# Copyright The Royal Society of Chemistry, 1998 data_erampj _audit_creation_date 97-09-25 _audit_creation_method from_xtal_archive_file_using_CIFIO _audit_update_record ? _chemical_compound_source ? #ActaC _chemical_name_systematic ? #ActaC _chemical_name_common ? #ActaC _chemical_formula_analytical ? #ActaC _chemical_formula_moiety ? #ActaC _chemical_formula_structural ? #ActaC _chemical_formula_sum C10.5_H28.5_Er.5_N3_Si1.5 #ActaC _chemical_formula_weight 322.62 #ActaC _chemical_melting_point ? #ActaC _computing_data_collection ? #ActaC _computing_cell_refinement ? #ActaC _computing_data_reduction xtal #ActaC _computing_structure_solution xtal #ActaC _computing_structure_refinement xtal_CRYLSQ #ActaC _computing_molecular_graphics xtal #ActaC _computing_publication_material xtal_BONDLA_CIFIO #ActaC _cell_length_a 19.075(12) #ActaC _cell_length_b 16.946(9) #ActaC _cell_length_c 10.156(4) #ActaC _cell_angle_alpha 90.00000 #ActaC _cell_angle_beta 90.00000 #ActaC _cell_angle_gamma 90.00000 #ActaC _cell_volume 3283(3) #ActaC _cell_formula_units_Z 8 #ActaC _cell_measurement_temperature 293 #ActaC _cell_measurement_reflns_used ? #ActaC _cell_measurement_theta_min ? #ActaC _cell_measurement_theta_max ? #ActaC _cell_special_details #ActaC ; ? ; _symmetry_cell_setting orthorhombic #ActaC _symmetry_space_group_name_H-M p_n_m_a #ActaC _symmetry_space_group_name_Hall -p_2ac_2n #ActaC loop_ _symmetry_equiv_pos_as_xyz #ActaC +x,+y,+z 1/2-x,-y,1/2+z 1/2+x,1/2-y,1/2-z -x,1/2+y,-z -x,-y,-z 1/2+x,+y,1/2-z 1/2-x,1/2+y,1/2+z +x,1/2-y,+z _exptl_crystal_description ? #ActaC _exptl_crystal_preparation ? _exptl_crystal_colour ? #ActaC _exptl_crystal_size_max ? #ActaC _exptl_crystal_size_mid ? #ActaC _exptl_crystal_size_min ? #ActaC _exptl_crystal_density_diffrn 1.305 #ActaC _exptl_crystal_density_meas ? #ActaC _exptl_crystal_density_method ? #ActaC _exptl_crystal_F_000 1340 #ActaC _exptl_absorpt_process_details ? _exptl_absorpt_coefficient_mu '26.8 cm-1' #ActaC _exptl_absorpt_correction_type gaussian #ActaC _exptl_absorpt_correction_T_min 2.036 #ActaC _exptl_absorpt_correction_T_max 2.287 #ActaC _exptl_special_details #ActaC ; ? ; _diffrn_special_details ; ? ; _diffrn_ambient_temperature 293 #ActaC _diffrn_radiation_wavelength 0.71073 #ActaC _diffrn_radiation_type xray_tube #ActaC _diffrn_radiation_source ? #ActaC _diffrn_radiation_monochromator graphite #ActaC _diffrn_radiation_detector ? #ActaC _diffrn_measurement_device CAD4 #ActaC _diffrn_measurement_method ? #ActaC _diffrn_standards_number ? #ActaC _diffrn_standards_interval_count ? #ActaC _diffrn_standards_interval_time ? #ActaC _diffrn_standards_decay_% ? #ActaC loop_ _diffrn_standard_refln_index_h #ActaC _diffrn_standard_refln_index_k #ActaC _diffrn_standard_refln_index_l #ActaC ? ? ? loop_ _diffrn_attenuator_code _diffrn_attenuator_scale ? ? _diffrn_reflns_number 7853 #ActaC _diffrn_reflns_av_R_equivalents .064 #ActaC _diffrn_reflns_av_sigmaI/netI .059 #ActaC _diffrn_reflns_limit_h_min -24 #ActaC _diffrn_reflns_limit_h_max 24 #ActaC _diffrn_reflns_limit_k_min -21 #ActaC _diffrn_reflns_limit_k_max 0 #ActaC _diffrn_reflns_limit_l_min -13 #ActaC _diffrn_reflns_limit_l_max 0 #ActaC _diffrn_reflns_theta_min 2.14 #ActaC _diffrn_reflns_theta_max 27.47 #ActaC _diffrn_reflns_reduction_process equatorial_monochr_Lp #ActaC loop_ _atom_type_symbol #ActaC _atom_type_description #ActaC _atom_type_oxidation_number _atom_type_number_in_cell _atom_type_scat_dispersion_real #ActaC _atom_type_scat_dispersion_imag #ActaC _atom_type_scat_source #ActaC C ? 0 84 .002 .002 Int_Tables_Vol_IV_Tables_2.2B_and_2.3.1 O ? 0 0 .008 .006 Int_Tables_Vol_IV_Tables_2.2B_and_2.3.1 H ? 0 228 0 0 Int_Tables_Vol_IV_Tables_2.2B_and_2.3.1 Er ? 0 4 -.723 4.958 Int_Tables_Vol_IV_Tables_2.2B_and_2.3.1 N ? 0 24 .004 .003 Int_Tables_Vol_IV_Tables_2.2B_and_2.3.1 Si ? 0 12 .072 .071 Int_Tables_Vol_IV_Tables_2.2B_and_2.3.1 loop_ _atom_site_label #ActaC _atom_site_fract_x #ActaC _atom_site_fract_y #ActaC _atom_site_fract_z #ActaC _atom_site_U_iso_or_equiv #ActaC _atom_site_thermal_displace_type #ActaC _atom_site_calc_flag #ActaC _atom_site_calc_attached_atom #ActaC Er .39974(2) .25000 .64976(4) .0522(3) Uani ? ? N11 .3155(7) .3388(8) .6111(12) .068(8) Uani ? ? Si1 .2978(3) .4024(3) .4916(5) .084(3) Uani ? ? C111 .2070(14) .417(2) .440(4) .21(3) Uani ? ? C112 .3248(15) .5027(15) .527(3) .15(2) Uani ? ? C113 .348(2) .374(3) .339(2) .21(3) Uani ? ? C11 .2640(11) .3455(18) .724(2) .13(2) Uani ? ? C12 .2765(15) .3203(13) .865(2) .15(2) Uani ? ? N12 .3178(7) .25000 .8632(9) .094(8) Uani ? ? C121 .2661(15) .198(2) .824(2) .23(4) Uani ? ? C122 .3348(14) .229(4) .9889(17) .19(4) Uani ? ? N21 .4896(7) .2801(9) .5161(11) .080(10) Uani ? ? Si2 .5236(2) .261(2) .3743(4) .073(7) Uani ? ? C211 .6171(11) .216(4) .397(2) .21(5) Uani ? ? C212 .4704(13) .1718(19) .294(2) .14(2) Uani ? ? C213 .5328(12) .3204(18) .242(2) .15(2) Uani ? ? C21 .5261(14) .355(2) .556(2) .16(2) Uani ? ? C22 .4826(14) .4114(16) .648(2) .12(2) Uani ? ? N22 .4736(11) .3733(11) .7724(18) .122(15) Uani ? ? C221 .448(2) .418(2) .871(3) .21(3) Uani ? ? C222 .5514(15) .343(3) .807(4) .23(4) Uani ? ? N31 .3588(7) .1338(8) .5738(13) .075(9) Uani ? ? Si3 .2899(4) .1086(4) .4765(7) .120(5) Uani ? ? C311 .307(3) .054(4) .331(3) .37(7) Uani ? ? C312 .234(3) .034(4) .560(5) .39(7) Uani ? ? C313 .222(2) .184(3) .456(5) .31(3) Uiso ? ? C31 .3985(15) .0622(17) .622(3) .16(3) Uani ? ? C32 .4402(16) .0708(16) .778(3) .15(2) Uani ? ? N32 .4813(8) .1457(10) .7746(13) .091(11) Uani ? ? C321 .5065(15) .151(2) .910(2) .15(2) Uani ? ? C322 .5459(12) .138(2) .704(3) .15(2) Uani ? ? H111a .18732 .36857 .41863 .22000 Uiso ? ? H111b .18183 .43561 .52212 .22000 Uiso ? ? H111c .19567 .45485 .37730 .22000 Uiso ? ? H112a .30094 .51770 .60707 .21000 Uiso ? ? H112b .37367 .50123 .54449 .21000 Uiso ? ? H112c .31447 .53798 .46127 .21000 Uiso ? ? H113a .39478 .37065 .34211 .24000 Uiso ? ? H113b .33014 .32086 .30100 .24000 Uiso ? ? H113c .33558 .40851 .25900 .24000 Uiso ? ? H11a .24651 .40002 .71889 .13000 Uiso ? ? H11b .22256 .31362 .69602 .13000 Uiso ? ? H12a .31606 .36302 .89782 .12000 Uiso ? ? H12b .24447 .32181 .92069 .12000 Uiso ? ? H121a .21743 .19289 .87821 .17500 Uiso ? ? H121b .23762 .20654 .73201 .17500 Uiso ? ? H121c .27737 .14233 .81447 .17500 Uiso ? ? H122a .37045 .26628 1.02606 .19000 Uiso ? ? H122b .29873 .22502 1.04726 .19000 Uiso ? ? H122c .36144 .17793 .99019 .19000 Uiso ? ? H211a .64596 .26345 .44440 .22000 Uiso ? ? H211b .61874 .17733 .45248 .22000 Uiso ? ? H211c .63854 .21347 .31661 .22000 Uiso ? ? H212a .47289 .12373 .34762 .16500 Uiso ? ? H212b .42076 .18291 .28445 .16500 Uiso ? ? H212c .48822 .15841 .20877 .16500 Uiso ? ? H213a .48864 .34157 .22489 .17000 Uiso ? ? H213b .56233 .36476 .27668 .17000 Uiso ? ? H213c .55397 .31216 .15892 .17000 Uiso ? ? H21a .56908 .34406 .59658 .16000 Uiso ? ? H21b .53485 .38486 .47590 .16000 Uiso ? ? H22a .50798 .45776 .66089 .15000 Uiso ? ? H22b .43902 .42071 .60860 .15000 Uiso ? ? H221a .48524 .45324 .89397 .24000 Uiso ? ? H221b .40765 .43730 .85669 .24000 Uiso ? ? H221c .44395 .38853 .96123 .24000 Uiso ? ? H222a .56884 .29917 .74443 .27000 Uiso ? ? H222b .58723 .37746 .81564 .27000 Uiso ? ? H222c .54626 .31161 .89073 .27000 Uiso ? ? H311a .33803 .08723 .27704 .40000 Uiso ? ? H311b .33060 .00815 .35271 .40000 Uiso ? ? H311c .26897 .04141 .27399 .40000 Uiso ? ? H312a .24962 -.00737 .58519 .36000 Uiso ? ? H312b .20768 .06456 .63734 .36000 Uiso ? ? H312c .18699 .02524 .50593 .36000 Uiso ? ? H313a .20744 .19391 .53454 .34000 Uiso ? ? H313b .24800 .22446 .41235 .34000 Uiso ? ? H313c .18750 .16575 .39612 .34000 Uiso ? ? H31a .36655 .01879 .61495 .13000 Uiso ? ? H31b .43512 .05441 .55828 .13000 Uiso ? ? H32a .40104 .06265 .84793 .15000 Uiso ? ? H32b .46587 .01781 .79403 .15000 Uiso ? ? H321a .47156 .15294 .96917 .21000 Uiso ? ? H321b .53786 .10721 .92441 .21000 Uiso ? ? H321c .53392 .19875 .90410 .21000 Uiso ? ? H322a .57297 .09688 .75476 .18000 Uiso ? ? H322b .53699 .11973 .62319 .18000 Uiso ? ? H322c .57184 .18406 .70933 .18000 Uiso ? ? loop_ _atom_site_aniso_label #ActaC _atom_site_aniso_U_11 #ActaC _atom_site_aniso_U_22 #ActaC _atom_site_aniso_U_33 #ActaC _atom_site_aniso_U_12 #ActaC _atom_site_aniso_U_13 #ActaC _atom_site_aniso_U_23 #ActaC Er .0548(3) .0569(3) .0449(3) .00118 -.0008(2) .00182 N11 .075(8) .052(7) .076(7) .010(7) .005(7) .012(7) Si1 .084(3) .080(3) .089(3) .015(3) .004(3) .022(3) C111 .12(2) .19(3) .32(4) .04(2) -.04(3) .15(3) C112 .17(3) .086(16) .20(3) .01(2) .01(2) .048(19) C113 .25(4) .29(5) .078(15) .19(4) .031(17) .04(2) C11 .092(14) .17(3) .127(17) .075(17) .040(14) .031(19) C12 .19(3) .061(13) .20(3) .029(18) .10(2) -.026(16) N12 .096(8) .105(9) .080(7) .00000 .015(6) .00000 C121 .17(2) .37(8) .134(18) -.09(3) .089(17) -.14(3) C122 .22(3) .28(8) .071(10) .14(5) .041(13) .06(3) N21 .064(7) .116(16) .059(6) -.008(8) .004(5) .008(7) Si2 .077(2) .079(18) .063(2) -.005(4) .0132(16) -.004(4) C211 .097(15) .42(12) .126(16) .13(4) -.045(14) .02(3) C212 .16(2) .21(3) .065(11) -.01(2) -.012(13) -.048(16) C213 .14(2) .23(3) .080(12) .03(3) .047(13) .048(18) C21 .18(3) .21(3) .088(14) -.12(3) .034(15) -.045(18) C22 .13(2) .12(2) .122(18) -.068(18) -.001(14) -.009(15) N22 .165(19) .090(12) .111(13) .035(14) .024(13) .007(12) C221 .23(4) .23(4) .15(2) -.10(4) .08(2) -.13(3) C222 .10(2) .32(5) .26(4) .01(3) -.06(2) -.12(4) N31 .073(9) .058(8) .094(9) .015(8) .007(8) .006(8) Si3 .141(6) .086(4) .133(5) -.029(4) -.046(5) -.019(4) C311 .40(7) .52(10) .19(3) -.21(8) -.00(4) -.22(5) C312 .36(6) .45(9) .36(6) -.31(7) -.11(6) .10(7) C31 .19(4) .067(14) .22(3) .018(18) -.00(2) -.03(2) C32 .17(2) .11(2) .18(3) .05(2) -.02(2) .02(2) N32 .092(10) .108(13) .075(9) .044(10) -.017(8) .040(9) C321 .15(2) .18(3) .126(17) -.00(3) -.03(2) .02(2) C322 .094(15) .22(3) .143(18) .09(2) .023(16) .05(2) _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens ? _refine_special_details sfls__F_____calc_weight_atomblock_matrix _refine_ls_structure_factor_coef F #ActaC _refine_ls_matrix_type atomblock #ActaC _refine_ls_weighting_scheme calc #ActaC _refine_ls_hydrogen_treatment ? #ActaC _refine_ls_extinction_method Zachariasen #ActaC _refine_ls_extinction_coef 1052(481) #ActaC _refine_ls_extinction_expression Eq22_p292_"Cryst._Comp."_Munksgaard_1970 _refine_ls_abs_structure_details none #ActaC _refine_ls_abs_structure_Flack 0 #ActaC _refine_ls_number_reflns 2355 #ActaC _refine_ls_number_parameters 271 #ActaC _refine_ls_number_restraints 0 #ActaC _refine_ls_number_constraints 0 #ActaC _refine_ls_R_factor_all .088 #ActaC _refine_ls_R_factor_obs .058 #ActaC _refine_ls_wR_factor_all .073 #ActaC _refine_ls_wR_factor_obs .065 #ActaC _refine_ls_goodness_of_fit_all 1.492 #ActaC _refine_ls_goodness_of_fit_obs 1.732 #ActaC _refine_ls_shift/esd_max .184 #ActaC _refine_ls_shift/esd_mean .012 #ActaC _refine_diff_density_min -5.661 #ActaC _refine_diff_density_max 1.568 #ActaC _geom_special_details ? #ActaC loop_ _geom_bond_atom_site_label_1 #ActaC _geom_bond_atom_site_label_2 #ActaC _geom_bond_distance #ActaC _geom_bond_site_symmetry_1 #ActaC _geom_bond_site_symmetry_2 #ActaC _geom_bond_publ_flag #ActaC Er N11 2.237(13) . . ? Er N12 2.673(11) . . ? Er N21 2.245(12) . . ? Er N22 2.81(2) . . ? Er N31 2.255(14) . . ? Er N32 2.675(15) . . ? Er N11 2.237(13) . 8 ? Er N21 2.245(12) . 8 ? Er N22 2.81(2) . 8 ? Er N31 2.255(14) . 8 ? Er N32 2.675(15) . 8 ? N11 Si1 1.657(14) . . ? N11 C11 1.51(3) . . ? N11 N31 1.02(2) . 8 ? N11 Si3 1.703(15) . 8 ? Si1 C111 1.83(3) . . ? Si1 C112 1.81(3) . . ? Si1 C113 1.88(3) . . ? Si1 N31 1.557(15) . 8 ? Si1 Si3 .285(9) . 8 ? Si1 C311 1.80(4) . 8 ? Si1 C312 1.77(6) . 8 ? Si1 C313 2.09(5) . 8 ? C111 H111a .92(3) . . ? C111 H111b 1.01(4) . . ? C111 H111c .93(4) . . ? C111 Si3 1.68(3) . 8 ? C111 C312 1.56(7) . 8 ? C111 C313 1.74(6) . 8 ? C111 H312c 1.25(4) . 8 ? C112 H112a .97(3) . . ? C112 H112b .95(3) . . ? C112 H112c .92(3) . . ? C112 Si3 2.07(3) . 8 ? C112 C312 1.87(7) . 8 ? C112 H31a 1.25(3) . 8 ? C113 H113a .90(4) . . ? C113 H113b 1.04(4) . . ? C113 H113c 1.03(3) . . ? C113 Si3 1.80(3) . 8 ? C113 C311 1.46(8) . 8 ? C113 H311a .93(4) . 8 ? C11 C12 1.52(3) . . ? C11 H11a .98(3) . . ? C11 H11b 1.00(2) . . ? C11 C121 1.26(4) . 8 ? C11 H121b 1.02(3) . 8 ? C11 H121c .98(2) . 8 ? C12 N12 1.43(3) . . ? C12 H12a 1.10(3) . . ? C12 H12b .83(3) . . ? C12 C121 .55(4) . 8 ? C12 C122 1.88(4) . 8 ? C12 H121a 1.16(3) . 8 ? C12 H121c .82(2) . 8 ? N12 C121 1.38(4) . . ? N12 C122 1.36(3) . . ? N12 C121 1.38(4) . 8 ? N12 C122 1.36(3) . 8 ? C121 H121a 1.08(3) . . ? C121 H121b 1.09(3) . . ? C121 H121c .97(4) . . ? C121 C121 1.77(6) . 8 ? C121 H12b 1.12(3) . 8 ? C122 H122a 1.00(5) . . ? C122 H122b .91(2) . . ? C122 H122c 1.01(6) . . ? C122 C122 .70(10) . 8 ? C122 H122a .78(2) . 8 ? C122 H122b 1.19(5) . 8 ? N21 Si2 1.613(14) . . ? N21 C21 1.50(3) . . ? N21 N21 1.02(2) . 8 ? N21 Si2 1.726(19) . 8 ? Si2 C211 1.95(3) . . ? Si2 C212 1.99(4) . . ? Si2 C213 1.69(3) . . ? Si2 Si2 .37(5) . 8 ? Si2 C211 1.84(3) . 8 ? Si2 C212 1.73(4) . 8 ? Si2 C213 1.93(4) . 8 ? C211 H211a 1.09(5) . . ? C211 H211b .86(5) . . ? C211 H211c .91(2) . . ? C211 C211 1.15(9) . 8 ? C211 H211a .81(3) . 8 ? C212 H212a .98(3) . . ? C212 H212b .97(3) . . ? C212 H212c .96(2) . . ? C212 C213 1.31(3) . 8 ? C212 H213a .81(2) . 8 ? C213 H213a .93(2) . . ? C213 H213b 1.00(3) . . ? C213 H213c .94(2) . . ? C213 H212c .98(2) . 8 ? C21 C22 1.58(4) . . ? C21 H21a .94(3) . . ? C21 H21b .97(3) . . ? C21 C322 1.56(3) . 8 ? C21 H322b .84(3) . 8 ? C22 N22 1.43(3) . . ? C22 H22a .93(3) . . ? C22 H22b .94(3) . . ? C22 C31 1.69(4) . 8 ? C22 C32 1.58(4) . 8 ? C22 N32 1.61(3) . 8 ? C22 C322 1.58(4) . 8 ? C22 H31b 1.41(2) . 8 ? C22 H322b 1.19(3) . 8 ? N22 C221 1.35(4) . . ? N22 C222 1.61(4) . . ? N22 C32 1.14(3) . 8 ? N22 N32 .35(3) . 8 ? N22 C321 1.58(3) . 8 ? N22 C322 1.56(3) . 8 ? C221 H221a .95(4) . . ? C221 H221b .86(4) . . ? C221 H221c 1.04(3) . . ? C221 C32 .98(4) . 8 ? C221 N32 1.59(4) . 8 ? C221 C321 1.66(5) . 8 ? C221 H32a .99(4) . 8 ? C221 H32b 1.39(4) . 8 ? C222 H222a 1.04(4) . . ? C222 H222b .90(4) . . ? C222 H222c 1.01(4) . . ? C222 N32 1.39(3) . 8 ? C222 C321 1.35(4) . 8 ? C222 C322 1.09(5) . 8 ? C222 H321b 1.48(4) . 8 ? C222 H321c 1.27(4) . 8 ? C222 H322a 1.21(4) . 8 ? C222 H322c 1.16(4) . 8 ? N31 Si3 1.699(16) . . ? N31 C31 1.51(3) . . ? Si3 C311 1.77(5) . . ? Si3 C312 1.86(6) . . ? Si3 C313 1.83(5) . . ? C311 H311a .99(5) . . ? C311 H311b .93(6) . . ? C311 H311c .94(5) . . ? C311 H113c 1.12(5) . 8 ? C312 H312a .80(7) . . ? C312 H312b 1.07(6) . . ? C312 H312c 1.06(6) . . ? C312 H111b 1.19(6) . 8 ? C313 H313a .87(5) . . ? C313 H313b .96(5) . . ? C313 H313c .94(5) . . ? C313 H111a 1.17(5) . 8 ? C31 C32 1.78(4) . . ? C31 H31a .96(3) . . ? C31 H31b .96(3) . . ? C31 H112b 1.41(3) . 8 ? C31 H22b .84(3) . 8 ? C32 N32 1.49(3) . . ? C32 H32a 1.04(3) . . ? C32 H32b 1.04(3) . . ? C32 H221b 1.02(3) . 8 ? N32 C321 1.46(3) . . ? N32 C322 1.43(3) . . ? C321 H321a .90(3) . . ? C321 H321b .97(3) . . ? C321 H321c .96(3) . . ? C321 H221c 1.47(3) . 8 ? C321 H222c 1.00(3) . 8 ? C322 H322a 1.01(3) . . ? C322 H322b .90(3) . . ? C322 H322c .92(3) . . ? C322 H21a 1.22(3) . 8 ? C322 H222a 1.22(3) . 8 ? C322 H222b 1.40(2) . 8 ? H111a H313c .6249(3) . 8 ? H111b H312c .6906(3) . 8 ? H112b H31a .8035(3) . 8 ? H113c H311a .20239(7) . 8 ? H11b H121b .57692(17) . 8 ? H12b H121a .7171(3) . 8 ? H122a H122a .5518(3) . 8 ? H122b H122b .8466(4) . 8 ? H211a H211a .4558(2) . 8 ? H212c H213a .16391(6) . 8 ? H21a H322b .9079(3) . 8 ? H22b H31b .6667(2) . 8 ? H221b H32a .15432(7) . 8 ? H221c H321a .8819(4) . 8 ? H222a H322c .45947(14) . 8 ? H222b H322a .8033(2) . 8 ? H222c H321c .32352(12) . 8 ? H313b H313b .8656(5) . 8 ? loop_ _geom_contact_atom_site_label_1 #ActaC _geom_contact_atom_site_label_2 #ActaC _geom_contact_distance #ActaC _geom_contact_site_symmetry_1 #ActaC _geom_contact_site_symmetry_2 #ActaC _geom_contact_publ_flag #ActaC Er Si1 3.609(6) . . ? Er Si1 3.609(6) . 8 ? Er C11 3.14(2) . 8 ? Er C11 3.14(2) . . ? Er C12 3.42(3) . 8 ? Er C12 3.42(3) . . ? Er C121 3.23(3) . 8 ? Er C121 3.23(3) . . ? Er C122 3.68(2) . . ? Er C122 3.68(2) . 8 ? Er Si2 3.666(5) . 8 ? Er Si2 3.666(5) . . ? Er C21 3.14(3) . 8 ? Er C21 3.14(3) . . ? Er C22 3.16(3) . 8 ? Er C22 3.16(3) . . ? Er C221 3.74(4) . . ? Er C221 3.74(4) . 8 ? Er C222 3.66(3) . . ? Er C222 3.66(3) . 8 ? Er Si3 3.638(7) . . ? Er Si3 3.638(7) . 8 ? Er C31 3.20(3) . 8 ? Er C31 3.20(3) . . ? Er C32 3.39(3) . . ? Er C32 3.39(3) . 8 ? Er C321 3.73(3) . 8 ? Er C321 3.73(3) . . ? Er C322 3.42(3) . . ? Er C322 3.42(3) . 8 ? Er H121b 3.2868(19) . 8 ? Er H121b 3.2868(19) . . ? Er H22b 3.0174(15) . . ? Er H22b 3.0174(15) . 8 ? N11 C112 2.91(3) . . ? N11 C113 2.89(3) . . ? N11 C12 2.70(3) . . ? N11 N12 2.971(15) . . ? N11 C121 2.44(3) . 8 ? N11 C312 2.71(7) . 8 ? N11 C313 2.41(5) . 8 ? N11 C31 2.31(3) . 8 ? N11 H11a 2.001(13) . . ? N11 H11b 2.017(13) . . ? N11 H121b 2.075(13) . 8 ? N11 H121c 2.213(13) . 8 ? N11 H313a 2.271(13) . 8 ? Si1 C11 2.63(3) . . ? Si1 C31 2.41(3) . 8 ? Si1 H111a 2.307(6) . . ? Si1 H111b 2.304(6) . . ? Si1 H111c 2.436(6) . . ? Si1 H112a 2.280(6) . . ? Si1 H112b 2.277(6) . . ? Si1 H112c 2.340(6) . . ? Si1 H113a 2.452(6) . . ? Si1 H113b 2.457(5) . . ? Si1 H113c 2.472(5) . . ? Si1 H11a 2.508(5) . . ? Si1 H311a 2.317(5) . 8 ? Si1 H311b 2.163(5) . 8 ? Si1 H311c 2.469(5) . 8 ? Si1 H312a 2.217(6) . 8 ? Si1 H312b 2.337(6) . 8 ? Si1 H312c 2.449(6) . 8 ? Si1 H313a 2.414(6) . 8 ? Si1 H313b 2.485(6) . 8 ? Si1 H313c 2.589(6) . 8 ? Si1 H31a 2.252(6) . 8 ? C111 C112 2.82(4) . . ? C111 C113 2.96(5) . . ? C111 C311 2.25(6) . 8 ? C111 H311c 2.18(4) . 8 ? C111 H312a 2.28(4) . 8 ? C111 H312b 2.03(4) . 8 ? C111 H313a 2.11(4) . 8 ? C111 H313c 1.51(4) . 8 ? C112 C113 2.93(5) . . ? C112 N31 2.45(3) . 8 ? C112 C311 2.24(5) . 8 ? C112 C31 2.03(4) . 8 ? C112 H311b 1.78(3) . 8 ? C112 H312a 1.55(3) . 8 ? C112 H31b 2.34(3) . 8 ? C113 C212 2.51(5) . 8 ? C113 N31 2.40(2) . 8 ? C113 C313 2.85(6) . 8 ? C113 H212a 2.39(4) . 8 ? C113 H212b 1.78(4) . 8 ? C113 H311b 2.03(5) . 8 ? C113 H311c 2.18(4) . 8 ? C11 N12 2.38(3) . . ? C11 C121 2.70(5) . . ? C11 N31 2.39(3) . 8 ? C11 Si3 2.67(3) . 8 ? C11 C312 2.69(7) . 8 ? C11 C313 2.88(5) . 8 ? C11 H12a 2.05(2) . . ? C11 H12b 2.07(2) . . ? C11 H121a 1.92(2) . 8 ? C11 H121b 2.41(3) . . ? C11 H312b 2.06(3) . 8 ? C11 H313a 2.30(2) . 8 ? C12 C12 2.38(3) . 8 ? C12 C121 2.12(5) . . ? C12 C122 2.28(5) . . ? C12 H11a 2.09(2) . . ? C12 H11b 2.00(3) . . ? C12 H121a 2.44(2) . . ? C12 H121b 1.61(3) . 8 ? C12 H121b 2.47(2) . . ? C12 H122b 2.05(2) . 8 ? C12 H122b 2.49(2) . . ? C12 H122c 2.06(3) . 8 ? N12 H12a 1.947(2) . . ? N12 H12a 1.947(2) . 8 ? N12 H12b 1.944(10) . 8 ? N12 H12b 1.944(10) . . ? N12 H121a 2.151(12) . . ? N12 H121a 2.151(12) . 8 ? N12 H121b 2.158(11) . . ? N12 H121b 2.158(11) . 8 ? N12 H121c 2.042(5) . . ? N12 H121c 2.042(5) . 8 ? N12 H122a 1.954(10) . . ? N12 H122a 1.954(10) . 8 ? N12 H122b 1.950(9) . . ? N12 H122b 1.950(9) . 8 ? N12 H122c 1.961(8) . 8 ? N12 H122c 1.961(8) . . ? C121 C122 2.19(4) . . ? C121 C122 2.46(5) . 8 ? C121 H11a 2.01(4) . 8 ? C121 H11b 2.49(4) . . ? C121 H11b 1.56(3) . 8 ? C121 H12a 1.59(3) . 8 ? C121 H12b 2.35(4) . . ? C121 H121a 2.14(4) . 8 ? C121 H121b 1.95(4) . 8 ? C121 H122b 2.40(2) . . ? C122 H12a 2.47(6) . . ? C122 H12a 1.85(6) . 8 ? C122 H12b 2.05(4) . 8 ? C122 H12b 2.43(5) . . ? C122 H122c 1.65(7) . 8 ? N21 C211 2.72(2) . 8 ? N21 C211 2.93(3) . . ? N21 C212 2.43(2) . 8 ? N21 C212 2.93(3) . . ? N21 C213 2.98(2) . . ? N21 C21 2.42(4) . 8 ? N21 C22 2.60(3) . . ? N21 N31 2.95(2) . 8 ? N21 N32 2.916(18) . 8 ? N21 C322 2.59(3) . 8 ? N21 H212a 2.385(13) . 8 ? N21 H21a 2.036(13) . . ? N21 H21b 2.016(14) . . ? N21 H322b 2.210(14) . 8 ? Si2 C21 2.43(4) . . ? Si2 C21 2.69(4) . 8 ? Si2 H211a 2.475(7) . 8 ? Si2 H211a 2.441(5) . . ? Si2 H211b 2.241(17) . 8 ? Si2 H211b 2.44(2) . . ? Si2 H211c 2.408(13) . . ? Si2 H211c 2.311(8) . 8 ? Si2 H212a 2.53(3) . . ? Si2 H212a 2.20(3) . 8 ? Si2 H212b 2.363(15) . 8 ? Si2 H212b 2.535(19) . . ? Si2 H212c 2.51(2) . . ? Si2 H212c 2.27(2) . 8 ? Si2 H213a 2.40(3) . 8 ? Si2 H213a 2.15(2) . . ? Si2 H213b 2.46(3) . 8 ? Si2 H213b 2.15(3) . . ? Si2 H213c 2.579(17) . 8 ? Si2 H213c 2.424(13) . . ? Si2 H21b 2.69(3) . 8 ? Si2 H21b 2.35(3) . . ? C211 C213 2.86(5) . . ? C211 C213 2.33(3) . 8 ? C211 C21 2.65(4) . 8 ? C211 H211b 1.89(6) . 8 ? C211 H211c 1.50(5) . 8 ? C211 H213b 2.11(4) . 8 ? C211 H21a 2.45(3) . 8 ? C211 H21b 2.45(5) . 8 ? C212 C212 2.65(5) . 8 ? C212 C213 2.83(4) . . ? C212 C21 2.90(3) . 8 ? C212 H113a 1.69(3) . 8 ? C212 H213b 1.87(3) . 8 ? C212 H213c 2.12(2) . 8 ? C212 H21b 2.42(2) . 8 ? C213 C213 2.38(4) . 8 ? C213 H211c 2.23(2) . 8 ? C213 H212a 1.83(2) . 8 ? C213 H212b 2.18(2) . 8 ? C213 H213c 2.43(3) . 8 ? C21 N22 2.44(3) . . ? C21 C222 2.60(4) . . ? C21 C31 2.89(4) . 8 ? C21 N32 2.38(3) . 8 ? C21 H211b 2.13(3) . 8 ? C21 H212a 2.37(2) . 8 ? C21 H22a 2.08(3) . . ? C21 H22b 2.07(3) . . ? C21 H222a 2.28(2) . . ? C21 H31b 2.32(3) . 8 ? C21 H322a 2.36(2) . 8 ? C21 H322c 1.90(2) . 8 ? C22 C221 2.37(3) . . ? C22 C222 2.38(4) . . ? C22 N31 2.59(3) . 8 ? C22 C321 2.90(3) . 8 ? C22 H21a 2.07(3) . . ? C22 H21b 2.06(2) . . ? C22 H32b 1.94(2) . 8 ? C22 H322a 2.04(2) . 8 ? C22 H322c 2.43(3) . 8 ? N22 N31 2.98(2) . 8 ? N22 C31 2.36(4) . 8 ? N22 H22a 1.939(19) . . ? N22 H22b 1.962(19) . . ? N22 H221a 1.846(19) . . ? N22 H221b 1.87(2) . . ? N22 H221c 2.016(18) . . ? N22 H222a 2.23(2) . . ? N22 H222b 2.21(2) . . ? N22 H222c 2.11(2) . . ? N22 H32a 1.92(2) . 8 ? N22 H32b 1.86(2) . 8 ? N22 H321a 2.048(18) . 8 ? N22 H321b 2.00(2) . 8 ? N22 H321c 2.15(2) . 8 ? N22 H322a 1.97(2) . 8 ? N22 H322b 1.94(2) . 8 ? N22 H322c 2.21(2) . 8 ? C221 C222 2.43(5) . . ? C221 C31 2.73(4) . 8 ? C221 C322 2.69(4) . 8 ? C221 H321a 1.62(4) . 8 ? C221 H321b 1.84(4) . 8 ? C222 C32 2.59(5) . 8 ? C222 H21a 2.16(4) . . ? C222 H221a 2.42(4) . . ? C222 H321a 2.25(3) . 8 ? C222 H322b 1.98(4) . 8 ? N31 C311 2.99(5) . . ? N31 C312 2.92(6) . . ? N31 C313 2.99(5) . . ? N31 C32 2.80(3) . . ? N31 H112b 2.325(14) . 8 ? N31 H113a 2.452(14) . 8 ? N31 H22b 1.822(14) . 8 ? N31 H31a 1.999(14) . . ? N31 H31b 1.989(14) . . ? Si3 C31 2.66(3) . . ? Si3 H111a 2.079(8) . 8 ? Si3 H111b 2.241(8) . 8 ? Si3 H111c 2.324(8) . 8 ? Si3 H112a 2.527(7) . 8 ? Si3 H112b 2.549(7) . 8 ? Si3 H112c 2.532(7) . 8 ? Si3 H113a 2.448(8) . 8 ? Si3 H113b 2.279(7) . 8 ? Si3 H113c 2.392(7) . 8 ? Si3 H11a 2.601(7) . 8 ? Si3 H311a 2.253(7) . . ? Si3 H311b 2.254(7) . . ? Si3 H311c 2.384(7) . . ? Si3 H312a 2.381(7) . . ? Si3 H312b 2.384(8) . . ? Si3 H312c 2.436(8) . . ? Si3 H313a 2.216(7) . . ? Si3 H313b 2.218(7) . . ? Si3 H313c 2.328(8) . . ? Si3 H31a 2.536(7) . . ? C311 C312 2.73(7) . . ? C311 H111c 2.17(5) . 8 ? C311 H112c 2.05(5) . 8 ? C311 H113a 2.12(6) . 8 ? C311 H113b 2.19(6) . 8 ? C312 C313 2.76(8) . . ? C312 H111a 2.36(6) . 8 ? C312 H111c 2.00(5) . 8 ? C312 H112a 1.62(6) . 8 ? C312 H112c 2.20(6) . 8 ? C312 H11a 1.98(6) . 8 ? C313 C313 2.24(7) . 8 ? C313 H111b 2.27(5) . 8 ? C313 H11b 2.44(5) . 8 ? C313 H313a 2.24(5) . 8 ? C313 H313b 1.69(5) . 8 ? C31 N32 2.63(3) . . ? C31 H112a 2.31(3) . 8 ? C31 H22a 2.15(3) . 8 ? C31 H221b 2.39(3) . 8 ? C31 H32a 2.30(3) . . ? C31 H32b 2.30(3) . . ? C32 C321 2.29(4) . . ? C32 C322 2.43(4) . . ? C32 H22a 1.82(3) . 8 ? C32 H22b 1.73(3) . 8 ? C32 H221a 1.51(3) . 8 ? C32 H221c 1.99(3) . 8 ? C32 H31a 2.34(3) . . ? C32 H31b 2.25(3) . . ? C32 H321a 2.46(3) . . ? C32 H321b 2.46(3) . . ? N32 H21a 2.471(14) . 8 ? N32 H22a 2.160(16) . 8 ? N32 H22b 2.182(15) . 8 ? N32 H221a 2.070(16) . 8 ? N32 H221b 2.155(15) . 8 ? N32 H221c 2.106(14) . 8 ? N32 H222a 1.938(15) . 8 ? N32 H222b 2.100(15) . 8 ? N32 H222c 1.857(14) . 8 ? N32 H32a 2.209(15) . . ? N32 H32b 2.196(17) . . ? N32 H321a 1.988(13) . . ? N32 H321b 1.975(14) . . ? N32 H321c 1.883(15) . . ? N32 H322a 1.945(15) . . ? N32 H322b 1.920(14) . . ? N32 H322c 1.961(15) . . ? C321 C322 2.23(4) . . ? C321 H221a 1.82(4) . 8 ? C321 H221b 2.47(3) . 8 ? C321 H222a 2.22(3) . 8 ? C321 H222b 1.87(3) . 8 ? C321 H322a 2.22(3) . . ? C321 H322c 2.45(3) . . ? C322 H21b 2.36(3) . 8 ? C322 H22a 1.83(3) . 8 ? C322 H22b 2.47(3) . 8 ? C322 H222c 2.08(3) . 8 ? C322 H321b 2.30(3) . . ? C322 H321c 2.29(3) . . ? H111a H111b 1.5512(5) . . ? H111a H111c 1.5295(7) . . ? H111a H313a 1.6291(5) . 8 ? H111a H313b 1.9568(8) . 8 ? H111b H111c 1.5295(6) . . ? H111b H312a 1.8871(7) . 8 ? H111b H312b 1.2698(4) . 8 ? H111c H311c 1.7492(7) . 8 ? H111c H312c 1.3594(5) . 8 ? H112a H112b 1.5513(8) . . ? H112a H112c 1.5419(6) . . ? H112a H312a 1.0190(6) . 8 ? H112a H31a 1.3982(7) . 8 ? H112b H112c 1.5419(6) . . ? H112b H22b 1.9595(7) . . ? H112b H31b 1.5108(7) . 8 ? H112c H311b 1.3861(4) . 8 ? H112c H312a 1.8393(6) . 8 ? H113a H113b 1.5513(7) . . ? H113a H113c 1.5490(6) . . ? H113a H212a 1.4940(9) . 8 ? H113a H212b 1.1884(4) . 8 ? H113a H311a 1.4553(6) . 8 ? H113b H113c 1.5488(8) . . ? H113b H212b 1.7379(11) . 8 ? H113b H311a 1.5836(8) . 8 ? H113c H311b 1.7057(7) . 8 ? H113c H311c 1.5355(7) . 8 ? H11a H11b 1.5512(7) . . ? H11a H121b 1.8186(10) . 8 ? H11a H121c 1.3431(4) . 8 ? H11a H312b 1.2629(4) . 8 ? H11b H121a 1.8562(7) . 8 ? H11b H121b 1.8732(9) . . ? H11b H121c 1.7600(5) . 8 ? H11b H313a 1.6700(6) . 8 ? H12a H12b 1.5513(8) . . ? H12a H121c 1.1267(4) . 8 ? H12a H122c 1.4529(4) . 8 ? H12b H121b 1.9799(7) . 8 ? H12b H121c 1.3881(4) . 8 ? H12b H122b 1.8312(5) . 8 ? H121a H121a 1.9356(10) . 8 ? H121a H121b 1.5513(6) . . ? H121a H121c 1.5686(6) . . ? H121b H121b 1.4729(8) . 8 ? H121b H121c 1.5685(5) . . ? H122a H122b 1.5514(8) . . ? H122a H122b 1.3927(8) . 8 ? H122a H122c 1.0276(5) . 8 ? H122a H122c 1.5504(8) . . ? H122b H122c 1.5504(6) . . ? H122c H221c 1.9575(9) . 8 ? H211a H211b 1.1329(5) . 8 ? H211a H211b 1.5512(7) . . ? H211a H211c 1.5562(5) . . ? H211a H211c 1.3629(5) . 8 ? H211b H211c 1.5562(5) . . ? H211b H21a 1.7806(6) . 8 ? H211b H21b 1.9308(9) . 8 ? H211c H211c 1.2381(7) . 8 ? H212a H212b 1.5512(5) . . ? H212a H212c 1.5555(5) . . ? H212a H213a 1.4106(5) . 8 ? H212a H213b 1.8622(10) . 8 ? H212a H21b 1.7650(6) . 8 ? H212b H212c 1.5553(7) . . ? H212b H213a 1.4881(7) . 8 ? H212c H213b 1.6212(8) . 8 ? H212c H213c 1.4415(7) . 8 ? H213a H213b 1.5514(8) . . ? H213a H213c 1.5001(7) . . ? H213b H213c 1.5001(5) . . ? H21a H21b 1.5513(4) . . ? H21a H222a 1.6833(6) . . ? H21a H322a 1.8942(6) . 8 ? H21a H322c 1.2414(4) . 8 ? H21b H322b 1.4985(6) . 8 ? H22a H22b 1.5513(7) . . ? H22a H31b 1.7493(7) . 8 ? H22a H32b 1.6263(5) . 8 ? H22a H322a 1.8174(6) . 8 ? H22a H322b 1.4755(6) . 8 ? H22b H31a 1.7223(8) . 8 ? H22b H322b 1.9960(11) . 8 ? H221a H221b 1.5514(9) . . ? H221a H221c 1.5131(5) . . ? H221a H32a 1.6943(10) . 8 ? H221a H32b 1.1863(4) . 8 ? H221a H321a 1.9720(9) . 8 ? H221a H321b 1.4671(6) . 8 ? H221b H221c 1.5132(4) . . ? H221b H32b 1.4889(6) . 8 ? H221c H32a 1.6366(5) . 8 ? H221c H321b 1.8314(11) . 8 ? H222a H222a 1.6665(9) . 8 ? H222a H222b 1.5512(6) . . ? H222a H222c 1.5613(6) . . ? H222a H321c 1.7534(6) . 8 ? H222a H322a 1.7664(9) . 8 ? H222a H322b 1.9427(6) . 8 ? H222a H322c 1.9838(10) . . ? H222b H222c 1.5613(5) . . ? H222b H321b 1.4747(5) . 8 ? H222b H321c 1.8732(6) . 8 ? H222b H322c 1.5293(5) . 8 ? H222c H321a 1.7395(8) . 8 ? H222c H321b 1.4266(7) . 8 ? H222c H321c 1.9317(10) . . ? H222c H322c 1.9072(7) . 8 ? H311a H311b 1.5513(6) . . ? H311a H311c 1.5294(7) . . ? H311b H311c 1.5293(6) . . ? H312a H312b 1.5512(6) . . ? H312a H312c 1.5429(6) . . ? H312b H312c 1.5430(5) . . ? H313a H313a 1.9010(10) . 8 ? H313a H313b 1.5513(5) . . ? H313a H313c 1.5325(5) . . ? H313b H313c 1.5326(6) . . ? H31a H31b 1.5513(7) . . ? H32a H32b 1.5512(7) . . ? H321a H321b 1.5513(7) . . ? H321a H321c 1.5666(6) . . ? H321b H321c 1.5667(8) . . ? H321b H322a 1.8568(6) . . ? H321c H321c 1.7370(9) . 8 ? H322a H322b 1.5513(5) . . ? H322a H322c 1.5479(8) . . ? H322b H322c 1.5478(5) . . ? loop_ _geom_angle_atom_site_label_1 #ActaC _geom_angle_atom_site_label_2 #ActaC _geom_angle_atom_site_label_3 #ActaC _geom_angle #ActaC _geom_angle_site_symmetry_1 #ActaC _geom_angle_site_symmetry_2 #ActaC _geom_angle_site_symmetry_3 #ActaC _geom_angle_publ_flag #ActaC N11 Er N12 73.9(4) . . . ? N11 Er N21 106.8(5) . . . ? N11 Er N22 86.4(5) . . . ? N11 Er N31 106.2(5) . . . ? N11 Er N32 161.1(4) . . . ? N11 Er N11 84.6(5) . . 8 ? N11 Er N21 126.5(5) . . 8 ? N11 Er N22 159.7(5) . . 8 ? N11 Er N31 26.3(5) . . 8 ? N11 Er N32 93.2(5) . . 8 ? N12 Er N21 159.5(4) . . . ? N12 Er N22 86.2(4) . . . ? N12 Er N31 94.3(4) . . . ? N12 Er N32 87.4(4) . . . ? N12 Er N11 73.9(4) . . 8 ? N12 Er N21 159.5(4) . . 8 ? N12 Er N22 86.2(4) . . 8 ? N12 Er N31 94.3(4) . . 8 ? N12 Er N32 87.4(4) . . 8 ? N21 Er N22 73.5(5) . . . ? N21 Er N31 104.8(5) . . . ? N21 Er N32 89.6(5) . . . ? N21 Er N11 126.5(5) . . 8 ? N21 Er N21 26.2(5) . . 8 ? N21 Er N22 93.1(5) . . 8 ? N21 Er N31 81.9(5) . . 8 ? N21 Er N32 72.1(4) . . 8 ? N22 Er N31 167.0(5) . . . ? N22 Er N32 89.4(5) . . . ? N22 Er N11 159.7(5) . . 8 ? N22 Er N21 93.1(5) . . 8 ? N22 Er N22 96.0(6) . . 8 ? N22 Er N31 71.1(5) . . 8 ? N22 Er N32 6.8(5) . . 8 ? N31 Er N32 77.7(5) . . . ? N31 Er N11 26.3(5) . . 8 ? N31 Er N21 81.9(5) . . 8 ? N31 Er N22 71.1(5) . . 8 ? N31 Er N31 121.7(5) . . 8 ? N31 Er N32 160.2(5) . . 8 ? N32 Er N11 93.2(5) . . 8 ? N32 Er N21 72.1(4) . . 8 ? N32 Er N22 6.8(5) . . 8 ? N32 Er N31 160.2(5) . . 8 ? N32 Er N32 82.7(5) . . 8 ? N11 Er N21 106.8(5) 8 . 8 ? N11 Er N22 86.4(5) 8 . 8 ? N11 Er N31 106.2(5) 8 . 8 ? N11 Er N32 161.1(4) 8 . 8 ? N21 Er N22 73.5(5) 8 . 8 ? N21 Er N31 104.8(5) 8 . 8 ? N21 Er N32 89.6(5) 8 . 8 ? N22 Er N31 167.0(5) 8 . 8 ? N22 Er N32 89.4(5) 8 . 8 ? N31 Er N32 77.7(5) 8 . 8 ? Er N11 Si1 135.4(8) . . . ? Er N11 C11 112.6(12) . . . ? Er N11 N31 77.9(11) . . 8 ? Er N11 Si3 134.3(7) . . 8 ? Si1 N11 C11 111.9(13) . . . ? Si1 N11 N31 66.2(11) . . 8 ? Si1 N11 Si3 9.6(3) . . 8 ? C11 N11 N31 140.6(17) . . 8 ? C11 N11 Si3 112.4(13) . . 8 ? N31 N11 Si3 72.3(11) 8 . 8 ? N11 Si1 C111 119.3(13) . . . ? N11 Si1 C112 114.0(11) . . . ? N11 Si1 C113 109.5(14) . . . ? N11 Si1 N31 36.8(7) . . 8 ? N11 Si1 Si3 94.5(18) . . 8 ? N11 Si1 C311 156(2) . . 8 ? N11 Si1 C312 104(2) . . 8 ? N11 Si1 C313 79.3(14) . . 8 ? C111 Si1 C112 101.6(15) . . . ? C111 Si1 C113 106.2(16) . . . ? C111 Si1 N31 156.1(13) . . 8 ? C111 Si1 Si3 55(2) . . 8 ? C111 Si1 C311 77(2) . . 8 ? C111 Si1 C312 52(2) . . 8 ? C111 Si1 C313 52.1(18) . . 8 ? C112 Si1 C113 105.1(17) . . . ? C112 Si1 N31 92.9(11) . . 8 ? C112 Si1 Si3 151(2) . . 8 ? C112 Si1 C311 77(2) . . 8 ? C112 Si1 C312 63(2) . . 8 ? C112 Si1 C313 152.6(17) . . 8 ? C113 Si1 N31 87.8(12) . . 8 ? C113 Si1 Si3 70(2) . . 8 ? C113 Si1 C311 47(2) . . 8 ? C113 Si1 C312 146(2) . . 8 ? C113 Si1 C313 91.5(19) . . 8 ? N31 Si1 Si3 115(2) 8 . 8 ? N31 Si1 C311 125.4(18) 8 . 8 ? N31 Si1 C312 122.9(19) 8 . 8 ? N31 Si1 C313 109.6(15) 8 . 8 ? Si3 Si1 C311 80(3) 8 . 8 ? Si3 Si1 C312 104(3) 8 . 8 ? Si3 Si1 C313 23(2) 8 . 8 ? C311 Si1 C312 100(3) 8 . 8 ? C311 Si1 C313 101(2) 8 . 8 ? C312 Si1 C313 91(3) 8 . 8 ? Si1 C111 H111a 110(3) . . . ? Si1 C111 H111b 105(3) . . . ? Si1 C111 H111c 121(2) . . . ? Si1 C111 Si3 8.0(3) . . 8 ? Si1 C111 C312 62(3) . . 8 ? Si1 C111 C313 72(2) . . 8 ? Si1 C111 H312c 104(2) . . 8 ? H111a C111 H111b 106(3) . . . ? H111a C111 H111c 111(4) . . . ? H111a C111 Si3 102(3) . . 8 ? H111a C111 C312 142(4) . . 8 ? H111a C111 C313 39(2) . . 8 ? H111a C111 H312c 134(3) . . 8 ? H111b C111 H111c 104(3) . . . ? H111b C111 Si3 110(3) . . 8 ? H111b C111 C312 49(3) . . 8 ? H111b C111 C313 108(3) . . 8 ? H111b C111 H312c 33.5(11) . . 8 ? H111c C111 Si3 123(3) . . 8 ? H111c C111 C312 104(4) . . 8 ? H111c C111 C313 141(4) . . 8 ? H111c C111 H312c 76(2) . . 8 ? Si3 C111 C312 70(3) 8 . 8 ? Si3 C111 C313 65(2) 8 . 8 ? Si3 C111 H312c 112(2) 8 . 8 ? C312 C111 C313 114(4) 8 . 8 ? C312 C111 H312c 43(3) 8 . 8 ? C313 C111 H312c 141(3) 8 . 8 ? Si1 C112 H112a 106(2) . . . ? Si1 C112 H112b 107(2) . . . ? Si1 C112 H112c 114(2) . . . ? Si1 C112 Si3 3.9(3) . . 8 ? Si1 C112 C312 57(2) . . 8 ? Si1 C112 H31a 92.8(15) . . 8 ? H112a C112 H112b 108(3) . . . ? H112a C112 H112c 110(3) . . . ? H112a C112 Si3 107(2) . . 8 ? H112a C112 C312 60(2) . . 8 ? H112a C112 H31a 77(2) . . 8 ? H112b C112 H112c 111(3) . . . ? H112b C112 Si3 110(2) . . 8 ? H112b C112 C312 150(3) . . 8 ? H112b C112 H31a 40.0(11) . . 8 ? H112c C112 Si3 110(2) . . 8 ? H112c C112 C312 98(3) . . 8 ? H112c C112 H31a 148(3) . . 8 ? Si3 C112 C312 56(2) 8 . 8 ? Si3 C112 H31a 96.7(15) 8 . 8 ? C312 C112 H31a 111(3) 8 . 8 ? Si1 C113 H113a 120(2) . . . ? Si1 C113 H113b 112(3) . . . ? Si1 C113 H113c 113(3) . . . ? Si1 C113 Si3 8.6(3) . . 8 ? Si1 C113 C311 64(2) . . 8 ? Si1 C113 H311a 106(3) . . 8 ? H113a C113 H113b 106(4) . . . ? H113a C113 H113c 107(3) . . . ? H113a C113 Si3 127(2) . . 8 ? H113a C113 C311 126(5) . . 8 ? H113a C113 H311a 105(4) . . 8 ? H113b C113 H113c 97(2) . . . ? H113b C113 Si3 104(3) . . 8 ? H113b C113 C311 122(4) . . 8 ? H113b C113 H311a 107(2) . . 8 ? H113c C113 Si3 112(3) . . 8 ? H113c C113 C311 50(2) . . 8 ? H113c C113 H311a 10.3(3) . . 8 ? Si3 C113 C311 65(2) 8 . 8 ? Si3 C113 H311a 107(3) 8 . 8 ? C311 C113 H311a 42(2) 8 . 8 ? N11 C11 C12 126(2) . . . ? N11 C11 H11a 105(2) . . . ? N11 C11 H11b 105(2) . . . ? N11 C11 C121 123(2) . . 8 ? N11 C11 H121b 109(2) . . 8 ? N11 C11 H121c 123.9(19) . . 8 ? C12 C11 H11a 111(2) . . . ? C12 C11 H11b 104(2) . . . ? C12 C11 C121 20.4(19) . . 8 ? C12 C11 H121b 75.8(18) . . 8 ? C12 C11 H121c 29.1(12) . . 8 ? H11a C11 H11b 103(2) . . . ? H11a C11 C121 127(3) . . 8 ? H11a C11 H121b 131(2) . . 8 ? H11a C11 H121c 86(2) . . 8 ? H11b C11 C121 86(2) . . 8 ? H11b C11 H121b 33.3(9) . . 8 ? H11b C11 H121c 126(2) . . 8 ? C121 C11 H121b 56(2) 8 . 8 ? C121 C11 H121c 50(2) 8 . 8 ? H121b C11 H121c 103(2) 8 . 8 ? C11 C12 N12 108.0(19) . . . ? C11 C12 H12a 102(2) . . . ? C11 C12 H12b 121(3) . . . ? C11 C12 C121 52(4) . . 8 ? C11 C12 C122 149(2) . . 8 ? C11 C12 H121a 90.6(19) . . 8 ? C11 C12 H121c 35.8(16) . . 8 ? N12 C12 H12a 100(2) . . . ? N12 C12 H12b 116(2) . . . ? N12 C12 C121 74(4) . . 8 ? N12 C12 C122 46.2(18) . . 8 ? N12 C12 H121a 112.2(18) . . 8 ? N12 C12 H121c 129(3) . . 8 ? H12a C12 H12b 106(2) . . . ? H12a C12 C121 147(5) . . 8 ? H12a C12 C122 72(2) . . 8 ? H12a C12 H121a 140(2) . . 8 ? H12a C12 H121c 70.4(18) . . 8 ? H12b C12 C121 105(5) . . 8 ? H12b C12 C122 90(2) . . 8 ? H12b C12 H121a 38.1(12) . . 8 ? H12b C12 H121c 115(3) . . 8 ? C121 C12 C122 118(5) 8 . 8 ? C121 C12 H121a 68(4) 8 . 8 ? C121 C12 H121c 88(5) 8 . 8 ? C122 C12 H121a 114(2) 8 . 8 ? C122 C12 H121c 139(3) 8 . 8 ? H121a C12 H121c 104(3) 8 . 8 ? Er N12 C12 109.5(11) . . . ? Er N12 C121 100.6(11) . . . ? Er N12 C122 128.4(14) . . . ? Er N12 C12 109.5(11) . . 8 ? Er N12 C121 100.6(11) . . 8 ? Er N12 C122 128.4(14) . . 8 ? C12 N12 C121 98(2) . . . ? C12 N12 C122 109(3) . . . ? C12 N12 C12 113.0(18) . . 8 ? C12 N12 C121 22.7(17) . . 8 ? C12 N12 C122 85(3) . . 8 ? C121 N12 C122 106(3) . . . ? C121 N12 C12 22.7(17) . . 8 ? C121 N12 C121 79(2) . . 8 ? C121 N12 C122 127(2) . . 8 ? C122 N12 C12 85(3) . . 8 ? C122 N12 C121 127(2) . . 8 ? C122 N12 C122 30(4) . . 8 ? C12 N12 C121 98(2) 8 . 8 ? C12 N12 C122 109(3) 8 . 8 ? C121 N12 C122 106(3) 8 . 8 ? N12 C121 H121a 121(3) . . . ? N12 C121 H121b 121(3) . . . ? N12 C121 H121c 119(3) . . . ? N12 C121 C11 129(2) . . 8 ? N12 C121 C12 83(4) . . 8 ? N12 C121 C121 50.3(17) . . 8 ? N12 C121 H12b 102(2) . . 8 ? H121a C121 H121b 91(2) . . . ? H121a C121 H121c 99(3) . . . ? H121a C121 C11 110(3) . . 8 ? H121a C121 C12 83(4) . . 8 ? H121a C121 C121 95(3) . . 8 ? H121a C121 H12b 38.0(9) . . 8 ? H121b C121 H121c 99(3) . . . ? H121b C121 C11 50.8(16) . . 8 ? H121b C121 C12 154(6) . . 8 ? H121b C121 C121 82(2) . . 8 ? H121b C121 H12b 128(3) . . 8 ? H121c C121 C11 50(2) . . 8 ? H121c C121 C12 57(4) . . 8 ? H121c C121 C121 166(3) . . 8 ? H121c C121 H12b 83(3) . . 8 ? C11 C121 C12 107(6) 8 . 8 ? C11 C121 C121 126(3) 8 . 8 ? C11 C121 H12b 122(4) 8 . 8 ? C12 C121 C121 124(5) 8 . 8 ? C12 C121 H12b 46(4) 8 . 8 ? C121 C121 H12b 107(2) 8 . 8 ? N12 C122 H122a 111(4) . . . ? N12 C122 H122b 117(3) . . . ? N12 C122 H122c 111(3) . . . ? N12 C122 C12 49.2(13) . . 8 ? N12 C122 C122 75(3) . . 8 ? N12 C122 H122a 130(4) . . 8 ? N12 C122 H122b 99(3) . . 8 ? H122a C122 H122b 109(4) . . . ? H122a C122 H122c 101(2) . . . ? H122a C122 C12 160(3) . . 8 ? H122a C122 C122 51(4) . . 8 ? H122a C122 H122a 33(2) . . 8 ? H122a C122 H122b 78(4) . . 8 ? H122b C122 H122c 107(6) . . . ? H122b C122 C12 87(3) . . 8 ? H122b C122 C122 95(5) . . 8 ? H122b C122 H122a 111(2) . . 8 ? H122b C122 H122b 45(2) . . 8 ? H122c C122 C12 85(3) . . 8 ? H122c C122 C122 150(4) . . 8 ? H122c C122 H122a 69(3) . . 8 ? H122c C122 H122b 147(3) . . 8 ? C12 C122 C122 117(3) 8 . 8 ? C12 C122 H122a 152(6) 8 . 8 ? C12 C122 H122b 106.4(18) 8 . 8 ? C122 C122 H122a 85(6) 8 . 8 ? C122 C122 H122b 50(3) 8 . 8 ? H122a C122 H122b 102(4) 8 . 8 ? Er N21 Si2 143.3(11) . . . ? Er N21 C21 112.6(11) . . . ? Er N21 N21 76.9(10) . . 8 ? Er N21 Si2 134.5(11) . . 8 ? Si2 N21 C21 102.9(15) . . . ? Si2 N21 N21 78.4(16) . . 8 ? Si2 N21 Si2 12.1(16) . . 8 ? C21 N21 N21 147.5(17) . . 8 ? C21 N21 Si2 112.9(14) . . 8 ? N21 N21 Si2 66.3(14) 8 . 8 ? N21 Si2 C211 109.9(9) . . . ? N21 Si2 C212 108.3(13) . . . ? N21 Si2 C213 129(2) . . . ? N21 Si2 N21 35.3(7) . . 8 ? N21 Si2 Si2 101.6(16) . . 8 ? N21 Si2 C211 103.6(12) . . 8 ? N21 Si2 C212 93.1(14) . . 8 ? N21 Si2 C213 143(2) . . 8 ? C211 Si2 C212 103(2) . . . ? C211 Si2 C213 103.4(14) . . . ? C211 Si2 N21 95.0(15) . . 8 ? C211 Si2 Si2 67(2) . . 8 ? C211 Si2 C211 35(3) . . 8 ? C211 Si2 C212 148.0(18) . . 8 ? C211 Si2 C213 73.8(17) . . 8 ? C212 Si2 C213 100.2(12) . . . ? C212 Si2 N21 81.2(14) . . 8 ? C212 Si2 Si2 40.8(13) . . 8 ? C212 Si2 C211 135(2) . . 8 ? C212 Si2 C212 90.4(13) . . 8 ? C212 Si2 C213 38.9(11) . . 8 ? C213 Si2 N21 160.7(17) . . 8 ? C213 Si2 Si2 126.6(16) . . 8 ? C213 Si2 C211 82.6(17) . . 8 ? C213 Si2 C212 45.0(13) . . 8 ? C213 Si2 C213 82.0(12) . . 8 ? N21 Si2 Si2 66.3(14) 8 . 8 ? N21 Si2 C211 110.2(11) 8 . 8 ? N21 Si2 C212 116.0(10) 8 . 8 ? N21 Si2 C213 109(2) 8 . 8 ? Si2 Si2 C211 102(2) 8 . 8 ? Si2 Si2 C212 131.2(16) 8 . 8 ? Si2 Si2 C213 44.6(13) 8 . 8 ? C211 Si2 C212 119(3) 8 . 8 ? C211 Si2 C213 98.7(17) 8 . 8 ? C212 Si2 C213 101.2(11) 8 . 8 ? Si2 C211 H211a 103(4) . . . ? Si2 C211 H211b 114(2) . . . ? Si2 C211 H211c 109(2) . . . ? Si2 C211 Si2 10.6(15) . . 8 ? Si2 C211 C211 67(2) . . 8 ? Si2 C211 H211a 121(5) . . 8 ? H211a C211 H211b 105(2) . . . ? H211a C211 H211c 102(4) . . . ? H211a C211 Si2 113(4) . . 8 ? H211a C211 C211 42(2) . . 8 ? H211a C211 H211a 22.2(17) . . 8 ? H211b C211 H211c 122(6) . . . ? H211b C211 Si2 106(2) . . 8 ? H211b C211 C211 139(4) . . 8 ? H211b C211 H211a 85(3) . . 8 ? H211c C211 Si2 109(2) . . 8 ? H211c C211 C211 93(4) . . 8 ? H211c C211 H211a 104(3) . . 8 ? Si2 C211 C211 78(3) 8 . 8 ? Si2 C211 H211a 130(4) 8 . 8 ? C211 C211 H211a 64(4) 8 . 8 ? Si2 C212 H212a 112.0(17) . . . ? Si2 C212 H212b 113(2) . . . ? Si2 C212 H212c 112(2) . . . ? Si2 C212 Si2 8.0(11) . . 8 ? Si2 C212 C213 68.0(17) . . 8 ? Si2 C212 H213a 110(2) . . 8 ? H212a C212 H212b 105(2) . . . ? H212a C212 H212c 107(3) . . . ? H212a C212 Si2 104.8(18) . . 8 ? H212a C212 C213 105(3) . . 8 ? H212a C212 H213a 103(3) . . 8 ? H212b C212 H212c 108(2) . . . ? H212b C212 Si2 119(3) . . 8 ? H212b C212 C213 146(3) . . 8 ? H212b C212 H213a 113(2) . . 8 ? H212c C212 Si2 112(2) . . 8 ? H212c C212 C213 48.4(14) . . 8 ? H212c C212 H213a 5.4(3) . . 8 ? Si2 C212 C213 65.8(16) 8 . 8 ? Si2 C212 H213a 110(2) 8 . 8 ? C213 C212 H213a 45.0(16) 8 . 8 ? Si2 C213 H213a 106.4(18) . . . ? Si2 C213 H213b 103.0(17) . . . ? Si2 C213 H213c 132(3) . . . ? Si2 C213 Si2 8.8(12) . . 8 ? Si2 C213 C212 69.2(16) . . 8 ? Si2 C213 H212c 113.6(18) . . 8 ? H213a C213 H213b 106(3) . . . ? H213a C213 H213c 106(2) . . . ? H213a C213 Si2 108.7(18) . . 8 ? H213a C213 C212 38.1(13) . . 8 ? H213a C213 H212c 9.3(2) . . 8 ? H213b C213 H213c 101(2) . . . ? H213b C213 Si2 109.8(16) . . 8 ? H213b C213 C212 107(2) . . 8 ? H213b C213 H212c 109(3) . . 8 ? H213c C213 Si2 124(3) . . 8 ? H213c C213 C212 140(2) . . 8 ? H213c C213 H212c 96.9(18) . . 8 ? Si2 C213 C212 73.1(17) 8 . 8 ? Si2 C213 H212c 114.8(19) 8 . 8 ? C212 C213 H212c 46.6(14) 8 . 8 ? N21 C21 C22 115(2) . . . ? N21 C21 H21a 111(3) . . . ? N21 C21 H21b 107(2) . . . ? N21 C21 C322 116(2) . . 8 ? N21 C21 H322b 141(3) . . 8 ? C22 C21 H21a 108(2) . . . ? C22 C21 H21b 105(3) . . . ? C22 C21 C322 60.4(16) . . 8 ? C22 C21 H322b 47.9(17) . . 8 ? H21a C21 H21b 109(3) . . . ? H21a C21 C322 51.3(13) . . 8 ? H21a C21 H322b 61.3(16) . . 8 ? H21b C21 C322 136(3) . . 8 ? H21b C21 H322b 111(3) . . 8 ? C322 C21 H322b 26.8(16) 8 . 8 ? C21 C22 N22 108(2) . . . ? C21 C22 H22a 109(2) . . . ? C21 C22 H22b 109(2) . . . ? C21 C22 C31 125(2) . . 8 ? C21 C22 C32 152(2) . . 8 ? C21 C22 N32 96.6(18) . . 8 ? C21 C22 C322 59.2(16) . . 8 ? C21 C22 H31b 101.9(15) . . 8 ? C21 C22 H322b 31.5(11) . . 8 ? N22 C22 H22a 108.4(19) . . . ? N22 C22 H22b 110(2) . . . ? N22 C22 C31 98(2) . . 8 ? N22 C22 C32 44.3(14) . . 8 ? N22 C22 N32 11.5(10) . . 8 ? N22 C22 C322 62.0(15) . . 8 ? N22 C22 H31b 133(2) . . 8 ? N22 C22 H322b 95.1(18) . . 8 ? H22a C22 H22b 112(3) . . . ? H22a C22 C31 107(2) . . 8 ? H22a C22 C32 89(2) . . 8 ? H22a C22 N32 113.5(18) . . 8 ? H22a C22 C322 90(2) . . 8 ? H22a C22 H31b 95(2) . . 8 ? H22a C22 H322b 87(2) . . 8 ? H22b C22 C31 16.8(13) . . 8 ? H22b C22 C32 82(2) . . 8 ? H22b C22 N32 115(2) . . 8 ? H22b C22 C322 158(3) . . 8 ? H22b C22 H31b 23.7(7) . . 8 ? H22b C22 H322b 140(2) . . 8 ? C31 C22 C32 66.0(18) 8 . 8 ? C31 C22 N32 105.6(18) 8 . 8 ? C31 C22 C322 158(2) 8 . 8 ? C31 C22 H31b 34.7(12) 8 . 8 ? C31 C22 H322b 156(2) 8 . 8 ? C32 C22 N32 55.7(14) 8 . 8 ? C32 C22 C322 100.9(18) 8 . 8 ? C32 C22 H31b 97.6(19) 8 . 8 ? C32 C22 H322b 135(2) 8 . 8 ? N32 C22 C322 53.3(13) 8 . 8 ? N32 C22 H31b 139(2) 8 . 8 ? N32 C22 H322b 85.1(15) 8 . 8 ? C322 C22 H31b 161(2) 8 . 8 ? C322 C22 H322b 34.3(11) 8 . 8 ? H31b C22 H322b 127.5(16) 8 . 8 ? Er N22 C22 90.2(13) . . . ? Er N22 C221 125(2) . . . ? Er N22 C222 109.0(19) . . . ? Er N22 C32 111(2) . . 8 ? Er N22 N32 64(4) . . 8 ? Er N22 C321 113.2(16) . . 8 ? Er N22 C322 98.9(14) . . 8 ? C22 N22 C221 117(2) . . . ? C22 N22 C222 103(2) . . . ? C22 N22 C32 75(2) . . 8 ? C22 N22 N32 115(4) . . 8 ? C22 N22 C321 148(2) . . 8 ? C22 N22 C322 63.6(17) . . 8 ? C221 N22 C222 110(2) . . . ? C221 N22 C32 45(2) . . 8 ? C221 N22 N32 128(4) . . 8 ? C221 N22 C321 68(2) . . 8 ? C221 N22 C322 136(2) . . 8 ? C222 N22 C32 140(3) . . 8 ? C222 N22 N32 47(4) . . 8 ? C222 N22 C321 50.2(17) . . 8 ? C222 N22 C322 40.4(17) . . 8 ? C32 N22 N32 169(5) 8 . 8 ? C32 N22 C321 113(2) 8 . 8 ? C32 N22 C322 128(2) 8 . 8 ? N32 N22 C321 63(4) 8 . 8 ? N32 N22 C322 63(4) 8 . 8 ? C321 N22 C322 90.5(17) 8 . 8 ? N22 C221 H221a 106(3) . . . ? N22 C221 H221b 114(3) . . . ? N22 C221 H221c 115(3) . . . ? N22 C221 C32 56(2) . . 8 ? N22 C221 N32 10.2(10) . . 8 ? N22 C221 C321 63(2) . . 8 ? N22 C221 H32a 110(3) . . 8 ? N22 C221 H32b 86.1(19) . . 8 ? H221a C221 H221b 118(4) . . . ? H221a C221 H221c 98(3) . . . ? H221a C221 C32 103(4) . . 8 ? H221a C221 N32 106(3) . . 8 ? H221a C221 C321 84(3) . . 8 ? H221a C221 H32a 121(4) . . 8 ? H221a C221 H32b 57(2) . . 8 ? H221b C221 H221c 105(3) . . . ? H221b C221 C32 67(3) . . 8 ? H221b C221 N32 121(3) . . 8 ? H221b C221 C321 157(4) . . 8 ? H221b C221 H32a 4.8(3) . . 8 ? H221b C221 H32b 79(3) . . 8 ? H221c C221 C32 158(5) . . 8 ? H221c C221 N32 105(3) . . 8 ? H221c C221 C321 61(2) . . 8 ? H221c C221 H32a 107(3) . . 8 ? H221c C221 H32b 153(3) . . 8 ? C32 C221 N32 66(3) 8 . 8 ? C32 C221 C321 118(3) 8 . 8 ? C32 C221 H32a 64(3) 8 . 8 ? C32 C221 H32b 48(2) 8 . 8 ? N32 C221 C321 53.2(17) 8 . 8 ? N32 C221 H32a 116(3) 8 . 8 ? N32 C221 H32b 95.0(18) 8 . 8 ? C321 C221 H32a 154(4) 8 . 8 ? C321 C221 H32b 122(3) 8 . 8 ? H32a C221 H32b 80(2) 8 . 8 ? N22 C222 H222a 113(3) . . . ? N22 C222 H222b 122(4) . . . ? N22 C222 H222c 105(2) . . . ? N22 C222 N32 10.8(11) . . 8 ? N22 C222 C321 64.0(18) . . 8 ? N22 C222 C322 67(2) . . 8 ? N22 C222 H321b 80.6(19) . . 8 ? N22 C222 H321c 96(2) . . 8 ? N22 C222 H322a 88(3) . . 8 ? N22 C222 H322c 105(2) . . 8 ? H222a C222 H222b 106(3) . . . ? H222a C222 H222c 99(4) . . . ? H222a C222 N32 105(3) . . 8 ? H222a C222 C321 136(4) . . 8 ? H222a C222 C322 70(3) . . 8 ? H222a C222 H321b 163(4) . . 8 ? H222a C222 H321c 99(4) . . 8 ? H222a C222 H322a 103(3) . . 8 ? H222a C222 H322c 23.3(8) . . 8 ? H222b C222 H222c 109(3) . . . ? H222b C222 N32 132(5) . . 8 ? H222b C222 C321 111(4) . . 8 ? H222b C222 C322 89(4) . . 8 ? H222b C222 H321b 72(3) . . 8 ? H222b C222 H321c 119(3) . . 8 ? H222b C222 H322a 42(2) . . 8 ? H222b C222 H322c 95(3) . . 8 ? H222c C222 N32 100(2) . . 8 ? H222c C222 C321 48(2) . . 8 ? H222c C222 C322 161(5) . . 8 ? H222c C222 H321b 67(2) . . 8 ? H222c C222 H321c 10.3(5) . . 8 ? H222c C222 H322a 147(4) . . 8 ? H222c C222 H322c 122(4) . . 8 ? N32 C222 C321 64.1(18) 8 . 8 ? N32 C222 C322 69(2) 8 . 8 ? N32 C222 H321b 87(2) 8 . 8 ? N32 C222 H321c 90(2) 8 . 8 ? N32 C222 H322a 97(3) 8 . 8 ? N32 C222 H322c 100(2) 8 . 8 ? C321 C222 C322 131(3) 8 . 8 ? C321 C222 H321b 39.6(18) 8 . 8 ? C321 C222 H321c 42.9(19) 8 . 8 ? C321 C222 H322a 120(4) 8 . 8 ? C321 C222 H322c 154(4) 8 . 8 ? C322 C222 H321b 126(4) 8 . 8 ? C322 C222 H321c 152(4) 8 . 8 ? C322 C222 H322a 52(2) 8 . 8 ? C322 C222 H322c 48(2) 8 . 8 ? H321b C222 H321c 69.0(17) 8 . 8 ? H321b C222 H322a 87(3) 8 . 8 ? H321b C222 H322c 167(4) 8 . 8 ? H321c C222 H322a 154(4) 8 . 8 ? H321c C222 H322c 122(4) 8 . 8 ? H322a C222 H322c 81(2) 8 . 8 ? Er N31 Si3 133.4(8) . . . ? Er N31 C31 114.7(13) . . . ? Er N31 N11 75.9(11) . . 8 ? Er N31 Si1 141.8(9) . . 8 ? Si3 N31 C31 111.9(14) . . . ? Si3 N31 N11 72.8(11) . . 8 ? Si3 N31 Si1 8.7(3) . . 8 ? C31 N31 N11 130.6(18) . . 8 ? C31 N31 Si1 103.3(14) . . 8 ? N11 N31 Si1 76.9(11) 8 . 8 ? N31 Si3 C311 118.5(18) . . . ? N31 Si3 C312 110.4(18) . . . ? N31 Si3 C313 116.1(17) . . . ? N31 Si3 N11 34.9(7) . . 8 ? N31 Si3 Si1 55.8(18) . . 8 ? N31 Si3 C111 157.0(15) . . 8 ? N31 Si3 C112 80.5(10) . . 8 ? N31 Si3 C113 86.3(12) . . 8 ? C311 Si3 C312 97(3) . . . ? C311 Si3 C313 113(2) . . . ? C311 Si3 N11 153.0(19) . . 8 ? C311 Si3 Si1 91(3) . . 8 ? C311 Si3 C111 81(2) . . 8 ? C311 Si3 C112 71(2) . . 8 ? C311 Si3 C113 48(2) . . 8 ? C312 Si3 C313 97(3) . . . ? C312 Si3 N11 98.8(18) . . 8 ? C312 Si3 Si1 67(3) . . 8 ? C312 Si3 C111 52(2) . . 8 ? C312 Si3 C112 57(2) . . 8 ? C312 Si3 C113 145(2) . . 8 ? C313 Si3 N11 86.1(16) . . 8 ? C313 Si3 Si1 153(2) . . 8 ? C313 Si3 C111 59(2) . . 8 ? C313 Si3 C112 153.3(18) . . 8 ? C313 Si3 C113 103(2) . . 8 ? N11 Si3 Si1 75.9(18) 8 . 8 ? N11 Si3 C111 125.5(14) 8 . 8 ? N11 Si3 C112 100.7(10) 8 . 8 ? N11 Si3 C113 111.0(14) 8 . 8 ? Si1 Si3 C111 117(2) 8 . 8 ? Si1 Si3 C112 25.6(18) 8 . 8 ? Si1 Si3 C113 101(2) 8 . 8 ? C111 Si3 C112 97.2(15) 8 . 8 ? C111 Si3 C113 116.6(17) 8 . 8 ? C112 Si3 C113 98.3(17) 8 . 8 ? Si3 C311 H311a 106(4) . . . ? Si3 C311 H311b 109(3) . . . ? Si3 C311 H311c 119(4) . . . ? Si3 C311 Si1 9.1(4) . . 8 ? Si3 C311 C113 67(2) . . 8 ? Si3 C311 H113c 109(4) . . 8 ? H311a C311 H311b 108(5) . . . ? H311a C311 H311c 104(3) . . . ? H311a C311 Si1 109(4) . . 8 ? H311a C311 C113 39(2) . . 8 ? H311a C311 H113c 8.6(4) . . 8 ? H311b C311 H311c 110(6) . . . ? H311b C311 Si1 100(3) . . 8 ? H311b C311 C113 115(5) . . 8 ? H311b C311 H113c 113(5) . . 8 ? H311c C311 Si1 125(4) . . 8 ? H311c C311 C113 129(5) . . 8 ? H311c C311 H113c 96(3) . . 8 ? Si1 C311 C113 70(2) 8 . 8 ? Si1 C311 H113c 114(4) 8 . 8 ? C113 C311 H113c 45(2) 8 . 8 ? Si3 C312 H312a 122(6) . . . ? Si3 C312 H312b 106(5) . . . ? Si3 C312 H312c 110(4) . . . ? Si3 C312 Si1 8.6(4) . . 8 ? Si3 C312 C111 58(2) . . 8 ? Si3 C312 C112 67(2) . . 8 ? Si3 C312 H111b 92(4) . . 8 ? H312a C312 H312b 111(6) . . . ? H312a C312 H312c 111(7) . . . ? H312a C312 Si1 114(5) . . 8 ? H312a C312 C111 147(6) . . 8 ? H312a C312 C112 55(4) . . 8 ? H312a C312 H111b 143(7) . . 8 ? H312b C312 H312c 93(5) . . . ? H312b C312 Si1 109(5) . . 8 ? H312b C312 C111 99(5) . . 8 ? H312b C312 C112 137(5) . . 8 ? H312b C312 H111b 68(4) . . 8 ? H312c C312 Si1 118(4) . . 8 ? H312c C312 C111 53(3) . . 8 ? H312c C312 C112 130(5) . . 8 ? H312c C312 H111b 35.3(19) . . 8 ? Si1 C312 C111 66(3) 8 . 8 ? Si1 C312 C112 60(2) 8 . 8 ? Si1 C312 H111b 101(4) 8 . 8 ? C111 C312 C112 110(3) 8 . 8 ? C111 C312 H111b 40(2) 8 . 8 ? C112 C312 H111b 150(4) 8 . 8 ? Si3 C313 H313a 105(4) . . . ? Si3 C313 H313b 101(3) . . . ? Si3 C313 H313c 110(4) . . . ? Si3 C313 Si1 3.5(3) . . 8 ? Si3 C313 C111 56.1(19) . . 8 ? Si3 C313 H111a 85(3) . . 8 ? H313a C313 H313b 117(6) . . . ? H313a C313 H313c 116(5) . . . ? H313a C313 Si1 101(4) . . 8 ? H313a C313 C111 103(4) . . 8 ? H313a C313 H111a 105(5) . . 8 ? H313b C313 H313c 108(5) . . . ? H313b C313 Si1 103(3) . . 8 ? H313b C313 C111 139(4) . . 8 ? H313b C313 H111a 134(5) . . 8 ? H313c C313 Si1 112(4) . . 8 ? H313c C313 C111 61(3) . . 8 ? H313c C313 H111a 32.2(17) . . 8 ? Si1 C313 C111 56.2(18) 8 . 8 ? Si1 C313 H111a 85(3) 8 . 8 ? C111 C313 H111a 29.7(17) 8 . 8 ? N31 C31 C32 116(2) . . . ? N31 C31 H31a 106(2) . . . ? N31 C31 H31b 105(2) . . . ? N31 C31 C22 108(2) . . 8 ? N31 C31 H112b 105(2) . . 8 ? N31 C31 H22b 98(2) . . 8 ? C32 C31 H31a 114(3) . . . ? C32 C31 H31b 106(2) . . . ? C32 C31 C22 54.1(15) . . 8 ? C32 C31 H112b 135(2) . . 8 ? C32 C31 H22b 73(2) . . 8 ? H31a C31 H31b 108(3) . . . ? H31a C31 C22 145(3) . . 8 ? H31a C31 H112b 33.1(10) . . 8 ? H31a C31 H22b 147(4) . . 8 ? H31b C31 C22 56.5(16) . . 8 ? H31b C31 H112b 76(2) . . 8 ? H31b C31 H22b 42.9(14) . . 8 ? C22 C31 H112b 127(2) 8 . 8 ? C22 C31 H22b 18.9(14) 8 . 8 ? H112b C31 H22b 119(3) 8 . 8 ? C31 C32 N32 107(2) . . . ? C31 C32 H32a 106(2) . . . ? C31 C32 H32b 106(2) . . . ? C31 C32 C22 59.9(17) . . 8 ? C31 C32 N22 106(2) . . 8 ? C31 C32 C221 162(4) . . 8 ? C31 C32 H221b 114(2) . . 8 ? N32 C32 H32a 120(2) . . . ? N32 C32 H32b 120(3) . . . ? N32 C32 C22 63.2(16) . . 8 ? N32 C32 N22 2.7(12) . . 8 ? N32 C32 C221 77(3) . . 8 ? N32 C32 H221b 117(2) . . 8 ? H32a C32 H32b 97(2) . . . ? H32a C32 C22 165(3) . . 8 ? H32a C32 N22 123(3) . . 8 ? H32a C32 C221 59(3) . . 8 ? H32a C32 H221b 8.5(3) . . 8 ? H32b C32 C22 93(2) . . 8 ? H32b C32 N22 118(3) . . 8 ? H32b C32 C221 87(3) . . 8 ? H32b C32 H221b 93(2) . . 8 ? C22 C32 N22 61(2) 8 . 8 ? C22 C32 C221 134(4) 8 . 8 ? C22 C32 H221b 173(3) 8 . 8 ? N22 C32 C221 78(3) 8 . 8 ? N22 C32 H221b 119(3) 8 . 8 ? C221 C32 H221b 51(3) 8 . 8 ? Er N32 C32 105.5(14) . . . ? Er N32 C321 126.6(16) . . . ? Er N32 C322 108.9(14) . . . ? Er N32 C22 91.5(11) . . 8 ? Er N32 N22 109(4) . . 8 ? Er N32 C221 120.7(16) . . 8 ? Er N32 C222 126(2) . . 8 ? C32 N32 C321 102(2) . . . ? C32 N32 C322 113(2) . . . ? C32 N32 C22 61.0(16) . . 8 ? C32 N32 N22 9(4) . . 8 ? C32 N32 C221 36.9(18) . . 8 ? C32 N32 C222 128(3) . . 8 ? C321 N32 C322 101.1(17) . . . ? C321 N32 C22 142(2) . . 8 ? C321 N32 N22 105(4) . . 8 ? C321 N32 C221 65.9(19) . . 8 ? C321 N32 C222 57(2) . . 8 ? C322 N32 C22 62.1(16) . . 8 ? C322 N32 N22 104(4) . . 8 ? C322 N32 C221 126(2) . . 8 ? C322 N32 C222 45.6(19) . . 8 ? C22 N32 N22 54(4) 8 . 8 ? C22 N32 C221 95.4(17) 8 . 8 ? C22 N32 C222 105(2) 8 . 8 ? N22 N32 C221 42(4) 8 . 8 ? N22 N32 C222 122(5) 8 . 8 ? C221 N32 C222 109(2) 8 . 8 ? N32 C321 H321a 113(2) . . . ? N32 C321 H321b 108(3) . . . ? N32 C321 H321c 100(2) . . . ? N32 C321 N22 12.5(10) . . 8 ? N32 C321 C221 60.8(16) . . 8 ? N32 C321 C222 59.1(18) . . 8 ? N32 C321 H221c 92.2(17) . . 8 ? N32 C321 H222c 96(2) . . 8 ? H321a C321 H321b 112(3) . . . ? H321a C321 H321c 114(3) . . . ? H321a C321 N22 108(2) . . 8 ? H321a C321 C221 72(2) . . 8 ? H321a C321 C222 170(4) . . 8 ? H321a C321 H221c 34.2(12) . . 8 ? H321a C321 H222c 132(4) . . 8 ? H321b C321 H321c 109(3) . . . ? H321b C321 N22 100(3) . . 8 ? H321b C321 C221 85(3) . . 8 ? H321b C321 C222 77(3) . . 8 ? H321b C321 H221c 95(3) . . 8 ? H321b C321 H222c 93(2) . . 8 ? H321c C321 N22 113(2) . . 8 ? H321c C321 C221 160(3) . . 8 ? H321c C321 C222 64(3) . . 8 ? H321c C321 H221c 148(3) . . 8 ? H321c C321 H222c 18.8(6) . . 8 ? N22 C321 C221 49.0(15) 8 . 8 ? N22 C321 C222 66(2) 8 . 8 ? N22 C321 H221c 82.6(16) 8 . 8 ? N22 C321 H222c 107(2) 8 . 8 ? C221 C321 C222 107(3) 8 . 8 ? C221 C321 H221c 38.3(13) 8 . 8 ? C221 C321 H222c 155(3) 8 . 8 ? C222 C321 H221c 145(3) 8 . 8 ? C222 C321 H222c 48(2) 8 . 8 ? H221c C321 H222c 166(3) 8 . 8 ? N32 C322 H322a 104(2) . . . ? N32 C322 H322b 109(2) . . . ? N32 C322 H322c 111(3) . . . ? N32 C322 C21 105.5(18) . . 8 ? N32 C322 C22 64.6(14) . . 8 ? N32 C322 N22 12.8(10) . . 8 ? N32 C322 C222 65(2) . . 8 ? N32 C322 H21a 138(2) . . 8 ? N32 C322 H222a 94(2) . . 8 ? N32 C322 H222b 95.6(16) . . 8 ? H322a C322 H322b 109(3) . . . ? H322a C322 H322c 106(2) . . . ? H322a C322 C21 132(3) . . 8 ? H322a C322 C22 102(3) . . 8 ? H322a C322 N22 98(2) . . 8 ? H322a C322 C222 70(3) . . 8 ? H322a C322 H21a 116(2) . . 8 ? H322a C322 H222a 104(2) . . 8 ? H322a C322 H222b 34.2(8) . . 8 ? H322b C322 H322c 116(3) . . . ? H322b C322 C21 25.0(16) . . 8 ? H322b C322 C22 48.4(15) . . 8 ? H322b C322 N22 101(2) . . 8 ? H322b C322 C222 173(4) . . 8 ? H322b C322 H21a 48.0(12) . . 8 ? H322b C322 H222a 133(3) . . 8 ? H322b C322 H222b 141(3) . . 8 ? H322c C322 C21 97(2) . . 8 ? H322c C322 C22 151(3) . . 8 ? H322c C322 N22 124(3) . . 8 ? H322c C322 C222 70(3) . . 8 ? H322c C322 H21a 69.3(17) . . 8 ? H322c C322 H222a 19.0(7) . . 8 ? H322c C322 H222b 79.2(17) . . 8 ? C21 C322 C22 60.4(16) 8 . 8 ? C21 C322 N22 103.0(18) 8 . 8 ? C21 C322 C222 157(4) 8 . 8 ? C21 C322 H21a 36.9(12) 8 . 8 ? C21 C322 H222a 110(2) 8 . 8 ? C21 C322 H222b 159(2) 8 . 8 ? C22 C322 N22 54.4(13) 8 . 8 ? C22 C322 C222 125(3) 8 . 8 ? C22 C322 H21a 94.8(18) 8 . 8 ? C22 C322 H222a 149(2) 8 . 8 ? C22 C322 H222b 129(2) 8 . 8 ? N22 C322 C222 72(2) 8 . 8 ? N22 C322 H21a 139(2) 8 . 8 ? N22 C322 H222a 106(2) 8 . 8 ? N22 C322 H222b 96.6(16) 8 . 8 ? C222 C322 H21a 139(3) 8 . 8 ? C222 C322 H222a 53(3) 8 . 8 ? C222 C322 H222b 40(2) 8 . 8 ? H21a C322 H222a 87(2) 8 . 8 ? H21a C322 H222b 124.5(18) 8 . 8 ? H222a C322 H222b 72.1(13) 8 . 8 ? C111 H111a C313 111(3) . . 8 ? C111 H111a H313c 154.9(19) . . 8 ? C313 H111a H313c 54(2) 8 . 8 ? C111 H111b C312 90(3) . . 8 ? C111 H111b H312c 92(2) . . 8 ? C312 H111b H312c 63(3) 8 . 8 ? C112 H112b C31 117(2) . . 8 ? C112 H112b H31a 90.6(18) . . 8 ? C31 H112b H31a 40.6(12) 8 . 8 ? C113 H113c C311 85(3) . . 8 ? C113 H113c H311a 56(2) . . 8 ? C311 H113c H311a 47(2) 8 . 8 ? C11 H11b H121b 75.4(16) . . 8 ? C12 H12b C121 29(2) . . 8 ? C12 H12b H121a 96.2(18) . . 8 ? C121 H12b H121a 68.5(15) 8 . 8 ? C121 H121a C12 28(2) . . 8 ? C121 H121a H12b 73.5(15) . . 8 ? C12 H121a H12b 45.7(12) 8 . 8 ? C121 H121b C11 73(2) . . 8 ? C121 H121b H11b 135(2) . . 8 ? C11 H121b H11b 71.3(13) 8 . 8 ? C121 H121c C11 80(2) . . 8 ? C121 H121c C12 35(2) . . 8 ? C11 H121c C12 115(2) 8 . 8 ? C122 H122a C122 44(6) . . 8 ? C122 H122a H122a 51(3) . . 8 ? C122 H122a H122a 95(5) 8 . 8 ? C122 H122b C122 36(5) . . 8 ? C122 H122b H122b 85(4) . . 8 ? C122 H122b H122b 50(3) 8 . 8 ? C211 H211a C211 73(5) . . 8 ? C211 H211a H211a 42(2) . . 8 ? C211 H211a H211a 116(4) 8 . 8 ? C212 H212c C213 85(2) . . 8 ? C212 H212c H213a 27.7(15) . . 8 ? C213 H212c H213a 67.4(12) 8 . 8 ? C213 H213a C212 97(2) . . 8 ? C213 H213a H212c 103.2(12) . . 8 ? C212 H213a H212c 146.9(18) 8 . 8 ? C21 H21a C322 91.8(18) . . 8 ? C21 H21a H322b 54.0(17) . . 8 ? C322 H21a H322b 47.1(14) 8 . 8 ? C22 H22b C31 144(3) . . 8 ? C22 H22b H31b 122.1(15) . . 8 ? C31 H22b H31b 78(2) 8 . 8 ? C221 H221b C32 62(3) . . 8 ? C221 H221b H32a 147(2) . . 8 ? C32 H221b H32a 92.7(18) 8 . 8 ? C221 H221c C321 81(2) . . 8 ? C221 H221c H321a 114(2) . . 8 ? C321 H221c H321a 35.1(13) 8 . 8 ? C222 H222a C322 57(3) . . 8 ? C222 H222a H322c 94(2) . . 8 ? C322 H222a H322c 41.0(11) 8 . 8 ? C222 H222b C322 51(3) . . 8 ? C222 H222b H322a 91(3) . . 8 ? C322 H222b H322a 44.8(14) 8 . 8 ? C222 H222c C321 84(3) . . 8 ? C222 H222c H321c 135.4(17) . . 8 ? C321 H222c H321c 73.2(19) 8 . 8 ? C311 H311a C113 99(4) . . 8 ? C311 H311a H113c 124(3) . . 8 ? C113 H311a H113c 114(2) 8 . 8 ? C312 H312c C111 85(4) . . 8 ? C312 H312c H111b 82(4) . . 8 ? C111 H312c H111b 54.2(16) 8 . 8 ? C313 H313b H313b 136(3) . . 8 ? C313 H313c H111a 94(3) . . 8 ? C31 H31a C112 133(2) . . 8 ? C31 H31a H112b 106.4(19) . . 8 ? C112 H31a H112b 49.4(13) 8 . 8 ? C31 H31b C22 89(2) . . 8 ? C31 H31b H22b 58.6(18) . . 8 ? C22 H31b H22b 34.2(10) 8 . 8 ? C32 H32a C221 58(2) . . 8 ? C32 H32a H221b 78.8(17) . . 8 ? C221 H32a H221b 28(2) 8 . 8 ? C32 H32b C221 45(2) . . 8 ? C321 H321a H221c 111(2) . . 8 ? C321 H321b C222 63(2) . . 8 ? C321 H321c C222 73(2) . . 8 ? C321 H321c H222c 88.0(18) . . 8 ? C222 H321c H222c 34.2(14) 8 . 8 ? C322 H322a C222 58(2) . . 8 ? C322 H322a H222b 101.0(17) . . 8 ? C222 H322a H222b 47.8(15) 8 . 8 ? C322 H322b C21 128(3) . . 8 ? C322 H322b C22 97.3(19) . . 8 ? C322 H322b H21a 84.9(18) . . 8 ? C21 H322b C22 101(2) 8 . 8 ? C21 H322b H21a 65(2) 8 . 8 ? C22 H322b H21a 161.8(13) 8 . 8 ? C322 H322c C222 62(3) . . 8 ? C322 H322c H222a 119.9(16) . . 8 ? C222 H322c H222a 63(2) 8 . 8 ? loop_ _geom_torsion_atom_site_label_1 #ActaC _geom_torsion_atom_site_label_2 #ActaC _geom_torsion_atom_site_label_3 #ActaC _geom_torsion_atom_site_label_4 #ActaC _geom_torsion #ActaC _geom_torsion_site_symmetry_1 #ActaC _geom_torsion_site_symmetry_2 #ActaC _geom_torsion_site_symmetry_3 #ActaC _geom_torsion_site_symmetry_4 #ActaC _geom_torsion_publ_flag #ActaC ? ? ? ? ? ? ? ? ? ? _reflns_limit_h_min 0 _reflns_limit_h_max 24 _reflns_limit_k_min 0 _reflns_limit_k_max 21 _reflns_limit_l_min 0 _reflns_limit_l_max 13 _reflns_number_total 3887 #ActaC _reflns_number_observed 2356 #ActaC _reflns_observed_criterion refl_observed_if_F____>_.000_sigma(F___) _reflns_d_resolution_high .77 _reflns_d_resolution_low 9.538 loop_ _reflns_scale_group_code _reflns_scale_meas_F ? 1.2632 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_meas _refln_F_calc _refln_F_sigma _refln_observed_status _refln_scale_group_code 0 0 2 33.346 33.093 .552 o 1 0 0 4 147.715 142.485 1.554 o 1 0 0 6 142.683 139.484 1.571 o 1 0 0 8 66.729 66.746 1.069 o 1 0 0 10 58.416 60.397 1.175 o 1 0 0 12 7.155 9.521 3.425 < 1 0 1 1 288.015 310.161 3.042 o 1 0 1 3 72.374 68.868 .880 o 1 0 1 5 156.202 163.588 1.655 o 1 0 1 7 40.334 38.566 .933 o 1 0 1 9 60.389 61.270 1.084 o 1 0 1 11 46.416 44.142 1.188 o 1 0 1 13 5.810 8.315 3.195 < 1 0 2 0 386.606 379.468 3.855 o 1 0 2 2 99.857 103.535 1.101 o 1 0 2 4 183.984 187.656 1.913 o 1 0 2 6 114.442 110.092 1.343 o 1 0 2 8 45.907 47.537 1.024 o 1 0 2 10 62.540 62.559 1.162 o 1 0 2 12 5.663 7.423 3.101 < 1 0 3 1 86.659 94.111 .978 o 1 0 3 3 58.029 54.642 .847 o 1 0 3 5 146.306 151.658 1.598 o 1 0 3 7 68.649 70.790 1.109 o 1 0 3 9 62.755 65.656 1.140 o 1 0 3 11 40.106 39.829 1.255 o 1 0 3 13 5.661 5.957 3.099 < 1 0 4 0 88.153 88.077 1.014 o 1 0 4 2 37.319 36.128 .810 o 1 0 4 4 214.611 209.323 2.232 o 1 0 4 6 119.802 119.009 1.425 o 1 0 4 8 40.327 41.212 1.118 o 1 0 4 10 59.986 62.357 1.219 o 1 0 4 12 4.483 7.407 2.899 < 1 0 5 1 120.673 122.444 1.323 o 1 0 5 3 34.839 35.072 .914 o 1 0 5 5 157.501 156.229 1.735 o 1 0 5 7 51.325 53.553 1.114 o 1 0 5 9 56.388 61.698 1.208 o 1 0 5 11 39.394 38.418 1.329 o 1 0 6 0 237.128 229.027 3.321 o 1 0 6 2 1.062 .753 2.551 < 1 0 6 4 135.103 135.546 1.522 o 1 0 6 6 130.722 131.835 1.570 o 1 0 6 8 49.699 49.997 1.197 o 1 0 6 10 53.707 53.509 1.319 o 1 0 6 12 9.976 9.395 3.664 < 1 0 7 1 103.080 128.962 1.208 o 1 0 7 3 .936 4.020 2.348 < 1 0 7 5 128.802 124.892 1.524 o 1 0 7 7 25.548 25.123 1.480 o 1 0 7 9 44.591 47.034 1.313 o 1 0 7 11 35.087 37.629 1.646 o 1 0 8 0 230.257 218.826 3.567 o 1 0 8 2 21.948 21.521 1.008 o 1 0 8 4 90.523 105.255 1.219 o 1 0 8 6 86.614 82.957 1.269 o 1 0 8 8 29.983 33.151 1.386 o 1 0 8 10 50.575 49.904 1.407 o 1 0 8 12 9.403 6.985 3.947 < 1 0 9 1 112.876 126.348 1.341 o 1 0 9 3 23.322 26.278 1.256 o 1 0 9 5 82.339 85.059 1.218 o 1 0 9 7 23.966 23.744 1.506 o 1 0 9 9 39.750 41.600 1.401 o 1 0 9 11 28.465 30.257 1.833 o 1 0 10 0 152.812 141.036 1.693 o 1 0 10 2 75.273 81.016 1.115 o 1 0 10 4 115.294 126.892 1.445 o 1 0 10 6 52.636 51.338 1.153 o 1 0 10 8 16.222 19.446 2.101 o 1 0 10 10 43.948 42.594 1.441 o 1 0 11 1 87.691 111.995 1.218 o 1 0 11 3 39.707 43.990 1.054 o 1 0 11 5 79.583 81.369 1.239 o 1 0 11 7 27.122 24.127 1.466 o 1 0 11 9 41.783 39.978 1.392 o 1 0 11 11 23.134 22.812 1.922 o 1 0 12 0 139.134 129.628 1.618 o 1 0 12 2 24.392 27.557 1.436 o 1 0 12 4 72.522 84.597 1.204 o 1 0 12 6 56.145 60.223 1.235 o 1 0 12 8 22.811 24.752 1.785 o 1 0 12 10 33.067 29.926 1.564 o 1 0 13 1 51.796 63.597 1.101 o 1 0 13 3 19.206 21.916 1.654 o 1 0 13 5 76.464 78.053 1.275 o 1 0 13 7 7.877 15.118 3.801 < 1 0 13 9 28.490 26.437 1.472 o 1 0 14 0 97.451 91.683 1.342 o 1 0 14 2 9.478 12.654 3.462 < 1 0 14 4 47.073 55.328 1.213 o 1 0 14 6 47.405 48.937 1.285 o 1 0 14 8 17.568 16.175 1.995 o 1 0 14 10 23.234 24.861 2.021 o 1 0 15 1 37.302 51.166 1.237 o 1 0 15 3 16.191 15.094 1.711 o 1 0 15 5 53.647 55.306 1.263 o 1 0 15 7 6.078 11.622 3.350 < 1 0 15 9 16.884 20.340 2.425 o 1 0 16 0 63.312 60.128 1.219 o 1 0 16 2 17.743 23.528 1.981 o 1 0 16 4 39.244 46.060 1.346 o 1 0 16 6 24.793 26.699 1.610 o 1 0 16 8 11.513 7.645 3.565 < 1 0 17 1 34.979 41.833 1.413 o 1 0 17 3 4.516 14.125 3.013 < 1 0 17 5 32.525 33.416 1.478 o 1 0 17 7 4.103 10.959 2.863 < 1 0 18 0 43.594 38.628 1.370 o 1 0 18 2 11.017 16.300 3.430 < 1 0 18 4 26.762 31.226 1.663 o 1 0 18 6 21.498 20.701 1.898 o 1 0 19 1 26.136 27.156 1.452 o 1 0 19 3 6.255 9.857 3.443 < 1 0 19 5 19.802 24.855 2.052 o 1 0 20 0 36.207 31.443 1.384 o 1 0 20 2 4.591 5.272 2.939 < 1 0 20 4 16.096 18.037 2.330 o 1 0 21 1 9.750 18.430 4.151 < 1 0 21 3 4.082 5.316 2.779 < 1 1 0 1 240.940 238.096 1.837 o 1 1 0 2 84.829 86.166 .651 o 1 1 0 3 179.627 167.100 2.110 o 1 1 0 4 41.073 41.892 .526 o 1 1 0 5 13.647 13.747 .982 o 1 1 0 6 72.678 69.127 2.532 o 1 1 0 7 118.920 118.209 1.621 o 1 1 0 8 34.650 36.532 .802 o 1 1 0 9 35.154 35.823 .802 o 1 1 0 10 8.535 2.567 3.654 < 1 1 0 11 26.064 26.319 .987 o 1 1 0 12 21.061 23.146 1.214 o 1 1 0 13 21.937 20.896 1.395 o 1 1 1 1 147.774 144.403 3.699 o 1 1 1 2 102.792 101.117 1.485 o 1 1 1 3 86.004 78.599 .696 o 1 1 1 4 63.558 63.332 1.102 o 1 1 1 5 17.730 17.997 .831 o 1 1 1 6 52.203 52.246 .694 o 1 1 1 7 65.891 66.826 .995 o 1 1 1 8 83.333 83.019 .821 o 1 1 1 9 25.566 26.539 .856 o 1 1 1 10 8.529 8.132 2.276 < 1 1 1 11 16.753 16.097 1.181 o 1 1 1 12 27.475 29.701 1.587 o 1 1 1 13 18.714 17.380 1.252 o 1 1 2 1 140.344 136.348 3.925 o 1 1 2 2 110.860 110.470 3.776 o 1 1 2 3 186.562 184.282 3.290 o 1 1 2 4 66.867 66.832 .896 o 1 1 2 5 17.863 16.442 .776 o 1 1 2 6 51.167 52.616 1.620 o 1 1 2 7 103.295 99.150 .931 o 1 1 2 8 50.881 52.030 .930 o 1 1 2 9 31.988 30.735 .828 o 1 1 2 10 2.810 1.135 1.940 < 1 1 2 11 27.470 27.938 1.027 o 1 1 2 12 21.391 21.504 1.152 o 1 1 2 13 18.783 20.902 2.149 o 1 1 3 1 76.523 88.479 7.552 o 1 1 3 2 137.103 127.324 3.365 o 1 1 3 3 153.222 146.470 5.518 o 1 1 3 4 97.691 97.808 3.543 o 1 1 3 5 26.494 26.287 .694 o 1 1 3 6 36.292 33.954 1.610 o 1 1 3 7 45.482 43.441 .762 o 1 1 3 8 74.088 75.089 .853 o 1 1 3 9 33.923 33.912 .875 o 1 1 3 10 3.152 2.511 2.174 < 1 1 3 11 18.857 20.144 2.235 o 1 1 3 12 26.884 28.741 1.105 o 1 1 3 13 12.055 15.592 2.581 < 1 1 4 1 126.826 117.596 1.613 o 1 1 4 2 129.635 138.123 7.868 o 1 1 4 3 178.361 172.204 5.301 o 1 1 4 4 40.313 42.986 1.119 o 1 1 4 5 17.907 16.668 .856 o 1 1 4 6 30.377 30.739 .763 o 1 1 4 7 91.196 92.476 3.379 o 1 1 4 8 61.771 61.353 1.631 o 1 1 4 9 22.715 23.946 1.283 o 1 1 4 10 3.675 3.276 2.414 < 1 1 4 11 26.289 27.553 1.214 o 1 1 4 12 16.604 19.656 1.512 o 1 1 5 1 40.323 42.013 .553 o 1 1 5 2 142.762 129.927 3.830 o 1 1 5 3 91.976 94.462 6.583 o 1 1 5 4 95.379 94.275 2.338 o 1 1 5 5 4.276 6.041 2.800 < 1 1 5 6 35.152 35.613 1.225 o 1 1 5 7 59.270 60.104 2.495 o 1 1 5 8 62.961 65.219 2.212 o 1 1 5 9 26.694 28.235 1.731 o 1 1 5 10 4.200 2.319 2.566 < 1 1 5 11 15.710 15.711 1.491 o 1 1 5 12 25.657 27.265 1.142 o 1 1 6 1 128.937 122.853 2.069 o 1 1 6 2 70.834 89.172 3.569 o 1 1 6 3 149.109 143.903 3.155 o 1 1 6 4 63.051 65.628 2.466 o 1 1 6 5 8.112 4.237 2.147 < 1 1 6 6 50.167 48.819 .935 o 1 1 6 7 89.309 92.669 2.216 o 1 1 6 8 44.525 45.085 .846 o 1 1 6 9 26.074 25.726 1.196 o 1 1 6 10 3.791 2.962 2.477 < 1 1 6 11 24.575 23.464 2.483 o 1 1 6 12 19.306 20.038 1.489 o 1 1 7 1 80.866 99.944 4.565 o 1 1 7 2 119.152 107.312 1.244 o 1 1 7 3 37.739 48.170 2.407 o 1 1 7 4 77.527 76.793 .770 o 1 1 7 5 24.424 23.114 .824 o 1 1 7 6 38.545 37.624 .784 o 1 1 7 7 59.502 60.249 .882 o 1 1 7 8 60.213 60.230 3.200 o 1 1 7 9 21.495 23.170 1.233 o 1 1 7 10 5.036 5.788 2.837 < 1 1 7 11 10.850 12.643 2.825 < 1 1 7 12 23.388 24.795 2.819 o 1 1 8 1 109.514 107.225 .912 o 1 1 8 2 71.269 87.874 3.295 o 1 1 8 3 122.496 117.413 1.005 o 1 1 8 4 43.574 48.607 1.908 o 1 1 8 5 12.098 8.075 1.417 o 1 1 8 6 39.820 38.756 .953 o 1 1 8 7 76.495 75.492 .889 o 1 1 8 8 34.320 36.850 1.004 o 1 1 8 9 30.342 28.421 1.633 o 1 1 8 10 5.355 2.967 3.496 < 1 1 8 11 20.979 20.301 1.608 o 1 1 8 12 16.671 17.304 2.364 o 1 1 9 1 29.855 34.585 1.607 o 1 1 9 2 96.603 91.764 1.095 o 1 1 9 3 79.185 91.485 2.415 o 1 1 9 4 51.864 49.535 .733 o 1 1 9 5 11.730 13.678 1.741 o 1 1 9 6 38.200 35.908 1.788 o 1 1 9 7 36.284 36.680 1.061 o 1 1 9 8 51.725 51.961 .908 o 1 1 9 9 24.828 24.417 1.167 o 1 1 9 10 3.495 3.960 2.306 < 1 1 9 11 13.464 13.409 1.903 o 1 1 9 12 18.614 20.923 3.981 < 1 1 10 1 65.001 64.108 .737 o 1 1 10 2 73.350 85.493 2.508 o 1 1 10 3 111.892 107.228 1.245 o 1 1 10 4 23.428 25.470 1.363 o 1 1 10 5 16.297 18.809 1.558 o 1 1 10 6 24.796 26.107 1.028 o 1 1 10 7 57.839 55.951 .879 o 1 1 10 8 35.509 34.850 .991 o 1 1 10 9 24.428 22.499 1.167 o 1 1 10 10 6.250 3.276 4.076 < 1 1 10 11 16.327 16.380 1.754 o 1 1 11 1 18.668 23.966 1.013 o 1 1 11 2 84.813 79.534 .840 o 1 1 11 3 64.373 73.514 .786 o 1 1 11 4 39.340 38.284 1.187 o 1 1 11 5 8.637 10.318 2.730 < 1 1 11 6 34.583 31.530 1.007 o 1 1 11 7 29.670 30.575 .971 o 1 1 11 8 45.162 42.544 .956 o 1 1 11 9 13.931 15.887 1.877 < 1 1 11 10 5.394 2.154 3.258 < 1 1 11 11 7.291 9.179 3.500 < 1 1 12 1 57.445 54.649 .777 o 1 1 12 2 52.390 59.207 1.799 o 1 1 12 3 83.276 78.027 .862 o 1 1 12 4 24.454 26.203 .942 o 1 1 12 5 3.632 3.800 2.373 < 1 1 12 6 21.042 21.351 1.182 o 1 1 12 7 49.049 47.365 1.622 o 1 1 12 8 22.926 27.573 2.041 o 1 1 12 9 15.882 15.522 1.588 o 1 1 12 10 4.785 1.801 3.227 < 1 1 12 11 14.834 13.382 1.996 < 1 1 13 1 37.258 41.034 .869 o 1 1 13 2 60.505 55.567 .799 o 1 1 13 3 24.927 29.918 .982 o 1 1 13 4 43.994 40.383 .874 o 1 1 13 5 12.896 11.670 1.609 o 1 1 13 6 28.003 26.137 1.070 o 1 1 13 7 33.303 32.700 1.278 o 1 1 13 8 30.825 31.690 1.106 o 1 1 13 9 5.155 8.577 2.856 < 1 1 13 10 6.632 1.557 3.228 < 1 1 14 1 41.763 39.208 .808 o 1 1 14 2 29.936 32.914 1.310 o 1 1 14 3 63.778 57.896 .837 o 1 1 14 4 25.074 29.086 1.222 o 1 1 14 5 6.297 .611 3.048 < 1 1 14 6 22.391 21.315 1.187 o 1 1 14 7 38.448 35.626 .954 o 1 1 14 8 13.899 17.449 1.853 < 1 1 14 9 15.158 12.719 1.713 o 1 1 14 10 8.328 1.439 3.107 < 1 1 15 1 19.162 22.966 1.187 o 1 1 15 2 49.399 44.310 1.150 o 1 1 15 3 23.444 29.947 1.113 o 1 1 15 4 28.170 29.461 1.654 o 1 1 15 5 2.942 2.038 2.129 < 1 1 15 6 23.002 19.332 1.132 o 1 1 15 7 18.237 19.559 1.593 o 1 1 15 8 23.352 24.069 1.301 o 1 1 15 9 8.963 11.141 3.306 < 1 1 16 1 28.097 27.611 1.007 o 1 1 16 2 23.880 29.011 1.086 o 1 1 16 3 47.493 43.271 .874 o 1 1 16 4 11.212 15.074 2.928 < 1 1 16 5 5.039 3.990 3.292 < 1 1 16 6 10.436 11.459 2.723 < 1 1 16 7 26.643 24.715 1.345 o 1 1 16 8 14.518 16.266 1.839 o 1 1 16 9 8.203 11.167 3.463 < 1 1 17 1 3.529 8.060 2.441 < 1 1 17 2 38.412 34.545 .884 o 1 1 17 3 20.927 28.487 1.303 o 1 1 17 4 18.940 17.896 1.246 o 1 1 17 5 3.779 2.752 2.482 < 1 1 17 6 16.300 13.644 1.583 o 1 1 17 7 5.277 13.010 3.004 < 1 1 17 8 18.387 19.134 1.706 o 1 1 18 1 21.043 18.869 1.197 o 1 1 18 2 18.810 22.315 1.354 o 1 1 18 3 32.448 29.659 1.001 o 1 1 18 4 6.454 9.927 3.095 < 1 1 18 5 2.492 1.561 1.806 < 1 1 18 6 4.112 6.949 2.674 < 1 1 18 7 21.818 18.538 1.396 o 1 1 19 1 8.727 12.682 4.648 < 1 1 19 2 28.589 25.140 1.193 o 1 1 19 3 12.744 16.187 1.768 o 1 1 19 4 14.783 13.999 3.161 < 1 1 19 5 7.242 2.105 3.096 < 1 1 19 6 16.511 10.361 2.291 o 1 1 20 1 17.629 14.709 1.404 o 1 1 20 2 16.074 15.884 1.441 o 1 1 20 3 18.187 20.307 1.604 o 1 1 20 4 5.357 9.761 2.955 < 1 1 20 5 2.958 .344 2.097 < 1 1 21 1 8.557 10.537 3.160 < 1 1 21 2 17.384 17.499 1.644 o 1 1 21 3 5.391 11.935 3.000 < 1 2 0 0 91.428 89.997 1.027 o 1 2 0 1 265.407 259.607 4.124 o 1 2 0 2 185.003 175.749 1.723 o 1 2 0 3 140.889 136.043 1.045 o 1 2 0 4 69.141 72.513 .628 o 1 2 0 5 168.017 167.055 1.252 o 1 2 0 6 4.861 .347 2.951 < 1 2 0 7 11.010 9.957 1.321 < 1 2 0 8 12.552 14.589 1.319 o 1 2 0 9 66.013 67.068 1.805 o 1 2 0 10 23.297 23.233 1.038 o 1 2 0 11 38.082 38.036 .967 o 1 2 0 12 4.321 1.700 2.685 < 1 2 0 13 10.032 9.910 4.814 < 1 2 1 0 346.839 329.833 6.696 o 1 2 1 1 43.400 41.000 2.638 o 1 2 1 2 43.509 40.865 .442 o 1 2 1 3 29.019 28.640 .476 o 1 2 1 4 142.548 139.826 1.067 o 1 2 1 5 9.923 5.229 .993 o 1 2 1 6 131.703 129.658 1.041 o 1 2 1 7 34.234 34.744 .701 o 1 2 1 8 34.595 34.166 .725 o 1 2 1 9 17.434 17.873 1.022 o 1 2 1 10 59.271 59.792 .838 o 1 2 1 11 15.512 14.637 1.347 o 1 2 1 12 16.406 12.504 2.275 o 1 2 1 13 3.778 .146 2.490 < 1 2 2 0 136.220 152.826 7.638 o 1 2 2 1 215.898 202.899 3.222 o 1 2 2 2 26.777 23.650 1.341 o 1 2 2 3 95.784 90.900 1.741 o 1 2 2 4 24.142 26.504 .561 o 1 2 2 5 170.466 168.816 1.436 o 1 2 2 6 37.241 37.218 .659 o 1 2 2 7 28.079 27.348 1.095 o 1 2 2 8 23.638 24.384 .861 o 1 2 2 9 69.501 66.721 .822 o 1 2 2 10 15.559 17.059 2.331 o 1 2 2 11 34.966 36.550 .969 o 1 2 2 12 4.564 .680 2.687 < 1 2 2 13 10.354 9.137 2.701 < 1 2 3 0 130.777 121.918 2.082 o 1 2 3 1 76.102 85.875 2.112 o 1 2 3 2 68.805 66.347 1.541 o 1 2 3 3 3.746 7.622 2.166 < 1 2 3 4 139.143 137.890 3.416 o 1 2 3 5 37.895 37.614 .605 o 1 2 3 6 107.583 103.031 1.211 o 1 2 3 7 16.458 15.616 1.068 o 1 2 3 8 23.738 24.094 1.134 o 1 2 3 9 4.956 7.252 2.696 < 1 2 3 10 59.950 60.470 .883 o 1 2 3 11 14.367 15.653 1.646 o 1 2 3 12 13.435 10.711 1.829 o 1 2 3 13 8.806 1.091 3.720 < 1 2 4 0 52.846 55.177 .750 o 1 2 4 1 203.123 197.792 2.554 o 1 2 4 2 58.039 55.046 3.990 o 1 2 4 3 64.843 68.339 2.159 o 1 2 4 4 45.511 48.079 1.483 o 1 2 4 5 159.385 156.393 4.422 o 1 2 4 6 56.484 54.894 1.147 o 1 2 4 7 41.670 43.023 .757 o 1 2 4 8 26.136 26.445 .895 o 1 2 4 9 64.733 65.275 .867 o 1 2 4 10 13.482 15.446 1.695 o 1 2 4 11 34.096 33.589 2.257 o 1 2 4 12 3.916 1.671 2.494 < 1 2 5 0 220.568 207.385 3.041 o 1 2 5 1 36.529 36.964 .554 o 1 2 5 2 77.339 73.563 1.364 o 1 2 5 3 3.552 .596 2.327 < 1 2 5 4 118.213 117.852 2.701 o 1 2 5 5 47.065 46.869 .749 o 1 2 5 6 107.239 109.409 3.024 o 1 2 5 7 15.636 15.419 1.242 o 1 2 5 8 29.442 29.233 .908 o 1 2 5 9 11.609 12.664 1.729 < 1 2 5 10 54.370 55.464 2.247 o 1 2 5 11 12.727 13.243 1.847 < 1 2 5 12 16.042 11.336 1.504 o 1 2 6 0 64.771 65.479 .904 o 1 2 6 1 180.059 167.985 4.056 o 1 2 6 2 27.597 29.065 .597 o 1 2 6 3 53.010 49.698 1.507 o 1 2 6 4 96.957 102.142 5.607 o 1 2 6 5 147.627 149.408 5.042 o 1 2 6 6 23.799 24.178 1.120 o 1 2 6 7 25.140 25.120 .976 o 1 2 6 8 15.746 15.386 1.706 o 1 2 6 9 52.368 53.300 2.314 o 1 2 6 10 19.055 20.422 1.403 o 1 2 6 11 33.714 32.394 1.037 o 1 2 6 12 4.513 .051 2.783 < 1 2 7 0 220.050 206.390 3.357 o 1 2 7 1 55.399 65.020 4.833 o 1 2 7 2 22.637 22.317 .739 o 1 2 7 3 10.700 5.708 1.222 < 1 2 7 4 94.202 85.747 3.310 o 1 2 7 5 12.523 13.372 1.467 o 1 2 7 6 92.639 93.644 2.659 o 1 2 7 7 20.166 19.370 1.088 o 1 2 7 8 26.537 27.123 1.006 o 1 2 7 9 10.192 16.648 4.303 < 1 2 7 10 47.913 49.108 .943 o 1 2 7 11 9.575 9.265 4.590 < 1 2 7 12 10.118 10.871 4.273 < 1 2 8 0 57.664 61.269 .933 o 1 2 8 1 134.750 128.332 2.143 o 1 2 8 2 29.617 32.703 .696 o 1 2 8 3 47.776 45.701 1.558 o 1 2 8 4 46.621 51.648 4.210 o 1 2 8 5 114.198 112.345 4.065 o 1 2 8 6 19.098 19.766 1.162 o 1 2 8 7 19.980 18.806 2.106 o 1 2 8 8 14.810 11.471 1.394 o 1 2 8 9 43.564 44.168 .897 o 1 2 8 10 14.327 14.471 1.708 o 1 2 8 11 29.080 28.361 4.241 o 1 2 8 12 6.388 1.589 3.791 < 1 2 9 0 149.562 140.383 1.649 o 1 2 9 1 27.919 32.555 2.933 o 1 2 9 2 52.294 49.381 .790 o 1 2 9 3 6.394 9.764 3.641 < 1 2 9 4 103.865 98.938 1.686 o 1 2 9 5 14.436 14.835 1.396 o 1 2 9 6 66.944 64.693 1.448 o 1 2 9 7 9.410 11.830 3.490 < 1 2 9 8 16.021 16.104 1.368 o 1 2 9 9 7.356 9.763 4.361 < 1 2 9 10 43.603 43.804 2.792 o 1 2 9 11 11.700 11.202 4.320 < 1 2 10 0 82.064 87.317 1.147 o 1 2 10 1 124.657 120.002 1.036 o 1 2 10 2 5.832 11.306 3.052 < 1 2 10 3 49.972 46.147 .740 o 1 2 10 4 10.050 11.444 2.150 < 1 2 10 5 96.630 94.491 2.320 o 1 2 10 6 29.473 28.272 .913 o 1 2 10 7 19.614 18.115 1.257 o 1 2 10 8 10.659 12.243 4.554 < 1 2 10 9 43.669 41.557 2.059 o 1 2 10 10 12.041 9.824 3.724 < 1 2 10 11 20.571 22.760 3.121 o 1 2 11 0 123.439 117.658 1.485 o 1 2 11 1 13.243 14.538 1.313 o 1 2 11 2 46.991 44.453 .745 o 1 2 11 3 4.712 5.222 2.735 < 1 2 11 4 89.034 86.889 1.430 o 1 2 11 5 23.955 26.096 1.114 o 1 2 11 6 57.192 56.605 .968 o 1 2 11 7 7.115 6.397 2.996 < 1 2 11 8 19.424 16.851 1.263 o 1 2 11 9 5.251 4.741 2.867 < 1 2 11 10 32.562 33.303 1.156 o 1 2 11 11 6.918 10.132 3.336 < 1 2 12 0 26.385 28.470 1.288 o 1 2 12 1 92.643 85.873 .906 o 1 2 12 2 12.479 12.071 1.449 o 1 2 12 3 36.911 36.143 .821 o 1 2 12 4 30.520 32.843 .919 o 1 2 12 5 84.620 77.093 1.665 o 1 2 12 6 12.691 14.197 1.626 o 1 2 12 7 14.587 14.915 1.609 o 1 2 12 8 5.510 3.418 2.930 < 1 2 12 9 34.608 33.753 1.088 o 1 2 12 10 13.210 10.965 1.931 < 1 2 13 0 94.950 89.002 1.318 o 1 2 13 1 3.535 8.261 2.370 < 1 2 13 2 18.373 16.702 1.232 o 1 2 13 3 7.141 7.731 2.998 < 1 2 13 4 57.746 51.486 .841 o 1 2 13 5 10.406 16.773 2.711 < 1 2 13 6 55.936 52.940 .895 o 1 2 13 7 10.085 9.940 4.289 < 1 2 13 8 16.214 16.180 4.236 < 1 2 13 9 9.299 7.035 4.934 < 1 2 13 10 27.551 26.029 1.313 o 1 2 14 0 5.288 7.727 3.046 < 1 2 14 1 60.325 56.513 .825 o 1 2 14 2 15.490 15.643 1.355 o 1 2 14 3 16.854 18.119 4.389 < 1 2 14 4 22.018 26.604 2.869 o 1 2 14 5 65.007 62.574 1.375 o 1 2 14 6 7.010 8.175 3.825 < 1 2 14 7 5.827 9.308 3.206 < 1 2 14 8 3.441 2.315 2.339 < 1 2 14 9 22.264 23.476 1.399 o 1 2 14 10 9.115 7.733 3.357 < 1 2 15 0 70.628 65.827 1.224 o 1 2 15 1 9.686 11.304 2.525 < 1 2 15 2 22.188 18.543 1.094 o 1 2 15 3 5.260 4.058 2.795 < 1 2 15 4 45.629 43.711 1.149 o 1 2 15 5 14.233 11.000 1.407 o 1 2 15 6 32.486 33.255 1.088 o 1 2 15 7 7.251 6.854 3.087 < 1 2 15 8 6.922 8.103 3.313 < 1 2 15 9 4.861 6.878 2.898 < 1 2 16 0 22.023 23.570 1.587 o 1 2 16 1 52.443 47.366 1.171 o 1 2 16 2 4.866 3.714 2.638 < 1 2 16 3 19.043 17.310 1.273 o 1 2 16 4 8.370 9.630 4.434 < 1 2 16 5 42.671 40.033 .955 o 1 2 16 6 3.988 10.203 2.633 < 1 2 16 7 8.231 9.923 4.372 < 1 2 16 8 5.965 6.318 3.201 < 1 2 17 0 49.197 44.798 1.270 o 1 2 17 1 9.155 12.301 2.834 < 1 2 17 2 19.205 17.413 1.745 o 1 2 17 3 3.834 .423 2.437 < 1 2 17 4 36.598 33.502 1.663 o 1 2 17 5 13.536 11.439 1.547 < 1 2 17 6 24.864 22.790 2.773 o 1 2 17 7 5.391 .735 2.863 < 1 2 17 8 3.846 6.008 2.577 < 1 2 18 0 19.215 18.550 1.885 o 1 2 18 1 33.950 32.026 .998 o 1 2 18 2 3.767 1.692 2.396 < 1 2 18 3 12.680 12.469 1.748 < 1 2 18 4 5.364 8.062 3.578 < 1 2 18 5 30.936 27.901 1.092 o 1 2 18 6 5.142 6.597 3.432 < 1 2 18 7 9.429 7.810 3.982 < 1 2 19 0 35.791 32.948 1.390 o 1 2 19 1 7.401 8.023 3.115 < 1 2 19 2 8.975 8.251 4.291 < 1 2 19 3 3.220 1.755 2.176 < 1 2 19 4 20.855 20.395 1.381 o 1 2 19 5 12.783 8.875 1.742 < 1 2 19 6 21.332 19.089 2.098 o 1 2 20 0 9.501 6.270 3.484 < 1 2 20 1 22.873 21.429 1.318 o 1 2 20 2 8.372 4.975 3.109 < 1 2 20 3 7.470 7.065 3.964 < 1 2 20 4 6.738 9.168 3.598 < 1 2 20 5 25.209 22.259 1.794 o 1 2 21 0 26.463 23.297 1.797 o 1 2 21 1 7.489 6.050 3.159 < 1 2 21 2 6.465 6.491 3.427 < 1 2 21 3 3.034 3.062 2.173 < 1 3 0 1 73.222 73.248 2.979 o 1 3 0 2 277.055 277.727 3.514 o 1 3 0 3 51.802 47.414 .521 o 1 3 0 4 69.830 66.893 .630 o 1 3 0 5 17.052 17.967 .678 o 1 3 0 6 97.123 95.799 .840 o 1 3 0 7 13.873 16.084 1.074 o 1 3 0 8 100.542 101.473 1.059 o 1 3 0 9 10.647 13.315 3.306 < 1 3 0 10 4.396 4.344 2.463 < 1 3 0 11 3.247 5.083 2.175 < 1 3 0 12 33.779 33.045 .929 o 1 3 0 13 13.383 11.486 1.760 < 1 3 1 1 64.198 68.292 3.768 o 1 3 1 2 90.368 89.430 .707 o 1 3 1 3 221.076 229.337 4.981 o 1 3 1 4 35.515 35.068 .510 o 1 3 1 5 9.857 7.742 1.030 o 1 3 1 6 47.213 47.184 .639 o 1 3 1 7 105.817 103.885 1.162 o 1 3 1 8 12.503 7.743 1.235 o 1 3 1 9 53.352 52.223 .781 o 1 3 1 10 4.609 3.072 2.500 < 1 3 1 11 26.180 28.061 1.946 o 1 3 1 12 13.946 13.398 1.486 o 1 3 1 13 26.611 27.414 1.410 o 1 3 2 1 64.328 61.978 .746 o 1 3 2 2 240.471 253.462 8.317 o 1 3 2 3 77.530 76.005 .723 o 1 3 2 4 104.544 102.779 .863 o 1 3 2 5 14.766 13.557 1.398 o 1 3 2 6 96.556 90.729 .845 o 1 3 2 7 2.533 6.685 2.224 < 1 3 2 8 90.132 89.915 .854 o 1 3 2 9 21.897 23.340 .967 o 1 3 2 10 3.347 3.179 2.182 < 1 3 2 11 4.530 6.848 2.483 < 1 3 2 12 34.334 34.323 .937 o 1 3 2 13 10.893 9.330 3.384 < 1 3 3 1 166.319 181.253 4.702 o 1 3 3 2 83.992 77.675 1.618 o 1 3 3 3 146.227 155.346 7.848 o 1 3 3 4 39.340 37.990 .551 o 1 3 3 5 42.941 41.098 .606 o 1 3 3 6 35.013 33.434 .649 o 1 3 3 7 107.202 108.003 1.559 o 1 3 3 8 36.596 36.822 .761 o 1 3 3 9 39.682 38.540 .821 o 1 3 3 10 3.807 3.857 2.339 < 1 3 3 11 23.747 26.027 1.075 o 1 3 3 12 11.780 11.395 1.728 < 1 3 4 1 52.255 51.331 1.202 o 1 3 4 2 189.763 207.385 16.283 o 1 3 4 3 62.070 61.253 1.069 o 1 3 4 4 120.864 119.471 7.492 o 1 3 4 5 5.384 7.261 2.307 < 1 3 4 6 88.035 87.319 .947 o 1 3 4 7 12.567 13.923 1.342 o 1 3 4 8 73.710 73.592 1.487 o 1 3 4 9 26.531 28.271 1.484 o 1 3 4 10 5.556 3.239 3.073 < 1 3 4 11 7.865 6.639 3.752 < 1 3 4 12 33.519 33.896 1.046 o 1 3 5 1 99.571 109.115 8.651 o 1 3 5 2 39.486 40.342 1.356 o 1 3 5 3 143.068 152.443 11.936 o 1 3 5 4 28.424 28.566 .815 o 1 3 5 5 9.827 8.736 1.367 < 1 3 5 6 35.175 34.941 .734 o 1 3 5 7 85.287 86.751 1.563 o 1 3 5 8 32.051 34.994 .859 o 1 3 5 9 37.998 38.062 .886 o 1 3 5 10 3.250 1.831 2.229 < 1 3 5 11 25.097 26.614 1.135 o 1 3 5 12 13.120 10.989 1.964 o 1 3 6 1 2.512 1.017 2.365 < 1 3 6 2 161.953 184.970 1.727 o 1 3 6 3 11.735 8.383 1.013 o 1 3 6 4 74.903 79.291 4.982 o 1 3 6 5 28.370 27.423 .736 o 1 3 6 6 62.490 61.585 .770 o 1 3 6 7 23.389 23.310 1.002 o 1 3 6 8 72.401 71.361 1.558 o 1 3 6 9 15.741 17.170 1.344 o 1 3 6 10 4.801 5.069 2.676 < 1 3 6 11 4.490 3.884 2.439 < 1 3 6 12 29.410 29.085 1.864 o 1 3 7 1 52.249 58.384 5.177 o 1 3 7 2 51.795 47.895 1.108 o 1 3 7 3 126.546 155.519 27.044 < 1 3 7 4 29.500 28.987 .747 o 1 3 7 5 13.260 12.635 1.281 o 1 3 7 6 35.379 34.907 .804 o 1 3 7 7 72.944 73.605 2.974 o 1 3 7 8 16.381 17.205 1.324 o 1 3 7 9 39.609 40.067 .938 o 1 3 7 10 3.475 .297 2.328 < 1 3 7 11 22.656 23.303 1.244 o 1 3 7 12 6.978 10.850 3.358 < 1 3 8 1 40.913 39.292 .818 o 1 3 8 2 127.033 144.028 3.384 o 1 3 8 3 16.804 15.966 1.007 o 1 3 8 4 56.110 64.357 6.055 o 1 3 8 5 14.489 12.618 1.263 o 1 3 8 6 55.830 55.229 2.160 o 1 3 8 7 16.828 13.535 1.203 o 1 3 8 8 63.564 64.904 2.574 o 1 3 8 9 15.510 14.933 1.492 o 1 3 8 10 4.508 4.388 2.722 < 1 3 8 11 3.606 6.117 2.407 < 1 3 8 12 25.848 25.898 1.362 o 1 3 9 1 67.547 83.328 9.789 o 1 3 9 2 61.598 60.345 2.033 o 1 3 9 3 80.340 99.926 20.897 < 1 3 9 4 23.142 21.237 1.948 o 1 3 9 5 6.024 4.616 3.395 < 1 3 9 6 19.272 21.024 1.162 o 1 3 9 7 72.641 73.430 4.657 o 1 3 9 8 16.449 15.862 1.390 o 1 3 9 9 29.140 30.023 1.611 o 1 3 9 10 4.390 4.259 2.662 < 1 3 9 11 12.667 17.292 4.667 < 1 3 10 1 2.517 5.176 2.272 < 1 3 10 2 89.356 114.904 4.151 o 1 3 10 3 52.831 51.798 1.086 o 1 3 10 4 55.627 60.868 6.593 o 1 3 10 5 2.616 8.504 1.931 < 1 3 10 6 58.776 57.534 .990 o 1 3 10 7 3.275 7.695 2.406 < 1 3 10 8 48.631 50.889 1.586 o 1 3 10 9 12.741 13.089 1.805 < 1 3 10 10 3.959 .575 2.560 < 1 3 10 11 5.450 5.606 3.627 < 1 3 11 1 65.133 73.761 3.508 o 1 3 11 2 55.589 53.387 .760 o 1 3 11 3 71.170 80.772 9.347 o 1 3 11 4 12.660 9.818 1.514 < 1 3 11 5 10.844 5.618 1.677 < 1 3 11 6 9.024 11.669 3.323 < 1 3 11 7 58.845 60.277 .915 o 1 3 11 8 20.020 18.164 1.313 o 1 3 11 9 23.746 24.355 1.272 o 1 3 11 10 5.656 5.428 3.064 < 1 3 11 11 15.670 15.539 1.798 < 1 3 12 1 21.759 18.155 1.001 o 1 3 12 2 75.276 88.461 5.264 o 1 3 12 3 12.353 12.476 1.500 < 1 3 12 4 44.290 50.510 1.829 o 1 3 12 5 7.032 9.207 3.032 < 1 3 12 6 39.877 42.522 .924 o 1 3 12 7 20.010 18.009 1.712 o 1 3 12 8 39.349 41.716 5.106 o 1 3 12 9 6.670 5.242 3.192 < 1 3 12 10 5.774 .640 3.095 < 1 3 13 1 29.690 34.198 .906 o 1 3 13 2 24.600 24.281 1.429 o 1 3 13 3 66.599 81.224 4.711 o 1 3 13 4 17.435 15.586 1.238 o 1 3 13 5 4.821 1.031 2.913 < 1 3 13 6 17.986 15.091 1.287 o 1 3 13 7 38.942 41.428 .973 o 1 3 13 8 9.807 10.739 3.035 < 1 3 13 9 22.736 21.928 1.435 o 1 3 13 10 5.817 .528 3.919 < 1 3 14 1 18.580 15.639 1.255 o 1 3 14 2 61.293 70.913 4.123 o 1 3 14 3 8.682 6.482 2.676 < 1 3 14 4 27.349 36.051 2.449 o 1 3 14 5 6.071 8.075 2.978 < 1 3 14 6 25.315 27.028 1.146 o 1 3 14 7 16.658 14.068 1.509 o 1 3 14 8 33.765 35.348 1.047 o 1 3 14 9 7.926 6.902 3.347 < 1 3 14 10 10.530 2.770 3.922 < 1 3 15 1 30.018 34.321 1.564 o 1 3 15 2 19.839 17.254 1.133 o 1 3 15 3 46.546 58.015 5.871 o 1 3 15 4 9.737 11.373 2.547 < 1 3 15 5 5.485 .460 3.285 < 1 3 15 6 5.207 10.236 2.893 < 1 3 15 7 31.133 34.549 2.295 o 1 3 15 8 9.838 9.351 3.045 < 1 3 15 9 15.096 14.134 1.740 o 1 3 16 1 13.066 4.442 1.453 o 1 3 16 2 41.096 55.668 6.214 o 1 3 16 3 17.069 15.217 1.365 o 1 3 16 4 20.816 24.377 1.218 o 1 3 16 5 4.294 .242 2.592 < 1 3 16 6 23.782 23.387 1.190 o 1 3 16 7 8.335 6.102 3.049 < 1 3 16 8 22.578 24.871 1.564 o 1 3 17 1 29.697 33.040 1.017 o 1 3 17 2 14.322 14.708 1.684 o 1 3 17 3 24.557 35.761 5.249 < 1 3 17 4 4.446 4.853 2.844 < 1 3 17 5 6.383 .554 3.113 < 1 3 17 6 3.970 3.102 2.543 < 1 3 17 7 23.651 26.583 1.336 o 1 3 17 8 8.933 8.917 3.296 < 1 3 18 1 6.380 3.556 3.038 < 1 3 18 2 31.694 35.849 1.002 o 1 3 18 3 10.905 10.611 2.332 < 1 3 18 4 18.652 18.392 1.355 o 1 3 18 5 3.956 1.337 2.857 < 1 3 18 6 17.202 17.422 1.481 o 1 3 18 7 3.905 6.356 2.679 < 1 3 19 1 14.465 18.061 1.700 o 1 3 19 2 12.898 10.342 1.668 < 1 3 19 3 21.522 27.592 1.314 o 1 3 19 4 3.051 4.278 2.181 < 1 3 19 5 4.455 .830 2.894 < 1 3 19 6 3.701 3.619 2.466 < 1 3 20 1 4.583 7.853 2.742 < 1 3 20 2 18.839 24.169 1.458 o 1 3 20 3 9.179 5.192 2.836 < 1 3 20 4 11.964 13.182 2.557 < 1 3 20 5 3.049 2.403 2.176 < 1 3 21 1 8.868 10.776 3.262 < 1 3 21 2 4.079 6.607 2.629 < 1 3 21 3 19.577 19.961 2.067 o 1 4 0 0 46.701 46.027 .724 o 1 4 0 1 128.557 120.539 9.315 o 1 4 0 2 25.737 26.589 .473 o 1 4 0 3 15.119 14.934 .687 o 1 4 0 4 158.482 161.548 1.181 o 1 4 0 5 85.483 84.665 .748 o 1 4 0 6 83.313 80.226 .770 o 1 4 0 7 21.293 22.522 .828 o 1 4 0 8 5.235 8.604 2.600 < 1 4 0 9 46.778 47.361 .989 o 1 4 0 10 50.747 52.647 .807 o 1 4 0 11 20.684 21.015 1.100 o 1 4 0 12 14.195 12.875 1.457 o 1 4 0 13 6.679 4.881 3.200 < 1 4 1 0 9.351 8.725 .491 o 1 4 1 1 106.799 104.082 6.806 o 1 4 1 2 66.131 67.425 1.070 o 1 4 1 3 79.349 72.218 2.543 o 1 4 1 4 66.486 71.514 .626 o 1 4 1 5 146.993 143.344 1.434 o 1 4 1 6 53.649 53.044 .652 o 1 4 1 7 23.034 19.219 1.514 o 1 4 1 8 2.566 2.095 1.951 < 1 4 1 9 56.566 56.310 1.092 o 1 4 1 10 35.848 36.538 .812 o 1 4 1 11 30.065 29.271 .912 o 1 4 1 12 4.722 6.451 3.050 < 1 4 2 0 119.370 118.381 1.205 o 1 4 2 1 56.349 50.740 .831 o 1 4 2 2 26.129 26.418 1.768 o 1 4 2 3 28.939 28.633 .516 o 1 4 2 4 108.916 107.238 .867 o 1 4 2 5 88.864 84.463 .791 o 1 4 2 6 89.726 86.842 .809 o 1 4 2 7 13.866 12.660 1.151 o 1 4 2 8 17.169 16.902 1.009 o 1 4 2 9 37.290 36.790 .762 o 1 4 2 10 48.051 49.433 .799 o 1 4 2 11 21.547 21.572 1.118 o 1 4 2 12 13.486 12.478 1.683 < 1 4 3 0 100.213 98.797 1.098 o 1 4 3 1 164.885 187.129 11.970 o 1 4 3 2 8.843 8.172 .887 o 1 4 3 3 39.242 35.661 2.068 o 1 4 3 4 21.249 22.563 .611 o 1 4 3 5 149.020 144.115 2.404 o 1 4 3 6 81.253 79.453 .778 o 1 4 3 7 14.562 12.147 1.063 o 1 4 3 8 7.011 12.706 2.612 < 1 4 3 9 56.008 55.520 .791 o 1 4 3 10 28.950 30.793 .888 o 1 4 3 11 30.300 30.840 .914 o 1 4 3 12 7.101 8.969 3.013 < 1 4 4 0 205.626 235.623 2.848 o 1 4 4 1 116.494 109.726 1.849 o 1 4 4 2 57.131 61.837 6.771 o 1 4 4 3 53.037 45.765 1.381 o 1 4 4 4 60.111 65.317 5.031 o 1 4 4 5 104.860 102.056 1.696 o 1 4 4 6 83.564 82.337 1.418 o 1 4 4 7 2.708 3.729 1.973 < 1 4 4 8 18.340 20.476 1.096 o 1 4 4 9 26.810 28.110 .951 o 1 4 4 10 44.681 45.151 .996 o 1 4 4 11 20.256 20.484 1.177 o 1 4 4 12 7.473 10.615 3.169 < 1 4 5 0 179.983 172.647 2.815 o 1 4 5 1 164.415 182.739 20.813 o 1 4 5 2 29.036 30.120 .698 o 1 4 5 3 37.470 44.964 4.042 o 1 4 5 4 75.030 75.311 1.915 o 1 4 5 5 128.216 129.604 2.468 o 1 4 5 6 45.901 46.910 1.036 o 1 4 5 7 14.475 14.047 1.188 o 1 4 5 8 4.322 9.484 2.419 < 1 4 5 9 48.155 50.488 1.935 o 1 4 5 10 33.181 35.114 .924 o 1 4 5 11 27.329 27.679 1.013 o 1 4 5 12 4.435 7.156 2.647 < 1 4 6 0 143.006 154.581 1.527 o 1 4 6 1 141.741 132.410 3.017 o 1 4 6 2 68.115 79.181 3.985 o 1 4 6 3 62.925 59.656 1.398 o 1 4 6 4 81.519 87.144 8.766 o 1 4 6 5 76.061 75.210 1.246 o 1 4 6 6 63.080 62.255 .747 o 1 4 6 7 14.489 14.662 1.246 o 1 4 6 8 6.525 9.786 3.596 < 1 4 6 9 34.382 34.113 1.912 o 1 4 6 10 41.293 42.949 2.299 o 1 4 6 11 15.384 14.575 1.470 o 1 4 6 12 4.104 9.027 2.679 < 1 4 7 0 57.966 51.572 .866 o 1 4 7 1 112.492 118.557 2.791 o 1 4 7 2 72.269 68.904 1.773 o 1 4 7 3 45.916 65.435 12.032 < 1 4 7 4 87.099 85.935 1.791 o 1 4 7 5 100.525 105.472 2.962 o 1 4 7 6 29.669 29.047 1.680 o 1 4 7 7 22.410 21.791 .984 o 1 4 7 8 6.018 6.971 2.852 < 1 4 7 9 43.871 43.731 1.099 o 1 4 7 10 32.580 31.777 .954 o 1 4 7 11 21.254 23.140 1.735 o 1 4 7 12 4.541 6.426 2.925 < 1 4 8 0 96.347 109.677 1.182 o 1 4 8 1 70.676 69.304 2.037 o 1 4 8 2 29.660 35.865 1.879 o 1 4 8 3 34.514 32.467 .820 o 1 4 8 4 74.091 86.167 6.653 o 1 4 8 5 58.058 56.733 1.366 o 1 4 8 6 66.055 62.766 .914 o 1 4 8 7 14.219 13.645 1.421 o 1 4 8 8 7.650 9.211 4.053 < 1 4 8 9 26.752 29.889 1.128 o 1 4 8 10 35.590 36.766 1.227 o 1 4 8 11 13.562 13.583 1.775 o 1 4 8 12 9.757 8.864 3.037 < 1 4 9 0 66.477 65.886 1.010 o 1 4 9 1 77.824 98.784 5.878 o 1 4 9 2 10.925 11.580 1.387 < 1 4 9 3 39.683 55.241 12.364 < 1 4 9 4 27.599 24.567 .829 o 1 4 9 5 90.605 97.096 3.097 o 1 4 9 6 47.366 46.585 .815 o 1 4 9 7 16.639 17.247 1.411 o 1 4 9 8 13.702 11.525 1.459 o 1 4 9 9 38.684 37.119 1.273 o 1 4 9 10 22.111 22.112 1.199 o 1 4 9 11 20.635 19.967 1.356 o 1 4 10 0 103.328 109.817 1.294 o 1 4 10 1 58.882 56.330 1.879 o 1 4 10 2 10.335 12.655 1.547 < 1 4 10 3 13.008 13.208 1.277 o 1 4 10 4 49.172 59.555 4.265 o 1 4 10 5 59.795 58.925 1.927 o 1 4 10 6 60.956 59.789 2.816 o 1 4 10 7 8.733 7.780 3.642 < 1 4 10 8 14.488 14.011 1.560 o 1 4 10 9 18.442 20.507 1.336 o 1 4 10 10 30.141 29.227 1.118 o 1 4 10 11 15.822 15.512 1.701 o 1 4 11 0 71.033 69.708 1.111 o 1 4 11 1 63.277 82.362 8.874 o 1 4 11 2 8.283 6.049 2.534 < 1 4 11 3 26.452 30.911 2.097 o 1 4 11 4 28.857 24.546 2.346 o 1 4 11 5 69.847 75.951 3.751 o 1 4 11 6 40.700 39.946 2.671 o 1 4 11 7 9.175 10.856 2.829 < 1 4 11 8 3.512 6.065 2.382 < 1 4 11 9 30.051 29.548 1.885 o 1 4 11 10 20.534 20.812 1.363 o 1 4 11 11 16.088 17.736 1.789 o 1 4 12 0 70.596 73.277 1.162 o 1 4 12 1 43.385 40.887 .800 o 1 4 12 2 17.075 19.959 1.803 o 1 4 12 3 16.320 12.625 1.270 o 1 4 12 4 40.365 41.671 3.007 o 1 4 12 5 48.577 47.101 1.276 o 1 4 12 6 39.785 41.813 1.336 o 1 4 12 7 9.046 7.764 2.793 < 1 4 12 8 9.478 11.253 2.928 < 1 4 12 9 17.426 17.535 1.621 o 1 4 12 10 24.630 25.785 2.784 o 1 4 13 0 22.737 22.759 1.575 o 1 4 13 1 53.494 57.480 1.107 o 1 4 13 2 26.771 25.429 .963 o 1 4 13 3 10.724 15.555 2.811 < 1 4 13 4 41.330 39.877 .906 o 1 4 13 5 48.575 51.696 .883 o 1 4 13 6 20.922 20.075 1.374 o 1 4 13 7 10.993 9.495 3.402 < 1 4 13 8 6.502 .442 3.651 < 1 4 13 9 26.146 24.866 2.698 o 1 4 13 10 19.861 17.441 1.498 o 1 4 14 0 43.072 47.761 1.208 o 1 4 14 1 35.673 33.255 1.372 o 1 4 14 2 24.560 25.300 1.066 o 1 4 14 3 22.304 18.496 1.482 o 1 4 14 4 31.621 37.893 4.113 o 1 4 14 5 27.989 26.021 1.302 o 1 4 14 6 25.475 29.797 1.184 o 1 4 14 7 14.437 11.321 1.669 o 1 4 14 8 2.959 7.366 2.132 < 1 4 14 9 17.197 16.628 1.708 o 1 4 15 0 34.834 31.151 1.289 o 1 4 15 1 35.575 45.894 .948 o 1 4 15 2 16.057 12.963 1.459 o 1 4 15 3 14.732 17.226 2.010 o 1 4 15 4 22.707 22.031 1.075 o 1 4 15 5 32.212 37.439 1.055 o 1 4 15 6 23.270 21.102 1.196 o 1 4 15 7 9.465 9.365 2.937 < 1 4 15 8 6.909 6.722 3.793 < 1 4 15 9 19.469 19.132 1.538 o 1 4 16 0 47.316 47.945 1.245 o 1 4 16 1 29.644 29.771 1.033 o 1 4 16 2 6.478 10.122 3.566 < 1 4 16 3 7.225 9.484 3.052 < 1 4 16 4 24.207 27.868 1.083 o 1 4 16 5 25.642 25.241 1.163 o 1 4 16 6 22.717 25.754 1.951 o 1 4 16 7 6.706 2.747 3.205 < 1 4 16 8 13.747 6.543 1.638 < 1 4 17 0 40.544 35.890 1.293 o 1 4 17 1 26.548 31.328 1.752 o 1 4 17 2 4.989 3.591 2.697 < 1 4 17 3 12.748 13.661 3.330 < 1 4 17 4 15.402 13.846 1.525 o 1 4 17 5 26.790 29.371 1.166 o 1 4 17 6 18.759 16.163 2.260 o 1 4 17 7 4.214 6.358 2.708 < 1 4 17 8 7.566 6.286 3.638 < 1 4 18 0 35.321 33.579 1.298 o 1 4 18 1 21.582 19.559 1.231 o 1 4 18 2 5.502 5.969 2.916 < 1 4 18 3 3.479 5.527 2.320 < 1 4 18 4 20.696 19.300 1.207 o 1 4 18 5 23.566 19.891 1.248 o 1 4 18 6 18.630 18.497 1.555 o 1 4 18 7 3.858 1.205 2.546 < 1 4 19 0 17.909 16.590 2.044 o 1 4 19 1 16.623 21.328 1.521 o 1 4 19 2 6.407 7.141 3.083 < 1 4 19 3 5.090 7.567 2.796 < 1 4 19 4 15.662 15.092 1.992 o 1 4 19 5 20.522 21.399 1.457 o 1 4 19 6 7.610 8.643 4.035 < 1 4 20 0 20.088 21.879 1.844 o 1 4 20 1 8.728 12.667 3.222 < 1 4 20 2 6.621 8.159 3.180 < 1 4 20 3 6.589 5.877 3.509 < 1 4 20 4 15.016 15.699 1.755 o 1 4 20 5 11.000 11.615 2.866 < 1 4 21 0 12.124 11.381 3.751 < 1 4 21 1 11.421 15.555 3.548 < 1 4 21 2 4.099 4.654 2.745 < 1 4 21 3 3.156 5.252 2.269 < 1 5 0 1 88.273 83.537 4.778 o 1 5 0 2 27.507 26.229 .582 o 1 5 0 3 236.404 240.908 2.251 o 1 5 0 4 3.044 3.520 1.995 < 1 5 0 5 38.275 37.088 .574 o 1 5 0 6 28.600 26.348 .830 o 1 5 0 7 76.161 77.574 .780 o 1 5 0 8 6.021 8.042 2.570 < 1 5 0 9 52.175 51.369 .776 o 1 5 0 10 7.230 4.535 2.702 < 1 5 0 11 30.374 29.550 1.762 o 1 5 0 12 5.185 .941 2.781 < 1 5 1 1 3.689 4.096 1.813 < 1 5 1 2 258.488 249.140 2.280 o 1 5 1 3 44.836 41.971 2.125 o 1 5 1 4 121.322 113.108 .947 o 1 5 1 5 22.910 22.783 .623 o 1 5 1 6 86.754 84.710 .912 o 1 5 1 7 2.580 4.192 1.764 < 1 5 1 8 94.035 91.321 .890 o 1 5 1 9 4.221 2.186 2.312 < 1 5 1 10 7.879 7.128 2.491 < 1 5 1 11 4.471 2.632 2.495 < 1 5 1 12 36.118 36.569 1.579 o 1 5 2 1 151.342 147.446 2.350 o 1 5 2 2 1.874 6.200 1.407 < 1 5 2 3 185.194 181.454 3.838 o 1 5 2 4 2.098 2.883 1.436 < 1 5 2 5 15.694 15.356 .824 o 1 5 2 6 14.861 15.148 .946 o 1 5 2 7 102.750 100.666 1.136 o 1 5 2 8 2.701 2.961 1.868 < 1 5 2 9 47.136 46.014 .768 o 1 5 2 10 7.473 6.243 3.202 < 1 5 2 11 25.197 25.791 1.018 o 1 5 2 12 3.264 .969 2.198 < 1 5 3 1 18.538 20.531 1.498 o 1 5 3 2 218.384 212.840 2.944 o 1 5 3 3 4.419 .553 1.889 < 1 5 3 4 125.501 121.291 .980 o 1 5 3 5 9.969 9.590 1.154 o 1 5 3 6 109.179 105.270 1.631 o 1 5 3 7 6.658 7.958 2.506 < 1 5 3 8 83.925 83.780 .888 o 1 5 3 9 4.613 .998 2.514 < 1 5 3 10 4.860 1.804 2.607 < 1 5 3 11 3.561 .376 2.323 < 1 5 3 12 38.324 36.206 .963 o 1 5 4 1 145.140 142.496 1.924 o 1 5 4 2 40.065 42.295 .538 o 1 5 4 3 141.021 135.048 2.910 o 1 5 4 4 12.943 12.568 .905 o 1 5 4 5 20.603 22.096 1.044 o 1 5 4 6 3.926 5.761 2.221 < 1 5 4 7 106.313 105.215 .943 o 1 5 4 8 3.299 2.849 2.132 < 1 5 4 9 42.312 42.624 1.685 o 1 5 4 10 7.253 6.435 2.716 < 1 5 4 11 23.123 23.319 1.107 o 1 5 4 12 4.297 .691 2.580 < 1 5 5 1 21.334 27.148 2.470 o 1 5 5 2 206.048 195.305 7.120 o 1 5 5 3 9.534 10.661 1.100 o 1 5 5 4 90.892 89.524 2.559 o 1 5 5 5 2.291 1.071 1.609 < 1 5 5 6 96.716 94.104 .879 o 1 5 5 7 7.455 6.291 3.199 < 1 5 5 8 76.851 78.536 .848 o 1 5 5 9 3.280 2.489 2.166 < 1 5 5 10 6.747 3.519 2.882 < 1 5 5 11 2.971 1.080 2.057 < 1 5 5 12 31.513 31.991 1.048 o 1 5 6 1 67.104 65.402 1.269 o 1 5 6 2 28.039 32.656 3.365 o 1 5 6 3 171.628 166.068 3.906 o 1 5 6 4 3.726 5.819 2.065 < 1 5 6 5 22.081 21.575 .835 o 1 5 6 6 4.581 7.476 2.503 < 1 5 6 7 75.421 74.930 1.597 o 1 5 6 8 3.043 .826 2.044 < 1 5 6 9 43.490 43.364 2.067 o 1 5 6 10 6.742 3.995 2.886 < 1 5 6 11 21.085 23.711 1.292 o 1 5 6 12 5.151 .211 3.343 < 1 5 7 1 3.066 .873 1.843 < 1 5 7 2 170.553 166.910 4.566 o 1 5 7 3 12.632 14.581 1.301 o 1 5 7 4 67.833 63.851 1.463 o 1 5 7 5 5.950 7.726 2.585 < 1 5 7 6 63.884 62.612 1.576 o 1 5 7 7 7.067 5.419 2.631 < 1 5 7 8 73.083 72.332 1.394 o 1 5 7 9 6.184 1.937 3.731 < 1 5 7 10 6.560 7.581 3.671 < 1 5 7 11 2.810 2.972 1.950 < 1 5 7 12 28.183 26.909 1.131 o 1 5 8 1 59.870 52.661 1.560 o 1 5 8 2 6.454 12.323 2.441 < 1 5 8 3 144.176 141.310 3.849 o 1 5 8 4 5.276 8.621 2.571 < 1 5 8 5 6.151 1.005 2.610 < 1 5 8 6 15.673 15.368 1.147 o 1 5 8 7 72.103 69.023 1.178 o 1 5 8 8 5.123 .746 3.074 < 1 5 8 9 32.060 32.537 .958 o 1 5 8 10 3.515 2.610 2.378 < 1 5 8 11 20.020 19.245 1.890 o 1 5 9 1 14.273 12.790 1.008 o 1 5 9 2 152.929 143.232 4.776 o 1 5 9 3 4.067 9.801 2.284 < 1 5 9 4 67.771 65.678 2.184 o 1 5 9 5 2.087 3.170 1.551 < 1 5 9 6 59.574 57.607 1.362 o 1 5 9 7 4.634 2.960 2.559 < 1 5 9 8 58.415 57.132 2.106 o 1 5 9 9 6.058 1.815 2.954 < 1 5 9 10 3.636 3.415 2.510 < 1 5 9 11 3.838 1.814 2.501 < 1 5 10 1 106.640 100.201 2.413 o 1 5 10 2 3.214 5.083 2.139 < 1 5 10 3 80.029 74.587 2.426 o 1 5 10 4 3.809 1.937 2.296 < 1 5 10 5 19.834 20.579 1.526 o 1 5 10 6 4.152 7.499 2.527 < 1 5 10 7 69.943 67.687 2.948 o 1 5 10 8 3.705 .499 2.400 < 1 5 10 9 24.068 24.057 1.427 o 1 5 10 10 4.285 2.427 2.583 < 1 5 10 11 16.500 16.501 1.639 o 1 5 11 1 8.669 11.151 4.246 < 1 5 11 2 108.218 104.154 1.784 o 1 5 11 3 4.327 1.532 2.411 < 1 5 11 4 64.843 63.478 .798 o 1 5 11 5 2.388 .017 1.691 < 1 5 11 6 52.815 51.344 1.805 o 1 5 11 7 2.799 3.196 2.046 < 1 5 11 8 46.765 44.723 .935 o 1 5 11 9 2.947 2.902 2.157 < 1 5 11 10 5.294 .236 2.925 < 1 5 11 11 3.606 .949 2.432 < 1 5 12 1 51.940 47.523 .781 o 1 5 12 2 5.628 6.809 2.763 < 1 5 12 3 82.185 81.406 2.551 o 1 5 12 4 3.072 2.287 2.223 < 1 5 12 5 5.823 .321 2.820 < 1 5 12 6 2.742 .914 1.991 < 1 5 12 7 47.724 45.972 2.255 o 1 5 12 8 5.893 1.059 3.155 < 1 5 12 9 28.166 25.916 1.165 o 1 5 12 10 4.071 1.877 2.654 < 1 5 13 1 3.597 .764 2.324 < 1 5 13 2 84.415 79.397 2.429 o 1 5 13 3 7.525 2.111 2.806 < 1 5 13 4 39.301 38.806 1.256 o 1 5 13 5 4.103 4.076 2.487 < 1 5 13 6 33.732 31.369 .966 o 1 5 13 7 2.828 3.768 2.005 < 1 5 13 8 44.819 41.361 3.077 o 1 5 13 9 6.209 .162 4.041 < 1 5 13 10 2.916 3.085 2.079 < 1 5 14 1 32.995 29.838 1.050 o 1 5 14 2 5.212 5.302 2.916 < 1 5 14 3 73.038 69.729 2.171 o 1 5 14 4 3.271 1.869 2.200 < 1 5 14 5 9.434 3.513 2.496 < 1 5 14 6 4.309 .454 2.600 < 1 5 14 7 40.392 37.719 1.005 o 1 5 14 8 3.751 1.740 2.526 < 1 5 14 9 22.071 18.715 1.842 o 1 5 15 1 4.000 .468 2.608 < 1 5 15 2 69.747 65.387 1.396 o 1 5 15 3 6.787 4.315 2.906 < 1 5 15 4 28.539 26.684 1.045 o 1 5 15 5 6.928 3.108 2.969 < 1 5 15 6 29.960 25.773 1.070 o 1 5 15 7 3.010 .550 2.166 < 1 5 15 8 33.186 31.794 1.119 o 1 5 15 9 5.434 1.087 3.522 < 1 5 16 1 43.333 39.492 .896 o 1 5 16 2 2.977 .183 2.132 < 1 5 16 3 46.393 41.596 .869 o 1 5 16 4 3.195 1.006 2.209 < 1 5 16 5 4.894 2.492 2.749 < 1 5 16 6 4.410 3.645 2.988 < 1 5 16 7 36.479 33.586 1.347 o 1 5 16 8 7.666 1.391 4.602 < 1 5 17 1 4.909 3.279 2.732 < 1 5 17 2 48.488 45.304 2.088 o 1 5 17 3 3.903 .249 2.635 < 1 5 17 4 23.753 22.017 1.260 o 1 5 17 5 6.348 1.220 3.074 < 1 5 17 6 24.169 22.549 1.244 o 1 5 17 7 3.497 .238 2.410 < 1 5 18 1 26.857 26.831 1.205 o 1 5 18 2 2.692 .358 1.916 < 1 5 18 3 32.153 29.783 1.086 o 1 5 18 4 3.486 .096 2.345 < 1 5 18 5 4.615 .015 3.007 < 1 5 18 6 3.020 1.070 2.181 < 1 5 18 7 19.578 20.936 4.186 < 1 5 19 1 4.357 1.903 2.625 < 1 5 19 2 31.830 28.594 1.076 o 1 5 19 3 2.921 .736 2.115 < 1 5 19 4 16.201 16.117 3.466 < 1 5 19 5 9.450 .153 2.962 < 1 5 19 6 14.534 13.649 1.898 < 1 5 20 1 10.697 11.941 2.783 < 1 5 20 2 5.480 .880 2.948 < 1 5 20 3 29.537 25.298 1.150 o 1 5 20 4 4.018 .591 2.611 < 1 5 21 1 9.013 1.167 2.828 < 1 5 21 2 25.459 20.434 1.270 o 1 6 0 0 66.044 66.466 1.369 o 1 6 0 1 62.585 63.499 2.665 o 1 6 0 2 98.617 99.254 3.894 o 1 6 0 3 50.659 49.709 .562 o 1 6 0 4 106.719 99.181 1.088 o 1 6 0 5 62.068 60.546 .653 o 1 6 0 6 79.435 75.976 .768 o 1 6 0 7 44.573 44.997 .718 o 1 6 0 8 8.391 8.370 2.196 < 1 6 0 9 23.817 24.934 .905 o 1 6 0 10 45.606 46.131 .811 o 1 6 0 11 22.097 22.002 1.561 o 1 6 0 12 10.970 9.828 2.353 < 1 6 1 0 104.037 100.841 1.527 o 1 6 1 1 155.248 165.613 9.706 o 1 6 1 2 48.489 48.517 .538 o 1 6 1 3 13.934 15.778 .732 o 1 6 1 4 112.989 110.328 1.314 o 1 6 1 5 139.150 133.775 1.378 o 1 6 1 6 45.987 43.482 .647 o 1 6 1 7 26.771 24.787 .762 o 1 6 1 8 15.749 14.978 1.078 o 1 6 1 9 46.582 46.790 1.399 o 1 6 1 10 37.027 38.134 .842 o 1 6 1 11 30.081 29.795 .932 o 1 6 1 12 4.840 5.136 2.632 < 1 6 2 0 122.825 121.454 .930 o 1 6 2 1 87.855 83.042 .722 o 1 6 2 2 58.139 62.149 3.077 o 1 6 2 3 15.465 15.522 .745 o 1 6 2 4 93.494 91.716 .791 o 1 6 2 5 73.927 73.008 .712 o 1 6 2 6 77.114 75.705 .760 o 1 6 2 7 26.072 25.502 .786 o 1 6 2 8 11.501 8.808 1.375 < 1 6 2 9 25.110 25.189 1.054 o 1 6 2 10 45.526 45.880 .814 o 1 6 2 11 24.879 24.768 1.062 o 1 6 2 12 9.059 9.849 3.346 < 1 6 3 0 176.598 177.876 2.744 o 1 6 3 1 115.646 137.953 6.665 o 1 6 3 2 18.956 19.023 .621 o 1 6 3 3 39.513 45.154 5.249 o 1 6 3 4 49.788 48.437 .595 o 1 6 3 5 122.282 121.033 2.057 o 1 6 3 6 74.996 73.403 1.537 o 1 6 3 7 13.322 14.492 1.274 o 1 6 3 8 34.626 34.077 1.660 o 1 6 3 9 43.362 45.123 .783 o 1 6 3 10 27.950 29.726 1.413 o 1 6 3 11 27.141 27.698 1.347 o 1 6 3 12 8.330 4.875 2.579 < 1 6 4 0 144.726 151.803 1.533 o 1 6 4 1 91.149 86.800 1.006 o 1 6 4 2 53.234 57.526 4.088 o 1 6 4 3 1.468 4.984 1.872 < 1 6 4 4 88.757 95.336 3.901 o 1 6 4 5 82.617 81.341 1.711 o 1 6 4 6 59.122 58.199 1.046 o 1 6 4 7 8.338 6.382 2.176 < 1 6 4 8 4.127 8.693 2.451 < 1 6 4 9 24.932 26.990 .946 o 1 6 4 10 42.650 43.154 .841 o 1 6 4 11 25.244 24.731 1.023 o 1 6 4 12 9.124 8.983 2.839 < 1 6 5 0 131.726 125.338 1.426 o 1 6 5 1 123.720 138.965 13.025 o 1 6 5 2 33.439 33.328 1.506 o 1 6 5 3 57.120 62.967 4.006 o 1 6 5 4 80.666 76.915 1.100 o 1 6 5 5 94.773 101.503 1.613 o 1 6 5 6 50.786 51.068 .860 o 1 6 5 7 11.287 12.077 1.416 < 1 6 5 8 20.978 22.414 1.026 o 1 6 5 9 42.630 42.407 .817 o 1 6 5 10 28.412 28.181 1.335 o 1 6 5 11 23.344 24.770 1.177 o 1 6 5 12 4.503 2.073 2.651 < 1 6 6 0 102.987 118.605 1.199 o 1 6 6 1 65.589 62.731 1.823 o 1 6 6 2 37.521 45.132 2.366 o 1 6 6 3 15.566 16.423 .887 o 1 6 6 4 71.701 85.151 5.775 o 1 6 6 5 56.312 55.871 1.063 o 1 6 6 6 55.149 53.631 .728 o 1 6 6 7 22.857 21.798 .926 o 1 6 6 8 5.043 11.531 2.772 < 1 6 6 9 28.529 29.353 .909 o 1 6 6 10 37.130 38.368 1.351 o 1 6 6 11 18.758 19.218 1.342 o 1 6 6 12 8.148 7.147 3.006 < 1 6 7 0 72.402 66.336 .986 o 1 6 7 1 77.351 88.620 5.710 o 1 6 7 2 60.664 56.952 1.786 o 1 6 7 3 37.344 48.536 9.774 < 1 6 7 4 106.313 104.423 2.248 o 1 6 7 5 88.140 90.899 1.720 o 1 6 7 6 39.099 36.552 .755 o 1 6 7 7 15.639 13.862 1.232 o 1 6 7 8 10.199 10.058 2.179 < 1 6 7 9 39.193 38.464 .875 o 1 6 7 10 26.904 27.239 2.147 o 1 6 7 11 19.404 20.943 1.392 o 1 6 7 12 3.128 2.209 2.215 < 1 6 8 0 54.568 64.108 .925 o 1 6 8 1 62.215 59.368 1.524 o 1 6 8 2 18.033 30.156 5.584 < 1 6 8 3 32.797 33.408 1.440 o 1 6 8 4 52.812 59.442 6.246 o 1 6 8 5 48.156 45.403 1.887 o 1 6 8 6 60.638 58.101 1.176 o 1 6 8 7 26.611 25.236 .936 o 1 6 8 8 14.941 12.480 1.322 o 1 6 8 9 23.960 25.848 1.523 o 1 6 8 10 31.425 31.508 1.024 o 1 6 8 11 17.726 16.760 1.421 o 1 6 9 0 111.428 109.074 1.333 o 1 6 9 1 64.240 75.254 2.604 o 1 6 9 2 4.341 .635 2.383 < 1 6 9 3 27.322 29.961 2.660 o 1 6 9 4 54.951 53.918 1.290 o 1 6 9 5 79.764 83.224 .931 o 1 6 9 6 49.442 48.500 2.443 o 1 6 9 7 16.340 16.870 2.413 o 1 6 9 8 17.867 16.977 1.801 o 1 6 9 9 31.243 32.702 1.642 o 1 6 9 10 20.400 20.010 1.251 o 1 6 9 11 19.999 19.348 1.332 o 1 6 10 0 76.870 84.427 1.124 o 1 6 10 1 52.684 47.064 1.501 o 1 6 10 2 15.320 22.884 3.988 < 1 6 10 3 16.241 16.444 1.175 o 1 6 10 4 39.973 47.665 2.677 o 1 6 10 5 53.232 50.501 1.611 o 1 6 10 6 50.961 50.575 .832 o 1 6 10 7 12.909 12.653 4.002 < 1 6 10 8 12.195 10.369 1.700 < 1 6 10 9 17.479 16.050 1.737 o 1 6 10 10 28.657 29.113 2.958 o 1 6 10 11 15.776 16.978 1.878 o 1 6 11 0 80.069 80.253 1.164 o 1 6 11 1 64.795 71.314 2.964 o 1 6 11 2 2.963 2.372 2.316 < 1 6 11 3 14.169 19.212 1.330 o 1 6 11 4 29.989 30.192 1.363 o 1 6 11 5 54.301 61.520 1.010 o 1 6 11 6 35.743 33.810 .864 o 1 6 11 7 8.139 14.155 2.993 < 1 6 11 8 16.984 13.396 1.327 o 1 6 11 9 25.968 27.176 1.648 o 1 6 11 10 18.960 18.953 1.441 o 1 6 12 0 57.394 63.307 1.125 o 1 6 12 1 34.358 31.560 .809 o 1 6 12 2 22.705 27.216 2.584 o 1 6 12 3 3.268 1.480 2.380 < 1 6 12 4 37.102 44.311 1.287 o 1 6 12 5 39.291 36.728 1.234 o 1 6 12 6 31.154 34.988 1.002 o 1 6 12 7 6.590 10.592 3.163 < 1 6 12 8 9.084 6.717 4.332 < 1 6 12 9 14.585 14.834 1.673 < 1 6 12 10 23.408 25.203 1.316 o 1 6 13 0 35.378 32.945 1.198 o 1 6 13 1 51.374 53.045 .794 o 1 6 13 2 33.042 31.118 1.407 o 1 6 13 3 13.320 21.489 4.919 < 1 6 13 4 39.274 37.794 1.145 o 1 6 13 5 37.069 41.489 2.371 o 1 6 13 6 18.937 18.053 1.341 o 1 6 13 7 5.743 11.969 3.433 < 1 6 13 8 6.819 6.065 3.256 < 1 6 13 9 21.554 23.374 3.233 o 1 6 13 10 18.368 17.666 1.537 o 1 6 14 0 49.451 55.381 1.175 o 1 6 14 1 34.534 32.348 .884 o 1 6 14 2 10.794 13.133 2.308 < 1 6 14 3 7.931 6.718 2.923 < 1 6 14 4 25.901 31.986 2.800 o 1 6 14 5 24.503 23.411 1.599 o 1 6 14 6 28.213 30.253 1.542 o 1 6 14 7 15.889 13.239 1.474 o 1 6 14 8 6.857 8.609 3.286 < 1 6 14 9 16.824 15.707 1.601 o 1 6 15 0 40.018 37.671 1.235 o 1 6 15 1 30.281 41.421 2.941 o 1 6 15 2 14.344 13.863 1.467 o 1 6 15 3 12.538 15.467 3.274 < 1 6 15 4 28.814 26.362 1.046 o 1 6 15 5 35.708 37.709 1.641 o 1 6 15 6 22.028 21.074 1.283 o 1 6 15 7 9.436 6.763 2.923 < 1 6 15 8 3.936 7.774 2.649 < 1 6 15 9 15.271 17.004 1.954 < 1 6 16 0 45.018 45.626 1.230 o 1 6 16 1 26.205 23.482 1.109 o 1 6 16 2 6.140 10.352 3.261 < 1 6 16 3 4.607 10.193 2.745 < 1 6 16 4 23.991 27.341 2.141 o 1 6 16 5 25.130 22.644 2.664 o 1 6 16 6 22.734 23.782 1.370 o 1 6 16 7 8.083 6.468 3.415 < 1 6 16 8 4.812 7.490 3.099 < 1 6 17 0 38.335 35.076 1.443 o 1 6 17 1 21.844 29.775 5.699 < 1 6 17 2 2.874 1.441 2.230 < 1 6 17 3 8.311 11.262 3.058 < 1 6 17 4 17.063 15.769 1.374 o 1 6 17 5 26.664 29.176 3.115 o 1 6 17 6 15.501 16.659 1.823 o 1 6 17 7 5.061 4.689 3.360 < 1 6 18 0 24.846 28.032 1.704 o 1 6 18 1 19.028 15.575 2.395 o 1 6 18 2 4.531 8.260 2.719 < 1 6 18 3 6.502 5.602 3.100 < 1 6 18 4 19.953 21.027 1.405 o 1 6 18 5 20.500 18.413 1.367 o 1 6 18 6 17.859 15.527 1.500 o 1 6 19 0 15.569 18.893 2.347 o 1 6 19 1 15.904 18.872 1.472 o 1 6 19 2 4.507 6.173 2.688 < 1 6 19 3 9.066 7.664 4.350 < 1 6 19 4 16.241 14.728 1.560 o 1 6 19 5 18.595 17.947 1.532 o 1 6 20 0 18.085 18.545 2.111 o 1 6 20 1 14.006 12.871 1.687 o 1 6 20 2 3.740 6.302 2.510 < 1 6 20 3 7.605 4.092 3.211 < 1 6 20 4 13.457 13.943 1.874 o 1 6 21 0 7.199 11.393 3.836 < 1 6 21 1 15.874 13.547 1.639 o 1 6 21 2 3.892 6.053 2.610 < 1 7 0 1 16.126 17.003 1.332 o 1 7 0 2 183.422 187.587 4.359 o 1 7 0 3 5.113 6.484 1.947 < 1 7 0 4 100.260 95.778 1.367 o 1 7 0 5 30.784 30.967 .647 o 1 7 0 6 37.278 35.937 1.763 o 1 7 0 7 28.063 24.376 1.449 o 1 7 0 8 73.577 72.174 1.317 o 1 7 0 9 4.073 2.322 2.251 < 1 7 0 10 2.611 .485 1.923 < 1 7 0 11 4.683 4.847 2.761 < 1 7 0 12 32.882 32.655 1.005 o 1 7 1 1 118.122 111.241 5.410 o 1 7 1 2 56.991 56.674 .580 o 1 7 1 3 180.171 173.888 10.993 o 1 7 1 4 36.425 36.389 .588 o 1 7 1 5 14.134 12.152 1.302 o 1 7 1 6 38.104 39.721 .663 o 1 7 1 7 97.721 95.263 .893 o 1 7 1 8 13.860 13.630 1.251 o 1 7 1 9 32.747 33.579 .836 o 1 7 1 10 3.079 2.051 2.071 < 1 7 1 11 30.478 29.574 1.190 o 1 7 1 12 12.170 11.739 1.768 < 1 7 2 1 5.141 3.735 1.974 < 1 7 2 2 122.983 146.467 12.845 o 1 7 2 3 57.461 52.287 .597 o 1 7 2 4 92.207 88.254 .794 o 1 7 2 5 3.254 1.854 1.953 < 1 7 2 6 52.210 51.508 .693 o 1 7 2 7 15.410 13.882 1.085 o 1 7 2 8 75.997 73.377 .821 o 1 7 2 9 10.986 13.556 3.422 < 1 7 2 10 10.794 2.992 1.550 < 1 7 2 11 5.888 7.270 2.816 < 1 7 2 12 31.745 31.914 .986 o 1 7 3 1 127.905 137.273 6.013 o 1 7 3 2 82.053 80.586 .850 o 1 7 3 3 120.506 147.968 31.363 < 1 7 3 4 14.883 16.008 .854 o 1 7 3 5 12.127 9.578 1.033 o 1 7 3 6 22.919 23.254 .802 o 1 7 3 7 107.086 107.636 3.063 o 1 7 3 8 27.183 27.471 .864 o 1 7 3 9 30.415 33.482 1.060 o 1 7 3 10 6.487 5.145 2.783 < 1 7 3 11 25.288 25.139 1.030 o 1 7 3 12 8.058 9.616 2.965 < 1 7 4 1 5.970 9.697 3.058 < 1 7 4 2 119.673 134.094 7.162 o 1 7 4 3 69.433 65.420 .675 o 1 7 4 4 74.245 79.381 6.800 o 1 7 4 5 20.502 20.633 .763 o 1 7 4 6 71.880 72.949 1.054 o 1 7 4 7 15.667 15.231 1.102 o 1 7 4 8 70.943 71.791 2.334 o 1 7 4 9 20.249 19.161 .979 o 1 7 4 10 6.553 4.495 3.673 < 1 7 4 11 3.673 6.641 2.378 < 1 7 4 12 27.511 29.299 1.082 o 1 7 5 1 82.596 116.804 25.630 < 1 7 5 2 57.461 55.484 .833 o 1 7 5 3 143.763 164.337 11.714 o 1 7 5 4 7.620 7.143 3.673 < 1 7 5 5 25.513 27.128 .755 o 1 7 5 6 24.002 24.326 .792 o 1 7 5 7 94.548 95.425 3.640 o 1 7 5 8 23.933 24.633 .906 o 1 7 5 9 32.342 30.802 1.480 o 1 7 5 10 4.607 2.262 3.005 < 1 7 5 11 23.370 23.252 1.071 o 1 7 5 12 9.924 9.029 3.079 < 1 7 6 1 36.590 36.583 1.731 o 1 7 6 2 111.030 132.216 10.823 o 1 7 6 3 5.671 5.026 2.254 < 1 7 6 4 51.394 61.418 3.825 o 1 7 6 5 18.109 16.284 .900 o 1 7 6 6 53.301 53.780 1.613 o 1 7 6 7 32.024 30.884 .809 o 1 7 6 8 63.633 68.545 4.579 o 1 7 6 9 7.440 9.388 2.728 < 1 7 6 10 5.074 1.701 2.746 < 1 7 6 11 3.346 2.878 2.221 < 1 7 6 12 24.894 25.201 1.220 o 1 7 7 1 79.952 92.441 7.366 o 1 7 7 2 42.324 43.416 1.347 o 1 7 7 3 107.212 151.094 39.471 < 1 7 7 4 34.239 34.261 .707 o 1 7 7 5 5.357 12.985 2.650 < 1 7 7 6 34.672 33.784 .971 o 1 7 7 7 75.159 77.648 4.386 o 1 7 7 8 15.440 15.774 1.460 o 1 7 7 9 25.115 24.628 1.591 o 1 7 7 10 3.248 .313 2.203 < 1 7 7 11 22.442 21.852 1.221 o 1 7 8 1 29.879 29.262 .790 o 1 7 8 2 99.018 116.520 13.825 o 1 7 8 3 17.860 19.132 .959 o 1 7 8 4 53.840 62.504 3.420 o 1 7 8 5 7.108 12.546 2.681 < 1 7 8 6 42.188 41.196 .783 o 1 7 8 7 21.967 21.272 1.026 o 1 7 8 8 52.796 56.615 3.174 o 1 7 8 9 5.232 7.065 2.881 < 1 7 8 10 3.616 1.974 2.373 < 1 7 8 11 6.620 5.580 3.166 < 1 7 9 1 79.140 97.744 7.797 o 1 7 9 2 41.471 39.818 .696 o 1 7 9 3 86.497 102.056 8.772 o 1 7 9 4 32.516 28.713 1.759 o 1 7 9 5 7.939 4.356 2.493 < 1 7 9 6 20.455 18.684 1.680 o 1 7 9 7 62.800 63.286 2.750 o 1 7 9 8 17.943 16.270 1.953 o 1 7 9 9 20.411 19.711 1.171 o 1 7 9 10 4.739 3.557 2.851 < 1 7 9 11 19.203 18.721 1.477 o 1 7 10 1 1.686 1.962 1.962 < 1 7 10 2 70.422 89.854 15.020 < 1 7 10 3 45.861 44.548 .745 o 1 7 10 4 49.865 59.068 5.538 o 1 7 10 5 6.531 9.408 3.668 < 1 7 10 6 34.353 34.238 .861 o 1 7 10 7 6.151 9.978 2.956 < 1 7 10 8 39.665 46.460 3.397 o 1 7 10 9 10.388 8.901 2.234 < 1 7 10 10 6.515 3.494 3.938 < 1 7 10 11 12.494 6.169 1.789 < 1 7 11 1 55.298 62.704 2.578 o 1 7 11 2 37.578 37.334 .802 o 1 7 11 3 63.847 84.002 8.627 o 1 7 11 4 5.888 3.637 2.806 < 1 7 11 5 6.024 3.721 3.253 < 1 7 11 6 9.170 5.780 3.847 < 1 7 11 7 45.778 51.502 3.965 o 1 7 11 8 13.910 14.928 1.601 < 1 7 11 9 19.804 20.000 2.447 o 1 7 11 10 5.751 4.353 3.891 < 1 7 12 1 19.775 18.121 1.041 o 1 7 12 2 55.520 64.798 7.864 o 1 7 12 3 16.258 14.836 1.717 o 1 7 12 4 32.584 40.858 3.128 o 1 7 12 5 2.985 3.457 2.086 < 1 7 12 6 24.959 27.153 1.329 o 1 7 12 7 10.255 12.809 2.678 < 1 7 12 8 34.043 38.196 2.669 o 1 7 12 9 5.700 4.227 3.018 < 1 7 12 10 5.143 1.112 2.863 < 1 7 13 1 32.565 37.630 2.520 o 1 7 13 2 25.228 23.674 1.253 o 1 7 13 3 49.539 67.903 12.941 < 1 7 13 4 3.672 7.000 2.419 < 1 7 13 5 4.180 7.173 2.549 < 1 7 13 6 8.397 9.378 3.102 < 1 7 13 7 40.124 41.042 2.150 o 1 7 13 8 10.420 8.345 2.713 < 1 7 13 9 7.471 17.163 3.641 < 1 7 14 1 24.017 22.500 1.046 o 1 7 14 2 45.621 55.364 3.674 o 1 7 14 3 4.699 3.447 2.829 < 1 7 14 4 24.059 27.032 1.730 o 1 7 14 5 4.924 6.334 2.773 < 1 7 14 6 21.230 22.168 1.282 o 1 7 14 7 13.333 11.942 1.834 < 1 7 14 8 28.995 31.518 3.548 o 1 7 14 9 3.432 3.802 2.329 < 1 7 15 1 29.963 37.519 3.713 o 1 7 15 2 12.105 13.421 1.763 < 1 7 15 3 36.096 46.864 7.717 < 1 7 15 4 10.099 11.354 2.646 < 1 7 15 5 3.616 1.056 2.428 < 1 7 15 6 9.440 10.560 5.043 < 1 7 15 7 31.870 34.146 3.356 o 1 7 15 8 6.012 6.813 3.183 < 1 7 16 1 7.213 2.518 3.014 < 1 7 16 2 36.447 42.296 5.466 o 1 7 16 3 16.026 15.057 2.245 o 1 7 16 4 21.276 24.128 2.070 o 1 7 16 5 7.833 2.414 3.806 < 1 7 16 6 16.713 20.441 2.094 o 1 7 16 7 6.028 6.771 3.184 < 1 7 16 8 21.757 20.843 1.366 o 1 7 17 1 27.339 28.657 2.367 o 1 7 17 2 8.305 10.596 3.064 < 1 7 17 3 28.435 33.620 4.338 o 1 7 17 4 3.269 5.719 2.224 < 1 7 17 5 4.017 1.291 2.606 < 1 7 17 6 4.757 4.175 3.158 < 1 7 17 7 19.820 22.126 1.605 o 1 7 18 1 6.530 1.557 3.106 < 1 7 18 2 20.440 29.569 6.346 < 1 7 18 3 10.394 10.420 2.718 < 1 7 18 4 13.924 16.778 1.954 o 1 7 18 5 4.093 .344 2.654 < 1 7 18 6 14.822 12.830 1.830 o 1 7 19 1 8.789 15.088 3.251 < 1 7 19 2 8.498 8.256 3.131 < 1 7 19 3 16.702 26.600 6.174 < 1 7 19 4 3.789 3.827 2.514 < 1 7 19 5 3.321 1.546 2.251 < 1 7 20 1 13.646 7.200 1.572 < 1 7 20 2 18.088 21.794 1.587 o 1 7 20 3 5.729 4.359 3.025 < 1 7 20 4 13.085 11.314 1.954 < 1 7 21 1 9.148 11.447 3.370 < 1 8 0 0 40.350 41.466 .720 o 1 8 0 1 115.306 122.598 5.390 o 1 8 0 2 35.780 35.750 .649 o 1 8 0 3 34.966 36.136 2.108 o 1 8 0 4 51.881 50.318 1.270 o 1 8 0 5 134.352 136.167 1.072 o 1 8 0 6 20.435 21.451 .956 o 1 8 0 7 35.542 35.481 .756 o 1 8 0 8 2.325 3.838 1.670 < 1 8 0 9 36.272 37.027 .780 o 1 8 0 10 16.551 17.917 1.355 o 1 8 0 11 36.404 36.151 1.816 o 1 8 0 12 6.382 2.723 3.384 < 1 8 1 0 204.976 198.376 2.882 o 1 8 1 1 36.366 35.344 1.252 o 1 8 1 2 44.564 41.730 .579 o 1 8 1 3 4.901 3.226 2.087 < 1 8 1 4 134.529 129.648 1.541 o 1 8 1 5 15.551 16.100 .921 o 1 8 1 6 92.080 91.463 .849 o 1 8 1 7 23.757 22.747 .822 o 1 8 1 8 36.521 35.549 .762 o 1 8 1 9 11.695 13.639 1.583 o 1 8 1 10 51.060 51.139 .855 o 1 8 1 11 10.768 11.490 2.301 < 1 8 1 12 5.854 6.868 3.199 < 1 8 2 0 100.171 99.114 .815 o 1 8 2 1 130.698 123.050 1.653 o 1 8 2 2 3.203 .939 1.812 < 1 8 2 3 38.558 37.556 1.177 o 1 8 2 4 20.001 21.128 .792 o 1 8 2 5 117.079 113.437 2.109 o 1 8 2 6 35.780 35.957 .709 o 1 8 2 7 36.495 36.179 .779 o 1 8 2 8 7.980 11.010 2.495 < 1 8 2 9 42.410 42.595 .994 o 1 8 2 10 16.335 14.503 1.230 o 1 8 2 11 34.323 33.889 .970 o 1 8 2 12 4.690 3.023 2.567 < 1 8 3 0 176.271 169.654 1.833 o 1 8 3 1 25.246 26.484 2.697 o 1 8 3 2 95.356 91.040 .799 o 1 8 3 3 11.720 12.583 3.797 < 1 8 3 4 156.112 152.327 1.931 o 1 8 3 5 38.679 39.028 1.376 o 1 8 3 6 65.661 62.535 .739 o 1 8 3 7 7.144 9.279 2.618 < 1 8 3 8 26.393 23.907 .853 o 1 8 3 9 9.092 10.521 2.360 < 1 8 3 10 52.096 51.278 .844 o 1 8 3 11 10.689 10.878 2.289 < 1 8 3 12 5.281 5.254 3.373 < 1 8 4 0 75.074 80.688 .977 o 1 8 4 1 120.048 112.921 2.128 o 1 8 4 2 2.825 3.998 1.920 < 1 8 4 3 30.988 30.208 .615 o 1 8 4 4 25.430 27.384 2.916 o 1 8 4 5 89.177 88.061 1.517 o 1 8 4 6 33.800 34.481 .717 o 1 8 4 7 33.514 32.255 .749 o 1 8 4 8 12.247 12.817 1.376 o 1 8 4 9 45.509 44.641 .808 o 1 8 4 10 14.094 12.522 1.409 o 1 8 4 11 31.630 30.493 .970 o 1 8 4 12 4.124 2.253 2.642 < 1 8 5 0 166.084 161.810 1.762 o 1 8 5 1 21.793 21.756 2.516 o 1 8 5 2 59.157 58.351 .640 o 1 8 5 3 9.265 7.883 4.412 < 1 8 5 4 118.387 119.894 1.647 o 1 8 5 5 35.449 35.737 1.198 o 1 8 5 6 73.108 70.115 1.518 o 1 8 5 7 10.866 10.520 1.510 < 1 8 5 8 23.996 25.063 .983 o 1 8 5 9 10.203 11.292 2.175 < 1 8 5 10 43.136 41.458 .880 o 1 8 5 11 7.072 7.835 2.986 < 1 8 5 12 7.973 5.077 4.216 < 1 8 6 0 27.401 32.019 .912 o 1 8 6 1 92.199 89.421 2.312 o 1 8 6 2 19.231 24.428 2.245 o 1 8 6 3 22.339 21.484 .762 o 1 8 6 4 44.600 51.658 4.017 o 1 8 6 5 90.585 88.771 1.979 o 1 8 6 6 20.139 19.944 .978 o 1 8 6 7 23.793 24.561 .987 o 1 8 6 8 4.977 6.661 2.638 < 1 8 6 9 35.644 36.610 .885 o 1 8 6 10 14.504 14.984 1.943 o 1 8 6 11 28.124 29.621 1.086 o 1 8 7 0 158.461 154.267 1.713 o 1 8 7 1 25.485 29.706 1.362 o 1 8 7 2 10.917 11.311 1.216 o 1 8 7 3 19.588 18.611 1.521 o 1 8 7 4 79.888 77.658 1.405 o 1 8 7 5 15.036 15.094 1.113 o 1 8 7 6 80.936 76.754 1.286 o 1 8 7 7 9.271 11.733 2.437 < 1 8 7 8 24.734 24.476 .950 o 1 8 7 9 12.421 12.791 1.437 o 1 8 7 10 35.023 34.391 1.105 o 1 8 7 11 3.475 7.041 2.364 < 1 8 8 0 44.642 50.109 .945 o 1 8 8 1 78.537 75.844 1.071 o 1 8 8 2 11.442 11.894 3.558 < 1 8 8 3 14.493 13.453 1.957 o 1 8 8 4 22.403 26.324 1.449 o 1 8 8 5 92.774 90.879 1.716 o 1 8 8 6 17.171 18.425 1.254 o 1 8 8 7 23.060 23.192 1.046 o 1 8 8 8 9.082 7.507 2.383 < 1 8 8 9 32.313 32.620 .975 o 1 8 8 10 9.340 12.324 2.899 < 1 8 8 11 25.369 26.057 1.141 o 1 8 9 0 111.882 108.226 1.350 o 1 8 9 1 25.648 26.781 1.996 o 1 8 9 2 33.098 35.594 1.347 o 1 8 9 3 7.053 8.138 2.582 < 1 8 9 4 87.054 85.706 1.839 o 1 8 9 5 17.907 18.627 2.441 o 1 8 9 6 54.223 52.175 .799 o 1 8 9 7 3.199 4.647 2.140 < 1 8 9 8 17.724 17.098 2.109 o 1 8 9 9 4.907 8.774 2.710 < 1 8 9 10 35.252 34.581 1.030 o 1 8 9 11 10.823 9.004 5.758 < 1 8 10 0 40.763 45.883 1.077 o 1 8 10 1 78.839 74.690 1.735 o 1 8 10 2 6.220 7.722 3.528 < 1 8 10 3 22.590 21.511 1.318 o 1 8 10 4 4.684 7.865 2.623 < 1 8 10 5 67.656 63.533 1.637 o 1 8 10 6 15.889 17.723 1.329 o 1 8 10 7 23.249 24.628 1.036 o 1 8 10 8 3.724 6.661 2.422 < 1 8 10 9 31.329 30.630 1.019 o 1 8 10 10 5.385 9.585 2.978 < 1 8 11 0 90.736 86.827 1.227 o 1 8 11 1 7.946 12.556 2.492 < 1 8 11 2 37.310 36.892 1.405 o 1 8 11 3 4.731 3.863 2.685 < 1 8 11 4 73.385 71.666 1.123 o 1 8 11 5 19.605 21.330 1.128 o 1 8 11 6 39.191 39.298 1.278 o 1 8 11 7 3.875 4.760 2.474 < 1 8 11 8 17.020 15.087 1.334 o 1 8 11 9 4.366 5.573 2.600 < 1 8 11 10 27.537 29.632 1.189 o 1 8 12 0 9.965 11.057 3.110 < 1 8 12 1 63.782 59.298 2.543 o 1 8 12 2 16.197 18.289 1.272 o 1 8 12 3 25.421 21.617 .926 o 1 8 12 4 18.341 20.165 1.464 o 1 8 12 5 48.691 46.963 1.378 o 1 8 12 6 7.759 12.165 3.265 < 1 8 12 7 14.375 16.178 1.734 o 1 8 12 8 8.728 .734 2.710 < 1 8 12 9 24.629 25.141 2.075 o 1 8 12 10 8.720 9.975 3.218 < 1 8 13 0 85.015 83.792 1.278 o 1 8 13 1 15.367 16.868 1.320 o 1 8 13 2 13.440 11.762 1.846 o 1 8 13 3 2.993 1.819 2.053 < 1 8 13 4 40.853 41.312 .840 o 1 8 13 5 10.992 14.156 2.344 < 1 8 13 6 40.232 38.335 1.572 o 1 8 13 7 3.689 8.822 2.484 < 1 8 13 8 15.557 15.516 1.645 o 1 8 13 9 4.036 7.836 2.621 < 1 8 14 0 8.609 15.523 3.641 < 1 8 14 1 48.685 46.510 .848 o 1 8 14 2 12.194 13.322 1.753 o 1 8 14 3 13.743 12.384 1.515 o 1 8 14 4 14.559 15.551 1.856 o 1 8 14 5 47.637 45.711 1.596 o 1 8 14 6 9.284 13.374 2.878 < 1 8 14 7 7.805 9.086 3.287 < 1 8 14 8 4.627 2.709 2.754 < 1 8 14 9 18.955 17.879 1.599 o 1 8 15 0 63.767 61.203 1.243 o 1 8 15 1 3.591 13.915 2.447 < 1 8 15 2 7.369 12.453 3.109 < 1 8 15 3 3.387 5.190 2.267 < 1 8 15 4 40.388 37.312 .956 o 1 8 15 5 10.554 13.413 2.747 < 1 8 15 6 30.627 28.169 2.744 o 1 8 15 7 6.697 4.293 4.323 < 1 8 15 8 7.018 9.639 3.372 < 1 8 16 0 17.431 20.021 2.033 o 1 8 16 1 35.907 33.464 .955 o 1 8 16 2 4.160 .998 2.918 < 1 8 16 3 15.910 11.231 2.430 o 1 8 16 4 8.453 9.292 3.096 < 1 8 16 5 36.995 34.977 1.365 o 1 8 16 6 8.434 9.704 4.645 < 1 8 16 7 7.113 8.250 3.412 < 1 8 17 0 36.389 32.832 1.413 o 1 8 17 1 3.844 9.448 2.518 < 1 8 17 2 15.169 13.367 3.973 < 1 8 17 3 6.364 4.870 3.048 < 1 8 17 4 34.169 30.632 1.018 o 1 8 17 5 12.082 10.878 3.757 < 1 8 17 6 21.361 18.556 1.398 o 1 8 17 7 5.373 .005 3.025 < 1 8 18 0 7.134 12.653 3.802 < 1 8 18 1 26.309 22.506 1.156 o 1 8 18 2 4.420 1.790 2.625 < 1 8 18 3 4.765 9.832 2.857 < 1 8 18 4 6.879 9.001 3.302 < 1 8 18 5 20.777 21.716 2.899 o 1 8 18 6 3.459 3.685 2.358 < 1 8 19 0 30.012 25.282 1.455 o 1 8 19 1 6.229 7.802 3.699 < 1 8 19 2 9.562 7.058 2.966 < 1 8 19 3 4.009 2.998 2.578 < 1 8 19 4 16.740 16.707 4.366 < 1 8 19 5 3.837 6.489 2.576 < 1 8 20 0 4.296 5.310 2.918 < 1 8 20 1 21.297 17.491 1.397 o 1 8 20 2 5.085 4.565 2.812 < 1 8 20 3 7.257 5.597 4.659 < 1 9 0 1 109.905 112.368 1.511 o 1 9 0 2 51.313 50.493 .598 o 1 9 0 3 86.424 93.733 4.020 o 1 9 0 4 68.387 69.716 1.240 o 1 9 0 5 11.825 13.413 1.261 o 1 9 0 6 24.454 22.555 .837 o 1 9 0 7 87.469 86.705 .868 o 1 9 0 8 28.223 28.433 .871 o 1 9 0 9 23.073 23.691 1.009 o 1 9 0 10 4.111 5.136 2.737 < 1 9 0 11 18.039 18.749 1.300 o 1 9 0 12 19.216 18.231 1.241 o 1 9 1 1 90.744 90.714 5.864 o 1 9 1 2 115.769 113.039 1.062 o 1 9 1 3 78.992 82.192 3.725 o 1 9 1 4 69.051 69.837 1.121 o 1 9 1 5 2.683 5.103 1.945 < 1 9 1 6 44.083 45.598 .700 o 1 9 1 7 55.450 56.933 1.344 o 1 9 1 8 58.057 58.590 .792 o 1 9 1 9 9.230 12.745 2.404 < 1 9 1 10 4.292 .642 2.768 < 1 9 1 11 18.284 14.965 1.238 o 1 9 1 12 21.094 22.353 1.261 o 1 9 2 1 99.772 95.367 1.117 o 1 9 2 2 56.072 63.127 1.282 o 1 9 2 3 114.587 105.798 1.536 o 1 9 2 4 46.271 46.635 1.187 o 1 9 2 5 3.853 2.294 2.153 < 1 9 2 6 17.938 16.092 .976 o 1 9 2 7 76.058 73.606 .821 o 1 9 2 8 35.869 36.574 1.956 o 1 9 2 9 27.467 27.219 .890 o 1 9 2 10 4.465 4.108 2.516 < 1 9 2 11 20.892 19.129 1.146 o 1 9 2 12 13.063 16.723 4.055 < 1 9 3 1 29.745 33.490 3.736 o 1 9 3 2 114.370 109.977 .923 o 1 9 3 3 107.976 116.651 12.761 o 1 9 3 4 54.287 52.961 .782 o 1 9 3 5 29.825 29.811 1.996 o 1 9 3 6 39.918 40.536 .719 o 1 9 3 7 48.595 47.723 .745 o 1 9 3 8 57.920 58.677 .793 o 1 9 3 9 19.351 19.867 1.119 o 1 9 3 10 5.109 2.659 2.745 < 1 9 3 11 15.073 14.914 1.421 o 1 9 3 12 22.016 20.707 1.144 o 1 9 4 1 74.670 73.484 1.539 o 1 9 4 2 48.264 55.173 3.830 o 1 9 4 3 134.967 129.675 2.100 o 1 9 4 4 20.329 24.640 5.285 < 1 9 4 5 14.239 12.619 1.049 o 1 9 4 6 14.621 14.414 1.118 o 1 9 4 7 64.418 63.134 .772 o 1 9 4 8 38.296 40.217 2.435 o 1 9 4 9 26.542 26.214 .943 o 1 9 4 10 3.663 4.075 2.558 < 1 9 4 11 18.237 18.857 1.284 o 1 9 4 12 15.872 14.927 1.416 o 1 9 5 1 55.487 62.442 3.911 o 1 9 5 2 129.098 121.989 2.032 o 1 9 5 3 60.969 74.846 15.918 < 1 9 5 4 51.265 50.394 1.009 o 1 9 5 5 7.433 10.196 2.346 < 1 9 5 6 43.527 42.310 .722 o 1 9 5 7 47.369 49.455 3.401 o 1 9 5 8 50.895 51.332 .823 o 1 9 5 9 12.625 13.248 1.547 < 1 9 5 10 4.491 2.527 2.488 < 1 9 5 11 13.923 12.289 1.565 o 1 9 6 1 104.197 102.082 .884 o 1 9 6 2 31.488 39.858 3.875 o 1 9 6 3 103.045 99.660 2.152 o 1 9 6 4 34.231 38.239 3.303 o 1 9 6 5 3.501 6.569 2.137 < 1 9 6 6 26.156 25.225 .846 o 1 9 6 7 68.055 66.894 .820 o 1 9 6 8 28.607 31.200 1.724 o 1 9 6 9 20.436 19.843 1.124 o 1 9 6 10 4.699 5.223 2.650 < 1 9 6 11 11.678 16.532 4.931 < 1 9 7 1 60.086 71.754 5.563 o 1 9 7 2 106.061 103.830 1.203 o 1 9 7 3 42.156 50.699 8.993 < 1 9 7 4 51.745 50.204 1.581 o 1 9 7 5 6.166 6.396 2.646 < 1 9 7 6 45.786 44.685 .791 o 1 9 7 7 37.863 42.141 3.280 o 1 9 7 8 42.975 41.931 .842 o 1 9 7 9 8.573 7.690 2.649 < 1 9 7 10 4.011 .214 2.423 < 1 9 7 11 9.466 12.733 2.943 < 1 9 8 1 74.298 71.137 1.011 o 1 9 8 2 35.037 40.363 2.552 o 1 9 8 3 78.674 75.175 1.488 o 1 9 8 4 37.437 44.344 3.774 o 1 9 8 5 6.958 3.884 2.604 < 1 9 8 6 19.337 18.169 1.045 o 1 9 8 7 54.114 53.406 .840 o 1 9 8 8 22.088 28.226 5.755 < 1 9 8 9 22.724 19.446 1.040 o 1 9 8 10 6.921 2.181 2.975 < 1 9 8 11 15.798 14.334 1.570 o 1 9 9 1 28.591 28.481 .789 o 1 9 9 2 77.212 76.228 1.052 o 1 9 9 3 58.696 70.669 8.751 o 1 9 9 4 48.223 45.651 1.806 o 1 9 9 5 10.519 8.366 4.530 < 1 9 9 6 35.452 34.390 1.390 o 1 9 9 7 29.128 29.750 1.799 o 1 9 9 8 38.662 38.128 .916 o 1 9 9 9 8.026 10.442 2.962 < 1 9 9 10 4.148 1.520 2.702 < 1 9 9 11 12.696 13.533 1.904 < 1 9 10 1 35.252 34.720 1.166 o 1 9 10 2 37.215 43.523 4.649 o 1 9 10 3 78.307 76.621 1.521 o 1 9 10 4 13.502 19.733 4.183 < 1 9 10 5 8.177 6.956 2.585 < 1 9 10 6 7.567 9.603 2.796 < 1 9 10 7 42.135 39.314 .900 o 1 9 10 8 19.254 26.643 5.034 < 1 9 10 9 22.202 20.137 2.629 o 1 9 10 10 3.931 1.423 2.541 < 1 9 11 1 28.201 31.941 2.004 o 1 9 11 2 64.710 63.290 1.109 o 1 9 11 3 32.205 47.790 8.425 < 1 9 11 4 33.607 31.886 .856 o 1 9 11 5 6.464 7.138 3.613 < 1 9 11 6 24.119 23.795 1.105 o 1 9 11 7 23.895 28.246 2.468 o 1 9 11 8 33.908 33.095 1.027 o 1 9 11 9 8.264 8.295 3.032 < 1 9 11 10 3.001 .049 2.159 < 1 9 12 1 31.839 31.917 .898 o 1 9 12 2 27.539 35.768 7.169 < 1 9 12 3 62.084 56.988 1.448 o 1 9 12 4 7.417 14.695 4.007 < 1 9 12 5 3.160 1.099 2.132 < 1 9 12 6 13.255 13.314 1.655 o 1 9 12 7 35.932 35.663 1.619 o 1 9 12 8 18.685 19.683 1.353 o 1 9 12 9 15.027 14.805 1.675 o 1 9 13 1 31.610 38.558 2.882 o 1 9 13 2 50.873 48.563 2.045 o 1 9 13 3 15.340 23.927 6.480 < 1 9 13 4 28.444 25.185 .936 o 1 9 13 5 3.599 .165 2.365 < 1 9 13 6 23.186 21.760 1.153 o 1 9 13 7 21.913 25.844 4.699 < 1 9 13 8 25.760 24.515 1.781 o 1 9 13 9 4.008 6.434 2.588 < 1 9 14 1 35.458 33.463 1.936 o 1 9 14 2 21.302 25.368 1.096 o 1 9 14 3 37.143 35.500 .918 o 1 9 14 4 14.711 18.505 1.899 o 1 9 14 5 4.294 3.251 2.603 < 1 9 14 6 14.203 14.617 1.656 < 1 9 14 7 30.678 28.978 1.056 o 1 9 14 8 14.651 14.166 1.720 o 1 9 15 1 14.875 17.895 1.416 o 1 9 15 2 38.872 34.732 1.234 o 1 9 15 3 22.441 27.286 2.511 o 1 9 15 4 21.401 22.780 1.231 o 1 9 15 5 7.660 3.065 2.860 < 1 9 15 6 18.883 18.525 1.409 o 1 9 15 7 10.217 16.624 3.178 < 1 9 15 8 18.972 17.368 1.461 o 1 9 16 1 23.231 19.119 1.528 o 1 9 16 2 14.138 19.596 1.745 o 1 9 16 3 33.821 33.368 1.040 o 1 9 16 4 6.675 13.026 3.216 < 1 9 16 5 5.605 1.831 3.015 < 1 9 16 6 4.606 7.731 2.759 < 1 9 16 7 18.968 17.959 1.521 o 1 9 17 1 4.225 7.052 2.560 < 1 9 17 2 32.103 28.699 1.009 o 1 9 17 3 17.406 21.389 6.427 < 1 9 17 4 17.587 15.038 1.692 o 1 9 17 5 5.735 .652 3.458 < 1 9 17 6 14.851 11.348 1.710 < 1 9 18 1 16.156 13.055 2.262 o 1 9 18 2 11.420 14.485 4.821 < 1 9 18 3 27.477 24.704 1.254 o 1 9 18 4 6.018 8.741 3.193 < 1 9 18 5 6.249 .983 3.472 < 1 9 19 1 4.109 10.366 2.703 < 1 9 19 2 24.201 20.702 1.274 o 1 9 19 3 7.873 11.193 4.188 < 1 9 19 4 10.812 10.355 2.816 < 1 9 20 1 13.636 11.340 1.978 < 1 9 20 2 6.759 11.191 3.724 < 1 10 0 0 181.236 189.323 1.837 o 1 10 0 1 35.356 36.925 1.110 o 1 10 0 2 11.217 10.049 .935 o 1 10 0 3 7.450 4.900 1.940 < 1 10 0 4 93.680 94.128 3.406 o 1 10 0 5 4.289 5.856 2.627 < 1 10 0 6 93.361 90.681 .878 o 1 10 0 7 10.869 10.537 1.587 < 1 10 0 8 32.494 32.077 .829 o 1 10 0 9 5.596 4.117 2.725 < 1 10 0 10 45.286 44.655 .861 o 1 10 0 11 5.521 .880 2.943 < 1 10 0 12 5.107 8.194 2.819 < 1 10 1 0 10.314 11.070 1.127 o 1 10 1 1 118.005 114.324 5.605 o 1 10 1 2 8.778 7.306 3.238 < 1 10 1 3 47.122 43.760 1.238 o 1 10 1 4 39.538 39.389 1.043 o 1 10 1 5 119.038 118.307 3.125 o 1 10 1 6 8.475 7.533 2.236 < 1 10 1 7 19.281 17.848 1.048 o 1 10 1 8 7.840 9.403 2.478 < 1 10 1 9 45.877 47.459 .828 o 1 10 1 10 3.203 .737 2.174 < 1 10 1 11 27.784 28.856 1.071 o 1 10 1 12 5.582 3.510 3.106 < 1 10 2 0 140.086 146.908 3.353 o 1 10 2 1 21.936 21.680 .666 o 1 10 2 2 41.135 45.356 .609 o 1 10 2 3 5.725 8.028 3.130 < 1 10 2 4 106.383 108.760 .912 o 1 10 2 5 7.853 7.625 2.088 < 1 10 2 6 75.146 73.343 1.719 o 1 10 2 7 4.532 4.126 3.002 < 1 10 2 8 21.874 22.111 1.232 o 1 10 2 9 3.101 4.000 2.118 < 1 10 2 10 48.103 47.009 1.830 o 1 10 2 11 2.562 .954 1.848 < 1 10 2 12 9.904 7.463 3.642 < 1 10 3 0 42.473 42.801 .846 o 1 10 3 1 124.618 126.797 10.027 o 1 10 3 2 2.517 .193 1.732 < 1 10 3 3 48.613 49.796 5.415 o 1 10 3 4 10.822 12.570 1.285 o 1 10 3 5 90.665 91.194 5.067 o 1 10 3 6 3.393 1.330 2.239 < 1 10 3 7 30.318 29.072 1.160 o 1 10 3 8 15.782 13.448 1.107 o 1 10 3 9 45.813 47.556 2.232 o 1 10 3 10 5.785 .596 2.799 < 1 10 3 11 24.892 25.626 1.120 o 1 10 4 0 130.475 134.047 1.457 o 1 10 4 1 3.561 1.642 2.189 < 1 10 4 2 58.975 68.323 3.258 o 1 10 4 3 25.960 25.163 .724 o 1 10 4 4 98.147 106.830 13.416 o 1 10 4 5 14.708 13.640 1.070 o 1 10 4 6 63.800 67.426 .923 o 1 10 4 7 2.840 .101 1.913 < 1 10 4 8 12.689 15.827 1.723 o 1 10 4 9 3.090 2.892 2.117 < 1 10 4 10 43.200 44.203 .899 o 1 10 4 11 2.986 3.156 2.093 < 1 10 5 0 41.516 41.202 .908 o 1 10 5 1 99.446 114.049 5.645 o 1 10 5 2 7.097 9.324 2.222 < 1 10 5 3 38.913 40.472 5.726 o 1 10 5 4 4.266 3.582 2.347 < 1 10 5 5 89.137 93.488 5.357 o 1 10 5 6 4.737 2.567 2.522 < 1 10 5 7 24.857 25.870 2.381 o 1 10 5 8 4.815 7.131 2.622 < 1 10 5 9 37.534 39.273 2.662 o 1 10 5 10 3.052 .923 2.090 < 1 10 5 11 28.016 24.832 .990 o 1 10 6 0 139.912 158.526 1.574 o 1 10 6 1 6.210 4.640 2.337 < 1 10 6 2 12.982 19.542 4.007 < 1 10 6 3 19.093 20.886 .900 o 1 10 6 4 54.749 66.047 6.087 o 1 10 6 5 4.317 6.584 2.343 < 1 10 6 6 75.132 77.112 1.370 o 1 10 6 7 5.005 4.604 3.300 < 1 10 6 8 18.345 20.114 1.098 o 1 10 6 9 5.066 .949 2.735 < 1 10 6 10 38.239 38.689 1.276 o 1 10 6 11 2.857 2.235 2.090 < 1 10 7 0 3.612 .332 2.392 < 1 10 7 1 78.079 91.261 8.250 o 1 10 7 2 10.333 8.422 1.414 < 1 10 7 3 21.084 23.562 2.530 o 1 10 7 4 20.153 21.398 2.628 o 1 10 7 5 92.043 95.752 2.974 o 1 10 7 6 6.144 2.580 3.415 < 1 10 7 7 16.016 16.882 1.316 o 1 10 7 8 4.475 2.320 2.493 < 1 10 7 9 29.960 33.557 1.708 o 1 10 7 10 6.190 .218 2.986 < 1 10 7 11 22.886 24.536 1.296 o 1 10 8 0 88.959 106.794 1.208 o 1 10 8 1 7.735 11.181 2.442 < 1 10 8 2 22.783 33.655 7.052 < 1 10 8 3 6.730 1.258 2.486 < 1 10 8 4 57.940 68.566 7.399 o 1 10 8 5 7.679 2.910 2.424 < 1 10 8 6 55.198 58.289 .792 o 1 10 8 7 8.752 7.595 2.330 < 1 10 8 8 11.313 17.088 4.772 < 1 10 8 9 4.101 .122 2.767 < 1 10 8 10 36.002 36.390 .960 o 1 10 8 11 3.667 .060 2.398 < 1 10 9 0 5.420 7.361 2.967 < 1 10 9 1 65.683 79.112 6.997 o 1 10 9 2 3.222 5.688 2.081 < 1 10 9 3 21.099 27.285 2.842 o 1 10 9 4 18.419 17.060 2.142 o 1 10 9 5 68.417 74.703 3.301 o 1 10 9 6 2.862 4.664 1.993 < 1 10 9 7 14.461 16.552 5.323 < 1 10 9 8 6.122 5.628 3.311 < 1 10 9 9 29.792 32.183 1.943 o 1 10 9 10 2.988 .243 2.151 < 1 10 10 0 60.727 71.099 1.071 o 1 10 10 1 4.465 5.861 2.417 < 1 10 10 2 37.878 43.062 1.927 o 1 10 10 3 6.275 1.734 2.656 < 1 10 10 4 66.840 74.344 9.626 o 1 10 10 5 5.853 .774 3.255 < 1 10 10 6 39.800 40.567 .861 o 1 10 10 7 4.542 .054 2.542 < 1 10 10 8 12.519 12.396 1.631 < 1 10 10 9 2.374 1.026 1.730 < 1 10 10 10 29.285 30.369 1.387 o 1 10 11 0 18.564 18.171 1.552 o 1 10 11 1 55.764 66.371 7.685 o 1 10 11 2 9.903 9.640 2.152 < 1 10 11 3 22.955 32.065 7.141 < 1 10 11 4 3.522 3.106 2.301 < 1 10 11 5 48.061 55.192 .828 o 1 10 11 6 4.322 .245 2.564 < 1 10 11 7 11.774 13.412 1.751 < 1 10 11 8 5.361 6.248 2.905 < 1 10 11 9 24.697 27.207 1.345 o 1 10 11 10 3.770 .616 2.538 < 1 10 12 0 67.933 78.472 1.181 o 1 10 12 1 2.306 2.949 1.686 < 1 10 12 2 14.435 15.660 1.654 o 1 10 12 3 3.422 3.358 2.256 < 1 10 12 4 34.331 47.818 8.944 < 1 10 12 5 3.946 3.145 2.365 < 1 10 12 6 36.319 38.960 .929 o 1 10 12 7 3.756 2.322 2.429 < 1 10 12 8 7.520 12.538 3.628 < 1 10 12 9 6.310 1.640 3.509 < 1 10 13 0 8.613 5.450 3.228 < 1 10 13 1 40.883 51.885 4.156 o 1 10 13 2 2.646 .426 1.922 < 1 10 13 3 13.500 17.768 2.046 o 1 10 13 4 3.195 3.292 2.192 < 1 10 13 5 45.291 49.093 .905 o 1 10 13 6 3.559 5.191 2.402 < 1 10 13 7 6.782 7.926 3.595 < 1 10 13 8 5.468 2.550 2.939 < 1 10 13 9 16.968 18.390 1.605 o 1 10 14 0 56.344 64.345 1.176 o 1 10 14 1 3.148 .763 2.276 < 1 10 14 2 5.321 11.415 2.860 < 1 10 14 3 4.615 2.602 2.571 < 1 10 14 4 28.707 34.764 3.362 o 1 10 14 5 5.463 4.083 2.939 < 1 10 14 6 29.381 30.310 1.093 o 1 10 14 7 3.909 .580 2.559 < 1 10 14 8 8.317 8.692 4.421 < 1 10 15 0 3.907 .420 2.627 < 1 10 15 1 24.216 37.550 7.521 < 1 10 15 2 4.402 3.668 2.887 < 1 10 15 3 14.106 11.528 1.470 o 1 10 15 4 5.429 2.046 2.944 < 1 10 15 5 36.177 37.220 1.438 o 1 10 15 6 4.422 1.509 2.658 < 1 10 15 7 6.304 6.880 3.338 < 1 10 15 8 3.767 .105 2.536 < 1 10 16 0 27.073 32.717 1.650 o 1 10 16 1 3.672 1.582 2.385 < 1 10 16 2 13.028 16.589 1.868 < 1 10 16 3 5.370 1.748 2.884 < 1 10 16 4 24.885 30.812 2.595 o 1 10 16 5 4.984 1.981 2.769 < 1 10 16 6 20.460 19.437 1.447 o 1 10 16 7 2.992 2.707 2.183 < 1 10 17 0 5.201 .024 3.097 < 1 10 17 1 22.267 25.924 1.270 o 1 10 17 2 2.647 1.559 1.891 < 1 10 17 3 10.447 10.417 2.730 < 1 10 17 4 2.954 1.441 2.131 < 1 10 17 5 20.321 24.471 1.470 o 1 10 17 6 5.644 2.505 3.044 < 1 10 18 0 21.312 24.383 2.137 o 1 10 18 1 2.911 2.790 2.102 < 1 10 18 2 7.700 9.737 3.253 < 1 10 18 3 2.864 1.661 2.035 < 1 10 18 4 16.093 19.116 1.766 o 1 10 18 5 3.402 .751 2.348 < 1 10 19 0 5.396 .489 3.255 < 1 10 19 1 18.054 19.374 1.585 o 1 10 19 2 3.331 1.391 2.298 < 1 10 19 3 5.700 6.210 3.668 < 1 10 20 0 22.420 23.362 1.936 o 1 10 20 1 9.341 .044 2.927 < 1 11 0 1 67.522 68.501 .692 o 1 11 0 2 87.042 91.686 1.846 o 1 11 0 3 87.281 94.633 1.695 o 1 11 0 4 42.410 46.643 2.935 o 1 11 0 5 2.212 1.180 1.582 < 1 11 0 6 61.059 59.345 .760 o 1 11 0 7 63.778 65.125 .794 o 1 11 0 8 35.559 37.442 1.203 o 1 11 0 9 23.830 25.376 1.026 o 1 11 0 10 2.311 .320 1.662 < 1 11 0 11 12.616 15.589 1.830 o 1 11 1 1 58.322 56.494 2.928 o 1 11 1 2 110.866 106.879 1.470 o 1 11 1 3 35.211 40.201 2.014 o 1 11 1 4 57.631 55.730 1.080 o 1 11 1 5 23.051 22.472 .857 o 1 11 1 6 43.091 45.389 2.367 o 1 11 1 7 46.198 44.212 1.038 o 1 11 1 8 48.212 49.122 .789 o 1 11 1 9 17.800 18.918 1.206 o 1 11 1 10 3.481 2.556 2.255 < 1 11 1 11 9.259 7.737 3.393 < 1 11 2 1 60.056 59.943 1.933 o 1 11 2 2 80.571 95.906 3.273 o 1 11 2 3 89.779 90.741 5.333 o 1 11 2 4 29.219 30.602 .740 o 1 11 2 5 5.927 3.977 3.305 < 1 11 2 6 39.716 40.485 1.306 o 1 11 2 7 61.041 58.692 2.090 o 1 11 2 8 35.925 37.749 .818 o 1 11 2 9 25.078 24.721 .971 o 1 11 2 10 5.032 4.026 3.057 < 1 11 2 11 11.978 14.891 3.129 < 1 11 3 1 3.352 8.255 2.384 < 1 11 3 2 97.693 96.816 1.005 o 1 11 3 3 68.104 71.141 7.396 o 1 11 3 4 45.784 44.400 .669 o 1 11 3 5 3.630 3.683 2.414 < 1 11 3 6 35.649 36.473 .791 o 1 11 3 7 26.625 26.646 .867 o 1 11 3 8 44.638 42.564 .813 o 1 11 3 9 21.707 21.739 1.059 o 1 11 3 10 5.892 .016 3.548 < 1 11 3 11 7.053 10.286 2.978 < 1 11 4 1 73.050 67.929 1.215 o 1 11 4 2 87.355 100.371 3.855 o 1 11 4 3 78.064 73.657 1.017 o 1 11 4 4 26.517 29.376 2.689 o 1 11 4 5 7.895 9.921 2.497 < 1 11 4 6 23.775 24.648 .903 o 1 11 4 7 52.478 50.903 .773 o 1 11 4 8 30.328 34.555 1.015 o 1 11 4 9 22.757 23.131 1.043 o 1 11 4 10 4.159 7.124 2.544 < 1 11 4 11 15.343 14.376 1.471 o 1 11 5 1 41.757 43.983 3.305 o 1 11 5 2 90.769 87.537 .969 o 1 11 5 3 44.821 54.626 11.658 < 1 11 5 4 38.775 39.381 .686 o 1 11 5 5 12.021 15.455 1.353 o 1 11 5 6 34.496 32.899 .790 o 1 11 5 7 30.551 33.439 3.023 o 1 11 5 8 37.727 38.130 .860 o 1 11 5 9 16.290 17.364 1.326 o 1 11 5 10 4.116 .207 2.484 < 1 11 5 11 7.134 9.059 3.000 < 1 11 6 1 53.618 51.663 .685 o 1 11 6 2 65.700 78.584 4.844 o 1 11 6 3 71.420 69.620 1.352 o 1 11 6 4 33.329 39.647 4.362 o 1 11 6 5 3.712 5.929 2.255 < 1 11 6 6 31.972 33.096 .911 o 1 11 6 7 42.079 42.751 1.181 o 1 11 6 8 23.583 26.247 3.280 o 1 11 6 9 20.478 20.148 2.323 o 1 11 6 10 6.102 3.702 3.399 < 1 11 6 11 11.231 14.243 4.140 < 1 11 7 1 44.396 50.027 4.126 o 1 11 7 2 74.045 73.106 1.719 o 1 11 7 3 22.364 29.254 6.904 < 1 11 7 4 39.160 38.914 .761 o 1 11 7 5 14.127 15.576 1.937 o 1 11 7 6 28.829 29.784 1.209 o 1 11 7 7 33.161 36.450 4.551 o 1 11 7 8 37.333 35.746 1.347 o 1 11 7 9 13.552 14.770 1.614 < 1 11 7 10 7.008 1.219 2.981 < 1 11 7 11 5.639 6.901 2.992 < 1 11 8 1 31.847 30.907 .744 o 1 11 8 2 35.852 54.844 11.142 < 1 11 8 3 69.252 63.914 .782 o 1 11 8 4 29.443 34.159 3.611 o 1 11 8 5 4.838 2.228 2.597 < 1 11 8 6 31.652 33.493 .909 o 1 11 8 7 40.206 40.318 .836 o 1 11 8 8 23.490 24.676 1.130 o 1 11 8 9 16.503 18.093 1.807 o 1 11 8 10 3.862 .944 2.520 < 1 11 9 1 5.283 9.222 2.765 < 1 11 9 2 61.810 59.663 1.428 o 1 11 9 3 32.641 44.821 10.132 < 1 11 9 4 30.355 31.123 1.201 o 1 11 9 5 6.396 5.106 2.737 < 1 11 9 6 27.793 26.236 1.120 o 1 11 9 7 22.246 24.517 2.066 o 1 11 9 8 32.067 31.720 .948 o 1 11 9 9 13.332 16.408 1.723 o 1 11 9 10 2.792 1.571 1.973 < 1 11 10 1 35.708 32.860 .785 o 1 11 10 2 45.657 54.174 4.617 o 1 11 10 3 56.049 53.482 2.046 o 1 11 10 4 16.147 18.136 1.283 o 1 11 10 5 3.111 1.511 2.117 < 1 11 10 6 21.320 21.377 1.118 o 1 11 10 7 37.922 37.529 1.116 o 1 11 10 8 21.152 24.499 1.751 o 1 11 10 9 16.448 14.974 1.419 o 1 11 10 10 7.524 2.230 3.666 < 1 11 11 1 9.468 15.509 2.465 < 1 11 11 2 54.887 53.966 1.308 o 1 11 11 3 30.276 40.641 11.153 < 1 11 11 4 25.623 26.195 1.406 o 1 11 11 5 4.589 1.253 2.985 < 1 11 11 6 26.865 25.763 1.012 o 1 11 11 7 19.686 20.951 1.913 o 1 11 11 8 28.242 25.564 1.078 o 1 11 11 9 7.229 12.328 3.862 < 1 11 12 1 39.150 37.249 .823 o 1 11 12 2 34.388 42.768 4.817 o 1 11 12 3 43.549 41.725 .829 o 1 11 12 4 9.229 16.829 2.875 < 1 11 12 5 4.695 .073 2.843 < 1 11 12 6 12.301 17.296 5.905 < 1 11 12 7 32.391 29.984 .998 o 1 11 12 8 10.973 18.243 4.651 < 1 11 12 9 10.514 11.653 2.742 < 1 11 13 1 23.968 26.706 1.944 o 1 11 13 2 45.188 44.809 .840 o 1 11 13 3 14.997 20.810 4.639 < 1 11 13 4 25.947 21.989 1.034 o 1 11 13 5 7.939 7.050 2.985 < 1 11 13 6 21.881 20.546 1.216 o 1 11 13 7 13.644 18.889 4.247 < 1 11 13 8 19.235 19.701 1.406 o 1 11 14 1 24.334 22.003 1.017 o 1 11 14 2 18.189 26.906 6.707 < 1 11 14 3 39.584 36.409 1.586 o 1 11 14 4 13.938 17.531 2.988 < 1 11 14 5 5.347 2.682 2.874 < 1 11 14 6 11.627 14.941 4.303 < 1 11 14 7 22.667 20.473 1.187 o 1 11 14 8 12.526 11.601 1.875 < 1 11 15 1 12.021 12.808 1.770 < 1 11 15 2 33.798 32.029 1.018 o 1 11 15 3 17.392 21.931 1.639 o 1 11 15 4 16.808 15.913 1.476 o 1 11 15 5 2.961 1.425 2.139 < 1 11 15 6 16.347 13.143 1.515 o 1 11 15 7 7.653 12.125 4.088 < 1 11 16 1 16.395 13.459 1.375 o 1 11 16 2 15.435 21.787 4.797 < 1 11 16 3 30.333 25.650 1.031 o 1 11 16 4 5.061 12.521 3.052 < 1 11 16 5 3.586 .390 2.415 < 1 11 16 6 8.748 9.843 4.652 < 1 11 17 1 5.705 5.807 3.014 < 1 11 17 2 21.945 21.626 1.258 o 1 11 17 3 13.157 20.001 4.862 < 1 11 17 4 12.807 12.810 1.859 < 1 11 17 5 5.660 1.284 3.051 < 1 11 18 1 9.234 11.856 4.439 < 1 11 18 2 12.879 16.323 1.931 < 1 11 18 3 15.031 17.108 2.272 o 1 11 18 4 5.553 7.305 3.561 < 1 11 19 1 6.597 8.537 3.512 < 1 11 19 2 16.460 15.504 3.518 < 1 11 19 3 6.637 10.705 3.958 < 1 12 0 0 .810 2.384 1.718 < 1 12 0 1 118.917 121.340 2.397 o 1 12 0 2 26.926 26.992 .717 o 1 12 0 3 40.130 41.730 3.963 o 1 12 0 4 33.011 32.348 .707 o 1 12 0 5 96.740 100.137 4.073 o 1 12 0 6 16.423 17.010 1.157 o 1 12 0 7 4.605 10.016 2.578 < 1 12 0 8 5.300 1.301 2.867 < 1 12 0 9 42.934 43.706 .873 o 1 12 0 10 12.216 12.847 1.846 o 1 12 0 11 17.584 20.656 1.834 o 1 12 1 0 126.997 120.004 1.394 o 1 12 1 1 39.746 39.593 .909 o 1 12 1 2 39.696 38.332 1.148 o 1 12 1 3 18.426 20.845 1.000 o 1 12 1 4 66.111 63.431 .729 o 1 12 1 5 19.912 19.931 2.397 o 1 12 1 6 59.011 63.872 3.201 o 1 12 1 7 9.321 5.403 3.444 < 1 12 1 8 14.494 15.097 1.287 o 1 12 1 9 15.394 15.596 1.354 o 1 12 1 10 37.574 35.322 2.212 o 1 12 1 11 5.925 3.337 2.824 < 1 12 2 0 44.207 43.533 1.247 o 1 12 2 1 116.979 114.849 2.873 o 1 12 2 2 3.804 2.414 2.513 < 1 12 2 3 46.008 45.502 1.230 o 1 12 2 4 11.683 12.496 1.338 o 1 12 2 5 97.803 93.177 .909 o 1 12 2 6 24.858 26.367 1.469 o 1 12 2 7 13.664 14.140 1.338 o 1 12 2 8 5.560 7.540 3.305 < 1 12 2 9 42.886 42.157 .864 o 1 12 2 10 12.196 10.479 1.786 o 1 12 2 11 19.085 20.704 2.273 o 1 12 3 0 99.473 103.291 1.235 o 1 12 3 1 35.935 36.178 2.110 o 1 12 3 2 32.644 32.225 .698 o 1 12 3 3 2.548 7.627 1.794 < 1 12 3 4 69.173 68.527 .759 o 1 12 3 5 30.092 29.784 .909 o 1 12 3 6 62.608 60.048 1.954 o 1 12 3 7 3.328 2.318 2.375 < 1 12 3 8 7.756 11.006 2.849 < 1 12 3 9 5.342 9.335 2.847 < 1 12 3 10 35.726 35.707 .908 o 1 12 3 11 3.896 5.070 2.665 < 1 12 4 0 63.935 64.055 1.009 o 1 12 4 1 102.515 99.187 1.370 o 1 12 4 2 5.735 7.679 2.951 < 1 12 4 3 54.337 51.811 .709 o 1 12 4 4 6.947 2.618 3.681 < 1 12 4 5 90.141 85.182 .875 o 1 12 4 6 24.203 26.999 .940 o 1 12 4 7 17.328 17.857 1.184 o 1 12 4 8 7.938 7.851 2.471 < 1 12 4 9 39.715 37.836 .868 o 1 12 4 10 7.881 9.603 2.903 < 1 12 4 11 22.084 20.619 1.300 o 1 12 5 0 107.303 102.005 1.306 o 1 12 5 1 29.412 31.453 2.564 o 1 12 5 2 18.063 17.338 .987 o 1 12 5 3 11.922 14.568 5.037 < 1 12 5 4 64.808 62.931 .746 o 1 12 5 5 26.390 26.835 2.692 o 1 12 5 6 60.646 58.138 1.583 o 1 12 5 7 2.555 2.339 1.795 < 1 12 5 8 9.303 12.085 2.418 < 1 12 5 9 8.928 9.485 3.281 < 1 12 5 10 31.932 34.705 1.595 o 1 12 5 11 4.427 4.716 2.627 < 1 12 6 0 14.236 11.658 1.466 o 1 12 6 1 90.620 87.498 2.195 o 1 12 6 2 14.278 22.184 4.487 < 1 12 6 3 36.874 36.087 .754 o 1 12 6 4 25.627 27.681 3.224 o 1 12 6 5 88.619 84.240 1.965 o 1 12 6 6 13.074 11.813 1.317 o 1 12 6 7 16.347 13.902 1.239 o 1 12 6 8 3.255 1.794 2.177 < 1 12 6 9 35.858 34.455 .914 o 1 12 6 10 8.019 11.569 3.397 < 1 12 7 0 84.149 82.877 1.157 o 1 12 7 1 20.078 23.374 1.809 o 1 12 7 2 29.407 29.927 .813 o 1 12 7 3 17.735 24.510 4.666 < 1 12 7 4 54.315 53.663 .808 o 1 12 7 5 18.282 18.663 1.364 o 1 12 7 6 51.164 48.904 .802 o 1 12 7 7 6.410 6.920 2.721 < 1 12 7 8 14.331 12.372 1.407 o 1 12 7 9 9.068 12.152 3.350 < 1 12 7 10 29.117 31.253 1.145 o 1 12 8 0 15.963 18.569 1.590 o 1 12 8 1 82.857 78.228 3.230 o 1 12 8 2 9.922 7.585 1.481 < 1 12 8 3 22.373 21.926 .966 o 1 12 8 4 17.385 21.324 2.322 o 1 12 8 5 71.376 71.736 1.292 o 1 12 8 6 13.891 14.370 1.430 o 1 12 8 7 14.824 11.505 1.411 o 1 12 8 8 3.150 5.804 2.140 < 1 12 8 9 31.641 31.262 1.026 o 1 12 8 10 9.969 9.469 2.602 < 1 12 9 0 66.577 65.738 1.125 o 1 12 9 1 11.581 16.235 3.600 < 1 12 9 2 32.206 35.452 6.914 < 1 12 9 3 7.930 11.431 2.470 < 1 12 9 4 54.353 50.947 2.011 o 1 12 9 5 18.489 18.854 1.150 o 1 12 9 6 42.181 39.644 .853 o 1 12 9 7 6.537 .122 2.827 < 1 12 9 8 5.334 10.072 2.932 < 1 12 9 9 5.595 8.683 2.977 < 1 12 9 10 25.828 25.883 1.219 o 1 12 10 0 29.671 31.224 1.235 o 1 12 10 1 67.775 64.037 2.044 o 1 12 10 2 3.176 2.827 2.370 < 1 12 10 3 26.512 25.462 .935 o 1 12 10 4 3.064 6.316 2.151 < 1 12 10 5 58.231 57.241 .828 o 1 12 10 6 15.118 15.722 1.583 o 1 12 10 7 9.889 9.240 2.576 < 1 12 10 8 3.141 7.576 2.162 < 1 12 10 9 27.210 25.527 1.089 o 1 12 11 0 65.772 64.582 1.198 o 1 12 11 1 9.647 15.919 2.518 < 1 12 11 2 17.256 17.714 1.369 o 1 12 11 3 3.981 1.818 2.347 < 1 12 11 4 42.722 43.225 .848 o 1 12 11 5 15.582 17.134 1.423 o 1 12 11 6 39.157 34.928 1.739 o 1 12 11 7 4.712 2.384 2.678 < 1 12 11 8 8.335 8.134 3.987 < 1 12 11 9 6.557 4.786 3.129 < 1 12 12 0 6.288 16.659 3.391 < 1 12 12 1 53.548 49.597 .824 o 1 12 12 2 6.267 8.705 3.343 < 1 12 12 3 24.469 23.155 .969 o 1 12 12 4 7.553 11.430 4.154 < 1 12 12 5 50.527 46.215 1.884 o 1 12 12 6 4.914 6.724 2.697 < 1 12 12 7 9.143 7.412 2.825 < 1 12 12 8 6.296 1.856 3.011 < 1 12 12 9 17.378 18.515 1.557 o 1 12 13 0 54.951 53.537 1.200 o 1 12 13 1 12.684 16.473 1.798 o 1 12 13 2 9.821 10.222 2.551 < 1 12 13 3 5.268 4.421 2.807 < 1 12 13 4 35.509 32.118 1.263 o 1 12 13 5 5.482 10.576 3.283 < 1 12 13 6 28.317 26.855 1.064 o 1 12 13 7 5.271 2.353 3.143 < 1 12 13 8 3.420 5.777 2.361 < 1 12 14 0 3.981 7.457 2.697 < 1 12 14 1 37.246 36.876 1.582 o 1 12 14 2 11.716 11.136 1.717 < 1 12 14 3 17.689 14.448 1.278 o 1 12 14 4 11.715 12.150 6.452 < 1 12 14 5 38.495 34.719 1.126 o 1 12 14 6 5.291 5.119 3.126 < 1 12 14 7 9.119 5.853 2.820 < 1 12 15 0 34.196 31.734 1.349 o 1 12 15 1 10.569 10.875 2.264 < 1 12 15 2 17.240 13.696 1.418 o 1 12 15 3 6.975 5.186 4.171 < 1 12 15 4 26.973 25.890 1.162 o 1 12 15 5 8.475 7.758 3.110 < 1 12 15 6 19.272 18.156 1.946 o 1 12 15 7 5.352 3.683 2.958 < 1 12 16 0 4.223 10.800 2.882 < 1 12 16 1 28.385 26.510 2.696 o 1 12 16 2 4.763 .409 3.276 < 1 12 16 3 10.379 9.004 2.712 < 1 12 16 4 3.517 4.925 2.386 < 1 12 16 5 25.466 24.480 1.260 o 1 12 16 6 7.707 7.971 3.266 < 1 12 17 0 27.016 23.256 1.581 o 1 12 17 1 3.912 4.811 2.525 < 1 12 17 2 8.923 10.554 4.747 < 1 12 17 3 3.922 2.613 2.519 < 1 12 17 4 18.221 17.499 1.591 o 1 12 17 5 8.571 8.457 4.118 < 1 12 18 0 13.354 6.740 2.864 < 1 12 18 1 21.852 19.192 1.352 o 1 12 18 2 5.038 .510 3.354 < 1 12 18 3 6.850 5.164 3.286 < 1 12 18 4 6.300 5.010 3.337 < 1 12 19 0 25.814 21.146 1.917 o 1 12 19 1 4.302 4.797 2.764 < 1 13 0 1 35.331 37.507 1.587 o 1 13 0 2 112.915 114.648 .965 o 1 13 0 3 31.254 32.512 1.415 o 1 13 0 4 46.452 43.428 1.991 o 1 13 0 5 7.382 2.668 2.317 < 1 13 0 6 49.958 50.022 2.961 o 1 13 0 7 19.662 20.945 1.657 o 1 13 0 8 53.510 54.210 .855 o 1 13 0 9 5.956 5.882 3.249 < 1 13 0 10 4.677 5.010 2.619 < 1 13 0 11 3.421 3.441 2.282 < 1 13 1 1 43.286 43.416 1.684 o 1 13 1 2 27.530 24.885 .749 o 1 13 1 3 90.516 90.569 5.040 o 1 13 1 4 23.519 23.661 1.040 o 1 13 1 5 3.251 .909 2.126 < 1 13 1 6 13.856 14.103 1.266 o 1 13 1 7 51.164 52.151 1.731 o 1 13 1 8 16.982 17.081 1.228 o 1 13 1 9 26.530 24.791 1.018 o 1 13 1 10 5.020 3.661 3.020 < 1 13 1 11 12.700 14.362 3.308 < 1 13 2 1 20.239 21.006 .967 o 1 13 2 2 88.692 102.632 1.097 o 1 13 2 3 37.795 39.228 3.316 o 1 13 2 4 47.328 48.148 .751 o 1 13 2 5 5.271 8.430 2.963 < 1 13 2 6 47.793 48.845 .773 o 1 13 2 7 13.651 16.325 1.408 o 1 13 2 8 45.163 47.341 1.629 o 1 13 2 9 6.062 7.092 2.899 < 1 13 2 10 4.951 2.655 2.669 < 1 13 2 11 5.061 4.364 2.777 < 1 13 3 1 71.417 71.602 5.334 o 1 13 3 2 26.451 26.468 .769 o 1 13 3 3 56.367 59.216 6.069 o 1 13 3 4 18.025 16.635 1.836 o 1 13 3 5 15.877 15.043 2.012 o 1 13 3 6 4.912 6.238 2.609 < 1 13 3 7 49.559 51.252 2.023 o 1 13 3 8 15.207 17.642 1.320 o 1 13 3 9 23.347 22.380 2.152 o 1 13 3 10 7.578 1.458 2.817 < 1 13 3 11 9.518 12.970 2.955 < 1 13 4 1 17.741 18.015 1.328 o 1 13 4 2 83.257 93.581 3.552 o 1 13 4 3 34.839 35.856 1.354 o 1 13 4 4 44.886 48.384 5.256 o 1 13 4 5 3.983 4.998 2.629 < 1 13 4 6 40.099 41.964 .787 o 1 13 4 7 16.622 15.066 1.113 o 1 13 4 8 37.009 40.352 3.317 o 1 13 4 9 6.915 6.823 2.906 < 1 13 4 10 5.219 1.221 3.133 < 1 13 5 1 51.969 51.435 4.112 o 1 13 5 2 22.461 21.232 .875 o 1 13 5 3 64.049 67.845 7.166 o 1 13 5 4 20.324 19.753 .932 o 1 13 5 5 9.484 6.304 2.065 < 1 13 5 6 5.667 5.756 2.714 < 1 13 5 7 42.134 43.629 2.801 o 1 13 5 8 13.470 14.737 1.443 o 1 13 5 9 24.122 23.669 1.075 o 1 13 5 10 5.302 1.780 2.848 < 1 13 6 1 25.142 23.257 .813 o 1 13 6 2 74.350 89.890 19.411 < 1 13 6 3 20.373 18.681 1.133 o 1 13 6 4 35.822 43.787 2.654 o 1 13 6 5 2.255 4.597 1.613 < 1 13 6 6 31.698 34.518 2.351 o 1 13 6 7 19.123 17.532 1.114 o 1 13 6 8 37.757 41.099 2.786 o 1 13 6 9 7.884 5.644 2.889 < 1 13 6 10 4.404 3.113 2.456 < 1 13 7 1 22.689 25.778 1.527 o 1 13 7 2 14.376 13.442 1.242 o 1 13 7 3 55.154 72.892 17.117 < 1 13 7 4 18.980 20.781 1.178 o 1 13 7 5 3.502 2.695 2.421 < 1 13 7 6 8.153 9.601 2.531 < 1 13 7 7 37.878 38.601 3.812 o 1 13 7 8 4.255 12.968 2.625 < 1 13 7 9 22.383 22.605 1.175 o 1 13 7 10 3.001 2.315 2.132 < 1 13 8 1 3.730 10.523 2.344 < 1 13 8 2 63.413 72.446 7.331 o 1 13 8 3 22.031 20.021 1.083 o 1 13 8 4 31.229 36.340 3.605 o 1 13 8 5 4.397 2.518 2.669 < 1 13 8 6 29.991 31.406 .977 o 1 13 8 7 9.736 13.423 4.666 < 1 13 8 8 32.086 37.503 2.390 o 1 13 8 9 4.361 6.260 2.595 < 1 13 8 10 5.082 2.728 2.830 < 1 13 9 1 32.734 36.175 2.139 o 1 13 9 2 18.864 19.421 1.147 o 1 13 9 3 42.414 50.564 5.761 o 1 13 9 4 13.552 10.555 1.478 o 1 13 9 5 4.467 5.547 2.520 < 1 13 9 6 3.719 7.311 2.401 < 1 13 9 7 34.869 39.364 9.092 < 1 13 9 8 14.812 13.138 1.512 o 1 13 9 9 16.635 16.974 1.528 o 1 13 10 1 9.346 11.372 2.425 < 1 13 10 2 51.391 58.358 3.906 o 1 13 10 3 22.667 22.923 1.726 o 1 13 10 4 30.912 33.959 2.071 o 1 13 10 5 2.546 4.889 1.844 < 1 13 10 6 32.613 31.747 .977 o 1 13 10 7 10.098 11.003 2.631 < 1 13 10 8 25.670 28.374 1.972 o 1 13 10 9 5.523 4.930 2.928 < 1 13 11 1 28.429 37.901 7.425 < 1 13 11 2 22.768 19.776 .963 o 1 13 11 3 35.931 43.914 3.400 o 1 13 11 4 4.197 6.012 2.512 < 1 13 11 5 6.817 3.476 2.934 < 1 13 11 6 4.351 5.056 2.571 < 1 13 11 7 26.285 31.626 8.154 < 1 13 11 8 5.269 10.001 2.920 < 1 13 11 9 7.011 13.700 3.400 < 1 13 12 1 18.266 18.512 1.420 o 1 13 12 2 35.718 52.782 13.159 < 1 13 12 3 12.424 12.166 2.648 < 1 13 12 4 17.326 25.489 6.392 < 1 13 12 5 4.685 1.911 2.605 < 1 13 12 6 21.022 23.741 2.078 o 1 13 12 7 8.395 10.720 3.102 < 1 13 12 8 17.244 22.590 2.245 o 1 13 13 1 16.723 21.910 4.347 < 1 13 13 2 12.869 12.680 3.348 < 1 13 13 3 31.732 40.557 8.284 < 1 13 13 4 7.305 8.213 3.513 < 1 13 13 5 3.836 3.043 2.780 < 1 13 13 6 5.510 5.328 2.931 < 1 13 13 7 19.211 20.331 1.382 o 1 13 13 8 7.197 5.867 3.813 < 1 13 14 1 7.206 10.844 3.052 < 1 13 14 2 30.920 39.394 2.516 o 1 13 14 3 8.120 11.129 2.991 < 1 13 14 4 12.719 16.590 1.836 < 1 13 14 5 3.555 1.068 2.386 < 1 13 14 6 13.749 14.952 2.938 < 1 13 14 7 5.587 7.142 2.970 < 1 13 15 1 12.218 16.151 1.776 < 1 13 15 2 4.752 9.716 3.086 < 1 13 15 3 24.944 28.387 2.390 o 1 13 15 4 4.525 7.963 2.697 < 1 13 15 5 4.549 .269 3.055 < 1 13 15 6 3.022 4.318 2.160 < 1 13 16 1 3.624 2.809 2.396 < 1 13 16 2 23.500 26.441 1.239 o 1 13 16 3 5.383 11.927 3.505 < 1 13 16 4 12.321 13.983 1.817 < 1 13 16 5 5.065 1.211 2.826 < 1 13 17 1 14.700 15.345 1.587 o 1 13 17 2 10.151 7.181 3.737 < 1 13 17 3 13.118 19.131 6.296 < 1 13 17 4 3.669 4.194 2.435 < 1 13 18 1 7.563 4.240 4.028 < 1 13 18 2 11.924 18.146 5.051 < 1 13 18 3 6.370 5.151 3.377 < 1 14 0 0 83.670 87.722 .815 o 1 14 0 1 59.419 63.673 2.277 o 1 14 0 2 42.487 44.640 .765 o 1 14 0 3 15.024 15.494 2.059 o 1 14 0 4 70.562 71.740 3.362 o 1 14 0 5 38.251 41.814 3.207 o 1 14 0 6 34.503 36.621 2.485 o 1 14 0 7 5.779 11.592 2.773 < 1 14 0 8 14.746 12.710 1.403 o 1 14 0 9 26.091 23.820 1.006 o 1 14 0 10 24.759 25.209 1.126 o 1 14 1 0 55.670 56.431 1.413 o 1 14 1 1 71.131 66.067 2.219 o 1 14 1 2 26.939 28.566 1.070 o 1 14 1 3 20.342 19.750 .942 o 1 14 1 4 25.973 27.004 .827 o 1 14 1 5 62.637 63.828 1.420 o 1 14 1 6 27.385 28.982 2.064 o 1 14 1 7 19.677 19.765 1.456 o 1 14 1 8 5.134 5.524 2.701 < 1 14 1 9 24.327 26.138 1.087 o 1 14 1 10 17.011 16.892 1.995 o 1 14 2 0 93.843 94.862 2.892 o 1 14 2 1 56.455 54.150 .779 o 1 14 2 2 22.036 26.536 .963 o 1 14 2 3 17.793 17.764 1.031 o 1 14 2 4 59.108 61.456 .760 o 1 14 2 5 47.431 46.675 1.565 o 1 14 2 6 38.479 40.678 .798 o 1 14 2 7 5.070 7.897 2.762 < 1 14 2 8 14.820 14.644 1.400 o 1 14 2 9 18.219 21.048 1.310 o 1 14 2 10 24.678 24.628 1.094 o 1 14 3 0 58.149 57.963 1.025 o 1 14 3 1 59.907 59.468 1.290 o 1 14 3 2 3.769 2.882 2.395 < 1 14 3 3 18.103 17.759 .976 o 1 14 3 4 20.084 22.306 1.004 o 1 14 3 5 59.759 60.468 2.704 o 1 14 3 6 36.099 32.985 .804 o 1 14 3 7 16.320 14.046 1.178 o 1 14 3 8 4.576 7.885 2.511 < 1 14 3 9 20.727 23.537 2.369 o 1 14 3 10 15.254 14.859 1.422 o 1 14 4 0 95.470 95.880 1.255 o 1 14 4 1 41.172 40.701 1.574 o 1 14 4 2 3.888 9.142 2.329 < 1 14 4 3 25.960 25.284 2.626 o 1 14 4 4 49.454 52.233 4.652 o 1 14 4 5 50.621 48.567 .775 o 1 14 4 6 40.450 41.282 1.171 o 1 14 4 7 3.326 5.446 2.204 < 1 14 4 8 16.055 14.408 1.866 o 1 14 4 9 19.544 18.643 1.272 o 1 14 4 10 21.744 24.626 4.646 < 1 14 5 0 33.880 34.257 1.070 o 1 14 5 1 54.276 56.401 3.072 o 1 14 5 2 3.664 1.390 2.466 < 1 14 5 3 16.958 18.028 2.411 o 1 14 5 4 34.838 34.373 .796 o 1 14 5 5 51.701 55.024 5.216 o 1 14 5 6 26.087 23.556 1.181 o 1 14 5 7 12.527 12.430 1.512 o 1 14 5 8 5.984 4.759 2.839 < 1 14 5 9 22.442 23.132 2.935 o 1 14 5 10 14.948 14.719 4.636 < 1 14 6 0 58.747 62.791 1.080 o 1 14 6 1 41.219 39.352 1.265 o 1 14 6 2 23.888 26.856 3.310 o 1 14 6 3 29.516 26.440 1.339 o 1 14 6 4 47.930 55.637 3.822 o 1 14 6 5 39.716 39.227 .819 o 1 14 6 6 30.175 31.909 1.606 o 1 14 6 7 5.966 6.639 3.164 < 1 14 6 8 7.144 10.661 3.800 < 1 14 6 9 18.722 19.176 1.353 o 1 14 6 10 24.031 23.459 1.175 o 1 14 7 0 30.905 31.617 1.154 o 1 14 7 1 51.850 54.937 4.409 o 1 14 7 2 16.533 15.440 1.299 o 1 14 7 3 8.282 13.982 2.580 < 1 14 7 4 31.577 30.240 .868 o 1 14 7 5 41.807 46.386 3.433 o 1 14 7 6 19.629 17.911 1.124 o 1 14 7 7 13.704 13.878 1.428 o 1 14 7 8 4.543 4.666 3.001 < 1 14 7 9 18.809 22.573 4.910 < 1 14 7 10 15.195 13.921 1.564 o 1 14 8 0 53.642 57.595 1.114 o 1 14 8 1 39.256 39.291 1.449 o 1 14 8 2 18.960 24.413 4.961 < 1 14 8 3 13.739 12.823 1.329 o 1 14 8 4 39.621 45.130 2.685 o 1 14 8 5 32.180 29.418 .851 o 1 14 8 6 29.350 30.928 3.262 o 1 14 8 7 3.143 4.046 2.150 < 1 14 8 8 8.595 10.204 3.169 < 1 14 8 9 15.527 16.498 1.556 o 1 14 9 0 41.560 41.054 1.137 o 1 14 9 1 39.185 44.459 2.727 o 1 14 9 2 7.759 11.014 3.685 < 1 14 9 3 13.023 11.877 1.381 o 1 14 9 4 14.533 12.046 1.300 o 1 14 9 5 41.227 41.181 4.581 o 1 14 9 6 21.512 21.134 1.150 o 1 14 9 7 11.593 11.044 1.733 < 1 14 9 8 4.332 6.344 2.577 < 1 14 9 9 16.705 18.164 2.034 o 1 14 10 0 57.572 59.282 1.175 o 1 14 10 1 31.499 31.023 .925 o 1 14 10 2 6.742 10.440 2.833 < 1 14 10 3 3.932 4.931 2.370 < 1 14 10 4 31.680 34.661 2.597 o 1 14 10 5 30.494 28.365 .977 o 1 14 10 6 31.141 30.293 .953 o 1 14 10 7 7.180 1.702 3.007 < 1 14 10 8 4.050 9.996 2.654 < 1 14 10 9 8.693 11.471 3.205 < 1 14 11 0 32.092 30.134 1.279 o 1 14 11 1 30.464 34.787 3.332 o 1 14 11 2 9.294 9.238 2.419 < 1 14 11 3 11.850 13.852 1.807 o 1 14 11 4 18.435 15.664 1.866 o 1 14 11 5 32.121 35.934 1.030 o 1 14 11 6 14.817 16.271 1.619 o 1 14 11 7 7.598 7.140 3.199 < 1 14 11 8 4.383 2.598 2.584 < 1 14 12 0 41.755 47.881 1.290 o 1 14 12 1 24.321 23.547 1.041 o 1 14 12 2 3.144 8.293 2.363 < 1 14 12 3 6.956 9.086 3.824 < 1 14 12 4 22.598 30.318 2.519 o 1 14 12 5 25.751 24.208 1.322 o 1 14 12 6 17.961 21.146 1.439 o 1 14 12 7 3.885 4.598 2.489 < 1 14 12 8 5.189 6.273 2.849 < 1 14 13 0 11.757 15.081 3.064 < 1 14 13 1 28.776 27.457 2.227 o 1 14 13 2 13.717 10.773 1.510 o 1 14 13 3 7.746 11.162 4.108 < 1 14 13 4 20.692 19.667 1.858 o 1 14 13 5 27.911 25.911 2.050 o 1 14 13 6 13.569 11.400 1.705 o 1 14 13 7 4.540 6.555 2.709 < 1 14 14 0 26.508 28.328 1.592 o 1 14 14 1 19.933 17.615 2.289 o 1 14 14 2 10.534 11.998 4.460 < 1 14 14 3 8.302 9.710 3.072 < 1 14 14 4 20.373 24.370 2.670 o 1 14 14 5 18.191 16.688 2.297 o 1 14 14 6 12.726 13.972 3.314 < 1 14 15 0 19.634 17.415 1.791 o 1 14 15 1 21.251 21.214 1.146 o 1 14 15 2 5.560 3.142 3.036 < 1 14 15 3 6.460 6.835 3.098 < 1 14 15 4 12.193 11.996 3.170 < 1 14 15 5 16.647 19.041 1.564 o 1 14 15 6 9.123 11.141 3.366 < 1 14 16 0 24.445 23.891 1.671 o 1 14 16 1 10.908 12.842 4.018 < 1 14 16 2 3.618 7.471 2.478 < 1 14 16 3 2.989 6.037 2.045 < 1 14 16 4 10.301 14.795 2.695 < 1 14 16 5 14.418 13.539 1.977 o 1 14 17 0 16.947 15.371 2.248 o 1 14 17 1 9.116 15.823 4.395 < 1 14 17 2 5.557 2.300 3.555 < 1 14 17 3 7.516 3.106 3.597 < 1 14 18 0 19.177 18.535 2.129 o 1 14 18 1 11.067 9.886 2.886 < 1 15 0 1 40.741 42.303 .728 o 1 15 0 2 5.291 2.834 2.614 < 1 15 0 3 83.093 91.831 5.180 o 1 15 0 4 6.929 1.364 2.559 < 1 15 0 5 14.003 10.434 2.004 o 1 15 0 6 3.800 6.480 2.328 < 1 15 0 7 45.091 44.833 2.635 o 1 15 0 8 3.606 1.980 2.362 < 1 15 0 9 18.737 19.990 1.284 o 1 15 0 10 7.698 1.115 2.863 < 1 15 1 1 6.765 3.306 2.519 < 1 15 1 2 75.831 74.303 .844 o 1 15 1 3 13.903 13.923 1.221 o 1 15 1 4 43.824 43.567 1.044 o 1 15 1 5 5.169 5.349 2.817 < 1 15 1 6 26.728 29.805 1.360 o 1 15 1 7 3.002 2.407 2.072 < 1 15 1 8 41.576 41.474 .943 o 1 15 1 9 2.660 .668 1.860 < 1 15 1 10 2.711 .197 1.972 < 1 15 2 1 57.224 56.003 1.717 o 1 15 2 2 3.494 4.936 2.165 < 1 15 2 3 75.043 76.129 5.235 o 1 15 2 4 2.882 1.626 1.959 < 1 15 2 5 3.181 3.444 2.148 < 1 15 2 6 4.272 3.614 2.399 < 1 15 2 7 50.004 48.544 1.308 o 1 15 2 8 4.237 2.353 2.569 < 1 15 2 9 18.083 17.938 1.274 o 1 15 2 10 3.167 2.881 2.189 < 1 15 3 1 10.253 9.088 1.518 < 1 15 3 2 71.191 69.242 1.374 o 1 15 3 3 4.671 4.501 2.500 < 1 15 3 4 45.442 44.785 .900 o 1 15 3 5 4.869 .652 3.290 < 1 15 3 6 33.561 33.665 1.211 o 1 15 3 7 5.752 5.330 3.111 < 1 15 3 8 38.099 36.830 .886 o 1 15 3 9 3.448 .525 2.291 < 1 15 3 10 4.993 2.087 2.791 < 1 15 4 1 63.346 58.959 .768 o 1 15 4 2 4.791 8.793 2.721 < 1 15 4 3 70.284 66.768 2.927 o 1 15 4 4 3.289 1.258 2.155 < 1 15 4 5 6.421 1.321 2.731 < 1 15 4 6 5.475 2.922 2.669 < 1 15 4 7 47.094 46.762 2.961 o 1 15 4 8 3.980 1.552 2.420 < 1 15 4 9 18.984 17.653 2.208 o 1 15 4 10 4.737 5.235 2.640 < 1 15 5 1 7.347 2.464 2.319 < 1 15 5 2 72.056 69.504 2.427 o 1 15 5 3 3.395 1.518 2.204 < 1 15 5 4 42.847 42.104 .812 o 1 15 5 5 4.237 .426 2.366 < 1 15 5 6 32.292 30.019 .890 o 1 15 5 7 4.526 3.269 2.522 < 1 15 5 8 37.448 35.946 1.682 o 1 15 5 9 4.553 1.677 2.714 < 1 15 5 10 3.280 1.766 2.276 < 1 15 6 1 37.926 36.603 1.538 o 1 15 6 2 9.682 12.023 2.115 < 1 15 6 3 76.948 75.512 3.304 o 1 15 6 4 2.255 2.439 1.632 < 1 15 6 5 7.647 8.616 2.876 < 1 15 6 6 4.579 5.034 2.565 < 1 15 6 7 39.876 38.895 2.535 o 1 15 6 8 2.857 1.142 1.949 < 1 15 6 9 12.971 18.319 6.223 < 1 15 7 1 3.889 5.915 2.356 < 1 15 7 2 64.768 62.536 1.503 o 1 15 7 3 5.646 4.592 2.763 < 1 15 7 4 35.251 33.637 .892 o 1 15 7 5 3.881 3.148 2.372 < 1 15 7 6 23.771 23.084 1.045 o 1 15 7 7 4.279 .619 2.772 < 1 15 7 8 37.671 34.807 1.446 o 1 15 7 9 3.503 1.296 2.347 < 1 15 8 1 37.477 36.693 1.399 o 1 15 8 2 7.054 6.020 2.650 < 1 15 8 3 59.403 58.984 2.677 o 1 15 8 4 2.020 .836 1.521 < 1 15 8 5 5.015 1.685 2.701 < 1 15 8 6 11.133 5.536 1.626 < 1 15 8 7 40.063 37.960 .931 o 1 15 8 8 4.290 2.310 2.569 < 1 15 8 9 14.059 14.522 1.629 o 1 15 9 1 2.624 3.693 1.901 < 1 15 9 2 51.469 50.015 1.131 o 1 15 9 3 10.214 3.896 1.554 < 1 15 9 4 32.018 29.510 1.381 o 1 15 9 5 3.346 .188 2.235 < 1 15 9 6 23.916 22.792 1.116 o 1 15 9 7 3.679 2.833 2.399 < 1 15 9 8 28.955 27.854 1.069 o 1 15 10 1 42.220 39.976 .845 o 1 15 10 2 2.803 1.274 1.966 < 1 15 10 3 45.719 43.707 2.074 o 1 15 10 4 3.153 1.296 2.109 < 1 15 10 5 3.235 2.440 2.199 < 1 15 10 6 2.288 2.831 1.702 < 1 15 10 7 32.601 33.458 1.199 o 1 15 10 8 2.841 .277 2.031 < 1 15 11 1 3.657 8.433 2.414 < 1 15 11 2 47.906 42.690 1.803 o 1 15 11 3 3.631 .919 2.334 < 1 15 11 4 26.759 25.531 1.034 o 1 15 11 5 3.678 2.081 2.392 < 1 15 11 6 20.082 19.995 1.393 o 1 15 11 7 3.284 2.634 2.273 < 1 15 11 8 24.616 21.752 1.958 o 1 15 12 1 28.533 26.101 2.049 o 1 15 12 2 2.529 .415 1.832 < 1 15 12 3 41.621 40.838 1.882 o 1 15 12 4 5.303 .501 2.843 < 1 15 12 5 5.182 3.332 2.802 < 1 15 12 6 5.370 1.188 2.884 < 1 15 12 7 22.051 21.852 1.368 o 1 15 13 1 2.610 3.006 1.846 < 1 15 13 2 36.728 34.149 1.734 o 1 15 13 3 3.661 2.330 2.471 < 1 15 13 4 15.539 17.475 1.601 o 1 15 13 5 7.271 1.061 3.111 < 1 15 13 6 12.830 12.328 1.911 < 1 15 13 7 3.605 .189 2.419 < 1 15 14 1 19.163 17.280 1.195 o 1 15 14 2 3.710 .011 2.427 < 1 15 14 3 33.510 31.350 2.164 o 1 15 14 4 3.797 .343 2.452 < 1 15 14 5 12.508 2.053 1.849 o 1 15 14 6 3.617 .953 2.447 < 1 15 15 1 3.204 .952 2.221 < 1 15 15 2 28.576 26.546 1.104 o 1 15 15 3 3.346 2.261 2.263 < 1 15 15 4 13.159 13.433 1.770 o 1 15 15 5 3.607 1.115 2.446 < 1 15 16 1 19.376 18.024 1.413 o 1 15 16 2 7.368 .758 3.576 < 1 15 16 3 19.644 19.785 1.446 o 1 15 16 4 6.541 .262 3.636 < 1 15 17 1 4.125 .305 2.784 < 1 15 17 2 21.791 18.603 3.238 o 1 16 0 0 64.585 66.957 .871 o 1 16 0 1 32.012 33.184 .840 o 1 16 0 2 17.871 18.498 .996 o 1 16 0 3 12.185 13.546 1.430 < 1 16 0 4 43.040 43.919 .780 o 1 16 0 5 31.089 31.824 1.505 o 1 16 0 6 32.479 32.482 1.635 o 1 16 0 7 13.392 11.082 1.862 o 1 16 0 8 12.678 12.311 1.561 o 1 16 0 9 17.023 15.095 1.342 o 1 16 0 10 22.261 21.019 1.201 o 1 16 1 0 44.649 41.727 1.080 o 1 16 1 1 43.133 41.380 1.951 o 1 16 1 2 20.578 22.873 1.001 o 1 16 1 3 14.065 13.391 1.240 o 1 16 1 4 44.996 45.533 .796 o 1 16 1 5 43.473 46.076 1.841 o 1 16 1 6 26.192 25.668 .927 o 1 16 1 7 13.535 12.729 1.525 o 1 16 1 8 9.325 8.409 2.440 < 1 16 1 9 19.805 18.745 1.902 o 1 16 1 10 19.267 17.320 2.926 o 1 16 2 0 60.403 63.180 2.252 o 1 16 2 1 34.845 34.696 1.019 o 1 16 2 2 15.326 17.564 1.156 o 1 16 2 3 6.507 10.064 2.735 < 1 16 2 4 43.827 45.115 1.837 o 1 16 2 5 33.546 33.730 .863 o 1 16 2 6 28.535 31.269 .960 o 1 16 2 7 4.190 8.279 2.519 < 1 16 2 8 10.124 11.826 3.739 < 1 16 2 9 10.712 12.531 2.789 < 1 16 3 0 65.277 65.228 1.121 o 1 16 3 1 40.383 40.809 1.216 o 1 16 3 2 6.481 9.520 2.703 < 1 16 3 3 12.505 14.954 4.583 < 1 16 3 4 30.724 31.013 1.441 o 1 16 3 5 44.914 43.223 .974 o 1 16 3 6 29.837 29.603 1.507 o 1 16 3 7 12.052 11.935 1.605 o 1 16 3 8 13.043 10.339 1.495 < 1 16 3 9 19.784 18.481 1.137 o 1 16 4 0 55.878 55.657 1.085 o 1 16 4 1 36.167 34.812 .897 o 1 16 4 2 16.041 17.629 1.276 o 1 16 4 3 4.716 7.728 2.798 < 1 16 4 4 46.019 46.670 6.183 o 1 16 4 5 32.944 31.515 1.315 o 1 16 4 6 23.031 28.360 1.102 o 1 16 4 7 5.597 6.872 2.969 < 1 16 4 8 8.812 10.975 2.741 < 1 16 4 9 5.579 10.340 3.017 < 1 16 5 0 52.107 52.684 1.126 o 1 16 5 1 43.126 42.976 1.646 o 1 16 5 2 16.190 16.171 1.223 o 1 16 5 3 11.375 14.899 1.658 < 1 16 5 4 33.436 34.449 .879 o 1 16 5 5 39.672 39.466 3.107 o 1 16 5 6 20.066 21.207 1.395 o 1 16 5 7 7.601 10.074 3.662 < 1 16 5 8 6.044 7.053 3.219 < 1 16 5 9 18.627 17.230 2.057 o 1 16 6 0 56.508 57.892 1.160 o 1 16 6 1 32.461 29.993 1.066 o 1 16 6 2 13.457 15.706 4.953 < 1 16 6 3 6.048 9.608 2.901 < 1 16 6 4 37.887 39.546 .880 o 1 16 6 5 25.524 25.449 1.161 o 1 16 6 6 24.554 26.321 1.400 o 1 16 6 7 9.385 10.138 3.972 < 1 16 6 8 9.329 10.651 4.972 < 1 16 6 9 12.260 11.368 1.775 < 1 16 7 0 35.273 34.024 1.195 o 1 16 7 1 41.084 40.278 2.661 o 1 16 7 2 19.344 18.101 1.033 o 1 16 7 3 5.872 9.095 2.830 < 1 16 7 4 35.643 35.254 .946 o 1 16 7 5 32.743 31.950 2.467 o 1 16 7 6 19.385 17.329 1.146 o 1 16 7 7 2.836 8.103 2.109 < 1 16 7 8 4.500 5.880 2.677 < 1 16 7 9 12.121 14.616 3.162 < 1 16 8 0 46.097 54.328 1.173 o 1 16 8 1 23.388 23.619 1.746 o 1 16 8 2 11.817 13.534 1.551 < 1 16 8 3 12.083 10.003 1.470 o 1 16 8 4 26.537 28.922 2.324 o 1 16 8 5 23.970 23.195 1.912 o 1 16 8 6 23.645 24.921 1.393 o 1 16 8 7 12.437 9.929 1.667 o 1 16 8 8 4.436 9.168 2.890 < 1 16 9 0 39.300 37.511 1.171 o 1 16 9 1 31.475 31.887 2.882 o 1 16 9 2 5.206 5.021 2.746 < 1 16 9 3 4.611 6.633 2.551 < 1 16 9 4 25.361 22.605 1.729 o 1 16 9 5 30.030 28.000 2.188 o 1 16 9 6 21.467 21.886 1.277 o 1 16 9 7 3.593 7.917 2.426 < 1 16 9 8 4.579 8.076 2.746 < 1 16 10 0 35.294 39.086 1.260 o 1 16 10 1 20.258 20.227 1.151 o 1 16 10 2 6.476 10.544 3.566 < 1 16 10 3 4.240 5.886 2.508 < 1 16 10 4 24.883 27.949 1.940 o 1 16 10 5 26.458 23.624 1.018 o 1 16 10 6 19.613 20.460 1.311 o 1 16 10 7 4.402 4.589 2.986 < 1 16 10 8 7.251 6.098 3.853 < 1 16 11 0 34.077 33.979 1.344 o 1 16 11 1 20.739 22.464 2.491 o 1 16 11 2 5.970 4.739 2.845 < 1 16 11 3 7.261 8.765 3.054 < 1 16 11 4 18.620 18.344 1.373 o 1 16 11 5 24.520 25.728 1.660 o 1 16 11 6 16.337 15.467 1.697 o 1 16 11 7 10.229 8.901 2.679 < 1 16 12 0 27.108 26.487 1.396 o 1 16 12 1 17.063 18.671 4.445 < 1 16 12 2 6.203 8.749 3.312 < 1 16 12 3 4.708 4.675 2.786 < 1 16 12 4 17.926 24.854 5.576 < 1 16 12 5 18.423 16.592 1.436 o 1 16 12 6 16.672 16.850 2.535 o 1 16 12 7 4.602 3.992 2.732 < 1 16 13 0 12.880 20.279 3.360 < 1 16 13 1 19.148 18.167 1.265 o 1 16 13 2 10.102 10.137 2.652 < 1 16 13 3 3.887 8.239 2.521 < 1 16 13 4 15.634 17.408 3.355 < 1 16 13 5 19.659 20.034 2.068 o 1 16 13 6 12.365 8.590 1.877 < 1 16 14 0 22.990 25.771 1.736 o 1 16 14 1 17.038 15.347 1.389 o 1 16 14 2 6.582 4.695 3.596 < 1 16 14 3 7.333 5.553 3.098 < 1 16 14 4 10.709 16.155 2.802 < 1 16 14 5 10.468 11.632 3.846 < 1 16 15 0 17.239 17.418 2.276 o 1 16 15 1 15.159 16.207 1.649 o 1 16 15 2 4.095 4.587 2.785 < 1 16 15 3 4.466 5.631 2.646 < 1 16 15 4 8.023 10.772 3.387 < 1 16 16 0 20.630 21.757 2.041 o 1 16 16 1 8.780 10.884 3.233 < 1 16 16 2 5.702 4.613 3.021 < 1 16 16 3 4.266 3.588 2.737 < 1 17 0 1 22.127 24.691 .961 o 1 17 0 2 50.223 53.075 .761 o 1 17 0 3 13.032 14.887 3.387 < 1 17 0 4 31.968 33.963 2.443 o 1 17 0 5 3.212 .377 2.145 < 1 17 0 6 21.062 21.356 1.755 o 1 17 0 7 15.923 15.818 1.345 o 1 17 0 8 30.153 28.939 .957 o 1 17 0 9 3.269 3.980 2.198 < 1 17 1 1 38.103 36.730 .773 o 1 17 1 2 10.866 13.777 3.973 < 1 17 1 3 60.642 62.861 3.509 o 1 17 1 4 11.862 9.858 1.468 o 1 17 1 5 4.293 1.265 2.386 < 1 17 1 6 10.120 7.276 2.159 < 1 17 1 7 38.091 38.660 1.073 o 1 17 1 8 11.886 8.583 1.592 < 1 17 1 9 11.928 16.371 3.703 < 1 17 2 1 11.272 12.500 1.641 < 1 17 2 2 44.606 54.522 1.874 o 1 17 2 3 22.606 22.682 1.194 o 1 17 2 4 30.804 32.603 .908 o 1 17 2 5 5.199 5.531 3.149 < 1 17 2 6 20.284 23.006 1.208 o 1 17 2 7 9.028 12.191 2.805 < 1 17 2 8 25.893 28.474 2.303 o 1 17 2 9 5.637 3.779 3.612 < 1 17 3 1 41.617 41.405 1.370 o 1 17 3 2 13.601 14.275 1.442 o 1 17 3 3 57.307 61.146 6.034 o 1 17 3 4 4.687 8.799 2.490 < 1 17 3 5 4.921 3.050 2.647 < 1 17 3 6 4.665 3.684 2.523 < 1 17 3 7 36.088 36.956 1.269 o 1 17 3 8 9.076 9.539 3.351 < 1 17 3 9 14.394 14.958 3.752 < 1 17 4 1 6.544 5.871 2.747 < 1 17 4 2 49.753 54.640 3.228 o 1 17 4 3 25.085 28.215 1.026 o 1 17 4 4 28.353 30.480 4.077 o 1 17 4 5 5.549 6.666 3.110 < 1 17 4 6 22.264 23.587 1.050 o 1 17 4 7 9.731 10.753 3.581 < 1 17 4 8 26.948 27.901 1.796 o 1 17 4 9 4.833 1.549 2.640 < 1 17 5 1 41.034 37.394 1.673 o 1 17 5 2 16.880 15.070 1.191 o 1 17 5 3 57.199 58.629 5.830 o 1 17 5 4 12.034 10.204 1.589 < 1 17 5 5 5.859 6.190 2.853 < 1 17 5 6 4.809 4.281 2.829 < 1 17 5 7 33.713 33.290 3.313 o 1 17 5 8 3.474 7.218 2.364 < 1 17 5 9 7.677 13.844 3.266 < 1 17 6 1 18.400 19.398 2.287 o 1 17 6 2 48.648 50.735 5.475 o 1 17 6 3 14.115 15.949 1.439 o 1 17 6 4 22.578 25.350 1.070 o 1 17 6 5 3.011 .254 2.086 < 1 17 6 6 20.743 20.447 1.175 o 1 17 6 7 14.822 13.185 1.521 o 1 17 6 8 19.990 26.166 5.218 < 1 17 7 1 33.413 32.874 3.695 o 1 17 7 2 8.296 10.901 3.477 < 1 17 7 3 46.511 48.193 6.645 o 1 17 7 4 7.830 8.497 2.894 < 1 17 7 5 4.638 3.317 2.576 < 1 17 7 6 5.435 6.633 2.885 < 1 17 7 7 30.944 30.659 2.715 o 1 17 7 8 3.970 4.995 2.556 < 1 17 8 1 16.048 14.483 1.824 o 1 17 8 2 34.802 41.017 3.056 o 1 17 8 3 9.700 12.527 2.532 < 1 17 8 4 20.415 23.261 1.165 o 1 17 8 5 3.834 4.499 2.497 < 1 17 8 6 18.638 18.501 1.285 o 1 17 8 7 6.659 9.243 3.201 < 1 17 8 8 19.749 22.584 1.430 o 1 17 9 1 30.003 30.551 3.510 o 1 17 9 2 10.306 8.088 2.194 < 1 17 9 3 30.979 38.809 9.609 < 1 17 9 4 4.266 3.049 2.536 < 1 17 9 5 3.500 .686 2.364 < 1 17 9 6 4.864 4.246 2.651 < 1 17 9 7 22.006 27.095 6.836 < 1 17 10 1 5.961 4.506 2.837 < 1 17 10 2 30.972 34.620 4.330 o 1 17 10 3 14.405 14.234 1.616 o 1 17 10 4 18.899 22.201 1.335 o 1 17 10 5 6.600 7.110 3.570 < 1 17 10 6 8.429 15.333 3.585 < 1 17 10 7 3.600 6.321 2.413 < 1 17 11 1 18.256 21.375 1.725 o 1 17 11 2 11.847 7.881 1.668 < 1 17 11 3 25.787 33.610 8.011 < 1 17 11 4 6.060 3.433 3.312 < 1 17 11 5 2.702 .692 1.923 < 1 17 11 6 9.826 1.817 2.558 < 1 17 12 1 9.599 6.382 2.515 < 1 17 12 2 22.655 28.252 2.168 o 1 17 12 3 5.596 9.282 2.979 < 1 17 12 4 12.932 16.255 4.759 < 1 17 12 5 4.140 .314 2.301 < 1 17 12 6 13.253 10.773 1.854 o 1 17 13 1 14.049 15.513 1.687 o 1 17 13 2 6.512 6.080 3.109 < 1 17 13 3 19.811 26.137 8.367 < 1 17 13 4 3.570 6.124 2.388 < 1 17 13 5 3.696 .325 2.405 < 1 17 14 1 9.134 7.996 2.855 < 1 17 14 2 19.961 23.701 2.420 o 1 17 14 3 5.071 5.999 2.773 < 1 17 14 4 7.451 11.680 3.589 < 1 17 15 1 14.268 16.171 3.728 < 1 17 15 2 2.988 5.232 2.144 < 1 17 15 3 15.167 18.152 3.955 < 1 18 0 0 4.198 10.124 2.466 < 1 18 0 1 35.756 35.479 .924 o 1 18 0 2 5.654 9.097 2.728 < 1 18 0 3 11.986 13.561 1.515 o 1 18 0 4 10.878 10.051 1.641 < 1 18 0 5 41.304 40.896 2.123 o 1 18 0 6 7.950 11.816 3.354 < 1 18 0 7 3.705 8.062 2.518 < 1 18 0 8 3.258 .909 2.190 < 1 18 0 9 15.139 16.490 1.783 < 1 18 1 0 57.217 55.424 .802 o 1 18 1 1 18.134 20.582 1.551 o 1 18 1 2 15.328 12.310 1.156 o 1 18 1 3 9.865 6.728 2.126 < 1 18 1 4 41.471 39.982 1.617 o 1 18 1 5 17.184 17.375 1.231 o 1 18 1 6 31.242 31.719 2.092 o 1 18 1 7 4.166 2.614 2.456 < 1 18 1 8 5.012 9.842 2.786 < 1 18 1 9 8.519 9.347 3.145 < 1 18 2 0 14.969 16.843 1.594 o 1 18 2 1 39.822 39.344 .817 o 1 18 2 2 2.817 3.478 1.920 < 1 18 2 3 9.714 12.732 4.096 < 1 18 2 4 4.168 7.457 2.721 < 1 18 2 5 41.825 39.051 .819 o 1 18 2 6 8.756 12.597 2.722 < 1 18 2 7 4.996 9.970 2.767 < 1 18 2 8 3.188 .843 2.149 < 1 18 3 0 51.514 52.088 1.136 o 1 18 3 1 19.348 19.815 2.839 o 1 18 3 2 25.087 24.453 .966 o 1 18 3 3 3.275 8.755 2.212 < 1 18 3 4 45.709 44.331 1.384 o 1 18 3 5 19.129 17.787 1.129 o 1 18 3 6 27.933 26.468 1.020 o 1 18 3 7 3.805 1.578 2.417 < 1 18 3 8 6.242 8.506 2.996 < 1 18 4 0 19.262 19.050 1.555 o 1 18 4 1 44.883 43.499 .800 o 1 18 4 2 2.524 1.226 1.771 < 1 18 4 3 12.229 11.655 3.189 < 1 18 4 4 4.554 7.489 2.517 < 1 18 4 5 37.361 36.602 .866 o 1 18 4 6 11.275 10.150 1.702 < 1 18 4 7 8.056 10.507 4.292 < 1 18 4 8 2.446 .486 1.811 < 1 18 5 0 56.411 55.915 1.187 o 1 18 5 1 17.695 17.853 2.011 o 1 18 5 2 18.471 19.695 2.261 o 1 18 5 3 7.733 10.690 2.869 < 1 18 5 4 36.727 36.243 1.512 o 1 18 5 5 15.010 15.158 1.835 o 1 18 5 6 27.642 25.710 1.166 o 1 18 5 7 5.396 2.130 2.854 < 1 18 5 8 12.665 9.592 1.701 < 1 18 6 0 8.194 10.024 3.437 < 1 18 6 1 40.905 38.777 2.079 o 1 18 6 2 9.258 6.382 2.429 < 1 18 6 3 6.571 11.031 3.509 < 1 18 6 4 5.031 9.501 3.014 < 1 18 6 5 34.258 34.447 2.706 o 1 18 6 6 6.245 7.797 2.994 < 1 18 6 7 7.297 7.693 3.072 < 1 18 6 8 3.186 .865 2.256 < 1 18 7 0 54.378 53.500 1.210 o 1 18 7 1 10.774 15.236 2.312 < 1 18 7 2 3.509 8.666 2.350 < 1 18 7 3 4.823 9.288 2.673 < 1 18 7 4 28.077 28.071 1.417 o 1 18 7 5 14.984 13.625 3.208 < 1 18 7 6 29.497 25.115 1.176 o 1 18 7 7 2.634 2.478 1.843 < 1 18 7 8 4.975 8.774 3.344 < 1 18 8 0 9.939 10.676 3.075 < 1 18 8 1 30.643 30.456 1.933 o 1 18 8 2 3.267 4.073 2.170 < 1 18 8 3 12.847 10.885 1.532 o 1 18 8 4 5.303 4.940 2.804 < 1 18 8 5 31.834 31.981 1.759 o 1 18 8 6 5.404 10.602 3.232 < 1 18 8 7 5.077 6.997 2.783 < 1 18 9 0 38.778 37.275 1.286 o 1 18 9 1 9.675 12.672 2.529 < 1 18 9 2 8.624 9.894 3.647 < 1 18 9 3 4.836 4.132 2.664 < 1 18 9 4 30.237 29.415 1.020 o 1 18 9 5 12.624 13.409 1.774 < 1 18 9 6 23.954 20.304 1.755 o 1 18 9 7 3.996 .605 2.700 < 1 18 10 0 9.401 11.683 3.460 < 1 18 10 1 25.432 24.663 1.175 o 1 18 10 2 4.431 3.706 2.833 < 1 18 10 3 7.192 10.851 3.827 < 1 18 10 4 7.085 3.598 2.966 < 1 18 10 5 27.347 26.238 1.204 o 1 18 10 6 5.679 7.987 3.025 < 1 18 11 0 28.739 26.718 1.407 o 1 18 11 1 5.449 10.739 2.916 < 1 18 11 2 14.380 10.468 1.445 o 1 18 11 3 2.946 2.355 2.109 < 1 18 11 4 24.119 23.723 1.282 o 1 18 11 5 9.189 9.133 2.856 < 1 18 11 6 19.723 17.918 1.375 o 1 18 12 0 5.899 6.754 3.220 < 1 18 12 1 19.575 21.369 5.104 < 1 18 12 2 3.795 5.701 2.549 < 1 18 12 3 6.490 7.577 3.114 < 1 18 12 4 4.887 6.150 2.686 < 1 18 12 5 21.738 20.489 2.542 o 1 18 13 0 27.762 27.602 1.626 o 1 18 13 1 7.533 8.836 3.183 < 1 18 13 2 5.410 5.588 3.461 < 1 18 13 3 3.561 4.516 2.391 < 1 18 13 4 17.853 14.059 1.313 o 1 18 14 0 7.029 6.767 3.723 < 1 18 14 1 17.493 18.419 2.595 o 1 18 14 2 4.914 1.885 3.165 < 1 18 14 3 9.258 5.011 2.869 < 1 18 15 0 19.515 22.492 2.268 o 1 18 15 1 8.641 6.228 3.186 < 1 19 0 1 23.161 24.395 .979 o 1 19 0 2 24.317 25.394 .980 o 1 19 0 3 27.327 30.728 .915 o 1 19 0 4 13.809 14.593 1.464 o 1 19 0 5 6.563 7.204 3.673 < 1 19 0 6 8.387 12.211 4.026 < 1 19 0 7 21.973 23.999 1.188 o 1 19 0 8 13.252 11.833 1.633 o 1 19 1 1 22.934 21.290 .976 o 1 19 1 2 45.208 43.901 1.037 o 1 19 1 3 26.675 27.661 1.564 o 1 19 1 4 22.807 23.675 1.052 o 1 19 1 5 3.152 2.288 2.155 < 1 19 1 6 16.157 20.702 5.029 < 1 19 1 7 16.445 17.394 1.416 o 1 19 1 8 19.342 21.033 1.349 o 1 19 2 1 22.041 21.655 1.053 o 1 19 2 2 22.039 25.021 1.087 o 1 19 2 3 33.703 34.895 2.304 o 1 19 2 4 13.639 13.939 1.491 o 1 19 2 5 2.635 3.177 1.918 < 1 19 2 6 8.936 11.108 2.769 < 1 19 2 7 21.988 22.139 2.771 o 1 19 2 8 13.057 12.702 1.752 < 1 19 3 1 13.820 12.785 1.358 o 1 19 3 2 45.365 45.207 1.104 o 1 19 3 3 29.671 32.016 4.153 o 1 19 3 4 20.696 20.179 1.124 o 1 19 3 5 6.966 4.350 3.869 < 1 19 3 6 19.481 19.479 1.811 o 1 19 3 7 16.953 15.610 1.342 o 1 19 3 8 20.593 21.055 2.452 o 1 19 4 1 20.779 19.223 1.409 o 1 19 4 2 21.850 23.612 1.183 o 1 19 4 3 35.931 35.224 1.062 o 1 19 4 4 10.344 13.650 3.203 < 1 19 4 5 2.755 .318 1.984 < 1 19 4 6 12.654 10.596 1.663 < 1 19 4 7 17.667 20.005 5.473 < 1 19 4 8 7.059 12.857 3.780 < 1 19 5 1 13.268 16.089 2.841 < 1 19 5 2 45.367 44.025 .855 o 1 19 5 3 20.587 23.389 3.147 o 1 19 5 4 15.695 16.532 1.692 o 1 19 5 5 3.313 1.015 2.217 < 1 19 5 6 20.445 18.656 1.173 o 1 19 5 7 16.985 16.184 2.111 o 1 19 6 1 21.015 22.014 1.173 o 1 19 6 2 19.134 19.583 2.657 o 1 19 6 3 27.309 27.466 1.853 o 1 19 6 4 8.826 11.772 2.741 < 1 19 6 5 4.151 2.788 2.721 < 1 19 6 6 5.250 11.525 2.912 < 1 19 6 7 19.767 20.042 2.898 o 1 19 7 1 18.856 17.093 1.228 o 1 19 7 2 38.668 37.070 .920 o 1 19 7 3 15.382 16.867 1.465 o 1 19 7 4 19.595 16.862 1.204 o 1 19 7 5 3.928 1.471 2.536 < 1 19 7 6 18.211 17.809 1.960 o 1 19 7 7 11.312 13.856 3.517 < 1 19 8 1 18.936 18.366 1.254 o 1 19 8 2 16.326 18.205 1.621 o 1 19 8 3 24.981 24.992 3.146 o 1 19 8 4 4.120 8.380 2.806 < 1 19 8 5 3.766 3.283 2.466 < 1 19 8 6 6.416 9.485 3.414 < 1 19 9 1 12.693 10.504 1.605 < 1 19 9 2 31.855 29.357 1.596 o 1 19 9 3 14.443 19.057 5.332 < 1 19 9 4 14.194 16.048 1.711 o 1 19 9 5 2.583 2.922 1.846 < 1 19 9 6 15.097 13.373 1.683 o 1 19 10 1 10.532 10.681 3.862 < 1 19 10 2 16.642 18.370 1.718 o 1 19 10 3 19.744 24.700 4.225 < 1 19 10 4 4.490 7.685 2.900 < 1 19 10 5 2.497 1.143 1.801 < 1 19 11 1 7.614 9.643 3.212 < 1 19 11 2 24.857 23.472 2.305 o 1 19 11 3 12.738 15.268 3.954 < 1 19 11 4 11.418 11.747 4.807 < 1 19 11 5 3.282 1.469 2.219 < 1 19 12 1 9.804 9.878 4.691 < 1 19 12 2 8.306 13.992 3.071 < 1 19 12 3 14.316 17.761 5.271 < 1 19 12 4 3.312 8.872 2.292 < 1 19 13 1 5.748 9.483 3.075 < 1 19 13 2 24.023 18.868 3.259 o 1 19 13 3 12.417 10.509 1.891 < 1 19 14 1 8.098 11.612 3.892 < 1 20 0 0 41.579 45.433 .866 o 1 20 0 1 3.580 .435 2.313 < 1 20 0 2 3.081 8.492 2.204 < 1 20 0 3 4.897 .887 2.633 < 1 20 0 4 24.829 23.804 2.796 o 1 20 0 5 3.051 2.478 2.100 < 1 20 0 6 26.916 26.589 2.171 o 1 20 0 7 4.790 1.526 2.643 < 1 20 1 0 4.445 .289 2.452 < 1 20 1 1 42.167 40.249 .854 o 1 20 1 2 3.537 1.873 2.320 < 1 20 1 3 15.324 15.012 1.449 o 1 20 1 4 5.466 3.903 3.305 < 1 20 1 5 37.500 36.806 .882 o 1 20 1 6 3.728 2.661 2.407 < 1 20 1 7 5.526 6.401 2.924 < 1 20 2 0 38.416 39.258 .863 o 1 20 2 1 5.110 .466 2.734 < 1 20 2 2 11.368 14.473 2.435 < 1 20 2 3 3.055 .676 2.101 < 1 20 2 4 26.035 26.766 1.023 o 1 20 2 5 4.144 .974 2.480 < 1 20 2 6 21.762 24.108 1.203 o 1 20 2 7 4.340 1.690 2.915 < 1 20 3 0 3.025 .473 2.182 < 1 20 3 1 40.653 39.062 3.619 o 1 20 3 2 3.477 .544 2.260 < 1 20 3 3 13.737 15.252 1.605 o 1 20 3 4 3.551 .157 2.301 < 1 20 3 5 35.193 33.989 1.025 o 1 20 3 6 3.372 .222 2.302 < 1 20 3 7 5.594 6.490 2.969 < 1 20 4 0 34.575 34.558 1.280 o 1 20 4 1 2.687 2.065 1.932 < 1 20 4 2 12.736 15.901 3.962 < 1 20 4 3 5.727 2.444 2.779 < 1 20 4 4 20.163 25.373 1.798 o 1 20 4 5 4.374 .919 2.962 < 1 20 4 6 21.114 22.190 1.259 o 1 20 4 7 4.814 1.613 3.123 < 1 20 5 0 3.219 2.477 2.296 < 1 20 5 1 36.165 35.442 2.848 o 1 20 5 2 4.767 .023 2.648 < 1 20 5 3 12.574 14.613 2.696 < 1 20 5 4 3.474 .741 2.331 < 1 20 5 5 31.032 31.853 1.649 o 1 20 5 6 6.554 .045 3.499 < 1 20 5 7 5.706 4.949 3.021 < 1 20 6 0 37.015 37.307 1.319 o 1 20 6 1 4.178 3.215 2.500 < 1 20 6 2 5.638 7.606 2.996 < 1 20 6 3 5.886 .442 2.851 < 1 20 6 4 16.686 20.595 1.659 o 1 20 6 5 4.516 .463 2.925 < 1 20 6 6 21.287 22.968 1.356 o 1 20 7 0 4.063 4.385 2.735 < 1 20 7 1 28.558 29.761 1.982 o 1 20 7 2 3.057 .651 2.128 < 1 20 7 3 12.683 13.084 1.692 o 1 20 7 4 4.227 1.131 2.557 < 1 20 7 5 31.474 29.855 1.657 o 1 20 7 6 3.316 1.657 2.272 < 1 20 8 0 30.459 30.281 1.353 o 1 20 8 1 2.392 .854 1.717 < 1 20 8 2 7.135 8.955 3.422 < 1 20 8 3 5.327 2.441 3.203 < 1 20 8 4 20.474 21.914 1.273 o 1 20 8 5 4.498 1.701 2.699 < 1 20 8 6 19.914 19.283 1.402 o 1 20 9 0 7.152 .069 3.476 < 1 20 9 1 24.516 25.873 2.582 o 1 20 9 2 6.262 .983 3.027 < 1 20 9 3 6.615 11.686 3.187 < 1 20 9 4 4.861 .049 2.686 < 1 20 9 5 23.771 24.316 2.418 o 1 20 10 0 21.498 23.278 1.816 o 1 20 10 1 3.775 .954 2.554 < 1 20 10 2 9.404 10.862 3.978 < 1 20 10 3 2.502 1.546 1.809 < 1 20 10 4 17.230 18.817 1.453 o 1 20 11 0 4.993 2.352 3.022 < 1 20 11 1 23.690 21.829 3.008 o 1 20 11 2 5.113 1.427 3.073 < 1 20 11 3 7.729 7.762 4.116 < 1 20 11 4 3.974 1.297 2.583 < 1 20 12 0 22.403 22.753 1.730 o 1 20 12 1 5.171 .100 3.365 < 1 20 12 2 8.421 6.491 3.094 < 1 21 0 1 14.104 16.397 5.178 < 1 21 0 2 20.494 22.001 1.110 o 1 21 0 3 22.291 25.037 1.167 o 1 21 0 4 10.909 14.019 2.338 < 1 21 0 5 4.168 1.233 2.519 < 1 21 0 6 8.388 9.712 3.093 < 1 21 1 1 20.213 17.292 1.963 o 1 21 1 2 33.838 33.520 1.731 o 1 21 1 3 18.061 18.123 1.232 o 1 21 1 4 13.032 13.787 1.548 < 1 21 1 5 3.265 2.115 2.200 < 1 21 1 6 14.532 14.416 1.665 o 1 21 2 1 13.951 15.135 1.510 o 1 21 2 2 18.258 22.390 2.138 o 1 21 2 3 23.865 23.304 1.092 o 1 21 2 4 5.357 11.928 2.985 < 1 21 2 5 2.707 1.702 1.977 < 1 21 2 6 5.100 8.572 2.817 < 1 21 3 1 12.205 11.570 1.721 < 1 21 3 2 30.171 30.340 1.449 o 1 21 3 3 22.630 21.839 3.464 o 1 21 3 4 14.146 13.410 1.587 o 1 21 3 5 3.584 1.787 2.349 < 1 21 3 6 15.382 14.858 1.687 o 1 21 4 1 13.669 13.561 1.535 o 1 21 4 2 15.668 21.359 1.562 o 1 21 4 3 20.835 20.452 2.866 o 1 21 4 4 7.998 9.913 2.946 < 1 21 4 5 4.798 2.108 2.903 < 1 21 4 6 9.575 7.749 3.519 < 1 21 5 1 10.977 14.686 2.349 < 1 21 5 2 28.278 25.705 .997 o 1 21 5 3 14.648 18.277 4.543 < 1 21 5 4 6.993 12.492 3.382 < 1 21 5 5 2.374 .487 1.720 < 1 21 5 6 14.447 13.860 1.747 < 1 21 6 1 8.257 12.325 3.049 < 1 21 6 2 13.388 19.010 4.158 < 1 21 6 3 17.835 19.312 1.377 o 1 21 6 4 9.130 11.044 3.855 < 1 21 6 5 4.607 1.114 3.119 < 1 21 7 1 13.445 15.457 1.655 < 1 21 7 2 24.641 24.187 1.138 o 1 21 7 3 15.164 15.674 1.578 o 1 21 7 4 12.874 10.741 1.730 < 1 21 7 5 4.903 .394 2.721 < 1 21 8 1 8.614 11.494 4.123 < 1 21 8 2 9.248 15.612 4.456 < 1 21 8 3 17.792 19.829 4.639 < 1 21 8 4 8.404 10.378 3.099 < 1 21 8 5 4.509 .798 3.111 < 1 21 9 1 5.705 7.787 3.390 < 1 21 9 2 22.178 22.630 1.305 o 1 21 9 3 13.598 16.180 4.225 < 1 21 9 4 14.014 10.345 1.660 o 1 21 10 1 14.962 11.629 1.537 o 1 21 10 2 12.770 12.571 3.962 < 1 21 10 3 16.722 16.448 2.312 o 1 21 11 1 8.796 6.473 3.702 < 1 21 11 2 20.161 17.446 1.381 o 1 22 0 0 4.867 5.659 2.643 < 1 22 0 1 26.030 26.562 1.103 o 1 22 0 2 4.208 4.706 2.522 < 1 22 0 3 6.283 9.056 3.013 < 1 22 0 4 6.181 7.288 3.386 < 1 22 0 5 24.464 24.137 1.393 o 1 22 0 6 4.477 3.626 2.647 < 1 22 1 0 38.237 35.373 .997 o 1 22 1 1 9.121 11.344 2.841 < 1 22 1 2 10.661 8.299 2.278 < 1 22 1 3 8.841 7.018 2.766 < 1 22 1 4 23.130 21.199 1.199 o 1 22 1 5 12.037 8.315 1.699 < 1 22 1 6 17.905 17.394 1.405 o 1 22 2 0 6.292 8.130 3.441 < 1 22 2 1 27.115 25.415 1.032 o 1 22 2 2 3.925 1.535 2.517 < 1 22 2 3 7.838 8.520 2.883 < 1 22 2 4 3.458 4.226 2.291 < 1 22 2 5 23.474 23.826 1.241 o 1 22 3 0 33.634 31.551 1.326 o 1 22 3 1 7.182 8.790 3.038 < 1 22 3 2 6.201 8.456 2.978 < 1 22 3 3 6.184 4.276 2.980 < 1 22 3 4 20.452 20.880 1.326 o 1 22 3 5 10.182 8.962 2.666 < 1 22 4 0 11.357 6.883 2.961 < 1 22 4 1 24.820 22.594 1.097 o 1 22 4 2 4.380 .537 2.591 < 1 22 4 3 8.703 7.124 3.664 < 1 22 4 4 3.963 2.686 2.328 < 1 22 4 5 23.230 23.043 2.460 o 1 22 5 0 32.031 29.811 1.410 o 1 22 5 1 6.326 6.676 3.042 < 1 22 5 2 7.096 6.871 2.986 < 1 22 5 3 4.957 3.325 2.733 < 1 22 5 4 17.654 19.786 1.480 o 1 22 5 5 5.687 7.345 3.392 < 1 22 6 0 4.998 2.743 2.938 < 1 22 6 1 19.959 21.053 1.278 o 1 22 6 2 3.643 4.123 2.361 < 1 22 6 3 7.352 6.529 2.702 < 1 22 6 4 3.491 5.021 2.331 < 1 22 7 0 28.630 26.547 1.562 o 1 22 7 1 5.109 7.287 2.816 < 1 22 7 2 4.394 6.716 2.622 < 1 22 7 3 4.377 3.766 2.834 < 1 22 7 4 20.398 18.713 2.557 o 1 22 8 0 6.874 6.584 3.633 < 1 22 8 1 17.414 18.967 2.306 o 1 22 8 2 2.881 2.602 2.062 < 1 22 8 3 8.847 6.396 2.744 < 1 22 9 0 22.774 21.790 1.812 o 1 22 9 1 2.872 7.116 2.038 < 1 22 9 2 6.592 6.753 3.163 < 1 22 10 0 4.897 8.221 3.155 < 1 23 0 1 5.498 8.462 2.940 < 1 23 0 2 23.912 25.070 1.137 o 1 23 0 3 6.377 9.188 3.066 < 1 23 0 4 9.262 11.659 2.878 < 1 23 1 1 12.876 17.162 3.358 < 1 23 1 2 10.235 6.726 2.181 < 1 23 1 3 24.184 23.080 1.126 o 1 23 1 4 6.463 5.056 3.097 < 1 23 2 1 2.882 6.688 2.088 < 1 23 2 2 22.300 22.815 1.132 o 1 23 2 3 8.915 10.077 3.770 < 1 23 2 4 10.713 12.646 3.948 < 1 23 3 1 18.524 17.360 1.342 o 1 23 3 2 7.214 6.930 3.030 < 1 23 3 3 19.757 19.643 1.345 o 1 23 3 4 3.290 4.985 2.196 < 1 23 4 1 4.442 5.963 2.864 < 1 23 4 2 15.321 19.840 3.281 < 1 23 4 3 9.207 9.478 2.864 < 1 23 4 4 15.411 13.516 1.548 o 1 23 5 1 11.033 13.989 3.427 < 1 23 5 2 7.171 6.856 3.012 < 1 23 5 3 20.043 19.797 1.325 o 1 23 6 1 4.451 6.533 2.881 < 1 23 6 2 20.755 19.331 1.303 o 1 23 6 3 3.649 7.575 2.466 < 1 23 7 1 13.229 11.814 1.732 < 1 23 7 2 4.472 6.063 2.653 < 1 24 0 0 20.325 22.261 1.351 o 1 24 0 1 8.265 10.060 3.044 < 1 24 0 2 6.056 7.203 3.225 < 1 24 0 3 3.984 4.759 2.556 < 1 24 1 0 13.300 15.028 1.849 < 1 24 1 1 16.014 15.771 1.512 o 1 24 1 2 7.034 2.502 2.972 < 1 24 1 3 5.057 5.198 2.997 < 1 24 2 0 16.758 21.611 5.210 < 1 24 2 1 9.089 9.763 2.818 < 1 24 2 2 2.704 5.690 1.924 < 1 24 2 3 3.578 3.685 2.376 < 1 24 3 0 16.001 15.306 2.152 o 1 24 3 1 16.691 13.979 1.408 o 1 24 3 2 3.343 1.804 2.260 < 1 24 4 0 23.011 19.621 1.572 o 1 24 4 1 8.422 9.606 4.470 < 1 24 4 2 5.165 4.918 3.060 < 1 24 5 0 10.555 12.879 3.888 < 1 24 5 1 13.571 13.011 1.743 o 1 _publ_requested_journal ? #ActaC _publ_requested_coeditor_name ? #ActaC _publ_contact_author #ActaC ; ? name ? institute ? department ? address ? city ? country ; _publ_contact_letter #ActaC ; ? letter to co-editor ; _publ_contact_author_phone ? #ActaC _publ_contact_author_fax ? #ActaC _publ_contact_author_email ? #ActaC loop_ _publ_author_name #ActaC _publ_author_address #ActaC '? surname, initials' ; ? institute ? department ? address ? city ? country ; _publ_section_title #ActaC ; ? ; _publ_section_abstract #ActaC ; ? ; _publ_section_comment #ActaC ; ? ; _publ_section_experimental #ActaC ; ? ; _publ_section_references #ActaC ; ? ; _publ_section_figure_captions #ActaC ; ? ; _publ_section_acknowledgements #ActaC ; ? ; #============================================================================== # (IUCr Office Use Only) _journal_date_recd_electronic ? _journal_date_to_coeditor ? _journal_date_from_coeditor ? _journal_date_accepted ? _journal_date_printers_first ? _journal_date_printers_final ? _journal_date_proofs_out ? _journal_date_proofs_in ? _journal_coeditor_name ? _journal_coeditor_code ? _journal_coeditor_notes ; ? ; _journal_techeditor_code ? _journal_techeditor_notes ; ? ; _journal_coden_ASTM ? _journal_name_full ? _journal_year ? _journal_volume ? _journal_issue ? _journal_page_first ? _journal_page_last ? _journal_suppl_publ_number ? _journal_suppl_publ_pages ? #=END data_euen2 _audit_creation_date 97-09-30 _audit_creation_method from_xtal_archive_file_using_CIFIO _audit_update_record ? _chemical_compound_source ? #ActaC _chemical_name_systematic ? #ActaC _chemical_name_common ? #ActaC _chemical_formula_analytical ? #ActaC _chemical_formula_moiety ? #ActaC _chemical_formula_structural ? #ActaC _chemical_formula_sum C10.5_H28.5_Eu.5_N3_Si1.5 #ActaC _chemical_formula_weight 314.97 #ActaC _chemical_melting_point ? #ActaC _computing_data_collection ? #ActaC _computing_cell_refinement ? #ActaC _computing_data_reduction xtal_DIFDAT_ABSORB_SORTRF_ADDREF #ActaC _computing_structure_solution xtal #ActaC _computing_structure_refinement xtal_CRYLSQ #ActaC _computing_molecular_graphics xtal #ActaC _computing_publication_material xtal_BONDLA_CIFIO #ActaC _cell_length_a 19.164(7) #ActaC _cell_length_b 17.042(5) #ActaC _cell_length_c 10.136(7) #ActaC _cell_angle_alpha 90.00000 #ActaC _cell_angle_beta 90.00000 #ActaC _cell_angle_gamma 90.00000 #ActaC _cell_volume 3310(3) #ActaC _cell_formula_units_Z 8 #ActaC _cell_measurement_temperature 293 #ActaC _cell_measurement_reflns_used ? #ActaC _cell_measurement_theta_min ? #ActaC _cell_measurement_theta_max ? #ActaC _cell_special_details #ActaC ; ? ; _symmetry_cell_setting orthorhombic #ActaC _symmetry_space_group_name_H-M p_n_m_a #ActaC _symmetry_space_group_name_Hall -p_2ac_2n #ActaC loop_ _symmetry_equiv_pos_as_xyz #ActaC +x,+y,+z 1/2-x,-y,1/2+z 1/2+x,1/2-y,1/2-z -x,1/2+y,-z -x,-y,-z 1/2+x,+y,1/2-z 1/2-x,1/2+y,1/2+z +x,1/2-y,+z _exptl_crystal_description ? #ActaC _exptl_crystal_preparation ? _exptl_crystal_colour ? #ActaC _exptl_crystal_size_max ? #ActaC _exptl_crystal_size_mid ? #ActaC _exptl_crystal_size_min ? #ActaC _exptl_crystal_density_diffrn 1.264 #ActaC _exptl_crystal_density_meas ? #ActaC _exptl_crystal_density_method ? #ActaC _exptl_crystal_F_000 1320 #ActaC _exptl_absorpt_process_details ? _exptl_absorpt_coefficient_mu '20.2 cm-1' #ActaC _exptl_absorpt_correction_type gaussian #ActaC _exptl_absorpt_correction_T_min 1.80 #ActaC _exptl_absorpt_correction_T_max 2.40 #ActaC _exptl_special_details #ActaC ; ? ; _diffrn_special_details ; ? ; _diffrn_ambient_temperature 293 #ActaC _diffrn_radiation_wavelength 0.71073 #ActaC _diffrn_radiation_type xray_tube #ActaC _diffrn_radiation_source ? #ActaC _diffrn_radiation_monochromator graphite #ActaC _diffrn_radiation_detector ? #ActaC _diffrn_measurement_device CAD4 #ActaC _diffrn_measurement_method ? #ActaC _diffrn_standards_number ? #ActaC _diffrn_standards_interval_count ? #ActaC _diffrn_standards_interval_time ? #ActaC _diffrn_standards_decay_% ? #ActaC loop_ _diffrn_standard_refln_index_h #ActaC _diffrn_standard_refln_index_k #ActaC _diffrn_standard_refln_index_l #ActaC ? ? ? loop_ _diffrn_attenuator_code _diffrn_attenuator_scale ? ? _diffrn_reflns_number 6922 #ActaC _diffrn_reflns_av_R_equivalents .055 #ActaC _diffrn_reflns_av_sigmaI/netI .059 #ActaC _diffrn_reflns_limit_h_min -22 #ActaC _diffrn_reflns_limit_h_max 0 #ActaC _diffrn_reflns_limit_k_min -20 #ActaC _diffrn_reflns_limit_k_max 20 #ActaC _diffrn_reflns_limit_l_min -12 #ActaC _diffrn_reflns_limit_l_max 1 #ActaC _diffrn_reflns_theta_min 2.13 #ActaC _diffrn_reflns_theta_max 24.99 #ActaC _diffrn_reflns_reduction_process perpendicular_monochr_Lp #ActaC loop_ _atom_type_symbol #ActaC _atom_type_description #ActaC _atom_type_oxidation_number _atom_type_number_in_cell _atom_type_scat_dispersion_real #ActaC _atom_type_scat_dispersion_imag #ActaC _atom_type_scat_source #ActaC C ? 0 84 .002 .002 Int_Tables_Vol_IV_Tables_2.2B_and_2.3.1 O ? 0 0 .008 .006 Int_Tables_Vol_IV_Tables_2.2B_and_2.3.1 H ? 0 228 0 0 Int_Tables_Vol_IV_Tables_2.2B_and_2.3.1 Eu ? 0 4 -.542 3.669 Int_Tables_Vol_IV_Tables_2.2B_and_2.3.1 N ? 0 24 .004 .003 Int_Tables_Vol_IV_Tables_2.2B_and_2.3.1 Si ? 0 12 .072 .071 Int_Tables_Vol_IV_Tables_2.2B_and_2.3.1 loop_ _atom_site_label #ActaC _atom_site_fract_x #ActaC _atom_site_fract_y #ActaC _atom_site_fract_z #ActaC _atom_site_U_iso_or_equiv #ActaC _atom_site_thermal_displace_type #ActaC _atom_site_calc_flag #ActaC _atom_site_calc_attached_atom #ActaC Eu .40052(3) .25000 .64854(6) .0530(4) Uani ? ? N11 .3152(6) .3361(8) .6149(14) .067(10) Uani ? ? Si1 .2973(3) .4030(4) .4976(7) .090(4) Uani ? ? C111 .2038(13) .4045(17) .432(3) .16(3) Uani ? ? C112 .3201(15) .5082(14) .536(4) .16(3) Uani ? ? C113 .3533(15) .378(2) .343(2) .16(3) Uani ? ? C11 .2613(13) .3420(15) .710(3) .14(2) Uani ? ? C12 .2832(13) .3267(17) .857(3) .21(3) Uani ? ? N12 .3161(6) .25000 .8713(12) .094(9) Uani ? ? C121 .2632(14) .197(2) .838(3) .22(4) Uani ? ? C122 .3361(14) .222(3) .994(2) .21(4) Uani ? ? N21 .4923(7) .2823(8) .5163(14) .077(11) Uani ? ? Si2 .5258(2) .25000 .3717(4) .089(3) Uani ? ? C211 .6152(11) .205(2) .391(2) .19(3) Uani ? ? C212 .4685(13) .1738(17) .296(2) .14(2) Uani ? ? C213 .5347(13) .3264(17) .241(2) .16(2) Uani ? ? C21 .5315(13) .353(2) .562(3) .18(3) Uani ? ? C22 .4861(16) .4100(17) .640(2) .16(2) Uani ? ? N22 .4952(6) .3607(10) .7762(17) .081(11) Uani ? ? C221 .4389(14) .4282(13) .828(3) .15(3) Uani ? ? C222 .5355(16) .346(2) .848(3) .23(4) Uani ? ? N31 .3594(7) .1291(9) .5771(16) .074(10) Uani ? ? Si3 .2914(4) .1059(4) .4747(8) .117(6) Uani ? ? C311 .315(2) .049(3) .331(4) .28(5) Uani ? ? C312 .2303(16) .037(2) .558(4) .21(3) Uani ? ? C313 .240(2) .185(2) .426(5) .36(5) Uani ? ? C31 .3950(11) .0601(14) .611(3) .12(2) Uani ? ? C32 .447(2) .072(3) .709(6) .30(2) Uiso ? ? N32 .4667(5) .1304(10) .7747(15) .069(10) Uani ? ? C321 .483(2) .123(4) .904(3) .31(5) Uani ? ? C322 .5478(11) .135(2) .709(3) .15(2) Uani ? ? H111a .19590 .35408 .39262 .26000 Uiso ? ? H111b .17247 .41097 .50358 .26000 Uiso ? ? H111c .19426 .44332 .36759 .26000 Uiso ? ? H112a .29175 .52165 .61305 .24000 Uiso ? ? H112b .36625 .51114 .55584 .24000 Uiso ? ? H112c .30843 .54778 .47240 .24000 Uiso ? ? H113a .40170 .37764 .36535 .25000 Uiso ? ? H113b .33971 .32835 .31227 .25000 Uiso ? ? H113c .34405 .41777 .28005 .25000 Uiso ? ? H11a .24448 .39519 .70949 .15000 Uiso ? ? H11b .22587 .30714 .69316 .15000 Uiso ? ? H12a .31835 .36449 .90167 .25000 Uiso ? ? H12b .24577 .32763 .92909 .25000 Uiso ? ? H121a .22318 .19961 .89303 .29000 Uiso ? ? H121b .24402 .21112 .74641 .29000 Uiso ? ? H121c .28096 .14673 .83078 .29000 Uiso ? ? H122a .36763 .25957 1.03553 .33000 Uiso ? ? H122b .29431 .22240 1.05277 .33000 Uiso ? ? H122c .35526 .17286 .99816 .33000 Uiso ? ? H211a .64436 .23708 .42296 .31000 Uiso ? ? H211b .60772 .15699 .44516 .31000 Uiso ? ? H211c .63055 .18182 .30554 .31000 Uiso ? ? H212a .46138 .13288 .35485 .21000 Uiso ? ? H212b .42267 .19962 .28084 .21000 Uiso ? ? H212c .48506 .15740 .21482 .21000 Uiso ? ? H213a .48918 .34780 .22440 .24000 Uiso ? ? H213b .56421 .36645 .27255 .24000 Uiso ? ? H213c .55242 .30789 .15908 .24000 Uiso ? ? H21a .56882 .33753 .62309 .21000 Uiso ? ? H21b .55220 .38009 .49150 .21000 Uiso ? ? H22a .50479 .46152 .64332 .17000 Uiso ? ? H22b .43946 .41197 .60830 .17000 Uiso ? ? H221a .45561 .48057 .83073 .25000 Uiso ? ? H221b .39391 .42672 .79050 .25000 Uiso ? ? H221c .44421 .39941 .90919 .25000 Uiso ? ? H222a .57055 .32307 .79047 .30000 Uiso ? ? H222b .55239 .39789 .87060 .30000 Uiso ? ? H222c .54190 .31849 .92550 .30000 Uiso ? ? H31a .35993 .02268 .64754 .19000 Uiso ? ? H31b .41357 .03601 .53513 .19000 Uiso ? ? H311a .34756 .08091 .27840 .39000 Uiso ? ? H311b .33692 .00303 .35503 .39000 Uiso ? ? H311c .27787 .03678 .26987 .39000 Uiso ? ? H312a .25400 -.00824 .58209 .31000 Uiso ? ? H312b .21141 .06283 .63366 .31000 Uiso ? ? H312c .19252 .02458 .49981 .31000 Uiso ? ? H313a .22183 .21070 .49866 .35000 Uiso ? ? H313b .27062 .22173 .37795 .35000 Uiso ? ? H313c .20362 .17242 .36543 .35000 Uiso ? ? H32a .43780 .03555 .77317 .45000 Uiso ? ? H32b .48934 .06040 .66280 .45000 Uiso ? ? H321a .44552 .10360 .94841 .24000 Uiso ? ? H321b .52233 .08827 .90754 .24000 Uiso ? ? H321c .49956 .16828 .95636 .24000 Uiso ? ? H322a .57446 .08902 .72529 .24000 Uiso ? ? H322b .54732 .14612 .61770 .24000 Uiso ? ? H322c .56224 .17837 .76150 .24000 Uiso ? ? loop_ _atom_site_aniso_label #ActaC _atom_site_aniso_U_11 #ActaC _atom_site_aniso_U_22 #ActaC _atom_site_aniso_U_33 #ActaC _atom_site_aniso_U_12 #ActaC _atom_site_aniso_U_13 #ActaC _atom_site_aniso_U_23 #ActaC Eu .0599(4) .0592(4) .0400(4) .00118 -.0013(4) .00182 N11 .056(8) .077(11) .070(10) .023(8) .010(7) .000(9) Si1 .096(4) .090(5) .084(4) .008(4) .012(4) .009(4) C111 .14(2) .17(3) .18(3) .05(2) -.05(2) .05(3) C112 .18(3) .071(17) .22(4) -.003(18) -.03(3) .05(2) C113 .20(3) .23(4) .049(14) .08(3) -.012(17) .02(2) C11 .15(2) .14(2) .15(2) .087(19) .01(2) .04(2) C12 .14(2) .13(2) .35(6) .011(19) .15(3) -.07(3) N12 .108(9) .092(9) .083(9) .00000 .012(8) .00000 C121 .17(2) .33(6) .16(3) -.02(3) .06(2) -.19(3) C122 .21(3) .33(9) .094(17) .06(4) -.022(19) .12(4) N21 .081(9) .094(15) .055(9) -.024(8) -.000(8) -.001(8) Si2 .081(3) .135(4) .051(3) .00000 .009(2) .00000 C211 .129(19) .35(7) .083(17) .10(3) .040(15) -.00(2) C212 .17(2) .18(3) .065(14) -.03(2) .021(17) -.065(18) C213 .17(2) .20(3) .10(2) -.01(2) .062(19) .08(2) C21 .17(3) .22(3) .13(2) -.10(2) .10(2) -.10(3) C22 .23(3) .15(3) .09(2) -.12(2) -.02(2) -.01(2) N22 .031(7) .107(13) .103(13) -.005(8) -.020(8) -.032(12) C221 .14(2) .064(15) .24(4) -.020(16) -.02(2) -.04(2) C222 .21(3) .17(3) .29(5) -.03(3) -.19(3) -.01(3) N31 .072(9) .065(10) .084(12) .018(8) -.007(9) -.011(10) Si3 .128(6) .105(6) .119(6) -.041(5) -.041(5) -.035(5) C311 .23(4) .38(6) .23(5) -.13(4) .03(3) -.19(5) C312 .17(3) .24(4) .21(4) -.10(3) -.00(3) -.07(4) C313 .33(5) .24(4) .50(7) .08(4) -.38(5) -.12(5) C31 .15(2) .083(16) .13(2) -.022(16) -.01(2) -.034(16) N32 .022(6) .107(12) .080(11) .001(7) -.032(7) .013(10) C321 .33(5) .51(7) .07(2) .23(5) .04(3) .12(4) C322 .090(15) .24(3) .12(2) .10(2) .022(16) .05(3) _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens ? _refine_special_details sfls__F_____calc_weight_atomblock_matrix _refine_ls_structure_factor_coef F #ActaC _refine_ls_matrix_type atomblock #ActaC _refine_ls_weighting_scheme calc #ActaC _refine_ls_hydrogen_treatment ? #ActaC _refine_ls_extinction_method none #ActaC _refine_ls_extinction_coef .00000 #ActaC _refine_ls_extinction_expression ? _refine_ls_abs_structure_details none #ActaC _refine_ls_abs_structure_Flack 0 #ActaC _refine_ls_number_reflns 1632 #ActaC _refine_ls_number_parameters 267 #ActaC _refine_ls_number_restraints 0 #ActaC _refine_ls_number_constraints 0 #ActaC _refine_ls_R_factor_all .084 #ActaC _refine_ls_R_factor_obs .047 #ActaC _refine_ls_wR_factor_all .067 #ActaC _refine_ls_wR_factor_obs .052 #ActaC _refine_ls_goodness_of_fit_all 1.172 #ActaC _refine_ls_goodness_of_fit_obs 1.293 #ActaC _refine_ls_shift/esd_max .127 #ActaC _refine_ls_shift/esd_mean .013 #ActaC _refine_diff_density_min -.724 #ActaC _refine_diff_density_max 1.242 #ActaC _geom_special_details ? #ActaC loop_ _geom_bond_atom_site_label_1 #ActaC _geom_bond_atom_site_label_2 #ActaC _geom_bond_distance #ActaC _geom_bond_site_symmetry_1 #ActaC _geom_bond_site_symmetry_2 #ActaC _geom_bond_publ_flag #ActaC Eu N11 2.222(13) . . ? Eu N12 2.777(12) . . ? Eu N21 2.279(13) . . ? Eu N22 2.920(15) . . ? Eu N31 2.321(15) . . ? Eu N32 2.721(15) . . ? Eu N11 2.222(13) . 8 ? Eu N21 2.279(13) . 8 ? Eu N22 2.920(15) . 8 ? Eu N31 2.321(15) . 8 ? Eu N32 2.721(15) . 8 ? N11 Si1 1.684(16) . . ? N11 C11 1.42(3) . . ? N11 N31 1.10(2) . 8 ? N11 Si3 1.790(16) . 8 ? Si1 C111 1.91(3) . . ? Si1 C112 1.88(3) . . ? Si1 C113 1.94(3) . . ? Si1 N31 1.539(16) . 8 ? Si1 Si3 .300(10) . 8 ? Si1 C311 1.91(4) . 8 ? Si1 C312 1.75(3) . 8 ? Si1 C313 2.00(4) . 8 ? C111 H111a .96(3) . . ? C111 H111b .95(3) . . ? C111 H111c .95(3) . . ? C111 Si3 1.74(3) . 8 ? C111 C312 1.70(5) . 8 ? C111 C313 1.68(5) . 8 ? C111 H312c 1.41(3) . 8 ? C111 H313c 1.47(3) . 8 ? C112 H112a .98(3) . . ? C112 H112b .91(3) . . ? C112 H112c .96(3) . . ? C112 Si3 2.11(3) . 8 ? C112 C312 1.90(4) . 8 ? C112 C31 2.00(4) . 8 ? C112 H31a 1.46(3) . 8 ? C112 H312a 1.35(3) . 8 ? C113 H113a .95(3) . . ? C113 H113b .94(4) . . ? C113 H113c .95(3) . . ? C113 Si3 1.80(3) . 8 ? C113 C311 1.44(6) . 8 ? C113 H311a .97(3) . 8 ? C11 C12 1.57(5) . . ? C11 H11a .96(3) . . ? C11 H11b .92(3) . . ? C11 C121 1.46(4) . 8 ? C11 H121b 1.03(3) . 8 ? C11 H121c 1.30(3) . 8 ? C12 N12 1.46(3) . . ? C12 H12a 1.04(3) . . ? C12 H12b 1.02(3) . . ? C12 C121 .59(4) . 8 ? C12 C122 1.91(5) . 8 ? C12 H121a 1.29(3) . 8 ? C12 H121b 1.49(3) . 8 ? C12 H121c .53(3) . 8 ? N12 C121 1.40(3) . . ? N12 C122 1.38(3) . . ? N12 C121 1.40(3) . 8 ? N12 C122 1.38(3) . 8 ? C121 H121a .95(3) . . ? C121 H121b 1.03(3) . . ? C121 H121c .92(3) . . ? C121 C121 1.81(5) . 8 ? C121 H12b 1.07(3) . 8 ? C122 H122a .98(4) . . ? C122 H122b 1.00(3) . . ? C122 H122c .92(6) . . ? C122 C122 .95(8) . 8 ? C122 H122a .80(3) . 8 ? C122 H122b 1.38(4) . 8 ? N21 Si2 1.692(14) . . ? N21 C21 1.49(3) . . ? N21 N21 1.101(19) . 8 ? Si2 C211 1.89(3) . . ? Si2 C212 1.87(3) . . ? Si2 C213 1.86(3) . . ? Si2 C211 1.89(3) . 8 ? Si2 C212 1.87(3) . 8 ? Si2 C213 1.86(3) . 8 ? C211 H211a .84(3) . . ? C211 H211b 1.00(3) . . ? C211 H211c 1.00(3) . . ? C211 C211 1.52(5) . 8 ? C211 H211a 1.17(3) . 8 ? C212 H212a .93(3) . . ? C212 H212b .99(3) . . ? C212 H212c .92(2) . . ? C212 C213 1.38(3) . 8 ? C212 H213a .90(2) . 8 ? C213 H213a .96(3) . . ? C213 H213b .94(3) . . ? C213 H213c .95(3) . . ? C213 H212c 1.03(3) . 8 ? C21 C22 1.52(4) . . ? C21 H21a .98(3) . . ? C21 H21b .94(3) . . ? C21 C322 1.54(4) . 8 ? C21 H322b .64(3) . 8 ? C22 N22 1.63(3) . . ? C22 H22a .95(3) . . ? C22 H22b .95(3) . . ? C22 C31 1.84(4) . 8 ? C22 C32 1.07(6) . 8 ? C22 N32 1.58(3) . 8 ? C22 C322 1.58(4) . 8 ? C22 H32b .56(3) . 8 ? N22 C221 1.66(3) . . ? N22 C222 1.09(4) . . ? N22 C32 1.62(5) . 8 ? N22 N32 .567(16) . 8 ? N22 C321 1.34(4) . 8 ? N22 C322 1.22(3) . 8 ? N22 H322c 1.454(13) . 8 ? C221 H221a .95(2) . . ? C221 H221b .94(3) . . ? C221 H221c .97(3) . . ? C221 C32 1.22(7) . 8 ? C221 N32 1.25(3) . 8 ? C221 C321 1.44(5) . 8 ? C221 H32a .83(3) . 8 ? C221 H321a 1.34(3) . 8 ? C222 H222a .97(3) . . ? C222 H222b .97(4) . . ? C222 H222c .92(4) . . ? C222 N32 1.57(3) . 8 ? C222 C321 1.26(5) . 8 ? C222 C322 1.46(4) . 8 ? C222 H321b 1.30(4) . 8 ? C222 H321c 1.32(3) . 8 ? C222 H322c 1.10(3) . 8 ? N31 Si3 1.713(16) . . ? N31 C31 1.40(3) . . ? Si3 C311 1.81(4) . . ? Si3 C312 1.86(4) . . ? Si3 C313 1.74(4) . . ? C311 H311a .97(4) . . ? C311 H311b .92(5) . . ? C311 H311c .97(4) . . ? C311 H113c .94(4) . 8 ? C312 H312a .93(4) . . ? C312 H312b .95(4) . . ? C312 H312c .96(3) . . ? C313 H313a .93(4) . . ? C313 H313b .98(4) . . ? C313 H313c .95(4) . . ? C313 H111a 1.13(4) . 8 ? C31 C32 1.41(6) . . ? C31 H31a 1.00(2) . . ? C31 H31b .94(3) . . ? C31 H112b 1.45(2) . 8 ? C31 H22b .98(2) . 8 ? C32 N32 1.26(5) . . ? C32 H32a .92(5) . . ? C32 H32b .96(5) . . ? C32 H22a 1.42(5) . 8 ? C32 H22b 1.06(6) . 8 ? C32 H221b 1.31(5) . 8 ? N32 C321 1.35(3) . . ? N32 C322 1.69(2) . . ? C321 H321a .92(4) . . ? C321 H321b .96(5) . . ? C321 H321c .99(5) . . ? C321 H221c .84(5) . 8 ? C321 H222b 1.41(4) . 8 ? C322 H322a .95(3) . . ? C322 H322b .95(3) . . ? C322 H322c .95(3) . . ? C322 H21a 1.07(3) . 8 ? C322 H222a 1.17(3) . 8 ? H111a H313c .54936(15) . 8 ? H112a H312a .8210(2) . 8 ? H113c H311a .07287(2) . 8 ? H11b H121b .7135(3) . 8 ? H12b H121a .73247(18) . 8 ? H122a H122a .32618(10) . 8 ? H122b H122b .9407(3) . 8 ? H211a H211a .44037(13) . 8 ? H212c H213a .15335(5) . 8 ? H21a H322b .50039(13) . 8 ? H22a H32b .51595(11) . 8 ? H221a H32a .7296(3) . 8 ? H221c H321a .4016(3) . 8 ? H222a H322c .33495(18) . 8 ? H222b H321b .7264(2) . 8 ? H222c H321c .8984(3) . 8 ? H313b H313b .9636(3) . 8 ? loop_ _geom_contact_atom_site_label_1 #ActaC _geom_contact_atom_site_label_2 #ActaC _geom_contact_distance #ActaC _geom_contact_site_symmetry_1 #ActaC _geom_contact_site_symmetry_2 #ActaC _geom_contact_publ_flag #ActaC Eu Si1 3.614(6) . 8 ? Eu Si1 3.614(6) . . ? Eu C113 3.89(3) . 8 ? Eu C113 3.89(3) . . ? Eu C11 3.16(2) . 8 ? Eu C11 3.16(2) . . ? Eu C12 3.35(3) . 8 ? Eu C12 3.35(3) . . ? Eu C121 3.38(3) . . ? Eu C121 3.38(3) . 8 ? Eu C122 3.74(3) . 8 ? Eu C122 3.74(3) . . ? Eu Si2 3.693(4) . . ? Eu C21 3.18(3) . 8 ? Eu C21 3.18(3) . . ? Eu C22 3.18(3) . 8 ? Eu C22 3.18(3) . . ? Eu C221 3.61(3) . . ? Eu C221 3.61(3) . 8 ? Eu C222 3.67(3) . . ? Eu C222 3.67(3) . 8 ? Eu Si3 3.675(7) . 8 ? Eu Si3 3.675(7) . . ? Eu C313 3.97(4) . 8 ? Eu C313 3.97(4) . . ? Eu C31 3.26(2) . 8 ? Eu C31 3.26(2) . . ? Eu C32 3.21(5) . 8 ? Eu C32 3.21(5) . . ? Eu C321 3.73(4) . . ? Eu C321 3.73(4) . 8 ? Eu C322 3.49(3) . . ? Eu C322 3.49(3) . 8 ? Eu H121b 3.2277(12) . 8 ? Eu H121b 3.2277(12) . . ? Eu H121c 3.4292(11) . 8 ? Eu H121c 3.4292(11) . . ? Eu H22b 2.8883(8) . 8 ? Eu H22b 2.8883(8) . . ? Eu H221b 3.3401(9) . 8 ? Eu H221b 3.3401(9) . . ? Eu H322b 3.3386(10) . 8 ? Eu H322b 3.3386(10) . . ? N11 N11 2.93(2) . 8 ? N11 C113 2.93(3) . . ? N11 C12 2.53(4) . . ? N11 N12 2.984(17) . . ? N11 C121 2.54(3) . 8 ? N11 C312 2.76(4) . 8 ? N11 C313 2.43(5) . 8 ? N11 C31 2.34(3) . 8 ? N11 H11a 1.942(13) . . ? N11 H11b 1.951(13) . . ? N11 H121b 2.071(13) . 8 ? N11 H121c 2.303(14) . 8 ? N11 H313a 2.287(13) . 8 ? Si1 C11 2.49(3) . . ? Si1 C31 2.29(2) . 8 ? Si1 H111a 2.367(6) . . ? Si1 H111b 2.397(6) . . ? Si1 H111c 2.471(6) . . ? Si1 H112a 2.338(6) . . ? Si1 H112b 2.343(6) . . ? Si1 H112c 2.489(6) . . ? Si1 H113a 2.446(6) . . ? Si1 H113b 2.410(7) . . ? Si1 H113c 2.393(7) . . ? Si1 H11a 2.379(7) . . ? Si1 H31a 2.314(6) . 8 ? Si1 H31b 2.488(6) . 8 ? Si1 H311a 2.436(7) . 8 ? Si1 H311b 2.286(6) . 8 ? Si1 H311c 2.553(7) . 8 ? Si1 H312a 2.153(6) . 8 ? Si1 H312b 2.225(6) . 8 ? Si1 H312c 2.357(6) . 8 ? Si1 H313a 2.419(6) . 8 ? Si1 H313b 2.501(6) . 8 ? Si1 H313c 2.583(6) . 8 ? C111 C311 2.50(5) . 8 ? C111 H311c 2.39(3) . 8 ? C111 H312b 2.13(3) . 8 ? C111 H313a 2.10(3) . 8 ? C112 N31 2.49(3) . 8 ? C112 C311 2.30(5) . 8 ? C112 H31b 1.94(3) . 8 ? C112 H311b 1.87(4) . 8 ? C113 C212 2.43(4) . 8 ? C113 N31 2.37(3) . 8 ? C113 C313 2.56(5) . 8 ? C113 H212a 2.08(3) . 8 ? C113 H212b 1.98(3) . 8 ? C113 H311b 2.05(4) . 8 ? C113 H311c 2.18(3) . 8 ? C113 H313b 2.35(3) . 8 ? C11 N12 2.50(3) . . ? C11 C121 2.79(4) . . ? C11 N31 2.36(3) . 8 ? C11 Si3 2.61(3) . 8 ? C11 C312 2.64(5) . 8 ? C11 C313 2.95(6) . 8 ? C11 H12a 2.26(3) . . ? C11 H12b 2.26(3) . . ? C11 H121a 2.12(3) . 8 ? C11 H121b 2.28(3) . . ? C11 H312b 2.04(3) . 8 ? C11 H313a 2.44(3) . 8 ? C12 C12 2.62(4) . 8 ? C12 C121 2.25(5) . . ? C12 C122 2.48(6) . . ? C12 H11a 2.03(3) . . ? C12 H11b 2.02(3) . . ? C12 H121a 2.48(3) . . ? C12 H121b 2.39(3) . . ? C12 H122b 2.17(3) . 8 ? C12 H122c 1.99(3) . 8 ? N12 H12a 1.976(2) . 8 ? N12 H12a 1.976(2) . . ? N12 H12b 1.978(9) . . ? N12 H12b 1.978(9) . 8 ? N12 H121a 1.990(11) . . ? N12 H121a 1.990(11) . 8 ? N12 H121b 1.988(11) . . ? N12 H121b 1.988(11) . 8 ? N12 H121c 1.929(5) . . ? N12 H121c 1.929(5) . 8 ? N12 H122a 1.942(12) . 8 ? N12 H122a 1.942(12) . . ? N12 H122b 1.944(12) . 8 ? N12 H122b 1.944(12) . . ? N12 H122c 1.986(9) . 8 ? N12 H122c 1.986(9) . . ? C121 C122 2.15(4) . . ? C121 C122 2.52(5) . 8 ? C121 H11a 2.07(3) . 8 ? C121 H11b 1.63(3) . 8 ? C121 H11b 2.49(3) . . ? C121 H12a 1.62(3) . 8 ? C121 H12b 2.43(3) . . ? C121 H121a 2.00(3) . 8 ? C121 H121b 1.86(3) . 8 ? C121 H122b 2.30(3) . . ? C121 H122c 2.43(3) . . ? C122 H12a 1.78(5) . 8 ? C122 H12b 2.03(3) . 8 ? C122 H121a 2.42(3) . . ? C122 H121c 2.34(4) . . ? C122 H122c 1.83(6) . 8 ? N21 C211 2.68(3) . 8 ? N21 C211 2.98(3) . . ? N21 C212 2.94(3) . . ? N21 C212 2.40(3) . 8 ? N21 C21 2.47(4) . 8 ? N21 C22 2.51(3) . . ? N21 N22 2.95(2) . . ? N21 C322 2.63(3) . 8 ? N21 H212a 2.263(14) . 8 ? N21 H21a 2.051(13) . . ? N21 H21b 2.039(13) . . ? N21 H322b 1.912(13) . 8 ? Si2 C21 2.61(3) . . ? Si2 C21 2.61(3) . 8 ? Si2 H211a 2.341(4) . 8 ? Si2 H211a 2.341(4) . . ? Si2 H211b 2.352(3) . 8 ? Si2 H211b 2.352(3) . . ? Si2 H211c 2.415(4) . 8 ? Si2 H211c 2.415(4) . . ? Si2 H212a 2.353(2) . . ? Si2 H212a 2.353(2) . 8 ? Si2 H212b 2.343(4) . 8 ? Si2 H212b 2.343(4) . . ? Si2 H212c 2.373(3) . 8 ? Si2 H212c 2.373(3) . . ? Si2 H213a 2.345(3) . 8 ? Si2 H213a 2.345(3) . . ? Si2 H213b 2.343(2) . 8 ? Si2 H213b 2.343(2) . . ? Si2 H213c 2.425(4) . . ? Si2 H213c 2.425(4) . 8 ? Si2 H21b 2.578(2) . . ? Si2 H21b 2.578(2) . 8 ? C211 C213 2.23(3) . 8 ? C211 C213 2.99(4) . . ? C211 C21 2.56(4) . 8 ? C211 H211b 2.41(4) . 8 ? C211 H211c 2.13(4) . 8 ? C211 H213b 1.98(3) . 8 ? C211 H21b 2.15(3) . 8 ? C212 C212 2.60(4) . 8 ? C212 C213 2.95(4) . . ? C212 C21 3.00(4) . 8 ? C212 H113a 1.70(3) . 8 ? C212 H113b 2.47(2) . 8 ? C212 H212b 2.33(3) . 8 ? C212 H213b 1.97(2) . 8 ? C212 H213c 2.14(2) . 8 ? C213 C213 2.61(4) . 8 ? C213 H211c 1.95(3) . 8 ? C213 H212a 1.95(3) . 8 ? C213 H212b 2.23(3) . 8 ? C213 H213c 2.46(3) . 8 ? C21 N22 2.28(3) . . ? C21 C222 2.90(4) . . ? C21 C32 2.54(6) . 8 ? C21 N32 2.50(3) . 8 ? C21 H211b 1.89(3) . 8 ? C21 H22a 2.09(3) . . ? C21 H22b 2.08(3) . . ? C21 H222a 2.48(3) . . ? C21 H32b 1.97(3) . 8 ? C21 H322a 2.09(3) . 8 ? C21 H322c 2.17(3) . 8 ? C22 C221 2.13(4) . . ? C22 C222 2.56(4) . . ? C22 N31 2.60(3) . 8 ? C22 C321 2.74(4) . 8 ? C22 H21a 2.02(3) . . ? C22 H21b 2.03(3) . . ? C22 H221a 2.35(3) . . ? C22 H221b 2.35(3) . . ? C22 H31b 1.97(3) . 8 ? C22 H32a 1.88(3) . 8 ? C22 H322a 1.90(3) . 8 ? C22 H322b 1.53(3) . 8 ? C22 H322c 2.43(3) . 8 ? N22 C31 2.88(3) . 8 ? N22 H21a 2.134(15) . . ? N22 H22a 2.191(17) . . ? N22 H22b 2.191(16) . . ? N22 H221a 2.249(16) . . ? N22 H221b 2.249(13) . . ? N22 H221c 1.791(16) . . ? N22 H222a 1.586(12) . . ? N22 H222b 1.587(15) . . ? N22 H222c 1.899(16) . . ? N22 H32a 2.083(15) . 8 ? N22 H32b 1.773(17) . 8 ? N22 H321a 2.080(16) . 8 ? N22 H321b 1.673(17) . 8 ? N22 H321c 1.894(17) . 8 ? N22 H322a 1.818(13) . 8 ? N22 H322b 1.895(16) . 8 ? C221 C222 2.33(4) . . ? C221 C31 2.36(4) . 8 ? C221 C322 2.64(4) . 8 ? C221 H22a 2.33(3) . . ? C221 H22b 2.24(3) . . ? C221 H222b 2.28(3) . . ? C221 H32b 1.94(3) . 8 ? C221 H321b 1.81(3) . 8 ? C221 H321c 2.40(3) . 8 ? C222 C32 2.62(6) . 8 ? C222 H21a 2.37(3) . . ? C222 H221c 2.07(3) . . ? C222 H321a 2.18(3) . 8 ? C222 H322a 1.83(3) . 8 ? C222 H322b 2.35(4) . 8 ? N31 C311 2.97(4) . . ? N31 C312 2.93(3) . . ? N31 C313 2.91(4) . . ? N31 C32 2.35(5) . . ? N31 N32 2.87(2) . . ? N31 H112b 2.404(15) . 8 ? N31 H113a 2.297(16) . 8 ? N31 H22b 1.716(14) . 8 ? N31 H221b 2.454(16) . 8 ? N31 H31a 1.950(15) . . ? N31 H31b 1.943(15) . . ? Si3 C31 2.54(2) . . ? Si3 H111a 2.122(7) . 8 ? Si3 H111b 2.315(7) . 8 ? Si3 H111c 2.312(7) . 8 ? Si3 H112a 2.587(7) . 8 ? Si3 H112b 2.591(7) . 8 ? Si3 H112c 2.640(7) . 8 ? Si3 H113a 2.404(7) . 8 ? Si3 H113b 2.196(8) . 8 ? Si3 H113c 2.253(8) . 8 ? Si3 H11a 2.544(8) . 8 ? Si3 H31a 2.609(8) . . ? Si3 H31b 2.698(7) . . ? Si3 H311a 2.302(8) . . ? Si3 H311b 2.304(7) . . ? Si3 H311c 2.402(8) . . ? Si3 H312a 2.342(7) . . ? Si3 H312b 2.342(8) . . ? Si3 H312c 2.361(7) . . ? Si3 H313a 2.241(7) . . ? Si3 H313b 2.239(7) . . ? Si3 H313c 2.311(7) . . ? C311 C312 2.83(5) . . ? C311 C313 2.89(6) . . ? C311 H111c 2.36(4) . 8 ? C311 H112c 2.20(4) . 8 ? C311 H113a 2.10(4) . 8 ? C311 H113b 2.14(5) . 8 ? C312 C313 2.86(5) . . ? C312 H111b 1.52(3) . 8 ? C312 H111c 2.08(4) . 8 ? C312 H112a 1.64(3) . 8 ? C312 H112c 2.26(3) . 8 ? C312 H11a 1.94(4) . 8 ? C312 H311c 2.50(4) . 2 ? C313 C313 2.21(5) . 8 ? C313 H111b 2.23(4) . 8 ? C313 H111c 2.43(4) . 8 ? C313 H113b 2.24(4) . 8 ? C313 H313a 1.96(4) . 8 ? C313 H313b 1.76(4) . 8 ? C31 N32 2.46(3) . . ? C31 H112a 2.42(2) . 8 ? C31 H22a 2.16(2) . 8 ? C31 H221b 1.83(3) . 8 ? C31 H32a 1.88(3) . . ? C31 H32b 1.88(2) . . ? C32 C321 2.27(7) . . ? C32 C322 2.21(5) . . ? C32 H221a 1.54(6) . 8 ? C32 H221c 2.09(6) . 8 ? C32 H31a 1.97(5) . . ? C32 H31b 1.97(6) . . ? C32 H321a 2.49(6) . . ? C32 H321b 2.50(6) . . ? C32 H322a 2.47(5) . . ? C32 H322b 2.48(5) . . ? N32 H22a 2.181(15) . 8 ? N32 H22b 1.908(15) . 8 ? N32 H221a 1.985(16) . 8 ? N32 H221b 1.709(12) . 8 ? N32 H221c 1.517(15) . 8 ? N32 H222a 2.148(11) . 8 ? N32 H222b 1.968(12) . 8 ? N32 H222c 2.274(13) . 8 ? N32 H32a 1.708(16) . . ? N32 H32b 1.702(15) . . ? N32 H321a 1.863(15) . . ? N32 H321b 1.861(14) . . ? N32 H321c 2.050(15) . . ? N32 H322a 2.238(11) . . ? N32 H322b 2.234(13) . . ? N32 H322c 2.009(11) . . ? C321 C322 2.33(4) . . ? C321 H221a 1.99(6) . 8 ? C321 H221b 2.23(4) . 8 ? C321 H222a 2.22(4) . 8 ? C321 H222c 1.52(5) . 8 ? C321 H32a 2.18(5) . . ? C321 H322c 2.29(4) . . ? C322 H21b 2.23(3) . 8 ? C322 H22a 1.96(3) . 8 ? C322 H22b 2.45(2) . 8 ? C322 H222b 1.73(3) . 8 ? C322 H222c 2.33(3) . 8 ? C322 H32b 1.76(3) . . ? C322 H321b 2.22(3) . . ? H111a H111b 1.5513(6) . . ? H111a H111c 1.5422(4) . . ? H111a H313a 1.6189(5) . 8 ? H111a H313b 1.9343(5) . 8 ? H111b H111c 1.5422(9) . . ? H111b H312b 1.5795(8) . 8 ? H111b H312c 1.1643(3) . 8 ? H111c H311c 1.9140(6) . 8 ? H111c H312c 1.4479(9) . 8 ? H111c H313c 1.9807(6) . 8 ? H112a H112b 1.5514(5) . . ? H112a H112c 1.5274(9) . . ? H112a H31a 1.5492(4) . 8 ? H112b H112c 1.5274(4) . . ? H112b H31a 1.1004(5) . 8 ? H112b H31b 1.2297(3) . 8 ? H112c H311b 1.5695(6) . 8 ? H112c H312a 1.6668(6) . 8 ? H113a H113b 1.5512(4) . . ? H113a H113c 1.5607(4) . . ? H113a H212a 1.1626(4) . 8 ? H113a H212b 1.6214(4) . 8 ? H113a H311a 1.5337(4) . 8 ? H113b H113c 1.5607(4) . . ? H113b H212b 1.6901(5) . 8 ? H113b H311a 1.5912(4) . 8 ? H113b H313b 1.7102(4) . 8 ? H113c H311b 1.5550(4) . 8 ? H113c H311c 1.4897(4) . 8 ? H11a H11b 1.5512(4) . . ? H11a H121b 1.8500(5) . 8 ? H11a H121c 1.5845(7) . 8 ? H11a H312b 1.2265(4) . 8 ? H11b H11b 1.9476(6) . 8 ? H11b H121b 1.7578(5) . . ? H11b H121c 1.9179(7) . 8 ? H11b H313a 1.9963(13) . 8 ? H12a H12b 1.5513(5) . . ? H12a H121c 1.0326(4) . 8 ? H12a H122c 1.3646(5) . 8 ? H12b H121b 1.9662(12) . 8 ? H12b H121c 1.2801(6) . 8 ? H12b H122b 1.7787(6) . 8 ? H121a H121a 1.7175(5) . 8 ? H121a H121b 1.5513(10) . . ? H121a H121c 1.5609(4) . . ? H121b H121b 1.3252(4) . 8 ? H121b H121c 1.5610(4) . . ? H122a H122b 1.4489(5) . 8 ? H122a H122b 1.5512(5) . . ? H122a H122c 1.2352(3) . 8 ? H122a H122c 1.5438(4) . . ? H122b H122c 1.5439(4) . . ? H211a H211b 1.9500(5) . 8 ? H211a H211b 1.5513(4) . . ? H211a H211c 1.8430(6) . 8 ? H211a H211c 1.5406(7) . . ? H211b H211c 1.5405(9) . . ? H211b H213b 1.9789(11) . 8 ? H211b H21a 1.9537(12) . 8 ? H211b H21b 1.3236(3) . 8 ? H211c H213b 1.5507(4) . 8 ? H212a H212b 1.5514(4) . . ? H212a H212c 1.5476(9) . . ? H212a H213a 1.4631(8) . 8 ? H212b H212b 1.7172(5) . 8 ? H212b H212c 1.5476(4) . . ? H212b H213a 1.6140(4) . 8 ? H212c H213b 1.6758(5) . 8 ? H212c H213c 1.5282(4) . 8 ? H213a H213b 1.5514(5) . . ? H213a H213c 1.5394(4) . . ? H213b H213c 1.5394(6) . . ? H213c H213c 1.9731(6) . 8 ? H21a H21b 1.5513(8) . . ? H21a H222a 1.7147(12) . . ? H21a H322a 1.6284(5) . 8 ? H21a H322c 1.4344(9) . 8 ? H21b H322b 1.3581(8) . 8 ? H22a H22b 1.5513(4) . . ? H22a H32a 1.8393(7) . 8 ? H22a H322a 1.7930(5) . 8 ? H22b H31a 1.9291(5) . 8 ? H22b H31b 1.2578(4) . 8 ? H22b H32a 1.8957(10) . 8 ? H22b H32b 1.2003(3) . 8 ? H221a H221b 1.5513(4) . . ? H221a H221c 1.6104(4) . . ? H221a H32b 1.9500(10) . 8 ? H221a H321a 1.8756(6) . 8 ? H221a H321b 1.9019(4) . 8 ? H221b H221c 1.6103(7) . . ? H221b H31a 1.8076(8) . 8 ? H221b H32a 1.0732(3) . 8 ? H221b H321a 1.9512(9) . 8 ? H221c H32a 1.7733(8) . 8 ? H221c H321b 1.5118(5) . 8 ? H221c H321c 1.6384(4) . 8 ? H222a H222b 1.5513(4) . . ? H222a H222c 1.4767(9) . . ? H222a H322a 1.6391(4) . 8 ? H222a H322b 1.8816(11) . 8 ? H222b H222c 1.4768(4) . . ? H222b H321c 1.7471(4) . 8 ? H222b H322a 1.5485(10) . 8 ? H222b H322c 1.7168(6) . 8 ? H222c H321b 1.6428(5) . 8 ? H222c H322c 1.7082(11) . 8 ? H31a H31b 1.5513(6) . . ? H31a H32a 1.9740(7) . . ? H31b H32b 1.9889(7) . . ? H311a H311b 1.5513(4) . . ? H311a H311c 1.5352(4) . . ? H311b H311c 1.5351(5) . . ? H312a H312b 1.5512(3) . . ? H312a H312c 1.5481(5) . . ? H312b H312c 1.5481(8) . . ? H313a H313a 1.3395(4) . 8 ? H313a H313b 1.9228(6) . 8 ? H313a H313b 1.5513(7) . . ? H313a H313c 1.5398(8) . . ? H313b H313c 1.5398(4) . . ? H32a H32b 1.5513(6) . . ? H32b H322a 1.8166(6) . . ? H32b H322b 1.8915(4) . . ? H321a H321b 1.5513(5) . . ? H321a H321c 1.5146(3) . . ? H321b H321c 1.5148(4) . . ? H322a H322b 1.5514(6) . . ? H322a H322c 1.5837(4) . . ? H322b H322c 1.5838(9) . . ? loop_ _geom_angle_atom_site_label_1 #ActaC _geom_angle_atom_site_label_2 #ActaC _geom_angle_atom_site_label_3 #ActaC _geom_angle #ActaC _geom_angle_site_symmetry_1 #ActaC _geom_angle_site_symmetry_2 #ActaC _geom_angle_site_symmetry_3 #ActaC _geom_angle_publ_flag #ActaC N11 Eu N12 72.3(4) . . . ? N11 Eu N21 108.5(5) . . . ? N11 Eu N22 95.7(5) . . . ? N11 Eu N31 106.8(5) . . . ? N11 Eu N32 155.5(4) . . . ? N11 Eu N11 82.6(5) . . 8 ? N11 Eu N21 129.6(5) . . 8 ? N11 Eu N22 162.1(5) . . 8 ? N11 Eu N31 28.0(5) . . 8 ? N11 Eu N32 85.4(4) . . 8 ? N12 Eu N21 158.1(4) . . . ? N12 Eu N22 90.1(4) . . . ? N12 Eu N31 93.2(4) . . . ? N12 Eu N32 83.6(3) . . . ? N12 Eu N11 72.3(4) . . 8 ? N12 Eu N21 158.1(4) . . 8 ? N12 Eu N22 90.1(4) . . 8 ? N12 Eu N31 93.2(4) . . 8 ? N12 Eu N32 83.6(3) . . 8 ? N21 Eu N22 68.0(5) . . . ? N21 Eu N31 107.0(5) . . . ? N21 Eu N32 95.6(4) . . . ? N21 Eu N11 129.6(5) . . 8 ? N21 Eu N21 28.0(5) . . 8 ? N21 Eu N22 86.4(4) . . 8 ? N21 Eu N31 82.2(5) . . 8 ? N21 Eu N32 74.7(4) . . 8 ? N22 Eu N31 157.3(5) . . . ? N22 Eu N32 89.2(4) . . . ? N22 Eu N11 162.1(5) . . 8 ? N22 Eu N21 86.4(4) . . 8 ? N22 Eu N22 80.5(4) . . 8 ? N22 Eu N31 77.1(5) . . 8 ? N22 Eu N32 10.8(4) . . 8 ? N31 Eu N32 68.9(5) . . . ? N31 Eu N11 28.0(5) . . 8 ? N31 Eu N21 82.2(5) . . 8 ? N31 Eu N22 77.1(5) . . 8 ? N31 Eu N31 125.1(5) . . 8 ? N31 Eu N32 165.9(5) . . 8 ? N32 Eu N11 85.4(4) . . 8 ? N32 Eu N21 74.7(4) . . 8 ? N32 Eu N22 10.8(4) . . 8 ? N32 Eu N31 165.9(5) . . 8 ? N32 Eu N32 97.1(4) . . 8 ? N11 Eu N21 108.5(5) 8 . 8 ? N11 Eu N22 95.7(5) 8 . 8 ? N11 Eu N31 106.8(5) 8 . 8 ? N11 Eu N32 155.5(4) 8 . 8 ? N21 Eu N22 68.0(5) 8 . 8 ? N21 Eu N31 107.0(5) 8 . 8 ? N21 Eu N32 95.6(4) 8 . 8 ? N22 Eu N31 157.3(5) 8 . 8 ? N22 Eu N32 89.2(4) 8 . 8 ? N31 Eu N32 68.9(5) 8 . 8 ? Eu N11 Si1 134.9(7) . . . ? Eu N11 C11 118.6(14) . . . ? Eu N11 N31 81.0(10) . . 8 ? Eu N11 Si3 132.4(7) . . 8 ? Si1 N11 C11 106.4(14) . . . ? Si1 N11 N31 63.1(10) . . 8 ? Si1 N11 Si3 9.3(3) . . 8 ? C11 N11 N31 139.3(18) . . 8 ? C11 N11 Si3 108.3(14) . . 8 ? N31 N11 Si3 67.9(11) 8 . 8 ? N11 Si1 C111 116.5(10) . . . ? N11 Si1 C112 116.8(12) . . . ? N11 Si1 C113 107.9(11) . . . ? N11 Si1 N31 39.7(7) . . 8 ? N11 Si1 Si3 106(2) . . 8 ? N11 Si1 C311 151.3(14) . . 8 ? N11 Si1 C312 107.3(14) . . 8 ? N11 Si1 C313 82.0(14) . . 8 ? C111 Si1 C112 106.1(13) . . . ? C111 Si1 C113 103.9(13) . . . ? C111 Si1 N31 155.8(11) . . 8 ? C111 Si1 Si3 52(2) . . 8 ? C111 Si1 C311 81.7(15) . . 8 ? C111 Si1 C312 55.0(15) . . 8 ? C111 Si1 C313 50.8(14) . . 8 ? C112 Si1 C113 104.2(15) . . . ? C112 Si1 N31 92.9(11) . . 8 ? C112 Si1 Si3 137(2) . . 8 ? C112 Si1 C311 74.8(18) . . 8 ? C112 Si1 C312 62.9(14) . . 8 ? C112 Si1 C313 156.6(15) . . 8 ? C113 Si1 N31 85.2(10) . . 8 ? C113 Si1 Si3 58(2) . . 8 ? C113 Si1 C311 43.9(17) . . 8 ? C113 Si1 C312 144.5(16) . . 8 ? C113 Si1 C313 81.0(16) . . 8 ? N31 Si1 Si3 121(2) 8 . 8 ? N31 Si1 C311 118.4(13) 8 . 8 ? N31 Si1 C312 126.3(14) 8 . 8 ? N31 Si1 C313 110.4(13) 8 . 8 ? Si3 Si1 C311 67(2) 8 . 8 ? Si3 Si1 C312 107(2) 8 . 8 ? Si3 Si1 C313 29(2) 8 . 8 ? C311 Si1 C312 101.3(18) 8 . 8 ? C311 Si1 C313 95.5(19) 8 . 8 ? C312 Si1 C313 99.4(16) 8 . 8 ? Si1 C111 H111a 106(2) . . . ? Si1 C111 H111b 109(2) . . . ? Si1 C111 H111c 115(2) . . . ? Si1 C111 Si3 7.8(4) . . 8 ? Si1 C111 C312 57.6(14) . . 8 ? Si1 C111 C313 67.2(16) . . 8 ? Si1 C111 H312c 89.1(14) . . 8 ? Si1 C111 H313c 98.7(14) . . 8 ? H111a C111 H111b 109(3) . . . ? H111a C111 H111c 108(3) . . . ? H111a C111 Si3 99(2) . . 8 ? H111a C111 C312 152(3) . . 8 ? H111a C111 C313 40.1(18) . . 8 ? H111a C111 H312c 161(2) . . 8 ? H111a C111 H313c 9.3(6) . . 8 ? H111b C111 H111c 109(3) . . . ? H111b C111 Si3 115(2) . . 8 ? H111b C111 C312 63(2) . . 8 ? H111b C111 C313 113(3) . . 8 ? H111b C111 H312c 55.1(15) . . 8 ? H111b C111 H313c 117(2) . . 8 ? H111c C111 Si3 115(2) . . 8 ? H111c C111 C312 100(3) . . 8 ? H111c C111 C313 134(3) . . 8 ? H111c C111 H312c 72.9(18) . . 8 ? H111c C111 H313c 108(3) . . 8 ? Si3 C111 C312 65.4(15) 8 . 8 ? Si3 C111 C313 61.1(16) 8 . 8 ? Si3 C111 H312c 96.5(16) 8 . 8 ? Si3 C111 H313c 91.5(14) 8 . 8 ? C312 C111 C313 116(3) 8 . 8 ? C312 C111 H312c 34.4(13) 8 . 8 ? C312 C111 H313c 150(2) 8 . 8 ? C313 C111 H312c 150(3) 8 . 8 ? C313 C111 H313c 34.4(16) 8 . 8 ? H312c C111 H313c 171(2) 8 . 8 ? Si1 C112 H112a 105(2) . . . ? Si1 C112 H112b 109(2) . . . ? Si1 C112 H112c 118(3) . . . ? Si1 C112 Si3 5.5(3) . . 8 ? Si1 C112 C312 55.1(13) . . 8 ? Si1 C112 C31 72.1(11) . . 8 ? Si1 C112 H31a 86.5(12) . . 8 ? Si1 C112 H312a 81.6(13) . . 8 ? H112a C112 H112b 111(3) . . . ? H112a C112 H112c 104(2) . . . ? H112a C112 Si3 108(2) . . 8 ? H112a C112 C312 59.9(18) . . 8 ? H112a C112 C31 103(2) . . 8 ? H112a C112 H31a 76(2) . . 8 ? H112a C112 H312a 37.1(10) . . 8 ? H112b C112 H112c 110(3) . . . ? H112b C112 Si3 112(2) . . 8 ? H112b C112 C312 152(3) . . 8 ? H112b C112 C31 41.3(14) . . 8 ? H112b C112 H31a 48.8(16) . . 8 ? H112b C112 H312a 147(4) . . 8 ? H112c C112 Si3 113(2) . . 8 ? H112c C112 C312 99(2) . . 8 ? H112c C112 C31 146(3) . . 8 ? H112c C112 H31a 153(3) . . 8 ? H112c C112 H312a 91(2) . . 8 ? Si3 C112 C312 54.8(13) 8 . 8 ? Si3 C112 C31 76.3(11) 8 . 8 ? Si3 C112 H31a 91.9(12) 8 . 8 ? Si3 C112 H312a 81.8(12) 8 . 8 ? C312 C112 C31 111.6(18) 8 . 8 ? C312 C112 H31a 104(2) 8 . 8 ? C312 C112 H312a 27.1(12) 8 . 8 ? C31 C112 H31a 28.5(9) 8 . 8 ? C31 C112 H312a 123(2) 8 . 8 ? H31a C112 H312a 103(2) 8 . 8 ? Si1 C113 H113a 110.6(17) . . . ? Si1 C113 H113b 108(2) . . . ? Si1 C113 H113c 107(2) . . . ? Si1 C113 Si3 8.2(3) . . 8 ? Si1 C113 C311 67(2) . . 8 ? Si1 C113 H311a 109(3) . . 8 ? H113a C113 H113b 110(3) . . . ? H113a C113 H113c 110(3) . . . ? H113a C113 Si3 118.0(17) . . 8 ? H113a C113 C311 121(4) . . 8 ? H113a C113 H311a 106(3) . . 8 ? H113b C113 H113c 111(2) . . . ? H113b C113 Si3 102(2) . . 8 ? H113b C113 C311 127(3) . . 8 ? H113b C113 H311a 113(2) . . 8 ? H113c C113 Si3 106(2) . . 8 ? H113c C113 C311 40(2) . . 8 ? H113c C113 H311a 4.24(14) . . 8 ? Si3 C113 C311 67(2) 8 . 8 ? Si3 C113 H311a 109(3) 8 . 8 ? C311 C113 H311a 42(2) 8 . 8 ? N11 C11 C12 116(2) . . . ? N11 C11 H11a 108(2) . . . ? N11 C11 H11b 112(3) . . . ? N11 C11 C121 124(2) . . 8 ? N11 C11 H121b 115(2) . . 8 ? N11 C11 H121c 116.2(18) . . 8 ? C12 C11 H11a 104(3) . . . ? C12 C11 H11b 105(3) . . . ? C12 C11 C121 22.0(16) . . 8 ? C12 C11 H121b 66.4(19) . . 8 ? C12 C11 H121c 18.1(11) . . 8 ? H11a C11 H11b 111(2) . . . ? H11a C11 C121 116(3) . . 8 ? H11a C11 H121b 136(3) . . 8 ? H11a C11 H121c 88(2) . . 8 ? H11b C11 C121 84(2) . . 8 ? H11b C11 H121b 42.4(11) . . 8 ? H11b C11 H121c 119(3) . . 8 ? C121 C11 H121b 44.8(17) 8 . 8 ? C121 C11 H121c 38.6(16) 8 . 8 ? H121b C11 H121c 83(2) 8 . 8 ? C11 C12 N12 111(2) . . . ? C11 C12 H12a 119(3) . . . ? C11 C12 H12b 119(2) . . . ? C11 C12 C121 68(4) . . 8 ? C11 C12 C122 155(2) . . 8 ? C11 C12 H121a 95(2) . . 8 ? C11 C12 H121b 39.3(13) . . 8 ? C11 C12 H121c 50(3) . . 8 ? N12 C12 H12a 103(2) . . . ? N12 C12 H12b 104(2) . . . ? N12 C12 C121 73(4) . . 8 ? N12 C12 C122 46.2(18) . . 8 ? N12 C12 H121a 92.6(18) . . 8 ? N12 C12 H121b 84.6(16) . . 8 ? N12 C12 H121c 149(4) . . 8 ? H12a C12 H12b 98(3) . . . ? H12a C12 C121 172(6) . . 8 ? H12a C12 C122 67(2) . . 8 ? H12a C12 H121a 132(3) . . 8 ? H12a C12 H121b 157(3) . . 8 ? H12a C12 H121c 75(3) . . 8 ? H12b C12 C121 78(4) . . 8 ? H12b C12 C122 82(2) . . 8 ? H12b C12 H121a 34.6(8) . . 8 ? H12b C12 H121b 101.0(19) . . 8 ? H12b C12 H121c 107(4) . . 8 ? C121 C12 C122 107(5) 8 . 8 ? C121 C12 H121a 43(3) 8 . 8 ? C121 C12 H121b 30(4) 8 . 8 ? C121 C12 H121c 112(6) 8 . 8 ? C122 C12 H121a 97(2) 8 . 8 ? C122 C12 H121b 129(2) 8 . 8 ? C122 C12 H121c 141(4) 8 . 8 ? H121a C12 H121b 67.3(13) 8 . 8 ? H121a C12 H121c 112(3) 8 . 8 ? H121b C12 H121c 87(4) 8 . 8 ? Eu N12 C12 99.8(14) . . . ? Eu N12 C121 103.1(12) . . . ? Eu N12 C122 124.6(14) . . . ? Eu N12 C12 99.8(14) . . 8 ? Eu N12 C121 103.1(12) . . 8 ? Eu N12 C122 124.6(14) . . 8 ? C12 N12 C121 103.9(18) . . . ? C12 N12 C122 121(3) . . . ? C12 N12 C12 127.2(17) . . 8 ? C12 N12 C121 23.6(17) . . 8 ? C12 N12 C122 84(3) . . 8 ? C121 N12 C122 101(2) . . . ? C121 N12 C12 23.6(17) . . 8 ? C121 N12 C121 80(2) . . 8 ? C121 N12 C122 130(2) . . 8 ? C122 N12 C12 84(3) . . 8 ? C122 N12 C121 130(2) . . 8 ? C122 N12 C122 40(3) . . 8 ? C12 N12 C121 103.9(18) 8 . 8 ? C12 N12 C122 121(3) 8 . 8 ? C121 N12 C122 101(2) 8 . 8 ? N12 C121 H121a 114(3) . . . ? N12 C121 H121b 109(3) . . . ? N12 C121 H121c 110(2) . . . ? N12 C121 C11 122(2) . . 8 ? N12 C121 C12 84(4) . . 8 ? N12 C121 C121 49.8(14) . . 8 ? N12 C121 H12b 106(2) . . 8 ? H121a C121 H121b 103(2) . . . ? H121a C121 H121c 113(3) . . . ? H121a C121 C11 122(3) . . 8 ? H121a C121 C12 112(5) . . 8 ? H121a C121 C121 87(2) . . 8 ? H121a C121 H12b 42.1(12) . . 8 ? H121b C121 H121c 106(3) . . . ? H121b C121 C11 45.1(16) . . 8 ? H121b C121 C12 133(5) . . 8 ? H121b C121 C121 76(2) . . 8 ? H121b C121 H12b 140(3) . . 8 ? H121c C121 C11 61(2) . . 8 ? H121c C121 C12 32(4) . . 8 ? H121c C121 C121 158(3) . . 8 ? H121c C121 H12b 80(2) . . 8 ? C11 C121 C12 90(5) 8 . 8 ? C11 C121 C121 117(2) 8 . 8 ? C11 C121 H12b 126(3) 8 . 8 ? C12 C121 C121 133(5) 8 . 8 ? C12 C121 H12b 70(4) 8 . 8 ? C121 C121 H12b 113(2) 8 . 8 ? N12 C122 H122a 109(4) . . . ? N12 C122 H122b 108(3) . . . ? N12 C122 H122c 118(3) . . . ? N12 C122 C12 49.5(14) . . 8 ? N12 C122 C122 70(3) . . 8 ? N12 C122 H122a 123(5) . . 8 ? N12 C122 H122b 90(3) . . 8 ? H122a C122 H122b 103(3) . . . ? H122a C122 H122c 109(3) . . . ? H122a C122 C12 158(3) . . 8 ? H122a C122 C122 49(3) . . 8 ? H122a C122 H122a 17.9(13) . . 8 ? H122a C122 H122b 74(3) . . 8 ? H122b C122 H122c 107(5) . . . ? H122b C122 C12 91(2) . . 8 ? H122b C122 C122 90(4) . . 8 ? H122b C122 H122a 107(3) . . 8 ? H122b C122 H122b 43.1(18) . . 8 ? H122c C122 C12 81(3) . . 8 ? H122c C122 C122 156(4) . . 8 ? H122c C122 H122a 92(3) . . 8 ? H122c C122 H122b 147(3) . . 8 ? C12 C122 C122 116(3) 8 . 8 ? C12 C122 H122a 163(3) 8 . 8 ? C12 C122 H122b 107.8(18) 8 . 8 ? C122 C122 H122a 67(4) 8 . 8 ? C122 C122 H122b 47(3) 8 . 8 ? H122a C122 H122b 87(4) 8 . 8 ? Eu N21 Si2 136.4(7) . . . ? Eu N21 C21 113.5(13) . . . ? Eu N21 N21 76.0(10) . . 8 ? Si2 N21 C21 110.0(13) . . . ? Si2 N21 N21 71.0(10) . . 8 ? C21 N21 N21 143.7(17) . . 8 ? N21 Si2 C211 112.6(9) . . . ? N21 Si2 C212 111.2(9) . . . ? N21 Si2 C213 115.0(10) . . . ? N21 Si2 N21 38.0(6) . . 8 ? N21 Si2 C211 97.0(9) . . 8 ? N21 Si2 C212 84.8(9) . . 8 ? N21 Si2 C213 151.3(9) . . 8 ? C211 Si2 C212 107.3(13) . . . ? C211 Si2 C213 105.9(12) . . . ? C211 Si2 N21 97.0(9) . . 8 ? C211 Si2 C211 47.7(15) . . 8 ? C211 Si2 C212 149.2(12) . . 8 ? C211 Si2 C213 73.1(12) . . 8 ? C212 Si2 C213 104.3(11) . . . ? C212 Si2 N21 84.8(9) . . 8 ? C212 Si2 C211 149.2(12) . . 8 ? C212 Si2 C212 88.1(12) . . 8 ? C212 Si2 C213 43.5(11) . . 8 ? C213 Si2 N21 151.3(9) . . 8 ? C213 Si2 C211 73.1(12) . . 8 ? C213 Si2 C212 43.5(11) . . 8 ? C213 Si2 C213 88.6(12) . . 8 ? N21 Si2 C211 112.6(9) 8 . 8 ? N21 Si2 C212 111.2(9) 8 . 8 ? N21 Si2 C213 115.0(10) 8 . 8 ? C211 Si2 C212 107.3(13) 8 . 8 ? C211 Si2 C213 105.9(12) 8 . 8 ? C212 Si2 C213 104.3(11) 8 . 8 ? Si2 C211 H211a 112(3) . . . ? Si2 C211 H211b 105.0(16) . . . ? Si2 C211 H211c 109.6(17) . . . ? Si2 C211 C211 66.2(14) . . 8 ? Si2 C211 H211a 97(2) . . 8 ? H211a C211 H211b 115(3) . . . ? H211a C211 H211c 113(2) . . . ? H211a C211 C211 50(2) . . 8 ? H211a C211 H211a 16.7(10) . . 8 ? H211b C211 H211c 101(3) . . . ? H211b C211 C211 146(2) . . 8 ? H211b C211 H211a 128(2) . . 8 ? H211c C211 C211 114(3) . . 8 ? H211c C211 H211a 116(2) . . 8 ? C211 C211 H211a 33.2(13) 8 . 8 ? Si2 C212 H212a 109.9(19) . . . ? Si2 C212 H212b 106(2) . . . ? Si2 C212 H212c 112(2) . . . ? Si2 C212 C213 68.1(16) . . 8 ? Si2 C212 H213a 111(2) . . 8 ? H212a C212 H212b 107(2) . . . ? H212a C212 H212c 113(3) . . . ? H212a C212 C213 113(3) . . 8 ? H212a C212 H213a 106(3) . . 8 ? H212b C212 H212c 108(2) . . . ? H212b C212 C213 139(3) . . 8 ? H212b C212 H213a 117(2) . . 8 ? H212c C212 C213 47.9(15) . . 8 ? H212c C212 H213a 9.6(3) . . 8 ? C213 C212 H213a 43.7(15) 8 . 8 ? Si2 C213 H213a 108(2) . . . ? Si2 C213 H213b 109(2) . . . ? Si2 C213 H213c 115(2) . . . ? Si2 C213 C212 68.4(16) . . 8 ? Si2 C213 H212c 106.7(19) . . 8 ? H213a C213 H213b 109(3) . . . ? H213a C213 H213c 107(2) . . . ? H213a C213 C212 40.4(14) . . 8 ? H213a C213 H212c 8.0(2) . . 8 ? H213b C213 H213c 109(3) . . . ? H213b C213 C212 115(3) . . 8 ? H213b C213 H212c 117(3) . . 8 ? H213c C213 C212 132(3) . . 8 ? H213c C213 H212c 101(2) . . 8 ? C212 C213 H212c 41.7(14) 8 . 8 ? N21 C21 C22 113(2) . . . ? N21 C21 H21a 110(3) . . . ? N21 C21 H21b 112(2) . . . ? N21 C21 C322 121(2) . . 8 ? N21 C21 H322b 122(4) . . 8 ? C22 C21 H21a 105(2) . . . ? C22 C21 H21b 108(3) . . . ? C22 C21 C322 62.1(18) . . 8 ? C22 C21 H322b 79(3) . . 8 ? H21a C21 H21b 108(2) . . . ? H21a C21 C322 43.7(14) . . 8 ? H21a C21 H322b 26.8(13) . . 8 ? H21b C21 C322 126(3) . . 8 ? H21b C21 H322b 117(4) . . 8 ? C322 C21 H322b 17.5(17) 8 . 8 ? C21 C22 N22 93(2) . . . ? C21 C22 H22a 113(3) . . . ? C21 C22 H22b 113(2) . . . ? C21 C22 C31 130(2) . . 8 ? C21 C22 C32 157(4) . . 8 ? C21 C22 N32 108(2) . . 8 ? C21 C22 C322 59.4(18) . . 8 ? C21 C22 H32b 137(4) . . 8 ? N22 C22 H22a 114(2) . . . ? N22 C22 H22b 114(2) . . . ? N22 C22 C31 112.2(18) . . 8 ? N22 C22 C32 71(3) . . 8 ? N22 C22 N32 20.3(7) . . 8 ? N22 C22 C322 44.5(12) . . 8 ? N22 C22 H32b 95(3) . . 8 ? H22a C22 H22b 110(3) . . . ? H22a C22 C31 96(2) . . 8 ? H22a C22 C32 89(3) . . 8 ? H22a C22 N32 117(2) . . 8 ? H22a C22 C322 99(2) . . 8 ? H22a C22 H32b 26.9(16) . . 8 ? H22b C22 C31 17.2(12) . . 8 ? H22b C22 C32 63(3) . . 8 ? H22b C22 N32 95(2) . . 8 ? H22b C22 C322 151(3) . . 8 ? H22b C22 H32b 102(4) . . 8 ? C31 C22 C32 50(3) 8 . 8 ? C31 C22 N32 91.9(17) 8 . 8 ? C31 C22 C322 156(2) 8 . 8 ? C31 C22 H32b 86(3) 8 . 8 ? C32 C22 N32 52(3) 8 . 8 ? C32 C22 C322 112(4) 8 . 8 ? C32 C22 H32b 63(4) 8 . 8 ? N32 C22 C322 64.8(14) 8 . 8 ? N32 C22 H32b 93(3) 8 . 8 ? C322 C22 H32b 100(3) 8 . 8 ? Eu N22 C22 83.7(12) . . . ? Eu N22 C221 100.5(10) . . . ? Eu N22 C222 126(2) . . . ? Eu N22 C32 85.0(18) . . 8 ? Eu N22 N32 64(2) . . 8 ? Eu N22 C321 117(2) . . 8 ? Eu N22 C322 107.8(17) . . 8 ? Eu N22 H322c 102.0(8) . . 8 ? C22 N22 C221 80.8(16) . . . ? C22 N22 C222 140(2) . . . ? C22 N22 C32 38(2) . . 8 ? C22 N22 N32 75(2) . . 8 ? C22 N22 C321 134(3) . . 8 ? C22 N22 C322 65.5(18) . . 8 ? C22 N22 H322c 104.1(14) . . 8 ? C221 N22 C222 114(2) . . . ? C221 N22 C32 43(2) . . 8 ? C221 N22 N32 37(2) . . 8 ? C221 N22 C321 56(3) . . 8 ? C221 N22 C322 132(2) . . 8 ? C221 N22 H322c 157.3(14) . . 8 ? C222 N22 C32 148(3) . . 8 ? C222 N22 N32 140(3) . . 8 ? C222 N22 C321 62(3) . . 8 ? C222 N22 C322 78(2) . . 8 ? C222 N22 H322c 48.5(18) . . 8 ? C32 N22 N32 41(3) 8 . 8 ? C32 N22 C321 100(3) 8 . 8 ? C32 N22 C322 101(3) 8 . 8 ? C32 N22 H322c 142(2) 8 . 8 ? N32 N22 C321 79(3) 8 . 8 ? N32 N22 C322 140(3) 8 . 8 ? N32 N22 H322c 166(3) 8 . 8 ? C321 N22 C322 132(2) 8 . 8 ? C321 N22 H322c 110(2) 8 . 8 ? C322 N22 H322c 40.4(15) 8 . 8 ? N22 C221 H221a 116(2) . . . ? N22 C221 H221b 117(2) . . . ? N22 C221 H221c 81.3(16) . . . ? N22 C221 C32 67(3) . . 8 ? N22 C221 N32 15.6(8) . . 8 ? N22 C221 C321 50.6(18) . . 8 ? N22 C221 H32a 109(3) . . 8 ? N22 C221 H321a 86.9(14) . . 8 ? H221a C221 H221b 110(2) . . . ? H221a C221 H221c 115(3) . . . ? H221a C221 C32 90(3) . . 8 ? H221a C221 N32 128(3) . . 8 ? H221a C221 C321 111(3) . . 8 ? H221a C221 H32a 47.9(12) . . 8 ? H221a C221 H321a 109(3) . . 8 ? H221b C221 H221c 115(3) . . . ? H221b C221 C32 73(3) . . 8 ? H221b C221 N32 101(2) . . 8 ? H221b C221 C321 138(3) . . 8 ? H221b C221 H32a 74(2) . . 8 ? H221b C221 H321a 116(2) . . 8 ? H221c C221 C32 146(3) . . 8 ? H221c C221 N32 85.2(18) . . 8 ? H221c C221 C321 34.3(16) . . 8 ? H221c C221 H32a 162(3) . . 8 ? H221c C221 H321a 6.8(5) . . 8 ? C32 C221 N32 61(3) 8 . 8 ? C32 C221 C321 117(3) 8 . 8 ? C32 C221 H32a 49(3) 8 . 8 ? C32 C221 H321a 153(3) 8 . 8 ? N32 C221 C321 60(2) 8 . 8 ? N32 C221 H32a 109(3) 8 . 8 ? N32 C221 H321a 91.7(17) 8 . 8 ? C321 C221 H32a 145(3) 8 . 8 ? C321 C221 H321a 38.2(15) 8 . 8 ? H32a C221 H321a 155(3) 8 . 8 ? N22 C222 H222a 100(3) . . . ? N22 C222 H222b 100(3) . . . ? N22 C222 H222c 141(4) . . . ? N22 C222 N32 13.6(11) . . 8 ? N22 C222 C321 69(2) . . 8 ? N22 C222 C322 55(2) . . 8 ? N22 C222 H321b 88(2) . . 8 ? N22 C222 H321c 103(2) . . 8 ? N22 C222 H322c 83(3) . . 8 ? H222a C222 H222b 106(3) . . . ? H222a C222 H222c 103(3) . . . ? H222a C222 N32 114(3) . . 8 ? H222a C222 C321 169(4) . . 8 ? H222a C222 C322 53(2) . . 8 ? H222a C222 H321b 139(3) . . 8 ? H222a C222 H321c 142(3) . . 8 ? H222a C222 H322c 17.3(6) . . 8 ? H222b C222 H222c 103(3) . . . ? H222b C222 N32 99(3) . . 8 ? H222b C222 C321 77(3) . . 8 ? H222b C222 C322 88(3) . . 8 ? H222b C222 H321b 33.5(12) . . 8 ? H222b C222 H321c 98(3) . . 8 ? H222b C222 H322c 112(3) . . 8 ? H222c C222 N32 130(3) . . 8 ? H222c C222 C321 86(3) . . 8 ? H222c C222 C322 156(3) . . 8 ? H222c C222 H321b 94(3) . . 8 ? H222c C222 H321c 42.9(14) . . 8 ? H222c C222 H322c 115(3) . . 8 ? N32 C222 C321 56(2) 8 . 8 ? N32 C222 C322 67.8(18) 8 . 8 ? N32 C222 H321b 80.4(18) 8 . 8 ? N32 C222 H321c 90.1(18) 8 . 8 ? N32 C222 H322c 96(2) 8 . 8 ? C321 C222 C322 118(3) 8 . 8 ? C321 C222 H321b 44(3) 8 . 8 ? C321 C222 H321c 45(2) 8 . 8 ? C321 C222 H322c 152(3) 8 . 8 ? C322 C222 H321b 107(3) 8 . 8 ? C322 C222 H321c 158(3) 8 . 8 ? C322 C222 H322c 40.4(17) 8 . 8 ? H321b C222 H321c 70.7(17) 8 . 8 ? H321b C222 H322c 142(3) 8 . 8 ? H321c C222 H322c 147(3) 8 . 8 ? Eu N31 Si3 130.7(8) . . . ? Eu N31 C31 120.1(13) . . . ? Eu N31 N11 71.0(10) . . 8 ? Eu N31 Si1 137.9(9) . . 8 ? Si3 N31 C31 109.0(14) . . . ? Si3 N31 N11 75.5(10) . . 8 ? Si3 N31 Si1 8.6(4) . . 8 ? C31 N31 N11 137.6(18) . . 8 ? C31 N31 Si1 101.9(13) . . 8 ? N11 N31 Si1 77.3(11) 8 . 8 ? N31 Si3 C311 114.7(14) . . . ? N31 Si3 C312 110.5(13) . . . ? N31 Si3 C313 115.1(15) . . . ? N31 Si3 N11 36.6(6) . . 8 ? N31 Si3 Si1 50.3(18) . . 8 ? N31 Si3 C111 155.2(12) . . 8 ? N31 Si3 C112 80.6(10) . . 8 ? N31 Si3 C113 84.9(10) . . 8 ? C311 Si3 C312 101.0(19) . . . ? C311 Si3 C313 109(2) . . . ? C311 Si3 N11 150.4(14) . . 8 ? C311 Si3 Si1 105(2) . . 8 ? C311 Si3 C111 89.4(16) . . 8 ? C311 Si3 C112 71.4(17) . . 8 ? C311 Si3 C113 46.9(18) . . 8 ? C312 Si3 C313 105.3(17) . . . ? C312 Si3 N11 98.5(13) . . 8 ? C312 Si3 Si1 64(2) . . 8 ? C312 Si3 C111 56.1(15) . . 8 ? C312 Si3 C112 56.7(13) . . 8 ? C312 Si3 C113 147.6(17) . . 8 ? C313 Si3 N11 86.8(16) . . 8 ? C313 Si3 Si1 146(3) . . 8 ? C313 Si3 C111 57.6(16) . . 8 ? C313 Si3 C112 160.7(15) . . 8 ? C313 Si3 C113 92.5(18) . . 8 ? N11 Si3 Si1 64.7(19) 8 . 8 ? N11 Si3 C111 120.0(12) 8 . 8 ? N11 Si3 C112 102.0(11) 8 . 8 ? N11 Si3 C113 109.5(11) 8 . 8 ? Si1 Si3 C111 120(2) 8 . 8 ? Si1 Si3 C112 37(2) 8 . 8 ? Si1 Si3 C113 113(2) 8 . 8 ? C111 Si3 C112 103.3(13) 8 . 8 ? C111 Si3 C113 117.7(14) 8 . 8 ? C112 Si3 C113 100.6(15) 8 . 8 ? Si3 C311 H311a 108(3) . . . ? Si3 C311 H311b 111(3) . . . ? Si3 C311 H311c 116(3) . . . ? Si3 C311 Si1 8.7(4) . . 8 ? Si3 C311 C113 66(2) . . 8 ? Si3 C311 H113c 106(4) . . 8 ? H311a C311 H311b 110(4) . . . ? H311a C311 H311c 104(4) . . . ? H311a C311 Si1 111(3) . . 8 ? H311a C311 C113 42(2) . . 8 ? H311a C311 H113c 3.76(18) . . 8 ? H311b C311 H311c 108(5) . . . ? H311b C311 Si1 102(3) . . 8 ? H311b C311 C113 119(4) . . 8 ? H311b C311 H113c 113(4) . . 8 ? H311c C311 Si1 121(3) . . 8 ? H311c C311 C113 128(4) . . 8 ? H311c C311 H113c 103(4) . . 8 ? Si1 C311 C113 69(2) 8 . 8 ? Si1 C311 H113c 110(3) 8 . 8 ? C113 C311 H113c 41(2) 8 . 8 ? Si3 C312 H312a 110(2) . . . ? Si3 C312 H312b 108(3) . . . ? Si3 C312 H312c 110(3) . . . ? Si3 C312 Si1 8.9(4) . . 8 ? Si3 C312 C111 58.5(15) . . 8 ? Si3 C312 C112 68.5(14) . . 8 ? H312a C312 H312b 111(4) . . . ? H312a C312 H312c 110(4) . . . ? H312a C312 Si1 103(2) . . 8 ? H312a C312 C111 146(4) . . 8 ? H312a C312 C112 41.4(16) . . 8 ? H312b C312 H312c 108(3) . . . ? H312b C312 Si1 107(3) . . 8 ? H312b C312 C111 103(3) . . 8 ? H312b C312 C112 129(3) . . 8 ? H312c C312 Si1 118(3) . . 8 ? H312c C312 C111 56(2) . . 8 ? H312c C312 C112 121(3) . . 8 ? Si1 C312 C111 67.4(16) 8 . 8 ? Si1 C312 C112 62.0(13) 8 . 8 ? C111 C312 C112 115(2) 8 . 8 ? Si3 C313 H313a 110(4) . . . ? Si3 C313 H313b 107(3) . . . ? Si3 C313 H313c 115(3) . . . ? Si3 C313 Si1 4.8(4) . . 8 ? Si3 C313 C111 61.3(16) . . 8 ? Si3 C313 H111a 93(2) . . 8 ? H313a C313 H313b 108(4) . . . ? H313a C313 H313c 110(4) . . . ? H313a C313 Si1 106(3) . . 8 ? H313a C313 C111 104(3) . . 8 ? H313a C313 H111a 103(3) . . 8 ? H313b C313 H313c 105(4) . . . ? H313b C313 Si1 109(3) . . 8 ? H313b C313 C111 148(4) . . 8 ? H313b C313 H111a 133(5) . . 8 ? H313c C313 Si1 118(3) . . 8 ? H313c C313 C111 61(2) . . 8 ? H313c C313 H111a 29.0(11) . . 8 ? Si1 C313 C111 62.0(16) 8 . 8 ? Si1 C313 H111a 94(2) 8 . 8 ? C111 C313 H111a 33.2(15) 8 . 8 ? N31 C31 C32 113(3) . . . ? N31 C31 H31a 107.4(19) . . . ? N31 C31 H31b 110(2) . . . ? N31 C31 C112 92.6(15) . . 8 ? N31 C31 C22 105.5(17) . . 8 ? N31 C31 H112b 115.0(17) . . 8 ? N31 C31 H22b 90.5(18) . . 8 ? C32 C31 H31a 108(3) . . . ? C32 C31 H31b 112(3) . . . ? C32 C31 C112 149(3) . . 8 ? C32 C31 C22 35(2) . . 8 ? C32 C31 H112b 131(3) . . 8 ? C32 C31 H22b 49(2) . . 8 ? H31a C31 H31b 106(2) . . . ? H31a C31 C112 44.3(14) . . 8 ? H31a C31 C22 139(2) . . 8 ? H31a C31 H112b 49.4(10) . . 8 ? H31a C31 H22b 156(3) . . 8 ? H31b C31 C112 72.9(17) . . 8 ? H31b C31 C22 83.7(17) . . 8 ? H31b C31 H112b 57.4(12) . . 8 ? H31b C31 H22b 81.8(18) . . 8 ? C112 C31 C22 154.4(18) 8 . 8 ? C112 C31 H112b 24.5(8) 8 . 8 ? C112 C31 H22b 154(2) 8 . 8 ? C22 C31 H112b 130.8(17) 8 . 8 ? C22 C31 H22b 16.7(11) 8 . 8 ? H112b C31 H22b 137(2) 8 . 8 ? C31 C32 N32 135(4) . . . ? C31 C32 H32a 105(4) . . . ? C31 C32 H32b 103(5) . . . ? C31 C32 C22 95(4) . . 8 ? C31 C32 N22 143(4) . . 8 ? C31 C32 C221 127(4) . . 8 ? C31 C32 H22a 100(4) . . 8 ? C31 C32 H22b 44(2) . . 8 ? C31 C32 H221b 84(3) . . 8 ? N32 C32 H32a 102(5) . . . ? N32 C32 H32b 99(4) . . . ? N32 C32 C22 85(4) . . 8 ? N32 C32 N22 17.4(10) . . 8 ? N32 C32 C221 61(3) . . 8 ? N32 C32 H22a 109(3) . . 8 ? N32 C32 H22b 111(4) . . 8 ? N32 C32 H221b 83(3) . . 8 ? H32a C32 H32b 111(5) . . . ? H32a C32 C22 142(5) . . 8 ? H32a C32 N22 107(5) . . 8 ? H32a C32 C221 43(3) . . 8 ? H32a C32 H22a 102(4) . . 8 ? H32a C32 H22b 146(6) . . 8 ? H32a C32 H221b 54(3) . . 8 ? H32b C32 C22 31(2) . . 8 ? H32b C32 N22 82(3) . . 8 ? H32b C32 C221 126(5) . . 8 ? H32b C32 H22a 11.9(10) . . 8 ? H32b C32 H22b 73(4) . . 8 ? H32b C32 H221b 165(5) . . 8 ? C22 C32 N22 71(3) 8 . 8 ? C22 C32 C221 137(5) 8 . 8 ? C22 C32 H22a 42(2) 8 . 8 ? C22 C32 H22b 53(3) 8 . 8 ? C22 C32 H221b 162(5) 8 . 8 ? N22 C32 C221 70(3) 8 . 8 ? N22 C32 H22a 92(3) 8 . 8 ? N22 C32 H22b 108(4) 8 . 8 ? N22 C32 H221b 100(3) 8 . 8 ? C221 C32 H22a 124(4) 8 . 8 ? C221 C32 H22b 159(5) 8 . 8 ? C221 C32 H221b 44(2) 8 . 8 ? H22a C32 H22b 76(3) 8 . 8 ? H22a C32 H221b 155(4) 8 . 8 ? H22b C32 H221b 120(4) 8 . 8 ? Eu N32 C32 101(2) . . . ? Eu N32 C321 129(3) . . . ? Eu N32 C322 102.0(12) . . . ? Eu N32 C22 91.6(12) . . 8 ? Eu N32 N22 105(2) . . 8 ? Eu N32 C221 126.9(14) . . 8 ? Eu N32 C222 114.9(15) . . 8 ? C32 N32 C321 121(4) . . . ? C32 N32 C322 96(3) . . . ? C32 N32 C22 43(3) . . 8 ? C32 N32 N22 121(3) . . 8 ? C32 N32 C221 58(3) . . 8 ? C32 N32 C222 136(3) . . 8 ? C321 N32 C322 100(2) . . . ? C321 N32 C22 138(3) . . 8 ? C321 N32 N22 77(3) . . 8 ? C321 N32 C221 67(3) . . 8 ? C321 N32 C222 51(2) . . 8 ? C322 N32 C22 57.6(15) . . 8 ? C322 N32 N22 27(2) . . 8 ? C322 N32 C221 126.7(19) . . 8 ? C322 N32 C222 53.1(16) . . 8 ? C22 N32 N22 85(3) 8 . 8 ? C22 N32 C221 97(2) 8 . 8 ? C22 N32 C222 109.1(18) 8 . 8 ? N22 N32 C221 128(3) 8 . 8 ? N22 N32 C222 27(2) 8 . 8 ? C221 N32 C222 111(2) 8 . 8 ? N32 C321 H321a 109(3) . . . ? N32 C321 H321b 106(3) . . . ? N32 C321 H321c 122(5) . . . ? N32 C321 N22 24.3(9) . . 8 ? N32 C321 C221 53.1(19) . . 8 ? N32 C321 C222 74(2) . . 8 ? N32 C321 H221c 84(3) . . 8 ? N32 C321 H222b 91(2) . . 8 ? H321a C321 H321b 112(6) . . . ? H321a C321 H321c 105(3) . . . ? H321a C321 N22 133(4) . . 8 ? H321a C321 C221 65(3) . . 8 ? H321a C321 C222 176(6) . . 8 ? H321a C321 H221c 25.9(12) . . 8 ? H321a C321 H222b 140(6) . . 8 ? H321b C321 H321c 103(4) . . . ? H321b C321 N22 92(3) . . 8 ? H321b C321 C221 96(4) . . 8 ? H321b C321 C222 70(3) . . 8 ? H321b C321 H221c 114(7) . . 8 ? H321b C321 H222b 28.2(12) . . 8 ? H321c C321 N22 108(4) . . 8 ? H321c C321 C221 161(5) . . 8 ? H321c C321 C222 71(3) . . 8 ? H321c C321 H221c 127(4) . . 8 ? H321c C321 H222b 92(3) . . 8 ? N22 C321 C221 73(2) 8 . 8 ? N22 C321 C222 49(2) 8 . 8 ? N22 C321 H221c 108(3) 8 . 8 ? N22 C321 H222b 70.4(17) 8 . 8 ? C221 C321 C222 119(3) 8 . 8 ? C221 C321 H221c 40(2) 8 . 8 ? C221 C321 H222b 106(3) 8 . 8 ? C222 C321 H221c 157(4) 8 . 8 ? C222 C321 H222b 42(2) 8 . 8 ? H221c C321 H222b 137(6) 8 . 8 ? N32 C322 H322a 113(2) . . . ? N32 C322 H322b 112.6(18) . . . ? N32 C322 H322c 95(2) . . . ? N32 C322 C21 101.5(16) . . 8 ? N32 C322 C22 57.6(13) . . 8 ? N32 C322 N22 12.4(10) . . 8 ? N32 C322 C222 59.1(16) . . 8 ? N32 C322 H21a 133(2) . . 8 ? N32 C322 H222a 95.5(17) . . 8 ? H322a C322 H322b 110(3) . . . ? H322a C322 H322c 113(2) . . . ? H322a C322 C21 113(3) . . 8 ? H322a C322 C22 94(2) . . 8 ? H322a C322 N22 114(3) . . 8 ? H322a C322 C222 96(2) . . 8 ? H322a C322 H21a 107(2) . . 8 ? H322a C322 H222a 101(2) . . 8 ? H322b C322 H322c 113(3) . . . ? H322b C322 C21 11.7(11) . . 8 ? H322b C322 C22 69.5(18) . . 8 ? H322b C322 N22 122(2) . . 8 ? H322b C322 C222 154(3) . . 8 ? H322b C322 H21a 27.9(8) . . 8 ? H322b C322 H222a 125(3) . . 8 ? H322c C322 C21 120(3) . . 8 ? H322c C322 C22 148(2) . . 8 ? H322c C322 N22 83(2) . . 8 ? H322c C322 C222 48.6(18) . . 8 ? H322c C322 H21a 90(2) . . 8 ? H322c C322 H222a 13.6(5) . . 8 ? C21 C322 C22 58.5(17) 8 . 8 ? C21 C322 N22 111(2) 8 . 8 ? C21 C322 C222 151(3) 8 . 8 ? C21 C322 H21a 39.2(14) 8 . 8 ? C21 C322 H222a 132(3) 8 . 8 ? C22 C322 N22 70.0(16) 8 . 8 ? C22 C322 C222 115(2) 8 . 8 ? C22 C322 H21a 97(2) 8 . 8 ? C22 C322 H222a 153(2) 8 . 8 ? N22 C322 C222 47.0(17) 8 . 8 ? N22 C322 H21a 138(3) 8 . 8 ? N22 C322 H222a 83(2) 8 . 8 ? C222 C322 H21a 139(3) 8 . 8 ? C222 C322 H222a 41.4(16) 8 . 8 ? H21a C322 H222a 100(2) 8 . 8 ? C111 H111a C313 107(3) . . 8 ? C111 H111a H313c 154.4(15) . . 8 ? C313 H111a H313c 57(2) 8 . 8 ? C112 H112a H312a 96.8(17) . . 8 ? C112 H112b C31 114.2(18) . . 8 ? C113 H113c C311 99(3) . . 8 ? C113 H113c H311a 101.7(18) . . 8 ? C311 H113c H311a 119(3) 8 . 8 ? C11 H11b H121b 77.4(18) . . 8 ? C12 H12b C121 33(2) . . 8 ? C12 H12b H121a 92.7(17) . . 8 ? C121 H12b H121a 60.3(16) 8 . 8 ? C121 H121a C12 25(2) . . 8 ? C121 H121a H12b 77.6(19) . . 8 ? C12 H121a H12b 52.7(15) 8 . 8 ? C121 H121b C11 90(3) . . 8 ? C121 H121b C12 17(2) . . 8 ? C121 H121b H11b 139(2) . . 8 ? C11 H121b C12 74(2) 8 . 8 ? C11 H121b H11b 60.2(15) 8 . 8 ? C12 H121b H11b 128.5(11) 8 . 8 ? C121 H121c C11 80(2) . . 8 ? C121 H121c C12 36(4) . . 8 ? C11 H121c C12 112(4) 8 . 8 ? C122 H122a C122 64(5) . . 8 ? C122 H122a H122a 49(3) . . 8 ? C122 H122a H122a 113(4) 8 . 8 ? C122 H122b C122 44(4) . . 8 ? C122 H122b H122b 90(3) . . 8 ? C122 H122b H122b 47(2) 8 . 8 ? C211 H211a C211 97(3) . . 8 ? C211 H211a H211a 130(2) . . 8 ? C211 H211a H211a 33.2(14) 8 . 8 ? C212 H212c C213 90(2) . . 8 ? C212 H212c H213a 77.9(16) . . 8 ? C213 H212c H213a 60.8(16) 8 . 8 ? C213 H213a C212 96(2) . . 8 ? C213 H213a H212c 111.2(16) . . 8 ? C212 H213a H212c 92.6(16) 8 . 8 ? C21 H21a C322 97(2) . . 8 ? C21 H21a H322b 35.1(17) . . 8 ? C322 H21a H322b 62.4(13) 8 . 8 ? C22 H22a C32 49(3) . . 8 ? C22 H22a H32b 29.4(16) . . 8 ? C32 H22a H32b 23(2) 8 . 8 ? C22 H22b C31 146(2) . . 8 ? C22 H22b C32 64(3) . . 8 ? C31 H22b C32 88(3) 8 . 8 ? C221 H221a H32a 58(2) . . 8 ? C221 H221b C32 63(3) . . 8 ? C221 H221c C321 106(3) . . 8 ? C221 H221c H321a 156.6(15) . . 8 ? C321 H221c H321a 87(2) 8 . 8 ? C222 H222a C322 85(2) . . 8 ? C222 H222a H322c 103(2) . . 8 ? C322 H222a H322c 41.6(15) 8 . 8 ? C222 H222b C321 61(3) . . 8 ? C222 H222b H321b 98.9(19) . . 8 ? C321 H222b H321b 38(2) 8 . 8 ? C222 H222c H321c 93(2) . . 8 ? C31 H31a C112 107(2) . . 8 ? C311 H311a C113 96(3) . . 8 ? C311 H311a H113c 57(3) . . 8 ? C113 H311a H113c 74.0(17) 8 . 8 ? C312 H312a C112 111(2) . . 8 ? C312 H312a H112a 140(2) . . 8 ? C112 H312a H112a 46.0(14) 8 . 8 ? C312 H312c C111 90(2) . . 8 ? C313 H313b H313b 130(2) . . 8 ? C313 H313c C111 85(3) . . 8 ? C313 H313c H111a 94(2) . . 8 ? C111 H313c H111a 16.3(10) 8 . 8 ? C32 H32a C221 88(4) . . 8 ? C32 H32a H221a 137(3) . . 8 ? C221 H32a H221a 75(2) 8 . 8 ? C32 H32b C22 85(4) . . 8 ? C32 H32b H22a 146(3) . . 8 ? C22 H32b H22a 124(3) 8 . 8 ? C321 H321a C221 77(3) . . 8 ? C321 H321a H221c 67(2) . . 8 ? C221 H321a H221c 16.6(10) 8 . 8 ? C321 H321b C222 66(3) . . 8 ? C321 H321b H222b 113(3) . . 8 ? C222 H321b H222b 47.6(14) 8 . 8 ? C321 H321c C222 65(3) . . 8 ? C321 H321c H222c 107(2) . . 8 ? C222 H321c H222c 44.3(14) 8 . 8 ? C322 H322b C21 151(3) . . 8 ? C322 H322b H21a 89.7(15) . . 8 ? C21 H322b H21a 118(3) 8 . 8 ? C322 H322c N22 56.2(15) . . 8 ? C322 H322c C222 91(2) . . 8 ? C322 H322c H222a 124.8(17) . . 8 ? N22 H322c C222 48.2(18) 8 . 8 ? N22 H322c H222a 107.3(7) 8 . 8 ? C222 H322c H222a 59.5(17) 8 . 8 ? loop_ _geom_torsion_atom_site_label_1 #ActaC _geom_torsion_atom_site_label_2 #ActaC _geom_torsion_atom_site_label_3 #ActaC _geom_torsion_atom_site_label_4 #ActaC _geom_torsion #ActaC _geom_torsion_site_symmetry_1 #ActaC _geom_torsion_site_symmetry_2 #ActaC _geom_torsion_site_symmetry_3 #ActaC _geom_torsion_site_symmetry_4 #ActaC _geom_torsion_publ_flag #ActaC ? ? ? ? ? ? ? ? ? ? _reflns_limit_h_min 0 _reflns_limit_h_max 22 _reflns_limit_k_min 0 _reflns_limit_k_max 20 _reflns_limit_l_min 0 _reflns_limit_l_max 12 _reflns_number_total 3011 #ActaC _reflns_number_observed 1632 #ActaC _reflns_observed_criterion refl_observed_if_F____>_.000_sigma(F___) _reflns_d_resolution_high .841 _reflns_d_resolution_low 9.582 loop_ _reflns_scale_group_code _reflns_scale_meas_F ? 3.8954 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_meas _refln_F_calc _refln_F_sigma _refln_observed_status _refln_scale_group_code 0 0 2 26.664 27.256 1.161 o 1 0 0 4 177.172 156.910 2.374 o 1 0 0 6 134.835 127.800 2.433 o 1 0 0 8 78.338 75.615 2.508 o 1 0 0 10 54.305 56.867 2.970 o 1 0 0 12 13.453 5.049 4.945 < 1 0 1 1 311.061 279.278 6.891 o 1 0 1 3 82.843 70.148 2.417 o 1 0 1 5 145.938 146.353 5.304 o 1 0 1 7 30.656 29.418 1.791 o 1 0 1 9 52.877 57.865 1.967 o 1 0 1 11 39.909 40.432 2.301 o 1 0 2 0 323.778 337.717 3.215 o 1 0 2 2 97.766 94.460 1.830 o 1 0 2 4 202.621 185.453 2.645 o 1 0 2 6 108.832 101.623 2.722 o 1 0 2 8 53.974 53.804 1.878 o 1 0 2 10 57.378 62.432 3.015 o 1 0 3 1 69.984 68.421 1.655 o 1 0 3 3 59.500 51.223 3.698 o 1 0 3 5 135.825 134.577 7.636 o 1 0 3 7 58.189 60.741 1.799 o 1 0 3 9 61.675 64.404 1.952 o 1 0 3 11 32.802 40.406 2.735 o 1 0 4 0 60.029 60.194 1.003 o 1 0 4 2 35.855 34.816 1.086 o 1 0 4 4 208.532 197.806 3.020 o 1 0 4 6 113.019 104.956 2.758 o 1 0 4 8 40.584 45.181 2.798 o 1 0 4 10 53.109 62.909 2.912 o 1 0 5 1 107.093 108.609 2.147 o 1 0 5 3 40.325 41.763 3.723 o 1 0 5 5 142.279 138.039 5.035 o 1 0 5 7 41.337 42.223 4.529 o 1 0 5 9 57.500 59.199 2.059 o 1 0 5 11 31.358 36.628 2.728 o 1 0 6 0 193.618 212.480 6.584 o 1 0 6 2 12.205 10.548 1.361 o 1 0 6 4 120.355 122.498 1.630 o 1 0 6 6 115.955 120.356 3.190 o 1 0 6 8 56.632 54.661 2.008 o 1 0 6 10 50.487 51.901 2.327 o 1 0 7 1 118.102 121.992 2.271 o 1 0 7 3 5.831 7.784 3.321 < 1 0 7 5 111.813 109.477 4.601 o 1 0 7 7 21.234 16.339 3.103 o 1 0 7 9 37.250 42.437 2.369 o 1 0 7 11 32.611 33.130 2.692 o 1 0 8 0 183.714 195.998 6.942 o 1 0 8 2 20.692 21.191 1.636 o 1 0 8 4 100.006 101.249 1.672 o 1 0 8 6 73.331 71.602 1.791 o 1 0 8 8 31.291 33.587 3.851 o 1 0 8 10 46.759 49.257 2.264 o 1 0 9 1 116.555 120.599 1.352 o 1 0 9 3 22.237 24.162 2.059 o 1 0 9 5 73.061 74.829 1.700 o 1 0 9 7 18.793 15.583 2.439 < 1 0 9 9 37.092 37.770 2.517 o 1 0 10 0 116.982 122.361 4.453 o 1 0 10 2 79.627 81.400 1.780 o 1 0 10 4 113.969 118.874 1.832 o 1 0 10 6 40.614 43.277 2.027 o 1 0 10 8 21.208 20.101 2.502 o 1 0 10 10 35.282 41.351 2.937 o 1 0 11 1 99.577 100.251 1.938 o 1 0 11 3 41.210 43.158 1.775 o 1 0 11 5 71.376 75.549 1.888 o 1 0 11 7 16.556 17.410 7.024 < 1 0 11 9 35.930 36.968 3.236 o 1 0 12 0 111.074 114.872 5.133 o 1 0 12 2 20.548 22.623 2.149 o 1 0 12 4 72.614 75.717 1.834 o 1 0 12 6 53.852 54.762 1.978 o 1 0 12 8 20.243 26.579 5.309 < 1 0 13 1 52.403 53.934 1.533 o 1 0 13 3 19.677 23.243 5.118 < 1 0 13 5 70.902 71.269 2.940 o 1 0 13 7 9.087 9.791 5.393 < 1 0 13 9 22.968 27.409 7.109 < 1 0 14 0 79.435 78.610 1.978 o 1 0 14 2 8.649 10.533 4.682 < 1 0 14 4 53.260 51.663 3.576 o 1 0 14 6 39.036 41.042 2.224 o 1 0 14 8 14.240 19.351 6.029 < 1 0 15 1 43.087 44.335 3.019 o 1 0 15 3 19.315 17.193 2.441 < 1 0 15 5 47.496 48.116 3.166 o 1 0 15 7 9.519 6.353 5.048 < 1 0 16 0 49.824 52.993 3.609 o 1 0 16 2 21.427 21.516 3.098 < 1 0 16 4 46.817 44.620 2.048 o 1 0 16 6 12.647 21.311 6.058 < 1 0 17 1 39.081 36.562 1.789 o 1 0 17 3 15.260 12.829 3.984 < 1 0 17 5 29.878 30.485 2.391 o 1 0 18 0 36.407 35.371 2.798 o 1 0 18 2 8.975 13.376 4.778 < 1 0 18 4 24.036 27.899 3.301 < 1 0 19 1 23.162 23.101 2.645 < 1 0 19 3 9.597 9.003 4.600 < 1 0 20 0 27.635 27.060 2.751 o 1 1 0 1 281.401 244.224 2.791 o 1 1 0 2 87.278 82.310 1.365 o 1 1 0 3 186.705 170.796 2.275 o 1 1 0 4 38.567 36.944 1.605 o 1 1 0 5 19.619 18.190 1.760 o 1 1 0 6 60.024 65.431 2.016 o 1 1 0 7 114.948 120.737 2.450 o 1 1 0 8 37.172 35.703 2.494 o 1 1 0 9 26.057 27.647 2.896 o 1 1 0 10 7.881 1.781 4.330 < 1 1 0 11 25.463 31.938 3.475 o 1 1 0 12 23.989 22.581 3.396 o 1 1 1 1 155.163 137.390 4.224 o 1 1 1 2 100.288 93.130 4.115 o 1 1 1 3 85.367 76.305 3.168 o 1 1 1 4 51.789 51.127 1.251 o 1 1 1 5 18.910 16.791 1.359 o 1 1 1 6 50.223 48.302 1.467 o 1 1 1 7 62.072 65.214 1.902 o 1 1 1 8 76.334 75.578 2.209 o 1 1 1 9 23.392 24.265 2.363 o 1 1 1 10 3.373 4.353 2.543 < 1 1 1 11 14.807 17.686 4.580 < 1 1 1 12 25.940 30.093 2.641 o 1 1 2 1 134.862 123.802 3.463 o 1 1 2 2 104.664 92.130 6.054 o 1 1 2 3 190.718 168.804 6.832 o 1 1 2 4 66.022 63.925 1.300 o 1 1 2 5 23.109 22.395 1.685 o 1 1 2 6 48.610 50.449 1.646 o 1 1 2 7 102.198 99.157 1.756 o 1 1 2 8 46.932 49.963 1.899 o 1 1 2 9 25.992 24.895 2.364 o 1 1 2 10 5.847 4.761 3.785 < 1 1 2 11 30.056 32.565 2.630 o 1 1 3 1 93.612 94.826 2.451 o 1 1 3 2 127.507 111.669 5.296 o 1 1 3 3 151.927 136.841 5.970 o 1 1 3 4 87.040 83.302 1.399 o 1 1 3 5 24.919 25.983 1.734 o 1 1 3 6 32.332 32.002 2.218 o 1 1 3 7 40.951 37.836 1.758 o 1 1 3 8 68.046 69.694 3.779 o 1 1 3 9 29.926 31.475 2.249 o 1 1 3 10 7.213 1.219 3.960 < 1 1 3 11 21.599 21.502 2.355 o 1 1 4 1 111.253 111.468 1.666 o 1 1 4 2 134.250 130.129 6.328 o 1 1 4 3 169.371 160.284 6.774 o 1 1 4 4 31.983 32.511 1.421 o 1 1 4 5 20.467 18.989 1.672 o 1 1 4 6 32.232 30.604 1.632 o 1 1 4 7 84.713 89.837 1.813 o 1 1 4 8 56.560 58.119 1.921 o 1 1 4 9 20.686 19.517 2.744 o 1 1 4 10 5.613 6.294 3.650 < 1 1 4 11 27.962 31.356 4.245 o 1 1 5 1 41.937 42.233 .843 o 1 1 5 2 124.084 125.835 5.254 o 1 1 5 3 80.798 81.280 4.589 o 1 1 5 4 84.334 85.186 1.834 o 1 1 5 5 4.787 5.185 2.928 < 1 1 5 6 31.562 33.821 1.804 o 1 1 5 7 54.829 54.823 2.735 o 1 1 5 8 58.256 60.097 1.891 o 1 1 5 9 22.090 23.342 2.596 o 1 1 5 10 4.009 .826 2.951 < 1 1 5 11 14.731 17.298 4.561 < 1 1 6 1 106.203 113.015 2.260 o 1 1 6 2 74.896 76.151 1.811 o 1 1 6 3 130.988 130.378 3.673 o 1 1 6 4 52.905 53.920 3.344 o 1 1 6 5 4.010 4.936 2.698 < 1 1 6 6 42.336 46.504 1.965 o 1 1 6 7 85.550 90.777 1.850 o 1 1 6 8 42.514 42.546 2.063 o 1 1 6 9 23.363 22.250 2.283 o 1 1 6 10 3.785 1.041 2.658 < 1 1 6 11 21.421 27.723 9.049 < 1 1 7 1 90.553 92.942 1.006 o 1 1 7 2 96.362 99.646 3.046 o 1 1 7 3 28.595 33.160 2.446 o 1 1 7 4 57.000 62.437 1.565 o 1 1 7 5 19.352 19.417 1.913 o 1 1 7 6 36.168 33.707 1.780 o 1 1 7 7 56.106 57.969 3.104 o 1 1 7 8 49.612 55.615 2.218 o 1 1 7 9 12.436 20.109 4.560 < 1 1 7 10 13.940 3.343 4.414 < 1 1 7 11 15.593 13.590 5.726 < 1 1 8 1 87.959 94.144 2.100 o 1 1 8 2 76.575 75.308 2.436 o 1 1 8 3 101.091 104.053 1.617 o 1 1 8 4 41.774 41.601 1.614 o 1 1 8 5 14.879 9.762 2.071 < 1 1 8 6 32.103 35.028 1.959 o 1 1 8 7 70.425 72.440 3.765 o 1 1 8 8 30.687 35.207 2.286 o 1 1 8 9 17.463 27.339 4.544 < 1 1 8 10 8.402 .336 5.011 < 1 1 8 11 13.956 23.627 5.903 < 1 1 9 1 24.037 24.029 1.423 o 1 1 9 2 76.208 80.286 1.657 o 1 1 9 3 82.614 83.153 1.916 o 1 1 9 4 38.906 39.152 1.794 o 1 1 9 5 19.180 15.658 2.613 o 1 1 9 6 36.911 34.528 2.015 o 1 1 9 7 30.870 33.786 2.847 o 1 1 9 8 41.944 48.108 1.992 o 1 1 9 9 24.557 24.020 2.148 o 1 1 9 10 3.621 1.531 2.645 < 1 1 10 1 56.180 54.958 1.289 o 1 1 10 2 72.531 73.494 1.628 o 1 1 10 3 95.648 97.759 1.748 o 1 1 10 4 19.806 23.485 2.332 o 1 1 10 5 13.597 19.835 5.821 < 1 1 10 6 21.720 23.674 2.353 o 1 1 10 7 47.984 53.019 2.017 o 1 1 10 8 30.927 34.278 2.573 o 1 1 10 9 21.665 20.451 2.407 o 1 1 10 10 8.603 4.587 5.584 < 1 1 11 1 17.203 19.783 2.255 o 1 1 11 2 66.402 67.613 1.784 o 1 1 11 3 60.433 62.152 1.818 o 1 1 11 4 26.241 30.739 2.054 o 1 1 11 5 12.368 6.445 3.268 < 1 1 11 6 31.458 31.710 2.261 o 1 1 11 7 28.065 29.794 2.022 o 1 1 11 8 38.366 37.409 2.356 o 1 1 11 9 8.863 14.544 4.714 < 1 1 11 10 5.203 .970 3.457 < 1 1 12 1 48.298 46.177 1.437 o 1 1 12 2 49.580 51.367 1.745 o 1 1 12 3 65.078 69.282 1.864 o 1 1 12 4 22.786 25.431 2.231 o 1 1 12 5 6.053 3.584 3.345 < 1 1 12 6 15.057 19.502 3.919 < 1 1 12 7 41.791 43.626 2.133 o 1 1 12 8 26.397 27.331 2.805 o 1 1 12 9 10.331 12.806 4.934 < 1 1 13 1 39.372 37.845 2.613 o 1 1 13 2 49.339 50.787 1.872 o 1 1 13 3 20.421 26.590 2.725 < 1 1 13 4 34.685 36.472 2.177 o 1 1 13 5 7.445 11.908 4.069 < 1 1 13 6 23.093 24.705 2.590 o 1 1 13 7 25.903 31.385 3.007 o 1 1 13 8 27.334 28.525 2.858 o 1 1 13 9 7.615 7.396 4.150 < 1 1 14 1 34.633 35.354 1.724 o 1 1 14 2 31.937 32.145 1.857 o 1 1 14 3 53.057 55.545 2.111 o 1 1 14 4 20.411 25.270 2.208 o 1 1 14 5 6.469 .558 3.571 < 1 1 14 6 22.735 20.171 2.322 o 1 1 14 7 29.982 33.670 2.352 o 1 1 14 8 11.327 16.763 5.416 < 1 1 15 1 19.831 21.996 2.145 o 1 1 15 2 46.510 42.152 1.938 o 1 1 15 3 23.927 28.594 2.571 o 1 1 15 4 21.484 24.842 2.581 o 1 1 15 5 4.742 1.631 3.072 < 1 1 15 6 21.421 19.461 6.641 < 1 1 15 7 13.600 17.714 4.996 < 1 1 15 8 14.273 21.681 5.253 < 1 1 16 1 26.100 23.573 1.911 o 1 1 16 2 28.587 26.343 2.285 o 1 1 16 3 36.842 37.860 4.032 o 1 1 16 4 13.536 12.144 3.531 < 1 1 16 5 5.142 6.154 3.347 < 1 1 16 6 7.196 12.128 3.953 < 1 1 16 7 10.872 23.546 5.243 < 1 1 17 1 9.638 6.670 4.025 < 1 1 17 2 28.362 29.194 2.553 o 1 1 17 3 23.367 24.716 2.592 o 1 1 17 4 15.491 14.262 4.037 < 1 1 17 5 10.470 4.070 3.291 < 1 1 17 6 16.807 13.736 4.379 < 1 1 18 1 15.102 15.518 3.938 < 1 1 18 2 14.499 18.584 4.500 < 1 1 18 3 24.252 25.588 2.574 o 1 1 18 4 4.432 8.365 3.105 < 1 1 18 5 4.303 2.177 2.890 < 1 1 19 1 7.543 11.672 3.624 < 1 1 19 2 19.268 21.619 4.116 < 1 1 19 3 10.368 12.352 4.953 < 1 1 19 4 11.006 12.074 4.050 < 1 1 20 1 9.412 13.015 4.517 < 1 2 0 0 84.496 85.945 1.115 o 1 2 0 1 271.991 248.500 2.516 o 1 2 0 2 210.418 178.106 2.385 o 1 2 0 3 154.967 134.902 2.061 o 1 2 0 4 72.634 70.922 1.654 o 1 2 0 5 163.746 153.444 2.386 o 1 2 0 6 5.428 3.407 3.273 < 1 2 0 7 7.918 .144 3.320 < 1 2 0 8 18.554 17.872 2.760 o 1 2 0 9 66.661 65.731 2.558 o 1 2 0 10 21.551 23.326 3.201 o 1 2 0 11 29.645 32.387 3.336 o 1 2 1 0 304.318 319.205 4.925 o 1 2 1 1 42.834 40.409 .774 o 1 2 1 2 34.255 32.897 .879 o 1 2 1 3 35.065 29.671 2.531 o 1 2 1 4 138.838 132.421 4.955 o 1 2 1 5 7.462 .056 2.796 < 1 2 1 6 122.851 115.580 6.606 o 1 2 1 7 30.033 28.750 1.814 o 1 2 1 8 37.278 35.491 2.371 o 1 2 1 9 6.997 16.513 3.838 < 1 2 1 10 57.509 58.029 3.708 o 1 2 1 11 18.570 14.652 2.237 o 1 2 2 0 138.006 137.465 2.071 o 1 2 2 1 198.925 183.704 3.836 o 1 2 2 2 32.108 28.160 2.401 o 1 2 2 3 95.933 86.417 5.240 o 1 2 2 4 22.583 22.147 1.448 o 1 2 2 5 173.327 158.829 11.766 o 1 2 2 6 37.285 37.166 3.522 o 1 2 2 7 13.030 18.316 6.227 < 1 2 2 8 24.503 25.884 2.187 o 1 2 2 9 65.319 67.443 3.377 o 1 2 2 10 11.163 18.477 4.707 < 1 2 2 11 26.479 33.434 8.203 < 1 2 3 0 99.822 100.456 1.058 o 1 2 3 1 97.713 92.307 1.851 o 1 2 3 2 61.107 56.616 3.983 o 1 2 3 3 6.801 6.412 3.544 < 1 2 3 4 137.414 125.507 3.705 o 1 2 3 5 31.819 27.429 2.748 o 1 2 3 6 97.273 87.548 5.064 o 1 2 3 7 12.701 17.459 3.333 < 1 2 3 8 19.818 25.022 6.111 < 1 2 3 9 9.693 7.748 3.515 < 1 2 3 10 52.375 59.263 2.193 o 1 2 3 11 11.901 15.576 5.736 < 1 2 4 0 45.257 45.762 1.782 o 1 2 4 1 175.062 174.626 3.575 o 1 2 4 2 62.350 62.506 3.224 o 1 2 4 3 65.450 64.670 2.570 o 1 2 4 4 45.930 42.590 1.384 o 1 2 4 5 153.877 149.483 7.139 o 1 2 4 6 59.314 55.531 2.490 o 1 2 4 7 32.361 31.696 1.873 o 1 2 4 8 26.525 29.462 7.007 < 1 2 4 9 65.759 66.786 2.168 o 1 2 4 10 12.605 17.941 4.633 < 1 2 4 11 23.948 32.104 2.709 o 1 2 5 0 193.240 197.730 1.721 o 1 2 5 1 36.163 37.101 1.860 o 1 2 5 2 66.295 65.122 1.991 o 1 2 5 3 3.168 1.892 2.403 < 1 2 5 4 108.408 107.575 4.985 o 1 2 5 5 46.084 41.418 4.791 o 1 2 5 6 96.185 93.223 2.130 o 1 2 5 7 9.900 14.569 4.208 < 1 2 5 8 33.756 33.238 1.992 o 1 2 5 9 9.602 12.815 4.555 < 1 2 5 10 48.653 52.097 2.428 o 1 2 5 11 11.795 11.278 4.358 < 1 2 6 0 61.627 59.431 2.791 o 1 2 6 1 147.585 152.377 2.089 o 1 2 6 2 30.904 31.388 2.151 o 1 2 6 3 53.094 52.015 1.384 o 1 2 6 4 105.035 102.257 3.192 o 1 2 6 5 136.994 136.311 5.792 o 1 2 6 6 18.195 22.122 2.349 < 1 2 6 7 12.818 15.941 3.956 < 1 2 6 8 16.118 16.687 2.231 < 1 2 6 9 53.190 51.517 2.037 o 1 2 6 10 20.779 22.676 3.046 < 1 2 6 11 24.951 29.619 3.566 o 1 2 7 0 184.571 190.656 4.235 o 1 2 7 1 61.420 62.312 1.955 o 1 2 7 2 13.464 17.848 2.032 < 1 2 7 3 6.197 4.477 3.269 < 1 2 7 4 83.269 82.655 2.746 o 1 2 7 5 9.567 10.967 4.540 < 1 2 7 6 77.879 80.175 2.127 o 1 2 7 7 19.910 17.932 2.946 o 1 2 7 8 27.984 28.736 2.378 o 1 2 7 9 8.488 17.029 4.648 < 1 2 7 10 45.182 46.478 2.456 o 1 2 7 11 5.069 8.057 3.460 < 1 2 8 0 56.199 58.172 1.664 o 1 2 8 1 108.132 114.629 2.214 o 1 2 8 2 30.834 32.647 1.485 o 1 2 8 3 41.679 43.140 1.638 o 1 2 8 4 44.857 46.333 2.115 o 1 2 8 5 97.739 100.752 3.998 o 1 2 8 6 15.180 21.843 4.702 < 1 2 8 7 5.090 13.194 3.426 < 1 2 8 8 10.538 14.272 5.833 < 1 2 8 9 44.611 42.793 2.236 o 1 2 8 10 7.013 16.497 4.529 < 1 2 8 11 24.208 26.067 2.408 o 1 2 9 0 117.100 121.461 2.780 o 1 2 9 1 28.303 29.882 1.481 o 1 2 9 2 41.643 45.085 2.596 o 1 2 9 3 7.795 10.021 3.918 < 1 2 9 4 90.977 94.295 2.099 o 1 2 9 5 11.800 14.050 3.637 < 1 2 9 6 54.265 54.802 2.177 o 1 2 9 7 11.783 11.141 4.376 < 1 2 9 8 11.014 17.380 5.821 < 1 2 9 9 4.429 9.472 2.966 < 1 2 9 10 33.675 41.695 2.764 o 1 2 10 0 78.766 80.412 1.588 o 1 2 10 1 101.261 103.362 1.540 o 1 2 10 2 14.241 10.066 1.799 < 1 2 10 3 42.380 41.539 1.751 o 1 2 10 4 15.312 12.037 1.907 o 1 2 10 5 84.919 87.803 1.899 o 1 2 10 6 23.702 28.172 3.557 o 1 2 10 7 14.842 12.212 2.179 < 1 2 10 8 15.604 12.511 2.306 < 1 2 10 9 42.037 40.809 2.219 o 1 2 10 10 7.662 11.154 4.908 < 1 2 11 0 97.552 102.841 3.592 o 1 2 11 1 11.548 11.016 2.986 < 1 2 11 2 34.067 35.218 1.803 o 1 2 11 3 4.211 1.940 3.106 < 1 2 11 4 73.444 78.531 1.925 o 1 2 11 5 22.817 25.822 2.784 o 1 2 11 6 47.924 49.790 2.095 o 1 2 11 7 4.034 6.277 2.816 < 1 2 11 8 19.893 17.721 2.525 < 1 2 11 9 7.954 4.059 4.182 < 1 2 11 10 34.990 31.264 2.340 o 1 2 12 0 18.902 20.731 2.326 < 1 2 12 1 74.156 75.192 2.158 o 1 2 12 2 6.898 13.475 3.807 < 1 2 12 3 29.836 31.670 1.924 o 1 2 12 4 32.100 34.643 2.182 o 1 2 12 5 68.963 70.228 1.942 o 1 2 12 6 9.879 12.535 4.147 < 1 2 12 7 9.284 11.254 5.085 < 1 2 12 8 6.031 2.219 3.874 < 1 2 12 9 30.830 33.819 3.377 o 1 2 13 0 75.351 77.031 2.200 o 1 2 13 1 6.601 4.903 3.501 < 1 2 13 2 11.764 14.198 3.618 < 1 2 13 3 7.434 9.368 3.938 < 1 2 13 4 51.021 46.528 1.825 o 1 2 13 5 17.854 15.897 2.032 < 1 2 13 6 45.735 46.408 2.205 o 1 2 13 7 6.485 7.983 3.591 < 1 2 13 8 8.989 16.997 5.792 < 1 2 13 9 7.696 7.026 4.078 < 1 2 14 0 8.472 5.276 4.034 < 1 2 14 1 51.204 50.062 2.607 o 1 2 14 2 12.761 14.791 5.448 < 1 2 14 3 22.540 18.113 2.199 o 1 2 14 4 19.111 23.617 2.790 < 1 2 14 5 55.502 54.440 2.649 o 1 2 14 6 5.197 7.187 3.067 < 1 2 14 7 5.207 5.952 3.450 < 1 2 14 8 7.429 3.197 3.955 < 1 2 15 0 59.543 58.981 2.381 o 1 2 15 1 14.910 10.227 2.195 < 1 2 15 2 18.816 15.390 2.577 < 1 2 15 3 5.498 2.925 3.534 < 1 2 15 4 43.228 41.166 1.963 o 1 2 15 5 4.552 10.076 3.045 < 1 2 15 6 28.053 27.251 1.989 o 1 2 15 7 5.691 4.609 3.694 < 1 2 15 8 6.475 9.567 4.150 < 1 2 16 0 25.322 22.430 2.509 o 1 2 16 1 43.259 41.819 1.640 o 1 2 16 2 4.328 4.188 2.850 < 1 2 16 3 18.815 17.358 2.464 o 1 2 16 4 6.550 7.589 3.573 < 1 2 16 5 37.879 36.006 2.280 o 1 2 16 6 6.877 9.696 4.109 < 1 2 16 7 8.051 6.515 4.277 < 1 2 17 0 41.016 39.657 4.370 o 1 2 17 1 11.237 12.509 5.381 < 1 2 17 2 11.608 14.644 5.584 < 1 2 17 3 5.473 .656 3.503 < 1 2 17 4 32.490 30.952 2.277 o 1 2 17 5 8.102 9.957 5.396 < 1 2 17 6 21.175 19.385 3.213 < 1 2 18 0 13.268 15.631 4.132 < 1 2 18 1 28.094 27.489 2.178 o 1 2 18 2 7.888 2.958 3.791 < 1 2 18 3 12.841 11.399 3.992 < 1 2 18 4 7.863 8.308 3.768 < 1 2 18 5 26.613 25.499 2.474 o 1 2 19 0 29.270 28.460 2.668 o 1 2 19 1 8.600 6.704 4.119 < 1 2 19 2 4.425 6.135 2.937 < 1 2 19 3 9.122 1.721 4.863 < 1 2 19 4 19.738 17.629 2.811 < 1 2 20 0 4.538 4.948 3.222 < 1 2 20 1 21.991 17.791 4.705 < 1 3 0 1 72.745 70.748 .872 o 1 3 0 2 288.756 260.691 3.131 o 1 3 0 3 50.563 45.752 1.428 o 1 3 0 4 63.496 59.722 1.627 o 1 3 0 5 16.199 15.091 2.347 o 1 3 0 6 102.595 102.813 2.238 o 1 3 0 7 16.329 15.255 2.140 o 1 3 0 8 99.485 93.983 2.484 o 1 3 0 9 7.765 11.135 4.610 < 1 3 0 10 11.265 11.103 4.192 < 1 3 0 11 6.308 3.117 3.987 < 1 3 1 1 56.070 56.987 .584 o 1 3 1 2 85.987 79.979 2.350 o 1 3 1 3 227.742 200.997 6.901 o 1 3 1 4 33.084 34.145 1.134 o 1 3 1 5 13.819 9.616 1.920 < 1 3 1 6 43.875 43.180 1.482 o 1 3 1 7 96.284 96.095 2.950 o 1 3 1 8 8.433 9.662 3.575 < 1 3 1 9 52.830 47.896 1.811 o 1 3 1 10 6.026 5.383 4.092 < 1 3 1 11 28.222 30.825 2.477 o 1 3 2 1 69.375 68.793 1.416 o 1 3 2 2 265.785 236.983 10.369 o 1 3 2 3 76.731 66.030 4.648 o 1 3 2 4 96.054 87.096 1.817 o 1 3 2 5 15.604 13.131 1.784 o 1 3 2 6 104.411 92.249 4.901 o 1 3 2 7 7.834 2.595 3.279 < 1 3 2 8 85.297 84.822 1.847 o 1 3 2 9 21.034 22.272 2.536 o 1 3 2 10 11.193 8.645 4.153 < 1 3 2 11 4.492 6.037 3.175 < 1 3 3 1 170.738 167.983 2.079 o 1 3 3 2 72.420 65.991 4.090 o 1 3 3 3 146.279 126.306 7.548 o 1 3 3 4 39.240 39.483 1.321 o 1 3 3 5 37.649 38.366 5.150 o 1 3 3 6 33.373 31.997 2.317 o 1 3 3 7 99.583 98.322 4.482 o 1 3 3 8 37.849 38.009 1.890 o 1 3 3 9 29.067 32.731 4.187 o 1 3 3 10 8.277 6.679 4.047 < 1 3 3 11 22.647 27.412 3.186 < 1 3 4 1 56.564 58.572 1.175 o 1 3 4 2 200.783 192.230 8.376 o 1 3 4 3 53.724 46.475 3.116 o 1 3 4 4 118.894 115.248 2.806 o 1 3 4 5 7.152 6.215 3.475 < 1 3 4 6 88.792 86.865 3.926 o 1 3 4 7 11.940 8.457 3.065 < 1 3 4 8 68.002 69.363 3.447 o 1 3 4 9 26.621 26.511 2.226 o 1 3 4 10 9.177 7.446 4.422 < 1 3 4 11 7.064 6.102 3.846 < 1 3 5 1 100.221 104.186 2.040 o 1 3 5 2 30.399 29.948 2.202 o 1 3 5 3 144.144 144.934 5.900 o 1 3 5 4 22.814 20.736 1.572 o 1 3 5 5 7.735 .900 4.361 < 1 3 5 6 31.614 33.105 1.815 o 1 3 5 7 79.970 79.136 2.088 o 1 3 5 8 31.048 34.070 3.755 o 1 3 5 9 33.269 32.689 3.875 o 1 3 5 10 6.221 4.687 3.764 < 1 3 5 11 23.208 28.395 2.747 o 1 3 6 1 3.376 5.120 2.527 < 1 3 6 2 169.051 173.354 5.284 o 1 3 6 3 1.429 2.596 2.396 < 1 3 6 4 73.926 70.581 4.332 o 1 3 6 5 24.223 26.872 1.896 o 1 3 6 6 62.488 63.295 2.644 o 1 3 6 7 19.261 20.549 2.610 o 1 3 6 8 64.591 64.868 2.018 o 1 3 6 9 6.050 13.883 3.889 < 1 3 6 10 10.973 9.126 4.076 < 1 3 6 11 5.787 2.336 3.800 < 1 3 7 1 51.901 53.569 .987 o 1 3 7 2 45.390 48.082 2.365 o 1 3 7 3 142.922 142.857 3.960 o 1 3 7 4 17.631 18.825 6.524 < 1 3 7 5 20.394 20.753 1.859 o 1 3 7 6 30.345 28.791 2.096 o 1 3 7 7 68.779 67.585 1.893 o 1 3 7 8 14.637 14.508 3.806 < 1 3 7 9 35.745 36.091 2.156 o 1 3 7 10 12.820 2.792 6.216 < 1 3 7 11 24.981 24.600 2.653 o 1 3 8 1 34.656 31.910 1.016 o 1 3 8 2 125.061 129.747 1.677 o 1 3 8 3 15.167 13.502 1.993 < 1 3 8 4 55.186 56.309 3.332 o 1 3 8 5 12.242 10.938 2.667 < 1 3 8 6 52.697 54.467 1.746 o 1 3 8 7 11.654 9.757 5.541 < 1 3 8 8 57.121 59.878 3.932 o 1 3 8 9 8.557 12.794 4.718 < 1 3 8 10 9.138 8.101 4.420 < 1 3 9 1 77.026 81.356 1.269 o 1 3 9 2 51.090 50.903 1.589 o 1 3 9 3 85.345 88.684 2.074 o 1 3 9 4 23.081 22.432 1.874 o 1 3 9 5 8.170 .509 4.445 < 1 3 9 6 14.562 17.373 3.818 < 1 3 9 7 68.415 71.447 4.921 o 1 3 9 8 7.718 15.490 4.255 < 1 3 9 9 22.967 25.127 2.594 o 1 3 9 10 4.081 5.962 2.915 < 1 3 10 1 4.326 6.914 2.793 < 1 3 10 2 101.434 105.599 1.733 o 1 3 10 3 45.356 44.416 2.208 o 1 3 10 4 52.010 53.256 1.766 o 1 3 10 5 6.844 5.220 3.702 < 1 3 10 6 54.287 56.071 1.822 o 1 3 10 7 5.501 7.166 3.507 < 1 3 10 8 46.954 46.056 2.164 o 1 3 10 9 13.502 11.058 4.220 < 1 3 10 10 5.058 5.575 3.452 < 1 3 11 1 67.561 65.493 1.398 o 1 3 11 2 46.368 46.140 1.724 o 1 3 11 3 71.120 71.061 1.792 o 1 3 11 4 10.081 12.468 5.327 < 1 3 11 5 7.577 .168 3.611 < 1 3 11 6 10.289 10.998 4.340 < 1 3 11 7 48.610 55.809 2.322 o 1 3 11 8 16.199 19.528 5.043 < 1 3 11 9 13.128 19.949 5.535 < 1 3 12 1 12.145 17.630 3.169 < 1 3 12 2 75.451 76.746 1.996 o 1 3 12 3 8.938 5.419 4.848 < 1 3 12 4 44.700 43.240 1.914 o 1 3 12 5 5.762 10.167 3.803 < 1 3 12 6 40.091 39.961 3.961 o 1 3 12 7 18.937 18.610 2.865 < 1 3 12 8 37.552 37.873 2.244 o 1 3 12 9 9.882 4.544 5.425 < 1 3 13 1 29.540 29.201 2.297 o 1 3 13 2 16.391 18.939 6.923 < 1 3 13 3 75.999 72.249 3.032 o 1 3 13 4 11.265 12.638 5.414 < 1 3 13 5 4.345 3.496 3.001 < 1 3 13 6 9.037 13.948 4.362 < 1 3 13 7 33.830 37.133 2.283 o 1 3 13 8 6.420 12.605 4.274 < 1 3 13 9 20.061 18.766 2.869 < 1 3 14 1 11.454 13.145 5.519 < 1 3 14 2 63.395 64.436 2.785 o 1 3 14 3 10.003 3.727 4.166 < 1 3 14 4 28.977 30.541 2.523 o 1 3 14 5 8.334 5.061 4.069 < 1 3 14 6 22.959 26.659 2.758 o 1 3 14 7 11.702 13.553 4.935 < 1 3 14 8 32.988 32.728 2.880 o 1 3 15 1 36.655 32.273 1.756 o 1 3 15 2 11.262 15.785 4.148 < 1 3 15 3 51.078 49.295 3.502 o 1 3 15 4 5.133 6.905 3.434 < 1 3 15 5 5.258 2.206 3.391 < 1 3 15 6 8.564 9.336 4.574 < 1 3 15 7 32.554 32.170 1.982 o 1 3 16 1 5.886 5.213 3.728 < 1 3 16 2 50.456 47.419 2.265 o 1 3 16 3 12.059 13.186 3.753 < 1 3 16 4 23.339 19.136 2.218 o 1 3 16 5 6.538 1.400 3.637 < 1 3 16 6 22.506 22.685 2.663 o 1 3 16 7 7.221 4.451 3.929 < 1 3 17 1 31.071 28.532 2.050 o 1 3 17 2 11.461 12.811 4.844 < 1 3 17 3 31.733 29.480 2.672 o 1 3 17 4 9.025 4.929 5.799 < 1 3 17 5 6.702 .413 3.682 < 1 3 17 6 6.405 3.072 3.799 < 1 3 18 1 6.650 3.931 3.521 < 1 3 18 2 32.400 30.789 2.355 o 1 3 18 3 5.619 8.237 3.740 < 1 3 18 4 10.364 16.610 4.974 < 1 3 18 5 9.667 2.012 3.601 < 1 3 19 1 12.393 15.433 4.554 < 1 3 19 2 8.892 7.793 4.268 < 1 3 19 3 25.558 25.560 3.152 o 1 3 20 1 5.134 5.342 3.438 < 1 4 0 0 64.970 62.371 1.251 o 1 4 0 1 125.300 122.419 1.192 o 1 4 0 2 20.842 21.263 1.457 o 1 4 0 3 12.955 12.310 1.587 o 1 4 0 4 156.335 147.351 2.230 o 1 4 0 5 87.075 86.610 2.009 o 1 4 0 6 69.752 65.488 2.029 o 1 4 0 7 15.740 19.413 3.375 < 1 4 0 8 7.416 9.354 4.025 < 1 4 0 9 51.643 50.855 2.526 o 1 4 0 10 53.244 50.995 2.762 o 1 4 0 11 16.049 19.886 4.170 < 1 4 1 0 21.215 21.130 .861 o 1 4 1 1 87.308 87.387 .727 o 1 4 1 2 65.501 66.939 1.027 o 1 4 1 3 78.459 73.905 1.438 o 1 4 1 4 64.334 60.039 1.245 o 1 4 1 5 139.195 127.951 1.615 o 1 4 1 6 47.921 44.988 1.490 o 1 4 1 7 14.960 14.403 3.886 < 1 4 1 8 3.914 1.478 3.065 < 1 4 1 9 58.240 55.619 2.532 o 1 4 1 10 37.001 36.114 2.003 o 1 4 1 11 28.446 26.544 1.920 o 1 4 2 0 97.408 98.506 1.200 o 1 4 2 1 47.047 46.980 .924 o 1 4 2 2 22.218 21.160 1.266 o 1 4 2 3 31.659 31.514 1.176 o 1 4 2 4 102.323 94.279 2.036 o 1 4 2 5 89.706 81.623 5.925 o 1 4 2 6 79.977 72.013 2.855 o 1 4 2 7 6.542 12.272 3.546 < 1 4 2 8 15.513 19.094 5.671 < 1 4 2 9 42.560 41.505 1.947 o 1 4 2 10 41.895 46.100 4.531 o 1 4 2 11 18.809 20.455 4.897 < 1 4 3 0 85.295 87.387 1.102 o 1 4 3 1 179.055 179.255 1.628 o 1 4 3 2 7.775 11.402 2.726 < 1 4 3 3 39.857 34.737 2.414 o 1 4 3 4 15.107 15.463 1.679 o 1 4 3 5 142.330 134.804 7.989 o 1 4 3 6 77.481 74.659 3.064 o 1 4 3 7 3.458 8.051 2.554 < 1 4 3 8 18.675 15.456 2.217 o 1 4 3 9 56.980 56.526 1.933 o 1 4 3 10 30.099 30.974 2.794 o 1 4 3 11 30.262 28.233 2.181 o 1 4 4 0 208.277 210.133 1.799 o 1 4 4 1 107.706 107.912 1.003 o 1 4 4 2 60.876 60.027 2.088 o 1 4 4 3 55.163 49.479 2.906 o 1 4 4 4 58.388 55.890 1.839 o 1 4 4 5 104.355 96.893 6.682 o 1 4 4 6 72.826 70.106 5.674 o 1 4 4 7 5.682 3.519 3.296 < 1 4 4 8 23.747 24.772 2.354 o 1 4 4 9 24.722 32.559 6.446 < 1 4 4 10 39.303 40.589 2.191 o 1 4 4 11 16.906 17.787 3.611 < 1 4 5 0 159.404 156.513 1.578 o 1 4 5 1 161.109 165.554 1.592 o 1 4 5 2 29.839 28.764 2.101 o 1 4 5 3 39.962 40.014 1.305 o 1 4 5 4 71.256 73.324 1.481 o 1 4 5 5 121.545 121.058 7.939 o 1 4 5 6 37.114 38.906 4.344 o 1 4 5 7 8.771 6.563 3.658 < 1 4 5 8 15.118 10.966 2.158 o 1 4 5 9 49.121 49.692 2.038 o 1 4 5 10 33.741 34.840 2.453 o 1 4 5 11 19.479 25.484 5.073 < 1 4 6 0 136.093 138.526 1.521 o 1 4 6 1 127.671 125.924 2.854 o 1 4 6 2 69.657 71.874 1.370 o 1 4 6 3 60.443 54.836 2.333 o 1 4 6 4 83.680 82.774 1.997 o 1 4 6 5 74.693 74.660 3.550 o 1 4 6 6 50.341 51.058 5.869 o 1 4 6 7 17.471 12.889 1.961 o 1 4 6 8 7.910 9.576 4.646 < 1 4 6 9 30.114 36.347 7.873 < 1 4 6 10 37.377 40.190 3.995 o 1 4 6 11 11.453 12.586 4.810 < 1 4 7 0 44.601 46.462 1.325 o 1 4 7 1 102.656 102.291 1.060 o 1 4 7 2 65.588 65.718 2.131 o 1 4 7 3 65.325 62.816 1.462 o 1 4 7 4 80.539 80.602 1.824 o 1 4 7 5 94.718 94.356 4.771 o 1 4 7 6 22.477 24.333 2.396 o 1 4 7 7 9.766 16.251 4.672 < 1 4 7 8 3.954 8.176 2.762 < 1 4 7 9 40.626 43.021 2.214 o 1 4 7 10 30.481 31.253 2.534 o 1 4 7 11 19.821 22.475 6.135 < 1 4 8 0 92.392 94.353 1.549 o 1 4 8 1 57.993 62.067 1.238 o 1 4 8 2 24.419 25.666 1.614 o 1 4 8 3 30.619 29.110 2.584 o 1 4 8 4 77.028 78.513 2.029 o 1 4 8 5 53.063 56.190 1.726 o 1 4 8 6 58.613 56.555 1.807 o 1 4 8 7 10.044 11.406 4.819 < 1 4 8 8 9.506 9.892 5.599 < 1 4 8 9 31.290 32.096 2.123 o 1 4 8 10 32.136 34.613 2.319 o 1 4 9 0 60.058 63.262 2.736 o 1 4 9 1 78.122 80.438 1.372 o 1 4 9 2 3.168 3.343 2.240 < 1 4 9 3 49.608 50.876 4.007 o 1 4 9 4 23.548 22.599 1.928 o 1 4 9 5 86.428 88.564 1.896 o 1 4 9 6 45.143 43.803 2.732 o 1 4 9 7 11.682 12.910 4.289 < 1 4 9 8 9.773 14.962 4.691 < 1 4 9 9 34.556 38.235 2.618 o 1 4 9 10 15.278 21.634 4.727 < 1 4 10 0 94.429 92.107 2.976 o 1 4 10 1 49.488 50.472 2.244 o 1 4 10 2 4.041 4.974 2.683 < 1 4 10 3 16.090 16.886 1.939 < 1 4 10 4 49.982 53.475 1.739 o 1 4 10 5 54.947 52.834 1.915 o 1 4 10 6 52.105 54.845 3.036 o 1 4 10 7 5.691 6.048 3.606 < 1 4 10 8 20.759 17.088 2.182 o 1 4 10 9 15.918 23.355 4.148 < 1 4 10 10 26.981 27.194 2.655 o 1 4 11 0 55.972 56.923 2.123 o 1 4 11 1 70.813 70.263 1.735 o 1 4 11 2 7.211 5.787 3.399 < 1 4 11 3 26.557 26.677 2.866 o 1 4 11 4 25.579 26.572 1.965 o 1 4 11 5 67.486 67.494 1.894 o 1 4 11 6 36.152 36.673 2.111 o 1 4 11 7 12.998 7.402 5.461 < 1 4 11 8 8.051 6.441 4.257 < 1 4 11 9 27.559 30.038 2.344 o 1 4 12 0 62.939 62.165 1.796 o 1 4 12 1 35.595 35.881 2.626 o 1 4 12 2 17.856 17.712 2.369 o 1 4 12 3 10.407 11.555 4.384 < 1 4 12 4 34.681 35.896 2.135 o 1 4 12 5 45.772 41.736 1.951 o 1 4 12 6 36.689 35.769 2.936 o 1 4 12 7 7.366 6.342 3.898 < 1 4 12 8 8.620 11.454 4.109 < 1 4 12 9 15.716 19.678 4.877 < 1 4 13 0 21.239 20.552 2.328 o 1 4 13 1 52.414 51.633 1.660 o 1 4 13 2 19.403 22.494 9.394 < 1 4 13 3 10.798 11.887 4.555 < 1 4 13 4 33.630 35.474 2.245 o 1 4 13 5 41.972 44.920 5.110 o 1 4 13 6 8.610 17.527 4.567 < 1 4 13 7 8.375 8.405 5.369 < 1 4 13 8 4.595 .063 3.302 < 1 4 14 0 45.791 44.745 1.987 o 1 4 14 1 27.724 28.987 1.914 o 1 4 14 2 18.285 21.202 2.733 < 1 4 14 3 7.210 14.368 4.313 < 1 4 14 4 27.802 33.929 2.717 o 1 4 14 5 27.331 23.925 1.886 o 1 4 14 6 25.024 26.013 2.375 o 1 4 14 7 10.665 8.352 5.142 < 1 4 14 8 8.292 7.406 3.952 < 1 4 15 0 33.076 28.065 2.199 o 1 4 15 1 44.949 41.067 1.701 o 1 4 15 2 8.201 11.198 4.495 < 1 4 15 3 18.431 17.225 2.653 < 1 4 15 4 16.737 18.335 2.363 < 1 4 15 5 31.655 33.434 4.145 o 1 4 15 6 14.737 18.594 4.576 < 1 4 15 7 4.969 7.671 3.316 < 1 4 16 0 44.501 43.912 5.008 o 1 4 16 1 29.213 26.412 2.077 o 1 4 16 2 11.247 6.385 3.483 < 1 4 16 3 5.538 8.365 3.564 < 1 4 16 4 26.793 25.397 2.293 o 1 4 16 5 26.719 23.160 2.210 o 1 4 16 6 20.269 22.144 5.291 < 1 4 16 7 10.632 2.936 5.112 < 1 4 17 0 34.096 32.650 2.274 o 1 4 17 1 28.243 26.818 1.893 o 1 4 17 2 5.096 2.917 3.350 < 1 4 17 3 9.836 13.326 5.233 < 1 4 17 4 8.210 13.165 4.482 < 1 4 17 5 25.033 25.882 2.788 o 1 4 17 6 13.890 15.355 2.978 < 1 4 18 0 29.603 27.706 3.360 o 1 4 18 1 13.736 16.927 4.260 < 1 4 18 2 4.475 4.794 3.118 < 1 4 18 3 10.571 6.092 3.897 < 1 4 18 4 16.491 16.878 7.887 < 1 4 18 5 16.206 18.336 5.975 < 1 4 19 0 17.387 13.308 3.710 < 1 4 19 1 22.963 17.869 4.916 < 1 4 19 2 7.433 6.230 3.971 < 1 4 19 3 6.796 6.553 4.364 < 1 5 0 1 79.155 76.146 1.795 o 1 5 0 2 20.298 19.555 1.826 o 1 5 0 3 239.302 223.585 2.832 o 1 5 0 4 10.258 13.344 2.709 < 1 5 0 5 49.148 45.156 1.889 o 1 5 0 6 37.307 29.347 2.033 o 1 5 0 7 68.441 67.395 2.363 o 1 5 0 8 9.165 15.955 4.437 < 1 5 0 9 50.647 44.345 2.611 o 1 5 0 10 4.189 4.972 3.057 < 1 5 0 11 33.037 31.246 2.931 o 1 5 1 1 3.761 4.595 1.868 < 1 5 1 2 235.952 228.527 3.063 o 1 5 1 3 41.976 39.901 1.160 o 1 5 1 4 107.102 99.489 1.411 o 1 5 1 5 19.912 21.266 1.698 o 1 5 1 6 85.915 84.856 3.749 o 1 5 1 7 5.484 .775 3.510 < 1 5 1 8 84.403 81.568 3.773 o 1 5 1 9 4.381 .077 2.922 < 1 5 1 10 10.021 9.983 4.861 < 1 5 1 11 8.498 3.533 5.766 < 1 5 2 1 136.581 134.062 .962 o 1 5 2 2 5.020 3.499 2.771 < 1 5 2 3 170.742 160.205 3.200 o 1 5 2 4 6.991 .974 2.600 < 1 5 2 5 7.466 9.164 5.004 < 1 5 2 6 23.410 18.855 1.458 o 1 5 2 7 98.399 94.919 2.199 o 1 5 2 8 6.060 5.920 3.358 < 1 5 2 9 36.571 37.771 4.299 o 1 5 2 10 6.111 7.064 3.702 < 1 5 2 11 27.211 27.431 2.355 o 1 5 3 1 24.798 23.187 .800 o 1 5 3 2 195.929 191.348 6.365 o 1 5 3 3 3.000 6.017 2.016 < 1 5 3 4 111.122 104.923 1.510 o 1 5 3 5 7.231 5.466 3.102 < 1 5 3 6 107.104 101.915 3.019 o 1 5 3 7 14.736 12.133 1.699 o 1 5 3 8 81.843 77.782 1.865 o 1 5 3 9 10.615 1.169 3.971 < 1 5 3 10 4.084 5.748 2.798 < 1 5 3 11 6.732 .931 4.068 < 1 5 4 1 121.894 125.302 1.434 o 1 5 4 2 50.770 52.023 1.234 o 1 5 4 3 126.226 119.643 4.689 o 1 5 4 4 9.278 14.487 2.917 < 1 5 4 5 7.350 14.608 3.709 < 1 5 4 6 7.634 8.177 4.267 < 1 5 4 7 104.759 102.780 2.549 o 1 5 4 8 10.231 4.070 3.804 < 1 5 4 9 30.620 35.664 7.984 < 1 5 4 10 5.589 7.967 3.671 < 1 5 4 11 22.757 24.921 2.876 o 1 5 5 1 24.605 24.073 1.163 o 1 5 5 2 179.587 182.599 4.126 o 1 5 5 3 8.432 8.131 3.630 < 1 5 5 4 79.206 77.323 4.580 o 1 5 5 5 7.520 2.575 3.611 < 1 5 5 6 92.954 92.055 3.568 o 1 5 5 7 3.937 7.608 2.779 < 1 5 5 8 71.214 71.644 1.942 o 1 5 5 9 4.835 1.281 3.281 < 1 5 5 10 8.142 8.432 4.362 < 1 5 5 11 7.747 1.059 4.185 < 1 5 6 1 52.862 55.681 .932 o 1 5 6 2 36.299 33.206 2.725 o 1 5 6 3 152.947 153.824 3.629 o 1 5 6 4 4.758 1.162 3.096 < 1 5 6 5 34.263 31.239 1.525 o 1 5 6 6 11.210 12.858 3.537 < 1 5 6 7 70.619 67.817 1.922 o 1 5 6 8 7.318 .536 3.923 < 1 5 6 9 36.506 39.079 4.431 o 1 5 6 10 5.392 5.343 3.525 < 1 5 6 11 24.173 25.456 2.884 o 1 5 7 1 4.261 11.708 2.385 < 1 5 7 2 146.334 148.614 5.895 o 1 5 7 3 10.014 13.036 4.333 < 1 5 7 4 58.167 58.264 1.559 o 1 5 7 5 4.447 4.324 2.961 < 1 5 7 6 61.619 63.190 1.764 o 1 5 7 7 7.501 9.329 3.618 < 1 5 7 8 65.384 64.227 2.042 o 1 5 7 9 6.829 1.773 3.794 < 1 5 7 10 9.836 10.827 4.772 < 1 5 8 1 52.500 53.911 1.566 o 1 5 8 2 15.062 14.204 2.215 < 1 5 8 3 123.956 125.893 1.705 o 1 5 8 4 6.207 10.951 3.740 < 1 5 8 5 6.699 3.645 3.213 < 1 5 8 6 17.377 19.579 2.419 < 1 5 8 7 65.082 64.387 1.926 o 1 5 8 8 4.648 1.839 3.183 < 1 5 8 9 21.152 26.380 7.786 < 1 5 8 10 7.480 3.202 4.499 < 1 5 9 1 13.027 11.577 1.982 < 1 5 9 2 132.189 133.569 1.792 o 1 5 9 3 5.610 7.524 3.697 < 1 5 9 4 54.475 56.451 1.754 o 1 5 9 5 4.292 .583 2.604 < 1 5 9 6 57.391 55.851 2.794 o 1 5 9 7 6.082 4.986 3.616 < 1 5 9 8 51.355 50.731 3.243 o 1 5 9 9 3.691 4.533 2.650 < 1 5 9 10 12.166 5.969 4.514 < 1 5 10 1 93.700 94.581 1.971 o 1 5 10 2 9.487 9.655 5.116 < 1 5 10 3 66.968 64.929 1.731 o 1 5 10 4 8.256 4.323 4.957 < 1 5 10 5 10.943 15.446 4.157 < 1 5 10 6 9.208 8.140 3.939 < 1 5 10 7 64.281 63.451 2.020 o 1 5 10 8 4.392 .276 3.019 < 1 5 10 9 24.101 18.399 2.235 o 1 5 10 10 5.818 2.978 3.932 < 1 5 11 1 12.029 8.606 1.830 < 1 5 11 2 89.985 93.033 1.783 o 1 5 11 3 7.810 4.811 3.323 < 1 5 11 4 55.193 53.279 1.766 o 1 5 11 5 3.604 .500 2.595 < 1 5 11 6 46.590 48.100 2.625 o 1 5 11 7 5.331 3.082 3.240 < 1 5 11 8 41.813 41.363 4.752 o 1 5 11 9 4.560 3.960 3.248 < 1 5 12 1 40.704 39.638 1.529 o 1 5 12 2 10.265 9.764 3.835 < 1 5 12 3 65.766 70.841 1.894 o 1 5 12 4 7.349 .244 4.083 < 1 5 12 5 5.876 3.786 3.254 < 1 5 12 6 7.095 .844 3.022 < 1 5 12 7 42.316 41.766 2.395 o 1 5 12 8 8.039 .703 4.311 < 1 5 12 9 17.018 21.992 5.293 < 1 5 13 1 5.020 3.807 2.997 < 1 5 13 2 69.994 68.047 1.930 o 1 5 13 3 5.327 1.145 3.632 < 1 5 13 4 35.152 32.933 2.038 o 1 5 13 5 4.232 4.545 2.939 < 1 5 13 6 31.982 30.369 2.503 o 1 5 13 7 4.444 3.873 3.072 < 1 5 13 8 37.581 38.422 2.462 o 1 5 14 1 30.877 28.789 2.168 o 1 5 14 2 8.578 7.360 3.663 < 1 5 14 3 58.035 57.867 4.307 o 1 5 14 4 4.787 .457 3.106 < 1 5 14 5 9.059 4.925 3.863 < 1 5 14 6 6.547 1.871 3.936 < 1 5 14 7 33.693 34.808 2.646 o 1 5 14 8 17.340 .124 2.314 < 1 5 15 1 3.432 .482 2.473 < 1 5 15 2 55.650 57.384 2.264 o 1 5 15 3 4.547 1.628 3.092 < 1 5 15 4 24.439 22.259 2.036 o 1 5 15 5 6.436 2.000 3.584 < 1 5 15 6 26.680 25.008 2.023 o 1 5 15 7 3.950 .109 2.724 < 1 5 16 1 40.512 36.347 3.148 o 1 5 16 2 5.729 .243 3.722 < 1 5 16 3 32.930 35.183 4.656 o 1 5 16 4 6.801 .804 3.773 < 1 5 16 5 5.301 1.442 3.628 < 1 5 16 6 10.717 4.677 3.365 < 1 5 17 1 5.114 2.401 3.461 < 1 5 17 2 42.224 39.806 3.509 o 1 5 17 3 4.611 .231 3.280 < 1 5 17 4 18.001 18.161 3.853 < 1 5 17 5 8.074 1.784 4.334 < 1 5 18 1 28.110 22.868 1.952 o 1 5 18 2 11.414 1.084 4.246 < 1 5 18 3 29.304 26.728 2.484 o 1 5 18 4 6.493 .127 3.595 < 1 5 19 1 4.725 .116 3.191 < 1 5 19 2 21.591 25.874 3.277 < 1 5 19 3 8.146 1.724 4.887 < 1 6 0 0 57.675 58.639 1.477 o 1 6 0 1 46.861 44.508 1.565 o 1 6 0 2 86.353 84.474 1.704 o 1 6 0 3 45.128 43.680 1.731 o 1 6 0 4 103.349 99.389 1.980 o 1 6 0 5 44.965 44.588 2.125 o 1 6 0 6 63.681 67.766 2.321 o 1 6 0 7 38.738 35.847 2.151 o 1 6 0 8 6.777 10.593 4.066 < 1 6 0 9 18.067 22.921 4.704 < 1 6 0 10 45.221 44.584 2.663 o 1 6 0 11 14.252 20.169 4.425 < 1 6 1 0 79.089 83.357 2.395 o 1 6 1 1 138.262 139.286 1.356 o 1 6 1 2 41.011 40.481 1.096 o 1 6 1 3 17.534 19.121 1.720 o 1 6 1 4 102.486 99.865 1.436 o 1 6 1 5 132.486 126.325 3.097 o 1 6 1 6 34.440 36.506 2.743 o 1 6 1 7 25.007 24.105 1.997 o 1 6 1 8 12.651 16.061 6.084 < 1 6 1 9 50.185 47.098 1.840 o 1 6 1 10 37.475 38.984 2.032 o 1 6 1 11 32.114 29.315 2.203 o 1 6 2 0 111.015 117.815 1.277 o 1 6 2 1 66.630 69.345 1.078 o 1 6 2 2 64.710 62.473 1.683 o 1 6 2 3 12.325 11.127 3.173 < 1 6 2 4 93.121 90.837 1.723 o 1 6 2 5 62.209 59.337 1.450 o 1 6 2 6 71.908 68.554 1.550 o 1 6 2 7 22.586 22.002 3.450 o 1 6 2 8 13.823 14.465 3.583 < 1 6 2 9 24.970 22.513 2.919 o 1 6 2 10 44.729 45.922 3.146 o 1 6 2 11 22.286 22.486 2.743 < 1 6 3 0 148.785 157.304 1.513 o 1 6 3 1 119.748 122.705 1.035 o 1 6 3 2 9.435 11.185 2.360 < 1 6 3 3 41.986 39.775 1.289 o 1 6 3 4 36.618 37.049 1.440 o 1 6 3 5 116.956 111.038 2.826 o 1 6 3 6 70.469 71.620 1.855 o 1 6 3 7 12.645 10.493 3.281 < 1 6 3 8 37.043 35.433 2.560 o 1 6 3 9 45.415 47.666 3.044 o 1 6 3 10 21.415 26.909 6.627 < 1 6 3 11 20.506 25.322 8.633 < 1 6 4 0 141.887 148.049 1.503 o 1 6 4 1 71.413 71.707 .993 o 1 6 4 2 55.700 56.629 1.271 o 1 6 4 3 10.965 8.495 1.564 o 1 6 4 4 91.391 89.177 2.818 o 1 6 4 5 69.983 67.777 2.086 o 1 6 4 6 52.307 51.579 1.915 o 1 6 4 7 3.710 6.942 2.509 < 1 6 4 8 11.870 15.082 4.342 < 1 6 4 9 19.675 23.945 2.870 < 1 6 4 10 46.028 43.440 2.116 o 1 6 4 11 23.868 21.967 5.122 < 1 6 5 0 104.960 104.538 1.407 o 1 6 5 1 133.712 132.273 1.092 o 1 6 5 2 27.473 26.139 1.439 o 1 6 5 3 60.346 61.938 1.399 o 1 6 5 4 76.652 72.808 1.488 o 1 6 5 5 92.907 91.293 1.741 o 1 6 5 6 42.544 43.839 1.841 o 1 6 5 7 6.818 9.937 4.372 < 1 6 5 8 20.189 21.601 2.124 o 1 6 5 9 44.452 44.661 2.752 o 1 6 5 10 21.933 26.307 6.807 < 1 6 5 11 23.663 22.593 2.519 o 1 6 6 0 98.724 104.209 1.489 o 1 6 6 1 47.666 49.253 1.647 o 1 6 6 2 38.872 40.391 3.600 o 1 6 6 3 14.934 14.175 1.952 < 1 6 6 4 78.803 77.716 2.781 o 1 6 6 5 46.850 44.366 1.696 o 1 6 6 6 50.193 50.623 1.674 o 1 6 6 7 18.653 17.886 2.408 < 1 6 6 8 9.526 12.612 4.545 < 1 6 6 9 29.771 27.838 2.211 o 1 6 6 10 35.358 36.873 2.543 o 1 6 6 11 20.854 16.974 2.544 < 1 6 7 0 58.248 58.686 1.399 o 1 6 7 1 74.505 77.141 1.050 o 1 6 7 2 49.466 50.994 2.083 o 1 6 7 3 44.160 45.065 3.835 o 1 6 7 4 96.859 97.301 2.761 o 1 6 7 5 82.560 83.952 2.363 o 1 6 7 6 33.783 30.901 1.748 o 1 6 7 7 9.826 13.162 5.372 < 1 6 7 8 7.200 10.898 3.949 < 1 6 7 9 39.611 39.657 2.466 o 1 6 7 10 19.131 25.942 4.997 < 1 6 8 0 53.230 55.644 1.507 o 1 6 8 1 46.091 47.117 1.109 o 1 6 8 2 22.126 22.486 1.839 o 1 6 8 3 28.113 28.100 1.805 o 1 6 8 4 54.416 55.074 2.520 o 1 6 8 5 38.413 38.641 2.878 o 1 6 8 6 54.164 55.136 1.725 o 1 6 8 7 24.959 20.915 1.910 o 1 6 8 8 14.444 13.385 3.757 < 1 6 8 9 21.937 24.682 2.532 o 1 6 8 10 27.107 30.572 2.833 o 1 6 9 0 100.282 101.733 1.689 o 1 6 9 1 67.856 67.506 1.475 o 1 6 9 2 8.827 3.205 3.461 < 1 6 9 3 34.178 33.002 2.817 o 1 6 9 4 43.534 45.103 2.826 o 1 6 9 5 72.814 74.940 1.856 o 1 6 9 6 42.675 44.629 2.012 o 1 6 9 7 7.177 12.044 3.915 < 1 6 9 8 9.042 20.708 4.868 < 1 6 9 9 30.171 35.350 7.873 < 1 6 9 10 12.648 19.567 6.923 < 1 6 10 0 79.010 79.039 1.870 o 1 6 10 1 39.408 37.994 1.376 o 1 6 10 2 12.218 13.897 3.775 < 1 6 10 3 12.605 16.473 3.262 < 1 6 10 4 42.298 44.963 4.301 o 1 6 10 5 39.929 41.618 1.993 o 1 6 10 6 45.532 44.143 2.017 o 1 6 10 7 14.161 10.278 3.702 < 1 6 10 8 7.029 13.193 4.167 < 1 6 10 9 21.209 15.178 2.588 o 1 6 11 0 64.116 65.097 3.003 o 1 6 11 1 62.560 65.784 2.555 o 1 6 11 2 4.503 .181 2.750 < 1 6 11 3 8.423 17.850 4.502 < 1 6 11 4 26.538 25.264 2.079 o 1 6 11 5 50.517 54.552 2.086 o 1 6 11 6 27.356 28.476 2.281 o 1 6 11 7 9.516 10.059 5.212 < 1 6 11 8 11.266 15.273 4.778 < 1 6 11 9 26.105 28.938 3.825 o 1 6 12 0 61.428 59.748 1.852 o 1 6 12 1 25.082 25.581 2.020 o 1 6 12 2 26.342 24.675 2.158 o 1 6 12 3 8.153 2.244 3.624 < 1 6 12 4 41.504 39.247 2.763 o 1 6 12 5 27.893 31.630 2.658 o 1 6 12 6 30.352 30.369 1.925 o 1 6 12 7 6.942 8.844 4.464 < 1 6 12 8 8.133 9.524 4.299 < 1 6 12 9 5.802 12.584 3.989 < 1 6 13 0 28.780 27.433 2.220 o 1 6 13 1 50.115 48.586 1.621 o 1 6 13 2 28.477 27.278 3.359 o 1 6 13 3 20.043 17.443 2.277 < 1 6 13 4 31.569 33.460 4.119 o 1 6 13 5 40.268 36.460 1.991 o 1 6 13 6 11.887 14.785 4.345 < 1 6 13 7 5.976 10.085 3.843 < 1 6 13 8 5.756 5.613 3.676 < 1 6 14 0 52.649 49.139 2.575 o 1 6 14 1 25.660 27.095 1.952 o 1 6 14 2 7.244 11.077 3.971 < 1 6 14 3 3.936 6.724 2.833 < 1 6 14 4 23.023 27.342 2.671 o 1 6 14 5 15.057 21.286 3.910 < 1 6 14 6 24.801 27.892 2.513 o 1 6 14 7 12.882 11.421 4.031 < 1 6 14 8 14.221 10.317 6.005 < 1 6 15 0 31.397 32.889 2.176 o 1 6 15 1 40.163 35.560 2.726 o 1 6 15 2 13.146 9.592 4.091 < 1 6 15 3 8.241 13.820 4.523 < 1 6 15 4 19.230 22.855 5.020 < 1 6 15 5 32.851 35.380 2.367 o 1 6 15 6 12.916 18.842 4.760 < 1 6 15 7 5.933 5.910 3.803 < 1 6 16 0 42.526 38.330 3.296 o 1 6 16 1 11.935 19.303 4.389 < 1 6 16 2 4.222 7.226 3.005 < 1 6 16 3 8.449 9.735 4.490 < 1 6 16 4 24.511 24.717 2.369 o 1 6 16 5 12.439 18.293 5.953 < 1 6 16 6 21.733 21.653 2.660 o 1 6 17 0 32.181 28.285 3.887 o 1 6 17 1 27.129 24.530 2.000 o 1 6 17 2 5.554 1.609 3.733 < 1 6 17 3 5.531 11.276 3.686 < 1 6 17 4 12.228 12.744 4.484 < 1 6 17 5 31.582 26.349 2.345 o 1 6 18 0 23.538 23.968 6.132 < 1 6 18 1 9.197 12.418 4.399 < 1 6 18 2 8.668 5.793 4.762 < 1 6 18 3 6.414 4.296 3.797 < 1 6 18 4 11.389 18.739 6.056 < 1 6 19 0 8.863 13.967 4.703 < 1 6 19 1 21.507 16.117 2.088 o 1 6 19 2 4.880 6.308 3.338 < 1 7 0 1 20.856 22.878 1.239 o 1 7 0 2 166.583 170.317 2.299 o 1 7 0 3 4.164 1.218 2.754 < 1 7 0 4 82.827 81.387 1.997 o 1 7 0 5 29.817 31.152 2.087 o 1 7 0 6 33.046 33.088 2.117 o 1 7 0 7 24.450 27.653 2.719 o 1 7 0 8 62.821 58.120 2.636 o 1 7 0 9 5.173 .025 3.408 < 1 7 0 10 4.949 .719 3.247 < 1 7 0 11 5.211 6.895 3.511 < 1 7 1 1 104.326 108.864 .919 o 1 7 1 2 54.300 55.978 1.183 o 1 7 1 3 157.118 155.927 1.634 o 1 7 1 4 33.848 34.634 1.362 o 1 7 1 5 18.403 18.870 1.684 o 1 7 1 6 35.613 37.558 1.565 o 1 7 1 7 93.302 86.548 3.659 o 1 7 1 8 16.460 15.522 2.189 < 1 7 1 9 29.439 27.779 2.130 o 1 7 1 10 4.220 2.043 3.028 < 1 7 1 11 32.761 31.255 4.923 o 1 7 2 1 6.398 7.579 3.042 < 1 7 2 2 117.932 120.293 1.425 o 1 7 2 3 58.882 58.276 1.256 o 1 7 2 4 78.290 77.609 1.419 o 1 7 2 5 5.408 8.645 3.000 < 1 7 2 6 48.354 48.400 3.145 o 1 7 2 7 11.034 15.505 3.400 < 1 7 2 8 66.146 62.318 1.883 o 1 7 2 9 13.473 13.364 3.532 < 1 7 2 10 5.740 .936 3.539 < 1 7 2 11 5.987 9.467 4.064 < 1 7 3 1 123.525 128.727 1.102 o 1 7 3 2 72.506 72.250 1.304 o 1 7 3 3 133.622 130.203 3.286 o 1 7 3 4 8.563 10.397 4.518 < 1 7 3 5 17.095 14.790 1.647 o 1 7 3 6 26.065 24.010 2.896 o 1 7 3 7 104.772 104.226 2.810 o 1 7 3 8 29.595 26.385 1.867 o 1 7 3 9 31.419 27.940 1.948 o 1 7 3 10 5.845 6.179 3.523 < 1 7 3 11 28.846 28.229 2.509 o 1 7 4 1 6.032 6.705 2.194 < 1 7 4 2 114.360 115.233 1.475 o 1 7 4 3 68.617 64.975 2.592 o 1 7 4 4 68.088 67.450 1.482 o 1 7 4 5 22.129 24.739 1.796 o 1 7 4 6 69.423 70.661 3.502 o 1 7 4 7 17.172 17.343 3.637 < 1 7 4 8 68.308 64.168 2.185 o 1 7 4 9 15.917 19.617 4.181 < 1 7 4 10 4.647 .679 3.226 < 1 7 4 11 7.141 8.024 3.783 < 1 7 5 1 107.118 109.366 1.437 o 1 7 5 2 46.531 47.215 1.457 o 1 7 5 3 145.437 143.423 3.667 o 1 7 5 4 12.613 8.531 3.897 < 1 7 5 5 32.482 32.231 1.636 o 1 7 5 6 20.370 25.173 2.364 o 1 7 5 7 89.331 92.149 1.922 o 1 7 5 8 22.211 23.915 2.482 o 1 7 5 9 26.760 24.077 2.189 o 1 7 5 10 6.509 4.493 3.607 < 1 7 5 11 24.465 26.173 2.741 o 1 7 6 1 34.567 36.118 1.120 o 1 7 6 2 114.849 118.249 1.609 o 1 7 6 3 4.497 2.382 2.849 < 1 7 6 4 52.478 49.823 3.157 o 1 7 6 5 9.310 17.468 4.055 < 1 7 6 6 52.535 54.078 1.740 o 1 7 6 7 31.506 33.644 1.926 o 1 7 6 8 61.129 60.313 4.349 o 1 7 6 9 9.374 7.594 3.936 < 1 7 6 10 6.665 1.144 3.640 < 1 7 7 1 79.428 80.451 1.087 o 1 7 7 2 35.177 39.385 1.613 o 1 7 7 3 135.262 137.514 2.805 o 1 7 7 4 32.797 32.915 3.182 o 1 7 7 5 12.843 14.087 3.402 < 1 7 7 6 28.276 31.412 2.181 o 1 7 7 7 73.999 72.612 3.625 o 1 7 7 8 10.421 15.390 4.375 < 1 7 7 9 23.354 18.123 1.833 o 1 7 7 10 7.232 1.997 4.670 < 1 7 8 1 25.840 26.914 1.190 o 1 7 8 2 103.947 100.786 1.674 o 1 7 8 3 20.673 19.777 2.825 o 1 7 8 4 50.627 50.709 3.231 o 1 7 8 5 8.910 10.239 4.834 < 1 7 8 6 39.952 40.540 1.905 o 1 7 8 7 21.960 20.074 2.084 o 1 7 8 8 49.946 49.476 2.615 o 1 7 8 9 8.367 6.341 4.018 < 1 7 8 10 7.142 1.146 4.879 < 1 7 9 1 87.608 89.975 2.000 o 1 7 9 2 38.249 38.520 1.788 o 1 7 9 3 88.872 87.617 1.978 o 1 7 9 4 27.853 30.305 1.851 o 1 7 9 5 4.343 3.422 2.864 < 1 7 9 6 22.937 19.545 3.287 o 1 7 9 7 63.315 58.251 4.259 o 1 7 9 8 17.395 16.235 2.378 < 1 7 9 9 10.500 16.059 4.416 < 1 7 9 10 9.918 4.333 4.801 < 1 7 10 1 3.079 .820 2.154 < 1 7 10 2 78.911 78.764 2.061 o 1 7 10 3 43.100 44.015 1.762 o 1 7 10 4 49.238 47.100 2.277 o 1 7 10 5 12.738 11.058 3.379 < 1 7 10 6 33.065 33.397 2.117 o 1 7 10 7 5.684 9.043 3.354 < 1 7 10 8 45.621 41.601 2.099 o 1 7 10 9 5.930 7.805 3.551 < 1 7 11 1 56.606 54.629 1.466 o 1 7 11 2 34.394 34.672 2.705 o 1 7 11 3 71.797 72.460 1.834 o 1 7 11 4 3.077 4.954 2.219 < 1 7 11 5 6.915 6.522 4.156 < 1 7 11 6 6.760 7.693 3.686 < 1 7 11 7 40.543 46.728 2.370 o 1 7 11 8 11.621 15.590 4.919 < 1 7 11 9 9.424 17.662 4.523 < 1 7 12 1 21.410 19.591 1.598 o 1 7 12 2 56.354 57.285 1.809 o 1 7 12 3 17.235 12.454 2.192 o 1 7 12 4 29.022 33.300 2.290 o 1 7 12 5 6.715 3.016 4.566 < 1 7 12 6 24.558 25.087 2.439 o 1 7 12 7 14.425 14.611 7.924 < 1 7 12 8 30.042 34.112 2.868 o 1 7 13 1 36.094 32.837 2.432 o 1 7 13 2 16.842 22.500 3.606 < 1 7 13 3 60.437 59.767 1.981 o 1 7 13 4 5.995 6.034 4.080 < 1 7 13 5 6.753 8.230 3.761 < 1 7 13 6 7.992 10.669 4.257 < 1 7 13 7 41.020 38.208 2.335 o 1 7 13 8 12.860 10.140 6.165 < 1 7 14 1 17.089 20.757 2.414 < 1 7 14 2 45.342 48.510 2.348 o 1 7 14 3 5.493 5.020 3.494 < 1 7 14 4 24.459 23.047 3.279 o 1 7 14 5 8.514 4.097 3.660 < 1 7 14 6 18.491 20.290 2.775 < 1 7 14 7 8.393 14.033 4.616 < 1 7 15 1 35.116 32.525 1.852 o 1 7 15 2 13.803 13.754 4.279 < 1 7 15 3 39.079 40.651 2.083 o 1 7 15 4 9.930 9.258 4.207 < 1 7 15 5 12.936 1.660 4.043 < 1 7 15 6 6.498 11.598 4.202 < 1 7 15 7 34.205 32.372 2.448 o 1 7 16 1 9.912 3.031 3.060 < 1 7 16 2 35.474 37.455 2.571 o 1 7 16 3 11.713 13.565 4.327 < 1 7 16 4 15.187 20.323 4.713 < 1 7 16 5 9.475 3.335 4.600 < 1 7 16 6 17.176 18.293 6.322 < 1 7 17 1 25.924 25.638 3.872 o 1 7 17 2 9.553 9.430 4.581 < 1 7 17 3 33.842 28.890 2.336 o 1 7 17 4 8.101 5.562 4.306 < 1 7 17 5 8.684 1.754 4.197 < 1 7 18 1 8.763 3.237 3.689 < 1 7 18 2 29.995 26.274 2.994 o 1 7 18 3 11.610 9.271 4.284 < 1 7 18 4 12.084 13.613 5.793 < 1 7 19 1 12.216 12.876 4.488 < 1 8 0 0 27.334 26.462 1.762 o 1 8 0 1 104.765 108.613 1.365 o 1 8 0 2 34.338 34.911 1.963 o 1 8 0 3 41.870 39.923 1.772 o 1 8 0 4 41.724 41.865 1.842 o 1 8 0 5 125.186 123.936 2.327 o 1 8 0 6 15.945 13.687 3.391 < 1 8 0 7 29.301 28.785 2.522 o 1 8 0 8 4.761 3.686 3.226 < 1 8 0 9 37.930 37.566 3.090 o 1 8 0 10 21.419 17.100 3.148 o 1 8 0 11 33.072 33.816 3.685 o 1 8 1 0 171.080 183.674 1.671 o 1 8 1 1 27.042 29.648 .942 o 1 8 1 2 30.726 31.080 2.225 o 1 8 1 3 3.602 4.926 2.523 < 1 8 1 4 123.918 122.264 1.996 o 1 8 1 5 5.159 6.233 3.221 < 1 8 1 6 83.810 84.589 1.661 o 1 8 1 7 12.311 18.639 5.229 < 1 8 1 8 40.385 39.492 1.969 o 1 8 1 9 11.256 14.550 4.135 < 1 8 1 10 52.979 49.592 2.323 o 1 8 1 11 6.551 10.431 3.889 < 1 8 2 0 81.824 83.400 1.295 o 1 8 2 1 107.116 110.212 .993 o 1 8 2 2 5.042 1.877 2.960 < 1 8 2 3 33.689 34.949 1.305 o 1 8 2 4 10.007 14.154 4.221 < 1 8 2 5 102.285 100.739 1.617 o 1 8 2 6 32.944 33.022 2.521 o 1 8 2 7 31.870 29.810 2.684 o 1 8 2 8 8.694 7.200 4.803 < 1 8 2 9 42.356 42.292 2.136 o 1 8 2 10 12.070 12.704 4.442 < 1 8 2 11 32.747 31.124 2.346 o 1 8 3 0 149.573 159.471 2.475 o 1 8 3 1 16.535 16.306 1.026 o 1 8 3 2 83.171 84.098 2.943 o 1 8 3 3 15.706 14.529 2.145 o 1 8 3 4 147.920 147.242 1.721 o 1 8 3 5 30.433 31.725 1.559 o 1 8 3 6 56.935 54.744 1.694 o 1 8 3 7 6.483 13.708 3.549 < 1 8 3 8 28.585 26.707 1.966 o 1 8 3 9 12.493 9.513 5.245 < 1 8 3 10 50.822 51.183 3.948 o 1 8 3 11 7.181 9.226 3.939 < 1 8 4 0 59.747 58.838 1.522 o 1 8 4 1 97.968 101.448 1.025 o 1 8 4 2 14.543 12.568 1.667 o 1 8 4 3 28.025 27.076 1.397 o 1 8 4 4 20.978 19.680 1.550 o 1 8 4 5 78.431 76.276 1.658 o 1 8 4 6 31.699 32.279 1.686 o 1 8 4 7 25.144 24.729 2.469 o 1 8 4 8 11.573 8.808 4.293 < 1 8 4 9 41.948 44.470 3.803 o 1 8 4 10 7.823 10.443 4.157 < 1 8 4 11 22.251 27.764 2.916 < 1 8 5 0 143.044 148.475 1.658 o 1 8 5 1 16.985 17.836 1.179 o 1 8 5 2 46.132 46.290 1.346 o 1 8 5 3 14.754 13.496 1.645 o 1 8 5 4 106.553 108.585 2.820 o 1 8 5 5 32.298 27.706 2.430 o 1 8 5 6 67.104 65.116 1.986 o 1 8 5 7 7.094 11.138 3.780 < 1 8 5 8 32.596 29.822 2.807 o 1 8 5 9 7.382 10.300 3.908 < 1 8 5 10 42.861 40.410 2.842 o 1 8 6 0 16.490 17.314 1.453 o 1 8 6 1 75.772 76.802 1.035 o 1 8 6 2 20.346 20.569 1.747 o 1 8 6 3 16.128 19.840 4.966 < 1 8 6 4 42.853 44.082 2.818 o 1 8 6 5 75.066 77.512 1.695 o 1 8 6 6 10.046 13.194 4.204 < 1 8 6 7 22.533 19.415 2.194 o 1 8 6 8 5.933 8.458 3.517 < 1 8 6 9 38.175 37.259 2.083 o 1 8 6 10 8.305 13.119 4.570 < 1 8 7 0 137.713 140.797 1.727 o 1 8 7 1 25.440 26.337 1.762 o 1 8 7 2 4.246 7.557 2.857 < 1 8 7 3 21.276 20.009 2.175 o 1 8 7 4 71.044 67.304 3.712 o 1 8 7 5 9.154 10.553 3.835 < 1 8 7 6 75.161 73.082 3.084 o 1 8 7 7 9.359 6.207 4.519 < 1 8 7 8 31.773 27.307 1.898 o 1 8 7 9 4.772 10.580 3.197 < 1 8 7 10 33.244 34.733 2.636 o 1 8 8 0 39.259 40.396 1.584 o 1 8 8 1 63.537 65.799 1.119 o 1 8 8 2 18.832 15.507 1.615 o 1 8 8 3 14.876 14.160 2.100 < 1 8 8 4 21.422 17.789 1.990 o 1 8 8 5 79.558 80.588 1.848 o 1 8 8 6 14.551 14.670 3.117 < 1 8 8 7 24.889 20.313 5.342 < 1 8 8 8 5.669 9.603 3.671 < 1 8 8 9 34.268 33.675 2.364 o 1 8 8 10 8.959 10.901 5.317 < 1 8 9 0 97.447 97.537 2.928 o 1 8 9 1 20.264 23.547 1.985 o 1 8 9 2 32.567 31.545 1.673 o 1 8 9 3 6.293 7.240 3.435 < 1 8 9 4 75.773 78.093 1.831 o 1 8 9 5 15.536 13.671 3.317 < 1 8 9 6 42.146 46.151 2.085 o 1 8 9 7 3.267 2.480 2.275 < 1 8 9 8 21.091 18.660 5.509 < 1 8 9 9 6.256 6.443 3.694 < 1 8 10 0 36.080 38.004 3.565 o 1 8 10 1 66.490 66.104 3.501 o 1 8 10 2 10.672 6.236 2.873 < 1 8 10 3 19.205 22.782 4.998 < 1 8 10 4 4.725 .577 3.030 < 1 8 10 5 58.037 57.827 1.891 o 1 8 10 6 13.012 14.689 3.410 < 1 8 10 7 17.143 20.247 5.351 < 1 8 10 8 4.345 5.523 3.080 < 1 8 10 9 33.703 29.408 2.227 o 1 8 11 0 84.459 80.759 1.871 o 1 8 11 1 4.492 7.508 2.930 < 1 8 11 2 32.940 31.156 1.978 o 1 8 11 3 7.575 5.121 4.643 < 1 8 11 4 67.085 64.777 3.602 o 1 8 11 5 12.979 17.068 4.782 < 1 8 11 6 34.948 32.800 2.067 o 1 8 11 7 7.323 3.875 3.514 < 1 8 11 8 10.678 17.308 5.126 < 1 8 11 9 6.162 5.269 4.086 < 1 8 12 0 3.496 1.815 2.629 < 1 8 12 1 55.082 53.291 1.525 o 1 8 12 2 13.495 16.761 5.019 < 1 8 12 3 19.827 22.000 2.940 o 1 8 12 4 16.992 17.418 2.541 < 1 8 12 5 41.853 40.931 2.773 o 1 8 12 6 7.053 8.478 3.842 < 1 8 12 7 11.193 13.833 5.976 < 1 8 12 8 9.119 .519 5.525 < 1 8 13 0 75.096 73.685 3.557 o 1 8 13 1 12.692 10.896 3.308 < 1 8 13 2 6.866 8.986 3.730 < 1 8 13 3 4.944 2.223 3.300 < 1 8 13 4 32.097 36.022 2.572 o 1 8 13 5 13.931 10.995 2.068 < 1 8 13 6 34.261 35.576 2.390 o 1 8 13 7 8.432 7.506 4.077 < 1 8 13 8 10.216 17.479 4.929 < 1 8 14 0 8.757 8.436 4.622 < 1 8 14 1 43.157 39.761 1.668 o 1 8 14 2 6.064 10.278 3.359 < 1 8 14 3 10.966 12.882 4.601 < 1 8 14 4 10.381 12.971 4.993 < 1 8 14 5 39.593 41.359 2.290 o 1 8 14 6 8.487 11.079 4.068 < 1 8 14 7 10.640 7.024 5.837 < 1 8 15 0 54.300 50.162 4.956 o 1 8 15 1 8.519 9.601 4.080 < 1 8 15 2 6.540 10.143 3.577 < 1 8 15 3 8.869 3.742 5.296 < 1 8 15 4 38.009 34.648 2.196 o 1 8 15 5 14.917 10.559 3.894 < 1 8 15 6 23.032 25.851 2.520 o 1 8 16 0 8.502 14.383 4.696 < 1 8 16 1 30.947 27.592 1.993 o 1 8 16 2 6.049 1.378 3.413 < 1 8 16 3 12.184 10.564 5.829 < 1 8 16 4 5.118 6.551 3.454 < 1 8 16 5 33.116 31.173 2.495 o 1 8 16 6 5.801 6.723 3.747 < 1 8 17 0 30.008 27.960 2.925 o 1 8 17 1 7.571 6.770 4.147 < 1 8 17 2 11.922 11.214 5.051 < 1 8 17 3 4.183 3.132 2.980 < 1 8 17 4 29.868 26.412 3.710 o 1 8 18 0 12.746 9.130 6.124 < 1 8 18 1 20.735 20.043 5.405 < 1 8 18 2 4.987 2.269 3.337 < 1 8 18 3 4.692 8.286 3.135 < 1 9 0 1 98.837 98.025 1.412 o 1 9 0 2 52.526 53.969 1.855 o 1 9 0 3 69.104 72.449 2.006 o 1 9 0 4 61.240 62.389 2.043 o 1 9 0 5 7.904 13.377 3.910 < 1 9 0 6 22.540 20.617 2.292 o 1 9 0 7 81.958 81.074 2.564 o 1 9 0 8 33.302 28.079 2.845 o 1 9 0 9 17.416 19.754 5.388 < 1 9 0 10 3.613 1.275 2.722 < 1 9 0 11 10.028 17.841 5.339 < 1 9 1 1 86.483 85.744 .963 o 1 9 1 2 91.522 94.934 1.405 o 1 9 1 3 71.340 73.488 2.481 o 1 9 1 4 53.466 54.521 1.430 o 1 9 1 5 6.393 4.513 3.085 < 1 9 1 6 43.065 41.245 2.074 o 1 9 1 7 60.792 56.662 1.779 o 1 9 1 8 49.266 51.765 1.998 o 1 9 1 9 8.798 9.812 4.784 < 1 9 1 10 5.987 2.467 4.076 < 1 9 1 11 10.076 18.762 4.856 < 1 9 2 1 80.052 81.003 .962 o 1 9 2 2 60.701 62.891 1.376 o 1 9 2 3 91.429 90.196 1.505 o 1 9 2 4 42.015 41.240 1.457 o 1 9 2 5 6.027 3.379 3.911 < 1 9 2 6 20.950 16.744 1.772 o 1 9 2 7 62.829 65.451 1.896 o 1 9 2 8 35.412 35.400 2.097 o 1 9 2 9 22.280 23.649 1.950 o 1 9 2 10 7.959 1.963 4.854 < 1 9 3 1 29.590 29.507 .980 o 1 9 3 2 92.222 95.031 1.912 o 1 9 3 3 108.855 109.335 1.567 o 1 9 3 4 40.707 40.997 1.719 o 1 9 3 5 28.763 31.911 1.722 o 1 9 3 6 38.230 35.706 2.274 o 1 9 3 7 49.660 50.928 2.153 o 1 9 3 8 51.792 51.061 1.858 o 1 9 3 9 21.639 19.859 2.492 < 1 9 3 10 4.042 4.513 2.770 < 1 9 4 1 58.290 60.652 .991 o 1 9 4 2 50.195 51.574 2.093 o 1 9 4 3 112.542 112.592 1.589 o 1 9 4 4 16.538 19.753 2.208 o 1 9 4 5 16.669 14.981 1.365 o 1 9 4 6 14.404 16.915 2.030 < 1 9 4 7 53.400 54.577 1.781 o 1 9 4 8 40.176 38.091 1.945 o 1 9 4 9 22.565 19.826 2.520 o 1 9 4 10 7.253 3.570 3.956 < 1 9 5 1 60.505 59.473 1.048 o 1 9 5 2 109.072 110.467 1.933 o 1 9 5 3 68.362 71.842 1.981 o 1 9 5 4 41.579 40.156 1.672 o 1 9 5 5 8.377 8.276 3.573 < 1 9 5 6 43.648 43.086 1.748 o 1 9 5 7 51.158 51.701 3.226 o 1 9 5 8 43.291 41.992 2.022 o 1 9 5 9 9.546 12.677 4.545 < 1 9 5 10 6.528 4.212 3.902 < 1 9 6 1 87.927 90.115 1.111 o 1 9 6 2 35.000 33.390 1.544 o 1 9 6 3 78.738 81.882 1.983 o 1 9 6 4 38.295 35.149 1.649 o 1 9 6 5 8.102 4.775 3.498 < 1 9 6 6 26.438 23.279 2.761 o 1 9 6 7 59.309 60.094 1.847 o 1 9 6 8 28.788 29.897 2.170 o 1 9 6 9 13.755 13.088 5.778 < 1 9 6 10 4.483 3.650 3.326 < 1 9 7 1 67.071 69.705 1.625 o 1 9 7 2 87.260 89.401 1.626 o 1 9 7 3 46.046 47.349 1.617 o 1 9 7 4 42.798 42.701 1.666 o 1 9 7 5 6.077 9.270 3.419 < 1 9 7 6 43.255 44.731 1.849 o 1 9 7 7 37.617 40.811 2.216 o 1 9 7 8 35.906 35.101 2.196 o 1 9 7 9 8.286 5.698 4.366 < 1 9 7 10 7.297 1.017 4.011 < 1 9 8 1 57.179 57.148 1.208 o 1 9 8 2 36.637 37.303 1.832 o 1 9 8 3 60.104 61.926 1.902 o 1 9 8 4 39.442 38.975 1.790 o 1 9 8 5 7.090 3.503 3.970 < 1 9 8 6 19.118 16.475 2.310 < 1 9 8 7 44.409 48.093 4.598 o 1 9 8 8 23.228 27.609 2.751 < 1 9 8 9 7.180 17.942 4.300 < 1 9 9 1 24.403 25.511 1.680 o 1 9 9 2 64.808 63.448 2.877 o 1 9 9 3 67.606 67.656 2.614 o 1 9 9 4 37.832 39.133 1.936 o 1 9 9 5 9.975 9.900 3.745 < 1 9 9 6 34.198 33.947 1.901 o 1 9 9 7 27.131 28.496 8.409 < 1 9 9 8 33.494 34.881 2.367 o 1 9 9 9 11.325 7.886 4.168 < 1 9 10 1 27.789 27.630 1.547 o 1 9 10 2 39.069 40.774 1.725 o 1 9 10 3 65.879 65.615 1.839 o 1 9 10 4 10.474 15.257 5.721 < 1 9 10 5 16.734 10.528 1.943 o 1 9 10 6 7.972 11.162 4.206 < 1 9 10 7 32.885 33.994 2.141 o 1 9 10 8 24.040 24.525 3.590 o 1 9 10 9 17.443 19.167 5.427 < 1 9 11 1 28.954 28.510 1.968 o 1 9 11 2 53.613 55.633 2.425 o 1 9 11 3 38.268 41.444 2.032 o 1 9 11 4 27.407 25.551 2.320 o 1 9 11 5 6.677 8.383 3.713 < 1 9 11 6 23.663 21.931 2.295 o 1 9 11 7 23.227 29.061 2.981 < 1 9 11 8 30.079 28.749 2.400 o 1 9 12 1 27.955 27.525 2.698 o 1 9 12 2 34.405 32.253 1.864 o 1 9 12 3 47.488 49.152 1.983 o 1 9 12 4 11.573 11.277 4.248 < 1 9 12 5 6.176 3.033 3.996 < 1 9 12 6 10.974 14.468 5.803 < 1 9 12 7 34.976 31.507 2.391 o 1 9 12 8 10.785 17.527 5.170 < 1 9 13 1 35.749 34.288 2.365 o 1 9 13 2 45.052 42.157 1.938 o 1 9 13 3 23.074 20.741 2.043 o 1 9 13 4 22.725 20.990 2.211 o 1 9 13 5 8.458 .611 4.064 < 1 9 13 6 15.680 19.085 4.086 < 1 9 13 7 29.880 27.464 2.565 o 1 9 14 1 30.805 26.884 2.127 o 1 9 14 2 21.351 24.432 2.907 < 1 9 14 3 28.750 29.964 2.268 o 1 9 14 4 13.907 16.635 5.877 < 1 9 14 5 5.691 2.116 3.733 < 1 9 14 6 10.956 15.261 5.253 < 1 9 14 7 23.384 25.591 2.716 o 1 9 15 1 12.734 16.280 3.950 < 1 9 15 2 27.067 29.942 3.136 o 1 9 15 3 25.810 25.623 2.551 o 1 9 15 4 22.554 19.475 3.400 o 1 9 15 5 8.272 4.041 4.014 < 1 9 15 6 15.925 17.294 4.161 < 1 9 16 1 16.625 16.238 2.503 o 1 9 16 2 19.082 17.743 2.657 < 1 9 16 3 27.484 28.910 3.458 o 1 9 16 4 9.561 11.437 4.579 < 1 9 16 5 5.673 3.654 3.688 < 1 9 17 1 8.133 5.764 4.294 < 1 9 17 2 26.160 24.196 3.873 o 1 9 17 3 12.055 19.249 5.101 < 1 9 17 4 10.924 11.627 4.603 < 1 9 18 1 13.503 11.139 3.517 < 1 9 18 2 19.510 13.280 2.490 < 1 10 0 0 169.539 170.178 2.465 o 1 10 0 1 26.564 26.884 1.550 o 1 10 0 2 14.679 15.493 3.379 < 1 10 0 3 8.205 7.460 3.924 < 1 10 0 4 79.080 75.771 2.143 o 1 10 0 5 5.226 .068 3.236 < 1 10 0 6 82.240 81.381 2.271 o 1 10 0 7 10.291 11.720 3.868 < 1 10 0 8 36.032 36.916 2.548 o 1 10 0 9 7.125 2.012 3.993 < 1 10 0 10 34.427 41.315 3.358 o 1 10 1 0 17.716 17.949 1.744 o 1 10 1 1 101.898 106.335 1.049 o 1 10 1 2 9.523 8.001 2.969 < 1 10 1 3 41.820 43.222 1.495 o 1 10 1 4 40.633 41.114 1.678 o 1 10 1 5 102.611 102.862 1.767 o 1 10 1 6 6.157 3.528 3.434 < 1 10 1 7 14.063 9.464 3.650 < 1 10 1 8 6.963 11.960 3.767 < 1 10 1 9 48.396 48.148 2.756 o 1 10 1 10 3.788 3.370 2.735 < 1 10 2 0 116.064 127.357 1.548 o 1 10 2 1 12.176 12.804 1.417 < 1 10 2 2 38.625 40.727 1.471 o 1 10 2 3 4.075 7.569 2.522 < 1 10 2 4 98.889 97.509 1.626 o 1 10 2 5 5.499 .998 3.029 < 1 10 2 6 64.049 66.478 1.678 o 1 10 2 7 3.515 1.921 2.536 < 1 10 2 8 24.719 23.569 2.128 o 1 10 2 9 6.956 3.403 3.418 < 1 10 2 10 43.763 44.066 5.273 o 1 10 3 0 46.517 46.365 1.448 o 1 10 3 1 111.299 116.056 1.617 o 1 10 3 2 3.617 1.712 2.394 < 1 10 3 3 50.679 51.663 3.444 o 1 10 3 4 8.298 13.814 4.039 < 1 10 3 5 83.399 83.694 1.642 o 1 10 3 6 6.444 3.254 3.894 < 1 10 3 7 18.633 22.736 2.669 < 1 10 3 8 18.854 15.885 5.941 < 1 10 3 9 49.050 44.430 2.089 o 1 10 3 10 6.956 .420 3.841 < 1 10 4 0 107.546 113.981 1.601 o 1 10 4 1 6.805 2.322 2.479 < 1 10 4 2 55.325 57.685 2.570 o 1 10 4 3 16.197 20.254 2.384 < 1 10 4 4 98.984 100.405 1.655 o 1 10 4 5 9.962 11.784 4.882 < 1 10 4 6 59.853 58.922 1.775 o 1 10 4 7 6.129 3.571 3.379 < 1 10 4 8 10.364 16.339 4.358 < 1 10 4 9 5.886 4.646 3.602 < 1 10 4 10 41.787 41.737 2.362 o 1 10 5 0 46.623 44.749 1.746 o 1 10 5 1 95.143 97.393 1.112 o 1 10 5 2 12.620 9.567 1.713 < 1 10 5 3 41.383 43.418 1.770 o 1 10 5 4 6.642 8.945 3.247 < 1 10 5 5 82.418 84.843 1.731 o 1 10 5 6 3.908 2.313 2.542 < 1 10 5 7 10.111 17.619 5.369 < 1 10 5 8 12.681 6.633 1.963 < 1 10 5 9 35.853 38.309 4.056 o 1 10 5 10 4.830 .297 3.317 < 1 10 6 0 137.812 139.473 1.777 o 1 10 6 1 3.699 3.459 2.297 < 1 10 6 2 5.895 12.285 3.244 < 1 10 6 3 16.566 16.543 2.105 o 1 10 6 4 55.069 56.715 2.117 o 1 10 6 5 5.328 5.921 2.921 < 1 10 6 6 68.972 66.106 1.831 o 1 10 6 7 3.504 4.902 2.534 < 1 10 6 8 15.954 23.389 5.891 < 1 10 6 9 4.556 1.067 2.780 < 1 10 6 10 33.772 37.146 2.520 o 1 10 7 0 4.132 2.883 2.782 < 1 10 7 1 78.203 77.857 1.163 o 1 10 7 2 8.627 10.612 4.670 < 1 10 7 3 24.703 21.595 1.662 o 1 10 7 4 25.242 23.764 3.569 o 1 10 7 5 86.528 86.434 1.825 o 1 10 7 6 4.615 2.221 3.074 < 1 10 7 7 6.782 12.316 3.692 < 1 10 7 8 5.928 4.151 3.853 < 1 10 7 9 35.552 35.455 3.159 o 1 10 8 0 95.978 93.774 1.703 o 1 10 8 1 5.220 7.581 2.857 < 1 10 8 2 28.608 30.127 1.860 o 1 10 8 3 6.420 4.871 3.418 < 1 10 8 4 59.217 58.738 1.823 o 1 10 8 5 6.080 .838 3.326 < 1 10 8 6 52.725 49.214 2.216 o 1 10 8 7 8.291 7.191 4.053 < 1 10 8 8 10.215 17.844 4.890 < 1 10 8 9 6.602 1.709 3.521 < 1 10 9 0 7.976 10.036 3.884 < 1 10 9 1 72.427 69.405 1.415 o 1 10 9 2 7.824 4.156 3.333 < 1 10 9 3 23.822 23.690 2.096 o 1 10 9 4 21.615 18.021 2.934 o 1 10 9 5 65.681 67.519 1.957 o 1 10 9 6 5.927 7.097 3.858 < 1 10 9 7 14.410 14.760 3.764 < 1 10 9 8 10.910 10.297 4.076 < 1 10 9 9 31.061 32.377 2.698 o 1 10 10 0 59.186 60.305 3.316 o 1 10 10 1 4.689 3.128 2.641 < 1 10 10 2 35.909 38.771 2.052 o 1 10 10 3 3.603 5.447 2.516 < 1 10 10 4 64.726 67.288 1.972 o 1 10 10 5 7.402 1.581 4.402 < 1 10 10 6 30.818 33.086 4.379 o 1 10 10 7 4.332 .560 2.961 < 1 10 10 8 7.255 11.814 4.293 < 1 10 10 9 5.603 1.006 3.893 < 1 10 11 0 22.044 20.598 2.039 o 1 10 11 1 57.829 57.451 1.795 o 1 10 11 2 10.589 7.980 3.339 < 1 10 11 3 29.399 31.350 2.093 o 1 10 11 4 4.371 3.297 2.825 < 1 10 11 5 49.219 47.772 2.125 o 1 10 11 6 6.049 2.262 3.646 < 1 10 11 7 4.409 10.939 3.187 < 1 10 11 8 9.108 7.722 4.430 < 1 10 12 0 68.426 67.627 1.995 o 1 10 12 1 5.267 1.187 2.888 < 1 10 12 2 10.937 9.907 4.002 < 1 10 12 3 4.654 1.707 3.062 < 1 10 12 4 42.885 41.625 1.961 o 1 10 12 5 8.851 .524 3.758 < 1 10 12 6 36.019 35.243 2.441 o 1 10 12 7 5.117 2.405 3.446 < 1 10 12 8 9.997 12.660 5.326 < 1 10 13 0 8.352 9.519 4.053 < 1 10 13 1 45.062 43.662 1.648 o 1 10 13 2 5.572 1.783 3.351 < 1 10 13 3 17.419 17.371 1.943 o 1 10 13 4 6.881 5.947 4.653 < 1 10 13 5 43.331 44.737 3.271 o 1 10 13 6 5.380 3.876 3.514 < 1 10 13 7 8.634 5.287 4.719 < 1 10 14 0 56.122 53.860 2.140 o 1 10 14 1 6.858 2.376 3.781 < 1 10 14 2 8.167 8.603 4.300 < 1 10 14 3 4.038 .156 2.876 < 1 10 14 4 30.401 32.820 2.666 o 1 10 14 5 6.337 1.977 4.296 < 1 10 14 6 31.498 27.084 2.370 o 1 10 15 0 4.488 3.095 2.898 < 1 10 15 1 33.977 32.063 1.895 o 1 10 15 2 8.142 2.755 3.955 < 1 10 15 3 10.708 10.918 5.859 < 1 10 15 4 9.433 3.725 5.241 < 1 10 15 5 30.952 33.717 2.197 o 1 10 15 6 5.011 .747 2.996 < 1 10 16 0 28.208 27.522 2.696 o 1 10 16 1 5.418 .167 3.237 < 1 10 16 2 5.972 14.983 4.023 < 1 10 16 3 6.125 .364 3.680 < 1 10 16 4 32.223 27.613 2.521 o 1 10 16 5 5.961 .583 4.040 < 1 10 17 0 5.412 .912 3.518 < 1 10 17 1 24.702 22.672 3.424 o 1 10 17 2 6.385 .680 4.309 < 1 10 17 3 8.122 8.263 3.898 < 1 10 18 0 25.267 22.704 2.512 o 1 10 18 1 4.452 1.382 3.011 < 1 11 0 1 61.075 63.879 2.210 o 1 11 0 2 77.068 79.364 2.121 o 1 11 0 3 82.191 83.874 2.165 o 1 11 0 4 33.500 36.886 2.120 o 1 11 0 5 8.028 .457 3.395 < 1 11 0 6 55.447 57.129 2.670 o 1 11 0 7 61.114 61.797 2.559 o 1 11 0 8 31.744 32.839 2.795 o 1 11 0 9 12.730 21.674 6.116 < 1 11 0 10 10.412 3.672 5.051 < 1 11 1 1 45.112 47.246 1.049 o 1 11 1 2 95.089 101.817 2.782 o 1 11 1 3 25.135 24.971 1.579 o 1 11 1 4 51.204 51.842 1.568 o 1 11 1 5 9.972 21.752 4.918 < 1 11 1 6 43.752 45.064 1.763 o 1 11 1 7 39.259 37.163 1.843 o 1 11 1 8 44.286 48.039 3.096 o 1 11 1 9 18.339 16.213 2.245 o 1 11 1 10 5.999 7.809 4.028 < 1 11 2 1 50.729 50.393 1.302 o 1 11 2 2 77.854 82.195 1.532 o 1 11 2 3 75.575 79.708 1.558 o 1 11 2 4 23.939 25.244 1.599 o 1 11 2 5 5.745 3.436 3.134 < 1 11 2 6 38.026 37.759 1.887 o 1 11 2 7 56.102 56.838 2.933 o 1 11 2 8 36.438 32.511 2.006 o 1 11 2 9 28.777 21.860 1.856 o 1 11 2 10 3.909 6.293 2.723 < 1 11 3 1 1.226 2.106 2.078 < 1 11 3 2 86.186 90.518 2.650 o 1 11 3 3 59.540 59.643 1.601 o 1 11 3 4 38.840 39.352 1.625 o 1 11 3 5 2.990 .865 2.099 < 1 11 3 6 35.862 38.909 2.859 o 1 11 3 7 12.045 17.771 6.357 < 1 11 3 8 40.324 40.596 1.992 o 1 11 3 9 11.372 18.867 6.280 < 1 11 3 10 5.123 2.736 3.421 < 1 11 4 1 62.117 64.275 1.500 o 1 11 4 2 80.300 85.100 1.587 o 1 11 4 3 64.224 65.107 1.589 o 1 11 4 4 25.785 24.963 1.645 o 1 11 4 5 5.715 7.153 3.928 < 1 11 4 6 22.924 22.790 2.219 o 1 11 4 7 45.819 47.090 2.352 o 1 11 4 8 28.595 29.059 2.027 o 1 11 4 9 18.346 21.351 5.695 < 1 11 4 10 10.125 8.074 4.339 < 1 11 5 1 32.286 34.661 1.209 o 1 11 5 2 83.823 80.490 1.619 o 1 11 5 3 39.933 41.659 1.647 o 1 11 5 4 31.901 31.538 1.862 o 1 11 5 5 6.711 9.857 3.775 < 1 11 5 6 29.731 32.936 3.147 o 1 11 5 7 26.089 25.560 2.143 o 1 11 5 8 33.121 36.520 2.304 o 1 11 5 9 8.859 14.222 4.866 < 1 11 5 10 7.153 1.794 3.937 < 1 11 6 1 43.083 44.797 1.248 o 1 11 6 2 60.843 62.448 1.696 o 1 11 6 3 59.365 62.357 3.254 o 1 11 6 4 36.109 35.145 2.651 o 1 11 6 5 5.041 5.240 3.077 < 1 11 6 6 28.807 30.343 2.143 o 1 11 6 7 38.046 38.235 2.015 o 1 11 6 8 15.101 22.900 3.935 < 1 11 6 9 15.249 18.709 4.738 < 1 11 7 1 42.372 41.259 1.184 o 1 11 7 2 63.339 65.163 1.725 o 1 11 7 3 17.934 18.088 1.897 o 1 11 7 4 34.060 34.723 1.861 o 1 11 7 5 14.590 11.754 2.061 < 1 11 7 6 30.225 27.808 2.107 o 1 11 7 7 25.873 29.416 2.483 o 1 11 7 8 34.901 37.059 3.250 o 1 11 7 9 13.243 13.706 4.878 < 1 11 8 1 27.105 25.307 1.303 o 1 11 8 2 43.440 40.339 1.643 o 1 11 8 3 58.221 57.023 1.926 o 1 11 8 4 31.186 31.038 1.868 o 1 11 8 5 4.345 .824 2.954 < 1 11 8 6 29.421 28.207 4.023 o 1 11 8 7 36.374 38.335 2.828 o 1 11 8 8 18.416 22.027 3.933 < 1 11 8 9 13.575 16.143 4.217 < 1 11 9 1 5.098 2.741 2.819 < 1 11 9 2 55.196 54.752 1.900 o 1 11 9 3 40.580 37.974 1.741 o 1 11 9 4 28.973 27.194 2.766 o 1 11 9 5 12.013 8.191 3.175 < 1 11 9 6 22.521 26.047 2.640 < 1 11 9 7 15.121 17.897 7.193 < 1 11 9 8 34.093 30.712 2.220 o 1 11 9 9 13.826 14.105 5.119 < 1 11 10 1 32.075 29.531 1.540 o 1 11 10 2 43.122 44.080 2.048 o 1 11 10 3 47.144 46.379 3.292 o 1 11 10 4 21.638 14.632 1.876 o 1 11 10 5 5.136 .984 3.047 < 1 11 10 6 16.799 18.252 3.596 < 1 11 10 7 38.805 36.125 3.955 o 1 11 10 8 19.031 20.502 7.021 < 1 11 11 1 6.092 12.839 3.321 < 1 11 11 2 49.479 49.050 2.000 o 1 11 11 3 36.993 34.302 4.785 o 1 11 11 4 24.633 22.570 2.082 o 1 11 11 5 6.899 3.673 3.701 < 1 11 11 6 24.080 25.866 2.668 o 1 11 11 7 13.078 16.533 5.494 < 1 11 11 8 22.557 21.914 2.763 o 1 11 12 1 37.186 32.885 1.648 o 1 11 12 2 37.356 35.340 2.054 o 1 11 12 3 34.822 36.525 2.253 o 1 11 12 4 11.583 12.272 3.585 < 1 11 12 5 4.846 2.458 3.226 < 1 11 12 6 12.893 15.777 4.006 < 1 11 12 7 28.387 27.161 2.491 o 1 11 13 1 22.863 21.749 2.222 o 1 11 13 2 40.293 39.835 4.093 o 1 11 13 3 10.112 14.481 4.807 < 1 11 13 4 18.327 20.718 2.758 < 1 11 13 5 8.984 6.061 4.395 < 1 11 13 6 14.448 20.329 4.488 < 1 11 13 7 17.136 16.315 3.671 < 1 11 14 1 19.913 19.011 2.246 o 1 11 14 2 20.115 19.727 2.926 < 1 11 14 3 30.637 33.941 2.551 o 1 11 14 4 8.047 14.266 4.293 < 1 11 14 5 5.245 3.766 3.404 < 1 11 14 6 10.629 13.977 4.506 < 1 11 15 1 5.579 9.179 3.314 < 1 11 15 2 31.381 28.334 3.204 o 1 11 15 3 18.573 17.666 2.793 < 1 11 15 4 11.641 14.448 5.572 < 1 11 15 5 7.227 .620 4.863 < 1 11 16 1 14.333 10.990 3.057 < 1 11 16 2 17.062 17.479 3.652 < 1 11 16 3 19.032 23.443 4.071 < 1 11 16 4 8.527 9.375 4.678 < 1 11 17 1 11.316 4.841 2.939 < 1 11 17 2 21.784 18.287 3.122 o 1 12 0 0 6.165 .552 3.292 < 1 12 0 1 108.881 107.857 1.641 o 1 12 0 2 24.348 26.431 2.771 o 1 12 0 3 37.219 38.195 2.522 o 1 12 0 4 27.362 33.637 2.754 o 1 12 0 5 90.107 88.813 2.446 o 1 12 0 6 17.778 14.499 3.783 < 1 12 0 7 9.527 1.867 2.932 < 1 12 0 8 8.300 4.958 4.363 < 1 12 0 9 39.801 44.881 3.436 o 1 12 0 10 19.182 15.140 2.582 o 1 12 1 0 98.854 101.042 1.613 o 1 12 1 1 40.888 39.862 1.103 o 1 12 1 2 29.178 30.737 2.797 o 1 12 1 3 19.031 17.423 2.528 o 1 12 1 4 49.995 52.137 1.652 o 1 12 1 5 20.570 22.927 1.891 o 1 12 1 6 48.664 47.927 1.854 o 1 12 1 7 5.578 3.433 3.320 < 1 12 1 8 10.669 15.239 3.899 < 1 12 1 9 17.893 19.446 5.572 < 1 12 1 10 33.441 31.460 2.323 o 1 12 2 0 42.181 43.204 1.627 o 1 12 2 1 97.100 99.699 1.679 o 1 12 2 2 5.376 .957 2.907 < 1 12 2 3 39.769 39.225 1.550 o 1 12 2 4 14.329 12.203 2.011 < 1 12 2 5 82.791 87.738 2.950 o 1 12 2 6 26.295 26.078 1.831 o 1 12 2 7 5.212 8.174 3.346 < 1 12 2 8 5.820 8.072 3.451 < 1 12 2 9 42.096 40.987 5.962 o 1 12 2 10 11.287 11.512 4.754 < 1 12 3 0 79.966 84.357 1.680 o 1 12 3 1 39.158 38.733 1.626 o 1 12 3 2 21.750 24.498 2.586 o 1 12 3 3 9.178 9.200 3.376 < 1 12 3 4 57.627 60.896 5.244 o 1 12 3 5 32.257 33.154 1.713 o 1 12 3 6 47.527 48.912 1.837 o 1 12 3 7 9.805 .959 2.619 < 1 12 3 8 10.412 10.316 5.486 < 1 12 3 9 10.907 11.259 5.780 < 1 12 3 10 26.805 31.830 2.714 o 1 12 4 0 63.376 63.719 1.645 o 1 12 4 1 81.838 82.844 1.135 o 1 12 4 2 12.758 11.135 4.091 < 1 12 4 3 47.728 49.411 3.001 o 1 12 4 4 11.943 4.094 2.514 < 1 12 4 5 76.227 78.815 1.828 o 1 12 4 6 29.609 26.686 1.983 o 1 12 4 7 15.841 13.069 2.312 < 1 12 4 8 7.256 5.534 3.855 < 1 12 4 9 32.996 35.396 2.543 o 1 12 5 0 84.087 86.274 1.645 o 1 12 5 1 30.667 30.542 1.185 o 1 12 5 2 9.820 10.980 4.689 < 1 12 5 3 19.363 18.389 2.033 o 1 12 5 4 56.929 55.886 1.718 o 1 12 5 5 27.369 29.799 2.338 o 1 12 5 6 49.380 47.017 1.942 o 1 12 5 7 5.639 1.653 3.333 < 1 12 5 8 14.822 12.197 3.157 < 1 12 5 9 7.833 10.681 4.161 < 1 12 6 0 13.001 9.966 2.738 < 1 12 6 1 73.841 71.572 1.180 o 1 12 6 2 18.040 19.718 1.824 o 1 12 6 3 30.772 31.810 1.715 o 1 12 6 4 29.558 28.811 1.912 o 1 12 6 5 71.659 73.045 3.342 o 1 12 6 6 5.032 9.146 3.216 < 1 12 6 7 13.188 10.522 2.811 < 1 12 6 8 4.564 2.077 3.196 < 1 12 6 9 37.000 33.572 2.155 o 1 12 7 0 66.331 66.981 1.676 o 1 12 7 1 23.200 24.384 1.522 o 1 12 7 2 23.996 26.039 2.031 o 1 12 7 3 23.553 24.825 1.909 o 1 12 7 4 40.901 45.776 1.967 o 1 12 7 5 17.231 22.059 2.620 < 1 12 7 6 39.275 39.716 2.143 o 1 12 7 7 7.845 3.608 3.789 < 1 12 7 8 12.752 11.867 3.936 < 1 12 7 9 9.809 14.083 4.721 < 1 12 8 0 22.097 19.117 1.881 o 1 12 8 1 67.058 66.794 1.499 o 1 12 8 2 5.043 8.473 3.274 < 1 12 8 3 20.394 18.440 2.240 o 1 12 8 4 18.004 19.895 2.397 < 1 12 8 5 60.703 59.699 1.838 o 1 12 8 6 13.028 12.327 7.144 < 1 12 8 7 9.718 10.073 4.647 < 1 12 8 8 6.182 8.854 3.669 < 1 12 8 9 25.017 30.328 6.537 < 1 12 9 0 56.389 55.826 1.870 o 1 12 9 1 19.048 19.065 2.026 o 1 12 9 2 30.942 30.248 1.844 o 1 12 9 3 12.835 11.328 3.366 < 1 12 9 4 47.285 45.694 3.031 o 1 12 9 5 22.750 20.669 1.984 o 1 12 9 6 34.373 32.936 2.128 o 1 12 9 7 4.826 2.246 3.298 < 1 12 9 8 6.267 9.866 3.701 < 1 12 10 0 33.803 33.062 3.181 o 1 12 10 1 56.434 54.134 1.531 o 1 12 10 2 5.139 2.518 3.213 < 1 12 10 3 22.624 23.666 2.410 o 1 12 10 4 4.490 5.113 3.023 < 1 12 10 5 47.029 47.959 2.403 o 1 12 10 6 10.288 14.630 4.369 < 1 12 10 7 7.175 5.645 3.926 < 1 12 10 8 6.993 8.061 4.178 < 1 12 11 0 59.307 56.600 2.005 o 1 12 11 1 13.922 16.849 2.978 < 1 12 11 2 11.547 11.564 4.240 < 1 12 11 3 6.885 1.838 3.645 < 1 12 11 4 37.094 38.365 2.751 o 1 12 11 5 17.515 18.094 6.473 < 1 12 11 6 31.808 28.818 2.367 o 1 12 11 7 4.434 2.766 3.112 < 1 12 12 0 15.461 15.603 4.785 < 1 12 12 1 44.318 40.777 1.658 o 1 12 12 2 6.999 9.009 3.863 < 1 12 12 3 18.286 21.001 2.643 < 1 12 12 4 9.599 13.694 5.272 < 1 12 12 5 43.115 40.553 1.978 o 1 12 12 6 5.444 5.350 3.212 < 1 12 12 7 5.992 3.382 3.534 < 1 12 13 0 45.942 44.403 2.340 o 1 12 13 1 13.146 15.557 3.435 < 1 12 13 2 7.697 8.156 4.063 < 1 12 13 3 3.725 5.579 2.617 < 1 12 13 4 31.950 29.014 2.377 o 1 12 13 5 6.678 11.198 4.292 < 1 12 13 6 13.264 21.897 7.052 < 1 12 14 0 5.392 7.568 3.560 < 1 12 14 1 32.271 31.257 2.731 o 1 12 14 2 5.897 9.232 3.549 < 1 12 14 3 13.163 12.242 4.088 < 1 12 14 4 20.161 13.804 2.827 o 1 12 14 5 29.788 30.446 2.799 o 1 12 15 0 30.521 27.734 2.345 o 1 12 15 1 5.222 9.752 3.367 < 1 12 15 2 11.516 12.389 6.141 < 1 12 15 3 5.822 5.670 3.481 < 1 12 15 4 22.125 22.651 2.563 o 1 12 15 5 6.559 8.214 3.880 < 1 12 16 0 9.874 9.636 5.258 < 1 12 16 1 22.407 22.707 4.795 < 1 12 16 2 4.768 .376 3.337 < 1 12 16 3 5.604 7.992 3.611 < 1 12 17 0 26.801 20.157 2.631 o 1 12 17 1 9.566 4.735 4.589 < 1 13 0 1 34.665 34.070 1.689 o 1 13 0 2 99.776 104.665 2.466 o 1 13 0 3 24.260 23.610 2.394 o 1 13 0 4 41.650 40.701 2.408 o 1 13 0 5 7.753 5.116 4.167 < 1 13 0 6 47.279 48.511 2.653 o 1 13 0 7 15.251 14.998 4.749 < 1 13 0 8 52.375 51.391 2.727 o 1 13 0 9 7.758 3.728 4.236 < 1 13 1 1 35.610 37.645 1.117 o 1 13 1 2 16.526 15.363 2.152 o 1 13 1 3 78.043 82.371 1.716 o 1 13 1 4 15.987 16.155 2.408 < 1 13 1 5 7.807 6.300 3.764 < 1 13 1 6 10.766 8.941 5.146 < 1 13 1 7 45.715 45.500 2.965 o 1 13 1 8 10.313 12.366 4.347 < 1 13 1 9 17.462 20.974 2.581 < 1 13 2 1 11.838 13.072 3.088 < 1 13 2 2 89.082 92.895 1.712 o 1 13 2 3 33.029 32.336 3.401 o 1 13 2 4 41.367 44.370 1.738 o 1 13 2 5 11.568 8.883 4.331 < 1 13 2 6 49.156 47.023 1.840 o 1 13 2 7 8.136 12.336 3.904 < 1 13 2 8 44.069 45.117 2.062 o 1 13 2 9 7.106 4.672 3.763 < 1 13 3 1 64.394 65.401 1.173 o 1 13 3 2 16.822 14.481 1.718 o 1 13 3 3 47.771 49.724 1.748 o 1 13 3 4 9.466 13.931 3.981 < 1 13 3 5 9.695 10.362 4.214 < 1 13 3 6 3.846 1.940 2.646 < 1 13 3 7 46.954 46.831 2.163 o 1 13 3 8 8.641 11.456 5.557 < 1 13 3 9 11.765 18.504 6.245 < 1 13 4 1 7.840 12.354 3.296 < 1 13 4 2 80.210 82.879 1.714 o 1 13 4 3 26.118 30.113 1.721 o 1 13 4 4 43.386 42.176 2.828 o 1 13 4 5 3.693 4.806 2.580 < 1 13 4 6 41.651 40.210 2.071 o 1 13 4 7 13.891 14.009 3.629 < 1 13 4 8 40.081 37.633 5.148 o 1 13 4 9 6.707 4.919 4.294 < 1 13 5 1 43.251 44.514 1.298 o 1 13 5 2 5.004 11.185 3.254 < 1 13 5 3 55.652 58.213 1.731 o 1 13 5 4 8.447 14.144 4.636 < 1 13 5 5 3.319 2.332 2.464 < 1 13 5 6 4.692 1.529 3.162 < 1 13 5 7 42.118 39.603 3.128 o 1 13 5 8 8.421 10.598 4.032 < 1 13 5 9 17.185 21.389 7.259 < 1 13 6 1 16.244 16.913 1.466 o 1 13 6 2 78.815 77.260 1.767 o 1 13 6 3 5.720 14.511 3.410 < 1 13 6 4 33.485 36.329 2.108 o 1 13 6 5 5.888 4.729 3.169 < 1 13 6 6 30.537 32.114 6.538 < 1 13 6 7 19.118 16.957 1.725 o 1 13 6 8 35.727 39.352 2.412 o 1 13 6 9 6.725 4.726 3.558 < 1 13 7 1 18.341 17.625 2.042 o 1 13 7 2 10.754 4.820 3.925 < 1 13 7 3 59.700 62.883 1.853 o 1 13 7 4 17.618 12.882 2.183 < 1 13 7 5 9.911 4.178 3.108 < 1 13 7 6 6.900 3.731 2.901 < 1 13 7 7 34.245 36.002 2.123 o 1 13 7 8 9.101 10.094 5.401 < 1 13 8 1 3.507 4.241 2.414 < 1 13 8 2 59.943 62.775 1.954 o 1 13 8 3 16.290 14.502 2.236 < 1 13 8 4 31.948 30.863 3.774 o 1 13 8 5 4.751 2.020 3.115 < 1 13 8 6 30.554 28.678 2.020 o 1 13 8 7 11.299 9.728 4.159 < 1 13 8 8 36.016 34.867 2.181 o 1 13 9 1 32.871 32.069 1.736 o 1 13 9 2 6.893 10.734 4.084 < 1 13 9 3 43.816 43.741 2.992 o 1 13 9 4 6.902 4.906 3.773 < 1 13 9 5 4.806 4.370 3.193 < 1 13 9 6 7.295 2.422 3.850 < 1 13 9 7 35.565 37.575 2.582 o 1 13 9 8 7.216 8.849 3.967 < 1 13 10 1 5.743 7.417 3.124 < 1 13 10 2 50.835 52.809 2.058 o 1 13 10 3 10.594 17.685 5.110 < 1 13 10 4 31.680 29.460 2.131 o 1 13 10 5 5.342 3.872 3.705 < 1 13 10 6 34.221 30.474 2.186 o 1 13 10 7 9.542 7.806 5.669 < 1 13 11 1 36.829 34.278 2.018 o 1 13 11 2 12.029 14.141 4.427 < 1 13 11 3 39.312 39.334 2.690 o 1 13 11 4 4.167 3.605 2.959 < 1 13 11 5 7.631 .907 3.735 < 1 13 11 6 3.766 3.903 2.625 < 1 13 11 7 31.482 27.849 2.571 o 1 13 12 1 11.054 15.077 4.106 < 1 13 12 2 44.081 46.262 2.191 o 1 13 12 3 6.619 7.876 3.608 < 1 13 12 4 23.224 22.128 2.373 o 1 13 12 5 4.226 2.210 3.064 < 1 13 12 6 17.307 22.697 6.386 < 1 13 13 1 17.558 17.799 2.467 < 1 13 13 2 4.508 7.606 3.207 < 1 13 13 3 37.734 37.268 3.174 o 1 13 13 4 4.353 6.503 2.914 < 1 13 13 5 4.969 4.409 3.355 < 1 13 13 6 4.637 4.361 2.987 < 1 13 14 1 6.862 7.019 3.663 < 1 13 14 2 31.350 33.274 3.128 o 1 13 14 3 5.806 7.407 3.445 < 1 13 14 4 9.943 14.691 5.443 < 1 13 14 5 6.410 .675 3.545 < 1 13 15 1 14.189 13.731 5.209 < 1 13 15 2 4.842 6.272 3.284 < 1 13 15 3 25.814 24.182 2.428 o 1 13 15 4 5.555 5.321 3.305 < 1 13 16 1 5.885 1.971 3.481 < 1 13 16 2 23.333 22.687 2.977 o 1 14 0 0 74.233 73.213 2.346 o 1 14 0 1 57.108 56.702 1.629 o 1 14 0 2 37.993 39.908 2.508 o 1 14 0 3 8.267 12.612 4.002 < 1 14 0 4 61.489 67.633 2.553 o 1 14 0 5 40.296 39.833 2.434 o 1 14 0 6 26.773 26.681 2.623 o 1 14 0 7 11.598 8.153 4.280 < 1 14 0 8 13.735 14.645 5.065 < 1 14 0 9 17.248 24.381 5.367 < 1 14 1 0 44.372 47.352 1.653 o 1 14 1 1 52.549 52.745 1.192 o 1 14 1 2 25.276 25.935 1.845 o 1 14 1 3 12.328 16.359 5.179 < 1 14 1 4 25.899 27.731 2.017 o 1 14 1 5 48.102 49.688 4.175 o 1 14 1 6 27.173 25.476 1.935 o 1 14 1 7 12.754 16.485 4.724 < 1 14 1 8 5.251 7.860 3.540 < 1 14 1 9 27.006 22.743 2.584 o 1 14 2 0 77.423 81.218 1.685 o 1 14 2 1 50.442 49.410 1.182 o 1 14 2 2 20.169 20.847 2.809 o 1 14 2 3 11.976 17.977 3.727 < 1 14 2 4 53.468 55.977 1.983 o 1 14 2 5 42.277 44.015 2.098 o 1 14 2 6 32.401 33.412 2.041 o 1 14 2 7 3.391 7.740 2.354 < 1 14 2 8 10.021 17.133 4.832 < 1 14 2 9 19.392 22.079 6.027 < 1 14 3 0 53.722 55.209 1.699 o 1 14 3 1 42.754 43.984 2.013 o 1 14 3 2 5.558 2.563 3.316 < 1 14 3 3 13.769 14.417 2.928 < 1 14 3 4 23.136 22.499 3.184 o 1 14 3 5 46.488 49.298 1.959 o 1 14 3 6 28.108 32.099 2.073 o 1 14 3 7 7.799 10.159 4.143 < 1 14 3 8 16.002 8.856 2.268 < 1 14 3 9 19.798 18.653 2.978 < 1 14 4 0 79.541 81.091 1.706 o 1 14 4 1 36.109 37.228 1.253 o 1 14 4 2 12.322 5.748 2.610 < 1 14 4 3 20.247 24.507 6.305 < 1 14 4 4 48.623 45.696 1.870 o 1 14 4 5 46.481 46.362 1.811 o 1 14 4 6 35.944 36.045 1.885 o 1 14 4 7 5.473 5.591 3.489 < 1 14 4 8 14.759 15.889 4.606 < 1 14 4 9 18.701 19.999 2.654 < 1 14 5 0 29.398 31.399 2.152 o 1 14 5 1 42.624 42.633 1.241 o 1 14 5 2 4.540 3.649 3.115 < 1 14 5 3 10.103 12.868 4.229 < 1 14 5 4 33.451 33.655 2.549 o 1 14 5 5 42.692 42.854 1.867 o 1 14 5 6 13.785 20.310 5.795 < 1 14 5 7 8.242 7.976 3.479 < 1 14 5 8 7.172 6.059 3.897 < 1 14 5 9 16.476 17.879 4.286 < 1 14 6 0 49.854 49.853 1.770 o 1 14 6 1 36.138 37.964 1.778 o 1 14 6 2 26.776 25.136 2.266 o 1 14 6 3 23.140 24.032 2.543 o 1 14 6 4 49.092 47.068 2.910 o 1 14 6 5 36.099 36.343 2.306 o 1 14 6 6 25.532 26.766 2.035 o 1 14 6 7 5.186 3.697 3.329 < 1 14 6 8 7.753 9.482 4.248 < 1 14 7 0 30.141 30.207 1.869 o 1 14 7 1 42.551 43.577 1.723 o 1 14 7 2 13.578 15.813 3.566 < 1 14 7 3 11.591 10.416 3.587 < 1 14 7 4 34.940 29.417 2.177 o 1 14 7 5 34.838 35.038 2.046 o 1 14 7 6 18.118 14.790 2.247 o 1 14 7 7 8.892 11.140 4.910 < 1 14 7 8 9.969 6.356 5.898 < 1 14 8 0 46.922 46.032 1.907 o 1 14 8 1 38.572 37.440 1.588 o 1 14 8 2 19.599 19.666 1.965 o 1 14 8 3 10.694 11.091 4.525 < 1 14 8 4 35.023 37.537 2.574 o 1 14 8 5 31.127 28.771 4.278 o 1 14 8 6 27.345 26.122 2.031 o 1 14 8 7 6.473 1.079 3.544 < 1 14 8 8 8.528 10.075 4.541 < 1 14 9 0 43.062 39.674 1.976 o 1 14 9 1 32.416 34.738 2.774 o 1 14 9 2 5.421 9.774 3.176 < 1 14 9 3 10.223 11.616 5.420 < 1 14 9 4 7.094 13.921 3.794 < 1 14 9 5 31.199 32.898 2.808 o 1 14 9 6 12.008 19.529 5.771 < 1 14 9 7 6.804 7.401 4.055 < 1 14 10 0 53.688 51.564 1.965 o 1 14 10 1 28.798 28.671 2.181 o 1 14 10 2 5.873 4.852 3.446 < 1 14 10 3 3.915 6.277 2.807 < 1 14 10 4 28.524 30.177 2.334 o 1 14 10 5 24.153 27.649 2.469 o 1 14 10 6 24.120 24.717 3.492 o 1 14 10 7 4.395 .415 2.963 < 1 14 11 0 27.737 25.631 2.170 o 1 14 11 1 29.591 28.284 1.597 o 1 14 11 2 9.510 8.408 5.214 < 1 14 11 3 12.467 14.001 5.249 < 1 14 11 4 21.537 17.130 2.416 o 1 14 11 5 31.011 30.145 2.473 o 1 14 11 6 15.779 14.334 4.112 < 1 14 12 0 44.434 39.459 2.278 o 1 14 12 1 18.538 20.447 4.838 < 1 14 12 2 7.153 6.165 4.585 < 1 14 12 3 5.000 8.993 3.412 < 1 14 12 4 24.242 26.031 2.319 o 1 14 12 5 17.662 21.896 4.610 < 1 14 12 6 8.761 15.354 4.660 < 1 14 13 0 8.443 13.452 4.623 < 1 14 13 1 20.397 22.462 2.247 < 1 14 13 2 15.496 9.760 2.101 < 1 14 13 3 10.815 8.977 5.183 < 1 14 13 4 19.167 18.835 2.882 < 1 14 13 5 23.434 20.827 2.363 o 1 14 14 0 25.994 24.580 3.151 o 1 14 14 1 18.619 15.382 2.160 o 1 14 14 2 4.992 10.638 3.354 < 1 14 14 3 9.848 8.955 4.173 < 1 14 14 4 15.804 19.497 4.133 < 1 14 15 0 19.302 15.457 2.952 < 1 14 15 1 19.648 17.382 2.315 < 1 14 15 2 7.969 2.756 3.819 < 1 14 15 3 5.587 5.623 3.320 < 1 15 0 1 35.820 34.083 1.742 o 1 15 0 2 8.467 6.787 4.106 < 1 15 0 3 82.070 83.321 2.541 o 1 15 0 4 3.888 2.754 2.776 < 1 15 0 5 13.785 14.936 3.654 < 1 15 0 6 7.849 7.582 4.232 < 1 15 0 7 44.715 44.571 2.757 o 1 15 0 8 7.719 .115 4.293 < 1 15 0 9 13.761 17.037 5.794 < 1 15 1 1 6.060 5.852 3.237 < 1 15 1 2 61.045 60.432 1.751 o 1 15 1 3 6.246 7.159 4.144 < 1 15 1 4 31.674 32.616 1.816 o 1 15 1 5 3.675 6.274 2.582 < 1 15 1 6 24.888 24.568 1.990 o 1 15 1 7 4.368 .464 2.903 < 1 15 1 8 34.840 35.935 2.303 o 1 15 1 9 4.634 .536 3.005 < 1 15 2 1 49.723 49.796 1.804 o 1 15 2 2 11.648 8.720 3.075 < 1 15 2 3 62.957 67.009 1.757 o 1 15 2 4 3.658 .392 2.515 < 1 15 2 5 4.464 5.345 2.997 < 1 15 2 6 6.457 6.053 4.201 < 1 15 2 7 44.492 47.209 2.102 o 1 15 2 8 7.156 2.723 4.645 < 1 15 3 1 11.451 6.334 1.680 o 1 15 3 2 54.827 56.847 2.062 o 1 15 3 3 5.728 2.134 3.697 < 1 15 3 4 30.286 35.139 2.370 o 1 15 3 5 2.812 1.862 1.989 < 1 15 3 6 29.838 27.267 1.936 o 1 15 3 7 4.642 1.319 3.195 < 1 15 3 8 27.559 30.516 2.549 o 1 15 4 1 52.971 52.259 1.265 o 1 15 4 2 15.525 12.316 2.102 < 1 15 4 3 58.577 59.801 1.879 o 1 15 4 4 10.308 1.189 5.700 < 1 15 4 5 7.431 2.861 4.100 < 1 15 4 6 3.188 5.137 2.262 < 1 15 4 7 42.702 43.458 2.205 o 1 15 4 8 4.794 4.871 3.240 < 1 15 5 1 5.238 .559 2.857 < 1 15 5 2 58.357 59.658 1.804 o 1 15 5 3 5.509 2.660 3.274 < 1 15 5 4 32.242 33.944 2.098 o 1 15 5 5 5.471 2.418 3.017 < 1 15 5 6 25.335 26.687 7.843 < 1 15 5 7 3.980 1.147 2.773 < 1 15 5 8 32.246 30.044 2.142 o 1 15 6 1 31.998 31.509 1.489 o 1 15 6 2 12.730 14.869 4.744 < 1 15 6 3 64.887 66.028 1.934 o 1 15 6 4 5.391 3.254 3.233 < 1 15 6 5 13.473 11.648 3.568 < 1 15 6 6 7.544 5.818 4.054 < 1 15 6 7 27.344 34.780 8.474 < 1 15 6 8 11.944 1.716 3.144 < 1 15 7 1 9.822 8.725 4.187 < 1 15 7 2 56.640 51.267 1.869 o 1 15 7 3 6.989 1.359 3.693 < 1 15 7 4 27.814 27.253 2.017 o 1 15 7 5 4.748 1.202 3.243 < 1 15 7 6 27.034 22.061 2.158 o 1 15 7 7 7.267 3.306 3.887 < 1 15 7 8 30.536 30.836 2.544 o 1 15 8 1 35.677 32.005 1.732 o 1 15 8 2 7.249 9.624 3.510 < 1 15 8 3 50.572 49.280 1.949 o 1 15 8 4 5.974 3.659 3.890 < 1 15 8 5 5.703 3.472 4.106 < 1 15 8 6 8.379 7.409 4.658 < 1 15 8 7 35.560 34.969 2.272 o 1 15 9 1 5.139 .404 3.111 < 1 15 9 2 41.949 42.043 2.050 o 1 15 9 3 5.590 2.327 3.328 < 1 15 9 4 25.584 24.742 2.357 o 1 15 9 5 5.400 2.232 3.626 < 1 15 9 6 23.829 22.145 3.305 o 1 15 9 7 4.947 1.360 3.375 < 1 15 10 1 39.003 35.870 1.651 o 1 15 10 2 4.837 3.910 3.323 < 1 15 10 3 37.861 37.312 2.163 o 1 15 10 4 10.798 .147 3.386 < 1 15 10 5 5.180 .849 3.397 < 1 15 10 6 5.231 3.523 3.515 < 1 15 11 1 5.506 6.408 3.097 < 1 15 11 2 39.102 37.286 2.520 o 1 15 11 3 7.039 1.992 3.897 < 1 15 11 4 25.276 21.483 2.152 o 1 15 11 5 3.741 2.493 2.665 < 1 15 11 6 14.213 18.031 5.230 < 1 15 12 1 24.405 22.596 2.334 o 1 15 12 2 4.276 1.400 2.879 < 1 15 12 3 36.198 35.516 2.131 o 1 15 12 4 10.116 .354 3.177 < 1 15 12 5 5.518 3.586 3.599 < 1 15 13 1 2.999 .572 2.136 < 1 15 13 2 30.581 28.136 2.472 o 1 15 13 3 9.367 .891 5.217 < 1 15 13 4 10.171 13.972 5.568 < 1 15 14 1 16.324 14.800 2.387 < 1 15 14 2 5.938 1.933 3.990 < 1 15 14 3 24.225 25.215 3.012 o 1 15 15 1 5.028 1.818 3.265 < 1 16 0 0 59.546 60.962 2.604 o 1 16 0 1 22.136 25.296 2.201 o 1 16 0 2 16.164 17.208 4.215 < 1 16 0 3 13.618 10.189 4.234 < 1 16 0 4 43.997 40.925 2.366 o 1 16 0 5 22.629 25.783 3.017 o 1 16 0 6 31.187 31.412 2.730 o 1 16 0 7 10.461 9.649 4.438 < 1 16 0 8 16.475 14.325 4.320 < 1 16 1 0 33.148 29.575 1.639 o 1 16 1 1 34.869 35.001 1.360 o 1 16 1 2 20.227 18.622 1.929 o 1 16 1 3 9.561 11.642 4.001 < 1 16 1 4 35.783 35.122 2.700 o 1 16 1 5 37.191 39.210 2.065 o 1 16 1 6 17.344 21.015 2.462 o 1 16 1 7 5.567 8.935 3.593 < 1 16 1 8 5.586 7.707 3.810 < 1 16 2 0 58.009 57.191 2.287 o 1 16 2 1 26.739 26.244 1.831 o 1 16 2 2 16.821 16.257 2.086 o 1 16 2 3 10.558 8.008 3.878 < 1 16 2 4 42.254 43.502 1.886 o 1 16 2 5 22.211 25.639 2.440 o 1 16 2 6 29.133 29.849 2.116 o 1 16 2 7 8.718 5.856 4.790 < 1 16 2 8 16.217 12.852 3.482 < 1 16 3 0 49.705 51.677 1.871 o 1 16 3 1 35.802 34.779 1.343 o 1 16 3 2 6.142 3.780 3.583 < 1 16 3 3 8.254 13.448 4.361 < 1 16 3 4 19.950 20.729 2.419 o 1 16 3 5 39.719 37.823 1.838 o 1 16 3 6 22.870 23.445 2.142 o 1 16 3 7 5.042 9.433 3.389 < 1 16 3 8 10.190 9.215 6.098 < 1 16 4 0 51.028 50.389 2.325 o 1 16 4 1 26.989 26.099 1.513 o 1 16 4 2 14.866 16.176 3.888 < 1 16 4 3 4.737 5.451 3.012 < 1 16 4 4 42.513 45.063 1.939 o 1 16 4 5 21.244 24.093 4.540 < 1 16 4 6 25.363 25.066 2.349 o 1 16 4 7 3.770 2.825 2.624 < 1 16 4 8 7.352 11.812 3.919 < 1 16 5 0 41.014 39.673 2.886 o 1 16 5 1 37.118 37.763 1.368 o 1 16 5 2 13.416 11.981 2.050 < 1 16 5 3 9.993 13.400 4.197 < 1 16 5 4 24.942 26.614 2.394 o 1 16 5 5 34.387 33.628 2.186 o 1 16 5 6 12.237 14.396 4.498 < 1 16 5 7 13.419 8.240 5.694 < 1 16 5 8 5.866 4.407 3.912 < 1 16 6 0 53.012 53.645 1.914 o 1 16 6 1 25.329 22.767 1.606 o 1 16 6 2 10.641 13.733 3.917 < 1 16 6 3 8.159 8.086 4.331 < 1 16 6 4 39.124 36.612 2.202 o 1 16 6 5 16.836 20.311 5.205 < 1 16 6 6 23.561 22.390 2.325 o 1 16 6 7 4.618 6.953 3.315 < 1 16 7 0 21.821 23.410 2.566 o 1 16 7 1 35.383 36.239 1.492 o 1 16 7 2 16.162 12.969 2.490 o 1 16 7 3 8.716 7.252 3.654 < 1 16 7 4 27.277 27.195 2.288 o 1 16 7 5 24.396 29.388 6.352 < 1 16 7 6 10.548 12.262 5.040 < 1 16 7 7 4.349 6.513 3.051 < 1 16 8 0 48.058 48.738 1.996 o 1 16 8 1 18.783 16.916 2.567 o 1 16 8 2 8.795 11.878 4.199 < 1 16 8 3 6.430 7.967 3.528 < 1 16 8 4 27.190 28.418 2.154 o 1 16 8 5 18.332 18.755 2.583 < 1 16 8 6 22.201 21.972 2.598 o 1 16 8 7 5.520 7.071 3.564 < 1 16 9 0 31.448 29.208 2.185 o 1 16 9 1 28.837 26.942 2.666 o 1 16 9 2 5.390 1.765 3.626 < 1 16 9 3 10.815 7.281 3.964 < 1 16 9 4 16.375 15.587 4.263 < 1 16 9 5 29.059 27.453 2.102 o 1 16 9 6 15.733 17.347 4.120 < 1 16 10 0 37.720 32.831 2.191 o 1 16 10 1 16.329 16.133 2.350 o 1 16 10 2 5.969 8.132 3.278 < 1 16 10 3 6.343 5.292 3.750 < 1 16 10 4 25.629 27.182 3.222 o 1 16 10 5 21.622 18.415 2.295 o 1 16 10 6 20.559 17.754 2.565 o 1 16 11 0 31.703 27.955 2.649 o 1 16 11 1 22.534 18.263 4.812 < 1 16 11 2 3.431 3.037 2.431 < 1 16 11 3 8.230 8.522 5.276 < 1 16 11 4 11.416 13.422 5.468 < 1 16 11 5 23.898 22.974 2.532 o 1 16 12 0 18.915 22.574 9.055 < 1 16 12 1 8.920 15.104 4.731 < 1 16 12 2 9.708 7.444 4.107 < 1 16 12 3 11.081 4.043 2.376 < 1 16 12 4 22.530 21.158 2.758 o 1 16 13 0 15.377 14.791 5.646 < 1 16 13 1 10.578 16.274 4.460 < 1 16 13 2 5.508 7.903 3.786 < 1 16 13 3 8.374 6.832 4.593 < 1 16 14 0 25.217 23.578 2.843 o 1 16 14 1 12.803 10.940 3.974 < 1 16 14 2 6.100 4.409 4.051 < 1 17 0 1 27.453 25.294 3.649 o 1 17 0 2 45.107 42.972 2.597 o 1 17 0 3 9.988 15.202 5.287 < 1 17 0 4 18.076 26.425 5.602 < 1 17 0 5 8.446 .445 3.127 < 1 17 0 6 17.914 23.513 5.550 < 1 17 0 7 10.812 15.230 5.779 < 1 17 0 8 29.860 25.630 3.183 o 1 17 1 1 27.385 28.697 1.487 o 1 17 1 2 9.959 12.230 5.242 < 1 17 1 3 46.215 48.445 1.977 o 1 17 1 4 8.341 9.923 3.523 < 1 17 1 5 7.402 .873 3.575 < 1 17 1 6 7.370 7.440 3.891 < 1 17 1 7 35.856 34.661 3.553 o 1 17 2 1 12.702 12.329 1.900 < 1 17 2 2 46.397 44.390 1.880 o 1 17 2 3 26.789 24.608 1.977 o 1 17 2 4 25.963 26.717 1.892 o 1 17 2 5 5.035 6.576 3.046 < 1 17 2 6 22.597 21.942 2.500 o 1 17 2 7 11.570 12.279 4.884 < 1 17 3 1 33.627 33.267 1.513 o 1 17 3 2 16.699 14.187 1.948 < 1 17 3 3 46.209 48.680 1.939 o 1 17 3 4 9.834 9.716 4.140 < 1 17 3 5 6.092 1.451 3.646 < 1 17 3 6 8.812 5.545 4.184 < 1 17 3 7 30.088 29.726 2.746 o 1 17 4 1 9.500 8.177 2.937 < 1 17 4 2 44.323 48.237 2.729 o 1 17 4 3 31.844 28.956 2.038 o 1 17 4 4 24.266 24.239 2.287 o 1 17 4 5 4.045 8.195 2.957 < 1 17 4 6 21.064 20.026 2.316 o 1 17 4 7 9.125 12.624 5.009 < 1 17 5 1 35.252 33.009 1.465 o 1 17 5 2 12.207 16.463 3.769 < 1 17 5 3 45.869 47.886 2.119 o 1 17 5 4 5.212 9.890 3.465 < 1 17 5 5 9.167 6.288 4.442 < 1 17 5 6 4.349 6.647 2.929 < 1 17 5 7 26.076 26.195 2.755 o 1 17 6 1 20.799 20.868 2.383 o 1 17 6 2 48.307 44.510 1.980 o 1 17 6 3 18.549 16.306 2.272 o 1 17 6 4 20.406 18.736 2.106 o 1 17 6 5 3.956 1.529 2.774 < 1 17 6 6 10.292 18.592 4.931 < 1 17 6 7 11.580 16.358 4.911 < 1 17 7 1 27.538 27.266 1.694 o 1 17 7 2 12.633 12.277 3.898 < 1 17 7 3 36.851 38.101 2.259 o 1 17 7 4 13.032 7.869 3.416 < 1 17 7 5 6.118 4.271 4.195 < 1 17 7 6 8.331 9.004 3.992 < 1 17 8 1 16.411 14.793 2.136 < 1 17 8 2 36.548 33.805 2.183 o 1 17 8 3 13.248 13.921 4.884 < 1 17 8 4 15.882 18.239 4.141 < 1 17 8 5 8.574 5.897 4.156 < 1 17 8 6 17.196 18.217 2.132 o 1 17 9 1 25.003 24.906 2.040 o 1 17 9 2 5.283 9.321 3.390 < 1 17 9 3 26.836 30.779 3.651 o 1 17 9 4 7.391 3.372 4.925 < 1 17 9 5 3.666 .755 2.629 < 1 17 10 1 7.401 4.690 3.527 < 1 17 10 2 27.245 29.384 2.549 o 1 17 10 3 15.088 14.678 8.066 < 1 17 10 4 16.915 17.487 3.620 < 1 17 10 5 8.967 5.871 3.836 < 1 17 11 1 11.429 17.470 5.472 < 1 17 11 2 9.857 7.599 4.148 < 1 17 11 3 28.788 27.710 4.388 o 1 17 11 4 6.444 4.161 4.130 < 1 17 12 1 8.365 6.964 4.028 < 1 17 12 2 23.319 23.147 2.694 o 1 17 12 3 10.046 8.816 4.235 < 1 17 13 1 11.292 12.957 4.753 < 1 17 13 2 8.190 6.629 5.247 < 1 18 0 0 4.328 2.159 2.989 < 1 18 0 1 33.248 33.274 2.093 o 1 18 0 2 11.389 6.828 4.226 < 1 18 0 3 14.681 11.080 4.546 < 1 18 0 4 5.250 3.558 3.462 < 1 18 0 5 40.918 36.860 2.598 o 1 18 0 6 6.226 11.047 3.996 < 1 18 0 7 12.919 4.797 4.760 < 1 18 1 0 50.185 48.356 1.950 o 1 18 1 1 11.501 14.259 3.016 < 1 18 1 2 6.725 10.380 3.671 < 1 18 1 3 4.006 4.279 2.894 < 1 18 1 4 31.683 31.156 2.254 o 1 18 1 5 7.531 13.679 4.153 < 1 18 1 6 27.269 26.152 2.242 o 1 18 1 7 4.151 1.956 2.752 < 1 18 2 0 4.867 8.597 3.111 < 1 18 2 1 39.151 34.549 1.329 o 1 18 2 2 10.183 1.885 3.170 < 1 18 2 3 8.217 11.856 4.877 < 1 18 2 4 4.547 .792 2.975 < 1 18 2 5 34.555 35.097 2.086 o 1 18 2 6 13.019 9.326 4.053 < 1 18 2 7 5.705 6.841 3.388 < 1 18 3 0 37.045 41.231 2.515 o 1 18 3 1 13.191 13.405 3.459 < 1 18 3 2 19.795 20.457 2.286 o 1 18 3 3 7.031 6.287 3.769 < 1 18 3 4 36.845 38.413 4.463 o 1 18 3 5 9.944 10.973 4.212 < 1 18 3 6 9.905 21.530 4.777 < 1 18 3 7 6.568 .048 3.685 < 1 18 4 0 6.157 11.544 3.634 < 1 18 4 1 40.032 36.779 1.510 o 1 18 4 2 6.815 .163 3.341 < 1 18 4 3 6.970 14.351 4.157 < 1 18 4 4 6.743 2.629 4.543 < 1 18 4 5 29.860 32.411 2.213 o 1 18 4 6 11.214 4.704 4.134 < 1 18 5 0 47.009 45.987 2.227 o 1 18 5 1 9.851 12.114 3.645 < 1 18 5 2 12.057 13.267 5.783 < 1 18 5 3 9.697 9.977 4.132 < 1 18 5 4 32.883 31.773 2.232 o 1 18 5 5 9.256 8.765 4.449 < 1 18 5 6 21.872 23.277 2.532 o 1 18 6 0 4.127 3.987 2.842 < 1 18 6 1 35.395 32.982 2.198 o 1 18 6 2 3.866 2.961 2.780 < 1 18 6 3 17.930 12.934 1.919 o 1 18 6 4 6.252 6.340 4.238 < 1 18 6 5 31.689 30.751 2.194 o 1 18 6 6 5.378 4.035 3.569 < 1 18 7 0 45.803 44.699 2.243 o 1 18 7 1 8.922 9.386 3.299 < 1 18 7 2 4.819 6.348 3.252 < 1 18 7 3 6.821 7.424 3.782 < 1 18 7 4 26.168 24.962 2.549 o 1 18 7 5 6.091 9.676 3.629 < 1 18 7 6 12.351 23.671 6.588 < 1 18 8 0 8.078 5.215 5.168 < 1 18 8 1 30.297 26.629 1.804 o 1 18 8 2 5.516 2.166 3.545 < 1 18 8 3 6.140 10.177 3.638 < 1 18 8 4 6.595 2.030 3.588 < 1 18 8 5 29.245 28.329 3.004 o 1 18 9 0 37.036 30.646 2.086 o 1 18 9 1 7.482 9.147 4.459 < 1 18 9 2 18.431 9.947 2.027 o 1 18 9 3 8.481 1.475 5.489 < 1 18 9 4 27.908 25.031 2.362 o 1 18 9 5 7.099 9.525 3.791 < 1 18 10 0 10.166 8.507 6.042 < 1 18 10 1 23.536 21.249 2.838 o 1 18 10 2 6.689 2.918 3.678 < 1 18 10 3 12.234 8.804 4.511 < 1 18 10 4 4.399 1.101 2.964 < 1 18 11 0 22.775 22.250 2.504 o 1 18 11 1 10.226 8.221 3.782 < 1 18 11 2 9.197 9.286 4.425 < 1 18 11 3 10.103 .801 5.409 < 1 18 12 0 5.518 3.299 3.513 < 1 18 12 1 19.502 17.923 2.894 o 1 19 0 1 16.657 18.719 4.345 < 1 19 0 2 20.063 24.653 4.286 < 1 19 0 3 15.237 20.673 5.578 < 1 19 0 4 11.652 11.598 4.910 < 1 19 0 5 5.826 5.815 2.858 < 1 19 0 6 9.743 14.558 5.346 < 1 19 1 1 20.487 18.846 1.704 o 1 19 1 2 32.712 33.290 2.081 o 1 19 1 3 25.812 23.670 2.323 o 1 19 1 4 19.659 18.158 2.657 < 1 19 1 5 5.701 3.633 3.402 < 1 19 1 6 19.615 18.324 2.835 o 1 19 2 1 19.075 15.219 1.691 o 1 19 2 2 27.236 25.240 3.235 o 1 19 2 3 26.225 25.690 2.179 o 1 19 2 4 12.638 12.348 5.324 < 1 19 2 5 5.380 1.960 3.247 < 1 19 2 6 13.777 12.081 3.593 < 1 19 3 1 13.603 11.681 1.990 < 1 19 3 2 34.044 35.431 2.321 o 1 19 3 3 27.307 28.724 2.171 o 1 19 3 4 12.307 14.653 5.890 < 1 19 3 5 6.974 2.623 3.859 < 1 19 3 6 11.121 15.436 5.918 < 1 19 4 1 15.813 14.981 1.978 < 1 19 4 2 24.607 24.087 2.503 o 1 19 4 3 22.531 27.197 2.769 o 1 19 4 4 9.683 13.020 3.559 < 1 19 4 5 6.691 .972 3.702 < 1 19 4 6 10.727 10.530 5.134 < 1 19 5 1 16.570 14.924 1.876 o 1 19 5 2 31.933 36.459 8.353 < 1 19 5 3 21.053 21.251 2.813 o 1 19 5 4 16.281 11.994 4.246 < 1 19 5 5 7.301 .412 3.556 < 1 19 6 1 13.357 19.477 3.484 < 1 19 6 2 19.899 19.476 2.417 o 1 19 6 3 19.396 20.672 2.946 < 1 19 6 4 5.301 9.897 3.419 < 1 19 6 5 6.952 2.309 3.760 < 1 19 7 1 14.962 15.294 4.655 < 1 19 7 2 27.805 29.455 2.209 o 1 19 7 3 13.477 14.707 4.172 < 1 19 7 4 15.664 13.662 4.093 < 1 19 7 5 3.703 1.938 2.610 < 1 19 8 1 18.593 14.432 2.110 o 1 19 8 2 13.745 17.037 5.788 < 1 19 8 3 23.933 19.296 2.382 o 1 19 8 4 7.968 6.090 4.225 < 1 19 9 1 4.527 8.800 2.910 < 1 19 9 2 21.029 22.231 5.491 < 1 19 9 3 17.905 16.436 4.679 < 1 19 10 1 6.934 7.478 3.656 < 1 19 10 2 13.529 16.354 4.981 < 1 19 11 1 7.941 8.804 3.804 < 1 20 0 0 38.063 38.564 3.138 o 1 20 0 1 7.048 5.589 3.775 < 1 20 0 2 8.925 7.208 4.867 < 1 20 0 3 4.756 2.440 3.428 < 1 20 0 4 13.873 19.589 5.823 < 1 20 0 5 6.368 1.319 4.414 < 1 20 1 0 5.669 4.409 3.372 < 1 20 1 1 34.389 33.453 2.011 o 1 20 1 2 5.933 3.758 3.571 < 1 20 1 3 14.616 12.557 3.824 < 1 20 1 4 10.737 4.277 4.565 < 1 20 1 5 33.514 30.474 4.052 o 1 20 2 0 35.714 31.829 3.138 o 1 20 2 1 6.705 3.682 3.237 < 1 20 2 2 10.675 11.273 5.864 < 1 20 2 3 3.696 1.990 2.608 < 1 20 2 4 22.814 22.136 2.617 o 1 20 2 5 5.306 1.886 3.553 < 1 20 3 0 4.856 2.764 3.259 < 1 20 3 1 35.137 30.881 1.604 o 1 20 3 2 7.805 .387 3.791 < 1 20 3 3 11.447 14.195 6.103 < 1 20 3 4 6.746 1.996 3.592 < 1 20 3 5 22.387 28.052 2.960 o 1 20 4 0 29.387 27.142 2.282 o 1 20 4 1 4.415 .396 2.890 < 1 20 4 2 5.647 10.565 3.646 < 1 20 4 3 4.587 .778 3.073 < 1 20 4 4 25.260 21.403 2.455 o 1 20 4 5 8.003 5.006 4.796 < 1 20 5 0 6.800 1.431 3.672 < 1 20 5 1 29.213 27.693 2.630 o 1 20 5 2 5.997 .174 3.328 < 1 20 5 3 11.213 13.574 4.742 < 1 20 5 4 4.369 2.146 2.918 < 1 20 6 0 32.196 30.514 2.530 o 1 20 6 1 2.949 .470 2.118 < 1 20 6 2 7.179 4.122 4.235 < 1 20 6 3 3.523 1.180 2.494 < 1 20 6 4 15.597 17.735 4.049 < 1 20 7 0 4.449 .663 2.929 < 1 20 7 1 25.912 24.406 1.772 o 1 20 7 2 7.686 1.967 3.732 < 1 20 7 3 5.278 10.587 3.402 < 1 20 8 0 27.833 25.302 2.650 o 1 20 8 1 9.493 2.853 2.971 < 1 20 8 2 6.049 7.693 3.885 < 1 20 8 3 4.578 2.591 3.147 < 1 20 9 0 4.726 3.854 3.168 < 1 20 9 1 24.294 22.138 1.887 o 1 20 9 2 6.773 .062 3.749 < 1 21 0 1 13.691 14.742 6.540 < 1 21 0 2 16.622 13.781 4.331 < 1 21 0 3 22.540 21.089 3.296 o 1 21 0 4 5.704 11.231 3.814 < 1 21 1 1 6.661 12.348 3.671 < 1 21 1 2 31.481 29.349 4.215 o 1 21 1 3 11.920 13.194 4.380 < 1 21 1 4 8.927 9.845 3.759 < 1 21 2 1 17.468 14.097 1.878 o 1 21 2 2 14.969 14.411 6.306 < 1 21 2 3 13.726 19.502 6.565 < 1 21 2 4 4.914 8.348 3.278 < 1 21 3 1 5.179 7.948 3.061 < 1 21 3 2 26.961 26.406 3.788 o 1 21 3 3 14.503 15.546 4.511 < 1 21 3 4 12.348 13.070 3.834 < 1 21 4 1 15.851 12.857 2.097 o 1 21 4 2 11.046 15.177 5.291 < 1 21 4 3 19.356 17.819 2.761 o 1 21 4 4 10.288 6.001 4.338 < 1 21 5 1 7.962 11.616 4.237 < 1 21 5 2 21.275 22.430 2.886 < 1 21 5 3 9.809 13.002 4.132 < 1 21 6 1 6.395 10.939 3.797 < 1 21 6 2 4.452 13.778 3.229 < 1 21 6 3 18.913 16.768 1.901 o 1 21 7 1 18.637 11.649 1.984 o 1 21 7 2 23.660 20.258 2.520 o 1 22 0 0 6.444 10.531 4.253 < 1 22 0 1 18.822 17.919 4.021 < 1 22 0 2 6.300 5.895 3.047 < 1 22 0 3 8.077 10.130 4.429 < 1 22 1 0 28.588 26.046 2.293 o 1 22 1 1 6.571 13.323 3.622 < 1 22 1 2 6.785 4.457 3.716 < 1 22 1 3 10.381 5.960 3.851 < 1 22 2 0 11.130 10.121 4.092 < 1 22 2 1 23.223 18.785 1.714 o 1 22 2 2 4.382 1.569 2.981 < 1 22 3 0 21.389 26.004 10.255 < 1 22 3 1 6.961 7.923 3.706 < 1 22 3 2 4.564 7.545 3.041 < 1 22 4 0 4.118 5.862 2.893 < 1 22 4 1 18.493 19.369 2.253 < 1 22 4 2 8.315 1.202 2.628 < 1 22 5 0 20.921 24.828 4.478 < 1 22 5 1 6.029 5.103 3.880 < 1 _publ_requested_journal ? #ActaC _publ_requested_coeditor_name ? #ActaC _publ_contact_author #ActaC ; ? name ? institute ? department ? address ? city ? country ; _publ_contact_letter #ActaC ; ? letter to co-editor ; _publ_contact_author_phone ? #ActaC _publ_contact_author_fax ? #ActaC _publ_contact_author_email ? #ActaC loop_ _publ_author_name #ActaC _publ_author_address #ActaC '? surname, initials' ; ? institute ? department ? address ? city ? country ; _publ_section_title #ActaC ; ? ; _publ_section_abstract #ActaC ; ? ; _publ_section_comment #ActaC ; ? ; _publ_section_experimental #ActaC ; ? ; _publ_section_references #ActaC ; ? ; _publ_section_figure_captions #ActaC ; ? ; _publ_section_acknowledgements #ActaC ; ? ; #============================================================================== # (IUCr Office Use Only) _journal_date_recd_electronic ? _journal_date_to_coeditor ? _journal_date_from_coeditor ? _journal_date_accepted ? _journal_date_printers_first ? _journal_date_printers_final ? _journal_date_proofs_out ? _journal_date_proofs_in ? _journal_coeditor_name ? _journal_coeditor_code ? _journal_coeditor_notes ; ? ; _journal_techeditor_code ? _journal_techeditor_notes ; ? ; _journal_coden_ASTM ? _journal_name_full ? _journal_year ? _journal_volume ? _journal_issue ? _journal_page_first ? _journal_page_last ? _journal_suppl_publ_number ? _journal_suppl_publ_pages ? #=END data_sm427 #------------------------------------------------------------------------------ _audit_creation_date 'Mon Feb 9 00:04:08 1998' _audit_creation_method 'from TEXRAY.INF file' _audit_update_record ? #------------------------------------------------------------------------------ _computing_data_collection 'MSC/AFC Diffractometer Control' _computing_cell_refinement 'MSC/AFC Diffractometer Control' _computing_data_reduction 'teXsan' _computing_structure_solution SHELXS86 _computing_structure_refinement 'teXsan' _computing_publication_material 'teXsan' #------------------------------------------------------------------------------ _cell_length_a 10.226(4) _cell_length_b 17.827(7) _cell_length_c 16.267(6) _cell_angle_alpha 90 _cell_angle_beta 97.92(3) _cell_angle_gamma 90 _cell_volume 2937(1) _cell_formula_units_Z 4 _cell_measurement_temperature 173.2 _cell_measurement_reflns_used 50 _cell_measurement_theta_min 9.3 _cell_measurement_theta_max 21.4 #------------------------------------------------------------------------------ _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M 'P 21/n ' _symmetry_Int_Tables_number 14 _symmetry_space_group_name_Hall ? loop_ _symmetry_equiv_pos_as_xyz ' +x, +y, +z' '1/2-x,1/2+y,1/2-z' ' -x, -y, -z' '1/2+x,1/2-y,1/2+z' #------------------------------------------------------------------------------ _exptl_crystal_description 'prismatic' _exptl_crystal_colour 'colourlessprismatic' _exptl_crystal_size_max 0.000 _exptl_crystal_size_mid 0.000 _exptl_crystal_size_min 0.000 _exptl_crystal_density_diffrn 1.011 _exptl_crystal_density_meas ? _chemical_formula_weight 447.03 _chemical_formula_analytical ? _chemical_formula_sum 'C18 H46 Cl Li3 N4 O Si2 ' _chemical_formula_moiety 'C18 H46 Cl Li3 N4 O Si2 ' _chemical_formula_structural ? _chemical_compound_source ? _exptl_crystal_F_000 976.00 _exptl_absorpt_coefficient_mu 0.225 _exptl_absorpt_correction_type refdelf _exptl_absorpt_process_details Walker&Stuart_DIFABS _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.648 #------------------------------------------------------------------------------ _diffrn_special_details none _diffrn_ambient_temperature 173.2 _diffrn_radiation_wavelength 0.7107 _diffrn_radiation_type MoKalpha _diffrn_radiation_source 'X-ray tube' _diffrn_radiation_monochromator graphite _diffrn_radiation_detector ? _diffrn_measurement_device 'NICOLET' _diffrn_measurement_method 'omega scans with profile analysis' _diffrn_standards_number 3 _diffrn_standards_interval_count 397 _diffrn_standards_decay_% 0.00 loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? ? ? ? ? ? ? _diffrn_reflns_number 4235 _reflns_number_total 3979 _reflns_number_observed 1186 _reflns_observed_criterion 2.00 _diffrn_reflns_av_R_equivalents 9.91 _diffrn_reflns_av_sigmaI/netI ? _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 0 _diffrn_reflns_limit_k_min 0 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_theta_min ? _diffrn_reflns_theta_max 22.50 _diffrn_reflns_reduction_process ? _diffrn_orient_matrix_UB_11 -0.03856 _diffrn_orient_matrix_UB_12 0.05164 _diffrn_orient_matrix_UB_13 -0.00342 _diffrn_orient_matrix_UB_21 0.02162 _diffrn_orient_matrix_UB_22 0.00513 _diffrn_orient_matrix_UB_23 -0.05785 _diffrn_orient_matrix_UB_31 -0.08828 _diffrn_orient_matrix_UB_32 -0.02130 _diffrn_orient_matrix_UB_33 -0.02223 #------------------------------------------------------------------------------ loop_ _atom_type_symbol _atom_type_oxidation_number _atom_type_number_in_cell _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C 0 72 0.003 0.002 'International Tables' H 0 184 0.000 0.000 'International Tables' N 0 16 0.006 0.003 'International Tables' Si 0 8 0.082 0.070 'International Tables' O 0 4 0.011 0.006 'International Tables' Li 0 12 0.000 0.000 'International Tables' Cl 0 4 0.148 0.159 'International Tables' #------------------------------------------------------------------------------ loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_thermal_displace_type _atom_site_calc_flag _atom_site_calc_attached_atom Cl(1) -0.0472(4) 0.5101(2) 0.6053(2) 0.044(1) Uij ? ? Si(1) 0.3530(5) 0.6323(3) 0.5647(3) 0.065(2) Uij ? ? Si(2) 0.2858(5) 0.5052(3) 0.8357(3) 0.056(2) Uij ? ? O(1) -0.112(1) 0.4380(7) 0.7973(9) 0.090(6) Uij ? ? N(1) 0.192(1) 0.6419(7) 0.5715(6) 0.034(4) Uij ? ? N(2) -0.057(1) 0.6795(7) 0.4679(8) 0.044(5) Uij ? ? N(3) 0.165(1) 0.5603(6) 0.7832(7) 0.038(4) Uij ? ? N(4) -0.093(1) 0.6214(8) 0.8010(8) 0.052(6) Uij ? ? C(1) 0.398(1) 0.5323(8) 0.5856(9) 0.060(6) Uij ? ? C(2) 0.403(2) 0.656(1) 0.461(1) 0.14(1) Uij ? ? C(3) 0.462(2) 0.691(1) 0.641(1) 0.143(10) Uij ? ? C(4) 0.144(2) 0.7198(10) 0.5655(10) 0.060(7) Uij ? ? C(5) -0.007(2) 0.7242(8) 0.5410(10) 0.054(7) Uij ? ? C(6) -0.012(2) 0.7126(9) 0.3937(10) 0.078(8) Uij ? ? C(7) -0.202(2) 0.6751(9) 0.4579(9) 0.069(7) Uij ? ? C(8) 0.457(1) 0.5451(9) 0.8447(10) 0.082(7) Uij ? ? C(9) 0.283(1) 0.4144(9) 0.7814(9) 0.069(7) Uij ? ? C(10) 0.260(2) 0.485(1) 0.9457(9) 0.119(9) Uij ? ? C(11) 0.150(2) 0.635(1) 0.8204(9) 0.065(7) Uij ? ? C(12) 0.019(2) 0.6689(10) 0.7915(9) 0.059(7) Uij ? ? C(13) -0.216(2) 0.6503(10) 0.757(1) 0.084(8) Uij ? ? C(14) -0.102(2) 0.6081(10) 0.889(1) 0.103(9) Uij ? ? C(15) -0.237(3) 0.418(2) 0.757(2) 0.20(2) Uij ? ? C(16) -0.305(2) 0.371(2) 0.804(2) 0.17(2) Uij ? ? C(17) -0.213(3) 0.349(1) 0.873(2) 0.15(2) Uij ? ? C(18) -0.093(3) 0.393(1) 0.868(2) 0.14(1) Uij ? ? Li(1) 0.048(2) 0.586(1) 0.499(2) 0.06(1) Uij ? ? Li(2) -0.019(2) 0.522(2) 0.759(2) 0.06(1) Uij ? ? Li(3) 0.151(2) 0.579(2) 0.663(2) 0.05(1) Uij ? ? loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cl(1) 0.056(3) 0.040(3) 0.035(3) -0.004(3) 0.006(2) -0.007(3) Si(1) 0.041(4) 0.061(4) 0.094(5) 0.002(3) 0.012(3) 0.020(4) Si(2) 0.060(4) 0.063(4) 0.043(3) 0.004(4) 0.003(3) 0.004(4) O(1) 0.09(1) 0.10(1) 0.09(1) -0.04(1) 0.031(10) 0.020(10) N(1) 0.046(9) 0.019(8) 0.040(8) -0.008(8) 0.014(7) 0.000(7) N(2) 0.038(10) 0.035(10) 0.06(1) 0.008(8) 0.005(8) -0.001(8) N(3) 0.049(9) 0.019(8) 0.044(9) 0.008(7) -0.004(7) -0.004(7) N(4) 0.04(1) 0.06(1) 0.06(1) 0.009(9) 0.016(9) 0.013(9) C(1) 0.06(1) 0.06(1) 0.07(1) 0.025(9) 0.03(1) 0.030(10) C(2) 0.07(2) 0.14(2) 0.21(2) 0.03(1) 0.07(2) 0.13(2) C(3) 0.06(1) 0.09(2) 0.25(3) -0.02(1) -0.07(2) 0.01(2) C(4) 0.04(1) 0.07(2) 0.07(1) -0.03(1) 0.00(1) -0.01(1) C(5) 0.08(1) 0.03(1) 0.05(1) -0.01(1) 0.01(1) -0.029(9) C(6) 0.10(2) 0.07(2) 0.06(1) 0.00(1) 0.00(1) 0.03(1) C(7) 0.05(1) 0.09(2) 0.07(1) 0.01(1) 0.00(1) -0.02(1) C(8) 0.06(1) 0.08(2) 0.10(2) 0.00(1) -0.02(1) -0.01(1) C(9) 0.07(1) 0.05(1) 0.08(2) 0.00(1) 0.01(1) 0.02(1) C(10) 0.12(2) 0.19(2) 0.05(1) 0.03(2) 0.01(1) 0.02(2) C(11) 0.08(1) 0.08(2) 0.04(1) 0.01(1) 0.00(1) -0.02(1) C(12) 0.05(1) 0.08(2) 0.05(1) 0.05(1) 0.01(1) -0.01(1) C(13) 0.04(1) 0.11(2) 0.11(2) 0.05(1) 0.03(1) 0.02(1) C(14) 0.15(2) 0.10(2) 0.06(1) 0.02(2) 0.05(2) 0.01(1) C(15) 0.17(3) 0.28(4) 0.18(3) -0.18(3) 0.07(2) 0.00(3) C(16) 0.06(2) 0.13(3) 0.32(5) -0.03(2) 0.03(2) 0.05(3) C(17) 0.17(3) 0.09(2) 0.21(3) -0.03(2) 0.12(3) -0.04(2) C(18) 0.15(3) 0.11(2) 0.17(3) -0.02(2) 0.04(2) 0.08(2) Li(1) 0.07(2) 0.04(2) 0.07(2) -0.01(2) 0.02(2) -0.01(2) Li(2) 0.04(2) 0.08(3) 0.07(2) -0.01(2) 0.01(2) 0.02(2) Li(3) 0.02(2) 0.06(2) 0.08(2) 0.01(1) 0.01(2) 0.00(2) #------------------------------------------------------------------------------ _refine_special_details ? _refine_ls_structure_factor_coef F _refine_ls_matrix_type full _refine_ls_weighting_scheme sigma _refine_ls_hydrogen_treatment ? _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_abs_structure_details ? _refine_ls_abs_structure_Flack ? _refine_ls_number_reflns 1186 _refine_ls_number_parameters 262 _refine_ls_number_restraints 0 _refine_ls_number_constraints ? _refine_ls_R_factor_all ? _refine_ls_R_factor_obs 0.0886 _refine_ls_wR_factor_all ? _refine_ls_wR_factor_obs 0.0561 _refine_ls_goodness_of_fit_all ? _refine_ls_goodness_of_fit_obs 1.510 _refine_ls_shift/esd_max 0.0030 _refine_ls_shift/esd_mean ? _refine_diff_density_min -0.43 _refine_diff_density_max 0.36 #------------------------------------------------------------------------------ _geom_special_details ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl(1) Li(1) 2.50(3) ? ? yes Cl(1) Li(1) 2.40(3) ? ? yes Cl(1) Li(2) 2.48(3) ? ? yes Cl(1) Li(3) 2.44(2) ? ? yes Si(1) N(1) 1.67(1) ? ? yes Si(1) C(1) 1.86(1) ? ? yes Si(1) C(2) 1.87(2) ? ? yes Si(1) C(3) 1.87(2) ? ? yes Si(2) N(3) 1.71(1) ? ? yes Si(2) C(8) 1.88(2) ? ? yes Si(2) C(9) 1.84(2) ? ? yes Si(2) C(10) 1.88(2) ? ? yes O(1) C(15) 1.40(3) ? ? yes O(1) C(18) 1.39(2) ? ? yes O(1) Li(2) 1.92(3) ? ? yes N(1) C(4) 1.47(2) ? ? yes N(1) Li(1) 2.03(3) ? ? yes N(1) Li(3) 1.96(3) ? ? yes N(2) C(5) 1.46(2) ? ? yes N(2) C(6) 1.48(2) ? ? yes N(2) C(7) 1.47(2) ? ? yes N(2) Li(1) 2.01(3) ? ? yes N(3) C(11) 1.48(2) ? ? yes N(3) Li(2) 1.99(3) ? ? yes N(3) Li(3) 1.97(3) ? ? yes N(4) C(12) 1.45(2) ? ? yes N(4) C(13) 1.46(2) ? ? yes N(4) C(14) 1.47(2) ? ? yes N(4) Li(2) 2.08(3) ? ? yes C(4) C(5) 1.55(2) ? ? yes C(11) C(12) 1.48(2) ? ? yes C(15) C(16) 1.38(3) ? ? yes C(16) C(17) 1.41(3) ? ? yes C(17) C(18) 1.47(3) ? ? yes Li(1) Li(3) 2.74(4) ? ? yes Li(2) Li(3) 2.69(4) ? ? yes #------------------------------------------------------------------------------ loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Li(1) Cl(1) Li(1) 81.7(9) ? ? ? yes Li(1) Cl(1) Li(2) 130.7(9) ? ? ? yes Li(1) Cl(1) Li(3) 67.5(9) ? ? ? yes Li(1) Cl(1) Li(2) 139.1(9) ? ? ? yes Li(1) Cl(1) Li(3) 123.2(8) ? ? ? yes Li(2) Cl(1) Li(3) 66.2(8) ? ? ? yes N(1) Si(1) C(1) 108.0(7) ? ? ? yes N(1) Si(1) C(2) 115.3(7) ? ? ? yes N(1) Si(1) C(3) 113.6(8) ? ? ? yes C(1) Si(1) C(2) 106.7(8) ? ? ? yes C(1) Si(1) C(3) 107.9(8) ? ? ? yes C(2) Si(1) C(3) 104.9(10) ? ? ? yes N(3) Si(2) C(8) 115.1(7) ? ? ? yes N(3) Si(2) C(9) 107.6(6) ? ? ? yes N(3) Si(2) C(10) 113.6(7) ? ? ? yes C(8) Si(2) C(9) 108.8(7) ? ? ? yes C(8) Si(2) C(10) 104.5(8) ? ? ? yes C(9) Si(2) C(10) 106.9(8) ? ? ? yes C(15) O(1) C(18) 105(1) ? ? ? yes C(15) O(1) Li(2) 120(1) ? ? ? yes C(18) O(1) Li(2) 133(1) ? ? ? yes Si(1) N(1) C(4) 114.5(10) ? ? ? yes Si(1) N(1) Li(1) 123.7(10) ? ? ? yes Si(1) N(1) Li(3) 107.9(9) ? ? ? yes C(4) N(1) Li(1) 102(1) ? ? ? yes C(4) N(1) Li(3) 119(1) ? ? ? yes Li(1) N(1) Li(3) 86(1) ? ? ? yes C(5) N(2) C(6) 109(1) ? ? ? yes C(5) N(2) C(7) 110(1) ? ? ? yes C(5) N(2) Li(1) 97(1) ? ? ? yes C(6) N(2) C(7) 110(1) ? ? ? yes C(6) N(2) Li(1) 108(1) ? ? ? yes C(7) N(2) Li(1) 118(1) ? ? ? yes Si(2) N(3) C(11) 114.9(10) ? ? ? yes Si(2) N(3) Li(2) 119(1) ? ? ? yes Si(2) N(3) Li(3) 122.5(10) ? ? ? yes C(11) N(3) Li(2) 104(1) ? ? ? yes C(11) N(3) Li(3) 105(1) ? ? ? yes Li(2) N(3) Li(3) 85(1) ? ? ? yes C(12) N(4) C(13) 112(1) ? ? ? yes C(12) N(4) C(14) 110(1) ? ? ? yes C(12) N(4) Li(2) 97(1) ? ? ? yes C(13) N(4) C(14) 112(1) ? ? ? yes C(13) N(4) Li(2) 117(1) ? ? ? yes C(14) N(4) Li(2) 105(1) ? ? ? yes N(1) C(4) C(5) 112(1) ? ? ? yes N(2) C(5) C(4) 114(1) ? ? ? yes N(3) C(11) C(12) 111(1) ? ? ? yes N(4) C(12) C(11) 114(1) ? ? ? yes O(1) C(15) C(16) 112(2) ? ? ? yes C(15) C(16) C(17) 106(2) ? ? ? yes C(16) C(17) C(18) 105(2) ? ? ? yes O(1) C(18) C(17) 109(2) ? ? ? yes Cl(1) Li(1) Cl(1) 98.3(9) ? ? ? yes Cl(1) Li(1) N(1) 100(1) ? ? ? yes Cl(1) Li(1) N(2) 112(1) ? ? ? yes Cl(1) Li(1) Li(3) 55.3(8) ? ? ? yes Cl(1) Li(1) N(1) 133(1) ? ? ? yes Cl(1) Li(1) N(2) 117(1) ? ? ? yes Cl(1) Li(1) Li(3) 128(1) ? ? ? yes N(1) Li(1) N(2) 93(1) ? ? ? yes N(1) Li(1) Li(3) 45.5(8) ? ? ? yes N(2) Li(1) Li(3) 113(1) ? ? ? yes Cl(1) Li(2) O(1) 105(1) ? ? ? yes Cl(1) Li(2) N(3) 101(1) ? ? ? yes Cl(1) Li(2) N(4) 113(1) ? ? ? yes Cl(1) Li(2) Li(3) 56.2(8) ? ? ? yes O(1) Li(2) N(3) 134(1) ? ? ? yes O(1) Li(2) N(4) 109(1) ? ? ? yes O(1) Li(2) Li(3) 150(1) ? ? ? yes N(3) Li(2) N(4) 90(1) ? ? ? yes N(3) Li(2) Li(3) 46.9(8) ? ? ? yes N(4) Li(2) Li(3) 99(1) ? ? ? yes Cl(1) Li(3) N(1) 104(1) ? ? ? yes Cl(1) Li(3) N(3) 103(1) ? ? ? yes Cl(1) Li(3) Li(1) 57.2(7) ? ? ? yes Cl(1) Li(3) Li(2) 57.7(8) ? ? ? yes N(1) Li(3) N(3) 149(1) ? ? ? yes N(1) Li(3) Li(1) 47.7(8) ? ? ? yes N(1) Li(3) Li(2) 151(1) ? ? ? yes N(3) Li(3) Li(1) 160(1) ? ? ? yes N(3) Li(3) Li(2) 47.5(9) ? ? ? yes Li(1) Li(3) Li(2) 112(1) ? ? ? yes #------------------------------------------------------------------------------ _publ_requested_journal ' ENTER JOURNAL NAME HERE' _publ_contact_author ; ENTER NAME ENTER ADDRESS ; _publ_contact_letter ; ENTER TEXT OF LETTER ; _publ_requested_coeditor_name ? _publ_contact_author_phone ' ENTER PHONE NUMBER ' _publ_contact_author_fax ' ENTER FAX NUMBER ' _publ_contact_author_email ' ENTER EMAIL ADDRESS ' loop_ _publ_author_name _publ_author_address ' FIRST AUTHORS NAME ' ; FIRST AUTHORS ADDRESS ; _publ_section_title ; ENTER SECTION TITLE ; _publ_section_abstract ; ENTER ABSTRACT ; _publ_section_experimental ; ENTER EXPERIMENTAL SECTION ; _publ_section_comment ; ENTER TEXT ; _publ_section_references ; ENTER OTHER REFERENCES Molecular Structure Corporation (1985, 1992). teXsan. Crystal Structure Analysis Package, The Woodlands, TX, USA 77381 ; _publ_section_acknowledgements ; ENTER ACKNOWLEDGEMENTS ; _publ_section_table_legends ; ENTER TABLE LEGENDS ; _publ_section_figure_captions ; ENTER FIGURE CAPTIONS ; #=END data_[Li(en')2Li(OEt2)] #------------------------------------------------------------------------------ _audit_creation_date 'Sun Feb 8 23:59:14 1998' _audit_creation_method 'from TEXRAY.INF file' _audit_update_record ? #------------------------------------------------------------------------------ _computing_data_collection 'MSC/AFC Diffractometer Control' _computing_cell_refinement 'MSC/AFC Diffractometer Control' _computing_data_reduction 'teXsan' _computing_structure_solution SHELXS86 _computing_structure_refinement 'teXsan' _computing_publication_material 'teXsan' #------------------------------------------------------------------------------ _cell_length_a 9.88(1) _cell_length_b 10.21(1) _cell_length_c 15.79(2) _cell_angle_alpha 76.75(10) _cell_angle_beta 78.65(9) _cell_angle_gamma 63.28(9) _cell_volume 1377(3) _cell_formula_units_Z 2 _cell_measurement_temperature 213.2 _cell_measurement_reflns_used 25 _cell_measurement_theta_min 8.0 _cell_measurement_theta_max 15.0 #------------------------------------------------------------------------------ _symmetry_cell_setting triclinic _symmetry_space_group_name_H-M 'P -1 ' _symmetry_Int_Tables_number 2 _symmetry_space_group_name_Hall ? loop_ _symmetry_equiv_pos_as_xyz ' +x, +y, +z' ' -x, -y, -z' #------------------------------------------------------------------------------ _exptl_crystal_description 'prismatic' _exptl_crystal_colour 'colorless' _exptl_crystal_size_max 0.000 _exptl_crystal_size_mid 0.000 _exptl_crystal_size_min 0.000 _exptl_crystal_density_diffrn 0.981 _exptl_crystal_density_meas ? _chemical_formula_weight 406.66 _chemical_formula_analytical ? _chemical_formula_sum 'C18 H48 Li2 N4 O Si2 ' _chemical_formula_moiety 'C18 H48 Li2 N4 O Si2 ' _chemical_formula_structural ? _chemical_compound_source ? _exptl_crystal_F_000 452.00 _exptl_absorpt_coefficient_mu 0.141 _exptl_absorpt_correction_type none #------------------------------------------------------------------------------ _diffrn_special_details none _diffrn_ambient_temperature 213.2 _diffrn_radiation_wavelength 0.7107 _diffrn_radiation_type MoKalpha _diffrn_radiation_source 'X-ray tube' _diffrn_radiation_monochromator graphite _diffrn_radiation_detector ? _diffrn_measurement_device 'NICOLET' _diffrn_measurement_method 'omega scans with profile analysis' _diffrn_standards_number 2 _diffrn_standards_interval_count 198 _diffrn_standards_decay_% 0.00 loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? ? ? ? _diffrn_reflns_number 3733 _reflns_number_total 3578 _reflns_number_observed 1159 _reflns_observed_criterion 2.00 _diffrn_reflns_av_R_equivalents 9.08 _diffrn_reflns_av_sigmaI/netI ? _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_limit_l_max 0 _diffrn_reflns_theta_min ? _diffrn_reflns_theta_max 22.50 _diffrn_reflns_reduction_process ? _diffrn_orient_matrix_UB_11 0.00000 _diffrn_orient_matrix_UB_12 0.00000 _diffrn_orient_matrix_UB_13 0.00000 _diffrn_orient_matrix_UB_21 0.00000 _diffrn_orient_matrix_UB_22 0.00000 _diffrn_orient_matrix_UB_23 0.00000 _diffrn_orient_matrix_UB_31 0.00000 _diffrn_orient_matrix_UB_32 0.00000 _diffrn_orient_matrix_UB_33 0.00000 #------------------------------------------------------------------------------ loop_ _atom_type_symbol _atom_type_oxidation_number _atom_type_number_in_cell _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C 0 36 0.003 0.002 'International Tables' H 0 96 0.000 0.000 'International Tables' N 0 8 0.006 0.003 'International Tables' Si 0 4 0.082 0.070 'International Tables' O 0 2 0.011 0.006 'International Tables' Li 0 4 0.000 0.000 'International Tables' #------------------------------------------------------------------------------ loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_thermal_displace_type _atom_site_calc_flag _atom_site_calc_attached_atom Si(1) -0.2892(6) 0.4653(6) 0.8519(4) 0.031(2) Uij ? ? Si(2) 0.2255(6) 0.0642(6) 0.6396(4) 0.033(2) Uij ? ? O(1) -0.237(1) 0.253(1) 0.6444(8) 0.051(7) Uij ? ? N(1) -0.140(1) 0.443(2) 0.7729(9) 0.047(7) Uij ? ? N(2) 0.152(2) 0.468(2) 0.740(1) 0.038(8) Uij ? ? N(3) 0.117(1) 0.116(1) 0.7318(9) 0.041(7) Uij ? ? N(4) 0.198(2) 0.143(2) 0.899(1) 0.01(1) Uij ? ? C(1) -0.271(2) 0.524(2) 0.950(1) 0.12(1) Uij ? ? C(2) -0.312(2) 0.290(2) 0.886(1) 0.08(1) Uij ? ? C(3) -0.477(2) 0.611(2) 0.816(1) 0.10(1) Uij ? ? C(4) -0.130(2) 0.582(2) 0.730(1) 0.031(9) Uij ? ? C(5) 0.027(2) 0.557(2) 0.688(1) 0.038(9) Uij ? ? C(6) 0.299(2) 0.435(2) 0.693(1) 0.07(1) Uij ? ? C(7) 0.138(2) 0.539(2) 0.817(1) 0.10(1) Uij ? ? C(8) 0.427(2) 0.035(2) 0.635(1) 0.070(10) Uij ? ? C(9) 0.140(2) 0.212(2) 0.544(1) 0.070(9) Uij ? ? C(10) 0.244(2) -0.115(2) 0.615(1) 0.08(1) Uij ? ? C(11) 0.151(2) -0.002(2) 0.808(2) 0.01(1) Uij ? ? C(12) 0.185(3) 0.024(3) 0.877(2) 0.23(2) Uij ? ? C(13) 0.345(3) 0.118(2) 0.893(1) 0.15(2) Uij ? ? C(14) 0.125(3) 0.179(2) 0.981(2) 0.13(1) Uij ? ? C(15) -0.310(2) 0.502(3) 0.577(1) 0.08(1) Uij ? ? C(16) -0.302(2) 0.360(3) 0.570(2) 0.07(1) Uij ? ? C(17) -0.221(2) 0.109(2) 0.635(1) 0.06(1) Uij ? ? C(18) -0.193(2) 0.009(2) 0.719(2) 0.08(1) Uij ? ? Li(1) 0.086(3) 0.294(3) 0.790(2) 0.039(10) Uij ? ? Li(2) -0.097(3) 0.270(3) 0.717(2) 0.05(1) Uij ? ? H(1) -0.1790 0.4582 0.9774 0.2021 Uij ? ? H(2) -0.2626 0.6225 0.9348 0.2021 Uij ? ? H(3) -0.3551 0.5404 0.9942 0.2021 Uij ? ? H(4) -0.3957 0.2968 0.9281 0.1365 Uij ? ? H(5) -0.3302 0.2600 0.8345 0.1365 Uij ? ? H(6) -0.2216 0.2079 0.9062 0.1365 Uij ? ? H(7) -0.4792 0.7087 0.7999 0.1643 Uij ? ? H(8) -0.5007 0.5907 0.7640 0.1643 Uij ? ? H(9) -0.5611 0.6168 0.8599 0.1643 Uij ? ? H(10) -0.2075 0.6376 0.6889 0.0660 Uij ? ? H(11) -0.1595 0.6495 0.7736 0.0660 Uij ? ? H(12) 0.0334 0.6528 0.6616 0.0804 Uij ? ? H(13) 0.0460 0.5104 0.6349 0.0804 Uij ? ? H(14) 0.3790 0.3621 0.7299 0.1463 Uij ? ? H(15) 0.3141 0.3889 0.6425 0.1463 Uij ? ? H(16) 0.3215 0.5189 0.6736 0.1463 Uij ? ? H(17) 0.2109 0.4687 0.8553 0.1784 Uij ? ? H(18) 0.1525 0.6251 0.7986 0.1784 Uij ? ? H(19) 0.0378 0.5607 0.8476 0.1784 Uij ? ? H(20) 0.4779 -0.0443 0.6841 0.1314 Uij ? ? H(21) 0.4874 0.0018 0.5832 0.1314 Uij ? ? H(22) 0.4350 0.1208 0.6430 0.1314 Uij ? ? H(23) 0.1362 0.3080 0.5484 0.1313 Uij ? ? H(24) 0.1988 0.1880 0.4883 0.1313 Uij ? ? H(25) 0.0374 0.2305 0.5391 0.1313 Uij ? ? H(26) 0.1470 -0.1135 0.6130 0.1417 Uij ? ? H(27) 0.3004 -0.1330 0.5567 0.1417 Uij ? ? H(28) 0.2987 -0.1991 0.6554 0.1417 Uij ? ? H(29) 0.0723 -0.0389 0.8221 0.0641 Uij ? ? H(30) 0.2443 -0.0931 0.7887 0.0641 Uij ? ? H(31) 0.2734 -0.0601 0.8992 0.3356 Uij ? ? H(32) 0.0990 0.0191 0.9244 0.3356 Uij ? ? H(33) 0.3948 0.0399 0.9364 0.2330 Uij ? ? H(34) 0.3938 0.0955 0.8364 0.2330 Uij ? ? H(35) 0.3503 0.2069 0.9002 0.2330 Uij ? ? H(36) 0.1269 0.2693 0.9906 0.2026 Uij ? ? H(37) 0.0194 0.1977 0.9870 0.2026 Uij ? ? H(38) 0.1720 0.1024 1.0276 0.2026 Uij ? ? H(39) -0.2099 0.4958 0.5781 0.1498 Uij ? ? H(40) -0.3540 0.5796 0.5286 0.1498 Uij ? ? H(41) -0.3707 0.5378 0.6297 0.1498 Uij ? ? H(42) -0.2439 0.3213 0.5160 0.1096 Uij ? ? H(43) -0.4045 0.3632 0.5676 0.1096 Uij ? ? H(44) -0.3115 0.1199 0.6109 0.1010 Uij ? ? H(45) -0.1368 0.0681 0.5885 0.1010 Uij ? ? H(46) -0.2801 0.0542 0.7632 0.1392 Uij ? ? H(47) -0.1850 -0.0858 0.7190 0.1392 Uij ? ? H(48) -0.1053 0.0015 0.7406 0.1392 Uij ? ? loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Si(1) 0.035(5) 0.031(5) 0.032(5) -0.019(4) 0.006(3) -0.011(3) Si(2) 0.029(5) 0.027(5) 0.044(5) -0.007(3) 0.001(3) -0.022(3) #------------------------------------------------------------------------------ _refine_special_details ? _refine_ls_structure_factor_coef F _refine_ls_matrix_type full _refine_ls_weighting_scheme sigma _refine_ls_hydrogen_treatment noref _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_abs_structure_details ? _refine_ls_abs_structure_Flack ? _refine_ls_number_reflns 1159 _refine_ls_number_parameters 144 _refine_ls_number_restraints 0 _refine_ls_number_constraints ? _refine_ls_R_factor_all ? _refine_ls_R_factor_obs 0.1324 _refine_ls_wR_factor_all ? _refine_ls_wR_factor_obs 0.0673 _refine_ls_goodness_of_fit_all ? _refine_ls_goodness_of_fit_obs 2.000 _refine_ls_shift/esd_max 0.9370 _refine_ls_shift/esd_mean ? _refine_diff_density_min -0.53 _refine_diff_density_max 0.63 #------------------------------------------------------------------------------ _geom_special_details ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_publ_flag Si(1) N(1) 1.70(1) ? ? yes Si(1) C(1) 1.85(2) ? ? yes Si(1) C(2) 1.85(2) ? ? yes Si(1) C(3) 1.88(2) ? ? yes Si(2) N(3) 1.67(1) ? ? yes Si(2) C(8) 1.86(2) ? ? yes Si(2) C(9) 1.89(2) ? ? yes Si(2) C(10) 1.87(2) ? ? yes O(1) C(16) 1.44(2) ? ? yes O(1) C(17) 1.44(2) ? ? yes O(1) Li(2) 2.04(3) ? ? yes N(1) C(4) 1.47(2) ? ? yes N(1) Li(1) 2.09(3) ? ? yes N(1) Li(2) 2.00(3) ? ? yes N(2) C(5) 1.44(2) ? ? yes N(2) C(6) 1.43(2) ? ? yes N(2) C(7) 1.51(2) ? ? yes N(2) Li(1) 2.09(3) ? ? yes N(3) C(11) 1.46(2) ? ? yes N(3) Li(1) 2.10(3) ? ? yes N(3) Li(2) 2.02(3) ? ? yes N(4) C(12) 1.40(3) ? ? yes N(4) C(13) 1.34(3) ? ? yes N(4) C(14) 1.39(3) ? ? yes N(4) Li(1) 2.13(3) ? ? yes C(4) C(5) 1.49(2) ? ? yes C(11) C(12) 1.32(3) ? ? yes C(15) C(16) 1.44(3) ? ? yes C(17) C(18) 1.46(2) ? ? yes Li(1) Li(2) 2.46(4) ? ? yes #------------------------------------------------------------------------------ loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N(1) Si(1) C(1) 114.1(8) ? ? ? yes N(1) Si(1) C(2) 109.7(8) ? ? ? yes N(1) Si(1) C(3) 114.0(8) ? ? ? yes C(1) Si(1) C(2) 108.8(9) ? ? ? yes C(1) Si(1) C(3) 103.8(10) ? ? ? yes C(2) Si(1) C(3) 106.0(8) ? ? ? yes N(3) Si(2) C(8) 114.6(7) ? ? ? yes N(3) Si(2) C(9) 109.1(8) ? ? ? yes N(3) Si(2) C(10) 115.2(8) ? ? ? yes C(8) Si(2) C(9) 107.4(8) ? ? ? yes C(8) Si(2) C(10) 103.5(8) ? ? ? yes C(9) Si(2) C(10) 106.5(8) ? ? ? yes C(16) O(1) C(17) 109(1) ? ? ? yes C(16) O(1) Li(2) 123(1) ? ? ? yes C(17) O(1) Li(2) 120(1) ? ? ? yes Si(1) N(1) C(4) 114(1) ? ? ? yes Si(1) N(1) Li(1) 124(1) ? ? ? yes Si(1) N(1) Li(2) 109(1) ? ? ? yes C(4) N(1) Li(1) 103(1) ? ? ? yes C(4) N(1) Li(2) 126(1) ? ? ? yes Li(1) N(1) Li(2) 74(1) ? ? ? yes C(5) N(2) C(6) 114(1) ? ? ? yes C(5) N(2) C(7) 111(1) ? ? ? yes C(5) N(2) Li(1) 96(1) ? ? ? yes C(6) N(2) C(7) 108(1) ? ? ? yes C(6) N(2) Li(1) 119(1) ? ? ? yes C(7) N(2) Li(1) 106(1) ? ? ? yes Si(2) N(3) C(11) 114(1) ? ? ? yes Si(2) N(3) Li(1) 127(1) ? ? ? yes Si(2) N(3) Li(2) 115(1) ? ? ? yes C(11) N(3) Li(1) 99(1) ? ? ? yes C(11) N(3) Li(2) 121(1) ? ? ? yes Li(1) N(3) Li(2) 73(1) ? ? ? yes C(12) N(4) C(13) 110(1) ? ? ? yes C(12) N(4) C(14) 114(1) ? ? ? yes C(12) N(4) Li(1) 92(1) ? ? ? yes C(13) N(4) C(14) 110(1) ? ? ? yes C(13) N(4) Li(1) 112(1) ? ? ? yes C(14) N(4) Li(1) 114(1) ? ? ? yes N(1) C(4) C(5) 112(1) ? ? ? yes N(2) C(5) C(4) 117(1) ? ? ? yes N(3) C(11) C(12) 117(2) ? ? ? yes N(4) C(12) C(11) 135(2) ? ? ? yes O(1) C(16) C(15) 109(1) ? ? ? yes O(1) C(17) C(18) 109(1) ? ? ? yes N(1) Li(1) N(2) 89(1) ? ? ? yes N(1) Li(1) N(3) 102(1) ? ? ? yes N(1) Li(1) N(4) 134(1) ? ? ? yes N(1) Li(1) Li(2) 51.2(9) ? ? ? yes N(2) Li(1) N(3) 129(1) ? ? ? yes N(2) Li(1) N(4) 115(1) ? ? ? yes N(2) Li(1) Li(2) 118(1) ? ? ? yes N(3) Li(1) N(4) 90(1) ? ? ? yes N(3) Li(1) Li(2) 51.7(10) ? ? ? yes N(4) Li(1) Li(2) 125(1) ? ? ? yes O(1) Li(2) N(1) 127(1) ? ? ? yes O(1) Li(2) N(3) 123(1) ? ? ? yes O(1) Li(2) Li(1) 174(1) ? ? ? yes N(1) Li(2) N(3) 109(1) ? ? ? yes N(1) Li(2) Li(1) 54.7(10) ? ? ? yes N(3) Li(2) Li(1) 54.9(10) ? ? ? yes #------------------------------------------------------------------------------ _publ_requested_journal ' ENTER JOURNAL NAME HERE' _publ_contact_author ; ENTER NAME ENTER ADDRESS ; _publ_contact_letter ; ENTER TEXT OF LETTER ; _publ_requested_coeditor_name ? _publ_contact_author_phone ' ENTER PHONE NUMBER ' _publ_contact_author_fax ' ENTER FAX NUMBER ' _publ_contact_author_email ' ENTER EMAIL ADDRESS ' loop_ _publ_author_name _publ_author_address ' FIRST AUTHORS NAME ' ; FIRST AUTHORS ADDRESS ; _publ_section_title ; ENTER SECTION TITLE ; _publ_section_abstract ; ENTER ABSTRACT ; _publ_section_experimental ; ENTER EXPERIMENTAL SECTION ; _publ_section_comment ; ENTER TEXT ; _publ_section_references ; ENTER OTHER REFERENCES Molecular Structure Corporation (1985, 1992). teXsan. Crystal Structure Analysis Package, The Woodlands, TX, USA 77381 ; _publ_section_acknowledgements ; ENTER ACKNOWLEDGEMENTS ; _publ_section_table_legends ; ENTER TABLE LEGENDS ; _publ_section_figure_captions ; ENTER FIGURE CAPTIONS ; #=END data_sm428 _audit_creation_date 97-09- _audit_creation_method from_xtal_archive_file_using_CIFIO _audit_update_record ? _chemical_compound_source ? _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_analytical ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_sum C10.5_H28.5_Lu.5_N3_Si1.5 _chemical_formula_weight 326.48 _chemical_melting_point ? _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction xtal_ADDREF_ABSORB_SORTRF _computing_structure_solution xtal _computing_structure_refinement xtal_CRYLSQ _computing_molecular_graphics xtal _computing_publication_material xtal_BONDLA_CIFIO _cell_length_a 18.713(15) _cell_length_b 16.776(12) _cell_length_c 10.155(6) _cell_angle_alpha 90.00000 _cell_angle_beta 90.00000 _cell_angle_gamma 90.00000 _cell_volume 3188(4) _cell_formula_units_Z 8 _cell_measurement_temperature 293 _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _cell_special_details ; ? ; _symmetry_cell_setting orthorhombic _symmetry_space_group_name_H-M p_n_m_a _symmetry_space_group_name_Hall -p_2ac_2n loop_ _symmetry_equiv_pos_as_xyz +x,+y,+z 1/2-x,-y,1/2+z 1/2+x,1/2-y,1/2-z -x,1/2+y,-z -x,-y,-z 1/2+x,+y,1/2-z 1/2-x,1/2+y,1/2+z +x,1/2-y,+z _exptl_crystal_description ? _exptl_crystal_preparation ? _exptl_crystal_colour ? _exptl_crystal_size_max ? _exptl_crystal_size_mid ? _exptl_crystal_size_min ? _exptl_crystal_density_diffrn 1.36 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 1352 _exptl_absorpt_process_details ? _exptl_absorpt_coefficient_mu ? _exptl_absorpt_correction_type gaussian _exptl_absorpt_correction_T_min 1.40 _exptl_absorpt_correction_T_max 1.66 _exptl_special_details ; ? ; _diffrn_special_details ; ? ; _diffrn_ambient_temperature 293 _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type xray_tube _diffrn_radiation_source ? _diffrn_radiation_monochromator graphite _diffrn_radiation_detector ? _diffrn_measurement_device ? _diffrn_measurement_method ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? loop_ _diffrn_attenuator_code _diffrn_attenuator_scale ? ? _diffrn_reflns_number 2135 _diffrn_reflns_av_R_equivalents ? _diffrn_reflns_av_sigmaI/netI .198 _diffrn_reflns_limit_h_min 0 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_k_min 0 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_l_min -10 _diffrn_reflns_limit_l_max 0 _diffrn_reflns_theta_min 2.18 _diffrn_reflns_theta_max 22.49 _diffrn_reflns_reduction_process ? loop_ _atom_type_symbol _atom_type_description _atom_type_oxidation_number _atom_type_number_in_cell _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C ? 0 84 .002 .002 Int_Tables_Vol_IV_Tables_2.2B_and_2.3.1 H ? 0 228 0 0 Int_Tables_Vol_IV_Tables_2.2B_and_2.3.1 Lu ? 0 4 -.988 5.858 Int_Tables_Vol_IV_Tables_2.2B_and_2.3.1 N ? 0 24 .004 .003 Int_Tables_Vol_IV_Tables_2.2B_and_2.3.1 Si ? 0 12 .072 .071 Int_Tables_Vol_IV_Tables_2.2B_and_2.3.1 loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_thermal_displace_type _atom_site_calc_flag _atom_site_calc_attached_atom Lu .39760(8) .25000 .65163(13) .0340(6) Uani ? ? N11 .3166(16) .3343(16) .619(3) .038(9) Uiso ? ? Si1 .299(2) .404(2) .491(3) .053(17) Uani ? ? C111 .199(2) .419(2) .465(4) .062(14) Uiso ? ? C112 .333(3) .500(4) .504(7) .14(2) Uiso ? ? C113 .338(3) .357(4) .329(7) .15(3) Uiso ? ? C11 .263(3) .344(3) .721(5) .086(18) Uiso ? ? C12 .287(3) .331(4) .873(7) .10(2) Uiso ? ? N12 .3142(17) .25000 .859(4) .100(10) Uiso ? ? C121 .258(3) .188(3) .832(6) .077(18) Uiso ? ? C122 .340(2) .222(3) .995(5) .10(2) Uiso ? ? N21 .4914(16) .2815(16) .527(3) .057(11) Uiso ? ? Si2 .5206(5) .25000 .3715(10) .061(6) Uani ? ? C211 .610(3) .199(3) .386(5) .12(2) Uiso ? ? C212 .460(3) .172(3) .298(5) .079(16) Uiso ? ? C213 .528(3) .328(3) .244(6) .12(2) Uiso ? ? C21 .526(3) .357(3) .559(6) .087(18) Uiso ? ? C22 .474(2) .421(3) .633(5) .070(13) Uiso ? ? N22 .477(2) .381(3) .753(5) .048(14) Uiso ? ? C221 .447(3) .419(3) .861(6) .079(15) Uiso ? ? C222 .543(6) .365(6) .776(10) .19(5) Uiso ? ? N31 .3543(16) .1346(19) .570(3) .042(9) Uiso ? ? Si3 .278(2) .115(2) .480(5) .08(2) Uani ? ? C311 .294(4) .064(4) .324(8) .17(3) Uiso ? ? C312 .228(3) .026(4) .575(6) .15(3) Uiso ? ? C313 .214(3) .195(3) .476(7) .16(3) Uiso ? ? C31 .396(3) .058(3) .602(4) .094(16) Uiso ? ? C32 .437(3) .065(4) .766(8) .12(2) Uiso ? ? N32 .475(2) .148(3) .785(4) .048(14) Uiso ? ? C321 .500(3) .154(4) .924(7) .12(2) Uiso ? ? C322 .549(4) .155(4) .719(7) .09(2) Uiso ? ? H111a .17781 .36954 .44087 .08500 Uiso ? ? H111b .17761 .43775 .54401 .08500 Uiso ? ? H111c .18973 .45680 .39658 .08500 Uiso ? ? H112a .31365 .52394 .58443 .21000 Uiso ? ? H112b .38319 .49749 .51366 .21000 Uiso ? ? H112c .32391 .53978 .43764 .21000 Uiso ? ? H113a .38680 .34560 .33615 .21000 Uiso ? ? H113b .31304 .30651 .30978 .21000 Uiso ? ? H113c .32811 .39288 .25980 .21000 Uiso ? ? H11a .23678 .38966 .71107 .12200 Uiso ? ? H11b .22749 .29780 .70714 .12200 Uiso ? ? H12a .32308 .37211 .88912 .12500 Uiso ? ? H12b .24894 .33925 .93063 .12500 Uiso ? ? H121a .22268 .19231 .90610 .13500 Uiso ? ? H121b .23220 .20262 .75531 .13500 Uiso ? ? H121c .27362 .13669 .82926 .13500 Uiso ? ? H122a .37585 .25861 1.02956 .16500 Uiso ? ? H122b .29990 .22557 1.05728 .16500 Uiso ? ? H122c .35722 .17110 .99247 .16500 Uiso ? ? H211a .64380 .23651 .42338 .17000 Uiso ? ? H211b .60627 .15491 .44287 .17000 Uiso ? ? H211c .62645 .18346 .30246 .17000 Uiso ? ? H212a .45819 .12639 .35211 .11500 Uiso ? ? H212b .41295 .19315 .28712 .11500 Uiso ? ? H212c .47567 .15486 .21107 .11500 Uiso ? ? H213a .48242 .35135 .23146 .17500 Uiso ? ? H213b .56082 .36729 .27354 .17500 Uiso ? ? H213c .54439 .31152 .15788 .17500 Uiso ? ? H21a .56499 .34649 .61400 .10700 Uiso ? ? H21b .54241 .37945 .47747 .10700 Uiso ? ? H22a .49305 .47419 .63170 .08600 Uiso ? ? H22b .42673 .42373 .59358 .08600 Uiso ? ? H221a .46855 .47002 .86992 .11900 Uiso ? ? H221b .39677 .42759 .83947 .11900 Uiso ? ? H221c .44821 .39300 .94245 .11900 Uiso ? ? H222a .55774 .31480 .70666 .29000 Uiso ? ? H222b .57954 .39395 .77465 .29000 Uiso ? ? H222c .54871 .32441 .85754 .29000 Uiso ? ? H311a .32612 .09413 .27403 .26000 Uiso ? ? H311b .31768 .01326 .34647 .26000 Uiso ? ? H311c .25271 .05224 .27846 .26000 Uiso ? ? H312a .25757 -.01993 .57251 .22500 Uiso ? ? H312b .21666 .04127 .65871 .22500 Uiso ? ? H312c .18567 .01584 .52270 .22500 Uiso ? ? H313a .20239 .21012 .56340 .25000 Uiso ? ? H313b .23867 .24203 .43657 .25000 Uiso ? ? H313c .17294 .18717 .42705 .25000 Uiso ? ? H31a .36407 .01475 .60122 .11000 Uiso ? ? H31b .43314 .05031 .54049 .11000 Uiso ? ? H32a .39899 .06056 .83044 .17000 Uiso ? ? H32b .46916 .02339 .77708 .17000 Uiso ? ? H321a .45901 .15046 .98423 .18000 Uiso ? ? H321b .53111 .11092 .94655 .18000 Uiso ? ? H321c .52267 .20297 .93773 .18000 Uiso ? ? H322a .57734 .10815 .75031 .16000 Uiso ? ? H322b .54132 .13949 .62283 .16000 Uiso ? ? H322c .57171 .19872 .72494 .16000 Uiso ? ? loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Lu .0341(6) .0417(7) .0262(6) .00118 -.0001(12) .00182 Si1 .07(2) .039(17) .048(12) -.016(12) -.002(14) .016(11) Si2 .054(6) .084(6) .044(7) .00000 .013(6) .00000 Si3 .07(2) .028(16) .13(2) .004(14) -.033(15) -.011(14) _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens ? _refine_special_details sfls__F_____calc_weight______full_matrix _refine_ls_structure_factor_coef F _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_hydrogen_treatment ? _refine_ls_extinction_method none _refine_ls_extinction_coef .00000 _refine_ls_extinction_expression ? _refine_ls_abs_structure_details none _refine_ls_abs_structure_Flack 0 _refine_ls_number_reflns 1032 _refine_ls_number_parameters 138 _refine_ls_number_restraints 0 _refine_ls_number_constraints 0 _refine_ls_R_factor_all .153 _refine_ls_R_factor_obs .056 _refine_ls_wR_factor_all .074 _refine_ls_wR_factor_obs .054 _refine_ls_goodness_of_fit_all 1.235 _refine_ls_goodness_of_fit_obs 1.341 _refine_ls_shift/esd_max .053 _refine_ls_shift/esd_mean .006 _refine_diff_density_min -3.069 _refine_diff_density_max 2.079 _geom_special_details ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_publ_flag Lu N11 2.10(3) . . ? Lu N12 2.62(4) . . ? Lu N21 2.23(3) . . ? Lu N22 2.84(4) . . ? Lu N31 2.25(3) . . ? Lu N32 2.62(4) . . ? Lu N11 2.10(3) . 8 ? Lu N21 2.23(3) . 8 ? Lu N22 2.84(4) . 8 ? Lu N31 2.25(3) . 8 ? Lu N32 2.62(4) . 8 ? N11 Si1 1.78(5) . . ? N11 C11 1.45(6) . . ? N11 N31 1.01(4) . 8 ? N11 Si3 1.80(5) . 8 ? Si1 C111 1.91(6) . . ? Si1 C112 1.73(8) . . ? Si1 C113 1.97(8) . . ? Si1 N31 1.47(5) . 8 ? Si1 Si3 .52(5) . 8 ? Si1 C311 1.78(8) . 8 ? Si1 C312 1.96(7) . 8 ? C111 H111a .95(4) . . ? C111 H111b .95(4) . . ? C111 H111c .96(4) . . ? C111 Si3 1.59(6) . 8 ? C111 C312 1.55(8) . 8 ? C111 C313 1.93(7) . 8 ? C111 H312c 1.26(4) . 8 ? C112 H112a .98(7) . . ? C112 H112b .94(6) . . ? C112 H112c .97(7) . . ? C112 Si3 2.19(8) . 8 ? C112 C31 1.81(8) . 8 ? C112 H31a 1.17(7) . 8 ? C113 H113a .95(6) . . ? C113 H113b .99(6) . . ? C113 H113c .94(7) . . ? C113 Si3 1.96(8) . 8 ? C113 C311 1.56(9) . 8 ? C113 H311a 1.01(7) . 8 ? C11 C12 1.63(9) . . ? C11 H11a .91(5) . . ? C11 H11b 1.03(5) . . ? C11 C121 1.26(8) . 8 ? C11 H121b 1.03(5) . 8 ? C11 H121c 1.17(6) . 8 ? C12 N12 1.46(6) . . ? C12 H12a .99(6) . . ? C12 H12b .93(6) . . ? C12 C121 .75(8) . 8 ? C12 C122 1.82(8) . 8 ? C12 H121a 1.30(6) . 8 ? C12 H121c .74(6) . 8 ? N12 C121 1.50(6) . . ? N12 C122 1.53(6) . . ? N12 C121 1.50(6) . 8 ? N12 C122 1.53(6) . 8 ? C121 H121a 1.00(6) . . ? C121 H121b .95(6) . . ? C121 H121c .92(5) . . ? C121 H11b 1.41(6) . 8 ? C121 H12b 1.11(6) . 8 ? C122 H122a .98(5) . . ? C122 H122b .98(4) . . ? C122 H122c .92(5) . . ? C122 C122 .94(7) . 8 ? C122 H122a .83(4) . 8 ? C122 H122b 1.31(5) . 8 ? N21 Si2 1.75(3) . . ? N21 C21 1.45(6) . . ? N21 N21 1.06(4) . 8 ? Si2 C211 1.88(6) . . ? Si2 C212 1.89(5) . . ? Si2 C213 1.85(6) . . ? Si2 C211 1.88(6) . 8 ? Si2 C212 1.89(5) . 8 ? Si2 C213 1.85(6) . 8 ? C211 H211a .97(5) . . ? C211 H211b .94(5) . . ? C211 H211c .94(5) . . ? C211 C211 1.71(6) . 8 ? C211 H211a 1.31(5) . 8 ? C212 H212a .94(4) . . ? C212 H212b .96(5) . . ? C212 H212c .97(5) . . ? C212 C213 1.39(8) . 8 ? C212 H113a 1.46(5) . 8 ? C212 H213a .88(5) . 8 ? C213 H213a .95(6) . . ? C213 H213b .94(6) . . ? C213 H213c .96(6) . . ? C213 H212c 1.08(6) . 8 ? C21 C22 1.64(7) . . ? C21 H21a .93(5) . . ? C21 H21b .97(6) . . ? C21 C322 1.68(9) . 8 ? C21 H322b .71(6) . 8 ? C22 N22 1.39(7) . . ? C22 H22a .96(4) . . ? C22 H22b .98(4) . . ? C22 C31 1.55(7) . 8 ? C22 C32 1.54(9) . 8 ? C22 N32 1.92(7) . 8 ? C22 H31b 1.31(5) . 8 ? N22 C221 1.40(7) . . ? N22 C222 1.29(12) . . ? N22 C32 1.19(8) . 8 ? N22 N32 .58(6) . 8 ? N22 C321 1.88(8) . 8 ? N22 C322 1.51(8) . 8 ? C221 H221a .95(5) . . ? C221 H221b .97(5) . . ? C221 H221c .94(6) . . ? C221 C32 1.02(10) . 8 ? C221 N32 1.47(7) . 8 ? C221 C321 1.70(8) . 8 ? C221 H32a 1.00(5) . 8 ? C221 H32b 1.35(5) . 8 ? C222 H222a 1.14(10) . . ? C222 H222b .84(11) . . ? C222 H222c 1.08(10) . . ? C222 N32 1.29(12) . 8 ? C222 C321 1.74(12) . 8 ? C222 C322 .68(12) . 8 ? C222 H322a .83(11) . 8 ? C222 H322c 1.31(11) . 8 ? N31 Si3 1.73(5) . . ? N31 C31 1.53(6) . . ? Si3 C311 1.82(9) . . ? Si3 C312 1.99(7) . . ? Si3 C313 1.80(7) . . ? C311 H311a .94(7) . . ? C311 H311b .99(7) . . ? C311 H311c .92(7) . . ? C311 H113c 1.17(7) . 8 ? C312 H312a .95(6) . . ? C312 H312b .91(6) . . ? C312 H312c .98(6) . . ? C312 H111b 1.17(6) . 8 ? C313 H313a .95(7) . . ? C313 H313b 1.01(6) . . ? C313 H313c .92(6) . . ? C313 C313 1.86(8) . 8 ? C313 H111a 1.32(6) . 8 ? C313 H313b 1.23(6) . 8 ? C31 C32 1.84(9) . . ? C31 H31a .94(5) . . ? C31 H31b .95(5) . . ? C31 H112b 1.31(5) . 8 ? C31 H22b .66(5) . 8 ? C32 N32 1.57(8) . . ? C32 H32a .97(7) . . ? C32 H32b .93(7) . . ? C32 H221a 1.35(7) . 8 ? C32 H221b 1.06(7) . 8 ? N32 C321 1.49(8) . . ? N32 C322 1.53(8) . . ? C321 H321a .98(7) . . ? C321 H321b .96(6) . . ? C321 H321c .94(6) . . ? C321 H221c 1.26(6) . 8 ? C321 H222c 1.20(7) . 8 ? C322 H322a 1.00(7) . . ? C322 H322b 1.02(7) . . ? C322 H322c .85(7) . . ? C322 H21a 1.11(7) . 8 ? C322 H222a .55(7) . 8 ? C322 H222b 1.15(7) . 8 ? C322 H222c 1.45(7) . 8 ? H111a H313c .9660(7) . 8 ? H111b H312c .8220(5) . 8 ? H112b H31a .9802(5) . 8 ? H113a H212b .9539(4) . 8 ? H113c H311a .26412(14) . 8 ? H11b H121b .4971(3) . 8 ? H12b H121a .7641(4) . 8 ? H122a H122a .2889(2) . 8 ? H122b H122b .8197(6) . 8 ? H211a H211a .4526(3) . 8 ? H212c H213a .26397(11) . 8 ? H21a H322b .5095(3) . 8 ? H22b H31b .7034(3) . 8 ? H221a H32b .9493(6) . 8 ? H221b H32a .22283(13) . 8 ? H221c H321a .8674(5) . 8 ? H222a H322c .39274(18) . 8 ? H222b H322a .25304(14) . 8 ? H313b H313b .2674(2) . 8 ?