# Electronic Supplementary Material (ESI) for Dalton Transactions
# This journal is © The Royal Society of Chemistry 2013


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#                 Cambridge Crystallographic Data Centre
#                                CCDC 
# 
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# 
#  This CIF contains data from an original supplementary publication 
#  deposited with the CCDC, and may include chemical, crystal,   
#  experimental, refinement, atomic coordinates, 
#  anisotropic displacement parameters and molecular geometry data,
#  as required by the journal to which it was submitted. 
# 
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#  fide research purposes only. It may contain copyright material 
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data_ag56
_database_code_depnum_ccdc_archive 'CCDC 884502'
#TrackingRef 'web_deposit_cif_file_0_DiSun_1362289851.Ag56 and Ag20-Revised.cif'
_audit_creation_date             2012-11-28
_audit_creation_method           
;
Olex2 1.2-ac2
(compiled 2012.03.06 svn.r2239, GUI svn.r4109)
;
_chemical_name_common            ?
_chemical_name_systematic        
;
?
;
_chemical_formula_moiety         'C80 H180 Ag56 S33'
_chemical_formula_sum            'C80 H180 Ag56 S33'
_chemical_formula_weight         8240.94
_chemical_melting_point          ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_space_group_crystal_system      cubic
_space_group_IT_number           205
_space_group_name_H-M_alt        'P a -3'
_space_group_name_Hall           '-P 2ac 2ab 3'
loop_
_space_group_symop_id
_space_group_symop_operation_xyz
1 'x, y, z'
2 '-x+1/2, -y, z+1/2'
3 '-x, y+1/2, -z+1/2'
4 'x+1/2, -y+1/2, -z'
5 'z, x, y'
6 'z+1/2, -x+1/2, -y'
7 '-z+1/2, -x, y+1/2'
8 '-z, x+1/2, -y+1/2'
9 'y, z, x'
10 '-y, z+1/2, -x+1/2'
11 'y+1/2, -z+1/2, -x'
12 '-y+1/2, -z, x+1/2'
13 '-x, -y, -z'
14 'x-1/2, y, -z-1/2'
15 'x, -y-1/2, z-1/2'
16 '-x-1/2, y-1/2, z'
17 '-z, -x, -y'
18 '-z-1/2, x-1/2, y'
19 'z-1/2, x, -y-1/2'
20 'z, -x-1/2, y-1/2'
21 '-y, -z, -x'
22 'y, -z-1/2, x-1/2'
23 '-y-1/2, z-1/2, x'
24 'y-1/2, z, -x-1/2'
_cell_length_a                   29.022(6)
_cell_length_b                   29.022(6)
_cell_length_c                   29.022(6)
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_volume                     24444(8)
_cell_formula_units_Z            4
_cell_measurement_reflns_used    6305
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      18.889
_cell_measurement_theta_min      2.328
_exptl_absorpt_coefficient_mu    4.666
_exptl_absorpt_correction_T_max  0.5412
_exptl_absorpt_correction_T_min  0.4555
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            RED
_exptl_crystal_density_diffrn    2.239
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             15280
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.15
_exptl_special_details           
;
?
;
_diffrn_reflns_av_R_equivalents  0.0489
_diffrn_reflns_av_unetI/netI     0.0502
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -34
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -33
_diffrn_reflns_limit_l_max       34
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            26664
_diffrn_reflns_theta_full        24.99
_diffrn_reflns_theta_max         24.99
_diffrn_reflns_theta_min         2.63
_diffrn_ambient_temperature      100(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.991
_diffrn_measured_fraction_theta_max 0.991
_diffrn_measurement_device_type  'Bruker SMART APEX II CCD area detector'
_diffrn_measurement_method       ?
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           'MO K\a'
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'fine-focus sealed tube'
_diffrn_source_current           30.0
_diffrn_source_power             1.5
_diffrn_source_voltage           50.0
_diffrn_standards_decay_%        ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_number         ?
_reflns_number_gt                4811
_reflns_number_total             7126
_reflns_threshold_expression     >2sigma(I)
_computing_data_collection       'APEX2 (Bruker, 2008)'
_computing_cell_refinement       'SAINT+ ver. (Bruker, 2001)'
_computing_data_reduction        'SAINT+ ver. (Bruker, 2001)'
_computing_structure_solution    'SHELXTL (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXTL (Sheldrick, 2008)'
_computing_molecular_graphics    'SHELXTL (Sheldrick, 2008)'
_computing_publication_material  'SHELXTL (Sheldrick, 2008)'
_refine_diff_density_max         2.121
_refine_diff_density_min         -0.899
_refine_diff_density_rms         0.227
_refine_ls_extinction_coef       ?
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.069
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     435
_refine_ls_number_reflns         7126
_refine_ls_number_restraints     244
_refine_ls_R_factor_all          0.1056
_refine_ls_R_factor_gt           0.0829
_refine_ls_restrained_S_all      1.118
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details     
'calc w=1/[\s^2^(Fo^2^)+(0.1725P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2422
_refine_ls_wR_factor_ref         0.2648
_refine_special_details          
;
Refinement of F^2^ against ALL reflections. The weighted R-factor wR and
goodness of fit S are based on F^2^, conventional R-factors R are based
on F, with F set to zero for negative F^2^. The threshold expression of
F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is
not relevant to the choice of reflections for refinement. R-factors based
on F^2^ are statistically about twice as large as those based on F, and R-
factors based on ALL data will be even larger.
The relatively high R1 and wR2 values in this structure are partially
due to the total instability of the crystals towards loss of initially
accumulated solvent and weak diffraction, and
in part due to disordering of Ag atoms as well as the solvent and anion.
It was not possible to improve present convergence,
although more then five different datasets were collected in total
(and more then 20 crystals were examined)
under different conditions, using either SMART CCD and Xcalibur, Eos, Gemin,
varying the crystal size, exposition and data reduction parameters.
Nine Ag atoms (Ag1-Ag9) were disordered and refined with splitting mode.
The occupancy factors of the disordered Ag atoms as follows:
Ag1A:Ag1B 0.95:0.05;
Ag2A:Ag2B 0.75:0.25;
Ag3A:Ag3B:Ag3C:Ag3D 0.40:0.15:0.05:0.40;
Ag4A:Ag4B 0.10:0.90;
Ag5A:Ag5B:Ag5C:Ag5D 0.15:0.60:0.20:0.05;
Ag6A:Ag6B:Ag6C 0.10:0.70:0.20;
Ag7A:Ag7B:Ag7C:Ag7D 0.20:0.55:0.15:0.10;
Ag8A:Ag8B:Ag8C:Ag8D 0.50:0.30:0.15:0.05;
Ag9A:Ag9B:Ag9C:Ag9D 0.40:0.40:0.10:0.10;
To assist the refinement of this cluster, several restraints
were applied: (1) some C-C and C-S bonds were restrained to be
similar (DFIX); (2) thermal parameters on adjacent
atoms in disordered moieties were restrained
to be similar (DELU, SIMU and ISOR).
;
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_secondary   difmap
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1A Ag 0.61836(3) 0.48030(3) 0.52679(3) 0.0440(3) Uani 0.95 1 d P . .
Ag1B Ag 0.5928(6) 0.4834(5) 0.5525(5) 0.038(3) Uani 0.05 1 d PU . .
Ag2A Ag 0.53311(8) 0.43793(10) 0.58112(8) 0.0647(7) Uani 0.75 1 d P . .
Ag2B Ag 0.5240(2) 0.4403(2) 0.5944(2) 0.0445(15) Uani 0.25 1 d PU . .
Ag3A Ag 0.6264(2) 0.3251(2) 0.50854(16) 0.0898(16) Uani 0.40 1 d PU . .
Ag3B Ag 0.6012(6) 0.3099(5) 0.5099(5) 0.099(4) Uani 0.15 1 d PU . .
Ag3C Ag 0.6741(11) 0.3683(13) 0.4760(13) 0.094(8) Uani 0.05 1 d PU . .
Ag3D Ag 0.6496(2) 0.34495(19) 0.49462(17) 0.0906(15) Uani 0.40 1 d PU . .
Ag4A Ag 0.5441(4) 0.6604(3) 0.6328(4) 0.064(3) Uani 0.10 1 d PU . .
Ag4B Ag 0.54706(4) 0.62365(5) 0.64769(4) 0.0696(4) Uani 0.90 1 d PU . .
Ag5A Ag 0.4575(3) 0.6787(3) 0.6275(3) 0.0566(19) Uani 0.15 1 d PU . .
Ag5B Ag 0.42876(14) 0.63661(13) 0.63000(18) 0.0512(8) Uani 0.60 1 d PU . .
Ag5C Ag 0.4418(5) 0.6509(5) 0.6285(5) 0.071(4) Uani 0.20 1 d PU . .
Ag5D Ag 0.4075(11) 0.6274(8) 0.6431(9) 0.052(6) Uani 0.05 1 d PU . .
Ag6A Ag 0.6858(3) 0.5577(5) 0.5755(5) 0.072(3) Uani 0.10 1 d PU . .
Ag6B Ag 0.70698(7) 0.52797(10) 0.54755(8) 0.0977(8) Uani 0.70 1 d PU . .
Ag6C Ag 0.7057(2) 0.5652(3) 0.5361(2) 0.0755(16) Uani 0.20 1 d PU . .
Ag7A Ag 0.74237(19) 0.4642(3) 0.55321(17) 0.0732(15) Uani 0.20 1 d PU . .
Ag7B Ag 0.69467(10) 0.41712(13) 0.54371(12) 0.0967(10) Uani 0.55 1 d PU . .
Ag7C Ag 0.6809(3) 0.3798(3) 0.5632(3) 0.078(2) Uani 0.15 1 d PU . .
Ag7D Ag 0.7094(7) 0.4387(6) 0.5510(6) 0.087(5) Uani 0.10 1 d PU . .
Ag8A Ag 0.55009(16) 0.29295(14) 0.46147(15) 0.0722(10) Uani 0.50 1 d P . .
Ag8B Ag 0.56298(18) 0.31254(19) 0.4808(2) 0.0799(15) Uani 0.30 1 d P . .
Ag8C Ag 0.5478(4) 0.2960(5) 0.4402(4) 0.072(3) Uani 0.15 1 d PU . .
Ag8D Ag 0.5096(9) 0.2936(7) 0.4762(8) 0.068(5) Uani 0.05 1 d PU . .
Ag9A Ag 0.67447(12) 0.39685(13) 0.42064(16) 0.0697(8) Uani 0.40 1 d PU . .
Ag9B Ag 0.66195(10) 0.39687(11) 0.44813(15) 0.0650(8) Uani 0.40 1 d PU . .
Ag9C Ag 0.3762(5) 0.6219(4) 0.6554(4) 0.068(3) Uani 0.10 1 d PU . .
Ag9D Ag 0.6739(5) 0.4347(7) 0.4213(5) 0.097(4) Uani 0.10 1 d P . .
Ag10 Ag 0.55864(3) 0.55864(3) 0.55864(3) 0.0473(4) Uani 1 3 d S . .
S1 S 0.62775(10) 0.62775(10) 0.62775(10) 0.0548(13) Uani 1 3 d S . .
S2 S 0.47916(12) 0.62137(10) 0.69596(9) 0.0523(8) Uani 1 1 d D . .
S3 S 0.60329(13) 0.40050(10) 0.54478(10) 0.0548(8) Uani 1 1 d . . .
S4 S 0.63192(9) 0.55944(9) 0.50725(10) 0.0425(6) Uani 1 1 d . . .
S5 S 0.5000 0.5000 0.5000 0.0306(12) Uani 1 6 d S . .
S6 S 0.72203(10) 0.45160(13) 0.46875(13) 0.0627(9) Uani 1 1 d D . .
S7 S 0.37526(10) 0.67689(10) 0.57965(11) 0.0506(7) Uani 1 1 d . . .
C1 C 0.7844(4) 0.4390(5) 0.4593(6) 0.113(6) Uani 1 1 d DU . .
C2 C 0.8016(7) 0.4684(6) 0.4201(7) 0.152(8) Uani 1 1 d DU . .
H2A H 0.8020 0.5001 0.4294 0.229 Uiso 1 1 calc R . .
H2B H 0.7816 0.4648 0.3940 0.229 Uiso 1 1 calc R . .
H2C H 0.8322 0.4589 0.4119 0.229 Uiso 1 1 calc R . .
C3 C 0.7890(6) 0.3882(5) 0.4493(7) 0.127(7) Uani 1 1 d DU . .
H3A H 0.8087 0.3743 0.4719 0.191 Uiso 1 1 calc R . .
H3B H 0.8020 0.3841 0.4192 0.191 Uiso 1 1 calc R . .
H3C H 0.7592 0.3740 0.4505 0.191 Uiso 1 1 calc R . .
C4 C 0.8105(7) 0.4513(8) 0.5034(6) 0.155(7) Uani 1 1 d DU . .
H7AA H 0.7892 0.4536 0.5286 0.232 Uiso 1 1 calc R . .
H4A H 0.8260 0.4803 0.4994 0.232 Uiso 1 1 calc R . .
H4B H 0.8328 0.4277 0.5099 0.232 Uiso 1 1 calc R . .
C5 C 0.4815(4) 0.6682(5) 0.7415(5) 0.107(6) Uani 1 1 d DU . .
C6 C 0.5168(6) 0.6533(7) 0.7760(6) 0.166(10) Uani 1 1 d DU . .
H6A H 0.5023 0.6487 0.8053 0.249 Uiso 1 1 calc R . .
H6B H 0.5401 0.6766 0.7787 0.249 Uiso 1 1 calc R . .
H6C H 0.5307 0.6249 0.7660 0.249 Uiso 1 1 calc R . .
C7 C 0.4342(5) 0.6735(8) 0.7629(7) 0.139(8) Uani 1 1 d DU . .
H7A H 0.4295 0.6496 0.7853 0.209 Uiso 1 1 calc R . .
H7B H 0.4111 0.6712 0.7393 0.209 Uiso 1 1 calc R . .
H7C H 0.4321 0.7030 0.7776 0.209 Uiso 1 1 calc R . .
C8 C 0.4956(7) 0.7119(3) 0.7168(6) 0.149(8) Uani 1 1 d DU . .
H8A H 0.5013 0.7358 0.7390 0.223 Uiso 1 1 calc R . .
H8B H 0.4714 0.7214 0.6964 0.223 Uiso 1 1 calc R . .
H8C H 0.5232 0.7064 0.6994 0.223 Uiso 1 1 calc R . .
C9 C 0.3396(4) 0.7252(4) 0.6048(4) 0.077(4) Uani 1 1 d DU . .
C10 C 0.3640(6) 0.7431(7) 0.6468(5) 0.121(7) Uani 1 1 d DU . .
H10A H 0.3431 0.7435 0.6724 0.181 Uiso 1 1 calc R . .
H10B H 0.3748 0.7738 0.6409 0.181 Uiso 1 1 calc R . .
H10C H 0.3897 0.7235 0.6538 0.181 Uiso 1 1 calc R . .
C11 C 0.2925(5) 0.7061(7) 0.6181(6) 0.130(7) Uani 1 1 d DU . .
H11A H 0.2880 0.6767 0.6036 0.195 Uiso 1 1 calc R . .
H11B H 0.2689 0.7271 0.6080 0.195 Uiso 1 1 calc R . .
H11C H 0.2908 0.7026 0.6509 0.195 Uiso 1 1 calc R . .
C12 C 0.3352(7) 0.7607(6) 0.5675(5) 0.135(8) Uani 1 1 d DU . .
H12A H 0.3044 0.7604 0.5555 0.203 Uiso 1 1 calc R . .
H12B H 0.3566 0.7539 0.5433 0.203 Uiso 1 1 calc R . .
H12C H 0.3418 0.7906 0.5800 0.203 Uiso 1 1 calc R . .
C13 C 0.6658(4) 0.6658(4) 0.6658(4) 0.077(7) Uani 1 3 d SDU . .
C14 C 0.7140(4) 0.6590(9) 0.6490(8) 0.130(8) Uani 1 1 d DU . .
H14A H 0.7209 0.6816 0.6259 0.195 Uiso 1 1 calc R . .
H14B H 0.7169 0.6287 0.6360 0.195 Uiso 1 1 calc R . .
H14C H 0.7351 0.6622 0.6743 0.195 Uiso 1 1 calc R . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Ag1A 0.0451(5) 0.0387(5) 0.0482(5) 0.0010(4) -0.0017(4) 0.0019(4)
Ag1B 0.041(5) 0.041(5) 0.033(5) -0.004(4) 0.005(4) 0.000(4)
Ag2A 0.0541(12) 0.0828(13) 0.0572(12) -0.0164(10) 0.0060(9) -0.0061(9)
Ag2B 0.047(2) 0.0401(18) 0.047(2) 0.0016(17) -0.0064(17) 0.0023(15)
Ag3A 0.109(4) 0.101(4) 0.059(2) -0.024(3) -0.016(3) 0.041(3)
Ag3B 0.119(8) 0.086(6) 0.091(7) 0.008(5) 0.015(7) -0.018(6)
Ag3C 0.083(11) 0.095(11) 0.104(12) -0.022(9) 0.015(9) -0.013(9)
Ag3D 0.096(3) 0.091(3) 0.085(3) -0.032(2) -0.007(2) 0.037(3)
Ag4A 0.071(6) 0.035(4) 0.087(6) -0.022(5) -0.002(5) 0.001(4)
Ag4B 0.0655(7) 0.0816(9) 0.0617(7) -0.0166(6) -0.0008(6) -0.0003(6)
Ag5A 0.064(4) 0.043(4) 0.063(4) -0.011(3) -0.015(3) 0.007(3)
Ag5B 0.049(2) 0.0498(16) 0.0543(14) 0.0012(13) -0.0070(16) 0.0052(12)
Ag5C 0.065(7) 0.091(9) 0.057(4) 0.005(7) 0.002(5) 0.025(6)
Ag5D 0.051(8) 0.050(8) 0.055(8) 0.006(5) -0.002(5) 0.005(5)
Ag6A 0.037(4) 0.094(7) 0.085(6) 0.033(6) 0.006(5) -0.007(5)
Ag6B 0.0594(10) 0.144(2) 0.0900(14) 0.0512(15) -0.0232(10) -0.0335(13)
Ag6C 0.056(3) 0.099(4) 0.071(3) 0.011(3) -0.003(3) -0.016(3)
Ag7A 0.057(3) 0.114(4) 0.048(2) -0.015(3) 0.001(2) 0.022(3)
Ag7B 0.0688(16) 0.106(2) 0.116(2) 0.0279(19) 0.0210(15) 0.0464(16)
Ag7C 0.067(3) 0.073(4) 0.093(4) -0.013(3) -0.014(3) 0.032(3)
Ag7D 0.097(7) 0.087(7) 0.077(6) 0.001(5) 0.008(5) -0.004(5)
Ag8A 0.086(2) 0.0505(17) 0.080(3) 0.0042(19) 0.010(2) 0.0064(15)
Ag8B 0.068(3) 0.060(3) 0.111(4) 0.035(3) 0.024(3) 0.021(2)
Ag8C 0.058(4) 0.070(5) 0.086(5) -0.010(4) 0.014(4) 0.008(3)
Ag8D 0.078(7) 0.057(6) 0.067(7) 0.002(5) -0.009(5) 0.010(5)
Ag9A 0.0584(17) 0.0580(18) 0.093(2) 0.0040(18) 0.0007(17) 0.0001(15)
Ag9B 0.0477(15) 0.0565(16) 0.091(2) -0.0058(18) -0.0038(16) -0.0025(13)
Ag9C 0.074(5) 0.055(4) 0.075(5) 0.016(4) 0.005(4) 0.007(4)
Ag9D 0.062(7) 0.133(15) 0.097(10) 0.024(10) -0.004(7) -0.012(8)
Ag10 0.0473(4) 0.0473(4) 0.0473(4) 0.0019(4) 0.0019(4) 0.0019(4)
S1 0.0548(13) 0.0548(13) 0.0548(13) -0.0088(13) -0.0088(13) -0.0088(13)
S2 0.075(2) 0.0481(15) 0.0335(13) -0.0103(12) -0.0037(13) 0.0181(15)
S3 0.077(2) 0.0457(15) 0.0419(15) 0.0053(13) 0.0033(15) 0.0095(15)
S4 0.0405(14) 0.0440(14) 0.0430(14) -0.0031(12) 0.0042(12) -0.0025(12)
S5 0.0306(12) 0.0306(12) 0.0306(12) -0.0017(13) -0.0017(13) -0.0017(13)
S6 0.0385(15) 0.081(2) 0.068(2) -0.0019(18) 0.0114(15) 0.0082(16)
S7 0.0482(15) 0.0423(15) 0.0613(17) -0.0020(14) -0.0003(14) 0.0115(13)
C1 0.056(8) 0.130(12) 0.154(15) 0.010(12) 0.044(9) 0.008(9)
C2 0.096(13) 0.139(16) 0.22(2) 0.013(16) 0.081(15) -0.008(13)
C3 0.074(11) 0.125(13) 0.18(2) 0.010(14) 0.023(13) 0.006(11)
C4 0.076(11) 0.178(17) 0.209(18) -0.008(15) 0.004(12) 0.016(13)
C5 0.111(12) 0.125(12) 0.085(10) -0.062(10) -0.024(9) 0.045(11)
C6 0.182(19) 0.20(2) 0.118(14) -0.109(13) -0.087(14) 0.103(17)
C7 0.124(13) 0.19(2) 0.100(14) -0.050(14) -0.021(11) 0.072(14)
C8 0.157(18) 0.073(10) 0.22(2) -0.061(11) -0.016(16) 0.029(12)
C9 0.076(8) 0.082(9) 0.072(8) -0.011(7) -0.015(7) 0.043(7)
C10 0.101(12) 0.138(17) 0.124(14) -0.051(12) -0.043(11) 0.028(12)
C11 0.106(12) 0.138(16) 0.146(17) -0.070(13) 0.022(12) 0.017(11)
C12 0.19(2) 0.121(15) 0.092(11) 0.001(10) 0.036(13) 0.088(14)
C13 0.077(7) 0.077(7) 0.077(7) -0.028(6) -0.028(6) -0.028(6)
C14 0.068(9) 0.159(18) 0.162(19) -0.049(15) -0.014(11) -0.032(12)
_geom_special_details            
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1A Ag2A 3.181(3) . ?
Ag1A Ag2A 2.978(3) 21_666 ?
Ag1A Ag2B 2.897(7) 5 ?
Ag1A Ag2B 3.125(7) 21_666 ?
Ag1A Ag6B 2.982(2) . ?
Ag1A Ag7B 2.917(3) . ?
Ag1A Ag7D 2.99(2) . ?
Ag1A Ag10 3.0044(12) . ?
Ag1A S3 2.414(3) . ?
Ag1A S4 2.398(3) . ?
Ag1B Ag2A 3.237(15) 21_666 ?
Ag1B Ag2B 3.308(17) 21_666 ?
Ag1B Ag4B 3.196(15) 5 ?
Ag1B Ag5B 3.103(16) 5 ?
Ag1B Ag5C 3.27(2) 5 ?
Ag1B S3 2.435(16) . ?
Ag1B S4 2.809(16) . ?
Ag1B S4 2.593(16) 9 ?
Ag2A Ag1A 2.978(3) 17_666 ?
Ag2A Ag1A 3.188(3) 9 ?
Ag2A Ag1B 3.237(15) 17_666 ?
Ag2A Ag2B 3.283(6) 21_666 ?
Ag2A Ag5B 3.251(6) 5 ?
Ag2A Ag8B 3.112(6) 17_666 ?
Ag2A Ag9B 3.018(4) 17_666 ?
Ag2A S3 2.538(4) . ?
Ag2A S3 2.613(4) 17_666 ?
Ag2A S4 2.608(4) 9 ?
Ag2B Ag1A 2.897(7) 9 ?
Ag2B Ag1A 3.125(7) 17_666 ?
Ag2B Ag2A 3.283(6) 17_666 ?
Ag2B Ag3A 3.178(8) 17_666 ?
Ag2B Ag3B 3.183(16) 17_666 ?
Ag2B Ag3D 3.192(8) 17_666 ?
Ag2B Ag8B 2.706(8) 17_666 ?
Ag2B Ag9B 3.086(7) 17_666 ?
Ag2B S3 2.367(8) 17_666 ?
Ag2B S3 2.951(7) . ?
Ag2B S4 2.454(7) 9 ?
Ag3A Ag7C 2.745(11) . ?
Ag3A Ag8A 2.765(8) . ?
Ag3A Ag8C 3.139(14) . ?
Ag3A Ag9A 3.067(7) 17_666 ?
Ag3A Ag9B 2.911(9) . ?
Ag3A S3 2.519(5) . ?
Ag3A S7 2.561(5) 13_666 ?
Ag3B Ag3C 2.89(4) . ?
Ag3B Ag8C 2.58(2) . ?
Ag3B Ag8D 2.87(3) . ?
Ag3B Ag9A 2.815(15) 17_666 ?
Ag3B S3 2.817(14) . ?
Ag3B S6 2.494(14) 17_666 ?
Ag3B S7 2.716(14) 13_666 ?
Ag3C Ag7D 3.16(4) . ?
Ag3C S6 2.80(4) . ?
Ag3C S7 2.53(3) 13_666 ?
Ag3D Ag2B 3.192(8) 21_666 ?
Ag3D Ag7B 2.851(7) . ?
Ag3D Ag8B 2.713(9) . ?
Ag3D Ag9A 2.720(8) . ?
Ag3D Ag9D 2.955(18) 17_666 ?
Ag3D S3 2.554(5) . ?
Ag3D S7 2.359(5) 13_666 ?
Ag4A Ag5C 2.984(17) . ?
Ag4A Ag6A 2.932(17) 9 ?
Ag4A Ag6B 3.330(13) 5 ?
Ag4A S1 2.611(11) . ?
Ag4A S2 2.863(12) . ?
Ag4A S4 2.522(11) 5 ?
Ag4B Ag1B 3.196(15) 9 ?
Ag4B Ag5A 3.107(7) . ?
Ag4B Ag5C 3.205(13) . ?
Ag4B Ag6A 3.281(12) 5 ?
Ag4B Ag6B 2.854(3) 9 ?
Ag4B Ag6C 3.092(7) 9 ?
Ag4B Ag10 3.2175(18) . ?
Ag4B S1 2.415(3) . ?
Ag4B S2 2.419(4) . ?
Ag4B S4 2.820(3) 5 ?
Ag5A Ag6C 3.015(12) 5 ?
Ag5A Ag8A 2.719(10) 13_666 ?
Ag5A Ag9C 2.990(15) . ?
Ag5A S2 2.666(9) . ?
Ag5A S4 2.798(8) 5 ?
Ag5A S7 2.761(8) . ?
Ag5B Ag1B 3.103(16) 9 ?
Ag5B Ag2A 3.251(5) 9 ?
Ag5B Ag5C 0.564(14) . ?
Ag5B Ag5D 0.77(3) . ?
Ag5B Ag7B 3.302(5) 9 ?
Ag5B Ag7C 2.956(9) 9 ?
Ag5B Ag8C 2.905(14) 13_666 ?
Ag5B Ag9C 1.748(13) . ?
Ag5B S2 2.449(5) . ?
Ag5B S3 2.894(5) 9 ?
Ag5B S7 2.432(5) . ?
Ag5C Ag1B 3.27(2) 9 ?
Ag5C Ag8A 3.086(16) 13_666 ?
Ag5C S2 2.397(15) . ?
Ag5C S4 2.816(15) 5 ?
Ag5D Ag7B 2.87(3) 9 ?
Ag5D Ag7D 3.07(3) 9 ?
Ag5D Ag9A 3.09(3) 13_666 ?
Ag5D S2 2.59(2) . ?
Ag5D S3 2.67(2) 9 ?
Ag5D S7 2.52(2) . ?
Ag6A Ag4A 2.476(17) 9 ?
Ag6A Ag4A 2.932(17) 5 ?
Ag6A Ag4B 3.281(12) 9 ?
Ag6A Ag4B 1.809(12) 5 ?
Ag6A Ag6B 1.333(15) . ?
Ag6A Ag6C 1.298(14) . ?
Ag6A Ag7A 3.237(15) . ?
Ag6A Ag8D 2.72(3) 21_666 ?
Ag6A S2 2.655(12) 5 ?
Ag6A S4 2.525(12) . ?
Ag6B Ag4B 2.854(3) 5 ?
Ag6B Ag7A 2.124(7) . ?
Ag6B Ag7B 3.239(5) . ?
Ag6B Ag8A 2.850(5) 21_666 ?
Ag6B Ag8C 2.919(13) 21_666 ?
Ag6B S2 2.588(4) 5 ?
Ag6B S4 2.636(3) . ?
Ag6C Ag4A 2.372(14) 9 ?
Ag6C Ag4B 3.092(7) 5 ?
Ag6C Ag5A 3.015(12) 9 ?
Ag6C Ag7A 3.160(10) . ?
Ag6C Ag8B 3.215(9) 21_666 ?
Ag6C S4 2.305(6) . ?
Ag7A Ag7C 3.043(12) . ?
Ag7A Ag8D 2.72(3) 21_666 ?
Ag7A S2 2.433(6) 5 ?
Ag7A S6 2.547(6) . ?
Ag7A C4 2.48(2) . ?
Ag7B Ag5D 2.87(3) 5 ?
Ag7B Ag9B 2.990(6) . ?
Ag7B Ag9C 2.803(11) 5 ?
Ag7B S2 2.885(5) 5 ?
Ag7B S3 2.696(5) . ?
Ag7B S6 2.523(5) . ?
Ag7C Ag5B 2.956(9) 5 ?
Ag7C Ag9D 3.349(18) 17_666 ?
Ag7C S3 2.391(8) . ?
Ag7D Ag5D 3.07(3) 5 ?
Ag7D Ag8D 3.03(3) 21_666 ?
Ag7D Ag9C 3.16(2) 5 ?
Ag7D S2 2.388(18) 5 ?
Ag7D S6 2.444(18) . ?
Ag8A Ag5A 2.719(10) 13_666 ?
Ag8A Ag5C 3.086(16) 13_666 ?
Ag8A Ag6B 2.850(5) 17_666 ?
Ag8A Ag6C 2.620(8) 17_666 ?
Ag8A S4 2.809(5) 17_666 ?
Ag8A S6 2.618(6) 17_666 ?
Ag8A S7 2.624(5) 13_666 ?
Ag8B Ag2A 3.112(6) 21_666 ?
Ag8B Ag2B 2.706(8) 21_666 ?
Ag8B S4 2.849(5) 17_666 ?
Ag8B S6 2.388(6) 17_666 ?
Ag8B S7 2.526(6) 13_666 ?
Ag8C Ag5B 2.905(14) 13_666 ?
Ag8C Ag5C 2.54(2) 13_666 ?
Ag8C Ag6B 2.919(13) 17_666 ?
Ag8C Ag6C 2.442(15) 17_666 ?
Ag8C S4 2.632(14) 17_666 ?
Ag8C S7 2.436(13) 13_666 ?
Ag8D Ag1A 3.04(2) 17_666 ?
Ag8D Ag6A 2.72(3) 17_666 ?
Ag8D Ag7A 2.72(3) 17_666 ?
Ag8D Ag7D 3.03(3) 17_666 ?
Ag8D S4 2.45(2) 17_666 ?
Ag8D S6 2.23(2) 17_666 ?
Ag9A Ag3A 3.067(7) 21_666 ?
Ag9A Ag3B 2.815(15) 21_666 ?
Ag9A Ag5D 3.09(3) 13_666 ?
Ag9A Ag9C 2.708(13) 13_666 ?
Ag9A S3 2.843(5) 21_666 ?
Ag9A S6 2.526(5) . ?
Ag9A S7 2.581(5) 13_666 ?
Ag9B Ag2A 3.018(4) 21_666 ?
Ag9B Ag2B 3.086(7) 21_666 ?
Ag9B Ag3B 3.167(15) 21_666 ?
Ag9B Ag9D 1.390(17) . ?
Ag9B S3 2.895(5) 21_666 ?
Ag9B S6 2.433(5) . ?
Ag9B S7 2.529(4) 13_666 ?
Ag9C Ag7B 2.803(11) 9 ?
Ag9C Ag7D 3.16(2) 9 ?
Ag9C Ag9A 2.708(13) 13_666 ?
Ag9C Ag9B 3.249(13) 13_666 ?
Ag9C Ag9D 3.12(2) 13_666 ?
Ag9C S3 2.792(12) 9 ?
Ag9C S7 2.718(11) . ?
Ag9D Ag3A 2.152(18) 21_666 ?
Ag9D Ag3D 2.955(18) 21_666 ?
Ag9D Ag7C 3.349(18) 21_666 ?
Ag9D Ag8A 3.27(2) 21_666 ?
Ag9D Ag9C 3.12(2) 13_666 ?
Ag9D S3 2.349(15) 21_666 ?
Ag9D S6 2.024(16) . ?
Ag10 Ag1A 3.0044(12) 5 ?
Ag10 Ag1A 3.0044(12) 9 ?
Ag10 Ag4B 3.2175(18) 9 ?
Ag10 Ag4B 3.2175(17) 5 ?
Ag10 S4 2.598(3) 5 ?
Ag10 S4 2.598(3) 9 ?
Ag10 S4 2.598(3) . ?
Ag10 S5 2.9476(17) . ?
S1 Ag4A 2.611(11) 5 ?
S1 Ag4A 2.611(11) 9 ?
S1 Ag4B 2.415(3) 9 ?
S1 Ag4B 2.415(3) 5 ?
S1 C13 1.91(2) . ?
S2 Ag6A 2.655(12) 9 ?
S2 Ag6B 2.588(4) 9 ?
S2 Ag7A 2.433(6) 9 ?
S2 Ag7B 2.885(5) 9 ?
S2 Ag7D 2.388(18) 9 ?
S2 C5 1.896(13) . ?
S3 Ag2A 2.613(4) 21_666 ?
S3 Ag2B 2.367(8) 21_666 ?
S3 Ag5D 2.67(2) 5 ?
S3 Ag9C 2.792(12) 5 ?
S3 Ag9D 2.349(15) 17_666 ?
S4 Ag1B 2.593(16) 5 ?
S4 Ag2A 2.608(4) 5 ?
S4 Ag2B 2.454(7) 5 ?
S4 Ag4A 2.522(11) 9 ?
S4 Ag5A 2.798(8) 9 ?
S4 Ag8C 2.632(14) 21_666 ?
S4 Ag8D 2.45(2) 21_666 ?
S5 Ag10 2.9476(17) 13_666 ?
S6 Ag3B 2.494(14) 21_666 ?
S6 Ag8A 2.618(6) 21_666 ?
S6 Ag8B 2.388(6) 21_666 ?
S6 Ag8D 2.23(2) 21_666 ?
S6 C1 1.866(12) . ?
S7 Ag3A 2.561(5) 13_666 ?
S7 Ag3C 2.53(3) 13_666 ?
S7 Ag3D 2.359(5) 13_666 ?
S7 Ag8A 2.624(5) 13_666 ?
S7 Ag8B 2.526(6) 13_666 ?
S7 Ag8C 2.436(13) 13_666 ?
S7 Ag9A 2.581(5) 13_666 ?
S7 Ag9B 2.529(4) 13_666 ?
S7 C9 1.889(12) . ?
C1 C2 1.507(9) . ?
C1 C3 1.508(9) . ?
C1 C4 1.529(10) . ?
C2 H2A 0.9600 . ?
C2 H2B 0.9600 . ?
C2 H2C 0.9600 . ?
C3 H3A 0.9600 . ?
C3 H3B 0.9600 . ?
C3 H3C 0.9600 . ?
C4 H7AA 0.9600 . ?
C4 H4A 0.9600 . ?
C4 H4B 0.9600 . ?
C5 C6 1.497(9) . ?
C5 C7 1.513(9) . ?
C5 C8 1.515(10) . ?
C6 H6A 0.9600 . ?
C6 H6B 0.9600 . ?
C6 H6C 0.9600 . ?
C7 H7A 0.9600 . ?
C7 H7B 0.9600 . ?
C7 H7C 0.9600 . ?
C8 H8A 0.9600 . ?
C8 H8B 0.9600 . ?
C8 H8C 0.9600 . ?
C9 C10 1.500(9) . ?
C9 C11 1.524(9) . ?
C9 C12 1.501(9) . ?
C10 H10A 0.9600 . ?
C10 H10B 0.9600 . ?
C10 H10C 0.9600 . ?
C11 H11A 0.9600 . ?
C11 H11B 0.9600 . ?
C11 H11C 0.9600 . ?
C12 H12A 0.9600 . ?
C12 H12B 0.9600 . ?
C12 H12C 0.9600 . ?
C13 C14 1.493(9) 5 ?
C13 C14 1.493(10) . ?
C13 C14 1.493(9) 9 ?
C14 H14A 0.9600 . ?
C14 H14B 0.9600 . ?
C14 H14C 0.9600 . ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Ag1B Ag1A Ag2A 94.5(8) . 21_666 ?
Ag1B Ag1A Ag2B 90.5(8) . 21_666 ?
Ag1B Ag1A Ag2B 114.0(9) . 5 ?
Ag1B Ag1A Ag6B 115.1(8) . . ?
Ag1B Ag1A Ag7B 117.8(9) . . ?
Ag1B Ag1A Ag7D 119.2(9) . . ?
Ag1B Ag1A Ag8D 143.2(9) . 21_666 ?
Ag1B Ag1A S3 78.5(9) . . ?
Ag1B Ag1A S4 101.6(9) . . ?
Ag2A Ag1A Ag2A 68.37(6) 21_666 . ?
Ag2A Ag1A Ag6B 150.32(8) 21_666 . ?
Ag2A Ag1A Ag7D 112.4(4) 21_666 . ?
Ag2A Ag1A Ag8D 120.5(5) 21_666 21_666 ?
Ag2A Ag1A Ag10 108.43(7) 21_666 . ?
Ag2B Ag1A Ag2A 114.32(11) 5 . ?
Ag2B Ag1A Ag6B 100.33(13) 5 . ?
Ag2B Ag1A Ag7B 127.10(14) 5 . ?
Ag2B Ag1A Ag7D 126.3(4) 5 . ?
Ag6B Ag1A Ag2A 138.59(7) . . ?
Ag6B Ag1A Ag2B 152.48(13) . 21_666 ?
Ag6B Ag1A Ag10 94.83(7) . . ?
Ag7B Ag1A Ag2A 105.31(9) . . ?
Ag7B Ag1A Ag2A 97.96(11) . 21_666 ?
Ag7B Ag1A Ag2B 93.26(15) . 21_666 ?
Ag7B Ag1A Ag10 149.53(9) . . ?
Ag7D Ag1A Ag2A 114.5(4) . . ?
Ag7D Ag1A Ag10 138.0(4) . . ?
Ag8D Ag1A Ag2A 170.6(5) 21_666 . ?
Ag8D Ag1A Ag2B 125.6(5) 21_666 21_666 ?
Ag10 Ag1A Ag2A 72.02(6) . . ?
Ag10 Ag1A Ag2B 110.83(12) . 21_666 ?
Ag10 Ag1A Ag8D 106.1(4) . 21_666 ?
S3 Ag1A Ag2B 124.31(16) . 5 ?
S3 Ag1A Ag6B 123.89(10) . . ?
S3 Ag1A Ag8D 128.8(4) . 21_666 ?
S3 Ag1A Ag10 123.70(9) . . ?
S4 Ag1A Ag2A 121.69(9) . 21_666 ?
S4 Ag1A Ag2A 127.95(9) . . ?
S4 Ag1A Ag2B 129.96(14) . 21_666 ?
S4 Ag1A Ag7B 121.15(11) . . ?
S4 Ag1A Ag7D 107.3(4) . . ?
Ag1A Ag1B Ag2A 136.6(11) . . ?
Ag1A Ag1B Ag2B 144.4(11) . . ?
Ag1A Ag1B Ag4B 98.9(9) . 5 ?
Ag1A Ag1B Ag5B 105.6(10) . 5 ?
Ag1A Ag1B Ag5C 111.3(10) . 5 ?
Ag1A Ag1B Ag10 114.7(11) . . ?
Ag1A Ag1B S4 155.9(12) . 9 ?
Ag2A Ag1B Ag4B 117.9(6) . 5 ?
Ag2A Ag1B Ag5C 123.0(5) 21_666 5 ?
Ag2A Ag1B Ag10 100.5(6) . . ?
Ag2A Ag1B S4 155.8(7) . . ?
Ag2B Ag1B Ag2A 82.6(4) . 21_666 ?
Ag2B Ag1B Ag2B 76.5(4) . 21_666 ?
Ag2B Ag1B Ag4B 110.7(5) . 5 ?
Ag2B Ag1B S4 152.8(7) . . ?
Ag4B Ag1B Ag2A 165.4(6) 5 21_666 ?
Ag4B Ag1B Ag2B 166.5(6) 5 21_666 ?
Ag5B Ag1B Ag2A 113.8(5) 5 21_666 ?
Ag5B Ag1B Ag2B 106.3(5) 5 21_666 ?
Ag5C Ag1B Ag2B 115.2(5) 5 21_666 ?
Ag10 Ag1B Ag2A 117.9(6) . 21_666 ?
Ag10 Ag1B Ag2B 123.3(6) . 21_666 ?
Ag10 Ag1B Ag2B 94.8(6) . . ?
Ag10 Ag1B Ag5B 123.3(6) . 5 ?
Ag10 Ag1B Ag5C 113.7(6) . 5 ?
Ag10 Ag1B S3 162.9(8) . . ?
S3 Ag1B Ag4B 124.6(6) . 5 ?
S3 Ag1B S4 113.1(6) . 9 ?
S3 Ag1B S4 133.0(7) . . ?
S4 Ag1B Ag2A 137.2(6) 9 21_666 ?
S4 Ag1B Ag2A 101.9(5) . 21_666 ?
S4 Ag1B Ag2B 132.1(6) 9 21_666 ?
S4 Ag1B Ag2B 109.8(5) . 21_666 ?
S4 Ag1B Ag5B 128.9(6) . 5 ?
S4 Ag1B Ag5C 124.8(6) . 5 ?
S4 Ag1B S4 110.9(6) 9 . ?
Ag1A Ag2A Ag1A 103.25(9) . 9 ?
Ag1A Ag2A Ag1A 111.46(8) 17_666 9 ?
Ag1A Ag2A Ag1A 111.67(7) 17_666 . ?
Ag1A Ag2A Ag1B 92.8(3) 9 17_666 ?
Ag1A Ag2A Ag1B 114.6(3) . 17_666 ?
Ag1A Ag2A Ag2B 131.22(16) 9 21_666 ?
Ag1A Ag2A Ag5B 108.31(10) 9 5 ?
Ag1A Ag2A Ag8B 120.88(16) 17_666 17_666 ?
Ag1B Ag2A Ag1A 91.2(4) . 9 ?
Ag1B Ag2A Ag1A 122.1(4) . 17_666 ?
Ag1B Ag2A Ag1B 121.4(6) . 17_666 ?
Ag1B Ag2A Ag5B 158.1(3) 17_666 5 ?
Ag1B Ag2A Ag8B 117.0(4) . 17_666 ?
Ag1B Ag2A Ag9B 119.0(4) . 17_666 ?
Ag1B Ag2A S3 59.9(4) . . ?
Ag1B Ag2A S3 167.2(4) . 17_666 ?
Ag5B Ag2A Ag2B 103.49(16) 5 21_666 ?
Ag8B Ag2A Ag1A 126.55(16) 17_666 . ?
Ag8B Ag2A Ag1A 66.96(10) 17_666 9 ?
Ag8B Ag2A Ag1B 118.1(3) 17_666 17_666 ?
Ag8B Ag2A Ag2B 161.66(19) 17_666 21_666 ?
Ag8B Ag2A Ag5B 67.68(16) 17_666 5 ?
Ag9B Ag2A Ag1A 142.36(11) 17_666 9 ?
Ag9B Ag2A Ag1A 109.63(11) 17_666 . ?
Ag9B Ag2A Ag1B 89.8(3) 17_666 17_666 ?
Ag9B Ag2A Ag2B 83.09(15) 17_666 21_666 ?
Ag9B Ag2A Ag5B 70.15(12) 17_666 5 ?
Ag9B Ag2A Ag8B 78.78(13) 17_666 17_666 ?
S3 Ag2A Ag1A 89.13(11) . 17_666 ?
S3 Ag2A Ag1A 48.34(8) . . ?
S3 Ag2A Ag1A 150.78(13) . 9 ?
S3 Ag2A Ag1A 83.41(10) 17_666 9 ?
S3 Ag2A Ag1A 50.65(9) 17_666 17_666 ?
S3 Ag2A Ag1A 162.01(11) 17_666 . ?
S3 Ag2A Ag1B 105.0(3) . 17_666 ?
S3 Ag2A Ag1B 47.7(3) 17_666 17_666 ?
S3 Ag2A Ag2B 105.20(12) 17_666 21_666 ?
S3 Ag2A Ag2B 45.81(15) . 21_666 ?
S3 Ag2A Ag5B 58.44(11) . 5 ?
S3 Ag2A Ag5B 127.57(14) 17_666 5 ?
S3 Ag2A Ag8B 71.44(17) 17_666 17_666 ?
S3 Ag2A Ag8B 120.82(16) . 17_666 ?
S3 Ag2A Ag9B 62.10(12) . 17_666 ?
S3 Ag2A Ag9B 70.92(13) 17_666 17_666 ?
S3 Ag2A S3 125.68(13) . 17_666 ?
S3 Ag2A S4 109.26(13) . 9 ?
S4 Ag2A Ag1A 158.81(13) 9 17_666 ?
S4 Ag2A Ag1A 75.77(9) 9 . ?
S4 Ag2A Ag1A 47.59(8) 9 9 ?
S4 Ag2A Ag1B 139.8(3) 9 17_666 ?
S4 Ag2A Ag2B 132.57(12) 9 21_666 ?
S4 Ag2A Ag5B 61.96(10) 9 5 ?
S4 Ag2A Ag8B 58.95(14) 9 17_666 ?
S4 Ag2A Ag9B 124.64(12) 9 17_666 ?
S4 Ag2A S3 119.42(13) 9 17_666 ?
Ag1A Ag2B Ag1A 115.6(2) 9 17_666 ?
Ag1A Ag2B Ag2A 59.47(10) 17_666 17_666 ?
Ag1A Ag2B Ag2A 57.21(13) 9 17_666 ?
Ag1A Ag2B Ag3A 92.2(2) 17_666 17_666 ?
Ag1A Ag2B Ag3A 102.8(2) 9 17_666 ?
Ag1A Ag2B Ag3B 104.7(4) 17_666 17_666 ?
Ag1A Ag2B Ag3B 89.0(3) 9 17_666 ?
Ag1A Ag2B Ag3D 120.1(2) 9 17_666 ?
Ag1A Ag2B Ag3D 81.83(19) 17_666 17_666 ?
Ag1A Ag2B Ag9B 158.2(2) 9 17_666 ?
Ag1A Ag2B S3 142.9(3) 9 . ?
Ag1B Ag2B Ag1A 107.1(4) . 17_666 ?
Ag1B Ag2B Ag1A 91.8(4) . 9 ?
Ag1B Ag2B Ag2A 117.3(4) . 17_666 ?
Ag1B Ag2B Ag3A 148.0(4) . 17_666 ?
Ag1B Ag2B Ag3B 144.2(5) . 17_666 ?
Ag1B Ag2B Ag3D 139.9(4) . 17_666 ?
Ag1B Ag2B Ag8B 120.8(4) . 17_666 ?
Ag1B Ag2B Ag9B 107.1(4) . 17_666 ?
Ag1B Ag2B S3 51.2(4) . . ?
Ag3A Ag2B Ag2A 94.5(2) 17_666 17_666 ?
Ag3B Ag2B Ag2A 92.9(3) 17_666 17_666 ?
Ag3D Ag2B Ag2A 101.1(2) 17_666 17_666 ?
Ag8B Ag2B Ag1A 130.5(3) 17_666 17_666 ?
Ag8B Ag2B Ag1A 76.61(19) 17_666 9 ?
Ag8B Ag2B Ag2A 104.3(2) 17_666 17_666 ?
Ag8B Ag2B Ag9B 84.1(2) 17_666 17_666 ?
Ag8B Ag2B S3 120.9(3) 17_666 . ?
Ag9B Ag2B Ag1A 69.94(16) 17_666 17_666 ?
Ag9B Ag2B Ag2A 119.6(2) 17_666 17_666 ?
Ag9B Ag2B Ag3A 55.4(2) 17_666 17_666 ?
Ag9B Ag2B Ag3B 69.3(3) 17_666 17_666 ?
S3 Ag2B Ag1A 79.40(17) . 17_666 ?
S3 Ag2B Ag1A 49.84(15) 17_666 17_666 ?
S3 Ag2B Ag1A 94.6(2) 17_666 9 ?
S3 Ag2B Ag1B 156.3(4) 17_666 . ?
S3 Ag2B Ag2A 50.24(13) 17_666 17_666 ?
S3 Ag2B Ag2A 132.6(2) . 17_666 ?
S3 Ag2B Ag3A 110.6(2) . 17_666 ?
S3 Ag2B Ag3B 121.3(3) . 17_666 ?
S3 Ag2B Ag3D 94.7(2) . 17_666 ?
S3 Ag2B Ag3D 52.16(17) 17_666 17_666 ?
S3 Ag2B Ag8B 82.9(3) 17_666 17_666 ?
S3 Ag2B Ag9B 72.7(2) 17_666 17_666 ?
S3 Ag2B S3 118.6(3) 17_666 . ?
S3 Ag2B S4 138.5(3) 17_666 9 ?
S4 Ag2B Ag2A 109.3(2) 9 17_666 ?
S4 Ag2B Ag3A 106.3(2) 9 17_666 ?
S4 Ag2B Ag3B 92.4(4) 9 17_666 ?
S4 Ag2B Ag3D 118.2(2) 9 17_666 ?
S4 Ag2B Ag8B 66.8(2) 9 17_666 ?
S4 Ag2B Ag9B 127.9(3) 9 17_666 ?
S4 Ag2B S3 101.5(2) 9 . ?
Ag3B Ag3A Ag3C 153.6(16) . . ?
Ag3B Ag3A Ag3D 156.3(13) . . ?
Ag3B Ag3A Ag7C 139.7(12) . . ?
Ag3B Ag3A Ag9A 65.0(11) . 17_666 ?
Ag3B Ag3A Ag9B 134.4(12) . . ?
Ag3B Ag3A Ag9D 54.6(12) . 17_666 ?
Ag3B Ag3A S3 101.5(11) . . ?
Ag3B Ag3A S7 91.1(11) . 13_666 ?
Ag3C Ag3A Ag8A 120.6(10) . . ?
Ag3C Ag3A Ag8C 110.9(10) . . ?
Ag3C Ag3A Ag9A 134.1(9) . 17_666 ?
Ag3C Ag3A Ag9D 139.7(9) . 17_666 ?
Ag3C Ag3A S3 81.0(9) . . ?
Ag3D Ag3A Ag8A 123.2(4) . . ?
Ag3D Ag3A Ag8B 124.3(5) . . ?
Ag3D Ag3A Ag8C 113.5(5) . . ?
Ag3D Ag3A Ag9A 132.6(5) . 17_666 ?
Ag3D Ag3A Ag9D 138.9(6) . 17_666 ?
Ag3D Ag3A S3 81.0(4) . . ?
Ag7C Ag3A Ag8A 160.4(2) . . ?
Ag7C Ag3A Ag8C 159.9(3) . . ?
Ag8A Ag3A Ag9B 103.16(17) . . ?
Ag8B Ag3A Ag3C 121.6(11) . . ?
Ag8B Ag3A Ag7C 148.2(3) . . ?
Ag8B Ag3A Ag9A 87.3(3) . 17_666 ?
Ag8B Ag3A Ag9B 102.1(2) . . ?
Ag8B Ag3A Ag9D 74.0(6) . 17_666 ?
Ag8B Ag3A S3 94.5(3) . . ?
Ag8B Ag3A S7 65.5(2) . 13_666 ?
Ag9A Ag3A Ag8C 104.1(3) 17_666 . ?
Ag9B Ag3A Ag8C 94.0(3) . . ?
Ag9B Ag3A Ag9A 133.9(2) . 17_666 ?
Ag9D Ag3A Ag7C 85.4(5) 17_666 . ?
Ag9D Ag3A Ag8A 82.4(6) 17_666 . ?
Ag9D Ag3A Ag8C 91.2(6) 17_666 . ?
Ag9D Ag3A Ag9B 132.7(4) 17_666 . ?
Ag9D Ag3A S3 59.8(4) 17_666 . ?
Ag9D Ag3A S7 138.9(6) 17_666 13_666 ?
S3 Ag3A Ag7C 53.8(2) . . ?
S3 Ag3A Ag8A 106.6(2) . . ?
S3 Ag3A Ag8C 107.7(3) . . ?
S3 Ag3A Ag9A 60.25(13) . 17_666 ?
S3 Ag3A Ag9B 74.0(2) . . ?
S3 Ag3A S7 115.6(2) . 13_666 ?
S7 Ag3A Ag7C 127.0(4) 13_666 . ?
S7 Ag3A Ag8A 58.88(14) 13_666 . ?
S7 Ag3A Ag8C 49.3(2) 13_666 . ?
S7 Ag3A Ag9A 152.4(3) 13_666 17_666 ?
S7 Ag3A Ag9B 54.61(17) 13_666 . ?
Ag3A Ag3B Ag8A 133.8(14) . . ?
Ag3A Ag3B Ag8B 128.5(15) . . ?
Ag3A Ag3B Ag8C 123.8(13) . . ?
Ag3A Ag3B Ag8D 149.4(15) . . ?
Ag3A Ag3B Ag9A 98.9(12) . 17_666 ?
Ag3A Ag3B Ag9D 102.6(14) . 17_666 ?
Ag3A Ag3B S3 61.2(9) . . ?
Ag3A Ag3B S6 155.4(14) . 17_666 ?
Ag3A Ag3B S7 70.5(10) . 13_666 ?
Ag3D Ag3B Ag8A 121.3(8) . . ?
Ag3D Ag3B Ag8C 111.4(7) . . ?
Ag3D Ag3B Ag8D 137.3(9) . . ?
Ag3D Ag3B Ag9A 108.9(7) . 17_666 ?
Ag3D Ag3B Ag9D 111.0(10) . 17_666 ?
Ag3D Ag3B S3 62.7(5) . . ?
Ag3D Ag3B S6 163.9(8) . 17_666 ?
Ag3D Ag3B S7 59.0(4) . 13_666 ?
Ag8A Ag3B Ag3C 115.2(9) . . ?
Ag8A Ag3B Ag9A 121.5(7) . 17_666 ?
Ag8A Ag3B S3 118.3(7) . . ?
Ag8A Ag3B S6 68.8(5) . 17_666 ?
Ag8A Ag3B S7 64.5(4) . 13_666 ?
Ag8B Ag3B Ag3C 110.1(11) . . ?
Ag8B Ag3B Ag3D 116.2(9) . . ?
Ag8B Ag3B Ag9A 113.3(9) . 17_666 ?
Ag8B Ag3B Ag9D 103.9(12) . 17_666 ?
Ag8B Ag3B S3 100.6(8) . . ?
Ag8B Ag3B S6 69.3(6) . 17_666 ?
Ag8B Ag3B S7 67.2(6) . 13_666 ?
Ag8C Ag3B Ag3C 105.3(9) . . ?
Ag8C Ag3B Ag8D 31.9(6) . . ?
Ag8C Ag3B Ag9A 130.1(7) . 17_666 ?
Ag8C Ag3B S3 116.1(7) . . ?
Ag8C Ag3B S7 54.7(4) . 13_666 ?
Ag8D Ag3B Ag3C 131.2(11) . . ?
Ag9A Ag3B Ag3C 113.5(8) 17_666 . ?
Ag9A Ag3B Ag8D 98.4(7) 17_666 . ?
Ag9A Ag3B S3 60.6(3) 17_666 . ?
Ag9D Ag3B Ag3C 114.7(10) 17_666 . ?
Ag9D Ag3B Ag8A 113.9(10) 17_666 . ?
Ag9D Ag3B Ag8C 121.7(10) 17_666 . ?
Ag9D Ag3B Ag8D 90.8(10) 17_666 . ?
Ag9D Ag3B Ag9A 10.5(6) 17_666 17_666 ?
Ag9D Ag3B S3 56.1(6) 17_666 . ?
Ag9D Ag3B S6 53.3(6) 17_666 17_666 ?
Ag9D Ag3B S7 155.6(9) 17_666 13_666 ?
S3 Ag3B Ag3C 63.8(7) . . ?
S3 Ag3B Ag8D 107.2(7) . . ?
S6 Ag3B Ag3C 165.5(9) 17_666 . ?
S6 Ag3B Ag8C 78.7(6) 17_666 . ?
S6 Ag3B Ag8D 48.6(6) 17_666 . ?
S6 Ag3B Ag9A 56.4(3) 17_666 17_666 ?
S6 Ag3B S3 101.8(5) 17_666 . ?
S6 Ag3B S7 133.3(7) 17_666 13_666 ?
S7 Ag3B Ag3C 53.5(7) 13_666 . ?
S7 Ag3B Ag8D 86.0(7) 13_666 . ?
S7 Ag3B Ag9A 162.6(5) 13_666 17_666 ?
S7 Ag3B S3 101.9(4) 13_666 . ?
Ag3A Ag3C Ag7B 98.2(14) . . ?
Ag3A Ag3C Ag7C 71.5(12) . . ?
Ag3A Ag3C Ag7D 106.9(14) . . ?
Ag3A Ag3C Ag9D 138.4(17) . . ?
Ag3A Ag3C S6 151.7(14) . . ?
Ag3A Ag3C S7 66.6(9) . 13_666 ?
Ag3B Ag3C Ag7D 112.5(12) . . ?
Ag3D Ag3C Ag7B 97(2) . . ?
Ag3D Ag3C Ag7C 69.5(18) . . ?
Ag3D Ag3C Ag7D 105(2) . . ?
Ag3D Ag3C Ag9A 135(3) . . ?
Ag3D Ag3C Ag9B 123(3) . . ?
Ag3D Ag3C Ag9D 140(3) . . ?
Ag3D Ag3C S6 151(2) . . ?
Ag3D Ag3C S7 68.6(15) . 13_666 ?
Ag7B Ag3C Ag3B 103.9(13) . . ?
Ag7B Ag3C Ag7C 29.4(4) . . ?
Ag7B Ag3C Ag9D 93.7(13) . . ?
Ag7B Ag3C S6 56.6(7) . . ?
Ag7B Ag3C S7 159.1(15) . 13_666 ?
Ag7C Ag3C Ag3B 78.2(11) . . ?
Ag7C Ag3C Ag7D 37.7(6) . . ?
Ag7C Ag3C S6 85.6(9) . . ?
Ag9A Ag3C Ag3A 132.9(18) . . ?
Ag9A Ag3C Ag3B 125.3(16) . . ?
Ag9A Ag3C Ag7B 116.0(18) . . ?
Ag9A Ag3C Ag7C 144.9(18) . . ?
Ag9A Ag3C Ag7D 108.3(16) . . ?
Ag9A Ag3C Ag9D 23.2(7) . . ?
Ag9A Ag3C S6 62.2(12) . . ?
Ag9A Ag3C S7 71.0(11) . 13_666 ?
Ag9B Ag3C Ag3A 121(2) . . ?
Ag9B Ag3C Ag3B 115(2) . . ?
Ag9B Ag3C Ag7B 101.9(19) . . ?
Ag9B Ag3C Ag7C 126(2) . . ?
Ag9B Ag3C Ag7D 96.4(18) . . ?
Ag9B Ag3C S6 60.2(15) . . ?
Ag9B Ag3C S7 76.4(16) . 13_666 ?
Ag9D Ag3C Ag3B 132.0(15) . . ?
Ag9D Ag3C Ag7C 121.9(14) . . ?
Ag9D Ag3C Ag7D 86.6(11) . . ?
Ag9D Ag3C S6 44.5(8) . . ?
Ag9D Ag3C S7 89.6(13) . 13_666 ?
S6 Ag3C Ag3B 153.9(13) . . ?
S6 Ag3C Ag7D 48.0(6) . . ?
S7 Ag3C Ag3B 59.8(8) 13_666 . ?
S7 Ag3C Ag7C 138.0(17) 13_666 . ?
S7 Ag3C Ag7D 164.0(14) 13_666 . ?
S7 Ag3C S6 133.1(17) 13_666 . ?
Ag3A Ag3D Ag2B 80.4(4) . 21_666 ?
Ag3A Ag3D Ag3C 175(2) . . ?
Ag3A Ag3D Ag7B 123.0(5) . . ?
Ag3A Ag3D Ag7C 99.6(5) . . ?
Ag3A Ag3D Ag8B 38.4(4) . . ?
Ag3A Ag3D Ag9A 147.1(5) . . ?
Ag3A Ag3D Ag9B 145.9(5) . . ?
Ag3A Ag3D Ag9D 28.6(4) . 17_666 ?
Ag3A Ag3D S3 76.9(4) . . ?
Ag3A Ag3D S7 90.5(4) . 13_666 ?
Ag3B Ag3D Ag2B 73.4(6) . 21_666 ?
Ag3B Ag3D Ag7B 130.8(6) . . ?
Ag3B Ag3D Ag9A 136.0(6) . . ?
Ag3B Ag3D Ag9B 135.8(6) . . ?
Ag3B Ag3D S3 78.7(5) . . ?
Ag3B Ag3D S7 80.5(6) . 13_666 ?
Ag3C Ag3D Ag2B 95.9(19) . 21_666 ?
Ag3C Ag3D Ag3B 164(2) . . ?
Ag3C Ag3D Ag7B 60.4(16) . . ?
Ag3C Ag3D Ag7C 84.6(17) . . ?
Ag3C Ag3D Ag8B 136.5(19) . . ?
Ag3C Ag3D Ag9D 152.6(16) . 17_666 ?
Ag3C Ag3D S3 103.1(16) . . ?
Ag3C Ag3D S7 85.1(17) . 13_666 ?
Ag7B Ag3D Ag2B 93.12(17) . 21_666 ?
Ag7B Ag3D Ag9D 96.2(3) . 17_666 ?
Ag7C Ag3D Ag2B 102.5(2) . 21_666 ?
Ag7C Ag3D Ag7B 26.6(2) . . ?
Ag7C Ag3D Ag8B 128.1(4) . . ?
Ag7C Ag3D Ag9A 108.6(4) . . ?
Ag7C Ag3D Ag9D 76.5(4) . 17_666 ?
Ag7C Ag3D S3 57.5(2) . . ?
Ag8B Ag3D Ag2B 53.81(17) . 21_666 ?
Ag8B Ag3D Ag7B 138.9(2) . . ?
Ag8B Ag3D Ag9A 108.7(2) . . ?
Ag8B Ag3D Ag9D 52.7(4) . 17_666 ?
Ag9A Ag3D Ag2B 77.19(18) . 21_666 ?
Ag9A Ag3D Ag7B 82.3(2) . . ?
Ag9A Ag3D Ag9D 146.6(4) . 17_666 ?
Ag9B Ag3D Ag2B 68.13(19) . 21_666 ?
Ag9B Ag3D Ag7B 73.1(2) . . ?
Ag9B Ag3D Ag7C 99.7(4) . . ?
Ag9B Ag3D Ag8B 108.6(2) . . ?
Ag9B Ag3D Ag9D 135.5(3) . 17_666 ?
Ag9B Ag3D S3 90.2(2) . . ?
Ag9B Ag3D S7 69.54(19) . 13_666 ?
Ag9D Ag3D Ag2B 69.6(4) 17_666 21_666 ?
S3 Ag3D Ag2B 47.04(16) . 21_666 ?
S3 Ag3D Ag7B 59.53(13) . . ?
S3 Ag3D Ag8B 79.4(2) . . ?
S3 Ag3D Ag9A 103.9(2) . . ?
S3 Ag3D Ag9D 49.8(3) . 17_666 ?
S7 Ag3D Ag2B 75.19(18) 13_666 21_666 ?
S7 Ag3D Ag7B 142.6(3) 13_666 . ?
S7 Ag3D Ag7C 169.2(4) 13_666 . ?
S7 Ag3D Ag8B 59.3(2) 13_666 . ?
S7 Ag3D Ag9A 60.58(17) 13_666 . ?
S7 Ag3D Ag9D 111.9(5) 13_666 17_666 ?
S7 Ag3D S3 122.0(2) 13_666 . ?
Ag4B Ag4A Ag5A 106.6(7) . . ?
Ag4B Ag4A Ag5C 90.3(6) . . ?
Ag4B Ag4A Ag6A 125.3(7) . 5 ?
Ag4B Ag4A Ag6B 135.6(6) . 5 ?
Ag4B Ag4A Ag6C 146.0(7) . 5 ?
Ag4B Ag4A S1 67.4(5) . . ?
Ag4B Ag4A S2 56.2(5) . . ?
Ag4B Ag4A S4 92.6(5) . 5 ?
Ag5A Ag4A Ag6A 109.6(5) . 9 ?
Ag5A Ag4A Ag6B 83.8(4) . 5 ?
Ag5A Ag4A S1 168.5(4) . . ?
Ag5C Ag4A Ag6B 91.7(4) . 5 ?
Ag6A Ag4A Ag5A 104.2(6) 5 . ?
Ag6A Ag4A Ag5C 94.5(5) 9 . ?
Ag6A Ag4A Ag5C 110.9(6) 5 . ?
Ag6A Ag4A Ag6A 131.5(6) 5 9 ?
Ag6A Ag4A Ag6B 20.5(3) 5 5 ?
Ag6A Ag4A Ag6B 144.7(4) 9 5 ?
Ag6A Ag4A S1 73.5(4) 5 . ?
Ag6A Ag4A S2 157.6(6) 5 . ?
Ag6A Ag4A S4 60.7(4) 5 5 ?
Ag6C Ag4A Ag5A 75.0(4) 5 . ?
Ag6C Ag4A Ag5C 85.4(5) 5 . ?
Ag6C Ag4A Ag6A 155.9(5) 5 9 ?
Ag6C Ag4A S1 104.2(5) 5 . ?
Ag6C Ag4A S2 133.2(5) 5 . ?
Ag6C Ag4A S4 56.1(3) 5 5 ?
S1 Ag4A Ag5C 152.8(5) . . ?
S1 Ag4A Ag6A 66.4(4) . 9 ?
S1 Ag4A Ag6B 93.9(3) . 5 ?
S1 Ag4A S2 120.3(4) . . ?
S2 Ag4A Ag5C 48.3(4) . . ?
S2 Ag4A Ag6A 54.5(3) . 9 ?
S2 Ag4A Ag6B 139.9(4) . 5 ?
S4 Ag4A Ag5A 66.6(3) 5 . ?
S4 Ag4A Ag5C 60.8(4) 5 . ?
S4 Ag4A Ag6A 103.0(4) 5 9 ?
S4 Ag4A Ag6B 51.3(2) 5 5 ?
S4 Ag4A S1 103.2(4) 5 . ?
S4 Ag4A S2 97.6(3) 5 . ?
Ag1B Ag4B Ag5C 61.4(4) 9 . ?
Ag1B Ag4B Ag6A 95.9(4) 9 5 ?
Ag1B Ag4B Ag10 44.0(3) 9 . ?
Ag4A Ag4B Ag1B 111.5(6) . 9 ?
Ag4A Ag4B Ag5A 52.5(6) . . ?
Ag4A Ag4B Ag5C 68.6(6) . . ?
Ag4A Ag4B Ag6A 38.0(6) . 5 ?
Ag4A Ag4B Ag6A 162.9(7) . 9 ?
Ag4A Ag4B Ag6B 157.9(6) . 9 ?
Ag4A Ag4B Ag6C 167.3(5) . 9 ?
Ag4A Ag4B Ag10 104.4(5) . . ?
Ag4A Ag4B S1 86.4(6) . . ?
Ag4A Ag4B S2 100.4(6) . . ?
Ag4A Ag4B S4 63.3(5) . 5 ?
Ag5A Ag4B Ag1B 75.7(3) . 9 ?
Ag5A Ag4B Ag5C 16.8(2) . . ?
Ag5A Ag4B Ag6A 77.2(3) . 5 ?
Ag5A Ag4B Ag10 103.73(15) . . ?
Ag5C Ag4B Ag6A 88.0(4) . 5 ?
Ag5C Ag4B Ag10 96.0(3) . . ?
Ag6A Ag4B Ag1B 84.5(5) 9 9 ?
Ag6A Ag4B Ag5A 130.9(5) 9 . ?
Ag6A Ag4B Ag5C 117.3(5) 9 . ?
Ag6A Ag4B Ag6A 150.4(5) 9 5 ?
Ag6A Ag4B Ag10 91.2(3) 9 . ?
Ag6A Ag4B S1 91.1(4) 9 . ?
Ag6A Ag4B S2 76.3(4) 9 . ?
Ag6A Ag4B S4 133.7(4) 9 5 ?
Ag6B Ag4B Ag1B 71.9(3) 9 9 ?
Ag6B Ag4B Ag5A 110.43(19) 9 . ?
Ag6B Ag4B Ag5C 96.4(3) 9 . ?
Ag6B Ag4B Ag6A 162.66(19) 9 5 ?
Ag6B Ag4B Ag10 92.91(5) 9 . ?
Ag6C Ag4B Ag1B 80.8(3) 9 9 ?
Ag6C Ag4B Ag5A 131.9(2) 9 . ?
Ag6C Ag4B Ag5C 117.4(3) 9 . ?
Ag6C Ag4B Ag6A 147.4(2) 9 5 ?
Ag6C Ag4B Ag10 86.43(12) 9 . ?
Ag10 Ag4B Ag6A 69.91(18) . 5 ?
S1 Ag4B Ag1B 118.2(3) . 9 ?
S1 Ag4B Ag5A 137.81(19) . . ?
S1 Ag4B Ag5C 150.5(3) . . ?
S1 Ag4B Ag6A 62.5(2) . 5 ?
S1 Ag4B Ag6B 111.76(7) . 9 ?
S1 Ag4B Ag6C 90.32(15) . 9 ?
S1 Ag4B Ag10 74.64(11) . . ?
S1 Ag4B S2 158.45(13) . . ?
S1 Ag4B S4 100.11(11) . 5 ?
S2 Ag4B Ag1B 78.5(3) . 9 ?
S2 Ag4B Ag5A 56.05(19) . . ?
S2 Ag4B Ag5C 48.0(3) . . ?
S2 Ag4B Ag6A 132.9(2) . 5 ?
S2 Ag4B Ag6B 58.10(9) . 9 ?
S2 Ag4B Ag6C 78.53(16) . 9 ?
S2 Ag4B Ag10 122.29(9) . . ?
S2 Ag4B S4 101.22(10) . 5 ?
S4 Ag4B Ag1B 50.6(3) 5 9 ?
S4 Ag4B Ag5A 56.09(16) 5 . ?
S4 Ag4B Ag5C 55.3(3) 5 . ?
S4 Ag4B Ag6A 48.2(3) 5 5 ?
S4 Ag4B Ag6B 122.27(8) 5 9 ?
S4 Ag4B Ag6C 129.35(13) 5 9 ?
S4 Ag4B Ag10 50.44(6) 5 . ?
Ag4A Ag5A Ag4B 20.9(3) . . ?
Ag4A Ag5A Ag6C 49.4(3) . 5 ?
Ag4A Ag5A Ag8A 101.4(4) . 13_666 ?
Ag4A Ag5A Ag9C 129.9(5) . . ?
Ag4A Ag5A S2 66.2(3) . . ?
Ag4A Ag5A S4 55.8(3) . 5 ?
Ag4A Ag5A S7 150.5(4) . . ?
Ag5B Ag5A Ag4A 112.2(5) . . ?
Ag5B Ag5A Ag4B 92.2(4) . . ?
Ag5B Ag5A Ag6C 132.1(5) . 5 ?
Ag5B Ag5A Ag8A 104.5(5) . 13_666 ?
Ag5B Ag5A Ag8C 107.0(6) . 13_666 ?
Ag5B Ag5A S2 65.3(4) . . ?
Ag5B Ag5A S4 85.7(4) . 5 ?
Ag5B Ag5A S7 61.5(4) . . ?
Ag5C Ag5A Ag4A 107.4(9) . . ?
Ag5C Ag5A Ag4B 87.6(8) . . ?
Ag5C Ag5A Ag6C 128.1(10) . 5 ?
Ag5C Ag5A Ag8A 104.7(10) . 13_666 ?
Ag5C Ag5A Ag8C 107.3(10) . 13_666 ?
Ag5C Ag5A S2 63.3(9) . . ?
Ag5C Ag5A S4 81.6(9) . 5 ?
Ag5C Ag5A S7 64.8(8) . . ?
Ag5D Ag5A Ag4A 120.6(8) . . ?
Ag5D Ag5A Ag4B 99.8(7) . . ?
Ag5D Ag5A Ag6C 145.7(8) . 5 ?
Ag5D Ag5A Ag8A 111.0(7) . 13_666 ?
Ag5D Ag5A Ag9C 11.0(7) . . ?
Ag5D Ag5A S2 64.3(7) . . ?
Ag5D Ag5A S4 99.4(8) . 5 ?
Ag5D Ag5A S7 60.3(6) . . ?
Ag6C Ag5A Ag4B 67.2(2) 5 . ?
Ag8A Ag5A Ag4B 113.7(3) 13_666 . ?
Ag8A Ag5A Ag6C 54.1(2) 13_666 5 ?
Ag8A Ag5A Ag9C 111.1(4) 13_666 . ?
Ag8A Ag5A S4 61.2(2) 13_666 5 ?
Ag8A Ag5A S7 57.2(2) 13_666 . ?
Ag8C Ag5A Ag4A 101.5(6) 13_666 . ?
Ag8C Ag5A Ag4B 114.6(5) 13_666 . ?
Ag8C Ag5A Ag5D 113.2(8) 13_666 . ?
Ag8C Ag5A Ag6C 53.5(4) 13_666 5 ?
Ag8C Ag5A Ag9C 112.9(5) 13_666 . ?
Ag8C Ag5A S2 158.6(5) 13_666 . ?
Ag8C Ag5A S4 63.1(4) 13_666 5 ?
Ag8C Ag5A S7 58.2(4) 13_666 . ?
Ag9C Ag5A Ag4B 109.0(3) . . ?
Ag9C Ag5A Ag6C 154.6(4) . 5 ?
S2 Ag5A Ag4B 48.80(14) . . ?
S2 Ag5A Ag6C 115.5(3) . 5 ?
S2 Ag5A Ag8A 156.3(3) . 13_666 ?
S2 Ag5A Ag9C 68.9(3) . . ?
S2 Ag5A S4 95.8(2) . 5 ?
S2 Ag5A S7 124.5(4) . . ?
S4 Ag5A Ag4B 56.76(15) 5 . ?
S4 Ag5A Ag6C 46.53(19) 5 5 ?
S4 Ag5A Ag9C 109.4(4) 5 . ?
S7 Ag5A Ag4B 143.9(3) . . ?
S7 Ag5A Ag6C 111.0(3) . 5 ?
S7 Ag5A Ag9C 56.2(3) . . ?
S7 Ag5A S4 94.7(2) . 5 ?
Ag1B Ag5B Ag2A 42.9(3) 9 9 ?
Ag1B Ag5B Ag7B 66.9(3) 9 9 ?
Ag2A Ag5B Ag7B 95.48(12) 9 9 ?
Ag5A Ag5B Ag1B 110.1(5) . 9 ?
Ag5A Ag5B Ag2A 108.7(5) . 9 ?
Ag5A Ag5B Ag7B 139.4(5) . 9 ?
Ag5A Ag5B Ag7C 152.8(5) . 9 ?
Ag5A Ag5B Ag8C 43.8(5) . 13_666 ?
Ag5A Ag5B Ag9C 135.6(6) . . ?
Ag5A Ag5B S2 81.4(4) . . ?
Ag5A Ag5B S3 155.0(5) . 9 ?
Ag5A Ag5B S7 86.2(4) . . ?
Ag5C Ag5B Ag1B 102.2(18) . 9 ?
Ag5C Ag5B Ag2A 104(2) . 9 ?
Ag5C Ag5B Ag5D 146(3) . . ?
Ag5C Ag5B Ag7B 135.6(19) . 9 ?
Ag5C Ag5B Ag7C 153(2) . 9 ?
Ag5C Ag5B Ag8C 45.0(19) . 13_666 ?
Ag5C Ag5B Ag9C 143(2) . . ?
Ag5C Ag5B S2 78.0(19) . . ?
Ag5C Ag5B S3 148(2) . 9 ?
Ag5C Ag5B S7 91.6(18) . . ?
Ag5D Ag5B Ag1B 107.8(17) . 9 ?
Ag5D Ag5B Ag2A 108.6(17) . 9 ?
Ag5D Ag5B Ag5A 139.5(18) . . ?
Ag5D Ag5B Ag7B 49.9(16) . 9 ?
Ag5D Ag5B Ag8C 139.9(16) . 13_666 ?
Ag5D Ag5B S2 91.7(16) . . ?
Ag5D Ag5B S3 65.5(17) . 9 ?
Ag5D Ag5B S7 87.3(16) . . ?
Ag7C Ag5B Ag1B 81.5(4) 9 9 ?
Ag7C Ag5B Ag2A 96.58(19) 9 9 ?
Ag7C Ag5B Ag7B 22.85(19) 9 9 ?
Ag8C Ag5B Ag1B 99.5(4) 13_666 9 ?
Ag8C Ag5B Ag2A 73.0(3) 13_666 9 ?
Ag8C Ag5B Ag7B 166.5(3) 13_666 9 ?
Ag8C Ag5B Ag7C 161.5(4) 13_666 9 ?
Ag9C Ag5B Ag1B 113.6(5) . 9 ?
Ag9C Ag5B Ag2A 108.4(4) . 9 ?
Ag9C Ag5B Ag7B 58.1(4) . 9 ?
Ag9C Ag5B Ag7C 36.2(4) . 9 ?
Ag9C Ag5B Ag8C 131.7(5) . 13_666 ?
Ag9C Ag5B S2 98.5(5) . . ?
Ag9C Ag5B S3 68.9(4) . 9 ?
Ag9C Ag5B S7 79.3(4) . . ?
S2 Ag5B Ag1B 79.9(3) . 9 ?
S2 Ag5B Ag2A 122.52(16) . 9 ?
S2 Ag5B Ag7B 57.97(14) . 9 ?
S2 Ag5B Ag7C 76.5(2) . 9 ?
S2 Ag5B Ag8C 122.0(3) . 13_666 ?
S2 Ag5B S3 102.26(16) . 9 ?
S3 Ag5B Ag1B 47.7(3) 9 9 ?
S3 Ag5B Ag2A 48.35(10) 9 9 ?
S3 Ag5B Ag7B 51.06(12) 9 9 ?
S3 Ag5B Ag7C 48.24(17) 9 9 ?
S3 Ag5B Ag8C 119.9(3) 9 13_666 ?
S7 Ag5B Ag1B 119.7(4) . 9 ?
S7 Ag5B Ag2A 76.74(16) . 9 ?
S7 Ag5B Ag7B 131.97(18) . 9 ?
S7 Ag5B Ag7C 109.9(2) . 9 ?
S7 Ag5B Ag8C 53.4(3) . 13_666 ?
S7 Ag5B S2 159.7(2) . . ?
S7 Ag5B S3 95.78(17) . 9 ?
Ag4A Ag5C Ag1B 74.1(4) . 9 ?
Ag4A Ag5C Ag4B 21.1(2) . . ?
Ag4A Ag5C Ag8A 84.9(5) . 13_666 ?
Ag4B Ag5C Ag1B 59.2(4) . 9 ?
Ag5A Ag5C Ag1B 124.6(11) . 9 ?
Ag5A Ag5C Ag4A 55.4(8) . . ?
Ag5A Ag5C Ag4B 75.6(8) . . ?
Ag5A Ag5C Ag5D 149.1(19) . . ?
Ag5A Ag5C Ag8A 58.4(9) . 13_666 ?
Ag5A Ag5C Ag8C 52.3(9) . 13_666 ?
Ag5A Ag5C Ag9C 139.7(12) . . ?
Ag5A Ag5C S2 96.6(10) . . ?
Ag5A Ag5C S4 79.4(9) . 5 ?
Ag5A Ag5C S7 95.7(9) . . ?
Ag5B Ag5C Ag1B 68.1(17) . 9 ?
Ag5B Ag5C Ag4A 137.0(18) . . ?
Ag5B Ag5C Ag4B 116.3(18) . . ?
Ag5B Ag5C Ag5A 167(2) . . ?
Ag5B Ag5C Ag8A 120(2) . 13_666 ?
Ag5B Ag5C Ag8C 126(2) . 13_666 ?
Ag5B Ag5C S2 88.6(19) . . ?
Ag5B Ag5C S4 111(2) . 5 ?
Ag5B Ag5C S7 75.5(17) . . ?
Ag5D Ag5C Ag1B 85.7(14) . 9 ?
Ag5D Ag5C Ag4A 144.0(15) . . ?
Ag5D Ag5C Ag4B 123.5(14) . . ?
Ag5D Ag5C Ag8A 128.4(14) . 13_666 ?
Ag5D Ag5C Ag8C 132.6(15) . 13_666 ?
Ag5D Ag5C S2 83.7(14) . . ?
Ag5D Ag5C S4 130.9(15) . 5 ?
Ag5D Ag5C S7 75.5(13) . . ?
Ag8A Ag5C Ag1B 99.5(5) 13_666 9 ?
Ag8A Ag5C Ag4B 101.8(4) 13_666 . ?
Ag8C Ag5C Ag1B 103.7(6) 13_666 9 ?
Ag8C Ag5C Ag4A 81.9(6) 13_666 . ?
Ag8C Ag5C Ag4B 100.0(5) 13_666 . ?
Ag8C Ag5C S4 58.6(4) 13_666 5 ?
Ag9C Ag5C Ag1B 95.5(6) . 9 ?
Ag9C Ag5C Ag4A 150.7(7) . . ?
Ag9C Ag5C Ag4B 131.4(7) . . ?
Ag9C Ag5C Ag8A 124.2(6) . 13_666 ?
Ag9C Ag5C Ag8C 127.5(7) . 13_666 ?
Ag9C Ag5C S2 88.0(6) . . ?
Ag9C Ag5C S4 138.9(7) . 5 ?
Ag9C Ag5C S7 69.8(5) . . ?
S2 Ag5C Ag1B 77.2(5) . 9 ?
S2 Ag5C Ag4A 63.2(4) . . ?
S2 Ag5C Ag4B 48.6(2) . . ?
S2 Ag5C Ag8A 147.7(6) . 13_666 ?
S2 Ag5C Ag8C 143.6(7) . 13_666 ?
S2 Ag5C S4 101.9(4) . 5 ?
S2 Ag5C S7 156.4(7) . . ?
S4 Ag5C Ag1B 49.8(4) 5 9 ?
S4 Ag5C Ag4A 51.4(3) 5 . ?
S4 Ag5C Ag4B 55.4(2) 5 . ?
S4 Ag5C Ag8A 56.6(3) 5 13_666 ?
S7 Ag5C Ag1B 111.5(6) . 9 ?
S7 Ag5C Ag4A 139.5(7) . . ?
S7 Ag5C Ag4B 154.8(6) . . ?
S7 Ag5C Ag8A 54.7(3) . 13_666 ?
S7 Ag5C Ag8C 57.7(4) . 13_666 ?
S7 Ag5C S4 100.1(5) . 5 ?
Ag5A Ag5D Ag7B 129.6(12) . 9 ?
Ag5A Ag5D Ag7C 154.7(12) . 9 ?
Ag5A Ag5D Ag7D 115.9(11) . 9 ?
Ag5A Ag5D Ag9A 123.8(10) . 13_666 ?
Ag5A Ag5D S2 68.0(9) . . ?
Ag5A Ag5D S3 126.0(14) . 9 ?
Ag5A Ag5D S7 72.4(8) . . ?
Ag5B Ag5D Ag5A 26.9(13) . . ?
Ag5B Ag5D Ag5C 14.2(12) . . ?
Ag5B Ag5D Ag7B 118(2) . 9 ?
Ag5B Ag5D Ag7C 142(2) . 9 ?
Ag5B Ag5D Ag7D 108.8(19) . 9 ?
Ag5B Ag5D Ag9A 113.5(19) . 13_666 ?
Ag5B Ag5D Ag9C 165(3) . . ?
Ag5B Ag5D S2 70.9(17) . . ?
Ag5B Ag5D S3 99(2) . 9 ?
Ag5B Ag5D S7 74.9(16) . . ?
Ag5C Ag5D Ag5A 12.9(8) . . ?
Ag5C Ag5D Ag7B 123.3(17) . 9 ?
Ag5C Ag5D Ag7C 149.3(18) . 9 ?
Ag5C Ag5D Ag7D 111.3(16) . 9 ?
Ag5C Ag5D Ag9A 121.4(16) . 13_666 ?
Ag5C Ag5D S2 66.9(14) . . ?
Ag5C Ag5D S3 113.3(18) . 9 ?
Ag5C Ag5D S7 75.0(14) . . ?
Ag7B Ag5D Ag9A 101.2(9) 9 13_666 ?
Ag7C Ag5D Ag7D 38.9(5) 9 9 ?
Ag7C Ag5D Ag9A 80.4(9) 9 13_666 ?
Ag7C Ag5D S2 86.8(8) 9 . ?
Ag7C Ag5D S3 56.9(6) 9 9 ?
Ag7C Ag5D S7 132.9(13) 9 . ?
Ag7D Ag5D Ag9A 115.9(10) 9 13_666 ?
Ag9C Ag5D Ag5A 145(2) . . ?
Ag9C Ag5D Ag5C 157(3) . . ?
Ag9C Ag5D Ag7B 76.4(17) . 9 ?
Ag9C Ag5D Ag7C 51.5(15) . 9 ?
Ag9C Ag5D Ag7D 85.9(17) . 9 ?
Ag9C Ag5D Ag9A 58.3(14) . 13_666 ?
Ag9C Ag5D S2 120.8(19) . . ?
Ag9C Ag5D S3 86.7(18) . 9 ?
Ag9C Ag5D S7 90.9(15) . . ?
S2 Ag5D Ag7B 63.6(5) . 9 ?
S2 Ag5D Ag7D 49.0(5) . 9 ?
S2 Ag5D Ag9A 163.0(9) . 13_666 ?
S2 Ag5D S3 104.9(8) . 9 ?
S3 Ag5D Ag7B 58.2(5) 9 9 ?
S3 Ag5D Ag7D 69.3(7) 9 9 ?
S3 Ag5D Ag9A 58.6(5) 9 13_666 ?
S7 Ag5D Ag7B 154.5(12) . 9 ?
S7 Ag5D Ag7D 168.6(11) . 9 ?
S7 Ag5D Ag9A 53.6(5) . 13_666 ?
S7 Ag5D S2 140.4(14) . . ?
S7 Ag5D S3 99.7(8) . 9 ?
Ag4A Ag6A Ag1A 105.4(4) 9 . ?
Ag4A Ag6A Ag1A 87.5(3) 5 . ?
Ag4A Ag6A Ag4A 105.8(6) 9 5 ?
Ag4A Ag6A Ag4B 16.7(2) 9 9 ?
Ag4A Ag6A Ag4B 91.7(4) 5 9 ?
Ag4A Ag6A Ag7A 108.8(4) 5 . ?
Ag4A Ag6A Ag7A 144.7(6) 9 . ?
Ag4A Ag6A Ag8D 92.8(7) 9 21_666 ?
Ag4A Ag6A S2 166.7(6) 9 5 ?
Ag4A Ag6A S4 60.6(3) 9 . ?
Ag4B Ag6A Ag1A 81.5(4) 5 . ?
Ag4B Ag6A Ag1A 96.2(3) 9 . ?
Ag4B Ag6A Ag4A 104.6(6) 5 9 ?
Ag4B Ag6A Ag4B 89.6(5) 5 9 ?
Ag4B Ag6A Ag7A 108.8(5) 5 . ?
Ag4B Ag6A Ag8D 140.6(8) 5 21_666 ?
Ag4B Ag6A S2 62.3(3) 5 5 ?
Ag4B Ag6A S4 103.3(4) 5 . ?
Ag6B Ag6A Ag1A 64.7(5) . . ?
Ag6B Ag6A Ag4A 131.8(7) . 5 ?
Ag6B Ag6A Ag4A 118.8(7) . 9 ?
Ag6B Ag6A Ag4B 129.9(8) . 5 ?
Ag6B Ag6A Ag4B 127.9(7) . 9 ?
Ag6B Ag6A Ag7A 26.2(3) . . ?
Ag6B Ag6A Ag8D 27.7(6) . 21_666 ?
Ag6B Ag6A S2 72.5(5) . 5 ?
Ag6B Ag6A S4 79.7(6) . . ?
Ag6C Ag6A Ag1A 90.1(7) . . ?
Ag6C Ag6A Ag4A 70.1(6) . 9 ?
Ag6C Ag6A Ag4A 174.5(8) . 5 ?
Ag6C Ag6A Ag4B 168.6(8) . 5 ?
Ag6C Ag6A Ag4B 83.6(6) . 9 ?
Ag6C Ag6A Ag6B 50.9(6) . . ?
Ag6C Ag6A Ag7A 75.0(7) . . ?
Ag6C Ag6A Ag8D 33.5(7) . 21_666 ?
Ag6C Ag6A S2 122.5(9) . 5 ?
Ag6C Ag6A S4 65.2(5) . . ?
Ag7A Ag6A Ag1A 69.2(3) . . ?
Ag7A Ag6A Ag4B 153.7(5) . 9 ?
Ag8D Ag6A Ag1A 59.7(5) 21_666 . ?
Ag8D Ag6A Ag4A 145.9(7) 21_666 5 ?
Ag8D Ag6A Ag4B 100.3(6) 21_666 9 ?
Ag8D Ag6A Ag7A 53.5(6) 21_666 . ?
S2 Ag6A Ag1A 72.3(3) 5 . ?
S2 Ag6A Ag4A 61.4(3) 5 5 ?
S2 Ag6A Ag4B 150.5(4) 5 9 ?
S2 Ag6A Ag7A 47.5(3) 5 . ?
S2 Ag6A Ag8D 96.9(7) 5 21_666 ?
S4 Ag6A Ag1A 46.3(2) . . ?
S4 Ag6A Ag4A 109.7(4) . 5 ?
S4 Ag6A Ag4B 56.3(2) . 9 ?
S4 Ag6A Ag7A 100.1(5) . . ?
S4 Ag6A Ag8D 55.4(5) . 21_666 ?
S4 Ag6A S2 118.7(5) . 5 ?
Ag1A Ag6B Ag7B 55.74(7) . . ?
Ag4B Ag6B Ag1A 74.12(6) 5 . ?
Ag4B Ag6B Ag7B 98.80(8) 5 . ?
Ag4B Ag6B Ag8C 130.9(3) 5 21_666 ?
Ag6A Ag6B Ag1A 91.5(5) . . ?
Ag6A Ag6B Ag7A 137.7(5) . . ?
Ag6A Ag6B Ag7B 127.7(5) . . ?
Ag6A Ag6B Ag7D 129.4(6) . . ?
Ag6A Ag6B Ag8A 122.4(5) . 21_666 ?
Ag6A Ag6B Ag8C 111.0(6) . 21_666 ?
Ag6A Ag6B Ag8D 130.5(9) . 21_666 ?
Ag6A Ag6B S2 78.1(5) . 5 ?
Ag6A Ag6B S4 70.5(5) . . ?
Ag6C Ag6B Ag1A 110.8(3) . . ?
Ag6C Ag6B Ag4B 91.2(4) . 5 ?
Ag6C Ag6B Ag6A 63.0(6) . . ?
Ag6C Ag6B Ag7A 150.7(4) . . ?
Ag6C Ag6B Ag7B 159.3(4) . . ?
Ag6C Ag6B Ag7D 165.2(6) . . ?
Ag6C Ag6B Ag8A 66.8(4) . 21_666 ?
Ag6C Ag6B Ag8C 54.5(4) . 21_666 ?
Ag6C Ag6B Ag8D 77.1(9) . 21_666 ?
Ag6C Ag6B S2 139.6(4) . 5 ?
Ag6C Ag6B S4 60.8(3) . . ?
Ag7A Ag6B Ag1A 91.6(2) . . ?
Ag7A Ag6B Ag4B 113.63(17) . 5 ?
Ag7A Ag6B Ag8A 99.80(19) . 21_666 ?
Ag7A Ag6B Ag8C 111.3(3) . 21_666 ?
Ag7A Ag6B S2 61.22(17) . 5 ?
Ag7A Ag6B S4 137.4(2) . . ?
Ag7D Ag6B Ag1A 64.4(5) . . ?
Ag7D Ag6B Ag4B 100.4(4) . 5 ?
Ag7D Ag6B Ag8A 98.4(4) . 21_666 ?
Ag7D Ag6B Ag8C 110.7(5) . 21_666 ?
Ag7D Ag6B S4 112.7(5) . . ?
Ag8A Ag6B Ag1A 81.35(10) 21_666 . ?
Ag8A Ag6B Ag4B 138.50(11) 21_666 5 ?
Ag8A Ag6B Ag7B 94.17(13) 21_666 . ?
Ag8C Ag6B Ag1A 86.0(3) 21_666 . ?
Ag8C Ag6B Ag7B 106.2(3) 21_666 . ?
Ag8D Ag6B Ag1A 75.9(8) 21_666 . ?
Ag8D Ag6B Ag4B 141.2(7) 21_666 5 ?
Ag8D Ag6B Ag7A 91.1(8) 21_666 . ?
Ag8D Ag6B Ag7B 83.8(8) 21_666 . ?
Ag8D Ag6B Ag7D 88.1(9) 21_666 . ?
Ag8D Ag6B S2 141.7(8) 21_666 5 ?
Ag8D Ag6B S4 64.8(7) 21_666 . ?
S2 Ag6B Ag1A 78.86(8) 5 . ?
S2 Ag6B Ag4B 52.50(9) 5 5 ?
S2 Ag6B Ag7B 58.08(11) 5 . ?
S2 Ag6B Ag7D 54.9(4) 5 . ?
S2 Ag6B Ag8A 151.87(16) 5 21_666 ?
S2 Ag6B Ag8C 162.6(3) 5 21_666 ?
S2 Ag6B S4 117.05(11) 5 . ?
S4 Ag6B Ag1A 50.08(7) . . ?
S4 Ag6B Ag4B 77.17(9) . 5 ?
S4 Ag6B Ag7B 103.75(10) . . ?
S4 Ag6B Ag8A 61.46(11) . 21_666 ?
S4 Ag6B Ag8C 56.3(3) . 21_666 ?
Ag4A Ag6C Ag4B 76.1(3) 9 5 ?
Ag4A Ag6C Ag5A 55.5(3) 9 9 ?
Ag4A Ag6C Ag7A 159.9(4) 9 . ?
Ag4A Ag6C Ag8A 110.2(4) 9 21_666 ?
Ag4A Ag6C Ag8B 109.8(4) 9 21_666 ?
Ag4A Ag6C Ag8C 98.0(5) 9 21_666 ?
Ag4B Ag6C Ag7A 84.0(2) 5 . ?
Ag4B Ag6C Ag8B 125.1(2) 5 21_666 ?
Ag5A Ag6C Ag4B 125.6(3) 9 5 ?
Ag5A Ag6C Ag7A 139.7(3) 9 . ?
Ag5A Ag6C Ag8B 61.9(2) 9 21_666 ?
Ag6A Ag6C Ag4A 78.9(7) . 9 ?
Ag6A Ag6C Ag5A 130.7(7) . 9 ?
Ag6A Ag6C Ag7A 81.6(7) . . ?
Ag6A Ag6C Ag8A 142.9(7) . 21_666 ?
Ag6A Ag6C Ag8B 130.1(7) . 21_666 ?
Ag6A Ag6C Ag8C 149.1(7) . 21_666 ?
Ag6A Ag6C Ag8D 122.9(11) . 21_666 ?
Ag6A Ag6C S4 84.0(5) . . ?
Ag6B Ag6C Ag4A 141.3(5) . 9 ?
Ag6B Ag6C Ag4B 67.3(3) . 5 ?
Ag6B Ag6C Ag5A 143.4(5) . 9 ?
Ag6B Ag6C Ag6A 66.1(7) . . ?
Ag6B Ag6C Ag8A 89.8(4) . 21_666 ?
Ag6B Ag6C Ag8B 82.6(4) . 21_666 ?
Ag6B Ag6C Ag8C 103.4(5) . 21_666 ?
Ag6B Ag6C Ag8D 64.9(9) . 21_666 ?
Ag6B Ag6C S4 93.9(4) . . ?
Ag7A Ag6C Ag8B 79.1(2) . 21_666 ?
Ag8A Ag6C Ag4B 137.9(2) 21_666 5 ?
Ag8A Ag6C Ag5A 57.2(2) 21_666 9 ?
Ag8A Ag6C Ag7A 82.5(2) 21_666 . ?
Ag8C Ag6C Ag4B 142.9(4) 21_666 5 ?
Ag8C Ag6C Ag5A 43.8(3) 21_666 9 ?
Ag8C Ag6C Ag7A 95.9(4) 21_666 . ?
Ag8D Ag6C Ag4A 129.3(9) 21_666 9 ?
Ag8D Ag6C Ag4B 120.0(8) 21_666 5 ?
Ag6B Ag7A Ag6A 16.1(2) . . ?
Ag6B Ag7A Ag6C 10.10(14) . . ?
Ag6B Ag7A Ag7C 115.2(3) . . ?
Ag6B Ag7A S2 68.84(18) . 5 ?
Ag6B Ag7A S6 86.5(2) . . ?
# SQUEEZE RESULTS (APPEND TO CIF)
# Note: Data are Listed for all Voids in the P1 Unit Cell
# i.e. Centre of Gravity, Solvent Accessible Volume,
# Recovered number of Electrons in the Void and
# Details about the Squeezed Material
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 0.000 -0.009 0.002 9009 2317 ' '
_platon_squeeze_details          
;
;


data_Ag20
_database_code_depnum_ccdc_archive 'CCDC 913216'
#TrackingRef 'web_deposit_cif_file_0_DiSun_1362289851.Ag56 and Ag20-Revised.cif'
_audit_creation_method           SHELXL-97
_chemical_name_systematic        
;
?
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C69 H142 Ag20 N4 O23 S10'
_chemical_formula_weight         3873.97
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   p2(1)/n
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
_cell_length_a                   11.887(2)
_cell_length_b                   19.864(4)
_cell_length_c                   25.881(5)
_cell_angle_alpha                90.00
_cell_angle_beta                 91.49(3)
_cell_angle_gamma                90.00
_cell_volume                     6109(2)
_cell_formula_units_Z            2
_cell_measurement_temperature    173(2)
_cell_measurement_reflns_used    35407
_cell_measurement_theta_min      6.12
_cell_measurement_theta_max      54.93
_exptl_crystal_description       Block
_exptl_crystal_colour            Colorless
_exptl_crystal_size_max          0.15
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.10
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    2.106
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             3736
_exptl_absorpt_coefficient_mu    3.347
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.6337
_exptl_absorpt_correction_T_max  0.7308
_exptl_absorpt_process_details   sadabs
_exptl_special_details           
;
?
;
_diffrn_ambient_temperature      173(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'Bruker SMART APEX II CCD area detector'
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            38879
_diffrn_reflns_av_R_equivalents  0.0577
_diffrn_reflns_av_unetI/netI     0.0560
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_theta_min         3.06
_diffrn_reflns_theta_max         25.00
_reflns_number_total             10716
_reflns_number_gt                9128
_reflns_threshold_expression     >2sigma(I)
_computing_data_collection       'APEX2 (Bruker, 2008)'
_computing_cell_refinement       'SAINT+ ver. (Bruker, 2001)'
_computing_data_reduction        'SAINT+ ver. (Bruker, 2001)'
_computing_structure_solution    'SHELXTL (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXTL (Sheldrick, 2008)'
_computing_molecular_graphics    'SHELXTL (Sheldrick, 2008)'
_computing_publication_material  'SHELXTL (Sheldrick, 2008)'
_refine_special_details          
;
Refinement of F^2^ against ALL reflections. The weighted R-factor wR and
goodness of fit S are based on F^2^, conventional R-factors R are based
on F, with F set to zero for negative F^2^. The threshold expression of
F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is
not relevant to the choice of reflections for refinement. R-factors based
on F^2^ are statistically about twice as large as those based on F, and R-
factors based on ALL data will be even larger.
Due to relatively large thermal motion of the tert-butyl groups,
the Ueq of C atoms on this tert-butyl group were
restrained by using the command SIMU. The Ag9 atom was disordered and
refined with splitting mode. The occupancy factor of the
disordered Ag atoms is Ag9:Ag9' 0.70:0.30.
;
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[\s^2^(Fo^2^)+(0.0504P)^2^+39.0902P] where P=(Fo^2^+2Fc^2^)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         10716
_refine_ls_number_parameters     628
_refine_ls_number_restraints     24
_refine_ls_R_factor_all          0.0560
_refine_ls_R_factor_gt           0.0485
_refine_ls_wR_factor_ref         0.1223
_refine_ls_wR_factor_gt          0.1179
_refine_ls_goodness_of_fit_ref   1.015
_refine_ls_restrained_S_all      1.015
_refine_ls_shift/su_max          0.012
_refine_ls_shift/su_mean         0.000
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.83952(5) 0.10141(3) 0.56307(2) 0.03625(14) Uani 1 1 d . . .
Ag2 Ag 0.98213(5) 0.14140(3) 0.66533(2) 0.04051(15) Uani 1 1 d . . .
Ag3 Ag 1.13206(5) 0.03422(3) 0.61239(2) 0.03600(14) Uani 1 1 d . . .
Ag4 Ag 0.98119(5) 0.23504(3) 0.57909(2) 0.04267(16) Uani 1 1 d . . .
Ag5 Ag 1.01102(5) -0.25624(3) 0.55253(2) 0.03914(15) Uani 1 1 d . . .
Ag6 Ag 0.98166(5) -0.02818(3) 0.69779(2) 0.03856(15) Uani 1 1 d . . .
Ag7 Ag 1.01406(6) -0.17665(3) 0.65076(2) 0.04555(16) Uani 1 1 d . . .
Ag8 Ag 1.14173(5) 0.14861(3) 0.50899(2) 0.04300(16) Uani 1 1 d . . .
Ag9 Ag 0.8501(2) 0.12168(11) 0.43859(10) 0.0348(4) Uani 0.70 1 d P . .
Ag9' Ag 0.8253(5) 0.1023(3) 0.4437(2) 0.0536(13) Uani 0.30 1 d P . .
Ag10 Ag 0.84190(6) -0.05355(3) 0.59585(3) 0.04974(18) Uani 1 1 d . . .
S1 S 0.84889(14) 0.20576(9) 0.50679(6) 0.0298(4) Uani 1 1 d . . .
S2 S 0.84449(14) 0.04856(8) 0.65035(6) 0.0287(3) Uani 1 1 d . . .
S3 S 0.85555(14) -0.17697(9) 0.58229(6) 0.0313(4) Uani 1 1 d . . .
S4 S 1.14603(14) 0.15570(8) 0.60277(6) 0.0284(3) Uani 1 1 d . . .
S5 S 1.14939(14) -0.07755(8) 0.65058(6) 0.0285(3) Uani 1 1 d . . .
C1 C 0.7183(6) 0.2568(4) 0.5086(3) 0.0360(16) Uani 1 1 d . . .
C2 C 0.6553(9) 0.2377(6) 0.5569(5) 0.086(4) Uani 1 1 d . . .
H2A H 0.5868 0.2649 0.5590 0.129 Uiso 1 1 calc R . .
H2B H 0.7035 0.2459 0.5876 0.129 Uiso 1 1 calc R . .
H2C H 0.6350 0.1899 0.5554 0.129 Uiso 1 1 calc R . .
C3 C 0.6474(9) 0.2412(5) 0.4615(4) 0.072(3) Uani 1 1 d . . .
H3A H 0.5739 0.2631 0.4643 0.108 Uiso 1 1 calc R . .
H3B H 0.6370 0.1924 0.4587 0.108 Uiso 1 1 calc R . .
H3C H 0.6849 0.2579 0.4308 0.108 Uiso 1 1 calc R . .
C4 C 0.7524(8) 0.3303(4) 0.5099(4) 0.057(2) Uani 1 1 d . . .
H4A H 0.6849 0.3586 0.5105 0.086 Uiso 1 1 calc R . .
H4B H 0.7953 0.3409 0.4790 0.086 Uiso 1 1 calc R . .
H4C H 0.7992 0.3390 0.5409 0.086 Uiso 1 1 calc R . .
C5 C 0.7136(6) 0.0609(4) 0.6871(3) 0.0413(18) Uani 1 1 d . . .
C6 C 0.705(3) 0.0092(19) 0.7241(13) 0.077(9) Uani 0.50 1 d PU . .
H6A H 0.6374 0.0150 0.7434 0.116 Uiso 0.50 1 d PR . .
H6B H 0.7018 -0.0334 0.7066 0.116 Uiso 0.50 1 d PR . .
H6C H 0.7690 0.0104 0.7472 0.116 Uiso 0.50 1 d PR . .
C6' C 0.668(3) -0.0065(17) 0.7016(14) 0.078(9) Uani 0.50 1 d PU . .
H6'A H 0.6007 -0.0020 0.7208 0.118 Uiso 0.50 1 d PR . .
H6'B H 0.6532 -0.0330 0.6712 0.118 Uiso 0.50 1 d PR . .
H6'C H 0.7251 -0.0283 0.7227 0.118 Uiso 0.50 1 d PR . .
C7 C 0.6379(19) 0.1090(14) 0.6610(10) 0.083(6) Uani 0.50 1 d PU . .
H7A H 0.5709 0.1149 0.6804 0.125 Uiso 0.50 1 d PR . .
H7B H 0.6763 0.1513 0.6583 0.125 Uiso 0.50 1 d PR . .
H7C H 0.6181 0.0928 0.6270 0.125 Uiso 0.50 1 d PR . .
C7' C 0.6153(16) 0.0508(14) 0.6433(8) 0.074(6) Uani 0.50 1 d PU . .
H7'A H 0.5431 0.0564 0.6585 0.111 Uiso 0.50 1 d PR . .
H7'B H 0.6249 0.0843 0.6171 0.111 Uiso 0.50 1 d PR . .
H7'C H 0.6198 0.0068 0.6282 0.111 Uiso 0.50 1 d PR . .
C8 C 0.752(2) 0.0957(15) 0.7409(8) 0.087(7) Uani 0.50 1 d PU . .
H8A H 0.6871 0.1034 0.7617 0.130 Uiso 0.50 1 d PR . .
H8B H 0.8039 0.0670 0.7593 0.130 Uiso 0.50 1 d PR . .
H8C H 0.7870 0.1378 0.7335 0.130 Uiso 0.50 1 d PR . .
C8' C 0.709(2) 0.1287(12) 0.7055(10) 0.080(6) Uani 0.50 1 d PU . .
H8'A H 0.6415 0.1354 0.7245 0.120 Uiso 0.50 1 d PR . .
H8'B H 0.7734 0.1379 0.7274 0.120 Uiso 0.50 1 d PR . .
H8'C H 0.7087 0.1586 0.6763 0.120 Uiso 0.50 1 d PR . .
C9 C 0.7295(6) -0.2257(4) 0.6022(3) 0.0372(17) Uani 1 1 d . . .
C10 C 0.7608(10) -0.2655(7) 0.6505(5) 0.100(5) Uani 1 1 d . . .
H10A H 0.6987 -0.2957 0.6590 0.150 Uiso 1 1 calc R . .
H10B H 0.7753 -0.2344 0.6793 0.150 Uiso 1 1 calc R . .
H10C H 0.8286 -0.2921 0.6444 0.150 Uiso 1 1 calc R . .
C11 C 0.6948(10) -0.2727(6) 0.5590(4) 0.077(3) Uani 1 1 d . . .
H11A H 0.6242 -0.2951 0.5676 0.115 Uiso 1 1 calc R . .
H11B H 0.7536 -0.3066 0.5544 0.115 Uiso 1 1 calc R . .
H11C H 0.6840 -0.2470 0.5269 0.115 Uiso 1 1 calc R . .
C12 C 0.6365(8) -0.1765(5) 0.6125(5) 0.082(4) Uani 1 1 d . . .
H12A H 0.5693 -0.2010 0.6229 0.122 Uiso 1 1 calc R . .
H12B H 0.6190 -0.1507 0.5810 0.122 Uiso 1 1 calc R . .
H12C H 0.6606 -0.1457 0.6402 0.122 Uiso 1 1 calc R . .
C13 C 1.2661(6) 0.2010(4) 0.6344(3) 0.0356(16) Uani 1 1 d . . .
C14 C 1.2758(14) 0.1760(9) 0.6891(5) 0.142(8) Uani 1 1 d . . .
H14A H 1.3387 0.1988 0.7070 0.213 Uiso 1 1 calc R . .
H14B H 1.2892 0.1274 0.6890 0.213 Uiso 1 1 calc R . .
H14C H 1.2058 0.1857 0.7069 0.213 Uiso 1 1 calc R . .
C15 C 1.3691(8) 0.1865(9) 0.6054(6) 0.125(7) Uani 1 1 d . . .
H15A H 1.4332 0.2099 0.6217 0.188 Uiso 1 1 calc R . .
H15B H 1.3589 0.2020 0.5696 0.188 Uiso 1 1 calc R . .
H15C H 1.3833 0.1379 0.6056 0.188 Uiso 1 1 calc R . .
C16 C 1.2400(10) 0.2739(6) 0.6339(6) 0.102(5) Uani 1 1 d . . .
H16A H 1.3024 0.2988 0.6503 0.154 Uiso 1 1 calc R . .
H16B H 1.1710 0.2819 0.6528 0.154 Uiso 1 1 calc R . .
H16C H 1.2293 0.2892 0.5981 0.154 Uiso 1 1 calc R . .
C17 C 1.2767(6) -0.0931(4) 0.6930(3) 0.0331(15) Uani 1 1 d . . .
C18 C 1.2437(10) -0.1355(8) 0.7357(5) 0.106(5) Uani 1 1 d . . .
H18A H 1.3093 -0.1443 0.7584 0.158 Uiso 1 1 calc R . .
H18B H 1.2138 -0.1782 0.7222 0.158 Uiso 1 1 calc R . .
H18C H 1.1856 -0.1126 0.7553 0.158 Uiso 1 1 calc R . .
C19 C 1.3646(9) -0.1234(8) 0.6601(4) 0.107(5) Uani 1 1 d . . .
H19A H 1.4327 -0.1321 0.6812 0.160 Uiso 1 1 calc R . .
H19B H 1.3823 -0.0922 0.6321 0.160 Uiso 1 1 calc R . .
H19C H 1.3366 -0.1658 0.6453 0.160 Uiso 1 1 calc R . .
C20 C 1.3205(10) -0.0255(6) 0.7132(5) 0.087(4) Uani 1 1 d . . .
H20A H 1.3873 -0.0328 0.7354 0.130 Uiso 1 1 calc R . .
H20B H 1.2620 -0.0034 0.7332 0.130 Uiso 1 1 calc R . .
H20C H 1.3401 0.0033 0.6840 0.130 Uiso 1 1 calc R . .
C21 C 1.0675(7) -0.3348(4) 0.6531(4) 0.050(2) Uani 1 1 d . . .
C22 C 1.0818(11) -0.3955(6) 0.6878(4) 0.076(3) Uani 1 1 d . . .
H22A H 1.1047 -0.3808 0.7227 0.114 Uiso 1 1 calc R . .
H22B H 1.1396 -0.4252 0.6740 0.114 Uiso 1 1 calc R . .
H22C H 1.0103 -0.4199 0.6892 0.114 Uiso 1 1 calc R . .
C23 C 0.9326(7) -0.1399(5) 0.7693(3) 0.050(2) Uani 1 1 d . . .
C24 C 0.9141(12) -0.1932(7) 0.8063(6) 0.123(6) Uani 1 1 d . . .
H24A H 0.9500 -0.1812 0.8396 0.184 Uiso 1 1 calc R . .
H24B H 0.9466 -0.2352 0.7937 0.184 Uiso 1 1 calc R . .
H24C H 0.8331 -0.1992 0.8107 0.184 Uiso 1 1 calc R . .
C25 C 0.9241(6) 0.2927(4) 0.6884(3) 0.0411(18) Uani 1 1 d . . .
C26 C 0.8978(8) 0.3496(5) 0.7251(4) 0.056(2) Uani 1 1 d . . .
H26A H 0.9043 0.3335 0.7608 0.084 Uiso 1 1 calc R . .
H26B H 0.8209 0.3657 0.7180 0.084 Uiso 1 1 calc R . .
H26C H 0.9510 0.3866 0.7201 0.084 Uiso 1 1 calc R . .
C27 C 0.6754(6) -0.0015(4) 0.4937(3) 0.0379(17) Uani 1 1 d . . .
C28 C 0.5945(12) -0.0129(7) 0.4514(4) 0.094(4) Uani 1 1 d . . .
H28A H 0.5756 -0.0598 0.4494 0.140 Uiso 1 1 d R . .
H28B H 0.6269 0.0012 0.4196 0.140 Uiso 1 1 d R . .
H28C H 0.5277 0.0129 0.4573 0.140 Uiso 1 1 d R . .
C29 C 1.0741(9) 0.0664(5) 0.7940(4) 0.059(2) Uani 1 1 d . . .
H29A H 1.0724 0.0214 0.8063 0.071 Uiso 1 1 calc R . .
C30 C 1.0944(11) 0.1825(6) 0.8155(4) 0.081(3) Uani 1 1 d . . .
H30A H 1.0604 0.1887 0.7810 0.122 Uiso 1 1 calc R . .
H30B H 1.1722 0.1989 0.8158 0.122 Uiso 1 1 calc R . .
H30C H 1.0513 0.2077 0.8408 0.122 Uiso 1 1 calc R . .
C31 C 1.1206(17) 0.1014(7) 0.8818(4) 0.128(7) Uani 1 1 d . . .
H31A H 1.1273 0.0528 0.8877 0.192 Uiso 1 1 calc R . .
H31B H 1.0608 0.1196 0.9031 0.192 Uiso 1 1 calc R . .
H31C H 1.1921 0.1234 0.8912 0.192 Uiso 1 1 calc R . .
C32 C 1.0851(10) 0.3917(6) 0.5143(6) 0.091(4) Uani 1 1 d . . .
H32A H 1.0841 0.4042 0.4789 0.109 Uiso 1 1 calc R . .
C33 C 1.1375(14) 0.5088(6) 0.5352(8) 0.132(7) Uani 1 1 d . . .
H33A H 1.1522 0.5127 0.4982 0.198 Uiso 1 1 calc R . .
H33B H 1.2054 0.5211 0.5553 0.198 Uiso 1 1 calc R . .
H33C H 1.0759 0.5391 0.5441 0.198 Uiso 1 1 calc R . .
C34 C 1.099(2) 0.4305(8) 0.6009(6) 0.152(9) Uani 1 1 d . . .
H34A H 1.0539 0.3903 0.6074 0.228 Uiso 1 1 calc R . .
H34B H 1.0634 0.4699 0.6164 0.228 Uiso 1 1 calc R . .
H34C H 1.1747 0.4246 0.6161 0.228 Uiso 1 1 calc R . .
C35 C 1.0000 0.0000 0.5000 0.030(2) Uani 1 2 d S . .
N1 N 1.0937(8) 0.1138(4) 0.8283(3) 0.062(2) Uani 1 1 d . . .
N2 N 1.1065(10) 0.4404(4) 0.5469(4) 0.089(3) Uani 1 1 d . . .
O1 O 0.9474(6) 0.2375(3) 0.7085(2) 0.0563(16) Uani 1 1 d . . .
O2 O 0.9211(6) 0.3053(3) 0.6411(2) 0.0613(18) Uani 1 1 d . . .
O3 O 0.7061(8) 0.0614(4) 0.4997(3) 0.097(3) Uani 1 1 d . . .
O4 O 0.7176(9) -0.0434(5) 0.5194(3) 0.110(3) Uani 1 1 d . . .
O5 O 1.0796(9) -0.2804(4) 0.6739(4) 0.122(4) Uani 1 1 d . . .
O6 O 1.0370(7) -0.3451(3) 0.6071(2) 0.068(2) Uani 1 1 d . . .
O7 O 0.9671(9) -0.0839(4) 0.7829(3) 0.104(3) Uani 1 1 d . . .
O8 O 0.8971(8) -0.1415(6) 0.7239(4) 0.116(3) Uani 1 1 d . . .
O9 O 1.0579(6) 0.0746(3) 0.7479(2) 0.0592(17) Uani 1 1 d . . .
O10 O 1.0667(7) 0.3342(3) 0.5224(3) 0.071(2) Uani 1 1 d . . .
O11 O 1.0183(9) -0.0223(6) 0.5476(4) 0.047(3) Uani 0.50 1 d P . .
O12 O 1.0193(10) 0.0472(6) 0.5337(4) 0.050(3) Uani 0.50 1 d P . .
O13 O 0.9916(11) 0.0611(6) 0.4914(6) 0.065(4) Uani 0.50 1 d P . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Ag1 0.0412(3) 0.0353(3) 0.0324(3) 0.0072(2) 0.0037(2) 0.0026(2)
Ag2 0.0390(3) 0.0358(3) 0.0471(3) 0.0007(2) 0.0067(3) -0.0065(2)
Ag3 0.0366(3) 0.0300(3) 0.0414(3) 0.0010(2) 0.0002(2) 0.0022(2)
Ag4 0.0442(4) 0.0459(4) 0.0375(3) -0.0024(2) -0.0075(2) 0.0095(3)
Ag5 0.0401(3) 0.0377(3) 0.0402(3) 0.0008(2) 0.0110(2) -0.0002(2)
Ag6 0.0389(3) 0.0410(3) 0.0358(3) 0.0034(2) 0.0026(2) 0.0089(2)
Ag7 0.0497(4) 0.0416(3) 0.0449(3) -0.0009(3) -0.0087(3) -0.0114(3)
Ag8 0.0455(4) 0.0525(4) 0.0311(3) 0.0000(2) 0.0026(2) -0.0074(3)
Ag9 0.0388(8) 0.0364(10) 0.0292(5) -0.0041(6) 0.0026(5) 0.0006(6)
Ag9' 0.065(4) 0.056(3) 0.039(2) -0.019(2) -0.017(2) 0.025(2)
Ag10 0.0511(4) 0.0424(3) 0.0563(4) -0.0168(3) 0.0130(3) -0.0097(3)
S1 0.0274(9) 0.0303(9) 0.0320(8) 0.0037(7) 0.0046(7) 0.0040(7)
S2 0.0256(9) 0.0314(9) 0.0293(8) 0.0018(7) 0.0044(6) 0.0002(7)
S3 0.0263(9) 0.0338(9) 0.0340(8) 0.0035(7) 0.0027(7) 0.0004(7)
S4 0.0246(9) 0.0309(9) 0.0294(8) -0.0018(7) -0.0020(6) -0.0023(7)
S5 0.0246(9) 0.0300(9) 0.0306(8) -0.0020(7) -0.0036(6) 0.0017(7)
C1 0.025(4) 0.039(4) 0.043(4) 0.004(3) 0.004(3) 0.013(3)
C2 0.068(7) 0.093(8) 0.100(8) 0.042(7) 0.053(7) 0.043(6)
C3 0.054(6) 0.064(6) 0.097(8) -0.018(6) -0.034(6) 0.011(5)
C4 0.044(5) 0.037(5) 0.091(7) -0.005(4) -0.001(5) 0.008(4)
C5 0.029(4) 0.039(4) 0.057(5) 0.009(4) 0.015(3) 0.004(3)
C6 0.07(2) 0.08(2) 0.09(2) 0.037(17) 0.035(15) 0.012(14)
C6' 0.06(2) 0.059(15) 0.11(3) 0.013(17) 0.051(18) -0.017(12)
C7 0.052(10) 0.112(14) 0.087(12) 0.019(11) 0.034(9) 0.041(10)
C7' 0.028(9) 0.116(16) 0.078(12) 0.010(12) 0.012(9) 0.018(11)
C8 0.082(14) 0.129(17) 0.051(11) -0.015(11) 0.033(10) 0.008(13)
C8' 0.061(11) 0.092(13) 0.088(12) -0.007(11) 0.042(10) 0.000(10)
C9 0.029(4) 0.045(4) 0.039(4) -0.004(3) 0.006(3) -0.006(3)
C10 0.066(8) 0.148(12) 0.086(8) 0.069(8) -0.009(6) -0.045(8)
C11 0.073(7) 0.078(7) 0.080(7) -0.032(6) 0.017(6) -0.041(6)
C12 0.043(6) 0.063(7) 0.140(11) -0.007(7) 0.034(7) 0.000(5)
C13 0.030(4) 0.037(4) 0.040(4) -0.005(3) -0.006(3) -0.005(3)
C14 0.167(16) 0.184(17) 0.070(8) 0.045(9) -0.072(9) -0.117(14)
C15 0.021(5) 0.201(16) 0.153(13) -0.109(12) 0.016(7) -0.031(7)
C16 0.066(8) 0.060(7) 0.180(14) -0.057(8) -0.045(8) -0.002(6)
C17 0.024(4) 0.039(4) 0.035(4) -0.001(3) -0.005(3) 0.007(3)
C18 0.058(8) 0.164(14) 0.092(9) 0.063(9) -0.042(6) -0.017(8)
C19 0.048(7) 0.205(16) 0.067(7) -0.021(8) -0.013(5) 0.059(9)
C20 0.070(8) 0.084(8) 0.105(9) -0.029(7) -0.049(7) 0.009(6)
C21 0.041(5) 0.043(5) 0.066(6) 0.002(4) -0.009(4) 0.008(4)
C22 0.098(9) 0.076(7) 0.054(6) 0.013(5) -0.003(6) -0.002(6)
C23 0.043(5) 0.072(7) 0.035(4) 0.001(4) 0.004(4) -0.003(4)
C24 0.090(10) 0.091(10) 0.184(16) 0.091(11) -0.047(10) -0.017(8)
C25 0.021(4) 0.054(5) 0.048(5) -0.015(4) -0.003(3) 0.001(3)
C26 0.051(6) 0.053(5) 0.064(5) -0.020(4) -0.006(4) 0.011(4)
C27 0.034(4) 0.046(5) 0.034(4) 0.000(3) -0.001(3) 0.005(3)
C28 0.112(11) 0.100(10) 0.068(7) -0.032(7) -0.009(7) 0.022(8)
C29 0.067(7) 0.056(6) 0.054(5) -0.003(4) -0.012(5) -0.008(5)
C30 0.106(10) 0.067(7) 0.069(7) -0.017(6) -0.013(6) 0.011(6)
C31 0.24(2) 0.095(10) 0.049(6) -0.003(6) -0.036(9) -0.022(12)
C32 0.061(7) 0.061(7) 0.151(12) -0.020(8) 0.013(7) -0.011(6)
C33 0.093(11) 0.057(8) 0.25(2) 0.003(11) -0.014(12) -0.014(7)
C34 0.29(3) 0.074(10) 0.089(10) -0.012(8) -0.026(13) 0.031(13)
C35 0.017(5) 0.041(6) 0.032(5) -0.008(5) 0.001(4) 0.005(4)
N1 0.082(6) 0.064(5) 0.040(4) -0.012(4) -0.011(4) -0.004(4)
N2 0.116(9) 0.045(5) 0.106(8) -0.026(5) -0.009(6) -0.007(5)
O1 0.079(5) 0.040(3) 0.049(3) -0.001(3) 0.008(3) 0.009(3)
O2 0.076(5) 0.064(4) 0.044(3) -0.011(3) -0.004(3) 0.034(3)
O3 0.123(8) 0.076(6) 0.092(6) 0.012(4) -0.019(5) -0.035(5)
O4 0.131(8) 0.123(8) 0.075(5) 0.014(5) -0.021(5) 0.047(7)
O5 0.143(9) 0.046(4) 0.171(9) -0.026(5) -0.112(7) 0.023(5)
O6 0.110(6) 0.045(4) 0.049(4) 0.012(3) 0.011(4) 0.018(4)
O7 0.155(9) 0.062(5) 0.100(6) -0.001(5) 0.066(6) -0.010(5)
O8 0.093(7) 0.164(10) 0.091(7) -0.005(6) 0.035(6) -0.011(6)
O9 0.082(5) 0.054(4) 0.041(3) -0.008(3) -0.018(3) -0.002(3)
O10 0.092(6) 0.041(4) 0.081(5) -0.003(3) 0.004(4) -0.016(4)
O11 0.043(7) 0.076(8) 0.023(5) -0.002(5) -0.005(4) -0.024(6)
O12 0.051(7) 0.055(7) 0.042(6) -0.012(6) -0.006(5) 0.024(6)
O13 0.061(9) 0.047(8) 0.086(10) 0.019(7) -0.040(7) -0.013(6)
_geom_special_details            
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 O3 2.388(9) . y
Ag1 S2 2.4902(17) . y
Ag1 O12 2.527(11) . y
Ag1 S1 2.5375(17) . y
Ag1 Ag4 3.1651(10) . y
Ag1 Ag10 3.1927(10) . y
Ag1 Ag2 3.2058(12) . y
Ag1 Ag9 3.252(3) . y
Ag2 O1 2.256(6) . y
Ag2 S2 2.4890(18) . y
Ag2 S4 2.5810(18) . y
Ag2 Ag4 2.9053(9) . y
Ag2 Ag3 3.1166(10) . y
Ag3 O11 2.404(10) . y
Ag3 O12 2.424(11) . y
Ag3 S4 2.4320(18) . y
Ag3 S5 2.4368(18) . y
Ag3 Ag9' 3.124(6) 3_756 ?
Ag3 Ag6 3.1341(11) . y
Ag3 Ag9 3.375(3) 3_756 y
Ag4 O2 2.256(5) . y
Ag4 S1 2.482(2) . y
Ag4 S4 2.5762(18) . y
Ag4 Ag8 3.1719(11) . y
Ag5 O6 2.277(6) . y
Ag5 S1 2.5038(18) 3_756 y
Ag5 S3 2.5615(18) . y
Ag5 Ag7 2.9931(9) . y
Ag5 Ag9 3.1473(19) 3_756 y
Ag5 Ag8 3.2021(11) 3_756 y
Ag6 O7 2.475(8) . y
Ag6 S2 2.5270(19) . y
Ag6 S5 2.5606(18) . y
Ag6 O8 2.563(11) . y
Ag6 O9 2.571(6) . y
Ag6 Ag10 3.1221(13) . y
Ag6 Ag7 3.2175(10) . y
Ag7 O5 2.278(8) . y
Ag7 O8 2.479(8) . y
Ag7 S5 2.5422(18) . y
Ag7 S3 2.553(2) . y
Ag7 Ag9 3.056(2) 3_756 y
Ag8 S4 2.4304(17) . y
Ag8 S3 2.4298(18) 3_756 y
Ag8 O13 2.524(12) . y
Ag8 O12 2.575(13) . y
Ag8 Ag5 3.2021(11) 3_756 y
Ag8 Ag10 3.3157(10) 3_756 y
Ag9 Ag9' 0.504(5) . ?
Ag9 S1 2.431(3) . y
Ag9 O13 2.455(13) . y
Ag9 S5 2.469(3) 3_756 y
Ag9 O11 2.538(13) 3_756 y
Ag9 Ag7 3.056(2) 3_756 y
Ag9 Ag5 3.1473(19) 3_756 y
Ag9 Ag3 3.375(3) 3_756 y
Ag9' O3 2.208(10) . ?
Ag9' O13 2.444(14) . ?
Ag9' O11 2.451(15) 3_756 ?
Ag9' S5 2.516(7) 3_756 ?
Ag9' S1 2.634(6) . ?
Ag9' Ag3 3.124(6) 3_756 ?
Ag10 O4 2.447(9) . y
Ag10 S2 2.4702(18) . y
Ag10 S3 2.4827(19) . y
Ag10 O11 2.545(10) . y
Ag10 Ag8 3.3157(10) 3_756 y
S1 C1 1.856(7) . ?
S1 Ag5 2.5038(17) 3_756 ?
S2 C5 1.861(7) . ?
S3 C9 1.868(7) . ?
S3 Ag8 2.4298(18) 3_756 ?
S4 C13 1.858(7) . ?
S5 C17 1.871(7) . ?
S5 Ag9 2.469(3) 3_756 ?
S5 Ag9' 2.516(7) 3_756 ?
C1 C3 1.496(12) . ?
C1 C2 1.522(11) . ?
C1 C4 1.515(11) . ?
C2 H2A 0.9800 . ?
C2 H2B 0.9800 . ?
C2 H2C 0.9800 . ?
C3 H3A 0.9800 . ?
C3 H3B 0.9800 . ?
C3 H3C 0.9800 . ?
C4 H4A 0.9800 . ?
C4 H4B 0.9800 . ?
C4 H4C 0.9800 . ?
C5 C6 1.41(3) . ?
C5 C8' 1.43(2) . ?
C5 C7 1.47(2) . ?
C5 C6' 1.49(3) . ?
C5 C8 1.61(2) . ?
C5 C7' 1.62(2) . ?
C6 C6' 0.78(4) . ?
C6 C8 1.85(4) . ?
C6 H6A 0.9599 . ?
C6 H6B 0.9600 . ?
C6 H6C 0.9599 . ?
C6 H6'A 1.2548 . ?
C6 H6'C 0.7857 . ?
C6' C7' 1.98(5) . ?
C6' H6A 1.2285 . ?
C6' H6B 0.6752 . ?
C6' H6'A 0.9601 . ?
C6' H6'B 0.9599 . ?
C6' H6'C 0.9600 . ?
C7 C7' 1.27(3) . ?
C7 C8' 1.46(4) . ?
C8 C8' 1.23(3) . ?
C9 C11 1.506(12) . ?
C9 C12 1.505(12) . ?
C9 C10 1.518(13) . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 H10C 0.9800 . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 C15 1.480(12) . ?
C13 C16 1.481(13) . ?
C13 C14 1.501(13) . ?
C14 H14A 0.9800 . ?
C14 H14B 0.9800 . ?
C14 H14C 0.9800 . ?
C15 H15A 0.9800 . ?
C15 H15B 0.9800 . ?
C15 H15C 0.9800 . ?
C16 H16A 0.9800 . ?
C16 H16B 0.9800 . ?
C16 H16C 0.9800 . ?
C17 C18 1.452(13) . ?
C17 C19 1.492(12) . ?
C17 C20 1.529(13) . ?
C18 H18A 0.9800 . ?
C18 H18B 0.9800 . ?
C18 H18C 0.9800 . ?
C19 H19A 0.9800 . ?
C19 H19B 0.9800 . ?
C19 H19C 0.9800 . ?
C20 H20A 0.9800 . ?
C20 H20B 0.9800 . ?
C20 H20C 0.9800 . ?
C21 O5 1.215(11) . ?
C21 O6 1.251(11) . ?
C21 C22 1.511(13) . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C23 O7 1.233(12) . ?
C23 O8 1.238(13) . ?
C23 C24 1.448(14) . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C25 O1 1.242(10) . ?
C25 O2 1.249(10) . ?
C25 C26 1.514(11) . ?
C26 H26A 0.9800 . ?
C26 H26B 0.9800 . ?
C26 H26C 0.9800 . ?
C27 O4 1.170(11) . ?
C27 O3 1.309(11) . ?
C27 C28 1.456(14) . ?
C28 H28A 0.9599 . ?
C28 H28B 0.9599 . ?
C28 H28C 0.9600 . ?
C29 O9 1.214(11) . ?
C29 N1 1.312(12) . ?
C29 H29A 0.9500 . ?
C30 N1 1.404(14) . ?
C30 H30A 0.9800 . ?
C30 H30B 0.9800 . ?
C30 H30C 0.9800 . ?
C31 N1 1.434(13) . ?
C31 H31A 0.9800 . ?
C31 H31B 0.9800 . ?
C31 H31C 0.9800 . ?
C32 O10 1.181(13) . ?
C32 N2 1.305(15) . ?
C32 H32A 0.9500 . ?
C33 N2 1.441(16) . ?
C33 H33A 0.9800 . ?
C33 H33B 0.9800 . ?
C33 H33C 0.9800 . ?
C34 N2 1.415(17) . ?
C34 H34A 0.9800 . ?
C34 H34B 0.9800 . ?
C34 H34C 0.9800 . ?
C35 O13 1.238(12) . ?
C35 O13 1.238(12) 3_756 ?
C35 O12 1.297(11) . ?
C35 O12 1.297(11) 3_756 ?
C35 O11 1.323(10) . ?
C35 O11 1.323(10) 3_756 ?
O11 O13 1.274(17) 3_756 ?
O11 O12 1.428(17) . ?
O11 Ag9' 2.451(15) 3_756 ?
O11 Ag9 2.538(13) 3_756 ?
O12 O13 1.167(16) . ?
O13 O11 1.274(17) 3_756 ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O3 Ag1 S2 118.8(2) . . ?
O3 Ag1 O12 101.7(4) . . ?
S2 Ag1 O12 95.3(3) . . ?
O3 Ag1 S1 85.2(2) . . ?
S2 Ag1 S1 149.84(6) . . ?
O12 Ag1 S1 97.2(3) . . ?
O3 Ag1 Ag9' 45.3(2) . . ?
S2 Ag1 Ag9' 155.35(11) . . ?
O12 Ag1 Ag9' 74.1(3) . . ?
S1 Ag1 Ag9' 54.79(11) . . ?
O3 Ag1 Ag4 135.29(19) . . ?
S2 Ag1 Ag4 103.57(5) . . ?
O12 Ag1 Ag4 86.9(3) . . ?
S1 Ag1 Ag4 50.13(5) . . ?
Ag9' Ag1 Ag4 98.12(9) . . ?
O3 Ag1 Ag10 82.1(2) . . ?
S2 Ag1 Ag10 49.66(4) . . ?
O12 Ag1 Ag10 70.6(3) . . ?
S1 Ag1 Ag10 160.03(4) . . ?
Ag9' Ag1 Ag10 105.74(10) . . ?
Ag4 Ag1 Ag10 140.60(3) . . ?
O3 Ag1 Ag2 167.7(2) . . ?
S2 Ag1 Ag2 49.91(4) . . ?
O12 Ag1 Ag2 85.5(3) . . ?
S1 Ag1 Ag2 103.96(5) . . ?
Ag9' Ag1 Ag2 146.94(10) . . ?
Ag4 Ag1 Ag2 54.26(2) . . ?
Ag10 Ag1 Ag2 91.07(2) . . ?
O3 Ag1 Ag9 53.3(2) . . ?
S2 Ag1 Ag9 161.82(6) . . ?
O12 Ag1 Ag9 72.5(3) . . ?
S1 Ag1 Ag9 47.70(6) . . ?
Ag9' Ag1 Ag9 8.63(10) . . ?
Ag4 Ag1 Ag9 89.54(4) . . ?
Ag10 Ag1 Ag9 112.47(5) . . ?
Ag2 Ag1 Ag9 138.94(4) . . ?
O1 Ag2 S2 125.17(18) . . ?
O1 Ag2 S4 111.64(17) . . ?
S2 Ag2 S4 119.19(6) . . ?
O1 Ag2 Ag4 80.91(15) . . ?
S2 Ag2 Ag4 111.42(5) . . ?
S4 Ag2 Ag4 55.64(4) . . ?
O1 Ag2 Ag3 155.53(18) . . ?
S2 Ag2 Ag3 78.84(4) . . ?
S4 Ag2 Ag3 49.45(4) . . ?
Ag4 Ag2 Ag3 95.19(3) . . ?
O1 Ag2 Ag1 121.28(17) . . ?
S2 Ag2 Ag1 49.94(4) . . ?
S4 Ag2 Ag1 84.32(4) . . ?
Ag4 Ag2 Ag1 62.16(2) . . ?
Ag3 Ag2 Ag1 76.35(2) . . ?
O11 Ag3 O12 34.4(4) . . ?
O11 Ag3 S4 115.5(3) . . ?
O12 Ag3 S4 81.1(3) . . ?
O11 Ag3 S5 84.1(3) . . ?
O12 Ag3 S5 118.5(3) . . ?
S4 Ag3 S5 160.09(6) . . ?
O11 Ag3 Ag2 107.9(3) . . ?
O12 Ag3 Ag2 89.2(2) . . ?
S4 Ag3 Ag2 53.74(4) . . ?
S5 Ag3 Ag2 119.17(5) . . ?
O11 Ag3 Ag9' 50.6(3) . 3_756 ?
O12 Ag3 Ag9' 78.1(3) . 3_756 ?
S4 Ag3 Ag9' 143.27(11) . 3_756 ?
S5 Ag3 Ag9' 52.02(12) . 3_756 ?
Ag2 Ag3 Ag9' 154.02(11) . 3_756 ?
O11 Ag3 Ag6 89.2(2) . . ?
O12 Ag3 Ag6 108.8(3) . . ?
S4 Ag3 Ag6 120.42(4) . . ?
S5 Ag3 Ag6 52.94(4) . . ?
Ag2 Ag3 Ag6 67.48(3) . . ?
Ag9' Ag3 Ag6 94.99(10) 3_756 . ?
O11 Ag3 Ag9 48.6(3) . 3_756 ?
O12 Ag3 Ag9 78.9(3) . 3_756 ?
S4 Ag3 Ag9 149.91(6) . 3_756 ?
S5 Ag3 Ag9 46.92(6) . 3_756 ?
Ag2 Ag3 Ag9 147.27(4) . 3_756 ?
Ag9' Ag3 Ag9 7.73(11) 3_756 3_756 ?
Ag6 Ag3 Ag9 87.46(4) . 3_756 ?
O2 Ag4 S1 118.38(18) . . ?
O2 Ag4 S4 117.49(16) . . ?
S1 Ag4 S4 119.95(6) . . ?
O2 Ag4 Ag2 81.04(16) . . ?
S1 Ag4 Ag2 114.77(5) . . ?
S4 Ag4 Ag2 55.79(4) . . ?
O2 Ag4 Ag1 115.76(19) . . ?
S1 Ag4 Ag1 51.69(4) . . ?
S4 Ag4 Ag1 85.24(5) . . ?
Ag2 Ag4 Ag1 63.59(3) . . ?
O2 Ag4 Ag8 161.38(18) . . ?
S1 Ag4 Ag8 79.68(4) . . ?
S4 Ag4 Ag8 48.68(4) . . ?
Ag2 Ag4 Ag8 95.88(3) . . ?
Ag1 Ag4 Ag8 78.29(3) . . ?
O6 Ag5 S1 127.5(2) . 3_756 ?
O6 Ag5 S3 112.16(18) . . ?
S1 Ag5 S3 115.77(6) 3_756 . ?
O6 Ag5 Ag7 83.33(17) . . ?
S1 Ag5 Ag7 108.40(5) 3_756 . ?
S3 Ag5 Ag7 54.05(5) . . ?
O6 Ag5 Ag9 123.4(2) . 3_756 ?
S1 Ag5 Ag9 49.35(6) 3_756 3_756 ?
S3 Ag5 Ag9 80.63(7) . 3_756 ?
Ag7 Ag5 Ag9 59.64(5) . 3_756 ?
O6 Ag5 Ag8 153.2(2) . 3_756 ?
S1 Ag5 Ag8 78.77(4) 3_756 3_756 ?
S3 Ag5 Ag8 48.31(4) . 3_756 ?
Ag7 Ag5 Ag8 93.66(3) . 3_756 ?
Ag9 Ag5 Ag8 76.05(6) 3_756 3_756 ?
O7 Ag6 S2 130.0(2) . . ?
O7 Ag6 S5 109.0(2) . . ?
S2 Ag6 S5 119.98(6) . . ?
O7 Ag6 O8 48.3(3) . . ?
S2 Ag6 O8 113.9(3) . . ?
S5 Ag6 O8 96.1(2) . . ?
O7 Ag6 O9 86.5(3) . . ?
S2 Ag6 O9 88.90(15) . . ?
S5 Ag6 O9 106.02(17) . . ?
O8 Ag6 O9 134.4(3) . . ?
O7 Ag6 Ag10 129.2(3) . . ?
S2 Ag6 Ag10 50.52(4) . . ?
S5 Ag6 Ag10 86.49(5) . . ?
O8 Ag6 Ag10 83.0(2) . . ?
O9 Ag6 Ag10 136.66(14) . . ?
O7 Ag6 Ag3 149.2(3) . . ?
S2 Ag6 Ag3 77.96(4) . . ?
S5 Ag6 Ag3 49.42(4) . . ?
O8 Ag6 Ag3 140.2(2) . . ?
O9 Ag6 Ag3 80.88(15) . . ?
Ag10 Ag6 Ag3 76.62(2) . . ?
O7 Ag6 Ag7 86.46(19) . . ?
S2 Ag6 Ag7 116.82(5) . . ?
S5 Ag6 Ag7 50.66(4) . . ?
O8 Ag6 Ag7 49.2(2) . . ?
O9 Ag6 Ag7 150.99(16) . . ?
Ag10 Ag6 Ag7 66.34(2) . . ?
Ag3 Ag6 Ag7 91.12(2) . . ?
O5 Ag7 O8 104.4(4) . . ?
O5 Ag7 S5 119.2(3) . . ?
O8 Ag7 S5 98.7(3) . . ?
O5 Ag7 S3 115.0(2) . . ?
O8 Ag7 S3 96.5(3) . . ?
S5 Ag7 S3 117.15(6) . . ?
O5 Ag7 Ag5 75.1(2) . . ?
O8 Ag7 Ag5 143.4(3) . . ?
S5 Ag7 Ag5 113.65(5) . . ?
S3 Ag7 Ag5 54.32(4) . . ?
O5 Ag7 Ag9 109.8(3) . 3_756 ?
O8 Ag7 Ag9 142.7(3) . 3_756 ?
S5 Ag7 Ag9 51.33(6) . 3_756 ?
S3 Ag7 Ag9 82.58(7) . 3_756 ?
Ag5 Ag7 Ag9 62.69(5) . 3_756 ?
O5 Ag7 Ag6 140.6(2) . . ?
O8 Ag7 Ag6 51.5(3) . . ?
S5 Ag7 Ag6 51.16(4) . . ?
S3 Ag7 Ag6 99.87(5) . . ?
Ag5 Ag7 Ag6 143.76(3) . . ?
Ag9 Ag7 Ag6 91.69(5) 3_756 . ?
S4 Ag8 S3 163.15(6) . 3_756 ?
S4 Ag8 O13 102.5(3) . . ?
S3 Ag8 O13 90.7(3) 3_756 . ?
S4 Ag8 O12 78.2(2) . . ?
S3 Ag8 O12 116.4(3) 3_756 . ?
O13 Ag8 O12 26.4(4) . . ?
S4 Ag8 Ag4 52.76(5) . . ?
S3 Ag8 Ag4 117.00(5) 3_756 . ?
O13 Ag8 Ag4 92.4(4) . . ?
O12 Ag8 Ag4 85.9(2) . . ?
S4 Ag8 Ag5 117.06(5) . 3_756 ?
S3 Ag8 Ag5 51.93(5) 3_756 3_756 ?
O13 Ag8 Ag5 88.9(3) . 3_756 ?
O12 Ag8 Ag5 109.2(3) . 3_756 ?
Ag4 Ag8 Ag5 65.24(2) . 3_756 ?
S4 Ag8 Ag10 148.22(5) . 3_756 ?
S3 Ag8 Ag10 48.23(5) 3_756 3_756 ?
O13 Ag8 Ag10 61.1(4) . 3_756 ?
O12 Ag8 Ag10 78.6(2) . 3_756 ?
Ag4 Ag8 Ag10 145.62(3) . 3_756 ?
Ag5 Ag8 Ag10 91.02(3) 3_756 3_756 ?
Ag9' Ag9 S1 108.5(10) . . ?
Ag9' Ag9 O13 82.8(12) . . ?
S1 Ag9 O13 87.1(4) . . ?
Ag9' Ag9 S5 89.6(10) . 3_756 ?
S1 Ag9 S5 157.38(11) . 3_756 ?
O13 Ag9 S5 109.2(4) . 3_756 ?
Ag9' Ag9 O11 74.4(11) . 3_756 ?
S1 Ag9 O11 116.6(3) . 3_756 ?
O13 Ag9 O11 29.5(4) . 3_756 ?
S5 Ag9 O11 80.7(2) 3_756 3_756 ?
Ag9' Ag9 Ag7 142.8(11) . 3_756 ?
S1 Ag9 Ag7 108.48(7) . 3_756 ?
O13 Ag9 Ag7 103.2(4) . 3_756 ?
S5 Ag9 Ag7 53.51(6) 3_756 3_756 ?
O11 Ag9 Ag7 92.8(2) 3_756 3_756 ?
Ag9' Ag9 Ag5 159.5(11) . 3_756 ?
S1 Ag9 Ag5 51.40(6) . 3_756 ?
O13 Ag9 Ag5 91.4(3) . 3_756 ?
S5 Ag9 Ag5 110.83(7) 3_756 3_756 ?
O11 Ag9 Ag5 109.3(3) 3_756 3_756 ?
Ag7 Ag9 Ag5 57.67(3) 3_756 3_756 ?
Ag9' Ag9 Ag1 66.8(10) . . ?
S1 Ag9 Ag1 50.55(6) . . ?
O13 Ag9 Ag1 55.3(4) . . ?
S5 Ag9 Ag1 152.02(9) 3_756 . ?
O11 Ag9 Ag1 78.7(2) 3_756 . ?
Ag7 Ag9 Ag1 145.93(9) 3_756 . ?
Ag5 Ag9 Ag1 93.81(7) 3_756 . ?
Ag9' Ag9 Ag3 56.4(10) . 3_756 ?
S1 Ag9 Ag3 156.36(11) . 3_756 ?
O13 Ag9 Ag3 73.7(3) . 3_756 ?
S5 Ag9 Ag3 46.14(6) 3_756 3_756 ?
O11 Ag9 Ag3 45.3(2) 3_756 3_756 ?
Ag7 Ag9 Ag3 89.55(7) 3_756 3_756 ?
Ag5 Ag9 Ag3 140.32(8) 3_756 3_756 ?
Ag1 Ag9 Ag3 106.15(6) . 3_756 ?
Ag9 Ag9' O3 147.5(12) . . ?
Ag9 Ag9' O13 85.4(12) . . ?
O3 Ag9' O13 94.0(5) . . ?
Ag9 Ag9' O11 94.2(11) . 3_756 ?
O3 Ag9' O11 101.5(4) . 3_756 ?
O13 Ag9' O11 30.2(4) . 3_756 ?
Ag9 Ag9' S5 78.9(10) . 3_756 ?
O3 Ag9' S5 131.3(3) . 3_756 ?
O13 Ag9' S5 108.0(5) . 3_756 ?
O11 Ag9' S5 81.5(3) 3_756 3_756 ?
Ag9 Ag9' S1 61.0(10) . . ?
O3 Ag9' S1 86.6(3) . . ?
O13 Ag9' S1 82.9(4) . . ?
O11 Ag9' S1 112.4(3) 3_756 . ?
S5 Ag9' S1 137.7(2) 3_756 . ?
Ag9 Ag9' Ag1 104.6(11) . . ?
O3 Ag9' Ag1 50.3(3) . . ?
O13 Ag9' Ag1 58.0(4) . . ?
O11 Ag9' Ag1 83.3(3) 3_756 . ?
S5 Ag9' Ag1 164.6(3) 3_756 . ?
S1 Ag9' Ag1 51.91(12) . . ?
Ag9 Ag9' Ag3 115.9(11) . 3_756 ?
O3 Ag9' Ag3 95.8(3) . 3_756 ?
O13 Ag9' Ag3 78.8(4) . 3_756 ?
O11 Ag9' Ag3 49.3(3) 3_756 3_756 ?
S5 Ag9' Ag3 49.77(12) 3_756 3_756 ?
S1 Ag9' Ag3 161.7(3) . 3_756 ?
Ag1 Ag9' Ag3 117.04(19) . 3_756 ?
O4 Ag10 S2 113.1(2) . . ?
O4 Ag10 S3 90.4(2) . . ?
S2 Ag10 S3 153.09(6) . . ?
O4 Ag10 O11 94.1(3) . . ?
S2 Ag10 O11 94.7(3) . . ?
S3 Ag10 O11 96.5(3) . . ?
O4 Ag10 Ag6 165.2(2) . . ?
S2 Ag10 Ag6 52.15(4) . . ?
S3 Ag10 Ag6 104.10(5) . . ?
O11 Ag10 Ag6 87.0(2) . . ?
O4 Ag10 Ag1 72.8(3) . . ?
S2 Ag10 Ag1 50.21(4) . . ?
S3 Ag10 Ag1 156.16(5) . . ?
O11 Ag10 Ag1 68.7(3) . . ?
Ag6 Ag10 Ag1 94.00(2) . . ?
O4 Ag10 Ag8 55.4(2) . 3_756 ?
S2 Ag10 Ag8 159.19(5) . 3_756 ?
S3 Ag10 Ag8 46.88(4) . 3_756 ?
O11 Ag10 Ag8 70.8(2) . 3_756 ?
Ag6 Ag10 Ag8 137.92(3) . 3_756 ?
Ag1 Ag10 Ag8 109.38(3) . 3_756 ?
C1 S1 Ag9 114.5(3) . . ?
C1 S1 Ag4 111.5(3) . . ?
Ag9 S1 Ag4 133.88(10) . . ?
C1 S1 Ag5 111.5(2) . 3_756 ?
Ag9 S1 Ag5 79.25(6) . 3_756 ?
Ag4 S1 Ag5 87.13(6) . 3_756 ?
C1 S1 Ag1 112.5(2) . . ?
Ag9 S1 Ag1 81.76(8) . . ?
Ag4 S1 Ag1 78.18(5) . . ?
Ag5 S1 Ag1 135.97(7) 3_756 . ?
C1 S1 Ag9' 111.5(3) . . ?
Ag9 S1 Ag9' 10.46(13) . . ?
Ag4 S1 Ag9' 134.82(17) . . ?
Ag5 S1 Ag9' 89.67(13) 3_756 . ?
Ag1 S1 Ag9' 73.31(14) . . ?
C5 S2 Ag10 113.7(3) . . ?
C5 S2 Ag2 112.2(3) . . ?
Ag10 S2 Ag2 134.09(7) . . ?
C5 S2 Ag1 114.1(3) . . ?
Ag10 S2 Ag1 80.13(5) . . ?
Ag2 S2 Ag1 80.16(6) . . ?
C5 S2 Ag6 111.6(3) . . ?
Ag10 S2 Ag6 77.32(6) . . ?
Ag2 S2 Ag6 87.59(6) . . ?
Ag1 S2 Ag6 134.02(7) . . ?
C9 S3 Ag8 114.8(2) . 3_756 ?
C9 S3 Ag10 114.7(2) . . ?
Ag8 S3 Ag10 84.90(6) 3_756 . ?
C9 S3 Ag7 113.1(3) . . ?
Ag8 S3 Ag7 130.25(7) 3_756 . ?
Ag10 S3 Ag7 87.09(6) . . ?
C9 S3 Ag5 110.8(2) . . ?
Ag8 S3 Ag5 79.77(6) 3_756 . ?
Ag10 S3 Ag5 134.42(7) . . ?
Ag7 S3 Ag5 71.64(5) . . ?
C13 S4 Ag8 117.6(2) . . ?
C13 S4 Ag3 119.3(2) . . ?
Ag8 S4 Ag3 92.58(6) . . ?
C13 S4 Ag4 112.3(2) . . ?
Ag8 S4 Ag4 78.56(6) . . ?
Ag3 S4 Ag4 125.30(7) . . ?
C13 S4 Ag2 111.2(2) . . ?
Ag8 S4 Ag2 128.56(7) . . ?
Ag3 S4 Ag2 76.82(5) . . ?
Ag4 S4 Ag2 68.57(5) . . ?
C17 S5 Ag3 116.5(2) . . ?
C17 S5 Ag9 117.9(2) . 3_756 ?
Ag3 S5 Ag9 86.94(8) . 3_756 ?
C17 S5 Ag9' 114.9(3) . 3_756 ?
Ag3 S5 Ag9' 78.20(14) . 3_756 ?
Ag9 S5 Ag9' 11.56(12) 3_756 3_756 ?
C17 S5 Ag7 111.9(2) . . ?
Ag3 S5 Ag7 131.25(7) . . ?
Ag9 S5 Ag7 75.16(6) 3_756 . ?
Ag9' S5 Ag7 86.67(12) 3_756 . ?
C17 S5 Ag6 114.3(2) . . ?
Ag3 S5 Ag6 77.64(5) . . ?
Ag9 S5 Ag6 127.09(10) 3_756 . ?
Ag9' S5 Ag6 130.70(17) 3_756 . ?
Ag7 S5 Ag6 78.18(5) . . ?
C3 C1 C2 109.8(9) . . ?
C3 C1 C4 111.2(7) . . ?
C2 C1 C4 111.1(8) . . ?
C3 C1 S1 108.6(6) . . ?
C2 C1 S1 108.3(6) . . ?
C4 C1 S1 107.7(5) . . ?
C1 C2 H2A 109.5 . . ?
C1 C2 H2B 109.5 . . ?
H2A C2 H2B 109.5 . . ?
C1 C2 H2C 109.5 . . ?
H2A C2 H2C 109.5 . . ?
H2B C2 H2C 109.5 . . ?
C1 C3 H3A 109.5 . . ?
C1 C3 H3B 109.5 . . ?
H3A C3 H3B 109.5 . . ?
C1 C3 H3C 109.5 . . ?
H3A C3 H3C 109.5 . . ?
H3B C3 H3C 109.5 . . ?
C1 C4 H4A 109.5 . . ?
C1 C4 H4B 109.5 . . ?
H4A C4 H4B 109.5 . . ?
C1 C4 H4C 109.5 . . ?
H4A C4 H4C 109.5 . . ?
H4B C4 H4C 109.5 . . ?
C6 C5 C8' 117.2(19) . . ?
C6 C5 C7 137.0(19) . . ?
C8' C5 C7 60.7(15) . . ?
C6 C5 C6' 31.0(17) . . ?
C8' C5 C6' 138.0(17) . . ?
C7 C5 C6' 119(2) . . ?
C6 C5 C8 75.5(17) . . ?
C8' C5 C8 47.2(14) . . ?
C7 C5 C8 105.9(16) . . ?
C6' C5 C8 105.2(17) . . ?
C6 C5 C7' 108.5(17) . . ?
C8' C5 C7' 108.4(15) . . ?
C7 C5 C7' 48.3(14) . . ?
C6' C5 C7' 78.8(18) . . ?
C8 C5 C7' 147.2(13) . . ?
C6 C5 S2 109.3(17) . . ?
C8' C5 S2 109.6(9) . . ?
C7 C5 S2 111.2(9) . . ?
C6' C5 S2 108.7(16) . . ?
C8 C5 S2 106.3(9) . . ?
C7' C5 S2 102.9(8) . . ?
C6' C6 C5 81(5) . . ?
C6' C6 C8 135(6) . . ?
C5 C6 C8 57.1(15) . . ?
C6' C6 H6A 89.2 . . ?
C5 C6 H6A 110.2 . . ?
C8 C6 H6A 90.9 . . ?
C6' C6 H6B 44.2 . . ?
C5 C6 H6B 108.8 . . ?
C8 C6 H6B 158.9 . . ?
H6A C6 H6B 109.5 . . ?
C6' C6 H6C 153.0 . . ?
C5 C6 H6C 109.3 . . ?
C8 C6 H6C 66.4 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
C5 C6 H6'A 100.1 . . ?
C8 C6 H6'A 118.0 . . ?
C6' C6 H6'C 75.7 . . ?
C5 C6 H6'C 129.1 . . ?
C8 C6 H6'C 142.9 . . ?
C6 C6' C5 68(4) . . ?
C6 C6' C7' 120(5) . . ?
C5 C6' C7' 53.4(15) . . ?
C6 C6' H6A 51.4 . . ?
C5 C6' H6A 91.6 . . ?
C7' C6' H6A 112.0 . . ?
C6 C6' H6B 82.2 . . ?
C5 C6' H6B 122.8 . . ?
C7' C6' H6B 140.5 . . ?
C6 C6' H6'A 91.7 . . ?
C5 C6' H6'A 111.0 . . ?
C7' C6' H6'A 94.9 . . ?
C6 C6' H6'B 156.8 . . ?
C5 C6' H6'B 110.2 . . ?
C7' C6' H6'B 68.9 . . ?
C6 C6' H6'C 52.5 . . ?
C5 C6' H6'C 107.2 . . ?
C7' C6' H6'C 153.9 . . ?
C7' C7 C5 72.2(16) . . ?
C7' C7 C8' 130(2) . . ?
C5 C7 C8' 58.4(14) . . ?
C7' C7 H7A 97.5 . . ?
C5 C7 H7A 110.3 . . ?
C8' C7 H7A 91.4 . . ?
C7' C7 H7B 150.2 . . ?
C5 C7 H7B 108.4 . . ?
C8' C7 H7B 63.6 . . ?
H7A C7 H7B 109.5 . . ?
C7' C7 H7C 47.2 . . ?
C5 C7 H7C 109.7 . . ?
C8' C7 H7C 159.0 . . ?
H7A C7 H7C 109.5 . . ?
H7B C7 H7C 109.5 . . ?
C7' C7 H7'A 38.5 . . ?
C5 C7 H7'A 91.0 . . ?
C8' C7 H7'A 128.5 . . ?
H7A C7 H7'A 59.2 . . ?
H7B C7 H7'A 160.4 . . ?
H7C C7 H7'A 64.7 . . ?
C7' C7 H7'B 44.9 . . ?
C5 C7 H7'B 103.0 . . ?
C8' C7 H7'B 151.6 . . ?
C7' C7 H8'C 153.6 . . ?
C5 C7 H8'C 88.2 . . ?
C8' C7 H8'C 39.7 . . ?
C7 C7' C5 59.5(15) . . ?
C7 C7' C6' 101(2) . . ?
C5 C7' C6' 47.8(10) . . ?
C5 C7' H7C 99.9 . . ?
C6' C7' H7C 147.3 . . ?
C7 C7' H7'A 86.0 . . ?
C5 C7' H7'A 109.6 . . ?
C6' C7' H7'A 91.4 . . ?
H7C C7' H7'A 97.1 . . ?
C7 C7' H7'B 66.1 . . ?
C5 C7' H7'B 108.1 . . ?
C6' C7' H7'B 153.7 . . ?
C7 C7' H7'C 164.3 . . ?
C5 C7' H7'C 110.6 . . ?
C6' C7' H7'C 76.6 . . ?
C8' C8 C5 58.8(15) . . ?
C8' C8 C6 102(2) . . ?
C5 C8 C6 47.4(12) . . ?
C8' C8 H8A 90.8 . . ?
C5 C8 H8A 110.2 . . ?
C6 C8 H8A 92.3 . . ?
C8' C8 H8B 159.6 . . ?
C5 C8 H8B 109.8 . . ?
C6 C8 H8B 75.8 . . ?
H8A C8 H8B 109.5 . . ?
C8' C8 H8C 63.8 . . ?
C5 C8 H8C 108.5 . . ?
C6 C8 H8C 153.3 . . ?
H8A C8 H8C 109.5 . . ?
H8B C8 H8C 109.5 . . ?
C8' C8 H8'A 37.5 . . ?
C5 C8 H8'A 76.7 . . ?
C6 C8 H8'A 99.1 . . ?
C8' C8 H8'B 50.4 . . ?
C5 C8 H8'B 97.8 . . ?
C6 C8 H8'B 144.9 . . ?
C8 C8' C5 74.0(18) . . ?
C8 C8' C7 132(3) . . ?
C5 C8' C7 60.9(14) . . ?
C8 C8' H7B 163.4 . . ?
C5 C8' H7B 91.5 . . ?
C7 C8' H7B 39.7 . . ?
C8 C8' H8A 37.8 . . ?
C5 C8' H8A 90.9 . . ?
C7 C8' H8A 122.6 . . ?
C8 C8' H8C 47.0 . . ?
C5 C8' H8C 108.2 . . ?
C7 C8' H8C 162.8 . . ?
H7B C8' H8C 135.2 . . ?
H8A C8' H8C 67.9 . . ?
C8 C8' H8'A 91.4 . . ?
C5 C8' H8'A 110.0 . . ?
C7 C8' H8'A 88.3 . . ?
C8 C8' H8'B 49.5 . . ?
C5 C8' H8'B 109.7 . . ?
C7 C8' H8'B 162.2 . . ?
C8 C8' H8'C 155.6 . . ?
C5 C8' H8'C 108.7 . . ?
C7 C8' H8'C 63.8 . . ?
C11 C9 C12 110.2(9) . . ?
C11 C9 C10 110.2(9) . . ?
C12 C9 C10 111.0(9) . . ?
C11 C9 S3 108.8(5) . . ?
C12 C9 S3 108.1(6) . . ?
C10 C9 S3 108.4(6) . . ?
C9 C10 H10A 109.5 . . ?
C9 C10 H10B 109.5 . . ?
H10A C10 H10B 109.5 . . ?
C9 C10 H10C 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C9 C11 H11A 109.5 . . ?
C9 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C9 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C9 C12 H12A 109.5 . . ?
C9 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C9 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C15 C13 C16 111.2(10) . . ?
C15 C13 C14 111.7(11) . . ?
C16 C13 C14 110.0(11) . . ?
C15 C13 S4 108.6(6) . . ?
C16 C13 S4 108.1(6) . . ?
C14 C13 S4 107.1(6) . . ?
C13 C14 H14A 109.5 . . ?
C13 C14 H14B 109.5 . . ?
H14A C14 H14B 109.5 . . ?
C13 C14 H14C 109.5 . . ?
H14A C14 H14C 109.5 . . ?
H14B C14 H14C 109.5 . . ?
C13 C15 H15A 109.5 . . ?
C13 C15 H15B 109.5 . . ?
H15A C15 H15B 109.5 . . ?
C13 C15 H15C 109.5 . . ?
H15A C15 H15C 109.5 . . ?
H15B C15 H15C 109.5 . . ?
C13 C16 H16A 109.5 . . ?
C13 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
C13 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
C18 C17 C19 114.1(10) . . ?
C18 C17 C20 110.2(9) . . ?
C19 C17 C20 108.2(9) . . ?
C18 C17 S5 108.2(6) . . ?
C19 C17 S5 107.4(6) . . ?
C20 C17 S5 108.6(6) . . ?
C17 C18 H18A 109.5 . . ?
C17 C18 H18B 109.5 . . ?
H18A C18 H18B 109.5 . . ?
C17 C18 H18C 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
C17 C19 H19A 109.5 . . ?
C17 C19 H19B 109.5 . . ?
H19A C19 H19B 109.5 . . ?
C17 C19 H19C 109.5 . . ?
H19A C19 H19C 109.5 . . ?
H19B C19 H19C 109.5 . . ?
C17 C20 H20A 109.5 . . ?
C17 C20 H20B 109.5 . . ?
H20A C20 H20B 109.5 . . ?
C17 C20 H20C 109.5 . . ?
H20A C20 H20C 109.5 . . ?
H20B C20 H20C 109.5 . . ?
O5 C21 O6 126.6(9) . . ?
O5 C21 C22 115.8(9) . . ?
O6 C21 C22 117.4(8) . . ?
C21 C22 H22A 109.5 . . ?
C21 C22 H22B 109.5 . . ?
H22A C22 H22B 109.5 . . ?
C21 C22 H22C 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
O7 C23 O8 113.3(10) . . ?
O7 C23 C24 121.7(11) . . ?
O8 C23 C24 123.7(11) . . ?
C23 C24 H24A 109.5 . . ?
C23 C24 H24B 109.5 . . ?
H24A C24 H24B 109.5 . . ?
C23 C24 H24C 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
O1 C25 O2 126.0(7) . . ?
O1 C25 C26 116.4(8) . . ?
O2 C25 C26 117.6(8) . . ?
C25 C26 H26A 109.5 . . ?
C25 C26 H26B 109.5 . . ?
H26A C26 H26B 109.5 . . ?
C25 C26 H26C 109.5 . . ?
H26A C26 H26C 109.5 . . ?
H26B C26 H26C 109.5 . . ?
O4 C27 O3 119.8(10) . . ?
O4 C27 C28 125.5(10) . . ?
O3 C27 C28 114.5(9) . . ?
C27 C28 H28A 110.0 . . ?
C27 C28 H28B 109.2 . . ?
H28A C28 H28B 109.5 . . ?
C27 C28 H28C 109.3 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
O9 C29 N1 126.2(9) . . ?
O9 C29 H29A 116.9 . . ?
N1 C29 H29A 116.9 . . ?
N1 C30 H30A 109.5 . . ?
N1 C30 H30B 109.5 . . ?
H30A C30 H30B 109.5 . . ?
N1 C30 H30C 109.5 . . ?
H30A C30 H30C 109.5 . . ?
H30B C30 H30C 109.5 . . ?
N1 C31 H31A 109.5 . . ?
N1 C31 H31B 109.5 . . ?
H31A C31 H31B 109.5 . . ?
N1 C31 H31C 109.5 . . ?
H31A C31 H31C 109.5 . . ?
H31B C31 H31C 109.5 . . ?
O10 C32 N2 129.5(15) . . ?
O10 C32 H32A 115.2 . . ?
N2 C32 H32A 115.2 . . ?
N2 C33 H33A 109.5 . . ?
N2 C33 H33B 109.5 . . ?
H33A C33 H33B 109.5 . . ?
N2 C33 H33C 109.5 . . ?
H33A C33 H33C 109.5 . . ?
H33B C33 H33C 109.5 . . ?
N2 C34 H34A 109.5 . . ?
N2 C34 H34B 109.5 . . ?
H34A C34 H34B 109.5 . . ?
N2 C34 H34C 109.5 . . ?
H34A C34 H34C 109.5 . . ?
H34B C34 H34C 109.5 . . ?
O13 C35 O13 180.0(13) . 3_756 ?
O13 C35 O12 54.8(8) . . ?
O13 C35 O12 125.2(8) 3_756 . ?
O13 C35 O12 125.2(8) . 3_756 ?
O13 C35 O12 54.8(8) 3_756 3_756 ?
O12 C35 O12 180.0(7) . 3_756 ?
O13 C35 O11 120.4(8) . . ?
O13 C35 O11 59.6(8) 3_756 . ?
O12 C35 O11 66.0(7) . . ?
O12 C35 O11 114.0(7) 3_756 . ?
O13 C35 O11 59.6(8) . 3_756 ?
O13 C35 O11 120.4(8) 3_756 3_756 ?
O12 C35 O11 114.0(7) . 3_756 ?
O12 C35 O11 66.0(7) 3_756 3_756 ?
O11 C35 O11 180.0(3) . 3_756 ?
C29 N1 C30 122.6(8) . . ?
C29 N1 C31 124.2(10) . . ?
C30 N1 C31 113.1(9) . . ?
C32 N2 C34 121.2(12) . . ?
C32 N2 C33 127.6(14) . . ?
C34 N2 C33 111.2(12) . . ?
C25 O1 Ag2 125.5(5) . . ?
C25 O2 Ag4 124.9(5) . . ?
C27 O3 Ag9' 117.0(7) . . ?
C27 O3 Ag1 125.2(6) . . ?
Ag9' O3 Ag1 84.4(3) . . ?
C27 O4 Ag10 139.4(9) . . ?
C21 O5 Ag7 130.7(7) . . ?
C21 O6 Ag5 119.6(6) . . ?
C23 O7 Ag6 100.4(7) . . ?
C23 O8 Ag7 123.2(8) . . ?
C23 O8 Ag6 95.9(8) . . ?
Ag7 O8 Ag6 79.3(3) . . ?
C29 O9 Ag6 115.7(6) . . ?
O13 O11 C35 56.9(7) 3_756 . ?
O13 O11 O12 112.7(10) 3_756 . ?
C35 O11 O12 56.1(6) . . ?
O13 O11 Ag3 151.0(10) 3_756 . ?
C35 O11 Ag3 124.7(7) . . ?
O12 O11 Ag3 73.6(6) . . ?
O13 O11 Ag9' 74.6(8) 3_756 3_756 ?
C35 O11 Ag9' 114.1(7) . 3_756 ?
O12 O11 Ag9' 129.8(8) . 3_756 ?
Ag3 O11 Ag9' 80.1(4) . 3_756 ?
O13 O11 Ag9 71.6(8) 3_756 3_756 ?
C35 O11 Ag9 118.5(7) . 3_756 ?
O12 O11 Ag9 141.2(8) . 3_756 ?
Ag3 O11 Ag9 86.1(4) . 3_756 ?
Ag9' O11 Ag9 11.43(13) 3_756 3_756 ?
O13 O11 Ag10 100.4(9) 3_756 . ?
C35 O11 Ag10 114.9(6) . . ?
O12 O11 Ag10 111.8(8) . . ?
Ag3 O11 Ag10 103.2(3) . . ?
Ag9' O11 Ag10 115.5(5) 3_756 . ?
Ag9 O11 Ag10 104.7(4) 3_756 . ?
O13 O12 C35 60.0(8) . . ?
O13 O12 O11 117.5(12) . . ?
C35 O12 O11 57.9(6) . . ?
O13 O12 Ag3 161.7(12) . . ?
C35 O12 Ag3 124.9(7) . . ?
O11 O12 Ag3 72.0(6) . . ?
O13 O12 Ag1 87.8(10) . . ?
C35 O12 Ag1 112.0(7) . . ?
O11 O12 Ag1 108.9(8) . . ?
Ag3 O12 Ag1 104.2(4) . . ?
O13 O12 Ag8 74.4(9) . . ?
C35 O12 Ag8 119.4(7) . . ?
O11 O12 Ag8 145.8(8) . . ?
Ag3 O12 Ag8 89.3(4) . . ?
Ag1 O12 Ag8 103.3(4) . . ?
O12 O13 C35 65.2(9) . . ?
O12 O13 O11 128.2(13) . 3_756 ?
C35 O13 O11 63.5(8) . 3_756 ?
O12 O13 Ag9' 139.2(12) . . ?
C35 O13 Ag9' 118.7(8) . . ?
O11 O13 Ag9' 75.2(8) 3_756 . ?
O12 O13 Ag9 144.1(12) . . ?
C35 O13 Ag9 129.2(8) . . ?
O11 O13 Ag9 78.9(8) 3_756 . ?
Ag9' O13 Ag9 11.81(13) . . ?
O12 O13 Ag8 79.2(9) . . ?
C35 O13 Ag8 126.1(8) . . ?
O11 O13 Ag8 127.6(10) 3_756 . ?
Ag9' O13 Ag8 114.8(5) . . ?
Ag9 O13 Ag8 103.5(4) . . ?
_diffrn_measured_fraction_theta_max 0.996
_diffrn_reflns_theta_full        25.00
_diffrn_measured_fraction_theta_full 0.996
_refine_diff_density_max         1.884
_refine_diff_density_min         -1.184
_refine_diff_density_rms         0.165
# SQUEEZE RESULTS (APPEND TO CIF)
# Note: Data are Listed for all Voids in the P1 Unit Cell
# i.e. Centre of Gravity, Solvent Accessible Volume,
# Recovered number of Electrons in the Void and
# Details about the Squeezed Material
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 0.000 0.000 0.000 368 61 ' '
2 0.500 0.500 0.500 368 60 ' '
_platon_squeeze_details          
;
;