# Electronic Supplementary Material (ESI) for Dalton Transactions
# This journal is © The Royal Society of Chemistry 2012


data_global
_journal_name_full               'Dalton Trans.'
_journal_coden_cambridge         0222
_journal_year                    ?
_journal_volume                  ?
_journal_page_first              ?
loop_
_publ_author_name
R.Ramirez-Contreras
O.Ozerov
_publ_contact_author_name        'Oleg Ozerov'
_publ_contact_author_email       ozerov@chem.tamu.edu

data_oz335_RC448
_database_code_depnum_ccdc_archive 'CCDC 859566'
#TrackingRef '- oz334_RRC448.cif'

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
;
?
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         'C11 H16 Ag B11 Cl11 F O'
_chemical_formula_sum            'C11 H16 Ag B11 Cl11 F O'
_chemical_formula_weight         799.97

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           Monoclinic
_symmetry_space_group_name_H-M   Cc
_symmetry_space_group_name_Hall  'C -2yc'

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'x, -y, z+1/2'
'x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z+1/2'

_cell_length_a                   8.931(5)
_cell_length_b                   16.763(9)
_cell_length_c                   18.452(10)
_cell_angle_alpha                90.00
_cell_angle_beta                 91.830(5)
_cell_angle_gamma                90.00
_cell_volume                     2761(2)
_cell_formula_units_Z            4
_cell_measurement_temperature    150(2)
_cell_measurement_reflns_used    9990
_cell_measurement_theta_min      2.21
_cell_measurement_theta_max      27.45

_exptl_crystal_description       prism
_exptl_crystal_colour            colorless
_exptl_crystal_size_max          0.46
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.13
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    1.924
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1552
_exptl_absorpt_coefficient_mu    1.813
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.5682
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_process_details   'SADABS; (Sheldrick, 2006)'

_exptl_special_details           
;
?
;

_diffrn_ambient_temperature      150(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            14456
_diffrn_reflns_av_R_equivalents  0.0272
_diffrn_reflns_av_sigmaI/netI    0.0355
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_theta_min         2.21
_diffrn_reflns_theta_max         27.50
_reflns_number_total             6241
_reflns_number_gt                6097
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'APEX-II (BRUKER-NONIUS, 2003)'
_computing_cell_refinement       
;
APEX-II(BRUKER-NONIUS, 2003)
;
_computing_data_reduction        APEX-II
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_molecular_graphics    'X-SEED (Barbour, 2001)'
_computing_publication_material  'Bruker SHELXTL'

_refine_special_details          
;
Refinement of F^2^ against ALL reflections. The weighted R-factor wR and
goodness of fit S are based on F^2^, conventional R-factors R are based
on F, with F set to zero for negative F^2^. The threshold expression of
F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is
not relevant to the choice of reflections for refinement. R-factors based
on F^2^ are statistically about twice as large as those based on F, and R-
factors based on ALL data will be even larger.
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[\s^2^(Fo^2^)+(0.0285P)^2^+0.2421P] where P=(Fo^2^+2Fc^2^)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   -0.001(15)
_refine_ls_number_reflns         6241
_refine_ls_number_parameters     335
_refine_ls_number_restraints     8
_refine_ls_R_factor_all          0.0233
_refine_ls_R_factor_gt           0.0225
_refine_ls_wR_factor_ref         0.0566
_refine_ls_wR_factor_gt          0.0561
_refine_ls_goodness_of_fit_ref   1.030
_refine_ls_restrained_S_all      1.033
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.83209(2) 0.784767(12) 0.188076(13) 0.03901(6) Uani 1 1 d . . .
Cl1 Cl 1.05902(7) 0.41903(4) 0.21460(3) 0.02706(12) Uani 1 1 d . . .
Cl2 Cl 1.33838(8) 0.57636(4) 0.20158(4) 0.03276(14) Uani 1 1 d . . .
Cl3 Cl 0.94397(8) 0.62835(4) 0.22452(3) 0.03459(14) Uani 1 1 d . . .
Cl4 Cl 0.71439(7) 0.48944(4) 0.11531(4) 0.03415(14) Uani 1 1 d . . .
Cl5 Cl 0.97286(9) 0.34750(4) 0.03195(4) 0.03670(15) Uani 1 1 d . . .
Cl6 Cl 1.35267(7) 0.40263(3) 0.07774(3) 0.02694(12) Uani 1 1 d . . .
Cl7 Cl 1.16145(8) 0.74366(3) 0.09783(4) 0.03693(15) Uani 1 1 d . . .
Cl8 Cl 0.78597(7) 0.68504(4) 0.04593(3) 0.03012(13) Uani 1 1 d . . .
Cl9 Cl 1.18356(7) 0.46490(4) -0.09757(3) 0.03058(13) Uani 1 1 d . . .
Cl10 Cl 1.42005(7) 0.60494(4) 0.00979(4) 0.03505(15) Uani 1 1 d . . .
Cl11 Cl 1.06372(7) 0.66839(4) -0.08551(3) 0.03174(14) Uani 1 1 d . . .
F1 F 1.3411(2) 0.76063(13) 0.29296(11) 0.0508(5) Uani 1 1 d . . .
B1 B 1.0644(3) 0.48302(15) 0.13766(13) 0.0194(5) Uani 1 1 d . . .
B2 B 1.2004(3) 0.56079(15) 0.13098(14) 0.0219(5) Uani 1 1 d . . .
B3 B 1.0084(3) 0.58492(16) 0.14296(14) 0.0222(5) Uani 1 1 d . . .
B4 B 0.8973(3) 0.51618(16) 0.09147(15) 0.0223(5) Uani 1 1 d . . .
B5 B 1.0203(3) 0.44841(15) 0.04817(14) 0.0214(5) Uani 1 1 d . . .
B6 B 1.2071(3) 0.47636(15) 0.07229(14) 0.0199(5) Uani 1 1 d . . .
B7 B 1.1169(3) 0.64177(15) 0.08086(15) 0.0231(5) Uani 1 1 d . . .
B8 B 0.9318(3) 0.61383(16) 0.05713(15) 0.0226(5) Uani 1 1 d . . .
B9 B 1.1286(3) 0.50486(15) -0.01401(14) 0.0216(5) Uani 1 1 d . . .
B10 B 1.2407(3) 0.57398(15) 0.03736(16) 0.0225(5) Uani 1 1 d . . .
B11 B 1.0726(3) 0.60689(16) -0.00792(15) 0.0212(5) Uani 1 1 d . . .
C1 C 0.9429(3) 0.53007(14) 0.00132(12) 0.0213(4) Uani 1 1 d . A .
C2 C 0.8178(4) 0.52238(16) -0.05702(16) 0.0369(6) Uani 1 1 d D . .
H2A H 0.7325 0.5553 -0.0416 0.044 Uiso 1 1 calc R A .
H2B H 0.8545 0.5466 -0.1021 0.044 Uiso 1 1 calc R . .
C3 C 0.7595(5) 0.4432(3) -0.0755(2) 0.0302(7) Uani 0.605(4) 1 d PD A -1
H3A H 0.7244 0.4166 -0.0312 0.036 Uiso 0.605(4) 1 calc PR A -1
H3B H 0.8401 0.4103 -0.0957 0.036 Uiso 0.605(4) 1 calc PR A -1
C4 C 0.6306(8) 0.4505(4) -0.1307(3) 0.0328(13) Uani 0.605(4) 1 d PD A -1
H4A H 0.6688 0.4691 -0.1775 0.039 Uiso 0.605(4) 1 calc PR A -1
H4B H 0.5575 0.4902 -0.1138 0.039 Uiso 0.605(4) 1 calc PR A -1
C5 C 0.5538(8) 0.3699(4) -0.1411(4) 0.0449(12) Uani 0.605(4) 1 d PD A -1
H5A H 0.4707 0.3752 -0.1767 0.067 Uiso 0.605(4) 1 calc PR A -1
H5B H 0.5152 0.3518 -0.0948 0.067 Uiso 0.605(4) 1 calc PR A -1
H5C H 0.6261 0.3309 -0.1585 0.067 Uiso 0.605(4) 1 calc PR A -1
C3A C 0.8178(7) 0.4739(4) -0.1223(3) 0.0302(7) Uani 0.395(4) 1 d PD A -2
H3AA H 0.8718 0.4236 -0.1111 0.036 Uiso 0.395(4) 1 calc PR A -2
H3AB H 0.8749 0.5026 -0.1594 0.036 Uiso 0.395(4) 1 calc PR A -2
C4A C 0.6632(13) 0.4530(7) -0.1552(5) 0.0328(13) Uani 0.395(4) 1 d PD A -2
H4AA H 0.5962 0.4996 -0.1506 0.039 Uiso 0.395(4) 1 calc PR A -2
H4AB H 0.6728 0.4417 -0.2075 0.039 Uiso 0.395(4) 1 calc PR A -2
C5A C 0.5928(13) 0.3815(6) -0.1192(6) 0.0449(12) Uani 0.395(4) 1 d PD A -2
H5AA H 0.4941 0.3711 -0.1420 0.067 Uiso 0.395(4) 1 calc PR A -2
H5AB H 0.5818 0.3925 -0.0675 0.067 Uiso 0.395(4) 1 calc PR A -2
H5AC H 0.6571 0.3347 -0.1249 0.067 Uiso 0.395(4) 1 calc PR A -2
C6 C 1.0049(3) 0.87591(16) 0.26355(14) 0.0330(6) Uani 1 1 d . . .
H6A H 0.9654 0.9220 0.2387 0.050 Uiso 1 1 d R . .
C7 C 0.9119(3) 0.84139(17) 0.31390(15) 0.0342(6) Uani 1 1 d . . .
H7A H 0.8167 0.8665 0.3204 0.051 Uiso 1 1 d R . .
C8 C 0.9663(4) 0.77900(17) 0.35710(15) 0.0361(6) Uani 1 1 d . . .
H8A H 0.9025 0.7548 0.3910 0.043 Uiso 1 1 calc R . .
C9 C 1.1103(3) 0.75190(15) 0.35147(14) 0.0332(6) Uani 1 1 d . . .
H9A H 1.1480 0.7102 0.3817 0.040 Uiso 1 1 calc R . .
C10 C 1.1995(3) 0.78739(15) 0.30006(15) 0.0294(5) Uani 1 1 d . . .
C11 C 1.1494(3) 0.84862(16) 0.25686(14) 0.0322(6) Uani 1 1 d . . .
H11A H 1.2134 0.8721 0.2227 0.039 Uiso 1 1 calc R . .
O1 O 0.5990(3) 0.72430(13) 0.19067(15) 0.0483(6) Uani 1 1 d . . .
H1O H 0.6047 0.6809 0.1671 0.072 Uiso 1 1 d R . .
H1P H 0.5129 0.7453 0.1937 0.072 Uiso 1 1 d R . .

loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Ag1 0.04232(12) 0.03284(11) 0.04134(12) 0.00362(9) -0.00712(8) -0.00643(9)
Cl1 0.0330(3) 0.0252(3) 0.0229(3) 0.0077(2) 0.0005(2) 0.0003(2)
Cl2 0.0362(3) 0.0261(3) 0.0350(3) -0.0006(2) -0.0138(3) -0.0049(2)
Cl3 0.0492(4) 0.0319(3) 0.0230(3) -0.0035(2) 0.0058(2) 0.0126(3)
Cl4 0.0214(3) 0.0422(4) 0.0390(3) 0.0141(3) 0.0031(2) -0.0030(2)
Cl5 0.0605(4) 0.0166(3) 0.0327(3) 0.0004(2) -0.0025(3) -0.0106(3)
Cl6 0.0284(3) 0.0212(3) 0.0315(3) 0.0041(2) 0.0043(2) 0.0082(2)
Cl7 0.0503(4) 0.0143(3) 0.0458(4) -0.0013(3) -0.0042(3) -0.0030(3)
Cl8 0.0289(3) 0.0258(3) 0.0358(3) 0.0046(2) 0.0030(2) 0.0103(2)
Cl9 0.0401(3) 0.0290(3) 0.0230(3) -0.0032(2) 0.0070(2) 0.0042(2)
Cl10 0.0229(3) 0.0343(3) 0.0483(4) 0.0141(3) 0.0066(3) -0.0023(2)
Cl11 0.0391(3) 0.0269(3) 0.0295(3) 0.0135(2) 0.0064(2) 0.0046(2)
F1 0.0294(9) 0.0581(12) 0.0643(13) -0.0208(10) -0.0057(8) 0.0101(8)
B1 0.0225(12) 0.0164(11) 0.0193(11) 0.0027(9) -0.0013(9) -0.0004(9)
B2 0.0268(13) 0.0164(11) 0.0225(12) -0.0005(9) -0.0019(10) -0.0010(10)
B3 0.0274(13) 0.0202(13) 0.0189(12) -0.0019(9) 0.0006(10) 0.0015(10)
B4 0.0221(12) 0.0203(12) 0.0245(12) 0.0047(10) 0.0001(10) -0.0021(10)
B5 0.0262(13) 0.0164(12) 0.0214(12) 0.0010(9) -0.0006(10) -0.0014(10)
B6 0.0209(12) 0.0165(11) 0.0223(12) 0.0023(9) 0.0000(9) 0.0009(9)
B7 0.0274(13) 0.0143(11) 0.0276(13) 0.0023(10) 0.0000(10) -0.0012(9)
B8 0.0247(13) 0.0207(12) 0.0226(12) 0.0033(10) 0.0056(10) 0.0024(10)
B9 0.0266(13) 0.0181(12) 0.0203(12) 0.0019(9) 0.0041(10) 0.0019(10)
B10 0.0197(12) 0.0203(12) 0.0278(13) 0.0045(10) 0.0065(10) 0.0006(9)
B11 0.0231(13) 0.0178(12) 0.0230(12) 0.0043(9) 0.0041(10) 0.0014(9)
C1 0.0235(11) 0.0187(11) 0.0217(11) 0.0027(8) -0.0013(8) -0.0007(8)
C2 0.0448(16) 0.0328(14) 0.0321(13) -0.0019(12) -0.0167(11) 0.0064(12)
C3 0.0296(18) 0.0333(19) 0.0270(17) 0.0020(14) -0.0085(13) -0.0046(14)
C4 0.038(3) 0.0325(17) 0.027(4) 0.000(3) -0.011(2) -0.006(2)
C5 0.053(4) 0.036(3) 0.044(4) -0.004(3) -0.022(2) -0.009(2)
C3A 0.0296(18) 0.0333(19) 0.0270(17) 0.0020(14) -0.0085(13) -0.0046(14)
C4A 0.038(3) 0.0325(17) 0.027(4) 0.000(3) -0.011(2) -0.006(2)
C5A 0.053(4) 0.036(3) 0.044(4) -0.004(3) -0.022(2) -0.009(2)
C6 0.0476(16) 0.0233(12) 0.0277(12) -0.0009(10) -0.0069(11) 0.0079(11)
C7 0.0341(14) 0.0374(15) 0.0311(13) -0.0097(11) 0.0017(10) 0.0057(11)
C8 0.0502(17) 0.0334(15) 0.0251(13) -0.0043(10) 0.0079(12) -0.0075(12)
C9 0.0526(17) 0.0206(12) 0.0260(12) 0.0013(10) -0.0080(11) 0.0007(11)
C10 0.0272(13) 0.0289(13) 0.0316(13) -0.0088(10) -0.0045(10) 0.0043(10)
C11 0.0424(15) 0.0289(13) 0.0255(12) 0.0007(10) 0.0041(11) -0.0073(11)
O1 0.0386(12) 0.0384(12) 0.0693(16) -0.0120(11) 0.0222(11) -0.0022(9)

_geom_special_details            
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 O1 2.317(2) . ?
Ag1 C6 2.553(3) . ?
Ag1 C7 2.587(3) . ?
Ag1 Cl6 2.8472(12) 3_455 ?
Ag1 Cl3 2.8780(14) . ?
Cl1 B1 1.781(3) . ?
Cl2 B2 1.784(3) . ?
Cl3 B3 1.784(3) . ?
Cl4 B4 1.763(3) . ?
Cl5 B5 1.767(3) . ?
Cl6 B6 1.794(3) . ?
Cl6 Ag1 2.8472(12) 3_545 ?
Cl7 B7 1.779(3) . ?
Cl8 B8 1.774(3) . ?
Cl9 B9 1.765(3) . ?
Cl10 B10 1.773(3) . ?
Cl11 B11 1.764(3) . ?
F1 C10 1.353(3) . ?
B1 B4 1.784(4) . ?
B1 B5 1.782(4) . ?
B1 B3 1.783(4) . ?
B1 B6 1.786(4) . ?
B1 B2 1.789(4) . ?
B2 B3 1.782(4) . ?
B2 B6 1.784(4) . ?
B2 B10 1.790(4) . ?
B2 B7 1.791(4) . ?
B3 B8 1.773(4) . ?
B3 B4 1.776(4) . ?
B3 B7 1.798(4) . ?
B4 C1 1.741(3) . ?
B4 B5 1.787(4) . ?
B4 B8 1.786(4) . ?
B5 C1 1.750(4) . ?
B5 B6 1.775(4) . ?
B5 B9 1.794(4) . ?
B6 B9 1.784(4) . ?
B6 B10 1.788(4) . ?
B7 B8 1.760(4) . ?
B7 B11 1.772(4) . ?
B7 B10 1.793(4) . ?
B8 C1 1.746(4) . ?
B8 B11 1.770(4) . ?
B9 C1 1.743(4) . ?
B9 B10 1.784(4) . ?
B9 B11 1.786(4) . ?
B10 B11 1.782(4) . ?
B11 C1 1.744(4) . ?
C1 C2 1.532(4) . ?
C2 C3A 1.453(7) . ?
C2 C3 1.462(5) . ?
C2 H2A 0.9900 . ?
C2 H2B 0.9900 . ?
C3 C4 1.517(7) . ?
C3 H3A 0.9900 . ?
C3 H3B 0.9900 . ?
C4 C5 1.524(8) . ?
C4 H4A 0.9900 . ?
C4 H4B 0.9900 . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C5 H5C 0.9800 . ?
C3A C4A 1.530(12) . ?
C3A H3AA 0.9900 . ?
C3A H3AB 0.9900 . ?
C4A C5A 1.517(13) . ?
C4A H4AA 0.9900 . ?
C4A H4AB 0.9900 . ?
C5A H5AA 0.9800 . ?
C5A H5AB 0.9800 . ?
C5A H5AC 0.9800 . ?
C6 C11 1.379(4) . ?
C6 C7 1.392(4) . ?
C6 H6A 0.9599 . ?
C7 C8 1.393(4) . ?
C7 H7A 0.9599 . ?
C8 C9 1.371(4) . ?
C8 H8A 0.9500 . ?
C9 C10 1.391(4) . ?
C9 H9A 0.9500 . ?
C10 C11 1.366(4) . ?
C11 H11A 0.9500 . ?
O1 H1O 0.8500 . ?
O1 H1P 0.8500 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Ag1 C6 141.10(9) . . ?
O1 Ag1 C7 111.34(9) . . ?
C6 Ag1 C7 31.40(9) . . ?
O1 Ag1 Cl6 113.39(7) . 3_455 ?
C6 Ag1 Cl6 85.59(7) . 3_455 ?
C7 Ag1 Cl6 111.40(8) . 3_455 ?
O1 Ag1 Cl3 84.37(7) . . ?
C6 Ag1 Cl3 102.62(7) . . ?
C7 Ag1 Cl3 92.34(7) . . ?
Cl6 Ag1 Cl3 140.31(2) 3_455 . ?
B3 Cl3 Ag1 107.08(9) . . ?
B6 Cl6 Ag1 117.06(9) . 3_545 ?
Cl1 B1 B4 121.68(17) . . ?
Cl1 B1 B5 122.12(17) . . ?
B4 B1 B5 60.13(15) . . ?
Cl1 B1 B3 121.22(17) . . ?
B4 B1 B3 59.74(15) . . ?
B5 B1 B3 107.98(17) . . ?
Cl1 B1 B6 122.60(16) . . ?
B4 B1 B6 107.51(18) . . ?
B5 B1 B6 59.68(14) . . ?
B3 B1 B6 107.71(18) . . ?
Cl1 B1 B2 121.96(17) . . ?
B4 B1 B2 107.43(18) . . ?
B5 B1 B2 107.69(17) . . ?
B3 B1 B2 59.85(15) . . ?
B6 B1 B2 59.89(14) . . ?
B3 B2 Cl2 121.41(17) . . ?
B3 B2 B6 107.83(18) . . ?
Cl2 B2 B6 121.58(17) . . ?
B3 B2 B1 59.92(15) . . ?
Cl2 B2 B1 120.74(17) . . ?
B6 B2 B1 59.97(15) . . ?
B3 B2 B10 108.41(18) . . ?
Cl2 B2 B10 122.10(18) . . ?
B6 B2 B10 60.02(15) . . ?
B1 B2 B10 108.33(18) . . ?
B3 B2 B7 60.40(15) . . ?
Cl2 B2 B7 122.18(17) . . ?
B6 B2 B7 108.00(18) . . ?
B1 B2 B7 108.39(19) . . ?
B10 B2 B7 60.09(15) . . ?
B8 B3 B4 60.41(15) . . ?
B8 B3 B2 107.25(18) . . ?
B4 B3 B2 108.04(18) . . ?
B8 B3 Cl3 121.10(18) . . ?
B4 B3 Cl3 121.75(18) . . ?
B2 B3 Cl3 122.34(18) . . ?
B8 B3 B1 108.28(18) . . ?
B4 B3 B1 60.13(15) . . ?
B2 B3 B1 60.22(15) . . ?
Cl3 B3 B1 122.40(17) . . ?
B8 B3 B7 59.07(15) . . ?
B4 B3 B7 107.83(18) . . ?
B2 B3 B7 60.06(15) . . ?
Cl3 B3 B7 121.11(18) . . ?
B1 B3 B7 108.36(18) . . ?
C1 B4 Cl4 121.29(18) . . ?
C1 B4 B3 106.30(18) . . ?
Cl4 B4 B3 122.52(18) . . ?
C1 B4 B1 106.30(18) . . ?
Cl4 B4 B1 124.69(17) . . ?
B3 B4 B1 60.13(15) . . ?
C1 B4 B5 59.45(14) . . ?
Cl4 B4 B5 122.53(18) . . ?
B3 B4 B5 108.10(19) . . ?
B1 B4 B5 59.90(15) . . ?
C1 B4 B8 59.34(14) . . ?
Cl4 B4 B8 119.56(17) . . ?
B3 B4 B8 59.69(15) . . ?
B1 B4 B8 107.70(18) . . ?
B5 B4 B8 107.98(18) . . ?
C1 B5 Cl5 125.20(18) . . ?
C1 B5 B6 105.70(18) . . ?
Cl5 B5 B6 120.89(17) . . ?
C1 B5 B1 105.98(17) . . ?
Cl5 B5 B1 120.88(16) . . ?
B6 B5 B1 60.26(15) . . ?
C1 B5 B4 58.97(14) . . ?
Cl5 B5 B4 122.48(18) . . ?
B6 B5 B4 107.83(19) . . ?
B1 B5 B4 59.97(15) . . ?
C1 B5 B9 58.92(14) . . ?
Cl5 B5 B9 121.86(17) . . ?
B6 B5 B9 59.99(15) . . ?
B1 B5 B9 108.26(18) . . ?
B4 B5 B9 107.60(18) . . ?
B5 B6 B9 60.52(14) . . ?
B5 B6 B2 108.19(18) . . ?
B9 B6 B2 108.03(18) . . ?
B5 B6 B1 60.06(14) . . ?
B9 B6 B1 108.52(18) . . ?
B2 B6 B1 60.14(15) . . ?
B5 B6 B10 108.59(18) . . ?
B9 B6 B10 59.94(15) . . ?
B2 B6 B10 60.13(15) . . ?
B1 B6 B10 108.55(18) . . ?
B5 B6 Cl6 120.37(17) . . ?
B9 B6 Cl6 119.85(16) . . ?
B2 B6 Cl6 123.40(17) . . ?
B1 B6 Cl6 122.45(16) . . ?
B10 B6 Cl6 121.38(17) . . ?
B8 B7 B11 60.13(15) . . ?
B8 B7 Cl7 120.14(17) . . ?
B11 B7 Cl7 121.43(17) . . ?
B8 B7 B2 107.39(18) . . ?
B11 B7 B2 107.71(18) . . ?
Cl7 B7 B2 123.34(18) . . ?
B8 B7 B10 107.92(19) . . ?
B11 B7 B10 59.98(15) . . ?
Cl7 B7 B10 123.35(18) . . ?
B2 B7 B10 59.90(15) . . ?
B8 B7 B3 59.76(15) . . ?
B11 B7 B3 107.78(19) . . ?
Cl7 B7 B3 121.24(18) . . ?
B2 B7 B3 59.55(15) . . ?
B10 B7 B3 107.58(18) . . ?
C1 B8 B7 106.87(18) . . ?
C1 B8 B11 59.49(14) . . ?
B7 B8 B11 60.27(16) . . ?
C1 B8 Cl8 121.85(18) . . ?
B7 B8 Cl8 122.02(18) . . ?
B11 B8 Cl8 120.01(17) . . ?
C1 B8 B3 106.24(18) . . ?
B7 B8 B3 61.17(16) . . ?
B11 B8 B3 109.01(19) . . ?
Cl8 B8 B3 123.30(17) . . ?
C1 B8 B4 59.05(14) . . ?
B7 B8 B4 109.09(19) . . ?
B11 B8 B4 108.35(18) . . ?
Cl8 B8 B4 121.59(17) . . ?
B3 B8 B4 59.90(15) . . ?
C1 B9 Cl9 121.77(18) . . ?
C1 B9 B10 106.09(18) . . ?
Cl9 B9 B10 122.92(17) . . ?
C1 B9 B6 105.58(17) . . ?
Cl9 B9 B6 124.45(17) . . ?
B10 B9 B6 60.12(15) . . ?
C1 B9 B11 59.22(14) . . ?
Cl9 B9 B11 120.30(17) . . ?
B10 B9 B11 59.88(15) . . ?
B6 B9 B11 107.62(18) . . ?
C1 B9 B5 59.27(14) . . ?
Cl9 B9 B5 121.95(17) . . ?
B10 B9 B5 107.91(18) . . ?
B6 B9 B5 59.49(14) . . ?
B11 B9 B5 107.89(18) . . ?
Cl10 B10 B11 121.99(18) . . ?
Cl10 B10 B9 122.30(18) . . ?
B11 B10 B9 60.12(15) . . ?
Cl10 B10 B6 122.35(17) . . ?
B11 B10 B6 107.67(18) . . ?
B9 B10 B6 59.94(15) . . ?
Cl10 B10 B2 121.63(19) . . ?
B11 B10 B2 107.36(18) . . ?
B9 B10 B2 107.81(18) . . ?
B6 B10 B2 59.84(14) . . ?
Cl10 B10 B7 121.22(18) . . ?
B11 B10 B7 59.43(15) . . ?
B9 B10 B7 107.80(19) . . ?
B6 B10 B7 107.79(18) . . ?
B2 B10 B7 60.01(15) . . ?
C1 B11 Cl11 119.86(18) . . ?
C1 B11 B8 59.58(14) . . ?
Cl11 B11 B8 119.83(17) . . ?
C1 B11 B7 106.42(17) . . ?
Cl11 B11 B7 124.09(18) . . ?
B8 B11 B7 59.60(15) . . ?
C1 B11 B10 106.13(18) . . ?
Cl11 B11 B10 125.24(17) . . ?
B8 B11 B10 107.97(19) . . ?
B7 B11 B10 60.59(16) . . ?
C1 B11 B9 59.15(14) . . ?
Cl11 B11 B9 120.92(17) . . ?
B8 B11 B9 108.17(18) . . ?
B7 B11 B9 108.63(19) . . ?
B10 B11 B9 60.00(15) . . ?
C2 C1 B4 118.2(2) . . ?
C2 C1 B9 122.8(2) . . ?
B4 C1 B9 112.05(18) . . ?
C2 C1 B11 117.7(2) . . ?
B4 C1 B11 111.62(18) . . ?
B9 C1 B11 61.63(15) . . ?
C2 C1 B8 115.36(19) . . ?
B4 C1 B8 61.61(15) . . ?
B9 C1 B8 111.28(18) . . ?
B11 C1 B8 60.93(15) . . ?
C2 C1 B5 123.3(2) . . ?
B4 C1 B5 61.57(15) . . ?
B9 C1 B5 61.81(15) . . ?
B11 C1 B5 111.88(19) . . ?
B8 C1 B5 111.51(18) . . ?
C3A C2 C3 46.3(3) . . ?
C3A C2 C1 127.6(3) . . ?
C3 C2 C1 119.1(3) . . ?
C3A C2 H2A 124.8 . . ?
C3 C2 H2A 107.5 . . ?
C1 C2 H2A 107.5 . . ?
C3A C2 H2B 61.6 . . ?
C3 C2 H2B 107.5 . . ?
C1 C2 H2B 107.5 . . ?
H2A C2 H2B 107.0 . . ?
C2 C3 C4 109.9(4) . . ?
C2 C3 H3A 109.7 . . ?
C4 C3 H3A 109.7 . . ?
C2 C3 H3B 109.7 . . ?
C4 C3 H3B 109.7 . . ?
H3A C3 H3B 108.2 . . ?
C3 C4 C5 110.0(5) . . ?
C3 C4 H4A 109.7 . . ?
C5 C4 H4A 109.7 . . ?
C3 C4 H4B 109.7 . . ?
C5 C4 H4B 109.7 . . ?
H4A C4 H4B 108.2 . . ?
C4 C5 H5A 109.5 . . ?
C4 C5 H5B 109.5 . . ?
H5A C5 H5B 109.5 . . ?
C4 C5 H5C 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
C2 C3A C4A 115.6(6) . . ?
C2 C3A H3AA 108.4 . . ?
C4A C3A H3AA 108.4 . . ?
C2 C3A H3AB 108.4 . . ?
C4A C3A H3AB 108.4 . . ?
H3AA C3A H3AB 107.4 . . ?
C5A C4A C3A 112.9(8) . . ?
C5A C4A H4AA 109.0 . . ?
C3A C4A H4AA 109.0 . . ?
C5A C4A H4AB 109.0 . . ?
C3A C4A H4AB 109.0 . . ?
H4AA C4A H4AB 107.8 . . ?
C4A C5A H5AA 109.5 . . ?
C4A C5A H5AB 109.5 . . ?
H5AA C5A H5AB 109.5 . . ?
C4A C5A H5AC 109.5 . . ?
H5AA C5A H5AC 109.5 . . ?
H5AB C5A H5AC 109.5 . . ?
C11 C6 C7 120.1(3) . . ?
C11 C6 Ag1 107.69(18) . . ?
C7 C6 Ag1 75.66(17) . . ?
C11 C6 H6A 123.7 . . ?
C7 C6 H6A 115.8 . . ?
Ag1 C6 H6A 90.9 . . ?
C6 C7 C8 119.3(3) . . ?
C6 C7 Ag1 72.93(16) . . ?
C8 C7 Ag1 108.60(19) . . ?
C6 C7 H7A 116.8 . . ?
C8 C7 H7A 123.5 . . ?
Ag1 C7 H7A 93.0 . . ?
C9 C8 C7 121.1(3) . . ?
C9 C8 H8A 119.5 . . ?
C7 C8 H8A 119.5 . . ?
C8 C9 C10 117.9(2) . . ?
C8 C9 H9A 121.0 . . ?
C10 C9 H9A 121.0 . . ?
F1 C10 C11 118.8(3) . . ?
F1 C10 C9 118.8(3) . . ?
C11 C10 C9 122.4(3) . . ?
C10 C11 C6 119.1(2) . . ?
C10 C11 H11A 120.4 . . ?
C6 C11 H11A 120.4 . . ?
Ag1 O1 H1O 107.2 . . ?
Ag1 O1 H1P 129.5 . . ?
H1O O1 H1P 117.2 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O1 Ag1 Cl3 B3 101.03(12) . . . . ?
C6 Ag1 Cl3 B3 -117.77(12) . . . . ?
C7 Ag1 Cl3 B3 -147.75(12) . . . . ?
Cl6 Ag1 Cl3 B3 -19.35(11) 3_455 . . . ?
Cl1 B1 B2 B3 -110.1(2) . . . . ?
B4 B1 B2 B3 37.52(17) . . . . ?
B5 B1 B2 B3 100.92(19) . . . . ?
B6 B1 B2 B3 138.03(19) . . . . ?
Cl1 B1 B2 Cl2 0.7(3) . . . . ?
B4 B1 B2 Cl2 148.39(18) . . . . ?
B5 B1 B2 Cl2 -148.21(18) . . . . ?
B3 B1 B2 Cl2 110.9(2) . . . . ?
B6 B1 B2 Cl2 -111.1(2) . . . . ?
Cl1 B1 B2 B6 111.9(2) . . . . ?
B4 B1 B2 B6 -100.51(19) . . . . ?
B5 B1 B2 B6 -37.11(17) . . . . ?
B3 B1 B2 B6 -138.03(19) . . . . ?
Cl1 B1 B2 B10 148.77(17) . . . . ?
B4 B1 B2 B10 -63.6(2) . . . . ?
B5 B1 B2 B10 -0.2(2) . . . . ?
B3 B1 B2 B10 -101.1(2) . . . . ?
B6 B1 B2 B10 36.92(17) . . . . ?
Cl1 B1 B2 B7 -147.55(17) . . . . ?
B4 B1 B2 B7 0.1(2) . . . . ?
B5 B1 B2 B7 63.5(2) . . . . ?
B3 B1 B2 B7 -37.42(17) . . . . ?
B6 B1 B2 B7 100.6(2) . . . . ?
Cl2 B2 B3 B8 148.64(17) . . . . ?
B6 B2 B3 B8 -64.1(2) . . . . ?
B1 B2 B3 B8 -101.6(2) . . . . ?
B10 B2 B3 B8 -0.6(2) . . . . ?
B7 B2 B3 B8 36.88(17) . . . . ?
Cl2 B2 B3 B4 -147.63(17) . . . . ?
B6 B2 B3 B4 -0.4(2) . . . . ?
B1 B2 B3 B4 -37.84(17) . . . . ?
B10 B2 B3 B4 63.1(2) . . . . ?
B7 B2 B3 B4 100.6(2) . . . . ?
Cl2 B2 B3 Cl3 1.8(3) . . . . ?
B6 B2 B3 Cl3 149.08(18) . . . . ?
B1 B2 B3 Cl3 111.6(2) . . . . ?
B10 B2 B3 Cl3 -147.42(18) . . . . ?
B7 B2 B3 Cl3 -109.9(2) . . . . ?
Cl2 B2 B3 B1 -109.8(2) . . . . ?
B6 B2 B3 B1 37.46(17) . . . . ?
B10 B2 B3 B1 100.97(19) . . . . ?
B7 B2 B3 B1 138.45(19) . . . . ?
Cl2 B2 B3 B7 111.8(2) . . . . ?
B6 B2 B3 B7 -101.0(2) . . . . ?
B1 B2 B3 B7 -138.45(19) . . . . ?
B10 B2 B3 B7 -37.48(18) . . . . ?
Ag1 Cl3 B3 B8 -26.8(2) . . . . ?
Ag1 Cl3 B3 B4 -99.04(19) . . . . ?
Ag1 Cl3 B3 B2 115.59(18) . . . . ?
Ag1 Cl3 B3 B1 -171.53(17) . . . . ?
Ag1 Cl3 B3 B7 43.5(2) . . . . ?
Cl1 B1 B3 B8 -148.82(18) . . . . ?
B4 B1 B3 B8 -37.89(17) . . . . ?
B5 B1 B3 B8 -0.6(2) . . . . ?
B6 B1 B3 B8 62.4(2) . . . . ?
B2 B1 B3 B8 99.8(2) . . . . ?
Cl1 B1 B3 B4 -110.9(2) . . . . ?
B5 B1 B3 B4 37.30(17) . . . . ?
B6 B1 B3 B4 100.33(19) . . . . ?
B2 B1 B3 B4 137.72(19) . . . . ?
Cl1 B1 B3 B2 111.3(2) . . . . ?
B4 B1 B3 B2 -137.72(19) . . . . ?
B5 B1 B3 B2 -100.42(19) . . . . ?
B6 B1 B3 B2 -37.40(17) . . . . ?
Cl1 B1 B3 Cl3 -0.2(3) . . . . ?
B4 B1 B3 Cl3 110.8(2) . . . . ?
B5 B1 B3 Cl3 148.05(18) . . . . ?
B6 B1 B3 Cl3 -148.92(18) . . . . ?
B2 B1 B3 Cl3 -111.5(2) . . . . ?
Cl1 B1 B3 B7 148.61(18) . . . . ?
B4 B1 B3 B7 -100.5(2) . . . . ?
B5 B1 B3 B7 -63.2(2) . . . . ?
B6 B1 B3 B7 -0.1(2) . . . . ?
B2 B1 B3 B7 37.27(18) . . . . ?
B8 B3 B4 C1 38.15(17) . . . . ?
B2 B3 B4 C1 -61.9(2) . . . . ?
Cl3 B3 B4 C1 148.47(18) . . . . ?
B1 B3 B4 C1 -99.74(19) . . . . ?
B7 B3 B4 C1 1.6(2) . . . . ?
B8 B3 B4 Cl4 -107.8(2) . . . . ?
B2 B3 B4 Cl4 152.23(18) . . . . ?
Cl3 B3 B4 Cl4 2.6(3) . . . . ?
B1 B3 B4 Cl4 114.3(2) . . . . ?
B7 B3 B4 Cl4 -144.30(18) . . . . ?
B8 B3 B4 B1 137.89(18) . . . . ?
B2 B3 B4 B1 37.88(17) . . . . ?
Cl3 B3 B4 B1 -111.8(2) . . . . ?
B7 B3 B4 B1 101.4(2) . . . . ?
B8 B3 B4 B5 100.66(19) . . . . ?
B2 B3 B4 B5 0.7(2) . . . . ?
Cl3 B3 B4 B5 -149.02(18) . . . . ?
B1 B3 B4 B5 -37.23(17) . . . . ?
B7 B3 B4 B5 64.1(2) . . . . ?
B2 B3 B4 B8 -100.0(2) . . . . ?
Cl3 B3 B4 B8 110.3(2) . . . . ?
B1 B3 B4 B8 -137.89(18) . . . . ?
B7 B3 B4 B8 -36.54(17) . . . . ?
Cl1 B1 B4 C1 -150.07(17) . . . . ?
B5 B1 B4 C1 -38.60(16) . . . . ?
B3 B1 B4 C1 99.75(19) . . . . ?
B6 B1 B4 C1 -0.9(2) . . . . ?
B2 B1 B4 C1 62.2(2) . . . . ?
Cl1 B1 B4 Cl4 -0.7(3) . . . . ?
B5 B1 B4 Cl4 110.8(2) . . . . ?
B3 B1 B4 Cl4 -110.9(2) . . . . ?
B6 B1 B4 Cl4 148.44(19) . . . . ?
B2 B1 B4 Cl4 -148.45(19) . . . . ?
Cl1 B1 B4 B3 110.2(2) . . . . ?
B5 B1 B4 B3 -138.34(18) . . . . ?
B6 B1 B4 B3 -100.67(19) . . . . ?
B2 B1 B4 B3 -37.57(17) . . . . ?
Cl1 B1 B4 B5 -111.5(2) . . . . ?
B3 B1 B4 B5 138.34(18) . . . . ?
B6 B1 B4 B5 37.67(17) . . . . ?
B2 B1 B4 B5 100.78(19) . . . . ?
Cl1 B1 B4 B8 147.60(17) . . . . ?
B5 B1 B4 B8 -100.92(19) . . . . ?
B3 B1 B4 B8 37.42(17) . . . . ?
B6 B1 B4 B8 -63.3(2) . . . . ?
B2 B1 B4 B8 -0.1(2) . . . . ?
Cl1 B1 B5 C1 149.06(17) . . . . ?
B4 B1 B5 C1 38.29(16) . . . . ?
B3 B1 B5 C1 1.2(2) . . . . ?
B6 B1 B5 C1 -99.24(19) . . . . ?
B2 B1 B5 C1 -62.0(2) . . . . ?
Cl1 B1 B5 Cl5 -1.4(3) . . . . ?
B4 B1 B5 Cl5 -112.1(2) . . . . ?
B3 B1 B5 Cl5 -149.27(18) . . . . ?
B6 B1 B5 Cl5 110.3(2) . . . . ?
B2 B1 B5 Cl5 147.52(18) . . . . ?
Cl1 B1 B5 B6 -111.7(2) . . . . ?
B4 B1 B5 B6 137.53(19) . . . . ?
B3 B1 B5 B6 100.4(2) . . . . ?
B2 B1 B5 B6 37.20(17) . . . . ?
Cl1 B1 B5 B4 110.8(2) . . . . ?
B3 B1 B5 B4 -37.12(17) . . . . ?
B6 B1 B5 B4 -137.53(19) . . . . ?
B2 B1 B5 B4 -100.33(19) . . . . ?
Cl1 B1 B5 B9 -149.04(17) . . . . ?
B4 B1 B5 B9 100.2(2) . . . . ?
B3 B1 B5 B9 63.1(2) . . . . ?
B6 B1 B5 B9 -37.34(17) . . . . ?
B2 B1 B5 B9 -0.1(2) . . . . ?
Cl4 B4 B5 C1 109.8(2) . . . . ?
B3 B4 B5 C1 -98.62(19) . . . . ?
B1 B4 B5 C1 -135.95(18) . . . . ?
B8 B4 B5 C1 -35.50(17) . . . . ?
C1 B4 B5 Cl5 -114.5(2) . . . . ?
Cl4 B4 B5 Cl5 -4.7(3) . . . . ?
B3 B4 B5 Cl5 146.89(18) . . . . ?
B1 B4 B5 Cl5 109.6(2) . . . . ?
B8 B4 B5 Cl5 -149.99(18) . . . . ?
C1 B4 B5 B6 97.94(19) . . . . ?
Cl4 B4 B5 B6 -152.25(18) . . . . ?
B3 B4 B5 B6 -0.7(2) . . . . ?
B1 B4 B5 B6 -38.01(17) . . . . ?
B8 B4 B5 B6 62.4(2) . . . . ?
C1 B4 B5 B1 135.95(18) . . . . ?
Cl4 B4 B5 B1 -114.2(2) . . . . ?
B3 B4 B5 B1 37.33(17) . . . . ?
B8 B4 B5 B1 100.4(2) . . . . ?
C1 B4 B5 B9 34.63(17) . . . . ?
Cl4 B4 B5 B9 144.44(19) . . . . ?
B3 B4 B5 B9 -64.0(2) . . . . ?
B1 B4 B5 B9 -101.3(2) . . . . ?
B8 B4 B5 B9 -0.9(2) . . . . ?
C1 B5 B6 B9 -38.59(16) . . . . ?
Cl5 B5 B6 B9 111.4(2) . . . . ?
B1 B5 B6 B9 -138.30(18) . . . . ?
B4 B5 B6 B9 -100.42(19) . . . . ?
C1 B5 B6 B2 62.3(2) . . . . ?
Cl5 B5 B6 B2 -147.74(17) . . . . ?
B1 B5 B6 B2 -37.43(17) . . . . ?
B4 B5 B6 B2 0.4(2) . . . . ?
B9 B5 B6 B2 100.87(19) . . . . ?
C1 B5 B6 B1 99.71(18) . . . . ?
Cl5 B5 B6 B1 -110.3(2) . . . . ?
B4 B5 B6 B1 37.88(17) . . . . ?
B9 B5 B6 B1 138.30(18) . . . . ?
C1 B5 B6 B10 -1.5(2) . . . . ?
Cl5 B5 B6 B10 148.53(17) . . . . ?
B1 B5 B6 B10 -101.17(19) . . . . ?
B4 B5 B6 B10 -63.3(2) . . . . ?
B9 B5 B6 B10 37.13(17) . . . . ?
C1 B5 B6 Cl6 -147.95(17) . . . . ?
Cl5 B5 B6 Cl6 2.0(3) . . . . ?
B1 B5 B6 Cl6 112.3(2) . . . . ?
B4 B5 B6 Cl6 150.22(17) . . . . ?
B9 B5 B6 Cl6 -109.4(2) . . . . ?
B3 B2 B6 B5 0.0(2) . . . . ?
Cl2 B2 B6 B5 147.13(17) . . . . ?
B1 B2 B6 B5 37.40(17) . . . . ?
B10 B2 B6 B5 -101.43(19) . . . . ?
B7 B2 B6 B5 -63.9(2) . . . . ?
B3 B2 B6 B9 64.0(2) . . . . ?
Cl2 B2 B6 B9 -148.83(17) . . . . ?
B1 B2 B6 B9 101.44(19) . . . . ?
B10 B2 B6 B9 -37.39(17) . . . . ?
B7 B2 B6 B9 0.2(2) . . . . ?
B3 B2 B6 B1 -37.44(17) . . . . ?
Cl2 B2 B6 B1 109.7(2) . . . . ?
B10 B2 B6 B1 -138.83(19) . . . . ?
B7 B2 B6 B1 -101.3(2) . . . . ?
B3 B2 B6 B10 101.4(2) . . . . ?
Cl2 B2 B6 B10 -111.4(2) . . . . ?
B1 B2 B6 B10 138.83(19) . . . . ?
B7 B2 B6 B10 37.56(17) . . . . ?
B3 B2 B6 Cl6 -148.69(17) . . . . ?
Cl2 B2 B6 Cl6 -1.5(3) . . . . ?
B1 B2 B6 Cl6 -111.3(2) . . . . ?
B10 B2 B6 Cl6 109.9(2) . . . . ?
B7 B2 B6 Cl6 147.48(18) . . . . ?
Cl1 B1 B6 B5 110.9(2) . . . . ?
B4 B1 B6 B5 -37.87(17) . . . . ?
B3 B1 B6 B5 -100.87(19) . . . . ?
B2 B1 B6 B5 -138.25(18) . . . . ?
Cl1 B1 B6 B9 148.56(17) . . . . ?
B4 B1 B6 B9 -0.2(2) . . . . ?
B5 B1 B6 B9 37.64(17) . . . . ?
B3 B1 B6 B9 -63.2(2) . . . . ?
B2 B1 B6 B9 -100.61(19) . . . . ?
Cl1 B1 B6 B2 -110.8(2) . . . . ?
B4 B1 B6 B2 100.38(19) . . . . ?
B5 B1 B6 B2 138.25(18) . . . . ?
B3 B1 B6 B2 37.38(17) . . . . ?
Cl1 B1 B6 B10 -147.85(18) . . . . ?
B4 B1 B6 B10 63.4(2) . . . . ?
B5 B1 B6 B10 101.2(2) . . . . ?
B3 B1 B6 B10 0.4(2) . . . . ?
B2 B1 B6 B10 -37.02(18) . . . . ?
Cl1 B1 B6 Cl6 1.9(3) . . . . ?
B4 B1 B6 Cl6 -146.85(17) . . . . ?
B5 B1 B6 Cl6 -109.0(2) . . . . ?
B3 B1 B6 Cl6 150.15(17) . . . . ?
B2 B1 B6 Cl6 112.8(2) . . . . ?
Ag1 Cl6 B6 B5 -65.8(2) 3_545 . . . ?
Ag1 Cl6 B6 B9 -137.01(15) 3_545 . . . ?
Ag1 Cl6 B6 B2 79.3(2) 3_545 . . . ?
Ag1 Cl6 B6 B1 6.0(2) 3_545 . . . ?
Ag1 Cl6 B6 B10 152.04(16) 3_545 . . . ?
B3 B2 B7 B8 -37.22(18) . . . . ?
Cl2 B2 B7 B8 -147.74(18) . . . . ?
B6 B2 B7 B8 63.5(2) . . . . ?
B1 B2 B7 B8 0.0(2) . . . . ?
B10 B2 B7 B8 101.0(2) . . . . ?
B3 B2 B7 B11 -100.6(2) . . . . ?
Cl2 B2 B7 B11 148.86(18) . . . . ?
B6 B2 B7 B11 0.1(2) . . . . ?
B1 B2 B7 B11 -63.4(2) . . . . ?
B10 B2 B7 B11 37.62(17) . . . . ?
B3 B2 B7 Cl7 109.5(2) . . . . ?
Cl2 B2 B7 Cl7 -1.0(3) . . . . ?
B6 B2 B7 Cl7 -149.82(18) . . . . ?
B1 B2 B7 Cl7 146.70(19) . . . . ?
B10 B2 B7 Cl7 -112.3(2) . . . . ?
B3 B2 B7 B10 -138.23(19) . . . . ?
Cl2 B2 B7 B10 111.2(2) . . . . ?
B6 B2 B7 B10 -37.53(17) . . . . ?
B1 B2 B7 B10 -101.0(2) . . . . ?
Cl2 B2 B7 B3 -110.5(2) . . . . ?
B6 B2 B7 B3 100.7(2) . . . . ?
B1 B2 B7 B3 37.22(18) . . . . ?
B10 B2 B7 B3 138.23(19) . . . . ?
B4 B3 B7 B8 37.12(18) . . . . ?
B2 B3 B7 B8 138.08(19) . . . . ?
Cl3 B3 B7 B8 -110.0(2) . . . . ?
B1 B3 B7 B8 100.7(2) . . . . ?
B8 B3 B7 B11 -37.59(17) . . . . ?
B4 B3 B7 B11 -0.5(2) . . . . ?
B2 B3 B7 B11 100.5(2) . . . . ?
Cl3 B3 B7 B11 -147.58(18) . . . . ?
B1 B3 B7 B11 63.1(2) . . . . ?
B8 B3 B7 Cl7 109.0(2) . . . . ?
B4 B3 B7 Cl7 146.15(18) . . . . ?
B2 B3 B7 Cl7 -112.9(2) . . . . ?
Cl3 B3 B7 Cl7 -1.0(3) . . . . ?
B1 B3 B7 Cl7 -150.23(18) . . . . ?
B8 B3 B7 B2 -138.08(19) . . . . ?
B4 B3 B7 B2 -101.0(2) . . . . ?
Cl3 B3 B7 B2 111.9(2) . . . . ?
B1 B3 B7 B2 -37.34(17) . . . . ?
B8 B3 B7 B10 -100.9(2) . . . . ?
B4 B3 B7 B10 -63.8(2) . . . . ?
B2 B3 B7 B10 37.19(18) . . . . ?
Cl3 B3 B7 B10 149.13(19) . . . . ?
B1 B3 B7 B10 -0.1(2) . . . . ?
B11 B7 B8 C1 38.35(16) . . . . ?
Cl7 B7 B8 C1 149.57(17) . . . . ?
B2 B7 B8 C1 -62.5(2) . . . . ?
B10 B7 B8 C1 0.7(2) . . . . ?
B3 B7 B8 C1 -99.59(19) . . . . ?
Cl7 B7 B8 B11 111.2(2) . . . . ?
B2 B7 B8 B11 -100.8(2) . . . . ?
B10 B7 B8 B11 -37.63(17) . . . . ?
B3 B7 B8 B11 -137.94(19) . . . . ?
B11 B7 B8 Cl8 -108.8(2) . . . . ?
Cl7 B7 B8 Cl8 2.4(3) . . . . ?
B2 B7 B8 Cl8 150.38(17) . . . . ?
B10 B7 B8 Cl8 -146.43(18) . . . . ?
B3 B7 B8 Cl8 113.3(2) . . . . ?
B11 B7 B8 B3 137.94(19) . . . . ?
Cl7 B7 B8 B3 -110.8(2) . . . . ?
B2 B7 B8 B3 37.12(17) . . . . ?
B10 B7 B8 B3 100.3(2) . . . . ?
B11 B7 B8 B4 100.7(2) . . . . ?
Cl7 B7 B8 B4 -148.06(18) . . . . ?
B2 B7 B8 B4 -0.1(2) . . . . ?
B10 B7 B8 B4 63.1(2) . . . . ?
B3 B7 B8 B4 -37.22(18) . . . . ?
B4 B3 B8 C1 -38.00(17) . . . . ?
B2 B3 B8 C1 63.3(2) . . . . ?
Cl3 B3 B8 C1 -149.36(18) . . . . ?
B1 B3 B8 C1 -0.2(2) . . . . ?
B7 B3 B8 C1 100.65(19) . . . . ?
B4 B3 B8 B7 -138.65(19) . . . . ?
B2 B3 B8 B7 -37.32(18) . . . . ?
Cl3 B3 B8 B7 110.0(2) . . . . ?
B1 B3 B8 B7 -100.9(2) . . . . ?
B4 B3 B8 B11 -100.7(2) . . . . ?
B2 B3 B8 B11 0.7(2) . . . . ?
Cl3 B3 B8 B11 147.96(18) . . . . ?
B1 B3 B8 B11 -62.9(2) . . . . ?
B7 B3 B8 B11 37.97(18) . . . . ?
B4 B3 B8 Cl8 110.1(2) . . . . ?
B2 B3 B8 Cl8 -148.58(18) . . . . ?
Cl3 B3 B8 Cl8 -1.3(3) . . . . ?
B1 B3 B8 Cl8 147.85(18) . . . . ?
B7 B3 B8 Cl8 -111.3(2) . . . . ?
B2 B3 B8 B4 101.3(2) . . . . ?
Cl3 B3 B8 B4 -111.4(2) . . . . ?
B1 B3 B8 B4 37.76(18) . . . . ?
B7 B3 B8 B4 138.65(19) . . . . ?
Cl4 B4 B8 C1 -111.0(2) . . . . ?
B3 B4 B8 C1 136.43(19) . . . . ?
B1 B4 B8 C1 98.82(19) . . . . ?
B5 B4 B8 C1 35.55(17) . . . . ?
C1 B4 B8 B7 -98.7(2) . . . . ?
Cl4 B4 B8 B7 150.37(18) . . . . ?
B3 B4 B8 B7 37.77(18) . . . . ?
B1 B4 B8 B7 0.2(2) . . . . ?
B5 B4 B8 B7 -63.1(2) . . . . ?
C1 B4 B8 B11 -34.65(18) . . . . ?
Cl4 B4 B8 B11 -145.61(19) . . . . ?
B3 B4 B8 B11 101.8(2) . . . . ?
B1 B4 B8 B11 64.2(2) . . . . ?
B5 B4 B8 B11 0.9(3) . . . . ?
C1 B4 B8 Cl8 110.7(2) . . . . ?
Cl4 B4 B8 Cl8 -0.3(3) . . . . ?
B3 B4 B8 Cl8 -112.9(2) . . . . ?
B1 B4 B8 Cl8 -150.48(18) . . . . ?
B5 B4 B8 Cl8 146.26(19) . . . . ?
C1 B4 B8 B3 -136.43(19) . . . . ?
Cl4 B4 B8 B3 112.6(2) . . . . ?
B1 B4 B8 B3 -37.62(17) . . . . ?
B5 B4 B8 B3 -100.9(2) . . . . ?
B5 B6 B9 C1 38.73(17) . . . . ?
B2 B6 B9 C1 -62.4(2) . . . . ?
B1 B6 B9 C1 1.3(2) . . . . ?
B10 B6 B9 C1 -99.88(19) . . . . ?
Cl6 B6 B9 C1 148.93(16) . . . . ?
B5 B6 B9 Cl9 -109.9(2) . . . . ?
B2 B6 B9 Cl9 148.95(18) . . . . ?
B1 B6 B9 Cl9 -147.36(18) . . . . ?
B10 B6 B9 Cl9 111.5(2) . . . . ?
Cl6 B6 B9 Cl9 0.3(3) . . . . ?
B5 B6 B9 B10 138.61(19) . . . . ?
B2 B6 B9 B10 37.48(17) . . . . ?
B1 B6 B9 B10 101.17(19) . . . . ?
Cl6 B6 B9 B10 -111.2(2) . . . . ?
B5 B6 B9 B11 100.77(19) . . . . ?
B2 B6 B9 B11 -0.4(2) . . . . ?
B1 B6 B9 B11 63.3(2) . . . . ?
B10 B6 B9 B11 -37.84(17) . . . . ?
Cl6 B6 B9 B11 -149.04(17) . . . . ?
B2 B6 B9 B5 -101.13(19) . . . . ?
B1 B6 B9 B5 -37.44(17) . . . . ?
B10 B6 B9 B5 -138.61(19) . . . . ?
Cl6 B6 B9 B5 110.2(2) . . . . ?
Cl5 B5 B9 C1 114.7(2) . . . . ?
B6 B5 B9 C1 -135.48(19) . . . . ?
B1 B5 B9 C1 -98.02(19) . . . . ?
B4 B5 B9 C1 -34.65(17) . . . . ?
C1 B5 B9 Cl9 -110.6(2) . . . . ?
Cl5 B5 B9 Cl9 4.1(3) . . . . ?
B6 B5 B9 Cl9 114.0(2) . . . . ?
B1 B5 B9 Cl9 151.43(18) . . . . ?
B4 B5 B9 Cl9 -145.21(18) . . . . ?
C1 B5 B9 B10 98.43(19) . . . . ?
Cl5 B5 B9 B10 -146.87(18) . . . . ?
B6 B5 B9 B10 -37.05(17) . . . . ?
B1 B5 B9 B10 0.4(2) . . . . ?
B4 B5 B9 B10 63.8(2) . . . . ?
C1 B5 B9 B6 135.48(19) . . . . ?
Cl5 B5 B9 B6 -109.8(2) . . . . ?
B1 B5 B9 B6 37.46(17) . . . . ?
B4 B5 B9 B6 100.8(2) . . . . ?
C1 B5 B9 B11 35.17(17) . . . . ?
Cl5 B5 B9 B11 149.86(18) . . . . ?
B6 B5 B9 B11 -100.3(2) . . . . ?
B1 B5 B9 B11 -62.9(2) . . . . ?
B4 B5 B9 B11 0.5(2) . . . . ?
C1 B9 B10 Cl10 -149.53(17) . . . . ?
Cl9 B9 B10 Cl10 -2.5(3) . . . . ?
B6 B9 B10 Cl10 111.4(2) . . . . ?
B11 B9 B10 Cl10 -111.1(2) . . . . ?
B5 B9 B10 Cl10 148.22(18) . . . . ?
C1 B9 B10 B11 -38.46(16) . . . . ?
Cl9 B9 B10 B11 108.6(2) . . . . ?
B6 B9 B10 B11 -137.48(18) . . . . ?
B5 B9 B10 B11 -100.71(19) . . . . ?
C1 B9 B10 B6 99.02(18) . . . . ?
Cl9 B9 B10 B6 -113.9(2) . . . . ?
B11 B9 B10 B6 137.48(18) . . . . ?
B5 B9 B10 B6 36.77(17) . . . . ?
C1 B9 B10 B2 61.7(2) . . . . ?
Cl9 B9 B10 B2 -151.19(18) . . . . ?
B6 B9 B10 B2 -37.30(17) . . . . ?
B11 B9 B10 B2 100.18(19) . . . . ?
B5 B9 B10 B2 -0.5(2) . . . . ?
C1 B9 B10 B7 -1.6(2) . . . . ?
Cl9 B9 B10 B7 145.44(18) . . . . ?
B6 B9 B10 B7 -100.7(2) . . . . ?
B11 B9 B10 B7 36.82(17) . . . . ?
B5 B9 B10 B7 -63.9(2) . . . . ?
B5 B6 B10 Cl10 -148.75(19) . . . . ?
B9 B6 B10 Cl10 -111.4(2) . . . . ?
B2 B6 B10 Cl10 110.5(2) . . . . ?
B1 B6 B10 Cl10 147.51(19) . . . . ?
Cl6 B6 B10 Cl10 -2.7(3) . . . . ?
B5 B6 B10 B11 0.6(2) . . . . ?
B9 B6 B10 B11 37.96(17) . . . . ?
B2 B6 B10 B11 -100.2(2) . . . . ?
B1 B6 B10 B11 -63.2(2) . . . . ?
Cl6 B6 B10 B11 146.65(18) . . . . ?
B5 B6 B10 B9 -37.39(17) . . . . ?
B2 B6 B10 B9 -138.15(19) . . . . ?
B1 B6 B10 B9 -101.12(19) . . . . ?
Cl6 B6 B10 B9 108.7(2) . . . . ?
B5 B6 B10 B2 100.76(19) . . . . ?
B9 B6 B10 B2 138.15(19) . . . . ?
B1 B6 B10 B2 37.03(17) . . . . ?
Cl6 B6 B10 B2 -113.2(2) . . . . ?
B5 B6 B10 B7 63.3(2) . . . . ?
B9 B6 B10 B7 100.7(2) . . . . ?
B2 B6 B10 B7 -37.47(18) . . . . ?
B1 B6 B10 B7 -0.4(2) . . . . ?
Cl6 B6 B10 B7 -150.63(18) . . . . ?
B3 B2 B10 Cl10 147.94(18) . . . . ?
Cl2 B2 B10 Cl10 -1.1(3) . . . . ?
B6 B2 B10 Cl10 -111.7(2) . . . . ?
B1 B2 B10 Cl10 -148.56(17) . . . . ?
B7 B2 B10 Cl10 110.3(2) . . . . ?
B3 B2 B10 B11 0.3(2) . . . . ?
Cl2 B2 B10 B11 -148.66(18) . . . . ?
B6 B2 B10 B11 100.7(2) . . . . ?
B1 B2 B10 B11 63.8(2) . . . . ?
B7 B2 B10 B11 -37.29(17) . . . . ?
B3 B2 B10 B9 -63.1(2) . . . . ?
Cl2 B2 B10 B9 147.94(18) . . . . ?
B6 B2 B10 B9 37.34(17) . . . . ?
B1 B2 B10 B9 0.4(2) . . . . ?
B7 B2 B10 B9 -100.7(2) . . . . ?
B3 B2 B10 B6 -100.40(19) . . . . ?
Cl2 B2 B10 B6 110.6(2) . . . . ?
B1 B2 B10 B6 -36.90(17) . . . . ?
B7 B2 B10 B6 -138.02(19) . . . . ?
B3 B2 B10 B7 37.62(18) . . . . ?
Cl2 B2 B10 B7 -111.4(2) . . . . ?
B6 B2 B10 B7 138.02(19) . . . . ?
B1 B2 B10 B7 101.1(2) . . . . ?
B8 B7 B10 Cl10 148.89(19) . . . . ?
B11 B7 B10 Cl10 111.2(2) . . . . ?
Cl7 B7 B10 Cl10 1.3(3) . . . . ?
B2 B7 B10 Cl10 -111.0(2) . . . . ?
B3 B7 B10 Cl10 -148.03(19) . . . . ?
B8 B7 B10 B11 37.70(17) . . . . ?
Cl7 B7 B10 B11 -109.9(2) . . . . ?
B2 B7 B10 B11 137.81(19) . . . . ?
B3 B7 B10 B11 100.8(2) . . . . ?
B8 B7 B10 B9 0.6(2) . . . . ?
B11 B7 B10 B9 -37.12(17) . . . . ?
Cl7 B7 B10 B9 -147.04(18) . . . . ?
B2 B7 B10 B9 100.69(19) . . . . ?
B3 B7 B10 B9 63.7(2) . . . . ?
B8 B7 B10 B6 -62.7(2) . . . . ?
B11 B7 B10 B6 -100.4(2) . . . . ?
Cl7 B7 B10 B6 149.67(18) . . . . ?
B2 B7 B10 B6 37.40(17) . . . . ?
B3 B7 B10 B6 0.4(2) . . . . ?
B8 B7 B10 B2 -100.1(2) . . . . ?
B11 B7 B10 B2 -137.81(19) . . . . ?
Cl7 B7 B10 B2 112.3(2) . . . . ?
B3 B7 B10 B2 -37.04(18) . . . . ?
B7 B8 B11 C1 136.43(19) . . . . ?
Cl8 B8 B11 C1 -111.5(2) . . . . ?
B3 B8 B11 C1 98.1(2) . . . . ?
B4 B8 B11 C1 34.47(18) . . . . ?
C1 B8 B11 Cl11 109.2(2) . . . . ?
B7 B8 B11 Cl11 -114.4(2) . . . . ?
Cl8 B8 B11 Cl11 -2.3(3) . . . . ?
B3 B8 B11 Cl11 -152.73(18) . . . . ?
B4 B8 B11 Cl11 143.67(19) . . . . ?
C1 B8 B11 B7 -136.43(19) . . . . ?
Cl8 B8 B11 B7 112.0(2) . . . . ?
B3 B8 B11 B7 -38.37(18) . . . . ?
B4 B8 B11 B7 -102.0(2) . . . . ?
C1 B8 B11 B10 -98.52(19) . . . . ?
B7 B8 B11 B10 37.91(18) . . . . ?
Cl8 B8 B11 B10 149.96(18) . . . . ?
B3 B8 B11 B10 -0.5(2) . . . . ?
B4 B8 B11 B10 -64.1(2) . . . . ?
C1 B8 B11 B9 -35.06(17) . . . . ?
B7 B8 B11 B9 101.4(2) . . . . ?
Cl8 B8 B11 B9 -146.58(19) . . . . ?
B3 B8 B11 B9 63.0(2) . . . . ?
B4 B8 B11 B9 -0.6(3) . . . . ?
B8 B7 B11 C1 -38.29(17) . . . . ?
Cl7 B7 B11 C1 -147.41(18) . . . . ?
B2 B7 B11 C1 62.0(2) . . . . ?
B10 B7 B11 C1 99.6(2) . . . . ?
B3 B7 B11 C1 -0.9(2) . . . . ?
B8 B7 B11 Cl11 107.4(2) . . . . ?
Cl7 B7 B11 Cl11 -1.7(3) . . . . ?
B2 B7 B11 Cl11 -152.30(18) . . . . ?
B10 B7 B11 Cl11 -114.7(2) . . . . ?
B3 B7 B11 Cl11 144.85(19) . . . . ?
Cl7 B7 B11 B8 -109.1(2) . . . . ?
B2 B7 B11 B8 100.3(2) . . . . ?
B10 B7 B11 B8 137.86(19) . . . . ?
B3 B7 B11 B8 37.43(17) . . . . ?
B8 B7 B11 B10 -137.86(19) . . . . ?
Cl7 B7 B11 B10 113.0(2) . . . . ?
B2 B7 B11 B10 -37.58(17) . . . . ?
B3 B7 B11 B10 -100.4(2) . . . . ?
B8 B7 B11 B9 -100.6(2) . . . . ?
Cl7 B7 B11 B9 150.29(18) . . . . ?
B2 B7 B11 B9 -0.3(2) . . . . ?
B10 B7 B11 B9 37.27(17) . . . . ?
B3 B7 B11 B9 -63.2(2) . . . . ?
Cl10 B10 B11 C1 150.01(18) . . . . ?
B9 B10 B11 C1 38.43(16) . . . . ?
B6 B10 B11 C1 0.6(2) . . . . ?
B2 B10 B11 C1 -62.5(2) . . . . ?
B7 B10 B11 C1 -100.06(19) . . . . ?
Cl10 B10 B11 Cl11 3.0(3) . . . . ?
B9 B10 B11 Cl11 -108.6(2) . . . . ?
B6 B10 B11 Cl11 -146.46(19) . . . . ?
B2 B10 B11 Cl11 150.47(19) . . . . ?
B7 B10 B11 Cl11 112.9(2) . . . . ?
Cl10 B10 B11 B8 -147.39(19) . . . . ?
B9 B10 B11 B8 101.0(2) . . . . ?
B6 B10 B11 B8 63.1(2) . . . . ?
B2 B10 B11 B8 0.1(2) . . . . ?
B7 B10 B11 B8 -37.47(18) . . . . ?
Cl10 B10 B11 B7 -109.9(2) . . . . ?
B9 B10 B11 B7 138.50(19) . . . . ?
B6 B10 B11 B7 100.6(2) . . . . ?
B2 B10 B11 B7 37.54(17) . . . . ?
Cl10 B10 B11 B9 111.6(2) . . . . ?
B6 B10 B11 B9 -37.88(17) . . . . ?
B2 B10 B11 B9 -100.95(19) . . . . ?
B7 B10 B11 B9 -138.50(19) . . . . ?
Cl9 B9 B11 C1 111.2(2) . . . . ?
B10 B9 B11 C1 -135.93(18) . . . . ?
B6 B9 B11 C1 -97.98(18) . . . . ?
B5 B9 B11 C1 -35.19(17) . . . . ?
C1 B9 B11 Cl11 -108.6(2) . . . . ?
Cl9 B9 B11 Cl11 2.6(3) . . . . ?
B10 B9 B11 Cl11 115.5(2) . . . . ?
B6 B9 B11 Cl11 153.46(17) . . . . ?
B5 B9 B11 Cl11 -143.75(18) . . . . ?
C1 B9 B11 B8 35.24(17) . . . . ?
Cl9 B9 B11 B8 146.44(18) . . . . ?
B10 B9 B11 B8 -100.7(2) . . . . ?
B6 B9 B11 B8 -62.7(2) . . . . ?
B5 B9 B11 B8 0.0(3) . . . . ?
C1 B9 B11 B7 98.40(19) . . . . ?
Cl9 B9 B11 B7 -150.40(17) . . . . ?
B10 B9 B11 B7 -37.53(17) . . . . ?
B6 B9 B11 B7 0.4(2) . . . . ?
B5 B9 B11 B7 63.2(2) . . . . ?
C1 B9 B11 B10 135.93(18) . . . . ?
Cl9 B9 B11 B10 -112.9(2) . . . . ?
B6 B9 B11 B10 37.95(17) . . . . ?
B5 B9 B11 B10 100.7(2) . . . . ?
Cl4 B4 C1 C2 2.9(3) . . . . ?
B3 B4 C1 C2 -143.5(2) . . . . ?
B1 B4 C1 C2 153.5(2) . . . . ?
B5 B4 C1 C2 114.7(2) . . . . ?
B8 B4 C1 C2 -105.2(2) . . . . ?
Cl4 B4 C1 B9 -148.82(18) . . . . ?
B3 B4 C1 B9 64.8(2) . . . . ?
B1 B4 C1 B9 1.8(2) . . . . ?
B5 B4 C1 B9 -36.98(18) . . . . ?
B8 B4 C1 B9 103.1(2) . . . . ?
Cl4 B4 C1 B11 144.19(18) . . . . ?
B3 B4 C1 B11 -2.2(2) . . . . ?
B1 B4 C1 B11 -65.2(2) . . . . ?
B5 B4 C1 B11 -104.0(2) . . . . ?
B8 B4 C1 B11 36.08(18) . . . . ?
Cl4 B4 C1 B8 108.1(2) . . . . ?
B3 B4 C1 B8 -38.31(17) . . . . ?
B1 B4 C1 B8 -101.24(19) . . . . ?
B5 B4 C1 B8 -140.04(19) . . . . ?
Cl4 B4 C1 B5 -111.8(2) . . . . ?
B3 B4 C1 B5 101.7(2) . . . . ?
B1 B4 C1 B5 38.81(17) . . . . ?
B8 B4 C1 B5 140.04(19) . . . . ?
Cl9 B9 C1 C2 -2.5(3) . . . . ?
B10 B9 C1 C2 145.1(2) . . . . ?
B6 B9 C1 C2 -152.2(2) . . . . ?
B11 B9 C1 C2 106.3(2) . . . . ?
B5 B9 C1 C2 -113.3(2) . . . . ?
Cl9 B9 C1 B4 147.74(17) . . . . ?
B10 B9 C1 B4 -64.7(2) . . . . ?
B6 B9 C1 B4 -2.0(2) . . . . ?
B11 B9 C1 B4 -103.5(2) . . . . ?
B5 B9 C1 B4 36.88(18) . . . . ?
Cl9 B9 C1 B11 -108.8(2) . . . . ?
B10 B9 C1 B11 38.77(17) . . . . ?
B6 B9 C1 B11 101.52(19) . . . . ?
B5 B9 C1 B11 140.36(19) . . . . ?
Cl9 B9 C1 B8 -145.38(17) . . . . ?
B10 B9 C1 B8 2.2(2) . . . . ?
B6 B9 C1 B8 64.9(2) . . . . ?
B11 B9 C1 B8 -36.60(17) . . . . ?
B5 B9 C1 B8 103.76(19) . . . . ?
Cl9 B9 C1 B5 110.9(2) . . . . ?
B10 B9 C1 B5 -101.6(2) . . . . ?
B6 B9 C1 B5 -38.84(17) . . . . ?
B11 B9 C1 B5 -140.36(19) . . . . ?
Cl11 B11 C1 C2 -4.0(3) . . . . ?
B8 B11 C1 C2 105.1(2) . . . . ?
B7 B11 C1 C2 143.4(2) . . . . ?
B10 B11 C1 C2 -153.2(2) . . . . ?
B9 B11 C1 C2 -114.3(2) . . . . ?
Cl11 B11 C1 B4 -145.50(18) . . . . ?
B8 B11 C1 B4 -36.35(18) . . . . ?
B7 B11 C1 B4 1.9(2) . . . . ?
B10 B11 C1 B4 65.3(2) . . . . ?
B9 B11 C1 B4 104.2(2) . . . . ?
Cl11 B11 C1 B9 110.3(2) . . . . ?
B8 B11 C1 B9 -140.53(19) . . . . ?
B7 B11 C1 B9 -102.2(2) . . . . ?
B10 B11 C1 B9 -38.83(17) . . . . ?
Cl11 B11 C1 B8 -109.2(2) . . . . ?
B7 B11 C1 B8 38.30(17) . . . . ?
B10 B11 C1 B8 101.7(2) . . . . ?
B9 B11 C1 B8 140.53(18) . . . . ?
Cl11 B11 C1 B5 147.62(17) . . . . ?
B8 B11 C1 B5 -103.2(2) . . . . ?
B7 B11 C1 B5 -64.9(2) . . . . ?
B10 B11 C1 B5 -1.5(2) . . . . ?
B9 B11 C1 B5 37.30(18) . . . . ?
B7 B8 C1 C2 -147.7(2) . . . . ?
B11 B8 C1 C2 -109.0(2) . . . . ?
Cl8 B8 C1 C2 -0.5(3) . . . . ?
B3 B8 C1 C2 148.2(2) . . . . ?
B4 B8 C1 C2 109.8(2) . . . . ?
B7 B8 C1 B4 102.5(2) . . . . ?
B11 B8 C1 B4 141.2(2) . . . . ?
Cl8 B8 C1 B4 -110.3(2) . . . . ?
B3 B8 C1 B4 38.39(17) . . . . ?
B7 B8 C1 B9 -1.8(2) . . . . ?
B11 B8 C1 B9 36.89(17) . . . . ?
Cl8 B8 C1 B9 145.40(17) . . . . ?
B3 B8 C1 B9 -65.9(2) . . . . ?
B4 B8 C1 B9 -104.33(19) . . . . ?
B7 B8 C1 B11 -38.71(17) . . . . ?
Cl8 B8 C1 B11 108.5(2) . . . . ?
B3 B8 C1 B11 -102.8(2) . . . . ?
B4 B8 C1 B11 -141.2(2) . . . . ?
B7 B8 C1 B5 65.1(2) . . . . ?
B11 B8 C1 B5 103.8(2) . . . . ?
Cl8 B8 C1 B5 -147.65(18) . . . . ?
B3 B8 C1 B5 1.0(2) . . . . ?
B4 B8 C1 B5 -37.38(18) . . . . ?
Cl5 B5 C1 C2 3.3(3) . . . . ?
B6 B5 C1 C2 151.6(2) . . . . ?
B1 B5 C1 C2 -145.5(2) . . . . ?
B4 B5 C1 C2 -106.7(3) . . . . ?
B9 B5 C1 C2 112.5(3) . . . . ?
Cl5 B5 C1 B4 110.0(2) . . . . ?
B6 B5 C1 B4 -101.66(19) . . . . ?
B1 B5 C1 B4 -38.76(17) . . . . ?
B9 B5 C1 B4 -140.76(19) . . . . ?
Cl5 B5 C1 B9 -109.2(2) . . . . ?
B6 B5 C1 B9 39.10(17) . . . . ?
B1 B5 C1 B9 102.00(19) . . . . ?
B4 B5 C1 B9 140.76(19) . . . . ?
Cl5 B5 C1 B11 -146.43(18) . . . . ?
B6 B5 C1 B11 1.9(2) . . . . ?
B1 B5 C1 B11 64.8(2) . . . . ?
B4 B5 C1 B11 103.5(2) . . . . ?
B9 B5 C1 B11 -37.22(18) . . . . ?
Cl5 B5 C1 B8 147.42(18) . . . . ?
B6 B5 C1 B8 -64.3(2) . . . . ?
B1 B5 C1 B8 -1.4(2) . . . . ?
B4 B5 C1 B8 37.39(18) . . . . ?
B9 B5 C1 B8 -103.37(19) . . . . ?
B4 C1 C2 C3A -128.6(4) . . . . ?
B9 C1 C2 C3A 19.9(5) . . . . ?
B11 C1 C2 C3A 92.4(5) . . . . ?
B8 C1 C2 C3A 161.5(4) . . . . ?
B5 C1 C2 C3A -55.7(5) . . . . ?
B4 C1 C2 C3 -73.3(4) . . . . ?
B9 C1 C2 C3 75.2(4) . . . . ?
B11 C1 C2 C3 147.7(3) . . . . ?
B8 C1 C2 C3 -143.3(3) . . . . ?
B5 C1 C2 C3 -0.4(4) . . . . ?
C3A C2 C3 C4 -67.8(5) . . . . ?
C1 C2 C3 C4 176.5(3) . . . . ?
C2 C3 C4 C5 -171.1(5) . . . . ?
C3 C2 C3A C4A 61.5(6) . . . . ?
C1 C2 C3A C4A 158.0(5) . . . . ?
C2 C3A C4A C5A -83.0(11) . . . . ?
O1 Ag1 C6 C11 140.93(18) . . . . ?
C7 Ag1 C6 C11 117.5(3) . . . . ?
Cl6 Ag1 C6 C11 -96.51(18) 3_455 . . . ?
Cl3 Ag1 C6 C11 44.17(19) . . . . ?
O1 Ag1 C6 C7 23.4(2) . . . . ?
Cl6 Ag1 C6 C7 145.96(16) 3_455 . . . ?
Cl3 Ag1 C6 C7 -73.36(16) . . . . ?
C11 C6 C7 C8 -0.2(4) . . . . ?
Ag1 C6 C7 C8 102.1(3) . . . . ?
C11 C6 C7 Ag1 -102.4(3) . . . . ?
O1 Ag1 C7 C6 -164.47(15) . . . . ?
Cl6 Ag1 C7 C6 -36.83(17) 3_455 . . . ?
Cl3 Ag1 C7 C6 110.65(16) . . . . ?
O1 Ag1 C7 C8 79.6(2) . . . . ?
C6 Ag1 C7 C8 -115.9(3) . . . . ?
Cl6 Ag1 C7 C8 -152.77(19) 3_455 . . . ?
Cl3 Ag1 C7 C8 -5.3(2) . . . . ?
C6 C7 C8 C9 0.9(4) . . . . ?
Ag1 C7 C8 C9 81.4(3) . . . . ?
C7 C8 C9 C10 -1.5(4) . . . . ?
C8 C9 C10 F1 -179.0(2) . . . . ?
C8 C9 C10 C11 1.4(4) . . . . ?
F1 C10 C11 C6 179.7(2) . . . . ?
C9 C10 C11 C6 -0.8(4) . . . . ?
C7 C6 C11 C10 0.2(4) . . . . ?
Ag1 C6 C11 C10 -83.2(3) . . . . ?

_diffrn_measured_fraction_theta_max 0.996
_diffrn_reflns_theta_full        27.50
_diffrn_measured_fraction_theta_full 0.996
_refine_diff_density_max         0.546
_refine_diff_density_min         -0.343
_refine_diff_density_rms         0.057