3.1(15) . . . . ?
B03R B012 B02N C011 -134.5(11) . . . . ?
B03R B012 B02N B01V -39.1(11) . . . . ?
B03R B012 B02N B02K -102.1(13) . . . . ?
B03R B01V B028 C01D -40.6(11) . . . . ?
B03R B01V B028 B03B -138.6(13) . . . . ?
B03R B01V B028 B049 -104.2(12) . . . . ?
B03R B01V B02K C011 6.0(14) . . . . ?
B03R B01V B02K B02N -33.9(10) . . . . ?
B03R B01V B02K B036 66.8(13) . . . . ?
B03R B01V B02K B03B 104.2(12) . . . . ?
B03R B01V B02N C011 102.1(11) . . . . ?
B03R B01V B02N B012 40.2(11) . . . . ?
B03R B01V B02N B02K 141.4(11) . . . . ?
B03R B01V B03B B028 37.9(12) . . . . ?
B03R B01V B03B B02K -99.3(13) . . . . ?
B03R B01V B03B B036 -60.5(16) . . . . ?
B03R B01V B03B B049 2.9(17) . . . . ?
B03R B028 B03B B01V -36.7(11) . . . . ?
B03R B028 B03B B02K 1.6(14) . . . . ?
B03R B028 B03B B036 66.7(13) . . . . ?
B03R B028 B03B B049 104.4(12) . . . . ?
B03R B028 B049 C01D 36.8(11) . . . . ?
B03R B028 B049 B01B 2.0(16) . . . . ?
B03R B028 B049 B036 -59.8(15) . . . . ?
B03R B028 B049 B03B -97.3(14) . . . . ?
B03S C010 B023 C01I 101.1(11) . . . . ?
B03S C010 B023 B01Z 39.4(10) . . . . ?
B03S C010 B023 B02F 141.5(12) . . . . ?
B03S C010 B026 B01P -63.3(15) . . . . ?
B03S C010 B026 B02F -104.7(13) . . . . ?
B03S C010 B026 B02H 36.9(12) . . . . ?
B03S C010 B026 B02Y 0.1(16) . . . . ?
B03S C010 B02F C01I 4.4(16) . . . . ?
B03S C010 B02F B01P 65.8(14) . . . . ?
B03S C010 B02F B023 -37.2(12) . . . . ?
B03S C010 B02F B026 105.5(14) . . . . ?
B03S C010 B02H B026 -141.9(12) . . . . ?
B03S C010 B02H B02Y -105.0(13) . . . . ?
B03S C010 B02H B03Q -40.2(12) . . . . ?
B03S B01Z B023 C010 -38.8(10) . . . . ?
B03S B01Z B023 C01I -134.9(13) . . . . ?
B03S B01Z B023 B02F -100.7(12) . . . . ?
B03S B01Z B03O C01I 97.5(12) . . . . ?
B03S B01Z B03O B01P 62.5(14) . . . . ?
B03S B01Z B03O B02Y -0.8(15) . . . . ?
B03S B01Z B03O B03Q -39.3(11) . . . . ?
B03S B01Z B03Q B02H 36.3(12) . . . . ?
B03S B01Z B03Q B02Y 99.4(12) . . . . ?
B03S B01Z B03Q B03O 137.5(11) . . . . ?
B03S B023 B02F C010 33.6(10) . . . . ?
B03S B023 B02F C01I -97.5(12) . . . . ?
B03S B023 B02F B01P -62.7(13) . . . . ?
B03S B023 B02F B026 0.5(14) . . . . ?
B03S B02H B02Y B01P -60.6(15) . . . . ?
B03S B02H B02Y B026 -97.4(14) . . . . ?
B03S B02H B02Y B03O 1.8(16) . . . . ?
B03S B02H B02Y B03Q 39.4(12) . . . . ?
B03S B02H B03Q B01Z -35.8(12) . . . . ?
B03S B02H B03Q B02Y -138.0(13) . . . . ?
B03S B02H B03Q B03O -100.4(14) . . . . ?
B049 C01D B012 C011 5.7(13) . . . . ?
B049 C01D B012 B01B -34.2(11) . . . . ?
B049 C01D B012 B02N 66.6(13) . . . . ?
B049 C01D B012 B03R 104.1(12) . . . . ?
B049 C01D B01B C011 101.6(12) . . . . ?
B049 C01D B01B B012 143.4(11) . . . . ?
B049 C01D B01B B036 39.8(11) . . . . ?
B049 C01D B028 B01V -100.0(13) . . . . ?
B049 C01D B028 B03B -39.9(11) . . . . ?
B049 C01D B028 B03R -140.1(13) . . . . ?
B049 C01D B03R B012 -104.7(13) . . . . ?
B049 C01D B03R B01V -1.4(16) . . . . ?
B049 C01D B03R B028 38.0(12) . . . . ?
B049 C01D B03R B02N -65.1(14) . . . . ?
B049 B01B B036 C011 136.1(12) . . . . ?
B049 B01B B036 B02K 101.3(13) . . . . ?
B049 B01B B036 B03B 40.0(12) . . . . ?
B049 B028 B03B B01V -141.1(13) . . . . ?
B049 B028 B03B B02K -102.8(13) . . . . ?
B049 B028 B03B B036 -37.7(11) . . . . ?
B049 B028 B03R C01D -36.5(11) . . . . ?
B049 B028 B03R B012 -3.9(17) . . . . ?
B049 B028 B03R B01V 98.2(14) . . . . ?
B049 B028 B03R B02N 59.6(15) . . . . ?
B049 B036 B03B B01V 100.4(13) . . . . ?
B049 B036 B03B B028 37.9(11) . . . . ?
B049 B036 B03B B02K 138.5(12) . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 -0.997 0.000 0.500 715.4 203.8 ?
2 -0.004 0.229 0.912 10.8 0.0 ?
3 -0.004 0.271 0.412 10.8 0.0 ?
4 -0.536 0.500 0.000 715.4 203.8 ?
5 0.004 0.729 0.588 10.8 0.0 ?
6 0.004 0.771 0.088 10.8 0.0 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_cu_ryz_75a_0m_pl
_database_code_depnum_ccdc_archive 'CCDC 2454646'
loop_
_audit_author_name
_audit_author_address
'xie haohui'
;NanJing University of Science and Technology
China
;
_audit_update_record             
;
2025-06-06 deposited with the CCDC.	2026-03-06 downloaded from the CCDC.
;
_audit_creation_date             2025-06-06
_audit_creation_method           
;
Olex2 1.5
(compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C52 H60 Au8 B20 P4 S4'
_chemical_formula_sum            'C52 H60 Au8 B20 P4 S4'
_chemical_formula_weight         2729.05
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -4.4197 7.2980 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   13.3714(5)
_cell_length_b                   23.3899(9)
_cell_length_c                   26.9799(9)
_cell_angle_alpha                90
_cell_angle_beta                 93.7000(10)
_cell_angle_gamma                90
_cell_volume                     8420.5(5)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    9554
_cell_measurement_temperature    100.15
_cell_measurement_theta_max      68.124
_cell_measurement_theta_min      3.283
_shelx_estimated_absorpt_T_max   ?
_shelx_estimated_absorpt_T_min   ?
_exptl_absorpt_coefficient_mu    27.369
_exptl_absorpt_correction_T_max  0.7530
_exptl_absorpt_correction_T_min  0.3240
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1157 before and 0.0538 after correction.
The Ratio of minimum to maximum transmission is 0.4303.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    2.153
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             4912
_exptl_crystal_size_max          0.076
_exptl_crystal_size_mid          0.058
_exptl_crystal_size_min          0.043
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0697
_diffrn_reflns_av_unetI/netI     0.0490
_diffrn_reflns_Laue_measured_fraction_full 0.983
_diffrn_reflns_Laue_measured_fraction_max 0.982
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_k_min       -28
_diffrn_reflns_limit_l_max       31
_diffrn_reflns_limit_l_min       -32
_diffrn_reflns_number            78873
_diffrn_reflns_point_group_measured_fraction_full 0.983
_diffrn_reflns_point_group_measured_fraction_max 0.982
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         68.145
_diffrn_reflns_theta_min         3.283
_diffrn_ambient_temperature      100.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.983
_diffrn_measured_fraction_theta_max 0.982
_diffrn_measurement_device_type  multi-scan
_diffrn_measurement_method       ?
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_source                   ?
_diffrn_source_current           1.1
_diffrn_source_power             0.05500000000000001
_diffrn_source_voltage           50.0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                13574
_reflns_number_total             15103
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.41 (?, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.41 (?, 2016)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'olex2.solve 1.5 (Bourhis et al., 2015)'
_refine_diff_density_max         3.409
_refine_diff_density_min         -2.890
_refine_diff_density_rms         0.391
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.099
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     793
_refine_ls_number_reflns         15103
_refine_ls_number_restraints     492
_refine_ls_R_factor_all          0.0549
_refine_ls_R_factor_gt           0.0386
_refine_ls_restrained_S_all      1.083
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0461P)²+225.5231P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1016
_refine_ls_wR_factor_ref         0.1153
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups
2. Uiso/Uaniso restraints and constraints
C11 \\sim C10 \\sim C9 \\sim C8 \\sim C7 \\sim C12: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
C15 \\sim C20 \\sim C19 \\sim C17 \\sim C18 \\sim C16: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
C21 \\sim C22 \\sim C23 \\sim C24 \\sim C25 \\sim C26: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
C34 \\sim C35 \\sim C36 \\sim C37 \\sim C38: within 2A with sigma of 0.01 and
sigma for terminal atoms of 0.02 within 2A
B7 \\sim B1 \\sim C33 \\sim B9 \\sim B8 \\sim B5 \\sim B6: within 2A with sigma
of 0.01 and sigma for terminal atoms of 0.02 within 2A
B4 \\sim B8 \\sim B3 \\sim C40 \\sim B5 \\sim C39: within 2A with sigma of 0.01
and sigma for terminal atoms of 0.02 within 2A
B16 \\sim B11 \\sim B20 \\sim C13 \\sim B15 \\sim B14: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
C47 \\sim C48 \\sim C49 \\sim C50 \\sim C51 \\sim C52: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
C16 \\sim C15 \\sim C20 \\sim C19 \\sim C18 \\sim C17: within 2A with sigma of
0.001 and sigma for terminal atoms of 0.002 within 2A
C12 \\sim C11 \\sim C10 \\sim C9 \\sim C8 \\sim C7: within 2A with sigma of
0.001 and sigma for terminal atoms of 0.002 within 2A
C42 \\sim C43 \\sim C44 \\sim C45 \\sim C46 \\sim C41: within 2A with sigma of
0.001 and sigma for terminal atoms of 0.002 within 2A
B17 \\sim B18 \\sim B19 \\sim B16: within 2A with sigma of 0.001 and sigma for
terminal atoms of 0.002 within 2A
C30 \\sim C31 \\sim C32 \\sim C28 \\sim C27 \\sim C29: within 2A with sigma of
0.001 and sigma for terminal atoms of 0.002 within 2A
C23 \\sim C22 \\sim C21 \\sim C26 \\sim C25 \\sim C24: within 2A with sigma of
0.001 and sigma for terminal atoms of 0.002 within 2A
C14 \\sim B17 \\sim B15 \\sim B14 \\sim B13 \\sim B19: within 2A with sigma of
0.001 and sigma for terminal atoms of 0.002 within 2A
3.a Aromatic/amide H refined with riding coordinates:
 C10(H10), C48(H48), C9(H9), C36(H36), C8(H8), C16(H16), C28(H28), C49(H49),
 C52(H52), C50(H50), C17(H17), C18(H18), C35(H35), C22(H22), C34(H34), C43(H43),
  C51(H51), C31(H31), C19(H19), C26(H26), C42(H42), C12(H12), C20(H20),
 C11(H11), C4(H4a), C38(H38), C25(H25), C32(H32), C23(H23), C5(H5), C46(H46),
 C24(H24), C37(H37), C3(H3), C30(H30), C29(H29), C1(H1), C44(H44), C6(H6),
 C45(H45)
3.b Boron cage BH refined with riding coordinates:
 B4(H4), B15(H15), B2(H2), B14(H14), B5(H5a), B3(H3a), B6(H6a), B12(H12a),
 B1(H1a), B16(H16a), B13(H13), B10(H10a), B8(H8a), B17(H17a), B9(H9a),
 B20(H20a), B18(H18a), B7(H7), B11(H11a), B19(H19a)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     iterative
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au2 Au -0.25108(3) 0.53069(2) 0.59089(2) 0.01238(10) Uani 1 1 d . . . . .
Au3 Au -0.28894(3) 0.42639(2) 0.64731(2) 0.01067(9) Uani 1 1 d . . . . .
Au4 Au -0.34621(3) 0.54169(2) 0.69585(2) 0.01290(10) Uani 1 1 d . . . . .
Au7 Au 0.05573(3) 0.58847(2) 0.71722(2) 0.01232(10) Uani 1 1 d . . . . .
Au5 Au -0.37767(3) 0.66268(2) 0.72753(2) 0.01286(10) Uani 1 1 d . . . . .
Au1 Au -0.21898(3) 0.62881(2) 0.52599(2) 0.01161(10) Uani 1 1 d . . . . .
Au8 Au -0.06987(3) 0.62224(2) 0.62769(2) 0.01427(10) Uani 1 1 d . . . . .
Au6 Au -0.15946(3) 0.63056(2) 0.73476(2) 0.01452(10) Uani 1 1 d . . . . .
S2 S -0.39981(19) 0.49865(9) 0.62169(8) 0.0140(5) Uani 1 1 d . . . . .
P4 P -0.47214(19) 0.73174(10) 0.68979(8) 0.0127(5) Uani 1 1 d . . . . .
S1 S -0.1033(2) 0.56350(11) 0.55966(9) 0.0170(5) Uani 1 1 d . . . . .
P1 P -0.17956(19) 0.35482(10) 0.66571(8) 0.0118(5) Uani 1 1 d . . . . .
P3 P -0.33664(19) 0.69039(10) 0.49529(8) 0.0117(5) Uani 1 1 d . . . . .
S3 S -0.2945(2) 0.58777(10) 0.76913(9) 0.0168(5) Uani 1 1 d . . . . .
P2 P 0.1422(2) 0.50561(10) 0.72433(9) 0.0125(5) Uani 1 1 d . . . . .
S4 S -0.0272(2) 0.67440(10) 0.69964(10) 0.0184(5) Uani 1 1 d . . . . .
C10 C -0.6498(9) 0.6080(5) 0.4839(4) 0.0216(10) Uani 1 1 d . U . . .
H10 H -0.714672 0.591387 0.483165 0.026 Uiso 1 1 calc R U . . .
C39 C -0.0863(7) 0.3746(4) 0.7168(3) 0.0092(16) Uani 1 1 d . U . . .
C48 C 0.2785(9) 0.4627(5) 0.6573(4) 0.021(2) Uani 1 1 d . U . . .
H48 H 0.320146 0.451942 0.685609 0.025 Uiso 1 1 calc R U . . .
C9 C -0.5681(8) 0.5801(5) 0.5072(4) 0.0215(10) Uani 1 1 d . U . . .
H9 H -0.576529 0.543864 0.522251 0.026 Uiso 1 1 calc R U . . .
C36 C -0.0177(9) 0.3215(5) 0.5233(4) 0.027(2) Uani 1 1 d . U . . .
H36 H 0.013498 0.315290 0.493076 0.033 Uiso 1 1 calc R U . . .
C8 C -0.4756(9) 0.6050(5) 0.5085(4) 0.0211(10) Uani 1 1 d . U . . .
H8 H -0.420240 0.585869 0.524963 0.025 Uiso 1 1 calc R U . . .
C16 C -0.5903(9) 0.6508(5) 0.6407(4) 0.0212(10) Uani 1 1 d . U . . .
H16 H -0.527930 0.633522 0.634658 0.025 Uiso 1 1 calc R U . . .
C28 C -0.3396(9) 0.2838(5) 0.6641(4) 0.0236(10) Uani 1 1 d . U . . .
H28 H -0.374477 0.316838 0.651907 0.028 Uiso 1 1 calc R U . . .
C49 C 0.3115(9) 0.4551(5) 0.6101(4) 0.024(2) Uani 1 1 d . U . . .
H49 H 0.376019 0.439435 0.606246 0.028 Uiso 1 1 calc R U . . .
C14 C -0.4177(8) 0.7632(4) 0.6338(4) 0.0142(8) Uani 1 1 d . U . . .
C21 C -0.4928(8) 0.7933(4) 0.7286(4) 0.0191(10) Uani 1 1 d . U . . .
B4 B -0.0560(8) 0.4462(4) 0.7179(4) 0.0104(17) Uani 1 1 d . U . . .
H4 H -0.085469 0.478326 0.689909 0.012 Uiso 1 1 calc R U . . .
C13 C -0.3557(7) 0.7457(4) 0.5433(4) 0.0130(16) Uani 1 1 d . U . . .
C40 C 0.0643(8) 0.4448(4) 0.7452(3) 0.0134(17) Uani 1 1 d . U . . .
C52 C 0.1239(9) 0.4992(4) 0.6218(4) 0.022(2) Uani 1 1 d . U . . .
H52 H 0.058579 0.513995 0.625247 0.027 Uiso 1 1 calc R U . . .
C50 C 0.2509(9) 0.4703(4) 0.5684(4) 0.021(2) Uani 1 1 d . U . . .
H50 H 0.274293 0.466219 0.536061 0.026 Uiso 1 1 calc R U . . .
C17 C -0.6814(8) 0.6246(5) 0.6224(4) 0.0213(10) Uani 1 1 d . U . . .
H17 H -0.680269 0.590857 0.602887 0.026 Uiso 1 1 calc R U . . .
C18 C -0.7690(9) 0.6484(5) 0.6330(4) 0.0217(10) Uani 1 1 d . U . . .
H18 H -0.829998 0.631893 0.619883 0.026 Uiso 1 1 calc R U . . .
C35 C -0.0428(9) 0.3761(5) 0.5369(4) 0.022(2) Uani 1 1 d . U . . .
H35 H -0.030197 0.407507 0.515876 0.026 Uiso 1 1 calc R U . . .
C47 C 0.1820(8) 0.4865(4) 0.6633(4) 0.0159(19) Uani 1 1 d . U . . .
C33 C -0.1097(8) 0.3394(4) 0.6117(3) 0.0124(19) Uani 1 1 d . . . . .
C22 C -0.4266(8) 0.7975(4) 0.7710(4) 0.0192(10) Uani 1 1 d . U . . .
H22 H -0.380439 0.767377 0.778595 0.023 Uiso 1 1 calc R U . . .
C27 C -0.2379(9) 0.2881(4) 0.6808(4) 0.0234(10) Uani 1 1 d . U . . .
C41 C 0.2608(9) 0.5099(5) 0.7598(4) 0.0229(10) Uani 1 1 d . U . . .
C34 C -0.0865(8) 0.3849(5) 0.5814(4) 0.019(2) Uani 1 1 d . U . . .
H34 H -0.100851 0.422849 0.591406 0.022 Uiso 1 1 calc R U . . .
C43 C 0.4198(9) 0.5630(5) 0.7628(4) 0.0232(10) Uani 1 1 d . U . . .
H43 H 0.460254 0.592532 0.750512 0.028 Uiso 1 1 calc R U . . .
C15 C -0.5923(8) 0.7021(5) 0.6677(4) 0.0211(10) Uani 1 1 d . U . . .
C51 C 0.1565(9) 0.4914(4) 0.5747(4) 0.021(2) Uani 1 1 d . U . . .
H51 H 0.113310 0.500561 0.546424 0.026 Uiso 1 1 calc R U . . .
C31 C -0.2397(9) 0.1881(5) 0.7024(4) 0.0242(10) Uani 1 1 d . U . . .
H31 H -0.207051 0.155757 0.717304 0.029 Uiso 1 1 calc R U . . .
C19 C -0.7718(9) 0.6968(5) 0.6631(4) 0.0218(10) Uani 1 1 d . U . . .
H19 H -0.834331 0.711800 0.671816 0.026 Uiso 1 1 calc R U . . .
C26 C -0.5582(8) 0.8384(4) 0.7164(4) 0.0193(10) Uani 1 1 d . U . . .
H26 H -0.601896 0.836273 0.687243 0.023 Uiso 1 1 calc R U . . .
C42 C 0.3197(9) 0.5562(5) 0.7448(4) 0.0229(10) Uani 1 1 d . U . . .
H42 H 0.290751 0.583397 0.721944 0.027 Uiso 1 1 calc R U . . .
C12 C -0.5448(8) 0.6852(5) 0.4618(4) 0.0211(10) Uani 1 1 d . U . . .
H12 H -0.536949 0.720861 0.445590 0.025 Uiso 1 1 calc R U . . .
C20 C -0.6835(8) 0.7230(5) 0.6801(4) 0.0214(10) Uani 1 1 d . U . . .
H20 H -0.685766 0.755975 0.700565 0.026 Uiso 1 1 calc R U . . .
C11 C -0.6352(9) 0.6606(5) 0.4616(4) 0.0214(10) Uani 1 1 d . U . . .
H11 H -0.691184 0.679686 0.445687 0.026 Uiso 1 1 calc R U . . .
B15 B -0.3421(9) 0.7190(5) 0.6025(4) 0.0142(8) Uani 1 1 d . U . . .
H15 H -0.327782 0.672912 0.611799 0.017 Uiso 1 1 calc R U . . .
C4 C -0.1939(10) 0.7248(5) 0.3710(4) 0.028(3) Uani 1 1 d . . . . .
H4A H -0.138547 0.708716 0.355526 0.034 Uiso 1 1 calc R U . . .
C7 C -0.4603(9) 0.6577(5) 0.4864(4) 0.0208(10) Uani 1 1 d . U . . .
C38 C -0.0846(9) 0.2846(5) 0.5975(4) 0.026(2) Uani 1 1 d . U . . .
H38 H -0.099558 0.253121 0.618065 0.032 Uiso 1 1 calc R U . . .
C25 C -0.5597(8) 0.8864(4) 0.7467(4) 0.0195(10) Uani 1 1 d . U . . .
H25 H -0.604833 0.916846 0.738567 0.023 Uiso 1 1 calc R U . . .
C2 C -0.3047(8) 0.7250(5) 0.4379(3) 0.018(2) Uani 1 1 d . . . . .
C32 C -0.1893(9) 0.2398(4) 0.6995(4) 0.0239(11) Uani 1 1 d . U . . .
H32 H -0.120548 0.241951 0.710603 0.029 Uiso 1 1 calc R U . . .
C23 C -0.4274(8) 0.8450(4) 0.8023(4) 0.0194(10) Uani 1 1 d . U . . .
H23 H -0.384080 0.847105 0.831541 0.023 Uiso 1 1 calc R U . . .
C5 C -0.2438(9) 0.7728(5) 0.3506(4) 0.026(3) Uani 1 1 d . . . . .
H5 H -0.222619 0.789242 0.320822 0.032 Uiso 1 1 calc R U . . .
C46 C 0.3058(9) 0.4728(5) 0.7955(4) 0.0231(10) Uani 1 1 d . U . . .
H46 H 0.268558 0.440985 0.806039 0.028 Uiso 1 1 calc R U . . .
C24 C -0.4941(8) 0.8896(4) 0.7892(4) 0.0197(10) Uani 1 1 d . U . . .
H24 H -0.494843 0.922672 0.809588 0.024 Uiso 1 1 calc R U . . .
C37 C -0.0382(10) 0.2749(6) 0.5540(4) 0.032(2) Uani 1 1 d . U . . .
H37 H -0.020295 0.237154 0.544887 0.038 Uiso 1 1 calc R U . . .
C3 C -0.2267(10) 0.7013(5) 0.4139(4) 0.026(3) Uani 1 1 d . . . . .
H3 H -0.194620 0.667994 0.427390 0.031 Uiso 1 1 calc R U . . .
C30 C -0.3390(9) 0.1843(5) 0.6831(4) 0.0242(10) Uani 1 1 d . U . . .
H30 H -0.371986 0.148317 0.682387 0.029 Uiso 1 1 calc R U . . .
C29 C -0.3894(9) 0.2319(5) 0.6653(4) 0.0241(10) Uani 1 1 d . U . . .
H29 H -0.457938 0.229229 0.653849 0.029 Uiso 1 1 calc R U . . .
C1 C -0.3531(9) 0.7722(4) 0.4170(4) 0.022(2) Uani 1 1 d . . . . .
H1 H -0.407882 0.788343 0.432826 0.026 Uiso 1 1 calc R U . . .
C44 C 0.4577(9) 0.5258(5) 0.7988(4) 0.0234(10) Uani 1 1 d . U . . .
H44 H 0.524352 0.531174 0.812371 0.028 Uiso 1 1 calc R U . . .
C6 C -0.3237(9) 0.7964(5) 0.3734(4) 0.025(3) Uani 1 1 d . . . . .
H6 H -0.357926 0.828821 0.359463 0.030 Uiso 1 1 calc R U . . .
C45 C 0.4017(9) 0.4807(5) 0.8159(4) 0.0234(10) Uani 1 1 d . U . . .
H45 H 0.429146 0.455899 0.841065 0.028 Uiso 1 1 calc R U . . .
B2 B 0.0124(9) 0.3310(5) 0.7386(4) 0.015(2) Uani 1 1 d . . . . .
H2 H 0.027440 0.287188 0.724143 0.018 Uiso 1 1 calc R U . . .
B14 B -0.4613(9) 0.7431(5) 0.5760(4) 0.0141(8) Uani 1 1 d . U . . .
H14 H -0.525545 0.713162 0.567838 0.017 Uiso 1 1 calc R U . . .
B5 B -0.1338(9) 0.4178(5) 0.7620(4) 0.0121(17) Uani 1 1 d . U . . .
H5A H -0.214342 0.430624 0.762814 0.014 Uiso 1 1 calc R U . . .
B3 B 0.0331(9) 0.3925(5) 0.7030(4) 0.0129(18) Uani 1 1 d . U . . .
H3A H 0.061823 0.389725 0.664997 0.015 Uiso 1 1 calc R U . . .
B6 B -0.0925(9) 0.3462(5) 0.7751(4) 0.0153(19) Uani 1 1 d . U . . .
H6A H -0.146568 0.311936 0.784560 0.018 Uiso 1 1 calc R U . . .
B12 B -0.3852(10) 0.8578(5) 0.5748(4) 0.021(3) Uani 1 1 d . . . . .
H12A H -0.399688 0.903956 0.565815 0.025 Uiso 1 1 calc R U . . .
B1 B 0.0327(10) 0.3487(5) 0.8027(4) 0.019(2) Uani 1 1 d . U . . .
H1A H 0.061355 0.316631 0.830980 0.022 Uiso 1 1 calc R U . . .
B16 B -0.2461(9) 0.7632(5) 0.5798(4) 0.0141(9) Uani 1 1 d . U . . .
H16A H -0.169300 0.746682 0.573556 0.017 Uiso 1 1 calc R U . . .
B13 B -0.4787(9) 0.8132(5) 0.5976(4) 0.0143(8) Uani 1 1 d . U . . .
H13 H -0.555067 0.830019 0.604394 0.017 Uiso 1 1 calc R U . . .
B10 B 0.1108(9) 0.3772(5) 0.7580(4) 0.015(2) Uani 1 1 d . . . . .
H10A H 0.191378 0.364669 0.756669 0.018 Uiso 1 1 calc R U . . .
B8 B -0.0323(10) 0.4653(5) 0.7811(4) 0.0173(18) Uani 1 1 d . U . . .
H8A H -0.043783 0.509916 0.794667 0.021 Uiso 1 1 calc R U . . .
B17 B -0.2876(9) 0.7745(5) 0.6403(4) 0.0142(8) Uani 1 1 d . U . . .
H17A H -0.238759 0.765344 0.674681 0.017 Uiso 1 1 calc R U . . .
B9 B 0.0683(9) 0.4219(5) 0.8064(4) 0.0153(19) Uani 1 1 d . U . . .
H9A H 0.121322 0.438377 0.836906 0.018 Uiso 1 1 calc R U . . .
B20 B -0.4400(9) 0.8015(4) 0.5365(4) 0.0138(19) Uani 1 1 d . U . . .
H20A H -0.489188 0.810021 0.502151 0.017 Uiso 1 1 calc R U . . .
B18 B -0.2678(9) 0.8337(5) 0.6006(4) 0.0143(8) Uani 1 1 d . U . . .
H18A H -0.204436 0.864349 0.608400 0.017 Uiso 1 1 calc R U . . .
B7 B -0.0586(9) 0.4027(5) 0.8174(4) 0.0163(18) Uani 1 1 d . U . . .
H7 H -0.089741 0.405906 0.854802 0.020 Uiso 1 1 calc R U . . .
B11 B -0.3071(9) 0.8141(5) 0.5391(4) 0.0169(19) Uani 1 1 d . U . . .
H11A H -0.269643 0.830765 0.506069 0.020 Uiso 1 1 calc R U . . .
B19 B -0.3725(9) 0.8326(5) 0.6371(4) 0.0143(8) Uani 1 1 d . U . . .
H19A H -0.378489 0.861493 0.669905 0.017 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au2 Au3 2.9366(5) . ?
Au2 Au4 3.1888(5) . ?
Au2 Au1 2.9350(5) . ?
Au2 Au8 3.3364(6) . ?
Au2 S2 2.328(2) . ?
Au2 S1 2.328(3) . ?
Au3 Au4 3.1151(5) . ?
Au3 S2 2.324(2) . ?
Au3 P1 2.257(2) . ?
Au4 Au5 2.9938(5) . ?
Au4 Au6 3.3645(6) . ?
Au4 S2 2.312(2) . ?
Au4 S3 2.318(2) . ?
Au7 Au8 2.9590(6) . ?
Au7 Au6 3.1062(6) . ?
Au7 P2 2.259(2) . ?
Au7 S4 2.329(2) . ?
Au5 Au6 3.0070(6) . ?
Au5 P4 2.253(3) . ?
Au5 S3 2.325(2) . ?
Au1 Au8 3.2896(6) . ?
Au1 S1 2.318(2) . ?
Au1 P3 2.251(2) . ?
Au8 Au6 3.2039(6) . ?
Au8 S1 2.313(2) . ?
Au8 S4 2.332(3) . ?
Au6 S3 2.310(3) . ?
Au6 S4 2.301(3) . ?
P4 C14 1.870(10) . ?
P4 C21 1.810(10) . ?
P4 C15 1.816(11) . ?
P1 C39 1.857(10) . ?
P1 C33 1.818(10) . ?
P1 C27 1.803(11) . ?
P3 C13 1.861(10) . ?
P3 C7 1.824(11) . ?
P3 C2 1.823(10) . ?
P2 C40 1.872(10) . ?
P2 C47 1.818(10) . ?
P2 C41 1.801(12) . ?
C10 H10 0.9500 . ?
C10 C9 1.388(16) . ?
C10 C11 1.388(16) . ?
C39 B4 1.722(14) . ?
C39 B2 1.739(14) . ?
C39 B5 1.734(14) . ?
C39 B3 1.715(15) . ?
C39 B6 1.713(13) . ?
C48 H48 0.9500 . ?
C48 C49 1.385(15) . ?
C48 C47 1.423(15) . ?
C9 H9 0.9500 . ?
C9 C8 1.366(16) . ?
C36 H36 0.9500 . ?
C36 C35 1.376(17) . ?
C36 C37 1.407(18) . ?
C8 H8 0.9500 . ?
C8 C7 1.389(16) . ?
C16 H16 0.9500 . ?
C16 C17 1.423(15) . ?
C16 C15 1.404(15) . ?
C28 H28 0.9500 . ?
C28 C27 1.408(17) . ?
C28 C29 1.387(15) . ?
C49 H49 0.9500 . ?
C49 C50 1.390(16) . ?
C14 B15 1.707(14) . ?
C14 B14 1.695(14) . ?
C14 B13 1.699(14) . ?
C14 B17 1.757(15) . ?
C14 B19 1.733(15) . ?
C21 C22 1.404(15) . ?
C21 C26 1.397(16) . ?
B4 H4 1.1200 . ?
B4 C40 1.725(14) . ?
B4 B5 1.759(15) . ?
B4 B3 1.794(15) . ?
B4 B8 1.771(15) . ?
C13 B15 1.712(14) . ?
C13 B14 1.712(15) . ?
C13 B16 1.759(15) . ?
C13 B20 1.727(14) . ?
C13 B11 1.734(14) . ?
C40 B3 1.704(14) . ?
C40 B10 1.725(14) . ?
C40 B8 1.731(15) . ?
C40 B9 1.733(14) . ?
C52 H52 0.9500 . ?
C52 C47 1.353(15) . ?
C52 C51 1.384(15) . ?
C50 H50 0.9500 . ?
C50 C51 1.376(17) . ?
C17 H17 0.9500 . ?
C17 C18 1.344(16) . ?
C18 H18 0.9500 . ?
C18 C19 1.395(15) . ?
C35 H35 0.9500 . ?
C35 C34 1.384(14) . ?
C33 C34 1.389(14) . ?
C33 C38 1.386(15) . ?
C22 H22 0.9500 . ?
C22 C23 1.396(14) . ?
C27 C32 1.383(16) . ?
C41 C42 1.414(15) . ?
C41 C46 1.403(16) . ?
C34 H34 0.9500 . ?
C43 H43 0.9500 . ?
C43 C42 1.404(16) . ?
C43 C44 1.375(16) . ?
C15 C20 1.374(16) . ?
C51 H51 0.9500 . ?
C31 H31 0.9500 . ?
C31 C32 1.387(15) . ?
C31 C30 1.397(17) . ?
C19 H19 0.9500 . ?
C19 C20 1.383(15) . ?
C26 H26 0.9500 . ?
C26 C25 1.389(14) . ?
C42 H42 0.9500 . ?
C12 H12 0.9500 . ?
C12 C11 1.339(16) . ?
C12 C7 1.426(16) . ?
C20 H20 0.9500 . ?
C11 H11 0.9500 . ?
B15 H15 1.1200 . ?
B15 B14 1.796(16) . ?
B15 B16 1.787(16) . ?
B15 B17 1.778(15) . ?
C4 H4A 0.9500 . ?
C4 C5 1.401(17) . ?
C4 C3 1.380(15) . ?
C38 H38 0.9500 . ?
C38 C37 1.382(16) . ?
C25 H25 0.9500 . ?
C25 C24 1.400(16) . ?
C2 C3 1.378(16) . ?
C2 C1 1.381(15) . ?
C32 H32 0.9500 . ?
C23 H23 0.9500 . ?
C23 C24 1.403(16) . ?
C5 H5 0.9500 . ?
C5 C6 1.383(18) . ?
C46 H46 0.9500 . ?
C46 C45 1.374(16) . ?
C24 H24 0.9500 . ?
C37 H37 0.9500 . ?
C3 H3 0.9500 . ?
C30 H30 0.9500 . ?
C30 C29 1.372(16) . ?
C29 H29 0.9500 . ?
C1 H1 0.9500 . ?
C1 C6 1.384(15) . ?
C44 H44 0.9500 . ?
C44 C45 1.389(16) . ?
C6 H6 0.9500 . ?
C45 H45 0.9500 . ?
B2 H2 1.1200 . ?
B2 B3 1.761(15) . ?
B2 B6 1.800(17) . ?
B2 B1 1.782(16) . ?
B2 B10 1.755(17) . ?
B14 H14 1.1200 . ?
B14 B13 1.760(15) . ?
B14 B20 1.766(15) . ?
B5 H5A 1.1200 . ?
B5 B6 1.790(16) . ?
B5 B8 1.804(17) . ?
B5 B7 1.782(15) . ?
B3 H3A 1.1200 . ?
B3 B10 1.790(16) . ?
B6 H6A 1.1200 . ?
B6 B1 1.789(17) . ?
B6 B7 1.785(16) . ?
B12 H12A 1.1200 . ?
B12 B13 1.769(17) . ?
B12 B20 1.799(16) . ?
B12 B18 1.768(18) . ?
B12 B11 1.787(17) . ?
B12 B19 1.780(16) . ?
B1 H1A 1.1200 . ?
B1 B10 1.777(16) . ?
B1 B9 1.777(16) . ?
B1 B7 1.816(17) . ?
B16 H16A 1.1200 . ?
B16 B17 1.779(15) . ?
B16 B18 1.771(15) . ?
B16 B11 1.781(16) . ?
B13 H13 1.1200 . ?
B13 B20 1.780(16) . ?
B13 B19 1.779(16) . ?
B10 H10A 1.1200 . ?
B10 B9 1.793(16) . ?
B8 H8A 1.1200 . ?
B8 B9 1.785(17) . ?
B8 B7 1.808(16) . ?
B17 H17A 1.1200 . ?
B17 B18 1.781(16) . ?
B17 B19 1.769(16) . ?
B9 H9A 1.1200 . ?
B9 B7 1.798(17) . ?
B20 H20A 1.1200 . ?
B20 B11 1.798(17) . ?
B18 H18A 1.1200 . ?
B18 B11 1.768(15) . ?
B18 B19 1.763(16) . ?
B7 H7 1.1200 . ?
B11 H11A 1.1200 . ?
B19 H19A 1.1200 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Au3 Au2 Au4 60.971(12) . . ?
Au3 Au2 Au8 121.675(16) . . ?
Au4 Au2 Au8 90.438(14) . . ?
Au1 Au2 Au3 174.583(18) . . ?
Au1 Au2 Au4 123.287(16) . . ?
Au1 Au2 Au8 62.891(13) . . ?
S2 Au2 Au3 50.79(6) . . ?
S2 Au2 Au4 46.38(6) . . ?
S2 Au2 Au1 128.74(6) . . ?
S2 Au2 Au8 136.15(6) . . ?
S2 Au2 S1 179.41(9) . . ?
S1 Au2 Au3 129.80(6) . . ?
S1 Au2 Au4 133.74(6) . . ?
S1 Au2 Au1 50.66(6) . . ?
S1 Au2 Au8 43.86(6) . . ?
Au2 Au3 Au4 63.515(13) . . ?
S2 Au3 Au2 50.92(6) . . ?
S2 Au3 Au4 47.62(6) . . ?
P1 Au3 Au2 126.82(6) . . ?
P1 Au3 Au4 136.30(6) . . ?
P1 Au3 S2 175.41(8) . . ?
Au2 Au4 Au6 89.791(14) . . ?
Au3 Au4 Au2 55.514(11) . . ?
Au3 Au4 Au6 117.930(16) . . ?
Au5 Au4 Au2 113.653(15) . . ?
Au5 Au4 Au3 168.887(18) . . ?
Au5 Au4 Au6 56.083(13) . . ?
S2 Au4 Au2 46.80(6) . . ?
S2 Au4 Au3 47.94(6) . . ?
S2 Au4 Au5 128.11(6) . . ?
S2 Au4 Au6 136.17(6) . . ?
S2 Au4 S3 178.06(8) . . ?
S3 Au4 Au2 132.91(7) . . ?
S3 Au4 Au3 133.90(6) . . ?
S3 Au4 Au5 49.95(6) . . ?
S3 Au4 Au6 43.28(6) . . ?
Au8 Au7 Au6 63.718(13) . . ?
P2 Au7 Au8 123.98(6) . . ?
P2 Au7 Au6 137.17(7) . . ?
P2 Au7 S4 172.75(9) . . ?
S4 Au7 Au8 50.64(6) . . ?
S4 Au7 Au6 47.48(7) . . ?
Au4 Au5 Au6 68.206(14) . . ?
P4 Au5 Au4 129.33(6) . . ?
P4 Au5 Au6 136.21(7) . . ?
P4 Au5 S3 174.43(9) . . ?
S3 Au5 Au4 49.74(6) . . ?
S3 Au5 Au6 49.35(7) . . ?
Au2 Au1 Au8 64.529(13) . . ?
S1 Au1 Au2 50.98(6) . . ?
S1 Au1 Au8 44.67(6) . . ?
P3 Au1 Au2 126.45(6) . . ?
P3 Au1 Au8 135.10(6) . . ?
P3 Au1 S1 177.42(9) . . ?
Au7 Au8 Au2 115.763(15) . . ?
Au7 Au8 Au1 167.135(17) . . ?
Au7 Au8 Au6 60.378(13) . . ?
Au1 Au8 Au2 52.580(11) . . ?
Au6 Au8 Au2 90.037(14) . . ?
Au6 Au8 Au1 120.495(17) . . ?
S1 Au8 Au2 44.22(6) . . ?
S1 Au8 Au7 124.02(6) . . ?
S1 Au8 Au1 44.79(6) . . ?
S1 Au8 Au6 133.42(6) . . ?
S1 Au8 S4 174.57(9) . . ?
S4 Au8 Au2 135.85(7) . . ?
S4 Au8 Au7 50.55(6) . . ?
S4 Au8 Au1 140.58(6) . . ?
S4 Au8 Au6 45.85(7) . . ?
Au7 Au6 Au4 115.646(15) . . ?
Au7 Au6 Au8 55.904(12) . . ?
Au5 Au6 Au4 55.711(12) . . ?
Au5 Au6 Au7 166.856(17) . . ?
Au5 Au6 Au8 111.986(16) . . ?
Au8 Au6 Au4 89.675(14) . . ?
S3 Au6 Au4 43.45(6) . . ?
S3 Au6 Au7 132.80(6) . . ?
S3 Au6 Au5 49.77(6) . . ?
S3 Au6 Au8 133.07(6) . . ?
S4 Au6 Au4 136.19(6) . . ?
S4 Au6 Au7 48.25(6) . . ?
S4 Au6 Au5 129.08(6) . . ?
S4 Au6 Au8 46.66(6) . . ?
S4 Au6 S3 178.84(9) . . ?
Au3 S2 Au2 78.29(8) . . ?
Au4 S2 Au2 86.81(8) . . ?
Au4 S2 Au3 84.44(8) . . ?
C14 P4 Au5 114.3(3) . . ?
C21 P4 Au5 114.2(4) . . ?
C21 P4 C14 103.7(5) . . ?
C21 P4 C15 109.2(5) . . ?
C15 P4 Au5 109.4(4) . . ?
C15 P4 C14 105.5(5) . . ?
Au1 S1 Au2 78.35(8) . . ?
Au8 S1 Au2 91.92(9) . . ?
Au8 S1 Au1 90.53(9) . . ?
C39 P1 Au3 111.9(3) . . ?
C33 P1 Au3 109.2(3) . . ?
C33 P1 C39 106.9(4) . . ?
C27 P1 Au3 114.1(4) . . ?
C27 P1 C39 109.1(5) . . ?
C27 P1 C33 105.1(5) . . ?
C13 P3 Au1 108.2(3) . . ?
C7 P3 Au1 112.7(4) . . ?
C7 P3 C13 102.6(5) . . ?
C2 P3 Au1 113.6(4) . . ?
C2 P3 C13 109.5(5) . . ?
C2 P3 C7 109.6(5) . . ?
Au4 S3 Au5 80.31(8) . . ?
Au6 S3 Au4 93.26(9) . . ?
Au6 S3 Au5 80.89(8) . . ?
C40 P2 Au7 112.7(3) . . ?
C47 P2 Au7 108.2(3) . . ?
C47 P2 C40 106.7(4) . . ?
C41 P2 Au7 115.2(4) . . ?
C41 P2 C40 111.8(5) . . ?
C41 P2 C47 101.3(5) . . ?
Au7 S4 Au8 78.81(7) . . ?
Au6 S4 Au7 84.26(8) . . ?
Au6 S4 Au8 87.49(9) . . ?
C9 C10 H10 120.5 . . ?
C11 C10 H10 120.5 . . ?
C11 C10 C9 119.0(11) . . ?
B4 C39 P1 113.6(6) . . ?
B4 C39 B2 113.0(7) . . ?
B4 C39 B5 61.2(6) . . ?
B2 C39 P1 124.3(7) . . ?
B5 C39 P1 114.1(6) . . ?
B5 C39 B2 114.1(7) . . ?
B3 C39 P1 119.3(6) . . ?
B3 C39 B4 62.9(6) . . ?
B3 C39 B2 61.3(6) . . ?
B3 C39 B5 113.5(7) . . ?
B6 C39 P1 121.0(7) . . ?
B6 C39 B4 112.7(7) . . ?
B6 C39 B2 62.9(6) . . ?
B6 C39 B5 62.6(6) . . ?
B6 C39 B3 113.3(7) . . ?
C49 C48 H48 120.0 . . ?
C49 C48 C47 120.0(10) . . ?
C47 C48 H48 120.0 . . ?
C10 C9 H9 120.1 . . ?
C8 C9 C10 119.7(11) . . ?
C8 C9 H9 120.1 . . ?
C35 C36 H36 119.9 . . ?
C35 C36 C37 120.1(10) . . ?
C37 C36 H36 119.9 . . ?
C9 C8 H8 119.2 . . ?
C9 C8 C7 121.6(11) . . ?
C7 C8 H8 119.2 . . ?
C17 C16 H16 119.9 . . ?
C15 C16 H16 119.9 . . ?
C15 C16 C17 120.2(11) . . ?
C27 C28 H28 119.7 . . ?
C29 C28 H28 119.7 . . ?
C29 C28 C27 120.7(11) . . ?
C48 C49 H49 119.7 . . ?
C48 C49 C50 120.6(11) . . ?
C50 C49 H49 119.7 . . ?
B15 C14 P4 115.8(7) . . ?
B15 C14 B17 61.7(6) . . ?
B15 C14 B19 112.2(8) . . ?
B14 C14 P4 120.4(7) . . ?
B14 C14 B15 63.7(6) . . ?
B14 C14 B13 62.5(6) . . ?
B14 C14 B17 114.4(8) . . ?
B14 C14 B19 113.9(8) . . ?
B13 C14 P4 122.5(7) . . ?
B13 C14 B15 114.3(8) . . ?
B13 C14 B17 112.9(8) . . ?
B13 C14 B19 62.5(6) . . ?
B17 C14 P4 114.4(6) . . ?
B19 C14 P4 118.6(6) . . ?
B19 C14 B17 60.9(6) . . ?
C22 C21 P4 114.6(8) . . ?
C26 C21 P4 125.5(8) . . ?
C26 C21 C22 119.4(9) . . ?
C39 B4 H4 124.7 . . ?
C39 B4 C40 101.6(7) . . ?
C39 B4 B5 59.7(6) . . ?
C39 B4 B3 58.3(6) . . ?
C39 B4 B8 106.8(7) . . ?
C40 B4 H4 125.3 . . ?
C40 B4 B5 106.3(7) . . ?
C40 B4 B3 57.9(6) . . ?
C40 B4 B8 59.3(6) . . ?
B5 B4 H4 120.8 . . ?
B5 B4 B3 108.5(7) . . ?
B5 B4 B8 61.5(6) . . ?
B3 B4 H4 121.9 . . ?
B8 B4 H4 120.9 . . ?
B8 B4 B3 108.2(7) . . ?
B15 C13 P3 112.6(6) . . ?
B15 C13 B16 61.9(6) . . ?
B15 C13 B20 113.9(8) . . ?
B15 C13 B11 112.4(7) . . ?
B14 C13 P3 119.3(7) . . ?
B14 C13 B15 63.3(6) . . ?
B14 C13 B16 113.9(7) . . ?
B14 C13 B20 61.8(6) . . ?
B14 C13 B11 113.0(8) . . ?
B16 C13 P3 113.8(6) . . ?
B20 C13 P3 124.7(7) . . ?
B20 C13 B16 113.4(7) . . ?
B20 C13 B11 62.6(7) . . ?
B11 C13 P3 121.8(7) . . ?
B11 C13 B16 61.3(6) . . ?
B4 C40 P2 112.3(6) . . ?
B4 C40 B8 61.7(6) . . ?
B4 C40 B9 112.5(8) . . ?
B3 C40 P2 117.5(6) . . ?
B3 C40 B4 63.1(6) . . ?
B3 C40 B10 62.9(6) . . ?
B3 C40 B8 114.4(8) . . ?
B3 C40 B9 113.9(7) . . ?
B10 C40 P2 123.8(7) . . ?
B10 C40 B4 114.6(8) . . ?
B10 C40 B8 114.5(8) . . ?
B10 C40 B9 62.5(6) . . ?
B8 C40 P2 114.1(7) . . ?
B8 C40 B9 62.0(6) . . ?
B9 C40 P2 122.5(7) . . ?
C47 C52 H52 118.9 . . ?
C47 C52 C51 122.3(11) . . ?
C51 C52 H52 118.9 . . ?
C49 C50 H50 120.6 . . ?
C51 C50 C49 118.9(10) . . ?
C51 C50 H50 120.6 . . ?
C16 C17 H17 120.4 . . ?
C18 C17 C16 119.1(10) . . ?
C18 C17 H17 120.4 . . ?
C17 C18 H18 119.5 . . ?
C17 C18 C19 121.1(11) . . ?
C19 C18 H18 119.5 . . ?
C36 C35 H35 120.2 . . ?
C36 C35 C34 119.6(10) . . ?
C34 C35 H35 120.2 . . ?
C48 C47 P2 121.3(8) . . ?
C52 C47 P2 120.6(9) . . ?
C52 C47 C48 117.9(10) . . ?
C34 C33 P1 117.8(8) . . ?
C38 C33 P1 123.4(8) . . ?
C38 C33 C34 118.7(10) . . ?
C21 C22 H22 119.3 . . ?
C23 C22 C21 121.3(10) . . ?
C23 C22 H22 119.3 . . ?
C28 C27 P1 114.4(8) . . ?
C32 C27 P1 126.2(9) . . ?
C32 C27 C28 118.7(10) . . ?
C42 C41 P2 112.2(8) . . ?
C46 C41 P2 130.9(9) . . ?
C46 C41 C42 116.6(11) . . ?
C35 C34 C33 121.2(10) . . ?
C35 C34 H34 119.4 . . ?
C33 C34 H34 119.4 . . ?
C42 C43 H43 120.9 . . ?
C44 C43 H43 120.9 . . ?
C44 C43 C42 118.2(11) . . ?
C16 C15 P4 116.8(9) . . ?
C20 C15 P4 124.3(8) . . ?
C20 C15 C16 118.5(10) . . ?
C52 C51 H51 119.8 . . ?
C50 C51 C52 120.4(10) . . ?
C50 C51 H51 119.8 . . ?
C32 C31 H31 120.4 . . ?
C32 C31 C30 119.2(11) . . ?
C30 C31 H31 120.4 . . ?
C18 C19 H19 120.1 . . ?
C20 C19 C18 119.9(11) . . ?
C20 C19 H19 120.1 . . ?
C21 C26 H26 119.8 . . ?
C25 C26 C21 120.3(11) . . ?
C25 C26 H26 119.8 . . ?
C41 C42 H42 119.2 . . ?
C43 C42 C41 121.6(10) . . ?
C43 C42 H42 119.2 . . ?
C11 C12 H12 120.2 . . ?
C11 C12 C7 119.7(10) . . ?
C7 C12 H12 120.2 . . ?
C15 C20 C19 120.9(10) . . ?
C15 C20 H20 119.6 . . ?
C19 C20 H20 119.6 . . ?
C10 C11 H11 118.9 . . ?
C12 C11 C10 122.1(11) . . ?
C12 C11 H11 118.9 . . ?
C14 B15 C13 102.1(7) . . ?
C14 B15 H15 124.7 . . ?
C14 B15 B14 57.8(6) . . ?
C14 B15 B16 106.3(8) . . ?
C14 B15 B17 60.5(6) . . ?
C13 B15 H15 124.5 . . ?
C13 B15 B14 58.4(6) . . ?
C13 B15 B16 60.3(6) . . ?
C13 B15 B17 106.5(8) . . ?
B14 B15 H15 121.7 . . ?
B16 B15 H15 121.2 . . ?
B16 B15 B14 108.6(8) . . ?
B17 B15 H15 121.1 . . ?
B17 B15 B14 108.6(8) . . ?
B17 B15 B16 59.9(6) . . ?
C5 C4 H4A 120.7 . . ?
C3 C4 H4A 120.7 . . ?
C3 C4 C5 118.7(12) . . ?
C8 C7 P3 118.2(9) . . ?
C8 C7 C12 117.8(10) . . ?
C12 C7 P3 123.8(8) . . ?
C33 C38 H38 119.5 . . ?
C37 C38 C33 121.1(11) . . ?
C37 C38 H38 119.5 . . ?
C26 C25 H25 120.2 . . ?
C26 C25 C24 119.5(10) . . ?
C24 C25 H25 120.2 . . ?
C3 C2 P3 116.5(8) . . ?
C3 C2 C1 118.6(10) . . ?
C1 C2 P3 124.9(9) . . ?
C27 C32 C31 120.9(11) . . ?
C27 C32 H32 119.5 . . ?
C31 C32 H32 119.5 . . ?
C22 C23 H23 121.0 . . ?
C22 C23 C24 118.0(10) . . ?
C24 C23 H23 121.0 . . ?
C4 C5 H5 119.7 . . ?
C6 C5 C4 120.5(10) . . ?
C6 C5 H5 119.7 . . ?
C41 C46 H46 118.7 . . ?
C45 C46 C41 122.6(11) . . ?
C45 C46 H46 118.7 . . ?
C25 C24 C23 121.4(9) . . ?
C25 C24 H24 119.3 . . ?
C23 C24 H24 119.3 . . ?
C36 C37 H37 120.4 . . ?
C38 C37 C36 119.2(11) . . ?
C38 C37 H37 120.4 . . ?
C4 C3 H3 119.2 . . ?
C2 C3 C4 121.7(11) . . ?
C2 C3 H3 119.2 . . ?
C31 C30 H30 119.6 . . ?
C29 C30 C31 120.8(10) . . ?
C29 C30 H30 119.6 . . ?
C28 C29 H29 120.2 . . ?
C30 C29 C28 119.5(11) . . ?
C30 C29 H29 120.2 . . ?
C2 C1 H1 119.2 . . ?
C2 C1 C6 121.5(11) . . ?
C6 C1 H1 119.2 . . ?
C43 C44 H44 118.9 . . ?
C43 C44 C45 122.2(11) . . ?
C45 C44 H44 118.9 . . ?
C5 C6 C1 119.0(11) . . ?
C5 C6 H6 120.5 . . ?
C1 C6 H6 120.5 . . ?
C46 C45 C44 118.6(11) . . ?
C46 C45 H45 120.7 . . ?
C44 C45 H45 120.7 . . ?
C39 B2 H2 124.6 . . ?
C39 B2 B3 58.7(6) . . ?
C39 B2 B6 57.9(6) . . ?
C39 B2 B1 104.9(8) . . ?
C39 B2 B10 106.1(8) . . ?
B3 B2 H2 121.3 . . ?
B3 B2 B6 107.0(8) . . ?
B3 B2 B1 108.7(8) . . ?
B6 B2 H2 122.3 . . ?
B1 B2 H2 122.1 . . ?
B1 B2 B6 59.9(7) . . ?
B10 B2 H2 121.3 . . ?
B10 B2 B3 61.2(6) . . ?
B10 B2 B6 108.1(8) . . ?
B10 B2 B1 60.3(7) . . ?
C14 B14 C13 102.6(8) . . ?
C14 B14 B15 58.5(6) . . ?
C14 B14 H14 124.6 . . ?
C14 B14 B13 58.9(6) . . ?
C14 B14 B20 106.4(8) . . ?
C13 B14 B15 58.4(6) . . ?
C13 B14 H14 124.7 . . ?
C13 B14 B13 105.6(8) . . ?
C13 B14 B20 59.5(6) . . ?
B15 B14 H14 122.1 . . ?
B13 B14 B15 107.1(8) . . ?
B13 B14 H14 122.1 . . ?
B13 B14 B20 60.7(6) . . ?
B20 B14 B15 108.1(8) . . ?
B20 B14 H14 121.2 . . ?
C39 B5 B4 59.1(6) . . ?
C39 B5 H5A 124.6 . . ?
C39 B5 B6 58.1(6) . . ?
C39 B5 B8 104.9(8) . . ?
C39 B5 B7 105.2(8) . . ?
B4 B5 H5A 121.6 . . ?
B4 B5 B6 107.4(8) . . ?
B4 B5 B8 59.6(6) . . ?
B4 B5 B7 108.4(8) . . ?
B6 B5 H5A 122.1 . . ?
B6 B5 B8 107.6(8) . . ?
B8 B5 H5A 122.4 . . ?
B7 B5 H5A 121.8 . . ?
B7 B5 B6 60.0(6) . . ?
B7 B5 B8 60.5(6) . . ?
C39 B3 B4 58.7(6) . . ?
C39 B3 B2 60.0(6) . . ?
C39 B3 H3A 124.3 . . ?
C39 B3 B10 105.7(7) . . ?
B4 B3 H3A 121.2 . . ?
C40 B3 C39 102.8(7) . . ?
C40 B3 B4 59.0(6) . . ?
C40 B3 B2 105.2(7) . . ?
C40 B3 H3A 124.7 . . ?
C40 B3 B10 59.1(6) . . ?
B2 B3 B4 108.6(8) . . ?
B2 B3 H3A 121.8 . . ?
B2 B3 B10 59.3(6) . . ?
B10 B3 B4 108.2(7) . . ?
B10 B3 H3A 122.2 . . ?
C39 B6 B2 59.3(6) . . ?
C39 B6 B5 59.3(6) . . ?
C39 B6 H6A 123.9 . . ?
C39 B6 B1 105.7(8) . . ?
C39 B6 B7 105.9(8) . . ?
B2 B6 H6A 121.4 . . ?
B5 B6 B2 108.5(8) . . ?
B5 B6 H6A 121.3 . . ?
B1 B6 B2 59.5(7) . . ?
B1 B6 B5 108.6(8) . . ?
B1 B6 H6A 121.9 . . ?
B7 B6 B2 108.7(8) . . ?
B7 B6 B5 59.8(6) . . ?
B7 B6 H6A 121.7 . . ?
B7 B6 B1 61.1(7) . . ?
B13 B12 H12A 121.9 . . ?
B13 B12 B20 59.8(6) . . ?
B13 B12 B11 107.5(8) . . ?
B13 B12 B19 60.2(6) . . ?
B20 B12 H12A 121.5 . . ?
B18 B12 H12A 122.0 . . ?
B18 B12 B13 107.7(8) . . ?
B18 B12 B20 108.0(8) . . ?
B18 B12 B11 59.6(7) . . ?
B18 B12 B19 59.6(7) . . ?
B11 B12 H12A 122.2 . . ?
B11 B12 B20 60.2(6) . . ?
B19 B12 H12A 121.9 . . ?
B19 B12 B20 108.1(8) . . ?
B19 B12 B11 107.2(9) . . ?
B2 B1 B6 60.5(6) . . ?
B2 B1 H1A 121.9 . . ?
B2 B1 B7 108.1(8) . . ?
B6 B1 H1A 122.1 . . ?
B6 B1 B7 59.3(7) . . ?
B10 B1 B2 59.1(6) . . ?
B10 B1 B6 107.7(8) . . ?
B10 B1 H1A 121.6 . . ?
B10 B1 B9 60.6(6) . . ?
B10 B1 B7 108.6(8) . . ?
B9 B1 B2 107.5(8) . . ?
B9 B1 B6 107.2(8) . . ?
B9 B1 H1A 121.9 . . ?
B9 B1 B7 60.0(7) . . ?
B7 B1 H1A 121.6 . . ?
C13 B16 B15 57.7(6) . . ?
C13 B16 H16A 125.1 . . ?
C13 B16 B17 104.4(8) . . ?
C13 B16 B18 104.2(8) . . ?
C13 B16 B11 58.7(6) . . ?
B15 B16 H16A 122.5 . . ?
B17 B16 B15 59.8(6) . . ?
B17 B16 H16A 122.1 . . ?
B17 B16 B11 108.0(8) . . ?
B18 B16 B15 107.1(8) . . ?
B18 B16 H16A 122.6 . . ?
B18 B16 B17 60.2(6) . . ?
B18 B16 B11 59.7(6) . . ?
B11 B16 B15 106.7(8) . . ?
B11 B16 H16A 121.8 . . ?
C14 B13 B14 58.7(6) . . ?
C14 B13 B12 106.4(9) . . ?
C14 B13 H13 123.9 . . ?
C14 B13 B20 105.6(8) . . ?
C14 B13 B19 59.7(6) . . ?
B14 B13 B12 108.8(8) . . ?
B14 B13 H13 121.5 . . ?
B14 B13 B20 59.8(6) . . ?
B14 B13 B19 108.5(8) . . ?
B12 B13 H13 121.4 . . ?
B12 B13 B20 60.9(6) . . ?
B12 B13 B19 60.2(7) . . ?
B20 B13 H13 121.9 . . ?
B19 B13 H13 120.9 . . ?
B19 B13 B20 109.0(8) . . ?
C40 B10 B2 104.5(8) . . ?
C40 B10 B3 58.0(6) . . ?
C40 B10 B1 105.0(8) . . ?
C40 B10 H10A 124.7 . . ?
C40 B10 B9 59.0(6) . . ?
B2 B10 B3 59.5(6) . . ?
B2 B10 B1 60.6(6) . . ?
B2 B10 H10A 122.2 . . ?
B2 B10 B9 108.0(8) . . ?
B3 B10 H10A 122.3 . . ?
B3 B10 B9 107.1(8) . . ?
B1 B10 B3 107.6(9) . . ?
B1 B10 H10A 122.1 . . ?
B1 B10 B9 59.7(6) . . ?
B9 B10 H10A 121.7 . . ?
B4 B8 B5 58.9(6) . . ?
B4 B8 H8A 122.0 . . ?
B4 B8 B9 107.9(8) . . ?
B4 B8 B7 106.7(8) . . ?
C40 B8 B4 59.0(6) . . ?
C40 B8 B5 104.1(8) . . ?
C40 B8 H8A 124.4 . . ?
C40 B8 B9 59.0(6) . . ?
C40 B8 B7 104.9(8) . . ?
B5 B8 H8A 123.4 . . ?
B5 B8 B7 59.1(6) . . ?
B9 B8 B5 107.0(8) . . ?
B9 B8 H8A 121.4 . . ?
B9 B8 B7 60.0(7) . . ?
B7 B8 H8A 122.8 . . ?
C14 B17 B15 57.7(6) . . ?
C14 B17 B16 104.5(7) . . ?
C14 B17 H17A 125.1 . . ?
C14 B17 B18 104.0(8) . . ?
C14 B17 B19 58.9(6) . . ?
B15 B17 B16 60.3(6) . . ?
B15 B17 H17A 122.1 . . ?
B15 B17 B18 107.1(8) . . ?
B16 B17 H17A 122.2 . . ?
B16 B17 B18 59.7(6) . . ?
B18 B17 H17A 123.0 . . ?
B19 B17 B15 107.2(8) . . ?
B19 B17 B16 107.9(8) . . ?
B19 B17 H17A 121.6 . . ?
B19 B17 B18 59.6(6) . . ?
C40 B9 B1 104.7(8) . . ?
C40 B9 B10 58.5(6) . . ?
C40 B9 B8 58.9(6) . . ?
C40 B9 H9A 125.0 . . ?
C40 B9 B7 105.2(8) . . ?
B1 B9 B10 59.7(6) . . ?
B1 B9 B8 109.5(9) . . ?
B1 B9 H9A 121.8 . . ?
B1 B9 B7 61.1(7) . . ?
B10 B9 H9A 121.5 . . ?
B10 B9 B7 108.7(8) . . ?
B8 B9 B10 108.6(8) . . ?
B8 B9 H9A 120.7 . . ?
B8 B9 B7 60.6(7) . . ?
B7 B9 H9A 121.6 . . ?
C13 B20 B14 58.7(6) . . ?
C13 B20 B12 104.7(8) . . ?
C13 B20 B13 104.1(7) . . ?
C13 B20 H20A 124.5 . . ?
C13 B20 B11 58.9(6) . . ?
B14 B20 B12 107.2(8) . . ?
B14 B20 B13 59.5(6) . . ?
B14 B20 H20A 121.8 . . ?
B14 B20 B11 107.5(8) . . ?
B12 B20 H20A 122.8 . . ?
B13 B20 B12 59.2(6) . . ?
B13 B20 H20A 123.3 . . ?
B13 B20 B11 106.6(8) . . ?
B11 B20 B12 59.6(7) . . ?
B11 B20 H20A 122.0 . . ?
B12 B18 B16 109.4(8) . . ?
B12 B18 B17 108.8(8) . . ?
B12 B18 H18A 120.8 . . ?
B16 B18 B17 60.1(6) . . ?
B16 B18 H18A 121.2 . . ?
B17 B18 H18A 121.7 . . ?
B11 B18 B12 60.7(7) . . ?
B11 B18 B16 60.4(6) . . ?
B11 B18 B17 108.5(8) . . ?
B11 B18 H18A 121.2 . . ?
B19 B18 B12 60.5(6) . . ?
B19 B18 B16 108.4(8) . . ?
B19 B18 B17 59.9(6) . . ?
B19 B18 H18A 121.5 . . ?
B19 B18 B11 108.8(8) . . ?
B5 B7 B6 60.2(6) . . ?
B5 B7 B1 107.8(8) . . ?
B5 B7 B8 60.3(6) . . ?
B5 B7 B9 107.5(8) . . ?
B5 B7 H7 121.4 . . ?
B6 B7 B1 59.6(7) . . ?
B6 B7 B8 107.7(8) . . ?
B6 B7 B9 106.4(8) . . ?
B6 B7 H7 122.1 . . ?
B1 B7 H7 122.5 . . ?
B8 B7 B1 106.8(8) . . ?
B8 B7 H7 122.0 . . ?
B9 B7 B1 58.9(7) . . ?
B9 B7 B8 59.4(6) . . ?
B9 B7 H7 122.8 . . ?
C13 B11 B12 104.9(8) . . ?
C13 B11 B16 60.0(6) . . ?
C13 B11 B20 58.5(6) . . ?
C13 B11 B18 105.5(8) . . ?
C13 B11 H11A 124.2 . . ?
B12 B11 B20 60.3(7) . . ?
B12 B11 H11A 122.5 . . ?
B16 B11 B12 108.1(8) . . ?
B16 B11 B20 109.0(8) . . ?
B16 B11 H11A 120.8 . . ?
B20 B11 H11A 121.2 . . ?
B18 B11 B12 59.7(7) . . ?
B18 B11 B16 59.9(6) . . ?
B18 B11 B20 108.2(8) . . ?
B18 B11 H11A 122.4 . . ?
C14 B19 B12 104.4(7) . . ?
C14 B19 B13 57.8(6) . . ?
C14 B19 B17 60.2(6) . . ?
C14 B19 B18 105.7(8) . . ?
C14 B19 H19A 124.4 . . ?
B12 B19 H19A 122.5 . . ?
B13 B19 B12 59.6(6) . . ?
B13 B19 H19A 122.1 . . ?
B17 B19 B12 108.8(8) . . ?
B17 B19 B13 108.6(8) . . ?
B17 B19 H19A 120.3 . . ?
B18 B19 B12 59.9(7) . . ?
B18 B19 B13 107.5(8) . . ?
B18 B19 B17 60.6(6) . . ?
B18 B19 H19A 122.2 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Au3 P1 C39 B4 -32.3(7) . . . . ?
Au3 P1 C39 B2 -176.9(6) . . . . ?
Au3 P1 C39 B5 35.3(7) . . . . ?
Au3 P1 C39 B3 -103.4(6) . . . . ?
Au3 P1 C39 B6 106.6(7) . . . . ?
Au3 P1 C33 C34 34.9(9) . . . . ?
Au3 P1 C33 C38 -140.7(9) . . . . ?
Au3 P1 C27 C28 19.4(10) . . . . ?
Au3 P1 C27 C32 -171.1(9) . . . . ?
Au7 P2 C40 B4 39.7(7) . . . . ?
Au7 P2 C40 B3 110.0(7) . . . . ?
Au7 P2 C40 B10 -175.6(6) . . . . ?
Au7 P2 C40 B8 -28.0(7) . . . . ?
Au7 P2 C40 B9 -99.1(7) . . . . ?
Au7 P2 C47 C48 140.5(8) . . . . ?
Au7 P2 C47 C52 -33.6(9) . . . . ?
Au7 P2 C41 C42 -48.8(9) . . . . ?
Au7 P2 C41 C46 137.5(10) . . . . ?
Au5 P4 C14 B15 28.3(8) . . . . ?
Au5 P4 C14 B14 101.7(7) . . . . ?
Au5 P4 C14 B13 176.5(6) . . . . ?
Au5 P4 C14 B17 -40.7(7) . . . . ?
Au5 P4 C14 B19 -109.6(7) . . . . ?
Au5 P4 C21 C22 16.8(9) . . . . ?
Au5 P4 C21 C26 -171.6(8) . . . . ?
Au5 P4 C15 C16 -48.6(9) . . . . ?
Au5 P4 C15 C20 124.3(9) . . . . ?
Au1 P3 C13 B15 -34.1(7) . . . . ?
Au1 P3 C13 B14 -105.1(7) . . . . ?
Au1 P3 C13 B16 34.0(7) . . . . ?
Au1 P3 C13 B20 -179.4(7) . . . . ?
Au1 P3 C13 B11 103.9(7) . . . . ?
Au1 P3 C7 C8 13.8(10) . . . . ?
Au1 P3 C7 C12 -171.8(8) . . . . ?
Au1 P3 C2 C3 14.1(10) . . . . ?
Au1 P3 C2 C1 -166.4(8) . . . . ?
P4 C14 B15 C13 152.7(6) . . . . ?
P4 C14 B15 B14 112.8(8) . . . . ?
P4 C14 B15 B16 -145.1(7) . . . . ?
P4 C14 B15 B17 -105.1(7) . . . . ?
P4 C14 B14 C13 -145.8(7) . . . . ?
P4 C14 B14 B15 -105.9(8) . . . . ?
P4 C14 B14 B13 113.4(8) . . . . ?
P4 C14 B14 B20 152.6(7) . . . . ?
P4 C14 B13 B14 -110.2(8) . . . . ?
P4 C14 B13 B12 147.5(7) . . . . ?
P4 C14 B13 B20 -148.9(7) . . . . ?
P4 C14 B13 B19 107.9(8) . . . . ?
P4 C14 B17 B15 107.4(7) . . . . ?
P4 C14 B17 B16 147.2(6) . . . . ?
P4 C14 B17 B18 -151.0(6) . . . . ?
P4 C14 B17 B19 -110.4(7) . . . . ?
P4 C14 B19 B12 -152.8(7) . . . . ?
P4 C14 B19 B13 -113.9(8) . . . . ?
P4 C14 B19 B17 103.6(8) . . . . ?
P4 C14 B19 B18 145.0(7) . . . . ?
P4 C21 C22 C23 174.5(8) . . . . ?
P4 C21 C26 C25 -172.9(8) . . . . ?
P4 C15 C20 C19 -177.8(9) . . . . ?
P1 C39 B4 C40 -152.3(6) . . . . ?
P1 C39 B4 B5 105.5(7) . . . . ?
P1 C39 B4 B3 -112.1(7) . . . . ?
P1 C39 B4 B8 146.5(7) . . . . ?
P1 C39 B2 B3 107.6(8) . . . . ?
P1 C39 B2 B6 -110.5(8) . . . . ?
P1 C39 B2 B1 -149.3(7) . . . . ?
P1 C39 B2 B10 147.9(7) . . . . ?
P1 C39 B5 B4 -104.8(7) . . . . ?
P1 C39 B5 B6 113.8(7) . . . . ?
P1 C39 B5 B8 -144.5(6) . . . . ?
P1 C39 B5 B7 152.6(6) . . . . ?
P1 C39 B3 B4 103.3(7) . . . . ?
P1 C39 B3 C40 144.2(6) . . . . ?
P1 C39 B3 B2 -115.4(8) . . . . ?
P1 C39 B3 B10 -154.7(6) . . . . ?
P1 C39 B6 B2 115.5(8) . . . . ?
P1 C39 B6 B5 -103.0(8) . . . . ?
P1 C39 B6 B1 154.4(7) . . . . ?
P1 C39 B6 B7 -141.9(7) . . . . ?
P1 C33 C34 C35 -173.2(9) . . . . ?
P1 C33 C38 C37 175.0(10) . . . . ?
P1 C27 C32 C31 -169.8(9) . . . . ?
P3 C13 B15 C14 -152.1(6) . . . . ?
P3 C13 B15 B14 -112.5(7) . . . . ?
P3 C13 B15 B16 105.9(7) . . . . ?
P3 C13 B15 B17 145.5(7) . . . . ?
P3 C13 B14 C14 142.1(7) . . . . ?
P3 C13 B14 B15 102.2(8) . . . . ?
P3 C13 B14 B13 -157.1(6) . . . . ?
P3 C13 B14 B20 -116.1(8) . . . . ?
P3 C13 B16 B15 -103.9(7) . . . . ?
P3 C13 B16 B17 -143.0(6) . . . . ?
P3 C13 B16 B18 154.6(6) . . . . ?
P3 C13 B16 B11 114.5(8) . . . . ?
P3 C13 B20 B14 107.7(8) . . . . ?
P3 C13 B20 B12 -150.9(7) . . . . ?
P3 C13 B20 B13 147.7(7) . . . . ?
P3 C13 B20 B11 -111.3(8) . . . . ?
P3 C13 B11 B12 155.7(7) . . . . ?
P3 C13 B11 B16 -101.7(8) . . . . ?
P3 C13 B11 B20 115.7(8) . . . . ?
P3 C13 B11 B18 -142.2(7) . . . . ?
P3 C2 C3 C4 -178.1(9) . . . . ?
P3 C2 C1 C6 179.3(8) . . . . ?
P2 C40 B3 C39 -143.3(6) . . . . ?
P2 C40 B3 B4 -102.5(7) . . . . ?
P2 C40 B3 B2 154.7(7) . . . . ?
P2 C40 B3 B10 116.0(8) . . . . ?
P2 C40 B10 B2 -145.1(7) . . . . ?
P2 C40 B10 B3 -106.4(8) . . . . ?
P2 C40 B10 B1 152.0(7) . . . . ?
P2 C40 B10 B9 112.4(8) . . . . ?
P2 C40 B8 B4 103.4(7) . . . . ?
P2 C40 B8 B5 142.9(6) . . . . ?
P2 C40 B8 B9 -115.5(7) . . . . ?
P2 C40 B8 B7 -155.8(6) . . . . ?
P2 C40 B9 B1 -153.8(7) . . . . ?
P2 C40 B9 B10 -114.3(9) . . . . ?
P2 C40 B9 B8 102.1(8) . . . . ?
P2 C40 B9 B7 142.8(7) . . . . ?
P2 C41 C42 C43 -171.4(9) . . . . ?
P2 C41 C46 C45 174.3(9) . . . . ?
C10 C9 C8 C7 -0.8(16) . . . . ?
C39 P1 C33 C34 -86.3(9) . . . . ?
C39 P1 C33 C38 98.1(10) . . . . ?
C39 P1 C27 C28 145.4(8) . . . . ?
C39 P1 C27 C32 -45.1(11) . . . . ?
C39 B4 C40 P2 150.9(6) . . . . ?
C39 B4 C40 B3 40.4(6) . . . . ?
C39 B4 C40 B10 2.9(10) . . . . ?
C39 B4 C40 B8 -102.8(7) . . . . ?
C39 B4 C40 B9 -66.0(9) . . . . ?
C39 B4 B5 B6 33.7(7) . . . . ?
C39 B4 B5 B8 134.3(8) . . . . ?
C39 B4 B5 B7 97.0(8) . . . . ?
C39 B4 B3 C40 -131.8(7) . . . . ?
C39 B4 B3 B2 -34.8(7) . . . . ?
C39 B4 B3 B10 -97.6(8) . . . . ?
C39 B4 B8 C40 93.7(8) . . . . ?
C39 B4 B8 B5 -40.2(7) . . . . ?
C39 B4 B8 B9 59.3(10) . . . . ?
C39 B4 B8 B7 -3.9(10) . . . . ?
C39 B2 B3 B4 34.3(7) . . . . ?
C39 B2 B3 C40 96.2(8) . . . . ?
C39 B2 B3 B10 134.9(8) . . . . ?
C39 B2 B6 B5 -34.4(7) . . . . ?
C39 B2 B6 B1 -135.6(8) . . . . ?
C39 B2 B6 B7 -97.8(8) . . . . ?
C39 B2 B1 B6 37.8(7) . . . . ?
C39 B2 B1 B10 -100.3(8) . . . . ?
C39 B2 B1 B9 -62.4(10) . . . . ?
C39 B2 B1 B7 1.0(10) . . . . ?
C39 B2 B10 C40 -1.1(9) . . . . ?
C39 B2 B10 B3 -39.1(7) . . . . ?
C39 B2 B10 B1 98.2(8) . . . . ?
C39 B2 B10 B9 60.5(9) . . . . ?
C39 B5 B6 B2 34.4(7) . . . . ?
C39 B5 B6 B1 97.5(8) . . . . ?
C39 B5 B6 B7 135.6(8) . . . . ?
C39 B5 B8 B4 39.4(6) . . . . ?
C39 B5 B8 C40 -0.1(9) . . . . ?
C39 B5 B8 B9 -61.6(9) . . . . ?
C39 B5 B8 B7 -99.2(8) . . . . ?
C39 B5 B7 B6 -38.0(7) . . . . ?
C39 B5 B7 B1 -0.7(10) . . . . ?
C39 B5 B7 B8 98.8(8) . . . . ?
C39 B5 B7 B9 61.4(9) . . . . ?
C39 B3 B10 C40 -95.7(8) . . . . ?
C39 B3 B10 B2 39.6(7) . . . . ?
C39 B3 B10 B1 1.3(10) . . . . ?
C39 B3 B10 B9 -61.6(9) . . . . ?
C39 B6 B1 B2 -38.7(7) . . . . ?
C39 B6 B1 B10 -1.8(10) . . . . ?
C39 B6 B1 B9 62.1(9) . . . . ?
C39 B6 B1 B7 99.8(8) . . . . ?
C39 B6 B7 B5 38.7(7) . . . . ?
C39 B6 B7 B1 -99.4(8) . . . . ?
C39 B6 B7 B8 0.0(11) . . . . ?
C39 B6 B7 B9 -62.4(9) . . . . ?
C48 C49 C50 C51 -1.9(16) . . . . ?
C9 C10 C11 C12 0.2(16) . . . . ?
C9 C8 C7 P3 174.3(8) . . . . ?
C9 C8 C7 C12 -0.4(16) . . . . ?
C36 C35 C34 C33 -2.9(17) . . . . ?
C16 C17 C18 C19 -2.3(17) . . . . ?
C16 C15 C20 C19 -5.0(16) . . . . ?
C28 C27 C32 C31 -0.6(17) . . . . ?
C49 C48 C47 P2 -172.0(8) . . . . ?
C49 C48 C47 C52 2.3(15) . . . . ?
C49 C50 C51 C52 2.3(16) . . . . ?
C14 P4 C21 C22 -108.2(8) . . . . ?
C14 P4 C21 C26 63.4(10) . . . . ?
C14 P4 C15 C16 74.8(9) . . . . ?
C14 P4 C15 C20 -112.3(10) . . . . ?
C14 B15 B14 C13 132.7(8) . . . . ?
C14 B15 B14 B13 34.5(7) . . . . ?
C14 B15 B14 B20 98.5(8) . . . . ?
C14 B15 B16 C13 -94.8(8) . . . . ?
C14 B15 B16 B17 40.3(7) . . . . ?
C14 B15 B16 B18 1.5(10) . . . . ?
C14 B15 B16 B11 -61.1(9) . . . . ?
C14 B15 B17 B16 -134.5(8) . . . . ?
C14 B15 B17 B18 -96.0(8) . . . . ?
C14 B15 B17 B19 -33.4(7) . . . . ?
C14 B14 B13 B12 98.2(9) . . . . ?
C14 B14 B13 B20 135.8(8) . . . . ?
C14 B14 B13 B19 34.2(7) . . . . ?
C14 B14 B20 C13 95.2(8) . . . . ?
C14 B14 B20 B12 -1.9(11) . . . . ?
C14 B14 B20 B13 -38.4(7) . . . . ?
C14 B14 B20 B11 60.8(9) . . . . ?
C14 B13 B20 C13 -1.5(10) . . . . ?
C14 B13 B20 B14 38.2(7) . . . . ?
C14 B13 B20 B12 -100.4(9) . . . . ?
C14 B13 B20 B11 -62.8(9) . . . . ?
C14 B13 B19 B12 135.3(8) . . . . ?
C14 B13 B19 B17 33.9(7) . . . . ?
C14 B13 B19 B18 97.9(8) . . . . ?
C14 B17 B18 B12 3.2(10) . . . . ?
C14 B17 B18 B16 -98.9(8) . . . . ?
C14 B17 B18 B11 -61.3(9) . . . . ?
C14 B17 B18 B19 40.2(7) . . . . ?
C14 B17 B19 B12 -96.2(8) . . . . ?
C14 B17 B19 B13 -32.9(7) . . . . ?
C14 B17 B19 B18 -133.0(8) . . . . ?
C21 P4 C14 B15 153.3(7) . . . . ?
C21 P4 C14 B14 -133.4(8) . . . . ?
C21 P4 C14 B13 -58.5(9) . . . . ?
C21 P4 C14 B17 84.3(7) . . . . ?
C21 P4 C14 B19 15.4(8) . . . . ?
C21 P4 C15 C16 -174.3(8) . . . . ?
C21 P4 C15 C20 -1.5(11) . . . . ?
C21 C22 C23 C24 -2.1(16) . . . . ?
C21 C26 C25 C24 0.9(16) . . . . ?
B4 C39 B2 B3 -37.2(7) . . . . ?
B4 C39 B2 B6 104.7(8) . . . . ?
B4 C39 B2 B1 65.9(9) . . . . ?
B4 C39 B2 B10 3.1(10) . . . . ?
B4 C39 B5 B6 -141.4(8) . . . . ?
B4 C39 B5 B8 -39.7(7) . . . . ?
B4 C39 B5 B7 -102.6(8) . . . . ?
B4 C39 B3 C40 41.0(6) . . . . ?
B4 C39 B3 B2 141.3(8) . . . . ?
B4 C39 B3 B10 102.1(8) . . . . ?
B4 C39 B6 B2 -105.2(8) . . . . ?
B4 C39 B6 B5 36.3(8) . . . . ?
B4 C39 B6 B1 -66.4(10) . . . . ?
B4 C39 B6 B7 -2.6(11) . . . . ?
B4 C40 B3 C39 -40.8(6) . . . . ?
B4 C40 B3 B2 -102.8(8) . . . . ?
B4 C40 B3 B10 -141.6(8) . . . . ?
B4 C40 B10 B2 -1.2(10) . . . . ?
B4 C40 B10 B3 37.6(8) . . . . ?
B4 C40 B10 B1 -64.1(10) . . . . ?
B4 C40 B10 B9 -103.7(9) . . . . ?
B4 C40 B8 B5 39.5(7) . . . . ?
B4 C40 B8 B9 141.1(8) . . . . ?
B4 C40 B8 B7 100.8(8) . . . . ?
B4 C40 B9 B1 67.5(10) . . . . ?
B4 C40 B9 B10 107.0(9) . . . . ?
B4 C40 B9 B8 -36.7(8) . . . . ?
B4 C40 B9 B7 4.0(10) . . . . ?
B4 B5 B6 C39 -34.1(7) . . . . ?
B4 B5 B6 B2 0.3(10) . . . . ?
B4 B5 B6 B1 63.4(9) . . . . ?
B4 B5 B6 B7 101.6(9) . . . . ?
B4 B5 B8 C40 -39.5(7) . . . . ?
B4 B5 B8 B9 -101.0(8) . . . . ?
B4 B5 B8 B7 -138.6(8) . . . . ?
B4 B5 B7 B6 -99.9(8) . . . . ?
B4 B5 B7 B1 -62.6(10) . . . . ?
B4 B5 B7 B8 36.9(7) . . . . ?
B4 B5 B7 B9 -0.5(10) . . . . ?
B4 B3 B10 C40 -34.1(7) . . . . ?
B4 B3 B10 B2 101.2(9) . . . . ?
B4 B3 B10 B1 62.9(10) . . . . ?
B4 B3 B10 B9 0.0(10) . . . . ?
B4 B8 B9 C40 34.4(7) . . . . ?
B4 B8 B9 B1 -61.3(10) . . . . ?
B4 B8 B9 B10 2.2(11) . . . . ?
B4 B8 B9 B7 -99.3(9) . . . . ?
B4 B8 B7 B5 -36.2(8) . . . . ?
B4 B8 B7 B6 2.4(11) . . . . ?
B4 B8 B7 B1 65.1(10) . . . . ?
B4 B8 B7 B9 101.4(8) . . . . ?
C13 P3 C7 C8 -102.3(9) . . . . ?
C13 P3 C7 C12 72.0(10) . . . . ?
C13 P3 C2 C3 135.2(9) . . . . ?
C13 P3 C2 C1 -45.3(11) . . . . ?
C13 B15 B14 C14 -132.7(8) . . . . ?
C13 B15 B14 B13 -98.1(8) . . . . ?
C13 B15 B14 B20 -34.2(7) . . . . ?
C13 B15 B16 B17 135.1(8) . . . . ?
C13 B15 B16 B18 96.3(8) . . . . ?
C13 B15 B16 B11 33.7(7) . . . . ?
C13 B15 B17 C14 94.8(8) . . . . ?
C13 B15 B17 B16 -39.8(7) . . . . ?
C13 B15 B17 B18 -1.3(10) . . . . ?
C13 B15 B17 B19 61.4(10) . . . . ?
C13 B14 B13 C14 -95.4(8) . . . . ?
C13 B14 B13 B12 2.7(10) . . . . ?
C13 B14 B13 B20 40.4(7) . . . . ?
C13 B14 B13 B19 -61.2(9) . . . . ?
C13 B14 B20 B12 -97.1(9) . . . . ?
C13 B14 B20 B13 -133.6(8) . . . . ?
C13 B14 B20 B11 -34.3(7) . . . . ?
C13 B16 B17 C14 -0.5(9) . . . . ?
C13 B16 B17 B15 38.0(7) . . . . ?
C13 B16 B17 B18 -98.4(8) . . . . ?
C13 B16 B17 B19 -62.0(9) . . . . ?
C13 B16 B18 B12 -2.4(10) . . . . ?
C13 B16 B18 B17 98.7(8) . . . . ?
C13 B16 B18 B11 -39.6(7) . . . . ?
C13 B16 B18 B19 62.0(9) . . . . ?
C13 B16 B11 B12 97.1(9) . . . . ?
C13 B16 B11 B20 33.2(7) . . . . ?
C13 B16 B11 B18 133.6(8) . . . . ?
C13 B20 B11 B12 -134.3(8) . . . . ?
C13 B20 B11 B16 -33.8(7) . . . . ?
C13 B20 B11 B18 -97.4(8) . . . . ?
C40 P2 C47 C48 -98.0(9) . . . . ?
C40 P2 C47 C52 87.8(9) . . . . ?
C40 P2 C41 C42 -179.1(8) . . . . ?
C40 P2 C41 C46 7.2(13) . . . . ?
C40 B4 B5 C39 -94.1(7) . . . . ?
C40 B4 B5 B6 -60.4(9) . . . . ?
C40 B4 B5 B8 40.2(7) . . . . ?
C40 B4 B5 B7 2.9(10) . . . . ?
C40 B4 B3 C39 131.8(7) . . . . ?
C40 B4 B3 B2 96.9(8) . . . . ?
C40 B4 B3 B10 34.2(7) . . . . ?
C40 B4 B8 B5 -133.9(8) . . . . ?
C40 B4 B8 B9 -34.4(7) . . . . ?
C40 B4 B8 B7 -97.6(9) . . . . ?
C40 B3 B10 B2 135.4(8) . . . . ?
C40 B3 B10 B1 97.0(9) . . . . ?
C40 B3 B10 B9 34.2(7) . . . . ?
C40 B10 B9 B1 134.5(9) . . . . ?
C40 B10 B9 B8 32.4(7) . . . . ?
C40 B10 B9 B7 96.7(8) . . . . ?
C40 B8 B9 B1 -95.8(8) . . . . ?
C40 B8 B9 B10 -32.2(7) . . . . ?
C40 B8 B9 B7 -133.7(8) . . . . ?
C40 B8 B7 B5 -97.8(8) . . . . ?
C40 B8 B7 B6 -59.1(10) . . . . ?
C40 B8 B7 B1 3.5(10) . . . . ?
C40 B8 B7 B9 39.9(7) . . . . ?
C40 B9 B7 B5 -2.0(10) . . . . ?
C40 B9 B7 B6 61.3(9) . . . . ?
C40 B9 B7 B1 98.6(8) . . . . ?
C40 B9 B7 B8 -39.9(7) . . . . ?
C17 C16 C15 P4 179.6(8) . . . . ?
C17 C16 C15 C20 6.3(16) . . . . ?
C17 C18 C19 C20 3.6(17) . . . . ?
C18 C19 C20 C15 0.1(17) . . . . ?
C35 C36 C37 C38 0.7(19) . . . . ?
C47 P2 C40 B4 -78.9(7) . . . . ?
C47 P2 C40 B3 -8.6(8) . . . . ?
C47 P2 C40 B10 65.8(8) . . . . ?
C47 P2 C40 B8 -146.6(7) . . . . ?
C47 P2 C40 B9 142.3(8) . . . . ?
C47 P2 C41 C42 67.7(9) . . . . ?
C47 P2 C41 C46 -106.0(12) . . . . ?
C47 C48 C49 C50 -0.4(16) . . . . ?
C47 C52 C51 C50 -0.4(16) . . . . ?
C33 P1 C39 B4 87.3(7) . . . . ?
C33 P1 C39 B2 -57.4(8) . . . . ?
C33 P1 C39 B5 154.9(6) . . . . ?
C33 P1 C39 B3 16.1(8) . . . . ?
C33 P1 C39 B6 -133.8(7) . . . . ?
C33 P1 C27 C28 -100.3(9) . . . . ?
C33 P1 C27 C32 69.3(11) . . . . ?
C33 C38 C37 C36 -1.0(19) . . . . ?
C22 C21 C26 C25 -1.7(16) . . . . ?
C22 C23 C24 C25 1.3(16) . . . . ?
C27 P1 C39 B4 -159.5(7) . . . . ?
C27 P1 C39 B2 55.8(9) . . . . ?
C27 P1 C39 B5 -91.9(7) . . . . ?
C27 P1 C39 B3 129.4(7) . . . . ?
C27 P1 C39 B6 -20.6(9) . . . . ?
C27 P1 C33 C34 157.8(8) . . . . ?
C27 P1 C33 C38 -17.8(11) . . . . ?
C27 C28 C29 C30 0.3(17) . . . . ?
C41 P2 C40 B4 171.3(6) . . . . ?
C41 P2 C40 B3 -118.4(8) . . . . ?
C41 P2 C40 B10 -44.0(9) . . . . ?
C41 P2 C40 B8 103.6(8) . . . . ?
C41 P2 C40 B9 32.5(9) . . . . ?
C41 P2 C47 C48 19.0(9) . . . . ?
C41 P2 C47 C52 -155.2(9) . . . . ?
C41 C46 C45 C44 -2.8(17) . . . . ?
C34 C33 C38 C37 -0.6(18) . . . . ?
C43 C44 C45 C46 0.9(18) . . . . ?
C15 P4 C14 B15 -92.0(8) . . . . ?
C15 P4 C14 B14 -18.6(9) . . . . ?
C15 P4 C14 B13 56.3(8) . . . . ?
C15 P4 C14 B17 -161.0(7) . . . . ?
C15 P4 C14 B19 130.2(7) . . . . ?
C15 P4 C21 C22 139.7(8) . . . . ?
C15 P4 C21 C26 -48.7(11) . . . . ?
C15 C16 C17 C18 -2.7(16) . . . . ?
C51 C52 C47 P2 172.4(8) . . . . ?
C51 C52 C47 C48 -2.0(15) . . . . ?
C31 C30 C29 C28 3.3(18) . . . . ?
C26 C21 C22 C23 2.3(16) . . . . ?
C26 C25 C24 C23 -0.7(16) . . . . ?
C42 C41 C46 C45 0.8(17) . . . . ?
C42 C43 C44 C45 3.0(17) . . . . ?
C11 C10 C9 C8 0.9(16) . . . . ?
C11 C12 C7 P3 -172.9(8) . . . . ?
C11 C12 C7 C8 1.5(15) . . . . ?
B15 C14 B14 C13 -39.9(7) . . . . ?
B15 C14 B14 B13 -140.7(8) . . . . ?
B15 C14 B14 B20 -101.5(9) . . . . ?
B15 C14 B13 B14 38.5(8) . . . . ?
B15 C14 B13 B12 -63.9(10) . . . . ?
B15 C14 B13 B20 -0.2(11) . . . . ?
B15 C14 B13 B19 -103.4(9) . . . . ?
B15 C14 B17 B16 39.8(7) . . . . ?
B15 C14 B17 B18 101.6(8) . . . . ?
B15 C14 B17 B19 142.1(8) . . . . ?
B15 C14 B19 B12 67.9(10) . . . . ?
B15 C14 B19 B13 106.8(8) . . . . ?
B15 C14 B19 B17 -35.7(7) . . . . ?
B15 C14 B19 B18 5.7(10) . . . . ?
B15 C13 B14 C14 39.9(7) . . . . ?
B15 C13 B14 B13 100.7(8) . . . . ?
B15 C13 B14 B20 141.7(8) . . . . ?
B15 C13 B16 B17 -39.0(7) . . . . ?
B15 C13 B16 B18 -101.4(8) . . . . ?
B15 C13 B16 B11 -141.6(8) . . . . ?
B15 C13 B20 B14 -37.3(8) . . . . ?
B15 C13 B20 B12 64.1(10) . . . . ?
B15 C13 B20 B13 2.8(10) . . . . ?
B15 C13 B20 B11 103.8(9) . . . . ?
B15 C13 B11 B12 -66.2(10) . . . . ?
B15 C13 B11 B16 36.4(8) . . . . ?
B15 C13 B11 B20 -106.3(8) . . . . ?
B15 C13 B11 B18 -4.1(11) . . . . ?
B15 B14 B13 C14 -34.4(7) . . . . ?
B15 B14 B13 B12 63.8(10) . . . . ?
B15 B14 B13 B20 101.5(8) . . . . ?
B15 B14 B13 B19 -0.2(10) . . . . ?
B15 B14 B20 C13 33.7(7) . . . . ?
B15 B14 B20 B12 -63.4(10) . . . . ?
B15 B14 B20 B13 -99.9(8) . . . . ?
B15 B14 B20 B11 -0.6(10) . . . . ?
B15 B16 B17 C14 -38.5(7) . . . . ?
B15 B16 B17 B18 -136.4(8) . . . . ?
B15 B16 B17 B19 -100.0(9) . . . . ?
B15 B16 B18 B12 -62.5(10) . . . . ?
B15 B16 B18 B17 38.6(7) . . . . ?
B15 B16 B18 B11 -99.8(8) . . . . ?
B15 B16 B18 B19 1.9(10) . . . . ?
B15 B16 B11 C13 -33.3(7) . . . . ?
B15 B16 B11 B12 63.8(9) . . . . ?
B15 B16 B11 B20 -0.1(10) . . . . ?
B15 B16 B11 B18 100.3(8) . . . . ?
B15 B17 B18 B12 63.2(10) . . . . ?
B15 B17 B18 B16 -38.8(8) . . . . ?
B15 B17 B18 B11 -1.2(11) . . . . ?
B15 B17 B18 B19 100.3(9) . . . . ?
B15 B17 B19 C14 32.9(7) . . . . ?
B15 B17 B19 B12 -63.3(10) . . . . ?
B15 B17 B19 B13 0.0(10) . . . . ?
B15 B17 B19 B18 -100.1(8) . . . . ?
C4 C5 C6 C1 0.5(17) . . . . ?
C7 P3 C13 B15 85.3(7) . . . . ?
C7 P3 C13 B14 14.3(8) . . . . ?
C7 P3 C13 B16 153.4(7) . . . . ?
C7 P3 C13 B20 -60.0(9) . . . . ?
C7 P3 C13 B11 -136.7(8) . . . . ?
C7 P3 C2 C3 -113.0(9) . . . . ?
C7 P3 C2 C1 66.5(10) . . . . ?
C7 C12 C11 C10 -1.4(16) . . . . ?
C38 C33 C34 C35 2.6(17) . . . . ?
C2 P3 C13 B15 -158.4(7) . . . . ?
C2 P3 C13 B14 130.6(7) . . . . ?
C2 P3 C13 B16 -90.3(7) . . . . ?
C2 P3 C13 B20 56.3(9) . . . . ?
C2 P3 C13 B11 -20.4(9) . . . . ?
C2 P3 C7 C8 141.4(9) . . . . ?
C2 P3 C7 C12 -44.2(10) . . . . ?
C2 C1 C6 C5 -0.2(17) . . . . ?
C32 C31 C30 C29 -5.4(17) . . . . ?
C5 C4 C3 C2 -2.1(18) . . . . ?
C46 C41 C42 C43 3.3(17) . . . . ?
C37 C36 C35 C34 1.2(18) . . . . ?
C3 C4 C5 C6 0.6(18) . . . . ?
C3 C2 C1 C6 -1.2(16) . . . . ?
C30 C31 C32 C27 4.1(17) . . . . ?
C29 C28 C27 P1 168.8(9) . . . . ?
C29 C28 C27 C32 -1.6(17) . . . . ?
C1 C2 C3 C4 2.4(17) . . . . ?
C44 C43 C42 C41 -5.1(17) . . . . ?
B2 C39 B4 C40 -3.6(9) . . . . ?
B2 C39 B4 B5 -105.8(8) . . . . ?
B2 C39 B4 B3 36.6(7) . . . . ?
B2 C39 B4 B8 -64.8(9) . . . . ?
B2 C39 B5 B4 104.1(8) . . . . ?
B2 C39 B5 B6 -37.4(8) . . . . ?
B2 C39 B5 B8 64.4(9) . . . . ?
B2 C39 B5 B7 1.5(10) . . . . ?
B2 C39 B3 B4 -141.3(8) . . . . ?
B2 C39 B3 C40 -100.4(8) . . . . ?
B2 C39 B3 B10 -39.3(7) . . . . ?
B2 C39 B6 B5 141.5(8) . . . . ?
B2 C39 B6 B1 38.8(7) . . . . ?
B2 C39 B6 B7 102.6(9) . . . . ?
B2 B3 B10 C40 -135.4(8) . . . . ?
B2 B3 B10 B1 -38.4(8) . . . . ?
B2 B3 B10 B9 -101.2(9) . . . . ?
B2 B6 B1 B10 36.9(7) . . . . ?
B2 B6 B1 B9 100.8(8) . . . . ?
B2 B6 B1 B7 138.5(8) . . . . ?
B2 B6 B7 B5 101.0(8) . . . . ?
B2 B6 B7 B1 -37.1(7) . . . . ?
B2 B6 B7 B8 62.3(10) . . . . ?
B2 B6 B7 B9 0.0(10) . . . . ?
B2 B1 B10 C40 98.5(8) . . . . ?
B2 B1 B10 B3 37.9(7) . . . . ?
B2 B1 B10 B9 137.7(9) . . . . ?
B2 B1 B9 C40 1.7(11) . . . . ?
B2 B1 B9 B10 -37.3(8) . . . . ?
B2 B1 B9 B8 63.4(10) . . . . ?
B2 B1 B9 B7 101.2(9) . . . . ?
B2 B1 B7 B5 -0.2(11) . . . . ?
B2 B1 B7 B6 37.4(7) . . . . ?
B2 B1 B7 B8 -63.7(10) . . . . ?
B2 B1 B7 B9 -100.2(8) . . . . ?
B2 B10 B9 C40 -96.5(8) . . . . ?
B2 B10 B9 B1 38.1(7) . . . . ?
B2 B10 B9 B8 -64.1(10) . . . . ?
B2 B10 B9 B7 0.2(10) . . . . ?
B14 C14 B15 C13 39.8(7) . . . . ?
B14 C14 B15 B16 102.1(8) . . . . ?
B14 C14 B15 B17 142.1(8) . . . . ?
B14 C14 B13 B12 -102.4(8) . . . . ?
B14 C14 B13 B20 -38.7(7) . . . . ?
B14 C14 B13 B19 -141.9(8) . . . . ?
B14 C14 B17 B15 -37.3(8) . . . . ?
B14 C14 B17 B16 2.5(10) . . . . ?
B14 C14 B17 B18 64.3(9) . . . . ?
B14 C14 B17 B19 104.9(9) . . . . ?
B14 C14 B19 B12 -2.0(11) . . . . ?
B14 C14 B19 B13 36.8(8) . . . . ?
B14 C14 B19 B17 -105.7(9) . . . . ?
B14 C14 B19 B18 -64.3(10) . . . . ?
B14 C13 B15 C14 -39.5(7) . . . . ?
B14 C13 B15 B16 -141.6(8) . . . . ?
B14 C13 B15 B17 -102.0(8) . . . . ?
B14 C13 B16 B15 37.4(8) . . . . ?
B14 C13 B16 B17 -1.6(10) . . . . ?
B14 C13 B16 B18 -64.0(9) . . . . ?
B14 C13 B16 B11 -104.2(9) . . . . ?
B14 C13 B20 B12 101.4(8) . . . . ?
B14 C13 B20 B13 40.0(7) . . . . ?
B14 C13 B20 B11 141.1(8) . . . . ?
B14 C13 B11 B12 3.1(10) . . . . ?
B14 C13 B11 B16 105.7(8) . . . . ?
B14 C13 B11 B20 -37.0(7) . . . . ?
B14 C13 B11 B18 65.1(10) . . . . ?
B14 B15 B16 C13 -34.0(7) . . . . ?
B14 B15 B16 B17 101.1(8) . . . . ?
B14 B15 B16 B18 62.4(9) . . . . ?
B14 B15 B16 B11 -0.3(10) . . . . ?
B14 B15 B17 C14 33.3(7) . . . . ?
B14 B15 B17 B16 -101.2(8) . . . . ?
B14 B15 B17 B18 -62.7(10) . . . . ?
B14 B15 B17 B19 -0.1(10) . . . . ?
B14 B13 B20 C13 -39.6(7) . . . . ?
B14 B13 B20 B12 -138.5(9) . . . . ?
B14 B13 B20 B11 -100.9(8) . . . . ?
B14 B13 B19 C14 -33.8(7) . . . . ?
B14 B13 B19 B12 101.5(9) . . . . ?
B14 B13 B19 B17 0.1(10) . . . . ?
B14 B13 B19 B18 64.1(10) . . . . ?
B14 B20 B11 C13 34.2(7) . . . . ?
B14 B20 B11 B12 -100.0(8) . . . . ?
B14 B20 B11 B16 0.4(10) . . . . ?
B14 B20 B11 B18 -63.1(9) . . . . ?
B5 C39 B4 C40 102.2(7) . . . . ?
B5 C39 B4 B3 142.4(8) . . . . ?
B5 C39 B4 B8 41.0(7) . . . . ?
B5 C39 B2 B3 -104.7(8) . . . . ?
B5 C39 B2 B6 37.2(8) . . . . ?
B5 C39 B2 B1 -1.6(10) . . . . ?
B5 C39 B2 B10 -64.4(9) . . . . ?
B5 C39 B3 B4 -35.7(7) . . . . ?
B5 C39 B3 C40 5.3(9) . . . . ?
B5 C39 B3 B2 105.6(8) . . . . ?
B5 C39 B3 B10 66.4(9) . . . . ?
B5 C39 B6 B2 -141.5(8) . . . . ?
B5 C39 B6 B1 -102.7(8) . . . . ?
B5 C39 B6 B7 -38.9(8) . . . . ?
B5 B4 C40 P2 -147.5(6) . . . . ?
B5 B4 C40 B3 102.0(8) . . . . ?
B5 B4 C40 B10 64.5(9) . . . . ?
B5 B4 C40 B8 -41.3(7) . . . . ?
B5 B4 C40 B9 -4.4(10) . . . . ?
B5 B4 B3 C39 33.8(7) . . . . ?
B5 B4 B3 C40 -98.0(8) . . . . ?
B5 B4 B3 B2 -1.0(10) . . . . ?
B5 B4 B3 B10 -63.8(10) . . . . ?
B5 B4 B8 C40 133.9(8) . . . . ?
B5 B4 B8 B9 99.5(9) . . . . ?
B5 B4 B8 B7 36.3(8) . . . . ?
B5 B6 B1 B2 -101.0(8) . . . . ?
B5 B6 B1 B10 -64.0(10) . . . . ?
B5 B6 B1 B9 -0.2(10) . . . . ?
B5 B6 B1 B7 37.5(7) . . . . ?
B5 B6 B7 B1 -138.1(8) . . . . ?
B5 B6 B7 B8 -38.7(8) . . . . ?
B5 B6 B7 B9 -101.0(8) . . . . ?
B5 B8 B9 C40 96.5(8) . . . . ?
B5 B8 B9 B1 0.7(10) . . . . ?
B5 B8 B9 B10 64.3(9) . . . . ?
B5 B8 B9 B7 -37.2(7) . . . . ?
B5 B8 B7 B6 38.6(8) . . . . ?
B5 B8 B7 B1 101.3(8) . . . . ?
B5 B8 B7 B9 137.6(8) . . . . ?
B3 C39 B4 C40 -40.1(6) . . . . ?
B3 C39 B4 B5 -142.4(8) . . . . ?
B3 C39 B4 B8 -101.3(8) . . . . ?
B3 C39 B2 B6 141.9(8) . . . . ?
B3 C39 B2 B1 103.1(8) . . . . ?
B3 C39 B2 B10 40.3(7) . . . . ?
B3 C39 B5 B4 36.4(7) . . . . ?
B3 C39 B5 B6 -105.0(8) . . . . ?
B3 C39 B5 B8 -3.3(10) . . . . ?
B3 C39 B5 B7 -66.2(9) . . . . ?
B3 C39 B6 B2 -36.1(7) . . . . ?
B3 C39 B6 B5 105.4(8) . . . . ?
B3 C39 B6 B1 2.7(10) . . . . ?
B3 C39 B6 B7 66.5(10) . . . . ?
B3 B4 C40 P2 110.6(7) . . . . ?
B3 B4 C40 B10 -37.5(7) . . . . ?
B3 B4 C40 B8 -143.2(8) . . . . ?
B3 B4 C40 B9 -106.4(8) . . . . ?
B3 B4 B5 C39 -33.2(7) . . . . ?
B3 B4 B5 B6 0.5(10) . . . . ?
B3 B4 B5 B8 101.1(8) . . . . ?
B3 B4 B5 B7 63.8(9) . . . . ?
B3 B4 B8 C40 32.3(7) . . . . ?
B3 B4 B8 B5 -101.7(8) . . . . ?
B3 B4 B8 B9 -2.2(10) . . . . ?
B3 B4 B8 B7 -65.4(10) . . . . ?
B3 C40 B10 B2 -38.7(7) . . . . ?
B3 C40 B10 B1 -101.7(9) . . . . ?
B3 C40 B10 B9 -141.2(9) . . . . ?
B3 C40 B8 B4 -35.9(7) . . . . ?
B3 C40 B8 B5 3.6(10) . . . . ?
B3 C40 B8 B9 105.2(9) . . . . ?
B3 C40 B8 B7 64.9(10) . . . . ?
B3 C40 B9 B1 -1.9(11) . . . . ?
B3 C40 B9 B10 37.6(8) . . . . ?
B3 C40 B9 B8 -106.1(9) . . . . ?
B3 C40 B9 B7 -65.4(10) . . . . ?
B3 B2 B6 C39 33.5(7) . . . . ?
B3 B2 B6 B5 -0.9(10) . . . . ?
B3 B2 B6 B1 -102.1(9) . . . . ?
B3 B2 B6 B7 -64.4(9) . . . . ?
B3 B2 B1 B6 99.3(9) . . . . ?
B3 B2 B1 B10 -38.9(8) . . . . ?
B3 B2 B1 B9 -1.0(11) . . . . ?
B3 B2 B1 B7 62.4(10) . . . . ?
B3 B2 B10 C40 38.0(7) . . . . ?
B3 B2 B10 B1 137.3(9) . . . . ?
B3 B2 B10 B9 99.6(8) . . . . ?
B3 B10 B9 C40 -33.7(7) . . . . ?
B3 B10 B9 B1 100.8(9) . . . . ?
B3 B10 B9 B8 -1.4(10) . . . . ?
B3 B10 B9 B7 63.0(9) . . . . ?
B6 C39 B4 C40 65.4(9) . . . . ?
B6 C39 B4 B5 -36.9(8) . . . . ?
B6 C39 B4 B3 105.5(8) . . . . ?
B6 C39 B4 B8 4.2(10) . . . . ?
B6 C39 B2 B3 -141.9(8) . . . . ?
B6 C39 B2 B1 -38.8(7) . . . . ?
B6 C39 B2 B10 -101.6(8) . . . . ?
B6 C39 B5 B4 141.4(8) . . . . ?
B6 C39 B5 B8 101.8(8) . . . . ?
B6 C39 B5 B7 38.8(7) . . . . ?
B6 C39 B3 B4 -104.6(8) . . . . ?
B6 C39 B3 C40 -63.6(9) . . . . ?
B6 C39 B3 B2 36.7(8) . . . . ?
B6 C39 B3 B10 -2.5(10) . . . . ?
B6 B2 B3 C39 -33.1(7) . . . . ?
B6 B2 B3 B4 1.2(10) . . . . ?
B6 B2 B3 C40 63.1(10) . . . . ?
B6 B2 B3 B10 101.7(9) . . . . ?
B6 B2 B1 B10 -138.2(8) . . . . ?
B6 B2 B1 B9 -100.2(9) . . . . ?
B6 B2 B1 B7 -36.8(7) . . . . ?
B6 B2 B10 C40 -61.9(9) . . . . ?
B6 B2 B10 B3 -99.9(8) . . . . ?
B6 B2 B10 B1 37.4(8) . . . . ?
B6 B2 B10 B9 -0.2(10) . . . . ?
B6 B5 B8 B4 100.2(8) . . . . ?
B6 B5 B8 C40 60.6(9) . . . . ?
B6 B5 B8 B9 -0.8(10) . . . . ?
B6 B5 B8 B7 -38.5(7) . . . . ?
B6 B5 B7 B1 37.2(8) . . . . ?
B6 B5 B7 B8 136.8(8) . . . . ?
B6 B5 B7 B9 99.3(9) . . . . ?
B6 B1 B10 C40 60.9(10) . . . . ?
B6 B1 B10 B2 -37.6(8) . . . . ?
B6 B1 B10 B3 0.3(10) . . . . ?
B6 B1 B10 B9 100.1(9) . . . . ?
B6 B1 B9 C40 -62.1(10) . . . . ?
B6 B1 B9 B10 -101.0(9) . . . . ?
B6 B1 B9 B8 -0.3(10) . . . . ?
B6 B1 B9 B7 37.4(7) . . . . ?
B6 B1 B7 B5 -37.5(7) . . . . ?
B6 B1 B7 B8 -101.0(8) . . . . ?
B6 B1 B7 B9 -137.6(8) . . . . ?
B12 B13 B20 C13 98.9(9) . . . . ?
B12 B13 B20 B14 138.5(9) . . . . ?
B12 B13 B20 B11 37.6(8) . . . . ?
B12 B13 B19 C14 -135.3(8) . . . . ?
B12 B13 B19 B17 -101.4(9) . . . . ?
B12 B13 B19 B18 -37.4(8) . . . . ?
B12 B20 B11 C13 134.3(8) . . . . ?
B12 B20 B11 B16 100.5(9) . . . . ?
B12 B20 B11 B18 36.9(8) . . . . ?
B12 B18 B11 C13 -98.5(9) . . . . ?
B12 B18 B11 B16 -139.1(9) . . . . ?
B12 B18 B11 B20 -37.2(7) . . . . ?
B12 B18 B19 C14 97.8(8) . . . . ?
B12 B18 B19 B13 37.2(7) . . . . ?
B12 B18 B19 B17 139.1(8) . . . . ?
B1 B2 B3 C39 -96.4(9) . . . . ?
B1 B2 B3 B4 -62.1(10) . . . . ?
B1 B2 B3 C40 -0.2(11) . . . . ?
B1 B2 B3 B10 38.5(8) . . . . ?
B1 B2 B6 C39 135.6(8) . . . . ?
B1 B2 B6 B5 101.2(8) . . . . ?
B1 B2 B6 B7 37.7(7) . . . . ?
B1 B2 B10 C40 -99.3(8) . . . . ?
B1 B2 B10 B3 -137.3(9) . . . . ?
B1 B2 B10 B9 -37.7(7) . . . . ?
B1 B6 B7 B5 138.1(8) . . . . ?
B1 B6 B7 B8 99.4(9) . . . . ?
B1 B6 B7 B9 37.0(7) . . . . ?
B1 B10 B9 C40 -134.5(9) . . . . ?
B1 B10 B9 B8 -102.2(9) . . . . ?
B1 B10 B9 B7 -37.8(8) . . . . ?
B1 B9 B7 B5 -100.6(8) . . . . ?
B1 B9 B7 B6 -37.3(7) . . . . ?
B1 B9 B7 B8 -138.5(8) . . . . ?
B16 C13 B15 C14 102.0(8) . . . . ?
B16 C13 B15 B14 141.6(8) . . . . ?
B16 C13 B15 B17 39.5(7) . . . . ?
B16 C13 B14 C14 3.1(10) . . . . ?
B16 C13 B14 B15 -36.9(7) . . . . ?
B16 C13 B14 B13 63.9(9) . . . . ?
B16 C13 B14 B20 104.8(8) . . . . ?
B16 C13 B20 B14 -105.6(8) . . . . ?
B16 C13 B20 B12 -4.2(10) . . . . ?
B16 C13 B20 B13 -65.6(9) . . . . ?
B16 C13 B20 B11 35.5(7) . . . . ?
B16 C13 B11 B12 -102.6(8) . . . . ?
B16 C13 B11 B20 -142.6(8) . . . . ?
B16 C13 B11 B18 -40.5(7) . . . . ?
B16 B15 B14 C14 -97.9(8) . . . . ?
B16 B15 B14 C13 34.8(7) . . . . ?
B16 B15 B14 B13 -63.4(9) . . . . ?
B16 B15 B14 B20 0.6(10) . . . . ?
B16 B15 B17 C14 134.5(8) . . . . ?
B16 B15 B17 B18 38.5(8) . . . . ?
B16 B15 B17 B19 101.1(8) . . . . ?
B16 B17 B18 B12 102.1(8) . . . . ?
B16 B17 B18 B11 37.6(8) . . . . ?
B16 B17 B18 B19 139.1(8) . . . . ?
B16 B17 B19 C14 96.5(8) . . . . ?
B16 B17 B19 B12 0.3(11) . . . . ?
B16 B17 B19 B13 63.6(10) . . . . ?
B16 B17 B19 B18 -36.4(7) . . . . ?
B16 B18 B11 C13 40.6(7) . . . . ?
B16 B18 B11 B12 139.1(9) . . . . ?
B16 B18 B11 B20 101.9(8) . . . . ?
B16 B18 B19 C14 -4.5(10) . . . . ?
B16 B18 B19 B12 -102.3(8) . . . . ?
B16 B18 B19 B13 -65.1(9) . . . . ?
B16 B18 B19 B17 36.8(7) . . . . ?
B13 C14 B15 C13 1.8(10) . . . . ?
B13 C14 B15 B14 -38.0(8) . . . . ?
B13 C14 B15 B16 64.1(10) . . . . ?
B13 C14 B15 B17 104.1(9) . . . . ?
B13 C14 B14 C13 100.8(8) . . . . ?
B13 C14 B14 B15 140.7(8) . . . . ?
B13 C14 B14 B20 39.3(8) . . . . ?
B13 C14 B17 B15 -106.2(8) . . . . ?
B13 C14 B17 B16 -66.4(9) . . . . ?
B13 C14 B17 B18 -4.6(10) . . . . ?
B13 C14 B17 B19 35.9(7) . . . . ?
B13 C14 B19 B12 -38.8(8) . . . . ?
B13 C14 B19 B17 -142.5(8) . . . . ?
B13 C14 B19 B18 -101.0(8) . . . . ?
B13 B14 B20 C13 133.6(8) . . . . ?
B13 B14 B20 B12 36.5(8) . . . . ?
B13 B14 B20 B11 99.3(8) . . . . ?
B13 B12 B20 C13 -97.9(8) . . . . ?
B13 B12 B20 B14 -36.7(8) . . . . ?
B13 B12 B20 B11 -137.3(8) . . . . ?
B13 B12 B18 B16 63.2(10) . . . . ?
B13 B12 B18 B17 -0.8(10) . . . . ?
B13 B12 B18 B11 100.3(8) . . . . ?
B13 B12 B18 B19 -37.6(7) . . . . ?
B13 B12 B11 C13 -1.2(11) . . . . ?
B13 B12 B11 B16 -64.1(10) . . . . ?
B13 B12 B11 B20 38.0(7) . . . . ?
B13 B12 B11 B18 -100.6(9) . . . . ?
B13 B12 B19 C14 37.9(7) . . . . ?
B13 B12 B19 B17 100.9(9) . . . . ?
B13 B12 B19 B18 138.0(8) . . . . ?
B13 B20 B11 C13 96.8(8) . . . . ?
B13 B20 B11 B12 -37.5(7) . . . . ?
B13 B20 B11 B16 63.0(9) . . . . ?
B13 B20 B11 B18 -0.6(10) . . . . ?
B10 C40 B3 C39 100.8(8) . . . . ?
B10 C40 B3 B4 141.6(8) . . . . ?
B10 C40 B3 B2 38.7(7) . . . . ?
B10 C40 B8 B4 -105.9(9) . . . . ?
B10 C40 B8 B5 -66.4(9) . . . . ?
B10 C40 B8 B9 35.2(8) . . . . ?
B10 C40 B8 B7 -5.1(11) . . . . ?
B10 C40 B9 B1 -39.5(8) . . . . ?
B10 C40 B9 B8 -143.7(8) . . . . ?
B10 C40 B9 B7 -102.9(8) . . . . ?
B10 B2 B3 C39 -134.9(8) . . . . ?
B10 B2 B3 B4 -100.5(8) . . . . ?
B10 B2 B3 C40 -38.7(7) . . . . ?
B10 B2 B6 C39 98.0(8) . . . . ?
B10 B2 B6 B5 63.6(9) . . . . ?
B10 B2 B6 B1 -37.6(7) . . . . ?
B10 B2 B6 B7 0.2(10) . . . . ?
B10 B2 B1 B6 138.2(8) . . . . ?
B10 B2 B1 B9 37.9(8) . . . . ?
B10 B2 B1 B7 101.3(9) . . . . ?
B10 B1 B9 C40 38.9(8) . . . . ?
B10 B1 B9 B8 100.7(9) . . . . ?
B10 B1 B9 B7 138.4(8) . . . . ?
B10 B1 B7 B5 62.4(10) . . . . ?
B10 B1 B7 B6 100.0(9) . . . . ?
B10 B1 B7 B8 -1.1(11) . . . . ?
B10 B1 B7 B9 -37.6(7) . . . . ?
B10 B9 B7 B5 -63.4(9) . . . . ?
B10 B9 B7 B6 -0.1(10) . . . . ?
B10 B9 B7 B1 37.2(7) . . . . ?
B10 B9 B7 B8 -101.3(8) . . . . ?
B8 B4 C40 P2 -106.2(7) . . . . ?
B8 B4 C40 B3 143.2(8) . . . . ?
B8 B4 C40 B10 105.7(9) . . . . ?
B8 B4 C40 B9 36.9(7) . . . . ?
B8 B4 B5 C39 -134.3(8) . . . . ?
B8 B4 B5 B6 -100.6(8) . . . . ?
B8 B4 B5 B7 -37.3(7) . . . . ?
B8 B4 B3 C39 99.0(8) . . . . ?
B8 B4 B3 C40 -32.8(7) . . . . ?
B8 B4 B3 B2 64.1(10) . . . . ?
B8 B4 B3 B10 1.3(10) . . . . ?
B8 C40 B3 C39 -5.4(10) . . . . ?
B8 C40 B3 B4 35.4(7) . . . . ?
B8 C40 B3 B2 -67.5(10) . . . . ?
B8 C40 B3 B10 -106.2(9) . . . . ?
B8 C40 B10 B2 67.4(10) . . . . ?
B8 C40 B10 B3 106.1(9) . . . . ?
B8 C40 B10 B1 4.5(11) . . . . ?
B8 C40 B10 B9 -35.1(8) . . . . ?
B8 C40 B9 B1 104.2(9) . . . . ?
B8 C40 B9 B10 143.7(8) . . . . ?
B8 C40 B9 B7 40.7(7) . . . . ?
B8 B5 B6 C39 -96.9(8) . . . . ?
B8 B5 B6 B2 -62.5(9) . . . . ?
B8 B5 B6 B1 0.6(10) . . . . ?
B8 B5 B6 B7 38.7(7) . . . . ?
B8 B5 B7 B6 -136.8(8) . . . . ?
B8 B5 B7 B1 -99.5(9) . . . . ?
B8 B5 B7 B9 -37.4(7) . . . . ?
B8 B9 B7 B5 37.9(7) . . . . ?
B8 B9 B7 B6 101.2(8) . . . . ?
B8 B9 B7 B1 138.5(8) . . . . ?
B17 C14 B15 C13 -102.3(8) . . . . ?
B17 C14 B15 B14 -142.1(8) . . . . ?
B17 C14 B15 B16 -40.0(7) . . . . ?
B17 C14 B14 C13 -3.4(10) . . . . ?
B17 C14 B14 B15 36.5(8) . . . . ?
B17 C14 B14 B13 -104.2(9) . . . . ?
B17 C14 B14 B20 -65.0(10) . . . . ?
B17 C14 B13 B14 106.6(8) . . . . ?
B17 C14 B13 B12 4.2(10) . . . . ?
B17 C14 B13 B20 67.9(9) . . . . ?
B17 C14 B13 B19 -35.3(7) . . . . ?
B17 C14 B19 B12 103.7(8) . . . . ?
B17 C14 B19 B13 142.5(8) . . . . ?
B17 C14 B19 B18 41.4(7) . . . . ?
B17 B15 B14 C14 -34.4(7) . . . . ?
B17 B15 B14 C13 98.3(8) . . . . ?
B17 B15 B14 B13 0.1(10) . . . . ?
B17 B15 B14 B20 64.1(9) . . . . ?
B17 B15 B16 C13 -135.1(8) . . . . ?
B17 B15 B16 B18 -38.8(7) . . . . ?
B17 B15 B16 B11 -101.4(8) . . . . ?
B17 B16 B18 B12 -101.0(9) . . . . ?
B17 B16 B18 B11 -138.3(9) . . . . ?
B17 B16 B18 B19 -36.7(7) . . . . ?
B17 B16 B11 C13 -96.3(8) . . . . ?
B17 B16 B11 B12 0.9(11) . . . . ?
B17 B16 B11 B20 -63.1(10) . . . . ?
B17 B16 B11 B18 37.4(8) . . . . ?
B17 B18 B11 C13 3.2(11) . . . . ?
B17 B18 B11 B12 101.7(9) . . . . ?
B17 B18 B11 B16 -37.4(8) . . . . ?
B17 B18 B11 B20 64.5(10) . . . . ?
B17 B18 B19 C14 -41.3(7) . . . . ?
B17 B18 B19 B12 -139.1(8) . . . . ?
B17 B18 B19 B13 -101.9(8) . . . . ?
B9 C40 B3 C39 63.4(9) . . . . ?
B9 C40 B3 B4 104.2(9) . . . . ?
B9 C40 B3 B2 1.3(11) . . . . ?
B9 C40 B3 B10 -37.4(8) . . . . ?
B9 C40 B10 B2 102.5(8) . . . . ?
B9 C40 B10 B3 141.2(9) . . . . ?
B9 C40 B10 B1 39.6(7) . . . . ?
B9 C40 B8 B4 -141.1(8) . . . . ?
B9 C40 B8 B5 -101.6(8) . . . . ?
B9 C40 B8 B7 -40.4(7) . . . . ?
B9 B1 B10 C40 -39.2(7) . . . . ?
B9 B1 B10 B2 -137.7(9) . . . . ?
B9 B1 B10 B3 -99.8(8) . . . . ?
B9 B1 B7 B5 100.0(8) . . . . ?
B9 B1 B7 B6 137.6(8) . . . . ?
B9 B1 B7 B8 36.5(7) . . . . ?
B9 B8 B7 B5 -137.6(8) . . . . ?
B9 B8 B7 B6 -99.0(9) . . . . ?
B9 B8 B7 B1 -36.3(7) . . . . ?
B20 C13 B15 C14 -2.8(10) . . . . ?
B20 C13 B15 B14 36.7(8) . . . . ?
B20 C13 B15 B16 -104.9(9) . . . . ?
B20 C13 B15 B17 -65.3(10) . . . . ?
B20 C13 B14 C14 -101.7(8) . . . . ?
B20 C13 B14 B15 -141.7(8) . . . . ?
B20 C13 B14 B13 -40.9(7) . . . . ?
B20 C13 B16 B15 105.6(8) . . . . ?
B20 C13 B16 B17 66.6(9) . . . . ?
B20 C13 B16 B18 4.2(10) . . . . ?
B20 C13 B16 B11 -35.9(8) . . . . ?
B20 C13 B11 B12 40.1(8) . . . . ?
B20 C13 B11 B16 142.6(8) . . . . ?
B20 C13 B11 B18 102.1(9) . . . . ?
B20 B14 B13 C14 -135.8(8) . . . . ?
B20 B14 B13 B12 -37.7(8) . . . . ?
B20 B14 B13 B19 -101.6(9) . . . . ?
B20 B12 B13 C14 99.0(8) . . . . ?
B20 B12 B13 B14 37.2(8) . . . . ?
B20 B12 B13 B19 138.3(8) . . . . ?
B20 B12 B18 B16 -0.1(11) . . . . ?
B20 B12 B18 B17 -64.0(10) . . . . ?
B20 B12 B18 B11 37.1(7) . . . . ?
B20 B12 B18 B19 -100.8(8) . . . . ?
B20 B12 B11 C13 -39.2(7) . . . . ?
B20 B12 B11 B16 -102.0(8) . . . . ?
B20 B12 B11 B18 -138.6(8) . . . . ?
B20 B12 B19 C14 0.7(11) . . . . ?
B20 B12 B19 B13 -37.2(8) . . . . ?
B20 B12 B19 B17 63.7(11) . . . . ?
B20 B12 B19 B18 100.7(9) . . . . ?
B20 B13 B19 C14 -97.3(8) . . . . ?
B20 B13 B19 B12 37.9(8) . . . . ?
B20 B13 B19 B17 -63.5(10) . . . . ?
B20 B13 B19 B18 0.6(10) . . . . ?
B18 B12 B13 C14 -2.0(10) . . . . ?
B18 B12 B13 B14 -63.8(9) . . . . ?
B18 B12 B13 B20 -101.0(8) . . . . ?
B18 B12 B13 B19 37.3(7) . . . . ?
B18 B12 B20 C13 2.5(10) . . . . ?
B18 B12 B20 B14 63.7(10) . . . . ?
B18 B12 B20 B13 100.4(9) . . . . ?
B18 B12 B20 B11 -36.9(7) . . . . ?
B18 B12 B11 C13 99.4(8) . . . . ?
B18 B12 B11 B16 36.6(8) . . . . ?
B18 B12 B11 B20 138.6(8) . . . . ?
B18 B12 B19 C14 -100.0(8) . . . . ?
B18 B12 B19 B13 -138.0(8) . . . . ?
B18 B12 B19 B17 -37.0(8) . . . . ?
B18 B16 B17 C14 97.9(8) . . . . ?
B18 B16 B17 B15 136.4(8) . . . . ?
B18 B16 B17 B19 36.4(8) . . . . ?
B18 B16 B11 C13 -133.6(8) . . . . ?
B18 B16 B11 B12 -36.5(8) . . . . ?
B18 B16 B11 B20 -100.4(9) . . . . ?
B18 B17 B19 C14 133.0(8) . . . . ?
B18 B17 B19 B12 36.7(8) . . . . ?
B18 B17 B19 B13 100.0(8) . . . . ?
B7 B5 B6 C39 -135.6(8) . . . . ?
B7 B5 B6 B2 -101.3(9) . . . . ?
B7 B5 B6 B1 -38.1(8) . . . . ?
B7 B5 B8 B4 138.6(8) . . . . ?
B7 B5 B8 C40 99.1(8) . . . . ?
B7 B5 B8 B9 37.6(7) . . . . ?
B7 B6 B1 B2 -138.5(8) . . . . ?
B7 B6 B1 B10 -101.6(9) . . . . ?
B7 B6 B1 B9 -37.7(7) . . . . ?
B7 B1 B10 C40 -1.9(10) . . . . ?
B7 B1 B10 B2 -100.4(9) . . . . ?
B7 B1 B10 B3 -62.5(10) . . . . ?
B7 B1 B10 B9 37.3(8) . . . . ?
B7 B1 B9 C40 -99.5(8) . . . . ?
B7 B1 B9 B10 -138.4(8) . . . . ?
B7 B1 B9 B8 -37.8(7) . . . . ?
B7 B8 B9 C40 133.7(8) . . . . ?
B7 B8 B9 B1 38.0(8) . . . . ?
B7 B8 B9 B10 101.5(8) . . . . ?
B11 C13 B15 C14 65.9(10) . . . . ?
B11 C13 B15 B14 105.4(9) . . . . ?
B11 C13 B15 B16 -36.1(8) . . . . ?
B11 C13 B15 B17 3.4(11) . . . . ?
B11 C13 B14 C14 -64.5(9) . . . . ?
B11 C13 B14 B15 -104.4(8) . . . . ?
B11 C13 B14 B13 -3.7(10) . . . . ?
B11 C13 B14 B20 37.3(8) . . . . ?
B11 C13 B16 B15 141.6(8) . . . . ?
B11 C13 B16 B17 102.5(8) . . . . ?
B11 C13 B16 B18 40.1(7) . . . . ?
B11 C13 B20 B14 -141.1(8) . . . . ?
B11 C13 B20 B12 -39.7(7) . . . . ?
B11 C13 B20 B13 -101.0(8) . . . . ?
B11 B12 B13 C14 60.9(10) . . . . ?
B11 B12 B13 B14 -0.9(11) . . . . ?
B11 B12 B13 B20 -38.1(7) . . . . ?
B11 B12 B13 B19 100.2(9) . . . . ?
B11 B12 B20 C13 39.4(7) . . . . ?
B11 B12 B20 B14 100.6(8) . . . . ?
B11 B12 B20 B13 137.3(8) . . . . ?
B11 B12 B18 B16 -37.1(8) . . . . ?
B11 B12 B18 B17 -101.1(8) . . . . ?
B11 B12 B18 B19 -137.9(8) . . . . ?
B11 B12 B19 C14 -62.7(10) . . . . ?
B11 B12 B19 B13 -100.7(8) . . . . ?
B11 B12 B19 B17 0.3(11) . . . . ?
B11 B12 B19 B18 37.3(8) . . . . ?
B11 B16 B17 C14 60.8(9) . . . . ?
B11 B16 B17 B15 99.3(9) . . . . ?
B11 B16 B17 B18 -37.1(8) . . . . ?
B11 B16 B17 B19 -0.7(10) . . . . ?
B11 B16 B18 B12 37.3(8) . . . . ?
B11 B16 B18 B17 138.3(9) . . . . ?
B11 B16 B18 B19 101.6(9) . . . . ?
B11 B18 B19 C14 59.6(9) . . . . ?
B11 B18 B19 B12 -38.2(7) . . . . ?
B11 B18 B19 B13 -0.9(10) . . . . ?
B11 B18 B19 B17 100.9(8) . . . . ?
B19 C14 B15 C13 -66.9(9) . . . . ?
B19 C14 B15 B14 -106.7(8) . . . . ?
B19 C14 B15 B16 -4.6(10) . . . . ?
B19 C14 B15 B17 35.4(7) . . . . ?
B19 C14 B14 C13 64.1(9) . . . . ?
B19 C14 B14 B15 104.0(9) . . . . ?
B19 C14 B14 B13 -36.8(8) . . . . ?
B19 C14 B14 B20 2.5(11) . . . . ?
B19 C14 B13 B14 141.9(8) . . . . ?
B19 C14 B13 B12 39.5(7) . . . . ?
B19 C14 B13 B20 103.2(8) . . . . ?
B19 C14 B17 B15 -142.1(8) . . . . ?
B19 C14 B17 B16 -102.3(8) . . . . ?
B19 C14 B17 B18 -40.5(7) . . . . ?
B19 B12 B13 C14 -39.3(7) . . . . ?
B19 B12 B13 B14 -101.1(8) . . . . ?
B19 B12 B13 B20 -138.3(8) . . . . ?
B19 B12 B20 C13 -60.5(10) . . . . ?
B19 B12 B20 B14 0.7(11) . . . . ?
B19 B12 B20 B13 37.4(8) . . . . ?
B19 B12 B20 B11 -99.9(9) . . . . ?
B19 B12 B18 B16 100.7(9) . . . . ?
B19 B12 B18 B17 36.7(7) . . . . ?
B19 B12 B18 B11 137.9(8) . . . . ?
B19 B12 B11 C13 62.1(10) . . . . ?
B19 B12 B11 B16 -0.7(11) . . . . ?
B19 B12 B11 B20 101.3(8) . . . . ?
B19 B12 B11 B18 -37.3(8) . . . . ?
B19 B13 B20 C13 61.3(9) . . . . ?
B19 B13 B20 B14 100.9(9) . . . . ?
B19 B13 B20 B12 -37.6(8) . . . . ?
B19 B13 B20 B11 0.0(10) . . . . ?
B19 B17 B18 B12 -37.0(7) . . . . ?
B19 B17 B18 B16 -139.1(8) . . . . ?
B19 B17 B18 B11 -101.5(9) . . . . ?
B19 B18 B11 C13 -60.4(10) . . . . ?
B19 B18 B11 B12 38.1(7) . . . . ?
B19 B18 B11 B16 -101.0(9) . . . . ?
B19 B18 B11 B20 0.9(10) . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 -0.702 0.000 0.500 1105.0 320.6 ?
2 -0.660 0.500 1.000 1105.0 320.6 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_cu_xhh_25091_0m
_database_code_depnum_ccdc_archive 'CCDC 2454645'
loop_
_audit_author_name
_audit_author_address
'Haohui Xie'
;NanJing University of Science and Technology
China
;
_audit_update_record             
;
2025-05-28 deposited with the CCDC.	2026-03-06 downloaded from the CCDC.
;
# start Validation Reply Form
_vrf_PLAT971_cu_xhh_25091_0m     
;
PROBLEM: Check Calcd Resid. Dens.  0.26Ang From Au11            4.56 eA-3
RESPONSE: The relatively large residual density is close to heavy gold atoms.
;
_vrf_PLAT972_cu_xhh_25091_0m     
;
PROBLEM: Check Calcd Resid. Dens.  0.77Ang From Au3            -6.62 eA-3
RESPONSE: The relatively large residual density is close to heavy gold atoms
;
_vrf_PLAT973_cu_xhh_25091_0m     
;
PROBLEM: Check Calcd Positive Resid. Density on       Au1       4.17 eA-3
RESPONSE: The relatively large residual density is close to heavy gold atoms
;
_vrf_PLAT342_cu_xhh_25091_0m     
;
PROBLEM: Low Bond Precision on  C-C Bonds ...............    0.03401 Ang.
RESPONSE: because of heavy gold atoms
;
_vrf_PLAT971_cu_xhh_25091_0m_2   
;
PROBLEM: Check Calcd Resid. Dens.  0.23Ang From Au15            3.50 eA-3
RESPONSE: The relatively large residual density is close to heavy gold atoms
;
# Added during the CSD deposition process: Wednesday 28 May 2025 04:03 AM
# end Validation Reply Form

_audit_creation_date             2025-05-22
_audit_creation_method           
;
Olex2 1.5
(compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         '2(C78 H90 Au9 B30 P6 S4), 2(Cl)'
_chemical_formula_sum            'C156 H180 Au18 B60 Cl2 P12 S8'
_chemical_formula_weight         6948.01
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -4.4197 7.2980 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_H-M_alt        'P -1'
_space_group_name_Hall           '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   19.8665(8)
_cell_length_b                   21.7317(9)
_cell_length_c                   27.7325(12)
_cell_angle_alpha                94.188(2)
_cell_angle_beta                 98.263(2)
_cell_angle_gamma                105.822(2)
_cell_volume                     11320.4(8)
_cell_formula_units_Z            2
_cell_measurement_reflns_used    9741
_cell_measurement_temperature    100.00
_cell_measurement_theta_max      75.156
_cell_measurement_theta_min      4.258
_shelx_estimated_absorpt_T_max   0.561
_shelx_estimated_absorpt_T_min   0.350
_exptl_absorpt_coefficient_mu    23.314
_exptl_absorpt_correction_T_max  0.7538
_exptl_absorpt_correction_T_min  0.5500
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1213 before and 0.0880 after correction.
The Ratio of minimum to maximum transmission is 0.7296.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    2.038
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             6360
_exptl_crystal_preparation       ?
_exptl_crystal_size_max          0.057
_exptl_crystal_size_mid          0.036
_exptl_crystal_size_min          0.028
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.0813
_diffrn_reflns_av_unetI/netI     0.0882
_diffrn_reflns_Laue_measured_fraction_full 0.979
_diffrn_reflns_Laue_measured_fraction_max 0.955
_diffrn_reflns_limit_h_max       24
_diffrn_reflns_limit_h_min       -24
_diffrn_reflns_limit_k_max       27
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       34
_diffrn_reflns_limit_l_min       -34
_diffrn_reflns_number            151725
_diffrn_reflns_point_group_measured_fraction_full 0.979
_diffrn_reflns_point_group_measured_fraction_max 0.955
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         75.227
_diffrn_reflns_theta_min         2.128
_diffrn_ambient_temperature      100.00
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.979
_diffrn_measured_fraction_theta_max 0.955
_diffrn_measurement_device_type  multi-scan
_diffrn_measurement_method       ?
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_source                   ?
_diffrn_source_current           1.1
_diffrn_source_power             0.05500000000000001
_diffrn_source_voltage           50.0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                32681
_reflns_number_total             44694
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.41 (?, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.41 (?, 2016)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXT 2018/2 (Sheldrick, 2018)'
_refine_diff_density_max         3.847
_refine_diff_density_min         -5.796
_refine_diff_density_rms         0.467
_refine_ls_extinction_coef       0.000030(3)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
_refine_ls_goodness_of_fit_ref   1.097
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2294
_refine_ls_number_reflns         44694
_refine_ls_number_restraints     1812
_refine_ls_R_factor_all          0.1270
_refine_ls_R_factor_gt           0.0946
_refine_ls_restrained_S_all      1.077
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1305P)²+529.6751P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2633
_refine_ls_wR_factor_ref         0.2808
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups
2. Rigid bond restraints
 All non-hydrogen atoms
 with sigma for 1-2 distances of 0.01 and sigma for 1-3 distances of 0.02
3. Uiso/Uaniso restraints and constraints
C16 \\sim C17 \\sim C18 \\sim C19 \\sim C20 \\sim C15: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
C115 \\sim C116 \\sim C117 \\sim C118 \\sim C113 \\sim C114: within 2A with
sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
C110 \\sim C111 \\sim C112 \\sim C107 \\sim C108 \\sim C109: within 2A with
sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
C70 \\sim C69 \\sim C71 \\sim C72 \\sim C67 \\sim C68: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
C55 \\sim C56 \\sim C60 \\sim C59 \\sim C58 \\sim C57: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
C61 \\sim C62 \\sim C66 \\sim C64 \\sim C65 \\sim C63: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
B35 \\sim B37 \\sim B38 \\sim B29: within 2A with sigma of 0.01 and sigma for
terminal atoms of 0.02 within 2A
B29 \\sim B30 \\sim B36 \\sim B35 \\sim B37 \\sim B38 \\sim B31 \\sim B33 \\sim
B34: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
B5 \\sim B40 \\sim B8 \\sim B6 \\sim B4 \\sim B7 \\sim B3 \\sim B9: within 2A
with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
B17 \\sim B11 \\sim B10 \\sim B18 \\sim B16: within 2A with sigma of 0.01 and
sigma for terminal atoms of 0.02 within 2A
C55 \\sim C56 \\sim C57 \\sim C58 \\sim C59 \\sim C60: within 2A with sigma of
0.001 and sigma for terminal atoms of 0.002 within 2A
C65 \\sim C66 \\sim C61 \\sim C62 \\sim C63 \\sim C64: within 2A with sigma of
0.001 and sigma for terminal atoms of 0.002 within 2A
C50 \\sim C51 \\sim C52 \\sim C47 \\sim C48 \\sim C49: within 2A with sigma of
0.001 and sigma for terminal atoms of 0.002 within 2A
C102 \\sim C101 \\sim C100 \\sim C103 \\sim C104 \\sim C99: within 2A with
sigma of 0.001 and sigma for terminal atoms of 0.002 within 2A
C124 \\sim C123 \\sim C122 \\sim C121 \\sim C120 \\sim C119: within 2A with
sigma of 0.001 and sigma for terminal atoms of 0.002 within 2A
C42 \\sim C43 \\sim C44 \\sim C45 \\sim C46 \\sim C41: within 2A with sigma of
0.001 and sigma for terminal atoms of 0.002 within 2A
B39 \\sim B48 \\sim B59 \\sim B47 \\sim B45 \\sim B44 \\sim B46 \\sim B43 \\sim
B42 \\sim B41: within 2A with sigma of 0.001 and sigma for terminal atoms of
0.002 within 2A
B60 \\sim B22 \\sim B21 \\sim B27 \\sim B20 \\sim B23 \\sim B25 \\sim B26 \\sim
B24: within 2A with sigma of 0.001 and sigma for terminal atoms of 0.002 within
2A
4.a Aromatic/amide H refined with riding coordinates:
 C94(H94), C29(H29), C48(H48), C100(H100), C104(H104), C63(H63), C142(H142),
 C153(H153), C121(H121), C118(H118), C60(H60), C95(H95), C62(H62), C72(H72),
 C120(H120), C127(H127), C16(H16), C20(H20), C19(H19), C18(H18), C17(H17),
 C143(H143), C156(H156), C122(H122), C154(H154), C148(H148), C64(H64),
 C134(H134), C82(H82), C11(H11), C145(H145), C141(H141), C26(H26A), C147(H147),
 C138(H138), C30(H30), C92(H92), C146(H146), C140(H140), C28(H28), C43(H43),
 C144(H144), C98(H98), C42(H42), C51(H51), C32(H32), C77(H77), C3(H3), C59(H59),
  C8(H8A), C34(H34), C23(H23A), C128(H128), C24(H24A), C84(H84), C37(H37),
 C85(H85), C124(H124), C2(H2), C50(H50), C44(H44), C25(H25A), C126(H126),
 C52(H52), C149(H149), C123(H123), C130(H130), C97(H97), C110(H110), C35(H35),
 C38(H38), C151(H151), C74(H74), C103(H103), C116(H116), C114(H114), C111(H111),
  C9(H9), C108(H108), C31(H31), C12(H12), C117(H117), C10(H10A), C102(H102),
 C88(H88), C112(H112), C86(H86), C45(H45), C129(H129), C109(H109), C58(H58),
 C136(H136), C96(H96), C89(H89), C137(H137), C22(H22A), C150(H150), C36(H36),
 C46(H46), C78(H78), C75(H75), C65(H65), C5(H5A), C90(H90), C135(H135),
 C83(H83), C101(H101), C56(H56), C6(H6A), C49(H49), C76(H76), C57(H57),
 C71(H71), C68(H68), C91(H91), C4(H4A), C115(H115), C70(H70), C69(H69), C66(H66)
4.b Fitted hexagon refined as free rotating group:
 C16(C15,C20,C19,C18,C17)
4.c Boron cage BH refined with riding coordinates:
 B45(H45A), B46(H46A), B13(H13), B24(H24), B8(H8), B53(H53), B25(H25),
 B50(H50A), B43(H43A), B26(H26), B56(H56A), B47(H47), B16(H16A), B51(H51A),
 B14(H14), B60(H60A), B23(H23), B17(H17A), B54(H54), B21(H21), B52(H52A),
 B41(H41), B22(H22), B59(H59A), B4(H4), B40(H40), B32(H32A), B1(H1), B18(H18A),
 B11(H11A), B10(H10), B27(H27), B19(H19A), B42(H42A), B49(H49A), B5(H5),
 B20(H20A), B44(H44A), B55(H55), B6(H6), B28(H28A), B57(H57A), B39(H39),
 B2(H2A), B3(H3A), B58(H58A), B9(H9A), B33(H33), B15(H15), B48(H48A), B7(H7),
 B34(H34A), B12(H12A), B31(H31A), B30(H30A), B36(H36A), B38(H38A), B29(H29A),
 B35(H35A), B37(H37A)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au5 Au 0.36260(4) 0.67434(3) 0.50342(2) 0.02463(16) Uani 1 1 d . U . . .
Au6 Au 0.28002(4) 0.55068(3) 0.54385(2) 0.02321(15) Uani 1 1 d . U . . .
Au8 Au 0.68197(4) 0.71374(3) 0.50499(2) 0.02513(16) Uani 1 1 d . U . . .
Au9 Au 0.76175(4) 0.62030(3) 0.54363(2) 0.02415(15) Uani 1 1 d . U . . .
Au4 Au 0.42852(4) 0.56296(3) 0.52266(2) 0.02516(16) Uani 1 1 d . U . . .
Au2 Au 0.50829(4) 0.45881(3) 0.57730(2) 0.02494(16) Uani 1 1 d . U . . .
Au13 Au 0.23947(4) 0.88083(3) 0.95457(2) 0.02463(16) Uani 1 1 d . U . . .
Au12 Au 0.40257(4) 0.91813(3) 0.97273(3) 0.02732(16) Uani 1 1 d . U . . .
Au7 Au 0.59933(4) 0.58276(3) 0.52341(2) 0.02537(16) Uani 1 1 d . U . . .
Au16 Au 0.72039(4) 0.95130(3) 0.95475(2) 0.02547(16) Uani 1 1 d . U . . .
Au1 Au 0.42901(4) 0.35806(4) 0.64491(3) 0.02771(16) Uani 1 1 d . U . . .
Au11 Au 0.49196(4) 1.04889(4) 0.92529(3) 0.02866(17) Uani 1 1 d . U . . .
Au3 Au 0.59506(4) 0.38967(4) 0.64163(3) 0.02739(16) Uani 1 1 d . U . . .
Au15 Au 0.57156(4) 0.93829(4) 0.97436(3) 0.02766(16) Uani 1 1 d . U . . .
Au18 Au 0.40390(4) 1.12095(4) 0.86553(3) 0.02843(17) Uani 1 1 d . U . . .
Au14 Au 0.31921(4) 0.78402(4) 0.98891(3) 0.02940(17) Uani 1 1 d . U . . .
Au10 Au 0.57420(4) 1.15353(4) 0.86485(3) 0.02848(17) Uani 1 1 d . U . . .
Au17 Au 0.63495(4) 0.82284(4) 0.98878(3) 0.03079(17) Uani 1 1 d . U . . .
S3 S 0.3263(2) 0.56760(19) 0.47120(14) 0.0240(7) Uani 1 1 d . U . . .
S4 S 0.6835(2) 0.61274(19) 0.47179(14) 0.0254(8) Uani 1 1 d . U . . .
S1 S 0.4935(2) 0.34929(18) 0.58344(14) 0.0223(7) Uani 1 1 d . U . . .
S8 S 0.5052(2) 1.1599(2) 0.92434(15) 0.0283(8) Uani 1 1 d . U . . .
P9 P 0.1535(2) 0.8752(2) 0.89049(15) 0.0247(8) Uani 1 1 d . U . . .
P5 P 0.2275(2) 0.5379(2) 0.61135(15) 0.0229(8) Uani 1 1 d . U . . .
S6 S 0.3200(2) 0.8840(2) 1.02444(15) 0.0270(8) Uani 1 1 d . U . . .
S7 S 0.4770(2) 0.9395(2) 0.91570(15) 0.0298(8) Uani 1 1 d . U . . .
S5 S 0.6720(2) 0.9280(2) 1.02532(15) 0.0277(8) Uani 1 1 d . U . . .
P10 P 0.3052(2) 1.0953(2) 0.80766(16) 0.0259(8) Uani 1 1 d . U . . .
S2 S 0.5253(2) 0.5683(2) 0.58132(15) 0.0267(8) Uani 1 1 d . U . . .
P4 P 0.3924(2) 0.77774(19) 0.53781(16) 0.0262(8) Uani 1 1 d . U . . .
P11 P 0.7754(2) 0.9685(2) 0.88887(15) 0.0258(8) Uani 1 1 d . U . . .
P2 P 0.8467(2) 0.6287(2) 0.60878(15) 0.0249(8) Uani 1 1 d . U . . .
P6 P 0.3589(3) 0.3645(3) 0.70214(18) 0.0330(10) Uani 1 1 d . U . . .
P1 P 0.6931(2) 0.4160(2) 0.69936(16) 0.0288(9) Uani 1 1 d . U . . .
P3 P 0.6930(2) 0.81208(19) 0.54283(15) 0.0241(8) Uani 1 1 d . U . . .
P8 P 0.3046(3) 0.6866(2) 0.94778(18) 0.0329(9) Uani 1 1 d . U . . .
P12 P 0.6453(2) 1.1519(2) 0.80851(16) 0.0288(9) Uani 1 1 d . U . . .
P7 P 0.6032(3) 0.7229(2) 0.9466(2) 0.0385(11) Uani 1 1 d . U . . .
C93 C 0.0977(9) 0.7939(9) 0.8678(7) 0.028(3) Uani 1 1 d . U . . .
C13 C 0.7394(9) 0.5024(8) 0.7070(6) 0.027(3) Uani 1 1 d . U . . .
C7 C 0.7578(11) 0.3738(9) 0.6856(8) 0.036(4) Uani 1 1 d . U . . .
C94 C 0.0366(9) 0.7826(10) 0.8317(6) 0.030(4) Uani 1 1 d . U . . .
H94 H 0.020291 0.817307 0.820796 0.037 Uiso 1 1 calc R U . . .
C119 C 0.8000(12) 0.8983(10) 0.8688(8) 0.0411(18) Uani 1 1 d . U . . .
C125 C 0.8541(10) 1.0382(9) 0.9018(6) 0.026(3) Uani 1 1 d . U . . .
C29 C 0.6562(14) 0.7475(9) 0.6721(8) 0.044(5) Uani 1 1 d . U . . .
H29 H 0.624979 0.711159 0.682305 0.052 Uiso 1 1 calc R U . . .
C48 C 0.4333(14) 0.7358(14) 0.6241(8) 0.056(2) Uani 1 1 d . U . . .
H48 H 0.443298 0.704660 0.602493 0.067 Uiso 1 1 calc R U . . .
C100 C 0.1329(11) 0.9888(10) 0.9271(7) 0.0341(16) Uani 1 1 d . U . . .
H100 H 0.182700 1.004847 0.928342 0.041 Uiso 1 1 calc R U . . .
C104 C 0.0264(10) 0.9004(10) 0.9077(7) 0.0343(16) Uani 1 1 d . U . . .
H104 H 0.002148 0.857006 0.894814 0.041 Uiso 1 1 calc R U . . .
C63 C 0.4381(11) 0.2636(12) 0.8017(8) 0.045(2) Uani 1 1 d . U . . .
H63 H 0.456958 0.227860 0.799763 0.054 Uiso 1 1 calc R U . . .
C152 C 0.2027(9) 0.6094(8) 0.6296(7) 0.026(3) Uani 1 1 d . U . . .
C142 C 0.5699(10) 1.2316(10) 0.6684(8) 0.038(4) Uani 1 1 d . U . . .
H142 H 0.553028 1.248664 0.640011 0.046 Uiso 1 1 calc R U . . .
C39 C 0.6133(11) 0.8412(9) 0.5230(7) 0.032(3) Uani 1 1 d . U . . .
B45 B 0.6087(12) 1.0165(11) 0.7442(7) 0.0334(12) Uani 1 1 d . U . . .
H45A H 0.571433 1.027631 0.714010 0.040 Uiso 1 1 calc R U . . .
C153 C 0.1568(11) 0.6111(10) 0.6627(8) 0.036(4) Uani 1 1 d . U . . .
H153 H 0.138719 0.573610 0.677808 0.043 Uiso 1 1 calc R U . . .
C53 C 0.2869(10) 0.5276(9) 0.6660(6) 0.031(3) Uani 1 1 d . U . . .
C121 C 0.8564(12) 0.8402(10) 0.8184(8) 0.0412(18) Uani 1 1 d . U . . .
H121 H 0.882365 0.838957 0.792259 0.049 Uiso 1 1 calc R U . . .
C118 C 0.3897(13) 1.1067(11) 0.7355(8) 0.042(3) Uani 1 1 d . U . . .
H118 H 0.420388 1.092316 0.758697 0.051 Uiso 1 1 calc R U . . .
C14 C 0.8132(10) 0.6009(8) 0.6650(6) 0.029(3) Uani 1 1 d . U . . .
C80 C 0.3810(12) 0.6527(10) 0.9618(9) 0.045(3) Uani 1 1 d . U . . .
B46 B 0.5872(12) 1.0065(11) 0.8056(7) 0.0333(12) Uani 1 1 d . U . . .
H46A H 0.535318 1.011183 0.814153 0.040 Uiso 1 1 calc R U . . .
B13 B 0.6849(12) 0.5546(11) 0.7011(8) 0.031(3) Uani 1 1 d . U . . .
H13 H 0.625421 0.539106 0.695420 0.038 Uiso 1 1 calc R U . . .
C131 C 0.7183(10) 0.9849(9) 0.8349(6) 0.029(3) Uani 1 1 d . U . . .
C60 C 0.2448(12) 0.2984(12) 0.6324(10) 0.050(2) Uani 1 1 d . U . . .
H60 H 0.275370 0.310109 0.609109 0.060 Uiso 1 1 calc R U . . .
C95 C 0.0011(12) 0.7198(11) 0.8128(9) 0.047(5) Uani 1 1 d . U . . .
H95 H -0.036991 0.711516 0.785999 0.057 Uiso 1 1 calc R U . . .
C155 C 0.1498(9) 0.4673(8) 0.6008(6) 0.025(3) Uani 1 1 d . U . . .
B24 B 0.3752(12) 0.5599(11) 0.6679(8) 0.0335(13) Uani 1 1 d . U . . .
H24 H 0.397538 0.589576 0.639470 0.040 Uiso 1 1 calc R U . . .
C62 C 0.4169(11) 0.2885(12) 0.7588(9) 0.044(2) Uani 1 1 d . U . . .
H62 H 0.421229 0.269765 0.727748 0.053 Uiso 1 1 calc R U . . .
C72 C 0.7326(16) 0.7148(14) 0.9898(13) 0.068(5) Uani 1 1 d . U . . .
H72 H 0.737507 0.757035 1.004553 0.081 Uiso 1 1 calc R U . . .
C120 C 0.8406(12) 0.8959(10) 0.8308(8) 0.0411(18) Uani 1 1 d . U . . .
H120 H 0.856574 0.932609 0.814290 0.049 Uiso 1 1 calc R U . . .
C1 C 0.6732(11) 0.4025(10) 0.7602(7) 0.038(4) Uani 1 1 d . U . . .
C127 C 0.9553(12) 1.1153(11) 0.8805(8) 0.047(5) Uani 1 1 d . U . . .
H127 H 0.985373 1.129327 0.857316 0.056 Uiso 1 1 calc R U . . .
C16 C 0.9735(6) 0.6038(4) 0.5900(4) 0.031(3) Uani 1 1 d G U . . .
H16 H 0.996915 0.648070 0.600449 0.037 Uiso 1 1 calc R U . . .
C15 C 0.9019(6) 0.5789(5) 0.5923(4) 0.029(3) Uani 1 1 d G U . . .
C20 C 0.8677(5) 0.5141(5) 0.5769(4) 0.033(3) Uani 1 1 d G U . . .
H20 H 0.818727 0.497049 0.578512 0.040 Uiso 1 1 calc R U . . .
C19 C 0.9050(6) 0.4743(4) 0.5593(5) 0.039(3) Uani 1 1 d G U . . .
H19 H 0.881621 0.429997 0.548825 0.047 Uiso 1 1 calc R U . . .
C18 C 0.9766(6) 0.4992(5) 0.5570(5) 0.037(3) Uani 1 1 d G U . . .
H18 H 1.002161 0.471981 0.544950 0.044 Uiso 1 1 calc R U . . .
C17 C 1.0109(5) 0.5640(6) 0.5723(5) 0.039(3) Uani 1 1 d G U . . .
H17 H 1.059810 0.581017 0.570762 0.047 Uiso 1 1 calc R U . . .
C143 C 0.6045(15) 1.1843(11) 0.6636(8) 0.050(6) Uani 1 1 d . U . . .
H143 H 0.612917 1.170733 0.632209 0.060 Uiso 1 1 calc R U . . .
B8 B 0.5768(10) 0.8208(10) 0.4639(8) 0.028(2) Uani 1 1 d . U . . .
H8 H 0.596940 0.791810 0.437347 0.033 Uiso 1 1 calc R U . . .
C156 C 0.1380(9) 0.4294(8) 0.5556(7) 0.025(3) Uani 1 1 d . U . . .
H156 H 0.167596 0.442035 0.531909 0.030 Uiso 1 1 calc R U . . .
B53 B 0.2635(11) 0.9597(10) 0.7437(7) 0.029(3) Uani 1 1 d . U . . .
H53 H 0.287875 0.978664 0.711788 0.035 Uiso 1 1 calc R U . . .
C133 C 0.7356(11) 1.2016(9) 0.8310(7) 0.034(3) Uani 1 1 d . U . . .
C73 C 0.5868(10) 0.7318(11) 0.8828(8) 0.041(4) Uani 1 1 d . U . . .
C122 C 0.8367(12) 0.7846(10) 0.8418(8) 0.0413(18) Uani 1 1 d . U . . .
H122 H 0.849997 0.746991 0.833323 0.050 Uiso 1 1 calc R U . . .
B25 B 0.3365(12) 0.4761(11) 0.6544(8) 0.0334(13) Uani 1 1 d . U . . .
H25 H 0.333288 0.449124 0.617729 0.040 Uiso 1 1 calc R U . . .
B50 B 0.1360(11) 0.9064(10) 0.7799(7) 0.029(3) Uani 1 1 d . U . . .
H50A H 0.076531 0.889077 0.772841 0.034 Uiso 1 1 calc R U . . .
C154 C 0.2284(13) 0.6655(9) 0.6074(7) 0.040(5) Uani 1 1 d . U . . .
H154 H 0.259881 0.665452 0.584706 0.049 Uiso 1 1 calc R U . . .
C148 C 0.1062(10) 0.4480(10) 0.6368(8) 0.036(4) Uani 1 1 d . U . . .
H148 H 0.112757 0.474526 0.666878 0.044 Uiso 1 1 calc R U . . .
C64 C 0.4321(11) 0.2896(12) 0.8451(8) 0.045(2) Uani 1 1 d . U . . .
H64 H 0.444836 0.270328 0.873409 0.054 Uiso 1 1 calc R U . . .
C132 C 0.6585(11) 1.0695(10) 0.7966(6) 0.034(3) Uani 1 1 d . U . . .
C40 C 0.4743(9) 0.8273(8) 0.5215(6) 0.026(3) Uani 1 1 d . U . . .
C41 C 0.3238(12) 0.8163(10) 0.5219(10) 0.045(2) Uani 1 1 d . U . . .
C134 C 0.7631(10) 1.2120(9) 0.8807(8) 0.034(4) Uani 1 1 d . U . . .
H134 H 0.733207 1.194788 0.903185 0.041 Uiso 1 1 calc R U . . .
C33 C 0.7691(11) 0.8723(10) 0.5313(7) 0.036(4) Uani 1 1 d . U . . .
C82 C 0.3404(11) 0.7481(10) 0.8688(8) 0.038(4) Uani 1 1 d . U . . .
H82 H 0.374323 0.778349 0.893093 0.046 Uiso 1 1 calc R U . . .
C106 C 0.2618(10) 1.0080(9) 0.7970(6) 0.029(3) Uani 1 1 d . U . . .
C27 C 0.6992(11) 0.8082(9) 0.6084(7) 0.032(3) Uani 1 1 d . U . . .
C11 C 0.8685(14) 0.3444(12) 0.7026(10) 0.054(6) Uani 1 1 d . U . . .
H11 H 0.913060 0.348840 0.722486 0.065 Uiso 1 1 calc R U . . .
B43 B 0.6285(12) 0.9527(11) 0.8302(7) 0.0333(12) Uani 1 1 d . U . . .
H43A H 0.603756 0.920640 0.856621 0.040 Uiso 1 1 calc R U . . .
C145 C 0.0806(9) 0.3713(9) 0.5460(7) 0.030(3) Uani 1 1 d . U . . .
H145 H 0.070923 0.345476 0.515268 0.036 Uiso 1 1 calc R U . . .
C141 C 0.5599(13) 1.2534(10) 0.7129(8) 0.041(5) Uani 1 1 d . U . . .
H141 H 0.537950 1.286922 0.715709 0.050 Uiso 1 1 calc R U . . .
B26 B 0.4180(12) 0.5070(11) 0.6960(8) 0.0336(13) Uani 1 1 d . U . . .
H26 H 0.468582 0.500079 0.686569 0.040 Uiso 1 1 calc R U . . .
C139 C 0.6185(11) 1.1791(9) 0.7517(7) 0.035(4) Uani 1 1 d . U . . .
B56 B 0.2692(12) 0.8904(10) 0.8283(8) 0.030(3) Uani 1 1 d . U . . .
H56A H 0.296733 0.862788 0.852847 0.036 Uiso 1 1 calc R U . . .
C26 C 0.8803(13) 0.7607(10) 0.6122(8) 0.043(4) Uani 1 1 d . U . . .
H26A H 0.839177 0.752393 0.587675 0.051 Uiso 1 1 calc R U . . .
C47 C 0.4072(14) 0.7843(14) 0.6041(8) 0.055(2) Uani 1 1 d . U . . .
C147 C 0.0543(10) 0.3896(11) 0.6268(9) 0.042(4) Uani 1 1 d . U . . .
H147 H 0.028311 0.374400 0.651857 0.051 Uiso 1 1 calc R U . . .
C138 C 0.7798(12) 1.2310(11) 0.7972(9) 0.047(5) Uani 1 1 d . U . . .
H138 H 0.761850 1.226546 0.763118 0.056 Uiso 1 1 calc R U . . .
B47 B 0.7037(12) 1.0499(11) 0.7536(7) 0.0334(12) Uani 1 1 d . U . . .
H47 H 0.728875 1.083801 0.728410 0.040 Uiso 1 1 calc R U . . .
C30 C 0.7058(12) 0.7908(10) 0.7068(7) 0.039(4) Uani 1 1 d . U . . .
H30 H 0.707641 0.783974 0.740345 0.046 Uiso 1 1 calc R U . . .
C92 C 0.2058(13) 0.5629(11) 0.9385(9) 0.048(5) Uani 1 1 d . U . . .
H92 H 0.230636 0.548429 0.915291 0.058 Uiso 1 1 calc R U . . .
C146 C 0.0384(13) 0.3523(10) 0.5818(9) 0.047(5) Uani 1 1 d . U . . .
H146 H -0.000622 0.314388 0.575274 0.056 Uiso 1 1 calc R U . . .
B16 B 0.8175(12) 0.5381(11) 0.7472(7) 0.031(3) Uani 1 1 d . U . . .
H16A H 0.844710 0.510521 0.772071 0.037 Uiso 1 1 calc R U . . .
C140 C 0.5819(11) 1.2269(11) 0.7556(8) 0.040(4) Uani 1 1 d . U . . .
H140 H 0.572399 1.240841 0.786492 0.047 Uiso 1 1 calc R U . . .
C28 C 0.6500(12) 0.7548(10) 0.6228(7) 0.037(4) Uani 1 1 d . U . . .
H28 H 0.614083 0.725213 0.599285 0.044 Uiso 1 1 calc R U . . .
C43 C 0.1977(12) 0.8019(10) 0.4886(9) 0.045(2) Uani 1 1 d . U . . .
H43 H 0.151945 0.774784 0.474284 0.055 Uiso 1 1 calc R U . . .
C144 C 0.6272(12) 1.1567(12) 0.7047(7) 0.043(5) Uani 1 1 d . U . . .
H144 H 0.648449 1.122782 0.700928 0.051 Uiso 1 1 calc R U . . .
B51 B 0.1825(10) 0.9794(9) 0.8182(6) 0.024(3) Uani 1 1 d . U . . .
H51A H 0.153629 1.010042 0.835820 0.029 Uiso 1 1 calc R U . . .
C98 C 0.1188(11) 0.7445(10) 0.8870(8) 0.038(4) Uani 1 1 d . U . . .
H98 H 0.159471 0.753120 0.911899 0.045 Uiso 1 1 calc R U . . .
C42 C 0.2589(12) 0.7776(11) 0.4985(9) 0.045(2) Uani 1 1 d . U . . .
H42 H 0.253773 0.733613 0.488444 0.054 Uiso 1 1 calc R U . . .
C51 C 0.4053(14) 0.8301(14) 0.6844(8) 0.056(2) Uani 1 1 d . U . . .
H51 H 0.401230 0.865474 0.704780 0.067 Uiso 1 1 calc R U . . .
C32 C 0.7506(11) 0.8540(9) 0.6436(7) 0.033(4) Uani 1 1 d . U . . .
H32 H 0.782482 0.890342 0.634019 0.039 Uiso 1 1 calc R U . . .
C77 C 0.5404(12) 0.7894(13) 0.8201(8) 0.048(5) Uani 1 1 d . U . . .
H77 H 0.513744 0.818105 0.810768 0.057 Uiso 1 1 calc R U . . .
B14 B 0.7348(12) 0.6253(12) 0.7359(8) 0.035(3) Uani 1 1 d . U . . .
H14 H 0.707110 0.657241 0.753306 0.041 Uiso 1 1 calc R U . . .
B60 B 0.2663(12) 0.4555(11) 0.6918(7) 0.0334(13) Uani 1 1 d . U . . .
H60A H 0.216979 0.414531 0.679297 0.040 Uiso 1 1 calc R U . . .
C3 C 0.5929(18) 0.4033(16) 0.8164(10) 0.071(8) Uani 1 1 d . U . . .
H3 H 0.549647 0.410144 0.822854 0.086 Uiso 1 1 calc R U . . .
C99 C 0.0978(10) 0.9249(10) 0.9071(7) 0.0341(16) Uani 1 1 d . U . . .
C59 C 0.1737(12) 0.2645(12) 0.6178(10) 0.050(2) Uani 1 1 d . U . . .
H59 H 0.154281 0.257503 0.583850 0.060 Uiso 1 1 calc R U . . .
C61 C 0.3896(11) 0.3410(12) 0.7618(8) 0.044(2) Uani 1 1 d . U . . .
C8 C 0.7366(12) 0.3292(12) 0.6429(8) 0.049(5) Uani 1 1 d . U . . .
H8A H 0.692555 0.323619 0.621963 0.058 Uiso 1 1 calc R U . . .
C34 C 0.8080(13) 0.8527(14) 0.4972(10) 0.054(6) Uani 1 1 d . U . . .
H34 H 0.791411 0.810293 0.480402 0.065 Uiso 1 1 calc R U . . .
B23 B 0.3310(12) 0.5904(11) 0.7102(8) 0.0336(13) Uani 1 1 d . U . . .
H23 H 0.323660 0.639612 0.709585 0.040 Uiso 1 1 calc R U . . .
C23 C 1.0018(11) 0.7874(10) 0.6815(8) 0.042(5) Uani 1 1 d . U . . .
H23A H 1.044220 0.797057 0.704853 0.050 Uiso 1 1 calc R U . . .
C79 C 0.5171(12) 0.6694(11) 0.9600(10) 0.048(4) Uani 1 1 d . U . . .
C128 C 0.9644(11) 1.1505(10) 0.9243(9) 0.043(4) Uani 1 1 d . U . . .
H128 H 1.002747 1.188868 0.931839 0.052 Uiso 1 1 calc R U . . .
B17 B 0.8654(11) 0.6014(10) 0.7197(7) 0.029(2) Uani 1 1 d . U . . .
H17A H 0.924858 0.617189 0.725544 0.035 Uiso 1 1 calc R U . . .
C24 C 0.9771(11) 0.8367(11) 0.6636(10) 0.049(5) Uani 1 1 d . U . . .
H24A H 1.002241 0.880107 0.675738 0.059 Uiso 1 1 calc R U . . .
C84 C 0.2824(14) 0.7177(10) 0.7856(7) 0.045(5) Uani 1 1 d . U . . .
H84 H 0.277082 0.726784 0.752466 0.053 Uiso 1 1 calc R U . . .
C37 C 0.8522(11) 0.9784(11) 0.5390(8) 0.043(4) Uani 1 1 d . U . . .
H37 H 0.866923 1.022213 0.552774 0.051 Uiso 1 1 calc R U . . .
C85 C 0.2353(14) 0.6635(10) 0.7986(8) 0.044(4) Uani 1 1 d . U . . .
H85 H 0.199541 0.635048 0.774387 0.053 Uiso 1 1 calc R U . . .
C21 C 0.9008(10) 0.7104(9) 0.6294(7) 0.032(3) Uani 1 1 d . U . . .
C124 C 0.7782(12) 0.8436(10) 0.8926(8) 0.0411(18) Uani 1 1 d . U . . .
H124 H 0.751297 0.843712 0.918277 0.049 Uiso 1 1 calc R U . . .
C2 C 0.6142(13) 0.4124(12) 0.7726(10) 0.053(5) Uani 1 1 d . U . . .
H2 H 0.584634 0.426868 0.748758 0.064 Uiso 1 1 calc R U . . .
B54 B 0.3159(11) 0.9577(10) 0.8023(7) 0.028(3) Uani 1 1 d . U . . .
H54 H 0.375359 0.975076 0.809020 0.033 Uiso 1 1 calc R U . . .
C50 C 0.4244(14) 0.7806(14) 0.7034(8) 0.056(2) Uani 1 1 d . U . . .
H50 H 0.424372 0.777239 0.737349 0.067 Uiso 1 1 calc R U . . .
C54 C 0.3493(10) 0.4470(9) 0.7104(6) 0.029(3) Uani 1 1 d . U . . .
B21 B 0.3043(12) 0.4736(11) 0.7521(8) 0.0336(13) Uani 1 1 d . U . . .
H21 H 0.280302 0.443995 0.780028 0.040 Uiso 1 1 calc R U . . .
C44 C 0.2105(12) 0.8673(10) 0.5015(9) 0.045(2) Uani 1 1 d . U . . .
H44 H 0.172215 0.885275 0.494080 0.055 Uiso 1 1 calc R U . . .
C55 C 0.2695(12) 0.3146(12) 0.6825(10) 0.050(2) Uani 1 1 d . U . . .
B52 B 0.1849(12) 0.9732(10) 0.7547(7) 0.029(3) Uani 1 1 d . U . . .
H52A H 0.157976 1.001531 0.730380 0.035 Uiso 1 1 calc R U . . .
C25 C 0.9184(12) 0.8241(10) 0.6297(10) 0.047(5) Uani 1 1 d . U . . .
H25A H 0.902777 0.858533 0.617585 0.056 Uiso 1 1 calc R U . . .
B41 B 0.7381(12) 1.0612(11) 0.8159(7) 0.0333(13) Uani 1 1 d . U . . .
H41 H 0.786377 1.101578 0.832375 0.040 Uiso 1 1 calc R U . . .
B22 B 0.2617(12) 0.5258(11) 0.7251(8) 0.0336(13) Uani 1 1 d . U . . .
H22 H 0.210615 0.531704 0.734308 0.040 Uiso 1 1 calc R U . . .
B59 B 0.7415(12) 0.9943(11) 0.7779(7) 0.0334(12) Uani 1 1 d . U . . .
H59A H 0.793356 0.990058 0.768828 0.040 Uiso 1 1 calc R U . . .
B4 B 0.4756(11) 0.8869(10) 0.4829(8) 0.032(2) Uani 1 1 d . U . . .
H4 H 0.427075 0.901295 0.468709 0.038 Uiso 1 1 calc R U . . .
B40 B 0.5362(11) 0.7858(10) 0.5101(8) 0.029(3) Uani 1 1 d . U . . .
H40 H 0.529222 0.733676 0.514428 0.034 Uiso 1 1 calc R U . . .
C126 C 0.9006(13) 1.0578(10) 0.8701(7) 0.041(4) Uani 1 1 d . U . . .
H126 H 0.895425 1.031378 0.840209 0.049 Uiso 1 1 calc R U . . .
C52 C 0.3919(14) 0.8267(14) 0.6338(8) 0.056(2) Uani 1 1 d . U . . .
H52 H 0.370290 0.856655 0.619710 0.067 Uiso 1 1 calc R U . . .
B32 B 0.4623(13) 0.7076(13) 0.9781(10) 0.041(4) Uani 1 1 d . U . . .
H32A H 0.471842 0.761066 0.980233 0.049 Uiso 1 1 calc R U . . .
C113 C 0.3266(13) 1.1143(11) 0.7477(7) 0.040(3) Uani 1 1 d . U . . .
C149 C 0.1363(11) 0.6672(10) 0.6747(8) 0.038(4) Uani 1 1 d . U . . .
H149 H 0.103131 0.667113 0.696237 0.046 Uiso 1 1 calc R U . . .
C123 C 0.7972(12) 0.7882(11) 0.8777(8) 0.0413(18) Uani 1 1 d . U . . .
H123 H 0.781527 0.750974 0.893619 0.050 Uiso 1 1 calc R U . . .
C130 C 0.8634(11) 1.0775(9) 0.9468(7) 0.033(4) Uani 1 1 d . U . . .
H130 H 0.830657 1.065773 0.968726 0.040 Uiso 1 1 calc R U . . .
C97 C 0.0785(16) 0.6802(12) 0.8690(10) 0.058(6) Uani 1 1 d . U . . .
H97 H 0.091216 0.644775 0.881813 0.070 Uiso 1 1 calc R U . . .
B1 B 0.5521(12) 0.8430(10) 0.5626(8) 0.032(3) Uani 1 1 d . U . . .
H1 H 0.555718 0.829424 0.600908 0.039 Uiso 1 1 calc R U . . .
B18 B 0.8164(11) 0.5292(10) 0.6843(7) 0.028(3) Uani 1 1 d . U . . .
H18A H 0.843231 0.496660 0.666669 0.034 Uiso 1 1 calc R U . . .
C110 C 0.1512(13) 1.2077(11) 0.8498(9) 0.046(4) Uani 1 1 d . U . . .
H110 H 0.120702 1.230986 0.860310 0.055 Uiso 1 1 calc R U . . .
C35 C 0.8701(15) 0.8946(14) 0.4879(10) 0.064(7) Uani 1 1 d . U . . .
H35 H 0.898601 0.879480 0.467856 0.076 Uiso 1 1 calc R U . . .
C38 C 0.7914(11) 0.9367(10) 0.5519(8) 0.039(4) Uani 1 1 d . U . . .
H38 H 0.765901 0.952150 0.574175 0.047 Uiso 1 1 calc R U . . .
C151 C 0.2084(15) 0.7212(12) 0.6182(10) 0.056(6) Uani 1 1 d . U . . .
H151 H 0.223465 0.757518 0.601219 0.067 Uiso 1 1 calc R U . . .
C74 C 0.6091(13) 0.6971(14) 0.8438(11) 0.061(6) Uani 1 1 d . U . . .
H74 H 0.632417 0.665289 0.851222 0.074 Uiso 1 1 calc R U . . .
C103 C -0.0103(11) 0.9404(10) 0.9276(7) 0.0344(16) Uani 1 1 d . U . . .
H103 H -0.058643 0.922028 0.930122 0.041 Uiso 1 1 calc R U . . .
C116 C 0.3650(14) 1.1415(13) 0.6582(9) 0.052(4) Uani 1 1 d . U . . .
H116 H 0.378141 1.150994 0.627356 0.062 Uiso 1 1 calc R U . . .
C67 C 0.6697(16) 0.6798(14) 0.9569(13) 0.066(4) Uani 1 1 d . U . . .
C107 C 0.2420(12) 1.1356(10) 0.8235(9) 0.042(3) Uani 1 1 d . U . . .
C114 C 0.2807(14) 1.1366(12) 0.7156(8) 0.046(3) Uani 1 1 d . U . . .
H114 H 0.237988 1.142414 0.724119 0.055 Uiso 1 1 calc R U . . .
C111 C 0.2199(13) 1.2185(11) 0.8751(9) 0.047(4) Uani 1 1 d . U . . .
H111 H 0.238236 1.253764 0.900239 0.056 Uiso 1 1 calc R U . . .
B11 B 0.8139(12) 0.6578(10) 0.7131(7) 0.030(3) Uani 1 1 d . U . . .
H11A H 0.838926 0.710900 0.714577 0.036 Uiso 1 1 calc R U . . .
C9 C 0.7828(16) 0.2931(15) 0.6322(11) 0.067(7) Uani 1 1 d . U . . .
H9 H 0.768528 0.262154 0.603922 0.081 Uiso 1 1 calc R U . . .
C108 C 0.1729(12) 1.1266(11) 0.7954(9) 0.043(3) Uani 1 1 d . U . . .
H108 H 0.157419 1.095738 0.767033 0.051 Uiso 1 1 calc R U . . .
B10 B 0.8182(12) 0.6178(11) 0.7668(7) 0.032(3) Uani 1 1 d . U . . .
H10 H 0.845922 0.644061 0.803582 0.038 Uiso 1 1 calc R U . . .
C31 C 0.7528(13) 0.8437(10) 0.6944(7) 0.044(5) Uani 1 1 d . U . . .
H31 H 0.786634 0.873349 0.719080 0.053 Uiso 1 1 calc R U . . .
C12 C 0.8237(12) 0.3816(10) 0.7146(8) 0.041(5) Uani 1 1 d . U . . .
H12 H 0.838607 0.412344 0.743008 0.050 Uiso 1 1 calc R U . . .
C117 C 0.4082(13) 1.1194(12) 0.6910(8) 0.046(3) Uani 1 1 d . U . . .
H117 H 0.450817 1.112926 0.682999 0.055 Uiso 1 1 calc R U . . .
B27 B 0.3982(12) 0.5051(11) 0.7570(8) 0.0337(13) Uani 1 1 d . U . . .
H27 H 0.435521 0.496095 0.788120 0.040 Uiso 1 1 calc R U . . .
B19 B 0.7334(11) 0.5380(10) 0.6554(7) 0.030(3) Uani 1 1 d . U . . .
H19A H 0.705235 0.511224 0.618798 0.036 Uiso 1 1 calc R U . . .
B42 B 0.6649(12) 1.0341(11) 0.8491(7) 0.0333(12) Uani 1 1 d . U . . .
H42A H 0.664379 1.056323 0.886721 0.040 Uiso 1 1 calc R U . . .
C10 C 0.8439(16) 0.3001(13) 0.6592(11) 0.061(6) Uani 1 1 d . U . . .
H10A H 0.873038 0.274886 0.649780 0.073 Uiso 1 1 calc R U . . .
C102 C 0.0194(10) 1.0023(10) 0.9430(7) 0.0343(16) Uani 1 1 d . U . . .
H102 H -0.008564 1.028799 0.952413 0.041 Uiso 1 1 calc R U . . .
C88 C 0.193(2) 0.6449(15) 0.9952(15) 0.089(12) Uani 1 1 d . U . . .
H88 H 0.207480 0.687835 1.010944 0.107 Uiso 1 1 calc R U . . .
C112 C 0.2627(13) 1.1798(10) 0.8652(9) 0.044(3) Uani 1 1 d . U . . .
H112 H 0.305790 1.183748 0.886781 0.052 Uiso 1 1 calc R U . . .
C86 C 0.2413(11) 0.6517(10) 0.8472(8) 0.038(4) Uani 1 1 d . U . . .
H86 H 0.209410 0.615133 0.856477 0.046 Uiso 1 1 calc R U . . .
B49 B 0.1888(12) 0.8947(11) 0.7344(7) 0.033(3) Uani 1 1 d . U . . .
H49A H 0.164548 0.869644 0.696680 0.039 Uiso 1 1 calc R U . . .
C45 C 0.2747(12) 0.9077(11) 0.5244(9) 0.046(2) Uani 1 1 d . U . . .
H45 H 0.280817 0.952096 0.533503 0.055 Uiso 1 1 calc R U . . .
C129 C 0.9209(12) 1.1337(10) 0.9592(9) 0.040(4) Uani 1 1 d . U . . .
H129 H 0.929619 1.159071 0.990028 0.048 Uiso 1 1 calc R U . . .
C109 C 0.1282(13) 1.1613(11) 0.8083(9) 0.049(4) Uani 1 1 d . U . . .
H109 H 0.082335 1.154043 0.789284 0.058 Uiso 1 1 calc R U . . .
B5 B 0.4881(10) 0.8125(10) 0.4618(8) 0.027(2) Uani 1 1 d . U . . .
H5 H 0.447576 0.777064 0.433353 0.033 Uiso 1 1 calc R U . . .
C58 C 0.1324(12) 0.2418(12) 0.6490(10) 0.050(2) Uani 1 1 d . U . . .
H58 H 0.085290 0.215899 0.636716 0.060 Uiso 1 1 calc R U . . .
B20 B 0.3470(12) 0.5591(11) 0.7652(8) 0.0336(13) Uani 1 1 d . U . . .
H20A H 0.351953 0.587693 0.801454 0.040 Uiso 1 1 calc R U . . .
C136 C 0.8733(13) 1.2723(14) 0.8672(11) 0.058(6) Uani 1 1 d . U . . .
H136 H 0.921089 1.296316 0.879650 0.070 Uiso 1 1 calc R U . . .
C96 C 0.0192(16) 0.6701(12) 0.8315(11) 0.063(7) Uani 1 1 d . U . . .
H96 H -0.008391 0.627373 0.819205 0.075 Uiso 1 1 calc R U . . .
C89 C 0.134(3) 0.5988(16) 1.0086(18) 0.119(19) Uani 1 1 d . U . . .
H89 H 0.109910 0.611372 1.033029 0.143 Uiso 1 1 calc R U . . .
B44 B 0.5943(12) 0.9377(11) 0.7669(7) 0.0334(12) Uani 1 1 d . U . . .
H44A H 0.547398 0.895740 0.750888 0.040 Uiso 1 1 calc R U . . .
B55 B 0.2682(11) 0.8861(10) 0.7657(8) 0.030(3) Uani 1 1 d . U . . .
H55 H 0.296987 0.854995 0.748486 0.036 Uiso 1 1 calc R U . . .
C137 C 0.8479(16) 1.2652(16) 0.8158(13) 0.080(10) Uani 1 1 d . U . . .
H137 H 0.878759 1.284478 0.794412 0.096 Uiso 1 1 calc R U . . .
B6 B 0.5391(11) 0.8855(10) 0.4453(8) 0.031(2) Uani 1 1 d . U . . .
H6 H 0.533045 0.899240 0.407121 0.037 Uiso 1 1 calc R U . . .
C22 C 0.9634(12) 0.7234(10) 0.6646(7) 0.038(4) Uani 1 1 d . U . . .
H22A H 0.979275 0.689046 0.676685 0.045 Uiso 1 1 calc R U . . .
C150 C 0.1669(13) 0.7232(10) 0.6535(9) 0.045(5) Uani 1 1 d . U . . .
H150 H 0.158595 0.762724 0.663749 0.055 Uiso 1 1 calc R U . . .
C36 C 0.8905(15) 0.9586(14) 0.5080(11) 0.062(7) Uani 1 1 d . U . . .
H36 H 0.931038 0.988269 0.499968 0.074 Uiso 1 1 calc R U . . .
B28 B 0.4159(13) 0.5781(12) 0.7309(8) 0.038(3) Uani 1 1 d . U . . .
H28A H 0.465576 0.618276 0.744361 0.046 Uiso 1 1 calc R U . . .
B57 B 0.1889(12) 0.8521(10) 0.7865(7) 0.030(3) Uani 1 1 d . U . . .
H57A H 0.163263 0.798902 0.783675 0.036 Uiso 1 1 calc R U . . .
C105 C 0.1902(10) 0.9063(9) 0.8350(6) 0.029(3) Uani 1 1 d . U . . .
B39 B 0.6655(12) 0.9672(11) 0.7348(7) 0.0334(12) Uani 1 1 d . U . . .
H39 H 0.665150 0.945467 0.696880 0.040 Uiso 1 1 calc R U . . .
C46 C 0.3302(12) 0.8810(10) 0.5335(9) 0.046(2) Uani 1 1 d . U . . .
H46 H 0.375382 0.908578 0.548553 0.055 Uiso 1 1 calc R U . . .
C78 C 0.5562(13) 0.7790(10) 0.8691(8) 0.043(5) Uani 1 1 d . U . . .
H78 H 0.545464 0.805568 0.893871 0.052 Uiso 1 1 calc R U . . .
C75 C 0.5959(15) 0.7111(15) 0.7952(10) 0.068(6) Uani 1 1 d . U . . .
H75 H 0.609265 0.687839 0.769679 0.081 Uiso 1 1 calc R U . . .
C87 C 0.2293(13) 0.6280(10) 0.9600(9) 0.045(4) Uani 1 1 d . U . . .
B2 B 0.6078(12) 0.9166(10) 0.5457(9) 0.034(3) Uani 1 1 d . U . . .
H2A H 0.649653 0.951235 0.573938 0.041 Uiso 1 1 calc R U . . .
B3 B 0.5607(12) 0.9426(10) 0.4983(9) 0.033(2) Uani 1 1 d . U . . .
H3A H 0.570441 0.995256 0.494974 0.039 Uiso 1 1 calc R U . . .
B58 B 0.2649(11) 0.9699(10) 0.8475(7) 0.027(3) Uani 1 1 d . U . . .
H58A H 0.290164 0.995213 0.885045 0.033 Uiso 1 1 calc R U . . .
C65 C 0.4086(11) 0.3421(12) 0.8512(9) 0.044(2) Uani 1 1 d . U . . .
H65 H 0.409373 0.362535 0.882796 0.053 Uiso 1 1 calc R U . . .
C5 C 0.6966(19) 0.3708(16) 0.8417(9) 0.071(8) Uani 1 1 d . U . . .
H5A H 0.725927 0.356679 0.866067 0.085 Uiso 1 1 calc R U . . .
C90 C 0.113(3) 0.5384(19) 0.9867(19) 0.14(2) Uani 1 1 d . U . . .
H90 H 0.073965 0.508294 0.996238 0.165 Uiso 1 1 calc R U . . .
C135 C 0.8319(12) 1.2463(12) 0.8981(10) 0.051(5) Uani 1 1 d . U . . .
H135 H 0.849968 1.251440 0.932282 0.061 Uiso 1 1 calc R U . . .
B9 B 0.5152(12) 0.9081(10) 0.5455(9) 0.036(3) Uani 1 1 d . U . . .
H9A H 0.494271 0.936367 0.572090 0.043 Uiso 1 1 calc R U . . .
C81 C 0.2949(12) 0.6943(11) 0.8830(8) 0.039(4) Uani 1 1 d . U . . .
C83 C 0.3372(14) 0.7585(10) 0.8202(8) 0.044(4) Uani 1 1 d . U . . .
H83 H 0.371601 0.792922 0.810470 0.053 Uiso 1 1 calc R U . . .
C101 C 0.0961(10) 1.0293(10) 0.9453(7) 0.0342(16) Uani 1 1 d . U . . .
H101 H 0.119882 1.072621 0.958564 0.041 Uiso 1 1 calc R U . . .
B33 B 0.5126(17) 0.6751(15) 1.0199(12) 0.058(3) Uani 1 1 d . U . . .
H33 H 0.554749 0.705030 1.050249 0.069 Uiso 1 1 calc R U . . .
B15 B 0.7379(13) 0.5531(12) 0.7587(9) 0.038(3) Uani 1 1 d . U . . .
H15 H 0.712950 0.535945 0.790898 0.045 Uiso 1 1 calc R U . . .
C56 C 0.2270(12) 0.2906(12) 0.7183(10) 0.050(2) Uani 1 1 d . U . . .
H56 H 0.245660 0.298575 0.752427 0.060 Uiso 1 1 calc R U . . .
B48 B 0.6771(12) 0.9261(12) 0.7867(7) 0.0335(12) Uani 1 1 d . U . . .
H48A H 0.685285 0.877100 0.784040 0.040 Uiso 1 1 calc R U . . .
C6 C 0.7151(13) 0.3784(11) 0.7943(7) 0.044(5) Uani 1 1 d . U . . .
H6A H 0.755432 0.367328 0.786045 0.053 Uiso 1 1 calc R U . . .
B7 B 0.6248(12) 0.9041(10) 0.4848(8) 0.033(3) Uani 1 1 d . U . . .
H7 H 0.675660 0.929485 0.472805 0.039 Uiso 1 1 calc R U . . .
C49 C 0.4450(14) 0.7319(14) 0.6745(8) 0.056(2) Uani 1 1 d . U . . .
H49 H 0.464520 0.700631 0.688673 0.067 Uiso 1 1 calc R U . . .
B34 B 0.4181(17) 0.6650(15) 1.0215(12) 0.057(3) Uani 1 1 d . U . . .
H34A H 0.397764 0.688333 1.051408 0.069 Uiso 1 1 calc R U . . .
B12 B 0.7326(11) 0.6188(9) 0.6721(8) 0.029(3) Uani 1 1 d . U . . .
H12A H 0.705753 0.645875 0.646561 0.034 Uiso 1 1 calc R U . . .
C76 C 0.5660(12) 0.7552(15) 0.7850(9) 0.064(6) Uani 1 1 d . U . . .
H76 H 0.560733 0.765332 0.752182 0.076 Uiso 1 1 calc R U . . .
C57 C 0.1557(12) 0.2545(12) 0.7003(10) 0.050(2) Uani 1 1 d . U . . .
H57 H 0.124122 0.239063 0.722293 0.060 Uiso 1 1 calc R U . . .
C71 C 0.7880(17) 0.6851(15) 1.0002(13) 0.072(5) Uani 1 1 d . U . . .
H71 H 0.830532 0.707620 1.022043 0.087 Uiso 1 1 calc R U . . .
C68 C 0.6588(17) 0.6177(14) 0.9325(13) 0.072(5) Uani 1 1 d . U . . .
H68 H 0.617454 0.595797 0.909336 0.086 Uiso 1 1 calc R U . . .
C91 C 0.1451(18) 0.5190(15) 0.9514(13) 0.076(9) Uani 1 1 d . U . . .
H91 H 0.127628 0.476238 0.935248 0.092 Uiso 1 1 calc R U . . .
C4 C 0.6374(19) 0.384(2) 0.8517(12) 0.085(10) Uani 1 1 d . U . . .
H4A H 0.625544 0.379167 0.883545 0.102 Uiso 1 1 calc R U . . .
C115 C 0.3004(14) 1.1503(12) 0.6697(8) 0.050(4) Uani 1 1 d . U . . .
H115 H 0.270497 1.165461 0.646437 0.060 Uiso 1 1 calc R U . . .
B31 B 0.4417(17) 0.6617(14) 0.9189(12) 0.054(3) Uani 1 1 d . U . . .
H31A H 0.438019 0.683562 0.883670 0.065 Uiso 1 1 calc R U . . .
C70 C 0.7798(17) 0.6220(14) 0.9780(13) 0.074(5) Uani 1 1 d . U . . .
H70 H 0.816175 0.601561 0.984615 0.088 Uiso 1 1 calc R U . . .
B30 B 0.4776(17) 0.5942(14) 0.9265(13) 0.058(3) Uani 1 1 d . U . . .
H30A H 0.498532 0.572097 0.896332 0.070 Uiso 1 1 calc R U . . .
B36 B 0.5198(19) 0.6030(15) 0.9862(13) 0.062(3) Uani 1 1 d . U . . .
H36A H 0.568510 0.586807 0.995379 0.075 Uiso 1 1 calc R U . . .
C69 C 0.7163(18) 0.5908(15) 0.9461(14) 0.077(5) Uani 1 1 d . U . . .
H69 H 0.710848 0.548084 0.932214 0.092 Uiso 1 1 calc R U . . .
B38 B 0.3836(18) 0.5846(14) 0.9256(13) 0.058(3) Uani 1 1 d . U . . .
H38A H 0.340093 0.558148 0.894689 0.070 Uiso 1 1 calc R U . . .
B29 B 0.4334(19) 0.5459(15) 0.9657(14) 0.062(3) Uani 1 1 d . U . . .
H29A H 0.422739 0.492275 0.960297 0.075 Uiso 1 1 calc R U . . .
B35 B 0.4565(18) 0.5950(15) 1.0238(13) 0.062(3) Uani 1 1 d . U . . .
H35A H 0.462747 0.571992 1.058352 0.075 Uiso 1 1 calc R U . . .
B37 B 0.3759(18) 0.5833(15) 0.9911(13) 0.061(3) Uani 1 1 d . U . . .
H37A H 0.328286 0.552808 1.004037 0.074 Uiso 1 1 calc R U . . .
C66 C 0.3829(11) 0.3648(12) 0.8077(8) 0.044(2) Uani 1 1 d . U . . .
H66 H 0.360023 0.397706 0.810247 0.053 Uiso 1 1 calc R U . . .
Cl1 Cl 0.0710(4) 0.3265(4) 0.9008(3) 0.074(2) Uani 1 1 d . . . . .
Cl2 Cl -0.0645(4) 0.1829(4) 0.6090(4) 0.085(2) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au5 Au6 3.1202(10) . ?
Au5 Au4 3.0943(9) . ?
Au5 S3 2.302(4) . ?
Au5 P4 2.260(4) . ?
Au6 Au4 3.0351(10) . ?
Au6 S3 2.345(4) . ?
Au6 P5 2.269(4) . ?
Au8 Au9 3.0607(9) . ?
Au8 Au7 2.9939(10) . ?
Au8 S4 2.327(4) . ?
Au8 P3 2.251(4) . ?
Au9 Au7 3.0609(10) . ?
Au9 S4 2.310(4) . ?
Au9 P2 2.248(4) . ?
Au4 Au2 3.2586(9) 2_666 ?
Au4 Au2 3.4200(9) . ?
Au4 Au7 3.2990(10) . ?
Au4 Au7 3.1965(10) 2_666 ?
Au4 S3 2.338(4) . ?
Au4 S2 2.304(4) . ?
Au2 Au7 3.1701(9) 2_666 ?
Au2 Au7 3.3866(10) . ?
Au2 Au1 3.2182(10) . ?
Au2 Au3 3.0548(9) . ?
Au2 S1 2.339(4) . ?
Au2 S2 2.302(4) . ?
Au13 Au12 3.0740(10) . ?
Au13 Au14 3.0852(10) . ?
Au13 P9 2.252(4) . ?
Au13 S6 2.313(4) . ?
Au12 Au11 3.1755(10) 2_677 ?
Au12 Au11 3.3801(10) . ?
Au12 Au15 3.2238(10) 2_677 ?
Au12 Au15 3.2582(10) . ?
Au12 Au14 3.0349(11) . ?
Au12 S6 2.338(4) . ?
Au12 S7 2.304(4) . ?
Au7 S4 2.345(4) . ?
Au7 S2 2.311(4) . ?
Au16 Au15 3.0244(10) . ?
Au16 Au17 3.1348(11) . ?
Au16 S5 2.330(4) . ?
Au16 P11 2.264(4) . ?
Au1 Au3 3.1972(10) . ?
Au1 S1 2.302(4) . ?
Au1 P6 2.277(5) . ?
Au11 Au15 3.4730(10) . ?
Au11 Au15 3.2408(10) 2_677 ?
Au11 Au18 3.0494(10) . ?
Au11 Au10 3.1572(10) . ?
Au11 S8 2.356(4) . ?
Au11 S7 2.305(5) . ?
Au3 S1 2.310(4) . ?
Au3 P1 2.246(4) . ?
Au15 Au17 3.1250(10) . ?
Au15 S7 2.309(4) . ?
Au15 S5 2.348(4) . ?
Au18 Au10 3.2652(10) . ?
Au18 S8 2.314(4) . ?
Au18 P10 2.259(4) . ?
Au14 S6 2.314(4) . ?
Au14 P8 2.254(5) . ?
Au10 S8 2.310(4) . ?
Au10 P12 2.256(4) . ?
Au17 S5 2.306(4) . ?
Au17 P7 2.269(5) . ?
P9 C93 1.820(18) . ?
P9 C99 1.825(19) . ?
P9 C105 1.887(18) . ?
P5 C152 1.813(17) . ?
P5 C53 1.849(18) . ?
P5 C155 1.827(18) . ?
P10 C106 1.840(19) . ?
P10 C113 1.824(19) . ?
P10 C107 1.80(2) . ?
P4 C40 1.827(19) . ?
P4 C41 1.81(2) . ?
P4 C47 1.81(2) . ?
P11 C119 1.80(2) . ?
P11 C125 1.83(2) . ?
P11 C131 1.863(18) . ?
P2 C14 1.859(18) . ?
P2 C15 1.818(9) . ?
P2 C21 1.809(19) . ?
P6 C61 1.84(2) . ?
P6 C54 1.856(19) . ?
P6 C55 1.79(2) . ?
P1 C13 1.833(19) . ?
P1 C7 1.84(2) . ?
P1 C1 1.814(19) . ?
P3 C39 1.887(18) . ?
P3 C33 1.79(2) . ?
P3 C27 1.814(19) . ?
P8 C80 1.87(2) . ?
P8 C87 1.77(2) . ?
P8 C81 1.80(2) . ?
P12 C133 1.82(2) . ?
P12 C132 1.892(19) . ?
P12 C139 1.783(19) . ?
P7 C73 1.79(2) . ?
P7 C79 1.89(2) . ?
P7 C67 1.82(2) . ?
C93 C94 1.41(2) . ?
C93 C98 1.37(3) . ?
C13 B13 1.77(3) . ?
C13 B16 1.72(3) . ?
C13 B18 1.71(3) . ?
C13 B19 1.68(3) . ?
C13 B15 1.75(3) . ?
C7 C8 1.41(3) . ?
C7 C12 1.40(3) . ?
C94 H94 0.9500 . ?
C94 C95 1.38(3) . ?
C119 C120 1.42(3) . ?
C119 C124 1.40(3) . ?
C125 C126 1.37(3) . ?
C125 C130 1.42(2) . ?
C29 H29 0.9500 . ?
C29 C30 1.37(3) . ?
C29 C28 1.38(3) . ?
C48 H48 0.9500 . ?
C48 C47 1.41(4) . ?
C48 C49 1.40(3) . ?
C100 H100 0.9500 . ?
C100 C99 1.40(3) . ?
C100 C101 1.40(2) . ?
C104 H104 0.9500 . ?
C104 C99 1.38(3) . ?
C104 C103 1.41(2) . ?
C63 H63 0.9500 . ?
C63 C62 1.40(3) . ?
C63 C64 1.33(3) . ?
C152 C153 1.39(3) . ?
C152 C154 1.41(2) . ?
C142 H142 0.9500 . ?
C142 C143 1.39(3) . ?
C142 C141 1.35(3) . ?
C39 B8 1.67(3) . ?
C39 B40 1.64(3) . ?
C39 B1 1.76(3) . ?
C39 B2 1.75(3) . ?
C39 B7 1.77(3) . ?
B45 H45A 1.1200 . ?
B45 B46 1.83(3) . ?
B45 C132 1.77(3) . ?
B45 B47 1.80(3) . ?
B45 B44 1.83(3) . ?
B45 B39 1.79(3) . ?
C153 H153 0.9500 . ?
C153 C149 1.42(3) . ?
C53 B24 1.69(3) . ?
C53 B25 1.72(3) . ?
C53 B60 1.74(3) . ?
C53 B23 1.71(3) . ?
C53 B22 1.78(3) . ?
C121 H121 0.9500 . ?
C121 C120 1.36(3) . ?
C121 C122 1.40(3) . ?
C118 H118 0.9500 . ?
C118 C113 1.39(3) . ?
C118 C117 1.36(3) . ?
C14 B17 1.71(3) . ?
C14 B18 1.70(3) . ?
C14 B11 1.75(3) . ?
C14 B19 1.76(3) . ?
C14 B12 1.78(3) . ?
C80 B32 1.70(3) . ?
C80 B34 1.68(4) . ?
C80 B31 1.79(4) . ?
C80 B38 1.74(4) . ?
C80 B37 1.75(4) . ?
B46 H46A 1.1200 . ?
B46 C132 1.74(3) . ?
B46 B43 1.73(3) . ?
B46 B42 1.75(3) . ?
B46 B44 1.82(3) . ?
B13 H13 1.1200 . ?
B13 B14 1.72(3) . ?
B13 B19 1.77(3) . ?
B13 B15 1.79(3) . ?
B13 B12 1.78(3) . ?
C131 B43 1.71(3) . ?
C131 B41 1.73(3) . ?
C131 B59 1.72(3) . ?
C131 B42 1.76(3) . ?
C131 B48 1.72(3) . ?
C60 H60 0.9500 . ?
C60 C59 1.39(3) . ?
C60 C55 1.39(4) . ?
C95 H95 0.9500 . ?
C95 C96 1.34(4) . ?
C155 C156 1.40(2) . ?
C155 C148 1.43(3) . ?
B24 H24 1.1200 . ?
B24 B25 1.76(3) . ?
B24 B26 1.77(3) . ?
B24 B23 1.75(3) . ?
B24 B28 1.78(3) . ?
C62 H62 0.9500 . ?
C62 C61 1.39(3) . ?
C72 H72 0.9500 . ?
C72 C67 1.42(4) . ?
C72 C71 1.43(3) . ?
C120 H120 0.9500 . ?
C1 C2 1.33(3) . ?
C1 C6 1.40(3) . ?
C127 H127 0.9500 . ?
C127 C128 1.35(3) . ?
C127 C126 1.39(3) . ?
C16 H16 0.9500 . ?
C16 C15 1.3900 . ?
C16 C17 1.3900 . ?
C15 C20 1.3900 . ?
C20 H20 0.9500 . ?
C20 C19 1.3900 . ?
C19 H19 0.9500 . ?
C19 C18 1.3900 . ?
C18 H18 0.9500 . ?
C18 C17 1.3900 . ?
C17 H17 0.9500 . ?
C143 H143 0.9500 . ?
C143 C144 1.40(3) . ?
B8 H8 1.1200 . ?
B8 B40 1.73(3) . ?
B8 B5 1.71(3) . ?
B8 B6 1.84(3) . ?
B8 B7 1.81(3) . ?
C156 H156 0.9500 . ?
C156 C145 1.43(2) . ?
B53 H53 1.1200 . ?
B53 C106 1.76(3) . ?
B53 B54 1.81(3) . ?
B53 B52 1.73(3) . ?
B53 B49 1.72(3) . ?
B53 B55 1.77(3) . ?
C133 C134 1.38(3) . ?
C133 C138 1.44(3) . ?
C73 C74 1.46(3) . ?
C73 C78 1.38(3) . ?
C122 H122 0.9500 . ?
C122 C123 1.36(3) . ?
B25 H25 1.1200 . ?
B25 B26 1.78(3) . ?
B25 B60 1.84(3) . ?
B25 C54 1.73(3) . ?
B50 H50A 1.1200 . ?
B50 B51 1.78(3) . ?
B50 B52 1.77(3) . ?
B50 B49 1.80(3) . ?
B50 B57 1.79(3) . ?
B50 C105 1.74(3) . ?
C154 H154 0.9500 . ?
C154 C151 1.40(3) . ?
C148 H148 0.9500 . ?
C148 C147 1.38(3) . ?
C64 H64 0.9500 . ?
C64 C65 1.35(3) . ?
C132 B47 1.69(3) . ?
C132 B41 1.66(3) . ?
C132 B42 1.70(3) . ?
C40 B4 1.74(3) . ?
C40 B40 1.76(3) . ?
C40 B1 1.72(3) . ?
C40 B5 1.74(3) . ?
C40 B9 1.76(3) . ?
C41 C42 1.37(3) . ?
C41 C46 1.38(3) . ?
C134 H134 0.9500 . ?
C134 C135 1.36(3) . ?
C33 C34 1.42(3) . ?
C33 C38 1.40(3) . ?
C82 H82 0.9500 . ?
C82 C81 1.39(3) . ?
C82 C83 1.38(3) . ?
C106 B51 1.73(3) . ?
C106 B54 1.73(3) . ?
C106 B52 1.73(3) . ?
C106 B58 1.68(3) . ?
C27 C28 1.42(3) . ?
C27 C32 1.42(3) . ?
C11 H11 0.9500 . ?
C11 C12 1.41(3) . ?
C11 C10 1.42(4) . ?
B43 H43A 1.1200 . ?
B43 B42 1.73(3) . ?
B43 B44 1.76(3) . ?
B43 B48 1.81(3) . ?
C145 H145 0.9500 . ?
C145 C146 1.40(3) . ?
C141 H141 0.9500 . ?
C141 C140 1.42(3) . ?
B26 H26 1.1200 . ?
B26 C54 1.73(3) . ?
B26 B27 1.79(3) . ?
B26 B28 1.77(3) . ?
C139 C140 1.43(3) . ?
C139 C144 1.41(3) . ?
B56 H56A 1.1200 . ?
B56 B54 1.77(3) . ?
B56 B55 1.73(3) . ?
B56 B57 1.78(3) . ?
B56 C105 1.73(3) . ?
B56 B58 1.80(3) . ?
C26 H26A 0.9500 . ?
C26 C21 1.36(3) . ?
C26 C25 1.39(3) . ?
C47 C52 1.32(4) . ?
C147 H147 0.9500 . ?
C147 C146 1.38(3) . ?
C138 H138 0.9500 . ?
C138 C137 1.36(4) . ?
B47 H47 1.1200 . ?
B47 B41 1.74(3) . ?
B47 B59 1.72(3) . ?
B47 B39 1.76(3) . ?
C30 H30 0.9500 . ?
C30 C31 1.37(3) . ?
C92 H92 0.9500 . ?
C92 C87 1.42(3) . ?
C92 C91 1.43(4) . ?
C146 H146 0.9500 . ?
B16 H16A 1.1200 . ?
B16 B17 1.74(3) . ?
B16 B18 1.74(3) . ?
B16 B10 1.77(3) . ?
B16 B15 1.77(3) . ?
C140 H140 0.9500 . ?
C28 H28 0.9500 . ?
C43 H43 0.9500 . ?
C43 C42 1.45(3) . ?
C43 C44 1.38(3) . ?
C144 H144 0.9500 . ?
B51 H51A 1.1200 . ?
B51 B52 1.76(3) . ?
B51 C105 1.73(3) . ?
B51 B58 1.79(3) . ?
C98 H98 0.9500 . ?
C98 C97 1.42(3) . ?
C42 H42 0.9500 . ?
C51 H51 0.9500 . ?
C51 C50 1.35(4) . ?
C51 C52 1.38(3) . ?
C32 H32 0.9500 . ?
C32 C31 1.44(3) . ?
C77 H77 0.9500 . ?
C77 C78 1.40(3) . ?
C77 C76 1.41(3) . ?
B14 H14 1.1200 . ?
B14 B11 1.76(3) . ?
B14 B10 1.81(3) . ?
B14 B15 1.75(3) . ?
B14 B12 1.76(3) . ?
B60 H60A 1.1200 . ?
B60 C54 1.72(3) . ?
B60 B21 1.70(3) . ?
B60 B22 1.76(3) . ?
C3 H3 0.9500 . ?
C3 C2 1.35(4) . ?
C3 C4 1.39(4) . ?
C59 H59 0.9500 . ?
C59 C58 1.31(3) . ?
C61 C66 1.38(3) . ?
C8 H8A 0.9500 . ?
C8 C9 1.41(4) . ?
C34 H34 0.9500 . ?
C34 C35 1.39(4) . ?
B23 H23 1.1200 . ?
B23 B22 1.80(3) . ?
B23 B20 1.74(3) . ?
B23 B28 1.80(3) . ?
C23 H23A 0.9500 . ?
C23 C24 1.39(3) . ?
C23 C22 1.40(3) . ?
C79 B32 1.65(3) . ?
C79 B33 1.67(4) . ?
C79 B31 1.71(4) . ?
C79 B30 1.74(4) . ?
C79 B36 1.67(4) . ?
C128 H128 0.9500 . ?
C128 C129 1.39(3) . ?
B17 H17A 1.1200 . ?
B17 B18 1.74(3) . ?
B17 B11 1.80(3) . ?
B17 B10 1.78(3) . ?
C24 H24A 0.9500 . ?
C24 C25 1.34(3) . ?
C84 H84 0.9500 . ?
C84 C85 1.40(3) . ?
C84 C83 1.39(3) . ?
C37 H37 0.9500 . ?
C37 C38 1.41(3) . ?
C37 C36 1.35(3) . ?
C85 H85 0.9500 . ?
C85 C86 1.38(3) . ?
C21 C22 1.41(3) . ?
C124 H124 0.9500 . ?
C124 C123 1.41(3) . ?
C2 H2 0.9500 . ?
B54 H54 1.1200 . ?
B54 B55 1.74(3) . ?
B54 B58 1.77(3) . ?
C50 H50 0.9500 . ?
C50 C49 1.46(4) . ?
C54 B21 1.72(3) . ?
C54 B27 1.71(3) . ?
B21 H21 1.1200 . ?
B21 B22 1.74(3) . ?
B21 B27 1.78(3) . ?
B21 B20 1.80(3) . ?
C44 H44 0.9500 . ?
C44 C45 1.37(3) . ?
C55 C56 1.43(3) . ?
B52 H52A 1.1200 . ?
B52 B49 1.78(3) . ?
C25 H25A 0.9500 . ?
B41 H41 1.1200 . ?
B41 B59 1.75(3) . ?
B41 B42 1.82(3) . ?
B22 H22 1.1200 . ?
B22 B20 1.82(3) . ?
B59 H59A 1.1200 . ?
B59 B39 1.72(3) . ?
B59 B48 1.73(3) . ?
B4 H4 1.1200 . ?
B4 B5 1.77(3) . ?
B4 B6 1.75(3) . ?
B4 B3 1.76(3) . ?
B4 B9 1.77(3) . ?
B40 H40 1.1200 . ?
B40 B1 1.78(3) . ?
B40 B5 1.76(3) . ?
C126 H126 0.9500 . ?
C52 H52 0.9500 . ?
B32 H32A 1.1200 . ?
B32 B33 1.73(4) . ?
B32 B34 1.76(4) . ?
B32 B31 1.79(4) . ?
C113 C114 1.39(3) . ?
C149 H149 0.9500 . ?
C149 C150 1.42(3) . ?
C123 H123 0.9500 . ?
C130 H130 0.9500 . ?
C130 C129 1.41(3) . ?
C97 H97 0.9500 . ?
C97 C96 1.41(4) . ?
B1 H1 1.1200 . ?
B1 B2 1.82(3) . ?
B1 B9 1.83(3) . ?
B18 H18A 1.1200 . ?
B18 B19 1.79(3) . ?
C110 H110 0.9500 . ?
C110 C111 1.39(3) . ?
C110 C109 1.41(3) . ?
C35 H35 0.9500 . ?
C35 C36 1.39(4) . ?
C38 H38 0.9500 . ?
C151 H151 0.9500 . ?
C151 C150 1.37(3) . ?
C74 H74 0.9500 . ?
C74 C75 1.41(4) . ?
C103 H103 0.9500 . ?
C103 C102 1.32(3) . ?
C116 H116 0.9500 . ?
C116 C117 1.36(3) . ?
C116 C115 1.43(3) . ?
C67 C68 1.41(4) . ?
C107 C108 1.43(3) . ?
C107 C112 1.38(3) . ?
C114 H114 0.9500 . ?
C114 C115 1.41(3) . ?
C111 H111 0.9500 . ?
C111 C112 1.39(3) . ?
B11 H11A 1.1200 . ?
B11 B10 1.78(3) . ?
B11 B12 1.79(3) . ?
C9 H9 0.9500 . ?
C9 C10 1.30(4) . ?
C108 H108 0.9500 . ?
C108 C109 1.38(3) . ?
B10 H10 1.1200 . ?
B10 B15 1.79(3) . ?
C31 H31 0.9500 . ?
C12 H12 0.9500 . ?
C117 H117 0.9500 . ?
B27 H27 1.1200 . ?
B27 B20 1.77(3) . ?
B27 B28 1.76(3) . ?
B19 H19A 1.1200 . ?
B19 B12 1.79(3) . ?
B42 H42A 1.1200 . ?
C10 H10A 0.9500 . ?
C102 H102 0.9500 . ?
C102 C101 1.47(3) . ?
C88 H88 0.9500 . ?
C88 C89 1.43(4) . ?
C88 C87 1.38(4) . ?
C112 H112 0.9500 . ?
C86 H86 0.9500 . ?
C86 C81 1.41(3) . ?
B49 H49A 1.1200 . ?
B49 B55 1.75(3) . ?
B49 B57 1.77(3) . ?
C45 H45 0.9500 . ?
C45 C46 1.38(3) . ?
C129 H129 0.9500 . ?
C109 H109 0.9500 . ?
B5 H5 1.1200 . ?
B5 B6 1.77(3) . ?
C58 H58 0.9500 . ?
C58 C57 1.42(4) . ?
B20 H20A 1.1200 . ?
B20 B28 1.75(3) . ?
C136 H136 0.9500 . ?
C136 C137 1.43(4) . ?
C136 C135 1.32(4) . ?
C96 H96 0.9500 . ?
C89 H89 0.9500 . ?
C89 C90 1.33(5) . ?
B44 H44A 1.1200 . ?
B44 B39 1.78(3) . ?
B44 B48 1.75(3) . ?
B55 H55 1.1200 . ?
B55 B57 1.75(3) . ?
C137 H137 0.9500 . ?
B6 H6 1.1200 . ?
B6 B3 1.77(3) . ?
B6 B7 1.81(3) . ?
C22 H22A 0.9500 . ?
C150 H150 0.9500 . ?
C36 H36 0.9500 . ?
B28 H28A 1.1200 . ?
B57 H57A 1.1200 . ?
B57 C105 1.72(2) . ?
C105 B58 1.70(3) . ?
B39 H39 1.1200 . ?
B39 B48 1.77(3) . ?
C46 H46 0.9500 . ?
C78 H78 0.9500 . ?
C75 H75 0.9500 . ?
C75 C76 1.29(4) . ?
B2 H2A 1.1200 . ?
B2 B3 1.72(3) . ?
B2 B9 1.80(3) . ?
B2 B7 1.79(3) . ?
B3 H3A 1.1200 . ?
B3 B9 1.79(3) . ?
B3 B7 1.77(3) . ?
B58 H58A 1.1200 . ?
C65 H65 0.9500 . ?
C65 C66 1.42(3) . ?
C5 H5A 0.9500 . ?
C5 C6 1.43(3) . ?
C5 C4 1.34(5) . ?
C90 H90 0.9500 . ?
C90 C91 1.35(5) . ?
C135 H135 0.9500 . ?
B9 H9A 1.1200 . ?
C83 H83 0.9500 . ?
C101 H101 0.9500 . ?
B33 H33 1.1200 . ?
B33 B34 1.84(5) . ?
B33 B36 1.82(5) . ?
B33 B35 1.81(4) . ?
B15 H15 1.1200 . ?
C56 H56 0.9500 . ?
C56 C57 1.42(3) . ?
B48 H48A 1.1200 . ?
C6 H6A 0.9500 . ?
B7 H7 1.1200 . ?
C49 H49 0.9500 . ?
B34 H34A 1.1200 . ?
B34 B35 1.88(4) . ?
B34 B37 1.83(5) . ?
B12 H12A 1.1200 . ?
C76 H76 0.9500 . ?
C57 H57 0.9500 . ?
C71 H71 0.9500 . ?
C71 C70 1.42(4) . ?
C68 H68 0.9500 . ?
C68 C69 1.44(4) . ?
C91 H91 0.9500 . ?
C4 H4A 0.9500 . ?
C115 H115 0.9500 . ?
B31 H31A 1.1200 . ?
B31 B30 1.81(4) . ?
B31 B38 1.80(4) . ?
C70 H70 0.9500 . ?
C70 C69 1.40(5) . ?
B30 H30A 1.1200 . ?
B30 B36 1.72(5) . ?
B30 B38 1.82(5) . ?
B30 B29 1.73(5) . ?
B36 H36A 1.1200 . ?
B36 B29 1.81(5) . ?
B36 B35 1.73(5) . ?
C69 H69 0.9500 . ?
B38 H38A 1.1200 . ?
B38 B29 1.79(4) . ?
B38 B37 1.85(5) . ?
B29 H29A 1.1200 . ?
B29 B35 1.79(5) . ?
B29 B37 1.76(5) . ?
B35 H35A 1.1200 . ?
B35 B37 1.67(5) . ?
B37 H37A 1.1200 . ?
C66 H66 0.9500 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Au4 Au5 Au6 58.47(2) . . ?
S3 Au5 Au6 48.40(10) . . ?
S3 Au5 Au4 48.68(10) . . ?
P4 Au5 Au6 128.29(11) . . ?
P4 Au5 Au4 132.33(12) . . ?
P4 Au5 S3 176.33(15) . . ?
Au4 Au6 Au5 60.34(2) . . ?
S3 Au6 Au5 47.24(10) . . ?
S3 Au6 Au4 49.51(10) . . ?
P5 Au6 Au5 131.23(11) . . ?
P5 Au6 Au4 135.17(11) . . ?
P5 Au6 S3 174.96(14) . . ?
Au7 Au8 Au9 60.72(2) . . ?
S4 Au8 Au9 48.46(10) . . ?
S4 Au8 Au7 50.41(11) . . ?
P3 Au8 Au9 125.03(11) . . ?
P3 Au8 Au7 130.87(12) . . ?
P3 Au8 S4 173.11(16) . . ?
Au8 Au9 Au7 58.56(2) . . ?
S4 Au9 Au8 48.93(10) . . ?
S4 Au9 Au7 49.38(11) . . ?
P2 Au9 Au8 132.86(11) . . ?
P2 Au9 Au7 136.38(12) . . ?
P2 Au9 S4 174.13(16) . . ?
Au5 Au4 Au2 163.86(3) . . ?
Au5 Au4 Au2 102.96(3) . 2_666 ?
Au5 Au4 Au7 120.77(3) . . ?
Au5 Au4 Au7 136.76(3) . 2_666 ?
Au6 Au4 Au5 61.19(2) . . ?
Au6 Au4 Au2 114.17(3) . . ?
Au6 Au4 Au2 133.52(3) . 2_666 ?
Au6 Au4 Au7 97.37(3) . 2_666 ?
Au6 Au4 Au7 168.65(3) . . ?
Au2 Au4 Au2 91.08(2) 2_666 . ?
Au2 Au4 Au7 57.82(2) 2_666 . ?
Au7 Au4 Au2 60.50(2) . . ?
Au7 Au4 Au2 63.28(2) 2_666 2_666 ?
Au7 Au4 Au2 57.14(2) 2_666 . ?
Au7 Au4 Au7 87.84(2) 2_666 . ?
S3 Au4 Au5 47.68(9) . . ?
S3 Au4 Au6 49.69(10) . . ?
S3 Au4 Au2 86.36(10) . 2_666 ?
S3 Au4 Au2 142.96(10) . . ?
S3 Au4 Au7 89.36(10) . 2_666 ?
S3 Au4 Au7 140.87(10) . . ?
S2 Au4 Au5 125.71(10) . . ?
S2 Au4 Au6 124.49(11) . . ?
S2 Au4 Au2 42.04(10) . . ?
S2 Au4 Au2 100.68(11) . 2_666 ?
S2 Au4 Au7 44.46(11) . . ?
S2 Au4 Au7 97.51(10) . 2_666 ?
S2 Au4 S3 171.81(14) . . ?
Au4 Au2 Au4 88.92(2) 2_666 . ?
Au4 Au2 Au7 57.46(2) 2_666 . ?
Au7 Au2 Au4 57.98(2) . . ?
Au7 Au2 Au4 57.88(2) 2_666 . ?
Au7 Au2 Au4 61.73(2) 2_666 2_666 ?
Au7 Au2 Au7 86.76(2) 2_666 . ?
Au7 Au2 Au1 100.93(3) 2_666 . ?
Au1 Au2 Au4 121.45(3) . . ?
Au1 Au2 Au4 131.41(3) . 2_666 ?
Au1 Au2 Au7 170.37(3) . . ?
Au3 Au2 Au4 168.24(3) . . ?
Au3 Au2 Au4 96.99(3) . 2_666 ?
Au3 Au2 Au7 133.86(3) . 2_666 ?
Au3 Au2 Au7 117.20(3) . . ?
Au3 Au2 Au1 61.22(2) . . ?
S1 Au2 Au4 86.70(10) . 2_666 ?
S1 Au2 Au4 142.45(10) . . ?
S1 Au2 Au7 141.58(10) . . ?
S1 Au2 Au7 87.66(10) . 2_666 ?
S1 Au2 Au1 45.62(10) . . ?
S1 Au2 Au3 48.51(10) . . ?
S2 Au2 Au4 42.07(11) . . ?
S2 Au2 Au4 99.06(11) . 2_666 ?
S2 Au2 Au7 98.27(11) . 2_666 ?
S2 Au2 Au7 42.88(10) . . ?
S2 Au2 Au1 129.21(11) . . ?
S2 Au2 Au3 126.53(11) . . ?
S2 Au2 S1 173.18(14) . . ?
Au12 Au13 Au14 59.04(2) . . ?
P9 Au13 Au12 136.02(12) . . ?
P9 Au13 Au14 132.48(11) . . ?
P9 Au13 S6 175.00(16) . . ?
S6 Au13 Au12 48.97(11) . . ?
S6 Au13 Au14 48.21(11) . . ?
Au13 Au12 Au11 118.45(3) . . ?
Au13 Au12 Au11 128.20(3) . 2_677 ?
Au13 Au12 Au15 96.61(3) . 2_677 ?
Au13 Au12 Au15 169.38(3) . . ?
Au11 Au12 Au11 94.15(3) 2_677 . ?
Au11 Au12 Au15 65.73(2) 2_677 2_677 ?
Au11 Au12 Au15 60.47(2) 2_677 . ?
Au15 Au12 Au11 58.72(2) 2_677 . ?
Au15 Au12 Au11 63.06(2) . . ?
Au15 Au12 Au15 92.88(3) 2_677 . ?
Au14 Au12 Au13 60.66(2) . . ?
Au14 Au12 Au11 165.24(3) . . ?
Au14 Au12 Au11 97.06(3) . 2_677 ?
Au14 Au12 Au15 135.20(3) . 2_677 ?
Au14 Au12 Au15 114.89(3) . . ?
S6 Au12 Au13 48.28(10) . . ?
S6 Au12 Au11 81.13(10) . 2_677 ?
S6 Au12 Au11 143.13(11) . . ?
S6 Au12 Au15 86.65(11) . 2_677 ?
S6 Au12 Au15 137.51(10) . . ?
S6 Au12 Au14 48.95(10) . . ?
S7 Au12 Au13 127.80(11) . . ?
S7 Au12 Au11 103.70(11) . 2_677 ?
S7 Au12 Au11 42.84(11) . . ?
S7 Au12 Au15 45.11(11) . . ?
S7 Au12 Au15 100.24(12) . 2_677 ?
S7 Au12 Au14 124.40(12) . . ?
S7 Au12 S6 172.75(16) . . ?
Au8 Au7 Au9 60.72(2) . . ?
Au8 Au7 Au4 115.26(3) . . ?
Au8 Au7 Au4 137.14(3) . 2_666 ?
Au8 Au7 Au2 162.82(3) . . ?
Au8 Au7 Au2 99.35(3) . 2_666 ?
Au9 Au7 Au4 97.84(3) . 2_666 ?
Au9 Au7 Au4 167.99(3) . . ?
Au9 Au7 Au2 118.52(3) . . ?
Au9 Au7 Au2 130.18(3) . 2_666 ?
Au4 Au7 Au4 92.16(2) 2_666 . ?
Au4 Au7 Au2 61.52(2) . . ?
Au4 Au7 Au2 59.26(2) 2_666 . ?
Au2 Au7 Au4 60.45(2) 2_666 . ?
Au2 Au7 Au4 64.98(2) 2_666 2_666 ?
Au2 Au7 Au2 93.24(2) 2_666 . ?
S4 Au7 Au8 49.88(10) . . ?
S4 Au7 Au9 48.40(10) . . ?
S4 Au7 Au4 87.67(10) . 2_666 ?
S4 Au7 Au4 139.26(10) . . ?
S4 Au7 Au2 83.07(10) . 2_666 ?
S4 Au7 Au2 144.36(10) . . ?
S2 Au7 Au8 122.12(11) . . ?
S2 Au7 Au9 126.49(11) . . ?
S2 Au7 Au4 100.62(11) . 2_666 ?
S2 Au7 Au4 44.28(11) . . ?
S2 Au7 Au2 42.67(10) . . ?
S2 Au7 Au2 103.07(11) . 2_666 ?
S2 Au7 S4 171.19(15) . . ?
Au15 Au16 Au17 60.95(2) . . ?
S5 Au16 Au15 49.97(11) . . ?
S5 Au16 Au17 47.13(11) . . ?
P11 Au16 Au15 135.25(12) . . ?
P11 Au16 Au17 130.51(12) . . ?
P11 Au16 S5 174.12(16) . . ?
Au3 Au1 Au2 56.87(2) . . ?
S1 Au1 Au2 46.58(10) . . ?
S1 Au1 Au3 46.22(10) . . ?
P6 Au1 Au2 133.64(13) . . ?
P6 Au1 Au3 137.35(14) . . ?
P6 Au1 S1 176.43(17) . . ?
Au12 Au11 Au12 85.85(3) 2_677 . ?
Au12 Au11 Au15 57.80(2) 2_677 . ?
Au12 Au11 Au15 56.76(2) . . ?
Au12 Au11 Au15 61.03(2) 2_677 2_677 ?
Au15 Au11 Au12 58.23(2) 2_677 . ?
Au15 Au11 Au15 88.73(2) 2_677 . ?
Au18 Au11 Au12 117.18(3) . . ?
Au18 Au11 Au12 134.69(3) . 2_677 ?
Au18 Au11 Au15 167.39(3) . . ?
Au18 Au11 Au15 96.87(3) . 2_677 ?
Au18 Au11 Au10 63.46(2) . . ?
Au10 Au11 Au12 169.85(3) . . ?
Au10 Au11 Au12 100.61(3) . 2_677 ?
Au10 Au11 Au15 120.29(3) . . ?
Au10 Au11 Au15 131.81(3) . 2_677 ?
S8 Au11 Au12 142.04(11) . . ?
S8 Au11 Au12 88.61(10) . 2_677 ?
S8 Au11 Au15 86.44(10) . 2_677 ?
S8 Au11 Au15 143.43(11) . . ?
S8 Au11 Au18 48.64(10) . . ?
S8 Au11 Au10 46.81(10) . . ?
S7 Au11 Au12 97.51(11) . 2_677 ?
S7 Au11 Au12 42.82(11) . . ?
S7 Au11 Au15 99.74(11) . 2_677 ?
S7 Au11 Au15 41.21(11) . . ?
S7 Au11 Au18 126.35(11) . . ?
S7 Au11 Au10 127.79(11) . . ?
S7 Au11 S8 172.85(15) . . ?
Au2 Au3 Au1 61.91(2) . . ?
S1 Au3 Au2 49.34(9) . . ?
S1 Au3 Au1 46.00(10) . . ?
P1 Au3 Au2 137.87(12) . . ?
P1 Au3 Au1 133.92(13) . . ?
P1 Au3 S1 172.78(15) . . ?
Au12 Au15 Au12 87.12(3) 2_677 . ?
Au12 Au15 Au11 56.46(2) 2_677 . ?
Au12 Au15 Au11 63.05(2) 2_677 2_677 ?
Au12 Au15 Au11 60.18(2) . . ?
Au16 Au15 Au12 98.50(3) . 2_677 ?
Au16 Au15 Au12 169.01(3) . . ?
Au16 Au15 Au11 132.49(3) . 2_677 ?
Au16 Au15 Au11 115.33(3) . . ?
Au16 Au15 Au17 61.27(2) . . ?
Au11 Au15 Au12 58.50(2) 2_677 . ?
Au11 Au15 Au11 91.27(2) 2_677 . ?
Au17 Au15 Au12 137.53(3) . 2_677 ?
Au17 Au15 Au12 119.97(3) . . ?
Au17 Au15 Au11 101.75(3) . 2_677 ?
Au17 Au15 Au11 164.45(3) . . ?
S7 Au15 Au12 45.00(11) . . ?
S7 Au15 Au12 96.11(12) . 2_677 ?
S7 Au15 Au16 124.54(11) . . ?
S7 Au15 Au11 101.67(11) . 2_677 ?
S7 Au15 Au11 41.12(11) . . ?
S7 Au15 Au17 126.31(12) . . ?
S7 Au15 S5 171.79(15) . . ?
S5 Au15 Au12 140.40(11) . . ?
S5 Au15 Au12 90.69(11) . 2_677 ?
S5 Au15 Au16 49.47(10) . . ?
S5 Au15 Au11 85.49(10) . 2_677 ?
S5 Au15 Au11 143.84(11) . . ?
S5 Au15 Au17 47.25(11) . . ?
Au11 Au18 Au10 59.88(2) . . ?
S8 Au18 Au11 49.83(11) . . ?
S8 Au18 Au10 45.03(11) . . ?
P10 Au18 Au11 136.98(12) . . ?
P10 Au18 Au10 135.39(12) . . ?
P10 Au18 S8 173.19(16) . . ?
Au12 Au14 Au13 60.29(2) . . ?
S6 Au14 Au13 48.16(10) . . ?
S6 Au14 Au12 49.61(11) . . ?
P8 Au14 Au13 124.35(13) . . ?
P8 Au14 Au12 131.41(13) . . ?
P8 Au14 S6 172.20(17) . . ?
Au11 Au10 Au18 56.66(2) . . ?
S8 Au10 Au11 48.03(11) . . ?
S8 Au10 Au18 45.13(11) . . ?
P12 Au10 Au11 133.99(12) . . ?
P12 Au10 Au18 136.97(13) . . ?
P12 Au10 S8 177.24(18) . . ?
Au15 Au17 Au16 57.78(2) . . ?
S5 Au17 Au16 47.78(10) . . ?
S5 Au17 Au15 48.38(11) . . ?
P7 Au17 Au16 126.74(15) . . ?
P7 Au17 Au15 130.38(14) . . ?
P7 Au17 S5 174.52(19) . . ?
Au5 S3 Au6 84.36(12) . . ?
Au5 S3 Au4 83.64(13) . . ?
Au4 S3 Au6 80.80(13) . . ?
Au8 S4 Au7 79.71(13) . . ?
Au9 S4 Au8 82.61(13) . . ?
Au9 S4 Au7 82.22(13) . . ?
Au1 S1 Au2 87.80(13) . . ?
Au1 S1 Au3 87.78(13) . . ?
Au3 S1 Au2 82.14(13) . . ?
Au18 S8 Au11 81.53(15) . . ?
Au10 S8 Au11 85.16(14) . . ?
Au10 S8 Au18 89.85(15) . . ?
C93 P9 Au13 114.5(6) . . ?
C93 P9 C99 109.3(9) . . ?
C93 P9 C105 103.9(8) . . ?
C99 P9 Au13 109.6(6) . . ?
C99 P9 C105 106.7(8) . . ?
C105 P9 Au13 112.5(6) . . ?
C152 P5 Au6 110.5(6) . . ?
C152 P5 C53 104.5(8) . . ?
C152 P5 C155 110.2(8) . . ?
C53 P5 Au6 113.3(6) . . ?
C155 P5 Au6 111.4(6) . . ?
C155 P5 C53 106.7(8) . . ?
Au13 S6 Au12 82.75(13) . . ?
Au13 S6 Au14 83.63(14) . . ?
Au14 S6 Au12 81.44(14) . . ?
Au12 S7 Au11 94.34(17) . . ?
Au12 S7 Au15 89.88(15) . . ?
Au11 S7 Au15 97.67(17) . . ?
Au16 S5 Au15 80.56(13) . . ?
Au17 S5 Au16 85.09(14) . . ?
Au17 S5 Au15 84.37(14) . . ?
C106 P10 Au18 112.0(6) . . ?
C113 P10 Au18 111.4(8) . . ?
C113 P10 C106 103.0(9) . . ?
C107 P10 Au18 111.7(8) . . ?
C107 P10 C106 108.9(10) . . ?
C107 P10 C113 109.6(10) . . ?
Au4 S2 Au7 91.26(15) . . ?
Au2 S2 Au4 95.89(16) . . ?
Au2 S2 Au7 94.45(15) . . ?
C40 P4 Au5 112.7(6) . . ?
C41 P4 Au5 113.0(8) . . ?
C41 P4 C40 107.8(9) . . ?
C41 P4 C47 104.8(13) . . ?
C47 P4 Au5 112.1(10) . . ?
C47 P4 C40 105.8(10) . . ?
C119 P11 Au16 110.4(8) . . ?
C119 P11 C125 109.5(9) . . ?
C119 P11 C131 106.0(9) . . ?
C125 P11 Au16 112.1(5) . . ?
C125 P11 C131 105.4(8) . . ?
C131 P11 Au16 113.2(6) . . ?
C14 P2 Au9 114.8(6) . . ?
C15 P2 Au9 107.8(4) . . ?
C15 P2 C14 107.1(7) . . ?
C21 P2 Au9 113.8(6) . . ?
C21 P2 C14 103.0(8) . . ?
C21 P2 C15 110.1(8) . . ?
C61 P6 Au1 114.3(7) . . ?
C61 P6 C54 109.9(10) . . ?
C54 P6 Au1 110.1(6) . . ?
C55 P6 Au1 112.1(9) . . ?
C55 P6 C61 106.1(11) . . ?
C55 P6 C54 103.7(10) . . ?
C13 P1 Au3 112.3(6) . . ?
C13 P1 C7 106.7(9) . . ?
C7 P1 Au3 112.6(7) . . ?
C1 P1 Au3 112.6(7) . . ?
C1 P1 C13 102.5(9) . . ?
C1 P1 C7 109.5(10) . . ?
C39 P3 Au8 112.2(6) . . ?
C33 P3 Au8 112.8(7) . . ?
C33 P3 C39 106.7(9) . . ?
C33 P3 C27 109.3(9) . . ?
C27 P3 Au8 109.1(6) . . ?
C27 P3 C39 106.5(9) . . ?
C80 P8 Au14 114.7(8) . . ?
C87 P8 Au14 112.0(8) . . ?
C87 P8 C80 105.9(10) . . ?
C87 P8 C81 109.8(11) . . ?
C81 P8 Au14 108.4(7) . . ?
C81 P8 C80 105.8(10) . . ?
C133 P12 Au10 111.8(7) . . ?
C133 P12 C132 101.8(9) . . ?
C132 P12 Au10 111.5(6) . . ?
C139 P12 Au10 115.3(7) . . ?
C139 P12 C133 105.8(9) . . ?
C139 P12 C132 109.7(9) . . ?
C73 P7 Au17 107.5(7) . . ?
C73 P7 C79 105.6(11) . . ?
C73 P7 C67 108.7(13) . . ?
C79 P7 Au17 112.9(8) . . ?
C67 P7 Au17 114.3(11) . . ?
C67 P7 C79 107.4(12) . . ?
C94 C93 P9 121.5(14) . . ?
C98 C93 P9 116.5(14) . . ?
C98 C93 C94 121.9(18) . . ?
B13 C13 P1 116.1(12) . . ?
B16 C13 P1 124.1(12) . . ?
B16 C13 B13 111.3(14) . . ?
B16 C13 B15 61.1(12) . . ?
B18 C13 P1 119.8(11) . . ?
B18 C13 B13 113.3(14) . . ?
B18 C13 B16 60.8(11) . . ?
B18 C13 B15 111.3(14) . . ?
B19 C13 P1 114.7(12) . . ?
B19 C13 B13 61.7(11) . . ?
B19 C13 B16 112.9(15) . . ?
B19 C13 B18 63.8(12) . . ?
B19 C13 B15 111.9(14) . . ?
B15 C13 P1 121.5(14) . . ?
B15 C13 B13 61.1(12) . . ?
C8 C7 P1 115.8(16) . . ?
C12 C7 P1 125.0(16) . . ?
C12 C7 C8 119.2(19) . . ?
C93 C94 H94 121.0 . . ?
C95 C94 C93 118.1(18) . . ?
C95 C94 H94 121.0 . . ?
C120 C119 P11 123.8(17) . . ?
C124 C119 P11 117.4(15) . . ?
C124 C119 C120 118.8(18) . . ?
C126 C125 P11 125.3(14) . . ?
C126 C125 C130 118.4(18) . . ?
C130 C125 P11 116.1(14) . . ?
C30 C29 H29 118.9 . . ?
C30 C29 C28 122(2) . . ?
C28 C29 H29 118.9 . . ?
C47 C48 H48 118.8 . . ?
C49 C48 H48 118.8 . . ?
C49 C48 C47 122(3) . . ?
C99 C100 H100 119.3 . . ?
C101 C100 H100 119.3 . . ?
C101 C100 C99 121.4(19) . . ?
C99 C104 H104 120.4 . . ?
C99 C104 C103 119.2(19) . . ?
C103 C104 H104 120.4 . . ?
C62 C63 H63 119.8 . . ?
C64 C63 H63 119.8 . . ?
C64 C63 C62 120(2) . . ?
C153 C152 P5 123.4(14) . . ?
C153 C152 C154 117.9(17) . . ?
C154 C152 P5 118.6(14) . . ?
C143 C142 H142 119.7 . . ?
C141 C142 H142 119.7 . . ?
C141 C142 C143 120.7(18) . . ?
B8 C39 P3 115.0(12) . . ?
B8 C39 B1 114.4(15) . . ?
B8 C39 B2 112.4(14) . . ?
B8 C39 B7 63.3(12) . . ?
B40 C39 P3 116.2(12) . . ?
B40 C39 B8 62.8(12) . . ?
B40 C39 B1 62.9(12) . . ?
B40 C39 B2 113.7(14) . . ?
B40 C39 B7 115.5(15) . . ?
B1 C39 P3 120.3(12) . . ?
B1 C39 B7 113.9(14) . . ?
B2 C39 P3 122.2(14) . . ?
B2 C39 B1 62.3(12) . . ?
B2 C39 B7 60.9(12) . . ?
B7 C39 P3 116.9(13) . . ?
B46 B45 H45A 122.3 . . ?
B46 B45 B44 59.8(12) . . ?
C132 B45 H45A 126.7 . . ?
C132 B45 B46 57.9(11) . . ?
C132 B45 B47 56.4(11) . . ?
C132 B45 B44 102.2(13) . . ?
C132 B45 B39 101.3(14) . . ?
B47 B45 H45A 123.8 . . ?
B47 B45 B46 105.1(14) . . ?
B47 B45 B44 104.8(14) . . ?
B44 B45 H45A 123.7 . . ?
B39 B45 H45A 124.0 . . ?
B39 B45 B46 106.2(14) . . ?
B39 B45 B47 58.6(13) . . ?
B39 B45 B44 58.8(12) . . ?
C152 C153 H153 119.0 . . ?
C152 C153 C149 122.0(19) . . ?
C149 C153 H153 119.0 . . ?
B24 C53 P5 116.8(12) . . ?
B24 C53 B25 62.1(13) . . ?
B24 C53 B60 113.2(14) . . ?
B24 C53 B23 62.1(12) . . ?
B24 C53 B22 113.3(14) . . ?
B25 C53 P5 114.2(12) . . ?
B25 C53 B60 64.0(12) . . ?
B25 C53 B22 113.8(14) . . ?
B60 C53 P5 119.4(13) . . ?
B60 C53 B22 59.8(12) . . ?
B23 C53 P5 121.9(12) . . ?
B23 C53 B25 113.1(15) . . ?
B23 C53 B60 110.4(14) . . ?
B23 C53 B22 61.9(12) . . ?
B22 C53 P5 122.0(13) . . ?
C120 C121 H121 118.0 . . ?
C120 C121 C122 124(2) . . ?
C122 C121 H121 118.0 . . ?
C113 C118 H118 119.4 . . ?
C117 C118 H118 119.4 . . ?
C117 C118 C113 121(2) . . ?
B17 C14 P2 125.0(13) . . ?
B17 C14 B11 62.9(11) . . ?
B17 C14 B19 112.3(14) . . ?
B17 C14 B12 113.0(13) . . ?
B18 C14 P2 122.6(12) . . ?
B18 C14 B17 61.6(11) . . ?
B18 C14 B11 112.6(13) . . ?
B18 C14 B19 62.4(12) . . ?
B18 C14 B12 112.6(14) . . ?
B11 C14 P2 119.3(12) . . ?
B11 C14 B19 110.3(14) . . ?
B11 C14 B12 61.0(11) . . ?
B19 C14 P2 115.9(11) . . ?
B19 C14 B12 60.7(11) . . ?
B12 C14 P2 112.8(12) . . ?
B32 C80 P8 115.8(14) . . ?
B32 C80 B31 61.5(15) . . ?
B32 C80 B38 112.5(19) . . ?
B32 C80 B37 111.7(19) . . ?
B34 C80 P8 114.1(18) . . ?
B34 C80 B32 62.7(16) . . ?
B34 C80 B31 116(2) . . ?
B34 C80 B38 119(2) . . ?
B34 C80 B37 64.2(18) . . ?
B31 C80 P8 116.8(16) . . ?
B38 C80 P8 119.6(17) . . ?
B38 C80 B31 61.0(16) . . ?
B38 C80 B37 63.8(18) . . ?
B37 C80 P8 123.3(18) . . ?
B37 C80 B31 112.1(19) . . ?
B45 B46 H46A 120.3 . . ?
C132 B46 B45 59.4(12) . . ?
C132 B46 H46A 125.8 . . ?
C132 B46 B42 58.3(12) . . ?
C132 B46 B44 103.7(14) . . ?
B43 B46 B45 108.1(14) . . ?
B43 B46 H46A 123.4 . . ?
B43 B46 C132 102.7(15) . . ?
B43 B46 B42 59.6(13) . . ?
B43 B46 B44 59.4(12) . . ?
B42 B46 B45 109.6(16) . . ?
B42 B46 H46A 121.0 . . ?
B42 B46 B44 107.8(15) . . ?
B44 B46 B45 60.3(12) . . ?
B44 B46 H46A 122.8 . . ?
C13 B13 H13 125.2 . . ?
C13 B13 B19 56.6(11) . . ?
C13 B13 B15 59.0(11) . . ?
C13 B13 B12 104.5(14) . . ?
B14 B13 C13 104.6(15) . . ?
B14 B13 H13 122.3 . . ?
B14 B13 B19 107.4(16) . . ?
B14 B13 B15 59.7(13) . . ?
B14 B13 B12 60.4(12) . . ?
B19 B13 H13 122.8 . . ?
B19 B13 B15 106.0(15) . . ?
B19 B13 B12 60.5(12) . . ?
B15 B13 H13 122.0 . . ?
B12 B13 H13 121.8 . . ?
B12 B13 B15 108.1(16) . . ?
B43 C131 P11 117.0(12) . . ?
B43 C131 B41 110.8(14) . . ?
B43 C131 B59 111.0(14) . . ?
B43 C131 B42 59.6(12) . . ?
B43 C131 B48 63.6(12) . . ?
B41 C131 P11 119.7(13) . . ?
B41 C131 B42 62.7(12) . . ?
B59 C131 P11 125.0(12) . . ?
B59 C131 B41 61.0(12) . . ?
B59 C131 B42 111.7(14) . . ?
B42 C131 P11 114.7(11) . . ?
B48 C131 P11 121.2(12) . . ?
B48 C131 B41 111.8(14) . . ?
B48 C131 B59 60.5(12) . . ?
B48 C131 B42 112.8(14) . . ?
C59 C60 H60 121.4 . . ?
C59 C60 C55 117(2) . . ?
C55 C60 H60 121.4 . . ?
C94 C95 H95 119.3 . . ?
C96 C95 C94 121(2) . . ?
C96 C95 H95 119.3 . . ?
C156 C155 P5 115.5(13) . . ?
C156 C155 C148 120.9(17) . . ?
C148 C155 P5 123.5(14) . . ?
C53 B24 H24 122.9 . . ?
C53 B24 B25 59.8(12) . . ?
C53 B24 B26 107.0(16) . . ?
C53 B24 B23 59.5(12) . . ?
C53 B24 B28 107.5(15) . . ?
B25 B24 H24 120.8 . . ?
B25 B24 B26 60.5(13) . . ?
B25 B24 B28 109.2(16) . . ?
B26 B24 H24 121.8 . . ?
B26 B24 B28 60.0(12) . . ?
B23 B24 H24 120.8 . . ?
B23 B24 B25 109.1(17) . . ?
B23 B24 B26 108.9(15) . . ?
B23 B24 B28 61.1(13) . . ?
B28 B24 H24 121.2 . . ?
C63 C62 H62 120.2 . . ?
C61 C62 C63 120(2) . . ?
C61 C62 H62 120.2 . . ?
C67 C72 H72 120.7 . . ?
C67 C72 C71 119(3) . . ?
C71 C72 H72 120.7 . . ?
C119 C120 H120 120.4 . . ?
C121 C120 C119 119(2) . . ?
C121 C120 H120 120.4 . . ?
C2 C1 P1 119.7(17) . . ?
C2 C1 C6 118(2) . . ?
C6 C1 P1 122.6(17) . . ?
C128 C127 H127 120.9 . . ?
C128 C127 C126 118(2) . . ?
C126 C127 H127 120.9 . . ?
C15 C16 H16 120.0 . . ?
C15 C16 C17 120.0 . . ?
C17 C16 H16 120.0 . . ?
C16 C15 P2 123.1(7) . . ?
C20 C15 P2 116.6(7) . . ?
C20 C15 C16 120.0 . . ?
C15 C20 H20 120.0 . . ?
C15 C20 C19 120.0 . . ?
C19 C20 H20 120.0 . . ?
C20 C19 H19 120.0 . . ?
C18 C19 C20 120.0 . . ?
C18 C19 H19 120.0 . . ?
C19 C18 H18 120.0 . . ?
C19 C18 C17 120.0 . . ?
C17 C18 H18 120.0 . . ?
C16 C17 H17 120.0 . . ?
C18 C17 C16 120.0 . . ?
C18 C17 H17 120.0 . . ?
C142 C143 H143 119.8 . . ?
C142 C143 C144 120(2) . . ?
C144 C143 H143 119.8 . . ?
C39 B8 H8 123.7 . . ?
C39 B8 B40 57.8(12) . . ?
C39 B8 B5 105.4(14) . . ?
C39 B8 B6 106.6(14) . . ?
C39 B8 B7 61.3(12) . . ?
B40 B8 H8 120.5 . . ?
B40 B8 B6 109.5(13) . . ?
B40 B8 B7 109.7(15) . . ?
B5 B8 H8 122.4 . . ?
B5 B8 B40 61.5(12) . . ?
B5 B8 B6 59.5(11) . . ?
B5 B8 B7 108.0(14) . . ?
B6 B8 H8 121.9 . . ?
B7 B8 H8 120.5 . . ?
B7 B8 B6 59.7(11) . . ?
C155 C156 H156 120.7 . . ?
C155 C156 C145 118.6(16) . . ?
C145 C156 H156 120.7 . . ?
C106 B53 H53 124.3 . . ?
C106 B53 B54 57.9(10) . . ?
C106 B53 B55 103.2(14) . . ?
B54 B53 H53 122.7 . . ?
B52 B53 H53 120.4 . . ?
B52 B53 C106 59.6(11) . . ?
B52 B53 B54 107.9(14) . . ?
B52 B53 B55 108.3(15) . . ?
B49 B53 H53 120.4 . . ?
B49 B53 C106 107.6(15) . . ?
B49 B53 B54 108.0(15) . . ?
B49 B53 B52 62.2(13) . . ?
B49 B53 B55 60.1(12) . . ?
B55 B53 H53 123.8 . . ?
B55 B53 B54 58.2(11) . . ?
C134 C133 P12 120.9(15) . . ?
C134 C133 C138 119(2) . . ?
C138 C133 P12 120.2(17) . . ?
C74 C73 P7 125.5(19) . . ?
C78 C73 P7 118.0(16) . . ?
C78 C73 C74 116(2) . . ?
C121 C122 H122 122.2 . . ?
C123 C122 C121 115.6(19) . . ?
C123 C122 H122 122.2 . . ?
C53 B25 B24 58.1(12) . . ?
C53 B25 H25 124.8 . . ?
C53 B25 B26 105.3(15) . . ?
C53 B25 B60 58.5(11) . . ?
C53 B25 C54 101.8(13) . . ?
B24 B25 H25 123.2 . . ?
B24 B25 B26 59.9(13) . . ?
B24 B25 B60 105.7(15) . . ?
B26 B25 H25 122.0 . . ?
B26 B25 B60 106.6(14) . . ?
B60 B25 H25 122.9 . . ?
C54 B25 B24 104.1(15) . . ?
C54 B25 H25 125.4 . . ?
C54 B25 B26 59.0(12) . . ?
C54 B25 B60 57.5(11) . . ?
B51 B50 H50A 121.2 . . ?
B51 B50 B49 107.9(15) . . ?
B51 B50 B57 107.9(14) . . ?
B52 B50 H50A 123.0 . . ?
B52 B50 B51 59.6(11) . . ?
B52 B50 B49 60.0(12) . . ?
B52 B50 B57 107.0(15) . . ?
B49 B50 H50A 122.8 . . ?
B57 B50 H50A 121.9 . . ?
B57 B50 B49 59.3(11) . . ?
C105 B50 H50A 125.5 . . ?
C105 B50 B51 58.8(10) . . ?
C105 B50 B52 103.5(14) . . ?
C105 B50 B49 103.4(14) . . ?
C105 B50 B57 58.2(11) . . ?
C152 C154 H154 119.4 . . ?
C151 C154 C152 121(2) . . ?
C151 C154 H154 119.4 . . ?
C155 C148 H148 120.9 . . ?
C147 C148 C155 118.1(19) . . ?
C147 C148 H148 120.9 . . ?
C63 C64 H64 118.3 . . ?
C63 C64 C65 123(2) . . ?
C65 C64 H64 118.3 . . ?
B45 C132 P12 119.9(12) . . ?
B46 C132 P12 113.7(12) . . ?
B46 C132 B45 62.6(12) . . ?
B47 C132 P12 123.9(14) . . ?
B47 C132 B45 62.7(12) . . ?
B47 C132 B46 114.1(15) . . ?
B47 C132 B42 116.5(15) . . ?
B41 C132 P12 117.9(14) . . ?
B41 C132 B45 115.4(14) . . ?
B41 C132 B46 115.2(15) . . ?
B41 C132 B47 62.6(12) . . ?
B41 C132 B42 65.5(13) . . ?
B42 C132 P12 111.3(12) . . ?
B42 C132 B45 114.5(16) . . ?
B42 C132 B46 61.0(12) . . ?
B4 C40 P4 122.8(12) . . ?
B4 C40 B40 110.6(14) . . ?
B4 C40 B9 60.9(12) . . ?
B40 C40 P4 115.0(11) . . ?
B1 C40 P4 118.8(13) . . ?
B1 C40 B4 112.3(15) . . ?
B1 C40 B40 61.4(11) . . ?
B1 C40 B5 111.1(14) . . ?
B1 C40 B9 63.3(12) . . ?
B5 C40 P4 116.9(12) . . ?
B5 C40 B4 61.3(11) . . ?
B5 C40 B40 60.4(11) . . ?
B5 C40 B9 111.3(14) . . ?
B9 C40 P4 124.0(13) . . ?
B9 C40 B40 112.5(14) . . ?
C42 C41 P4 117.0(16) . . ?
C42 C41 C46 117.4(19) . . ?
C46 C41 P4 125.5(19) . . ?
C133 C134 H134 119.1 . . ?
C135 C134 C133 122(2) . . ?
C135 C134 H134 119.1 . . ?
C34 C33 P3 116.5(17) . . ?
C38 C33 P3 125.5(16) . . ?
C38 C33 C34 118(2) . . ?
C81 C82 H82 119.4 . . ?
C83 C82 H82 119.4 . . ?
C83 C82 C81 121(2) . . ?
B53 C106 P10 122.9(13) . . ?
B51 C106 P10 117.6(11) . . ?
B51 C106 B53 110.6(14) . . ?
B51 C106 B52 61.2(11) . . ?
B54 C106 P10 117.4(13) . . ?
B54 C106 B53 62.5(11) . . ?
B54 C106 B51 114.0(14) . . ?
B54 C106 B52 111.4(14) . . ?
B52 C106 P10 123.0(13) . . ?
B52 C106 B53 59.3(11) . . ?
B58 C106 P10 114.7(12) . . ?
B58 C106 B53 112.9(13) . . ?
B58 C106 B51 63.3(11) . . ?
B58 C106 B54 62.5(11) . . ?
B58 C106 B52 112.6(15) . . ?
C28 C27 P3 115.9(15) . . ?
C32 C27 P3 123.0(15) . . ?
C32 C27 C28 121.1(18) . . ?
C12 C11 H11 121.6 . . ?
C12 C11 C10 117(2) . . ?
C10 C11 H11 121.6 . . ?
B46 B43 H43A 120.0 . . ?
B46 B43 B44 63.0(12) . . ?
B46 B43 B48 109.7(15) . . ?
C131 B43 B46 108.4(17) . . ?
C131 B43 H43A 123.2 . . ?
C131 B43 B42 61.6(13) . . ?
C131 B43 B44 105.9(15) . . ?
C131 B43 B48 58.4(12) . . ?
B42 B43 B46 60.8(13) . . ?
B42 B43 H43A 119.0 . . ?
B42 B43 B44 111.7(16) . . ?
B42 B43 B48 110.2(17) . . ?
B44 B43 H43A 121.1 . . ?
B44 B43 B48 58.7(11) . . ?
B48 B43 H43A 121.9 . . ?
C156 C145 H145 119.9 . . ?
C146 C145 C156 120.2(18) . . ?
C146 C145 H145 119.9 . . ?
C142 C141 H141 119.6 . . ?
C142 C141 C140 120.8(19) . . ?
C140 C141 H141 119.6 . . ?
B24 B26 B25 59.6(13) . . ?
B24 B26 H26 123.1 . . ?
B24 B26 B27 106.5(14) . . ?
B24 B26 B28 60.4(12) . . ?
B25 B26 H26 121.0 . . ?
B25 B26 B27 107.8(16) . . ?
C54 B26 B24 103.9(15) . . ?
C54 B26 B25 59.2(12) . . ?
C54 B26 H26 124.9 . . ?
C54 B26 B27 58.2(12) . . ?
C54 B26 B28 104.5(15) . . ?
B27 B26 H26 122.5 . . ?
B28 B26 B25 108.8(15) . . ?
B28 B26 H26 122.0 . . ?
B28 B26 B27 59.2(12) . . ?
C140 C139 P12 114.6(15) . . ?
C144 C139 P12 127.0(16) . . ?
C144 C139 C140 118.3(18) . . ?
B54 B56 H56A 122.5 . . ?
B54 B56 B57 107.5(15) . . ?
B54 B56 B58 59.5(11) . . ?
B55 B56 H56A 123.1 . . ?
B55 B56 B54 59.8(12) . . ?
B55 B56 B57 59.5(12) . . ?
B55 B56 B58 106.3(15) . . ?
B57 B56 H56A 122.0 . . ?
B57 B56 B58 106.3(14) . . ?
C105 B56 H56A 125.3 . . ?
C105 B56 B54 104.0(14) . . ?
C105 B56 B55 103.7(15) . . ?
C105 B56 B57 58.4(11) . . ?
C105 B56 B58 57.7(11) . . ?
B58 B56 H56A 122.8 . . ?
C21 C26 H26A 119.4 . . ?
C21 C26 C25 121(2) . . ?
C25 C26 H26A 119.4 . . ?
C48 C47 P4 114.6(19) . . ?
C52 C47 P4 126(2) . . ?
C52 C47 C48 119(2) . . ?
C148 C147 H147 118.6 . . ?
C148 C147 C146 123(2) . . ?
C146 C147 H147 118.6 . . ?
C133 C138 H138 121.1 . . ?
C137 C138 C133 118(2) . . ?
C137 C138 H138 121.1 . . ?
B45 B47 H47 120.1 . . ?
C132 B47 B45 60.9(12) . . ?
C132 B47 H47 124.3 . . ?
C132 B47 B41 57.9(12) . . ?
C132 B47 B59 104.5(15) . . ?
C132 B47 B39 106.0(17) . . ?
B41 B47 B45 109.9(16) . . ?
B41 B47 H47 120.6 . . ?
B41 B47 B39 109.0(16) . . ?
B59 B47 B45 108.2(17) . . ?
B59 B47 H47 122.7 . . ?
B59 B47 B41 61.0(12) . . ?
B59 B47 B39 59.2(13) . . ?
B39 B47 B45 60.3(13) . . ?
B39 B47 H47 122.0 . . ?
C29 C30 H30 119.1 . . ?
C29 C30 C31 121.7(19) . . ?
C31 C30 H30 119.1 . . ?
C87 C92 H92 119.7 . . ?
C87 C92 C91 121(3) . . ?
C91 C92 H92 119.7 . . ?
C145 C146 H146 120.4 . . ?
C147 C146 C145 119.1(19) . . ?
C147 C146 H146 120.4 . . ?
C13 B16 H16A 123.0 . . ?
C13 B16 B17 106.6(14) . . ?
C13 B16 B18 59.1(11) . . ?
C13 B16 B10 107.9(15) . . ?
C13 B16 B15 60.3(12) . . ?
B17 B16 H16A 121.6 . . ?
B17 B16 B10 61.0(12) . . ?
B17 B16 B15 109.4(16) . . ?
B18 B16 H16A 121.1 . . ?
B18 B16 B17 60.2(12) . . ?
B18 B16 B10 109.6(15) . . ?
B18 B16 B15 109.3(15) . . ?
B10 B16 H16A 120.8 . . ?
B15 B16 H16A 120.5 . . ?
B15 B16 B10 60.7(13) . . ?
C141 C140 C139 119(2) . . ?
C141 C140 H140 120.3 . . ?
C139 C140 H140 120.3 . . ?
C29 C28 C27 118(2) . . ?
C29 C28 H28 121.1 . . ?
C27 C28 H28 121.1 . . ?
C42 C43 H43 122.2 . . ?
C44 C43 H43 122.2 . . ?
C44 C43 C42 116(2) . . ?
C143 C144 C139 120(2) . . ?
C143 C144 H144 120.0 . . ?
C139 C144 H144 120.0 . . ?
B50 B51 H51A 121.4 . . ?
B50 B51 B58 107.5(14) . . ?
C106 B51 B50 105.8(14) . . ?
C106 B51 H51A 125.3 . . ?
C106 B51 B52 59.5(11) . . ?
C106 B51 B58 56.9(11) . . ?
B52 B51 B50 59.8(11) . . ?
B52 B51 H51A 122.6 . . ?
B52 B51 B58 106.1(15) . . ?
C105 B51 B50 59.4(11) . . ?
C105 B51 C106 100.5(14) . . ?
C105 B51 H51A 125.8 . . ?
C105 B51 B52 104.1(14) . . ?
C105 B51 B58 57.8(11) . . ?
B58 B51 H51A 122.9 . . ?
C93 C98 H98 120.7 . . ?
C93 C98 C97 119(2) . . ?
C97 C98 H98 120.7 . . ?
C41 C42 C43 122(2) . . ?
C41 C42 H42 119.1 . . ?
C43 C42 H42 119.1 . . ?
C50 C51 H51 121.6 . . ?
C50 C51 C52 117(3) . . ?
C52 C51 H51 121.6 . . ?
C27 C32 H32 121.1 . . ?
C27 C32 C31 117.8(19) . . ?
C31 C32 H32 121.1 . . ?
C78 C77 H77 121.5 . . ?
C78 C77 C76 117(2) . . ?
C76 C77 H77 121.5 . . ?
B13 B14 H14 119.0 . . ?
B13 B14 B11 110.8(15) . . ?
B13 B14 B10 111.4(15) . . ?
B13 B14 B15 62.3(13) . . ?
B13 B14 B12 61.4(12) . . ?
B11 B14 H14 121.2 . . ?
B11 B14 B10 59.9(12) . . ?
B10 B14 H14 120.7 . . ?
B15 B14 H14 120.5 . . ?
B15 B14 B11 108.9(16) . . ?
B15 B14 B10 60.4(13) . . ?
B15 B14 B12 110.9(16) . . ?
B12 B14 H14 120.0 . . ?
B12 B14 B11 61.1(12) . . ?
B12 B14 B10 110.1(15) . . ?
C53 B60 B25 57.5(12) . . ?
C53 B60 H60A 125.0 . . ?
C53 B60 B22 61.3(12) . . ?
B25 B60 H60A 121.7 . . ?
C54 B60 C53 101.5(16) . . ?
C54 B60 B25 58.2(11) . . ?
C54 B60 H60A 124.6 . . ?
C54 B60 B22 107.4(16) . . ?
B21 B60 C53 106.3(16) . . ?
B21 B60 B25 108.6(16) . . ?
B21 B60 H60A 121.2 . . ?
B21 B60 C54 60.2(12) . . ?
B21 B60 B22 60.3(12) . . ?
B22 B60 B25 109.6(17) . . ?
B22 B60 H60A 120.0 . . ?
C2 C3 H3 121.5 . . ?
C2 C3 C4 117(3) . . ?
C4 C3 H3 121.5 . . ?
C100 C99 P9 116.7(15) . . ?
C104 C99 P9 123.1(16) . . ?
C104 C99 C100 119.5(18) . . ?
C60 C59 H59 118.7 . . ?
C58 C59 C60 123(3) . . ?
C58 C59 H59 118.7 . . ?
C62 C61 P6 114.3(18) . . ?
C66 C61 P6 128.1(16) . . ?
C66 C61 C62 117.3(19) . . ?
C7 C8 H8A 121.1 . . ?
C9 C8 C7 118(2) . . ?
C9 C8 H8A 121.1 . . ?
C33 C34 H34 119.5 . . ?
C35 C34 C33 121(2) . . ?
C35 C34 H34 119.5 . . ?
C53 B23 B24 58.4(12) . . ?
C53 B23 H23 123.0 . . ?
C53 B23 B22 61.0(12) . . ?
C53 B23 B20 108.2(16) . . ?
C53 B23 B28 106.0(15) . . ?
B24 B23 H23 121.6 . . ?
B24 B23 B22 109.6(16) . . ?
B24 B23 B28 60.2(12) . . ?
B22 B23 H23 119.5 . . ?
B22 B23 B28 109.6(15) . . ?
B20 B23 B24 108.4(15) . . ?
B20 B23 H23 121.2 . . ?
B20 B23 B22 61.9(13) . . ?
B20 B23 B28 59.4(12) . . ?
B28 B23 H23 122.3 . . ?
C24 C23 H23A 120.4 . . ?
C24 C23 C22 119(2) . . ?
C22 C23 H23A 120.4 . . ?
B32 C79 P7 115.1(15) . . ?
B32 C79 B33 62.9(16) . . ?
B32 C79 B31 64.4(16) . . ?
B32 C79 B30 116(2) . . ?
B32 C79 B36 116(2) . . ?
B33 C79 P7 112.4(18) . . ?
B33 C79 B31 118(2) . . ?
B33 C79 B30 117(2) . . ?
B31 C79 P7 117.5(17) . . ?
B31 C79 B30 63.5(17) . . ?
B30 C79 P7 120.5(18) . . ?
B36 C79 P7 117.9(17) . . ?
B36 C79 B33 65.7(19) . . ?
B36 C79 B31 115(2) . . ?
B36 C79 B30 60.4(18) . . ?
C127 C128 H128 118.1 . . ?
C127 C128 C129 124(2) . . ?
C129 C128 H128 118.1 . . ?
C14 B17 B16 105.5(15) . . ?
C14 B17 H17A 123.4 . . ?
C14 B17 B18 58.9(11) . . ?
C14 B17 B11 59.6(11) . . ?
C14 B17 B10 106.8(14) . . ?
B16 B17 H17A 122.6 . . ?
B16 B17 B18 59.8(12) . . ?
B16 B17 B11 107.1(15) . . ?
B16 B17 B10 60.4(12) . . ?
B18 B17 H17A 121.5 . . ?
B18 B17 B11 107.8(14) . . ?
B18 B17 B10 108.9(16) . . ?
B11 B17 H17A 122.0 . . ?
B10 B17 H17A 121.4 . . ?
B10 B17 B11 59.6(11) . . ?
C23 C24 H24A 119.4 . . ?
C25 C24 C23 121(2) . . ?
C25 C24 H24A 119.4 . . ?
C85 C84 H84 119.4 . . ?
C83 C84 H84 119.4 . . ?
C83 C84 C85 121.2(19) . . ?
C38 C37 H37 118.6 . . ?
C36 C37 H37 118.6 . . ?
C36 C37 C38 123(2) . . ?
C84 C85 H85 120.3 . . ?
C86 C85 C84 119(2) . . ?
C86 C85 H85 120.3 . . ?
C26 C21 P2 120.0(16) . . ?
C26 C21 C22 118.9(19) . . ?
C22 C21 P2 121.1(15) . . ?
C119 C124 H124 120.8 . . ?
C119 C124 C123 118.4(19) . . ?
C123 C124 H124 120.8 . . ?
C1 C2 C3 125(3) . . ?
C1 C2 H2 117.3 . . ?
C3 C2 H2 117.3 . . ?
B53 B54 H54 122.0 . . ?
C106 B54 B53 59.5(11) . . ?
C106 B54 B56 105.9(14) . . ?
C106 B54 H54 123.9 . . ?
C106 B54 B55 105.7(14) . . ?
C106 B54 B58 57.3(11) . . ?
B56 B54 B53 107.4(15) . . ?
B56 B54 H54 121.9 . . ?
B56 B54 B58 61.1(11) . . ?
B55 B54 B53 59.9(12) . . ?
B55 B54 B56 59.0(12) . . ?
B55 B54 H54 122.7 . . ?
B55 B54 B58 107.0(15) . . ?
B58 B54 B53 106.3(14) . . ?
B58 B54 H54 122.6 . . ?
C51 C50 H50 118.2 . . ?
C51 C50 C49 124(2) . . ?
C49 C50 H50 118.2 . . ?
B25 C54 P6 110.8(12) . . ?
B26 C54 P6 115.1(11) . . ?
B26 C54 B25 61.8(12) . . ?
B60 C54 P6 117.0(14) . . ?
B60 C54 B25 64.3(12) . . ?
B60 C54 B26 114.3(14) . . ?
B21 C54 P6 125.3(13) . . ?
B21 C54 B25 112.8(13) . . ?
B21 C54 B26 113.8(15) . . ?
B21 C54 B60 59.4(11) . . ?
B27 C54 P6 124.0(12) . . ?
B27 C54 B25 113.6(15) . . ?
B27 C54 B26 62.7(12) . . ?
B27 C54 B60 112.1(14) . . ?
B27 C54 B21 62.7(12) . . ?
B60 B21 C54 60.4(11) . . ?
B60 B21 H21 120.0 . . ?
B60 B21 B22 61.4(12) . . ?
B60 B21 B27 109.5(16) . . ?
B60 B21 B20 109.5(16) . . ?
C54 B21 H21 123.7 . . ?
C54 B21 B22 108.3(14) . . ?
C54 B21 B27 58.6(12) . . ?
C54 B21 B20 104.7(16) . . ?
B22 B21 H21 119.7 . . ?
B22 B21 B27 110.3(17) . . ?
B22 B21 B20 61.7(13) . . ?
B27 B21 H21 121.3 . . ?
B27 B21 B20 59.2(13) . . ?
B20 B21 H21 122.4 . . ?
C43 C44 H44 117.9 . . ?
C45 C44 C43 124(2) . . ?
C45 C44 H44 117.9 . . ?
C60 C55 P6 118.2(18) . . ?
C60 C55 C56 122(2) . . ?
C56 C55 P6 120(2) . . ?
B53 B52 B50 108.7(15) . . ?
B53 B52 C106 61.0(11) . . ?
B53 B52 B51 110.5(14) . . ?
B53 B52 H52A 120.6 . . ?
B53 B52 B49 58.6(12) . . ?
B50 B52 H52A 121.7 . . ?
B50 B52 B49 60.9(12) . . ?
C106 B52 B50 106.3(14) . . ?
C106 B52 B51 59.3(10) . . ?
C106 B52 H52A 123.3 . . ?
C106 B52 B49 105.9(14) . . ?
B51 B52 B50 60.6(11) . . ?
B51 B52 H52A 120.2 . . ?
B51 B52 B49 109.4(14) . . ?
B49 B52 H52A 122.3 . . ?
C26 C25 H25A 119.9 . . ?
C24 C25 C26 120(2) . . ?
C24 C25 H25A 119.9 . . ?
C131 B41 B47 105.7(16) . . ?
C131 B41 H41 124.2 . . ?
C131 B41 B59 59.1(12) . . ?
C131 B41 B42 59.3(12) . . ?
C132 B41 C131 102.8(16) . . ?
C132 B41 B47 59.5(11) . . ?
C132 B41 H41 125.0 . . ?
C132 B41 B59 104.1(15) . . ?
C132 B41 B42 58.4(12) . . ?
B47 B41 H41 121.9 . . ?
B47 B41 B59 58.9(12) . . ?
B47 B41 B42 108.2(16) . . ?
B59 B41 H41 123.0 . . ?
B59 B41 B42 107.4(17) . . ?
B42 B41 H41 121.4 . . ?
C53 B22 B23 57.1(11) . . ?
C53 B22 H22 126.0 . . ?
C53 B22 B20 101.8(15) . . ?
B60 B22 C53 59.0(11) . . ?
B60 B22 B23 105.9(15) . . ?
B60 B22 H22 122.3 . . ?
B60 B22 B20 106.5(15) . . ?
B23 B22 H22 123.6 . . ?
B23 B22 B20 57.5(12) . . ?
B21 B22 C53 103.0(14) . . ?
B21 B22 B60 58.3(12) . . ?
B21 B22 B23 105.7(16) . . ?
B21 B22 H22 123.1 . . ?
B21 B22 B20 60.9(13) . . ?
B20 B22 H22 123.6 . . ?
C131 B59 B41 59.9(12) . . ?
C131 B59 H59A 123.0 . . ?
C131 B59 B48 59.6(12) . . ?
B47 B59 C131 107.3(14) . . ?
B47 B59 B41 60.1(12) . . ?
B47 B59 H59A 120.9 . . ?
B47 B59 B39 61.5(13) . . ?
B47 B59 B48 111.0(16) . . ?
B41 B59 H59A 120.7 . . ?
B39 B59 C131 108.0(16) . . ?
B39 B59 B41 110.1(15) . . ?
B39 B59 H59A 120.3 . . ?
B39 B59 B48 61.6(13) . . ?
B48 B59 B41 110.1(15) . . ?
B48 B59 H59A 119.8 . . ?
C40 B4 H4 122.8 . . ?
C40 B4 B5 59.3(11) . . ?
C40 B4 B6 108.3(14) . . ?
C40 B4 B3 106.3(15) . . ?
C40 B4 B9 60.1(12) . . ?
B5 B4 H4 122.3 . . ?
B6 B4 H4 120.0 . . ?
B6 B4 B5 60.1(11) . . ?
B6 B4 B3 60.6(12) . . ?
B6 B4 B9 111.5(16) . . ?
B3 B4 H4 122.7 . . ?
B3 B4 B5 106.7(14) . . ?
B3 B4 B9 60.8(13) . . ?
B9 B4 H4 119.7 . . ?
B9 B4 B5 109.0(15) . . ?
C39 B40 B8 59.3(12) . . ?
C39 B40 C40 104.3(14) . . ?
C39 B40 H40 123.5 . . ?
C39 B40 B1 61.8(12) . . ?
C39 B40 B5 104.5(14) . . ?
B8 B40 C40 106.2(14) . . ?
B8 B40 H40 121.3 . . ?
B8 B40 B1 110.6(15) . . ?
B8 B40 B5 59.0(11) . . ?
C40 B40 H40 124.3 . . ?
C40 B40 B1 58.1(11) . . ?
B1 B40 H40 120.2 . . ?
B5 B40 C40 59.1(10) . . ?
B5 B40 H40 123.4 . . ?
B5 B40 B1 107.4(14) . . ?
C125 C126 C127 122.0(19) . . ?
C125 C126 H126 119.0 . . ?
C127 C126 H126 119.0 . . ?
C47 C52 C51 124(3) . . ?
C47 C52 H52 118.1 . . ?
C51 C52 H52 118.1 . . ?
C80 B32 H32A 124.4 . . ?
C80 B32 B33 107.1(19) . . ?
C80 B32 B34 58.1(16) . . ?
C80 B32 B31 61.8(16) . . ?
C79 B32 C80 103.8(19) . . ?
C79 B32 H32A 124.2 . . ?
C79 B32 B33 59.2(17) . . ?
C79 B32 B34 108.7(19) . . ?
C79 B32 B31 59.4(16) . . ?
B33 B32 H32A 120.2 . . ?
B33 B32 B34 63.4(17) . . ?
B33 B32 B31 111(2) . . ?
B34 B32 H32A 119.4 . . ?
B34 B32 B31 112(2) . . ?
B31 B32 H32A 118.7 . . ?
C118 C113 P10 118.5(15) . . ?
C114 C113 P10 119.8(16) . . ?
C114 C113 C118 121.7(19) . . ?
C153 C149 H149 121.2 . . ?
C150 C149 C153 117.6(18) . . ?
C150 C149 H149 121.2 . . ?
C122 C123 C124 124(2) . . ?
C122 C123 H123 117.9 . . ?
C124 C123 H123 117.9 . . ?
C125 C130 H130 119.9 . . ?
C129 C130 C125 120.3(18) . . ?
C129 C130 H130 119.9 . . ?
C98 C97 H97 120.8 . . ?
C96 C97 C98 118(2) . . ?
C96 C97 H97 120.8 . . ?
C39 B1 B40 55.3(11) . . ?
C39 B1 H1 126.2 . . ?
C39 B1 B2 58.6(11) . . ?
C39 B1 B9 104.8(15) . . ?
C40 B1 C39 101.2(14) . . ?
C40 B1 B40 60.4(11) . . ?
C40 B1 H1 124.5 . . ?
C40 B1 B2 103.9(15) . . ?
C40 B1 B9 59.3(11) . . ?
B40 B1 H1 122.6 . . ?
B40 B1 B2 104.4(15) . . ?
B40 B1 B9 108.5(15) . . ?
B2 B1 H1 123.8 . . ?
B2 B1 B9 59.2(12) . . ?
B9 B1 H1 121.5 . . ?
C13 B18 B16 60.1(11) . . ?
C13 B18 B17 107.2(14) . . ?
C13 B18 H18A 123.8 . . ?
C13 B18 B19 57.4(11) . . ?
C14 B18 C13 104.3(14) . . ?
C14 B18 B16 106.0(14) . . ?
C14 B18 B17 59.5(11) . . ?
C14 B18 H18A 123.4 . . ?
C14 B18 B19 60.4(12) . . ?
B16 B18 B17 60.0(12) . . ?
B16 B18 H18A 122.2 . . ?
B16 B18 B19 107.1(15) . . ?
B17 B18 H18A 121.1 . . ?
B17 B18 B19 109.0(14) . . ?
B19 B18 H18A 121.8 . . ?
C111 C110 H110 121.0 . . ?
C111 C110 C109 118.0(19) . . ?
C109 C110 H110 121.0 . . ?
C34 C35 H35 120.1 . . ?
C36 C35 C34 120(2) . . ?
C36 C35 H35 120.1 . . ?
C33 C38 C37 119(2) . . ?
C33 C38 H38 120.6 . . ?
C37 C38 H38 120.6 . . ?
C154 C151 H151 120.1 . . ?
C150 C151 C154 120(2) . . ?
C150 C151 H151 120.1 . . ?
C73 C74 H74 120.2 . . ?
C75 C74 C73 120(2) . . ?
C75 C74 H74 120.2 . . ?
C104 C103 H103 118.4 . . ?
C102 C103 C104 123(2) . . ?
C102 C103 H103 118.4 . . ?
C117 C116 H116 119.7 . . ?
C117 C116 C115 121(2) . . ?
C115 C116 H116 119.7 . . ?
C72 C67 P7 114(2) . . ?
C68 C67 P7 121(2) . . ?
C68 C67 C72 124(2) . . ?
C108 C107 P10 124.7(17) . . ?
C112 C107 P10 117.3(17) . . ?
C112 C107 C108 117.9(19) . . ?
C113 C114 H114 121.5 . . ?
C113 C114 C115 117(2) . . ?
C115 C114 H114 121.5 . . ?
C110 C111 H111 118.6 . . ?
C112 C111 C110 123(2) . . ?
C112 C111 H111 118.6 . . ?
C14 B11 B14 104.9(15) . . ?
C14 B11 B17 57.5(10) . . ?
C14 B11 H11A 124.5 . . ?
C14 B11 B10 105.2(14) . . ?
C14 B11 B12 60.5(11) . . ?
B14 B11 B17 107.2(16) . . ?
B14 B11 H11A 122.7 . . ?
B14 B11 B10 61.2(13) . . ?
B14 B11 B12 59.3(12) . . ?
B17 B11 H11A 122.5 . . ?
B10 B11 B17 59.6(12) . . ?
B10 B11 H11A 121.3 . . ?
B10 B11 B12 109.7(16) . . ?
B12 B11 B17 108.2(14) . . ?
B12 B11 H11A 120.5 . . ?
C8 C9 H9 118.5 . . ?
C10 C9 C8 123(3) . . ?
C10 C9 H9 118.5 . . ?
C107 C108 H108 119.0 . . ?
C109 C108 C107 122(2) . . ?
C109 C108 H108 119.0 . . ?
B16 B10 B14 104.7(15) . . ?
B16 B10 B17 58.6(12) . . ?
B16 B10 B11 106.5(14) . . ?
B16 B10 H10 123.3 . . ?
B16 B10 B15 59.5(13) . . ?
B14 B10 H10 123.9 . . ?
B17 B10 B14 106.2(14) . . ?
B17 B10 H10 122.2 . . ?
B17 B10 B15 106.6(15) . . ?
B11 B10 B14 58.9(12) . . ?
B11 B10 B17 60.7(11) . . ?
B11 B10 H10 122.1 . . ?
B11 B10 B15 106.3(15) . . ?
B15 B10 B14 58.2(13) . . ?
B15 B10 H10 122.8 . . ?
C30 C31 C32 119(2) . . ?
C30 C31 H31 120.3 . . ?
C32 C31 H31 120.3 . . ?
C7 C12 C11 121(2) . . ?
C7 C12 H12 119.4 . . ?
C11 C12 H12 119.4 . . ?
C118 C117 H117 120.2 . . ?
C116 C117 C118 120(2) . . ?
C116 C117 H117 120.2 . . ?
B26 B27 H27 121.9 . . ?
C54 B27 B26 59.0(12) . . ?
C54 B27 B21 58.7(12) . . ?
C54 B27 H27 123.7 . . ?
C54 B27 B20 106.3(15) . . ?
C54 B27 B28 105.8(14) . . ?
B21 B27 B26 107.6(15) . . ?
B21 B27 H27 121.4 . . ?
B20 B27 B26 107.7(15) . . ?
B20 B27 B21 61.0(13) . . ?
B20 B27 H27 121.9 . . ?
B28 B27 B26 59.9(12) . . ?
B28 B27 B21 108.1(15) . . ?
B28 B27 H27 122.3 . . ?
B28 B27 B20 59.5(13) . . ?
C13 B19 C14 102.8(14) . . ?
C13 B19 B13 61.7(11) . . ?
C13 B19 B18 58.8(11) . . ?
C13 B19 H19A 123.2 . . ?
C13 B19 B12 107.9(14) . . ?
C14 B19 B13 106.4(14) . . ?
C14 B19 B18 57.1(11) . . ?
C14 B19 H19A 125.0 . . ?
C14 B19 B12 60.3(11) . . ?
B13 B19 B18 109.2(14) . . ?
B13 B19 H19A 120.6 . . ?
B13 B19 B12 59.8(11) . . ?
B18 B19 H19A 122.1 . . ?
B12 B19 B18 107.9(14) . . ?
B12 B19 H19A 121.1 . . ?
B46 B42 C131 105.3(15) . . ?
B46 B42 B41 107.2(14) . . ?
B46 B42 H42A 121.2 . . ?
C131 B42 B41 58.0(11) . . ?
C131 B42 H42A 125.6 . . ?
C132 B42 B46 60.7(12) . . ?
C132 B42 C131 100.0(14) . . ?
C132 B42 B43 104.5(15) . . ?
C132 B42 B41 56.1(12) . . ?
C132 B42 H42A 125.9 . . ?
B43 B42 B46 59.7(13) . . ?
B43 B42 C131 58.7(12) . . ?
B43 B42 B41 106.2(15) . . ?
B43 B42 H42A 122.6 . . ?
B41 B42 H42A 123.1 . . ?
C11 C10 H10A 119.0 . . ?
C9 C10 C11 122(2) . . ?
C9 C10 H10A 119.0 . . ?
C103 C102 H102 120.6 . . ?
C103 C102 C101 118.9(18) . . ?
C101 C102 H102 120.6 . . ?
C89 C88 H88 119.4 . . ?
C87 C88 H88 119.4 . . ?
C87 C88 C89 121(3) . . ?
C107 C112 C111 119(2) . . ?
C107 C112 H112 120.4 . . ?
C111 C112 H112 120.4 . . ?
C85 C86 H86 120.0 . . ?
C85 C86 C81 120(2) . . ?
C81 C86 H86 120.0 . . ?
B53 B49 B50 107.7(15) . . ?
B53 B49 B52 59.2(12) . . ?
B53 B49 H49A 120.9 . . ?
B53 B49 B55 61.5(12) . . ?
B53 B49 B57 109.2(15) . . ?
B50 B49 H49A 122.3 . . ?
B52 B49 B50 59.1(12) . . ?
B52 B49 H49A 123.0 . . ?
B55 B49 B50 107.1(14) . . ?
B55 B49 B52 107.0(15) . . ?
B55 B49 H49A 121.9 . . ?
B55 B49 B57 59.4(12) . . ?
B57 B49 B50 60.0(12) . . ?
B57 B49 B52 106.9(14) . . ?
B57 B49 H49A 121.7 . . ?
C44 C45 H45 121.5 . . ?
C44 C45 C46 117(2) . . ?
C46 C45 H45 121.5 . . ?
C128 C129 C130 117(2) . . ?
C128 C129 H129 121.4 . . ?
C130 C129 H129 121.4 . . ?
C110 C109 H109 120.3 . . ?
C108 C109 C110 119(2) . . ?
C108 C109 H109 120.3 . . ?
B8 B5 C40 107.8(14) . . ?
B8 B5 B4 109.9(15) . . ?
B8 B5 B40 59.6(11) . . ?
B8 B5 H5 120.4 . . ?
B8 B5 B6 63.6(12) . . ?
C40 B5 B4 59.4(11) . . ?
C40 B5 B40 60.5(11) . . ?
C40 B5 H5 122.7 . . ?
C40 B5 B6 107.8(14) . . ?
B4 B5 H5 121.6 . . ?
B40 B5 B4 109.1(15) . . ?
B40 B5 H5 120.5 . . ?
B40 B5 B6 111.2(15) . . ?
B6 B5 B4 59.4(12) . . ?
B6 B5 H5 119.9 . . ?
C59 C58 H58 118.9 . . ?
C59 C58 C57 122(2) . . ?
C57 C58 H58 118.9 . . ?
B23 B20 B21 105.4(15) . . ?
B23 B20 B22 60.7(13) . . ?
B23 B20 B27 108.4(15) . . ?
B23 B20 H20A 121.6 . . ?
B23 B20 B28 62.0(13) . . ?
B21 B20 B22 57.4(12) . . ?
B21 B20 H20A 124.0 . . ?
B22 B20 H20A 121.5 . . ?
B27 B20 B21 59.9(13) . . ?
B27 B20 B22 107.4(16) . . ?
B27 B20 H20A 121.9 . . ?
B28 B20 B21 107.6(15) . . ?
B28 B20 B22 110.7(15) . . ?
B28 B20 B27 59.9(13) . . ?
B28 B20 H20A 120.0 . . ?
C137 C136 H136 119.2 . . ?
C135 C136 H136 119.2 . . ?
C135 C136 C137 122(3) . . ?
C95 C96 C97 121(2) . . ?
C95 C96 H96 119.4 . . ?
C97 C96 H96 119.4 . . ?
C88 C89 H89 119.9 . . ?
C90 C89 C88 120(3) . . ?
C90 C89 H89 119.9 . . ?
B45 B44 H44A 122.2 . . ?
B46 B44 B45 59.9(12) . . ?
B46 B44 H44A 122.9 . . ?
B43 B44 B45 106.4(16) . . ?
B43 B44 B46 57.6(11) . . ?
B43 B44 H44A 122.3 . . ?
B43 B44 B39 108.0(16) . . ?
B39 B44 B45 59.4(12) . . ?
B39 B44 B46 106.8(17) . . ?
B39 B44 H44A 122.1 . . ?
B48 B44 B45 108.3(17) . . ?
B48 B44 B46 107.9(15) . . ?
B48 B44 B43 61.9(12) . . ?
B48 B44 H44A 120.5 . . ?
B48 B44 B39 60.2(12) . . ?
B53 B55 H55 121.6 . . ?
B56 B55 B53 110.8(14) . . ?
B56 B55 B54 61.2(12) . . ?
B56 B55 B49 111.3(15) . . ?
B56 B55 H55 119.1 . . ?
B56 B55 B57 61.8(12) . . ?
B54 B55 B53 62.0(11) . . ?
B54 B55 B49 109.8(14) . . ?
B54 B55 H55 119.9 . . ?
B54 B55 B57 110.4(14) . . ?
B49 B55 B53 58.4(12) . . ?
B49 B55 H55 121.0 . . ?
B57 B55 B53 107.9(15) . . ?
B57 B55 B49 60.9(13) . . ?
B57 B55 H55 120.9 . . ?
C138 C137 C136 120(3) . . ?
C138 C137 H137 119.9 . . ?
C136 C137 H137 119.9 . . ?
B8 B6 H6 124.4 . . ?
B4 B6 B8 105.4(14) . . ?
B4 B6 B5 60.5(11) . . ?
B4 B6 H6 121.7 . . ?
B4 B6 B3 59.9(12) . . ?
B4 B6 B7 107.6(16) . . ?
B5 B6 B8 56.8(10) . . ?
B5 B6 H6 123.3 . . ?
B5 B6 B3 106.4(15) . . ?
B5 B6 B7 105.5(14) . . ?
B3 B6 B8 105.0(15) . . ?
B3 B6 H6 122.8 . . ?
B3 B6 B7 59.2(12) . . ?
B7 B6 B8 59.4(11) . . ?
B7 B6 H6 122.3 . . ?
C23 C22 C21 119.3(19) . . ?
C23 C22 H22A 120.4 . . ?
C21 C22 H22A 120.4 . . ?
C149 C150 H150 119.5 . . ?
C151 C150 C149 121(2) . . ?
C151 C150 H150 119.5 . . ?
C37 C36 C35 119(2) . . ?
C37 C36 H36 120.3 . . ?
C35 C36 H36 120.3 . . ?
B24 B28 B23 58.7(12) . . ?
B24 B28 H28A 122.9 . . ?
B26 B28 B24 59.6(12) . . ?
B26 B28 B23 106.7(16) . . ?
B26 B28 H28A 121.0 . . ?
B23 B28 H28A 123.6 . . ?
B27 B28 B24 107.2(17) . . ?
B27 B28 B26 60.9(13) . . ?
B27 B28 B23 106.2(17) . . ?
B27 B28 H28A 121.8 . . ?
B20 B28 B24 106.5(16) . . ?
B20 B28 B26 109.3(17) . . ?
B20 B28 B23 58.6(12) . . ?
B20 B28 B27 60.6(13) . . ?
B20 B28 H28A 121.6 . . ?
B50 B57 H57A 120.5 . . ?
B56 B57 B50 109.2(14) . . ?
B56 B57 H57A 121.5 . . ?
B49 B57 B50 60.8(12) . . ?
B49 B57 B56 107.8(15) . . ?
B49 B57 H57A 122.0 . . ?
B55 B57 B50 107.9(15) . . ?
B55 B57 B56 58.7(12) . . ?
B55 B57 B49 59.7(13) . . ?
B55 B57 H57A 123.6 . . ?
C105 B57 B50 59.5(11) . . ?
C105 B57 B56 59.1(11) . . ?
C105 B57 B49 105.6(14) . . ?
C105 B57 B55 103.5(14) . . ?
C105 B57 H57A 124.5 . . ?
B50 C105 P9 122.5(13) . . ?
B56 C105 P9 113.8(12) . . ?
B56 C105 B50 114.2(13) . . ?
B56 C105 B51 115.5(15) . . ?
B51 C105 P9 119.6(11) . . ?
B51 C105 B50 61.8(11) . . ?
B57 C105 P9 118.9(13) . . ?
B57 C105 B50 62.2(11) . . ?
B57 C105 B56 62.5(12) . . ?
B57 C105 B51 113.7(14) . . ?
B58 C105 P9 115.2(11) . . ?
B58 C105 B50 113.6(14) . . ?
B58 C105 B56 63.2(11) . . ?
B58 C105 B51 62.9(11) . . ?
B58 C105 B57 114.1(14) . . ?
B45 B39 H39 119.8 . . ?
B47 B39 B45 61.1(13) . . ?
B47 B39 B44 109.1(15) . . ?
B47 B39 H39 121.6 . . ?
B47 B39 B48 107.6(15) . . ?
B59 B39 B45 108.8(15) . . ?
B59 B39 B47 59.2(13) . . ?
B59 B39 B44 107.1(15) . . ?
B59 B39 H39 122.5 . . ?
B59 B39 B48 59.6(13) . . ?
B44 B39 B45 61.9(13) . . ?
B44 B39 H39 121.5 . . ?
B48 B39 B45 109.5(15) . . ?
B48 B39 B44 59.1(12) . . ?
B48 B39 H39 122.0 . . ?
C41 C46 H46 118.1 . . ?
C45 C46 C41 124(2) . . ?
C45 C46 H46 118.1 . . ?
C73 C78 C77 123(2) . . ?
C73 C78 H78 118.7 . . ?
C77 C78 H78 118.7 . . ?
C74 C75 H75 119.7 . . ?
C76 C75 C74 121(2) . . ?
C76 C75 H75 119.7 . . ?
C92 C87 P8 124.8(19) . . ?
C88 C87 P8 118.5(19) . . ?
C88 C87 C92 117(2) . . ?
C39 B2 B1 59.1(11) . . ?
C39 B2 H2A 124.0 . . ?
C39 B2 B9 106.3(16) . . ?
C39 B2 B7 60.3(11) . . ?
B1 B2 H2A 120.5 . . ?
B3 B2 C39 105.9(16) . . ?
B3 B2 B1 109.4(17) . . ?
B3 B2 H2A 121.8 . . ?
B3 B2 B9 61.0(13) . . ?
B3 B2 B7 60.6(12) . . ?
B9 B2 B1 60.7(12) . . ?
B9 B2 H2A 120.9 . . ?
B7 B2 B1 110.7(15) . . ?
B7 B2 H2A 119.4 . . ?
B7 B2 B9 111.0(17) . . ?
B4 B3 B6 59.4(12) . . ?
B4 B3 H3A 122.6 . . ?
B4 B3 B9 59.8(13) . . ?
B4 B3 B7 109.0(15) . . ?
B6 B3 H3A 120.8 . . ?
B6 B3 B9 109.7(15) . . ?
B2 B3 B4 108.0(16) . . ?
B2 B3 B6 110.0(15) . . ?
B2 B3 H3A 120.7 . . ?
B2 B3 B9 61.6(13) . . ?
B2 B3 B7 61.4(12) . . ?
B9 B3 H3A 119.8 . . ?
B7 B3 B6 61.5(12) . . ?
B7 B3 H3A 119.5 . . ?
B7 B3 B9 112.0(15) . . ?
C106 B58 B56 106.8(13) . . ?
C106 B58 B51 59.7(11) . . ?
C106 B58 B54 60.1(11) . . ?
C106 B58 C105 103.8(14) . . ?
C106 B58 H58A 123.4 . . ?
B56 B58 H58A 121.7 . . ?
B51 B58 B56 109.0(14) . . ?
B51 B58 H58A 120.5 . . ?
B54 B58 B56 59.4(11) . . ?
B54 B58 B51 109.2(14) . . ?
B54 B58 H58A 122.0 . . ?
C105 B58 B56 59.1(11) . . ?
C105 B58 B51 59.3(11) . . ?
C105 B58 B54 105.0(13) . . ?
C105 B58 H58A 124.8 . . ?
C64 C65 H65 121.9 . . ?
C64 C65 C66 116(2) . . ?
C66 C65 H65 121.9 . . ?
C6 C5 H5A 120.3 . . ?
C4 C5 H5A 120.3 . . ?
C4 C5 C6 119(3) . . ?
C89 C90 H90 119.2 . . ?
C89 C90 C91 122(3) . . ?
C91 C90 H90 119.2 . . ?
C134 C135 H135 120.2 . . ?
C136 C135 C134 120(3) . . ?
C136 C135 H135 120.2 . . ?
C40 B9 B4 59.0(11) . . ?
C40 B9 B1 57.3(11) . . ?
C40 B9 B2 103.1(15) . . ?
C40 B9 B3 104.4(15) . . ?
C40 B9 H9A 124.8 . . ?
B4 B9 B1 106.0(15) . . ?
B4 B9 B2 104.4(16) . . ?
B4 B9 B3 59.3(13) . . ?
B4 B9 H9A 122.9 . . ?
B1 B9 H9A 122.5 . . ?
B2 B9 B1 60.1(12) . . ?
B2 B9 H9A 124.4 . . ?
B3 B9 B1 106.1(16) . . ?
B3 B9 B2 57.4(12) . . ?
B3 B9 H9A 123.4 . . ?
C82 C81 P8 116.8(17) . . ?
C82 C81 C86 119(2) . . ?
C86 C81 P8 123.9(17) . . ?
C82 C83 C84 119(2) . . ?
C82 C83 H83 120.6 . . ?
C84 C83 H83 120.6 . . ?
C100 C101 C102 117.4(19) . . ?
C100 C101 H101 121.3 . . ?
C102 C101 H101 121.3 . . ?
C79 B33 B32 57.8(15) . . ?
C79 B33 H33 126.6 . . ?
C79 B33 B34 104(2) . . ?
C79 B33 B36 57.1(17) . . ?
C79 B33 B35 100(2) . . ?
B32 B33 H33 123.3 . . ?
B32 B33 B34 59.0(15) . . ?
B32 B33 B36 105(2) . . ?
B32 B33 B35 105(2) . . ?
B34 B33 H33 121.1 . . ?
B36 B33 H33 123.3 . . ?
B36 B33 B34 108(2) . . ?
B35 B33 H33 124.6 . . ?
B35 B33 B34 62.0(18) . . ?
B35 B33 B36 56.8(18) . . ?
C13 B15 B13 60.0(11) . . ?
C13 B15 B16 58.6(11) . . ?
C13 B15 B10 105.9(15) . . ?
C13 B15 H15 124.2 . . ?
B13 B15 H15 121.4 . . ?
B16 B15 B13 108.3(15) . . ?
B16 B15 B10 59.8(13) . . ?
B16 B15 H15 121.8 . . ?
B14 B15 C13 104.2(15) . . ?
B14 B15 B13 58.1(13) . . ?
B14 B15 B16 107.4(17) . . ?
B14 B15 B10 61.4(13) . . ?
B14 B15 H15 123.2 . . ?
B10 B15 B13 108.9(16) . . ?
B10 B15 H15 121.2 . . ?
C55 C56 H56 121.7 . . ?
C57 C56 C55 117(2) . . ?
C57 C56 H56 121.7 . . ?
C131 B48 B43 58.0(12) . . ?
C131 B48 B59 59.8(12) . . ?
C131 B48 B44 106.1(15) . . ?
C131 B48 B39 105.8(16) . . ?
C131 B48 H48A 123.3 . . ?
B43 B48 H48A 123.2 . . ?
B59 B48 B43 106.0(16) . . ?
B59 B48 B44 107.6(16) . . ?
B59 B48 B39 58.7(13) . . ?
B59 B48 H48A 122.4 . . ?
B44 B48 B43 59.4(12) . . ?
B44 B48 B39 60.7(12) . . ?
B44 B48 H48A 121.7 . . ?
B39 B48 B43 106.5(14) . . ?
B39 B48 H48A 122.6 . . ?
C1 C6 C5 119(2) . . ?
C1 C6 H6A 120.5 . . ?
C5 C6 H6A 120.5 . . ?
C39 B7 B8 55.5(11) . . ?
C39 B7 B6 103.1(14) . . ?
C39 B7 B2 58.9(11) . . ?
C39 B7 H7 126.0 . . ?
B8 B7 B6 60.9(11) . . ?
B8 B7 H7 123.2 . . ?
B6 B7 H7 122.7 . . ?
B2 B7 B8 104.5(15) . . ?
B2 B7 B6 105.5(15) . . ?
B2 B7 H7 123.4 . . ?
B3 B7 C39 102.9(15) . . ?
B3 B7 B8 106.2(15) . . ?
B3 B7 B6 59.3(12) . . ?
B3 B7 B2 57.9(12) . . ?
B3 B7 H7 123.6 . . ?
C48 C49 C50 113(3) . . ?
C48 C49 H49 123.3 . . ?
C50 C49 H49 123.3 . . ?
C80 B34 B32 59.2(15) . . ?
C80 B34 B33 103(2) . . ?
C80 B34 H34A 124.6 . . ?
C80 B34 B35 99(2) . . ?
C80 B34 B37 59.7(17) . . ?
B32 B34 B33 57.6(15) . . ?
B32 B34 H34A 123.5 . . ?
B32 B34 B35 101(2) . . ?
B32 B34 B37 106(2) . . ?
B33 B34 H34A 124.2 . . ?
B33 B34 B35 58.4(17) . . ?
B35 B34 H34A 128.0 . . ?
B37 B34 B33 103(2) . . ?
B37 B34 H34A 124.3 . . ?
B37 B34 B35 53.4(17) . . ?
C14 B12 B11 58.6(11) . . ?
C14 B12 B19 59.0(11) . . ?
C14 B12 H12A 124.2 . . ?
B13 B12 C14 105.3(14) . . ?
B13 B12 B11 107.1(15) . . ?
B13 B12 B19 59.6(12) . . ?
B13 B12 H12A 122.7 . . ?
B14 B12 C14 103.7(15) . . ?
B14 B12 B13 58.2(12) . . ?
B14 B12 B11 59.7(12) . . ?
B14 B12 B19 105.0(15) . . ?
B14 B12 H12A 124.2 . . ?
B11 B12 H12A 121.8 . . ?
B19 B12 B11 107.1(15) . . ?
B19 B12 H12A 122.5 . . ?
C77 C76 H76 118.3 . . ?
C75 C76 C77 123(3) . . ?
C75 C76 H76 118.3 . . ?
C58 C57 C56 119(2) . . ?
C58 C57 H57 120.7 . . ?
C56 C57 H57 120.7 . . ?
C72 C71 H71 120.0 . . ?
C70 C71 C72 120(3) . . ?
C70 C71 H71 120.0 . . ?
C67 C68 H68 123.3 . . ?
C67 C68 C69 113(3) . . ?
C69 C68 H68 123.3 . . ?
C92 C91 H91 120.2 . . ?
C90 C91 C92 120(3) . . ?
C90 C91 H91 120.2 . . ?
C3 C4 H4A 119.3 . . ?
C5 C4 C3 121(3) . . ?
C5 C4 H4A 119.3 . . ?
C116 C115 H115 120.0 . . ?
C114 C115 C116 120(2) . . ?
C114 C115 H115 120.0 . . ?
C80 B31 H31A 127.6 . . ?
C80 B31 B30 103(2) . . ?
C80 B31 B38 58.1(16) . . ?
C79 B31 C80 98(2) . . ?
C79 B31 B32 56.2(15) . . ?
C79 B31 H31A 126.6 . . ?
C79 B31 B30 59.1(16) . . ?
C79 B31 B38 105(2) . . ?
B32 B31 C80 56.7(15) . . ?
B32 B31 H31A 123.5 . . ?
B32 B31 B30 106(2) . . ?
B32 B31 B38 106(2) . . ?
B30 B31 H31A 122.4 . . ?
B38 B31 H31A 121.8 . . ?
B38 B31 B30 60.6(17) . . ?
C71 C70 H70 121.0 . . ?
C69 C70 C71 118(3) . . ?
C69 C70 H70 121.0 . . ?
C79 B30 B31 57.5(15) . . ?
C79 B30 H30A 126.1 . . ?
C79 B30 B38 102(2) . . ?
B31 B30 H30A 122.0 . . ?
B31 B30 B38 59.3(16) . . ?
B36 B30 C79 57.9(17) . . ?
B36 B30 B31 108(2) . . ?
B36 B30 H30A 120.4 . . ?
B36 B30 B38 109(3) . . ?
B36 B30 B29 63(2) . . ?
B38 B30 H30A 123.1 . . ?
B29 B30 C79 106(2) . . ?
B29 B30 B31 109(2) . . ?
B29 B30 H30A 119.8 . . ?
B29 B30 B38 60.5(18) . . ?
C79 B36 B33 57.2(16) . . ?
C79 B36 B30 61.7(17) . . ?
C79 B36 H36A 124.9 . . ?
C79 B36 B29 106(2) . . ?
C79 B36 B35 104(2) . . ?
B33 B36 H36A 119.8 . . ?
B30 B36 B33 111(2) . . ?
B30 B36 H36A 120.4 . . ?
B30 B36 B29 58.7(19) . . ?
B30 B36 B35 108(3) . . ?
B29 B36 B33 111(2) . . ?
B29 B36 H36A 121.5 . . ?
B35 B36 B33 61.5(19) . . ?
B35 B36 H36A 122.4 . . ?
B35 B36 B29 61(2) . . ?
C68 C69 H69 117.1 . . ?
C70 C69 C68 126(3) . . ?
C70 C69 H69 117.1 . . ?
C80 B38 B31 60.9(16) . . ?
C80 B38 B30 105(2) . . ?
C80 B38 H38A 123.4 . . ?
C80 B38 B29 105(2) . . ?
C80 B38 B37 58.3(16) . . ?
B31 B38 B30 60.1(17) . . ?
B31 B38 H38A 120.2 . . ?
B31 B38 B37 108(2) . . ?
B30 B38 H38A 124.9 . . ?
B30 B38 B37 103(2) . . ?
B29 B38 B31 107(2) . . ?
B29 B38 B30 57.3(18) . . ?
B29 B38 H38A 123.7 . . ?
B29 B38 B37 58.0(19) . . ?
B37 B38 H38A 124.0 . . ?
B30 B29 B36 58.0(19) . . ?
B30 B29 B38 62.2(18) . . ?
B30 B29 H29A 121.1 . . ?
B30 B29 B35 105(2) . . ?
B30 B29 B37 110(2) . . ?
B36 B29 H29A 125.0 . . ?
B38 B29 B36 107(2) . . ?
B38 B29 H29A 120.3 . . ?
B38 B29 B35 106(2) . . ?
B35 B29 B36 57(2) . . ?
B35 B29 H29A 125.5 . . ?
B37 B29 B36 103(2) . . ?
B37 B29 B38 62.6(19) . . ?
B37 B29 H29A 122.4 . . ?
B37 B29 B35 55.8(19) . . ?
B33 B35 B34 59.6(17) . . ?
B33 B35 H35A 120.2 . . ?
B34 B35 H35A 120.8 . . ?
B36 B35 B33 61.7(19) . . ?
B36 B35 B34 110(2) . . ?
B36 B35 B29 62(2) . . ?
B36 B35 H35A 120.0 . . ?
B29 B35 B33 112(2) . . ?
B29 B35 B34 111(2) . . ?
B29 B35 H35A 119.3 . . ?
B37 B35 B33 111(2) . . ?
B37 B35 B34 61.7(19) . . ?
B37 B35 B36 111(3) . . ?
B37 B35 B29 61(2) . . ?
B37 B35 H35A 119.9 . . ?
C80 B37 B34 56.1(15) . . ?
C80 B37 B38 57.9(16) . . ?
C80 B37 B29 105(2) . . ?
C80 B37 H37A 126.8 . . ?
B34 B37 B38 107(2) . . ?
B34 B37 H37A 118.9 . . ?
B38 B37 H37A 123.0 . . ?
B29 B37 B34 115(2) . . ?
B29 B37 B38 59.4(18) . . ?
B29 B37 H37A 119.3 . . ?
B35 B37 C80 105(2) . . ?
B35 B37 B34 65(2) . . ?
B35 B37 B38 109(3) . . ?
B35 B37 B29 63(2) . . ?
B35 B37 H37A 119.7 . . ?
C61 C66 C65 123(2) . . ?
C61 C66 H66 118.7 . . ?
C65 C66 H66 118.7 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Au5 P4 C40 B4 109.8(13) . . . . ?
Au5 P4 C40 B40 -29.9(13) . . . . ?
Au5 P4 C40 B1 -99.7(12) . . . . ?
Au5 P4 C40 B5 38.1(13) . . . . ?
Au5 P4 C40 B9 -175.4(12) . . . . ?
Au5 P4 C41 C42 10(2) . . . . ?
Au5 P4 C41 C46 -173(2) . . . . ?
Au5 P4 C47 C48 30(2) . . . . ?
Au5 P4 C47 C52 -145(2) . . . . ?
Au6 P5 C152 C153 166.0(15) . . . . ?
Au6 P5 C152 C154 -11.0(18) . . . . ?
Au6 P5 C53 B24 26.0(15) . . . . ?
Au6 P5 C53 B25 -43.7(15) . . . . ?
Au6 P5 C53 B60 -116.4(12) . . . . ?
Au6 P5 C53 B23 98.2(14) . . . . ?
Au6 P5 C53 B22 172.8(12) . . . . ?
Au6 P5 C155 C156 5.2(13) . . . . ?
Au6 P5 C155 C148 -179.5(13) . . . . ?
Au8 P3 C39 B8 -36.7(15) . . . . ?
Au8 P3 C39 B40 33.9(14) . . . . ?
Au8 P3 C39 B1 106.5(13) . . . . ?
Au8 P3 C39 B2 -179.0(12) . . . . ?
Au8 P3 C39 B7 -108.0(13) . . . . ?
Au8 P3 C33 C34 6(2) . . . . ?
Au8 P3 C33 C38 -176.6(15) . . . . ?
Au8 P3 C27 C28 -44.9(16) . . . . ?
Au8 P3 C27 C32 133.6(15) . . . . ?
Au9 P2 C14 B17 179.8(12) . . . . ?
Au9 P2 C14 B18 103.8(14) . . . . ?
Au9 P2 C14 B11 -104.4(13) . . . . ?
Au9 P2 C14 B19 31.2(14) . . . . ?
Au9 P2 C14 B12 -36.0(13) . . . . ?
Au9 P2 C15 C16 116.7(6) . . . . ?
Au9 P2 C15 C20 -57.1(7) . . . . ?
Au9 P2 C21 C26 12(2) . . . . ?
Au9 P2 C21 C22 -169.7(15) . . . . ?
Au13 P9 C93 C94 172.5(12) . . . . ?
Au13 P9 C93 C98 -8.4(17) . . . . ?
Au13 P9 C99 C100 51.5(16) . . . . ?
Au13 P9 C99 C104 -118.5(15) . . . . ?
Au13 P9 C105 B50 178.9(11) . . . . ?
Au13 P9 C105 B56 34.6(13) . . . . ?
Au13 P9 C105 B51 -107.5(12) . . . . ?
Au13 P9 C105 B57 105.1(13) . . . . ?
Au13 P9 C105 B58 -35.7(13) . . . . ?
Au16 P11 C119 C120 -174.5(18) . . . . ?
Au16 P11 C119 C124 5(2) . . . . ?
Au16 P11 C125 C126 175.5(15) . . . . ?
Au16 P11 C125 C130 -10.0(14) . . . . ?
Au16 P11 C131 B43 -27.3(14) . . . . ?
Au16 P11 C131 B41 111.1(12) . . . . ?
Au16 P11 C131 B59 -175.2(13) . . . . ?
Au16 P11 C131 B42 39.7(15) . . . . ?
Au16 P11 C131 B48 -101.3(14) . . . . ?
Au1 P6 C61 C62 -39(2) . . . . ?
Au1 P6 C61 C66 147(2) . . . . ?
Au1 P6 C54 B25 42.1(14) . . . . ?
Au1 P6 C54 B26 -25.5(13) . . . . ?
Au1 P6 C54 B60 113.0(12) . . . . ?
Au1 P6 C54 B21 -176.8(13) . . . . ?
Au1 P6 C54 B27 -98.4(14) . . . . ?
Au1 P6 C55 C60 -24(2) . . . . ?
Au1 P6 C55 C56 153.5(17) . . . . ?
Au3 P1 C13 B13 36.6(14) . . . . ?
Au3 P1 C13 B16 -178.4(12) . . . . ?
Au3 P1 C13 B18 -105.3(12) . . . . ?
Au3 P1 C13 B19 -32.5(14) . . . . ?
Au3 P1 C13 B15 107.2(13) . . . . ?
Au3 P1 C7 C8 -3.0(19) . . . . ?
Au3 P1 C7 C12 179.1(18) . . . . ?
Au3 P1 C1 C2 -35(2) . . . . ?
Au3 P1 C1 C6 141.3(17) . . . . ?
Au18 P10 C106 B53 -107.6(13) . . . . ?
Au18 P10 C106 B51 108.1(11) . . . . ?
Au18 P10 C106 B54 -34.0(13) . . . . ?
Au18 P10 C106 B52 -179.9(12) . . . . ?
Au18 P10 C106 B58 36.5(13) . . . . ?
Au18 P10 C113 C118 35(2) . . . . ?
Au18 P10 C113 C114 -144.3(19) . . . . ?
Au18 P10 C107 C108 -176.7(18) . . . . ?
Au18 P10 C107 C112 5(2) . . . . ?
Au14 P8 C80 B32 -29.6(19) . . . . ?
Au14 P8 C80 B34 40.3(18) . . . . ?
Au14 P8 C80 B31 -99.1(17) . . . . ?
Au14 P8 C80 B38 -169.4(16) . . . . ?
Au14 P8 C80 B37 114(2) . . . . ?
Au14 P8 C87 C92 178.4(18) . . . . ?
Au14 P8 C87 C88 -6(3) . . . . ?
Au14 P8 C81 C82 42.6(17) . . . . ?
Au14 P8 C81 C86 -132.7(16) . . . . ?
Au10 P12 C133 C134 28.3(16) . . . . ?
Au10 P12 C133 C138 -151.6(14) . . . . ?
Au10 P12 C132 B45 99.9(13) . . . . ?
Au10 P12 C132 B46 28.9(13) . . . . ?
Au10 P12 C132 B47 175.4(14) . . . . ?
Au10 P12 C132 B41 -110.4(13) . . . . ?
Au10 P12 C132 B42 -37.7(15) . . . . ?
Au10 P12 C139 C140 30.7(17) . . . . ?
Au10 P12 C139 C144 -146.6(17) . . . . ?
Au17 P7 C73 C74 138.0(19) . . . . ?
Au17 P7 C73 C78 -35.8(19) . . . . ?
Au17 P7 C79 B32 26(2) . . . . ?
Au17 P7 C79 B33 -43.7(17) . . . . ?
Au17 P7 C79 B31 98.7(18) . . . . ?
Au17 P7 C79 B30 172.6(15) . . . . ?
Au17 P7 C79 B36 -117(2) . . . . ?
Au17 P7 C67 C72 0(3) . . . . ?
Au17 P7 C67 C68 -178(2) . . . . ?
P9 C93 C94 C95 173.6(16) . . . . ?
P9 C93 C98 C97 -177.5(19) . . . . ?
P9 C105 B58 C106 -153.3(11) . . . . ?
P9 C105 B58 B56 105.2(14) . . . . ?
P9 C105 B58 B51 -111.9(13) . . . . ?
P9 C105 B58 B54 144.4(12) . . . . ?
P5 C152 C153 C149 -177.4(16) . . . . ?
P5 C152 C154 C151 177(2) . . . . ?
P5 C53 B24 B25 -104.7(14) . . . . ?
P5 C53 B24 B26 -143.9(13) . . . . ?
P5 C53 B24 B23 113.7(14) . . . . ?
P5 C53 B24 B28 152.9(13) . . . . ?
P5 C53 B25 B24 108.7(15) . . . . ?
P5 C53 B25 B26 147.3(13) . . . . ?
P5 C53 B25 B60 -112.4(15) . . . . ?
P5 C53 B25 C54 -151.9(13) . . . . ?
P5 C53 B60 B25 104.4(15) . . . . ?
P5 C53 B60 C54 144.3(12) . . . . ?
P5 C53 B60 B21 -153.6(13) . . . . ?
P5 C53 B60 B22 -112.0(15) . . . . ?
P5 C53 B23 B24 -105.7(16) . . . . ?
P5 C53 B23 B22 112.0(16) . . . . ?
P5 C53 B23 B20 153.4(13) . . . . ?
P5 C53 B23 B28 -144.1(14) . . . . ?
P5 C53 B22 B60 107.9(16) . . . . ?
P5 C53 B22 B23 -111.9(16) . . . . ?
P5 C53 B22 B21 147.7(14) . . . . ?
P5 C53 B22 B20 -149.8(13) . . . . ?
P5 C155 C156 C145 176.4(12) . . . . ?
P5 C155 C148 C147 -172.2(15) . . . . ?
P10 C106 B51 B50 153.8(12) . . . . ?
P10 C106 B51 B52 114.5(15) . . . . ?
P10 C106 B51 C105 -145.3(12) . . . . ?
P10 C106 B51 B58 -105.4(14) . . . . ?
P10 C106 B54 B53 -114.9(15) . . . . ?
P10 C106 B54 B56 143.9(13) . . . . ?
P10 C106 B54 B55 -154.5(12) . . . . ?
P10 C106 B54 B58 105.2(14) . . . . ?
P10 C106 B52 B53 111.7(16) . . . . ?
P10 C106 B52 B50 -145.6(13) . . . . ?
P10 C106 B52 B51 -105.8(14) . . . . ?
P10 C106 B52 B49 150.7(13) . . . . ?
P10 C106 B58 B56 -147.6(12) . . . . ?
P10 C106 B58 B51 109.8(13) . . . . ?
P10 C106 B58 B54 -109.4(14) . . . . ?
P10 C106 B58 C105 151.1(11) . . . . ?
P10 C113 C114 C115 -179.9(19) . . . . ?
P10 C107 C108 C109 -176.7(19) . . . . ?
P10 C107 C112 C111 171.1(19) . . . . ?
P4 C40 B4 B5 -105.1(15) . . . . ?
P4 C40 B4 B6 -141.4(14) . . . . ?
P4 C40 B4 B3 154.9(12) . . . . ?
P4 C40 B4 B9 113.8(16) . . . . ?
P4 C40 B40 C39 -153.4(12) . . . . ?
P4 C40 B40 B8 144.9(13) . . . . ?
P4 C40 B40 B1 -110.6(14) . . . . ?
P4 C40 B40 B5 108.0(14) . . . . ?
P4 C40 B1 C39 143.3(12) . . . . ?
P4 C40 B1 B40 104.5(14) . . . . ?
P4 C40 B1 B2 -156.6(11) . . . . ?
P4 C40 B1 B9 -116.0(15) . . . . ?
P4 C40 B5 B8 -142.4(12) . . . . ?
P4 C40 B5 B4 114.5(14) . . . . ?
P4 C40 B5 B40 -104.9(13) . . . . ?
P4 C40 B5 B6 150.3(12) . . . . ?
P4 C40 B9 B4 -111.8(15) . . . . ?
P4 C40 B9 B1 108.2(16) . . . . ?
P4 C40 B9 B2 149.1(13) . . . . ?
P4 C40 B9 B3 -151.7(13) . . . . ?
P4 C41 C42 C43 173.3(19) . . . . ?
P4 C41 C46 C45 -174(2) . . . . ?
P4 C47 C52 C51 -179(2) . . . . ?
P11 C119 C120 C121 179.9(18) . . . . ?
P11 C119 C124 C123 -179.6(17) . . . . ?
P11 C125 C126 C127 173.1(17) . . . . ?
P11 C125 C130 C129 -177.5(15) . . . . ?
P11 C131 B43 B46 144.4(13) . . . . ?
P11 C131 B43 B42 104.2(14) . . . . ?
P11 C131 B43 B44 -149.4(13) . . . . ?
P11 C131 B43 B48 -113.4(14) . . . . ?
P11 C131 B41 C132 -144.9(12) . . . . ?
P11 C131 B41 B47 153.5(13) . . . . ?
P11 C131 B41 B59 116.1(15) . . . . ?
P11 C131 B41 B42 -104.3(14) . . . . ?
P11 C131 B59 B47 -146.0(15) . . . . ?
P11 C131 B59 B41 -107.6(17) . . . . ?
P11 C131 B59 B39 149.1(14) . . . . ?
P11 C131 B59 B48 109.3(16) . . . . ?
P11 C131 B42 B46 -146.9(13) . . . . ?
P11 C131 B42 C132 151.0(13) . . . . ?
P11 C131 B42 B43 -108.0(14) . . . . ?
P11 C131 B42 B41 112.1(15) . . . . ?
P11 C131 B48 B43 106.9(15) . . . . ?
P11 C131 B48 B59 -115.4(15) . . . . ?
P11 C131 B48 B44 143.3(14) . . . . ?
P11 C131 B48 B39 -153.3(13) . . . . ?
P2 C14 B17 B16 -150.8(13) . . . . ?
P2 C14 B17 B18 -111.7(16) . . . . ?
P2 C14 B17 B11 108.2(16) . . . . ?
P2 C14 B17 B10 146.1(13) . . . . ?
P2 C14 B18 C13 -142.9(13) . . . . ?
P2 C14 B18 B16 154.7(13) . . . . ?
P2 C14 B18 B17 115.3(16) . . . . ?
P2 C14 B18 B19 -104.5(15) . . . . ?
P2 C14 B11 B14 142.0(14) . . . . ?
P2 C14 B11 B17 -116.8(16) . . . . ?
P2 C14 B11 B10 -154.3(13) . . . . ?
P2 C14 B11 B12 101.3(15) . . . . ?
P2 C14 B19 C13 153.7(12) . . . . ?
P2 C14 B19 B13 -142.4(12) . . . . ?
P2 C14 B19 B18 115.0(14) . . . . ?
P2 C14 B19 B12 -102.8(14) . . . . ?
P2 C14 B12 B13 147.1(12) . . . . ?
P2 C14 B12 B14 -152.6(12) . . . . ?
P2 C14 B12 B11 -112.0(14) . . . . ?
P2 C14 B12 B19 107.9(13) . . . . ?
P2 C15 C20 C19 173.9(8) . . . . ?
P2 C21 C22 C23 -176.7(17) . . . . ?
P6 C61 C66 C65 179.6(19) . . . . ?
P6 C54 B21 B60 -103.2(17) . . . . ?
P6 C54 B21 B22 -143.0(15) . . . . ?
P6 C54 B21 B27 113.9(16) . . . . ?
P6 C54 B21 B20 152.5(13) . . . . ?
P6 C54 B27 B26 103.2(15) . . . . ?
P6 C54 B27 B21 -115.9(16) . . . . ?
P6 C54 B27 B20 -155.6(13) . . . . ?
P6 C54 B27 B28 142.2(14) . . . . ?
P6 C55 C56 C57 176.6(18) . . . . ?
P1 C13 B13 B14 153.2(13) . . . . ?
P1 C13 B13 B19 -105.3(14) . . . . ?
P1 C13 B13 B15 113.2(16) . . . . ?
P1 C13 B13 B12 -144.2(13) . . . . ?
P1 C13 B16 B17 146.5(13) . . . . ?
P1 C13 B16 B18 108.0(15) . . . . ?
P1 C13 B16 B10 -149.4(13) . . . . ?
P1 C13 B16 B15 -110.3(17) . . . . ?
P1 C13 B18 C14 144.6(12) . . . . ?
P1 C13 B18 B16 -114.9(15) . . . . ?
P1 C13 B18 B17 -153.4(12) . . . . ?
P1 C13 B18 B19 104.8(14) . . . . ?
P1 C13 B19 C14 -150.5(11) . . . . ?
P1 C13 B19 B13 107.6(14) . . . . ?
P1 C13 B19 B18 -112.5(13) . . . . ?
P1 C13 B19 B12 146.9(12) . . . . ?
P1 C13 B15 B13 -104.5(15) . . . . ?
P1 C13 B15 B16 114.4(15) . . . . ?
P1 C13 B15 B14 -143.6(14) . . . . ?
P1 C13 B15 B10 152.6(12) . . . . ?
P1 C7 C8 C9 -177(2) . . . . ?
P1 C7 C12 C11 176.4(19) . . . . ?
P1 C1 C2 C3 179(2) . . . . ?
P1 C1 C6 C5 179(2) . . . . ?
P3 C39 B8 B40 107.9(14) . . . . ?
P3 C39 B8 B5 148.7(12) . . . . ?
P3 C39 B8 B6 -149.1(12) . . . . ?
P3 C39 B8 B7 -108.9(15) . . . . ?
P3 C39 B40 B8 -106.1(14) . . . . ?
P3 C39 B40 C40 153.3(12) . . . . ?
P3 C39 B40 B1 112.3(14) . . . . ?
P3 C39 B40 B5 -145.5(12) . . . . ?
P3 C39 B1 C40 -147.5(13) . . . . ?
P3 C39 B1 B40 -106.0(15) . . . . ?
P3 C39 B1 B2 113.0(17) . . . . ?
P3 C39 B1 B9 151.5(13) . . . . ?
P3 C39 B2 B1 -110.1(15) . . . . ?
P3 C39 B2 B3 146.5(14) . . . . ?
P3 C39 B2 B9 -149.7(14) . . . . ?
P3 C39 B2 B7 105.2(16) . . . . ?
P3 C39 B7 B8 106.0(14) . . . . ?
P3 C39 B7 B6 146.0(13) . . . . ?
P3 C39 B7 B2 -113.6(16) . . . . ?
P3 C39 B7 B3 -153.0(13) . . . . ?
P3 C33 C34 C35 -176(2) . . . . ?
P3 C33 C38 C37 -179.6(16) . . . . ?
P3 C27 C28 C29 175.4(16) . . . . ?
P3 C27 C32 C31 -176.5(15) . . . . ?
P8 C80 B32 C79 -151.3(16) . . . . ?
P8 C80 B32 B33 147.1(19) . . . . ?
P8 C80 B32 B34 105(2) . . . . ?
P8 C80 B32 B31 -107.9(19) . . . . ?
P8 C80 B34 B32 -107.8(17) . . . . ?
P8 C80 B34 B33 -146.2(16) . . . . ?
P8 C80 B34 B35 154.3(16) . . . . ?
P8 C80 B34 B37 117(2) . . . . ?
P8 C80 B31 C79 146.8(15) . . . . ?
P8 C80 B31 B32 106.2(18) . . . . ?
P8 C80 B31 B30 -153.2(18) . . . . ?
P8 C80 B31 B38 -111(2) . . . . ?
P8 C80 B38 B31 106(2) . . . . ?
P8 C80 B38 B30 149.0(18) . . . . ?
P8 C80 B38 B29 -151.7(18) . . . . ?
P8 C80 B38 B37 -115(2) . . . . ?
P8 C80 B37 B34 -103(2) . . . . ?
P8 C80 B37 B38 110(2) . . . . ?
P8 C80 B37 B29 147(2) . . . . ?
P8 C80 B37 B35 -148(2) . . . . ?
P12 C133 C134 C135 176.4(17) . . . . ?
P12 C133 C138 C137 -177(2) . . . . ?
P12 C132 B47 B45 -109.2(17) . . . . ?
P12 C132 B47 B41 106.6(18) . . . . ?
P12 C132 B47 B59 147.8(15) . . . . ?
P12 C132 B47 B39 -150.6(14) . . . . ?
P12 C132 B41 C131 143.3(12) . . . . ?
P12 C132 B41 B47 -115.9(16) . . . . ?
P12 C132 B41 B59 -155.8(13) . . . . ?
P12 C132 B41 B42 102.2(14) . . . . ?
P12 C132 B42 B46 106.1(15) . . . . ?
P12 C132 B42 C131 -151.9(13) . . . . ?
P12 C132 B42 B43 148.0(13) . . . . ?
P12 C132 B42 B41 -112.0(16) . . . . ?
P12 C139 C140 C141 178.2(17) . . . . ?
P12 C139 C144 C143 -178.5(19) . . . . ?
P7 C73 C74 C75 -177(2) . . . . ?
P7 C73 C78 C77 -179.2(18) . . . . ?
P7 C79 B32 C80 154.6(16) . . . . ?
P7 C79 B32 B33 -103(2) . . . . ?
P7 C79 B32 B34 -144.8(19) . . . . ?
P7 C79 B32 B31 110(2) . . . . ?
P7 C79 B33 B32 107.8(18) . . . . ?
P7 C79 B33 B34 146.0(16) . . . . ?
P7 C79 B33 B36 -111.7(19) . . . . ?
P7 C79 B33 B35 -150.6(17) . . . . ?
P7 C79 B31 C80 -147.2(16) . . . . ?
P7 C79 B31 B32 -106.4(19) . . . . ?
P7 C79 B31 B30 112(2) . . . . ?
P7 C79 B31 B38 153.8(18) . . . . ?
P7 C79 B30 B31 -108(2) . . . . ?
P7 C79 B30 B36 107(2) . . . . ?
P7 C79 B30 B38 -148.1(18) . . . . ?
P7 C79 B30 B29 149.3(18) . . . . ?
P7 C79 B36 B33 104(2) . . . . ?
P7 C79 B36 B30 -111(2) . . . . ?
P7 C79 B36 B29 -151(2) . . . . ?
P7 C79 B36 B35 145(2) . . . . ?
P7 C67 C68 C69 -179(3) . . . . ?
C93 P9 C99 C100 177.7(14) . . . . ?
C93 P9 C99 C104 7.7(19) . . . . ?
C93 P9 C105 B50 54.5(14) . . . . ?
C93 P9 C105 B56 -89.7(13) . . . . ?
C93 P9 C105 B51 128.1(13) . . . . ?
C93 P9 C105 B57 -19.2(15) . . . . ?
C93 P9 C105 B58 -160.1(12) . . . . ?
C93 C94 C95 C96 7(4) . . . . ?
C93 C98 C97 C96 1(4) . . . . ?
C13 P1 C7 C8 -126.7(17) . . . . ?
C13 P1 C7 C12 55(2) . . . . ?
C13 P1 C1 C2 86(2) . . . . ?
C13 P1 C1 C6 -98(2) . . . . ?
C13 B13 B14 B11 61.3(18) . . . . ?
C13 B13 B14 B10 -3(2) . . . . ?
C13 B13 B14 B15 -39.6(14) . . . . ?
C13 B13 B14 B12 98.6(15) . . . . ?
C13 B13 B19 C14 -95.9(15) . . . . ?
C13 B13 B19 B18 -35.7(13) . . . . ?
C13 B13 B19 B12 -135.8(15) . . . . ?
C13 B13 B15 B16 34.4(14) . . . . ?
C13 B13 B15 B14 133.9(16) . . . . ?
C13 B13 B15 B10 97.9(16) . . . . ?
C13 B13 B12 C14 -1.9(17) . . . . ?
C13 B13 B12 B14 -98.8(15) . . . . ?
C13 B13 B12 B11 -63.1(17) . . . . ?
C13 B13 B12 B19 37.0(13) . . . . ?
C13 B16 B17 C14 0.7(18) . . . . ?
C13 B16 B17 B18 -38.0(13) . . . . ?
C13 B16 B17 B11 63.0(16) . . . . ?
C13 B16 B17 B10 101.6(15) . . . . ?
C13 B16 B18 C14 97.5(15) . . . . ?
C13 B16 B18 B17 136.6(15) . . . . ?
C13 B16 B18 B19 34.2(13) . . . . ?
C13 B16 B10 B14 0.8(19) . . . . ?
C13 B16 B10 B17 -99.5(15) . . . . ?
C13 B16 B10 B11 -60.6(19) . . . . ?
C13 B16 B10 B15 38.9(14) . . . . ?
C13 B16 B15 B13 -34.9(14) . . . . ?
C13 B16 B15 B14 -96.2(17) . . . . ?
C13 B16 B15 B10 -136.5(15) . . . . ?
C13 B18 B19 C14 134.4(14) . . . . ?
C13 B18 B19 B13 36.9(14) . . . . ?
C13 B18 B19 B12 100.4(15) . . . . ?
C13 B19 B12 C14 94.8(15) . . . . ?
C13 B19 B12 B13 -40.2(14) . . . . ?
C13 B19 B12 B14 -2.4(19) . . . . ?
C13 B19 B12 B11 59.9(18) . . . . ?
C7 P1 C13 B13 160.5(13) . . . . ?
C7 P1 C13 B16 -54.5(16) . . . . ?
C7 P1 C13 B18 18.6(15) . . . . ?
C7 P1 C13 B19 91.3(14) . . . . ?
C7 P1 C13 B15 -128.9(14) . . . . ?
C7 P1 C1 C2 -160.9(19) . . . . ?
C7 P1 C1 C6 15(2) . . . . ?
C7 C8 C9 C10 -1(4) . . . . ?
C94 C93 C98 C97 2(3) . . . . ?
C94 C95 C96 C97 -5(5) . . . . ?
C119 P11 C125 C126 52.7(19) . . . . ?
C119 P11 C125 C130 -132.8(14) . . . . ?
C119 P11 C131 B43 93.8(15) . . . . ?
C119 P11 C131 B41 -127.8(14) . . . . ?
C119 P11 C131 B59 -54.1(18) . . . . ?
C119 P11 C131 B42 160.8(14) . . . . ?
C119 P11 C131 B48 19.8(17) . . . . ?
C119 C124 C123 C122 1(4) . . . . ?
C125 P11 C119 C120 -51(2) . . . . ?
C125 P11 C119 C124 128.5(18) . . . . ?
C125 P11 C131 B43 -150.2(13) . . . . ?
C125 P11 C131 B41 -11.7(15) . . . . ?
C125 P11 C131 B59 61.9(17) . . . . ?
C125 P11 C131 B42 -83.1(15) . . . . ?
C125 P11 C131 B48 135.8(14) . . . . ?
C125 C130 C129 C128 4(3) . . . . ?
C29 C30 C31 C32 0(3) . . . . ?
C48 C47 C52 C51 6(4) . . . . ?
C104 C103 C102 C101 -8(3) . . . . ?
C63 C62 C61 P6 -176.2(18) . . . . ?
C63 C62 C61 C66 -2(3) . . . . ?
C63 C64 C65 C66 7(4) . . . . ?
C152 P5 C53 B24 -94.4(14) . . . . ?
C152 P5 C53 B25 -164.0(14) . . . . ?
C152 P5 C53 B60 123.3(13) . . . . ?
C152 P5 C53 B23 -22.1(17) . . . . ?
C152 P5 C53 B22 52.5(16) . . . . ?
C152 P5 C155 C156 128.2(12) . . . . ?
C152 P5 C155 C148 -56.5(16) . . . . ?
C152 C153 C149 C150 -3(3) . . . . ?
C152 C154 C151 C150 5(4) . . . . ?
C142 C143 C144 C139 -3(4) . . . . ?
C142 C141 C140 C139 3(3) . . . . ?
C39 P3 C33 C34 -118.0(18) . . . . ?
C39 P3 C33 C38 59.8(19) . . . . ?
C39 P3 C27 C28 76.5(16) . . . . ?
C39 P3 C27 C32 -105.1(17) . . . . ?
C39 B8 B40 C40 97.3(14) . . . . ?
C39 B8 B40 B1 35.8(13) . . . . ?
C39 B8 B40 B5 134.2(14) . . . . ?
C39 B8 B5 C40 -1.0(17) . . . . ?
C39 B8 B5 B4 62.1(18) . . . . ?
C39 B8 B5 B40 -39.0(13) . . . . ?
C39 B8 B5 B6 100.5(15) . . . . ?
C39 B8 B6 B4 -60.7(18) . . . . ?
C39 B8 B6 B5 -98.4(16) . . . . ?
C39 B8 B6 B3 1.7(18) . . . . ?
C39 B8 B6 B7 41.0(14) . . . . ?
C39 B8 B7 B6 -134.2(15) . . . . ?
C39 B8 B7 B2 -34.3(13) . . . . ?
C39 B8 B7 B3 -94.6(16) . . . . ?
C39 B40 B1 C40 131.6(15) . . . . ?
C39 B40 B1 B2 33.6(13) . . . . ?
C39 B40 B1 B9 95.5(16) . . . . ?
C39 B40 B5 B8 39.5(13) . . . . ?
C39 B40 B5 C40 -98.2(14) . . . . ?
C39 B40 B5 B4 -62.9(17) . . . . ?
C39 B40 B5 B6 0.9(18) . . . . ?
C39 B1 B2 B3 97.4(16) . . . . ?
C39 B1 B2 B9 135.5(16) . . . . ?
C39 B1 B2 B7 32.4(14) . . . . ?
C39 B1 B9 C40 94.4(15) . . . . ?
C39 B1 B9 B4 59.4(18) . . . . ?
C39 B1 B9 B2 -38.3(14) . . . . ?
C39 B1 B9 B3 -2.6(19) . . . . ?
C39 B2 B3 B4 61.1(18) . . . . ?
C39 B2 B3 B6 -2(2) . . . . ?
C39 B2 B3 B9 100.2(16) . . . . ?
C39 B2 B3 B7 -41.2(14) . . . . ?
C39 B2 B9 C40 -0.6(19) . . . . ?
C39 B2 B9 B4 -61.5(18) . . . . ?
C39 B2 B9 B1 38.8(13) . . . . ?
C39 B2 B9 B3 -99.5(16) . . . . ?
C39 B2 B7 B8 32.9(13) . . . . ?
C39 B2 B7 B6 96.2(15) . . . . ?
C39 B2 B7 B3 133.2(16) . . . . ?
B45 B46 C132 P12 112.7(13) . . . . ?
B45 B46 C132 B47 -37.1(14) . . . . ?
B45 B46 C132 B41 -106.9(16) . . . . ?
B45 B46 C132 B42 -145.2(15) . . . . ?
B45 B46 B43 C131 61.9(19) . . . . ?
B45 B46 B43 B42 102.5(18) . . . . ?
B45 B46 B43 B44 -36.9(16) . . . . ?
B45 B46 B43 B48 0(2) . . . . ?
B45 B46 B42 C131 -61.6(19) . . . . ?
B45 B46 B42 C132 31.4(14) . . . . ?
B45 B46 B42 B43 -100.0(16) . . . . ?
B45 B46 B42 B41 -1(2) . . . . ?
B45 B46 B44 B43 138.9(17) . . . . ?
B45 B46 B44 B39 37.9(14) . . . . ?
B45 B46 B44 B48 101.2(17) . . . . ?
B45 C132 B47 B41 -144.2(16) . . . . ?
B45 C132 B47 B59 -103.1(17) . . . . ?
B45 C132 B47 B39 -41.4(14) . . . . ?
B45 C132 B41 C131 -65.7(18) . . . . ?
B45 C132 B41 B47 35.2(16) . . . . ?
B45 C132 B41 B59 -5(2) . . . . ?
B45 C132 B41 B42 -106.8(18) . . . . ?
B45 C132 B42 B46 -33.9(15) . . . . ?
B45 C132 B42 C131 68.2(18) . . . . ?
B45 C132 B42 B43 8(2) . . . . ?
B45 C132 B42 B41 108.1(17) . . . . ?
B45 B47 B41 C131 62.8(18) . . . . ?
B45 B47 B41 C132 -33.0(15) . . . . ?
B45 B47 B41 B59 100.4(18) . . . . ?
B45 B47 B41 B42 1(2) . . . . ?
B45 B47 B59 C131 -64.9(18) . . . . ?
B45 B47 B59 B41 -103.2(16) . . . . ?
B45 B47 B59 B39 36.6(14) . . . . ?
B45 B47 B59 B48 -1.5(19) . . . . ?
B45 B47 B39 B59 -139.3(15) . . . . ?
B45 B47 B39 B44 -40.4(14) . . . . ?
B45 B47 B39 B48 -103.0(16) . . . . ?
B45 B44 B39 B47 40.0(14) . . . . ?
B45 B44 B39 B59 102.6(17) . . . . ?
B45 B44 B39 B48 139.6(16) . . . . ?
B45 B44 B48 C131 63.4(17) . . . . ?
B45 B44 B48 B43 99.2(16) . . . . ?
B45 B44 B48 B59 0.6(18) . . . . ?
B45 B44 B48 B39 -36.0(14) . . . . ?
B45 B39 B48 C131 -63(2) . . . . ?
B45 B39 B48 B43 -2(2) . . . . ?
B45 B39 B48 B59 -100.9(18) . . . . ?
B45 B39 B48 B44 37.4(16) . . . . ?
C153 C152 C154 C151 0(3) . . . . ?
C153 C149 C150 C151 7(4) . . . . ?
C53 P5 C152 C153 -71.8(18) . . . . ?
C53 P5 C152 C154 111.2(17) . . . . ?
C53 P5 C155 C156 -118.9(13) . . . . ?
C53 P5 C155 C148 56.4(16) . . . . ?
C53 B24 B25 B26 -135.9(15) . . . . ?
C53 B24 B25 B60 -35.6(13) . . . . ?
C53 B24 B25 C54 -95.3(14) . . . . ?
C53 B24 B26 B25 38.9(14) . . . . ?
C53 B24 B26 C54 -1.8(18) . . . . ?
C53 B24 B26 B27 -62.3(19) . . . . ?
C53 B24 B26 B28 -100.8(16) . . . . ?
C53 B24 B23 B22 34.6(14) . . . . ?
C53 B24 B23 B20 100.4(18) . . . . ?
C53 B24 B23 B28 136.5(16) . . . . ?
C53 B24 B28 B26 99.8(17) . . . . ?
C53 B24 B28 B23 -38.5(15) . . . . ?
C53 B24 B28 B27 60.4(19) . . . . ?
C53 B24 B28 B20 -3(2) . . . . ?
C53 B25 B26 B24 -37.8(14) . . . . ?
C53 B25 B26 C54 94.7(15) . . . . ?
C53 B25 B26 B27 61.3(19) . . . . ?
C53 B25 B26 B28 -1(2) . . . . ?
C53 B25 B60 C54 -132.3(16) . . . . ?
C53 B25 B60 B21 -97.8(17) . . . . ?
C53 B25 B60 B22 -33.6(14) . . . . ?
C53 B25 C54 P6 151.0(13) . . . . ?
C53 B25 C54 B26 -100.9(16) . . . . ?
C53 B25 C54 B60 40.1(14) . . . . ?
C53 B25 C54 B21 5(2) . . . . ?
C53 B25 C54 B27 -64.1(18) . . . . ?
C53 B60 C54 P6 -140.8(12) . . . . ?
C53 B60 C54 B25 -39.5(13) . . . . ?
C53 B60 C54 B26 -2.0(18) . . . . ?
C53 B60 C54 B21 102.3(16) . . . . ?
C53 B60 C54 B27 67.0(17) . . . . ?
C53 B60 B21 C54 -94.1(16) . . . . ?
C53 B60 B21 B22 42.1(14) . . . . ?
C53 B60 B21 B27 -61.0(18) . . . . ?
C53 B60 B21 B20 2.1(19) . . . . ?
C53 B60 B22 B23 -33.9(13) . . . . ?
C53 B60 B22 B21 -132.8(17) . . . . ?
C53 B60 B22 B20 -94.0(16) . . . . ?
C53 B23 B22 B60 34.7(13) . . . . ?
C53 B23 B22 B21 95.5(15) . . . . ?
C53 B23 B22 B20 134.5(15) . . . . ?
C53 B23 B20 B21 -3.8(19) . . . . ?
C53 B23 B20 B22 -41.0(14) . . . . ?
C53 B23 B20 B27 59(2) . . . . ?
C53 B23 B20 B28 98.3(17) . . . . ?
C53 B23 B28 B24 37.6(15) . . . . ?
C53 B23 B28 B26 1(2) . . . . ?
C53 B23 B28 B27 -63.0(18) . . . . ?
C53 B23 B28 B20 -101.9(17) . . . . ?
C53 B22 B20 B23 37.7(13) . . . . ?
C53 B22 B20 B21 -98.4(15) . . . . ?
C53 B22 B20 B27 -64.0(17) . . . . ?
C53 B22 B20 B28 -0.3(19) . . . . ?
C121 C122 C123 C124 -2(4) . . . . ?
C118 C113 C114 C115 1(4) . . . . ?
C14 P2 C15 C16 -119.4(9) . . . . ?
C14 P2 C15 C20 66.9(9) . . . . ?
C14 P2 C21 C26 -112.6(18) . . . . ?
C14 P2 C21 C22 65.4(19) . . . . ?
C14 B17 B18 C13 -96.8(15) . . . . ?
C14 B17 B18 B16 -135.3(15) . . . . ?
C14 B17 B18 B19 -36.1(14) . . . . ?
C14 B17 B11 B14 97.0(15) . . . . ?
C14 B17 B11 B10 137.1(16) . . . . ?
C14 B17 B11 B12 34.5(14) . . . . ?
C14 B17 B10 B16 98.5(16) . . . . ?
C14 B17 B10 B14 1(2) . . . . ?
C14 B17 B10 B11 -37.8(14) . . . . ?
C14 B17 B10 B15 61.9(18) . . . . ?
C14 B18 B19 C13 -134.4(14) . . . . ?
C14 B18 B19 B13 -97.5(15) . . . . ?
C14 B18 B19 B12 -34.0(13) . . . . ?
C14 B11 B10 B16 -1.4(19) . . . . ?
C14 B11 B10 B14 -98.9(16) . . . . ?
C14 B11 B10 B17 36.5(13) . . . . ?
C14 B11 B10 B15 -63.7(17) . . . . ?
C14 B11 B12 B13 97.8(15) . . . . ?
C14 B11 B12 B14 132.8(15) . . . . ?
C14 B11 B12 B19 35.1(13) . . . . ?
C14 B19 B12 B13 -135.0(15) . . . . ?
C14 B19 B12 B14 -97.2(15) . . . . ?
C14 B19 B12 B11 -34.9(13) . . . . ?
C80 P8 C87 C92 -56(2) . . . . ?
C80 P8 C87 C88 120(3) . . . . ?
C80 P8 C81 C82 -80.9(17) . . . . ?
C80 P8 C81 C86 103.8(18) . . . . ?
C80 B32 B33 C79 96(2) . . . . ?
C80 B32 B33 B34 -39(2) . . . . ?
C80 B32 B33 B36 63(2) . . . . ?
C80 B32 B33 B35 3(3) . . . . ?
C80 B32 B34 B33 134(2) . . . . ?
C80 B32 B34 B35 94(2) . . . . ?
C80 B32 B34 B37 39.0(18) . . . . ?
C80 B32 B31 C79 -129.2(18) . . . . ?
C80 B32 B31 B30 -95(2) . . . . ?
C80 B32 B31 B38 -32.0(17) . . . . ?
C80 B34 B35 B33 100(2) . . . . ?
C80 B34 B35 B36 63(3) . . . . ?
C80 B34 B35 B29 -3(3) . . . . ?
C80 B34 B35 B37 -41(2) . . . . ?
C80 B34 B37 B38 28.5(19) . . . . ?
C80 B34 B37 B29 92(2) . . . . ?
C80 B34 B37 B35 132(2) . . . . ?
C80 B31 B30 C79 -91(2) . . . . ?
C80 B31 B30 B36 -61(3) . . . . ?
C80 B31 B30 B38 41(2) . . . . ?
C80 B31 B30 B29 6(3) . . . . ?
C80 B31 B38 B30 -131(2) . . . . ?
C80 B31 B38 B29 -97(2) . . . . ?
C80 B31 B38 B37 -36.1(18) . . . . ?
C80 B38 B29 B30 -98(2) . . . . ?
C80 B38 B29 B36 -60(3) . . . . ?
C80 B38 B29 B35 0(3) . . . . ?
C80 B38 B29 B37 37(2) . . . . ?
C80 B38 B37 B34 -27.8(19) . . . . ?
C80 B38 B37 B29 -137(2) . . . . ?
C80 B38 B37 B35 -97(2) . . . . ?
B46 B45 C132 P12 -103.0(15) . . . . ?
B46 B45 C132 B47 141.7(15) . . . . ?
B46 B45 C132 B41 106.6(17) . . . . ?
B46 B45 C132 B42 33.3(15) . . . . ?
B46 B45 B47 C132 -33.0(13) . . . . ?
B46 B45 B47 B41 -1(2) . . . . ?
B46 B45 B47 B59 63.9(18) . . . . ?
B46 B45 B47 B39 100.0(15) . . . . ?
B46 B45 B44 B43 -35.4(14) . . . . ?
B46 B45 B44 B39 -136.9(16) . . . . ?
B46 B45 B44 B48 -100.5(16) . . . . ?
B46 B45 B39 B47 -98.1(16) . . . . ?
B46 B45 B39 B59 -62(2) . . . . ?
B46 B45 B39 B44 37.9(15) . . . . ?
B46 B45 B39 B48 2(2) . . . . ?
B46 C132 B47 B45 37.1(15) . . . . ?
B46 C132 B47 B41 -107.1(17) . . . . ?
B46 C132 B47 B59 -65.9(19) . . . . ?
B46 C132 B47 B39 -4.3(19) . . . . ?
B46 C132 B41 C131 4.5(18) . . . . ?
B46 C132 B41 B47 105.4(17) . . . . ?
B46 C132 B41 B59 65.4(18) . . . . ?
B46 C132 B41 B42 -36.6(14) . . . . ?
B46 C132 B42 C131 102.0(15) . . . . ?
B46 C132 B42 B43 41.9(14) . . . . ?
B46 C132 B42 B41 141.9(15) . . . . ?
B46 B43 B42 C131 -135.4(15) . . . . ?
B46 B43 B42 C132 -42.5(14) . . . . ?
B46 B43 B42 B41 -100.8(15) . . . . ?
B46 B43 B44 B45 36.4(15) . . . . ?
B46 B43 B44 B39 98.8(17) . . . . ?
B46 B43 B44 B48 138.8(18) . . . . ?
B46 B43 B48 C131 100.0(18) . . . . ?
B46 B43 B48 B59 63(2) . . . . ?
B46 B43 B48 B44 -38.6(17) . . . . ?
B46 B43 B48 B39 1(2) . . . . ?
B46 B44 B39 B45 -38.2(13) . . . . ?
B46 B44 B39 B47 1.9(18) . . . . ?
B46 B44 B39 B59 64.5(18) . . . . ?
B46 B44 B39 B48 101.4(16) . . . . ?
B46 B44 B48 C131 0(2) . . . . ?
B46 B44 B48 B43 35.8(15) . . . . ?
B46 B44 B48 B59 -62.8(18) . . . . ?
B46 B44 B48 B39 -99.4(17) . . . . ?
B13 C13 B16 B17 -67.1(17) . . . . ?
B13 C13 B16 B18 -105.6(16) . . . . ?
B13 C13 B16 B10 -3(2) . . . . ?
B13 C13 B16 B15 36.1(15) . . . . ?
B13 C13 B18 C14 1.7(18) . . . . ?
B13 C13 B18 B16 102.2(16) . . . . ?
B13 C13 B18 B17 63.7(17) . . . . ?
B13 C13 B18 B19 -38.1(14) . . . . ?
B13 C13 B19 C14 101.9(15) . . . . ?
B13 C13 B19 B18 139.9(15) . . . . ?
B13 C13 B19 B12 39.3(14) . . . . ?
B13 C13 B15 B16 -141.1(16) . . . . ?
B13 C13 B15 B14 -39.1(14) . . . . ?
B13 C13 B15 B10 -102.9(16) . . . . ?
B13 B14 B11 C14 -4(2) . . . . ?
B13 B14 B11 B17 -64.0(18) . . . . ?
B13 B14 B11 B10 -103.3(17) . . . . ?
B13 B14 B11 B12 37.4(15) . . . . ?
B13 B14 B10 B16 2(2) . . . . ?
B13 B14 B10 B17 63(2) . . . . ?
B13 B14 B10 B11 102.4(16) . . . . ?
B13 B14 B10 B15 -37.1(15) . . . . ?
B13 B14 B15 C13 40.0(14) . . . . ?
B13 B14 B15 B16 101.1(16) . . . . ?
B13 B14 B15 B10 140.7(15) . . . . ?
B13 B14 B12 C14 -99.6(14) . . . . ?
B13 B14 B12 B11 -139.8(15) . . . . ?
B13 B14 B12 B19 -38.5(14) . . . . ?
B13 B19 B12 C14 135.0(15) . . . . ?
B13 B19 B12 B14 37.8(14) . . . . ?
B13 B19 B12 B11 100.1(16) . . . . ?
C131 P11 C119 C120 63(2) . . . . ?
C131 P11 C119 C124 -118.3(18) . . . . ?
C131 P11 C125 C126 -60.9(18) . . . . ?
C131 P11 C125 C130 113.6(13) . . . . ?
C131 B43 B42 B46 135.4(15) . . . . ?
C131 B43 B42 C132 93.0(15) . . . . ?
C131 B43 B42 B41 34.6(13) . . . . ?
C131 B43 B44 B45 -66.5(17) . . . . ?
C131 B43 B44 B46 -102.9(17) . . . . ?
C131 B43 B44 B39 -4(2) . . . . ?
C131 B43 B44 B48 35.9(15) . . . . ?
C131 B43 B48 B59 -37.2(13) . . . . ?
C131 B43 B48 B44 -138.5(17) . . . . ?
C131 B43 B48 B39 -98.7(17) . . . . ?
C131 B41 B59 B47 136.9(17) . . . . ?
C131 B41 B59 B39 99.6(18) . . . . ?
C131 B41 B59 B48 33.5(14) . . . . ?
C131 B41 B42 B46 -97.5(16) . . . . ?
C131 B41 B42 C132 -131.8(15) . . . . ?
C131 B41 B42 B43 -35.0(13) . . . . ?
C131 B59 B39 B45 63.3(19) . . . . ?
C131 B59 B39 B47 100.3(16) . . . . ?
C131 B59 B39 B44 -2(2) . . . . ?
C131 B59 B39 B48 -38.8(14) . . . . ?
C131 B59 B48 B43 36.4(12) . . . . ?
C131 B59 B48 B44 98.8(15) . . . . ?
C131 B59 B48 B39 136.3(15) . . . . ?
C60 C59 C58 C57 5(4) . . . . ?
C60 C55 C56 C57 -6(4) . . . . ?
C155 P5 C152 C153 42.5(19) . . . . ?
C155 P5 C152 C154 -134.5(16) . . . . ?
C155 P5 C53 B24 148.9(13) . . . . ?
C155 P5 C53 B25 79.2(15) . . . . ?
C155 P5 C53 B60 6.5(15) . . . . ?
C155 P5 C53 B23 -138.8(15) . . . . ?
C155 P5 C53 B22 -64.2(16) . . . . ?
C155 C156 C145 C146 -2(3) . . . . ?
C155 C148 C147 C146 -6(3) . . . . ?
B24 C53 B25 B26 38.6(14) . . . . ?
B24 C53 B25 B60 139.0(15) . . . . ?
B24 C53 B25 C54 99.4(16) . . . . ?
B24 C53 B60 B25 -39.2(15) . . . . ?
B24 C53 B60 C54 0.7(18) . . . . ?
B24 C53 B60 B21 62.8(18) . . . . ?
B24 C53 B60 B22 104.4(16) . . . . ?
B24 C53 B23 B22 -142.3(15) . . . . ?
B24 C53 B23 B20 -100.9(16) . . . . ?
B24 C53 B23 B28 -38.5(14) . . . . ?
B24 C53 B22 B60 -104.2(17) . . . . ?
B24 C53 B22 B23 36.0(15) . . . . ?
B24 C53 B22 B21 -64.4(19) . . . . ?
B24 C53 B22 B20 -1.9(19) . . . . ?
B24 B25 B26 C54 132.5(15) . . . . ?
B24 B25 B26 B27 99.0(16) . . . . ?
B24 B25 B26 B28 36.4(15) . . . . ?
B24 B25 B60 C53 35.4(13) . . . . ?
B24 B25 B60 C54 -96.9(16) . . . . ?
B24 B25 B60 B21 -62.4(18) . . . . ?
B24 B25 B60 B22 1.8(19) . . . . ?
B24 B25 C54 P6 -149.3(12) . . . . ?
B24 B25 C54 B26 -41.1(14) . . . . ?
B24 B25 C54 B60 99.8(16) . . . . ?
B24 B25 C54 B21 64.6(19) . . . . ?
B24 B25 C54 B27 -4.4(19) . . . . ?
B24 B26 C54 P6 142.1(12) . . . . ?
B24 B26 C54 B25 40.9(13) . . . . ?
B24 B26 C54 B60 2.4(19) . . . . ?
B24 B26 C54 B21 -63.3(17) . . . . ?
B24 B26 C54 B27 -100.9(15) . . . . ?
B24 B26 B27 C54 96.5(16) . . . . ?
B24 B26 B27 B21 62(2) . . . . ?
B24 B26 B27 B20 -2(2) . . . . ?
B24 B26 B27 B28 -39.1(16) . . . . ?
B24 B26 B28 B23 36.4(15) . . . . ?
B24 B26 B28 B27 136.0(17) . . . . ?
B24 B26 B28 B20 98.3(17) . . . . ?
B24 B23 B22 C53 -33.6(13) . . . . ?
B24 B23 B22 B60 1.2(19) . . . . ?
B24 B23 B22 B21 62.0(18) . . . . ?
B24 B23 B22 B20 100.9(16) . . . . ?
B24 B23 B20 B21 -66(2) . . . . ?
B24 B23 B20 B22 -102.9(18) . . . . ?
B24 B23 B20 B27 -3(2) . . . . ?
B24 B23 B20 B28 36.4(16) . . . . ?
B24 B23 B28 B26 -36.8(15) . . . . ?
B24 B23 B28 B27 -100.6(17) . . . . ?
B24 B23 B28 B20 -139.6(18) . . . . ?
C62 C63 C64 C65 -3(4) . . . . ?
C62 C61 C66 C65 6(4) . . . . ?
C72 C67 C68 C69 3(5) . . . . ?
C72 C71 C70 C69 0(5) . . . . ?
C120 C119 C124 C123 0(3) . . . . ?
C120 C121 C122 C123 3(4) . . . . ?
C1 P1 C13 B13 -84.5(14) . . . . ?
C1 P1 C13 B16 60.6(16) . . . . ?
C1 P1 C13 B18 133.6(14) . . . . ?
C1 P1 C13 B19 -153.6(13) . . . . ?
C1 P1 C13 B15 -13.8(16) . . . . ?
C1 P1 C7 C8 123.1(18) . . . . ?
C1 P1 C7 C12 -55(2) . . . . ?
C127 C128 C129 C130 -2(3) . . . . ?
C16 C15 C20 C19 0.0 . . . . ?
C15 P2 C14 B17 60.3(15) . . . . ?
C15 P2 C14 B18 -15.8(16) . . . . ?
C15 P2 C14 B11 136.1(13) . . . . ?
C15 P2 C14 B19 -88.3(13) . . . . ?
C15 P2 C14 B12 -155.5(10) . . . . ?
C15 P2 C21 C26 133.5(17) . . . . ?
C15 P2 C21 C22 -48.5(19) . . . . ?
C15 C16 C17 C18 0.0 . . . . ?
C15 C20 C19 C18 0.0 . . . . ?
C20 C19 C18 C17 0.0 . . . . ?
C19 C18 C17 C16 0.0 . . . . ?
C17 C16 C15 P2 -173.5(9) . . . . ?
C17 C16 C15 C20 0.0 . . . . ?
C143 C142 C141 C140 -3(3) . . . . ?
B8 C39 B40 C40 -100.6(14) . . . . ?
B8 C39 B40 B1 -141.5(14) . . . . ?
B8 C39 B40 B5 -39.3(12) . . . . ?
B8 C39 B1 C40 -4.1(19) . . . . ?
B8 C39 B1 B40 37.4(15) . . . . ?
B8 C39 B1 B2 -103.6(16) . . . . ?
B8 C39 B1 B9 -65.1(18) . . . . ?
B8 C39 B2 B1 106.7(17) . . . . ?
B8 C39 B2 B3 3(2) . . . . ?
B8 C39 B2 B9 67.1(19) . . . . ?
B8 C39 B2 B7 -38.0(15) . . . . ?
B8 C39 B7 B6 40.0(13) . . . . ?
B8 C39 B7 B2 140.4(15) . . . . ?
B8 C39 B7 B3 101.0(15) . . . . ?
B8 B40 B1 C39 -34.9(13) . . . . ?
B8 B40 B1 C40 96.7(16) . . . . ?
B8 B40 B1 B2 -1.2(19) . . . . ?
B8 B40 B1 B9 60.7(19) . . . . ?
B8 B40 B5 C40 -137.7(15) . . . . ?
B8 B40 B5 B4 -102.4(16) . . . . ?
B8 B40 B5 B6 -38.7(14) . . . . ?
B8 B5 B6 B4 -137.3(16) . . . . ?
B8 B5 B6 B3 -97.4(15) . . . . ?
B8 B5 B6 B7 -35.6(14) . . . . ?
B8 B6 B3 B4 -99.4(15) . . . . ?
B8 B6 B3 B2 0.3(19) . . . . ?
B8 B6 B3 B9 -65.7(17) . . . . ?
B8 B6 B3 B7 39.4(13) . . . . ?
B8 B6 B7 C39 -37.3(12) . . . . ?
B8 B6 B7 B2 -98.2(15) . . . . ?
B8 B6 B7 B3 -134.6(15) . . . . ?
C156 C155 C148 C147 3(3) . . . . ?
C156 C145 C146 C147 -2(3) . . . . ?
B53 C106 B51 B50 5.3(17) . . . . ?
B53 C106 B51 B52 -34.0(14) . . . . ?
B53 C106 B51 C105 66.2(15) . . . . ?
B53 C106 B51 B58 106.1(15) . . . . ?
B53 C106 B54 B56 -101.2(15) . . . . ?
B53 C106 B54 B55 -39.6(13) . . . . ?
B53 C106 B54 B58 -139.9(15) . . . . ?
B53 C106 B52 B50 102.7(16) . . . . ?
B53 C106 B52 B51 142.5(15) . . . . ?
B53 C106 B52 B49 39.1(13) . . . . ?
B53 C106 B58 B56 0(2) . . . . ?
B53 C106 B58 B51 -102.5(16) . . . . ?
B53 C106 B58 B54 38.3(15) . . . . ?
B53 C106 B58 C105 -61.2(17) . . . . ?
B53 B54 B55 B56 -138.8(15) . . . . ?
B53 B54 B55 B49 -34.7(14) . . . . ?
B53 B54 B55 B57 -100.0(16) . . . . ?
B53 B54 B58 C106 -35.3(13) . . . . ?
B53 B54 B58 B56 101.2(16) . . . . ?
B53 B54 B58 B51 0.0(19) . . . . ?
B53 B54 B58 C105 62.2(17) . . . . ?
B53 B52 B49 B50 140.3(15) . . . . ?
B53 B52 B49 B55 40.2(14) . . . . ?
B53 B52 B49 B57 102.6(16) . . . . ?
B53 B49 B55 B56 102.0(16) . . . . ?
B53 B49 B55 B54 36.2(14) . . . . ?
B53 B49 B55 B57 139.1(14) . . . . ?
B53 B49 B57 B50 99.8(16) . . . . ?
B53 B49 B57 B56 -2.7(19) . . . . ?
B53 B49 B57 B55 -37.6(14) . . . . ?
B53 B49 B57 C105 59.2(19) . . . . ?
B53 B55 B57 B50 -2.5(18) . . . . ?
B53 B55 B57 B56 -104.5(15) . . . . ?
B53 B55 B57 B49 35.9(13) . . . . ?
B53 B55 B57 C105 -64.4(17) . . . . ?
C133 P12 C132 B45 -140.8(15) . . . . ?
C133 P12 C132 B46 148.3(12) . . . . ?
C133 P12 C132 B47 -65.3(17) . . . . ?
C133 P12 C132 B41 8.9(15) . . . . ?
C133 P12 C132 B42 81.7(15) . . . . ?
C133 P12 C139 C140 -93.3(16) . . . . ?
C133 P12 C139 C144 89(2) . . . . ?
C133 C134 C135 C136 2(4) . . . . ?
C133 C138 C137 C136 -1(5) . . . . ?
C73 P7 C79 B32 -91.4(19) . . . . ?
C73 P7 C79 B33 -160.8(16) . . . . ?
C73 P7 C79 B31 -18(2) . . . . ?
C73 P7 C79 B30 55.4(19) . . . . ?
C73 P7 C79 B36 126(2) . . . . ?
C73 P7 C67 C72 120(2) . . . . ?
C73 P7 C67 C68 -58(3) . . . . ?
C73 C74 C75 C76 2(4) . . . . ?
C122 C121 C120 C119 -2(4) . . . . ?
B25 C53 B24 B26 -39.3(14) . . . . ?
B25 C53 B24 B23 -141.6(15) . . . . ?
B25 C53 B24 B28 -102.4(17) . . . . ?
B25 C53 B60 C54 39.9(13) . . . . ?
B25 C53 B60 B21 102.0(16) . . . . ?
B25 C53 B60 B22 143.6(16) . . . . ?
B25 C53 B23 B24 36.6(15) . . . . ?
B25 C53 B23 B22 -105.7(16) . . . . ?
B25 C53 B23 B20 -64.2(19) . . . . ?
B25 C53 B23 B28 -2(2) . . . . ?
B25 C53 B22 B60 -35.7(16) . . . . ?
B25 C53 B22 B23 104.5(17) . . . . ?
B25 C53 B22 B21 4(2) . . . . ?
B25 C53 B22 B20 66.6(19) . . . . ?
B25 B24 B26 C54 -40.7(13) . . . . ?
B25 B24 B26 B27 -101.3(17) . . . . ?
B25 B24 B26 B28 -139.7(17) . . . . ?
B25 B24 B23 C53 -34.6(14) . . . . ?
B25 B24 B23 B22 0(2) . . . . ?
B25 B24 B23 B20 66(2) . . . . ?
B25 B24 B23 B28 101.9(17) . . . . ?
B25 B24 B28 B26 36.5(15) . . . . ?
B25 B24 B28 B23 -101.8(18) . . . . ?
B25 B24 B28 B27 -3(2) . . . . ?
B25 B24 B28 B20 -66.5(19) . . . . ?
B25 B26 C54 P6 101.2(13) . . . . ?
B25 B26 C54 B60 -38.5(14) . . . . ?
B25 B26 C54 B21 -104.2(15) . . . . ?
B25 B26 C54 B27 -141.9(15) . . . . ?
B25 B26 B27 C54 33.8(14) . . . . ?
B25 B26 B27 B21 -1(2) . . . . ?
B25 B26 B27 B20 -65(2) . . . . ?
B25 B26 B27 B28 -101.7(17) . . . . ?
B25 B26 B28 B24 -36.1(15) . . . . ?
B25 B26 B28 B23 0(2) . . . . ?
B25 B26 B28 B27 99.9(17) . . . . ?
B25 B26 B28 B20 62.2(19) . . . . ?
B25 B60 C54 P6 -101.3(14) . . . . ?
B25 B60 C54 B26 37.5(15) . . . . ?
B25 B60 C54 B21 141.8(17) . . . . ?
B25 B60 C54 B27 106.5(17) . . . . ?
B25 B60 B21 C54 -33.7(14) . . . . ?
B25 B60 B21 B22 102.5(17) . . . . ?
B25 B60 B21 B27 -1(2) . . . . ?
B25 B60 B21 B20 62.6(18) . . . . ?
B25 B60 B22 C53 32.1(13) . . . . ?
B25 B60 B22 B23 -1.8(19) . . . . ?
B25 B60 B22 B21 -100.7(17) . . . . ?
B25 B60 B22 B20 -61.9(18) . . . . ?
B25 C54 B21 B60 37.2(17) . . . . ?
B25 C54 B21 B22 -3(2) . . . . ?
B25 C54 B21 B27 -105.7(17) . . . . ?
B25 C54 B21 B20 -67.2(19) . . . . ?
B25 C54 B27 B26 -36.4(14) . . . . ?
B25 C54 B27 B21 104.6(15) . . . . ?
B25 C54 B27 B20 64.8(18) . . . . ?
B25 C54 B27 B28 3(2) . . . . ?
B50 B51 B52 B53 -100.5(16) . . . . ?
B50 B51 B52 C106 -135.2(15) . . . . ?
B50 B51 B52 B49 -37.8(14) . . . . ?
B50 B51 C105 P9 -113.3(15) . . . . ?
B50 B51 C105 B56 105.1(15) . . . . ?
B50 B51 C105 B57 35.6(15) . . . . ?
B50 B51 C105 B58 141.7(14) . . . . ?
B50 B51 B58 C106 97.8(14) . . . . ?
B50 B51 B58 B56 -0.9(18) . . . . ?
B50 B51 B58 B54 62.3(18) . . . . ?
B50 B51 B58 C105 -34.0(12) . . . . ?
B50 B52 B49 B53 -140.3(15) . . . . ?
B50 B52 B49 B55 -100.1(16) . . . . ?
B50 B52 B49 B57 -37.7(14) . . . . ?
B50 B49 B55 B53 -101.2(16) . . . . ?
B50 B49 B55 B56 1(2) . . . . ?
B50 B49 B55 B54 -65.1(19) . . . . ?
B50 B49 B55 B57 37.8(13) . . . . ?
B50 B49 B57 B56 -102.5(15) . . . . ?
B50 B49 B57 B55 -137.4(15) . . . . ?
B50 B49 B57 C105 -40.6(13) . . . . ?
B50 B57 C105 P9 113.7(15) . . . . ?
B50 B57 C105 B56 -142.9(15) . . . . ?
B50 B57 C105 B51 -35.4(14) . . . . ?
B50 B57 C105 B58 -105.1(16) . . . . ?
B50 C105 B58 C106 -4.9(17) . . . . ?
B50 C105 B58 B56 -106.4(15) . . . . ?
B50 C105 B58 B51 36.6(13) . . . . ?
B50 C105 B58 B54 -67.1(16) . . . . ?
C154 C152 C153 C149 0(3) . . . . ?
C154 C151 C150 C149 -8(4) . . . . ?
C148 C155 C156 C145 1(2) . . . . ?
C148 C147 C146 C145 6(4) . . . . ?
C64 C63 C62 C61 0(4) . . . . ?
C64 C65 C66 C61 -8(3) . . . . ?
C132 P12 C133 C134 -90.9(16) . . . . ?
C132 P12 C133 C138 89.2(17) . . . . ?
C132 P12 C139 C140 157.6(15) . . . . ?
C132 P12 C139 C144 -20(2) . . . . ?
C132 B45 B46 B43 -94.3(17) . . . . ?
C132 B45 B46 B42 -31.0(14) . . . . ?
C132 B45 B46 B44 -130.9(15) . . . . ?
C132 B45 B47 B41 31.8(14) . . . . ?
C132 B45 B47 B59 96.8(15) . . . . ?
C132 B45 B47 B39 132.9(15) . . . . ?
C132 B45 B44 B46 41.0(13) . . . . ?
C132 B45 B44 B43 5.6(18) . . . . ?
C132 B45 B44 B39 -95.9(15) . . . . ?
C132 B45 B44 B48 -59.6(17) . . . . ?
C132 B45 B39 B47 -38.4(13) . . . . ?
C132 B45 B39 B59 -2(2) . . . . ?
C132 B45 B39 B44 97.6(15) . . . . ?
C132 B45 B39 B48 61.3(19) . . . . ?
C132 B46 B43 C131 0.3(17) . . . . ?
C132 B46 B43 B42 40.9(13) . . . . ?
C132 B46 B43 B44 -98.6(15) . . . . ?
C132 B46 B43 B48 -61.9(18) . . . . ?
C132 B46 B42 C131 -93.0(15) . . . . ?
C132 B46 B42 B43 -131.4(15) . . . . ?
C132 B46 B42 B41 -32.4(13) . . . . ?
C132 B46 B44 B45 -42.1(13) . . . . ?
C132 B46 B44 B43 96.8(16) . . . . ?
C132 B46 B44 B39 -4.2(17) . . . . ?
C132 B46 B44 B48 59.2(18) . . . . ?
C132 B47 B41 C131 95.8(16) . . . . ?
C132 B47 B41 B59 133.3(18) . . . . ?
C132 B47 B41 B42 33.5(14) . . . . ?
C132 B47 B59 C131 -1(2) . . . . ?
C132 B47 B59 B41 -39.5(15) . . . . ?
C132 B47 B59 B39 100.2(17) . . . . ?
C132 B47 B59 B48 62.2(19) . . . . ?
C132 B47 B39 B45 41.7(13) . . . . ?
C132 B47 B39 B59 -97.6(16) . . . . ?
C132 B47 B39 B44 1.3(19) . . . . ?
C132 B47 B39 B48 -61.3(18) . . . . ?
C132 B41 B59 C131 -96.6(16) . . . . ?
C132 B41 B59 B47 40.3(15) . . . . ?
C132 B41 B59 B39 3(2) . . . . ?
C132 B41 B59 B48 -63.1(18) . . . . ?
C132 B41 B42 B46 34.2(14) . . . . ?
C132 B41 B42 C131 131.8(15) . . . . ?
C132 B41 B42 B43 96.8(16) . . . . ?
C40 P4 C41 C42 135.6(19) . . . . ?
C40 P4 C41 C46 -48(2) . . . . ?
C40 P4 C47 C48 -93(2) . . . . ?
C40 P4 C47 C52 92(3) . . . . ?
C40 B4 B5 B8 -99.4(16) . . . . ?
C40 B4 B5 B40 -35.8(13) . . . . ?
C40 B4 B5 B6 -139.7(15) . . . . ?
C40 B4 B6 B8 -0.2(19) . . . . ?
C40 B4 B6 B5 35.9(14) . . . . ?
C40 B4 B6 B3 -98.8(16) . . . . ?
C40 B4 B6 B7 -62.4(18) . . . . ?
C40 B4 B3 B6 102.2(15) . . . . ?
C40 B4 B3 B2 -0.9(19) . . . . ?
C40 B4 B3 B9 -40.7(14) . . . . ?
C40 B4 B3 B7 64.3(18) . . . . ?
C40 B4 B9 B1 34.3(13) . . . . ?
C40 B4 B9 B2 96.8(15) . . . . ?
C40 B4 B9 B3 133.8(15) . . . . ?
C40 B40 B1 C39 -131.6(15) . . . . ?
C40 B40 B1 B2 -98.0(15) . . . . ?
C40 B40 B1 B9 -36.1(14) . . . . ?
C40 B40 B5 B8 137.7(15) . . . . ?
C40 B40 B5 B4 35.3(13) . . . . ?
C40 B40 B5 B6 99.0(15) . . . . ?
C40 B1 B2 C39 -94.8(14) . . . . ?
C40 B1 B2 B3 2.6(18) . . . . ?
C40 B1 B2 B9 40.7(13) . . . . ?
C40 B1 B2 B7 -62.4(17) . . . . ?
C40 B1 B9 B4 -35.0(14) . . . . ?
C40 B1 B9 B2 -132.6(16) . . . . ?
C40 B1 B9 B3 -97.0(16) . . . . ?
C40 B5 B6 B8 101.5(15) . . . . ?
C40 B5 B6 B4 -35.8(13) . . . . ?
C40 B5 B6 B3 4.1(17) . . . . ?
C40 B5 B6 B7 65.9(16) . . . . ?
C41 P4 C40 B4 -15.6(17) . . . . ?
C41 P4 C40 B40 -155.3(13) . . . . ?
C41 P4 C40 B1 134.9(14) . . . . ?
C41 P4 C40 B5 -87.3(14) . . . . ?
C41 P4 C40 B9 59.2(17) . . . . ?
C41 P4 C47 C48 153.4(19) . . . . ?
C41 P4 C47 C52 -22(3) . . . . ?
C134 C133 C138 C137 3(3) . . . . ?
C33 P3 C39 B8 87.3(15) . . . . ?
C33 P3 C39 B40 158.0(13) . . . . ?
C33 P3 C39 B1 -129.5(15) . . . . ?
C33 P3 C39 B2 -55.0(16) . . . . ?
C33 P3 C39 B7 16.0(16) . . . . ?
C33 P3 C27 C28 -168.6(15) . . . . ?
C33 P3 C27 C32 9.8(19) . . . . ?
C33 C34 C35 C36 -7(5) . . . . ?
C106 P10 C113 C118 -85(2) . . . . ?
C106 P10 C113 C114 95(2) . . . . ?
C106 P10 C107 C108 -52(2) . . . . ?
C106 P10 C107 C112 129.5(18) . . . . ?
C106 B53 B54 B56 98.5(15) . . . . ?
C106 B53 B54 B55 134.8(15) . . . . ?
C106 B53 B54 B58 34.4(13) . . . . ?
C106 B53 B52 B50 -98.7(14) . . . . ?
C106 B53 B52 B51 -34.0(13) . . . . ?
C106 B53 B52 B49 -134.8(15) . . . . ?
C106 B53 B49 B50 4.9(19) . . . . ?
C106 B53 B49 B52 40.0(13) . . . . ?
C106 B53 B49 B55 -95.4(15) . . . . ?
C106 B53 B49 B57 -58.7(18) . . . . ?
C106 B53 B55 B56 0.0(19) . . . . ?
C106 B53 B55 B54 -38.1(13) . . . . ?
C106 B53 B55 B49 102.9(15) . . . . ?
C106 B53 B55 B57 65.9(17) . . . . ?
C106 B51 B52 B53 34.6(14) . . . . ?
C106 B51 B52 B50 135.2(15) . . . . ?
C106 B51 B52 B49 97.4(16) . . . . ?
C106 B51 C105 P9 144.4(12) . . . . ?
C106 B51 C105 B50 -102.3(13) . . . . ?
C106 B51 C105 B56 2.9(17) . . . . ?
C106 B51 C105 B57 -66.7(16) . . . . ?
C106 B51 C105 B58 39.4(11) . . . . ?
C106 B51 B58 B56 -98.7(15) . . . . ?
C106 B51 B58 B54 -35.5(13) . . . . ?
C106 B51 B58 C105 -131.9(13) . . . . ?
C106 B54 B55 B53 39.4(13) . . . . ?
C106 B54 B55 B56 -99.4(15) . . . . ?
C106 B54 B55 B49 4.7(19) . . . . ?
C106 B54 B55 B57 -60.6(18) . . . . ?
C106 B54 B58 B56 136.5(15) . . . . ?
C106 B54 B58 B51 35.3(13) . . . . ?
C106 B54 B58 C105 97.5(14) . . . . ?
C106 B52 B49 B53 -40.2(13) . . . . ?
C106 B52 B49 B50 100.1(15) . . . . ?
C106 B52 B49 B55 0.0(19) . . . . ?
C106 B52 B49 B57 62.4(18) . . . . ?
C27 P3 C39 B8 -156.0(13) . . . . ?
C27 P3 C39 B40 -85.3(15) . . . . ?
C27 P3 C39 B1 -12.8(17) . . . . ?
C27 P3 C39 B2 61.7(16) . . . . ?
C27 P3 C39 B7 132.7(14) . . . . ?
C27 P3 C33 C34 127.2(18) . . . . ?
C27 P3 C33 C38 -55(2) . . . . ?
C27 C32 C31 C30 0(3) . . . . ?
B43 B46 C132 P12 -143.6(12) . . . . ?
B43 B46 C132 B45 103.7(15) . . . . ?
B43 B46 C132 B47 66.6(17) . . . . ?
B43 B46 C132 B41 -3.2(19) . . . . ?
B43 B46 C132 B42 -41.5(13) . . . . ?
B43 B46 B42 C131 38.4(14) . . . . ?
B43 B46 B42 C132 131.4(15) . . . . ?
B43 B46 B42 B41 99.0(16) . . . . ?
B43 B46 B44 B45 -138.9(17) . . . . ?
B43 B46 B44 B39 -101.0(17) . . . . ?
B43 B46 B44 B48 -37.6(16) . . . . ?
B43 C131 B41 C132 -4.2(17) . . . . ?
B43 C131 B41 B47 -65.7(17) . . . . ?
B43 C131 B41 B59 -103.1(15) . . . . ?
B43 C131 B41 B42 36.5(13) . . . . ?
B43 C131 B59 B47 64(2) . . . . ?
B43 C131 B59 B41 102.9(16) . . . . ?
B43 C131 B59 B39 0(2) . . . . ?
B43 C131 B59 B48 -40.2(15) . . . . ?
B43 C131 B42 B46 -38.9(14) . . . . ?
B43 C131 B42 C132 -101.0(16) . . . . ?
B43 C131 B42 B41 -139.9(15) . . . . ?
B43 C131 B48 B59 137.7(15) . . . . ?
B43 C131 B48 B44 36.4(14) . . . . ?
B43 C131 B48 B39 99.8(16) . . . . ?
B43 B44 B39 B45 -98.8(16) . . . . ?
B43 B44 B39 B47 -58.7(18) . . . . ?
B43 B44 B39 B59 4(2) . . . . ?
B43 B44 B39 B48 40.8(15) . . . . ?
B43 B44 B48 C131 -35.8(15) . . . . ?
B43 B44 B48 B59 -98.6(17) . . . . ?
B43 B44 B48 B39 -135.2(17) . . . . ?
C141 C142 C143 C144 3(4) . . . . ?
B26 B24 B25 C53 135.9(15) . . . . ?
B26 B24 B25 B60 100.3(15) . . . . ?
B26 B24 B25 C54 40.7(13) . . . . ?
B26 B24 B23 C53 -99.0(17) . . . . ?
B26 B24 B23 B22 -64(2) . . . . ?
B26 B24 B23 B20 1(2) . . . . ?
B26 B24 B23 B28 37.5(16) . . . . ?
B26 B24 B28 B23 -138.3(18) . . . . ?
B26 B24 B28 B27 -39.5(15) . . . . ?
B26 B24 B28 B20 -103.1(18) . . . . ?
B26 B25 B60 C53 98.0(16) . . . . ?
B26 B25 B60 C54 -34.3(14) . . . . ?
B26 B25 B60 B21 0(2) . . . . ?
B26 B25 B60 B22 64.5(18) . . . . ?
B26 B25 C54 P6 -108.1(13) . . . . ?
B26 B25 C54 B60 141.0(15) . . . . ?
B26 B25 C54 B21 105.7(17) . . . . ?
B26 B25 C54 B27 36.8(14) . . . . ?
B26 C54 B21 B60 105.2(16) . . . . ?
B26 C54 B21 B22 65(2) . . . . ?
B26 C54 B21 B27 -37.7(14) . . . . ?
B26 C54 B21 B20 0.9(18) . . . . ?
B26 C54 B27 B21 141.0(15) . . . . ?
B26 C54 B27 B20 101.2(16) . . . . ?
B26 C54 B27 B28 39.0(14) . . . . ?
B26 B27 B20 B23 3(2) . . . . ?
B26 B27 B20 B21 100.7(17) . . . . ?
B26 B27 B20 B22 67(2) . . . . ?
B26 B27 B20 B28 -37.0(16) . . . . ?
B26 B27 B28 B24 38.9(15) . . . . ?
B26 B27 B28 B23 100.4(16) . . . . ?
B26 B27 B28 B20 138.5(16) . . . . ?
C139 P12 C133 C134 154.5(15) . . . . ?
C139 P12 C133 C138 -25.4(18) . . . . ?
C139 P12 C132 B45 -29.1(17) . . . . ?
C139 P12 C132 B46 -100.0(13) . . . . ?
C139 P12 C132 B47 46.4(18) . . . . ?
C139 P12 C132 B41 120.6(14) . . . . ?
C139 P12 C132 B42 -166.6(14) . . . . ?
B56 B54 B55 B53 138.8(15) . . . . ?
B56 B54 B55 B49 104.1(16) . . . . ?
B56 B54 B55 B57 38.8(15) . . . . ?
B56 B54 B58 C106 -136.5(15) . . . . ?
B56 B54 B58 B51 -101.2(16) . . . . ?
B56 B54 B58 C105 -39.1(13) . . . . ?
B56 B55 B57 B50 102.0(15) . . . . ?
B56 B55 B57 B49 140.4(15) . . . . ?
B56 B55 B57 C105 40.1(13) . . . . ?
B56 B57 C105 P9 -103.4(15) . . . . ?
B56 B57 C105 B50 142.9(15) . . . . ?
B56 B57 C105 B51 107.5(16) . . . . ?
B56 B57 C105 B58 37.8(15) . . . . ?
B56 C105 B58 C106 101.5(14) . . . . ?
B56 C105 B58 B51 143.0(14) . . . . ?
B56 C105 B58 B54 39.2(13) . . . . ?
C26 C21 C22 C23 1(3) . . . . ?
C47 P4 C40 B4 -127.3(16) . . . . ?
C47 P4 C40 B40 92.9(15) . . . . ?
C47 P4 C40 B1 23.2(16) . . . . ?
C47 P4 C40 B5 160.9(14) . . . . ?
C47 P4 C40 B9 -52.6(18) . . . . ?
C47 P4 C41 C42 -112(2) . . . . ?
C47 P4 C41 C46 65(2) . . . . ?
C47 C48 C49 C50 3(4) . . . . ?
C138 C133 C134 C135 -4(3) . . . . ?
B47 B45 B46 C132 32.3(13) . . . . ?
B47 B45 B46 B43 -62(2) . . . . ?
B47 B45 B46 B42 1(2) . . . . ?
B47 B45 B46 B44 -98.6(16) . . . . ?
B47 B45 C132 P12 115.3(16) . . . . ?
B47 B45 C132 B46 -141.7(15) . . . . ?
B47 B45 C132 B41 -35.1(16) . . . . ?
B47 B45 C132 B42 -108.4(17) . . . . ?
B47 B45 B44 B46 99.1(15) . . . . ?
B47 B45 B44 B43 63.7(17) . . . . ?
B47 B45 B44 B39 -37.8(13) . . . . ?
B47 B45 B44 B48 -1.5(18) . . . . ?
B47 B45 B39 B59 36.3(15) . . . . ?
B47 B45 B39 B44 136.0(15) . . . . ?
B47 B45 B39 B48 99.8(17) . . . . ?
B47 C132 B41 C131 -100.8(16) . . . . ?
B47 C132 B41 B59 -39.9(15) . . . . ?
B47 C132 B41 B42 -142.0(17) . . . . ?
B47 C132 B42 B46 -104.2(18) . . . . ?
B47 C132 B42 C131 -2(2) . . . . ?
B47 C132 B42 B43 -62(2) . . . . ?
B47 C132 B42 B41 37.7(17) . . . . ?
B47 B41 B59 C131 -136.9(17) . . . . ?
B47 B41 B59 B39 -37.2(16) . . . . ?
B47 B41 B59 B48 -103.3(17) . . . . ?
B47 B41 B42 B46 0(2) . . . . ?
B47 B41 B42 C131 97.8(16) . . . . ?
B47 B41 B42 C132 -34.0(14) . . . . ?
B47 B41 B42 B43 62.8(18) . . . . ?
B47 B59 B39 B45 -37.1(15) . . . . ?
B47 B59 B39 B44 -102.5(16) . . . . ?
B47 B59 B39 B48 -139.2(15) . . . . ?
B47 B59 B48 C131 -98.3(16) . . . . ?
B47 B59 B48 B43 -61.8(18) . . . . ?
B47 B59 B48 B44 0.5(19) . . . . ?
B47 B59 B48 B39 38.0(14) . . . . ?
B47 B39 B48 C131 2.3(19) . . . . ?
B47 B39 B48 B43 63(2) . . . . ?
B47 B39 B48 B59 -36.1(14) . . . . ?
B47 B39 B48 B44 102.2(16) . . . . ?
C30 C29 C28 C27 2(3) . . . . ?
B16 C13 B13 B14 3.9(19) . . . . ?
B16 C13 B13 B19 105.3(16) . . . . ?
B16 C13 B13 B15 -36.1(15) . . . . ?
B16 C13 B13 B12 66.5(18) . . . . ?
B16 C13 B18 C14 -100.5(14) . . . . ?
B16 C13 B18 B17 -38.5(13) . . . . ?
B16 C13 B18 B19 -140.4(15) . . . . ?
B16 C13 B19 C14 -0.8(18) . . . . ?
B16 C13 B19 B13 -102.7(16) . . . . ?
B16 C13 B19 B18 37.2(13) . . . . ?
B16 C13 B19 B12 -63.3(18) . . . . ?
B16 C13 B15 B13 141.1(16) . . . . ?
B16 C13 B15 B14 102.0(18) . . . . ?
B16 C13 B15 B10 38.2(14) . . . . ?
B16 B17 B18 C13 38.6(13) . . . . ?
B16 B17 B18 C14 135.3(15) . . . . ?
B16 B17 B18 B19 99.2(16) . . . . ?
B16 B17 B11 C14 -98.2(15) . . . . ?
B16 B17 B11 B14 -1.2(18) . . . . ?
B16 B17 B11 B10 38.9(14) . . . . ?
B16 B17 B11 B12 -63.8(17) . . . . ?
B16 B17 B10 B14 -97.6(16) . . . . ?
B16 B17 B10 B11 -136.4(15) . . . . ?
B16 B17 B10 B15 -36.7(14) . . . . ?
B16 B18 B19 C13 -35.3(13) . . . . ?
B16 B18 B19 C14 99.1(15) . . . . ?
B16 B18 B19 B13 2(2) . . . . ?
B16 B18 B19 B12 65.1(18) . . . . ?
B16 B10 B15 C13 -37.6(13) . . . . ?
B16 B10 B15 B13 -100.7(16) . . . . ?
B16 B10 B15 B14 -135.4(15) . . . . ?
C140 C139 C144 C143 4(3) . . . . ?
C28 C29 C30 C31 -1(3) . . . . ?
C28 C27 C32 C31 2(3) . . . . ?
C43 C44 C45 C46 2(4) . . . . ?
C144 C139 C140 C141 -4(3) . . . . ?
B51 B50 B52 B53 103.5(15) . . . . ?
B51 B50 B52 C106 39.2(12) . . . . ?
B51 B50 B52 B49 138.6(15) . . . . ?
B51 B50 B49 B53 -1.7(19) . . . . ?
B51 B50 B49 B52 -36.9(13) . . . . ?
B51 B50 B49 B55 63.1(18) . . . . ?
B51 B50 B49 B57 100.6(15) . . . . ?
B51 B50 B57 B56 -0.4(19) . . . . ?
B51 B50 B57 B49 -100.6(16) . . . . ?
B51 B50 B57 B55 -62.7(17) . . . . ?
B51 B50 B57 C105 32.8(13) . . . . ?
B51 B50 C105 P9 108.9(14) . . . . ?
B51 B50 C105 B56 -107.1(16) . . . . ?
B51 B50 C105 B57 -143.0(15) . . . . ?
B51 B50 C105 B58 -37.1(13) . . . . ?
B51 C106 B54 B53 101.7(15) . . . . ?
B51 C106 B54 B56 0.5(18) . . . . ?
B51 C106 B54 B55 62.1(17) . . . . ?
B51 C106 B54 B58 -38.2(14) . . . . ?
B51 C106 B52 B53 -142.5(15) . . . . ?
B51 C106 B52 B50 -39.8(13) . . . . ?
B51 C106 B52 B49 -103.5(15) . . . . ?
B51 C106 B58 B56 102.6(15) . . . . ?
B51 C106 B58 B54 140.8(14) . . . . ?
B51 C106 B58 C105 41.2(12) . . . . ?
B51 B52 B49 B53 -102.7(16) . . . . ?
B51 B52 B49 B50 37.7(14) . . . . ?
B51 B52 B49 B55 -62.4(19) . . . . ?
B51 B52 B49 B57 0(2) . . . . ?
B51 C105 B58 C106 -41.5(12) . . . . ?
B51 C105 B58 B56 -143.0(14) . . . . ?
B51 C105 B58 B54 -103.8(14) . . . . ?
C98 C93 C94 C95 -6(3) . . . . ?
C98 C97 C96 C95 0(5) . . . . ?
C42 C41 C46 C45 2(4) . . . . ?
C42 C43 C44 C45 -3(4) . . . . ?
C51 C50 C49 C48 -9(4) . . . . ?
C32 C27 C28 C29 -3(3) . . . . ?
B14 B13 B19 C13 96.3(16) . . . . ?
B14 B13 B19 C14 0.4(19) . . . . ?
B14 B13 B19 B18 60.6(18) . . . . ?
B14 B13 B19 B12 -39.4(14) . . . . ?
B14 B13 B15 C13 -133.9(16) . . . . ?
B14 B13 B15 B16 -99.5(18) . . . . ?
B14 B13 B15 B10 -36.0(14) . . . . ?
B14 B13 B12 C14 96.9(15) . . . . ?
B14 B13 B12 B11 35.7(13) . . . . ?
B14 B13 B12 B19 135.8(16) . . . . ?
B14 B11 B10 B16 97.5(16) . . . . ?
B14 B11 B10 B17 135.4(15) . . . . ?
B14 B11 B10 B15 35.2(14) . . . . ?
B14 B11 B12 C14 -132.8(15) . . . . ?
B14 B11 B12 B13 -35.0(14) . . . . ?
B14 B11 B12 B19 -97.7(16) . . . . ?
B14 B10 B15 C13 97.7(16) . . . . ?
B14 B10 B15 B13 34.6(13) . . . . ?
B14 B10 B15 B16 135.4(15) . . . . ?
B60 C53 B24 B25 40.0(14) . . . . ?
B60 C53 B24 B26 0.7(19) . . . . ?
B60 C53 B24 B23 -101.6(16) . . . . ?
B60 C53 B24 B28 -62.4(19) . . . . ?
B60 C53 B25 B24 -139.0(15) . . . . ?
B60 C53 B25 B26 -100.3(16) . . . . ?
B60 C53 B25 C54 -39.6(14) . . . . ?
B60 C53 B23 B24 106.2(16) . . . . ?
B60 C53 B23 B22 -36.1(14) . . . . ?
B60 C53 B23 B20 5(2) . . . . ?
B60 C53 B23 B28 67.7(19) . . . . ?
B60 C53 B22 B23 140.2(16) . . . . ?
B60 C53 B22 B21 39.8(15) . . . . ?
B60 C53 B22 B20 102.3(15) . . . . ?
B60 B25 B26 B24 -98.8(15) . . . . ?
B60 B25 B26 C54 33.6(13) . . . . ?
B60 B25 B26 B27 0.2(19) . . . . ?
B60 B25 B26 B28 -62.4(19) . . . . ?
B60 B25 C54 P6 110.9(15) . . . . ?
B60 B25 C54 B26 -141.0(15) . . . . ?
B60 B25 C54 B21 -35.3(16) . . . . ?
B60 B25 C54 B27 -104.2(16) . . . . ?
B60 C54 B21 B22 -39.8(16) . . . . ?
B60 C54 B21 B27 -142.9(16) . . . . ?
B60 C54 B21 B20 -104.4(16) . . . . ?
B60 C54 B27 B26 -106.9(16) . . . . ?
B60 C54 B27 B21 34.1(15) . . . . ?
B60 C54 B27 B20 -6(2) . . . . ?
B60 C54 B27 B28 -67.9(19) . . . . ?
B60 B21 B22 C53 -40.2(15) . . . . ?
B60 B21 B22 B23 -99.2(16) . . . . ?
B60 B21 B22 B20 -136.6(16) . . . . ?
B60 B21 B27 B26 1(2) . . . . ?
B60 B21 B27 C54 -33.8(14) . . . . ?
B60 B21 B27 B20 101.6(17) . . . . ?
B60 B21 B27 B28 64.0(19) . . . . ?
B60 B21 B20 B23 1(2) . . . . ?
B60 B21 B20 B22 39.8(14) . . . . ?
B60 B21 B20 B27 -101.6(16) . . . . ?
B60 B21 B20 B28 -63.9(19) . . . . ?
B60 B22 B20 B23 98.6(16) . . . . ?
B60 B22 B20 B21 -37.6(14) . . . . ?
B60 B22 B20 B27 -3(2) . . . . ?
B60 B22 B20 B28 61(2) . . . . ?
C99 P9 C93 C94 49.1(17) . . . . ?
C99 P9 C93 C98 -131.8(16) . . . . ?
C99 P9 C105 B50 -60.9(15) . . . . ?
C99 P9 C105 B56 154.9(13) . . . . ?
C99 P9 C105 B51 12.7(15) . . . . ?
C99 P9 C105 B57 -134.6(14) . . . . ?
C99 P9 C105 B58 84.5(13) . . . . ?
C99 C100 C101 C102 1(3) . . . . ?
C99 C104 C103 C102 5(3) . . . . ?
C59 C60 C55 P6 -174.5(18) . . . . ?
C59 C60 C55 C56 8(4) . . . . ?
C59 C58 C57 C56 -3(4) . . . . ?
C61 P6 C54 B25 168.9(13) . . . . ?
C61 P6 C54 B26 101.3(14) . . . . ?
C61 P6 C54 B60 -120.2(13) . . . . ?
C61 P6 C54 B21 -50.0(18) . . . . ?
C61 P6 C54 B27 28.4(17) . . . . ?
C61 P6 C55 C60 -149.5(19) . . . . ?
C61 P6 C55 C56 28(2) . . . . ?
C8 C7 C12 C11 -1(4) . . . . ?
C8 C9 C10 C11 1(5) . . . . ?
C34 C33 C38 C37 -2(3) . . . . ?
C34 C35 C36 C37 4(5) . . . . ?
B23 C53 B24 B25 141.6(15) . . . . ?
B23 C53 B24 B26 102.3(16) . . . . ?
B23 C53 B24 B28 39.2(15) . . . . ?
B23 C53 B25 B24 -36.6(15) . . . . ?
B23 C53 B25 B26 2(2) . . . . ?
B23 C53 B25 B60 102.3(16) . . . . ?
B23 C53 B25 C54 62.7(19) . . . . ?
B23 C53 B60 B25 -106.6(16) . . . . ?
B23 C53 B60 C54 -66.7(17) . . . . ?
B23 C53 B60 B21 -5(2) . . . . ?
B23 C53 B60 B22 37.0(15) . . . . ?
B23 C53 B22 B60 -140.2(16) . . . . ?
B23 C53 B22 B21 -100.4(17) . . . . ?
B23 C53 B22 B20 -37.9(13) . . . . ?
B23 B24 B25 C53 34.5(13) . . . . ?
B23 B24 B25 B26 -101.4(16) . . . . ?
B23 B24 B25 B60 -1.1(19) . . . . ?
B23 B24 B25 C54 -60.8(18) . . . . ?
B23 B24 B26 B25 101.8(18) . . . . ?
B23 B24 B26 C54 61.0(19) . . . . ?
B23 B24 B26 B27 1(2) . . . . ?
B23 B24 B26 B28 -38.0(16) . . . . ?
B23 B24 B28 B26 138.3(18) . . . . ?
B23 B24 B28 B27 98.9(18) . . . . ?
B23 B24 B28 B20 35.3(16) . . . . ?
B23 B22 B20 B21 -136.1(15) . . . . ?
B23 B22 B20 B27 -101.7(16) . . . . ?
B23 B22 B20 B28 -38.0(15) . . . . ?
B23 B20 B28 B24 -35.3(15) . . . . ?
B23 B20 B28 B26 -98.2(17) . . . . ?
B23 B20 B28 B27 -136.1(17) . . . . ?
C23 C24 C25 C26 1(4) . . . . ?
C79 P7 C73 C74 -101(2) . . . . ?
C79 P7 C73 C78 84.9(19) . . . . ?
C79 P7 C67 C72 -126(2) . . . . ?
C79 P7 C67 C68 55(3) . . . . ?
C79 B32 B33 B34 -136(2) . . . . ?
C79 B32 B33 B36 -33.6(19) . . . . ?
C79 B32 B33 B35 -93(2) . . . . ?
C79 B32 B34 C80 -95(2) . . . . ?
C79 B32 B34 B33 39(2) . . . . ?
C79 B32 B34 B35 -1(3) . . . . ?
C79 B32 B34 B37 -56(3) . . . . ?
C79 B32 B31 C80 129.2(18) . . . . ?
C79 B32 B31 B30 33.9(18) . . . . ?
C79 B32 B31 B38 97(2) . . . . ?
C79 B33 B34 C80 2(2) . . . . ?
C79 B33 B34 B32 -37.7(18) . . . . ?
C79 B33 B34 B35 94(2) . . . . ?
C79 B33 B34 B37 63(2) . . . . ?
C79 B33 B36 B30 -32(2) . . . . ?
C79 B33 B36 B29 -96(2) . . . . ?
C79 B33 B36 B35 -132(2) . . . . ?
C79 B33 B35 B34 -101(2) . . . . ?
C79 B33 B35 B36 39(2) . . . . ?
C79 B33 B35 B29 2(3) . . . . ?
C79 B33 B35 B37 -64(3) . . . . ?
C79 B31 B30 B36 30(2) . . . . ?
C79 B31 B30 B38 133(2) . . . . ?
C79 B31 B30 B29 97(3) . . . . ?
C79 B31 B38 C80 90(2) . . . . ?
C79 B31 B38 B30 -41(2) . . . . ?
C79 B31 B38 B29 -7(3) . . . . ?
C79 B31 B38 B37 54(3) . . . . ?
C79 B30 B36 B33 31(2) . . . . ?
C79 B30 B36 B29 133(2) . . . . ?
C79 B30 B36 B35 96(2) . . . . ?
C79 B30 B38 C80 -4(3) . . . . ?
C79 B30 B38 B31 39.4(19) . . . . ?
C79 B30 B38 B29 -102(2) . . . . ?
C79 B30 B38 B37 -64(2) . . . . ?
C79 B30 B29 B36 -40(2) . . . . ?
C79 B30 B29 B38 95(2) . . . . ?
C79 B30 B29 B35 -5(3) . . . . ?
C79 B30 B29 B37 53(3) . . . . ?
C79 B36 B29 B30 42(2) . . . . ?
C79 B36 B29 B38 1(3) . . . . ?
C79 B36 B29 B35 -97(3) . . . . ?
C79 B36 B29 B37 -64(3) . . . . ?
C79 B36 B35 B33 -40(2) . . . . ?
C79 B36 B35 B34 -3(3) . . . . ?
C79 B36 B35 B29 101(2) . . . . ?
C79 B36 B35 B37 63(3) . . . . ?
C128 C127 C126 C125 4(4) . . . . ?
B17 C14 B18 C13 101.8(14) . . . . ?
B17 C14 B18 B16 39.3(14) . . . . ?
B17 C14 B18 B19 140.2(14) . . . . ?
B17 C14 B11 B14 -101.1(16) . . . . ?
B17 C14 B11 B10 -37.5(14) . . . . ?
B17 C14 B11 B12 -141.9(15) . . . . ?
B17 C14 B19 C13 1.2(18) . . . . ?
B17 C14 B19 B13 65.1(18) . . . . ?
B17 C14 B19 B18 -37.5(13) . . . . ?
B17 C14 B19 B12 104.7(15) . . . . ?
B17 C14 B12 B13 -64.3(18) . . . . ?
B17 C14 B12 B14 -4.0(19) . . . . ?
B17 C14 B12 B11 36.7(15) . . . . ?
B17 C14 B12 B19 -103.5(16) . . . . ?
B17 B16 B18 C13 -136.6(15) . . . . ?
B17 B16 B18 C14 -39.1(14) . . . . ?
B17 B16 B18 B19 -102.4(15) . . . . ?
B17 B16 B10 B14 100.3(15) . . . . ?
B17 B16 B10 B11 38.9(14) . . . . ?
B17 B16 B10 B15 138.4(15) . . . . ?
B17 B16 B15 C13 98.5(15) . . . . ?
B17 B16 B15 B13 63.6(19) . . . . ?
B17 B16 B15 B14 2(2) . . . . ?
B17 B16 B15 B10 -38.0(14) . . . . ?
B17 B18 B19 C13 -98.7(15) . . . . ?
B17 B18 B19 C14 35.7(13) . . . . ?
B17 B18 B19 B13 -61.8(19) . . . . ?
B17 B18 B19 B12 1.7(19) . . . . ?
B17 B11 B10 B16 -37.9(14) . . . . ?
B17 B11 B10 B14 -135.4(15) . . . . ?
B17 B11 B10 B15 -100.2(16) . . . . ?
B17 B11 B12 C14 -33.3(13) . . . . ?
B17 B11 B12 B13 64.5(17) . . . . ?
B17 B11 B12 B14 99.5(16) . . . . ?
B17 B11 B12 B19 1.8(19) . . . . ?
B17 B10 B15 C13 -1.4(19) . . . . ?
B17 B10 B15 B13 -64.5(18) . . . . ?
B17 B10 B15 B16 36.3(14) . . . . ?
B17 B10 B15 B14 -99.1(15) . . . . ?
C24 C23 C22 C21 1(3) . . . . ?
C84 C85 C86 C81 0(3) . . . . ?
C85 C84 C83 C82 -6(3) . . . . ?
C85 C86 C81 P8 176.1(15) . . . . ?
C85 C86 C81 C82 1(3) . . . . ?
C21 P2 C14 B17 -55.9(16) . . . . ?
C21 P2 C14 B18 -131.9(15) . . . . ?
C21 P2 C14 B11 19.9(16) . . . . ?
C21 P2 C14 B19 155.5(13) . . . . ?
C21 P2 C14 B12 88.3(13) . . . . ?
C21 P2 C15 C16 -8.0(10) . . . . ?
C21 P2 C15 C20 178.3(8) . . . . ?
C21 C26 C25 C24 1(4) . . . . ?
C124 C119 C120 C121 1(3) . . . . ?
C2 C1 C6 C5 -5(4) . . . . ?
C2 C3 C4 C5 -4(6) . . . . ?
B54 B53 C106 P10 106.4(16) . . . . ?
B54 B53 C106 B51 -107.1(15) . . . . ?
B54 B53 C106 B52 -141.9(16) . . . . ?
B54 B53 C106 B58 -38.3(14) . . . . ?
B54 B53 B52 B50 -65.3(17) . . . . ?
B54 B53 B52 C106 33.3(13) . . . . ?
B54 B53 B52 B51 -1(2) . . . . ?
B54 B53 B52 B49 -101.4(16) . . . . ?
B54 B53 B49 B50 66.1(18) . . . . ?
B54 B53 B49 B52 101.1(15) . . . . ?
B54 B53 B49 B55 -34.2(13) . . . . ?
B54 B53 B49 B57 2.5(19) . . . . ?
B54 B53 B55 B56 38.1(15) . . . . ?
B54 B53 B55 B49 141.0(15) . . . . ?
B54 B53 B55 B57 104.0(15) . . . . ?
B54 C106 B51 B50 -62.9(17) . . . . ?
B54 C106 B51 B52 -102.2(15) . . . . ?
B54 C106 B51 C105 -2.0(17) . . . . ?
B54 C106 B51 B58 37.9(13) . . . . ?
B54 C106 B52 B53 -36.0(14) . . . . ?
B54 C106 B52 B50 66.7(17) . . . . ?
B54 C106 B52 B51 106.5(15) . . . . ?
B54 C106 B52 B49 3.0(19) . . . . ?
B54 C106 B58 B56 -38.2(14) . . . . ?
B54 C106 B58 B51 -140.8(14) . . . . ?
B54 C106 B58 C105 -99.5(14) . . . . ?
B54 B56 B55 B53 -38.5(15) . . . . ?
B54 B56 B55 B49 -101.5(16) . . . . ?
B54 B56 B55 B57 -138.2(15) . . . . ?
B54 B56 B57 B50 -62.6(17) . . . . ?
B54 B56 B57 B49 1.8(18) . . . . ?
B54 B56 B57 B55 37.1(13) . . . . ?
B54 B56 B57 C105 -96.0(15) . . . . ?
B54 B56 C105 P9 -146.5(12) . . . . ?
B54 B56 C105 B50 66.3(18) . . . . ?
B54 B56 C105 B51 -2.7(18) . . . . ?
B54 B56 C105 B57 102.1(15) . . . . ?
B54 B56 C105 B58 -39.1(13) . . . . ?
B54 B56 B58 C106 38.5(14) . . . . ?
B54 B56 B58 B51 101.6(15) . . . . ?
B54 B56 B58 C105 134.8(15) . . . . ?
B54 B55 B57 B50 63.5(18) . . . . ?
B54 B55 B57 B56 -38.5(14) . . . . ?
B54 B55 B57 B49 101.9(16) . . . . ?
B54 B55 B57 C105 1.6(19) . . . . ?
C50 C51 C52 C47 -11(4) . . . . ?
C54 P6 C61 C62 -163.3(17) . . . . ?
C54 P6 C61 C66 23(3) . . . . ?
C54 P6 C55 C60 95(2) . . . . ?
C54 P6 C55 C56 -88(2) . . . . ?
C54 B25 B26 B24 -132.5(15) . . . . ?
C54 B25 B26 B27 -33.4(13) . . . . ?
C54 B25 B26 B28 -96.1(16) . . . . ?
C54 B25 B60 C53 132.3(16) . . . . ?
C54 B25 B60 B21 34.5(14) . . . . ?
C54 B25 B60 B22 98.7(16) . . . . ?
C54 B26 B27 B21 -34.4(13) . . . . ?
C54 B26 B27 B20 -98.7(17) . . . . ?
C54 B26 B27 B28 -135.5(16) . . . . ?
C54 B26 B28 B24 -98.0(16) . . . . ?
C54 B26 B28 B23 -61.6(18) . . . . ?
C54 B26 B28 B27 38.0(14) . . . . ?
C54 B26 B28 B20 0.3(19) . . . . ?
C54 B60 B21 B22 136.2(17) . . . . ?
C54 B60 B21 B27 33.1(14) . . . . ?
C54 B60 B21 B20 96.2(17) . . . . ?
C54 B60 B22 C53 93.8(16) . . . . ?
C54 B60 B22 B23 59.8(18) . . . . ?
C54 B60 B22 B21 -39.0(14) . . . . ?
C54 B60 B22 B20 -0.2(19) . . . . ?
C54 B21 B22 C53 -1(2) . . . . ?
C54 B21 B22 B60 39.3(15) . . . . ?
C54 B21 B22 B23 -59.9(19) . . . . ?
C54 B21 B22 B20 -97.2(17) . . . . ?
C54 B21 B27 B26 34.5(13) . . . . ?
C54 B21 B27 B20 135.4(15) . . . . ?
C54 B21 B27 B28 97.8(15) . . . . ?
C54 B21 B20 B23 64.3(17) . . . . ?
C54 B21 B20 B22 103.1(15) . . . . ?
C54 B21 B20 B27 -38.3(13) . . . . ?
C54 B21 B20 B28 -0.6(18) . . . . ?
C54 B27 B20 B23 -59(2) . . . . ?
C54 B27 B20 B21 38.7(14) . . . . ?
C54 B27 B20 B22 5(2) . . . . ?
C54 B27 B20 B28 -99.0(16) . . . . ?
C54 B27 B28 B24 0(2) . . . . ?
C54 B27 B28 B26 -38.6(14) . . . . ?
C54 B27 B28 B23 61.8(17) . . . . ?
C54 B27 B28 B20 99.9(16) . . . . ?
B21 B60 C54 P6 116.8(15) . . . . ?
B21 B60 C54 B25 -141.8(17) . . . . ?
B21 B60 C54 B26 -104.3(17) . . . . ?
B21 B60 C54 B27 -35.3(16) . . . . ?
B21 B60 B22 C53 132.8(17) . . . . ?
B21 B60 B22 B23 98.9(17) . . . . ?
B21 B60 B22 B20 38.8(15) . . . . ?
B21 C54 B27 B26 -141.0(15) . . . . ?
B21 C54 B27 B20 -39.8(14) . . . . ?
B21 C54 B27 B28 -101.9(16) . . . . ?
B21 B22 B20 B23 136.1(15) . . . . ?
B21 B22 B20 B27 34.4(14) . . . . ?
B21 B22 B20 B28 98.1(17) . . . . ?
B21 B27 B20 B23 -97.5(17) . . . . ?
B21 B27 B20 B22 -33.4(14) . . . . ?
B21 B27 B20 B28 -137.7(15) . . . . ?
B21 B27 B28 B24 -61.4(19) . . . . ?
B21 B27 B28 B26 -100.3(16) . . . . ?
B21 B27 B28 B23 0.2(19) . . . . ?
B21 B27 B28 B20 38.2(14) . . . . ?
B21 B20 B28 B24 63.1(19) . . . . ?
B21 B20 B28 B26 0(2) . . . . ?
B21 B20 B28 B23 98.5(16) . . . . ?
B21 B20 B28 B27 -37.6(14) . . . . ?
C44 C43 C42 C41 4(4) . . . . ?
C44 C45 C46 C41 -2(4) . . . . ?
C55 P6 C61 C62 85.2(19) . . . . ?
C55 P6 C61 C66 -88(2) . . . . ?
C55 P6 C54 B25 -78.0(15) . . . . ?
C55 P6 C54 B26 -145.7(14) . . . . ?
C55 P6 C54 B60 -7.1(15) . . . . ?
C55 P6 C54 B21 63.0(17) . . . . ?
C55 P6 C54 B27 141.5(16) . . . . ?
C55 C60 C59 C58 -8(4) . . . . ?
C55 C56 C57 C58 3(3) . . . . ?
B52 B53 C106 P10 -111.7(16) . . . . ?
B52 B53 C106 B51 34.7(14) . . . . ?
B52 B53 C106 B54 141.9(16) . . . . ?
B52 B53 C106 B58 103.6(17) . . . . ?
B52 B53 B54 C106 -34.0(14) . . . . ?
B52 B53 B54 B56 64.5(17) . . . . ?
B52 B53 B54 B55 100.8(16) . . . . ?
B52 B53 B54 B58 0.3(19) . . . . ?
B52 B53 B49 B50 -35.1(13) . . . . ?
B52 B53 B49 B55 -135.4(14) . . . . ?
B52 B53 B49 B57 -98.7(16) . . . . ?
B52 B53 B55 B56 -62.0(18) . . . . ?
B52 B53 B55 B54 -100.1(15) . . . . ?
B52 B53 B55 B49 40.9(13) . . . . ?
B52 B53 B55 B57 3.9(18) . . . . ?
B52 B50 B51 C106 -39.2(13) . . . . ?
B52 B50 B51 C105 -132.2(15) . . . . ?
B52 B50 B51 B58 -98.8(15) . . . . ?
B52 B50 B49 B53 35.1(14) . . . . ?
B52 B50 B49 B55 99.9(16) . . . . ?
B52 B50 B49 B57 137.5(15) . . . . ?
B52 B50 B57 B56 62.4(17) . . . . ?
B52 B50 B57 B49 -37.7(13) . . . . ?
B52 B50 B57 B55 0.2(18) . . . . ?
B52 B50 B57 C105 95.6(14) . . . . ?
B52 B50 C105 P9 150.0(12) . . . . ?
B52 B50 C105 B56 -66.0(17) . . . . ?
B52 B50 C105 B51 41.1(13) . . . . ?
B52 B50 C105 B57 -101.8(15) . . . . ?
B52 B50 C105 B58 4.1(17) . . . . ?
B52 C106 B51 B50 39.3(13) . . . . ?
B52 C106 B51 C105 100.2(14) . . . . ?
B52 C106 B51 B58 140.1(14) . . . . ?
B52 C106 B54 B53 34.8(14) . . . . ?
B52 C106 B54 B56 -66.4(17) . . . . ?
B52 C106 B54 B55 -4.8(18) . . . . ?
B52 C106 B54 B58 -105.2(16) . . . . ?
B52 C106 B58 B56 65.1(17) . . . . ?
B52 C106 B58 B51 -37.5(13) . . . . ?
B52 C106 B58 B54 103.3(15) . . . . ?
B52 C106 B58 C105 3.7(17) . . . . ?
B52 B51 C105 P9 -154.6(13) . . . . ?
B52 B51 C105 B50 -41.3(13) . . . . ?
B52 B51 C105 B56 63.8(17) . . . . ?
B52 B51 C105 B57 -5.7(19) . . . . ?
B52 B51 C105 B58 100.4(15) . . . . ?
B52 B51 B58 C106 35.1(13) . . . . ?
B52 B51 B58 B56 -63.6(17) . . . . ?
B52 B51 B58 B54 -0.4(18) . . . . ?
B52 B51 B58 C105 -96.7(14) . . . . ?
B52 B49 B55 B53 -39.1(13) . . . . ?
B52 B49 B55 B56 62.9(19) . . . . ?
B52 B49 B55 B54 -3(2) . . . . ?
B52 B49 B55 B57 99.9(15) . . . . ?
B52 B49 B57 B50 37.3(14) . . . . ?
B52 B49 B57 B56 -65.2(18) . . . . ?
B52 B49 B57 B55 -100.1(16) . . . . ?
B52 B49 B57 C105 -3(2) . . . . ?
C25 C26 C21 P2 175.9(19) . . . . ?
C25 C26 C21 C22 -2(3) . . . . ?
B41 C131 B43 B46 2.5(19) . . . . ?
B41 C131 B43 B42 -37.7(14) . . . . ?
B41 C131 B43 B44 68.7(18) . . . . ?
B41 C131 B43 B48 104.7(15) . . . . ?
B41 C131 B59 B47 -38.4(15) . . . . ?
B41 C131 B59 B39 -103.3(17) . . . . ?
B41 C131 B59 B48 -143.0(15) . . . . ?
B41 C131 B42 B46 101.0(16) . . . . ?
B41 C131 B42 C132 38.9(14) . . . . ?
B41 C131 B42 B43 139.9(15) . . . . ?
B41 C131 B48 B43 -103.2(16) . . . . ?
B41 C131 B48 B59 34.5(14) . . . . ?
B41 C131 B48 B44 -66.8(19) . . . . ?
B41 C131 B48 B39 -3.4(19) . . . . ?
B41 C132 B47 B45 144.2(16) . . . . ?
B41 C132 B47 B59 41.1(16) . . . . ?
B41 C132 B47 B39 102.7(17) . . . . ?
B41 C132 B42 B46 -141.9(15) . . . . ?
B41 C132 B42 C131 -39.9(14) . . . . ?
B41 C132 B42 B43 -100.0(16) . . . . ?
B41 B47 B59 C131 38.3(15) . . . . ?
B41 B47 B59 B39 139.7(17) . . . . ?
B41 B47 B59 B48 101.7(17) . . . . ?
B41 B47 B39 B45 102.6(16) . . . . ?
B41 B47 B39 B59 -36.7(15) . . . . ?
B41 B47 B39 B44 62.2(19) . . . . ?
B41 B47 B39 B48 0(2) . . . . ?
B41 B59 B39 B45 0(2) . . . . ?
B41 B59 B39 B47 36.6(15) . . . . ?
B41 B59 B39 B44 -66(2) . . . . ?
B41 B59 B39 B48 -102.5(17) . . . . ?
B41 B59 B48 C131 -33.6(13) . . . . ?
B41 B59 B48 B43 2.8(19) . . . . ?
B41 B59 B48 B44 65.2(18) . . . . ?
B41 B59 B48 B39 102.7(16) . . . . ?
B22 C53 B24 B25 105.7(16) . . . . ?
B22 C53 B24 B26 66.4(18) . . . . ?
B22 C53 B24 B23 -36.0(14) . . . . ?
B22 C53 B24 B28 3(2) . . . . ?
B22 C53 B25 B24 -104.8(17) . . . . ?
B22 C53 B25 B26 -66(2) . . . . ?
B22 C53 B25 B60 34.1(15) . . . . ?
B22 C53 B25 C54 -5(2) . . . . ?
B22 C53 B60 B25 -143.6(16) . . . . ?
B22 C53 B60 C54 -103.7(15) . . . . ?
B22 C53 B60 B21 -41.6(14) . . . . ?
B22 C53 B23 B24 142.3(15) . . . . ?
B22 C53 B23 B20 41.4(14) . . . . ?
B22 C53 B23 B28 103.9(16) . . . . ?
B22 B60 C54 P6 155.9(13) . . . . ?
B22 B60 C54 B25 -102.7(17) . . . . ?
B22 B60 C54 B26 -65.2(18) . . . . ?
B22 B60 C54 B21 39.1(15) . . . . ?
B22 B60 C54 B27 4(2) . . . . ?
B22 B60 B21 C54 -136.2(17) . . . . ?
B22 B60 B21 B27 -103.1(18) . . . . ?
B22 B60 B21 B20 -39.9(15) . . . . ?
B22 B23 B20 B21 37.3(13) . . . . ?
B22 B23 B20 B27 100.0(17) . . . . ?
B22 B23 B20 B28 139.3(16) . . . . ?
B22 B23 B28 B24 102.0(17) . . . . ?
B22 B23 B28 B26 65.2(18) . . . . ?
B22 B23 B28 B27 1.4(19) . . . . ?
B22 B23 B28 B20 -37.6(15) . . . . ?
B22 B21 B27 B26 -65.0(19) . . . . ?
B22 B21 B27 C54 -99.5(16) . . . . ?
B22 B21 B27 B20 35.9(14) . . . . ?
B22 B21 B27 B28 -2(2) . . . . ?
B22 B21 B20 B23 -38.8(14) . . . . ?
B22 B21 B20 B27 -141.4(15) . . . . ?
B22 B21 B20 B28 -103.7(16) . . . . ?
B22 B20 B28 B24 2(2) . . . . ?
B22 B20 B28 B26 -60.8(19) . . . . ?
B22 B20 B28 B23 37.5(15) . . . . ?
B22 B20 B28 B27 -98.6(17) . . . . ?
B59 C131 B43 B46 -63.4(18) . . . . ?
B59 C131 B43 B42 -103.6(15) . . . . ?
B59 C131 B43 B44 3(2) . . . . ?
B59 C131 B43 B48 38.9(14) . . . . ?
B59 C131 B41 C132 99.0(15) . . . . ?
B59 C131 B41 B47 37.4(14) . . . . ?
B59 C131 B41 B42 139.6(15) . . . . ?
B59 C131 B42 B46 63(2) . . . . ?
B59 C131 B42 C132 1(2) . . . . ?
B59 C131 B42 B43 102.3(16) . . . . ?
B59 C131 B42 B41 -37.6(15) . . . . ?
B59 C131 B48 B43 -137.7(15) . . . . ?
B59 C131 B48 B44 -101.3(16) . . . . ?
B59 C131 B48 B39 -37.9(14) . . . . ?
B59 B47 B41 C131 -37.5(14) . . . . ?
B59 B47 B41 C132 -133.3(18) . . . . ?
B59 B47 B41 B42 -99.8(17) . . . . ?
B59 B47 B39 B45 139.3(15) . . . . ?
B59 B47 B39 B44 98.9(16) . . . . ?
B59 B47 B39 B48 36.3(14) . . . . ?
B59 B41 B42 B46 -61.9(18) . . . . ?
B59 B41 B42 C131 35.7(13) . . . . ?
B59 B41 B42 C132 -96.1(16) . . . . ?
B59 B41 B42 B43 0.7(18) . . . . ?
B59 B39 B48 C131 38.4(14) . . . . ?
B59 B39 B48 B43 99.0(17) . . . . ?
B59 B39 B48 B44 138.3(16) . . . . ?
B4 C40 B40 C39 62.1(17) . . . . ?
B4 C40 B40 B8 0.4(19) . . . . ?
B4 C40 B40 B1 104.9(16) . . . . ?
B4 C40 B40 B5 -36.5(14) . . . . ?
B4 C40 B1 C39 -63.3(16) . . . . ?
B4 C40 B1 B40 -102.1(15) . . . . ?
B4 C40 B1 B2 -3.2(18) . . . . ?
B4 C40 B1 B9 37.4(14) . . . . ?
B4 C40 B5 B8 103.1(16) . . . . ?
B4 C40 B5 B40 140.6(15) . . . . ?
B4 C40 B5 B6 35.8(13) . . . . ?
B4 C40 B9 B1 -140.0(15) . . . . ?
B4 C40 B9 B2 -99.1(16) . . . . ?
B4 C40 B9 B3 -39.8(13) . . . . ?
B4 B5 B6 B8 137.3(16) . . . . ?
B4 B5 B6 B3 39.9(14) . . . . ?
B4 B5 B6 B7 101.7(16) . . . . ?
B4 B6 B3 B2 99.6(17) . . . . ?
B4 B6 B3 B9 33.7(14) . . . . ?
B4 B6 B3 B7 138.7(16) . . . . ?
B4 B6 B7 C39 60.5(17) . . . . ?
B4 B6 B7 B8 97.8(15) . . . . ?
B4 B6 B7 B2 -0.4(18) . . . . ?
B4 B6 B7 B3 -36.8(14) . . . . ?
B4 B3 B9 C40 39.7(13) . . . . ?
B4 B3 B9 B1 99.3(16) . . . . ?
B4 B3 B9 B2 136.2(16) . . . . ?
B4 B3 B7 C39 -60.8(19) . . . . ?
B4 B3 B7 B8 -3(2) . . . . ?
B4 B3 B7 B6 36.9(15) . . . . ?
B4 B3 B7 B2 -100.6(17) . . . . ?
B40 C39 B8 B5 40.8(13) . . . . ?
B40 C39 B8 B6 102.9(14) . . . . ?
B40 C39 B8 B7 143.1(14) . . . . ?
B40 C39 B1 C40 -41.5(13) . . . . ?
B40 C39 B1 B2 -141.0(16) . . . . ?
B40 C39 B1 B9 -102.5(16) . . . . ?
B40 C39 B2 B1 37.7(15) . . . . ?
B40 C39 B2 B3 -65.7(19) . . . . ?
B40 C39 B2 B9 -2(2) . . . . ?
B40 C39 B2 B7 -107.1(16) . . . . ?
B40 C39 B7 B8 -36.3(14) . . . . ?
B40 C39 B7 B6 3.8(19) . . . . ?
B40 C39 B7 B2 104.1(17) . . . . ?
B40 C39 B7 B3 64.8(19) . . . . ?
B40 B8 B5 C40 38.0(13) . . . . ?
B40 B8 B5 B4 101.0(16) . . . . ?
B40 B8 B5 B6 139.4(15) . . . . ?
B40 B8 B6 B4 0(2) . . . . ?
B40 B8 B6 B5 -37.3(14) . . . . ?
B40 B8 B6 B3 62.8(18) . . . . ?
B40 B8 B6 B7 102.0(16) . . . . ?
B40 B8 B7 C39 32.7(13) . . . . ?
B40 B8 B7 B6 -101.6(15) . . . . ?
B40 B8 B7 B2 -1.7(18) . . . . ?
B40 B8 B7 B3 -62.0(18) . . . . ?
B40 C40 B4 B5 36.1(14) . . . . ?
B40 C40 B4 B6 0(2) . . . . ?
B40 C40 B4 B3 -63.9(18) . . . . ?
B40 C40 B4 B9 -104.9(16) . . . . ?
B40 C40 B1 C39 38.8(12) . . . . ?
B40 C40 B1 B2 98.9(15) . . . . ?
B40 C40 B1 B9 139.5(15) . . . . ?
B40 C40 B5 B8 -37.5(13) . . . . ?
B40 C40 B5 B4 -140.6(15) . . . . ?
B40 C40 B5 B6 -104.8(15) . . . . ?
B40 C40 B9 B4 101.9(15) . . . . ?
B40 C40 B9 B1 -38.1(14) . . . . ?
B40 C40 B9 B2 2.8(19) . . . . ?
B40 C40 B9 B3 62.0(18) . . . . ?
B40 B1 B2 C39 -32.3(13) . . . . ?
B40 B1 B2 B3 65.1(17) . . . . ?
B40 B1 B2 B9 103.2(16) . . . . ?
B40 B1 B2 B7 0.1(19) . . . . ?
B40 B1 B9 C40 36.5(14) . . . . ?
B40 B1 B9 B4 2(2) . . . . ?
B40 B1 B9 B2 -96.1(16) . . . . ?
B40 B1 B9 B3 -60.4(19) . . . . ?
B40 B5 B6 B8 37.0(13) . . . . ?
B40 B5 B6 B4 -100.3(16) . . . . ?
B40 B5 B6 B3 -60.5(17) . . . . ?
B40 B5 B6 B7 1.4(18) . . . . ?
C126 C125 C130 C129 -3(3) . . . . ?
C126 C127 C128 C129 -2(4) . . . . ?
C52 C51 C50 C49 13(4) . . . . ?
B32 C80 B34 B33 -38.4(17) . . . . ?
B32 C80 B34 B35 -98(2) . . . . ?
B32 C80 B34 B37 -135(2) . . . . ?
B32 C80 B31 C79 40.6(15) . . . . ?
B32 C80 B31 B30 101(2) . . . . ?
B32 C80 B31 B38 143(2) . . . . ?
B32 C80 B38 B31 -35(2) . . . . ?
B32 C80 B38 B30 8(3) . . . . ?
B32 C80 B38 B29 67(2) . . . . ?
B32 C80 B38 B37 104(2) . . . . ?
B32 C80 B37 B34 42(2) . . . . ?
B32 C80 B37 B38 -105(2) . . . . ?
B32 C80 B37 B29 -68(3) . . . . ?
B32 C80 B37 B35 -2(3) . . . . ?
B32 C79 B33 B34 38.2(18) . . . . ?
B32 C79 B33 B36 141(2) . . . . ?
B32 C79 B33 B35 102(2) . . . . ?
B32 C79 B31 C80 -40.9(15) . . . . ?
B32 C79 B31 B30 -141(2) . . . . ?
B32 C79 B31 B38 -100(2) . . . . ?
B32 C79 B30 B31 39(2) . . . . ?
B32 C79 B30 B36 -107(2) . . . . ?
B32 C79 B30 B38 -2(3) . . . . ?
B32 C79 B30 B29 -64(3) . . . . ?
B32 C79 B36 B33 -39(2) . . . . ?
B32 C79 B36 B30 106(2) . . . . ?
B32 C79 B36 B29 66(3) . . . . ?
B32 C79 B36 B35 3(3) . . . . ?
B32 B33 B34 C80 39.2(18) . . . . ?
B32 B33 B34 B35 132(2) . . . . ?
B32 B33 B34 B37 101(2) . . . . ?
B32 B33 B36 C79 33.9(18) . . . . ?
B32 B33 B36 B30 2(3) . . . . ?
B32 B33 B36 B29 -62(3) . . . . ?
B32 B33 B36 B35 -99(2) . . . . ?
B32 B33 B35 B34 -41(2) . . . . ?
B32 B33 B35 B36 98(2) . . . . ?
B32 B33 B35 B29 61(3) . . . . ?
B32 B33 B35 B37 -5(3) . . . . ?
B32 B34 B35 B33 40(2) . . . . ?
B32 B34 B35 B36 3(3) . . . . ?
B32 B34 B35 B29 -64(3) . . . . ?
B32 B34 B35 B37 -101(2) . . . . ?
B32 B34 B37 C80 -38.8(17) . . . . ?
B32 B34 B37 B38 -10(3) . . . . ?
B32 B34 B37 B29 53(3) . . . . ?
B32 B34 B37 B35 93(2) . . . . ?
B32 B31 B30 C79 -32.7(18) . . . . ?
B32 B31 B30 B36 -2(3) . . . . ?
B32 B31 B30 B38 100(2) . . . . ?
B32 B31 B30 B29 65(3) . . . . ?
B32 B31 B38 C80 31.5(17) . . . . ?
B32 B31 B38 B30 -99(2) . . . . ?
B32 B31 B38 B29 -66(3) . . . . ?
B32 B31 B38 B37 -5(3) . . . . ?
C113 P10 C106 B53 12.1(16) . . . . ?
C113 P10 C106 B51 -132.2(13) . . . . ?
C113 P10 C106 B54 85.7(14) . . . . ?
C113 P10 C106 B52 -60.2(16) . . . . ?
C113 P10 C106 B58 156.3(13) . . . . ?
C113 P10 C107 C108 59(2) . . . . ?
C113 P10 C107 C112 -118.5(19) . . . . ?
C113 C118 C117 C116 2(4) . . . . ?
C113 C114 C115 C116 0(4) . . . . ?
C130 C125 C126 C127 -1(3) . . . . ?
B1 C39 B8 B40 -37.5(14) . . . . ?
B1 C39 B8 B5 3.3(19) . . . . ?
B1 C39 B8 B6 65.5(18) . . . . ?
B1 C39 B8 B7 105.7(16) . . . . ?
B1 C39 B40 B8 141.5(14) . . . . ?
B1 C39 B40 C40 41.0(13) . . . . ?
B1 C39 B40 B5 102.2(14) . . . . ?
B1 C39 B2 B3 -103.4(17) . . . . ?
B1 C39 B2 B9 -39.6(14) . . . . ?
B1 C39 B2 B7 -144.8(16) . . . . ?
B1 C39 B7 B8 -106.4(17) . . . . ?
B1 C39 B7 B6 -66.4(18) . . . . ?
B1 C39 B7 B2 34.0(15) . . . . ?
B1 C39 B7 B3 -5(2) . . . . ?
B1 C40 B4 B5 102.7(15) . . . . ?
B1 C40 B4 B6 66.4(18) . . . . ?
B1 C40 B4 B3 2.6(19) . . . . ?
B1 C40 B4 B9 -38.4(14) . . . . ?
B1 C40 B40 C39 -42.8(14) . . . . ?
B1 C40 B40 B8 -104.5(16) . . . . ?
B1 C40 B40 B5 -141.4(15) . . . . ?
B1 C40 B5 B8 -1.6(18) . . . . ?
B1 C40 B5 B4 -104.6(15) . . . . ?
B1 C40 B5 B40 36.0(14) . . . . ?
B1 C40 B5 B6 -68.8(16) . . . . ?
B1 C40 B9 B4 140.0(15) . . . . ?
B1 C40 B9 B2 40.9(14) . . . . ?
B1 C40 B9 B3 100.1(16) . . . . ?
B1 B40 B5 B8 104.0(16) . . . . ?
B1 B40 B5 C40 -33.7(13) . . . . ?
B1 B40 B5 B4 1.6(19) . . . . ?
B1 B40 B5 B6 65.3(18) . . . . ?
B1 B2 B3 B4 -1.1(19) . . . . ?
B1 B2 B3 B6 -64.3(18) . . . . ?
B1 B2 B3 B9 37.9(14) . . . . ?
B1 B2 B3 B7 -103.4(16) . . . . ?
B1 B2 B9 C40 -39.5(13) . . . . ?
B1 B2 B9 B4 -100.4(15) . . . . ?
B1 B2 B9 B3 -138.3(16) . . . . ?
B1 B2 B7 C39 -32.0(14) . . . . ?
B1 B2 B7 B8 0.9(19) . . . . ?
B1 B2 B7 B6 64.2(17) . . . . ?
B1 B2 B7 B3 101.2(17) . . . . ?
B18 C13 B13 B14 -62.4(18) . . . . ?
B18 C13 B13 B19 39.0(14) . . . . ?
B18 C13 B13 B15 -102.4(16) . . . . ?
B18 C13 B13 B12 0.2(19) . . . . ?
B18 C13 B16 B17 38.5(13) . . . . ?
B18 C13 B16 B10 102.6(16) . . . . ?
B18 C13 B16 B15 141.7(16) . . . . ?
B18 C13 B19 C14 -37.9(12) . . . . ?
B18 C13 B19 B13 -139.9(15) . . . . ?
B18 C13 B19 B12 -100.5(15) . . . . ?
B18 C13 B15 B13 105.6(16) . . . . ?
B18 C13 B15 B16 -35.5(14) . . . . ?
B18 C13 B15 B14 66.5(18) . . . . ?
B18 C13 B15 B10 2.7(19) . . . . ?
B18 C14 B17 B16 -39.1(13) . . . . ?
B18 C14 B17 B11 -140.1(15) . . . . ?
B18 C14 B17 B10 -102.3(16) . . . . ?
B18 C14 B11 B14 -63.5(18) . . . . ?
B18 C14 B11 B17 37.7(15) . . . . ?
B18 C14 B11 B10 0(2) . . . . ?
B18 C14 B11 B12 -104.2(16) . . . . ?
B18 C14 B19 C13 38.8(12) . . . . ?
B18 C14 B19 B13 102.6(15) . . . . ?
B18 C14 B19 B12 142.2(14) . . . . ?
B18 C14 B12 B13 3.2(18) . . . . ?
B18 C14 B12 B14 63.5(17) . . . . ?
B18 C14 B12 B11 104.2(15) . . . . ?
B18 C14 B12 B19 -36.0(14) . . . . ?
B18 B16 B17 C14 38.7(13) . . . . ?
B18 B16 B17 B11 101.0(15) . . . . ?
B18 B16 B17 B10 139.5(15) . . . . ?
B18 B16 B10 B14 63.5(19) . . . . ?
B18 B16 B10 B17 -36.7(14) . . . . ?
B18 B16 B10 B11 2(2) . . . . ?
B18 B16 B10 B15 101.6(17) . . . . ?
B18 B16 B15 C13 34.3(14) . . . . ?
B18 B16 B15 B13 -1(2) . . . . ?
B18 B16 B15 B14 -62(2) . . . . ?
B18 B16 B15 B10 -102.2(17) . . . . ?
B18 B17 B11 C14 -35.2(13) . . . . ?
B18 B17 B11 B14 61.8(18) . . . . ?
B18 B17 B11 B10 101.9(17) . . . . ?
B18 B17 B11 B12 -0.8(19) . . . . ?
B18 B17 B10 B16 36.4(14) . . . . ?
B18 B17 B10 B14 -61.2(18) . . . . ?
B18 B17 B10 B11 -100.0(15) . . . . ?
B18 B17 B10 B15 -0.3(19) . . . . ?
B18 B19 B12 C14 32.7(13) . . . . ?
B18 B19 B12 B13 -102.3(16) . . . . ?
B18 B19 B12 B14 -64.5(18) . . . . ?
B18 B19 B12 B11 -2.2(19) . . . . ?
C110 C111 C112 C107 11(4) . . . . ?
C38 C33 C34 C35 6(4) . . . . ?
C38 C37 C36 C35 -1(4) . . . . ?
C74 C73 C78 C77 6(3) . . . . ?
C74 C75 C76 C77 -4(4) . . . . ?
C103 C104 C99 P9 170.9(14) . . . . ?
C103 C104 C99 C100 1(3) . . . . ?
C103 C102 C101 C100 5(3) . . . . ?
C67 P7 C73 C74 14(2) . . . . ?
C67 P7 C73 C78 -160.1(19) . . . . ?
C67 P7 C79 B32 152.7(19) . . . . ?
C67 P7 C79 B33 83.3(19) . . . . ?
C67 P7 C79 B31 -134(2) . . . . ?
C67 P7 C79 B30 -60(2) . . . . ?
C67 P7 C79 B36 10(3) . . . . ?
C67 C72 C71 C70 0(5) . . . . ?
C67 C68 C69 C70 -3(5) . . . . ?
C107 P10 C106 B53 128.4(15) . . . . ?
C107 P10 C106 B51 -15.9(16) . . . . ?
C107 P10 C106 B54 -158.0(13) . . . . ?
C107 P10 C106 B52 56.1(16) . . . . ?
C107 P10 C106 B58 -87.5(14) . . . . ?
C107 P10 C113 C118 159.0(19) . . . . ?
C107 P10 C113 C114 -20(2) . . . . ?
C107 C108 C109 C110 1(4) . . . . ?
C111 C110 C109 C108 3(4) . . . . ?
B11 C14 B17 B16 101.0(16) . . . . ?
B11 C14 B17 B18 140.1(15) . . . . ?
B11 C14 B17 B10 37.8(14) . . . . ?
B11 C14 B18 C13 63.6(17) . . . . ?
B11 C14 B18 B16 1(2) . . . . ?
B11 C14 B18 B17 -38.2(15) . . . . ?
B11 C14 B18 B19 102.0(16) . . . . ?
B11 C14 B19 C13 -66.8(17) . . . . ?
B11 C14 B19 B13 -3.0(19) . . . . ?
B11 C14 B19 B18 -105.6(15) . . . . ?
B11 C14 B19 B12 36.7(14) . . . . ?
B11 C14 B12 B13 -100.9(16) . . . . ?
B11 C14 B12 B14 -40.7(14) . . . . ?
B11 C14 B12 B19 -140.2(15) . . . . ?
B11 B14 B10 B16 -100.7(15) . . . . ?
B11 B14 B10 B17 -39.7(14) . . . . ?
B11 B14 B10 B15 -139.4(15) . . . . ?
B11 B14 B15 C13 -64.1(19) . . . . ?
B11 B14 B15 B13 -104.2(16) . . . . ?
B11 B14 B15 B16 -3(2) . . . . ?
B11 B14 B15 B10 36.5(14) . . . . ?
B11 B14 B12 C14 40.1(13) . . . . ?
B11 B14 B12 B13 139.8(15) . . . . ?
B11 B14 B12 B19 101.2(16) . . . . ?
B11 B17 B18 C13 -61.2(17) . . . . ?
B11 B17 B18 C14 35.5(13) . . . . ?
B11 B17 B18 B16 -99.8(16) . . . . ?
B11 B17 B18 B19 -0.6(19) . . . . ?
B11 B17 B10 B16 136.4(15) . . . . ?
B11 B17 B10 B14 38.8(14) . . . . ?
B11 B17 B10 B15 99.7(16) . . . . ?
B11 B10 B15 C13 62.3(17) . . . . ?
B11 B10 B15 B13 -0.8(19) . . . . ?
B11 B10 B15 B16 99.9(15) . . . . ?
B11 B10 B15 B14 -35.5(14) . . . . ?
C108 C107 C112 C111 -7(3) . . . . ?
B10 B16 B17 C14 -100.9(15) . . . . ?
B10 B16 B17 B18 -139.5(15) . . . . ?
B10 B16 B17 B11 -38.5(13) . . . . ?
B10 B16 B18 C13 -99.6(16) . . . . ?
B10 B16 B18 C14 -2(2) . . . . ?
B10 B16 B18 B17 37.1(15) . . . . ?
B10 B16 B18 B19 -65.4(19) . . . . ?
B10 B16 B15 C13 136.5(15) . . . . ?
B10 B16 B15 B13 101.6(17) . . . . ?
B10 B16 B15 B14 40.3(15) . . . . ?
B10 B14 B11 C14 99.4(15) . . . . ?
B10 B14 B11 B17 39.4(13) . . . . ?
B10 B14 B11 B12 140.7(15) . . . . ?
B10 B14 B15 C13 -100.6(16) . . . . ?
B10 B14 B15 B13 -140.7(15) . . . . ?
B10 B14 B15 B16 -39.5(14) . . . . ?
B10 B14 B12 C14 4.5(19) . . . . ?
B10 B14 B12 B13 104.1(17) . . . . ?
B10 B14 B12 B11 -35.7(15) . . . . ?
B10 B14 B12 B19 65.6(19) . . . . ?
B10 B17 B18 C13 1.9(18) . . . . ?
B10 B17 B18 C14 98.7(15) . . . . ?
B10 B17 B18 B16 -36.6(14) . . . . ?
B10 B17 B18 B19 62.6(18) . . . . ?
B10 B17 B11 C14 -137.1(16) . . . . ?
B10 B17 B11 B14 -40.1(14) . . . . ?
B10 B17 B11 B12 -102.6(16) . . . . ?
B10 B11 B12 C14 -96.7(15) . . . . ?
B10 B11 B12 B13 1.1(18) . . . . ?
B10 B11 B12 B14 36.1(14) . . . . ?
B10 B11 B12 B19 -61.6(17) . . . . ?
C12 C7 C8 C9 2(4) . . . . ?
C12 C11 C10 C9 -1(4) . . . . ?
C117 C118 C113 P10 179(2) . . . . ?
C117 C118 C113 C114 -2(4) . . . . ?
C117 C116 C115 C114 0(4) . . . . ?
B27 B26 C54 P6 -116.9(13) . . . . ?
B27 B26 C54 B25 141.9(15) . . . . ?
B27 B26 C54 B60 103.4(16) . . . . ?
B27 B26 C54 B21 37.7(14) . . . . ?
B27 B26 B28 B24 -136.0(17) . . . . ?
B27 B26 B28 B23 -99.6(17) . . . . ?
B27 B26 B28 B20 -37.7(15) . . . . ?
B27 C54 B21 B60 142.9(16) . . . . ?
B27 C54 B21 B22 103.1(18) . . . . ?
B27 C54 B21 B20 38.6(13) . . . . ?
B27 B21 B22 C53 61.6(18) . . . . ?
B27 B21 B22 B60 101.7(17) . . . . ?
B27 B21 B22 B23 2.5(19) . . . . ?
B27 B21 B22 B20 -34.8(14) . . . . ?
B27 B21 B20 B23 102.6(16) . . . . ?
B27 B21 B20 B22 141.4(15) . . . . ?
B27 B21 B20 B28 37.6(14) . . . . ?
B27 B20 B28 B24 100.8(17) . . . . ?
B27 B20 B28 B26 37.8(15) . . . . ?
B27 B20 B28 B23 136.1(17) . . . . ?
B19 C13 B13 B14 -101.4(16) . . . . ?
B19 C13 B13 B15 -141.5(16) . . . . ?
B19 C13 B13 B12 -38.8(13) . . . . ?
B19 C13 B16 B17 0.1(19) . . . . ?
B19 C13 B16 B18 -38.4(14) . . . . ?
B19 C13 B16 B10 64.2(18) . . . . ?
B19 C13 B16 B15 103.3(16) . . . . ?
B19 C13 B18 C14 39.9(12) . . . . ?
B19 C13 B18 B16 140.4(15) . . . . ?
B19 C13 B18 B17 101.9(15) . . . . ?
B19 C13 B15 B13 36.2(15) . . . . ?
B19 C13 B15 B16 -104.9(17) . . . . ?
B19 C13 B15 B14 -3(2) . . . . ?
B19 C13 B15 B10 -66.7(18) . . . . ?
B19 C14 B17 B16 -1.2(18) . . . . ?
B19 C14 B17 B18 37.9(14) . . . . ?
B19 C14 B17 B11 -102.2(15) . . . . ?
B19 C14 B17 B10 -64.4(18) . . . . ?
B19 C14 B18 C13 -38.4(12) . . . . ?
B19 C14 B18 B16 -100.8(15) . . . . ?
B19 C14 B18 B17 -140.2(14) . . . . ?
B19 C14 B11 B14 4.2(19) . . . . ?
B19 C14 B11 B17 105.3(16) . . . . ?
B19 C14 B11 B10 67.8(18) . . . . ?
B19 C14 B11 B12 -36.5(14) . . . . ?
B19 C14 B12 B13 39.2(13) . . . . ?
B19 C14 B12 B14 99.5(15) . . . . ?
B19 C14 B12 B11 140.2(15) . . . . ?
B19 B13 B14 B11 2(2) . . . . ?
B19 B13 B14 B10 -62.4(19) . . . . ?
B19 B13 B14 B15 -98.7(16) . . . . ?
B19 B13 B14 B12 39.5(14) . . . . ?
B19 B13 B15 C13 -32.8(14) . . . . ?
B19 B13 B15 B16 2(2) . . . . ?
B19 B13 B15 B14 101.1(17) . . . . ?
B19 B13 B15 B10 65.1(18) . . . . ?
B19 B13 B12 C14 -38.9(13) . . . . ?
B19 B13 B12 B14 -135.8(16) . . . . ?
B19 B13 B12 B11 -100.1(15) . . . . ?
B42 B46 C132 P12 -102.1(13) . . . . ?
B42 B46 C132 B45 145.2(15) . . . . ?
B42 B46 C132 B47 108.1(16) . . . . ?
B42 B46 C132 B41 38.3(15) . . . . ?
B42 B46 B43 C131 -40.6(14) . . . . ?
B42 B46 B43 B44 -139.4(17) . . . . ?
B42 B46 B43 B48 -102.7(18) . . . . ?
B42 B46 B44 B45 -102.8(18) . . . . ?
B42 B46 B44 B43 36.1(16) . . . . ?
B42 B46 B44 B39 -64.9(18) . . . . ?
B42 B46 B44 B48 -2(2) . . . . ?
B42 C131 B43 B46 40.2(14) . . . . ?
B42 C131 B43 B44 106.4(16) . . . . ?
B42 C131 B43 B48 142.4(15) . . . . ?
B42 C131 B41 C132 -40.6(13) . . . . ?
B42 C131 B41 B47 -102.2(16) . . . . ?
B42 C131 B41 B59 -139.6(15) . . . . ?
B42 C131 B59 B47 0(2) . . . . ?
B42 C131 B59 B41 38.3(15) . . . . ?
B42 C131 B59 B39 -65(2) . . . . ?
B42 C131 B59 B48 -104.7(17) . . . . ?
B42 C131 B48 B43 -34.8(15) . . . . ?
B42 C131 B48 B59 102.9(16) . . . . ?
B42 C131 B48 B44 2(2) . . . . ?
B42 C131 B48 B39 65.0(19) . . . . ?
B42 C132 B47 B45 105.4(19) . . . . ?
B42 C132 B47 B41 -38.8(18) . . . . ?
B42 C132 B47 B59 2(2) . . . . ?
B42 C132 B47 B39 64(2) . . . . ?
B42 C132 B41 C131 41.1(13) . . . . ?
B42 C132 B41 B47 142.0(17) . . . . ?
B42 C132 B41 B59 102.0(17) . . . . ?
B42 B43 B44 B45 -1(2) . . . . ?
B42 B43 B44 B46 -37.6(16) . . . . ?
B42 B43 B44 B39 61.2(19) . . . . ?
B42 B43 B44 B48 101.1(18) . . . . ?
B42 B43 B48 C131 34.8(14) . . . . ?
B42 B43 B48 B59 -2.4(19) . . . . ?
B42 B43 B48 B44 -103.7(17) . . . . ?
B42 B43 B48 B39 -63.8(19) . . . . ?
B42 B41 B59 C131 -35.8(13) . . . . ?
B42 B41 B59 B47 101.1(17) . . . . ?
B42 B41 B59 B39 63.9(19) . . . . ?
B42 B41 B59 B48 -2.2(19) . . . . ?
C10 C11 C12 C7 1(4) . . . . ?
C88 C89 C90 C91 -1(10) . . . . ?
C112 C107 C108 C109 1(4) . . . . ?
B49 B53 C106 P10 -153.0(13) . . . . ?
B49 B53 C106 B51 -6.5(18) . . . . ?
B49 B53 C106 B54 100.7(16) . . . . ?
B49 B53 C106 B52 -41.2(14) . . . . ?
B49 B53 C106 B58 62.3(18) . . . . ?
B49 B53 B54 C106 -99.8(16) . . . . ?
B49 B53 B54 B56 -1.3(19) . . . . ?
B49 B53 B54 B55 35.0(14) . . . . ?
B49 B53 B54 B58 -65.5(18) . . . . ?
B49 B53 B52 B50 36.1(13) . . . . ?
B49 B53 B52 C106 134.8(15) . . . . ?
B49 B53 B52 B51 100.8(16) . . . . ?
B49 B53 B55 B56 -102.9(17) . . . . ?
B49 B53 B55 B54 -141.0(15) . . . . ?
B49 B53 B55 B57 -37.0(14) . . . . ?
B49 B50 B51 C106 -2.1(17) . . . . ?
B49 B50 B51 B52 37.0(14) . . . . ?
B49 B50 B51 C105 -95.2(15) . . . . ?
B49 B50 B51 B58 -61.8(17) . . . . ?
B49 B50 B52 B53 -35.1(13) . . . . ?
B49 B50 B52 C106 -99.4(15) . . . . ?
B49 B50 B52 B51 -138.6(15) . . . . ?
B49 B50 B57 B56 100.1(16) . . . . ?
B49 B50 B57 B55 37.9(14) . . . . ?
B49 B50 B57 C105 133.4(15) . . . . ?
B49 B50 C105 P9 -148.2(13) . . . . ?
B49 B50 C105 B56 -4.1(19) . . . . ?
B49 B50 C105 B51 103.0(15) . . . . ?
B49 B50 C105 B57 -40.0(14) . . . . ?
B49 B50 C105 B58 65.9(17) . . . . ?
B49 B55 B57 B50 -38.4(14) . . . . ?
B49 B55 B57 B56 -140.4(15) . . . . ?
B49 B55 B57 C105 -100.3(15) . . . . ?
B49 B57 C105 P9 154.9(13) . . . . ?
B49 B57 C105 B50 41.2(14) . . . . ?
B49 B57 C105 B56 -101.7(16) . . . . ?
B49 B57 C105 B51 6(2) . . . . ?
B49 B57 C105 B58 -63.9(19) . . . . ?
C109 C110 C111 C112 -9(4) . . . . ?
B5 B8 B40 C39 -134.2(14) . . . . ?
B5 B8 B40 C40 -37.0(13) . . . . ?
B5 B8 B40 B1 -98.4(16) . . . . ?
B5 B8 B6 B4 37.7(14) . . . . ?
B5 B8 B6 B3 100.1(15) . . . . ?
B5 B8 B6 B7 139.3(16) . . . . ?
B5 B8 B7 C39 98.0(15) . . . . ?
B5 B8 B7 B6 -36.2(14) . . . . ?
B5 B8 B7 B2 63.7(18) . . . . ?
B5 B8 B7 B3 3(2) . . . . ?
B5 C40 B4 B6 -36.2(14) . . . . ?
B5 C40 B4 B3 -100.0(15) . . . . ?
B5 C40 B4 B9 -141.1(15) . . . . ?
B5 C40 B40 C39 98.6(15) . . . . ?
B5 C40 B40 B8 36.9(14) . . . . ?
B5 C40 B40 B1 141.4(15) . . . . ?
B5 C40 B1 C39 3.3(17) . . . . ?
B5 C40 B1 B40 -35.5(14) . . . . ?
B5 C40 B1 B2 63.4(16) . . . . ?
B5 C40 B1 B9 104.0(15) . . . . ?
B5 C40 B9 B4 36.3(14) . . . . ?
B5 C40 B9 B1 -103.7(15) . . . . ?
B5 C40 B9 B2 -62.8(17) . . . . ?
B5 C40 B9 B3 -3.6(19) . . . . ?
B5 B4 B6 B8 -36.1(13) . . . . ?
B5 B4 B6 B3 -134.7(15) . . . . ?
B5 B4 B6 B7 -98.2(15) . . . . ?
B5 B4 B3 B6 40.0(14) . . . . ?
B5 B4 B3 B2 -63.0(19) . . . . ?
B5 B4 B3 B9 -102.8(16) . . . . ?
B5 B4 B3 B7 2(2) . . . . ?
B5 B4 B9 C40 -34.8(13) . . . . ?
B5 B4 B9 B1 -1(2) . . . . ?
B5 B4 B9 B2 62.0(18) . . . . ?
B5 B4 B9 B3 99.0(16) . . . . ?
B5 B40 B1 C39 -97.5(15) . . . . ?
B5 B40 B1 C40 34.1(13) . . . . ?
B5 B40 B1 B2 -63.8(17) . . . . ?
B5 B40 B1 B9 -2(2) . . . . ?
B5 B6 B3 B4 -40.1(13) . . . . ?
B5 B6 B3 B2 59.5(18) . . . . ?
B5 B6 B3 B9 -6.4(19) . . . . ?
B5 B6 B3 B7 98.6(15) . . . . ?
B5 B6 B7 C39 -2.8(17) . . . . ?
B5 B6 B7 B8 34.5(13) . . . . ?
B5 B6 B7 B2 -63.7(17) . . . . ?
B5 B6 B7 B3 -100.1(15) . . . . ?
B20 B23 B22 C53 -134.5(15) . . . . ?
B20 B23 B22 B60 -99.8(15) . . . . ?
B20 B23 B22 B21 -39.0(14) . . . . ?
B20 B23 B28 B24 139.6(18) . . . . ?
B20 B23 B28 B26 102.8(18) . . . . ?
B20 B23 B28 B27 39.0(14) . . . . ?
B20 B21 B22 C53 96.4(16) . . . . ?
B20 B21 B22 B60 136.6(16) . . . . ?
B20 B21 B22 B23 37.3(13) . . . . ?
B20 B21 B27 B26 -100.9(16) . . . . ?
B20 B21 B27 C54 -135.4(15) . . . . ?
B20 B21 B27 B28 -37.6(14) . . . . ?
B20 B27 B28 B24 -99.6(17) . . . . ?
B20 B27 B28 B26 -138.5(16) . . . . ?
B20 B27 B28 B23 -38.1(14) . . . . ?
C89 C88 C87 P8 -177(4) . . . . ?
C89 C88 C87 C92 -1(6) . . . . ?
C89 C90 C91 C92 3(9) . . . . ?
B44 B45 B46 C132 130.9(15) . . . . ?
B44 B45 B46 B43 36.6(16) . . . . ?
B44 B45 B46 B42 99.9(17) . . . . ?
B44 B45 C132 P12 -145.0(13) . . . . ?
B44 B45 C132 B46 -42.0(13) . . . . ?
B44 B45 C132 B47 99.7(15) . . . . ?
B44 B45 C132 B41 64.6(19) . . . . ?
B44 B45 C132 B42 -8.7(19) . . . . ?
B44 B45 B47 C132 -95.0(14) . . . . ?
B44 B45 B47 B41 -63.2(18) . . . . ?
B44 B45 B47 B59 1.8(18) . . . . ?
B44 B45 B47 B39 37.9(13) . . . . ?
B44 B45 B39 B47 -136.0(15) . . . . ?
B44 B45 B39 B59 -99.7(17) . . . . ?
B44 B45 B39 B48 -36.2(15) . . . . ?
B44 B46 C132 P12 155.2(11) . . . . ?
B44 B46 C132 B45 42.5(13) . . . . ?
B44 B46 C132 B47 5.4(19) . . . . ?
B44 B46 C132 B41 -64.4(17) . . . . ?
B44 B46 C132 B42 -102.7(15) . . . . ?
B44 B46 B43 C131 98.9(16) . . . . ?
B44 B46 B43 B42 139.4(17) . . . . ?
B44 B46 B43 B48 36.7(16) . . . . ?
B44 B46 B42 C131 2(2) . . . . ?
B44 B46 B42 C132 95.4(16) . . . . ?
B44 B46 B42 B43 -36.0(15) . . . . ?
B44 B46 B42 B41 63.0(19) . . . . ?
B44 B43 B42 B46 38.6(15) . . . . ?
B44 B43 B42 C131 -96.9(16) . . . . ?
B44 B43 B42 C132 -4(2) . . . . ?
B44 B43 B42 B41 -62.2(19) . . . . ?
B44 B43 B48 C131 138.5(17) . . . . ?
B44 B43 B48 B59 101.3(17) . . . . ?
B44 B43 B48 B39 39.8(16) . . . . ?
B44 B39 B48 C131 -99.9(16) . . . . ?
B44 B39 B48 B43 -39.2(15) . . . . ?
B44 B39 B48 B59 -138.3(16) . . . . ?
B55 B53 C106 P10 144.6(13) . . . . ?
B55 B53 C106 B51 -68.9(16) . . . . ?
B55 B53 C106 B54 38.2(13) . . . . ?
B55 B53 C106 B52 -103.7(16) . . . . ?
B55 B53 C106 B58 -0.1(19) . . . . ?
B55 B53 B54 C106 -134.8(15) . . . . ?
B55 B53 B54 B56 -36.3(13) . . . . ?
B55 B53 B54 B58 -100.5(16) . . . . ?
B55 B53 B52 B50 -3.8(18) . . . . ?
B55 B53 B52 C106 94.8(15) . . . . ?
B55 B53 B52 B51 60.9(18) . . . . ?
B55 B53 B52 B49 -39.9(13) . . . . ?
B55 B53 B49 B50 100.3(15) . . . . ?
B55 B53 B49 B52 135.4(14) . . . . ?
B55 B53 B49 B57 36.7(14) . . . . ?
B55 B56 B54 B53 36.7(13) . . . . ?
B55 B56 B54 C106 99.1(15) . . . . ?
B55 B56 B54 B58 136.1(15) . . . . ?
B55 B56 B57 B50 -99.7(16) . . . . ?
B55 B56 B57 B49 -35.3(14) . . . . ?
B55 B56 B57 C105 -133.1(15) . . . . ?
B55 B56 C105 P9 151.8(12) . . . . ?
B55 B56 C105 B50 4.5(19) . . . . ?
B55 B56 C105 B51 -64.4(17) . . . . ?
B55 B56 C105 B57 40.3(14) . . . . ?
B55 B56 C105 B58 -100.8(15) . . . . ?
B55 B56 B58 C106 -0.1(19) . . . . ?
B55 B56 B58 B51 62.9(18) . . . . ?
B55 B56 B58 B54 -38.7(14) . . . . ?
B55 B56 B58 C105 96.1(16) . . . . ?
B55 B54 B58 C106 -98.1(15) . . . . ?
B55 B54 B58 B56 38.5(14) . . . . ?
B55 B54 B58 B51 -62.7(17) . . . . ?
B55 B54 B58 C105 -0.6(17) . . . . ?
B55 B49 B57 B50 137.4(15) . . . . ?
B55 B49 B57 B56 34.9(13) . . . . ?
B55 B49 B57 C105 96.8(15) . . . . ?
B55 B57 C105 P9 -143.3(13) . . . . ?
B55 B57 C105 B50 103.0(16) . . . . ?
B55 B57 C105 B56 -39.9(14) . . . . ?
B55 B57 C105 B51 67.6(18) . . . . ?
B55 B57 C105 B58 -2(2) . . . . ?
C137 C136 C135 C134 0(4) . . . . ?
B6 B8 B40 C39 -97.8(15) . . . . ?
B6 B8 B40 C40 -0.5(19) . . . . ?
B6 B8 B40 B1 -61.9(19) . . . . ?
B6 B8 B40 B5 36.5(14) . . . . ?
B6 B8 B5 C40 -101.5(15) . . . . ?
B6 B8 B5 B4 -38.4(14) . . . . ?
B6 B8 B5 B40 -139.4(15) . . . . ?
B6 B8 B7 C39 134.2(15) . . . . ?
B6 B8 B7 B2 99.9(15) . . . . ?
B6 B8 B7 B3 39.6(14) . . . . ?
B6 B4 B5 B8 40.3(15) . . . . ?
B6 B4 B5 C40 139.7(15) . . . . ?
B6 B4 B5 B40 103.9(16) . . . . ?
B6 B4 B3 B2 -103.0(16) . . . . ?
B6 B4 B3 B9 -142.8(15) . . . . ?
B6 B4 B3 B7 -37.8(15) . . . . ?
B6 B4 B9 C40 -99.3(15) . . . . ?
B6 B4 B9 B1 -65.1(19) . . . . ?
B6 B4 B9 B2 -2.5(19) . . . . ?
B6 B4 B9 B3 34.5(14) . . . . ?
B6 B3 B9 C40 6.1(19) . . . . ?
B6 B3 B9 B4 -33.6(14) . . . . ?
B6 B3 B9 B1 65.7(18) . . . . ?
B6 B3 B9 B2 102.6(16) . . . . ?
B6 B3 B7 C39 -97.8(15) . . . . ?
B6 B3 B7 B8 -40.4(14) . . . . ?
B6 B3 B7 B2 -137.6(16) . . . . ?
C22 C23 C24 C25 -2(4) . . . . ?
C36 C37 C38 C33 -1(4) . . . . ?
B28 B24 B25 C53 99.6(16) . . . . ?
B28 B24 B25 B26 -36.3(15) . . . . ?
B28 B24 B25 B60 64.0(18) . . . . ?
B28 B24 B25 C54 4.3(19) . . . . ?
B28 B24 B26 B25 139.7(17) . . . . ?
B28 B24 B26 C54 99.0(16) . . . . ?
B28 B24 B26 B27 38.5(16) . . . . ?
B28 B24 B23 C53 -136.5(16) . . . . ?
B28 B24 B23 B22 -101.9(17) . . . . ?
B28 B24 B23 B20 -36.0(16) . . . . ?
B28 B26 C54 P6 -155.3(12) . . . . ?
B28 B26 C54 B25 103.5(15) . . . . ?
B28 B26 C54 B60 65.0(18) . . . . ?
B28 B26 C54 B21 -0.7(19) . . . . ?
B28 B26 C54 B27 -38.4(13) . . . . ?
B28 B26 B27 C54 135.5(16) . . . . ?
B28 B26 B27 B21 101.2(17) . . . . ?
B28 B26 B27 B20 36.8(16) . . . . ?
B28 B23 B22 C53 -97.9(15) . . . . ?
B28 B23 B22 B60 -63.2(18) . . . . ?
B28 B23 B22 B21 -2.4(19) . . . . ?
B28 B23 B22 B20 36.6(14) . . . . ?
B28 B23 B20 B21 -102.0(16) . . . . ?
B28 B23 B20 B22 -139.3(16) . . . . ?
B28 B23 B20 B27 -39.2(16) . . . . ?
B28 B27 B20 B23 40.2(16) . . . . ?
B28 B27 B20 B21 137.7(15) . . . . ?
B28 B27 B20 B22 104.3(16) . . . . ?
B57 B50 B51 C106 60.5(16) . . . . ?
B57 B50 B51 B52 99.6(15) . . . . ?
B57 B50 B51 C105 -32.6(13) . . . . ?
B57 B50 B51 B58 0.8(18) . . . . ?
B57 B50 B52 B53 2.3(17) . . . . ?
B57 B50 B52 C106 -62.0(16) . . . . ?
B57 B50 B52 B51 -101.2(15) . . . . ?
B57 B50 B52 B49 37.4(13) . . . . ?
B57 B50 B49 B53 -102.4(16) . . . . ?
B57 B50 B49 B52 -137.5(15) . . . . ?
B57 B50 B49 B55 -37.6(14) . . . . ?
B57 B50 C105 P9 -108.2(15) . . . . ?
B57 B50 C105 B56 35.9(15) . . . . ?
B57 B50 C105 B51 143.0(15) . . . . ?
B57 B50 C105 B58 105.9(15) . . . . ?
B57 B56 B54 B53 -0.4(18) . . . . ?
B57 B56 B54 C106 62.0(16) . . . . ?
B57 B56 B54 B55 -37.0(13) . . . . ?
B57 B56 B54 B58 99.0(15) . . . . ?
B57 B56 B55 B53 99.7(16) . . . . ?
B57 B56 B55 B54 138.2(15) . . . . ?
B57 B56 B55 B49 36.7(15) . . . . ?
B57 B56 C105 P9 111.4(14) . . . . ?
B57 B56 C105 B50 -35.8(15) . . . . ?
B57 B56 C105 B51 -104.7(15) . . . . ?
B57 B56 C105 B58 -141.2(15) . . . . ?
B57 B56 B58 C106 -62.4(17) . . . . ?
B57 B56 B58 B51 0.6(19) . . . . ?
B57 B56 B58 B54 -101.0(15) . . . . ?
B57 B56 B58 C105 33.8(13) . . . . ?
B57 B49 B55 B53 -139.1(15) . . . . ?
B57 B49 B55 B56 -37.1(14) . . . . ?
B57 B49 B55 B54 -102.9(15) . . . . ?
B57 C105 B58 C106 64.0(17) . . . . ?
B57 C105 B58 B56 -37.5(15) . . . . ?
B57 C105 B58 B51 105.4(16) . . . . ?
B57 C105 B58 B54 1.7(19) . . . . ?
C105 P9 C93 C94 -64.4(16) . . . . ?
C105 P9 C93 C98 114.7(16) . . . . ?
C105 P9 C99 C100 -70.6(16) . . . . ?
C105 P9 C99 C104 119.4(17) . . . . ?
C105 B50 B51 C106 93.0(14) . . . . ?
C105 B50 B51 B52 132.2(15) . . . . ?
C105 B50 B51 B58 33.4(12) . . . . ?
C105 B50 B52 B53 62.8(15) . . . . ?
C105 B50 B52 C106 -1.5(17) . . . . ?
C105 B50 B52 B51 -40.7(12) . . . . ?
C105 B50 B52 B49 97.9(14) . . . . ?
C105 B50 B49 B53 -62.9(17) . . . . ?
C105 B50 B49 B52 -98.0(14) . . . . ?
C105 B50 B49 B55 1.9(19) . . . . ?
C105 B50 B49 B57 39.5(13) . . . . ?
C105 B50 B57 B56 -33.2(14) . . . . ?
C105 B50 B57 B49 -133.4(15) . . . . ?
C105 B50 B57 B55 -95.5(15) . . . . ?
C105 B56 B54 B53 -61.2(16) . . . . ?
C105 B56 B54 C106 1.2(17) . . . . ?
C105 B56 B54 B55 -97.9(15) . . . . ?
C105 B56 B54 B58 38.2(12) . . . . ?
C105 B56 B55 B53 59.9(18) . . . . ?
C105 B56 B55 B54 98.4(15) . . . . ?
C105 B56 B55 B49 -3.1(19) . . . . ?
C105 B56 B55 B57 -39.8(13) . . . . ?
C105 B56 B57 B50 33.4(13) . . . . ?
C105 B56 B57 B49 97.8(15) . . . . ?
C105 B56 B57 B55 133.1(15) . . . . ?
C105 B56 B58 C106 -96.3(15) . . . . ?
C105 B56 B58 B51 -33.2(13) . . . . ?
C105 B56 B58 B54 -134.8(15) . . . . ?
C105 B51 B52 B53 -59.4(18) . . . . ?
C105 B51 B52 B50 41.1(13) . . . . ?
C105 B51 B52 C106 -94.1(14) . . . . ?
C105 B51 B52 B49 3.3(19) . . . . ?
C105 B51 B58 C106 131.9(13) . . . . ?
C105 B51 B58 B56 33.1(13) . . . . ?
C105 B51 B58 B54 96.3(15) . . . . ?
B39 B45 B46 C132 93.4(16) . . . . ?
B39 B45 B46 B43 -1(2) . . . . ?
B39 B45 B46 B42 62(2) . . . . ?
B39 B45 B46 B44 -37.5(15) . . . . ?
B39 B45 C132 P12 154.9(13) . . . . ?
B39 B45 C132 B46 -102.1(15) . . . . ?
B39 B45 C132 B47 39.6(14) . . . . ?
B39 B45 C132 B41 4(2) . . . . ?
B39 B45 C132 B42 -68.8(19) . . . . ?
B39 B45 B47 C132 -132.9(15) . . . . ?
B39 B45 B47 B41 -101.1(17) . . . . ?
B39 B45 B47 B59 -36.1(14) . . . . ?
B39 B45 B44 B46 136.9(16) . . . . ?
B39 B45 B44 B43 101.5(16) . . . . ?
B39 B45 B44 B48 36.4(14) . . . . ?
B39 B47 B41 C131 -2(2) . . . . ?
B39 B47 B41 C132 -97.4(17) . . . . ?
B39 B47 B41 B59 36.0(15) . . . . ?
B39 B47 B41 B42 -63.8(19) . . . . ?
B39 B47 B59 C131 -101.5(17) . . . . ?
B39 B47 B59 B41 -139.7(17) . . . . ?
B39 B47 B59 B48 -38.1(14) . . . . ?
B39 B59 B48 C131 -136.3(15) . . . . ?
B39 B59 B48 B43 -99.9(15) . . . . ?
B39 B59 B48 B44 -37.5(14) . . . . ?
B39 B44 B48 C131 99.4(17) . . . . ?
B39 B44 B48 B43 135.2(17) . . . . ?
B39 B44 B48 B59 36.6(14) . . . . ?
C46 C41 C42 C43 -4(4) . . . . ?
C78 C73 C74 C75 -3(3) . . . . ?
C78 C77 C76 C75 7(4) . . . . ?
C87 P8 C80 B32 -153.7(17) . . . . ?
C87 P8 C80 B34 -83.7(18) . . . . ?
C87 P8 C80 B31 136.8(18) . . . . ?
C87 P8 C80 B38 67(2) . . . . ?
C87 P8 C80 B37 -10(2) . . . . ?
C87 P8 C81 C82 165.2(16) . . . . ?
C87 P8 C81 C86 -10(2) . . . . ?
C87 C92 C91 C90 -4(6) . . . . ?
C87 C88 C89 C90 0(8) . . . . ?
B2 C39 B8 B40 -106.1(16) . . . . ?
B2 C39 B8 B5 -65.3(18) . . . . ?
B2 C39 B8 B6 -3.1(19) . . . . ?
B2 C39 B8 B7 37.1(15) . . . . ?
B2 C39 B40 B8 104.1(16) . . . . ?
B2 C39 B40 C40 3.5(19) . . . . ?
B2 C39 B40 B1 -37.4(15) . . . . ?
B2 C39 B40 B5 64.7(18) . . . . ?
B2 C39 B1 C40 99.5(15) . . . . ?
B2 C39 B1 B40 141.0(16) . . . . ?
B2 C39 B1 B9 38.6(14) . . . . ?
B2 C39 B7 B8 -140.4(15) . . . . ?
B2 C39 B7 B6 -100.4(16) . . . . ?
B2 C39 B7 B3 -39.3(14) . . . . ?
B2 B1 B9 C40 132.6(16) . . . . ?
B2 B1 B9 B4 97.7(17) . . . . ?
B2 B1 B9 B3 35.7(14) . . . . ?
B2 B3 B9 C40 -96.5(16) . . . . ?
B2 B3 B9 B4 -136.2(15) . . . . ?
B2 B3 B9 B1 -36.9(14) . . . . ?
B2 B3 B7 C39 39.8(14) . . . . ?
B2 B3 B7 B8 97.2(16) . . . . ?
B2 B3 B7 B6 137.6(16) . . . . ?
B3 B4 B5 B8 0(2) . . . . ?
B3 B4 B5 C40 99.4(16) . . . . ?
B3 B4 B5 B40 63.6(18) . . . . ?
B3 B4 B5 B6 -40.3(14) . . . . ?
B3 B4 B6 B8 98.6(15) . . . . ?
B3 B4 B6 B5 134.7(15) . . . . ?
B3 B4 B6 B7 36.5(14) . . . . ?
B3 B4 B9 C40 -133.8(15) . . . . ?
B3 B4 B9 B1 -99.5(16) . . . . ?
B3 B4 B9 B2 -37.0(13) . . . . ?
B3 B6 B7 C39 97.3(15) . . . . ?
B3 B6 B7 B8 134.6(15) . . . . ?
B3 B6 B7 B2 36.4(13) . . . . ?
B3 B2 B9 C40 98.9(16) . . . . ?
B3 B2 B9 B4 37.9(14) . . . . ?
B3 B2 B9 B1 138.3(16) . . . . ?
B3 B2 B7 C39 -133.2(16) . . . . ?
B3 B2 B7 B8 -100.3(16) . . . . ?
B3 B2 B7 B6 -37.0(14) . . . . ?
B58 C106 B51 B50 -100.8(14) . . . . ?
B58 C106 B51 B52 -140.1(14) . . . . ?
B58 C106 B51 C105 -39.9(11) . . . . ?
B58 C106 B54 B53 139.9(15) . . . . ?
B58 C106 B54 B56 38.8(13) . . . . ?
B58 C106 B54 B55 100.4(15) . . . . ?
B58 C106 B52 B53 -104.1(15) . . . . ?
B58 C106 B52 B50 -1.4(18) . . . . ?
B58 C106 B52 B51 38.4(14) . . . . ?
B58 C106 B52 B49 -65.1(17) . . . . ?
B58 B56 B54 B53 -99.4(15) . . . . ?
B58 B56 B54 C106 -37.0(13) . . . . ?
B58 B56 B54 B55 -136.1(15) . . . . ?
B58 B56 B55 B53 0(2) . . . . ?
B58 B56 B55 B54 38.5(14) . . . . ?
B58 B56 B55 B49 -63.0(19) . . . . ?
B58 B56 B55 B57 -99.7(16) . . . . ?
B58 B56 B57 B50 -0.1(19) . . . . ?
B58 B56 B57 B49 64.3(17) . . . . ?
B58 B56 B57 B55 99.6(15) . . . . ?
B58 B56 B57 C105 -33.5(13) . . . . ?
B58 B56 C105 P9 -107.4(13) . . . . ?
B58 B56 C105 B50 105.4(16) . . . . ?
B58 B56 C105 B51 36.4(13) . . . . ?
B58 B56 C105 B57 141.2(15) . . . . ?
B58 B51 B52 B53 0.6(19) . . . . ?
B58 B51 B52 B50 101.2(15) . . . . ?
B58 B51 B52 C106 -34.0(12) . . . . ?
B58 B51 B52 B49 63.4(18) . . . . ?
B58 B51 C105 P9 105.0(14) . . . . ?
B58 B51 C105 B50 -141.7(14) . . . . ?
B58 B51 C105 B56 -36.6(14) . . . . ?
B58 B51 C105 B57 -106.1(16) . . . . ?
B58 B54 B55 B53 99.4(15) . . . . ?
B58 B54 B55 B56 -39.4(13) . . . . ?
B58 B54 B55 B49 64.7(18) . . . . ?
B58 B54 B55 B57 -0.6(19) . . . . ?
C135 C136 C137 C138 0(5) . . . . ?
B9 C40 B4 B5 141.1(15) . . . . ?
B9 C40 B4 B6 104.8(17) . . . . ?
B9 C40 B4 B3 41.0(14) . . . . ?
B9 C40 B40 C39 -4.0(19) . . . . ?
B9 C40 B40 B8 -65.6(18) . . . . ?
B9 C40 B40 B1 38.9(15) . . . . ?
B9 C40 B40 B5 -102.5(16) . . . . ?
B9 C40 B1 C39 -100.7(16) . . . . ?
B9 C40 B1 B40 -139.5(15) . . . . ?
B9 C40 B1 B2 -40.6(13) . . . . ?
B9 C40 B5 B8 67.0(17) . . . . ?
B9 C40 B5 B4 -36.1(14) . . . . ?
B9 C40 B5 B40 104.5(15) . . . . ?
B9 C40 B5 B6 -0.3(18) . . . . ?
B9 B4 B5 B8 -64.2(19) . . . . ?
B9 B4 B5 C40 35.2(14) . . . . ?
B9 B4 B5 B40 -1(2) . . . . ?
B9 B4 B5 B6 -104.5(17) . . . . ?
B9 B4 B6 B8 64.1(18) . . . . ?
B9 B4 B6 B5 100.2(16) . . . . ?
B9 B4 B6 B3 -34.6(14) . . . . ?
B9 B4 B6 B7 2(2) . . . . ?
B9 B4 B3 B6 142.8(15) . . . . ?
B9 B4 B3 B2 39.8(15) . . . . ?
B9 B4 B3 B7 105.0(17) . . . . ?
B9 B1 B2 C39 -135.5(16) . . . . ?
B9 B1 B2 B3 -38.1(14) . . . . ?
B9 B1 B2 B7 -103.1(17) . . . . ?
B9 B2 B3 B4 -39.0(14) . . . . ?
B9 B2 B3 B6 -102.2(17) . . . . ?
B9 B2 B3 B7 -141.3(16) . . . . ?
B9 B2 B7 C39 -97.4(17) . . . . ?
B9 B2 B7 B8 -64.5(17) . . . . ?
B9 B2 B7 B6 -1.2(19) . . . . ?
B9 B2 B7 B3 35.8(14) . . . . ?
B9 B3 B7 C39 3(2) . . . . ?
B9 B3 B7 B8 61(2) . . . . ?
B9 B3 B7 B6 101.2(17) . . . . ?
B9 B3 B7 B2 -36.4(16) . . . . ?
C81 P8 C80 B32 89.8(18) . . . . ?
C81 P8 C80 B34 159.8(16) . . . . ?
C81 P8 C80 B31 20.3(19) . . . . ?
C81 P8 C80 B38 -50(2) . . . . ?
C81 P8 C80 B37 -126(2) . . . . ?
C81 P8 C87 C92 58(2) . . . . ?
C81 P8 C87 C88 -127(3) . . . . ?
C81 C82 C83 C84 7(3) . . . . ?
C83 C82 C81 P8 -179.8(16) . . . . ?
C83 C82 C81 C86 -4(3) . . . . ?
C83 C84 C85 C86 3(3) . . . . ?
C101 C100 C99 P9 -174.0(15) . . . . ?
C101 C100 C99 C104 -4(3) . . . . ?
B33 C79 B32 C80 -102(2) . . . . ?
B33 C79 B32 B34 -41(2) . . . . ?
B33 C79 B32 B31 -147(2) . . . . ?
B33 C79 B31 C80 -7(2) . . . . ?
B33 C79 B31 B32 34(2) . . . . ?
B33 C79 B31 B30 -108(2) . . . . ?
B33 C79 B31 B38 -66(3) . . . . ?
B33 C79 B30 B31 110(2) . . . . ?
B33 C79 B30 B36 -35(2) . . . . ?
B33 C79 B30 B38 70(3) . . . . ?
B33 C79 B30 B29 7(3) . . . . ?
B33 C79 B36 B30 145(2) . . . . ?
B33 C79 B36 B29 105(3) . . . . ?
B33 C79 B36 B35 42(2) . . . . ?
B33 B32 B34 C80 -134(2) . . . . ?
B33 B32 B34 B35 -40(2) . . . . ?
B33 B32 B34 B37 -95(2) . . . . ?
B33 B32 B31 C80 99(2) . . . . ?
B33 B32 B31 C79 -30.4(19) . . . . ?
B33 B32 B31 B30 4(3) . . . . ?
B33 B32 B31 B38 67(2) . . . . ?
B33 B34 B35 B36 -37(2) . . . . ?
B33 B34 B35 B29 -104(3) . . . . ?
B33 B34 B35 B37 -141(3) . . . . ?
B33 B34 B37 C80 -98(2) . . . . ?
B33 B34 B37 B38 -70(2) . . . . ?
B33 B34 B37 B29 -6(3) . . . . ?
B33 B34 B37 B35 33(2) . . . . ?
B33 B36 B29 B30 102(2) . . . . ?
B33 B36 B29 B38 61(3) . . . . ?
B33 B36 B29 B35 -37(2) . . . . ?
B33 B36 B29 B37 -4(3) . . . . ?
B33 B36 B35 B34 36(2) . . . . ?
B33 B36 B35 B29 140(2) . . . . ?
B33 B36 B35 B37 103(2) . . . . ?
B33 B35 B37 C80 5(3) . . . . ?
B33 B35 B37 B34 -35(2) . . . . ?
B33 B35 B37 B38 65(3) . . . . ?
B33 B35 B37 B29 104(3) . . . . ?
B15 C13 B13 B14 40.0(15) . . . . ?
B15 C13 B13 B19 141.5(16) . . . . ?
B15 C13 B13 B12 102.6(17) . . . . ?
B15 C13 B16 B17 -103.2(16) . . . . ?
B15 C13 B16 B18 -141.7(16) . . . . ?
B15 C13 B16 B10 -39.1(15) . . . . ?
B15 C13 B18 C14 -64.9(16) . . . . ?
B15 C13 B18 B16 35.6(14) . . . . ?
B15 C13 B18 B17 -2.9(19) . . . . ?
B15 C13 B18 B19 -104.7(15) . . . . ?
B15 C13 B19 C14 65.9(17) . . . . ?
B15 C13 B19 B13 -36.0(15) . . . . ?
B15 C13 B19 B18 103.9(16) . . . . ?
B15 C13 B19 B12 3(2) . . . . ?
B15 B13 B14 B11 101.0(17) . . . . ?
B15 B13 B14 B10 36.3(15) . . . . ?
B15 B13 B14 B12 138.2(16) . . . . ?
B15 B13 B19 C13 33.7(14) . . . . ?
B15 B13 B19 C14 -62.2(18) . . . . ?
B15 B13 B19 B18 -2(2) . . . . ?
B15 B13 B19 B12 -102.0(17) . . . . ?
B15 B13 B12 C14 59.6(17) . . . . ?
B15 B13 B12 B14 -37.2(14) . . . . ?
B15 B13 B12 B11 -1.6(18) . . . . ?
B15 B13 B12 B19 98.6(15) . . . . ?
B15 B16 B17 C14 -63.0(17) . . . . ?
B15 B16 B17 B18 -101.6(16) . . . . ?
B15 B16 B17 B11 -0.6(18) . . . . ?
B15 B16 B17 B10 37.9(14) . . . . ?
B15 B16 B18 C13 -34.8(14) . . . . ?
B15 B16 B18 C14 62.8(19) . . . . ?
B15 B16 B18 B17 101.8(17) . . . . ?
B15 B16 B18 B19 -1(2) . . . . ?
B15 B16 B10 B14 -38.1(14) . . . . ?
B15 B16 B10 B17 -138.4(15) . . . . ?
B15 B16 B10 B11 -99.5(16) . . . . ?
B15 B14 B11 C14 62.7(18) . . . . ?
B15 B14 B11 B17 2.7(19) . . . . ?
B15 B14 B11 B10 -36.7(15) . . . . ?
B15 B14 B11 B12 104.0(17) . . . . ?
B15 B14 B10 B16 38.8(14) . . . . ?
B15 B14 B10 B17 99.8(16) . . . . ?
B15 B14 B10 B11 139.4(15) . . . . ?
B15 B14 B12 C14 -60.5(19) . . . . ?
B15 B14 B12 B13 39.2(16) . . . . ?
B15 B14 B12 B11 -100.6(17) . . . . ?
B15 B14 B12 B19 1(2) . . . . ?
B48 C131 B43 B46 -102.2(16) . . . . ?
B48 C131 B43 B42 -142.4(15) . . . . ?
B48 C131 B43 B44 -36.0(14) . . . . ?
B48 C131 B41 C132 64.6(17) . . . . ?
B48 C131 B41 B47 3.1(19) . . . . ?
B48 C131 B41 B59 -34.3(15) . . . . ?
B48 C131 B41 B42 105.3(16) . . . . ?
B48 C131 B59 B47 104.7(17) . . . . ?
B48 C131 B59 B41 143.0(15) . . . . ?
B48 C131 B59 B39 39.7(15) . . . . ?
B48 C131 B42 B46 -3(2) . . . . ?
B48 C131 B42 C132 -64.7(19) . . . . ?
B48 C131 B42 B43 36.3(15) . . . . ?
B48 C131 B42 B41 -103.6(16) . . . . ?
B48 B43 B42 B46 101.8(16) . . . . ?
B48 B43 B42 C131 -33.6(13) . . . . ?
B48 B43 B42 C132 59.4(18) . . . . ?
B48 B43 B42 B41 1.0(19) . . . . ?
B48 B43 B44 B45 -102.4(17) . . . . ?
B48 B43 B44 B46 -138.8(18) . . . . ?
B48 B43 B44 B39 -40.0(15) . . . . ?
B48 B59 B39 B45 102.1(17) . . . . ?
B48 B59 B39 B47 139.2(15) . . . . ?
B48 B59 B39 B44 36.7(14) . . . . ?
B48 B44 B39 B45 -139.6(16) . . . . ?
B48 B44 B39 B47 -99.5(16) . . . . ?
B48 B44 B39 B59 -36.9(15) . . . . ?
C6 C1 C2 C3 3(4) . . . . ?
C6 C5 C4 C3 1(6) . . . . ?
B7 C39 B8 B40 -143.1(14) . . . . ?
B7 C39 B8 B5 -102.4(15) . . . . ?
B7 C39 B8 B6 -40.2(13) . . . . ?
B7 C39 B40 B8 36.4(14) . . . . ?
B7 C39 B40 C40 -64.2(18) . . . . ?
B7 C39 B40 B1 -105.1(16) . . . . ?
B7 C39 B40 B5 -2.9(19) . . . . ?
B7 C39 B1 C40 66.0(18) . . . . ?
B7 C39 B1 B40 107.6(17) . . . . ?
B7 C39 B1 B2 -33.5(15) . . . . ?
B7 C39 B1 B9 5(2) . . . . ?
B7 C39 B2 B1 144.8(16) . . . . ?
B7 C39 B2 B3 41.4(14) . . . . ?
B7 C39 B2 B9 105.2(17) . . . . ?
B7 B8 B40 C39 -34.0(13) . . . . ?
B7 B8 B40 C40 63.3(17) . . . . ?
B7 B8 B40 B1 2(2) . . . . ?
B7 B8 B40 B5 100.3(15) . . . . ?
B7 B8 B5 C40 -65.2(17) . . . . ?
B7 B8 B5 B4 -2(2) . . . . ?
B7 B8 B5 B40 -103.2(16) . . . . ?
B7 B8 B5 B6 36.3(14) . . . . ?
B7 B8 B6 B4 -101.6(17) . . . . ?
B7 B8 B6 B5 -139.3(16) . . . . ?
B7 B8 B6 B3 -39.3(14) . . . . ?
B7 B6 B3 B4 -138.7(16) . . . . ?
B7 B6 B3 B2 -39.1(15) . . . . ?
B7 B6 B3 B9 -105.0(17) . . . . ?
B7 B2 B3 B4 102.3(16) . . . . ?
B7 B2 B3 B6 39.1(15) . . . . ?
B7 B2 B3 B9 141.3(16) . . . . ?
B7 B2 B9 C40 63.2(18) . . . . ?
B7 B2 B9 B4 2.3(19) . . . . ?
B7 B2 B9 B1 102.6(16) . . . . ?
B7 B2 B9 B3 -35.7(14) . . . . ?
B7 B3 B9 C40 -60.2(19) . . . . ?
B7 B3 B9 B4 -99.9(17) . . . . ?
B7 B3 B9 B1 -1(2) . . . . ?
B7 B3 B9 B2 36.3(15) . . . . ?
C49 C48 C47 P4 -177(2) . . . . ?
C49 C48 C47 C52 -2(4) . . . . ?
B34 C80 B32 C79 104(2) . . . . ?
B34 C80 B32 B33 42(2) . . . . ?
B34 C80 B32 B31 147(2) . . . . ?
B34 C80 B31 C79 8(2) . . . . ?
B34 C80 B31 B32 -32.5(19) . . . . ?
B34 C80 B31 B30 68(2) . . . . ?
B34 C80 B31 B38 111(2) . . . . ?
B34 C80 B38 B31 -105(2) . . . . ?
B34 C80 B38 B30 -62(3) . . . . ?
B34 C80 B38 B29 -3(3) . . . . ?
B34 C80 B38 B37 34(2) . . . . ?
B34 C80 B37 B38 -147(2) . . . . ?
B34 C80 B37 B29 -110(3) . . . . ?
B34 C80 B37 B35 -45(2) . . . . ?
B34 B32 B33 C79 136(2) . . . . ?
B34 B32 B33 B36 102(2) . . . . ?
B34 B32 B33 B35 43(2) . . . . ?
B34 B32 B31 C80 30.0(17) . . . . ?
B34 B32 B31 C79 -99(2) . . . . ?
B34 B32 B31 B30 -65(2) . . . . ?
B34 B32 B31 B38 -2(3) . . . . ?
B34 B33 B36 C79 96(2) . . . . ?
B34 B33 B36 B30 63(3) . . . . ?
B34 B33 B36 B29 0(3) . . . . ?
B34 B33 B36 B35 -37(2) . . . . ?
B34 B33 B35 B36 140(2) . . . . ?
B34 B33 B35 B29 102(3) . . . . ?
B34 B33 B35 B37 36(3) . . . . ?
B34 B35 B37 C80 40(2) . . . . ?
B34 B35 B37 B38 101(2) . . . . ?
B34 B35 B37 B29 140(2) . . . . ?
B12 C14 B17 B16 65.1(17) . . . . ?
B12 C14 B17 B18 104.2(15) . . . . ?
B12 C14 B17 B11 -35.9(14) . . . . ?
B12 C14 B17 B10 1.9(19) . . . . ?
B12 C14 B18 C13 -3.1(17) . . . . ?
B12 C14 B18 B16 -65.5(18) . . . . ?
B12 C14 B18 B17 -104.8(15) . . . . ?
B12 C14 B18 B19 35.3(13) . . . . ?
B12 C14 B11 B14 40.7(13) . . . . ?
B12 C14 B11 B17 141.9(15) . . . . ?
B12 C14 B11 B10 104.4(16) . . . . ?
B12 C14 B19 C13 -103.5(14) . . . . ?
B12 C14 B19 B13 -39.6(13) . . . . ?
B12 C14 B19 B18 -142.2(14) . . . . ?
B12 B13 B14 B11 -37.2(15) . . . . ?
B12 B13 B14 B10 -101.9(17) . . . . ?
B12 B13 B14 B15 -138.2(16) . . . . ?
B12 B13 B19 C13 135.8(15) . . . . ?
B12 B13 B19 C14 39.8(14) . . . . ?
B12 B13 B19 B18 100.0(16) . . . . ?
B12 B13 B15 C13 -96.4(15) . . . . ?
B12 B13 B15 B16 -62.0(19) . . . . ?
B12 B13 B15 B14 37.5(14) . . . . ?
B12 B13 B15 B10 1.5(19) . . . . ?
B12 B14 B11 C14 -41.3(13) . . . . ?
B12 B14 B11 B17 -101.4(15) . . . . ?
B12 B14 B11 B10 -140.7(15) . . . . ?
B12 B14 B10 B16 -64.5(19) . . . . ?
B12 B14 B10 B17 -4(2) . . . . ?
B12 B14 B10 B11 36.2(14) . . . . ?
B12 B14 B10 B15 -103.3(17) . . . . ?
B12 B14 B15 C13 1(2) . . . . ?
B12 B14 B15 B13 -38.8(15) . . . . ?
B12 B14 B15 B16 62(2) . . . . ?
B12 B14 B15 B10 101.9(17) . . . . ?
B12 B11 B10 B16 62.2(18) . . . . ?
B12 B11 B10 B14 -35.3(14) . . . . ?
B12 B11 B10 B17 100.1(15) . . . . ?
B12 B11 B10 B15 -0.2(19) . . . . ?
C76 C77 C78 C73 -9(4) . . . . ?
C71 C72 C67 P7 -180(2) . . . . ?
C71 C72 C67 C68 -2(5) . . . . ?
C71 C70 C69 C68 2(6) . . . . ?
C91 C92 C87 P8 179(2) . . . . ?
C91 C92 C87 C88 3(4) . . . . ?
C4 C3 C2 C1 2(5) . . . . ?
C4 C5 C6 C1 3(5) . . . . ?
C115 C116 C117 C118 -1(4) . . . . ?
B31 C80 B32 C79 -43.4(17) . . . . ?
B31 C80 B32 B33 -105(2) . . . . ?
B31 C80 B32 B34 -147(2) . . . . ?
B31 C80 B34 B32 32.1(19) . . . . ?
B31 C80 B34 B33 -6(2) . . . . ?
B31 C80 B34 B35 -66(2) . . . . ?
B31 C80 B34 B37 -103(2) . . . . ?
B31 C80 B38 B30 42.8(19) . . . . ?
B31 C80 B38 B29 102(2) . . . . ?
B31 C80 B38 B37 139(2) . . . . ?
B31 C80 B37 B34 109(2) . . . . ?
B31 C80 B37 B38 -38(2) . . . . ?
B31 C80 B37 B29 -1(3) . . . . ?
B31 C80 B37 B35 64(3) . . . . ?
B31 C79 B32 C80 44.7(18) . . . . ?
B31 C79 B32 B33 147(2) . . . . ?
B31 C79 B32 B34 105(2) . . . . ?
B31 C79 B33 B32 -34(2) . . . . ?
B31 C79 B33 B34 4(3) . . . . ?
B31 C79 B33 B36 106(2) . . . . ?
B31 C79 B33 B35 67(3) . . . . ?
B31 C79 B30 B36 -145(2) . . . . ?
B31 C79 B30 B38 -40(2) . . . . ?
B31 C79 B30 B29 -103(2) . . . . ?
B31 C79 B36 B33 -111(2) . . . . ?
B31 C79 B36 B30 34(2) . . . . ?
B31 C79 B36 B29 -6(3) . . . . ?
B31 C79 B36 B35 -69(3) . . . . ?
B31 B32 B33 C79 30.4(19) . . . . ?
B31 B32 B33 B34 -105(2) . . . . ?
B31 B32 B33 B36 -3(3) . . . . ?
B31 B32 B33 B35 -62(3) . . . . ?
B31 B32 B34 C80 -31.2(19) . . . . ?
B31 B32 B34 B33 103(2) . . . . ?
B31 B32 B34 B35 63(2) . . . . ?
B31 B32 B34 B37 8(3) . . . . ?
B31 B30 B36 C79 -30(2) . . . . ?
B31 B30 B36 B33 1(3) . . . . ?
B31 B30 B36 B29 103(2) . . . . ?
B31 B30 B36 B35 66(3) . . . . ?
B31 B30 B38 C80 -43.2(19) . . . . ?
B31 B30 B38 B29 -141(3) . . . . ?
B31 B30 B38 B37 -103(2) . . . . ?
B31 B30 B29 B36 -100(3) . . . . ?
B31 B30 B29 B38 35(2) . . . . ?
B31 B30 B29 B35 -66(3) . . . . ?
B31 B30 B29 B37 -7(3) . . . . ?
B31 B38 B29 B30 -35(2) . . . . ?
B31 B38 B29 B36 4(3) . . . . ?
B31 B38 B29 B35 64(3) . . . . ?
B31 B38 B29 B37 100(2) . . . . ?
B31 B38 B37 C80 37.2(19) . . . . ?
B31 B38 B37 B34 9(3) . . . . ?
B31 B38 B37 B29 -100(2) . . . . ?
B31 B38 B37 B35 -59(3) . . . . ?
B30 C79 B32 C80 6(3) . . . . ?
B30 C79 B32 B33 108(2) . . . . ?
B30 C79 B32 B34 67(3) . . . . ?
B30 C79 B32 B31 -38(2) . . . . ?
B30 C79 B33 B32 -107(2) . . . . ?
B30 C79 B33 B34 -69(2) . . . . ?
B30 C79 B33 B36 34(2) . . . . ?
B30 C79 B33 B35 -5(3) . . . . ?
B30 C79 B31 C80 100(2) . . . . ?
B30 C79 B31 B32 141(2) . . . . ?
B30 C79 B31 B38 41(2) . . . . ?
B30 C79 B36 B33 -145(2) . . . . ?
B30 C79 B36 B29 -40(2) . . . . ?
B30 C79 B36 B35 -103(3) . . . . ?
B30 B31 B38 C80 131(2) . . . . ?
B30 B31 B38 B29 33(2) . . . . ?
B30 B31 B38 B37 95(2) . . . . ?
B30 B36 B29 B38 -41(2) . . . . ?
B30 B36 B29 B35 -139(2) . . . . ?
B30 B36 B29 B37 -105(2) . . . . ?
B30 B36 B35 B33 -104(2) . . . . ?
B30 B36 B35 B34 -68(3) . . . . ?
B30 B36 B35 B29 36(2) . . . . ?
B30 B36 B35 B37 -1(3) . . . . ?
B30 B38 B29 B36 39(2) . . . . ?
B30 B38 B29 B35 98(2) . . . . ?
B30 B38 B29 B37 135(2) . . . . ?
B30 B38 B37 C80 100(2) . . . . ?
B30 B38 B37 B34 72(2) . . . . ?
B30 B38 B37 B29 -38(2) . . . . ?
B30 B38 B37 B35 3(3) . . . . ?
B30 B29 B35 B33 2(3) . . . . ?
B30 B29 B35 B34 67(3) . . . . ?
B30 B29 B35 B36 -35(2) . . . . ?
B30 B29 B35 B37 104(2) . . . . ?
B30 B29 B37 C80 5(3) . . . . ?
B30 B29 B37 B34 -54(3) . . . . ?
B30 B29 B37 B38 42(2) . . . . ?
B30 B29 B37 B35 -95(3) . . . . ?
B36 C79 B32 C80 -62(3) . . . . ?
B36 C79 B32 B33 40(2) . . . . ?
B36 C79 B32 B34 -1(3) . . . . ?
B36 C79 B32 B31 -107(2) . . . . ?
B36 C79 B33 B32 -141(2) . . . . ?
B36 C79 B33 B34 -102(2) . . . . ?
B36 C79 B33 B35 -39(2) . . . . ?
B36 C79 B31 C80 68(3) . . . . ?
B36 C79 B31 B32 108(2) . . . . ?
B36 C79 B31 B30 -33(2) . . . . ?
B36 C79 B31 B38 9(3) . . . . ?
B36 C79 B30 B31 145(2) . . . . ?
B36 C79 B30 B38 105(2) . . . . ?
B36 C79 B30 B29 42(2) . . . . ?
B36 B33 B34 C80 -58(2) . . . . ?
B36 B33 B34 B32 -97(2) . . . . ?
B36 B33 B34 B35 35(2) . . . . ?
B36 B33 B34 B37 3(2) . . . . ?
B36 B33 B35 B34 -140(2) . . . . ?
B36 B33 B35 B29 -37(2) . . . . ?
B36 B33 B35 B37 -103(3) . . . . ?
B36 B30 B38 C80 56(3) . . . . ?
B36 B30 B38 B31 100(2) . . . . ?
B36 B30 B38 B29 -42(2) . . . . ?
B36 B30 B38 B37 -4(3) . . . . ?
B36 B30 B29 B38 135(2) . . . . ?
B36 B30 B29 B35 35(2) . . . . ?
B36 B30 B29 B37 93(3) . . . . ?
B36 B29 B35 B33 37(2) . . . . ?
B36 B29 B35 B34 102(2) . . . . ?
B36 B29 B35 B37 139(2) . . . . ?
B36 B29 B37 C80 65(3) . . . . ?
B36 B29 B37 B34 6(3) . . . . ?
B36 B29 B37 B38 102(2) . . . . ?
B36 B29 B37 B35 -34(2) . . . . ?
B36 B35 B37 C80 -62(3) . . . . ?
B36 B35 B37 B34 -102(2) . . . . ?
B36 B35 B37 B38 -1(3) . . . . ?
B36 B35 B37 B29 38(2) . . . . ?
B38 C80 B32 C79 -9(2) . . . . ?
B38 C80 B32 B33 -70(3) . . . . ?
B38 C80 B32 B34 -112(2) . . . . ?
B38 C80 B32 B31 34.6(19) . . . . ?
B38 C80 B34 B32 102(2) . . . . ?
B38 C80 B34 B33 63(3) . . . . ?
B38 C80 B34 B35 4(3) . . . . ?
B38 C80 B34 B37 -34(2) . . . . ?
B38 C80 B31 C79 -103(2) . . . . ?
B38 C80 B31 B32 -143(2) . . . . ?
B38 C80 B31 B30 -43(2) . . . . ?
B38 C80 B37 B34 147(2) . . . . ?
B38 C80 B37 B29 37(2) . . . . ?
B38 C80 B37 B35 103(3) . . . . ?
B38 B31 B30 C79 -133(2) . . . . ?
B38 B31 B30 B36 -102(3) . . . . ?
B38 B31 B30 B29 -35(2) . . . . ?
B38 B30 B36 C79 -93(2) . . . . ?
B38 B30 B36 B33 -62(3) . . . . ?
B38 B30 B36 B29 41(2) . . . . ?
B38 B30 B36 B35 3(3) . . . . ?
B38 B30 B29 B36 -135(2) . . . . ?
B38 B30 B29 B35 -100(2) . . . . ?
B38 B30 B29 B37 -42(2) . . . . ?
B38 B29 B35 B33 -63(3) . . . . ?
B38 B29 B35 B34 2(3) . . . . ?
B38 B29 B35 B36 -100(2) . . . . ?
B38 B29 B35 B37 40(2) . . . . ?
B38 B29 B37 C80 -37(2) . . . . ?
B38 B29 B37 B34 -96(2) . . . . ?
B38 B29 B37 B35 -136(2) . . . . ?
B29 B30 B36 C79 -133(2) . . . . ?
B29 B30 B36 B33 -103(3) . . . . ?
B29 B30 B36 B35 -37(2) . . . . ?
B29 B30 B38 C80 98(2) . . . . ?
B29 B30 B38 B31 141(3) . . . . ?
B29 B30 B38 B37 38(2) . . . . ?
B29 B36 B35 B33 -140(2) . . . . ?
B29 B36 B35 B34 -104(2) . . . . ?
B29 B36 B35 B37 -38(2) . . . . ?
B29 B38 B37 C80 137(2) . . . . ?
B29 B38 B37 B34 109(3) . . . . ?
B29 B38 B37 B35 41(2) . . . . ?
B29 B35 B37 C80 -100(2) . . . . ?
B29 B35 B37 B34 -140(2) . . . . ?
B29 B35 B37 B38 -39(2) . . . . ?
B35 B33 B34 C80 -93(2) . . . . ?
B35 B33 B34 B32 -132(2) . . . . ?
B35 B33 B34 B37 -31(2) . . . . ?
B35 B33 B36 C79 132(2) . . . . ?
B35 B33 B36 B30 100(3) . . . . ?
B35 B33 B36 B29 37(2) . . . . ?
B35 B34 B37 C80 -132(2) . . . . ?
B35 B34 B37 B38 -103(3) . . . . ?
B35 B34 B37 B29 -39(2) . . . . ?
B35 B36 B29 B30 139(2) . . . . ?
B35 B36 B29 B38 98(3) . . . . ?
B35 B36 B29 B37 33(2) . . . . ?
B35 B29 B37 C80 100(2) . . . . ?
B35 B29 B37 B34 40(2) . . . . ?
B35 B29 B37 B38 136(2) . . . . ?
B37 C80 B32 C79 61(2) . . . . ?
B37 C80 B32 B33 -1(3) . . . . ?
B37 C80 B32 B34 -43(2) . . . . ?
B37 C80 B32 B31 104(2) . . . . ?
B37 C80 B34 B32 135(2) . . . . ?
B37 C80 B34 B33 97(2) . . . . ?
B37 C80 B34 B35 37.4(19) . . . . ?
B37 C80 B31 C79 -63(2) . . . . ?
B37 C80 B31 B32 -104(2) . . . . ?
B37 C80 B31 B30 -3(3) . . . . ?
B37 C80 B31 B38 40(2) . . . . ?
B37 C80 B38 B31 -139(2) . . . . ?
B37 C80 B38 B30 -96(2) . . . . ?
B37 C80 B38 B29 -37(2) . . . . ?
B37 B34 B35 B33 141(3) . . . . ?
B37 B34 B35 B36 104(3) . . . . ?
B37 B34 B35 B29 37(2) . . . . ?
B37 B38 B29 B30 -135(2) . . . . ?
B37 B38 B29 B36 -96(3) . . . . ?
B37 B38 B29 B35 -36(2) . . . . ?
B37 B29 B35 B33 -102(2) . . . . ?
B37 B29 B35 B34 -38(2) . . . . ?
B37 B29 B35 B36 -139(2) . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 -0.980 -0.682 -0.182 2191.9 617.4 ?
2 0.422 0.452 0.191 26.2 3.7 ?
3 0.578 0.548 0.809 26.2 0.0 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_mo_97_0m_pl
_database_code_depnum_ccdc_archive 'CCDC 2495510'
loop_
_audit_author_name
_audit_author_address
'Hao-Hui Xie'
;NanJing University of Science and Technology
China
;
_audit_update_record             
;
2025-10-15 deposited with the CCDC.	2026-03-06 downloaded from the CCDC.
;
_audit_creation_date             2025-10-07
_audit_creation_method           
;
Olex2 1.5
(compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C52 H60 Au8 B20 P4 S4, [+ solvents]'
_chemical_formula_sum            'C52 H60 Au8 B20 P4 S4'
_chemical_formula_weight         2729.05
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_H-M_alt        'P 1 21/c 1'
_space_group_name_Hall           '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   13.314(5)
_cell_length_b                   23.337(10)
_cell_length_c                   26.678(10)
_cell_angle_alpha                90
_cell_angle_beta                 93.510(15)
_cell_angle_gamma                90
_cell_volume                     8274(6)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    635
_cell_measurement_temperature    100.15
_cell_measurement_theta_max      14.078
_cell_measurement_theta_min      2.416
_shelx_estimated_absorpt_T_max   0.598
_shelx_estimated_absorpt_T_min   0.434
_exptl_absorpt_coefficient_mu    14.337
_exptl_absorpt_correction_T_max  0.7438
_exptl_absorpt_correction_T_min  0.3304
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
SADABS-2016/2 (Bruker,2016/2) was used for absorption correction.
wR2(int) was 0.1835 before and 0.1269 after correction.
The Ratio of minimum to maximum transmission is 0.4442.
The λ/2 correction factor is Not present.
;
_exptl_absorpt_special_details   ?
_exptl_crystal_colour            yellow
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    2.191
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             4912
_exptl_crystal_size_max          0.07
_exptl_crystal_size_mid          0.05
_exptl_crystal_size_min          0.04
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.2694
_diffrn_reflns_av_unetI/netI     0.1047
_diffrn_reflns_Laue_measured_fraction_full 0.994
_diffrn_reflns_Laue_measured_fraction_max 0.994
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            36877
_diffrn_reflns_point_group_measured_fraction_full 0.994
_diffrn_reflns_point_group_measured_fraction_max 0.994
_diffrn_reflns_theta_full        14.526
_diffrn_reflns_theta_max         14.526
_diffrn_reflns_theta_min         1.884
_diffrn_ambient_temperature      100.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  multi-scan
_diffrn_measurement_method       ?
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_diffrn_source_current           1.6
_diffrn_source_power             0.08
_diffrn_source_voltage           50.0
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                2241
_reflns_number_total             3030
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       'SAINT V8.41 (?, 2016)'
_computing_data_collection       ?
_computing_data_reduction        'SAINT V8.41 (?, 2016)'
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'olex2.solve 1.5 (Bourhis et al., 2015)'
_refine_diff_density_max         3.647
_refine_diff_density_min         -1.552
_refine_diff_density_rms         0.353
_refine_ls_extinction_coef       .
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.045
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     337
_refine_ls_number_reflns         3030
_refine_ls_number_restraints     49
_refine_ls_R_factor_all          0.1091
_refine_ls_R_factor_gt           0.0807
_refine_ls_restrained_S_all      1.035
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.1208P)²+1336.2887P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2110
_refine_ls_wR_factor_ref         0.2428
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, All C(H) groups
2. Restrained distances
 H035-H03P
 2.1 with sigma of 0.01
3. Uiso/Uaniso restraints and constraints
P00M \\sim C02O \\sim C03X \\sim C03S \\sim C03O \\sim C03V \\sim C045: within
2A with sigma of 0.001 and sigma for terminal atoms of 0.002 within 2A
P00U \\sim C14 \\sim C1 \\sim C6 \\sim C39 \\sim C13 \\sim C16: within 2A with
sigma of 0.001 and sigma for terminal atoms of 0.002 within 2A
C66 \\sim C37 \\sim C035 \\sim C046 \\sim C3 \\sim C45 \\sim P00N \\sim C018
\\sim C03E \\sim C01A \\sim C01G \\sim C03P \\sim C02A: within 2A with sigma of
0.001 and sigma for terminal atoms of 0.002 within 2A
C3 \\sim C45 \\sim C046 \\sim C035 \\sim C37 \\sim C66: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
C035 \\sim C046 \\sim C45 \\sim C3 \\sim C66 \\sim C37: within 2A with sigma of
0.001 and sigma for terminal atoms of 0.002 within 2A
4.a Aromatic/amide H refined with riding coordinates:
 C00Z(H00Z), C03J(H03J), C021(H021), C69(H69), C044(H044), C014(H014),
 C03Y(H03Y), C27(H27), C03L(H03L), C039(H039), C6(H6), C39(H39), C13(H13),
 C16(H16), C1(H1), C03P(H03P), C02A(H02A), C01G(H01G), C01A(H01A), C03E(H03E),
 C01C(H01C), C01N(H01N), C01F(H01F), C026(H026), C038(H038), C01Z(H01Z),
 C03M(H03M), C03Q(H03Q), C02D(H02D), C02K(H02K), C03X(H03X), C03S(H03S),
 C03O(H03O), C03V(H03V), C045(H045), C37(H37), C035(H035), C45(H45), C3(H3),
 C66(H66)
4.b Fitted hexagon refined as free rotating group:
 C00Z(C25,C03J,C021,C69,C044), C014(C03Y,C27,C03L,C039,C02G), C6(C39,C13,C16,
 C14,C1), C018(C03P,C02A,C01G,C01A,C03E), C01C(C01N,C01F,C01T,C026,C038),
 C01Z(C03M,C03Q,C70,C02D,C02K), C02O(C03X,C03S,C03O,C03V,C045), C37(C035,C046,
 C45,C3,C66)
4.c Boron cage BH refined with riding coordinates:
 B5(H5), B027(H027), B02P(H02P), B037(H037), B1(H1a), B03A(H03A), B03B(H03B),
 B7(H7), B03H(H03H), B03I(H03I), B03R(H03R), B15(H15), B18(H18), B21(H21),
 B26(H26), B28(H28), B44(H44), B49(H49), B94(H94), B22(H22)
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     iterative
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au4 Au 0.2945(2) 0.57362(14) 0.85057(12) 0.0347(14) Uani 1 1 d . . . . .
Au3 Au 0.2520(2) 0.47191(14) 0.91183(12) 0.0354(14) Uani 1 1 d . . . . .
Au8 Au 0.2177(2) 0.37346(14) 0.97707(13) 0.0364(14) Uani 1 1 d . . . . .
Au5 Au 0.3570(2) 0.45557(14) 0.80658(13) 0.0378(14) Uani 1 1 d . . . . .
Au1 Au -0.0431(3) 0.40597(14) 0.78235(13) 0.0398(14) Uani 1 1 d . . . . .
Au2 Au 0.0762(2) 0.37857(14) 0.87674(13) 0.0391(14) Uani 1 1 d . . . . .
Au6 Au 0.3926(3) 0.33211(15) 0.77653(13) 0.0424(14) Uani 1 1 d . . . . .
Au7 Au 0.1744(3) 0.36537(15) 0.76954(13) 0.0430(14) Uani 1 1 d . . . . .
S00H S 0.0426(15) 0.3206(9) 0.8055(8) 0.038(7) Uani 1 1 d . . . . .
S00I S 0.1030(15) 0.4416(9) 0.9442(7) 0.034(7) Uani 1 1 d . . . . .
S00L S 0.4036(16) 0.5008(10) 0.8801(8) 0.047(7) Uani 1 1 d . . . . .
S00T S 0.3114(17) 0.4061(9) 0.7325(8) 0.046(7) Uani 1 1 d . . . . .
P00M P 0.3343(16) 0.3113(10) 1.0083(8) 0.036(5) Uani 1 1 d . U . . .
P00N P -0.1354(19) 0.4866(11) 0.7689(9) 0.061(5) Uani 1 1 d . U . . .
P00S P 0.1822(16) 0.6437(9) 0.8302(8) 0.029(7) Uani 1 1 d . . . . .
P00U P 0.4815(17) 0.2607(10) 0.8149(9) 0.048(6) Uani 1 1 d . U . . .
C00Z C 0.426(3) 0.195(2) 0.731(2) 0.07(3) Uiso 1 1 d G . . . .
H00Z H 0.381596 0.225225 0.721461 0.088 Uiso 1 1 calc R U . . .
C25 C 0.487(4) 0.1984(18) 0.7748(18) 0.01(2) Uiso 1 1 d G . . . .
C03J C 0.552(3) 0.154(2) 0.7887(15) 0.06(3) Uiso 1 1 d G . . . .
H03J H 0.594173 0.156187 0.818623 0.073 Uiso 1 1 calc R U . . .
C021 C 0.554(3) 0.105(2) 0.759(2) 0.07(3) Uiso 1 1 d G . . . .
H021 H 0.598339 0.074059 0.768473 0.082 Uiso 1 1 calc R U . . .
C69 C 0.492(4) 0.1009(19) 0.7152(18) 0.03(2) Uiso 1 1 d G . . . .
H69 H 0.494134 0.067513 0.694817 0.034 Uiso 1 1 calc R U . . .
C044 C 0.428(4) 0.146(2) 0.7012(15) 0.07(3) Uiso 1 1 d G . . . .
H044 H 0.385762 0.143096 0.671310 0.088 Uiso 1 1 calc R U . . .
B5 B 0.451(7) 0.254(4) 0.927(3) 0.02(3) Uiso 1 1 d . . . . .
H5 H 0.510430 0.287541 0.933860 0.023 Uiso 1 1 calc R U . . .
C014 C 0.338(4) 0.713(2) 0.8279(18) 0.05(3) Uiso 1 1 d G . . . .
H014 H 0.371467 0.680741 0.843024 0.059 Uiso 1 1 calc R U . . .
C03Y C 0.390(3) 0.764(3) 0.8224(19) 0.10(4) Uiso 1 1 d G . . . .
H03Y H 0.458412 0.766854 0.833707 0.124 Uiso 1 1 calc R U . . .
C27 C 0.340(4) 0.811(2) 0.800(2) 0.05(3) Uiso 1 1 d G . . . .
H27 H 0.375742 0.845986 0.796454 0.057 Uiso 1 1 calc R U . . .
C03L C 0.240(5) 0.807(2) 0.7836(18) 0.08(3) Uiso 1 1 d G . . . .
H03L H 0.206129 0.839006 0.768517 0.099 Uiso 1 1 calc R U . . .
C039 C 0.188(3) 0.756(3) 0.7892(19) 0.07(3) Uiso 1 1 d G . . . .
H039 H 0.119183 0.752893 0.777833 0.083 Uiso 1 1 calc R U . . .
C02G C 0.237(4) 0.709(2) 0.8113(19) 0.04(3) Uiso 1 1 d G . . . .
C6 C 0.783(3) 0.286(2) 0.8559(18) 0.048(6) Uiso 1 1 d G U . . .
H6 H 0.846400 0.267467 0.854178 0.058 Uiso 1 1 calc R U . . .
C39 C 0.779(3) 0.341(2) 0.8756(17) 0.048(6) Uiso 1 1 d G U . . .
H39 H 0.838884 0.360114 0.887284 0.058 Uiso 1 1 calc R U . . .
C13 C 0.686(4) 0.3684(17) 0.8781(17) 0.048(6) Uiso 1 1 d G U . . .
H13 H 0.683416 0.406057 0.891524 0.058 Uiso 1 1 calc R U . . .
C16 C 0.599(3) 0.341(2) 0.8609(18) 0.048(6) Uiso 1 1 d G U . . .
H16 H 0.535462 0.359354 0.862658 0.058 Uiso 1 1 calc R U . . .
C14 C 0.603(3) 0.286(2) 0.8413(18) 0.048(6) Uiso 1 1 d G U . . .
C1 C 0.695(5) 0.2584(17) 0.8388(17) 0.048(6) Uiso 1 1 d G U . . .
H1 H 0.698443 0.220763 0.825311 0.058 Uiso 1 1 calc R U . . .
C018 C -0.194(4) 0.504(2) 0.8291(16) 0.061(5) Uiso 1 1 d G U . . .
C03P C -0.292(4) 0.521(2) 0.8367(14) 0.061(5) Uiso 1 1 d G U . . .
H03P H -0.339393 0.524508 0.808852 0.073 Uiso 1 1 calc DR U . . .
C02A C -0.320(3) 0.531(2) 0.8850(18) 0.061(5) Uiso 1 1 d G U . . .
H02A H -0.387451 0.542919 0.890214 0.073 Uiso 1 1 calc R U . . .
C01G C -0.251(4) 0.526(2) 0.9257(14) 0.061(5) Uiso 1 1 d G U . . .
H01G H -0.270424 0.533050 0.958757 0.073 Uiso 1 1 calc R U . . .
C01A C -0.153(4) 0.509(2) 0.9181(18) 0.061(5) Uiso 1 1 d G U . . .
H01A H -0.105338 0.504771 0.945938 0.073 Uiso 1 1 calc R U . . .
C03E C -0.124(3) 0.498(2) 0.870(2) 0.060(5) Uiso 1 1 d G U . . .
H03E H -0.057278 0.486360 0.864575 0.073 Uiso 1 1 calc R U . . .
C01C C 0.021(3) 0.680(2) 0.9712(14) 0.04(3) Uiso 1 1 d G . . . .
H01C H -0.010772 0.687635 1.001629 0.054 Uiso 1 1 calc R U . . .
C01N C 0.045(3) 0.6247(19) 0.9581(17) 0.03(2) Uiso 1 1 d G . . . .
H01N H 0.029538 0.593769 0.979450 0.036 Uiso 1 1 calc R U . . .
C01F C 0.091(4) 0.6143(16) 0.9136(19) 0.06(3) Uiso 1 1 d G . . . .
H01F H 0.106990 0.576177 0.904563 0.071 Uiso 1 1 calc R U . . .
C01T C 0.113(3) 0.660(2) 0.8823(14) 0.02(2) Uiso 1 1 d G . . . .
C026 C 0.089(3) 0.7154(19) 0.8954(16) 0.01(2) Uiso 1 1 d G . . . .
H026 H 0.103823 0.746319 0.874030 0.015 Uiso 1 1 calc R U . . .
C038 C 0.043(3) 0.7258(17) 0.9399(18) 0.04(2) Uiso 1 1 d G . . . .
H038 H 0.026371 0.763912 0.948918 0.045 Uiso 1 1 calc R U . . .
C19 C 0.420(5) 0.233(3) 0.871(2) 0.01(2) Uiso 1 1 d . . . . .
C01Z C 0.237(3) 0.237(2) 1.1587(13) 0.01(2) Uiso 1 1 d G . . . .
H01Z H 0.216722 0.222615 1.189864 0.013 Uiso 1 1 calc R U . . .
C03M C 0.314(3) 0.2087(16) 1.1349(17) 0.03(2) Uiso 1 1 d G . . . .
H03M H 0.345037 0.175811 1.149833 0.031 Uiso 1 1 calc R U . . .
C03Q C 0.344(3) 0.229(2) 1.0892(17) 0.03(2) Uiso 1 1 d G . . . .
H03Q H 0.396149 0.210062 1.072989 0.031 Uiso 1 1 calc R U . . .
C70 C 0.298(4) 0.277(2) 1.0674(14) 0.05(3) Uiso 1 1 d G . . . .
C02D C 0.222(4) 0.3050(17) 1.0912(18) 0.05(3) Uiso 1 1 d G . . . .
H02D H 0.190632 0.337922 1.076205 0.058 Uiso 1 1 calc R U . . .
C02K C 0.192(3) 0.2847(19) 1.1368(18) 0.04(3) Uiso 1 1 d G . . . .
H02K H 0.139518 0.303671 1.153050 0.050 Uiso 1 1 calc R U . . .
C025 C 0.091(6) 0.624(3) 0.777(3) 0.04(3) Uiso 1 1 d . . . . .
B027 B -0.110(8) 0.619(4) 0.736(3) 0.05(4) Uiso 1 1 d . . . . .
H027 H -0.189826 0.633605 0.735480 0.062 Uiso 1 1 calc R U . . .
C02O C 0.464(3) 0.345(2) 1.0168(18) 0.036(5) Uiso 1 1 d G U . . .
C03X C 0.545(4) 0.3188(17) 1.0433(16) 0.036(5) Uiso 1 1 d G U . . .
H03X H 0.534284 0.284519 1.061458 0.043 Uiso 1 1 calc R U . . .
C03S C 0.640(3) 0.343(2) 1.0432(16) 0.036(5) Uiso 1 1 d G U . . .
H03S H 0.695107 0.324952 1.061383 0.043 Uiso 1 1 calc R U . . .
C03O C 0.655(3) 0.393(2) 1.0167(17) 0.036(5) Uiso 1 1 d G U . . .
H03O H 0.720295 0.409454 1.016634 0.043 Uiso 1 1 calc R U . . .
C03V C 0.574(4) 0.4192(16) 0.9901(16) 0.036(5) Uiso 1 1 d G U . . .
H03V H 0.584662 0.453524 0.971960 0.043 Uiso 1 1 calc R U . . .
C045 C 0.479(3) 0.395(2) 0.9902(16) 0.036(5) Uiso 1 1 d G U . . .
H045 H 0.423839 0.413092 0.972036 0.043 Uiso 1 1 calc R U . . .
C37 C -0.366(3) 0.513(2) 0.6665(18) 0.061(5) Uiso 1 1 d G U . . .
H37 H -0.421976 0.536804 0.659586 0.073 Uiso 1 1 calc R U . . .
C035 C -0.306(4) 0.5193(19) 0.7108(14) 0.061(5) Uiso 1 1 d G U . . .
H035 H -0.321780 0.548252 0.734077 0.073 Uiso 1 1 calc DR U . . .
C046 C -0.223(4) 0.484(2) 0.7209(16) 0.061(5) Uiso 1 1 d G U . . .
C45 C -0.200(3) 0.442(2) 0.687(2) 0.061(5) Uiso 1 1 d G U . . .
H45 H -0.143896 0.417278 0.693662 0.073 Uiso 1 1 calc R U . . .
C3 C -0.260(4) 0.4347(19) 0.6425(18) 0.061(5) Uiso 1 1 d G U . . .
H3 H -0.244091 0.405829 0.619171 0.073 Uiso 1 1 calc R U . . .
C66 C -0.342(4) 0.470(2) 0.6324(15) 0.061(5) Uiso 1 1 d G U . . .
H66 H -0.383131 0.465591 0.602132 0.073 Uiso 1 1 calc R U . . .
C029 C -0.050(5) 0.547(3) 0.750(3) 0.03(2) Uiso 1 1 d . . . . .
B02P B 0.291(6) 0.226(3) 0.864(3) 0.00(3) Uiso 1 1 d . . . . .
H02P H 0.244413 0.235333 0.828135 0.006 Uiso 1 1 calc R U . . .
B037 B 0.058(6) 0.555(4) 0.780(3) 0.02(3) Uiso 1 1 d . . . . .
H037 H 0.083887 0.525068 0.811622 0.024 Uiso 1 1 calc R U . . .
B1 B 0.255(9) 0.242(5) 0.923(4) 0.07(4) Uiso 1 1 d . . . . .
H1A H 0.181797 0.263278 0.928933 0.082 Uiso 1 1 calc R U . . .
B03A B 0.260(7) 0.167(4) 0.907(3) 0.03(3) Uiso 1 1 d . . . . .
H03A H 0.193429 0.137683 0.902150 0.037 Uiso 1 1 calc R U . . .
B03B B -0.009(6) 0.659(4) 0.756(3) 0.02(3) Uiso 1 1 d . . . . .
H03B H -0.028493 0.702911 0.769635 0.026 Uiso 1 1 calc R U . . .
B7 B 0.374(6) 0.139(4) 0.932(3) 0.03(3) Uiso 1 1 d . . . . .
H7 H 0.380349 0.091834 0.940304 0.036 Uiso 1 1 calc R U . . .
B03H B -0.025(7) 0.602(4) 0.797(4) 0.04(3) Uiso 1 1 d . . . . .
H03H H -0.051143 0.604202 0.835711 0.050 Uiso 1 1 calc R U . . .
B03I B -0.065(6) 0.571(3) 0.691(3) 0.00(2) Uiso 1 1 d . . . . .
H03I H -0.120202 0.552566 0.661813 0.003 Uiso 1 1 calc R U . . .
B03R B 0.366(7) 0.169(4) 0.867(3) 0.04(3) Uiso 1 1 d . . . . .
H03R H 0.368625 0.141077 0.832831 0.046 Uiso 1 1 calc R U . . .
B15 B 0.342(6) 0.277(4) 0.900(3) 0.03(3) Uiso 1 1 d . . . . .
H15 H 0.327890 0.322775 0.888666 0.037 Uiso 1 1 calc R U . . .
C17 C 0.358(5) 0.255(3) 0.961(2) 0.02(2) Uiso 1 1 d . . . . .
B18 B 0.043(6) 0.534(4) 0.717(3) 0.02(3) Uiso 1 1 d . . . . .
H18 H 0.059610 0.489635 0.703597 0.025 Uiso 1 1 calc R U . . .
B21 B 0.092(6) 0.645(4) 0.726(3) 0.02(3) Uiso 1 1 d . . . . .
H21 H 0.146389 0.680586 0.719864 0.021 Uiso 1 1 calc R U . . .
B26 B 0.489(7) 0.185(3) 0.913(3) 0.02(3) Uiso 1 1 d . . . . .
H26 H 0.568331 0.170601 0.910484 0.020 Uiso 1 1 calc R U . . .
B28 B 0.143(6) 0.580(3) 0.734(3) 0.00(3) Uiso 1 1 d . . . . .
H28 H 0.224227 0.567445 0.732407 0.006 Uiso 1 1 calc R U . . .
B44 B -0.027(7) 0.641(4) 0.694(4) 0.04(3) Uiso 1 1 d . . . . .
H44 H -0.054632 0.670728 0.663680 0.050 Uiso 1 1 calc R U . . .
B49 B 0.066(7) 0.595(4) 0.681(4) 0.05(3) Uiso 1 1 d . . . . .
H49 H 0.097716 0.594169 0.642835 0.060 Uiso 1 1 calc R U . . .
B94 B 0.438(7) 0.194(4) 0.969(4) 0.05(3) Uiso 1 1 d . . . . .
H94 H 0.486388 0.181836 1.003369 0.055 Uiso 1 1 calc R U . . .
B22 B 0.307(8) 0.189(4) 0.964(4) 0.06(4) Uiso 1 1 d . . . . .
H22 H 0.267819 0.175682 0.997733 0.071 Uiso 1 1 calc R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au4 Au3 2.956(5) . ?
Au4 Au5 3.127(5) . ?
Au4 S00L 2.34(2) . ?
Au4 P00S 2.26(2) . ?
Au3 Au8 2.935(5) . ?
Au3 Au5 3.235(5) . ?
Au3 Au2 3.291(5) . ?
Au3 S00I 2.32(2) . ?
Au3 S00L 2.34(2) . ?
Au8 Au2 3.180(5) . ?
Au8 S00I 2.34(2) . ?
Au8 P00M 2.25(2) . ?
Au5 Au6 3.036(5) . ?
Au5 Au7 3.320(5) . ?
Au5 S00L 2.28(2) . ?
Au5 S00T 2.34(2) . ?
Au1 Au2 2.963(5) . ?
Au1 Au7 3.086(5) . ?
Au1 S00H 2.36(2) . ?
Au1 P00N 2.26(3) . ?
Au2 Au7 3.231(5) . ?
Au2 S00H 2.35(2) . ?
Au2 S00I 2.34(2) . ?
Au6 Au7 3.002(5) . ?
Au6 S00T 2.32(2) . ?
Au6 P00U 2.25(2) . ?
Au7 S00H 2.30(2) . ?
Au7 S00T 2.33(2) . ?
P00M C70 1.86(4) . ?
P00M C02O 1.90(4) . ?
P00M C17 1.85(7) . ?
P00N C018 1.87(4) . ?
P00N C046 1.68(4) . ?
P00N C029 1.90(8) . ?
P00S C02G 1.77(5) . ?
P00S C01T 1.75(4) . ?
P00S C025 1.87(8) . ?
P00U C25 1.81(4) . ?
P00U C14 1.82(4) . ?
P00U C19 1.86(7) . ?
C00Z H00Z 0.9500 . ?
C00Z C25 1.3900 . ?
C00Z C044 1.3900 . ?
C25 C03J 1.3900 . ?
C03J H03J 0.9500 . ?
C03J C021 1.3900 . ?
C021 H021 0.9500 . ?
C021 C69 1.3900 . ?
C69 H69 0.9500 . ?
C69 C044 1.3900 . ?
C044 H044 0.9500 . ?
B5 H5 1.1200 . ?
B5 C19 1.61(9) . ?
B5 B15 1.66(11) . ?
B5 C17 1.58(10) . ?
B5 B26 1.73(11) . ?
B5 B94 1.81(13) . ?
C014 H014 0.9500 . ?
C014 C03Y 1.3900 . ?
C014 C02G 1.3900 . ?
C03Y H03Y 0.9500 . ?
C03Y C27 1.3900 . ?
C27 H27 0.9500 . ?
C27 C03L 1.3900 . ?
C03L H03L 0.9500 . ?
C03L C039 1.3900 . ?
C039 H039 0.9500 . ?
C039 C02G 1.3900 . ?
C6 H6 0.9500 . ?
C6 C39 1.3900 . ?
C6 C1 1.3900 . ?
C39 H39 0.9500 . ?
C39 C13 1.3900 . ?
C13 H13 0.9500 . ?
C13 C16 1.3900 . ?
C16 H16 0.9500 . ?
C16 C14 1.3900 . ?
C14 C1 1.3900 . ?
C1 H1 0.9500 . ?
C018 C03P 1.3900 . ?
C018 C03E 1.3900 . ?
C03P H03P 0.9500 . ?
C03P C02A 1.3900 . ?
C02A H02A 0.9500 . ?
C02A C01G 1.3900 . ?
C01G H01G 0.9500 . ?
C01G C01A 1.3900 . ?
C01A H01A 0.9500 . ?
C01A C03E 1.3900 . ?
C03E H03E 0.9500 . ?
C01C H01C 0.9500 . ?
C01C C01N 1.3900 . ?
C01C C038 1.3900 . ?
C01N H01N 0.9500 . ?
C01N C01F 1.3900 . ?
C01F H01F 0.9500 . ?
C01F C01T 1.3900 . ?
C01T C026 1.3900 . ?
C026 H026 0.9500 . ?
C026 C038 1.3900 . ?
C038 H038 0.9500 . ?
C19 B02P 1.72(10) . ?
C19 B03R 1.65(10) . ?
C19 B15 1.70(10) . ?
C19 B26 1.78(10) . ?
C01Z H01Z 0.9500 . ?
C01Z C03M 1.3900 . ?
C01Z C02K 1.3900 . ?
C03M H03M 0.9500 . ?
C03M C03Q 1.3900 . ?
C03Q H03Q 0.9500 . ?
C03Q C70 1.3900 . ?
C70 C02D 1.3900 . ?
C02D H02D 0.9500 . ?
C02D C02K 1.3900 . ?
C02K H02K 0.9500 . ?
C025 B037 1.68(11) . ?
C025 B03B 1.63(10) . ?
C025 B03H 1.73(12) . ?
C025 B21 1.45(9) . ?
C025 B28 1.72(10) . ?
B027 H027 1.1200 . ?
B027 C029 1.89(12) . ?
B027 B03B 1.70(12) . ?
B027 B03H 1.96(14) . ?
B027 B03I 1.77(12) . ?
B027 B44 1.68(13) . ?
C02O C03X 1.3900 . ?
C02O C045 1.3900 . ?
C03X H03X 0.9500 . ?
C03X C03S 1.3900 . ?
C03S H03S 0.9500 . ?
C03S C03O 1.3900 . ?
C03O H03O 0.9500 . ?
C03O C03V 1.3900 . ?
C03V H03V 0.9500 . ?
C03V C045 1.3900 . ?
C045 H045 0.9500 . ?
C37 H37 0.9500 . ?
C37 C035 1.3900 . ?
C37 C66 1.3900 . ?
C035 H035 0.9500 . ?
C035 C046 1.3900 . ?
C046 C45 1.3900 . ?
C45 H45 0.9500 . ?
C45 C3 1.3900 . ?
C3 H3 0.9500 . ?
C3 C66 1.3900 . ?
C66 H66 0.9500 . ?
C029 B037 1.61(10) . ?
C029 B03H 1.80(12) . ?
C029 B03I 1.67(9) . ?
C029 B18 1.58(10) . ?
B02P H02P 1.1200 . ?
B02P B1 1.73(12) . ?
B02P B03A 1.87(12) . ?
B02P B03R 1.67(11) . ?
B02P B15 1.66(11) . ?
B037 H037 1.1200 . ?
B037 B03H 1.64(12) . ?
B037 B18 1.76(11) . ?
B037 B28 1.82(11) . ?
B1 H1A 1.1200 . ?
B1 B03A 1.80(14) . ?
B1 B15 1.58(13) . ?
B1 C17 1.67(12) . ?
B1 B22 1.74(14) . ?
B03A H03A 1.1200 . ?
B03A B7 1.75(12) . ?
B03A B03R 1.82(13) . ?
B03A B22 1.69(12) . ?
B03B H03B 1.1200 . ?
B03B B03H 1.74(12) . ?
B03B B21 1.64(11) . ?
B03B B44 1.71(12) . ?
B7 H7 1.1200 . ?
B7 B03R 1.87(12) . ?
B7 B26 1.97(12) . ?
B7 B94 1.80(12) . ?
B7 B22 1.73(13) . ?
B03H H03H 1.1200 . ?
B03I H03I 1.1200 . ?
B03I B18 1.78(11) . ?
B03I B44 1.70(11) . ?
B03I B49 1.86(13) . ?
B03R H03R 1.1200 . ?
B03R B26 2.01(13) . ?
B15 H15 1.1200 . ?
B15 C17 1.71(10) . ?
C17 B94 1.79(11) . ?
C17 B22 1.68(12) . ?
B18 H18 1.1200 . ?
B18 B28 1.76(11) . ?
B18 B49 1.76(12) . ?
B21 H21 1.1200 . ?
B21 B28 1.67(11) . ?
B21 B44 1.76(12) . ?
B21 B49 1.71(12) . ?
B26 H26 1.1200 . ?
B26 B94 1.70(12) . ?
B28 H28 1.1200 . ?
B28 B49 1.75(12) . ?
B44 H44 1.1200 . ?
B44 B49 1.69(13) . ?
B49 H49 1.1200 . ?
B94 H94 1.1200 . ?
B94 B22 1.74(13) . ?
B22 H22 1.1200 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Au3 Au4 Au5 64.18(11) . . ?
S00L Au4 Au3 50.7(5) . . ?
S00L Au4 Au5 46.6(6) . . ?
P00S Au4 Au3 124.6(6) . . ?
P00S Au4 Au5 137.3(5) . . ?
P00S Au4 S00L 173.9(8) . . ?
Au4 Au3 Au5 60.48(11) . . ?
Au4 Au3 Au2 122.07(14) . . ?
Au8 Au3 Au4 176.79(16) . . ?
Au8 Au3 Au5 120.90(14) . . ?
Au8 Au3 Au2 61.11(11) . . ?
Au5 Au3 Au2 90.73(12) . . ?
S00I Au3 Au4 130.3(5) . . ?
S00I Au3 Au8 51.2(5) . . ?
S00I Au3 Au5 135.4(5) . . ?
S00I Au3 Au2 45.2(5) . . ?
S00I Au3 S00L 178.8(8) . . ?
S00L Au3 Au4 50.9(5) . . ?
S00L Au3 Au8 127.6(6) . . ?
S00L Au3 Au5 44.8(6) . . ?
S00L Au3 Au2 134.7(6) . . ?
Au3 Au8 Au2 64.98(11) . . ?
S00I Au8 Au3 50.7(5) . . ?
S00I Au8 Au2 47.1(5) . . ?
P00M Au8 Au3 126.6(6) . . ?
P00M Au8 Au2 134.1(6) . . ?
P00M Au8 S00I 177.0(8) . . ?
Au4 Au5 Au3 55.34(10) . . ?
Au4 Au5 Au7 117.60(13) . . ?
Au3 Au5 Au7 89.17(12) . . ?
Au6 Au5 Au4 169.96(15) . . ?
Au6 Au5 Au3 115.08(13) . . ?
Au6 Au5 Au7 56.15(11) . . ?
S00L Au5 Au4 48.2(6) . . ?
S00L Au5 Au3 46.2(5) . . ?
S00L Au5 Au6 128.9(6) . . ?
S00L Au5 Au7 134.9(6) . . ?
S00L Au5 S00T 177.9(8) . . ?
S00T Au5 Au4 133.7(6) . . ?
S00T Au5 Au3 133.5(6) . . ?
S00T Au5 Au6 49.0(5) . . ?
S00T Au5 Au7 44.6(5) . . ?
Au2 Au1 Au7 64.54(12) . . ?
S00H Au1 Au2 51.0(5) . . ?
S00H Au1 Au7 47.7(5) . . ?
P00N Au1 Au2 124.8(6) . . ?
P00N Au1 Au7 137.9(7) . . ?
P00N Au1 S00H 173.0(8) . . ?
Au8 Au2 Au3 53.90(10) . . ?
Au8 Au2 Au7 119.36(13) . . ?
Au1 Au2 Au3 115.71(14) . . ?
Au1 Au2 Au8 169.25(15) . . ?
Au1 Au2 Au7 59.57(11) . . ?
Au7 Au2 Au3 89.75(12) . . ?
S00H Au2 Au3 135.0(5) . . ?
S00H Au2 Au8 137.1(5) . . ?
S00H Au2 Au1 51.1(5) . . ?
S00H Au2 Au7 45.4(5) . . ?
S00I Au2 Au3 44.9(5) . . ?
S00I Au2 Au8 47.2(5) . . ?
S00I Au2 Au1 124.6(5) . . ?
S00I Au2 Au7 133.7(5) . . ?
S00I Au2 S00H 175.7(7) . . ?
Au7 Au6 Au5 66.72(11) . . ?
S00T Au6 Au5 49.6(6) . . ?
S00T Au6 Au7 49.9(6) . . ?
P00U Au6 Au5 131.9(6) . . ?
P00U Au6 Au7 134.3(6) . . ?
P00U Au6 S00T 175.3(8) . . ?
Au1 Au7 Au5 116.58(13) . . ?
Au1 Au7 Au2 55.90(10) . . ?
Au2 Au7 Au5 90.27(12) . . ?
Au6 Au7 Au5 57.13(11) . . ?
Au6 Au7 Au1 169.66(16) . . ?
Au6 Au7 Au2 114.35(14) . . ?
S00H Au7 Au5 136.6(6) . . ?
S00H Au7 Au1 49.3(5) . . ?
S00H Au7 Au2 46.7(5) . . ?
S00H Au7 Au6 128.1(5) . . ?
S00H Au7 S00T 177.1(8) . . ?
S00T Au7 Au5 44.7(5) . . ?
S00T Au7 Au1 133.3(6) . . ?
S00T Au7 Au2 134.9(6) . . ?
S00T Au7 Au6 49.6(6) . . ?
Au2 S00H Au1 77.9(6) . . ?
Au7 S00H Au1 82.9(7) . . ?
Au7 S00H Au2 87.9(7) . . ?
Au3 S00I Au8 78.1(6) . . ?
Au3 S00I Au2 89.9(7) . . ?
Au2 S00I Au8 85.8(7) . . ?
Au3 S00L Au4 78.4(7) . . ?
Au5 S00L Au4 85.2(7) . . ?
Au5 S00L Au3 89.0(8) . . ?
Au6 S00T Au5 81.4(7) . . ?
Au6 S00T Au7 80.4(7) . . ?
Au7 S00T Au5 90.7(8) . . ?
C70 P00M Au8 112(2) . . ?
C70 P00M C02O 111(2) . . ?
C02O P00M Au8 112.3(19) . . ?
C17 P00M Au8 110(2) . . ?
C17 P00M C70 110(3) . . ?
C17 P00M C02O 101(3) . . ?
C018 P00N Au1 107(2) . . ?
C018 P00N C029 111(3) . . ?
C046 P00N Au1 116(2) . . ?
C046 P00N C018 111(3) . . ?
C046 P00N C029 103(3) . . ?
C029 P00N Au1 109(2) . . ?
C02G P00S Au4 114(2) . . ?
C02G P00S C025 105(3) . . ?
C01T P00S Au4 109.6(19) . . ?
C01T P00S C02G 107(3) . . ?
C01T P00S C025 108(3) . . ?
C025 P00S Au4 113(2) . . ?
C25 P00U Au6 111(2) . . ?
C25 P00U C14 115(3) . . ?
C25 P00U C19 103(3) . . ?
C14 P00U Au6 112(2) . . ?
C14 P00U C19 103(3) . . ?
C19 P00U Au6 112(2) . . ?
C25 C00Z H00Z 120.0 . . ?
C25 C00Z C044 120.0 . . ?
C044 C00Z H00Z 120.0 . . ?
C00Z C25 P00U 120(3) . . ?
C03J C25 P00U 120(3) . . ?
C03J C25 C00Z 120.0 . . ?
C25 C03J H03J 120.0 . . ?
C25 C03J C021 120.0 . . ?
C021 C03J H03J 120.0 . . ?
C03J C021 H021 120.0 . . ?
C03J C021 C69 120.0 . . ?
C69 C021 H021 120.0 . . ?
C021 C69 H69 120.0 . . ?
C044 C69 C021 120.0 . . ?
C044 C69 H69 120.0 . . ?
C00Z C044 H044 120.0 . . ?
C69 C044 C00Z 120.0 . . ?
C69 C044 H044 120.0 . . ?
C19 B5 H5 120.3 . . ?
C19 B5 B15 62(5) . . ?
C19 B5 B26 64(4) . . ?
C19 B5 B94 108(6) . . ?
B15 B5 H5 115.6 . . ?
B15 B5 B26 118(7) . . ?
B15 B5 B94 114(7) . . ?
C17 B5 H5 118.0 . . ?
C17 B5 C19 112(6) . . ?
C17 B5 B15 64(5) . . ?
C17 B5 B26 113(6) . . ?
C17 B5 B94 63(5) . . ?
B26 B5 H5 117.9 . . ?
B26 B5 B94 57(5) . . ?
B94 B5 H5 122.1 . . ?
C03Y C014 H014 120.0 . . ?
C03Y C014 C02G 120.0 . . ?
C02G C014 H014 120.0 . . ?
C014 C03Y H03Y 120.0 . . ?
C014 C03Y C27 120.00(6) . . ?
C27 C03Y H03Y 120.0 . . ?
C03Y C27 H27 120.0 . . ?
C03Y C27 C03L 120.00(7) . . ?
C03L C27 H27 120.0 . . ?
C27 C03L H03L 120.0 . . ?
C039 C03L C27 120.0 . . ?
C039 C03L H03L 120.0 . . ?
C03L C039 H039 120.0 . . ?
C03L C039 C02G 120.00(6) . . ?
C02G C039 H039 120.0 . . ?
C014 C02G P00S 112(4) . . ?
C039 C02G P00S 127(4) . . ?
C039 C02G C014 120.00(7) . . ?
C39 C6 H6 120.0 . . ?
C39 C6 C1 120.0 . . ?
C1 C6 H6 120.0 . . ?
C6 C39 H39 120.0 . . ?
C13 C39 C6 120.0 . . ?
C13 C39 H39 120.0 . . ?
C39 C13 H13 120.0 . . ?
C39 C13 C16 120.0 . . ?
C16 C13 H13 120.0 . . ?
C13 C16 H16 120.0 . . ?
C14 C16 C13 120.0 . . ?
C14 C16 H16 120.0 . . ?
C16 C14 P00U 113(4) . . ?
C16 C14 C1 120.00(5) . . ?
C1 C14 P00U 127(4) . . ?
C6 C1 H1 120.0 . . ?
C14 C1 C6 120.0 . . ?
C14 C1 H1 120.0 . . ?
C03P C018 P00N 129(3) . . ?
C03P C018 C03E 120.0 . . ?
C03E C018 P00N 111(3) . . ?
C018 C03P H03P 120.0 . . ?
C02A C03P C018 120.0 . . ?
C02A C03P H03P 120.0 . . ?
C03P C02A H02A 120.0 . . ?
C03P C02A C01G 120.0 . . ?
C01G C02A H02A 120.0 . . ?
C02A C01G H01G 120.0 . . ?
C01A C01G C02A 120.0 . . ?
C01A C01G H01G 120.0 . . ?
C01G C01A H01A 120.0 . . ?
C01G C01A C03E 120.0 . . ?
C03E C01A H01A 120.0 . . ?
C018 C03E H03E 120.0 . . ?
C01A C03E C018 120.0 . . ?
C01A C03E H03E 120.0 . . ?
C01N C01C H01C 120.0 . . ?
C01N C01C C038 120.0 . . ?
C038 C01C H01C 120.0 . . ?
C01C C01N H01N 120.0 . . ?
C01C C01N C01F 120.0 . . ?
C01F C01N H01N 120.0 . . ?
C01N C01F H01F 120.0 . . ?
C01N C01F C01T 120.0 . . ?
C01T C01F H01F 120.0 . . ?
C01F C01T P00S 117(3) . . ?
C026 C01T P00S 123(3) . . ?
C026 C01T C01F 120.0 . . ?
C01T C026 H026 120.0 . . ?
C01T C026 C038 120.0 . . ?
C038 C026 H026 120.0 . . ?
C01C C038 H038 120.0 . . ?
C026 C038 C01C 120.0 . . ?
C026 C038 H038 120.0 . . ?
B5 C19 P00U 122(5) . . ?
B5 C19 B02P 109(5) . . ?
B5 C19 B03R 115(6) . . ?
B5 C19 B15 60(4) . . ?
B5 C19 B26 61(4) . . ?
B02P C19 P00U 115(4) . . ?
B02P C19 B26 119(5) . . ?
B03R C19 P00U 119(5) . . ?
B03R C19 B02P 59(4) . . ?
B03R C19 B15 108(6) . . ?
B03R C19 B26 72(5) . . ?
B15 C19 P00U 118(5) . . ?
B15 C19 B02P 58(4) . . ?
B15 C19 B26 113(5) . . ?
B26 C19 P00U 119(4) . . ?
C03M C01Z H01Z 120.0 . . ?
C03M C01Z C02K 120.0 . . ?
C02K C01Z H01Z 120.0 . . ?
C01Z C03M H03M 120.0 . . ?
C01Z C03M C03Q 120.0 . . ?
C03Q C03M H03M 120.0 . . ?
C03M C03Q H03Q 120.0 . . ?
C70 C03Q C03M 120.0 . . ?
C70 C03Q H03Q 120.0 . . ?
C03Q C70 P00M 125(3) . . ?
C03Q C70 C02D 120.0 . . ?
C02D C70 P00M 115(3) . . ?
C70 C02D H02D 120.0 . . ?
C02K C02D C70 120.0 . . ?
C02K C02D H02D 120.0 . . ?
C01Z C02K H02K 120.0 . . ?
C02D C02K C01Z 120.0 . . ?
C02D C02K H02K 120.0 . . ?
B037 C025 P00S 111(5) . . ?
B037 C025 B03H 57(5) . . ?
B037 C025 B28 65(5) . . ?
B03B C025 P00S 128(5) . . ?
B03B C025 B037 107(6) . . ?
B03B C025 B03H 62(5) . . ?
B03B C025 B28 115(6) . . ?
B03H C025 P00S 113(5) . . ?
B21 C025 P00S 126(6) . . ?
B21 C025 B037 113(7) . . ?
B21 C025 B03B 64(5) . . ?
B21 C025 B03H 117(7) . . ?
B21 C025 B28 63(5) . . ?
B28 C025 P00S 112(5) . . ?
B28 C025 B03H 116(6) . . ?
C029 B027 H027 131.3 . . ?
C029 B027 B03H 56(4) . . ?
B03B B027 H027 124.9 . . ?
B03B B027 C029 96(6) . . ?
B03B B027 B03H 56(5) . . ?
B03B B027 B03I 106(7) . . ?
B03H B027 H027 124.5 . . ?
B03I B027 H027 123.1 . . ?
B03I B027 C029 54(4) . . ?
B03I B027 B03H 103(6) . . ?
B44 B027 H027 124.5 . . ?
B44 B027 C029 97(6) . . ?
B44 B027 B03B 61(5) . . ?
B44 B027 B03H 104(7) . . ?
B44 B027 B03I 59(5) . . ?
C03X C02O P00M 123(3) . . ?
C03X C02O C045 120.00(6) . . ?
C045 C02O P00M 117(3) . . ?
C02O C03X H03X 120.0 . . ?
C03S C03X C02O 120.0 . . ?
C03S C03X H03X 120.0 . . ?
C03X C03S H03S 120.0 . . ?
C03O C03S C03X 120.0 . . ?
C03O C03S H03S 120.0 . . ?
C03S C03O H03O 120.0 . . ?
C03S C03O C03V 120.00(6) . . ?
C03V C03O H03O 120.0 . . ?
C03O C03V H03V 120.0 . . ?
C03O C03V C045 120.0 . . ?
C045 C03V H03V 120.0 . . ?
C02O C045 H045 120.0 . . ?
C03V C045 C02O 120.0 . . ?
C03V C045 H045 120.0 . . ?
C035 C37 H37 120.0 . . ?
C035 C37 C66 120.0 . . ?
C66 C37 H37 120.0 . . ?
C37 C035 H035 120.0 . . ?
C37 C035 C046 120.0 . . ?
C046 C035 H035 120.0 . . ?
C035 C046 P00N 129(4) . . ?
C035 C046 C45 120.0 . . ?
C45 C046 P00N 111(4) . . ?
C046 C45 H45 120.0 . . ?
C3 C45 C046 120.0 . . ?
C3 C45 H45 120.0 . . ?
C45 C3 H3 120.0 . . ?
C45 C3 C66 120.0 . . ?
C66 C3 H3 120.0 . . ?
C37 C66 H66 120.0 . . ?
C3 C66 C37 120.0 . . ?
C3 C66 H66 120.0 . . ?
B027 C029 P00N 117(5) . . ?
B037 C029 P00N 118(5) . . ?
B037 C029 B027 111(6) . . ?
B037 C029 B03H 57(5) . . ?
B037 C029 B03I 119(6) . . ?
B03H C029 P00N 116(5) . . ?
B03H C029 B027 64(5) . . ?
B03I C029 P00N 117(5) . . ?
B03I C029 B027 59(4) . . ?
B03I C029 B03H 115(6) . . ?
B18 C029 P00N 120(5) . . ?
B18 C029 B027 113(6) . . ?
B18 C029 B037 67(5) . . ?
B18 C029 B03H 114(6) . . ?
B18 C029 B03I 66(5) . . ?
C19 B02P H02P 125.0 . . ?
C19 B02P B1 102(6) . . ?
C19 B02P B03A 105(5) . . ?
B1 B02P H02P 124.6 . . ?
B1 B02P B03A 60(5) . . ?
B03A B02P H02P 122.4 . . ?
B03R B02P C19 58(4) . . ?
B03R B02P H02P 120.2 . . ?
B03R B02P B1 108(7) . . ?
B03R B02P B03A 62(5) . . ?
B15 B02P C19 60(4) . . ?
B15 B02P H02P 122.9 . . ?
B15 B02P B1 56(5) . . ?
B15 B02P B03A 105(6) . . ?
B15 B02P B03R 109(6) . . ?
C025 B037 H037 124.1 . . ?
C025 B037 B18 103(6) . . ?
C025 B037 B28 59(4) . . ?
C029 B037 C025 108(6) . . ?
C029 B037 H037 122.2 . . ?
C029 B037 B03H 67(5) . . ?
C029 B037 B18 56(4) . . ?
C029 B037 B28 106(6) . . ?
B03H B037 C025 63(5) . . ?
B03H B037 H037 113.5 . . ?
B03H B037 B18 114(7) . . ?
B03H B037 B28 114(6) . . ?
B18 B037 H037 124.0 . . ?
B18 B037 B28 59(4) . . ?
B28 B037 H037 121.7 . . ?
B02P B1 H1A 120.4 . . ?
B02P B1 B03A 64(5) . . ?
B02P B1 B22 108(8) . . ?
B03A B1 H1A 121.0 . . ?
B15 B1 B02P 60(5) . . ?
B15 B1 H1A 118.7 . . ?
B15 B1 B03A 112(8) . . ?
B15 B1 C17 63(6) . . ?
B15 B1 B22 110(8) . . ?
C17 B1 B02P 110(7) . . ?
C17 B1 H1A 121.5 . . ?
C17 B1 B03A 107(7) . . ?
C17 B1 B22 59(5) . . ?
B22 B1 H1A 123.6 . . ?
B22 B1 B03A 57(5) . . ?
B02P B03A H03A 125.5 . . ?
B1 B03A B02P 56(5) . . ?
B1 B03A H03A 125.0 . . ?
B1 B03A B03R 99(7) . . ?
B7 B03A B02P 107(6) . . ?
B7 B03A B1 108(7) . . ?
B7 B03A H03A 119.0 . . ?
B7 B03A B03R 63(5) . . ?
B03R B03A B02P 54(4) . . ?
B03R B03A H03A 126.0 . . ?
B22 B03A B02P 104(7) . . ?
B22 B03A B1 60(5) . . ?
B22 B03A H03A 122.7 . . ?
B22 B03A B7 60(5) . . ?
B22 B03A B03R 105(7) . . ?
C025 B03B B027 116(7) . . ?
C025 B03B H03B 123.3 . . ?
C025 B03B B03H 62(5) . . ?
C025 B03B B21 52(4) . . ?
C025 B03B B44 106(6) . . ?
B027 B03B H03B 114.2 . . ?
B027 B03B B03H 70(6) . . ?
B027 B03B B44 59(5) . . ?
B03H B03B H03B 117.3 . . ?
B21 B03B B027 113(7) . . ?
B21 B03B H03B 123.8 . . ?
B21 B03B B03H 106(7) . . ?
B21 B03B B44 63(5) . . ?
B44 B03B H03B 121.3 . . ?
B44 B03B B03H 113(7) . . ?
B03A B7 H7 119.3 . . ?
B03A B7 B03R 60(5) . . ?
B03A B7 B26 111(6) . . ?
B03A B7 B94 108(7) . . ?
B03R B7 H7 123.2 . . ?
B03R B7 B26 63(5) . . ?
B26 B7 H7 123.1 . . ?
B94 B7 H7 124.4 . . ?
B94 B7 B03R 104(6) . . ?
B94 B7 B26 53(4) . . ?
B22 B7 B03A 58(5) . . ?
B22 B7 H7 127.1 . . ?
B22 B7 B03R 101(7) . . ?
B22 B7 B26 101(6) . . ?
B22 B7 B94 59(5) . . ?
C025 B03H B027 100(6) . . ?
C025 B03H C029 98(6) . . ?
C025 B03H B03B 56(5) . . ?
C025 B03H H03H 127.2 . . ?
B027 B03H H03H 124.3 . . ?
C029 B03H B027 60(5) . . ?
C029 B03H H03H 128.0 . . ?
B037 B03H C025 60(5) . . ?
B037 B03H B027 106(7) . . ?
B037 B03H C029 56(5) . . ?
B037 B03H B03B 104(7) . . ?
B037 B03H H03H 122.0 . . ?
B03B B03H B027 54(5) . . ?
B03B B03H C029 98(6) . . ?
B03B B03H H03H 127.2 . . ?
B027 B03I H03I 118.6 . . ?
B027 B03I B18 110(6) . . ?
B027 B03I B49 105(6) . . ?
C029 B03I B027 66(5) . . ?
C029 B03I H03I 124.2 . . ?
C029 B03I B18 54(4) . . ?
C029 B03I B44 104(6) . . ?
C029 B03I B49 100(5) . . ?
B18 B03I H03I 124.2 . . ?
B18 B03I B49 58(5) . . ?
B44 B03I B027 58(5) . . ?
B44 B03I H03I 125.7 . . ?
B44 B03I B18 102(6) . . ?
B44 B03I B49 57(5) . . ?
B49 B03I H03I 126.3 . . ?
C19 B03R B02P 62(5) . . ?
C19 B03R B03A 110(6) . . ?
C19 B03R B7 106(6) . . ?
C19 B03R H03R 122.2 . . ?
C19 B03R B26 57(4) . . ?
B02P B03R B03A 65(5) . . ?
B02P B03R B7 111(6) . . ?
B02P B03R H03R 117.5 . . ?
B02P B03R B26 110(6) . . ?
B03A B03R B7 57(5) . . ?
B03A B03R H03R 121.6 . . ?
B03A B03R B26 106(6) . . ?
B7 B03R H03R 122.7 . . ?
B7 B03R B26 61(4) . . ?
B26 B03R H03R 122.8 . . ?
B5 B15 C19 57(4) . . ?
B5 B15 B02P 110(7) . . ?
B5 B15 H15 123.9 . . ?
B5 B15 C17 56(4) . . ?
C19 B15 H15 123.7 . . ?
C19 B15 C17 102(6) . . ?
B02P B15 C19 62(4) . . ?
B02P B15 H15 117.5 . . ?
B02P B15 C17 111(6) . . ?
B1 B15 B5 107(8) . . ?
B1 B15 C19 110(7) . . ?
B1 B15 B02P 64(6) . . ?
B1 B15 H15 119.2 . . ?
B1 B15 C17 61(5) . . ?
C17 B15 H15 124.0 . . ?
B5 C17 P00M 125(5) . . ?
B5 C17 B1 107(6) . . ?
B5 C17 B15 60(5) . . ?
B5 C17 B94 65(5) . . ?
B5 C17 B22 110(6) . . ?
B1 C17 P00M 112(5) . . ?
B1 C17 B15 56(5) . . ?
B1 C17 B94 112(6) . . ?
B1 C17 B22 63(5) . . ?
B15 C17 P00M 115(5) . . ?
B15 C17 B94 113(6) . . ?
B94 C17 P00M 128(5) . . ?
B22 C17 P00M 122(5) . . ?
B22 C17 B15 107(6) . . ?
B22 C17 B94 60(5) . . ?
C029 B18 B037 57(4) . . ?
C029 B18 B03I 59(4) . . ?
C029 B18 H18 122.6 . . ?
C029 B18 B28 110(6) . . ?
C029 B18 B49 108(7) . . ?
B037 B18 B03I 107(6) . . ?
B037 B18 H18 123.3 . . ?
B037 B18 B28 62(5) . . ?
B037 B18 B49 107(6) . . ?
B03I B18 H18 119.8 . . ?
B28 B18 B03I 113(6) . . ?
B28 B18 H18 118.7 . . ?
B49 B18 B03I 63(5) . . ?
B49 B18 H18 121.3 . . ?
B49 B18 B28 60(5) . . ?
C025 B21 B03B 63(5) . . ?
C025 B21 H21 116.1 . . ?
C025 B21 B28 67(5) . . ?
C025 B21 B44 112(7) . . ?
C025 B21 B49 115(7) . . ?
B03B B21 H21 118.5 . . ?
B03B B21 B28 117(7) . . ?
B03B B21 B44 60(5) . . ?
B03B B21 B49 110(7) . . ?
B28 B21 H21 115.7 . . ?
B28 B21 B44 111(6) . . ?
B28 B21 B49 62(5) . . ?
B44 B21 H21 122.6 . . ?
B49 B21 H21 120.7 . . ?
B49 B21 B44 58(5) . . ?
B5 B26 C19 55(4) . . ?
B5 B26 B7 102(6) . . ?
B5 B26 B03R 94(6) . . ?
B5 B26 H26 126.0 . . ?
C19 B26 B7 98(5) . . ?
C19 B26 B03R 51(4) . . ?
C19 B26 H26 127.7 . . ?
B7 B26 B03R 56(4) . . ?
B7 B26 H26 126.3 . . ?
B03R B26 H26 130.2 . . ?
B94 B26 B5 64(5) . . ?
B94 B26 C19 106(6) . . ?
B94 B26 B7 58(5) . . ?
B94 B26 B03R 102(6) . . ?
B94 B26 H26 120.4 . . ?
C025 B28 B037 57(4) . . ?
C025 B28 B18 102(6) . . ?
C025 B28 H28 128.2 . . ?
C025 B28 B49 101(6) . . ?
B037 B28 H28 125.8 . . ?
B18 B28 B037 59(4) . . ?
B18 B28 H28 123.2 . . ?
B21 B28 C025 51(4) . . ?
B21 B28 B037 97(6) . . ?
B21 B28 B18 103(6) . . ?
B21 B28 H28 128.1 . . ?
B21 B28 B49 60(5) . . ?
B49 B28 B037 105(6) . . ?
B49 B28 B18 60(5) . . ?
B49 B28 H28 122.5 . . ?
B027 B44 B03B 60(5) . . ?
B027 B44 B03I 63(5) . . ?
B027 B44 B21 108(7) . . ?
B027 B44 H44 117.9 . . ?
B027 B44 B49 118(8) . . ?
B03B B44 B21 56(5) . . ?
B03B B44 H44 124.5 . . ?
B03I B44 B03B 108(7) . . ?
B03I B44 B21 110(7) . . ?
B03I B44 H44 118.4 . . ?
B21 B44 H44 124.3 . . ?
B49 B44 B03B 108(7) . . ?
B49 B44 B03I 66(5) . . ?
B49 B44 B21 59(5) . . ?
B49 B44 H44 116.9 . . ?
B03I B49 H49 122.8 . . ?
B18 B49 B03I 59(5) . . ?
B18 B49 H49 125.5 . . ?
B21 B49 B03I 105(6) . . ?
B21 B49 B18 101(7) . . ?
B21 B49 B28 58(5) . . ?
B21 B49 H49 124.8 . . ?
B28 B49 B03I 110(6) . . ?
B28 B49 B18 60(5) . . ?
B28 B49 H49 119.7 . . ?
B44 B49 B03I 57(5) . . ?
B44 B49 B18 104(7) . . ?
B44 B49 B21 62(5) . . ?
B44 B49 B28 111(7) . . ?
B44 B49 H49 121.5 . . ?
B5 B94 H94 128.9 . . ?
B7 B94 B5 106(6) . . ?
B7 B94 H94 119.9 . . ?
C17 B94 B5 52(4) . . ?
C17 B94 B7 104(6) . . ?
C17 B94 H94 127.1 . . ?
B26 B94 B5 59(5) . . ?
B26 B94 B7 68(5) . . ?
B26 B94 C17 105(6) . . ?
B26 B94 H94 117.2 . . ?
B26 B94 B22 112(7) . . ?
B22 B94 B5 97(7) . . ?
B22 B94 B7 58(5) . . ?
B22 B94 C17 57(5) . . ?
B22 B94 H94 124.8 . . ?
B1 B22 H22 120.5 . . ?
B03A B22 B1 63(6) . . ?
B03A B22 B7 62(5) . . ?
B03A B22 B94 114(7) . . ?
B03A B22 H22 118.1 . . ?
B7 B22 B1 112(7) . . ?
B7 B22 B94 63(5) . . ?
B7 B22 H22 119.1 . . ?
C17 B22 B1 59(5) . . ?
C17 B22 B03A 112(7) . . ?
C17 B22 B7 113(7) . . ?
C17 B22 B94 63(5) . . ?
C17 B22 H22 120.0 . . ?
B94 B22 B1 111(8) . . ?
B94 B22 H22 118.0 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Au4 P00S C02G C014 -20(3) . . . . ?
Au4 P00S C02G C039 169(2) . . . . ?
Au4 P00S C01T C01F -35(3) . . . . ?
Au4 P00S C01T C026 139(2) . . . . ?
Au4 P00S C025 B037 37(5) . . . . ?
Au4 P00S C025 B03B 172(6) . . . . ?
Au4 P00S C025 B03H 100(5) . . . . ?
Au4 P00S C025 B21 -105(6) . . . . ?
Au4 P00S C025 B28 -33(5) . . . . ?
Au8 P00M C70 C03Q 166(2) . . . . ?
Au8 P00M C70 C02D -17(3) . . . . ?
Au8 P00M C02O C03X 168(2) . . . . ?
Au8 P00M C02O C045 -19(3) . . . . ?
Au8 P00M C17 B5 101(6) . . . . ?
Au8 P00M C17 B1 -30(6) . . . . ?
Au8 P00M C17 B15 31(5) . . . . ?
Au8 P00M C17 B94 -176(5) . . . . ?
Au8 P00M C17 B22 -101(6) . . . . ?
Au1 P00N C018 C03P -136(3) . . . . ?
Au1 P00N C018 C03E 44(3) . . . . ?
Au1 P00N C046 C035 163(3) . . . . ?
Au1 P00N C046 C45 -22(3) . . . . ?
Au6 P00U C25 C00Z -12(3) . . . . ?
Au6 P00U C25 C03J 170(2) . . . . ?
Au6 P00U C14 C16 37(3) . . . . ?
Au6 P00U C14 C1 -136(3) . . . . ?
Au6 P00U C19 B5 -96(5) . . . . ?
Au6 P00U C19 B02P 40(5) . . . . ?
Au6 P00U C19 B03R 107(5) . . . . ?
Au6 P00U C19 B15 -26(5) . . . . ?
Au6 P00U C19 B26 -169(4) . . . . ?
P00M C70 C02D C02K -177(3) . . . . ?
P00M C02O C03X C03S 173(3) . . . . ?
P00M C02O C045 C03V -173(3) . . . . ?
P00M C17 B94 B5 -116(7) . . . . ?
P00M C17 B94 B7 145(5) . . . . ?
P00M C17 B94 B26 -144(6) . . . . ?
P00M C17 B94 B22 110(7) . . . . ?
P00M C17 B22 B1 100(7) . . . . ?
P00M C17 B22 B03A 135(6) . . . . ?
P00M C17 B22 B7 -157(5) . . . . ?
P00M C17 B22 B94 -118(6) . . . . ?
P00N C018 C03P C02A -180(4) . . . . ?
P00N C018 C03E C01A 180(3) . . . . ?
P00N C046 C45 C3 -176(3) . . . . ?
P00N C029 B037 C025 -153(5) . . . . ?
P00N C029 B037 B03H -104(6) . . . . ?
P00N C029 B037 B18 113(6) . . . . ?
P00N C029 B037 B28 146(5) . . . . ?
P00N C029 B03H C025 154(5) . . . . ?
P00N C029 B03H B027 -110(6) . . . . ?
P00N C029 B03H B037 108(6) . . . . ?
P00N C029 B03H B03B -150(5) . . . . ?
P00N C029 B03I B027 107(6) . . . . ?
P00N C029 B03I B18 -113(6) . . . . ?
P00N C029 B03I B44 152(5) . . . . ?
P00N C029 B03I B49 -150(5) . . . . ?
P00N C029 B18 B037 -110(6) . . . . ?
P00N C029 B18 B03I 109(6) . . . . ?
P00N C029 B18 B28 -146(5) . . . . ?
P00N C029 B18 B49 151(5) . . . . ?
P00S C01T C026 C038 -173(3) . . . . ?
P00S C025 B037 C029 157(5) . . . . ?
P00S C025 B037 B03H 105(6) . . . . ?
P00S C025 B037 B18 -145(5) . . . . ?
P00S C025 B037 B28 -106(5) . . . . ?
P00S C025 B03B B027 -144(6) . . . . ?
P00S C025 B03B B03H -99(7) . . . . ?
P00S C025 B03B B21 116(8) . . . . ?
P00S C025 B03B B44 153(6) . . . . ?
P00S C025 B03H B027 156(5) . . . . ?
P00S C025 B03H C029 -143(5) . . . . ?
P00S C025 B03H B037 -101(6) . . . . ?
P00S C025 B03H B03B 122(6) . . . . ?
P00S C025 B21 B03B -120(7) . . . . ?
P00S C025 B21 B28 99(7) . . . . ?
P00S C025 B21 B44 -157(6) . . . . ?
P00S C025 B21 B49 139(6) . . . . ?
P00S C025 B28 B037 104(6) . . . . ?
P00S C025 B28 B18 143(5) . . . . ?
P00S C025 B28 B21 -120(6) . . . . ?
P00S C025 B28 B49 -156(5) . . . . ?
P00U C25 C03J C021 178(3) . . . . ?
P00U C14 C1 C6 173(4) . . . . ?
P00U C19 B02P B1 -146(5) . . . . ?
P00U C19 B02P B03A 152(4) . . . . ?
P00U C19 B02P B03R 110(6) . . . . ?
P00U C19 B02P B15 -108(5) . . . . ?
P00U C19 B03R B02P -104(5) . . . . ?
P00U C19 B03R B03A -149(5) . . . . ?
P00U C19 B03R B7 151(5) . . . . ?
P00U C19 B03R B26 114(5) . . . . ?
P00U C19 B15 B5 -113(6) . . . . ?
P00U C19 B15 B02P 104(5) . . . . ?
P00U C19 B15 B1 148(6) . . . . ?
P00U C19 B15 C17 -148(5) . . . . ?
P00U C19 B26 B5 113(6) . . . . ?
P00U C19 B26 B7 -147(4) . . . . ?
P00U C19 B26 B03R -113(6) . . . . ?
P00U C19 B26 B94 154(5) . . . . ?
C00Z C25 C03J C021 0.0 . . . . ?
C25 P00U C14 C16 165(3) . . . . ?
C25 P00U C14 C1 -8(4) . . . . ?
C25 P00U C19 B5 144(5) . . . . ?
C25 P00U C19 B02P -80(5) . . . . ?
C25 P00U C19 B03R -13(6) . . . . ?
C25 P00U C19 B15 -146(5) . . . . ?
C25 P00U C19 B26 71(5) . . . . ?
C25 C00Z C044 C69 0.0 . . . . ?
C25 C03J C021 C69 0.0 . . . . ?
C03J C021 C69 C044 0.0 . . . . ?
C021 C69 C044 C00Z 0.0 . . . . ?
C044 C00Z C25 P00U -178(3) . . . . ?
C044 C00Z C25 C03J 0.0 . . . . ?
B5 C19 B02P B1 -4(7) . . . . ?
B5 C19 B02P B03A -66(6) . . . . ?
B5 C19 B02P B03R -108(6) . . . . ?
B5 C19 B02P B15 34(6) . . . . ?
B5 C19 B03R B02P 98(6) . . . . ?
B5 C19 B03R B03A 53(8) . . . . ?
B5 C19 B03R B7 -7(8) . . . . ?
B5 C19 B03R B26 -44(5) . . . . ?
B5 C19 B15 B02P -143(6) . . . . ?
B5 C19 B15 B1 -98(8) . . . . ?
B5 C19 B15 C17 -35(5) . . . . ?
B5 C19 B26 B7 100(6) . . . . ?
B5 C19 B26 B03R 133(6) . . . . ?
B5 C19 B26 B94 41(6) . . . . ?
B5 B15 C17 P00M 117(6) . . . . ?
B5 B15 C17 B1 -142(8) . . . . ?
B5 B15 C17 B94 -39(6) . . . . ?
B5 B15 C17 B22 -104(7) . . . . ?
B5 C17 B94 B7 -99(6) . . . . ?
B5 C17 B94 B26 -28(6) . . . . ?
B5 C17 B94 B22 -135(7) . . . . ?
B5 C17 B22 B1 -99(7) . . . . ?
B5 C17 B22 B03A -64(8) . . . . ?
B5 C17 B22 B7 4(9) . . . . ?
B5 C17 B22 B94 43(6) . . . . ?
B5 B26 B94 B7 126(6) . . . . ?
B5 B26 B94 C17 26(5) . . . . ?
B5 B26 B94 B22 85(7) . . . . ?
B5 B94 B22 B1 0(8) . . . . ?
B5 B94 B22 B03A 69(8) . . . . ?
B5 B94 B22 B7 104(6) . . . . ?
B5 B94 B22 C17 -34(5) . . . . ?
C014 C03Y C27 C03L 0.0 . . . . ?
C03Y C014 C02G P00S -171(3) . . . . ?
C03Y C014 C02G C039 0.0 . . . . ?
C03Y C27 C03L C039 0.0 . . . . ?
C27 C03L C039 C02G 0.0 . . . . ?
C03L C039 C02G P00S 170(4) . . . . ?
C03L C039 C02G C014 0.0 . . . . ?
C02G P00S C01T C01F -159(3) . . . . ?
C02G P00S C01T C026 14(4) . . . . ?
C02G P00S C025 B037 163(5) . . . . ?
C02G P00S C025 B03B -63(7) . . . . ?
C02G P00S C025 B03H -135(5) . . . . ?
C02G P00S C025 B21 20(7) . . . . ?
C02G P00S C025 B28 92(5) . . . . ?
C02G C014 C03Y C27 0.0 . . . . ?
C6 C39 C13 C16 0.0 . . . . ?
C39 C6 C1 C14 0.0 . . . . ?
C39 C13 C16 C14 0.0 . . . . ?
C13 C16 C14 P00U -174(3) . . . . ?
C13 C16 C14 C1 0.0 . . . . ?
C16 C14 C1 C6 0.0 . . . . ?
C14 P00U C25 C00Z -140(3) . . . . ?
C14 P00U C25 C03J 42(4) . . . . ?
C14 P00U C19 B5 24(6) . . . . ?
C14 P00U C19 B02P 161(4) . . . . ?
C14 P00U C19 B03R -132(5) . . . . ?
C14 P00U C19 B15 95(5) . . . . ?
C14 P00U C19 B26 -48(5) . . . . ?
C1 C6 C39 C13 0.0 . . . . ?
C018 P00N C046 C035 41(4) . . . . ?
C018 P00N C046 C45 -144(2) . . . . ?
C018 C03P C02A C01G 0.0 . . . . ?
C03P C018 C03E C01A 0.0 . . . . ?
C03P C02A C01G C01A 0.0 . . . . ?
C02A C01G C01A C03E 0.0 . . . . ?
C01G C01A C03E C018 0.0 . . . . ?
C03E C018 C03P C02A 0.0 . . . . ?
C01C C01N C01F C01T 0.0 . . . . ?
C01N C01C C038 C026 0.0 . . . . ?
C01N C01F C01T P00S 174(3) . . . . ?
C01N C01F C01T C026 0.0 . . . . ?
C01F C01T C026 C038 0.0 . . . . ?
C01T P00S C02G C014 101(3) . . . . ?
C01T P00S C02G C039 -70(4) . . . . ?
C01T P00S C025 B037 -84(5) . . . . ?
C01T P00S C025 B03B 51(7) . . . . ?
C01T P00S C025 B03H -21(6) . . . . ?
C01T P00S C025 B21 134(6) . . . . ?
C01T P00S C025 B28 -154(4) . . . . ?
C01T C026 C038 C01C 0.0 . . . . ?
C038 C01C C01N C01F 0.0 . . . . ?
C19 P00U C25 C00Z 108(3) . . . . ?
C19 P00U C25 C03J -69(3) . . . . ?
C19 P00U C14 C16 -84(3) . . . . ?
C19 P00U C14 C1 103(3) . . . . ?
C19 B5 B15 B02P 35(5) . . . . ?
C19 B5 B15 B1 103(7) . . . . ?
C19 B5 B15 C17 138(6) . . . . ?
C19 B5 C17 P00M -141(5) . . . . ?
C19 B5 C17 B1 -8(8) . . . . ?
C19 B5 C17 B15 -40(6) . . . . ?
C19 B5 C17 B94 99(7) . . . . ?
C19 B5 C17 B22 59(8) . . . . ?
C19 B5 B26 B7 -91(5) . . . . ?
C19 B5 B26 B03R -35(4) . . . . ?
C19 B5 B26 B94 -136(6) . . . . ?
C19 B5 B94 B7 -11(8) . . . . ?
C19 B5 B94 C17 -106(6) . . . . ?
C19 B5 B94 B26 41(6) . . . . ?
C19 B5 B94 B22 -70(7) . . . . ?
C19 B02P B1 B03A -100(6) . . . . ?
C19 B02P B1 B15 40(6) . . . . ?
C19 B02P B1 C17 -1(8) . . . . ?
C19 B02P B1 B22 -63(7) . . . . ?
C19 B02P B03A B1 96(6) . . . . ?
C19 B02P B03A B7 -5(7) . . . . ?
C19 B02P B03A B03R -41(5) . . . . ?
C19 B02P B03A B22 58(7) . . . . ?
C19 B02P B03R B03A 132(6) . . . . ?
C19 B02P B03R B7 98(6) . . . . ?
C19 B02P B03R B26 33(5) . . . . ?
C19 B02P B15 B5 -33(5) . . . . ?
C19 B02P B15 B1 -133(7) . . . . ?
C19 B02P B15 C17 -93(6) . . . . ?
C19 B15 C17 P00M 153(5) . . . . ?
C19 B15 C17 B5 36(5) . . . . ?
C19 B15 C17 B1 -106(7) . . . . ?
C19 B15 C17 B94 -4(7) . . . . ?
C19 B15 C17 B22 -68(7) . . . . ?
C19 B26 B94 B5 -36(5) . . . . ?
C19 B26 B94 B7 89(6) . . . . ?
C19 B26 B94 C17 -10(7) . . . . ?
C19 B26 B94 B22 49(8) . . . . ?
C01Z C03M C03Q C70 0.0 . . . . ?
C03M C01Z C02K C02D 0.0 . . . . ?
C03M C03Q C70 P00M 177(4) . . . . ?
C03M C03Q C70 C02D 0.0 . . . . ?
C03Q C70 C02D C02K 0.0 . . . . ?
C70 P00M C02O C03X 42(3) . . . . ?
C70 P00M C02O C045 -145(3) . . . . ?
C70 P00M C17 B5 -135(6) . . . . ?
C70 P00M C17 B1 94(5) . . . . ?
C70 P00M C17 B15 155(4) . . . . ?
C70 P00M C17 B94 -52(6) . . . . ?
C70 P00M C17 B22 23(7) . . . . ?
C70 C02D C02K C01Z 0.0 . . . . ?
C02K C01Z C03M C03Q 0.0 . . . . ?
C025 P00S C02G C014 -145(3) . . . . ?
C025 P00S C02G C039 44(4) . . . . ?
C025 P00S C01T C01F 89(3) . . . . ?
C025 P00S C01T C026 -98(3) . . . . ?
C025 B037 B03H B027 92(6) . . . . ?
C025 B037 B03H C029 126(6) . . . . ?
C025 B037 B03H B03B 36(5) . . . . ?
C025 B037 B18 C029 -102(6) . . . . ?
C025 B037 B18 B03I -68(7) . . . . ?
C025 B037 B18 B28 40(5) . . . . ?
C025 B037 B18 B49 -1(7) . . . . ?
C025 B037 B28 B18 -133(6) . . . . ?
C025 B037 B28 B21 -32(5) . . . . ?
C025 B037 B28 B49 -93(6) . . . . ?
C025 B03B B03H B027 -137(7) . . . . ?
C025 B03B B03H C029 -94(6) . . . . ?
C025 B03B B03H B037 -37(6) . . . . ?
C025 B03B B21 B28 40(6) . . . . ?
C025 B03B B21 B44 140(7) . . . . ?
C025 B03B B21 B49 109(8) . . . . ?
C025 B03B B44 B027 112(7) . . . . ?
C025 B03B B44 B03I 70(7) . . . . ?
C025 B03B B44 B21 -32(5) . . . . ?
C025 B03B B44 B49 -1(8) . . . . ?
C025 B21 B28 B037 35(5) . . . . ?
C025 B21 B28 B18 95(6) . . . . ?
C025 B21 B28 B49 138(7) . . . . ?
C025 B21 B44 B027 5(9) . . . . ?
C025 B21 B44 B03B 38(6) . . . . ?
C025 B21 B44 B03I -62(8) . . . . ?
C025 B21 B44 B49 -107(8) . . . . ?
C025 B21 B49 B03I 62(8) . . . . ?
C025 B21 B49 B18 1(9) . . . . ?
C025 B21 B49 B28 -42(6) . . . . ?
C025 B21 B49 B44 101(8) . . . . ?
C025 B28 B49 B03I -64(7) . . . . ?
C025 B28 B49 B18 -98(6) . . . . ?
C025 B28 B49 B21 31(5) . . . . ?
C025 B28 B49 B44 -3(8) . . . . ?
B027 C029 B037 C025 -13(8) . . . . ?
B027 C029 B037 B03H 37(6) . . . . ?
B027 C029 B037 B18 -107(6) . . . . ?
B027 C029 B037 B28 -74(7) . . . . ?
B027 C029 B03H C025 -97(6) . . . . ?
B027 C029 B03H B037 -142(7) . . . . ?
B027 C029 B03H B03B -40(5) . . . . ?
B027 C029 B03I B18 140(6) . . . . ?
B027 C029 B03I B44 45(5) . . . . ?
B027 C029 B03I B49 103(6) . . . . ?
B027 C029 B18 B037 104(6) . . . . ?
B027 C029 B18 B03I -37(6) . . . . ?
B027 C029 B18 B28 68(7) . . . . ?
B027 C029 B18 B49 5(8) . . . . ?
B027 B03B B03H C025 137(7) . . . . ?
B027 B03B B03H C029 44(6) . . . . ?
B027 B03B B03H B037 100(7) . . . . ?
B027 B03B B21 C025 -106(7) . . . . ?
B027 B03B B21 B28 -66(8) . . . . ?
B027 B03B B21 B44 34(6) . . . . ?
B027 B03B B21 B49 2(9) . . . . ?
B027 B03B B44 B03I -42(6) . . . . ?
B027 B03B B44 B21 -144(7) . . . . ?
B027 B03B B44 B49 -112(8) . . . . ?
B027 B03I B18 C029 39(6) . . . . ?
B027 B03I B18 B037 5(8) . . . . ?
B027 B03I B18 B28 -62(7) . . . . ?
B027 B03I B18 B49 -96(6) . . . . ?
B027 B03I B44 B03B 40(6) . . . . ?
B027 B03I B44 B21 101(7) . . . . ?
B027 B03I B44 B49 142(7) . . . . ?
B027 B03I B49 B18 104(6) . . . . ?
B027 B03I B49 B21 9(8) . . . . ?
B027 B03I B49 B28 70(7) . . . . ?
B027 B03I B49 B44 -33(6) . . . . ?
B027 B44 B49 B03I 38(7) . . . . ?
B027 B44 B49 B18 1(10) . . . . ?
B027 B44 B49 B21 -95(8) . . . . ?
B027 B44 B49 B28 -63(9) . . . . ?
C02O P00M C70 C03Q -68(3) . . . . ?
C02O P00M C70 C02D 110(3) . . . . ?
C02O P00M C17 B5 -18(6) . . . . ?
C02O P00M C17 B1 -149(5) . . . . ?
C02O P00M C17 B15 -88(5) . . . . ?
C02O P00M C17 B94 65(6) . . . . ?
C02O P00M C17 B22 140(6) . . . . ?
C02O C03X C03S C03O 0.0 . . . . ?
C03X C02O C045 C03V 0.0 . . . . ?
C03X C03S C03O C03V 0.0 . . . . ?
C03S C03O C03V C045 0.0 . . . . ?
C03O C03V C045 C02O 0.0 . . . . ?
C045 C02O C03X C03S 0.0 . . . . ?
C37 C035 C046 P00N 175(4) . . . . ?
C37 C035 C046 C45 0.0 . . . . ?
C035 C37 C66 C3 0.0 . . . . ?
C035 C046 C45 C3 0.0 . . . . ?
C046 P00N C018 C03P -9(4) . . . . ?
C046 P00N C018 C03E 171(3) . . . . ?
C046 C45 C3 C66 0.0 . . . . ?
C45 C3 C66 C37 0.0 . . . . ?
C66 C37 C035 C046 0.0 . . . . ?
C029 P00N C018 C03P 105(4) . . . . ?
C029 P00N C018 C03E -75(3) . . . . ?
C029 P00N C046 C035 -78(4) . . . . ?
C029 P00N C046 C45 97(3) . . . . ?
C029 B027 B03B C025 1(8) . . . . ?
C029 B027 B03B B03H -41(5) . . . . ?
C029 B027 B03B B21 59(7) . . . . ?
C029 B027 B03B B44 94(6) . . . . ?
C029 B027 B03I B18 -34(5) . . . . ?
C029 B027 B03I B44 -126(7) . . . . ?
C029 B027 B03I B49 -94(6) . . . . ?
C029 B027 B44 B03B -94(6) . . . . ?
C029 B027 B44 B03I 41(5) . . . . ?
C029 B027 B44 B21 -62(7) . . . . ?
C029 B027 B44 B49 2(9) . . . . ?
C029 B037 B03H C025 -126(6) . . . . ?
C029 B037 B03H B027 -34(6) . . . . ?
C029 B037 B03H B03B -90(6) . . . . ?
C029 B037 B18 B03I 35(5) . . . . ?
C029 B037 B18 B28 142(7) . . . . ?
C029 B037 B18 B49 101(7) . . . . ?
C029 B037 B28 C025 101(6) . . . . ?
C029 B037 B28 B18 -32(5) . . . . ?
C029 B037 B28 B21 69(6) . . . . ?
C029 B037 B28 B49 8(7) . . . . ?
C029 B03I B18 B037 -34(5) . . . . ?
C029 B03I B18 B28 -100(6) . . . . ?
C029 B03I B18 B49 -135(6) . . . . ?
C029 B03I B44 B027 -50(6) . . . . ?
C029 B03I B44 B03B -9(7) . . . . ?
C029 B03I B44 B21 51(7) . . . . ?
C029 B03I B44 B49 93(6) . . . . ?
C029 B03I B49 B18 36(5) . . . . ?
C029 B03I B49 B21 -59(7) . . . . ?
C029 B03I B49 B28 2(7) . . . . ?
C029 B03I B49 B44 -101(6) . . . . ?
C029 B18 B28 C025 -5(7) . . . . ?
C029 B18 B28 B037 34(6) . . . . ?
C029 B18 B28 B21 -56(7) . . . . ?
C029 B18 B28 B49 -100(7) . . . . ?
C029 B18 B49 B03I -40(5) . . . . ?
C029 B18 B49 B21 61(7) . . . . ?
C029 B18 B49 B28 103(7) . . . . ?
C029 B18 B49 B44 -3(8) . . . . ?
B02P C19 B03R B03A -45(5) . . . . ?
B02P C19 B03R B7 -105(6) . . . . ?
B02P C19 B03R B26 -142(5) . . . . ?
B02P C19 B15 B5 143(6) . . . . ?
B02P C19 B15 B1 44(6) . . . . ?
B02P C19 B15 C17 108(6) . . . . ?
B02P C19 B26 B5 -97(6) . . . . ?
B02P C19 B26 B7 3(7) . . . . ?
B02P C19 B26 B03R 37(5) . . . . ?
B02P C19 B26 B94 -56(7) . . . . ?
B02P B1 B03A B7 99(7) . . . . ?
B02P B1 B03A B03R 34(5) . . . . ?
B02P B1 B03A B22 136(7) . . . . ?
B02P B1 B15 B5 -104(7) . . . . ?
B02P B1 B15 C19 -43(6) . . . . ?
B02P B1 B15 C17 -136(7) . . . . ?
B02P B1 C17 P00M 145(6) . . . . ?
B02P B1 C17 B5 5(9) . . . . ?
B02P B1 C17 B15 39(6) . . . . ?
B02P B1 C17 B94 -64(8) . . . . ?
B02P B1 C17 B22 -99(8) . . . . ?
B02P B1 B22 B03A -40(6) . . . . ?
B02P B1 B22 B7 -1(9) . . . . ?
B02P B1 B22 C17 103(7) . . . . ?
B02P B1 B22 B94 67(9) . . . . ?
B02P B03A B7 B03R -32(5) . . . . ?
B02P B03A B7 B26 7(7) . . . . ?
B02P B03A B7 B94 64(7) . . . . ?
B02P B03A B7 B22 97(7) . . . . ?
B02P B03A B03R C19 44(5) . . . . ?
B02P B03A B03R B7 141(6) . . . . ?
B02P B03A B03R B26 105(6) . . . . ?
B02P B03A B22 B1 36(6) . . . . ?
B02P B03A B22 B7 -102(6) . . . . ?
B02P B03A B22 C17 3(8) . . . . ?
B02P B03A B22 B94 -67(8) . . . . ?
B02P B15 C17 P00M -143(5) . . . . ?
B02P B15 C17 B5 100(7) . . . . ?
B02P B15 C17 B1 -42(7) . . . . ?
B02P B15 C17 B94 60(7) . . . . ?
B02P B15 C17 B22 -4(8) . . . . ?
B037 C025 B03B B027 -8(9) . . . . ?
B037 C025 B03B B03H 37(6) . . . . ?
B037 C025 B03B B21 -108(7) . . . . ?
B037 C025 B03B B44 -71(7) . . . . ?
B037 C025 B03H B027 -103(7) . . . . ?
B037 C025 B03H C029 -42(5) . . . . ?
B037 C025 B03H B03B -137(7) . . . . ?
B037 C025 B21 B03B 99(7) . . . . ?
B037 C025 B21 B28 -43(6) . . . . ?
B037 C025 B21 B44 62(8) . . . . ?
B037 C025 B21 B49 -2(9) . . . . ?
B037 C025 B28 B18 39(5) . . . . ?
B037 C025 B28 B21 136(7) . . . . ?
B037 C025 B28 B49 101(6) . . . . ?
B037 C029 B03H C025 45(5) . . . . ?
B037 C029 B03H B027 142(7) . . . . ?
B037 C029 B03H B03B 102(7) . . . . ?
B037 C029 B03I B027 -98(7) . . . . ?
B037 C029 B03I B18 42(6) . . . . ?
B037 C029 B03I B44 -54(8) . . . . ?
B037 C029 B03I B49 4(8) . . . . ?
B037 C029 B18 B03I -141(6) . . . . ?
B037 C029 B18 B28 -36(6) . . . . ?
B037 C029 B18 B49 -99(7) . . . . ?
B037 B18 B28 C025 -38(5) . . . . ?
B037 B18 B28 B21 -90(6) . . . . ?
B037 B18 B28 B49 -134(6) . . . . ?
B037 B18 B49 B03I -101(6) . . . . ?
B037 B18 B49 B21 0(7) . . . . ?
B037 B18 B49 B28 42(6) . . . . ?
B037 B18 B49 B44 -64(7) . . . . ?
B037 B28 B49 B03I -6(7) . . . . ?
B037 B28 B49 B18 -40(5) . . . . ?
B037 B28 B49 B21 89(6) . . . . ?
B037 B28 B49 B44 55(8) . . . . ?
B1 B02P B03A B7 -101(7) . . . . ?
B1 B02P B03A B03R -136(7) . . . . ?
B1 B02P B03A B22 -38(6) . . . . ?
B1 B02P B03R C19 -93(6) . . . . ?
B1 B02P B03R B03A 39(6) . . . . ?
B1 B02P B03R B7 5(8) . . . . ?
B1 B02P B03R B26 -60(7) . . . . ?
B1 B02P B15 B5 100(8) . . . . ?
B1 B02P B15 C19 133(7) . . . . ?
B1 B02P B15 C17 40(6) . . . . ?
B1 B03A B7 B03R -91(7) . . . . ?
B1 B03A B7 B26 -52(7) . . . . ?
B1 B03A B7 B94 5(8) . . . . ?
B1 B03A B7 B22 37(7) . . . . ?
B1 B03A B03R C19 9(8) . . . . ?
B1 B03A B03R B02P -36(6) . . . . ?
B1 B03A B03R B7 106(7) . . . . ?
B1 B03A B03R B26 69(7) . . . . ?
B1 B03A B22 B7 -138(7) . . . . ?
B1 B03A B22 C17 -34(7) . . . . ?
B1 B03A B22 B94 -103(8) . . . . ?
B1 B15 C17 P00M -101(7) . . . . ?
B1 B15 C17 B5 142(8) . . . . ?
B1 B15 C17 B94 102(7) . . . . ?
B1 B15 C17 B22 38(7) . . . . ?
B1 C17 B94 B5 99(7) . . . . ?
B1 C17 B94 B7 -1(8) . . . . ?
B1 C17 B94 B26 70(8) . . . . ?
B1 C17 B94 B22 -36(7) . . . . ?
B1 C17 B22 B03A 35(7) . . . . ?
B1 C17 B22 B7 103(8) . . . . ?
B1 C17 B22 B94 142(7) . . . . ?
B03A B02P B1 B15 140(7) . . . . ?
B03A B02P B1 C17 99(8) . . . . ?
B03A B02P B1 B22 37(6) . . . . ?
B03A B02P B03R C19 -132(6) . . . . ?
B03A B02P B03R B7 -34(6) . . . . ?
B03A B02P B03R B26 -99(6) . . . . ?
B03A B02P B15 B5 65(7) . . . . ?
B03A B02P B15 C19 98(5) . . . . ?
B03A B02P B15 B1 -35(7) . . . . ?
B03A B02P B15 C17 5(7) . . . . ?
B03A B1 B15 B5 -66(8) . . . . ?
B03A B1 B15 C19 -5(9) . . . . ?
B03A B1 B15 B02P 38(6) . . . . ?
B03A B1 B15 C17 -98(8) . . . . ?
B03A B1 C17 P00M -148(5) . . . . ?
B03A B1 C17 B5 72(7) . . . . ?
B03A B1 C17 B15 107(8) . . . . ?
B03A B1 C17 B94 3(9) . . . . ?
B03A B1 C17 B22 -32(6) . . . . ?
B03A B1 B22 B7 39(7) . . . . ?
B03A B1 B22 C17 143(7) . . . . ?
B03A B1 B22 B94 107(8) . . . . ?
B03A B7 B03R C19 103(7) . . . . ?
B03A B7 B03R B02P 37(6) . . . . ?
B03A B7 B03R B26 139(6) . . . . ?
B03A B7 B94 B5 -57(7) . . . . ?
B03A B7 B94 C17 -3(8) . . . . ?
B03A B7 B94 B26 -103(7) . . . . ?
B03A B7 B94 B22 32(6) . . . . ?
B03A B7 B22 B1 -40(7) . . . . ?
B03A B7 B22 C17 -104(8) . . . . ?
B03A B7 B22 B94 -143(7) . . . . ?
B03B C025 B037 C029 13(8) . . . . ?
B03B C025 B037 B03H -39(6) . . . . ?
B03B C025 B037 B18 71(7) . . . . ?
B03B C025 B037 B28 110(6) . . . . ?
B03B C025 B03H B027 34(5) . . . . ?
B03B C025 B03H C029 94(6) . . . . ?
B03B C025 B03H B037 137(7) . . . . ?
B03B C025 B21 B28 -141(6) . . . . ?
B03B C025 B21 B44 -37(6) . . . . ?
B03B C025 B21 B49 -101(7) . . . . ?
B03B C025 B28 B037 -98(7) . . . . ?
B03B C025 B28 B18 -59(7) . . . . ?
B03B C025 B28 B21 39(6) . . . . ?
B03B C025 B28 B49 3(8) . . . . ?
B03B B027 C029 P00N 148(5) . . . . ?
B03B B027 C029 B037 7(7) . . . . ?
B03B B027 C029 B03H 41(5) . . . . ?
B03B B027 C029 B03I -105(6) . . . . ?
B03B B027 C029 B18 -65(7) . . . . ?
B03B B027 B03I C029 86(6) . . . . ?
B03B B027 B03I B18 52(7) . . . . ?
B03B B027 B03I B44 -40(6) . . . . ?
B03B B027 B03I B49 -8(8) . . . . ?
B03B B027 B44 B03I 135(7) . . . . ?
B03B B027 B44 B21 31(6) . . . . ?
B03B B027 B44 B49 95(8) . . . . ?
B03B B21 B28 C025 -39(6) . . . . ?
B03B B21 B28 B037 -4(8) . . . . ?
B03B B21 B28 B18 56(7) . . . . ?
B03B B21 B28 B49 99(8) . . . . ?
B03B B21 B44 B027 -33(6) . . . . ?
B03B B21 B44 B03I -100(7) . . . . ?
B03B B21 B44 B49 -145(7) . . . . ?
B03B B21 B49 B03I -7(8) . . . . ?
B03B B21 B49 B18 -68(7) . . . . ?
B03B B21 B49 B28 -111(7) . . . . ?
B03B B21 B49 B44 32(6) . . . . ?
B03B B44 B49 B03I 103(7) . . . . ?
B03B B44 B49 B18 65(8) . . . . ?
B03B B44 B49 B21 -30(6) . . . . ?
B03B B44 B49 B28 2(9) . . . . ?
B7 B03A B03R C19 -97(6) . . . . ?
B7 B03A B03R B02P -141(6) . . . . ?
B7 B03A B03R B26 -37(6) . . . . ?
B7 B03A B22 B1 138(7) . . . . ?
B7 B03A B22 C17 105(8) . . . . ?
B7 B03A B22 B94 35(7) . . . . ?
B7 B26 B94 B5 -126(6) . . . . ?
B7 B26 B94 C17 -100(6) . . . . ?
B7 B26 B94 B22 -40(6) . . . . ?
B7 B94 B22 B1 -104(8) . . . . ?
B7 B94 B22 B03A -35(7) . . . . ?
B7 B94 B22 C17 -138(7) . . . . ?
B03H C025 B037 C029 52(6) . . . . ?
B03H C025 B037 B18 110(7) . . . . ?
B03H C025 B037 B28 150(6) . . . . ?
B03H C025 B03B B027 -45(7) . . . . ?
B03H C025 B03B B21 -145(7) . . . . ?
B03H C025 B03B B44 -108(7) . . . . ?
B03H C025 B21 B03B 35(7) . . . . ?
B03H C025 B21 B28 -107(7) . . . . ?
B03H C025 B21 B44 -2(9) . . . . ?
B03H C025 B21 B49 -66(9) . . . . ?
B03H C025 B28 B037 -28(6) . . . . ?
B03H C025 B28 B18 11(7) . . . . ?
B03H C025 B28 B21 108(7) . . . . ?
B03H C025 B28 B49 72(7) . . . . ?
B03H B027 C029 P00N 107(6) . . . . ?
B03H B027 C029 B037 -34(6) . . . . ?
B03H B027 C029 B03I -146(6) . . . . ?
B03H B027 C029 B18 -106(7) . . . . ?
B03H B027 B03B C025 42(6) . . . . ?
B03H B027 B03B B21 100(7) . . . . ?
B03H B027 B03B B44 135(7) . . . . ?
B03H B027 B03I C029 28(5) . . . . ?
B03H B027 B03I B18 -6(7) . . . . ?
B03H B027 B03I B44 -98(7) . . . . ?
B03H B027 B03I B49 -66(7) . . . . ?
B03H B027 B44 B03B -37(6) . . . . ?
B03H B027 B44 B03I 98(6) . . . . ?
B03H B027 B44 B21 -6(8) . . . . ?
B03H B027 B44 B49 58(9) . . . . ?
B03H C029 B037 C025 -49(6) . . . . ?
B03H C029 B037 B18 -144(6) . . . . ?
B03H C029 B037 B28 -110(7) . . . . ?
B03H C029 B03I B027 -33(6) . . . . ?
B03H C029 B03I B18 107(7) . . . . ?
B03H C029 B03I B44 11(8) . . . . ?
B03H C029 B03I B49 69(7) . . . . ?
B03H C029 B18 B037 33(6) . . . . ?
B03H C029 B18 B03I -108(6) . . . . ?
B03H C029 B18 B28 -3(8) . . . . ?
B03H C029 B18 B49 -66(7) . . . . ?
B03H B037 B18 C029 -37(6) . . . . ?
B03H B037 B18 B03I -2(8) . . . . ?
B03H B037 B18 B28 105(7) . . . . ?
B03H B037 B18 B49 65(8) . . . . ?
B03H B037 B28 C025 30(6) . . . . ?
B03H B037 B28 B18 -104(7) . . . . ?
B03H B037 B28 B21 -3(8) . . . . ?
B03H B037 B28 B49 -64(8) . . . . ?
B03H B03B B21 C025 -32(6) . . . . ?
B03H B03B B21 B28 8(9) . . . . ?
B03H B03B B21 B44 108(7) . . . . ?
B03H B03B B21 B49 77(7) . . . . ?
B03H B03B B44 B027 46(7) . . . . ?
B03H B03B B44 B03I 4(9) . . . . ?
B03H B03B B44 B21 -97(7) . . . . ?
B03H B03B B44 B49 -66(8) . . . . ?
B03I B027 C029 P00N -107(6) . . . . ?
B03I B027 C029 B037 113(7) . . . . ?
B03I B027 C029 B03H 146(6) . . . . ?
B03I B027 C029 B18 40(6) . . . . ?
B03I B027 B03B C025 -54(8) . . . . ?
B03I B027 B03B B03H -96(7) . . . . ?
B03I B027 B03B B21 4(8) . . . . ?
B03I B027 B03B B44 39(6) . . . . ?
B03I B027 B44 B03B -135(7) . . . . ?
B03I B027 B44 B21 -103(7) . . . . ?
B03I B027 B44 B49 -39(7) . . . . ?
B03I C029 B037 C025 53(8) . . . . ?
B03I C029 B037 B03H 102(7) . . . . ?
B03I C029 B037 B18 -42(6) . . . . ?
B03I C029 B037 B28 -8(8) . . . . ?
B03I C029 B03H C025 -65(7) . . . . ?
B03I C029 B03H B027 32(6) . . . . ?
B03I C029 B03H B037 -110(7) . . . . ?
B03I C029 B03H B03B -8(7) . . . . ?
B03I C029 B18 B037 141(6) . . . . ?
B03I C029 B18 B28 105(6) . . . . ?
B03I C029 B18 B49 42(6) . . . . ?
B03I B18 B28 C025 59(6) . . . . ?
B03I B18 B28 B037 98(6) . . . . ?
B03I B18 B28 B21 8(7) . . . . ?
B03I B18 B28 B49 -36(6) . . . . ?
B03I B18 B49 B21 101(6) . . . . ?
B03I B18 B49 B28 143(6) . . . . ?
B03I B18 B49 B44 37(6) . . . . ?
B03I B44 B49 B18 -37(6) . . . . ?
B03I B44 B49 B21 -133(7) . . . . ?
B03I B44 B49 B28 -101(7) . . . . ?
B03R C19 B02P B1 104(7) . . . . ?
B03R C19 B02P B03A 42(5) . . . . ?
B03R C19 B02P B15 142(7) . . . . ?
B03R C19 B15 B5 109(6) . . . . ?
B03R C19 B15 B02P -34(6) . . . . ?
B03R C19 B15 B1 10(8) . . . . ?
B03R C19 B15 C17 74(6) . . . . ?
B03R C19 B26 B5 -133(6) . . . . ?
B03R C19 B26 B7 -34(5) . . . . ?
B03R C19 B26 B94 -93(6) . . . . ?
B03R B02P B1 B03A -40(6) . . . . ?
B03R B02P B1 B15 100(7) . . . . ?
B03R B02P B1 C17 60(8) . . . . ?
B03R B02P B1 B22 -3(9) . . . . ?
B03R B02P B03A B1 136(7) . . . . ?
B03R B02P B03A B7 36(6) . . . . ?
B03R B02P B03A B22 98(7) . . . . ?
B03R B02P B15 B5 1(8) . . . . ?
B03R B02P B15 C19 34(5) . . . . ?
B03R B02P B15 B1 -100(7) . . . . ?
B03R B02P B15 C17 -60(7) . . . . ?
B03R B03A B7 B26 39(6) . . . . ?
B03R B03A B7 B94 96(7) . . . . ?
B03R B03A B7 B22 129(7) . . . . ?
B03R B03A B22 B1 92(7) . . . . ?
B03R B03A B22 B7 -46(6) . . . . ?
B03R B03A B22 C17 58(8) . . . . ?
B03R B03A B22 B94 -11(9) . . . . ?
B03R B7 B94 B5 6(7) . . . . ?
B03R B7 B94 C17 60(7) . . . . ?
B03R B7 B94 B26 -40(6) . . . . ?
B03R B7 B94 B22 95(7) . . . . ?
B03R B7 B22 B1 4(9) . . . . ?
B03R B7 B22 B03A 44(6) . . . . ?
B03R B7 B22 C17 -60(8) . . . . ?
B03R B7 B22 B94 -100(6) . . . . ?
B03R B26 B94 B5 -89(6) . . . . ?
B03R B26 B94 B7 36(5) . . . . ?
B03R B26 B94 C17 -63(6) . . . . ?
B03R B26 B94 B22 -4(8) . . . . ?
B15 B5 C19 P00U 106(6) . . . . ?
B15 B5 C19 B02P -33(6) . . . . ?
B15 B5 C19 B03R -97(6) . . . . ?
B15 B5 C19 B26 -146(6) . . . . ?
B15 B5 C17 P00M -101(6) . . . . ?
B15 B5 C17 B1 32(6) . . . . ?
B15 B5 C17 B94 140(6) . . . . ?
B15 B5 C17 B22 99(7) . . . . ?
B15 B5 B26 C19 34(6) . . . . ?
B15 B5 B26 B7 -57(7) . . . . ?
B15 B5 B26 B03R -1(8) . . . . ?
B15 B5 B26 B94 -102(8) . . . . ?
B15 B5 B94 B7 57(8) . . . . ?
B15 B5 B94 C17 -39(6) . . . . ?
B15 B5 B94 B26 108(7) . . . . ?
B15 B5 B94 B22 -3(8) . . . . ?
B15 C19 B02P B1 -38(6) . . . . ?
B15 C19 B02P B03A -100(6) . . . . ?
B15 C19 B02P B03R -142(7) . . . . ?
B15 C19 B03R B02P 33(5) . . . . ?
B15 C19 B03R B03A -12(8) . . . . ?
B15 C19 B03R B7 -72(7) . . . . ?
B15 C19 B03R B26 -109(6) . . . . ?
B15 C19 B26 B5 -31(6) . . . . ?
B15 C19 B26 B7 68(6) . . . . ?
B15 C19 B26 B03R 102(6) . . . . ?
B15 C19 B26 B94 9(8) . . . . ?
B15 B02P B1 B03A -140(7) . . . . ?
B15 B02P B1 C17 -41(6) . . . . ?
B15 B02P B1 B22 -103(8) . . . . ?
B15 B02P B03A B1 33(6) . . . . ?
B15 B02P B03A B7 -68(7) . . . . ?
B15 B02P B03A B03R -103(7) . . . . ?
B15 B02P B03A B22 -5(7) . . . . ?
B15 B02P B03R C19 -34(6) . . . . ?
B15 B02P B03R B03A 98(6) . . . . ?
B15 B02P B03R B7 64(7) . . . . ?
B15 B02P B03R B26 -1(8) . . . . ?
B15 B1 B03A B02P -37(6) . . . . ?
B15 B1 B03A B7 62(9) . . . . ?
B15 B1 B03A B03R -2(9) . . . . ?
B15 B1 B03A B22 100(9) . . . . ?
B15 B1 C17 P00M 105(6) . . . . ?
B15 B1 C17 B5 -34(7) . . . . ?
B15 B1 C17 B94 -103(7) . . . . ?
B15 B1 C17 B22 -138(8) . . . . ?
B15 B1 B22 B03A -104(8) . . . . ?
B15 B1 B22 B7 -65(9) . . . . ?
B15 B1 B22 C17 39(6) . . . . ?
B15 B1 B22 B94 3(10) . . . . ?
B15 C17 B94 B5 38(6) . . . . ?
B15 C17 B94 B7 -61(7) . . . . ?
B15 C17 B94 B26 9(8) . . . . ?
B15 C17 B94 B22 -97(7) . . . . ?
B15 C17 B22 B1 -35(6) . . . . ?
B15 C17 B22 B03A 0(9) . . . . ?
B15 C17 B22 B7 68(8) . . . . ?
B15 C17 B22 B94 107(6) . . . . ?
C17 P00M C70 C03Q 43(4) . . . . ?
C17 P00M C70 C02D -140(3) . . . . ?
C17 P00M C02O C03X -74(3) . . . . ?
C17 P00M C02O C045 99(3) . . . . ?
C17 B5 C19 P00U 146(5) . . . . ?
C17 B5 C19 B02P 8(7) . . . . ?
C17 B5 C19 B03R -56(8) . . . . ?
C17 B5 C19 B15 41(6) . . . . ?
C17 B5 C19 B26 -106(7) . . . . ?
C17 B5 B15 C19 -138(6) . . . . ?
C17 B5 B15 B02P -103(7) . . . . ?
C17 B5 B15 B1 -35(6) . . . . ?
C17 B5 B26 C19 105(7) . . . . ?
C17 B5 B26 B7 14(7) . . . . ?
C17 B5 B26 B03R 70(7) . . . . ?
C17 B5 B26 B94 -31(6) . . . . ?
C17 B5 B94 B7 96(6) . . . . ?
C17 B5 B94 B26 148(7) . . . . ?
C17 B5 B94 B22 37(5) . . . . ?
C17 B1 B03A B02P -104(7) . . . . ?
C17 B1 B03A B7 -5(9) . . . . ?
C17 B1 B03A B03R -70(7) . . . . ?
C17 B1 B03A B22 33(6) . . . . ?
C17 B1 B15 B5 33(6) . . . . ?
C17 B1 B15 C19 94(6) . . . . ?
C17 B1 B15 B02P 136(7) . . . . ?
C17 B1 B22 B03A -143(7) . . . . ?
C17 B1 B22 B7 -104(8) . . . . ?
C17 B1 B22 B94 -36(6) . . . . ?
C17 B94 B22 B1 34(6) . . . . ?
C17 B94 B22 B03A 104(8) . . . . ?
C17 B94 B22 B7 138(7) . . . . ?
B18 C029 B037 C025 95(6) . . . . ?
B18 C029 B037 B03H 144(6) . . . . ?
B18 C029 B037 B28 33(6) . . . . ?
B18 C029 B03H C025 9(8) . . . . ?
B18 C029 B03H B027 105(7) . . . . ?
B18 C029 B03H B037 -36(6) . . . . ?
B18 C029 B03H B03B 65(7) . . . . ?
B18 C029 B03I B027 -140(6) . . . . ?
B18 C029 B03I B44 -95(6) . . . . ?
B18 C029 B03I B49 -37(5) . . . . ?
B18 B037 B03H C025 -93(7) . . . . ?
B18 B037 B03H B027 -1(8) . . . . ?
B18 B037 B03H C029 32(5) . . . . ?
B18 B037 B03H B03B -58(8) . . . . ?
B18 B037 B28 C025 133(6) . . . . ?
B18 B037 B28 B21 101(6) . . . . ?
B18 B037 B28 B49 40(5) . . . . ?
B18 B03I B44 B027 -106(6) . . . . ?
B18 B03I B44 B03B -65(7) . . . . ?
B18 B03I B44 B21 -5(7) . . . . ?
B18 B03I B44 B49 37(6) . . . . ?
B18 B03I B49 B21 -94(7) . . . . ?
B18 B03I B49 B28 -34(6) . . . . ?
B18 B03I B49 B44 -136(7) . . . . ?
B18 B28 B49 B03I 34(6) . . . . ?
B18 B28 B49 B21 129(7) . . . . ?
B18 B28 B49 B44 95(7) . . . . ?
B21 C025 B037 C029 -56(8) . . . . ?
B21 C025 B037 B03H -108(7) . . . . ?
B21 C025 B037 B18 2(8) . . . . ?
B21 C025 B037 B28 42(6) . . . . ?
B21 C025 B03B B027 100(8) . . . . ?
B21 C025 B03B B03H 145(7) . . . . ?
B21 C025 B03B B44 37(6) . . . . ?
B21 C025 B03H B027 -2(8) . . . . ?
B21 C025 B03H C029 59(8) . . . . ?
B21 C025 B03H B037 102(8) . . . . ?
B21 C025 B03H B03B -35(7) . . . . ?
B21 C025 B28 B037 -136(7) . . . . ?
B21 C025 B28 B18 -97(6) . . . . ?
B21 C025 B28 B49 -36(6) . . . . ?
B21 B03B B03H C025 28(5) . . . . ?
B21 B03B B03H B027 -109(7) . . . . ?
B21 B03B B03H C029 -65(7) . . . . ?
B21 B03B B03H B037 -9(8) . . . . ?
B21 B03B B44 B027 144(7) . . . . ?
B21 B03B B44 B03I 102(7) . . . . ?
B21 B03B B44 B49 31(6) . . . . ?
B21 B28 B49 B03I -95(7) . . . . ?
B21 B28 B49 B18 -129(7) . . . . ?
B21 B28 B49 B44 -34(6) . . . . ?
B21 B44 B49 B03I 133(7) . . . . ?
B21 B44 B49 B18 96(7) . . . . ?
B21 B44 B49 B28 33(6) . . . . ?
B26 B5 C19 P00U -108(5) . . . . ?
B26 B5 C19 B02P 113(5) . . . . ?
B26 B5 C19 B03R 49(6) . . . . ?
B26 B5 C19 B15 146(6) . . . . ?
B26 B5 B15 C19 -34(6) . . . . ?
B26 B5 B15 B02P 0(9) . . . . ?
B26 B5 B15 B1 69(9) . . . . ?
B26 B5 B15 C17 103(7) . . . . ?
B26 B5 C17 P00M 149(5) . . . . ?
B26 B5 C17 B1 -78(8) . . . . ?
B26 B5 C17 B15 -110(7) . . . . ?
B26 B5 C17 B94 29(6) . . . . ?
B26 B5 C17 B22 -12(8) . . . . ?
B26 B5 B94 B7 -52(6) . . . . ?
B26 B5 B94 C17 -148(7) . . . . ?
B26 B5 B94 B22 -111(7) . . . . ?
B26 C19 B02P B1 63(7) . . . . ?
B26 C19 B02P B03A 1(7) . . . . ?
B26 C19 B02P B03R -41(6) . . . . ?
B26 C19 B02P B15 101(6) . . . . ?
B26 C19 B03R B02P 142(5) . . . . ?
B26 C19 B03R B03A 97(6) . . . . ?
B26 C19 B03R B7 37(5) . . . . ?
B26 C19 B15 B5 32(6) . . . . ?
B26 C19 B15 B02P -111(6) . . . . ?
B26 C19 B15 B1 -67(8) . . . . ?
B26 C19 B15 C17 -3(7) . . . . ?
B26 B7 B03R C19 -36(5) . . . . ?
B26 B7 B03R B02P -102(6) . . . . ?
B26 B7 B03R B03A -139(6) . . . . ?
B26 B7 B94 B5 46(5) . . . . ?
B26 B7 B94 C17 100(6) . . . . ?
B26 B7 B94 B22 135(7) . . . . ?
B26 B7 B22 B1 68(8) . . . . ?
B26 B7 B22 B03A 108(6) . . . . ?
B26 B7 B22 C17 5(8) . . . . ?
B26 B7 B22 B94 -35(5) . . . . ?
B26 B94 B22 B1 -60(9) . . . . ?
B26 B94 B22 B03A 10(10) . . . . ?
B26 B94 B22 B7 45(7) . . . . ?
B26 B94 B22 C17 -94(7) . . . . ?
B28 C025 B037 C029 -98(6) . . . . ?
B28 C025 B037 B03H -150(6) . . . . ?
B28 C025 B037 B18 -40(5) . . . . ?
B28 C025 B03B B027 62(8) . . . . ?
B28 C025 B03B B03H 107(7) . . . . ?
B28 C025 B03B B21 -38(6) . . . . ?
B28 C025 B03B B44 -2(8) . . . . ?
B28 C025 B03H B027 -73(7) . . . . ?
B28 C025 B03H C029 -12(7) . . . . ?
B28 C025 B03H B037 30(6) . . . . ?
B28 C025 B03H B03B -107(7) . . . . ?
B28 C025 B21 B03B 141(6) . . . . ?
B28 C025 B21 B44 104(7) . . . . ?
B28 C025 B21 B49 40(6) . . . . ?
B28 B037 B03H C025 -28(6) . . . . ?
B28 B037 B03H B027 64(8) . . . . ?
B28 B037 B03H C029 97(7) . . . . ?
B28 B037 B03H B03B 7(8) . . . . ?
B28 B037 B18 C029 -142(7) . . . . ?
B28 B037 B18 B03I -107(6) . . . . ?
B28 B037 B18 B49 -41(6) . . . . ?
B28 B18 B49 B03I -143(6) . . . . ?
B28 B18 B49 B21 -42(5) . . . . ?
B28 B18 B49 B44 -106(7) . . . . ?
B28 B21 B44 B027 78(8) . . . . ?
B28 B21 B44 B03B 110(7) . . . . ?
B28 B21 B44 B03I 11(8) . . . . ?
B28 B21 B44 B49 -34(6) . . . . ?
B28 B21 B49 B03I 104(6) . . . . ?
B28 B21 B49 B18 44(5) . . . . ?
B28 B21 B49 B44 143(7) . . . . ?
B44 B027 C029 P00N -151(5) . . . . ?
B44 B027 C029 B037 69(7) . . . . ?
B44 B027 C029 B03H 102(7) . . . . ?
B44 B027 C029 B03I -44(5) . . . . ?
B44 B027 C029 B18 -4(8) . . . . ?
B44 B027 B03B C025 -93(7) . . . . ?
B44 B027 B03B B03H -135(7) . . . . ?
B44 B027 B03B B21 -35(7) . . . . ?
B44 B027 B03I C029 126(6) . . . . ?
B44 B027 B03I B18 93(7) . . . . ?
B44 B027 B03I B49 32(6) . . . . ?
B44 B03B B03H C025 96(7) . . . . ?
B44 B03B B03H B027 -41(6) . . . . ?
B44 B03B B03H C029 2(8) . . . . ?
B44 B03B B03H B037 58(8) . . . . ?
B44 B03B B21 C025 -140(7) . . . . ?
B44 B03B B21 B28 -100(7) . . . . ?
B44 B03B B21 B49 -31(6) . . . . ?
B44 B03I B18 C029 99(6) . . . . ?
B44 B03I B18 B037 65(7) . . . . ?
B44 B03I B18 B28 -1(7) . . . . ?
B44 B03I B18 B49 -36(6) . . . . ?
B44 B03I B49 B18 136(7) . . . . ?
B44 B03I B49 B21 42(6) . . . . ?
B44 B03I B49 B28 102(7) . . . . ?
B44 B21 B28 C025 -105(7) . . . . ?
B44 B21 B28 B037 -70(7) . . . . ?
B44 B21 B28 B18 -11(7) . . . . ?
B44 B21 B28 B49 33(6) . . . . ?
B44 B21 B49 B03I -39(6) . . . . ?
B44 B21 B49 B18 -100(7) . . . . ?
B44 B21 B49 B28 -143(7) . . . . ?
B49 B03I B18 C029 135(6) . . . . ?
B49 B03I B18 B037 101(7) . . . . ?
B49 B03I B18 B28 35(6) . . . . ?
B49 B03I B44 B027 -142(7) . . . . ?
B49 B03I B44 B03B -102(7) . . . . ?
B49 B03I B44 B21 -42(6) . . . . ?
B49 B18 B28 C025 96(6) . . . . ?
B49 B18 B28 B037 134(6) . . . . ?
B49 B18 B28 B21 44(6) . . . . ?
B49 B21 B28 C025 -138(7) . . . . ?
B49 B21 B28 B037 -103(6) . . . . ?
B49 B21 B28 B18 -44(6) . . . . ?
B49 B21 B44 B027 112(8) . . . . ?
B49 B21 B44 B03B 145(7) . . . . ?
B49 B21 B44 B03I 45(6) . . . . ?
B94 B5 C19 P00U -146(5) . . . . ?
B94 B5 C19 B02P 75(6) . . . . ?
B94 B5 C19 B03R 11(8) . . . . ?
B94 B5 C19 B15 108(7) . . . . ?
B94 B5 C19 B26 -38(5) . . . . ?
B94 B5 B15 C19 -98(7) . . . . ?
B94 B5 B15 B02P -64(8) . . . . ?
B94 B5 B15 B1 5(9) . . . . ?
B94 B5 B15 C17 39(6) . . . . ?
B94 B5 C17 P00M 120(6) . . . . ?
B94 B5 C17 B1 -107(6) . . . . ?
B94 B5 C17 B15 -140(6) . . . . ?
B94 B5 C17 B22 -41(6) . . . . ?
B94 B5 B26 C19 136(6) . . . . ?
B94 B5 B26 B7 45(5) . . . . ?
B94 B5 B26 B03R 101(6) . . . . ?
B94 B7 B03R C19 0(7) . . . . ?
B94 B7 B03R B02P -66(7) . . . . ?
B94 B7 B03R B03A -103(7) . . . . ?
B94 B7 B03R B26 35(5) . . . . ?
B94 B7 B22 B1 104(8) . . . . ?
B94 B7 B22 B03A 143(7) . . . . ?
B94 B7 B22 C17 40(6) . . . . ?
B94 C17 B22 B1 -142(7) . . . . ?
B94 C17 B22 B03A -107(8) . . . . ?
B94 C17 B22 B7 -40(6) . . . . ?
B22 B1 B03A B02P -136(7) . . . . ?
B22 B1 B03A B7 -38(6) . . . . ?
B22 B1 B03A B03R -102(7) . . . . ?
B22 B1 B15 B5 -4(9) . . . . ?
B22 B1 B15 C19 56(9) . . . . ?
B22 B1 B15 B02P 99(8) . . . . ?
B22 B1 B15 C17 -37(6) . . . . ?
B22 B1 C17 P00M -116(6) . . . . ?
B22 B1 C17 B5 104(7) . . . . ?
B22 B1 C17 B15 138(8) . . . . ?
B22 B1 C17 B94 35(7) . . . . ?
B22 B03A B7 B03R -129(7) . . . . ?
B22 B03A B7 B26 -90(7) . . . . ?
B22 B03A B7 B94 -33(6) . . . . ?
B22 B03A B03R C19 -52(8) . . . . ?
B22 B03A B03R B02P -97(7) . . . . ?
B22 B03A B03R B7 45(6) . . . . ?
B22 B03A B03R B26 8(8) . . . . ?
B22 B7 B03R C19 60(7) . . . . ?
B22 B7 B03R B02P -6(8) . . . . ?
B22 B7 B03R B03A -43(6) . . . . ?
B22 B7 B03R B26 96(6) . . . . ?
B22 B7 B94 B5 -89(7) . . . . ?
B22 B7 B94 C17 -35(6) . . . . ?
B22 B7 B94 B26 -135(7) . . . . ?
B22 C17 B94 B5 135(7) . . . . ?
B22 C17 B94 B7 36(6) . . . . ?
B22 C17 B94 B26 107(7) . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 -0.013 0.000 0.000 982.9 0.0 '0.5 ?'
2 -0.541 0.500 0.500 982.9 0.0 '0.5 ?'
3 0.423 0.581 0.238 19.5 0.0 ?
4 0.423 0.919 0.738 19.5 0.0 ?
5 0.577 0.081 0.262 19.5 0.0 ?
6 0.577 0.419 0.762 19.5 0.0 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_xhh_25070_2-s7_c_pl
_database_code_depnum_ccdc_archive 'CCDC 2495585'
loop_
_audit_author_name
_audit_author_address
'Hao-Hui Xie'
;NanJing University of Science and Technology
China
;
_audit_update_record             
;
2025-10-15 deposited with the CCDC.	2026-03-06 downloaded from the CCDC.
;
_audit_creation_date             2025-09-30
_audit_creation_method           
;
Olex2 1.5
(compiled 2024.02.16 svn.r378c4104 for OlexSys, GUI svn.r6928)
;
_shelx_SHELXL_version_number     2018/3
_chemical_name_common            ?
_chemical_name_systematic        ?
_chemical_formula_moiety         'C52 H60 Au2 B18 P4'
_chemical_formula_sum            'C52 H60 Au2 B18 P4'
_chemical_formula_weight         1397.39
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_H-M_alt        'C 1 2/c 1'
_space_group_name_Hall           '-C 2yc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   25.395(3)
_cell_length_b                   11.2877(13)
_cell_length_c                   22.043(2)
_cell_angle_alpha                90
_cell_angle_beta                 98.439(4)
_cell_angle_gamma                90
_cell_volume                     6250.2(12)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    68146
_cell_measurement_temperature    100.15
_cell_measurement_theta_max      56.566
_cell_measurement_theta_min      3.956
_shelx_estimated_absorpt_T_max   0.794
_shelx_estimated_absorpt_T_min   0.699
_exptl_absorpt_coefficient_mu    4.825
_exptl_absorpt_correction_T_max  0.9883
_exptl_absorpt_correction_T_min  0.8246
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   
;
 SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D.,
 J. Appl. Cryst. 48 (2015) 3-10
;
_exptl_crystal_colour            brown
_exptl_crystal_colour_primary    brown
_exptl_crystal_density_diffrn    1.485
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_description       block
_exptl_crystal_F_000             2720
_exptl_crystal_size_max          0.08
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.05
_exptl_transmission_factor_max   ?
_exptl_transmission_factor_min   ?
_diffrn_reflns_av_R_equivalents  0.1981
_diffrn_reflns_av_unetI/netI     0.0930
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max       30
_diffrn_reflns_limit_h_min       -30
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            54795
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full        25.027
_diffrn_reflns_theta_max         25.027
_diffrn_reflns_theta_min         1.978
_diffrn_ambient_temperature      100.15
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  multi-scan
_diffrn_measurement_method       ?
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   ?
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_full    .
_reflns_Friedel_fraction_max     .
_reflns_number_gt                3471
_reflns_number_total             5530
_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 Structure factors included contributions from the .fab file.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
_reflns_threshold_expression     'I > 2σ(I)'
_computing_cell_refinement       ?
_computing_data_collection       ?
_computing_data_reduction        ?
_computing_molecular_graphics    'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.5 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'olex2.solve 1.5 (Bourhis et al., 2015)'
_refine_diff_density_max         5.390
_refine_diff_density_min         -1.884
_refine_diff_density_rms         0.253
_refine_ls_extinction_coef       0.00015(5)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
_refine_ls_goodness_of_fit_ref   1.058
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     382
_refine_ls_number_reflns         5530
_refine_ls_number_restraints     257
_refine_ls_R_factor_all          0.1280
_refine_ls_R_factor_gt           0.0747
_refine_ls_restrained_S_all      1.051
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'w=1/[σ²(Fo²)+(0.0776P)²+362.0410P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1720
_refine_ls_wR_factor_ref         0.2257
_refine_special_details          ?
_olex2_refinement_description    
;
1. Fixed Uiso
 At 1.2 times of:
  All B(H) groups, H5 of C5, H23A of C23A, H3 of C3, H2 of C2, H24A of C24A,
  H6 of C6, H17 of C17, H4 of C4, H16 of C16, H22A of C22A, H26A of C26A, H25A
  of C25A, H19 of C19, H10 of C10, H8 of C8, H12 of C12, H18 of C18, H20 of C20,
   H9 of C9, H11 of C11, H24 of C24, H22 of C22, H26 of C26, H23 of C23, All
  C(H,H,H,H) groups
 At 1.5 times of:
  H4B of C25
2. Restrained distances
 B1-H1 = B8-H8A = B4-H4A = B3-H3A
 1.12 with sigma of 0.01
 B4-H4A = B1-H1
 1 with sigma of 0.01
 C24A-C23A \\sim C24-C23
 with sigma of 0.02
 C24A-C25A \\sim C24-C25
 with sigma of 0.02
 C23A-C22A \\sim C23-C22
 with sigma of 0.02
 C22A-C21A \\sim C22-C21
 with sigma of 0.02
 C21A-C26A \\sim C21-C26
 with sigma of 0.02
 C26A-C25A \\sim C26-C25
 with sigma of 0.02
 P2-C22A \\sim P2-C22
 with sigma of 0.04
 P2-C26A \\sim P2-C26
 with sigma of 0.04
 C24A-C22A \\sim C24-C22
 with sigma of 0.04
 C24A-C26A \\sim C24-C26
 with sigma of 0.04
 C23A-C21A \\sim C23-C21
 with sigma of 0.04
 C23A-C25A \\sim C23-C25
 with sigma of 0.04
 C22A-C26A \\sim C22-C26
 with sigma of 0.04
 C21A-C25A \\sim C21-C25
 with sigma of 0.04
 P2-C21A \\sim P2-C21
 with sigma of 0.02
 B1-H1 \\sim B3-H3A
 with sigma of 0.02
 B1-H4B \\sim B4-H4B
 with sigma of 0.02
3. Uiso/Uaniso restraints and constraints
C21A \\sim C26A \\sim C25A \\sim C24A \\sim C23A \\sim C22A: within 2A with
sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A
C11 \\sim C12 \\sim C7 \\sim C8 \\sim C9 \\sim C10: within 2A with sigma of
0.001 and sigma for terminal atoms of 0.002 within 2A
B1 \\sim B8 \\sim B5 \\sim B3 \\sim B4 \\sim B2: within 2A with sigma of 0.01
and sigma for terminal atoms of 0.02 within 2A
C21 \\sim C26 \\sim C25 \\sim C24 \\sim C23 \\sim C22: within 2A with sigma of
0.01 and sigma for terminal atoms of 0.02 within 2A
4. Rigid body (RIGU) restrains
 C24, C23, C22, C21, C26, C25
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C24A, C23A, C22A, C21A, C26A, C25A
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
5. Others
 Sof(C24)=Sof(H24)=Sof(C23)=Sof(H23)=Sof(C22)=Sof(H22)=Sof(C21)=Sof(C26)=
 Sof(H26)=Sof(C25)=Sof(H25)=1-FVAR(1)
 Sof(C24A)=Sof(H24A)=Sof(C23A)=Sof(H23A)=Sof(C22A)=Sof(H22A)=Sof(C21A)=
 Sof(C26A)=Sof(H26A)=Sof(C25A)=Sof(H25A)=FVAR(1)
 Fixed X: H1(-0.19376)
 Fixed Y: H4A(0.708261) H1(0.72095)
 Fixed Z: H4A(0.20368) H1(0.06263)
6.a Aromatic/amide H refined with riding coordinates:
 C5(H5), C3(H3), C2(H2), C4(H4), C6(H6), C16(H16), C17(H17), C24A(H24A),
 C23A(H23A), C22A(H22A), C26A(H26A), C25A(H25A), C20(H20), C18(H18), C19(H19),
 C10(H10), C9(H9), C8(H8), C12(H12), C11(H11), C24(H24), C23(H23), C22(H22),
 C26(H26), C25(H25)
6.b Fitted hexagon refined as free rotating group:
 C24A(C23A,C22A,C21A,C26A,C25A), C24(C23,C22,C21,C26,C25)
6.c Boron cage BH refined with riding coordinates:
 B5(H5A), B6(H6A), B8(H8A), B2(H2A), B3(H3A), B7(H7)
;
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au1 Au 0.03745(2) 0.71147(6) 0.13903(3) 0.0347(3) Uani 1 1 d . . . . .
P1 P -0.04745(14) 0.7186(4) 0.08405(17) 0.0284(8) Uani 1 1 d . . . . .
P2 P -0.12308(15) 0.6970(4) 0.30862(18) 0.0299(9) Uani 1 1 d D . . . .
C15 C -0.1712(6) 0.7476(14) 0.3568(7) 0.034(4) Uani 1 1 d . . . . .
C1 C -0.0480(7) 0.7937(13) 0.0110(8) 0.036(4) Uani 1 1 d . . . . .
C5 C 0.0031(7) 0.8886(16) -0.0602(8) 0.046(4) Uani 1 1 d . . . . .
H5 H 0.036293 0.912217 -0.071436 0.056 Uiso 1 1 calc R U . . .
C13 C -0.0955(5) 0.7880(13) 0.1271(6) 0.028(3) Uani 1 1 d . . . . .
C3 C -0.0926(8) 0.8715(19) -0.0853(8) 0.057(5) Uani 1 1 d . . . . .
H3 H -0.124083 0.883364 -0.113689 0.068 Uiso 1 1 calc R U . . .
C2 C -0.0950(7) 0.8161(17) -0.0290(7) 0.045(4) Uani 1 1 d . . . . .
H2 H -0.128370 0.793871 -0.017962 0.054 Uiso 1 1 calc R U . . .
C4 C -0.0437(8) 0.9089(17) -0.0993(8) 0.050(5) Uani 1 1 d . . . . .
H4 H -0.042364 0.949510 -0.136740 0.060 Uiso 1 1 calc R U . . .
C6 C 0.0011(7) 0.8335(15) -0.0044(7) 0.038(4) Uani 1 1 d . . . . .
H6 H 0.032901 0.822445 0.023641 0.046 Uiso 1 1 calc R U . . .
C14 C -0.1307(5) 0.7753(14) 0.2363(6) 0.029(3) Uani 1 1 d . . . . .
C16 C -0.1571(7) 0.8464(17) 0.3930(8) 0.051(5) Uani 1 1 d . . . . .
H16 H -0.124152 0.885660 0.391734 0.061 Uiso 1 1 calc R U . . .
C17 C -0.1922(8) 0.8865(18) 0.4313(9) 0.056(5) Uani 1 1 d . . . . .
H17 H -0.182713 0.953944 0.456322 0.067 Uiso 1 1 calc R U . . .
C24A C -0.1529(10) 0.3075(14) 0.2532(12) 0.070(7) Uani 0.563(19) 1 d DG U P A 1
H24A H -0.157900 0.226984 0.241126 0.084 Uiso 0.563(19) 1 calc R U P A 1
C23A C -0.1065(9) 0.3418(16) 0.2906(12) 0.071(7) Uani 0.563(19) 1 d DG U P A 1
H23A H -0.079834 0.284759 0.304117 0.086 Uiso 0.563(19) 1 calc R U P A 1
C22A C -0.0991(8) 0.4596(18) 0.3082(10) 0.069(7) Uani 0.563(19) 1 d DG U P A 1
H22A H -0.067430 0.483034 0.333792 0.082 Uiso 0.563(19) 1 calc R U P A 1
C21A C -0.1381(9) 0.5430(13) 0.2884(11) 0.063(7) Uani 0.563(19) 1 d DG U P A 1
C26A C -0.1845(8) 0.5087(16) 0.2510(10) 0.064(6) Uani 0.563(19) 1 d DG U P A 1
H26A H -0.211157 0.565763 0.237482 0.077 Uiso 0.563(19) 1 calc R U P A 1
C25A C -0.1919(8) 0.3909(19) 0.2334(10) 0.067(6) Uani 0.563(19) 1 d DG U P A 1
H25A H -0.223562 0.367488 0.207807 0.081 Uiso 0.563(19) 1 calc R U P A 1
C20 C -0.2202(6) 0.6940(15) 0.3584(8) 0.039(4) Uani 1 1 d . . . . .
H20 H -0.231339 0.630367 0.331340 0.047 Uiso 1 1 calc R U . . .
C18 C -0.2396(7) 0.8329(17) 0.4341(7) 0.044(4) Uani 1 1 d . . . . .
H18 H -0.263440 0.863236 0.459693 0.052 Uiso 1 1 calc R U . . .
C19 C -0.2522(7) 0.7327(17) 0.3986(9) 0.052(5) Uani 1 1 d . . . . .
H19 H -0.283805 0.690145 0.402506 0.062 Uiso 1 1 calc R U . . .
C10 C -0.1109(11) 0.343(2) 0.0444(10) 0.077(3) Uani 1 1 d . U . . .
H10 H -0.115656 0.259838 0.038362 0.092 Uiso 1 1 calc R U . . .
C9 C -0.1035(11) 0.4117(19) -0.0007(10) 0.077(3) Uani 1 1 d . U . . .
H9 H -0.113624 0.385094 -0.041632 0.092 Uiso 1 1 calc R U . . .
C8 C -0.0808(11) 0.5253(19) 0.0098(10) 0.077(3) Uani 1 1 d . U . . .
H8 H -0.071191 0.569924 -0.023480 0.092 Uiso 1 1 calc R U . . .
C7 C -0.0728(11) 0.5705(19) 0.0673(10) 0.076(3) Uani 1 1 d . U . . .
C12 C -0.0883(11) 0.5010(19) 0.1104(10) 0.077(3) Uani 1 1 d . U . . .
H12 H -0.083127 0.528713 0.151522 0.092 Uiso 1 1 calc R U . . .
C11 C -0.1116(11) 0.3901(19) 0.0985(10) 0.077(3) Uani 1 1 d . U . . .
H11 H -0.127621 0.349809 0.128916 0.092 Uiso 1 1 calc R U . . .
B9 B -0.0807(7) 0.7687(18) 0.2014(8) 0.033(4) Uani 1 1 d . . . . .
B5 B -0.1314(8) 0.986(2) 0.1783(10) 0.050(3) Uani 1 1 d . U . . .
H5A H -0.133627 1.084680 0.179882 0.060 Uiso 1 1 calc R U . . .
B4 B -0.1868(8) 0.755(2) 0.1851(11) 0.049(4) Uani 1 1 d D U . . .
B6 B -0.0951(8) 0.9027(16) 0.2390(9) 0.038(4) Uani 1 1 d . . . . .
H6A H -0.071383 0.942572 0.280885 0.046 Uiso 1 1 calc R U . . .
B1 B -0.1660(6) 0.7612(18) 0.0985(7) 0.056(4) Uani 1 1 d D U . . .
B8 B -0.1272(8) 0.914(2) 0.1099(11) 0.050(3) Uani 1 1 d D U . . .
H8A H -0.125177 0.968042 0.067645 0.060 Uiso 1 1 calc DR U . . .
B2 B -0.1868(9) 0.898(2) 0.1438(11) 0.053(3) Uani 1 1 d . U . . .
H2A H -0.225780 0.937852 0.123446 0.064 Uiso 1 1 calc R U . . .
B3 B -0.1664(8) 0.901(2) 0.2243(10) 0.049(3) Uani 1 1 d D U . . .
H3A H -0.190978 0.943564 0.256408 0.059 Uiso 1 1 calc DR U . . .
B7 B -0.0717(8) 0.9103(16) 0.1683(8) 0.039(4) Uani 1 1 d . . . . .
H7 H -0.032683 0.954490 0.165255 0.046 Uiso 1 1 calc R U . . .
C24 C -0.1647(11) 0.2989(13) 0.2752(10) 0.041(6) Uani 0.437(19) 1 d DG U P A 2
H24 H -0.172515 0.217159 0.268661 0.050 Uiso 0.437(19) 1 calc R U P A 2
C23 C -0.1672(11) 0.3496(16) 0.3321(9) 0.044(6) Uani 0.437(19) 1 d DG U P A 2
H23 H -0.176708 0.302501 0.364578 0.053 Uiso 0.437(19) 1 calc R U P A 2
C22 C -0.1558(11) 0.4692(17) 0.3417(7) 0.043(6) Uani 0.437(19) 1 d DG U P A 2
H22 H -0.157482 0.503802 0.380604 0.051 Uiso 0.437(19) 1 calc R U P A 2
C21 C -0.1419(11) 0.5380(13) 0.2942(9) 0.036(6) Uani 0.437(19) 1 d DG U P A 2
C26 C -0.1394(10) 0.4873(16) 0.2372(8) 0.039(6) Uani 0.437(19) 1 d DG U P A 2
H26 H -0.129868 0.534422 0.204798 0.047 Uiso 0.437(19) 1 calc R U P A 2
C25 C -0.1508(11) 0.3678(17) 0.2277(8) 0.041(6) Uani 0.437(19) 1 d DG U P A 2
H25 H -0.149094 0.333121 0.188771 0.049 Uiso 0.437(19) 1 calc R U P A 2
H4A H -0.2171(13) 0.708261 0.203680 0.049 Uiso 1 1 d D U . . .
H9A H -0.048(7) 0.724(15) 0.216(8) 0.049 Uiso 1 1 d . U . . .
H1 H -0.193760 0.720950 0.062630 0.049 Uiso 1 1 d D U . . .
H4B H -0.163(7) 0.720(16) 0.147(3) 0.061 Uiso 1 1 d D U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au1 P1 2.314(4) . ?
Au1 P2 2.313(4) 2 ?
P1 C1 1.819(16) . ?
P1 C13 1.829(15) . ?
P1 C7 1.81(2) . ?
P2 C15 1.825(15) . ?
P2 C14 1.808(15) . ?
P2 C21A 1.821(14) . ?
P2 C21 1.872(14) . ?
C15 C16 1.39(2) . ?
C15 C20 1.39(2) . ?
C1 C2 1.40(2) . ?
C1 C6 1.41(2) . ?
C5 H5 0.9500 . ?
C5 C4 1.38(3) . ?
C5 C6 1.39(2) . ?
C13 B9 1.64(2) . ?
C13 B1 1.832(18) . ?
C13 B8 1.65(3) . ?
C13 B7 1.71(2) . ?
C3 H3 0.9500 . ?
C3 C2 1.40(2) . ?
C3 C4 1.39(3) . ?
C2 H2 0.9500 . ?
C4 H4 0.9500 . ?
C6 H6 0.9500 . ?
C14 B9 1.58(2) . ?
C14 B4 1.70(3) . ?
C14 B6 1.69(2) . ?
C14 B3 1.68(3) . ?
C16 H16 0.9500 . ?
C16 C17 1.39(2) . ?
C17 H17 0.9500 . ?
C17 C18 1.36(3) . ?
C24A H24A 0.9500 . ?
C24A C23A 1.3900 . ?
C24A C25A 1.3900 . ?
C23A H23A 0.9500 . ?
C23A C22A 1.3900 . ?
C22A H22A 0.9500 . ?
C22A C21A 1.3900 . ?
C21A C26A 1.3900 . ?
C26A H26A 0.9500 . ?
C26A C25A 1.3900 . ?
C25A H25A 0.9500 . ?
C20 H20 0.9500 . ?
C20 C19 1.36(2) . ?
C18 H18 0.9500 . ?
C18 C19 1.39(3) . ?
C19 H19 0.9500 . ?
C10 H10 0.9500 . ?
C10 C9 1.30(3) . ?
C10 C11 1.31(3) . ?
C9 H9 0.9500 . ?
C9 C8 1.41(3) . ?
C8 H8 0.9500 . ?
C8 C7 1.35(3) . ?
C7 C12 1.34(3) . ?
C12 H12 0.9500 . ?
C12 C11 1.39(3) . ?
C11 H11 0.9500 . ?
B9 B6 1.79(3) . ?
B9 B7 1.79(3) . ?
B9 H9A 0.98(17) . ?
B5 H5A 1.1200 . ?
B5 B6 1.78(3) . ?
B5 B8 1.73(3) . ?
B5 B2 1.80(3) . ?
B5 B3 1.73(3) . ?
B5 B7 1.78(3) . ?
B4 B1 2.05(3) . ?
B4 B2 1.85(3) . ?
B4 B3 1.89(3) . ?
B4 H4A 1.064(7) . ?
B4 H4B 1.16(9) . ?
B6 H6A 1.1200 . ?
B6 B3 1.79(3) . ?
B6 B7 1.75(3) . ?
B1 B8 1.98(3) . ?
B1 B2 1.95(3) . ?
B1 H1 1.080(7) . ?
B1 H1 1.080(7) . ?
B1 H4B 1.16(9) . ?
B8 H8A 1.1200 . ?
B8 B2 1.79(3) . ?
B8 B7 1.76(3) . ?
B2 H2A 1.1200 . ?
B2 B3 1.77(3) . ?
B3 H3A 1.1200 . ?
B7 H7 1.1200 . ?
C24 H24 0.9500 . ?
C24 C23 1.3900 . ?
C24 C25 1.3900 . ?
C23 H23 0.9500 . ?
C23 C22 1.3900 . ?
C22 H22 0.9500 . ?
C22 C21 1.3900 . ?
C21 C26 1.3900 . ?
C26 H26 0.9500 . ?
C26 C25 1.3900 . ?
C25 H25 0.9500 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P2 Au1 P1 177.41(15) 2 . ?
C1 P1 Au1 111.4(5) . . ?
C1 P1 C13 109.9(7) . . ?
C13 P1 Au1 112.7(5) . . ?
C7 P1 Au1 110.5(9) . . ?
C7 P1 C1 107.1(9) . . ?
C7 P1 C13 104.9(9) . . ?
C15 P2 Au1 110.4(6) . 2 ?
C15 P2 C21 102.9(9) . . ?
C14 P2 Au1 112.1(5) . 2 ?
C14 P2 C15 111.5(7) . . ?
C14 P2 C21A 105.0(9) . . ?
C14 P2 C21 109.1(8) . . ?
C21A P2 Au1 109.7(8) . 2 ?
C21A P2 C15 107.8(9) . . ?
C16 C15 P2 116.6(12) . . ?
C16 C15 C20 119.6(14) . . ?
C20 C15 P2 123.9(12) . . ?
C2 C1 P1 122.5(13) . . ?
C2 C1 C6 119.5(15) . . ?
C6 C1 P1 118.0(12) . . ?
C4 C5 H5 120.4 . . ?
C4 C5 C6 119.2(16) . . ?
C6 C5 H5 120.4 . . ?
P1 C13 B1 116.4(9) . . ?
B9 C13 P1 112.8(11) . . ?
B9 C13 B1 113.0(12) . . ?
B9 C13 B8 112.1(14) . . ?
B9 C13 B7 64.3(10) . . ?
B8 C13 P1 126.2(11) . . ?
B8 C13 B1 69.3(12) . . ?
B8 C13 B7 63.2(12) . . ?
B7 C13 P1 114.1(10) . . ?
B7 C13 B1 124.5(13) . . ?
C2 C3 H3 120.4 . . ?
C4 C3 H3 120.4 . . ?
C4 C3 C2 119.3(16) . . ?
C1 C2 H2 120.1 . . ?
C3 C2 C1 119.7(16) . . ?
C3 C2 H2 120.1 . . ?
C5 C4 C3 121.9(15) . . ?
C5 C4 H4 119.1 . . ?
C3 C4 H4 119.1 . . ?
C1 C6 H6 119.9 . . ?
C5 C6 C1 120.3(16) . . ?
C5 C6 H6 119.9 . . ?
B9 C14 P2 114.6(11) . . ?
B9 C14 B4 109.1(13) . . ?
B9 C14 B6 66.1(11) . . ?
B9 C14 B3 114.6(14) . . ?
B4 C14 P2 119.4(12) . . ?
B6 C14 P2 113.4(11) . . ?
B6 C14 B4 121.8(14) . . ?
B3 C14 P2 122.4(11) . . ?
B3 C14 B4 68.0(12) . . ?
B3 C14 B6 64.1(11) . . ?
C15 C16 H16 120.8 . . ?
C15 C16 C17 118.4(16) . . ?
C17 C16 H16 120.8 . . ?
C16 C17 H17 118.8 . . ?
C18 C17 C16 122.4(18) . . ?
C18 C17 H17 118.8 . . ?
C23A C24A H24A 120.0 . . ?
C23A C24A C25A 120.0 . . ?
C25A C24A H24A 120.0 . . ?
C24A C23A H23A 120.0 . . ?
C24A C23A C22A 120.0 . . ?
C22A C23A H23A 120.0 . . ?
C23A C22A H22A 120.0 . . ?
C21A C22A C23A 120.0 . . ?
C21A C22A H22A 120.0 . . ?
C22A C21A P2 117.1(13) . . ?
C26A C21A P2 122.7(13) . . ?
C26A C21A C22A 120.0 . . ?
C21A C26A H26A 120.0 . . ?
C21A C26A C25A 120.0 . . ?
C25A C26A H26A 120.0 . . ?
C24A C25A H25A 120.0 . . ?
C26A C25A C24A 120.0 . . ?
C26A C25A H25A 120.0 . . ?
C15 C20 H20 120.0 . . ?
C19 C20 C15 120.0(17) . . ?
C19 C20 H20 120.0 . . ?
C17 C18 H18 120.9 . . ?
C17 C18 C19 118.1(16) . . ?
C19 C18 H18 120.9 . . ?
C20 C19 C18 121.3(16) . . ?
C20 C19 H19 119.4 . . ?
C18 C19 H19 119.4 . . ?
C9 C10 H10 120.8 . . ?
C9 C10 C11 118(2) . . ?
C11 C10 H10 120.8 . . ?
C10 C9 H9 119.3 . . ?
C10 C9 C8 121(2) . . ?
C8 C9 H9 119.3 . . ?
C9 C8 H8 120.1 . . ?
C7 C8 C9 120(2) . . ?
C7 C8 H8 120.1 . . ?
C8 C7 P1 122.7(16) . . ?
C12 C7 P1 122.0(17) . . ?
C12 C7 C8 115(2) . . ?
C7 C12 H12 118.1 . . ?
C7 C12 C11 124(2) . . ?
C11 C12 H12 118.1 . . ?
C10 C11 C12 118(2) . . ?
C10 C11 H11 120.8 . . ?
C12 C11 H11 120.8 . . ?
C13 B9 B6 108.5(14) . . ?
C13 B9 B7 59.8(10) . . ?
C13 B9 H9A 117(10) . . ?
C14 B9 C13 113.4(13) . . ?
C14 B9 B6 60.1(10) . . ?
C14 B9 B7 108.5(14) . . ?
C14 B9 H9A 124(10) . . ?
B6 B9 H9A 120(10) . . ?
B7 B9 B6 58.7(11) . . ?
B7 B9 H9A 117(10) . . ?
B6 B5 H5A 121.7 . . ?
B6 B5 B2 108.4(16) . . ?
B6 B5 B7 59.0(10) . . ?
B8 B5 H5A 120.3 . . ?
B8 B5 B6 108.7(15) . . ?
B8 B5 B2 61.1(13) . . ?
B8 B5 B3 110.7(17) . . ?
B8 B5 B7 60.4(11) . . ?
B2 B5 H5A 121.5 . . ?
B3 B5 H5A 120.0 . . ?
B3 B5 B6 61.4(12) . . ?
B3 B5 B2 60.3(13) . . ?
B3 B5 B7 109.1(15) . . ?
B7 B5 H5A 122.0 . . ?
B7 B5 B2 108.2(15) . . ?
C14 B4 B1 107.9(12) . . ?
C14 B4 B2 98.6(15) . . ?
C14 B4 B3 55.6(11) . . ?
C14 B4 H4A 113(2) . . ?
C14 B4 H4B 93(9) . . ?
B1 B4 H4A 132.2(17) . . ?
B1 B4 H4B 28(8) . . ?
B2 B4 B1 59.7(11) . . ?
B2 B4 B3 56.6(12) . . ?
B2 B4 H4A 132.6(19) . . ?
B2 B4 H4B 85(9) . . ?
B3 B4 B1 107.8(14) . . ?
B3 B4 H4A 115.0(17) . . ?
B3 B4 H4B 119(9) . . ?
H4A B4 H4B 126(9) . . ?
C14 B6 B9 53.8(9) . . ?
C14 B6 B5 101.9(14) . . ?
C14 B6 H6A 126.1 . . ?
C14 B6 B3 57.6(11) . . ?
C14 B6 B7 105.0(13) . . ?
B9 B6 H6A 126.8 . . ?
B9 B6 B3 100.1(13) . . ?
B5 B6 B9 102.5(14) . . ?
B5 B6 H6A 124.5 . . ?
B5 B6 B3 58.1(12) . . ?
B3 B6 H6A 124.2 . . ?
B7 B6 B9 60.6(10) . . ?
B7 B6 B5 60.6(11) . . ?
B7 B6 H6A 120.2 . . ?
B7 B6 B3 107.8(15) . . ?
C13 B1 B4 93.3(9) . . ?
C13 B1 B8 51.1(8) . . ?
C13 B1 B2 91.0(9) . . ?
C13 B1 H1 145.2(17) . . ?
C13 B1 H4B 80(9) . . ?
B4 B1 H1 115.9(16) . . ?
B4 B1 H4B 28(8) . . ?
B8 B1 B4 95.8(11) . . ?
B8 B1 H1 135.8(18) . . ?
B8 B1 H4B 106(9) . . ?
B2 B1 B4 54.9(10) . . ?
B2 B1 B8 54.1(10) . . ?
B2 B1 H1 120.7(15) . . ?
B2 B1 H4B 80(8) . . ?
H1 B1 C13 145.2(17) . . ?
H1 B1 B4 115.9(16) . . ?
H1 B1 B8 135.8(18) . . ?
H1 B1 B2 120.7(15) . . ?
H1 B1 H1 0.0 . . ?
H1 B1 H4B 117(9) . . ?
H1 B1 H4B 117(9) . . ?
C13 B8 B5 107.1(16) . . ?
C13 B8 B1 59.7(10) . . ?
C13 B8 H8A 125.4 . . ?
C13 B8 B2 103.3(15) . . ?
C13 B8 B7 60.1(10) . . ?
B5 B8 B1 115.1(15) . . ?
B5 B8 H8A 119.1 . . ?
B5 B8 B2 61.3(13) . . ?
B5 B8 B7 61.3(12) . . ?
B1 B8 H8A 116.8 . . ?
B2 B8 B1 62.0(12) . . ?
B2 B8 H8A 123.1 . . ?
B7 B8 B1 113.5(14) . . ?
B7 B8 H8A 119.4 . . ?
B7 B8 B2 109.1(16) . . ?
B5 B2 B4 109.2(15) . . ?
B5 B2 B1 113.5(13) . . ?
B5 B2 H2A 122.7 . . ?
B4 B2 B1 65.3(12) . . ?
B4 B2 H2A 118.8 . . ?
B1 B2 H2A 113.7 . . ?
B8 B2 B5 57.6(12) . . ?
B8 B2 B4 110.8(14) . . ?
B8 B2 B1 63.8(11) . . ?
B8 B2 H2A 123.0 . . ?
B3 B2 B5 58.1(12) . . ?
B3 B2 B4 62.9(13) . . ?
B3 B2 B1 117.6(15) . . ?
B3 B2 B8 106.0(16) . . ?
B3 B2 H2A 120.2 . . ?
C14 B3 B5 104.2(14) . . ?
C14 B3 B4 56.4(10) . . ?
C14 B3 B6 58.3(10) . . ?
C14 B3 B2 102.4(14) . . ?
C14 B3 H3A 127.0 . . ?
B5 B3 B4 110.0(15) . . ?
B5 B3 B6 60.5(12) . . ?
B5 B3 B2 61.6(13) . . ?
B5 B3 H3A 120.9 . . ?
B4 B3 H3A 121.5 . . ?
B6 B3 B4 107.2(13) . . ?
B6 B3 H3A 121.4 . . ?
B2 B3 B4 60.5(13) . . ?
B2 B3 B6 108.6(14) . . ?
B2 B3 H3A 122.2 . . ?
C13 B7 B9 55.9(9) . . ?
C13 B7 B5 102.1(14) . . ?
C13 B7 B6 107.1(13) . . ?
C13 B7 B8 56.7(10) . . ?
C13 B7 H7 125.1 . . ?
B9 B7 H7 126.2 . . ?
B5 B7 B9 102.4(14) . . ?
B5 B7 H7 124.8 . . ?
B6 B7 B9 60.7(10) . . ?
B6 B7 B5 60.4(11) . . ?
B6 B7 B8 108.2(15) . . ?
B6 B7 H7 119.6 . . ?
B8 B7 B9 100.6(13) . . ?
B8 B7 B5 58.4(12) . . ?
B8 B7 H7 124.4 . . ?
C23 C24 H24 120.0 . . ?
C23 C24 C25 120.0 . . ?
C25 C24 H24 120.0 . . ?
C24 C23 H23 120.0 . . ?
C22 C23 C24 120.0 . . ?
C22 C23 H23 120.0 . . ?
C23 C22 H22 120.0 . . ?
C23 C22 C21 120.0 . . ?
C21 C22 H22 120.0 . . ?
C22 C21 P2 119.7(11) . . ?
C26 C21 P2 120.2(11) . . ?
C26 C21 C22 120.0 . . ?
C21 C26 H26 120.0 . . ?
C21 C26 C25 120.0 . . ?
C25 C26 H26 120.0 . . ?
C24 C25 H25 120.0 . . ?
C26 C25 C24 120.0 . . ?
C26 C25 H25 120.0 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Au1 P1 C1 C2 -175.8(13) . . . . ?
Au1 P1 C1 C6 2.1(14) . . . . ?
Au1 P1 C13 B9 -30.0(12) . . . . ?
Au1 P1 C13 B1 -163.0(10) . . . . ?
Au1 P1 C13 B8 114.4(13) . . . . ?
Au1 P1 C13 B7 40.9(11) . . . . ?
Au1 P1 C7 C8 -111(2) . . . . ?
Au1 P1 C7 C12 73(3) . . . . ?
Au1 P2 C15 C16 39.8(15) 2 . . . ?
Au1 P2 C15 C20 -141.0(13) 2 . . . ?
Au1 P2 C14 B9 36.8(13) 2 . . . ?
Au1 P2 C14 B4 168.9(11) 2 . . . ?
Au1 P2 C14 B6 -36.5(11) 2 . . . ?
Au1 P2 C14 B3 -109.7(12) 2 . . . ?
Au1 P2 C21A C22A 2.4(14) 2 . . . ?
Au1 P2 C21A C26A -172.8(11) 2 . . . ?
Au1 P2 C21 C22 76.9(14) 2 . . . ?
Au1 P2 C21 C26 -99.9(13) 2 . . . ?
P1 C1 C2 C3 -178.3(15) . . . . ?
P1 C1 C6 C5 178.4(13) . . . . ?
P1 C13 B9 C14 -154.6(12) . . . . ?
P1 C13 B9 B6 140.8(11) . . . . ?
P1 C13 B9 B7 106.8(12) . . . . ?
P1 C13 B1 B4 144.1(11) . . . . ?
P1 C13 B1 B8 -121.1(13) . . . . ?
P1 C13 B1 B2 -161.0(11) . . . . ?
P1 C13 B1 H1 -4(4) . . . . ?
P1 C13 B8 B5 -142.3(13) . . . . ?
P1 C13 B8 B1 108.1(13) . . . . ?
P1 C13 B8 B2 154.0(12) . . . . ?
P1 C13 B8 B7 -101.4(14) . . . . ?
P1 C13 B7 B9 -104.8(12) . . . . ?
P1 C13 B7 B5 158.3(11) . . . . ?
P1 C13 B7 B6 -139.3(12) . . . . ?
P1 C13 B7 B8 119.9(13) . . . . ?
P1 C7 C12 C11 175(2) . . . . ?
P2 C15 C16 C17 -178.9(15) . . . . ?
P2 C15 C20 C19 175.7(14) . . . . ?
P2 C14 B9 C13 155.5(12) . . . . ?
P2 C14 B9 B6 -105.9(13) . . . . ?
P2 C14 B9 B7 -140.2(11) . . . . ?
P2 C14 B4 B1 -144.5(12) . . . . ?
P2 C14 B4 B2 154.6(11) . . . . ?
P2 C14 B4 B3 115.8(14) . . . . ?
P2 C14 B6 B9 107.7(12) . . . . ?
P2 C14 B6 B5 -155.4(10) . . . . ?
P2 C14 B6 B3 -116.1(13) . . . . ?
P2 C14 B6 B7 142.1(11) . . . . ?
P2 C14 B3 B5 143.3(13) . . . . ?
P2 C14 B3 B4 -111.8(14) . . . . ?
P2 C14 B3 B6 102.4(13) . . . . ?
P2 C14 B3 B2 -153.2(12) . . . . ?
P2 C21A C26A C25A 175.0(19) . . . . ?
P2 C21 C26 C25 177(2) . . . . ?
C15 P2 C14 B9 161.1(12) . . . . ?
C15 P2 C14 B4 -66.7(14) . . . . ?
C15 P2 C14 B6 87.8(12) . . . . ?
C15 P2 C14 B3 14.6(15) . . . . ?
C15 P2 C21A C22A -117.9(12) . . . . ?
C15 P2 C21A C26A 66.9(15) . . . . ?
C15 P2 C21 C22 -41.0(15) . . . . ?
C15 P2 C21 C26 142.3(14) . . . . ?
C15 C16 C17 C18 0(3) . . . . ?
C15 C20 C19 C18 7(3) . . . . ?
C1 P1 C13 B9 -154.9(11) . . . . ?
C1 P1 C13 B1 72.2(13) . . . . ?
C1 P1 C13 B8 -10.5(16) . . . . ?
C1 P1 C13 B7 -84.0(12) . . . . ?
C1 P1 C7 C8 10(3) . . . . ?
C1 P1 C7 C12 -165(2) . . . . ?
C13 P1 C1 C2 -50.2(16) . . . . ?
C13 P1 C1 C6 127.7(12) . . . . ?
C13 P1 C7 C8 127(2) . . . . ?
C13 P1 C7 C12 -49(3) . . . . ?
C13 B9 B6 C14 106.8(13) . . . . ?
C13 B9 B6 B5 11.1(16) . . . . ?
C13 B9 B6 B3 70.4(15) . . . . ?
C13 B9 B6 B7 -34.4(12) . . . . ?
C13 B9 B7 B5 96.4(13) . . . . ?
C13 B9 B7 B6 141.7(14) . . . . ?
C13 B9 B7 B8 36.7(11) . . . . ?
C13 B8 B2 B5 102.4(16) . . . . ?
C13 B8 B2 B4 2(2) . . . . ?
C13 B8 B2 B1 -44.6(12) . . . . ?
C13 B8 B2 B3 68.8(18) . . . . ?
C13 B8 B7 B9 -36.4(11) . . . . ?
C13 B8 B7 B5 -134.5(15) . . . . ?
C13 B8 B7 B6 -98.8(13) . . . . ?
C2 C1 C6 C5 -4(2) . . . . ?
C2 C3 C4 C5 3(3) . . . . ?
C4 C5 C6 C1 3(3) . . . . ?
C4 C3 C2 C1 -3(3) . . . . ?
C6 C1 C2 C3 4(3) . . . . ?
C6 C5 C4 C3 -3(3) . . . . ?
C14 P2 C15 C16 -85.5(15) . . . . ?
C14 P2 C15 C20 93.7(15) . . . . ?
C14 P2 C21A C22A 123.0(12) . . . . ?
C14 P2 C21A C26A -52.1(15) . . . . ?
C14 P2 C21 C22 -159.5(12) . . . . ?
C14 P2 C21 C26 23.8(16) . . . . ?
C14 B9 B6 B5 -95.8(14) . . . . ?
C14 B9 B6 B3 -36.4(12) . . . . ?
C14 B9 B6 B7 -141.2(14) . . . . ?
C14 B9 B7 C13 -106.8(14) . . . . ?
C14 B9 B7 B5 -10.4(16) . . . . ?
C14 B9 B7 B6 34.9(13) . . . . ?
C14 B9 B7 B8 -70.1(15) . . . . ?
C14 B4 B2 B5 -2.0(17) . . . . ?
C14 B4 B2 B1 105.7(12) . . . . ?
C14 B4 B2 B8 59.6(18) . . . . ?
C14 B4 B2 B3 -38.2(12) . . . . ?
C14 B4 B3 B5 94.1(15) . . . . ?
C14 B4 B3 B6 30.0(12) . . . . ?
C14 B4 B3 B2 132.1(14) . . . . ?
C14 B6 B3 B5 -133.0(15) . . . . ?
C14 B6 B3 B4 -29.3(12) . . . . ?
C14 B6 B3 B2 -93.3(16) . . . . ?
C14 B6 B7 C13 0.9(17) . . . . ?
C14 B6 B7 B9 -31.6(11) . . . . ?
C14 B6 B7 B5 95.4(15) . . . . ?
C14 B6 B7 B8 60.6(16) . . . . ?
C16 C15 C20 C19 -5(3) . . . . ?
C16 C17 C18 C19 2(3) . . . . ?
C17 C18 C19 C20 -5(3) . . . . ?
C24A C23A C22A C21A 0.0 . . . . ?
C23A C24A C25A C26A 0.0 . . . . ?
C23A C22A C21A P2 -175.3(18) . . . . ?
C23A C22A C21A C26A 0.0 . . . . ?
C22A C21A C26A C25A 0.0 . . . . ?
C21A P2 C15 C16 159.6(15) . . . . ?
C21A P2 C15 C20 -21.1(18) . . . . ?
C21A P2 C14 B9 -82.3(14) . . . . ?
C21A P2 C14 B4 49.8(15) . . . . ?
C21A P2 C14 B6 -155.6(12) . . . . ?
C21A P2 C14 B3 131.2(15) . . . . ?
C21A C26A C25A C24A 0.0 . . . . ?
C25A C24A C23A C22A 0.0 . . . . ?
C20 C15 C16 C17 2(3) . . . . ?
C10 C9 C8 C7 -9(4) . . . . ?
C9 C10 C11 C12 -20(4) . . . . ?
C9 C8 C7 P1 -176(2) . . . . ?
C9 C8 C7 C12 -1(4) . . . . ?
C8 C7 C12 C11 -1(4) . . . . ?
C7 P1 C1 C2 63.2(17) . . . . ?
C7 P1 C1 C6 -118.8(15) . . . . ?
C7 P1 C13 B9 90.3(13) . . . . ?
C7 P1 C13 B1 -42.6(14) . . . . ?
C7 P1 C13 B8 -125.3(15) . . . . ?
C7 P1 C13 B7 161.2(12) . . . . ?
C7 C12 C11 C10 11(4) . . . . ?
C11 C10 C9 C8 19(4) . . . . ?
B9 C13 B1 B4 11.2(16) . . . . ?
B9 C13 B1 B8 106.0(15) . . . . ?
B9 C13 B1 B2 66.2(16) . . . . ?
B9 C13 B1 H1 -137(3) . . . . ?
B9 C13 B8 B5 2.3(19) . . . . ?
B9 C13 B8 B1 -107.3(13) . . . . ?
B9 C13 B8 B2 -61.4(17) . . . . ?
B9 C13 B8 B7 43.2(13) . . . . ?
B9 C13 B7 B5 -96.9(14) . . . . ?
B9 C13 B7 B6 -34.4(12) . . . . ?
B9 C13 B7 B8 -135.3(14) . . . . ?
B9 C14 B4 B1 -10.0(19) . . . . ?
B9 C14 B4 B2 -70.9(16) . . . . ?
B9 C14 B4 B3 -109.6(15) . . . . ?
B9 C14 B6 B5 96.8(13) . . . . ?
B9 C14 B6 B3 136.2(14) . . . . ?
B9 C14 B6 B7 34.4(13) . . . . ?
B9 C14 B3 B5 -3.1(19) . . . . ?
B9 C14 B3 B4 101.7(15) . . . . ?
B9 C14 B3 B6 -44.1(14) . . . . ?
B9 C14 B3 B2 60.3(18) . . . . ?
B9 B6 B3 C14 34.6(11) . . . . ?
B9 B6 B3 B5 -98.5(14) . . . . ?
B9 B6 B3 B4 5.2(17) . . . . ?
B9 B6 B3 B2 -58.7(17) . . . . ?
B9 B6 B7 C13 32.5(12) . . . . ?
B9 B6 B7 B5 127.0(15) . . . . ?
B9 B6 B7 B8 92.2(14) . . . . ?
B5 B6 B3 C14 133.0(15) . . . . ?
B5 B6 B3 B4 103.7(16) . . . . ?
B5 B6 B3 B2 39.7(15) . . . . ?
B5 B6 B7 C13 -94.5(15) . . . . ?
B5 B6 B7 B9 -127.0(15) . . . . ?
B5 B6 B7 B8 -34.8(14) . . . . ?
B5 B8 B2 B4 -100.1(17) . . . . ?
B5 B8 B2 B1 -146.9(15) . . . . ?
B5 B8 B2 B3 -33.6(15) . . . . ?
B5 B8 B7 C13 134.5(15) . . . . ?
B5 B8 B7 B9 98.1(15) . . . . ?
B5 B8 B7 B6 35.6(14) . . . . ?
B5 B2 B3 C14 -99.7(15) . . . . ?
B5 B2 B3 B4 -138.9(14) . . . . ?
B5 B2 B3 B6 -39.2(14) . . . . ?
B4 C14 B9 C13 19(2) . . . . ?
B4 C14 B9 B6 117.2(15) . . . . ?
B4 C14 B9 B7 82.8(16) . . . . ?
B4 C14 B6 B9 -98.4(15) . . . . ?
B4 C14 B6 B5 -1.5(18) . . . . ?
B4 C14 B6 B3 37.8(15) . . . . ?
B4 C14 B6 B7 -64.0(18) . . . . ?
B4 C14 B3 B5 -104.8(16) . . . . ?
B4 C14 B3 B6 -145.8(14) . . . . ?
B4 C14 B3 B2 -41.4(14) . . . . ?
B4 B2 B3 C14 39.2(12) . . . . ?
B4 B2 B3 B5 138.9(14) . . . . ?
B4 B2 B3 B6 99.7(15) . . . . ?
B6 C14 B9 C13 -98.6(16) . . . . ?
B6 C14 B9 B7 -34.3(12) . . . . ?
B6 C14 B4 B1 63.2(18) . . . . ?
B6 C14 B4 B2 2.3(18) . . . . ?
B6 C14 B4 B3 -36.5(14) . . . . ?
B6 C14 B3 B5 41.0(14) . . . . ?
B6 C14 B3 B4 145.8(14) . . . . ?
B6 C14 B3 B2 104.4(15) . . . . ?
B6 B9 B7 C13 -141.7(14) . . . . ?
B6 B9 B7 B5 -45.3(13) . . . . ?
B6 B9 B7 B8 -105.0(15) . . . . ?
B6 B5 B8 C13 5(2) . . . . ?
B6 B5 B8 B1 69.1(18) . . . . ?
B6 B5 B8 B2 101.2(17) . . . . ?
B6 B5 B8 B7 -35.2(14) . . . . ?
B6 B5 B2 B4 1.4(19) . . . . ?
B6 B5 B2 B1 -69.3(18) . . . . ?
B6 B5 B2 B8 -101.6(16) . . . . ?
B6 B5 B2 B3 39.6(13) . . . . ?
B6 B5 B3 C14 -39.9(13) . . . . ?
B6 B5 B3 B4 -98.9(15) . . . . ?
B6 B5 B3 B2 -136.5(15) . . . . ?
B6 B5 B7 C13 102.9(13) . . . . ?
B6 B5 B7 B9 45.5(12) . . . . ?
B6 B5 B7 B8 140.5(16) . . . . ?
B1 C13 B9 C14 -20.1(19) . . . . ?
B1 C13 B9 B6 -84.7(15) . . . . ?
B1 C13 B9 B7 -118.6(14) . . . . ?
B1 C13 B8 B5 109.5(15) . . . . ?
B1 C13 B8 B2 45.9(13) . . . . ?
B1 C13 B8 B7 150.4(13) . . . . ?
B1 C13 B7 B9 101.2(15) . . . . ?
B1 C13 B7 B5 4.3(18) . . . . ?
B1 C13 B7 B6 66.8(18) . . . . ?
B1 C13 B7 B8 -34.1(15) . . . . ?
B1 B4 B2 B5 -107.7(14) . . . . ?
B1 B4 B2 B8 -46.1(13) . . . . ?
B1 B4 B2 B3 -144.0(13) . . . . ?
B1 B4 B3 C14 -99.9(13) . . . . ?
B1 B4 B3 B5 -5.7(18) . . . . ?
B1 B4 B3 B6 -69.8(16) . . . . ?
B1 B4 B3 B2 32.3(12) . . . . ?
B1 B8 B2 B5 146.9(15) . . . . ?
B1 B8 B2 B4 46.9(14) . . . . ?
B1 B8 B2 B3 113.4(16) . . . . ?
B1 B8 B7 C13 27.7(12) . . . . ?
B1 B8 B7 B9 -8.7(17) . . . . ?
B1 B8 B7 B5 -106.8(16) . . . . ?
B1 B8 B7 B6 -71.2(17) . . . . ?
B1 B2 B3 C14 2(2) . . . . ?
B1 B2 B3 B5 101.8(17) . . . . ?
B1 B2 B3 B4 -37.1(14) . . . . ?
B1 B2 B3 B6 63(2) . . . . ?
B8 C13 B9 C14 55.9(18) . . . . ?
B8 C13 B9 B6 -8.7(17) . . . . ?
B8 C13 B9 B7 -42.7(14) . . . . ?
B8 C13 B1 B4 -94.8(13) . . . . ?
B8 C13 B1 B2 -39.9(12) . . . . ?
B8 C13 B1 H1 117(3) . . . . ?
B8 C13 B7 B9 135.3(14) . . . . ?
B8 C13 B7 B5 38.4(13) . . . . ?
B8 C13 B7 B6 100.8(16) . . . . ?
B8 B5 B6 C14 -64.9(17) . . . . ?
B8 B5 B6 B9 -9.7(18) . . . . ?
B8 B5 B6 B3 -104.0(18) . . . . ?
B8 B5 B6 B7 35.7(14) . . . . ?
B8 B5 B2 B4 103.0(16) . . . . ?
B8 B5 B2 B1 32.3(15) . . . . ?
B8 B5 B2 B3 141.2(16) . . . . ?
B8 B5 B3 C14 60.7(18) . . . . ?
B8 B5 B3 B4 2(2) . . . . ?
B8 B5 B3 B6 100.6(16) . . . . ?
B8 B5 B3 B2 -35.9(14) . . . . ?
B8 B5 B7 C13 -37.6(13) . . . . ?
B8 B5 B7 B9 -94.9(14) . . . . ?
B8 B5 B7 B6 -140.5(16) . . . . ?
B8 B2 B3 C14 -66.3(18) . . . . ?
B8 B2 B3 B5 33.4(14) . . . . ?
B8 B2 B3 B4 -105.5(16) . . . . ?
B8 B2 B3 B6 -6(2) . . . . ?
B2 B5 B6 C14 0.0(17) . . . . ?
B2 B5 B6 B9 55.1(16) . . . . ?
B2 B5 B6 B3 -39.1(14) . . . . ?
B2 B5 B6 B7 100.6(15) . . . . ?
B2 B5 B8 C13 -96.1(16) . . . . ?
B2 B5 B8 B1 -32.1(14) . . . . ?
B2 B5 B8 B7 -136.4(15) . . . . ?
B2 B5 B3 C14 96.6(15) . . . . ?
B2 B5 B3 B4 37.5(14) . . . . ?
B2 B5 B3 B6 136.5(15) . . . . ?
B2 B5 B7 C13 1.9(17) . . . . ?
B2 B5 B7 B9 -55.5(17) . . . . ?
B2 B5 B7 B6 -101.0(16) . . . . ?
B2 B5 B7 B8 39.5(14) . . . . ?
B2 B4 B3 C14 -132.1(14) . . . . ?
B2 B4 B3 B5 -38.0(14) . . . . ?
B2 B4 B3 B6 -102.1(16) . . . . ?
B2 B8 B7 C13 94.7(16) . . . . ?
B2 B8 B7 B9 58.3(17) . . . . ?
B2 B8 B7 B5 -39.8(15) . . . . ?
B2 B8 B7 B6 -4.2(19) . . . . ?
B3 C14 B9 C13 -55.4(19) . . . . ?
B3 C14 B9 B6 43.3(14) . . . . ?
B3 C14 B9 B7 8.9(18) . . . . ?
B3 C14 B4 B1 99.7(15) . . . . ?
B3 C14 B4 B2 38.8(13) . . . . ?
B3 C14 B6 B9 -136.2(14) . . . . ?
B3 C14 B6 B5 -39.4(13) . . . . ?
B3 C14 B6 B7 -101.8(15) . . . . ?
B3 B5 B6 C14 39.1(13) . . . . ?
B3 B5 B6 B9 94.3(14) . . . . ?
B3 B5 B6 B7 139.7(15) . . . . ?
B3 B5 B8 C13 -60.5(18) . . . . ?
B3 B5 B8 B1 3(2) . . . . ?
B3 B5 B8 B2 35.6(14) . . . . ?
B3 B5 B8 B7 -100.8(16) . . . . ?
B3 B5 B2 B4 -38.3(14) . . . . ?
B3 B5 B2 B1 -109.0(17) . . . . ?
B3 B5 B2 B8 -141.2(16) . . . . ?
B3 B5 B7 C13 66.0(17) . . . . ?
B3 B5 B7 B9 8.6(18) . . . . ?
B3 B5 B7 B6 -36.9(14) . . . . ?
B3 B5 B7 B8 103.5(18) . . . . ?
B3 B4 B2 B5 36.2(13) . . . . ?
B3 B4 B2 B1 144.0(13) . . . . ?
B3 B4 B2 B8 97.8(17) . . . . ?
B3 B6 B7 C13 -59.3(17) . . . . ?
B3 B6 B7 B9 -91.8(14) . . . . ?
B3 B6 B7 B5 35.2(14) . . . . ?
B3 B6 B7 B8 0.4(18) . . . . ?
B7 C13 B9 C14 98.5(16) . . . . ?
B7 C13 B9 B6 33.9(13) . . . . ?
B7 C13 B1 B4 -62.5(17) . . . . ?
B7 C13 B1 B8 32.3(14) . . . . ?
B7 C13 B1 B2 -7.5(18) . . . . ?
B7 C13 B1 H1 149(3) . . . . ?
B7 C13 B8 B5 -40.9(14) . . . . ?
B7 C13 B8 B1 -150.4(13) . . . . ?
B7 C13 B8 B2 -104.5(16) . . . . ?
B7 B9 B6 C14 141.2(14) . . . . ?
B7 B9 B6 B5 45.5(13) . . . . ?
B7 B9 B6 B3 104.8(14) . . . . ?
B7 B5 B6 C14 -100.6(13) . . . . ?
B7 B5 B6 B9 -45.5(12) . . . . ?
B7 B5 B6 B3 -139.7(15) . . . . ?
B7 B5 B8 C13 40.3(13) . . . . ?
B7 B5 B8 B1 104.3(16) . . . . ?
B7 B5 B8 B2 136.4(15) . . . . ?
B7 B5 B2 B4 63.9(18) . . . . ?
B7 B5 B2 B1 -7(2) . . . . ?
B7 B5 B2 B8 -39.1(14) . . . . ?
B7 B5 B2 B3 102.1(16) . . . . ?
B7 B5 B3 C14 -4.0(19) . . . . ?
B7 B5 B3 B4 -63.0(18) . . . . ?
B7 B5 B3 B6 35.9(13) . . . . ?
B7 B5 B3 B2 -100.5(16) . . . . ?
B7 B6 B3 C14 96.8(13) . . . . ?
B7 B6 B3 B5 -36.3(14) . . . . ?
B7 B6 B3 B4 67.5(17) . . . . ?
B7 B6 B3 B2 3.5(19) . . . . ?
B7 B8 B2 B5 39.8(14) . . . . ?
B7 B8 B2 B4 -60(2) . . . . ?
B7 B8 B2 B1 -107.2(15) . . . . ?
B7 B8 B2 B3 6(2) . . . . ?
C24 C23 C22 C21 0.0 . . . . ?
C23 C24 C25 C26 0.0 . . . . ?
C23 C22 C21 P2 -176.8(19) . . . . ?
C23 C22 C21 C26 0.0 . . . . ?
C22 C21 C26 C25 0.0 . . . . ?
C21 P2 C15 C16 157.7(15) . . . . ?
C21 P2 C15 C20 -23.1(17) . . . . ?
C21 P2 C14 B9 -85.9(15) . . . . ?
C21 P2 C14 B4 46.2(16) . . . . ?
C21 P2 C14 B6 -159.2(13) . . . . ?
C21 P2 C14 B3 127.6(15) . . . . ?
C21 C26 C25 C24 0.0 . . . . ?
C25 C24 C23 C22 0.0 . . . . ?

_smtbx_masks_special_details     ?
loop_
_smtbx_masks_void_nr
_smtbx_masks_void_average_x
_smtbx_masks_void_average_y
_smtbx_masks_void_average_z
_smtbx_masks_void_volume
_smtbx_masks_void_count_electrons
_smtbx_masks_void_content
1 0.000 0.310 0.250 114.9 30.6 ?
2 0.000 0.690 0.750 114.9 27.8 ?
3 0.250 0.250 0.000 157.3 14.3 ?
4 0.250 0.750 0.500 157.3 14.3 ?
5 0.500 0.190 0.750 114.9 27.8 ?
6 0.500 0.810 0.250 114.9 30.6 ?
7 0.750 0.250 0.500 157.3 14.3 ?
8 0.750 0.750 0.000 157.3 14.3 ?

_smtbx_masks_void_probe_radius   1.2
_smtbx_masks_void_truncation_radius 1.2
_olex2_submission_special_instructions 'No special instructions were received'
