# Electronic Supplementary Material (ESI) for Dalton Transactions
# This journal is © The Royal Society of Chemistry 2013

#######################################################################
#
#                 Cambridge Crystallographic Data Centre
#                                CCDC 
# 
#######################################################################
# 
#  This CIF contains data from an original supplementary publication
#  deposited with the CCDC, and may include chemical, crystal,
#  experimental, refinement, atomic coordinates,
#  anisotropic displacement parameters and molecular geometry data,
#  as required by the journal to which it was submitted.
#
#  This CIF is provided on the understanding that it is used for bona
#  fide research purposes only. It may contain copyright material
#  of the CCDC or of third parties, and may not be copied or further
#  disseminated in any form, whether machine-readable or not,
#  except for the purpose of generating routine backup copies
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#  data retrieval see:
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#  from this site to visualise CIF-encoded structures and 
#  to carry out CIF format checking respectively.
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data_2a
#TrackingRef 'revised-compound-2a.cif'


_audit_creation_method           SHELXL-97
_chemical_name_systematic        
;
?
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C22 H20 Cl4 I2 N2 O4 Pt2 S2'
_chemical_formula_weight         1226.30

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           Monoclinic
_symmetry_space_group_name_H-M   P2(1)/c

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   7.2336(4)
_cell_length_b                   20.5641(10)
_cell_length_c                   20.2197(10)
_cell_angle_alpha                90.00
_cell_angle_beta                 92.9860(10)
_cell_angle_gamma                90.00
_cell_volume                     3003.6(3)
_cell_formula_units_Z            4
_cell_measurement_temperature    230(2)
_cell_measurement_reflns_used    5168
_cell_measurement_theta_min      2.2227
_cell_measurement_theta_max      24.3302

_exptl_crystal_description       Prismatic
_exptl_crystal_colour            Yellow
_exptl_crystal_size_max          0.431
_exptl_crystal_size_mid          0.273
_exptl_crystal_size_min          0.222
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    2.712
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             2240
_exptl_absorpt_coefficient_mu    11.888
_exptl_absorpt_correction_type   MULTI-SCAN
_exptl_absorpt_correction_T_min  0.4046
_exptl_absorpt_correction_T_max  0.7453
_exptl_absorpt_process_details   SADABS

_exptl_special_details           
;
?
;

_diffrn_ambient_temperature      230(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'omega scan'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            20653
_diffrn_reflns_av_R_equivalents  0.0368
_diffrn_reflns_av_sigmaI/netI    0.0364
_diffrn_reflns_limit_h_min       -7
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_k_min       -25
_diffrn_reflns_limit_k_max       25
_diffrn_reflns_limit_l_min       -24
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_theta_min         1.98
_diffrn_reflns_theta_max         25.70
_reflns_number_total             5695
_reflns_number_gt                4837
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'Bruker APEX'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'

_refine_special_details          
;
Refinement of F^2^ against ALL reflections. The weighted R-factor wR and
goodness of fit S are based on F^2^, conventional R-factors R are based
on F, with F set to zero for negative F^2^. The threshold expression of
F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is
not relevant to the choice of reflections for refinement. R-factors based
on F^2^ are statistically about twice as large as those based on F, and R-
factors based on ALL data will be even larger.
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[\s^2^(Fo^2^)+(0.0372P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         5695
_refine_ls_number_parameters     347
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0367
_refine_ls_R_factor_gt           0.0283
_refine_ls_wR_factor_ref         0.0624
_refine_ls_wR_factor_gt          0.0595
_refine_ls_goodness_of_fit_ref   1.017
_refine_ls_restrained_S_all      1.017
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.47235(3) 0.271770(10) 0.136105(11) 0.03552(8) Uani 1 1 d . . .
I1 I 0.51438(7) 0.52766(2) 0.14139(2) 0.05052(13) Uani 1 1 d . . .
Cl1 Cl 0.5072(2) 0.27316(7) 0.02358(7) 0.0483(4) Uani 1 1 d . . .
Cl2 Cl 0.4147(3) 0.46379(9) 0.41087(8) 0.0686(6) Uani 1 1 d . . .
S1 S 0.4720(2) 0.16508(7) 0.13353(8) 0.0441(4) Uani 1 1 d . . .
O1 O 0.4875(6) 0.37025(18) 0.13868(17) 0.0368(10) Uani 1 1 d . . .
O2 O 0.3991(8) 0.1290(2) 0.1883(2) 0.0695(16) Uani 1 1 d . . .
N1 N 0.4425(7) 0.2842(2) 0.2342(2) 0.0351(11) Uani 1 1 d . . .
C1 C 0.4183(10) 0.2403(3) 0.2806(3) 0.0506(18) Uani 1 1 d . . .
H1 H 0.4108 0.1967 0.2684 0.061 Uiso 1 1 calc R . .
C2 C 0.4037(10) 0.2564(3) 0.3464(3) 0.0504(18) Uani 1 1 d . . .
H2 H 0.3908 0.2238 0.3778 0.061 Uiso 1 1 calc R . .
C3 C 0.4080(10) 0.3195(3) 0.3655(3) 0.0502(17) Uani 1 1 d . . .
H3 H 0.3962 0.3303 0.4097 0.060 Uiso 1 1 calc R . .
C4 C 0.4305(8) 0.3690(3) 0.3180(3) 0.0383(14) Uani 1 1 d . . .
C5 C 0.4483(8) 0.3487(2) 0.2518(3) 0.0316(13) Uani 1 1 d . . .
C6 C 0.4722(8) 0.3931(3) 0.1990(3) 0.0341(13) Uani 1 1 d . . .
C7 C 0.4780(8) 0.4581(3) 0.2153(3) 0.0348(13) Uani 1 1 d . . .
C8 C 0.4618(9) 0.4797(3) 0.2803(3) 0.0449(16) Uani 1 1 d . . .
H8 H 0.4680 0.5239 0.2897 0.054 Uiso 1 1 calc R . .
C9 C 0.4368(10) 0.4361(3) 0.3305(3) 0.0452(16) Uani 1 1 d . . .
C10 C 0.3618(14) 0.1329(4) 0.0619(4) 0.092(3) Uani 1 1 d . . .
H10A H 0.3539 0.0865 0.0660 0.139 Uiso 1 1 calc R . .
H10B H 0.4313 0.1437 0.0243 0.139 Uiso 1 1 calc R . .
H10C H 0.2394 0.1508 0.0562 0.139 Uiso 1 1 calc R . .
C11 C 0.7047(11) 0.1415(3) 0.1279(5) 0.076(3) Uani 1 1 d . . .
H11A H 0.7782 0.1606 0.1638 0.115 Uiso 1 1 calc R . .
H11B H 0.7490 0.1562 0.0866 0.115 Uiso 1 1 calc R . .
H11C H 0.7137 0.0950 0.1304 0.115 Uiso 1 1 calc R . .
Pt1A Pt 0.98336(3) 0.347217(11) 0.151618(11) 0.03450(7) Uani 1 1 d . . .
I1A I 0.90883(9) 0.17420(2) 0.33826(2) 0.07298(17) Uani 1 1 d . . .
Cl1A Cl 1.0032(2) 0.26305(7) 0.07783(8) 0.0489(4) Uani 1 1 d . . .
Cl2A Cl 0.8981(3) 0.41348(11) 0.48075(9) 0.0809(7) Uani 1 1 d . . .
S1A S 0.9974(2) 0.41678(7) 0.06896(7) 0.0361(3) Uani 1 1 d . . .
O1A O 0.9595(6) 0.28167(19) 0.22528(19) 0.0450(11) Uani 1 1 d . . .
O2A O 1.0125(6) 0.48644(19) 0.08522(19) 0.0458(11) Uani 1 1 d . . .
N1A N 0.9656(7) 0.4107(2) 0.2282(2) 0.0357(11) Uani 1 1 d . . .
C1A C 0.9707(9) 0.4750(3) 0.2284(3) 0.0445(16) Uani 1 1 d . . .
H1A H 0.9858 0.4968 0.1887 0.053 Uiso 1 1 calc R . .
C2A C 0.9544(9) 0.5112(3) 0.2859(3) 0.0527(18) Uani 1 1 d . . .
H2A H 0.9575 0.5564 0.2842 0.063 Uiso 1 1 calc R . .
C3A C 0.9338(9) 0.4806(3) 0.3449(3) 0.0508(17) Uani 1 1 d . . .
H3A H 0.9220 0.5048 0.3833 0.061 Uiso 1 1 calc R . .
C4A C 0.9307(9) 0.4121(3) 0.3475(3) 0.0441(16) Uani 1 1 d . . .
C5A C 0.9456(8) 0.3775(3) 0.2871(3) 0.0390(14) Uani 1 1 d . . .
C6A C 0.9402(9) 0.3092(3) 0.2828(3) 0.0407(15) Uani 1 1 d . . .
C7A C 0.9202(10) 0.2752(3) 0.3414(3) 0.0481(17) Uani 1 1 d . . .
C8A C 0.9061(10) 0.3076(4) 0.4014(3) 0.060(2) Uani 1 1 d . . .
H8A H 0.8933 0.2836 0.4399 0.072 Uiso 1 1 calc R . .
C9A C 0.9106(10) 0.3740(4) 0.4048(3) 0.0519(18) Uani 1 1 d . . .
C10A C 1.1783(9) 0.3983(3) 0.0165(3) 0.0469(16) Uani 1 1 d . . .
H10D H 1.1720 0.4271 -0.0209 0.070 Uiso 1 1 calc R . .
H10E H 1.1659 0.3541 0.0014 0.070 Uiso 1 1 calc R . .
H10F H 1.2954 0.4036 0.0405 0.070 Uiso 1 1 calc R . .
C11A C 0.7984(8) 0.4057(3) 0.0157(3) 0.0444(16) Uani 1 1 d . . .
H11D H 0.6899 0.4161 0.0390 0.067 Uiso 1 1 calc R . .
H11E H 0.7920 0.3613 0.0012 0.067 Uiso 1 1 calc R . .
H11F H 0.8052 0.4338 -0.0220 0.067 Uiso 1 1 calc R . .

loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Pt1 0.04710(17) 0.02445(12) 0.03504(13) 0.00032(9) 0.00244(10) -0.00015(10)
I1 0.0700(3) 0.0307(2) 0.0507(3) 0.00642(18) 0.0015(2) 0.0005(2)
Cl1 0.0674(12) 0.0396(8) 0.0384(8) -0.0034(7) 0.0082(8) -0.0014(8)
Cl2 0.1132(17) 0.0515(10) 0.0414(9) -0.0110(8) 0.0075(10) -0.0003(11)
S1 0.0614(12) 0.0262(7) 0.0450(9) -0.0007(7) 0.0057(8) -0.0011(7)
O1 0.057(3) 0.026(2) 0.028(2) 0.0006(16) 0.0049(19) -0.0041(18)
O2 0.115(5) 0.029(2) 0.068(3) 0.002(2) 0.035(3) -0.008(3)
N1 0.044(3) 0.030(2) 0.032(2) 0.003(2) 0.003(2) 0.001(2)
C1 0.072(5) 0.034(3) 0.046(4) 0.007(3) 0.002(3) -0.002(3)
C2 0.077(5) 0.041(4) 0.033(3) 0.005(3) 0.004(3) -0.009(3)
C3 0.065(5) 0.053(4) 0.033(3) 0.006(3) 0.009(3) 0.002(4)
C4 0.035(4) 0.037(3) 0.043(3) -0.004(3) 0.001(3) 0.000(3)
C5 0.035(3) 0.026(3) 0.033(3) -0.001(2) -0.004(2) -0.002(2)
C6 0.033(4) 0.032(3) 0.037(3) -0.001(3) -0.002(3) 0.003(3)
C7 0.038(4) 0.028(3) 0.038(3) 0.002(3) 0.003(3) -0.002(3)
C8 0.054(4) 0.031(3) 0.050(4) -0.009(3) -0.001(3) 0.000(3)
C9 0.063(5) 0.037(3) 0.035(3) -0.008(3) 0.004(3) 0.003(3)
C10 0.145(9) 0.044(4) 0.083(6) -0.010(4) -0.045(6) -0.020(5)
C11 0.074(6) 0.034(4) 0.123(7) 0.001(4) 0.021(5) 0.008(4)
Pt1A 0.04036(15) 0.03159(13) 0.03143(12) 0.00730(10) 0.00061(10) -0.00289(10)
I1A 0.1149(5) 0.0479(3) 0.0562(3) 0.0211(2) 0.0049(3) -0.0095(3)
Cl1A 0.0617(12) 0.0369(8) 0.0480(9) 0.0002(7) 0.0030(8) -0.0029(8)
Cl2A 0.121(2) 0.0870(15) 0.0353(9) -0.0006(10) 0.0090(11) 0.0019(13)
S1A 0.0429(10) 0.0337(7) 0.0317(7) 0.0068(6) 0.0016(7) -0.0024(7)
O1A 0.064(3) 0.036(2) 0.035(2) 0.0122(19) 0.003(2) -0.003(2)
O2A 0.066(3) 0.033(2) 0.038(2) 0.0057(19) 0.002(2) -0.007(2)
N1A 0.039(3) 0.038(3) 0.030(2) 0.009(2) 0.000(2) -0.003(2)
C1A 0.055(4) 0.033(3) 0.045(4) 0.005(3) -0.002(3) -0.006(3)
C2A 0.065(5) 0.039(4) 0.053(4) -0.001(3) -0.001(4) -0.001(3)
C3A 0.061(5) 0.051(4) 0.041(4) -0.009(3) 0.004(3) 0.003(3)
C4A 0.047(4) 0.055(4) 0.030(3) 0.007(3) 0.004(3) -0.004(3)
C5A 0.035(4) 0.044(3) 0.037(3) 0.011(3) 0.001(3) -0.001(3)
C6A 0.041(4) 0.044(4) 0.036(3) 0.012(3) -0.003(3) -0.007(3)
C7A 0.056(5) 0.048(4) 0.040(3) 0.012(3) 0.000(3) -0.002(3)
C8A 0.067(5) 0.071(5) 0.041(4) 0.021(4) 0.005(4) -0.006(4)
C9A 0.059(5) 0.066(5) 0.031(3) 0.000(3) 0.004(3) -0.003(4)
C10A 0.045(4) 0.050(4) 0.046(4) 0.012(3) 0.008(3) -0.001(3)
C11A 0.044(4) 0.051(4) 0.038(3) 0.009(3) -0.004(3) -0.003(3)

_geom_special_details            
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 N1 2.022(4) . ?
Pt1 O1 2.029(4) . ?
Pt1 S1 2.1946(15) . ?
Pt1 Cl1 2.3024(15) . ?
I1 C7 2.094(5) . ?
Cl2 C9 1.738(6) . ?
S1 O2 1.455(5) . ?
S1 C10 1.746(8) . ?
S1 C11 1.761(8) . ?
O1 C6 1.317(6) . ?
N1 C1 1.320(7) . ?
N1 C5 1.374(6) . ?
C1 C2 1.382(8) . ?
C2 C3 1.353(9) . ?
C3 C4 1.414(8) . ?
C4 C9 1.403(8) . ?
C4 C5 1.415(8) . ?
C5 C6 1.421(7) . ?
C6 C7 1.378(7) . ?
C7 C8 1.399(8) . ?
C8 C9 1.373(8) . ?
Pt1A O1A 2.023(4) . ?
Pt1A N1A 2.035(5) . ?
Pt1A S1A 2.2062(14) . ?
Pt1A Cl1A 2.2944(16) . ?
I1A C7A 2.079(7) . ?
Cl2A C9A 1.744(6) . ?
S1A O2A 1.473(4) . ?
S1A C11A 1.766(6) . ?
S1A C10A 1.769(6) . ?
O1A C6A 1.308(7) . ?
N1A C1A 1.323(7) . ?
N1A C5A 1.387(7) . ?
C1A C2A 1.391(9) . ?
C2A C3A 1.364(9) . ?
C3A C4A 1.409(9) . ?
C4A C9A 1.413(8) . ?
C4A C5A 1.421(8) . ?
C5A C6A 1.407(8) . ?
C6A C7A 1.390(8) . ?
C7A C8A 1.392(9) . ?
C8A C9A 1.369(10) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 Pt1 O1 81.81(16) . . ?
N1 Pt1 S1 98.58(13) . . ?
O1 Pt1 S1 176.98(12) . . ?
N1 Pt1 Cl1 172.05(13) . . ?
O1 Pt1 Cl1 90.25(10) . . ?
S1 Pt1 Cl1 89.37(6) . . ?
O2 S1 C10 105.6(4) . . ?
O2 S1 C11 107.1(4) . . ?
C10 S1 C11 103.8(5) . . ?
O2 S1 Pt1 119.50(19) . . ?
C10 S1 Pt1 113.5(3) . . ?
C11 S1 Pt1 106.0(2) . . ?
C6 O1 Pt1 111.9(3) . . ?
C1 N1 C5 118.7(5) . . ?
C1 N1 Pt1 129.5(4) . . ?
C5 N1 Pt1 111.9(3) . . ?
N1 C1 C2 122.7(6) . . ?
C3 C2 C1 120.2(6) . . ?
C2 C3 C4 119.9(6) . . ?
C9 C4 C3 126.1(6) . . ?
C9 C4 C5 117.2(5) . . ?
C3 C4 C5 116.7(5) . . ?
N1 C5 C4 121.8(5) . . ?
N1 C5 C6 115.4(5) . . ?
C4 C5 C6 122.8(5) . . ?
O1 C6 C7 124.3(5) . . ?
O1 C6 C5 119.1(5) . . ?
C7 C6 C5 116.6(5) . . ?
C6 C7 C8 121.9(5) . . ?
C6 C7 I1 119.7(4) . . ?
C8 C7 I1 118.3(4) . . ?
C9 C8 C7 120.6(5) . . ?
C8 C9 C4 120.9(5) . . ?
C8 C9 Cl2 119.9(5) . . ?
C4 C9 Cl2 119.2(5) . . ?
O1A Pt1A N1A 81.70(17) . . ?
O1A Pt1A S1A 177.28(13) . . ?
N1A Pt1A S1A 99.67(13) . . ?
O1A Pt1A Cl1A 89.24(12) . . ?
N1A Pt1A Cl1A 170.92(13) . . ?
S1A Pt1A Cl1A 89.40(6) . . ?
O2A S1A C11A 108.1(3) . . ?
O2A S1A C10A 107.1(3) . . ?
C11A S1A C10A 102.2(3) . . ?
O2A S1A Pt1A 117.87(17) . . ?
C11A S1A Pt1A 108.1(2) . . ?
C10A S1A Pt1A 112.3(2) . . ?
C6A O1A Pt1A 112.6(4) . . ?
C1A N1A C5A 119.6(5) . . ?
C1A N1A Pt1A 129.8(4) . . ?
C5A N1A Pt1A 110.6(4) . . ?
N1A C1A C2A 122.3(6) . . ?
C3A C2A C1A 120.1(6) . . ?
C2A C3A C4A 119.8(6) . . ?
C3A C4A C9A 125.9(6) . . ?
C3A C4A C5A 117.9(5) . . ?
C9A C4A C5A 116.2(6) . . ?
N1A C5A C6A 116.2(5) . . ?
N1A C5A C4A 120.4(5) . . ?
C6A C5A C4A 123.4(5) . . ?
O1A C6A C7A 124.1(6) . . ?
O1A C6A C5A 118.9(5) . . ?
C7A C6A C5A 117.0(6) . . ?
C6A C7A C8A 121.2(6) . . ?
C6A C7A I1A 118.9(5) . . ?
C8A C7A I1A 120.0(5) . . ?
C9A C8A C7A 121.2(6) . . ?
C8A C9A C4A 121.1(6) . . ?
C8A C9A Cl2A 120.4(5) . . ?
C4A C9A Cl2A 118.5(5) . . ?

_diffrn_measured_fraction_theta_max 0.998
_diffrn_reflns_theta_full        25.70
_diffrn_measured_fraction_theta_full 0.998
_refine_diff_density_max         0.891
_refine_diff_density_min         -1.112
_refine_diff_density_rms         0.127


#=======================================================================_eof


# End of Crystallographic Information File





_database_code_depnum_ccdc_archive 'CCDC 883224'