data_global _journal_coden_Cambridge 182 loop_ _publ_author_name 'Lhoste, Jerome' 'Henry, Natacha' 'Roussel, Pascal' 'Loiseau, Thierry' 'Abraham, Francis' _publ_contact_author_name 'Loiseau, Thierry' _publ_contact_author_email thierry.loiseau@ensc-lille.fr _publ_section_title ; An uranyl citrate coordination polymer with a 3D open-framework involving uranyl cation-cation interactions ; # Attachment '- corrsadabsnumoptimise.cif' #======================================================================= data_(I) _database_code_depnum_ccdc_archive 'CCDC 798373' #TrackingRef '- corrsadabsnumoptimise.cif' #======================================================================= # 5. CHEMICAL DATA _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_formula_moiety 'C6 H4 O20 U4, 2(H2 O)' _chemical_formula_structural 'C6 H4 O20 U4, 2(O)' _chemical_formula_analytical ? _chemical_formula_iupac ? _chemical_formula_sum 'C6 H4 O22 U4' _chemical_formula_weight 1380.2 _chemical_melting_point ? _chemical_compound_source ? _chemical_absolute_configuration . #======================================================================= # 6. CRYSTAL DATA _symmetry_cell_setting triclinic _symmetry_space_group_name_H-M 'P -1' _symmetry_space_group_name_Hall '-P 1' loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 x,y,z 2 -x,-y,-z _cell_length_a 8.0495(2) _cell_length_b 11.8852(5) _cell_length_c 11.9209(4) _cell_angle_alpha 79.881(2) _cell_angle_beta 86.231(2) _cell_angle_gamma 81.912(2) _cell_volume 1110.58(7) _cell_formula_units_Z 2 _cell_measurement_reflns_used 6704 _cell_measurement_theta_min 2.25 _cell_measurement_theta_max 32.13 _cell_measurement_temperature 293 _cell_special_details ; ? ; _exptl_crystal_density_diffrn 4.126 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 1168 _exptl_absorpt_coefficient_mu 29.175 _exptl_crystal_description Irregular _exptl_crystal_size_max 0.13 _exptl_crystal_size_mid 0.05 _exptl_crystal_size_min 0.025 _exptl_crystal_size_rad ? _exptl_crystal_colour yellow-greeen _exptl_absorpt_correction_type Numerical _exptl_absorpt_process_details 'optimized using Stoe X-shape' _exptl_absorpt_correction_T_min 0.2116 _exptl_absorpt_correction_T_max 0.43439 #======================================================================= # 7. EXPERIMENTAL DATA _exptl_special_details ? _diffrn_ambient_temperature 293 _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_source 'X-ray tube' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator graphite _diffrn_measurement_device 'four-cycle diffractometer' _diffrn_measurement_device_type 'Bruker CCD' _diffrn_detector_area_resol_mean ? _diffrn_measurement_method '\f & \w scans' _diffrn_reflns_number 21659 _diffrn_reflns_theta_min 1.74 _diffrn_reflns_theta_max 33.31 _diffrn_reflns_theta_full 30.95 _diffrn_measured_fraction_theta_max 0.85 _diffrn_measured_fraction_theta_full 0.98 _diffrn_reflns_av_R_equivalents 0.045 _diffrn_reflns_av_sigmaI/netI 0.0574 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_reduction_process ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? #======================================================================= # 8. REFINEMENT DATA _refine_special_details ; ? ; _reflns_number_total 7369 _reflns_number_gt 5262 _reflns_threshold_expression I>3\s(I) _refine_ls_structure_factor_coef F _refine_ls_R_factor_gt 0.0514 _refine_ls_wR_factor_gt 0.0598 _refine_ls_R_factor_all 0.0766 _refine_ls_wR_factor_ref 0.0791 _refine_ls_goodness_of_fit_ref 3.98 _refine_ls_goodness_of_fit_gt 3.56 _refine_ls_restrained_S_gt ? _refine_ls_restrained_S_all ? _refine_ls_number_reflns 7369 _refine_ls_number_parameters 199 _refine_ls_number_restraints 0 _refine_ls_number_constraints 17 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details ? _refine_ls_hydrogen_treatment constr _refine_ls_shift/su_max 0.0033 _refine_ls_shift/su_mean 0.0012 _refine_diff_density_max 4.63 _refine_diff_density_min -4.56 _refine_ls_extinction_method 'B-C type 2 (Becker & Coppens, 1974)' _refine_ls_extinction_coef 1610(180) _refine_ls_abs_structure_details ? _refine_ls_abs_structure_Flack ? _refine_ls_abs_structure_Rogers ? loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source U -9.677 9.665 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' C 0.003 0.002 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' O 0.011 0.006 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' H 0.000 0.000 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' _computing_data_collection unknown _computing_cell_refinement unknown _computing_data_reduction unknown _computing_structure_solution unknown _computing_structure_refinement ? _computing_molecular_graphics unknown _computing_publication_material ? #======================================================================= # 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group U1 U -0.04212(6) 0.43608(5) 0.29792(4) Uani 0.01834(14) 2 1 d . . . U2 U -0.22304(6) 0.50507(5) -0.02365(4) Uani 0.01586(13) 2 1 d . . . U3 U -0.3918(3) 0.8485(2) -0.0096(2) Uani 0.0538(10) 2 1 d . . . U4 U -0.3168(6) 0.9375(4) 0.2814(4) Uani 0.0899(18) 2 1 d . . . O1 O -0.7575(12) 1.4337(8) 0.2236(8) Uiso 0.0185(18) 2 1 d . . . O2 O -0.3192(18) 1.4282(12) 0.2422(12) Uiso 0.039(3) 2 1 d . . . O3 O -0.2637(14) 0.6523(10) 0.0054(10) Uiso 0.025(2) 2 1 d . . . O4 O -0.0269(13) 0.4602(9) 0.1066(9) Uiso 0.0195(18) 2 1 d . . . O5 O 0.4798(18) 0.2339(12) 0.1648(12) Uiso 0.037(3) 2 1 d . . . C1 C -0.537(2) 1.2004(16) 0.2709(15) Uiso 0.031(3) 2 1 d . . . O6 O -0.8676(14) 1.4252(10) 0.4534(10) Uiso 0.026(2) 2 1 d . . . O7 O -0.214(2) 0.8120(15) 0.1512(15) Uiso 0.053(4) 2 1 d . . . C2 C -0.6106(16) 1.4181(11) 0.2854(11) Uiso 0.017(2) 2 1 d . . . O9 O -0.552(3) 0.7984(17) 0.0804(17) Uiso 0.064(5) 2 1 d . . . C3 C -0.625(2) 1.5065(14) 0.3655(14) Uiso 0.028(3) 2 1 d . . . O10 O -0.4875(14) 1.4797(10) 0.1004(10) Uiso 0.026(2) 2 1 d . . . O11 O -0.0711(17) 0.5874(11) 0.2849(11) Uiso 0.034(3) 2 1 d . . . O12 O -0.318(3) 0.978(2) 0.479(2) Uiso 0.082(6) 2 1 d . . . O13 O -0.0180(17) 0.2846(11) 0.3200(11) Uiso 0.034(3) 2 1 d . . . C4 C -0.763(2) 1.4966(15) 0.4567(15) Uiso 0.031(3) 2 1 d . . . O16 O -0.229(3) 0.9002(18) -0.0991(18) Uiso 0.067(5) 2 1 d . . . O17 O -0.594(3) 0.993(2) -0.092(2) Uiso 0.084(7) 2 1 d . . . O18 O -0.099(3) 0.7931(17) 0.3795(17) Uiso 0.064(5) 2 1 d . . . O19 O -0.1937(16) 0.3588(11) -0.0443(11) Uiso 0.031(2) 2 1 d . . . C5 C -0.574(2) 1.2905(14) 0.3478(15) Uiso 0.029(3) 2 1 d . . . O20 O -0.7708(17) 1.5606(11) 0.5304(11) Uiso 0.034(3) 2 1 d . . . O21 O -0.474(3) 0.844(2) 0.335(2) Uiso 0.083(7) 2 1 d . . . O14 O -0.524(3) 1.0981(18) 0.3169(18) Uiso 0.068(5) 2 1 d . . . C6 C -0.4631(18) 1.4445(13) 0.2055(12) Uiso 0.021(3) 2 1 d . . . O8 O -0.160(3) 1.0238(19) 0.2447(19) Uiso 0.070(5) 2 1 d . . . Ow1 O -0.105(5) 0.113(3) -0.010(3) Uiso 0.139(9) 2 1 d . . . Ow2 O 0.186(5) 0.856(3) 0.268(3) Uiso 0.139(9) 2 1 d . . . H1c3 H -0.519934 1.502585 0.400124 Uiso 0.0332 2 1 d . . . H2c3 H -0.638786 1.582852 0.321649 Uiso 0.0332 2 1 d . . . H1c5 H -0.483668 1.283495 0.397967 Uiso 0.0343 2 1 d . . . H2c5 H -0.666998 1.272501 0.39978 Uiso 0.0343 2 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 U1 U 0.00808(19) 0.0365(3) 0.0120(2) -0.00305(17) 0.00013(14) -0.00843(18) U2 U 0.00845(18) 0.0267(2) 0.0136(2) -0.00406(15) -0.00055(14) -0.00497(16) U3 U 0.0410(14) 0.0479(16) 0.0754(17) 0.0003(11) -0.0095(12) -0.0202(13) U4 U 0.104(3) 0.087(3) 0.080(3) -0.009(2) -0.005(2) -0.019(2) #======================================================================= # 10. MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag U1 O1 . 1_645 2.403(8) yes U1 O2 . 1_545 2.387(16) yes U1 O4 . . 2.245(11) yes U1 O6 . 1_645 2.367(11) yes U1 O11 . . 1.757(12) yes U1 O13 . . 1.753(12) yes U1 O20 . 2_476 2.465(13) yes U2 O1 . 2_475 2.376(9) yes U2 O3 . . 1.819(12) yes U2 O4 . . 2.232(9) yes U2 O4 . 2_565 2.242(9) yes U2 O19 . . 1.776(12) yes U3 O3 . . 2.397(11) yes U3 O5 . 2_565 2.430(14) yes U3 O7 . . 2.41(2) yes U3 O9 . . 1.72(2) yes U3 O16 . . 1.74(2) yes U3 O17 . . 2.32(2) yes U3 O17 . 2_475 2.40(3) yes U4 O7 . . 2.37(2) yes U4 O12 . . 2.48(3) yes U4 O17 . 2_475 2.38(2) yes U4 O18 . . 2.47(2) yes U4 O21 . . 1.81(2) yes U4 O14 . . 2.43(2) yes U4 O8 . . 1.72(3) yes O1 C2 . . 1.398(18) yes O1 C3 . . 2.406(18) yes O1 C5 . . 2.444(15) yes O1 C6 . . 2.381(18) yes O2 C2 . . 2.39(2) yes O2 O10 . . 2.185(17) yes O2 C6 . . 1.24(2) yes O5 C1 . 1_645 1.26(3) yes O5 C5 . 1_645 2.386(18) yes O5 O14 . 1_645 2.21(2) yes C1 C5 . . 1.51(3) yes C1 O14 . . 1.23(3) yes O6 C3 . . 2.401(18) yes O6 C4 . . 1.29(2) yes O6 O20 . . 2.244(19) yes C2 C3 . . 1.541(18) yes C2 O10 . . 2.398(16) yes C2 C5 . . 1.571(16) yes C2 C6 . . 1.51(2) yes C3 C4 . . 1.50(2) yes C3 O20 . . 2.354(18) yes C3 H1c3 . . 0.9533 yes C3 H2c3 . . 0.9574 yes O10 O10 . 2_485 2.365(17) yes O10 C6 . . 1.268(16) yes C4 O20 . . 1.25(3) yes C5 O14 . . 2.35(3) yes C5 H1c5 . . 0.9563 yes C5 H2c5 . . 0.9605 yes #======================================================================= loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2846.91 186.24 22.37 o 2 0 0 2832.39 2285.17 63.21 o 3 0 0 16402.96 14319.02 362.01 o 4 0 0 8984.20 11809.54 312.19 o 5 0 0 18828.77 18968.10 429.07 o 6 0 0 2949.66 3369.17 122.79 o 7 0 0 12324.60 12521.64 421.63 o 8 0 0 174.65 9.38 110.98 < 9 0 0 2.94 103.95 128.44 < 10 0 0 268.52 591.32 171.14 o 11 0 0 15819.56 16821.74 748.62 o -11 1 0 10208.66 9626.86 778.34 o -10 1 0 2063.86 2575.46 278.76 o -9 1 0 3286.50 4049.75 319.18 o -8 1 0 41.69 112.55 102.39 < -7 1 0 1376.07 1085.16 127.57 o -6 1 0 3819.93 3936.18 204.65 o -5 1 0 26569.40 28323.71 738.56 o -4 1 0 72678.84 78698.76 1560.68 o -3 1 0 14382.70 10279.96 228.52 o -2 1 0 44952.64 36935.89 741.13 o -1 1 0 24381.90 25852.01 511.11 o 1 1 0 168716.53 160053.53 4553.23 o 2 1 0 22750.20 23074.31 1304.47 o 3 1 0 1638.82 1661.73 88.50 o 4 1 0 33548.52 37555.97 920.11 o 5 1 0 3526.95 3697.76 111.30 o 6 1 0 7395.69 6615.72 201.95 o 7 1 0 35852.54 38611.57 1123.30 o 8 1 0 131.66 327.20 101.86 o 9 1 0 10.94 -9.12 101.08 < 10 1 0 7541.69 8282.46 409.94 o 11 1 0 6513.19 6963.43 573.75 o -11 2 0 3255.21 3434.71 544.96 o -10 2 0 493.75 517.03 288.60 < -9 2 0 4469.43 4059.51 346.83 o -8 2 0 1093.34 1467.58 165.87 o -7 2 0 1635.94 1780.36 134.33 o -6 2 0 8311.72 8312.02 236.11 o -5 2 0 4022.73 4529.95 160.42 o -4 2 0 49373.93 51822.78 1123.18 o -3 2 0 36332.86 33410.63 753.96 o -2 2 0 84425.93 69805.10 1296.03 o -1 2 0 89494.84 76617.00 1412.56 o 0 2 0 122743.26 121006.71 3370.33 o 1 2 0 6408.50 2490.89 57.37 o 2 2 0 77.47 152.14 39.34 o 3 2 0 4752.82 4118.80 338.86 o 4 2 0 4042.11 4243.56 384.50 o 5 2 0 8.98 10.68 48.46 < 6 2 0 12639.37 14231.39 473.26 o 7 2 0 24695.80 28448.31 826.83 o 8 2 0 10482.94 9517.47 393.54 o 9 2 0 1322.14 1872.57 164.03 o 10 2 0 2643.88 2797.78 314.85 o 11 2 0 18104.61 18790.49 1105.06 o -11 3 0 4187.92 3447.45 573.84 o -10 3 0 488.68 428.73 316.99 < -9 3 0 4087.24 4336.65 525.80 o -8 3 0 10635.33 9624.35 414.01 o -7 3 0 1030.53 930.15 150.77 o -6 3 0 185.66 318.34 95.60 o -5 3 0 71993.41 68579.86 1723.15 o -4 3 0 5455.13 6034.53 225.24 o -3 3 0 2000.00 2330.82 135.85 o -2 3 0 26502.43 20657.44 500.70 o -1 3 0 18543.58 11361.58 250.65 o 0 3 0 102048.59 96394.97 1779.97 o 1 3 0 5204.58 5167.60 127.03 o 2 3 0 29167.62 27274.66 519.11 o 3 3 0 22018.20 22440.20 559.16 o 4 3 0 569.29 304.73 54.43 o 5 3 0 2617.40 2504.76 135.81 o 6 3 0 35271.30 34885.34 1055.52 o 7 3 0 32691.61 33158.59 2052.04 o 8 3 0 197.08 317.29 104.46 o 9 3 0 1676.30 1748.35 213.47 o 10 3 0 52.24 315.23 161.52 < 11 3 0 7268.17 7342.63 361.94 o 12 3 0 3888.41 3781.46 358.33 o -11 4 0 1763.66 1825.27 546.38 o -10 4 0 925.25 1503.11 420.57 o -9 4 0 13023.54 12399.94 914.14 o -8 4 0 1252.07 1781.50 256.21 o -7 4 0 7685.85 7446.00 363.94 o -6 4 0 2.11 63.31 90.14 < -5 4 0 7092.86 7811.51 286.61 o -4 4 0 98654.20 98063.61 2433.56 o -3 4 0 7673.88 6700.14 168.92 o -2 4 0 8265.90 7039.07 244.08 o -1 4 0 16830.99 12852.83 315.20 o 0 4 0 1963.13 3408.75 140.27 o 1 4 0 29.57 86.23 42.99 < 2 4 0 11236.35 14508.95 299.35 o 3 4 0 7129.85 7305.11 178.31 o 4 4 0 2518.67 2092.17 77.54 o 5 4 0 3051.13 3552.29 180.79 o 6 4 0 1087.85 1711.79 135.14 o 7 4 0 53076.67 53403.95 3118.68 o 8 4 0 2114.38 2251.86 455.47 o 9 4 0 4151.39 3986.77 205.94 o 10 4 0 2792.44 3454.31 209.71 o 11 4 0 2066.42 2032.49 176.21 o 12 4 0 671.92 586.78 175.54 o -11 5 0 25.11 568.72 504.89 < -10 5 0 180.01 -131.82 363.14 < -9 5 0 15264.42 14526.71 735.97 o -8 5 0 12371.77 12263.25 636.98 o -7 5 0 3978.05 3733.98 348.20 o -6 5 0 12152.66 12436.25 422.46 o -5 5 0 13792.06 12451.21 411.44 o -4 5 0 4495.04 4343.35 223.29 o -3 5 0 17352.24 17248.35 457.53 o -2 5 0 26095.55 25196.50 696.05 o -1 5 0 1805.88 1946.36 117.65 o 0 5 0 5354.65 5057.43 202.37 o 1 5 0 971.84 853.04 88.79 o 2 5 0 23668.87 21180.91 522.70 o 3 5 0 51894.33 54897.94 1043.19 o 4 5 0 6062.71 5258.00 169.60 o 5 5 0 2302.90 2006.36 101.49 o 6 5 0 23910.57 24698.96 786.85 o 7 5 0 4250.19 5509.18 251.68 o 8 5 0 6193.21 5881.08 294.33 o 9 5 0 1418.79 1550.69 174.70 o -10 6 0 4875.00 3507.18 693.74 o -9 6 0 3434.11 3354.42 408.38 o -8 6 0 9002.55 7159.46 514.74 o -7 6 0 1966.38 1711.93 275.91 o -6 6 0 8124.27 9515.43 412.13 o -5 6 0 29034.62 31171.07 875.63 o -4 6 0 13327.75 13916.56 382.78 o -3 6 0 10172.67 8726.90 323.47 o -2 6 0 4936.97 4744.65 200.62 o -1 6 0 6080.49 5804.60 201.53 o 0 6 0 1965.90 2789.45 168.65 o 1 6 0 18461.15 17805.76 517.53 o 2 6 0 24885.93 28079.50 692.17 o 3 6 0 19487.87 20882.54 523.80 o 4 6 0 21728.33 21258.30 599.55 o 5 6 0 9992.20 9380.86 236.69 o 6 6 0 9074.73 8408.27 284.81 o 7 6 0 27173.27 28255.47 1159.82 o 8 6 0 2427.99 2841.24 208.19 o 9 6 0 1158.06 860.06 145.30 o 10 6 0 1321.79 1367.97 465.54 < -10 7 0 480.74 600.90 538.12 < -9 7 0 16373.79 13006.30 784.65 o -8 7 0 47.06 -17.45 230.30 < -7 7 0 1.64 -521.31 186.28 < -6 7 0 721.42 924.30 180.48 o -5 7 0 737.97 1152.69 187.51 o -4 7 0 10183.32 11073.17 318.61 o -3 7 0 2842.13 3057.67 212.29 o -2 7 0 23422.39 27234.23 786.20 o -1 7 0 9841.75 10227.94 325.32 o 0 7 0 362.98 219.06 81.79 < 1 7 0 45.24 615.61 90.66 o 2 7 0 73503.80 72732.03 1842.58 o 3 7 0 15950.59 14385.66 399.52 o 4 7 0 4180.05 4084.64 177.83 o 5 7 0 6909.23 5908.33 240.70 o 6 7 0 301.39 489.98 99.51 o 7 7 0 7902.33 6878.68 324.45 o 8 7 0 505.10 653.25 135.18 o 9 7 0 11503.03 10809.54 588.00 o 10 7 0 1994.85 1807.95 200.68 o -9 8 0 1896.00 1144.25 477.90 < -8 8 0 8446.51 7010.38 810.19 o -7 8 0 6424.26 8027.80 642.38 o -6 8 0 1052.26 1133.00 211.45 o -5 8 0 2584.86 3268.78 290.14 o -4 8 0 47.26 86.49 93.27 < -3 8 0 2501.91 2409.81 244.08 o -2 8 0 27501.45 25571.71 876.00 o -1 8 0 1053.92 1289.97 141.39 o 0 8 0 3681.14 3102.60 180.99 o 1 8 0 5491.04 5891.39 249.16 o 2 8 0 645.07 1332.95 139.08 o 3 8 0 52265.55 50179.66 1194.69 o 4 8 0 1446.80 1360.55 121.84 o 5 8 0 13343.42 12922.44 431.25 o 6 8 0 7547.30 7837.54 309.18 o 7 8 0 338.03 404.01 134.67 o 8 8 0 1149.13 1124.36 172.64 o 9 8 0 6192.74 5500.41 328.37 o 10 8 0 5429.15 5555.45 354.20 o 11 8 0 38.83 -28.14 206.85 < -9 9 0 1042.35 648.13 480.43 < -8 9 0 8.83 1095.25 457.22 < -7 9 0 40.73 153.19 381.66 < -6 9 0 6178.48 6651.05 501.91 o -5 9 0 15.80 94.05 186.01 < -4 9 0 53.29 74.77 125.57 < -3 9 0 1435.35 1434.00 241.34 o -2 9 0 12921.35 14667.03 694.36 o -1 9 0 14488.71 14596.42 557.71 o 0 9 0 8132.96 9092.60 353.94 o 1 9 0 6214.65 5857.94 299.73 o 2 9 0 24965.55 25849.69 738.75 o 3 9 0 644.58 1242.32 139.34 o 4 9 0 978.20 1054.12 125.52 o 5 9 0 7202.71 7747.32 321.43 o 6 9 0 2194.08 2331.93 191.81 o 7 9 0 3526.21 3772.27 288.45 o 8 9 0 2537.79 2629.82 260.22 o 9 9 0 8184.48 7712.54 425.65 o 10 9 0 4725.44 4508.82 333.25 o 11 9 0 2.92 -113.33 266.00 < -8 10 0 1.97 -60.44 405.38 < -7 10 0 4297.23 5626.06 782.63 o -6 10 0 2781.55 2576.44 359.85 o -5 10 0 297.93 -78.15 189.90 < -4 10 0 290.78 375.63 214.65 < -3 10 0 10947.02 13120.57 676.74 o -2 10 0 3213.29 4238.04 381.87 o -1 10 0 1599.09 1155.33 221.54 o 0 10 0 3365.75 3377.47 261.41 o 1 10 0 9063.47 10476.40 443.29 o 2 10 0 7346.02 7995.09 365.53 o 3 10 0 11241.71 9940.57 341.01 o 4 10 0 13884.87 13538.65 412.80 o 5 10 0 2777.88 2710.38 224.54 o 6 10 0 250.02 209.70 130.25 < 7 10 0 2.53 122.45 163.35 < 8 10 0 887.11 531.52 183.86 < 9 10 0 8016.41 6473.86 431.38 o 10 10 0 2250.02 2523.38 299.81 o 11 10 0 1.17 -221.97 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