# Electronic Supplementary Material (ESI) for Dalton Transactions
# This journal is © The Royal Society of Chemistry 2013
#######################################################################
#
# Cambridge Crystallographic Data Centre
# CCDC
#
#######################################################################
#
# This CIF contains data from an original supplementary publication
# deposited with the CCDC, and may include chemical, crystal,
# experimental, refinement, atomic coordinates,
# anisotropic displacement parameters and molecular geometry data,
# as required by the journal to which it was submitted.
#
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# fide research purposes only. It may contain copyright material
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data_13jul08a
_audit_creation_date 2013-07-08
_audit_creation_method
;
Olex2 1.2
(compiled Apr 23 2013 17:54:37, GUI svn.r4466)
;
_chemical_name_common ?
_chemical_name_systematic
;
?
;
_chemical_formula_moiety 'C58 H59 N4 O Si Y'
_chemical_formula_sum 'C58 H59 N4 O Si Y'
_chemical_formula_weight 945.09
_chemical_melting_point ?
_chemical_oxdiff_formula 'C58 H30 N4 Y Si'
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Y Y -2.7962 3.5667 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_space_group_crystal_system monoclinic
_space_group_IT_number 14
_space_group_name_H-M_alt 'P 1 21/c 1'
_space_group_name_Hall '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
_cell_length_a 13.1931(9)
_cell_length_b 19.6695(15)
_cell_length_c 20.343(2)
_cell_angle_alpha 90
_cell_angle_beta 106.481(9)
_cell_angle_gamma 90
_cell_volume 5062.2(8)
_cell_formula_units_Z 4
_cell_measurement_reflns_used 2343
_cell_measurement_temperature 180.00(10)
_cell_measurement_theta_max 22.0270
_cell_measurement_theta_min 3.4490
_exptl_absorpt_coefficient_mu 1.219
_exptl_absorpt_correction_T_max 1.00000
_exptl_absorpt_correction_T_min 0.97845
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb 1 2013,16:14:44)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour '? yellow'
_exptl_crystal_colour_lustre ?
_exptl_crystal_colour_primary yellow
_exptl_crystal_density_diffrn 1.240
_exptl_crystal_density_meas ?
_exptl_crystal_density_method ?
_exptl_crystal_description block
_exptl_crystal_F_000 1984
_exptl_crystal_size_max 0.2
_exptl_crystal_size_mid 0.2
_exptl_crystal_size_min 0.2
_exptl_special_details
;
?
;
_exptl_transmission_factor_max ?
_exptl_transmission_factor_min ?
_diffrn_reflns_av_R_equivalents 0.0715
_diffrn_reflns_av_unetI/netI 0.1421
_diffrn_reflns_Laue_measured_fraction_full 0.996
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max 16
_diffrn_reflns_limit_h_min -13
_diffrn_reflns_limit_k_max 19
_diffrn_reflns_limit_k_min -24
_diffrn_reflns_limit_l_max 18
_diffrn_reflns_limit_l_min -25
_diffrn_reflns_number 19286
_diffrn_reflns_point_group_measured_fraction_full 0.996
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 26.022
_diffrn_reflns_theta_min 3.259
_diffrn_ambient_temperature 180.00(10)
_diffrn_detector_area_resol_mean 10.3914
_diffrn_measured_fraction_theta_full 0.9939
_diffrn_measured_fraction_theta_max 0.8315
_diffrn_measurement_details
;
#__ type_ start__ end____ width___ exp.time_
1 omega -49.00 21.00 1.0000 20.0000
omega____ theta____ kappa____ phi______ frames
- 11.4055 -38.0000 -90.0000 70
#__ type_ start__ end____ width___ exp.time_
2 omega -80.00 13.00 1.0000 20.0000
omega____ theta____ kappa____ phi______ frames
- -12.1867 -57.0000 150.0000 93
;
_diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method '\w scans'
_diffrn_orient_matrix_UB_11 0.0093004000
_diffrn_orient_matrix_UB_12 -0.0343542000
_diffrn_orient_matrix_UB_13 -0.0071979000
_diffrn_orient_matrix_UB_21 -0.0059046000
_diffrn_orient_matrix_UB_22 -0.0099049000
_diffrn_orient_matrix_UB_23 0.0322627000
_diffrn_orient_matrix_UB_31 -0.0549244000
_diffrn_orient_matrix_UB_32 -0.0047384000
_diffrn_orient_matrix_UB_33 -0.0151945000
_diffrn_radiation_monochromator mirror
_diffrn_radiation_type 'Mo K\a'
_diffrn_radiation_wavelength 0.7107
_diffrn_source 'SuperNova (Mo) X-ray Source'
_reflns_Friedel_coverage 0.000
_reflns_Friedel_fraction_full .
_reflns_Friedel_fraction_max .
_reflns_number_gt 5568
_reflns_number_total 9934
_reflns_odcompleteness_completeness 99.39
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta 26.32
_reflns_special_details
;
Reflections were merged by SHELXL according to the crystal
class for the calculation of statistics and refinement.
_reflns_Friedel_fraction is defined as the number of unique
Friedel pairs measured divided by the number that would be
possible theoretically, ignoring centric projections and
systematic absences.
;
_reflns_threshold_expression 'I > 2\s(I)'
_computing_cell_refinement
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb 1 2013,16:14:44)
;
_computing_data_collection
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb 1 2013,16:14:44)
;
_computing_data_reduction
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb 1 2013,16:14:44)
;
_computing_molecular_graphics
;
O. V. Dolomanov, L. J. Bourhis, R. J. Gildea, J. A. K. Howard and H. Puschmann,
OLEX2: a complete structure solution, refinement and analysis program.
J. Appl. Cryst. (2009). 42, 339-341.
;
_computing_publication_material
;
O. V. Dolomanov, L. J. Bourhis, R. J. Gildea, J. A. K. Howard and H. Puschmann,
OLEX2: a complete structure solution, refinement and analysis program.
J. Appl. Cryst. (2009). 42, 339-341.
;
_computing_structure_refinement
;
SHELXL, G.M. Sheldrick, Acta Cryst.
(2008). A64, 112-122
;
_computing_structure_solution
;
SHELXS, G.M. Sheldrick, Acta Cryst.
(2008). A64, 112-122
;
_refine_diff_density_max 0.633
_refine_diff_density_min -0.717
_refine_diff_density_rms 0.077
_refine_ls_extinction_coef .
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.013
_refine_ls_hydrogen_treatment constr
_refine_ls_matrix_type full
_refine_ls_number_parameters 587
_refine_ls_number_reflns 9934
_refine_ls_number_restraints 0
_refine_ls_R_factor_all 0.1444
_refine_ls_R_factor_gt 0.0640
_refine_ls_restrained_S_all 1.013
_refine_ls_shift/su_max 0.000
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0388P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.1057
_refine_ls_wR_factor_ref 0.1344
_refine_special_details
;
?
;
_olex2_refinement_description
;
1. Fixed Uiso
At 1.2 times of:
All C(H) groups, All C(H,H) groups
At 1.5 times of:
All C(H,H,H) groups
2. Uiso/Uaniso restraints and constraints
Uanis(C56) = Uanis(C57)
3.a Secondary CH2 refined with riding coordinates:
C55(H55A,H55B), C56(H56A,H56B), C57(H57A,H57B), C58(H58A,H58B)
3.b Aromatic/amide H refined with riding coordinates:
C17(H17), C18(H18), C19(H19), C20(H20), C21(H21), C23(H23), C24(H24),
C25(H25), C26(H26), C27(H27), C29(H29), C30(H30), C31(H31), C32(H32), C33(H33),
C38(H38), C39(H39), C40(H40), C41(H41), C42(H42), C44(H44), C45(H45),
C46(H46), C47(H47), C48(H48), C50(H50), C51(H51), C52(H52), C53(H53), C54(H54)
3.c Idealised Me refined as rotating group:
C6(H6A,H6B,H6C), C7(H7A,H7B,H7C), C8(H8A,H8B,H8C), C9(H9A,H9B,H9C), C10(H10A,
H10B,H10C), C11(H11A,H11B,H11C), C12(H12A,H12B,H12C)
;
_atom_sites_solution_hydrogens geom
_atom_sites_solution_primary direct
_atom_sites_solution_secondary ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Y1 Y 0.28375(3) 0.70464(2) 0.27625(2) 0.02750(13) Uani 1 1 d . . . . .
Si1 Si 0.06316(9) 0.65160(7) 0.09612(7) 0.0419(4) Uani 1 1 d . . . . .
O1 O 0.3776(2) 0.77963(15) 0.22048(17) 0.0420(8) Uani 1 1 d . . . . .
N1 N 0.1312(2) 0.77971(17) 0.25246(19) 0.0322(9) Uani 1 1 d . . . . .
N2 N 0.1523(2) 0.70043(17) 0.33506(17) 0.0278(8) Uani 1 1 d . . . . .
N3 N 0.4395(2) 0.68981(17) 0.37054(19) 0.0361(9) Uani 1 1 d . . . . .
N4 N 0.3534(2) 0.78940(18) 0.36732(18) 0.0332(9) Uani 1 1 d . . . . .
C1 C 0.1800(3) 0.6293(2) 0.1697(2) 0.0305(10) Uani 1 1 d . . . . .
C2 C 0.2876(3) 0.6289(2) 0.1676(2) 0.0320(11) Uani 1 1 d . . . . .
C3 C 0.3484(3) 0.5921(2) 0.2240(2) 0.0343(11) Uani 1 1 d . . . . .
C4 C 0.2809(3) 0.5686(2) 0.2626(2) 0.0353(11) Uani 1 1 d . . . . .
C5 C 0.1777(3) 0.5899(2) 0.2281(2) 0.0327(11) Uani 1 1 d . . . . .
C6 C 0.0493(4) 0.5838(3) 0.0314(3) 0.089(2) Uani 1 1 d . . . . .
H6A H 0.1115 0.5826 0.0158 0.134 Uiso 1 1 calc R U . . .
H6B H -0.0114 0.5929 -0.0067 0.134 Uiso 1 1 calc R U . . .
H6C H 0.0407 0.5408 0.0514 0.134 Uiso 1 1 calc R U . . .
C7 C 0.0764(4) 0.7346(3) 0.0560(3) 0.0581(15) Uani 1 1 d . . . . .
H7A H 0.0928 0.7693 0.0906 0.087 Uiso 1 1 calc R U . . .
H7B H 0.0111 0.7455 0.0224 0.087 Uiso 1 1 calc R U . . .
H7C H 0.1321 0.7319 0.0343 0.087 Uiso 1 1 calc R U . . .
C8 C -0.0641(3) 0.6526(3) 0.1200(3) 0.075(2) Uani 1 1 d . . . . .
H8A H -0.0858 0.6068 0.1249 0.113 Uiso 1 1 calc R U . . .
H8B H -0.1175 0.6751 0.0847 0.113 Uiso 1 1 calc R U . . .
H8C H -0.0540 0.6764 0.1626 0.113 Uiso 1 1 calc R U . . .
C9 C 0.3292(3) 0.6534(2) 0.1100(3) 0.0465(13) Uani 1 1 d . . . . .
H9A H 0.2804 0.6854 0.0823 0.070 Uiso 1 1 calc R U . . .
H9B H 0.3373 0.6155 0.0822 0.070 Uiso 1 1 calc R U . . .
H9C H 0.3965 0.6750 0.1287 0.070 Uiso 1 1 calc R U . . .
C10 C 0.4636(3) 0.5736(3) 0.2370(3) 0.0550(15) Uani 1 1 d . . . . .
H10A H 0.5030 0.6133 0.2317 0.083 Uiso 1 1 calc R U . . .
H10B H 0.4705 0.5394 0.2049 0.083 Uiso 1 1 calc R U . . .
H10C H 0.4907 0.5564 0.2828 0.083 Uiso 1 1 calc R U . . .
C11 C 0.3122(4) 0.5215(2) 0.3236(3) 0.0541(14) Uani 1 1 d . . . . .
H11A H 0.3866 0.5258 0.3455 0.081 Uiso 1 1 calc R U . . .
H11B H 0.2963 0.4754 0.3086 0.081 Uiso 1 1 calc R U . . .
H11C H 0.2735 0.5333 0.3554 0.081 Uiso 1 1 calc R U . . .
C12 C 0.0809(3) 0.5685(2) 0.2487(3) 0.0496(14) Uani 1 1 d . . . . .
H12A H 0.1023 0.5482 0.2934 0.074 Uiso 1 1 calc R U . . .
H12B H 0.0412 0.5361 0.2162 0.074 Uiso 1 1 calc R U . . .
H12C H 0.0377 0.6076 0.2495 0.074 Uiso 1 1 calc R U . . .
C13 C 0.0970(3) 0.7532(2) 0.3026(2) 0.0305(10) Uani 1 1 d . . . . .
C14 C 0.0116(3) 0.7845(2) 0.3237(2) 0.0333(11) Uani 1 1 d . . . . .
C15 C -0.0544(3) 0.8124(2) 0.3426(2) 0.0338(11) Uani 1 1 d . . . . .
C16 C -0.1352(3) 0.8459(2) 0.3659(2) 0.0306(11) Uani 1 1 d . . . . .
C17 C -0.1878(3) 0.8117(2) 0.4055(3) 0.0429(13) Uani 1 1 d . . . . .
H17 H -0.1729 0.7663 0.4168 0.052 Uiso 1 1 calc R U . . .
C18 C -0.2637(4) 0.8463(3) 0.4285(3) 0.0571(15) Uani 1 1 d . . . . .
H18 H -0.2996 0.8239 0.4554 0.069 Uiso 1 1 calc R U . . .
C19 C -0.2856(3) 0.9132(3) 0.4114(3) 0.0544(15) Uani 1 1 d . . . . .
H19 H -0.3357 0.9361 0.4273 0.065 Uiso 1 1 calc R U . . .
C20 C -0.2347(4) 0.9465(3) 0.3715(3) 0.0503(14) Uani 1 1 d . . . . .
H20 H -0.2502 0.9919 0.3601 0.060 Uiso 1 1 calc R U . . .
C21 C -0.1608(3) 0.9135(2) 0.3480(2) 0.0399(12) Uani 1 1 d . . . . .
H21 H -0.1273 0.9362 0.3199 0.048 Uiso 1 1 calc R U . . .
C22 C 0.0803(3) 0.8375(2) 0.2163(2) 0.0368(11) Uani 1 1 d . . . . .
C23 C -0.0204(4) 0.8351(3) 0.1716(3) 0.0540(14) Uani 1 1 d . . . . .
H23 H -0.0579 0.7944 0.1666 0.065 Uiso 1 1 calc R U . . .
C24 C -0.0667(5) 0.8906(3) 0.1344(3) 0.0661(17) Uani 1 1 d . . . . .
H24 H -0.1345 0.8871 0.1046 0.079 Uiso 1 1 calc R U . . .
C25 C -0.0152(5) 0.9495(3) 0.1407(3) 0.0671(18) Uani 1 1 d . . . . .
H25 H -0.0470 0.9869 0.1151 0.081 Uiso 1 1 calc R U . . .
C26 C 0.0829(5) 0.9551(3) 0.1840(3) 0.0640(16) Uani 1 1 d . . . . .
H26 H 0.1182 0.9965 0.1886 0.077 Uiso 1 1 calc R U . . .
C27 C 0.1318(4) 0.8985(3) 0.2222(3) 0.0532(14) Uani 1 1 d . . . . .
H27 H 0.1997 0.9026 0.2518 0.064 Uiso 1 1 calc R U . . .
C28 C 0.1311(3) 0.6662(2) 0.3904(2) 0.0309(11) Uani 1 1 d . . . . .
C29 C 0.2178(3) 0.6445(2) 0.4426(3) 0.0379(12) Uani 1 1 d . . . . .
H29 H 0.2855 0.6552 0.4405 0.045 Uiso 1 1 calc R U . . .
C30 C 0.2058(4) 0.6077(2) 0.4974(3) 0.0451(13) Uani 1 1 d . . . . .
H30 H 0.2652 0.5932 0.5313 0.054 Uiso 1 1 calc R U . . .
C31 C 0.1074(4) 0.5923(2) 0.5024(3) 0.0518(14) Uani 1 1 d . . . . .
H31 H 0.0993 0.5682 0.5400 0.062 Uiso 1 1 calc R U . . .
C32 C 0.0211(4) 0.6126(2) 0.4515(3) 0.0477(13) Uani 1 1 d . . . . .
H32 H -0.0461 0.6020 0.4546 0.057 Uiso 1 1 calc R U . . .
C33 C 0.0316(3) 0.6487(2) 0.3953(3) 0.0404(12) Uani 1 1 d . . . . .
H33 H -0.0282 0.6612 0.3607 0.048 Uiso 1 1 calc R U . . .
C34 C 0.4295(3) 0.7491(2) 0.4012(2) 0.0336(11) Uani 1 1 d . . . . .
C35 C 0.4970(3) 0.7651(2) 0.4687(3) 0.0370(12) Uani 1 1 d . . . . .
C36 C 0.5525(3) 0.7712(2) 0.5260(3) 0.0391(12) Uani 1 1 d . . . . .
C37 C 0.6198(3) 0.7775(2) 0.5948(2) 0.0365(11) Uani 1 1 d . . . . .
C38 C 0.6765(3) 0.7224(3) 0.6277(3) 0.0493(14) Uani 1 1 d . . . . .
H38 H 0.6720 0.6812 0.6047 0.059 Uiso 1 1 calc R U . . .
C39 C 0.7400(4) 0.7277(3) 0.6944(3) 0.0584(15) Uani 1 1 d . . . . .
H39 H 0.7762 0.6898 0.7164 0.070 Uiso 1 1 calc R U . . .
C40 C 0.7497(3) 0.7881(3) 0.7277(3) 0.0580(15) Uani 1 1 d . . . . .
H40 H 0.7934 0.7915 0.7723 0.070 Uiso 1 1 calc R U . . .
C41 C 0.6959(4) 0.8439(3) 0.6962(3) 0.0600(16) Uani 1 1 d . . . . .
H41 H 0.7030 0.8853 0.7193 0.072 Uiso 1 1 calc R U . . .
C42 C 0.6309(3) 0.8387(3) 0.6300(3) 0.0484(14) Uani 1 1 d . . . . .
H42 H 0.5941 0.8768 0.6087 0.058 Uiso 1 1 calc R U . . .
C43 C 0.5267(3) 0.6475(2) 0.4044(3) 0.0460(13) Uani 1 1 d . . . . .
C44 C 0.5224(4) 0.6020(3) 0.4538(3) 0.0713(19) Uani 1 1 d . . . . .
H44 H 0.4606 0.5971 0.4668 0.086 Uiso 1 1 calc R U . . .
C45 C 0.6127(5) 0.5617(3) 0.4856(4) 0.088(2) Uani 1 1 d . . . . .
H45 H 0.6113 0.5320 0.5209 0.105 Uiso 1 1 calc R U . . .
C46 C 0.7016(5) 0.5671(3) 0.4640(4) 0.096(3) Uani 1 1 d . . . . .
H46 H 0.7602 0.5401 0.4838 0.115 Uiso 1 1 calc R U . . .
C47 C 0.7044(4) 0.6114(4) 0.4140(4) 0.096(3) Uani 1 1 d . . . . .
H47 H 0.7650 0.6150 0.3995 0.116 Uiso 1 1 calc R U . . .
C48 C 0.6181(4) 0.6515(3) 0.3842(3) 0.0678(18) Uani 1 1 d . . . . .
H48 H 0.6213 0.6819 0.3499 0.081 Uiso 1 1 calc R U . . .
C49 C 0.3424(3) 0.8559(2) 0.3906(2) 0.0348(11) Uani 1 1 d . . . . .
C50 C 0.4218(4) 0.9036(2) 0.3973(3) 0.0591(16) Uani 1 1 d . . . . .
H50 H 0.4855 0.8908 0.3898 0.071 Uiso 1 1 calc R U . . .
C51 C 0.4078(4) 0.9698(3) 0.4149(3) 0.0733(19) Uani 1 1 d . . . . .
H51 H 0.4624 1.0010 0.4197 0.088 Uiso 1 1 calc R U . . .
C52 C 0.3143(5) 0.9902(3) 0.4253(3) 0.0670(17) Uani 1 1 d . . . . .
H52 H 0.3048 1.0351 0.4366 0.080 Uiso 1 1 calc R U . . .
C53 C 0.2358(4) 0.9443(3) 0.4189(3) 0.0587(15) Uani 1 1 d . . . . .
H53 H 0.1719 0.9578 0.4255 0.070 Uiso 1 1 calc R U . . .
C54 C 0.2498(4) 0.8773(3) 0.4027(3) 0.0497(14) Uani 1 1 d . . . . .
H54 H 0.1957 0.8461 0.3998 0.060 Uiso 1 1 calc R U . . .
C55 C 0.4895(3) 0.7937(2) 0.2464(3) 0.0530(14) Uani 1 1 d . . . . .
H55A H 0.5298 0.7620 0.2273 0.064 Uiso 1 1 calc R U . . .
H55B H 0.5125 0.7898 0.2960 0.064 Uiso 1 1 calc R U . . .
C56 C 0.5048(4) 0.8650(3) 0.2249(4) 0.1031(19) Uani 1 1 d . . . . .
H56A H 0.5243 0.8949 0.2644 0.124 Uiso 1 1 calc R U . . .
H56B H 0.5601 0.8665 0.2020 0.124 Uiso 1 1 calc R U . . .
C57 C 0.4057(4) 0.8854(3) 0.1789(4) 0.1031(19) Uani 1 1 d . . . . .
H57A H 0.4163 0.9028 0.1367 0.124 Uiso 1 1 calc R U . . .
H57B H 0.3744 0.9212 0.1996 0.124 Uiso 1 1 calc R U . . .
C58 C 0.3353(4) 0.8259(3) 0.1643(3) 0.0566(15) Uani 1 1 d . . . . .
H58A H 0.2635 0.8388 0.1621 0.068 Uiso 1 1 calc R U . . .
H58B H 0.3355 0.8052 0.1210 0.068 Uiso 1 1 calc R U . . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Y1 0.0276(2) 0.0286(2) 0.0255(2) 0.0037(2) 0.00626(16) 0.0018(2)
Si1 0.0398(7) 0.0400(8) 0.0397(10) -0.0048(7) 0.0012(6) 0.0008(6)
O1 0.0405(17) 0.043(2) 0.044(2) 0.0104(17) 0.0132(15) -0.0068(15)
N1 0.0371(19) 0.033(2) 0.027(2) 0.0080(18) 0.0097(16) 0.0084(16)
N2 0.0312(17) 0.029(2) 0.024(2) 0.0040(19) 0.0094(15) 0.0037(17)
N3 0.0334(19) 0.031(2) 0.035(3) 0.0006(19) -0.0041(16) 0.0023(17)
N4 0.0356(19) 0.030(2) 0.029(2) 0.0012(19) 0.0005(16) 0.0028(18)
C1 0.034(2) 0.033(2) 0.028(3) -0.002(2) 0.0148(19) -0.003(2)
C2 0.037(2) 0.030(2) 0.030(3) -0.002(2) 0.011(2) -0.004(2)
C3 0.033(2) 0.037(3) 0.035(3) -0.002(2) 0.012(2) 0.004(2)
C4 0.050(3) 0.028(2) 0.030(3) -0.002(2) 0.014(2) 0.002(2)
C5 0.044(2) 0.032(3) 0.026(3) -0.005(2) 0.017(2) -0.005(2)
C6 0.100(4) 0.074(4) 0.059(5) -0.030(4) -0.032(3) 0.016(4)
C7 0.056(3) 0.066(4) 0.043(4) 0.012(3) 0.000(3) 0.003(3)
C8 0.041(3) 0.072(4) 0.108(6) 0.020(4) 0.013(3) 0.007(3)
C9 0.050(3) 0.054(3) 0.040(3) -0.001(3) 0.020(2) -0.005(2)
C10 0.045(3) 0.054(3) 0.063(4) -0.004(3) 0.011(3) 0.008(2)
C11 0.073(3) 0.045(3) 0.041(4) 0.011(3) 0.011(3) 0.002(3)
C12 0.053(3) 0.053(3) 0.048(4) -0.007(3) 0.023(3) -0.020(3)
C13 0.032(2) 0.030(3) 0.029(3) -0.003(2) 0.006(2) -0.001(2)
C14 0.031(2) 0.033(3) 0.033(3) 0.005(2) 0.005(2) 0.003(2)
C15 0.034(2) 0.035(3) 0.028(3) 0.000(2) 0.002(2) 0.000(2)
C16 0.025(2) 0.037(3) 0.029(3) -0.004(2) 0.0053(19) 0.003(2)
C17 0.041(2) 0.043(3) 0.047(3) 0.007(3) 0.016(2) -0.003(2)
C18 0.046(3) 0.079(4) 0.055(4) -0.003(3) 0.028(3) -0.006(3)
C19 0.037(3) 0.071(4) 0.055(4) -0.015(3) 0.014(3) 0.015(3)
C20 0.050(3) 0.045(3) 0.055(4) -0.003(3) 0.012(3) 0.018(3)
C21 0.043(3) 0.039(3) 0.037(3) 0.004(2) 0.009(2) 0.005(2)
C22 0.049(3) 0.036(3) 0.030(3) 0.008(2) 0.018(2) 0.014(2)
C23 0.052(3) 0.057(3) 0.049(4) 0.009(3) 0.008(3) 0.020(3)
C24 0.074(4) 0.071(4) 0.053(4) 0.017(4) 0.017(3) 0.037(4)
C25 0.107(5) 0.058(4) 0.043(4) 0.016(3) 0.034(4) 0.046(4)
C26 0.110(5) 0.036(3) 0.055(4) 0.010(3) 0.040(4) 0.011(3)
C27 0.073(3) 0.045(3) 0.042(4) 0.001(3) 0.017(3) 0.005(3)
C28 0.039(2) 0.024(2) 0.032(3) -0.004(2) 0.013(2) 0.004(2)
C29 0.045(3) 0.035(3) 0.034(3) 0.004(2) 0.012(2) 0.005(2)
C30 0.056(3) 0.045(3) 0.032(3) 0.004(3) 0.009(2) 0.007(3)
C31 0.080(4) 0.044(3) 0.040(4) 0.009(3) 0.031(3) 0.010(3)
C32 0.056(3) 0.046(3) 0.054(4) 0.003(3) 0.036(3) 0.002(3)
C33 0.041(3) 0.038(3) 0.046(4) 0.004(3) 0.019(2) 0.004(2)
C34 0.033(2) 0.038(3) 0.029(3) 0.004(2) 0.007(2) -0.007(2)
C35 0.029(2) 0.040(3) 0.038(3) 0.005(3) 0.003(2) -0.002(2)
C36 0.030(2) 0.047(3) 0.039(3) 0.009(3) 0.008(2) 0.004(2)
C37 0.031(2) 0.046(3) 0.031(3) 0.002(3) 0.007(2) 0.000(2)
C38 0.042(3) 0.064(4) 0.040(4) -0.002(3) 0.009(2) 0.005(3)
C39 0.049(3) 0.077(4) 0.043(4) 0.013(3) 0.003(3) 0.012(3)
C40 0.036(3) 0.094(5) 0.038(3) -0.005(4) 0.001(2) 0.003(3)
C41 0.047(3) 0.074(4) 0.058(4) -0.028(4) 0.014(3) -0.010(3)
C42 0.035(2) 0.063(4) 0.046(4) 0.001(3) 0.010(2) -0.001(2)
C43 0.036(3) 0.034(3) 0.055(4) 0.005(3) -0.009(2) 0.004(2)
C44 0.057(3) 0.057(4) 0.085(5) 0.033(4) -0.005(3) 0.003(3)
C45 0.086(4) 0.050(4) 0.092(6) 0.027(4) -0.030(4) -0.006(4)
C46 0.053(4) 0.049(4) 0.147(8) -0.004(5) -0.034(4) 0.011(3)
C47 0.048(4) 0.085(5) 0.137(8) 0.019(5) -0.004(4) 0.019(4)
C48 0.039(3) 0.063(4) 0.091(5) 0.011(4) 0.002(3) 0.007(3)
C49 0.036(2) 0.038(3) 0.030(3) 0.000(2) 0.008(2) -0.006(2)
C50 0.055(3) 0.041(3) 0.088(5) -0.018(3) 0.032(3) -0.006(3)
C51 0.078(4) 0.043(3) 0.108(6) -0.020(4) 0.043(4) -0.016(3)
C52 0.091(4) 0.045(3) 0.077(5) -0.016(3) 0.042(4) -0.003(3)
C53 0.072(4) 0.062(4) 0.052(4) -0.013(3) 0.033(3) 0.010(3)
C54 0.049(3) 0.060(4) 0.044(4) -0.010(3) 0.018(2) -0.004(3)
C55 0.039(3) 0.054(3) 0.069(4) 0.011(3) 0.021(2) -0.002(3)
C56 0.079(3) 0.075(3) 0.124(5) 0.043(3) -0.022(3) -0.033(3)
C57 0.079(3) 0.075(3) 0.124(5) 0.043(3) -0.022(3) -0.033(3)
C58 0.056(3) 0.054(3) 0.056(4) 0.018(3) 0.010(3) -0.005(3)
_geom_special_details
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Y1 O1 2.407(3) . ?
Y1 N1 2.431(3) . ?
Y1 N2 2.371(3) . ?
Y1 N3 2.398(3) . ?
Y1 N4 2.468(4) . ?
Y1 C1 2.662(4) . ?
Y1 C2 2.679(4) . ?
Y1 C3 2.696(4) . ?
Y1 C4 2.690(4) . ?
Y1 C5 2.689(4) . ?
Y1 C13 2.832(4) . ?
Y1 C34 2.856(5) . ?
Si1 C1 1.871(4) . ?
Si1 C6 1.846(6) . ?
Si1 C7 1.855(5) . ?
Si1 C8 1.875(5) . ?
O1 C55 1.446(5) . ?
O1 C58 1.444(5) . ?
N1 C13 1.334(5) . ?
N1 C22 1.416(5) . ?
N2 C13 1.331(5) . ?
N2 C28 1.406(5) . ?
N3 C34 1.348(5) . ?
N3 C43 1.428(5) . ?
N4 C34 1.310(5) . ?
N4 C49 1.413(5) . ?
C1 C2 1.433(5) . ?
C1 C5 1.425(6) . ?
C2 C3 1.401(6) . ?
C2 C9 1.508(6) . ?
C3 C4 1.421(6) . ?
C3 C10 1.511(5) . ?
C4 C5 1.408(6) . ?
C4 C11 1.509(6) . ?
C5 C12 1.512(5) . ?
C13 C14 1.451(6) . ?
C14 C15 1.183(5) . ?
C15 C16 1.443(6) . ?
C16 C17 1.378(6) . ?
C16 C21 1.395(6) . ?
C17 C18 1.396(6) . ?
C18 C19 1.372(7) . ?
C19 C20 1.360(7) . ?
C20 C21 1.366(6) . ?
C22 C23 1.382(6) . ?
C22 C27 1.367(6) . ?
C23 C24 1.370(7) . ?
C24 C25 1.330(7) . ?
C25 C26 1.347(8) . ?
C26 C27 1.406(7) . ?
C28 C29 1.389(6) . ?
C28 C33 1.387(5) . ?
C29 C30 1.375(6) . ?
C30 C31 1.365(6) . ?
C31 C32 1.363(7) . ?
C32 C33 1.387(6) . ?
C34 C35 1.443(6) . ?
C35 C36 1.194(6) . ?
C36 C37 1.435(7) . ?
C37 C38 1.377(6) . ?
C37 C42 1.387(6) . ?
C38 C39 1.381(7) . ?
C39 C40 1.355(7) . ?
C40 C41 1.365(7) . ?
C41 C42 1.381(7) . ?
C43 C44 1.361(7) . ?
C43 C48 1.381(6) . ?
C44 C45 1.424(7) . ?
C45 C46 1.368(9) . ?
C46 C47 1.349(9) . ?
C47 C48 1.376(7) . ?
C49 C50 1.384(6) . ?
C49 C54 1.378(6) . ?
C50 C51 1.376(6) . ?
C51 C52 1.370(6) . ?
C52 C53 1.352(7) . ?
C53 C54 1.383(6) . ?
C55 C56 1.501(7) . ?
C56 C57 1.432(7) . ?
C57 C58 1.472(7) . ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Y1 N1 92.37(11) . . ?
O1 Y1 N4 78.93(11) . . ?
O1 Y1 C1 99.91(12) . . ?
O1 Y1 C2 79.59(12) . . ?
O1 Y1 C3 93.13(12) . . ?
O1 Y1 C4 123.70(12) . . ?
O1 Y1 C5 128.81(12) . . ?
O1 Y1 C13 118.31(11) . . ?
O1 Y1 C34 85.72(11) . . ?
N1 Y1 N4 81.39(11) . . ?
N1 Y1 C1 88.32(12) . . ?
N1 Y1 C2 112.46(12) . . ?
N1 Y1 C3 139.17(13) . . ?
N1 Y1 C4 126.67(12) . . ?
N1 Y1 C5 96.96(12) . . ?
N1 Y1 C13 28.06(11) . . ?
N1 Y1 C34 107.54(12) . . ?
N2 Y1 O1 143.79(11) . . ?
N2 Y1 N1 55.89(11) . . ?
N2 Y1 N3 100.11(12) . . ?
N2 Y1 N4 79.34(11) . . ?
N2 Y1 C1 96.34(11) . . ?
N2 Y1 C2 125.78(11) . . ?
N2 Y1 C3 121.92(12) . . ?
N2 Y1 C4 91.54(12) . . ?
N2 Y1 C5 76.98(12) . . ?
N2 Y1 C13 27.88(11) . . ?
N2 Y1 C34 88.03(12) . . ?
N3 Y1 O1 90.75(11) . . ?
N3 Y1 N1 134.92(12) . . ?
N3 Y1 N4 55.21(11) . . ?
N3 Y1 C1 135.20(12) . . ?
N3 Y1 C2 112.33(12) . . ?
N3 Y1 C3 85.42(13) . . ?
N3 Y1 C4 86.87(13) . . ?
N3 Y1 C5 115.37(13) . . ?
N3 Y1 C13 118.91(13) . . ?
N3 Y1 C34 28.03(11) . . ?
N4 Y1 C1 169.56(12) . . ?
N4 Y1 C2 154.85(11) . . ?
N4 Y1 C3 139.30(12) . . ?
N4 Y1 C4 137.83(13) . . ?
N4 Y1 C5 152.22(12) . . ?
N4 Y1 C13 77.81(11) . . ?
N4 Y1 C34 27.27(11) . . ?
C1 Y1 C2 31.12(11) . . ?
C1 Y1 C3 50.89(12) . . ?
C1 Y1 C4 51.15(13) . . ?
C1 Y1 C5 30.89(12) . . ?
C1 Y1 C13 93.90(12) . . ?
C1 Y1 C34 163.04(13) . . ?
C2 Y1 C3 30.21(13) . . ?
C2 Y1 C4 50.50(13) . . ?
C2 Y1 C5 50.38(12) . . ?
C2 Y1 C13 124.42(12) . . ?
C2 Y1 C34 137.71(12) . . ?
C3 Y1 C13 137.83(12) . . ?
C3 Y1 C34 113.20(13) . . ?
C4 Y1 C3 30.59(12) . . ?
C4 Y1 C13 111.58(12) . . ?
C4 Y1 C34 112.54(14) . . ?
C5 Y1 C3 50.06(12) . . ?
C5 Y1 C4 30.34(12) . . ?
C5 Y1 C13 87.77(12) . . ?
C5 Y1 C34 136.96(13) . . ?
C13 Y1 C34 97.48(12) . . ?
C1 Si1 C8 113.0(2) . . ?
C6 Si1 C1 107.1(2) . . ?
C6 Si1 C7 108.9(3) . . ?
C6 Si1 C8 106.1(3) . . ?
C7 Si1 C1 113.5(2) . . ?
C7 Si1 C8 107.9(2) . . ?
C55 O1 Y1 123.6(3) . . ?
C58 O1 Y1 128.7(2) . . ?
C58 O1 C55 107.1(3) . . ?
C13 N1 Y1 92.9(2) . . ?
C13 N1 C22 119.9(3) . . ?
C22 N1 Y1 146.6(3) . . ?
C13 N2 Y1 95.7(2) . . ?
C13 N2 C28 124.4(3) . . ?
C28 N2 Y1 139.5(2) . . ?
C34 N3 Y1 95.2(2) . . ?
C34 N3 C43 116.9(4) . . ?
C43 N3 Y1 147.8(3) . . ?
C34 N4 Y1 93.1(3) . . ?
C34 N4 C49 121.3(4) . . ?
C49 N4 Y1 145.6(3) . . ?
Si1 C1 Y1 129.6(2) . . ?
C2 C1 Y1 75.1(2) . . ?
C2 C1 Si1 125.1(3) . . ?
C5 C1 Y1 75.6(2) . . ?
C5 C1 Si1 125.9(3) . . ?
C5 C1 C2 106.1(4) . . ?
C1 C2 Y1 73.8(2) . . ?
C1 C2 C9 127.2(4) . . ?
C3 C2 Y1 75.6(3) . . ?
C3 C2 C1 108.7(4) . . ?
C3 C2 C9 123.5(4) . . ?
C9 C2 Y1 124.0(3) . . ?
C2 C3 Y1 74.2(2) . . ?
C2 C3 C4 108.5(3) . . ?
C2 C3 C10 125.6(4) . . ?
C4 C3 Y1 74.5(2) . . ?
C4 C3 C10 125.6(4) . . ?
C10 C3 Y1 122.9(3) . . ?
C3 C4 Y1 74.9(2) . . ?
C3 C4 C11 125.9(4) . . ?
C5 C4 Y1 74.8(2) . . ?
C5 C4 C3 107.3(4) . . ?
C5 C4 C11 126.4(4) . . ?
C11 C4 Y1 122.2(3) . . ?
C1 C5 Y1 73.5(2) . . ?
C1 C5 C12 127.0(4) . . ?
C4 C5 Y1 74.9(2) . . ?
C4 C5 C1 109.3(3) . . ?
C4 C5 C12 123.6(4) . . ?
C12 C5 Y1 121.8(3) . . ?
N1 C13 Y1 59.0(2) . . ?
N1 C13 C14 121.3(4) . . ?
N2 C13 Y1 56.43(19) . . ?
N2 C13 N1 115.3(3) . . ?
N2 C13 C14 123.2(4) . . ?
C14 C13 Y1 171.5(3) . . ?
C15 C14 C13 176.7(5) . . ?
C14 C15 C16 179.5(5) . . ?
C17 C16 C15 120.7(4) . . ?
C17 C16 C21 119.6(4) . . ?
C21 C16 C15 119.7(4) . . ?
C16 C17 C18 119.1(4) . . ?
C19 C18 C17 120.2(5) . . ?
C20 C19 C18 120.6(5) . . ?
C19 C20 C21 120.2(5) . . ?
C20 C21 C16 120.3(4) . . ?
C23 C22 N1 122.6(4) . . ?
C27 C22 N1 120.6(4) . . ?
C27 C22 C23 116.7(5) . . ?
C24 C23 C22 122.0(5) . . ?
C25 C24 C23 120.4(6) . . ?
C24 C25 C26 120.3(6) . . ?
C25 C26 C27 120.1(6) . . ?
C22 C27 C26 120.5(5) . . ?
C29 C28 N2 116.8(4) . . ?
C33 C28 N2 125.7(4) . . ?
C33 C28 C29 117.3(4) . . ?
C30 C29 C28 121.5(4) . . ?
C31 C30 C29 120.6(5) . . ?
C32 C31 C30 119.0(5) . . ?
C31 C32 C33 121.2(4) . . ?
C32 C33 C28 120.3(4) . . ?
N3 C34 Y1 56.7(2) . . ?
N3 C34 C35 121.0(4) . . ?
N4 C34 Y1 59.7(2) . . ?
N4 C34 N3 116.1(4) . . ?
N4 C34 C35 122.9(4) . . ?
C35 C34 Y1 172.6(3) . . ?
C36 C35 C34 173.1(5) . . ?
C35 C36 C37 179.1(6) . . ?
C38 C37 C36 120.4(5) . . ?
C38 C37 C42 118.0(5) . . ?
C42 C37 C36 121.6(4) . . ?
C37 C38 C39 120.8(5) . . ?
C40 C39 C38 120.1(5) . . ?
C39 C40 C41 120.5(5) . . ?
C40 C41 C42 119.6(5) . . ?
C41 C42 C37 120.9(5) . . ?
C44 C43 N3 122.8(4) . . ?
C44 C43 C48 118.7(5) . . ?
C48 C43 N3 118.4(5) . . ?
C43 C44 C45 119.8(6) . . ?
C46 C45 C44 119.6(6) . . ?
C47 C46 C45 120.1(6) . . ?
C46 C47 C48 120.4(7) . . ?
C47 C48 C43 121.3(6) . . ?
C50 C49 N4 120.9(4) . . ?
C54 C49 N4 121.6(4) . . ?
C54 C49 C50 117.4(4) . . ?
C51 C50 C49 120.8(5) . . ?
C52 C51 C50 120.7(5) . . ?
C53 C52 C51 119.2(5) . . ?
C52 C53 C54 120.6(5) . . ?
C49 C54 C53 121.2(5) . . ?
O1 C55 C56 106.3(4) . . ?
C57 C56 C55 106.2(5) . . ?
C56 C57 C58 108.4(5) . . ?
O1 C58 C57 105.2(4) . . ?
_shelx_estimated_absorpt_T_max ?
_shelx_estimated_absorpt_T_min ?
_shelx_hkl_checksum 1630
_shelx_hkl_file
;
0 0 -4 6888.16 248.036 1
0 0 -5 96.9975 66.1621 1
0 0 -6 32088.0 649.138 1
0 0 -7 339.651 107.142 1
0 0 -8 13184.6 485.770 1
0 0 -9-27.1338 96.9655 1
0 0 -10 1778.84 206.627 1
0 0 -11 197.998 130.978 1
0 0 -12 172.067 136.946 1
0 0 -13 68.8901 151.212 1
0 0 -14-20.7780 145.881 1
0 0 -15-65.5763 147.438 1
0 0 -16 5290.03 461.483 1
0 0 -17 124.796 144.096 1
0 0 -18 3962.55 429.101 1
0 0 -19 65.4446 157.980 1
0 0 -20 1557.46 327.720 1
0 0 -21-201.041 197.069 1
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17 -6 -3 0.64313 149.152 2
17 -6 -2 173.199 195.904 2
17 -6 -1 64.1028 133.021 2
17 -7 -12-372.149 209.592 2
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17 -7 -9 197.476 216.006 2
17 -7 -8-0.64601 169.240 2
17 -7 -7 427.198 230.226 2
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17 -7 -5 306.436 196.841 2
17 -7 -4 31.0575 153.410 2
17 -7 -3 46.9802 183.156 2
0 0 0 0.00 0.00 0
TITL 13Jul08a in P2(1)/c
REM P2(1)/c (#14 in standard setting)
CELL 0.71073 13.193064 19.669489 20.343121 90.0000 106.4808 90.0000
ZERR 4.00 0.000932 0.001453 0.002216 0.0000 0.0086 0.0000
LATT 1
SYMM -x, y+1/2,-z+1/2
SFAC C H N Si Y
UNIT 232.00 120.00 16.00 4.00 4.00
TREF
HKLF 4
END
;
_shelx_res_checksum 75567
_shelx_res_file
;
TITL 13Jul08a in P21/c #14
CELL 0.71073 13.19306 19.66949 20.34312 90 106.4808 90
ZERR 4 0.00093 0.00145 0.00222 0 0.0086 0
LATT 1
SYMM -X,0.5+Y,0.5-Z
SFAC C H N Si Y O
UNIT 232 236 16 4 4 4
EADP C56 C57
L.S. 8
PLAN 10
REM reset to P21/c #14
BOND
fmap 2
ACTA
SHEL 999 0.81
REM G:/13Jul08a/13Jul08a/struct/olex2_13Jul08a/13Jul08a.hkl
WGHT 0.038800
FVAR 0.93019
Y1 5 0.283755 0.704644 0.276254 11.00000 0.02758 0.02864 =
0.02549 0.00370 0.00626 0.00184
SI1 4 0.063164 0.651599 0.096124 11.00000 0.03977 0.04004 =
0.03974 -0.00477 0.00118 0.00083
O1 6 0.377604 0.779634 0.220485 11.00000 0.04052 0.04267 =
0.04359 0.01039 0.01318 -0.00682
N1 3 0.131232 0.779711 0.252461 11.00000 0.03707 0.03256 =
0.02727 0.00803 0.00975 0.00838
N2 3 0.152305 0.700431 0.335057 11.00000 0.03117 0.02927 =
0.02390 0.00403 0.00936 0.00370
N3 3 0.439472 0.689812 0.370539 11.00000 0.03342 0.03140 =
0.03496 0.00058 -0.00406 0.00235
N4 3 0.353444 0.789404 0.367321 11.00000 0.03556 0.02981 =
0.02880 0.00124 0.00051 0.00283
C1 1 0.179993 0.629275 0.169716 11.00000 0.03396 0.03267 =
0.02848 -0.00229 0.01480 -0.00344
C2 1 0.287603 0.628857 0.167563 11.00000 0.03662 0.03048 =
0.02996 -0.00182 0.01136 -0.00432
C3 1 0.348439 0.592127 0.224025 11.00000 0.03279 0.03669 =
0.03489 -0.00156 0.01180 0.00367
C4 1 0.280917 0.568567 0.262557 11.00000 0.04964 0.02782 =
0.03005 -0.00186 0.01378 0.00184
C5 1 0.177672 0.589938 0.228119 11.00000 0.04425 0.03172 =
0.02608 -0.00513 0.01661 -0.00515
C6 1 0.049342 0.583842 0.031374 11.00000 0.10033 0.07422 =
0.05918 -0.02981 -0.03157 0.01626
AFIX 137
H6A 2 0.111491 0.582627 0.015757 11.00000 -1.50000
H6B 2 -0.011400 0.592857 -0.006709 11.00000 -1.50000
H6C 2 0.040748 0.540808 0.051404 11.00000 -1.50000
AFIX 0
C7 1 0.076397 0.734571 0.056026 11.00000 0.05568 0.06624 =
0.04348 0.01211 -0.00048 0.00279
AFIX 137
H7A 2 0.092810 0.769284 0.090609 11.00000 -1.50000
H7B 2 0.011135 0.745504 0.022385 11.00000 -1.50000
H7C 2 0.132095 0.731871 0.034331 11.00000 -1.50000
AFIX 0
C8 1 -0.064069 0.652588 0.119989 11.00000 0.04071 0.07168 =
0.10773 0.02031 0.01282 0.00718
AFIX 137
H8A 2 -0.085844 0.606750 0.124887 11.00000 -1.50000
H8B 2 -0.117534 0.675135 0.084732 11.00000 -1.50000
H8C 2 -0.053968 0.676387 0.162566 11.00000 -1.50000
AFIX 0
C9 1 0.329226 0.653414 0.109968 11.00000 0.04997 0.05400 =
0.03989 -0.00094 0.02003 -0.00470
AFIX 137
H9A 2 0.280404 0.685414 0.082336 11.00000 -1.50000
H9B 2 0.337270 0.615453 0.082212 11.00000 -1.50000
H9C 2 0.396508 0.675013 0.128678 11.00000 -1.50000
AFIX 0
C10 1 0.463645 0.573614 0.237044 11.00000 0.04522 0.05373 =
0.06349 -0.00405 0.01117 0.00806
AFIX 137
H10A 2 0.502972 0.613273 0.231694 11.00000 -1.50000
H10B 2 0.470468 0.539446 0.204870 11.00000 -1.50000
H10C 2 0.490667 0.556364 0.282837 11.00000 -1.50000
AFIX 0
C11 1 0.312197 0.521493 0.323572 11.00000 0.07310 0.04523 =
0.04064 0.01108 0.01098 0.00239
AFIX 137
H11A 2 0.386602 0.525816 0.345534 11.00000 -1.50000
H11B 2 0.296346 0.475431 0.308561 11.00000 -1.50000
H11C 2 0.273539 0.533287 0.355433 11.00000 -1.50000
AFIX 0
C12 1 0.080895 0.568512 0.248685 11.00000 0.05311 0.05301 =
0.04810 -0.00657 0.02313 -0.01991
AFIX 137
H12A 2 0.102342 0.548208 0.293418 11.00000 -1.50000
H12B 2 0.041165 0.536111 0.216175 11.00000 -1.50000
H12C 2 0.037731 0.607614 0.249519 11.00000 -1.50000
AFIX 0
C13 1 0.097021 0.753196 0.302628 11.00000 0.03185 0.02968 =
0.02853 -0.00271 0.00637 -0.00067
C14 1 0.011635 0.784527 0.323651 11.00000 0.03063 0.03345 =
0.03322 0.00465 0.00492 0.00337
C15 1 -0.054389 0.812400 0.342613 11.00000 0.03374 0.03536 =
0.02834 0.00044 0.00234 0.00001
C16 1 -0.135246 0.845852 0.365894 11.00000 0.02474 0.03684 =
0.02876 -0.00429 0.00535 0.00310
C17 1 -0.187805 0.811696 0.405529 11.00000 0.04122 0.04313 =
0.04674 0.00738 0.01622 -0.00300
AFIX 43
H17 2 -0.172900 0.766254 0.416844 11.00000 -1.20000
AFIX 0
C18 1 -0.263742 0.846290 0.428452 11.00000 0.04604 0.07918 =
0.05477 -0.00289 0.02843 -0.00560
AFIX 43
H18 2 -0.299597 0.823867 0.455362 11.00000 -1.20000
AFIX 0
C19 1 -0.285619 0.913242 0.411403 11.00000 0.03671 0.07149 =
0.05547 -0.01500 0.01381 0.01480
AFIX 43
H19 2 -0.335718 0.936104 0.427298 11.00000 -1.20000
AFIX 0
C20 1 -0.234685 0.946489 0.371455 11.00000 0.04979 0.04450 =
0.05475 -0.00348 0.01194 0.01769
AFIX 43
H20 2 -0.250238 0.991857 0.360101 11.00000 -1.20000
AFIX 0
C21 1 -0.160784 0.913493 0.347954 11.00000 0.04255 0.03896 =
0.03659 0.00351 0.00877 0.00465
AFIX 43
H21 2 -0.127310 0.936217 0.319852 11.00000 -1.20000
AFIX 0
C22 1 0.080348 0.837532 0.216274 11.00000 0.04880 0.03597 =
0.02992 0.00800 0.01791 0.01393
C23 1 -0.020367 0.835055 0.171582 11.00000 0.05199 0.05703 =
0.04919 0.00916 0.00825 0.02038
AFIX 43
H23 2 -0.057870 0.794438 0.166587 11.00000 -1.20000
AFIX 0
C24 1 -0.066687 0.890618 0.134390 11.00000 0.07440 0.07080 =
0.05254 0.01693 0.01722 0.03714
AFIX 43
H24 2 -0.134500 0.887149 0.104587 11.00000 -1.20000
AFIX 0
C25 1 -0.015177 0.949499 0.140684 11.00000 0.10732 0.05833 =
0.04322 0.01600 0.03366 0.04559
AFIX 43
H25 2 -0.046979 0.986919 0.115090 11.00000 -1.20000
AFIX 0
C26 1 0.082859 0.955126 0.183984 11.00000 0.11029 0.03638 =
0.05525 0.00978 0.03969 0.01092
AFIX 43
H26 2 0.118225 0.996529 0.188586 11.00000 -1.20000
AFIX 0
C27 1 0.131820 0.898538 0.222231 11.00000 0.07324 0.04512 =
0.04185 0.00051 0.01734 0.00468
AFIX 43
H27 2 0.199713 0.902632 0.251798 11.00000 -1.20000
AFIX 0
C28 1 0.131085 0.666187 0.390353 11.00000 0.03857 0.02405 =
0.03189 -0.00447 0.01301 0.00381
C29 1 0.217788 0.644535 0.442612 11.00000 0.04512 0.03519 =
0.03375 0.00382 0.01172 0.00483
AFIX 43
H29 2 0.285478 0.655183 0.440508 11.00000 -1.20000
AFIX 0
C30 1 0.205784 0.607717 0.497378 11.00000 0.05632 0.04480 =
0.03197 0.00427 0.00899 0.00708
AFIX 43
H30 2 0.265206 0.593223 0.531288 11.00000 -1.20000
AFIX 0
C31 1 0.107370 0.592265 0.502386 11.00000 0.07965 0.04396 =
0.04011 0.00864 0.03061 0.01005
AFIX 43
H31 2 0.099318 0.568247 0.539963 11.00000 -1.20000
AFIX 0
C32 1 0.021080 0.612550 0.451508 11.00000 0.05613 0.04562 =
0.05381 0.00257 0.03598 0.00210
AFIX 43
H32 2 -0.046140 0.601980 0.454567 11.00000 -1.20000
AFIX 0
C33 1 0.031647 0.648658 0.395266 11.00000 0.04125 0.03783 =
0.04610 0.00432 0.01904 0.00429
AFIX 43
H33 2 -0.028243 0.661185 0.360666 11.00000 -1.20000
AFIX 0
C34 1 0.429510 0.749146 0.401237 11.00000 0.03288 0.03809 =
0.02872 0.00424 0.00718 -0.00686
C35 1 0.497034 0.765133 0.468683 11.00000 0.02940 0.03969 =
0.03765 0.00543 0.00262 -0.00177
C36 1 0.552476 0.771206 0.526006 11.00000 0.03001 0.04722 =
0.03875 0.00905 0.00777 0.00378
C37 1 0.619829 0.777525 0.594834 11.00000 0.03133 0.04632 =
0.03084 0.00245 0.00694 0.00037
C38 1 0.676525 0.722446 0.627676 11.00000 0.04217 0.06358 =
0.04036 -0.00224 0.00901 0.00516
AFIX 43
H38 2 0.672006 0.681195 0.604680 11.00000 -1.20000
AFIX 0
C39 1 0.740022 0.727711 0.694353 11.00000 0.04921 0.07712 =
0.04261 0.01271 0.00305 0.01226
AFIX 43
H39 2 0.776179 0.689756 0.716419 11.00000 -1.20000
AFIX 0
C40 1 0.749746 0.788076 0.727688 11.00000 0.03650 0.09408 =
0.03757 -0.00544 0.00082 0.00310
AFIX 43
H40 2 0.793446 0.791467 0.772343 11.00000 -1.20000
AFIX 0
C41 1 0.695909 0.843932 0.696242 11.00000 0.04696 0.07425 =
0.05789 -0.02847 0.01364 -0.00989
AFIX 43
H41 2 0.702953 0.885256 0.719317 11.00000 -1.20000
AFIX 0
C42 1 0.630938 0.838749 0.629989 11.00000 0.03511 0.06331 =
0.04563 0.00105 0.00958 -0.00079
AFIX 43
H42 2 0.594141 0.876807 0.608655 11.00000 -1.20000
AFIX 0
C43 1 0.526719 0.647534 0.404352 11.00000 0.03560 0.03420 =
0.05503 0.00487 -0.00858 0.00429
C44 1 0.522395 0.601967 0.453829 11.00000 0.05667 0.05656 =
0.08514 0.03319 -0.00492 0.00268
AFIX 43
H44 2 0.460649 0.597128 0.466832 11.00000 -1.20000
AFIX 0
C45 1 0.612748 0.561712 0.485633 11.00000 0.08584 0.05030 =
0.09224 0.02701 -0.03018 -0.00616
AFIX 43
H45 2 0.611345 0.531957 0.520892 11.00000 -1.20000
AFIX 0
C46 1 0.701589 0.567077 0.464009 11.00000 0.05326 0.04903 =
0.14672 -0.00378 -0.03431 0.01103
AFIX 43
H46 2 0.760167 0.540082 0.483822 11.00000 -1.20000
AFIX 0
C47 1 0.704390 0.611450 0.413998 11.00000 0.04844 0.08493 =
0.13749 0.01920 -0.00369 0.01894
AFIX 43
H47 2 0.765035 0.614983 0.399546 11.00000 -1.20000
AFIX 0
C48 1 0.618077 0.651517 0.384234 11.00000 0.03938 0.06305 =
0.09069 0.01128 0.00158 0.00714
AFIX 43
H48 2 0.621342 0.681900 0.349866 11.00000 -1.20000
AFIX 0
C49 1 0.342409 0.855916 0.390636 11.00000 0.03646 0.03753 =
0.02950 -0.00023 0.00797 -0.00569
C50 1 0.421849 0.903629 0.397313 11.00000 0.05506 0.04083 =
0.08845 -0.01827 0.03161 -0.00610
AFIX 43
H50 2 0.485523 0.890797 0.389846 11.00000 -1.20000
AFIX 0
C51 1 0.407777 0.969784 0.414857 11.00000 0.07844 0.04305 =
0.10841 -0.02031 0.04279 -0.01577
AFIX 43
H51 2 0.462366 1.000993 0.419712 11.00000 -1.20000
AFIX 0
C52 1 0.314261 0.990197 0.425253 11.00000 0.09078 0.04483 =
0.07664 -0.01586 0.04192 -0.00293
AFIX 43
H52 2 0.304847 1.035109 0.436557 11.00000 -1.20000
AFIX 0
C53 1 0.235804 0.944275 0.418884 11.00000 0.07198 0.06167 =
0.05163 -0.01334 0.03265 0.00965
AFIX 43
H53 2 0.171858 0.957838 0.425463 11.00000 -1.20000
AFIX 0
C54 1 0.249816 0.877318 0.402673 11.00000 0.04870 0.05998 =
0.04362 -0.01005 0.01849 -0.00362
AFIX 43
H54 2 0.195743 0.846144 0.399840 11.00000 -1.20000
AFIX 0
C55 1 0.489469 0.793700 0.246420 11.00000 0.03911 0.05395 =
0.06927 0.01056 0.02063 -0.00225
AFIX 23
H55A 2 0.529801 0.761972 0.227319 11.00000 -1.20000
H55B 2 0.512457 0.789782 0.295980 11.00000 -1.20000
AFIX 0
C56 1 0.504769 0.865026 0.224855 11.00000 0.07907 0.07516 =
0.12412 0.04291 -0.02153 -0.03344
AFIX 23
H56A 2 0.524286 0.894897 0.264392 11.00000 -1.20000
H56B 2 0.560055 0.866512 0.202020 11.00000 -1.20000
AFIX 0
C57 1 0.405724 0.885435 0.178908 11.00000 0.07907 0.07516 =
0.12412 0.04291 -0.02153 -0.03344
AFIX 23
H57A 2 0.416332 0.902786 0.136717 11.00000 -1.20000
H57B 2 0.374389 0.921170 0.199601 11.00000 -1.20000
AFIX 0
C58 1 0.335328 0.825875 0.164281 11.00000 0.05633 0.05424 =
0.05554 0.01773 0.00989 -0.00523
AFIX 23
H58A 2 0.263479 0.838757 0.162108 11.00000 -1.20000
H58B 2 0.335532 0.805161 0.121047 11.00000 -1.20000
AFIX 0
HKLF 4
REM 13Jul08a in P21/c #14
REM R1 = 0.0640 for 5568 Fo > 4sig(Fo) and 0.1444 for all 9934 data
REM 587 parameters refined using 0 restraints
END
WGHT 0.0385 0.0000
REM Highest difference peak 0.633, deepest hole -0.717, 1-sigma level 0.077
Q1 1 0.4373 0.8548 0.1485 11.00000 0.05 0.61
Q2 1 0.2775 0.7743 0.2591 11.00000 0.05 0.40
Q3 1 0.3653 0.8821 0.1943 11.00000 0.05 0.37
Q4 1 0.1856 0.7129 0.2732 11.00000 0.05 0.36
Q5 1 0.2858 0.8906 0.2770 11.00000 0.05 0.36
Q6 1 0.1610 0.7013 0.1710 11.00000 0.05 0.35
Q7 1 0.3592 0.7452 0.2663 11.00000 0.05 0.35
Q8 1 0.1989 0.7639 0.2500 11.00000 0.05 0.32
Q9 1 0.3271 0.7289 0.3074 11.00000 0.05 0.32
Q10 1 0.3198 0.6688 0.3907 11.00000 0.05 0.32
;
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelxl_version_number 2013-3
_database_code_depnum_ccdc_archive 'CCDC 949450'
#######################################################################
#
# Cambridge Crystallographic Data Centre
# CCDC
#
#######################################################################
#
# This CIF contains data from an original supplementary publication
# deposited with the CCDC, and may include chemical, crystal,
# experimental, refinement, atomic coordinates,
# anisotropic displacement parameters and molecular geometry data,
# as required by the journal to which it was submitted.
#
# This CIF is provided on the understanding that it is used for bona
# fide research purposes only. It may contain copyright material
# of the CCDC or of third parties, and may not be copied or further
# disseminated in any form, whether machine-readable or not,
# except for the purpose of generating routine backup copies
# on your local computer system.
#
# For further information on the CCDC, data deposition and
# data retrieval see:
# www.ccdc.cam.ac.uk
#
# Bona fide researchers may freely download Mercury and enCIFer
# from this site to visualise CIF-encoded structures and
# to carry out CIF format checking respectively.
#
data_13mar11g
_audit_creation_date 2013-06-17
_audit_creation_method
;
Olex2 1.2
(compiled Apr 9 2013 14:06:00, GUI svn.r4458)
;
_chemical_name_common ?
_chemical_name_systematic
;
?
;
_chemical_formula_moiety '2(C41 H41 N2 Si Y)'
_chemical_formula_sum 'C82 H82 N4 Si2 Y2'
_chemical_formula_weight 1357.51
_chemical_melting_point ?
_chemical_oxdiff_formula 'C82 H82 N4 Si2 Y2'
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Y Y -2.7962 3.5667 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_space_group_crystal_system triclinic
_space_group_IT_number 2
_space_group_name_H-M_alt 'P -1'
_space_group_name_Hall '-P 1'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
_cell_length_a 13.1259(3)
_cell_length_b 16.2231(5)
_cell_length_c 16.4294(5)
_cell_angle_alpha 90.497(2)
_cell_angle_beta 90.033(2)
_cell_angle_gamma 93.204(2)
_cell_volume 3492.93(16)
_cell_formula_units_Z 2
_cell_measurement_reflns_used 17636
_cell_measurement_temperature 100.00(10)
_cell_measurement_theta_max 29.0730
_cell_measurement_theta_min 3.2240
_exptl_absorpt_coefficient_mu 1.735
_exptl_absorpt_correction_T_max 1.00000
_exptl_absorpt_correction_T_min 0.78296
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb 1 2013,16:14:44)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_density_diffrn 1.291
_exptl_crystal_density_meas ?
_exptl_crystal_density_method ?
_exptl_crystal_F_000 1416
_exptl_crystal_size_max 0.1
_exptl_crystal_size_mid 0.1
_exptl_crystal_size_min 0.1
_exptl_special_details
;
?
;
_exptl_transmission_factor_max ?
_exptl_transmission_factor_min ?
_diffrn_reflns_av_R_equivalents 0.0715
_diffrn_reflns_av_unetI/netI 0.0637
_diffrn_reflns_Laue_measured_fraction_full 0.995
_diffrn_reflns_Laue_measured_fraction_max 0.995
_diffrn_reflns_limit_h_max 16
_diffrn_reflns_limit_h_min -16
_diffrn_reflns_limit_k_max 20
_diffrn_reflns_limit_k_min -20
_diffrn_reflns_limit_l_max 20
_diffrn_reflns_limit_l_min -20
_diffrn_reflns_number 52519
_diffrn_reflns_point_group_measured_fraction_full 0.995
_diffrn_reflns_point_group_measured_fraction_max 0.995
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 26.022
_diffrn_reflns_theta_min 2.925
_diffrn_ambient_temperature 100.00(10)
_diffrn_detector_area_resol_mean 10.3914
_diffrn_measured_fraction_theta_full 0.9983
_diffrn_measured_fraction_theta_max 0.8271
_diffrn_measurement_details
;
#__ type_ start__ end____ width___ exp.time_
1 omega -64.00 36.00 1.0000 60.0000
omega____ theta____ kappa____ phi______ frames
- 10.8993 -38.0000 -120.0000 100
#__ type_ start__ end____ width___ exp.time_
2 omega -10.00 77.00 1.0000 60.0000
omega____ theta____ kappa____ phi______ frames
- 10.8993 57.0000 -180.0000 87
#__ type_ start__ end____ width___ exp.time_
3 omega -14.00 86.00 1.0000 60.0000
omega____ theta____ kappa____ phi______ frames
- 10.8993 77.0000 -60.0000 100
#__ type_ start__ end____ width___ exp.time_
4 omega -16.00 72.00 1.0000 60.0000
omega____ theta____ kappa____ phi______ frames
- 10.8993 38.0000 90.0000 88
#__ type_ start__ end____ width___ exp.time_
5 omega -63.00 40.00 1.0000 60.0000
omega____ theta____ kappa____ phi______ frames
- 10.8993 -57.0000 30.0000 103
#__ type_ start__ end____ width___ exp.time_
6 omega -20.00 53.00 1.0000 60.0000
omega____ theta____ kappa____ phi______ frames
- 10.8993 -99.0000 150.0000 73
#__ type_ start__ end____ width___ exp.time_
7 omega -70.00 -25.00 1.0000 60.0000
omega____ theta____ kappa____ phi______ frames
- -11.6805 126.0000 -131.8788 45
#__ type_ start__ end____ width___ exp.time_
8 omega -74.00 -34.00 1.0000 60.0000
omega____ theta____ kappa____ phi______ frames
- -11.6805 133.0000 102.6494 40
;
_diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, Atlas'
_diffrn_measurement_method '\w scans'
_diffrn_orient_matrix_UB_11 0.0142992000
_diffrn_orient_matrix_UB_12 0.0337781000
_diffrn_orient_matrix_UB_13 0.0260554000
_diffrn_orient_matrix_UB_21 0.0517885000
_diffrn_orient_matrix_UB_22 -0.0100505000
_diffrn_orient_matrix_UB_23 -0.0028136000
_diffrn_orient_matrix_UB_31 0.0065390000
_diffrn_orient_matrix_UB_32 0.0259942000
_diffrn_orient_matrix_UB_33 -0.0343106000
_diffrn_radiation_monochromator mirror
_diffrn_radiation_type 'Mo K\a'
_diffrn_radiation_wavelength 0.7107
_diffrn_source 'SuperNova (Mo) X-ray Source'
_reflns_Friedel_coverage 0.000
_reflns_Friedel_fraction_full .
_reflns_Friedel_fraction_max .
_reflns_number_gt 11383
_reflns_number_total 13686
_reflns_odcompleteness_completeness 99.83
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta 25.97
_reflns_special_details
;
Reflections were merged by SHELXL according to the crystal
class for the calculation of statistics and refinement.
_reflns_Friedel_fraction is defined as the number of unique
Friedel pairs measured divided by the number that would be
possible theoretically, ignoring centric projections and
systematic absences.
;
_reflns_threshold_expression 'I > 2\s(I)'
_computing_cell_refinement
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb 1 2013,16:14:44)
;
_computing_data_collection
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb 1 2013,16:14:44)
;
_computing_data_reduction
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb 1 2013,16:14:44)
;
_computing_molecular_graphics
;
O. V. Dolomanov, L. J. Bourhis, R. J. Gildea, J. A. K. Howard and H. Puschmann,
OLEX2: a complete structure solution, refinement and analysis program.
J. Appl. Cryst. (2009). 42, 339-341.
;
_computing_publication_material
;
O. V. Dolomanov, L. J. Bourhis, R. J. Gildea, J. A. K. Howard and H. Puschmann,
OLEX2: a complete structure solution, refinement and analysis program.
J. Appl. Cryst. (2009). 42, 339-341.
;
_computing_structure_refinement
;
SHELXL, G.M. Sheldrick, Acta Cryst.
(2008). A64, 112-122
;
_computing_structure_solution 'SUPERFLIP, J. Appl. Cryst. (2007) 40, 786-790'
_refine_diff_density_max 0.938
_refine_diff_density_min -1.043
_refine_diff_density_rms 0.115
_refine_ls_extinction_coef .
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.144
_refine_ls_hydrogen_treatment constr
_refine_ls_matrix_type full
_refine_ls_number_parameters 863
_refine_ls_number_reflns 13686
_refine_ls_number_restraints 12
_refine_ls_R_factor_all 0.0989
_refine_ls_R_factor_gt 0.0848
_refine_ls_restrained_S_all 1.144
_refine_ls_shift/su_max 0.000
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0127P)^2^+29.1785P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.1825
_refine_ls_wR_factor_ref 0.1888
_refine_special_details
;
?
;
_olex2_refinement_description
;
1. Fixed Uiso
At 1.2 times of:
All C(H) groups
At 1.5 times of:
All C(H,H,H) groups
2. Restrained distances
Si1A-C8A = Si1A-C6A = Si1A-C7A = Si2A-C48A = Si2A-C49A = Si2A-C47A = Si1-C8 =
Si1-C7 = Si1-C6 = Si2-C49 = Si2-C48 = Si2-C47
1.87 with sigma of 0.03
3. Uiso/Uaniso restraints and constraints
Uanis(Si1) = Uanis(Si1A)
Uanis(C6) = Uanis(C7A)
Uanis(C7) = Uanis(C6A)
Uanis(C8) = Uanis(C8A)
Uanis(C48) = Uanis(C48A)
Uanis(C44) = Uanis(C51)
Uanis(C47) = Uanis(C47A)
4. Others
1*Sof(Si2)=1-1*Sof(Si2A)=1*Sof(C47)=1*Sof(H47A)=1*Sof(H47B)=1*Sof(H47C)=1-1*
Sof(C47A)=1-1*Sof(H47D)=1-1*Sof(H47E)=1-1*Sof(H47F)=1*Sof(C48)=1*Sof(H48A)=1*
Sof(H48B)=1*Sof(H48C)=1-1*Sof(C48A)=1-1*Sof(H48D)=1-1*Sof(H48E)=1-1*Sof(H48F)=
1*Sof(C49)=1*Sof(H49A)=1*Sof(H49B)=1*Sof(H49C)=1-1*Sof(C49A)=1-1*Sof(H49D)=1-1*
Sof(H49E)=1-1*Sof(H49F)
1*Sof(Si1)=1-1*Sof(Si1A)=1*Sof(C6)=1*Sof(H6A)=1*Sof(H6B)=1*Sof(H6C)=1-1*
Sof(C6A)=1-1*Sof(H6AA)=1-1*Sof(H6AB)=1-1*Sof(H6AC)=1*Sof(C7)=1*Sof(H7A)=1*
Sof(H7B)=1*Sof(H7C)=1-1*Sof(C7A)=1-1*Sof(H7AA)=1-1*Sof(H7AB)=1-1*Sof(H7AC)=1*
Sof(C8)=1*Sof(H8A)=1*Sof(H8B)=1*Sof(H8C)=1-1*Sof(C8A)=1-1*Sof(H8AA)=1-1*
Sof(H8AB)=1-1*Sof(H8AC)
5.a Aromatic/amide H refined with riding coordinates:
C16(H16), C17(H17), C18(H18), C19(H19), C20(H20), C22(H22), C23(H23),
C24(H24), C25(H25), C26(H26), C31(H31), C32(H32), C33(H33), C34(H34), C35(H35),
C37(H37), C38(H38), C39(H39), C40(H40), C41(H41), C57(H57), C58(H58),
C59(H59), C60(H60), C61(H61), C63(H63), C64(H64), C65(H65), C66(H66), C67(H67),
C72(H72), C73(H73), C74(H74), C75(H75), C76(H76), C78(H78), C79(H79),
C80(H80), C81(H81), C82(H82)
5.b Idealised Me refined as rotating group:
C6(H6A,H6B,H6C), C6A(H6AA,H6AB,H6AC), C7(H7A,H7B,H7C), C7A(H7AA,H7AB,H7AC),
C8(H8A,H8B,H8C), C8A(H8AA,H8AB,H8AC), C9(H9A,H9B,H9C), C10(H10A,H10B,H10C),
C11(H11A,H11B,H11C), C12(H12A,H12B,H12C), C47(H47A,H47B,H47C), C47A(H47D,H47E,
H47F), C48(H48A,H48B,H48C), C48A(H48D,H48E,H48F), C49(H49A,H49B,H49C),
C49A(H49D,H49E,H49F), C50(H50A,H50B,H50C), C51(H51A,H51B,H51C), C52(H52A,H52B,
H52C), C53(H53A,H53B,H53C)
;
_atom_sites_solution_hydrogens geom
_atom_sites_solution_primary iterative
_atom_sites_solution_secondary ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Y1 Y 0.97517(4) 0.39778(3) 0.05167(3) 0.01890(14) Uani 1 1 d . . . . .
Y2 Y 0.46709(5) -0.10240(4) 0.44799(4) 0.02338(15) Uani 1 1 d . . . . .
Si1 Si 0.8896(2) 0.16147(15) 0.10866(18) 0.0257(6) Uani 0.850(7) 1 d D . P A 1
Si1A Si 0.9127(14) 0.1560(11) 0.0834(10) 0.0257(6) Uani 0.150(7) 1 d D . P A 2
Si2 Si 0.4148(3) -0.3465(2) 0.4087(2) 0.0244(8) Uani 0.784(8) 1 d D . P B 1
Si2A Si 0.3820(15) -0.3355(10) 0.3860(12) 0.060(5) Uani 0.216(8) 1 d D . P B 2
N1 N 1.0877(4) 0.3756(3) 0.1628(3) 0.0256(11) Uani 1 1 d . . . . .
N2 N 0.9232(4) 0.3997(3) 0.1902(3) 0.0277(12) Uani 1 1 d . . . . .
N3 N 0.4084(4) -0.1032(3) 0.3108(3) 0.0297(12) Uani 1 1 d . . . . .
N4 N 0.5711(4) -0.1289(3) 0.3339(3) 0.0296(12) Uani 1 1 d . . . . .
C1 C 0.8987(4) 0.2474(3) 0.0315(4) 0.0212(12) Uani 1 1 d . . . . .
C2 C 0.8187(5) 0.2988(4) 0.0094(4) 0.0266(13) Uani 1 1 d . . . . .
C3 C 0.8474(5) 0.3396(4) -0.0637(4) 0.0306(15) Uani 1 1 d . . . . .
C4 C 0.9429(5) 0.3149(4) -0.0869(4) 0.0307(15) Uani 1 1 d . . . . .
C5 C 0.9756(5) 0.2585(4) -0.0299(4) 0.0261(13) Uani 1 1 d . . . . .
C6 C 0.8929(7) 0.0634(4) 0.0504(5) 0.038(2) Uani 0.850(7) 1 d D . P A 1
H6A H 0.8363 0.0596 0.0114 0.057 Uiso 0.850(7) 1 calc R U P A 1
H6B H 0.8863 0.0168 0.0880 0.057 Uiso 0.850(7) 1 calc R U P A 1
H6C H 0.9577 0.0620 0.0211 0.057 Uiso 0.850(7) 1 calc R U P A 1
C6A C 1.033(3) 0.101(3) 0.079(3) 0.043(2) Uani 0.150(7) 1 d D . P A 2
H6AA H 1.0319 0.0641 0.0315 0.065 Uiso 0.150(7) 1 calc R U P A 2
H6AB H 1.0389 0.0676 0.1287 0.065 Uiso 0.150(7) 1 calc R U P A 2
H6AC H 1.0913 0.1407 0.0759 0.065 Uiso 0.150(7) 1 calc R U P A 2
C7 C 0.9934(7) 0.1673(6) 0.1854(5) 0.043(2) Uani 0.850(7) 1 d D . P A 1
H7A H 1.0595 0.1666 0.1578 0.065 Uiso 0.850(7) 1 calc R U P A 1
H7B H 0.9854 0.1199 0.2219 0.065 Uiso 0.850(7) 1 calc R U P A 1
H7C H 0.9902 0.2186 0.2171 0.065 Uiso 0.850(7) 1 calc R U P A 1
C7A C 0.905(4) 0.178(3) 0.1965(17) 0.038(2) Uani 0.150(7) 1 d D . P A 2
H7AA H 0.9407 0.2319 0.2085 0.057 Uiso 0.150(7) 1 calc R U P A 2
H7AB H 0.9380 0.1350 0.2265 0.057 Uiso 0.150(7) 1 calc R U P A 2
H7AC H 0.8337 0.1797 0.2129 0.057 Uiso 0.150(7) 1 calc R U P A 2
C8 C 0.7661(7) 0.1572(6) 0.1656(5) 0.044(2) Uani 0.850(7) 1 d D . P A 1
H8A H 0.7574 0.2105 0.1925 0.066 Uiso 0.850(7) 1 calc R U P A 1
H8B H 0.7666 0.1137 0.2066 0.066 Uiso 0.850(7) 1 calc R U P A 1
H8C H 0.7096 0.1452 0.1275 0.066 Uiso 0.850(7) 1 calc R U P A 1
C8A C 0.803(3) 0.080(3) 0.069(3) 0.044(2) Uani 0.150(7) 1 d D . P A 2
H8AA H 0.7482 0.0932 0.1067 0.066 Uiso 0.150(7) 1 calc R U P A 2
H8AB H 0.8248 0.0245 0.0802 0.066 Uiso 0.150(7) 1 calc R U P A 2
H8AC H 0.7783 0.0826 0.0130 0.066 Uiso 0.150(7) 1 calc R U P A 2
C9 C 0.7177(5) 0.3102(5) 0.0521(5) 0.0451(19) Uani 1 1 d . . . . .
H9A H 0.7235 0.2951 0.1094 0.068 Uiso 1 1 calc R U . . .
H9B H 0.6640 0.2748 0.0259 0.068 Uiso 1 1 calc R U . . .
H9C H 0.7005 0.3680 0.0483 0.068 Uiso 1 1 calc R U . . .
C10 C 0.7812(7) 0.3937(5) -0.1141(5) 0.058(3) Uani 1 1 d . . . . .
H10A H 0.7215 0.4079 -0.0821 0.087 Uiso 1 1 calc R U . . .
H10B H 0.7586 0.3637 -0.1635 0.087 Uiso 1 1 calc R U . . .
H10C H 0.8206 0.4443 -0.1291 0.087 Uiso 1 1 calc R U . . .
C11 C 0.9973(7) 0.3361(6) -0.1654(4) 0.054(2) Uani 1 1 d . . . . .
H11A H 1.0068 0.3962 -0.1700 0.081 Uiso 1 1 calc R U . . .
H11B H 0.9565 0.3140 -0.2115 0.081 Uiso 1 1 calc R U . . .
H11C H 1.0640 0.3118 -0.1658 0.081 Uiso 1 1 calc R U . . .
C12 C 1.0733(6) 0.2116(5) -0.0339(5) 0.0450(19) Uani 1 1 d . . . . .
H12A H 1.1309 0.2500 -0.0479 0.068 Uiso 1 1 calc R U . . .
H12B H 1.0659 0.1681 -0.0756 0.068 Uiso 1 1 calc R U . . .
H12C H 1.0858 0.1868 0.0190 0.068 Uiso 1 1 calc R U . . .
C13 C 0.8876(4) 0.5257(4) 0.0236(4) 0.0226(12) Uani 1 1 d . . . . .
C14 C 0.8076(5) 0.5600(4) 0.0333(4) 0.0281(14) Uani 1 1 d . . . . .
C15 C 0.7127(5) 0.5971(4) 0.0474(4) 0.0324(15) Uani 1 1 d . . . . .
C16 C 0.6302(6) 0.5818(6) -0.0047(6) 0.054(2) Uani 1 1 d . . . . .
H16 H 0.6363 0.5471 -0.0512 0.065 Uiso 1 1 calc R U . . .
C17 C 0.5390(6) 0.6175(6) 0.0119(7) 0.068(3) Uani 1 1 d . . . . .
H17 H 0.4831 0.6075 -0.0243 0.082 Uiso 1 1 calc R U . . .
C18 C 0.5270(6) 0.6664(6) 0.0784(7) 0.062(3) Uani 1 1 d . . . . .
H18 H 0.4634 0.6894 0.0891 0.074 Uiso 1 1 calc R U . . .
C19 C 0.6078(6) 0.6820(5) 0.1294(6) 0.048(2) Uani 1 1 d . . . . .
H19 H 0.6001 0.7172 0.1753 0.058 Uiso 1 1 calc R U . . .
C20 C 0.6997(5) 0.6481(4) 0.1164(5) 0.0374(16) Uani 1 1 d . . . . .
H20 H 0.7544 0.6588 0.1536 0.045 Uiso 1 1 calc R U . . .
C21 C 1.1924(5) 0.3682(4) 0.1830(4) 0.0302(14) Uani 1 1 d . . . . .
C22 C 1.2426(6) 0.3034(5) 0.1501(5) 0.0449(19) Uani 1 1 d . . . . .
H22 H 1.2068 0.2647 0.1153 0.054 Uiso 1 1 calc R U . . .
C23 C 1.3443(6) 0.2941(5) 0.1672(6) 0.057(2) Uani 1 1 d . . . . .
H23 H 1.3777 0.2487 0.1449 0.068 Uiso 1 1 calc R U . . .
C24 C 1.3971(6) 0.3503(5) 0.2163(5) 0.049(2) Uani 1 1 d . . . . .
H24 H 1.4668 0.3431 0.2285 0.059 Uiso 1 1 calc R U . . .
C25 C 1.3503(6) 0.4164(4) 0.2478(4) 0.0382(17) Uani 1 1 d . . . . .
H25 H 1.3879 0.4563 0.2802 0.046 Uiso 1 1 calc R U . . .
C26 C 1.2477(5) 0.4251(4) 0.2322(4) 0.0308(14) Uani 1 1 d . . . . .
H26 H 1.2147 0.4704 0.2553 0.037 Uiso 1 1 calc R U . . .
C27 C 1.0154(5) 0.3878(3) 0.2194(4) 0.0258(13) Uani 1 1 d . . . . .
C28 C 1.0385(5) 0.3879(4) 0.3049(4) 0.0301(14) Uani 1 1 d . . . . .
C29 C 1.0526(5) 0.3894(4) 0.3769(4) 0.0292(14) Uani 1 1 d . . . . .
C30 C 1.0670(5) 0.3952(4) 0.4639(4) 0.0248(13) Uani 1 1 d . . . . .
C31 C 1.1642(5) 0.4015(4) 0.4981(4) 0.0330(15) Uani 1 1 d . . . . .
H31 H 1.2233 0.3964 0.4654 0.040 Uiso 1 1 calc R U . . .
C32 C 1.1723(6) 0.4156(5) 0.5816(5) 0.0440(19) Uani 1 1 d . . . . .
H32 H 1.2379 0.4238 0.6058 0.053 Uiso 1 1 calc R U . . .
C33 C 1.0877(7) 0.4177(4) 0.6291(4) 0.0440(19) Uani 1 1 d . . . . .
H33 H 1.0949 0.4257 0.6862 0.053 Uiso 1 1 calc R U . . .
C34 C 0.9933(6) 0.4085(4) 0.5959(4) 0.0369(16) Uani 1 1 d . . . . .
H34 H 0.9346 0.4092 0.6297 0.044 Uiso 1 1 calc R U . . .
C35 C 0.9828(5) 0.3983(4) 0.5140(4) 0.0289(14) Uani 1 1 d . . . . .
H35 H 0.9164 0.3932 0.4908 0.035 Uiso 1 1 calc R U . . .
C36 C 0.8356(5) 0.4017(4) 0.2391(4) 0.0247(13) Uani 1 1 d . . . . .
C37 C 0.8134(6) 0.3472(4) 0.3022(4) 0.0343(16) Uani 1 1 d . . . . .
H37 H 0.8610 0.3077 0.3164 0.041 Uiso 1 1 calc R U . . .
C38 C 0.7229(6) 0.3500(5) 0.3446(4) 0.0412(18) Uani 1 1 d . . . . .
H38 H 0.7088 0.3123 0.3876 0.049 Uiso 1 1 calc R U . . .
C39 C 0.6538(6) 0.4062(5) 0.3254(4) 0.0409(18) Uani 1 1 d . . . . .
H39 H 0.5922 0.4082 0.3555 0.049 Uiso 1 1 calc R U . . .
C40 C 0.6729(5) 0.4605(5) 0.2620(4) 0.0380(17) Uani 1 1 d . . . . .
H40 H 0.6245 0.4994 0.2480 0.046 Uiso 1 1 calc R U . . .
C41 C 0.7641(5) 0.4572(4) 0.2191(4) 0.0324(15) Uani 1 1 d . . . . .
H41 H 0.7773 0.4940 0.1752 0.039 Uiso 1 1 calc R U . . .
C42 C 0.4047(5) -0.2545(4) 0.4754(4) 0.0260(13) Uani 1 1 d . . . . .
C43 C 0.4699(5) -0.2322(4) 0.5425(4) 0.0351(16) Uani 1 1 d . . . . .
C44 C 0.4235(7) -0.1742(5) 0.5896(4) 0.0503(16) Uani 1 1 d . . . . .
C45 C 0.3266(5) -0.1594(4) 0.5547(4) 0.0315(15) Uani 1 1 d . . . . .
C46 C 0.3154(5) -0.2065(4) 0.4856(4) 0.0266(13) Uani 1 1 d . . . . .
C47 C 0.3096(7) -0.4223(6) 0.4322(6) 0.040(2) Uani 0.784(8) 1 d D . P B 1
H47A H 0.3121 -0.4365 0.4899 0.060 Uiso 0.784(8) 1 calc R U P B 1
H47B H 0.3164 -0.4721 0.3990 0.060 Uiso 0.784(8) 1 calc R U P B 1
H47C H 0.2443 -0.3985 0.4201 0.060 Uiso 0.784(8) 1 calc R U P B 1
C47A C 0.494(2) -0.337(2) 0.320(2) 0.040(2) Uani 0.216(8) 1 d D . P B 2
H47D H 0.5252 -0.2806 0.3155 0.060 Uiso 0.216(8) 1 calc R U P B 2
H47E H 0.4740 -0.3578 0.2663 0.060 Uiso 0.216(8) 1 calc R U P B 2
H47F H 0.5440 -0.3726 0.3440 0.060 Uiso 0.216(8) 1 calc R U P B 2
C48 C 0.4158(9) -0.3230(6) 0.2989(6) 0.048(3) Uani 0.784(8) 1 d D . P B 1
H48A H 0.3571 -0.2909 0.2857 0.073 Uiso 0.784(8) 1 calc R U P B 1
H48B H 0.4120 -0.3747 0.2674 0.073 Uiso 0.784(8) 1 calc R U P B 1
H48C H 0.4790 -0.2910 0.2853 0.073 Uiso 0.784(8) 1 calc R U P B 1
C48A C 0.392(3) -0.4335(17) 0.445(2) 0.048(3) Uani 0.216(8) 1 d D . P B 2
H48D H 0.4517 -0.4281 0.4807 0.073 Uiso 0.216(8) 1 calc R U P B 2
H48E H 0.3999 -0.4796 0.4066 0.073 Uiso 0.216(8) 1 calc R U P B 2
H48F H 0.3303 -0.4439 0.4771 0.073 Uiso 0.216(8) 1 calc R U P B 2
C49 C 0.5348(7) -0.4028(6) 0.4266(7) 0.050(3) Uani 0.784(8) 1 d D . P B 1
H49A H 0.5946 -0.3662 0.4143 0.074 Uiso 0.784(8) 1 calc R U P B 1
H49B H 0.5346 -0.4518 0.3913 0.074 Uiso 0.784(8) 1 calc R U P B 1
H49C H 0.5376 -0.4197 0.4837 0.074 Uiso 0.784(8) 1 calc R U P B 1
C49A C 0.261(2) -0.339(2) 0.331(3) 0.057(11) Uani 0.216(8) 1 d D . P B 2
H49D H 0.2059 -0.3272 0.3680 0.085 Uiso 0.216(8) 1 calc R U P B 2
H49E H 0.2482 -0.3946 0.3069 0.085 Uiso 0.216(8) 1 calc R U P B 2
H49F H 0.2650 -0.2984 0.2870 0.085 Uiso 0.216(8) 1 calc R U P B 2
C50 C 0.5716(6) -0.2669(6) 0.5626(7) 0.069(3) Uani 1 1 d . . . . .
H50A H 0.6120 -0.2712 0.5128 0.104 Uiso 1 1 calc R U . . .
H50B H 0.5601 -0.3217 0.5866 0.104 Uiso 1 1 calc R U . . .
H50C H 0.6085 -0.2301 0.6015 0.104 Uiso 1 1 calc R U . . .
C51 C 0.4575(6) -0.1330(5) 0.6688(4) 0.0503(16) Uani 1 1 d . . . . .
H51A H 0.5294 -0.1430 0.6788 0.075 Uiso 1 1 calc R U . . .
H51B H 0.4158 -0.1560 0.7136 0.075 Uiso 1 1 calc R U . . .
H51C H 0.4493 -0.0735 0.6655 0.075 Uiso 1 1 calc R U . . .
C52 C 0.2461(7) -0.1067(5) 0.5903(5) 0.056(2) Uani 1 1 d . . . . .
H52A H 0.2787 -0.0558 0.6131 0.084 Uiso 1 1 calc R U . . .
H52B H 0.2092 -0.1372 0.6334 0.084 Uiso 1 1 calc R U . . .
H52C H 0.1980 -0.0929 0.5475 0.084 Uiso 1 1 calc R U . . .
C53 C 0.2232(5) -0.2135(6) 0.4320(5) 0.049(2) Uani 1 1 d . . . . .
H53A H 0.1942 -0.1593 0.4276 0.073 Uiso 1 1 calc R U . . .
H53B H 0.1723 -0.2528 0.4556 0.073 Uiso 1 1 calc R U . . .
H53C H 0.2425 -0.2328 0.3778 0.073 Uiso 1 1 calc R U . . .
C54 C 0.3881(5) 0.0293(4) 0.4814(4) 0.0292(14) Uani 1 1 d . . . . .
C55 C 0.3075(5) 0.0637(4) 0.4746(4) 0.0326(15) Uani 1 1 d . . . . .
C56 C 0.2113(6) 0.1014(5) 0.4631(5) 0.0435(19) Uani 1 1 d . . . . .
C57 C 0.1344(6) 0.0907(6) 0.5200(7) 0.066(3) Uani 1 1 d . . . . .
H57 H 0.1445 0.0582 0.5668 0.079 Uiso 1 1 calc R U . . .
C58 C 0.0428(7) 0.1272(7) 0.5090(9) 0.085(4) Uani 1 1 d . . . . .
H58 H -0.0102 0.1200 0.5481 0.102 Uiso 1 1 calc R U . . .
C59 C 0.0292(7) 0.1745(6) 0.4398(8) 0.076(3) Uani 1 1 d . . . . .
H59 H -0.0334 0.2001 0.4321 0.092 Uiso 1 1 calc R U . . .
C60 C 0.1052(7) 0.1847(5) 0.3828(7) 0.063(3) Uani 1 1 d . . . . .
H60 H 0.0953 0.2170 0.3358 0.076 Uiso 1 1 calc R U . . .
C61 C 0.1947(6) 0.1480(5) 0.3944(5) 0.048(2) Uani 1 1 d . . . . .
H61 H 0.2469 0.1544 0.3546 0.058 Uiso 1 1 calc R U . . .
C62 C 0.3187(5) -0.0968(4) 0.2637(4) 0.0286(14) Uani 1 1 d . . . . .
C63 C 0.2494(5) -0.0402(4) 0.2895(4) 0.0341(15) Uani 1 1 d . . . . .
H63 H 0.2642 -0.0066 0.3362 0.041 Uiso 1 1 calc R U . . .
C64 C 0.1589(6) -0.0325(5) 0.2475(4) 0.0410(17) Uani 1 1 d . . . . .
H64 H 0.1124 0.0064 0.2659 0.049 Uiso 1 1 calc R U . . .
C65 C 0.1350(6) -0.0795(5) 0.1804(5) 0.0444(19) Uani 1 1 d . . . . .
H65 H 0.0732 -0.0728 0.1518 0.053 Uiso 1 1 calc R U . . .
C66 C 0.2019(6) -0.1373(5) 0.1541(4) 0.045(2) Uani 1 1 d . . . . .
H66 H 0.1855 -0.1706 0.1075 0.054 Uiso 1 1 calc R U . . .
C67 C 0.2929(6) -0.1469(4) 0.1957(4) 0.0347(16) Uani 1 1 d . . . . .
H67 H 0.3378 -0.1874 0.1780 0.042 Uiso 1 1 calc R U . . .
C68 C 0.4993(6) -0.1164(4) 0.2793(4) 0.0310(15) Uani 1 1 d . . . . .
C69 C 0.5203(5) -0.1147(4) 0.1925(4) 0.0307(14) Uani 1 1 d . . . . .
C70 C 0.5413(5) -0.1118(4) 0.1227(4) 0.0282(14) Uani 1 1 d . . . . .
C71 C 0.5658(5) -0.1060(4) 0.0382(4) 0.0303(14) Uani 1 1 d . . . . .
C72 C 0.4922(6) -0.1035(4) -0.0212(4) 0.0380(17) Uani 1 1 d . . . . .
H72 H 0.4226 -0.1126 -0.0064 0.046 Uiso 1 1 calc R U . . .
C73 C 0.5160(6) -0.0885(4) -0.1003(4) 0.0390(17) Uani 1 1 d . . . . .
H73 H 0.4636 -0.0849 -0.1398 0.047 Uiso 1 1 calc R U . . .
C74 C 0.6169(7) -0.0785(4) -0.1226(4) 0.046(2) Uani 1 1 d . . . . .
H74 H 0.6339 -0.0676 -0.1778 0.055 Uiso 1 1 calc R U . . .
C75 C 0.6946(6) -0.0841(5) -0.0654(5) 0.0446(19) Uani 1 1 d . . . . .
H75 H 0.7642 -0.0779 -0.0812 0.054 Uiso 1 1 calc R U . . .
C76 C 0.6683(6) -0.0987(5) 0.0139(4) 0.0401(17) Uani 1 1 d . . . . .
H76 H 0.7205 -0.1041 0.0533 0.048 Uiso 1 1 calc R U . . .
C77 C 0.6743(5) -0.1360(4) 0.3098(4) 0.0313(15) Uani 1 1 d . . . . .
C78 C 0.7283(6) -0.0757(4) 0.2655(4) 0.0339(15) Uani 1 1 d . . . . .
H78 H 0.6956 -0.0281 0.2482 0.041 Uiso 1 1 calc R U . . .
C79 C 0.8305(6) -0.0849(4) 0.2464(4) 0.0415(18) Uani 1 1 d . . . . .
H79 H 0.8668 -0.0436 0.2156 0.050 Uiso 1 1 calc R U . . .
C80 C 0.8788(7) -0.1519(5) 0.2711(5) 0.054(2) Uani 1 1 d . . . . .
H80 H 0.9483 -0.1576 0.2573 0.065 Uiso 1 1 calc R U . . .
C81 C 0.8269(7) -0.2114(5) 0.3161(6) 0.060(3) Uani 1 1 d . . . . .
H81 H 0.8604 -0.2584 0.3338 0.072 Uiso 1 1 calc R U . . .
C82 C 0.7249(6) -0.2026(5) 0.3355(5) 0.049(2) Uani 1 1 d . . . . .
H82 H 0.6896 -0.2436 0.3674 0.058 Uiso 1 1 calc R U . . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Y1 0.0188(3) 0.0155(3) 0.0222(3) 0.0013(2) 0.0006(2) -0.0016(2)
Y2 0.0251(3) 0.0198(3) 0.0247(3) 0.0013(2) 0.0019(2) -0.0032(2)
Si1 0.0383(15) 0.0214(10) 0.0166(14) 0.0053(10) 0.0029(10) -0.0068(10)
Si1A 0.0383(15) 0.0214(10) 0.0166(14) 0.0053(10) 0.0029(10) -0.0068(10)
Si2 0.0294(16) 0.0177(15) 0.0260(16) 0.0001(11) 0.0098(12) -0.0013(12)
Si2A 0.092(14) 0.013(6) 0.077(12) -0.007(6) -0.013(9) 0.006(7)
N1 0.027(3) 0.024(3) 0.026(3) -0.005(2) 0.001(2) 0.007(2)
N2 0.037(3) 0.025(3) 0.021(3) 0.004(2) 0.001(2) 0.000(2)
N3 0.035(3) 0.025(3) 0.028(3) -0.004(2) 0.003(2) -0.001(2)
N4 0.034(3) 0.029(3) 0.026(3) -0.002(2) 0.005(2) 0.001(2)
C1 0.022(3) 0.013(3) 0.028(3) 0.001(2) -0.003(2) -0.002(2)
C2 0.019(3) 0.022(3) 0.039(4) -0.008(3) -0.006(3) -0.001(2)
C3 0.038(4) 0.017(3) 0.036(4) 0.002(3) -0.020(3) -0.006(3)
C4 0.040(4) 0.028(3) 0.022(3) -0.005(3) 0.000(3) -0.018(3)
C5 0.026(3) 0.021(3) 0.031(3) -0.007(3) 0.001(3) -0.004(2)
C6 0.061(6) 0.018(4) 0.034(4) 0.006(3) 0.003(4) -0.006(4)
C6A 0.046(5) 0.040(5) 0.043(5) 0.015(4) -0.023(4) -0.008(4)
C7 0.046(5) 0.040(5) 0.043(5) 0.015(4) -0.023(4) -0.008(4)
C7A 0.061(6) 0.018(4) 0.034(4) 0.006(3) 0.003(4) -0.006(4)
C8 0.053(6) 0.041(5) 0.038(5) 0.007(4) 0.014(4) -0.013(4)
C8A 0.053(6) 0.041(5) 0.038(5) 0.007(4) 0.014(4) -0.013(4)
C9 0.013(3) 0.053(5) 0.070(5) -0.015(4) 0.001(3) 0.003(3)
C10 0.083(6) 0.028(4) 0.062(5) 0.005(4) -0.055(5) 0.002(4)
C11 0.071(6) 0.065(6) 0.023(4) 0.002(4) -0.003(4) -0.027(5)
C12 0.039(4) 0.049(5) 0.046(5) -0.013(4) -0.003(3) 0.002(4)
C13 0.015(3) 0.026(3) 0.028(3) 0.002(2) 0.002(2) 0.004(2)
C14 0.027(3) 0.025(3) 0.033(3) 0.004(3) 0.000(3) -0.001(3)
C15 0.025(3) 0.027(3) 0.046(4) 0.006(3) 0.004(3) 0.004(3)
C16 0.032(4) 0.062(6) 0.068(6) -0.021(5) -0.004(4) 0.017(4)
C17 0.028(4) 0.081(7) 0.097(8) -0.033(6) -0.007(4) 0.018(4)
C18 0.029(4) 0.059(6) 0.099(8) -0.020(5) 0.009(4) 0.016(4)
C19 0.031(4) 0.043(4) 0.072(6) -0.004(4) 0.017(4) 0.014(3)
C20 0.030(4) 0.032(4) 0.051(4) -0.001(3) 0.006(3) 0.009(3)
C21 0.036(4) 0.024(3) 0.031(3) 0.002(3) -0.009(3) 0.006(3)
C22 0.038(4) 0.033(4) 0.064(5) -0.019(4) -0.017(4) 0.005(3)
C23 0.044(5) 0.036(4) 0.092(7) -0.021(4) -0.021(5) 0.018(4)
C24 0.035(4) 0.042(4) 0.071(6) -0.009(4) -0.029(4) 0.014(3)
C25 0.041(4) 0.032(4) 0.041(4) -0.004(3) -0.019(3) -0.002(3)
C26 0.040(4) 0.021(3) 0.032(3) -0.002(3) -0.007(3) 0.005(3)
C27 0.037(4) 0.012(3) 0.028(3) 0.002(2) -0.004(3) 0.001(2)
C28 0.041(4) 0.019(3) 0.030(4) 0.001(3) 0.001(3) -0.001(3)
C29 0.034(4) 0.021(3) 0.032(4) 0.005(3) 0.003(3) -0.002(3)
C30 0.026(3) 0.019(3) 0.029(3) 0.001(2) -0.001(3) 0.001(2)
C31 0.025(3) 0.031(4) 0.043(4) 0.006(3) -0.001(3) -0.002(3)
C32 0.051(5) 0.040(4) 0.039(4) 0.008(3) -0.022(4) -0.008(4)
C33 0.080(6) 0.027(4) 0.025(4) 0.004(3) 0.003(4) 0.001(4)
C34 0.048(4) 0.028(4) 0.035(4) 0.000(3) 0.009(3) 0.005(3)
C35 0.023(3) 0.032(4) 0.031(3) 0.001(3) 0.001(3) -0.003(3)
C36 0.033(3) 0.017(3) 0.024(3) -0.004(2) 0.000(3) -0.002(3)
C37 0.048(4) 0.023(3) 0.031(4) 0.001(3) -0.001(3) -0.010(3)
C38 0.048(4) 0.041(4) 0.032(4) 0.004(3) 0.004(3) -0.024(4)
C39 0.033(4) 0.059(5) 0.029(4) -0.007(3) 0.012(3) -0.013(4)
C40 0.029(4) 0.043(4) 0.041(4) -0.010(3) 0.008(3) -0.003(3)
C41 0.035(4) 0.037(4) 0.024(3) 0.001(3) 0.008(3) -0.006(3)
C42 0.028(3) 0.019(3) 0.031(3) 0.005(3) 0.009(3) 0.001(2)
C43 0.024(3) 0.043(4) 0.038(4) 0.020(3) -0.002(3) -0.002(3)
C44 0.059(4) 0.062(4) 0.025(3) 0.002(3) 0.005(2) -0.041(3)
C45 0.035(4) 0.022(3) 0.038(4) 0.006(3) 0.014(3) 0.002(3)
C46 0.023(3) 0.024(3) 0.032(3) 0.006(3) 0.004(3) -0.001(3)
C47 0.040(5) 0.032(5) 0.047(5) -0.011(4) 0.020(4) -0.007(4)
C47A 0.040(5) 0.032(5) 0.047(5) -0.011(4) 0.020(4) -0.007(4)
C48 0.075(8) 0.032(5) 0.038(5) -0.005(4) 0.004(5) -0.002(5)
C48A 0.075(8) 0.032(5) 0.038(5) -0.005(4) 0.004(5) -0.002(5)
C49 0.040(6) 0.028(5) 0.081(8) -0.003(5) 0.016(5) 0.003(4)
C49A 0.06(2) 0.022(17) 0.09(3) -0.015(18) 0.00(2) -0.016(16)
C50 0.023(4) 0.082(7) 0.103(8) 0.057(6) -0.005(4) -0.003(4)
C51 0.059(4) 0.062(4) 0.025(3) 0.002(3) 0.005(2) -0.041(3)
C52 0.072(6) 0.036(4) 0.060(5) -0.003(4) 0.038(5) -0.001(4)
C53 0.024(4) 0.072(6) 0.050(5) 0.021(4) 0.003(3) -0.005(4)
C54 0.032(4) 0.023(3) 0.031(3) 0.001(3) -0.001(3) -0.008(3)
C55 0.031(4) 0.027(3) 0.040(4) -0.002(3) -0.002(3) 0.003(3)
C56 0.035(4) 0.031(4) 0.065(5) -0.004(4) -0.014(4) 0.009(3)
C57 0.033(5) 0.073(7) 0.094(8) 0.018(6) 0.005(5) 0.016(4)
C58 0.026(4) 0.083(8) 0.149(11) 0.023(8) 0.011(6) 0.022(5)
C59 0.039(5) 0.065(7) 0.129(10) 0.007(6) -0.014(6) 0.026(5)
C60 0.057(6) 0.038(5) 0.095(8) 0.001(5) -0.035(5) 0.013(4)
C61 0.050(5) 0.036(4) 0.059(5) -0.006(4) -0.018(4) 0.004(4)
C62 0.033(3) 0.026(3) 0.027(3) 0.005(3) -0.006(3) -0.007(3)
C63 0.037(4) 0.033(4) 0.032(4) 0.000(3) -0.004(3) -0.003(3)
C64 0.036(4) 0.049(4) 0.038(4) 0.006(3) -0.004(3) 0.001(3)
C65 0.033(4) 0.062(5) 0.037(4) 0.014(4) -0.003(3) -0.012(4)
C66 0.053(5) 0.049(5) 0.029(4) 0.006(3) -0.011(3) -0.026(4)
C67 0.048(4) 0.024(3) 0.032(4) 0.001(3) 0.003(3) -0.007(3)
C68 0.051(4) 0.019(3) 0.023(3) 0.002(2) 0.008(3) -0.001(3)
C69 0.038(4) 0.023(3) 0.031(4) 0.001(3) 0.001(3) 0.009(3)
C70 0.027(3) 0.026(3) 0.032(4) 0.000(3) 0.001(3) 0.003(3)
C71 0.044(4) 0.022(3) 0.025(3) 0.001(3) 0.002(3) -0.006(3)
C72 0.042(4) 0.036(4) 0.034(4) 0.002(3) -0.004(3) -0.007(3)
C73 0.048(4) 0.038(4) 0.031(4) -0.004(3) -0.006(3) 0.011(3)
C74 0.084(6) 0.026(4) 0.028(4) 0.001(3) 0.020(4) 0.000(4)
C75 0.034(4) 0.048(5) 0.051(5) -0.005(4) 0.018(3) -0.010(3)
C76 0.041(4) 0.040(4) 0.038(4) 0.003(3) 0.001(3) -0.010(3)
C77 0.041(4) 0.028(3) 0.026(3) 0.000(3) 0.007(3) 0.001(3)
C78 0.045(4) 0.024(3) 0.033(4) 0.001(3) 0.008(3) 0.003(3)
C79 0.050(5) 0.034(4) 0.040(4) 0.007(3) 0.021(3) -0.001(3)
C80 0.058(5) 0.042(5) 0.063(6) 0.007(4) 0.028(4) 0.011(4)
C81 0.059(6) 0.035(4) 0.087(7) 0.018(4) 0.033(5) 0.018(4)
C82 0.055(5) 0.032(4) 0.060(5) 0.015(4) 0.025(4) 0.010(4)
_geom_special_details
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Y1 Y1 3.7637(11) 2_765 ?
Y1 N1 2.391(5) . ?
Y1 N2 2.377(5) . ?
Y1 C1 2.604(5) . ?
Y1 C2 2.625(6) . ?
Y1 C3 2.662(6) . ?
Y1 C4 2.656(6) . ?
Y1 C5 2.618(6) . ?
Y1 C13 2.469(6) 2_765 ?
Y1 C13 2.474(6) . ?
Y1 C27 2.814(6) . ?
Y2 Y2 3.7797(12) 2_656 ?
Y2 N3 2.382(5) . ?
Y2 N4 2.370(5) . ?
Y2 C42 2.599(6) . ?
Y2 C43 2.629(6) . ?
Y2 C44 2.660(7) . ?
Y2 C45 2.678(6) . ?
Y2 C46 2.616(6) . ?
Y2 C54 2.484(7) . ?
Y2 C54 2.467(6) 2_656 ?
Y2 C68 2.813(6) . ?
Si1 C1 1.892(6) . ?
Si1 C6 1.852(8) . ?
Si1 C7 1.854(8) . ?
Si1 C8 1.869(9) . ?
Si1A C1 1.736(18) . ?
Si1A C6A 1.86(3) . ?
Si1A C7A 1.89(3) . ?
Si1A C8A 1.85(3) . ?
Si2 C42 1.855(7) . ?
Si2 C47 1.841(9) . ?
Si2 C48 1.846(10) . ?
Si2 C49 1.890(10) . ?
Si2A C42 1.97(2) . ?
Si2A C47A 1.83(2) . ?
Si2A C48A 1.88(2) . ?
Si2A C49A 1.82(3) . ?
N1 C21 1.425(8) . ?
N1 C27 1.350(8) . ?
N2 C27 1.327(8) . ?
N2 C36 1.405(8) . ?
N3 C62 1.418(8) . ?
N3 C68 1.328(9) . ?
N4 C68 1.326(9) . ?
N4 C77 1.422(9) . ?
C1 C2 1.426(8) . ?
C1 C5 1.433(8) . ?
C2 C3 1.418(9) . ?
C2 C9 1.519(9) . ?
C3 C4 1.389(10) . ?
C3 C10 1.519(9) . ?
C4 C5 1.398(9) . ?
C4 C11 1.508(9) . ?
C5 C12 1.529(10) . ?
C6 H6A 0.9800 . ?
C6 H6B 0.9800 . ?
C6 H6C 0.9800 . ?
C6A H6AA 0.9800 . ?
C6A H6AB 0.9800 . ?
C6A H6AC 0.9800 . ?
C7 H7A 0.9800 . ?
C7 H7B 0.9800 . ?
C7 H7C 0.9800 . ?
C7A H7AA 0.9800 . ?
C7A H7AB 0.9800 . ?
C7A H7AC 0.9800 . ?
C8 H8A 0.9800 . ?
C8 H8B 0.9800 . ?
C8 H8C 0.9800 . ?
C8A H8AA 0.9800 . ?
C8A H8AB 0.9800 . ?
C8A H8AC 0.9800 . ?
C9 H9A 0.9800 . ?
C9 H9B 0.9800 . ?
C9 H9C 0.9800 . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 H10C 0.9800 . ?
C11 H11A 0.9800 . ?
C11 H11B 0.9800 . ?
C11 H11C 0.9800 . ?
C12 H12A 0.9800 . ?
C12 H12B 0.9800 . ?
C12 H12C 0.9800 . ?
C13 Y1 2.469(6) 2_765 ?
C13 C14 1.226(8) . ?
C14 C15 1.432(9) . ?
C15 C16 1.390(10) . ?
C15 C20 1.415(10) . ?
C16 H16 0.9500 . ?
C16 C17 1.385(11) . ?
C17 H17 0.9500 . ?
C17 C18 1.360(13) . ?
C18 H18 0.9500 . ?
C18 C19 1.362(12) . ?
C19 H19 0.9500 . ?
C19 C20 1.369(10) . ?
C20 H20 0.9500 . ?
C21 C22 1.378(10) . ?
C21 C26 1.395(9) . ?
C22 H22 0.9500 . ?
C22 C23 1.380(10) . ?
C23 H23 0.9500 . ?
C23 C24 1.370(11) . ?
C24 H24 0.9500 . ?
C24 C25 1.364(11) . ?
C25 H25 0.9500 . ?
C25 C26 1.386(10) . ?
C26 H26 0.9500 . ?
C27 C28 1.436(9) . ?
C28 C29 1.197(9) . ?
C29 C30 1.443(9) . ?
C30 C31 1.391(9) . ?
C30 C35 1.382(9) . ?
C31 H31 0.9500 . ?
C31 C32 1.392(10) . ?
C32 H32 0.9500 . ?
C32 C33 1.360(11) . ?
C33 H33 0.9500 . ?
C33 C34 1.354(11) . ?
C34 H34 0.9500 . ?
C34 C35 1.361(9) . ?
C35 H35 0.9500 . ?
C36 C37 1.389(9) . ?
C36 C41 1.378(9) . ?
C37 H37 0.9500 . ?
C37 C38 1.379(10) . ?
C38 H38 0.9500 . ?
C38 C39 1.362(11) . ?
C39 H39 0.9500 . ?
C39 C40 1.382(10) . ?
C40 H40 0.9500 . ?
C40 C41 1.393(9) . ?
C41 H41 0.9500 . ?
C42 C43 1.427(9) . ?
C42 C46 1.451(9) . ?
C43 C44 1.381(12) . ?
C43 C50 1.515(10) . ?
C44 C45 1.429(11) . ?
C44 C51 1.513(10) . ?
C45 C46 1.366(9) . ?
C45 C52 1.511(10) . ?
C46 C53 1.495(9) . ?
C47 H47A 0.9800 . ?
C47 H47B 0.9800 . ?
C47 H47C 0.9800 . ?
C47A H47D 0.9800 . ?
C47A H47E 0.9800 . ?
C47A H47F 0.9800 . ?
C48 H48A 0.9800 . ?
C48 H48B 0.9800 . ?
C48 H48C 0.9800 . ?
C48A H48D 0.9800 . ?
C48A H48E 0.9800 . ?
C48A H48F 0.9800 . ?
C49 H49A 0.9800 . ?
C49 H49B 0.9800 . ?
C49 H49C 0.9800 . ?
C49A H49D 0.9800 . ?
C49A H49E 0.9800 . ?
C49A H49F 0.9800 . ?
C50 H50A 0.9800 . ?
C50 H50B 0.9800 . ?
C50 H50C 0.9800 . ?
C51 H51A 0.9800 . ?
C51 H51B 0.9800 . ?
C51 H51C 0.9800 . ?
C52 H52A 0.9800 . ?
C52 H52B 0.9800 . ?
C52 H52C 0.9800 . ?
C53 H53A 0.9800 . ?
C53 H53B 0.9800 . ?
C53 H53C 0.9800 . ?
C54 Y2 2.467(6) 2_656 ?
C54 C55 1.229(9) . ?
C55 C56 1.446(10) . ?
C56 C57 1.381(12) . ?
C56 C61 1.389(11) . ?
C57 H57 0.9500 . ?
C57 C58 1.382(12) . ?
C58 H58 0.9500 . ?
C58 C59 1.395(16) . ?
C59 H59 0.9500 . ?
C59 C60 1.372(15) . ?
C60 H60 0.9500 . ?
C60 C61 1.360(11) . ?
C61 H61 0.9500 . ?
C62 C63 1.392(10) . ?
C62 C67 1.406(9) . ?
C63 H63 0.9500 . ?
C63 C64 1.386(10) . ?
C64 H64 0.9500 . ?
C64 C65 1.362(11) . ?
C65 H65 0.9500 . ?
C65 C66 1.385(12) . ?
C66 H66 0.9500 . ?
C66 C67 1.393(10) . ?
C67 H67 0.9500 . ?
C68 C69 1.453(9) . ?
C69 C70 1.179(9) . ?
C70 C71 1.429(9) . ?
C71 C72 1.375(10) . ?
C71 C76 1.403(10) . ?
C72 H72 0.9500 . ?
C72 C73 1.358(10) . ?
C73 H73 0.9500 . ?
C73 C74 1.375(11) . ?
C74 H74 0.9500 . ?
C74 C75 1.394(12) . ?
C75 H75 0.9500 . ?
C75 C76 1.367(10) . ?
C76 H76 0.9500 . ?
C77 C78 1.386(9) . ?
C77 C82 1.369(10) . ?
C78 H78 0.9500 . ?
C78 C79 1.394(10) . ?
C79 H79 0.9500 . ?
C79 C80 1.353(11) . ?
C80 H80 0.9500 . ?
C80 C81 1.372(11) . ?
C81 H81 0.9500 . ?
C81 C82 1.391(11) . ?
C82 H82 0.9500 . ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 Y1 Y1 113.94(13) . 2_765 ?
N1 Y1 C1 99.15(18) . . ?
N1 Y1 C2 125.09(19) . . ?
N1 Y1 C3 150.60(18) . . ?
N1 Y1 C4 131.2(2) . . ?
N1 Y1 C5 103.00(19) . . ?
N1 Y1 C13 91.32(18) . 2_765 ?
N1 Y1 C13 126.46(19) . . ?
N1 Y1 C27 28.62(18) . . ?
N2 Y1 Y1 117.62(13) . 2_765 ?
N2 Y1 N1 56.60(18) . . ?
N2 Y1 C1 91.72(18) . . ?
N2 Y1 C2 92.32(19) . . ?
N2 Y1 C3 120.5(2) . . ?
N2 Y1 C4 141.76(18) . . ?
N2 Y1 C5 120.59(19) . . ?
N2 Y1 C13 132.81(19) . 2_765 ?
N2 Y1 C13 91.56(19) . . ?
N2 Y1 C27 28.03(19) . . ?
C1 Y1 Y1 144.06(13) . 2_765 ?
C1 Y1 C2 31.65(18) . . ?
C1 Y1 C3 51.79(18) . . ?
C1 Y1 C4 51.83(18) . . ?
C1 Y1 C5 31.86(18) . . ?
C1 Y1 C27 97.26(17) . . ?
C2 Y1 Y1 120.74(14) . 2_765 ?
C2 Y1 C3 31.1(2) . . ?
C2 Y1 C4 51.1(2) . . ?
C2 Y1 C27 111.20(19) . . ?
C3 Y1 Y1 93.53(13) . 2_765 ?
C3 Y1 C27 142.28(19) . . ?
C4 Y1 Y1 94.01(14) . 2_765 ?
C4 Y1 C3 30.3(2) . . ?
C4 Y1 C27 146.26(19) . . ?
C5 Y1 Y1 121.37(14) . 2_765 ?
C5 Y1 C2 51.74(19) . . ?
C5 Y1 C3 50.8(2) . . ?
C5 Y1 C4 30.7(2) . . ?
C5 Y1 C27 115.81(18) . . ?
C13 Y1 Y1 40.46(13) 2_765 2_765 ?
C13 Y1 Y1 40.35(13) . 2_765 ?
C13 Y1 C1 126.13(19) . . ?
C13 Y1 C1 130.1(2) 2_765 . ?
C13 Y1 C2 94.49(19) . . ?
C13 Y1 C2 134.5(2) 2_765 . ?
C13 Y1 C3 104.3(2) 2_765 . ?
C13 Y1 C3 81.2(2) . . ?
C13 Y1 C4 85.11(19) 2_765 . ?
C13 Y1 C4 101.0(2) . . ?
C13 Y1 C5 130.5(2) . . ?
C13 Y1 C5 98.2(2) 2_765 . ?
C13 Y1 C13 80.8(2) 2_765 . ?
C13 Y1 C27 109.59(19) . . ?
C13 Y1 C27 112.98(19) 2_765 . ?
C27 Y1 Y1 118.46(12) . 2_765 ?
N3 Y2 Y2 118.91(13) . 2_656 ?
N3 Y2 C42 94.69(19) . . ?
N3 Y2 C43 125.4(2) . . ?
N3 Y2 C44 140.2(2) . . ?
N3 Y2 C45 113.9(2) . . ?
N3 Y2 C46 89.51(19) . . ?
N3 Y2 C54 93.3(2) . . ?
N3 Y2 C54 133.1(2) . 2_656 ?
N3 Y2 C68 28.1(2) . . ?
N4 Y2 Y2 113.88(13) . 2_656 ?
N4 Y2 N3 56.02(19) . . ?
N4 Y2 C42 97.18(19) . . ?
N4 Y2 C43 107.0(2) . . ?
N4 Y2 C44 136.6(3) . . ?
N4 Y2 C45 148.15(19) . . ?
N4 Y2 C46 119.95(19) . . ?
N4 Y2 C54 91.1(2) . 2_656 ?
N4 Y2 C54 126.7(2) . . ?
N4 Y2 C68 28.0(2) . . ?
C42 Y2 Y2 142.97(14) . 2_656 ?
C42 Y2 C43 31.7(2) . . ?
C42 Y2 C44 51.4(2) . . ?
C42 Y2 C45 51.56(19) . . ?
C42 Y2 C46 32.31(19) . . ?
C42 Y2 C68 98.23(19) . . ?
C43 Y2 Y2 115.20(17) . 2_656 ?
C43 Y2 C44 30.3(3) . . ?
C43 Y2 C45 51.0(2) . . ?
C43 Y2 C68 121.0(2) . . ?
C44 Y2 Y2 91.57(17) . 2_656 ?
C44 Y2 C45 31.1(2) . . ?
C44 Y2 C68 149.3(2) . . ?
C45 Y2 Y2 97.49(15) . 2_656 ?
C45 Y2 C68 136.4(2) . . ?
C46 Y2 Y2 126.04(15) . 2_656 ?
C46 Y2 C43 51.8(2) . . ?
C46 Y2 C44 50.7(2) . . ?
C46 Y2 C45 29.9(2) . . ?
C46 Y2 C68 107.4(2) . . ?
C54 Y2 Y2 40.06(15) . 2_656 ?
C54 Y2 Y2 40.41(16) 2_656 2_656 ?
C54 Y2 C42 130.8(2) . . ?
C54 Y2 C42 124.4(2) 2_656 . ?
C54 Y2 C43 93.6(2) 2_656 . ?
C54 Y2 C43 125.9(2) . . ?
C54 Y2 C44 86.7(2) 2_656 . ?
C54 Y2 C44 95.7(3) . . ?
C54 Y2 C45 110.9(2) 2_656 . ?
C54 Y2 C45 81.0(2) . . ?
C54 Y2 C46 137.4(2) 2_656 . ?
C54 Y2 C46 99.5(2) . . ?
C54 Y2 C54 80.5(2) 2_656 . ?
C54 Y2 C68 112.4(2) 2_656 . ?
C54 Y2 C68 110.6(2) . . ?
C68 Y2 Y2 118.70(13) . 2_656 ?
C6 Si1 C1 106.6(3) . . ?
C6 Si1 C7 109.7(5) . . ?
C6 Si1 C8 106.6(4) . . ?
C7 Si1 C1 113.9(3) . . ?
C7 Si1 C8 107.1(5) . . ?
C8 Si1 C1 112.6(4) . . ?
C1 Si1A C6A 122.1(17) . . ?
C1 Si1A C7A 108.4(16) . . ?
C1 Si1A C8A 113.1(19) . . ?
C6A Si1A C7A 100(2) . . ?
C8A Si1A C6A 109(3) . . ?
C8A Si1A C7A 101(2) . . ?
C42 Si2 C49 113.3(4) . . ?
C47 Si2 C42 109.1(4) . . ?
C47 Si2 C48 110.2(5) . . ?
C47 Si2 C49 104.9(5) . . ?
C48 Si2 C42 113.9(4) . . ?
C48 Si2 C49 105.0(5) . . ?
C47A Si2A C42 110.6(15) . . ?
C47A Si2A C48A 102(2) . . ?
C48A Si2A C42 99.5(14) . . ?
C49A Si2A C42 119.3(16) . . ?
C49A Si2A C47A 114(2) . . ?
C49A Si2A C48A 109(2) . . ?
C21 N1 Y1 142.9(4) . . ?
C27 N1 Y1 93.4(4) . . ?
C27 N1 C21 122.7(5) . . ?
C27 N2 Y1 94.6(4) . . ?
C27 N2 C36 123.4(5) . . ?
C36 N2 Y1 141.6(4) . . ?
C62 N3 Y2 141.8(4) . . ?
C68 N3 Y2 94.3(4) . . ?
C68 N3 C62 123.9(6) . . ?
C68 N4 Y2 94.9(4) . . ?
C68 N4 C77 120.8(5) . . ?
C77 N4 Y2 142.7(4) . . ?
Si1 C1 Y1 128.0(3) . . ?
Si1A C1 Y1 133.4(6) . . ?
C2 C1 Y1 75.0(3) . . ?
C2 C1 Si1 126.1(5) . . ?
C2 C1 Si1A 138.3(8) . . ?
C2 C1 C5 106.3(5) . . ?
C5 C1 Y1 74.6(3) . . ?
C5 C1 Si1 125.8(5) . . ?
C5 C1 Si1A 110.5(7) . . ?
C1 C2 Y1 73.4(3) . . ?
C1 C2 C9 128.9(6) . . ?
C3 C2 Y1 75.9(3) . . ?
C3 C2 C1 108.0(6) . . ?
C3 C2 C9 123.2(6) . . ?
C9 C2 Y1 117.7(4) . . ?
C2 C3 Y1 73.0(3) . . ?
C2 C3 C10 126.2(7) . . ?
C4 C3 Y1 74.6(4) . . ?
C4 C3 C2 108.5(5) . . ?
C4 C3 C10 124.9(7) . . ?
C10 C3 Y1 123.7(4) . . ?
C3 C4 Y1 75.1(4) . . ?
C3 C4 C5 108.7(6) . . ?
C3 C4 C11 126.2(7) . . ?
C5 C4 Y1 73.1(3) . . ?
C5 C4 C11 124.7(7) . . ?
C11 C4 Y1 123.8(4) . . ?
C1 C5 Y1 73.5(3) . . ?
C1 C5 C12 124.8(6) . . ?
C4 C5 Y1 76.1(4) . . ?
C4 C5 C1 108.6(6) . . ?
C4 C5 C12 126.5(6) . . ?
C12 C5 Y1 119.4(4) . . ?
Si1 C6 H6A 109.5 . . ?
Si1 C6 H6B 109.5 . . ?
Si1 C6 H6C 109.5 . . ?
H6A C6 H6B 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
Si1A C6A H6AA 109.5 . . ?
Si1A C6A H6AB 109.5 . . ?
Si1A C6A H6AC 109.5 . . ?
H6AA C6A H6AB 109.5 . . ?
H6AA C6A H6AC 109.5 . . ?
H6AB C6A H6AC 109.5 . . ?
Si1 C7 H7A 109.5 . . ?
Si1 C7 H7B 109.5 . . ?
Si1 C7 H7C 109.5 . . ?
H7A C7 H7B 109.5 . . ?
H7A C7 H7C 109.5 . . ?
H7B C7 H7C 109.5 . . ?
Si1A C7A H7AA 109.5 . . ?
Si1A C7A H7AB 109.5 . . ?
Si1A C7A H7AC 109.5 . . ?
H7AA C7A H7AB 109.5 . . ?
H7AA C7A H7AC 109.5 . . ?
H7AB C7A H7AC 109.5 . . ?
Si1 C8 H8A 109.5 . . ?
Si1 C8 H8B 109.5 . . ?
Si1 C8 H8C 109.5 . . ?
H8A C8 H8B 109.5 . . ?
H8A C8 H8C 109.5 . . ?
H8B C8 H8C 109.5 . . ?
Si1A C8A H8AA 109.5 . . ?
Si1A C8A H8AB 109.5 . . ?
Si1A C8A H8AC 109.5 . . ?
H8AA C8A H8AB 109.5 . . ?
H8AA C8A H8AC 109.5 . . ?
H8AB C8A H8AC 109.5 . . ?
C2 C9 H9A 109.5 . . ?
C2 C9 H9B 109.5 . . ?
C2 C9 H9C 109.5 . . ?
H9A C9 H9B 109.5 . . ?
H9A C9 H9C 109.5 . . ?
H9B C9 H9C 109.5 . . ?
C3 C10 H10A 109.5 . . ?
C3 C10 H10B 109.5 . . ?
C3 C10 H10C 109.5 . . ?
H10A C10 H10B 109.5 . . ?
H10A C10 H10C 109.5 . . ?
H10B C10 H10C 109.5 . . ?
C4 C11 H11A 109.5 . . ?
C4 C11 H11B 109.5 . . ?
C4 C11 H11C 109.5 . . ?
H11A C11 H11B 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C5 C12 H12A 109.5 . . ?
C5 C12 H12B 109.5 . . ?
C5 C12 H12C 109.5 . . ?
H12A C12 H12B 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
Y1 C13 Y1 99.2(2) 2_765 . ?
C14 C13 Y1 143.7(5) . . ?
C14 C13 Y1 117.1(5) . 2_765 ?
C13 C14 C15 177.3(7) . . ?
C16 C15 C14 121.0(7) . . ?
C16 C15 C20 118.4(6) . . ?
C20 C15 C14 120.6(6) . . ?
C15 C16 H16 120.4 . . ?
C17 C16 C15 119.3(8) . . ?
C17 C16 H16 120.4 . . ?
C16 C17 H17 119.0 . . ?
C18 C17 C16 122.0(9) . . ?
C18 C17 H17 119.0 . . ?
C17 C18 H18 120.5 . . ?
C17 C18 C19 119.0(8) . . ?
C19 C18 H18 120.5 . . ?
C18 C19 H19 119.1 . . ?
C18 C19 C20 121.7(8) . . ?
C20 C19 H19 119.1 . . ?
C15 C20 H20 120.2 . . ?
C19 C20 C15 119.6(7) . . ?
C19 C20 H20 120.2 . . ?
C22 C21 N1 118.6(6) . . ?
C22 C21 C26 118.2(6) . . ?
C26 C21 N1 123.2(6) . . ?
C21 C22 H22 119.6 . . ?
C21 C22 C23 120.8(7) . . ?
C23 C22 H22 119.6 . . ?
C22 C23 H23 119.9 . . ?
C24 C23 C22 120.2(7) . . ?
C24 C23 H23 119.9 . . ?
C23 C24 H24 119.8 . . ?
C25 C24 C23 120.4(7) . . ?
C25 C24 H24 119.8 . . ?
C24 C25 H25 120.2 . . ?
C24 C25 C26 119.6(6) . . ?
C26 C25 H25 120.2 . . ?
C21 C26 H26 119.6 . . ?
C25 C26 C21 120.8(6) . . ?
C25 C26 H26 119.6 . . ?
N1 C27 Y1 58.0(3) . . ?
N1 C27 C28 121.5(6) . . ?
N2 C27 Y1 57.3(3) . . ?
N2 C27 N1 115.2(5) . . ?
N2 C27 C28 123.2(6) . . ?
C28 C27 Y1 176.4(4) . . ?
C29 C28 C27 176.5(8) . . ?
C28 C29 C30 177.1(7) . . ?
C31 C30 C29 121.3(6) . . ?
C35 C30 C29 119.3(6) . . ?
C35 C30 C31 119.3(6) . . ?
C30 C31 H31 121.0 . . ?
C30 C31 C32 118.0(7) . . ?
C32 C31 H31 121.0 . . ?
C31 C32 H32 119.5 . . ?
C33 C32 C31 121.0(7) . . ?
C33 C32 H32 119.5 . . ?
C32 C33 H33 119.6 . . ?
C34 C33 C32 120.7(7) . . ?
C34 C33 H33 119.6 . . ?
C33 C34 H34 120.2 . . ?
C33 C34 C35 119.7(7) . . ?
C35 C34 H34 120.2 . . ?
C30 C35 H35 119.4 . . ?
C34 C35 C30 121.2(6) . . ?
C34 C35 H35 119.4 . . ?
C37 C36 N2 124.0(6) . . ?
C41 C36 N2 117.6(5) . . ?
C41 C36 C37 118.2(6) . . ?
C36 C37 H37 119.7 . . ?
C38 C37 C36 120.6(7) . . ?
C38 C37 H37 119.7 . . ?
C37 C38 H38 119.7 . . ?
C39 C38 C37 120.6(7) . . ?
C39 C38 H38 119.7 . . ?
C38 C39 H39 119.9 . . ?
C38 C39 C40 120.1(7) . . ?
C40 C39 H39 119.9 . . ?
C39 C40 H40 120.5 . . ?
C39 C40 C41 119.1(7) . . ?
C41 C40 H40 120.5 . . ?
C36 C41 C40 121.3(6) . . ?
C36 C41 H41 119.3 . . ?
C40 C41 H41 119.3 . . ?
Si2 C42 Y2 128.7(3) . . ?
Si2A C42 Y2 121.7(6) . . ?
C43 C42 Y2 75.3(4) . . ?
C43 C42 Si2 125.8(5) . . ?
C43 C42 Si2A 143.4(8) . . ?
C43 C42 C46 105.6(6) . . ?
C46 C42 Y2 74.5(3) . . ?
C46 C42 Si2 126.4(5) . . ?
C46 C42 Si2A 110.1(7) . . ?
C42 C43 Y2 73.0(3) . . ?
C42 C43 C50 127.2(8) . . ?
C44 C43 Y2 76.1(4) . . ?
C44 C43 C42 108.6(6) . . ?
C44 C43 C50 124.1(8) . . ?
C50 C43 Y2 118.8(4) . . ?
C43 C44 Y2 73.6(4) . . ?
C43 C44 C45 108.7(6) . . ?
C43 C44 C51 130.2(8) . . ?
C45 C44 Y2 75.2(4) . . ?
C45 C44 C51 120.9(8) . . ?
C51 C44 Y2 120.5(5) . . ?
C44 C45 Y2 73.8(4) . . ?
C44 C45 C52 126.7(7) . . ?
C46 C45 Y2 72.5(4) . . ?
C46 C45 C44 107.9(6) . . ?
C46 C45 C52 125.2(7) . . ?
C52 C45 Y2 123.1(4) . . ?
C42 C46 Y2 73.2(3) . . ?
C42 C46 C53 124.7(6) . . ?
C45 C46 Y2 77.6(4) . . ?
C45 C46 C42 109.1(6) . . ?
C45 C46 C53 126.0(6) . . ?
C53 C46 Y2 119.4(4) . . ?
Si2 C47 H47A 109.5 . . ?
Si2 C47 H47B 109.5 . . ?
Si2 C47 H47C 109.5 . . ?
H47A C47 H47B 109.5 . . ?
H47A C47 H47C 109.5 . . ?
H47B C47 H47C 109.5 . . ?
Si2A C47A H47D 109.5 . . ?
Si2A C47A H47E 109.5 . . ?
Si2A C47A H47F 109.5 . . ?
H47D C47A H47E 109.5 . . ?
H47D C47A H47F 109.5 . . ?
H47E C47A H47F 109.5 . . ?
Si2 C48 H48A 109.5 . . ?
Si2 C48 H48B 109.5 . . ?
Si2 C48 H48C 109.5 . . ?
H48A C48 H48B 109.5 . . ?
H48A C48 H48C 109.5 . . ?
H48B C48 H48C 109.5 . . ?
Si2A C48A H48D 109.5 . . ?
Si2A C48A H48E 109.5 . . ?
Si2A C48A H48F 109.5 . . ?
H48D C48A H48E 109.5 . . ?
H48D C48A H48F 109.5 . . ?
H48E C48A H48F 109.5 . . ?
Si2 C49 H49A 109.5 . . ?
Si2 C49 H49B 109.5 . . ?
Si2 C49 H49C 109.5 . . ?
H49A C49 H49B 109.5 . . ?
H49A C49 H49C 109.5 . . ?
H49B C49 H49C 109.5 . . ?
Si2A C49A H49D 109.5 . . ?
Si2A C49A H49E 109.5 . . ?
Si2A C49A H49F 109.5 . . ?
H49D C49A H49E 109.5 . . ?
H49D C49A H49F 109.5 . . ?
H49E C49A H49F 109.5 . . ?
C43 C50 H50A 109.5 . . ?
C43 C50 H50B 109.5 . . ?
C43 C50 H50C 109.5 . . ?
H50A C50 H50B 109.5 . . ?
H50A C50 H50C 109.5 . . ?
H50B C50 H50C 109.5 . . ?
C44 C51 H51A 109.5 . . ?
C44 C51 H51B 109.5 . . ?
C44 C51 H51C 109.5 . . ?
H51A C51 H51B 109.5 . . ?
H51A C51 H51C 109.5 . . ?
H51B C51 H51C 109.5 . . ?
C45 C52 H52A 109.5 . . ?
C45 C52 H52B 109.5 . . ?
C45 C52 H52C 109.5 . . ?
H52A C52 H52B 109.5 . . ?
H52A C52 H52C 109.5 . . ?
H52B C52 H52C 109.5 . . ?
C46 C53 H53A 109.5 . . ?
C46 C53 H53B 109.5 . . ?
C46 C53 H53C 109.5 . . ?
H53A C53 H53B 109.5 . . ?
H53A C53 H53C 109.5 . . ?
H53B C53 H53C 109.5 . . ?
Y2 C54 Y2 99.5(2) 2_656 . ?
C55 C54 Y2 119.1(5) . 2_656 ?
C55 C54 Y2 141.4(5) . . ?
C54 C55 C56 177.0(8) . . ?
C57 C56 C55 120.4(7) . . ?
C57 C56 C61 119.1(8) . . ?
C61 C56 C55 120.5(8) . . ?
C56 C57 H57 119.9 . . ?
C56 C57 C58 120.3(10) . . ?
C58 C57 H57 119.9 . . ?
C57 C58 H58 120.5 . . ?
C57 C58 C59 119.1(10) . . ?
C59 C58 H58 120.5 . . ?
C58 C59 H59 119.6 . . ?
C60 C59 C58 120.9(8) . . ?
C60 C59 H59 119.6 . . ?
C59 C60 H60 120.4 . . ?
C61 C60 C59 119.3(9) . . ?
C61 C60 H60 120.4 . . ?
C56 C61 H61 119.3 . . ?
C60 C61 C56 121.4(9) . . ?
C60 C61 H61 119.3 . . ?
C63 C62 N3 117.4(6) . . ?
C63 C62 C67 118.3(6) . . ?
C67 C62 N3 124.2(6) . . ?
C62 C63 H63 119.9 . . ?
C64 C63 C62 120.3(7) . . ?
C64 C63 H63 119.9 . . ?
C63 C64 H64 119.2 . . ?
C65 C64 C63 121.5(8) . . ?
C65 C64 H64 119.2 . . ?
C64 C65 H65 120.3 . . ?
C64 C65 C66 119.4(7) . . ?
C66 C65 H65 120.3 . . ?
C65 C66 H66 119.8 . . ?
C65 C66 C67 120.3(7) . . ?
C67 C66 H66 119.8 . . ?
C62 C67 H67 119.9 . . ?
C66 C67 C62 120.2(7) . . ?
C66 C67 H67 119.9 . . ?
N3 C68 Y2 57.6(3) . . ?
N3 C68 C69 123.3(6) . . ?
N4 C68 Y2 57.1(3) . . ?
N4 C68 N3 114.5(6) . . ?
N4 C68 C69 122.2(6) . . ?
C69 C68 Y2 174.0(5) . . ?
C70 C69 C68 177.2(8) . . ?
C69 C70 C71 178.4(7) . . ?
C72 C71 C70 122.4(7) . . ?
C72 C71 C76 117.8(6) . . ?
C76 C71 C70 119.7(6) . . ?
C71 C72 H72 119.0 . . ?
C73 C72 C71 122.0(7) . . ?
C73 C72 H72 119.0 . . ?
C72 C73 H73 120.4 . . ?
C72 C73 C74 119.2(7) . . ?
C74 C73 H73 120.4 . . ?
C73 C74 H74 119.5 . . ?
C73 C74 C75 121.0(7) . . ?
C75 C74 H74 119.5 . . ?
C74 C75 H75 120.8 . . ?
C76 C75 C74 118.4(7) . . ?
C76 C75 H75 120.8 . . ?
C71 C76 H76 119.4 . . ?
C75 C76 C71 121.3(7) . . ?
C75 C76 H76 119.4 . . ?
C78 C77 N4 122.9(6) . . ?
C82 C77 N4 118.8(6) . . ?
C82 C77 C78 118.2(7) . . ?
C77 C78 H78 120.0 . . ?
C77 C78 C79 120.1(7) . . ?
C79 C78 H78 120.0 . . ?
C78 C79 H79 119.6 . . ?
C80 C79 C78 120.9(7) . . ?
C80 C79 H79 119.6 . . ?
C79 C80 H80 120.1 . . ?
C79 C80 C81 119.7(8) . . ?
C81 C80 H80 120.1 . . ?
C80 C81 H81 120.2 . . ?
C80 C81 C82 119.7(8) . . ?
C82 C81 H81 120.2 . . ?
C77 C82 C81 121.4(7) . . ?
C77 C82 H82 119.3 . . ?
C81 C82 H82 119.3 . . ?
_shelx_estimated_absorpt_T_max 0.846
_shelx_estimated_absorpt_T_min 0.846
_shelx_hkl_checksum 23986
_shelx_hkl_file
;
-17 -3 4 222.098 206.944 1
-17 -3 5 2077.31 518.819 1
-17 -2 3-110.163 167.016 1
-17 -2 4 1251.81 385.752 1
-17 -2 5 62.6554 133.544 1
-17 -1 2 1771.22 465.042 1
-17 -1 3 735.136 323.763 1
-17 -1 4 2482.86 544.390 1
-17 -1 5 1479.91 421.154 1
-17 -1 6 65.6283 179.383 1
-17 0 2 80.7517 233.076 1
-17 0 3 1569.64 437.783 1
-17 0 4 397.315 225.571 1
-17 0 5 713.802 346.887 1
-17 0 6 804.027 330.859 1
-17 1 2 1502.64 420.107 1
-17 1 3 557.799 302.403 1
-17 1 4 1056.41 420.463 1
-17 1 5 192.271 224.564 1
-17 1 6-214.899 179.944 1
-17 2 3 830.203 378.697 1
-17 2 4 2531.54 587.605 1
-17 2 5 45.5598 186.918 1
-17 2 6 2628.66 539.286 1
-17 3 3 2145.32 542.763 1
-17 3 4 938.632 357.256 1
-17 3 5 2101.20 495.922 1
-17 3 6 286.641 225.626 1
-17 4 4 50.9599 169.717 2
-17 4 5 81.3187 151.960 1
-17 4 5 88.9040 148.821 2
-17 4 6 198.530 184.767 1
-17 5 3-305.272 210.633 2
-17 5 4 292.759 190.118 2
-17 5 5-341.032 273.583 2
-17 6 3 1492.92 412.989 2
-17 6 4 628.262 281.522 2
-17 6 5-196.102 180.537 2
-16 -7 3 285.859 212.213 1
-16 -7 4 1838.70 494.039 1
-16 -7 5 570.867 321.303 1
-16 -6 1 18.2273 143.036 1
-16 -6 2 2974.82 590.461 1
-16 -6 3 573.575 307.876 1
-16 -6 4 2387.74 552.973 1
-16 -6 5 1621.66 428.370 1
-16 -5 0 12.3908 247.908 1
-16 -5 1 3142.61 627.523 1
-16 -5 2-39.7286 132.694 1
-16 -5 3 3289.20 623.591 1
-16 -5 4-259.083 236.508 1
-16 -5 5 1019.65 328.714 1
-16 -5 6 1640.07 419.151 1
-16 -4 -1 462.864 311.274 1
-16 -4 0 1453.00 477.892 1
-16 -4 1 188.950 177.789 1
-16 -4 2 177.897 186.467 1
-16 -4 3 927.444 326.951 1
-16 -4 4 1100.15 352.008 1
-16 -4 5 2359.92 516.259 1
-16 -4 6 337.463 205.928 1
-16 -3 -3 457.782 303.126 4
-16 -3 -2 3062.22 627.891 1
-16 -3 -2 2167.54 612.111 4
-16 -3 -1-59.5932 183.792 1
-16 -3 0 246.629 180.621 1
-16 -3 1-112.731 214.892 1
-16 -3 2 499.109 256.677 1
-16 -3 3 240.857 231.384 1
-16 -3 4 2006.93 461.925 1
-16 -3 5-39.8122 128.012 1
-16 -3 6 1705.27 417.038 1
-16 -2 -7 1367.97 479.081 4
-16 -2 -6 386.849 332.429 4
-16 -2 -5 1317.36 454.616 4
-16 -2 -4 1140.94 443.571 4
-16 -2 -3 2501.70 621.568 4
-16 -2 -3 1807.62 433.281 1
-16 -2 -2 768.242 360.469 4
-16 -2 -2 139.725 154.478 1
-16 -2 -1 2071.79 502.456 1
-16 -2 -1 2455.27 610.247 4
-16 -2 0 837.881 385.000 4
-16 -2 0 398.376 150.358 1
-16 -2 1 1118.47 362.295 1
-16 -2 1 1805.77 500.763 4
-16 -2 2 327.428 233.258 1
-16 -2 3 1174.07 356.045 1
-16 -2 4 815.870 316.533 1
-16 -2 5 2287.53 504.884 1
-16 -2 6 242.385 210.204 1
-16 -2 7 2015.78 442.316 1
-16 -1 -3 1724.97 455.863 1
-16 -1 -2 105.012 170.462 1
-16 -1 -1 983.525 314.872 1
-16 -1 0 417.264 212.601 1
-16 -1 1 2017.16 452.783 1
-16 -1 2 765.849 317.340 1
-16 -1 3 3494.73 609.632 1
-16 -1 4 880.525 343.087 1
-16 -1 5 643.337 282.334 1
-16 -1 6 76.4536 151.379 1
-16 -1 7 2271.31 480.007 1
-16 0 -3 183.664 216.912 1
-16 0 -2 1900.53 497.581 1
-16 0 -1 63.6758 197.545 1
-16 0 0 4249.63 700.136 1
-16 0 1 137.503 188.142 1
-16 0 2 1763.29 467.403 1
-16 0 3-255.352 234.094 1
-16 0 4 1680.37 447.712 1
-16 0 5 211.760 195.452 1
-16 0 6 586.556 269.500 1
-16 0 7-25.3987 139.549 1
-16 1 -3 391.340 300.277 1
-16 1 -2 1183.99 387.765 1
-16 1 -1 1638.99 452.100 1
-16 1 0 290.642 223.657 1
-16 1 1 1948.16 472.572 1
-16 1 2 544.316 308.179 1
-16 1 3 709.813 302.977 1
-16 1 4 1726.14 454.208 1
-16 1 5 468.116 242.836 1
-16 1 6 1236.59 363.079 1
-16 1 7 394.009 240.965 1
-16 2 -3 2848.02 637.288 1
-16 2 -2 1101.74 387.724 1
-16 2 -1 2816.09 601.624 1
-16 2 0 1137.46 387.163 1
-16 2 1 1549.44 451.521 1
-16 2 2 907.264 365.059 1
-16 2 3 1289.33 414.697 1
-16 2 4 502.818 282.968 1
-16 2 5 2153.29 493.188 1
-16 2 6 9.37382 125.803 1
-16 2 7 1852.54 450.736 1
-16 2 7 1630.05 452.295 2
-16 3 -3 1583.04 526.054 1
-16 3 -2 1668.70 457.260 1
-16 3 -1 2629.96 591.604 1
-16 3 0 3730.02 679.084 1
-16 3 1 3347.24 645.096 1
-16 3 2 928.954 353.399 1
-16 3 3 3554.52 616.304 1
-16 3 4 2438.93 526.702 1
-16 3 5 150.307 205.131 1
-16 3 6 2777.80 545.731 1
-16 3 6 2593.23 554.566 2
-16 3 7 1242.09 419.721 2
-16 3 7 1100.83 318.611 1
-16 4 -2 2431.98 564.581 1
-16 4 -1-100.995 244.218 1
-16 4 0 3121.79 620.041 1
-16 4 1 135.126 210.336 1
-16 4 2 3074.15 632.334 1
-16 4 3 245.639 227.423 1
-16 4 4 2853.63 573.505 1
-16 4 5 803.571 326.167 1
-16 4 5 313.923 233.108 2
-16 4 6 1175.25 376.311 2
-16 4 6 1200.74 383.993 1
-16 4 7-77.5097 195.833 2
-16 4 7 24.0007 154.050 1
-16 5 -2 17.0020 176.666 1
-16 5 -1 2100.46 519.552 1
-16 5 0 1119.11 391.287 1
-16 5 1 2405.54 546.426 1
-16 5 2-14.9404 158.161 1
-16 5 3 894.169 335.383 1
-16 5 3 1249.86 355.576 2
-16 5 4 192.774 182.859 1
-16 5 4-221.203 209.502 2
-16 5 5 1457.88 435.658 2
-16 5 5 1956.56 487.833 1
-16 5 6 544.036 254.305 2
-16 5 6 528.230 271.104 1
-16 5 7 899.608 320.866 1
-16 5 7 783.284 345.918 2
-16 5 8 354.091 196.229 1
-16 6 0 1098.99 394.647 1
-16 6 1 974.062 398.341 1
-16 6 2 1370.42 361.807 2
-16 6 2 1938.59 524.563 1
-16 6 3 569.676 234.900 2
-16 6 3 553.188 295.291 1
-16 6 4 1134.57 352.100 2
-16 6 4 1063.52 366.260 1
-16 6 5 690.375 297.142 1
-16 6 5 580.358 254.000 2
-16 6 6-368.554 263.457 2
-16 6 6 28.6947 148.278 1
-16 6 7 1517.14 448.397 1
-16 6 7 1583.00 442.114 2
-16 6 8 308.532 192.104 1
-16 7 2 1569.43 377.239 2
-16 7 2 1767.64 468.808 1
-16 7 3 1540.89 468.299 1
-16 7 3 1078.74 331.535 2
-16 7 4 3034.92 611.078 1
-16 7 4 2778.10 533.978 2
-16 7 5 37.7032 159.752 1
-16 7 5 149.384 145.032 2
-16 7 6 2411.58 495.698 2
-16 7 6 2203.05 519.124 1
-16 7 7 340.281 247.362 2
-16 7 7-87.9696 185.331 1
-16 8 5 420.582 262.172 2
-16 8 6 211.598 198.268 2
-16 8 7 502.557 273.467 1
-16 8 7 867.419 354.602 2
-15 -10 4 1093.91 341.625 1
-15 -9 1 619.559 265.342 1
-15 -9 2 1203.80 383.358 1
-15 -9 3 1082.36 390.048 1
-15 -9 4 1137.58 380.805 1
-15 -9 5 1439.16 419.258 1
-15 -8 -1 682.044 320.969 1
-15 -8 0 1249.94 436.779 1
-15 -8 1 669.637 282.525 1
-15 -8 2 1274.58 419.647 1
-15 -8 3 202.904 143.857 1
-15 -8 4 2513.92 531.598 1
-15 -8 5 113.545 201.674 1
-15 -8 6 1900.09 477.702 1
-15 -7 -2 710.469 329.797 1
-15 -7 -1 1612.92 464.087 1
-15 -7 0 2179.18 504.671 1
-15 -7 1 613.855 333.406 1
-15 -7 2 730.423 310.749 1
-15 -7 3 786.420 342.627 1
-15 -7 4 286.078 228.880 1
-15 -7 5 2476.53 531.286 1
-15 -7 6 924.865 335.629 1
-15 -6 -7 2846.79 668.227 4
-15 -6 -6 290.765 359.196 4
-15 -6 -5 949.502 463.538 4
-15 -6 -4 771.223 388.920 4
-15 -6 -3 1911.53 539.162 1
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-15 -6 -2 196.152 216.831 4
-15 -6 -2-20.9820 150.077 1
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-15 -6 2 49.9988 147.399 1
-15 -6 2 41.7821 175.431 4
-15 -6 3 3586.98 715.220 4
-15 -6 3 2991.20 562.122 1
-15 -6 4 774.861 352.488 1
-15 -6 5 976.345 351.381 1
-15 -6 6 2875.87 531.356 1
-15 -5 -10 1177.31 421.735 4
-15 -5 -9 489.838 306.027 4
-15 -5 -8 1722.01 498.423 4
-15 -5 -7 1320.09 491.269 4
-15 -5 -6 5883.71 914.720 4
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-15 -5 -5 560.531 340.059 1
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-15 -5 -4 1508.36 534.110 1
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-15 -5 -1 1190.90 466.026 4
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-15 -5 1 174.260 230.266 4
-15 -5 2 822.596 358.165 1
-15 -5 2 1453.93 466.695 4
-15 -5 3 556.432 317.207 4
-15 -5 3 543.566 306.224 1
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-15 -5 4 1316.86 428.339 4
-15 -5 5 425.697 230.312 1
-15 -5 5 1003.50 423.188 4
-15 -5 6 2188.93 564.466 4
-15 -5 6 2515.08 506.792 1
-15 -5 7 3168.91 536.531 1
-15 -4 -11 734.944 352.929 4
-15 -4 -10 162.731 178.495 4
-15 -4 -9 2125.78 512.922 4
-15 -4 -8 498.598 398.711 4
-15 -4 -7 2041.54 536.842 4
-15 -4 -6 5242.89 890.275 4
-15 -4 -5 2041.24 521.247 1
-15 -4 -5 2207.39 582.553 4
-15 -4 -4 5269.93 834.194 1
-15 -4 -4 5423.35 851.967 4
-15 -4 -3 48.6740 190.769 4
-15 -4 -3-103.531 219.013 1
-15 -4 -2 1578.99 502.272 4
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-15 -4 -1 835.381 333.701 1
-15 -4 -1 671.636 356.037 4
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-15 -4 0 1164.30 374.433 1
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-15 -4 2 1167.78 451.463 4
-15 -4 2 1492.39 417.671 1
-15 -4 3 158.906 168.201 4
-15 -4 3 188.029 241.215 1
-15 -4 4 3519.69 596.450 1
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-15 -4 6 6456.00 930.915 4
-15 -4 6 5727.54 737.064 1
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-15 -3 -11 1700.18 498.671 4
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-15 -3 -9 687.955 329.454 4
-15 -3 -8-28.1360 166.849 4
-15 -3 -7 1063.28 510.948 4
-15 -3 -6 345.219 211.787 4
-15 -3 -6 306.244 272.331 1
-15 -3 -5 4801.74 797.621 4
-15 -3 -5 5552.42 849.708 1
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-15 -3 -4 222.200 253.776 4
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-15 -3 2 397.556 309.134 4
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-15 -3 3 2842.84 645.541 4
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-15 -3 6 1050.61 461.510 4
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-15 -2 -9 1071.77 419.942 4
-15 -2 -8 468.136 275.207 4
-15 -2 -7 2835.59 614.641 4
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-15 -2 -6 3204.10 709.274 1
-15 -2 -6 2517.62 587.881 4
-15 -2 -5 869.456 386.768 1
-15 -2 -5 182.165 220.068 4
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-15 -2 -4 3031.73 657.442 4
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-15 -2 -3 1503.89 401.734 1
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-15 -2 1 2217.53 540.836 4
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-15 -2 4 3443.76 691.438 4
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-15 -2 6 4530.33 639.150 1
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-15 -1 -6 2166.74 558.523 4
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-15 -1 -5 451.714 158.028 1
-15 -1 -4 531.487 284.032 1
-15 -1 -4 775.208 403.271 4
-15 -1 -3 342.196 182.022 1
-15 -1 -3 597.099 322.969 4
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-15 -1 -1 293.017 254.186 4
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-15 -1 3 203.075 163.163 1
-15 -1 4 1826.83 430.031 1
-15 -1 5 481.288 240.939 1
-15 -1 6 1024.40 363.586 1
-15 -1 7-195.848 185.084 1
-15 -1 8 3393.13 552.255 1
-15 0 -7 3484.82 680.958 1
-15 0 -6 2580.20 568.884 1
-15 0 -5 72.6200 327.505 1
-15 0 -4 1168.65 401.081 1
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17 2 5 181.265 196.500 5
17 3 3 3216.50 649.531 5
0 0 0 0.00 0.00 0
TITL 13mar11g in P1
REM P1 (#1 in standard setting)
CELL 0.71073 13.125907 16.223138 16.429402 90.4970 90.0334 93.2036
ZERR 6.00 0.000291 0.000472 0.000459 0.0023 0.0020 0.0021
LATT -1
SFAC C H Si P Pd
UNIT 180.00 120.00 6.00 6.00 6.00
TREF
HKLF 4
END
;
_shelx_res_checksum 51418
_shelx_res_file
;
TITL 13mar11g in P-1 #2
CELL 0.71073 13.12591 16.22314 16.4294 90.497 90.0334 93.2036
ZERR 2 0.00029 0.00047 0.00046 0.0023 0.002 0.0021
LATT 1
SFAC C H Y Si N
UNIT 164 164 4 4 8
DFIX 1.87 0.03 Si1A C8A Si1A C6A Si1A C7A Si2A C48A Si2A C49A Si2A C47A Si1 =
C8 SI1 C7 SI1 C6 SI2 C49 SI2 C48 SI2 C47
EADP Si1 Si1A
EADP C6 C7A
EADP C7 C6A
EADP C8 C8A
EADP C48 C48A
EADP C44 C51
EADP C47 C47A
L.S. 4
PLAN 5
SIZE 0.1 0.1 0.1
TEMP -93
REM reset to P-1 #2
BOND $H
fmap 2
acta
SHEL 999 0.81
OMIT 0 4 3
OMIT -4 4 2
OMIT 7 3 4
OMIT -10 1 2
OMIT -6 1 5
OMIT -6 -1 2
OMIT 2 5 3
OMIT 2 5 1
OMIT -10 3 7
OMIT 6 -7 2
OMIT -4 1 5
OMIT -4 10 4
OMIT 4 2 4
OMIT 8 -4 2
OMIT 4 -7 3
OMIT -10 -4 1
OMIT -5 4 3
OMIT -4 1 2
OMIT 0 4 2
OMIT -7 -1 2
OMIT -10 9 2
OMIT -8 4 1
OMIT -9 5 1
OMIT -7 6 5
OMIT 3 -5 1
OMIT -6 9 7
OMIT -9 3 6
OMIT -6 2 8
OMIT 5 4 5
OMIT 3 -11 4
OMIT -3 8 7
OMIT 10 -9 3
OMIT 6 0 1
OMIT -12 -1 7
OMIT 7 -12 3
OMIT -12 3 5
OMIT -3 12 7
OMIT 7 0 3
OMIT 9 -1 2
OMIT 7 -8 3
REM E:/360?/?/?/?$: ?/?/?/?' /13mar11gx/13mar11g.hkl
WGHT 0.012700 29.178499
FVAR 1.89818 0.78420 0.84988
Y1 3 0.975170 0.397780 0.051674 11.00000 0.01875 0.01545 =
0.02222 0.00133 0.00058 -0.00163
Y2 3 0.467086 -0.102403 0.447991 11.00000 0.02508 0.01985 =
0.02474 0.00134 0.00193 -0.00317
PART 1
SI1 4 0.889566 0.161465 0.108658 31.00000 0.03827 0.02142 =
0.01661 0.00526 0.00287 -0.00681
PART 0
PART 2
SI1A 4 0.912715 0.155974 0.083364 -31.00000 0.03827 0.02142 =
0.01661 0.00526 0.00287 -0.00681
PART 0
PART 1
SI2 4 0.414817 -0.346463 0.408666 21.00000 0.02940 0.01768 =
0.02598 0.00007 0.00981 -0.00127
PART 0
PART 2
SI2A 4 0.382041 -0.335495 0.386022 -21.00000 0.09183 0.01295 =
0.07689 -0.00720 -0.01262 0.00616
PART 0
N1 5 1.087702 0.375577 0.162835 11.00000 0.02700 0.02436 =
0.02581 -0.00489 0.00140 0.00656
N2 5 0.923215 0.399694 0.190215 11.00000 0.03675 0.02490 =
0.02142 0.00352 0.00105 0.00029
N3 5 0.408411 -0.103227 0.310768 11.00000 0.03509 0.02535 =
0.02838 -0.00374 0.00281 -0.00078
N4 5 0.571106 -0.128950 0.333883 11.00000 0.03417 0.02889 =
0.02551 -0.00155 0.00517 0.00068
C1 1 0.898658 0.247442 0.031524 11.00000 0.02236 0.01290 =
0.02800 0.00129 -0.00331 -0.00244
C2 1 0.818663 0.298842 0.009405 11.00000 0.01912 0.02152 =
0.03880 -0.00831 -0.00584 -0.00132
C3 1 0.847428 0.339648 -0.063740 11.00000 0.03808 0.01674 =
0.03612 0.00159 -0.02005 -0.00563
C4 1 0.942884 0.314868 -0.086895 11.00000 0.03984 0.02766 =
0.02236 -0.00458 0.00038 -0.01754
C5 1 0.975559 0.258473 -0.029922 11.00000 0.02557 0.02148 =
0.03063 -0.00693 0.00056 -0.00424
PART 1
C6 1 0.892863 0.063419 0.050432 31.00000 0.06144 0.01815 =
0.03363 0.00605 0.00331 -0.00600
AFIX 137
H6A 2 0.836284 0.059581 0.011391 31.00000 -1.50000
H6B 2 0.886314 0.016822 0.087985 31.00000 -1.50000
H6C 2 0.957737 0.061961 0.021101 31.00000 -1.50000
AFIX 0
PART 0
PART 2
C6A 1 1.032900 0.100530 0.079411 -31.00000 0.04639 0.04048 =
0.04258 0.01526 -0.02288 -0.00845
AFIX 137
H6AA 2 1.031861 0.064054 0.031523 -31.00000 -1.50000
H6AB 2 1.038875 0.067620 0.128749 -31.00000 -1.50000
H6AC 2 1.091288 0.140706 0.075878 -31.00000 -1.50000
AFIX 0
PART 0
PART 1
C7 1 0.993385 0.167323 0.185428 31.00000 0.04639 0.04048 =
0.04258 0.01526 -0.02288 -0.00845
AFIX 137
H7A 2 1.059493 0.166578 0.157819 31.00000 -1.50000
H7B 2 0.985351 0.119931 0.221905 31.00000 -1.50000
H7C 2 0.990180 0.218557 0.217135 31.00000 -1.50000
AFIX 0
PART 0
PART 2
C7A 1 0.905390 0.178344 0.196468 -31.00000 0.06144 0.01815 =
0.03363 0.00605 0.00331 -0.00600
AFIX 137
H7AA 2 0.940693 0.231889 0.208514 -31.00000 -1.50000
H7AB 2 0.937952 0.135007 0.226536 -31.00000 -1.50000
H7AC 2 0.833733 0.179713 0.212882 -31.00000 -1.50000
AFIX 0
PART 0
PART 1
C8 1 0.766137 0.157230 0.165564 31.00000 0.05285 0.04062 =
0.03782 0.00682 0.01366 -0.01266
AFIX 137
H8A 2 0.757431 0.210521 0.192472 31.00000 -1.50000
H8B 2 0.766631 0.113735 0.206561 31.00000 -1.50000
H8C 2 0.709638 0.145214 0.127492 31.00000 -1.50000
AFIX 0
PART 0
PART 2
C8A 1 0.803091 0.080117 0.069155 -31.00000 0.05285 0.04062 =
0.03782 0.00682 0.01366 -0.01266
AFIX 137
H8AA 2 0.748232 0.093211 0.106745 -31.00000 -1.50000
H8AB 2 0.824808 0.024481 0.080203 -31.00000 -1.50000
H8AC 2 0.778278 0.082554 0.013004 -31.00000 -1.50000
AFIX 0
PART 0
C9 1 0.717720 0.310192 0.052052 11.00000 0.01261 0.05281 =
0.06973 -0.01539 0.00129 0.00253
AFIX 137
H9A 2 0.723513 0.295053 0.109417 11.00000 -1.50000
H9B 2 0.664036 0.274809 0.025929 11.00000 -1.50000
H9C 2 0.700475 0.368039 0.048328 11.00000 -1.50000
AFIX 0
C10 1 0.781153 0.393685 -0.114092 11.00000 0.08311 0.02790 =
0.06207 0.00541 -0.05537 0.00232
AFIX 137
H10A 2 0.721492 0.407887 -0.082143 11.00000 -1.50000
H10B 2 0.758579 0.363707 -0.163514 11.00000 -1.50000
H10C 2 0.820623 0.444329 -0.129108 11.00000 -1.50000
AFIX 0
C11 1 0.997311 0.336084 -0.165426 11.00000 0.07063 0.06504 =
0.02315 0.00228 -0.00331 -0.02717
AFIX 137
H11A 2 1.006806 0.396208 -0.170049 11.00000 -1.50000
H11B 2 0.956486 0.314049 -0.211461 11.00000 -1.50000
H11C 2 1.064006 0.311782 -0.165794 11.00000 -1.50000
AFIX 0
C12 1 1.073329 0.211632 -0.033949 11.00000 0.03933 0.04908 =
0.04637 -0.01310 -0.00316 0.00181
AFIX 137
H12A 2 1.130923 0.249955 -0.047858 11.00000 -1.50000
H12B 2 1.065934 0.168110 -0.075615 11.00000 -1.50000
H12C 2 1.085805 0.186801 0.019044 11.00000 -1.50000
AFIX 0
C13 1 0.887614 0.525673 0.023600 11.00000 0.01450 0.02563 =
0.02792 0.00185 0.00202 0.00424
C14 1 0.807625 0.560002 0.033318 11.00000 0.02681 0.02480 =
0.03264 0.00441 -0.00011 -0.00069
C15 1 0.712653 0.597120 0.047390 11.00000 0.02497 0.02663 =
0.04594 0.00613 0.00410 0.00365
C16 1 0.630206 0.581761 -0.004703 11.00000 0.03217 0.06229 =
0.06818 -0.02106 -0.00391 0.01725
AFIX 43
H16 2 0.636330 0.547136 -0.051170 11.00000 -1.20000
AFIX 0
C17 1 0.538984 0.617491 0.011866 11.00000 0.02797 0.08109 =
0.09669 -0.03318 -0.00733 0.01767
AFIX 43
H17 2 0.483103 0.607503 -0.024332 11.00000 -1.20000
AFIX 0
C18 1 0.527046 0.666443 0.078413 11.00000 0.02894 0.05889 =
0.09931 -0.01981 0.00899 0.01642
AFIX 43
H18 2 0.463377 0.689438 0.089137 11.00000 -1.20000
AFIX 0
C19 1 0.607788 0.681989 0.129447 11.00000 0.03079 0.04281 =
0.07205 -0.00363 0.01717 0.01380
AFIX 43
H19 2 0.600145 0.717241 0.175252 11.00000 -1.20000
AFIX 0
C20 1 0.699659 0.648136 0.116444 11.00000 0.02998 0.03197 =
0.05108 -0.00138 0.00580 0.00902
AFIX 43
H20 2 0.754391 0.658844 0.153593 11.00000 -1.20000
AFIX 0
C21 1 1.192355 0.368188 0.183040 11.00000 0.03602 0.02413 =
0.03103 0.00231 -0.00875 0.00597
C22 1 1.242597 0.303418 0.150147 11.00000 0.03772 0.03276 =
0.06429 -0.01931 -0.01745 0.00490
AFIX 43
H22 2 1.206831 0.264716 0.115321 11.00000 -1.20000
AFIX 0
C23 1 1.344265 0.294111 0.167200 11.00000 0.04432 0.03622 =
0.09189 -0.02093 -0.02084 0.01807
AFIX 43
H23 2 1.377680 0.248657 0.144859 11.00000 -1.20000
AFIX 0
C24 1 1.397125 0.350284 0.216286 11.00000 0.03513 0.04182 =
0.07075 -0.00940 -0.02906 0.01376
AFIX 43
H24 2 1.466819 0.343108 0.228462 11.00000 -1.20000
AFIX 0
C25 1 1.350335 0.416433 0.247780 11.00000 0.04082 0.03189 =
0.04125 -0.00402 -0.01851 -0.00203
AFIX 43
H25 2 1.387862 0.456306 0.280178 11.00000 -1.20000
AFIX 0
C26 1 1.247714 0.425115 0.232222 11.00000 0.04032 0.02055 =
0.03169 -0.00247 -0.00687 0.00458
AFIX 43
H26 2 1.214686 0.470387 0.255336 11.00000 -1.20000
AFIX 0
C27 1 1.015446 0.387807 0.219438 11.00000 0.03711 0.01229 =
0.02795 0.00200 -0.00412 0.00062
C28 1 1.038488 0.387948 0.304904 11.00000 0.04121 0.01874 =
0.03003 0.00143 0.00102 -0.00083
C29 1 1.052557 0.389419 0.376921 11.00000 0.03382 0.02141 =
0.03204 0.00505 0.00342 -0.00163
C30 1 1.067033 0.395157 0.463899 11.00000 0.02558 0.01933 =
0.02933 0.00072 -0.00093 0.00062
C31 1 1.164215 0.401501 0.498054 11.00000 0.02512 0.03064 =
0.04294 0.00631 -0.00050 -0.00166
AFIX 43
H31 2 1.223256 0.396389 0.465382 11.00000 -1.20000
AFIX 0
C32 1 1.172262 0.415572 0.581591 11.00000 0.05098 0.04036 =
0.03949 0.00766 -0.02239 -0.00808
AFIX 43
H32 2 1.237855 0.423805 0.605752 11.00000 -1.20000
AFIX 0
C33 1 1.087670 0.417708 0.629106 11.00000 0.08025 0.02655 =
0.02504 0.00385 0.00282 0.00140
AFIX 43
H33 2 1.094898 0.425745 0.686207 11.00000 -1.20000
AFIX 0
C34 1 0.993255 0.408507 0.595925 11.00000 0.04777 0.02811 =
0.03524 -0.00031 0.00878 0.00472
AFIX 43
H34 2 0.934564 0.409197 0.629679 11.00000 -1.20000
AFIX 0
C35 1 0.982806 0.398266 0.514001 11.00000 0.02311 0.03221 =
0.03086 0.00102 0.00122 -0.00259
AFIX 43
H35 2 0.916400 0.393162 0.490834 11.00000 -1.20000
AFIX 0
C36 1 0.835581 0.401668 0.239097 11.00000 0.03293 0.01726 =
0.02360 -0.00372 0.00049 -0.00172
C37 1 0.813405 0.347198 0.302243 11.00000 0.04752 0.02310 =
0.03109 0.00127 -0.00064 -0.00997
AFIX 43
H37 2 0.860972 0.307655 0.316381 11.00000 -1.20000
AFIX 0
C38 1 0.722944 0.349996 0.344615 11.00000 0.04823 0.04078 =
0.03187 0.00431 0.00350 -0.02353
AFIX 43
H38 2 0.708776 0.312323 0.387630 11.00000 -1.20000
AFIX 0
C39 1 0.653760 0.406237 0.325378 11.00000 0.03313 0.05880 =
0.02881 -0.00711 0.01247 -0.01306
AFIX 43
H39 2 0.592210 0.408215 0.355548 11.00000 -1.20000
AFIX 0
C40 1 0.672892 0.460464 0.262042 11.00000 0.02875 0.04289 =
0.04148 -0.00967 0.00793 -0.00327
AFIX 43
H40 2 0.624519 0.499394 0.247987 11.00000 -1.20000
AFIX 0
C41 1 0.764077 0.457220 0.219131 11.00000 0.03534 0.03667 =
0.02448 0.00148 0.00819 -0.00582
AFIX 43
H41 2 0.777255 0.494018 0.175235 11.00000 -1.20000
AFIX 0
C42 1 0.404680 -0.254471 0.475365 11.00000 0.02786 0.01912 =
0.03117 0.00494 0.00916 0.00110
C43 1 0.469865 -0.232193 0.542494 11.00000 0.02430 0.04299 =
0.03789 0.02050 -0.00211 -0.00220
C44 1 0.423518 -0.174208 0.589644 11.00000 0.05918 0.06157 =
0.02515 0.00217 0.00534 -0.04120
C45 1 0.326564 -0.159409 0.554682 11.00000 0.03511 0.02151 =
0.03796 0.00622 0.01405 0.00171
C46 1 0.315418 -0.206530 0.485603 11.00000 0.02293 0.02441 =
0.03233 0.00571 0.00411 -0.00063
PART 1
C47 1 0.309593 -0.422262 0.432156 21.00000 0.03967 0.03241 =
0.04653 -0.01128 0.02002 -0.00654
AFIX 137
H47A 2 0.312078 -0.436488 0.489946 21.00000 -1.50000
H47B 2 0.316386 -0.472128 0.398954 21.00000 -1.50000
H47C 2 0.244289 -0.398529 0.420074 21.00000 -1.50000
AFIX 0
PART 0
PART 2
C47A 1 0.494347 -0.336802 0.320328 -21.00000 0.03967 0.03241 =
0.04653 -0.01128 0.02002 -0.00654
AFIX 137
H47D 2 0.525181 -0.280638 0.315492 -21.00000 -1.50000
H47E 2 0.474020 -0.357841 0.266283 -21.00000 -1.50000
H47F 2 0.544034 -0.372628 0.344001 -21.00000 -1.50000
AFIX 0
PART 0
PART 1
C48 1 0.415838 -0.323046 0.298882 21.00000 0.07461 0.03221 =
0.03754 -0.00520 0.00399 -0.00220
AFIX 137
H48A 2 0.357051 -0.290947 0.285667 21.00000 -1.50000
H48B 2 0.412038 -0.374730 0.267427 21.00000 -1.50000
H48C 2 0.478966 -0.291031 0.285283 21.00000 -1.50000
AFIX 0
PART 0
PART 2
C48A 1 0.392223 -0.433477 0.444590 -21.00000 0.07461 0.03221 =
0.03754 -0.00520 0.00399 -0.00220
AFIX 137
H48D 2 0.451703 -0.428116 0.480719 -21.00000 -1.50000
H48E 2 0.399949 -0.479566 0.406550 -21.00000 -1.50000
H48F 2 0.330336 -0.443924 0.477091 -21.00000 -1.50000
AFIX 0
PART 0
PART 1
C49 1 0.534840 -0.402834 0.426630 21.00000 0.04044 0.02779 =
0.08079 -0.00291 0.01638 0.00336
AFIX 137
H49A 2 0.594617 -0.366197 0.414257 21.00000 -1.50000
H49B 2 0.534568 -0.451809 0.391273 21.00000 -1.50000
H49C 2 0.537582 -0.419731 0.483677 21.00000 -1.50000
AFIX 0
PART 0
PART 2
C49A 1 0.261327 -0.339380 0.330575 -21.00000 0.05516 0.02172 =
0.09034 -0.01494 -0.00024 -0.01623
AFIX 137
H49D 2 0.205946 -0.327163 0.368006 -21.00000 -1.50000
H49E 2 0.248173 -0.394621 0.306934 -21.00000 -1.50000
H49F 2 0.265038 -0.298443 0.287010 -21.00000 -1.50000
AFIX 0
PART 0
C50 1 0.571587 -0.266876 0.562615 11.00000 0.02296 0.08166 =
0.10289 0.05707 -0.00526 -0.00346
AFIX 137
H50A 2 0.611954 -0.271213 0.512756 11.00000 -1.50000
H50B 2 0.560082 -0.321725 0.586556 11.00000 -1.50000
H50C 2 0.608524 -0.230126 0.601549 11.00000 -1.50000
AFIX 0
C51 1 0.457512 -0.133050 0.668836 11.00000 0.05918 0.06157 =
0.02515 0.00217 0.00534 -0.04120
AFIX 137
H51A 2 0.529393 -0.143030 0.678770 11.00000 -1.50000
H51B 2 0.415834 -0.155955 0.713586 11.00000 -1.50000
H51C 2 0.449330 -0.073502 0.665450 11.00000 -1.50000
AFIX 0
C52 1 0.246059 -0.106667 0.590288 11.00000 0.07151 0.03582 =
0.05967 -0.00325 0.03834 -0.00108
AFIX 137
H52A 2 0.278721 -0.055768 0.613053 11.00000 -1.50000
H52B 2 0.209234 -0.137166 0.633421 11.00000 -1.50000
H52C 2 0.198020 -0.092865 0.547479 11.00000 -1.50000
AFIX 0
C53 1 0.223155 -0.213455 0.432047 11.00000 0.02413 0.07171 =
0.05012 0.02076 0.00331 -0.00538
AFIX 137
H53A 2 0.194225 -0.159275 0.427636 11.00000 -1.50000
H53B 2 0.172284 -0.252842 0.455568 11.00000 -1.50000
H53C 2 0.242480 -0.232786 0.377831 11.00000 -1.50000
AFIX 0
C54 1 0.388114 0.029335 0.481431 11.00000 0.03239 0.02346 =
0.03070 0.00142 -0.00073 -0.00780
C55 1 0.307489 0.063728 0.474631 11.00000 0.03125 0.02685 =
0.03980 -0.00178 -0.00189 0.00313
C56 1 0.211317 0.101365 0.463094 11.00000 0.03463 0.03139 =
0.06533 -0.00440 -0.01381 0.00934
C57 1 0.134401 0.090728 0.519973 11.00000 0.03350 0.07266 =
0.09379 0.01786 0.00451 0.01625
AFIX 43
H57 2 0.144526 0.058232 0.566811 11.00000 -1.20000
AFIX 0
C58 1 0.042776 0.127154 0.509040 11.00000 0.02591 0.08325 =
0.14894 0.02270 0.01050 0.02180
AFIX 43
H58 2 -0.010249 0.120034 0.548104 11.00000 -1.20000
AFIX 0
C59 1 0.029244 0.174528 0.439837 11.00000 0.03859 0.06493 =
0.12867 0.00700 -0.01440 0.02608
AFIX 43
H59 2 -0.033358 0.200098 0.432063 11.00000 -1.20000
AFIX 0
C60 1 0.105181 0.184690 0.382821 11.00000 0.05741 0.03761 =
0.09548 0.00121 -0.03461 0.01274
AFIX 43
H60 2 0.095341 0.216996 0.335805 11.00000 -1.20000
AFIX 0
C61 1 0.194694 0.147999 0.394361 11.00000 0.04971 0.03595 =
0.05941 -0.00568 -0.01841 0.00361
AFIX 43
H61 2 0.246937 0.154417 0.354554 11.00000 -1.20000
AFIX 0
C62 1 0.318654 -0.096772 0.263663 11.00000 0.03280 0.02560 =
0.02666 0.00480 -0.00569 -0.00673
C63 1 0.249388 -0.040156 0.289546 11.00000 0.03684 0.03287 =
0.03193 -0.00049 -0.00360 -0.00312
AFIX 43
H63 2 0.264216 -0.006620 0.336214 11.00000 -1.20000
AFIX 0
C64 1 0.158871 -0.032526 0.247492 11.00000 0.03637 0.04860 =
0.03807 0.00601 -0.00429 0.00085
AFIX 43
H64 2 0.112393 0.006394 0.265922 11.00000 -1.20000
AFIX 0
C65 1 0.135041 -0.079548 0.180355 11.00000 0.03275 0.06226 =
0.03681 0.01371 -0.00328 -0.01214
AFIX 43
H65 2 0.073159 -0.072796 0.151784 11.00000 -1.20000
AFIX 0
C66 1 0.201862 -0.137305 0.154120 11.00000 0.05334 0.04872 =
0.02860 0.00560 -0.01057 -0.02589
AFIX 43
H66 2 0.185505 -0.170566 0.107544 11.00000 -1.20000
AFIX 0
C67 1 0.292922 -0.146880 0.195666 11.00000 0.04796 0.02352 =
0.03153 0.00145 0.00344 -0.00711
AFIX 43
H67 2 0.337759 -0.187384 0.177999 11.00000 -1.20000
AFIX 0
C68 1 0.499339 -0.116353 0.279291 11.00000 0.05091 0.01932 =
0.02253 0.00221 0.00774 -0.00059
C69 1 0.520287 -0.114696 0.192457 11.00000 0.03815 0.02315 =
0.03150 0.00059 0.00114 0.00915
C70 1 0.541255 -0.111822 0.122746 11.00000 0.02679 0.02605 =
0.03197 -0.00015 0.00057 0.00270
C71 1 0.565827 -0.105997 0.038171 11.00000 0.04365 0.02165 =
0.02466 0.00114 0.00175 -0.00563
C72 1 0.492232 -0.103493 -0.021194 11.00000 0.04230 0.03628 =
0.03439 0.00154 -0.00415 -0.00674
AFIX 43
H72 2 0.422573 -0.112552 -0.006407 11.00000 -1.20000
AFIX 0
C73 1 0.516017 -0.088474 -0.100311 11.00000 0.04824 0.03827 =
0.03132 -0.00409 -0.00633 0.01051
AFIX 43
H73 2 0.463584 -0.084901 -0.139799 11.00000 -1.20000
AFIX 0
C74 1 0.616911 -0.078494 -0.122611 11.00000 0.08418 0.02551 =
0.02797 0.00055 0.02017 0.00007
AFIX 43
H74 2 0.633874 -0.067622 -0.177835 11.00000 -1.20000
AFIX 0
C75 1 0.694630 -0.084087 -0.065434 11.00000 0.03415 0.04763 =
0.05062 -0.00493 0.01760 -0.00983
AFIX 43
H75 2 0.764244 -0.077873 -0.081184 11.00000 -1.20000
AFIX 0
C76 1 0.668345 -0.098726 0.013861 11.00000 0.04114 0.04031 =
0.03759 0.00269 0.00078 -0.00956
AFIX 43
H76 2 0.720516 -0.104078 0.053256 11.00000 -1.20000
AFIX 0
C77 1 0.674286 -0.135989 0.309751 11.00000 0.04055 0.02750 =
0.02563 0.00045 0.00660 0.00073
C78 1 0.728283 -0.075727 0.265517 11.00000 0.04530 0.02373 =
0.03278 0.00060 0.00815 0.00270
AFIX 43
H78 2 0.695577 -0.028117 0.248205 11.00000 -1.20000
AFIX 0
C79 1 0.830526 -0.084902 0.246405 11.00000 0.04987 0.03421 =
0.04015 0.00668 0.02099 -0.00115
AFIX 43
H79 2 0.866805 -0.043567 0.215633 11.00000 -1.20000
AFIX 0
C80 1 0.878757 -0.151861 0.271086 11.00000 0.05836 0.04204 =
0.06320 0.00747 0.02784 0.01132
AFIX 43
H80 2 0.948297 -0.157645 0.257327 11.00000 -1.20000
AFIX 0
C81 1 0.826855 -0.211409 0.316078 11.00000 0.05915 0.03510 =
0.08746 0.01814 0.03322 0.01843
AFIX 43
H81 2 0.860395 -0.258442 0.333845 11.00000 -1.20000
AFIX 0
C82 1 0.724878 -0.202570 0.335548 11.00000 0.05549 0.03160 =
0.05969 0.01492 0.02501 0.01006
AFIX 43
H82 2 0.689615 -0.243575 0.367399 11.00000 -1.20000
AFIX 0
HKLF 4
REM 13mar11g in P-1 #2
REM R1 = 0.0848 for 11383 Fo > 4sig(Fo) and 0.0989 for all 13686 data
REM 863 parameters refined using 12 restraints
END
WGHT 0.0135 29.1533
REM Highest difference peak 0.938, deepest hole -1.043, 1-sigma level 0.115
Q1 1 0.9759 0.3809 0.1062 11.00000 0.05 0.94
Q2 1 0.9996 0.3985 -0.1511 11.00000 0.05 0.91
Q3 1 0.5162 -0.0991 0.4831 11.00000 0.05 0.89
Q4 1 0.4738 -0.0787 0.3980 11.00000 0.05 0.80
Q5 1 0.4430 -0.1624 0.6036 11.00000 0.05 0.72
;
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelxl_version_number 2013-3
_database_code_depnum_ccdc_archive 'CCDC 949451'
#######################################################################
#
# Cambridge Crystallographic Data Centre
# CCDC
#
#######################################################################
#
# This CIF contains data from an original supplementary publication
# deposited with the CCDC, and may include chemical, crystal,
# experimental, refinement, atomic coordinates,
# anisotropic displacement parameters and molecular geometry data,
# as required by the journal to which it was submitted.
#
# This CIF is provided on the understanding that it is used for bona
# fide research purposes only. It may contain copyright material
# of the CCDC or of third parties, and may not be copied or further
# disseminated in any form, whether machine-readable or not,
# except for the purpose of generating routine backup copies
# on your local computer system.
#
# For further information on the CCDC, data deposition and
# data retrieval see:
# www.ccdc.cam.ac.uk
#
# Bona fide researchers may freely download Mercury and enCIFer
# from this site to visualise CIF-encoded structures and
# to carry out CIF format checking respectively.
#
data_a
_audit_creation_date 2013-09-14
_audit_creation_method
;
Olex2 1.2
(compiled Apr 23 2013 17:54:37, GUI svn.r4466)
;
_chemical_name_common ?
_chemical_name_systematic
;
?
;
_chemical_formula_moiety 'C45 H57 N6 Y1'
_chemical_formula_sum 'C45 H57 N6 Y'
_chemical_formula_weight 770.87
_chemical_absolute_configuration ?
_chemical_melting_point ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Y Y -2.7962 3.5667 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_space_group_crystal_system hexagonal
_space_group_IT_number 173
_space_group_name_H-M_alt 'P 63'
_space_group_name_Hall 'P 6c'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'-x, -y, z+1/2'
'y, -x+y, z+1/2'
'x-y, x, z+1/2'
_cell_length_a 16.124(2)
_cell_length_b 16.124(2)
_cell_length_c 9.945(2)
_cell_angle_alpha 90
_cell_angle_beta 90
_cell_angle_gamma 120
_cell_volume 2239.1(8)
_cell_formula_units_Z 2
_cell_measurement_reflns_used ?
_cell_measurement_temperature 173(2)
_cell_measurement_theta_max ?
_cell_measurement_theta_min ?
_exptl_absorpt_coefficient_mu 1.337
_exptl_absorpt_correction_T_max ?
_exptl_absorpt_correction_T_min ?
_exptl_absorpt_correction_type ?
_exptl_absorpt_process_details ?
_exptl_crystal_colour ?
_exptl_crystal_density_diffrn 1.143
_exptl_crystal_density_meas ?
_exptl_crystal_density_method ?
_exptl_crystal_description ?
_exptl_crystal_F_000 816
_exptl_crystal_size_max 0.21
_exptl_crystal_size_mid 0.2
_exptl_crystal_size_min 0.17
_exptl_special_details
;
?
;
_exptl_transmission_factor_max ?
_exptl_transmission_factor_min ?
_diffrn_reflns_av_R_equivalents 0.0760
_diffrn_reflns_av_unetI/netI 0.0490
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.999
_diffrn_reflns_limit_h_max 19
_diffrn_reflns_limit_h_min -19
_diffrn_reflns_limit_k_max 19
_diffrn_reflns_limit_k_min -19
_diffrn_reflns_limit_l_max 12
_diffrn_reflns_limit_l_min -12
_diffrn_reflns_number 14012
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.999
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 26.022
_diffrn_reflns_theta_min 2.526
_diffrn_ambient_temperature 173(2)
_diffrn_detector_area_resol_mean ?
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type ?
_diffrn_measurement_method ?
_diffrn_radiation_type MoK\a
_diffrn_radiation_wavelength 0.71073
_diffrn_source ?
_reflns_Friedel_coverage 0.887
_reflns_Friedel_fraction_full 0.999
_reflns_Friedel_fraction_max 0.999
_reflns_number_gt 2764
_reflns_number_total 2910
_reflns_special_details
;
Reflections were merged by SHELXL according to the crystal
class for the calculation of statistics and refinement.
_reflns_Friedel_fraction is defined as the number of unique
Friedel pairs measured divided by the number that would be
possible theoretically, ignoring centric projections and
systematic absences.
;
_reflns_threshold_expression 'I > 2\s(I)'
_computing_cell_refinement ?
_computing_data_collection ?
_computing_data_reduction ?
_computing_molecular_graphics
;
O. V. Dolomanov, L. J. Bourhis, R. J. Gildea, J. A. K. Howard and H. Puschmann,
OLEX2: a complete structure solution, refinement and analysis program.
J. Appl. Cryst. (2009). 42, 339-341.
;
_computing_publication_material
;
O. V. Dolomanov, L. J. Bourhis, R. J. Gildea, J. A. K. Howard and H. Puschmann,
OLEX2: a complete structure solution, refinement and analysis program.
J. Appl. Cryst. (2009). 42, 339-341.
;
_computing_structure_refinement
;
SHELXL, G.M. Sheldrick, Acta Cryst.
(2008). A64, 112-122
;
_computing_structure_solution 'SUPERFLIP, J. Appl. Cryst. (2007) 40, 786-790'
_refine_diff_density_max 0.390
_refine_diff_density_min -0.223
_refine_diff_density_rms 0.052
_refine_ls_abs_structure_details
;
Refined as an inversion twin.
;
_refine_ls_abs_structure_Flack 0.113(16)
_refine_ls_extinction_coef .
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 1.130
_refine_ls_hydrogen_treatment constr
_refine_ls_matrix_type full
_refine_ls_number_parameters 162
_refine_ls_number_reflns 2910
_refine_ls_number_restraints 1
_refine_ls_R_factor_all 0.0575
_refine_ls_R_factor_gt 0.0536
_refine_ls_restrained_S_all 1.129
_refine_ls_shift/su_max 0.000
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0387P)^2^+1.5495P] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.1123
_refine_ls_wR_factor_ref 0.1142
_refine_special_details
;
Refined as a 2-component inversion twin.
;
_olex2_refinement_description
;
1. Others
Fixed U13: Y1(0)
Fixed U23: Y1(0)
Fixed Uiso: H1(0.056) H2A(0.139) H2B(0.139) H2C(0.139) H3A(0.1) H3B(0.1)
H3C(0.1) H4(0.059) H5A(0.154) H5B(0.154) H5C(0.154) H6A(0.143) H6B(0.143)
H6C(0.143) H11(0.097) H12(0.127) H13(0.124) H14(0.104) H15(0.077)
Fixed X: Y1(0.3333) H1(0.2129) H2A(0.3306) H2B(0.228) H2C(0.2801) H3A(0.1337)
H3B(0.0862) H3C(0.0948) H4(0.3836) H5A(0.3284) H5B(0.4312) H5C(0.4218)
H6A(0.5482) H6B(0.5219) H6C(0.5408) H11(0.1802) H12(0.1489) H13(0.2093)
H14(0.3051) H15(0.3348)
Fixed Y: Y1(0.6667) H1(0.3879) H2A(0.4921) H2B(0.449) H2C(0.5557) H3A(0.5099)
H3B(0.4045) H3C(0.4187) H4(0.4567) H5A(0.5304) H5B(0.5493) H5C(0.6321)
H6A(0.5605) H6B(0.5499) H6C(0.6439) H11(0.1682) H12(0.0093) H13(-0.043)
H14(0.0628) H15(0.2198)
Fixed Z: H1(0.8353) H2A(0.9846) H2B(1.0551) H2C(0.9964) H3A(0.8569)
H3B(0.9196) H3C(0.76) H4(0.4322) H5A(0.2832) H5B(0.2353) H5C(0.3103)
H6A(0.4022) H6B(0.5588) H6C(0.4787) H11(0.4695) H12(0.4732) H13(0.6419)
H14(0.8073) H15(0.8112)
;
_atom_sites_solution_hydrogens geom
_atom_sites_solution_primary iterative
_atom_sites_solution_secondary ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Y1 Y 0.3333 0.6667 0.63858(12) 0.0323(2) Uani 1 3 d S T P . .
N1 N 0.2825(4) 0.5171(3) 0.7430(5) 0.0424(11) Uani 1 1 d . . . . .
N2 N 0.3593(4) 0.5479(3) 0.5427(5) 0.0418(11) Uani 1 1 d . . . . .
C1 C 0.2213(4) 0.4531(4) 0.8498(6) 0.0464(15) Uani 1 1 d . . . . .
H1 H 0.2129 0.3879 0.8353 0.056 Uiso 1 1 calc R U . . .
C2 C 0.2691(6) 0.4907(7) 0.9830(8) 0.093(3) Uani 1 1 d . . . . .
H2A H 0.3306 0.4921 0.9846 0.139 Uiso 1 1 calc R U . . .
H2B H 0.2280 0.4490 1.0551 0.139 Uiso 1 1 calc R U . . .
H2C H 0.2801 0.5557 0.9964 0.139 Uiso 1 1 calc R U . . .
C3 C 0.1259(5) 0.4460(5) 0.8463(8) 0.067(2) Uani 1 1 d . . . . .
H3A H 0.1337 0.5099 0.8569 0.100 Uiso 1 1 calc R U . . .
H3B H 0.0862 0.4045 0.9196 0.100 Uiso 1 1 calc R U . . .
H3C H 0.0948 0.4187 0.7600 0.100 Uiso 1 1 calc R U . . .
C4 C 0.4103(5) 0.5275(5) 0.4377(6) 0.0493(15) Uani 1 1 d . . . . .
H4 H 0.3836 0.4567 0.4322 0.059 Uiso 1 1 calc R U . . .
C5 C 0.3967(7) 0.5628(8) 0.3052(8) 0.102(4) Uani 1 1 d . . . . .
H5A H 0.3284 0.5304 0.2832 0.154 Uiso 1 1 calc R U . . .
H5B H 0.4312 0.5493 0.2353 0.154 Uiso 1 1 calc R U . . .
H5C H 0.4218 0.6321 0.3103 0.154 Uiso 1 1 calc R U . . .
C6 C 0.5142(6) 0.5745(8) 0.4723(9) 0.096(3) Uani 1 1 d . . . . .
H6A H 0.5482 0.5605 0.4022 0.143 Uiso 1 1 calc R U . . .
H6B H 0.5219 0.5499 0.5588 0.143 Uiso 1 1 calc R U . . .
H6C H 0.5408 0.6439 0.4787 0.143 Uiso 1 1 calc R U . . .
C7 C 0.3129(3) 0.4858(3) 0.6431(10) 0.0386(10) Uani 1 1 d . . . . .
C8 C 0.2955(3) 0.3877(3) 0.6381(10) 0.0430(11) Uani 1 1 d . . . . .
C9 C 0.2776(3) 0.3064(3) 0.6412(11) 0.0459(11) Uani 1 1 d . . . . .
C10 C 0.2576(4) 0.2086(3) 0.6433(11) 0.0500(13) Uani 1 1 d . . . . .
C11 C 0.2044(6) 0.1469(5) 0.5404(10) 0.081(2) Uani 1 1 d . . . . .
H11 H 0.1802 0.1682 0.4695 0.097 Uiso 1 1 calc R U . . .
C12 C 0.1867(8) 0.0523(6) 0.5423(13) 0.106(3) Uani 1 1 d . . . . .
H12 H 0.1489 0.0093 0.4732 0.127 Uiso 1 1 calc R U . . .
C13 C 0.2226(6) 0.0214(5) 0.6411(19) 0.103(3) Uani 1 1 d . . . . .
H13 H 0.2093 -0.0430 0.6419 0.124 Uiso 1 1 calc R U . . .
C14 C 0.2783(6) 0.0839(6) 0.7396(11) 0.087(3) Uani 1 1 d . . . . .
H14 H 0.3051 0.0628 0.8073 0.104 Uiso 1 1 calc R U . . .
C15 C 0.2962(5) 0.1774(5) 0.7420(8) 0.0641(19) Uani 1 1 d . . . . .
H15 H 0.3348 0.2198 0.8112 0.077 Uiso 1 1 calc R U . . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Y1 0.0305(3) 0.0305(3) 0.0358(4) 0.000 0.000 0.01524(13)
N1 0.054(3) 0.035(2) 0.041(3) 0.008(2) 0.018(2) 0.025(2)
N2 0.051(3) 0.038(2) 0.041(3) 0.004(2) 0.015(2) 0.025(2)
C1 0.050(3) 0.039(3) 0.051(4) 0.013(3) 0.019(3) 0.023(3)
C2 0.061(5) 0.130(8) 0.052(5) 0.035(5) 0.012(4) 0.022(5)
C3 0.042(3) 0.064(4) 0.078(6) 0.029(4) 0.018(4) 0.014(3)
C4 0.058(4) 0.050(3) 0.048(4) 0.001(3) 0.019(3) 0.033(3)
C5 0.153(9) 0.167(10) 0.042(5) -0.006(5) 0.013(5) 0.121(9)
C6 0.066(5) 0.159(10) 0.069(6) -0.010(6) 0.022(4) 0.061(6)
C7 0.037(2) 0.035(2) 0.045(3) 0.007(4) 0.007(4) 0.0195(19)
C8 0.043(2) 0.043(3) 0.046(3) 0.001(5) 0.003(5) 0.024(2)
C9 0.046(3) 0.042(3) 0.053(3) 0.003(5) 0.011(4) 0.024(2)
C10 0.051(3) 0.036(2) 0.062(4) 0.002(5) 0.014(5) 0.021(2)
C11 0.093(6) 0.051(4) 0.097(6) 0.006(4) -0.004(5) 0.034(4)
C12 0.120(8) 0.042(4) 0.139(9) -0.013(5) -0.018(7) 0.028(5)
C13 0.114(6) 0.043(4) 0.152(8) 0.008(9) -0.016(12) 0.040(4)
C14 0.090(6) 0.054(5) 0.123(8) 0.036(5) 0.018(6) 0.041(5)
C15 0.069(4) 0.052(4) 0.072(5) 0.018(4) 0.009(4) 0.031(4)
_geom_special_details
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Y1 N1 2.363(4) 3_565 ?
Y1 N1 2.363(4) . ?
Y1 N1 2.364(4) 2_665 ?
Y1 N2 2.356(4) 3_565 ?
Y1 N2 2.356(4) 2_665 ?
Y1 N2 2.356(4) . ?
Y1 C7 2.766(4) . ?
Y1 C7 2.766(4) 2_665 ?
Y1 C7 2.766(4) 3_565 ?
N1 C1 1.467(7) . ?
N1 C7 1.316(9) . ?
N2 C4 1.465(7) . ?
N2 C7 1.345(9) . ?
C1 H1 1.0000 . ?
C1 C2 1.500(10) . ?
C1 C3 1.484(9) . ?
C2 H2A 0.9800 . ?
C2 H2B 0.9800 . ?
C2 H2C 0.9800 . ?
C3 H3A 0.9800 . ?
C3 H3B 0.9800 . ?
C3 H3C 0.9800 . ?
C4 H4 1.0000 . ?
C4 C5 1.495(11) . ?
C4 C6 1.493(10) . ?
C5 H5A 0.9800 . ?
C5 H5B 0.9800 . ?
C5 H5C 0.9800 . ?
C6 H6A 0.9800 . ?
C6 H6B 0.9800 . ?
C6 H6C 0.9800 . ?
C7 C8 1.463(6) . ?
C8 C9 1.194(6) . ?
C9 C10 1.443(6) . ?
C10 C11 1.385(13) . ?
C10 C15 1.386(11) . ?
C11 H11 0.9500 . ?
C11 C12 1.404(11) . ?
C12 H12 0.9500 . ?
C12 C13 1.356(17) . ?
C13 H13 0.9500 . ?
C13 C14 1.370(17) . ?
C14 H14 0.9500 . ?
C14 C15 1.386(10) . ?
C15 H15 0.9500 . ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 Y1 N1 102.15(15) 3_565 . ?
N1 Y1 N1 102.15(15) . 2_665 ?
N1 Y1 N1 102.15(15) 3_565 2_665 ?
N1 Y1 C7 104.25(18) . 3_565 ?
N1 Y1 C7 127.78(18) 2_665 3_565 ?
N1 Y1 C7 127.78(18) 3_565 . ?
N1 Y1 C7 28.4(2) 3_565 3_565 ?
N1 Y1 C7 28.4(2) . . ?
N1 Y1 C7 104.25(18) 3_565 2_665 ?
N1 Y1 C7 104.25(18) 2_665 . ?
N1 Y1 C7 28.4(2) 2_665 2_665 ?
N1 Y1 C7 127.78(18) . 2_665 ?
N2 Y1 N1 57.38(16) . . ?
N2 Y1 N1 57.38(16) 3_565 3_565 ?
N2 Y1 N1 100.90(17) 3_565 . ?
N2 Y1 N1 152.07(15) 2_665 . ?
N2 Y1 N1 100.90(17) 2_665 3_565 ?
N2 Y1 N1 57.38(16) 2_665 2_665 ?
N2 Y1 N1 100.90(17) . 2_665 ?
N2 Y1 N1 152.07(16) . 3_565 ?
N2 Y1 N1 152.07(15) 3_565 2_665 ?
N2 Y1 N2 104.72(14) 3_565 2_665 ?
N2 Y1 N2 104.72(15) 3_565 . ?
N2 Y1 N2 104.72(14) 2_665 . ?
N2 Y1 C7 29.1(2) . . ?
N2 Y1 C7 131.27(18) 2_665 . ?
N2 Y1 C7 103.53(17) 2_665 3_565 ?
N2 Y1 C7 131.27(18) . 3_565 ?
N2 Y1 C7 29.1(2) 3_565 3_565 ?
N2 Y1 C7 29.1(2) 2_665 2_665 ?
N2 Y1 C7 103.53(17) . 2_665 ?
N2 Y1 C7 103.53(17) 3_565 . ?
N2 Y1 C7 131.27(18) 3_565 2_665 ?
C7 Y1 C7 119.974(14) 2_665 . ?
C7 Y1 C7 119.975(16) 3_565 . ?
C7 Y1 C7 119.974(14) 3_565 2_665 ?
C1 N1 Y1 143.6(4) . . ?
C7 N1 Y1 93.1(4) . . ?
C7 N1 C1 121.7(4) . . ?
C4 N2 Y1 145.0(4) . . ?
C7 N2 Y1 92.6(3) . . ?
C7 N2 C4 121.8(5) . . ?
N1 C1 H1 108.9 . . ?
N1 C1 C2 109.0(5) . . ?
N1 C1 C3 110.1(5) . . ?
C2 C1 H1 108.9 . . ?
C3 C1 H1 108.9 . . ?
C3 C1 C2 110.9(6) . . ?
C1 C2 H2A 109.5 . . ?
C1 C2 H2B 109.5 . . ?
C1 C2 H2C 109.5 . . ?
H2A C2 H2B 109.5 . . ?
H2A C2 H2C 109.5 . . ?
H2B C2 H2C 109.5 . . ?
C1 C3 H3A 109.5 . . ?
C1 C3 H3B 109.5 . . ?
C1 C3 H3C 109.5 . . ?
H3A C3 H3B 109.5 . . ?
H3A C3 H3C 109.5 . . ?
H3B C3 H3C 109.5 . . ?
N2 C4 H4 109.0 . . ?
N2 C4 C5 109.6(5) . . ?
N2 C4 C6 109.6(6) . . ?
C5 C4 H4 109.0 . . ?
C6 C4 H4 109.0 . . ?
C6 C4 C5 110.5(7) . . ?
C4 C5 H5A 109.5 . . ?
C4 C5 H5B 109.5 . . ?
C4 C5 H5C 109.5 . . ?
H5A C5 H5B 109.5 . . ?
H5A C5 H5C 109.5 . . ?
H5B C5 H5C 109.5 . . ?
C4 C6 H6A 109.5 . . ?
C4 C6 H6B 109.5 . . ?
C4 C6 H6C 109.5 . . ?
H6A C6 H6B 109.5 . . ?
H6A C6 H6C 109.5 . . ?
H6B C6 H6C 109.5 . . ?
N1 C7 Y1 58.6(2) . . ?
N1 C7 N2 116.7(4) . . ?
N1 C7 C8 122.2(7) . . ?
N2 C7 Y1 58.3(2) . . ?
N2 C7 C8 121.0(7) . . ?
C8 C7 Y1 175.3(5) . . ?
C9 C8 C7 175.8(9) . . ?
C8 C9 C10 178.9(8) . . ?
C11 C10 C9 119.6(8) . . ?
C15 C10 C9 120.8(8) . . ?
C15 C10 C11 119.4(6) . . ?
C10 C11 H11 120.4 . . ?
C10 C11 C12 119.2(9) . . ?
C12 C11 H11 120.4 . . ?
C11 C12 H12 119.5 . . ?
C13 C12 C11 121.1(10) . . ?
C13 C12 H12 119.5 . . ?
C12 C13 H13 120.3 . . ?
C12 C13 C14 119.5(7) . . ?
C14 C13 H13 120.3 . . ?
C13 C14 H14 119.5 . . ?
C13 C14 C15 121.1(9) . . ?
C15 C14 H14 119.5 . . ?
C10 C15 H15 120.1 . . ?
C14 C15 C10 119.7(8) . . ?
C14 C15 H15 120.1 . . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Y1 N1 C1 C2 -76.3(9) . . . . ?
Y1 N1 C1 C3 45.5(10) . . . . ?
Y1 N1 C7 N2 3.8(6) . . . . ?
Y1 N1 C7 C8 -174.6(5) . . . . ?
Y1 N2 C4 C5 -49.9(10) . . . . ?
Y1 N2 C4 C6 71.6(9) . . . . ?
Y1 N2 C7 N1 -3.8(6) . . . . ?
Y1 N2 C7 C8 174.6(5) . . . . ?
C1 N1 C7 Y1 168.8(7) . . . . ?
C1 N1 C7 N2 172.5(5) . . . . ?
C1 N1 C7 C8 -5.8(10) . . . . ?
C4 N2 C7 Y1 173.4(6) . . . . ?
C4 N2 C7 N1 169.6(5) . . . . ?
C4 N2 C7 C8 -12.0(9) . . . . ?
C7 N1 C1 C2 122.8(7) . . . . ?
C7 N1 C1 C3 -115.4(7) . . . . ?
C7 N2 C4 C5 141.7(8) . . . . ?
C7 N2 C4 C6 -96.8(8) . . . . ?
C9 C10 C11 C12 178.9(8) . . . . ?
C9 C10 C15 C14 -178.0(7) . . . . ?
C10 C11 C12 C13 -1.6(17) . . . . ?
C11 C10 C15 C14 -2.4(12) . . . . ?
C11 C12 C13 C14 -1(2) . . . . ?
C12 C13 C14 C15 1.9(18) . . . . ?
C13 C14 C15 C10 -0.2(14) . . . . ?
C15 C10 C11 C12 3.2(13) . . . . ?
_shelx_estimated_absorpt_T_max 0.805
_shelx_estimated_absorpt_T_min 0.767
_shelx_hkl_checksum 94090
_shelx_hkl_file
;
0 0 -1 3.55 1.15
0 0 1 4.25 1.07
0 0 -2 4620.55 178.04
0 0 -3 3.07 2.23
0 0 3 0.75 2.12
0 0 -4 291.37 9.38
0 0 4 247.21 11.20
0 0 -5 5.83 2.73
0 0 5 2.75 1.87
0 0 -6 1371.92 61.61
0 0 6 1212.03 53.79
0 0 -7 5.82 5.49
0 0 -8 585.98 45.32
0 0 -9 125.50 10.06
0 0 -10 617.03 36.57
0 0 -11 23.71 8.11
0 0 -12 121.74 21.79
-1 1 0 0.14 0.13
0 1 0 -0.54 0.50
1 0 0 -0.89 0.45
-1 1 0 -0.05 0.14
-1 0 0 -1.05 0.35
-1 1 -1 1.38 0.54
-1 0 -2 291.99 7.81
0 -1 -2 268.71 7.41
0 1 -2 287.12 8.24
-1 1 -2 308.28 8.25
0 -1 2 313.56 8.78
1 0 -2 284.13 8.12
-1 0 2 320.17 8.85
1 -1 2 343.23 8.89
1 -1 -2 337.30 8.98
-1 1 2 351.03 9.58
-1 0 -2 295.71 7.55
0 -1 -2 328.11 8.73
-1 0 -2 307.90 8.30
0 1 2 311.10 7.81
1 0 2 337.03 8.64
-1 0 -3 1141.80 28.33
0 -1 -3 1182.83 31.62
0 1 -3 1167.29 29.37
-1 1 -3 1227.64 30.45
1 0 -3 1173.67 29.51
0 -1 3 1070.29 26.66
1 -1 -3 1118.79 27.92
-1 0 3 1080.78 26.84
-1 0 -3 1153.77 28.14
0 -1 -3 1105.77 27.17
-1 1 3 1061.78 26.27
0 1 3 1088.23 26.41
1 0 3 1007.30 24.81
-1 0 -4 67.48 9.51
0 -1 -4 61.48 4.14
0 1 -4 52.70 4.07
-1 1 -4 58.19 3.98
1 0 -4 62.27 4.34
1 -1 -4 49.46 3.04
-1 0 -4 65.23 3.92
0 -1 4 56.21 3.17
0 -1 -4 59.55 3.96
1 -1 4 67.34 3.27
0 1 4 63.52 2.61
1 0 4 66.05 3.32
-1 0 -5 476.67 20.60
0 -1 -5 475.84 24.72
0 1 -5 527.34 22.58
-1 1 -5 541.61 22.95
-1 0 -5 503.36 21.21
0 -1 -5 522.13 22.16
0 -1 5 467.78 19.26
-1 0 5 472.69 19.74
1 -1 5 455.65 18.57
-1 1 5 477.27 19.69
0 1 5 452.98 19.18
1 0 5 477.80 19.36
-1 0 -6 128.63 19.72
0 1 -6 177.52 10.39
-1 1 -6 156.14 9.04
1 0 -6 187.18 11.44
-1 0 -6 147.35 9.16
1 -1 -6 185.32 11.14
0 -1 -6 155.17 9.42
0 -1 6 145.01 8.02
1 -1 6 146.71 7.69
0 1 -7 81.65 9.88
-1 1 -7 82.10 10.28
1 0 -7 45.92 7.39
1 -1 -7 52.84 8.46
-1 0 -7 55.70 7.34
0 -1 -7 55.61 7.86
-1 1 -8 18.58 5.43
0 1 -8 29.15 6.46
1 -1 -8 23.97 7.27
0 -1 -8 15.16 5.99
-1 1 -9 349.28 18.75
0 1 -9 449.28 23.18
1 0 -9 319.79 18.29
-1 0 -9 417.47 22.31
1 -1 -9 497.07 25.73
0 -1 -9 378.38 19.89
-1 1 -10 33.39 7.51
0 1 -10 68.51 10.56
-1 0 -10 15.56 6.48
1 -1 -10 25.97 6.42
0 -1 -10 57.18 10.32
0 1 -11 87.55 14.20
-1 1 -11 77.42 10.22
1 0 -11 89.51 11.94
-1 0 -11 57.56 8.63
1 -1 -11 90.95 12.66
0 -1 -11 72.97 11.53
0 1 -12 17.36 5.84
-1 1 -12 21.53 7.31
1 0 -12 5.98 5.03
-1 0 -12 13.07 6.87
1 -1 -12 3.27 4.45
0 -1 -12 15.95 5.63
-1 2 0 1054.07 25.33
1 -2 0 1016.66 24.42
1 1 0 1084.75 26.33
-1 -1 0 1048.24 25.47
2 -1 0 1008.81 24.22
-2 1 0 946.18 22.70
-2 1 0 956.44 22.85
2 -1 0 951.15 22.69
-1 -1 0 1041.41 24.87
1 1 0 964.10 23.02
-1 2 1 618.12 15.42
1 -2 -1 607.14 15.05
1 1 1 567.29 14.22
-1 -1 -1 566.09 13.97
-1 2 -1 568.27 14.05
1 -2 1 697.19 17.20
1 1 -1 552.20 14.26
-1 -1 1 639.29 16.28
2 -1 -1 611.37 15.41
-2 1 1 616.60 15.42
-2 1 -1 651.37 15.97
2 -1 1 510.12 12.69
-1 -1 -1 624.19 15.12
1 1 1 567.77 13.76
-2 1 1 568.11 13.74
2 -1 -1 574.87 13.92
-1 -1 1 548.57 13.49
-1 2 2 547.13 16.21
-2 1 -2 606.97 14.93
1 -2 -2 545.87 14.40
-1 -1 -2 575.99 14.31
1 -2 2 605.44 15.68
1 1 -2 588.88 16.27
2 -1 -2 559.33 14.72
-2 1 -2 595.22 14.49
-2 1 2 433.47 11.56
-2 1 -2 552.43 13.94
2 -1 2 444.57 11.40
-1 -1 -2 608.37 15.10
1 1 2 535.13 13.30
-2 1 2 445.18 11.12
1 -2 -3 865.14 23.48
-1 -1 -3 839.11 20.96
-1 2 -3 810.81 20.93
1 1 -3 839.14 22.35
-1 -1 3 793.60 20.46
2 -1 -3 878.38 22.63
-2 1 3 857.44 21.60
1 -2 -3 896.77 22.78
-1 -1 -3 988.72 24.48
2 -1 3 977.27 23.66
-1 -1 -3 921.40 22.75
2 -1 3 867.42 21.51
1 1 3 884.93 21.70
1 -2 -4 102.43 6.23
2 -1 -4 93.59 5.74
1 -2 4 41.41 3.50
1 -2 -4 85.93 4.35
-2 1 4 41.04 2.74
2 -1 4 50.08 2.55
2 -1 4 39.68 3.33
1 -2 -5 78.32 10.78
-1 -1 -5 79.08 5.66
-1 2 -5 84.86 5.95
-2 1 -5 104.87 6.60
2 -1 -5 100.58 7.19
1 -2 5 76.17 4.26
-1 -1 5 73.85 4.95
1 -2 -5 81.51 5.25
-1 -1 -5 91.67 5.49
-2 1 5 70.61 4.63
1 1 5 80.97 10.48
-2 1 -6 108.15 7.40
-1 -1 -6 110.66 8.13
-1 2 -6 162.07 10.64
1 1 -6 144.17 10.60
-2 1 -6 132.93 8.45
2 -1 -6 145.30 10.60
1 -2 -6 128.64 8.94
-1 -1 -6 146.17 9.58
1 -2 6 119.87 6.87
-1 2 6 115.54 6.49
-2 1 -7 35.15 6.13
-1 2 -7 71.26 9.33
1 1 -7 54.55 8.12
-2 1 -7 56.21 7.33
2 -1 -7 36.08 6.56
1 -2 -7 54.24 7.24
-1 -1 -7 58.15 7.41
-1 2 -8 139.06 14.07
1 1 -8 142.19 14.35
-2 1 -8 154.85 13.68
2 -1 -8 125.12 13.24
-1 -1 -8 141.11 12.92
1 -2 -8 139.58 13.52
-1 2 -9 78.60 9.00
-2 1 -9 58.12 7.26
2 -1 -9 130.88 12.37
-1 -1 -9 44.92 5.80
1 -2 -9 94.31 10.84
-1 2 -10 57.17 7.44
1 1 -10 59.45 9.18
-2 1 -10 68.09 8.42
2 -1 -10 80.52 10.89
-1 -1 -10 41.35 5.71
1 -2 -10 85.41 11.03
-1 2 -11 4.19 4.02
1 1 -11 5.85 5.96
-2 1 -11 8.86 4.71
2 -1 -11 -3.91 5.44
-1 -1 -11 11.85 7.53
1 -2 -11 2.68 5.38
1 1 -12 35.61 9.61
2 -1 -12 70.11 16.31
-1 -1 -12 28.33 7.81
1 -2 -12 17.50 8.24
-2 2 0 1803.15 43.09
2 -2 0 1462.36 34.93
0 2 0 1640.44 39.32
0 -2 0 1764.14 42.26
2 0 0 1885.85 45.21
-2 0 0 1851.26 44.38
-2 2 0 1862.42 44.18
2 -2 0 1911.91 45.31
2 0 0 1699.50 40.39
2 -2 -1 3058.82 73.25
0 2 1 2980.52 70.84
0 -2 -1 3084.89 73.29
-2 0 -1 2932.28 69.44
0 2 -1 3635.46 86.62
0 -2 1 3284.14 78.39
2 0 -1 3324.47 79.42
-2 0 1 2703.84 64.77
2 -2 -1 2951.38 70.10
-2 2 -1 3080.73 73.06
2 -2 1 3351.68 79.40
-2 0 -1 3063.68 72.63
2 0 1 3101.48 73.47
0 2 1 3119.98 73.59
-2 0 1 2747.11 65.08
2 0 -1 3103.46 73.50
0 2 2 2501.55 59.98
2 0 2 2362.25 56.11
0 -2 -2 2434.71 58.25
-2 0 -2 2495.13 59.18
-2 2 -2 2522.53 59.99
0 2 -2 2860.87 68.75
0 -2 2 2452.91 59.24
2 0 -2 2569.08 62.27
-2 0 2 2615.33 63.19
2 -2 -2 2737.71 65.46
-2 2 2 3141.93 75.02
2 -2 2 2587.45 61.76
0 -2 -2 2561.79 60.68
-2 0 -2 2707.56 64.51
2 0 2 3132.05 74.49
0 2 2 2843.54 67.30
-2 0 2 2797.45 66.55
-2 2 2 2549.02 60.30
0 2 3 582.62 19.33
-2 0 -3 411.22 10.68
0 2 -3 446.17 13.43
0 -2 3 509.54 14.02
2 0 -3 437.58 13.27
-2 0 3 538.45 14.57
2 -2 3 540.67 13.74
2 -2 -3 436.06 12.08
-2 2 3 543.38 14.57
2 -2 3 543.81 14.08
-2 0 -3 466.37 12.30
2 0 3 561.28 14.35
-2 0 -4 158.39 5.39
0 2 -4 213.41 8.37
-2 2 -4 186.07 6.67
2 0 -4 201.55 8.17
0 -2 4 158.05 6.33
2 -2 -4 183.31 6.99
-2 0 4 131.59 5.39
2 -2 4 147.76 4.82
-2 0 -4 180.83 5.90
0 -2 -4 176.86 6.21
-2 2 4 166.00 5.94
2 -2 4 162.46 5.58
0 2 4 151.16 4.61
2 0 4 154.25 5.28
0 -2 -5 16.10 3.24
-2 0 -5 14.45 2.20
0 2 -5 19.85 4.80
-2 2 -5 28.14 3.48
2 0 -5 13.68 3.07
0 -2 5 13.70 2.99
2 -2 -5 16.94 3.19
-2 0 -5 24.75 3.40
-2 0 5 11.81 2.69
0 -2 -5 12.54 1.93
2 -2 5 15.64 2.07
0 2 5 11.97 2.47
2 0 5 12.28 1.79
-2 0 -6 33.87 5.68
0 2 -6 54.69 5.92
-2 2 -6 46.62 4.43
2 0 -6 49.27 5.96
-2 0 -6 60.00 5.27
2 -2 -6 49.05 5.36
0 -2 -6 39.74 4.27
2 -2 6 53.12 3.84
0 2 6 54.54 4.80
-2 0 -7 102.09 14.96
0 2 -7 154.97 16.01
-2 2 -7 161.26 16.00
2 0 -7 159.08 17.19
-2 0 -7 165.67 15.48
2 -2 -7 159.43 16.29
0 -2 -7 148.45 14.88
2 -2 7 102.84 9.66
0 2 -8 180.68 16.03
-2 2 -8 196.21 16.74
2 0 -8 170.67 16.92
-2 0 -8 158.73 13.06
2 -2 -8 196.81 17.22
0 -2 -8 190.32 15.84
0 2 -9 132.54 11.19
-2 2 -9 115.48 10.40
2 0 -9 210.41 14.74
-2 0 -9 133.18 10.09
2 -2 -9 115.95 12.42
0 -2 -9 152.66 11.63
0 2 -10 71.45 10.57
-2 2 -10 57.17 8.22
2 0 -10 46.17 6.47
-2 0 -10 33.57 4.97
2 -2 -10 79.93 11.29
0 -2 -10 63.88 9.41
0 2 -11 40.01 9.88
-2 2 -11 40.04 7.29
2 0 -11 49.07 10.08
-2 0 -11 49.79 8.35
2 -2 -11 52.06 11.84
0 -2 -11 39.44 8.82
0 2 -12 11.31 7.07
2 0 -12 21.52 11.43
2 -2 -12 14.90 6.51
0 -2 -12 5.95 4.79
-1 3 0 7.55 1.22
1 -3 0 11.03 1.67
2 1 0 5.91 1.64
-2 -1 0 3.86 1.81
3 -2 0 6.98 1.03
-3 2 0 9.89 1.08
-3 2 0 11.67 1.48
3 -2 0 10.31 2.39
-2 -1 0 9.89 1.11
2 1 0 6.77 0.88
1 -3 -1 38.78 4.56
3 -2 -1 39.62 3.08
-3 2 -1 36.47 5.12
2 1 -1 43.37 2.51
-1 3 2 103.11 10.19
1 -3 -2 97.17 4.36
2 1 2 70.75 3.00
-2 -1 -2 104.99 3.52
-1 3 -2 117.80 4.74
1 -3 2 89.03 3.88
2 1 -2 98.01 5.07
-2 -1 2 82.00 4.94
3 -2 -2 110.52 4.48
-3 2 2 79.43 3.84
-3 2 -2 108.35 3.75
3 -2 2 68.38 2.70
-2 -1 -2 116.25 5.58
2 1 2 75.41 2.73
-3 2 2 70.72 2.48
-2 -1 2 76.22 3.17
3 -2 -2 101.51 3.21
-1 3 3 1533.73 40.83
2 1 3 1553.54 38.03
1 -3 -3 1223.66 30.38
-2 -1 -3 1328.90 32.22
-1 3 -3 1252.53 31.54
-3 2 -3 1360.73 32.77
2 1 -3 1396.82 36.09
1 -3 3 1304.09 32.56
-2 -1 3 1313.88 33.14
3 -2 -3 1332.58 33.63
-3 2 3 1313.69 32.41
3 -2 3 1491.32 35.48
3 -2 3 1493.28 36.43
-2 -1 -3 1484.52 36.07
-1 3 3 1437.38 34.36
2 1 3 1451.98 35.16
1 -3 -4 15.52 3.52
-2 -1 -4 21.38 3.64
-1 3 -4 27.60 3.24
2 1 -4 15.97 3.89
-3 2 -4 24.66 2.58
1 -3 4 11.28 2.16
-2 -1 4 17.12 2.23
3 -2 -4 19.62 3.55
-3 2 4 13.30 1.92
1 -3 -4 20.02 2.75
3 -2 4 15.61 1.65
-2 -1 -4 27.02 2.59
-1 3 4 12.96 1.91
3 -2 4 15.90 2.26
2 1 4 18.63 2.55
-2 -1 -5 146.44 6.78
-1 3 -5 173.80 9.64
2 1 -5 162.14 10.05
-3 2 -5 157.66 8.05
1 -3 5 89.69 5.54
3 -2 -5 152.15 9.54
1 -3 -5 148.76 8.34
-2 -1 -5 141.63 7.06
3 -2 5 109.70 5.40
-1 3 5 103.72 4.90
2 1 5 94.00 5.17
-3 2 -6 12.42 2.46
-2 -1 -6 7.97 1.35
-1 3 -6 29.80 5.81
2 1 -6 8.16 4.81
-3 2 -6 14.41 3.49
3 -2 -6 11.00 6.17
1 -3 6 11.21 2.34
-2 -1 -6 15.72 3.32
1 -3 -6 13.73 4.54
-1 3 6 9.13 1.98
-3 2 -7 115.77 17.56
-1 3 -7 172.94 17.15
2 1 -7 138.58 14.98
-3 2 -7 158.02 14.69
3 -2 -7 161.66 16.43
-2 -1 -7 148.19 13.78
1 -3 -7 169.78 16.53
-1 3 -8 8.81 4.77
2 1 -8 5.41 5.58
-3 2 -8 19.56 4.62
3 -2 -8 4.21 5.21
-2 -1 -8 2.28 3.69
-1 3 -9 59.51 9.87
-3 2 -9 51.40 6.61
2 1 -9 47.05 10.65
3 -2 -9 94.23 11.73
-2 -1 -9 52.43 6.93
1 -3 -9 60.74 7.22
-1 3 -10 11.07 5.81
-3 2 -10 2.16 3.52
2 1 -10 4.02 5.61
3 -2 -10 18.09 6.27
-2 -1 -10 -0.24 3.43
1 -3 -10 8.89 4.36
-1 3 -11 17.75 6.29
2 1 -11 24.85 9.70
3 -2 -11 51.60 14.10
-2 -1 -11 32.24 9.32
1 -3 -11 21.27 8.13
2 1 -12 8.66 6.68
3 -2 -12 -4.84 5.17
1 -3 -12 22.55 8.11
-2 3 0 2035.54 48.61
2 -3 0 2185.98 52.34
1 2 0 2080.60 50.07
-1 -2 0 1824.14 44.05
3 -1 0 2193.91 52.54
-3 1 0 1867.80 44.82
2 -3 0 1988.49 47.13
-3 1 0 1819.72 43.33
3 -1 0 1984.52 47.24
-1 -2 0 1820.76 43.31
1 2 0 1862.62 44.31
2 -3 -1 117.16 3.99
-2 3 -1 111.18 3.51
-1 -2 -1 104.25 3.58
1 2 -1 113.64 4.54
-3 1 -1 107.93 3.34
3 -1 -1 131.93 5.05
-3 1 -1 118.31 3.73
-1 -2 -1 126.91 3.60
3 -1 -1 126.08 3.77
2 -3 -2 3140.87 75.42
1 2 2 3179.38 75.75
-1 -2 -2 3166.96 75.59
-2 3 -2 3228.55 76.82
1 2 -2 2973.24 71.83
-1 -2 2 2741.33 66.35
3 -1 -2 3196.60 77.10
-1 -2 -2 3544.43 83.97
3 -1 2 3527.60 83.90
1 2 2 3371.08 79.81
-3 1 2 3300.84 78.31
3 -1 -2 3416.19 81.06
2 -3 -3 537.70 14.89
1 2 3 566.02 15.49
-3 1 -3 572.45 13.99
-1 -2 -3 587.16 16.42
1 2 -3 608.13 17.23
-1 -2 3 524.52 14.65
3 -1 -3 538.87 15.29
-3 1 3 504.96 14.24
-3 1 -3 589.31 14.48
2 -3 -3 572.64 15.45
-3 1 -3 592.26 15.30
3 -1 3 500.53 13.12
-3 1 3 581.12 14.81
1 2 4 244.85 13.46
2 -3 -4 128.38 7.73
-3 1 -4 129.11 6.00
-1 -2 -4 129.30 9.49
-2 3 -4 153.79 7.64
1 2 -4 147.81 8.64
-1 -2 4 158.12 8.24
3 -1 -4 152.16 8.46
2 -3 4 175.28 8.24
-3 1 -4 149.72 6.71
-3 1 4 166.81 8.12
2 -3 -4 146.36 7.82
3 -1 4 172.20 7.63
1 2 4 175.56 8.05
-3 1 -5 310.73 13.43
-1 -2 -5 294.84 12.71
-2 3 -5 347.54 15.85
3 -1 -5 365.17 17.92
-3 1 -5 380.81 16.21
-1 -2 5 298.98 13.75
2 -3 5 302.57 13.60
2 -3 -5 372.92 16.82
-1 -2 -5 357.28 15.52
1 2 5 323.01 13.54
-3 1 -6 183.91 12.33
-2 3 -6 194.88 13.88
1 2 -6 212.64 15.44
3 -1 -6 200.53 14.70
-3 1 -6 223.40 15.07
2 -3 -6 193.38 13.66
2 -3 6 161.24 11.10
-1 -2 -6 195.05 13.32
1 2 6 133.06 8.88
-3 1 -7 222.56 22.82
-2 3 -7 272.54 24.96
1 2 -7 276.83 26.50
-3 1 -7 272.12 24.86
3 -1 -7 304.82 28.53
2 -3 -7 278.98 25.93
-1 -2 -7 268.37 24.29
2 -3 7 223.35 19.67
-2 3 -8 187.27 15.79
1 2 -8 209.17 19.38
3 -1 -8 146.97 15.44
-3 1 -8 188.02 15.04
2 -3 -8 169.03 16.12
-1 -2 -8 172.74 23.03
-2 3 -9 26.58 5.45
1 2 -9 72.34 8.96
-3 1 -9 31.51 5.97
3 -1 -9 37.80 10.61
2 -3 -9 61.07 9.22
-1 -2 -9 42.37 6.67
-2 3 -10 45.78 6.98
1 2 -10 60.49 8.79
-3 1 -10 51.65 6.86
3 -1 -10 40.08 8.96
-1 -2 -10 62.21 8.79
2 -3 -10 40.43 7.29
-2 3 -11 14.37 4.75
1 2 -11 21.64 7.16
-3 1 -11 34.85 8.49
3 -1 -11 6.25 6.12
2 -3 -11 22.51 9.98
-1 -2 -11 25.57 7.24
1 2 -12 36.81 10.24
3 -1 -12 8.60 6.38
-1 -2 -12 20.71 7.25
2 -3 -12 39.31 12.84
-3 3 0 275.57 7.60
3 -3 0 268.04 7.39
0 3 0 276.75 7.85
0 -3 0 305.99 8.65
3 0 0 255.03 7.78
-3 0 0 277.55 8.23
-3 3 0 302.77 7.75
3 -3 0 282.77 7.22
3 0 0 282.31 7.57
0 -3 0 335.53 8.56
3 -3 -1 3896.92 93.37
0 3 1 4915.82 189.53
0 -3 -1 4701.46 181.30
0 3 -1 4894.13 188.91
3 0 1 4266.08 101.14
0 -3 1 5176.54 199.83
-3 0 -1 4255.10 100.97
3 0 -1 4699.19 181.78
-3 0 1 4014.96 96.05
3 -3 -1 4615.64 177.91
-3 3 -1 4419.96 104.82
3 -3 1 4687.50 180.67
-3 0 -1 4854.20 186.99
-3 0 1 4668.78 179.83
3 0 -1 4128.20 97.76
3 -3 -2 2291.05 56.48
0 3 2 2412.10 57.96
0 -3 -2 2469.14 59.37
3 -3 2 2543.14 60.48
-3 0 2 2249.58 55.01
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TITL A in P6(3)
CELL 0.71073 16.1242 16.1242 9.9447 90 90 120
ZERR 2 0.0023 0.0023 0.002 0 0 0
LATT -1
SYMM -Y,+X-Y,+Z
SYMM +Y-X,-X,+Z
SYMM -X,-Y,0.5+Z
SYMM +Y,-X+Y,0.5+Z
SYMM -Y+X,+X,0.5+Z
SFAC C H N Y
UNIT 90 114 12 2
L.S. 8
PLAN 5
SIZE 0.21 0.2 0.17
TEMP -100
BOND
BOND $H
CONF
fmap 2
acta
SHEL 999 0.81
TWIN -1 0 0 0 -1 0 0 0 -1 2
OMIT 0 1 0
OMIT 0 1 -1
REM E:/360\"i?/?/?$: \"i?/?/?' /\"i?/?/?( *\"i?/?/?%71\"i?/?/?' \"i?/?/?& \"i?/?/?'+ /Cp\"i?/?/?& \"i?/?/?$8 \"i?/?/?& %/Dalton%20\"i?/?/?',,\"i?/?/?$8 \"i?/?/?&,!\"i?/?/?&
WGHT 0.038700 1.549500
BASF 0.11344
FVAR 0.50298
Y1 4 0.333333 0.666667 0.638582 10.33333 0.03047 0.03047 =
0.03585 0.00000 0.00000 0.01524
N1 3 0.282492 0.517148 0.742984 11.00000 0.05353 0.03523 =
0.04147 0.00767 0.01793 0.02456
N2 3 0.359282 0.547934 0.542670 11.00000 0.05066 0.03755 =
0.04088 0.00353 0.01535 0.02490
C1 1 0.221253 0.453068 0.849841 11.00000 0.05046 0.03862 =
0.05137 0.01294 0.01935 0.02316
AFIX 13
H1 2 0.212874 0.387945 0.835281 11.00000 -1.20000
AFIX 0
C2 1 0.269124 0.490705 0.983045 11.00000 0.06081 0.13049 =
0.05235 0.03537 0.01183 0.02213
AFIX 137
H2A 2 0.330563 0.492065 0.984648 11.00000 -1.50000
H2B 2 0.227971 0.448974 1.055125 11.00000 -1.50000
H2C 2 0.280111 0.555661 0.996381 11.00000 -1.50000
AFIX 0
C3 1 0.125887 0.445961 0.846272 11.00000 0.04182 0.06405 =
0.07779 0.02888 0.01781 0.01355
AFIX 137
H3A 2 0.133679 0.509906 0.856863 11.00000 -1.50000
H3B 2 0.086189 0.404549 0.919631 11.00000 -1.50000
H3C 2 0.094821 0.418736 0.759965 11.00000 -1.50000
AFIX 0
C4 1 0.410300 0.527463 0.437722 11.00000 0.05801 0.04969 =
0.04825 0.00073 0.01894 0.03302
AFIX 13
H4 2 0.383567 0.456661 0.432248 11.00000 -1.20000
AFIX 0
C5 1 0.396738 0.562842 0.305219 11.00000 0.15305 0.16671 =
0.04152 -0.00560 0.01320 0.12061
AFIX 137
H5A 2 0.328363 0.530362 0.283183 11.00000 -1.50000
H5B 2 0.431156 0.549301 0.235292 11.00000 -1.50000
H5C 2 0.421805 0.632057 0.310311 11.00000 -1.50000
AFIX 0
C6 1 0.514202 0.574481 0.472331 11.00000 0.06570 0.15912 =
0.06877 -0.00997 0.02247 0.06117
AFIX 137
H6A 2 0.548166 0.560512 0.402201 11.00000 -1.50000
H6B 2 0.521875 0.549908 0.558779 11.00000 -1.50000
H6C 2 0.540751 0.643878 0.478725 11.00000 -1.50000
AFIX 0
C7 1 0.312943 0.485842 0.643051 11.00000 0.03740 0.03514 =
0.04506 0.00720 0.00736 0.01952
C8 1 0.295492 0.387721 0.638121 11.00000 0.04298 0.04262 =
0.04633 0.00058 0.00344 0.02354
C9 1 0.277619 0.306384 0.641150 11.00000 0.04553 0.04239 =
0.05320 0.00281 0.01127 0.02443
C10 1 0.257595 0.208609 0.643265 11.00000 0.05097 0.03588 =
0.06223 0.00163 0.01428 0.02113
C11 1 0.204388 0.146871 0.540395 11.00000 0.09271 0.05132 =
0.09680 0.00581 -0.00392 0.03409
AFIX 43
H11 2 0.180200 0.168248 0.469494 11.00000 -1.20000
AFIX 0
C12 1 0.186673 0.052309 0.542274 11.00000 0.11985 0.04174 =
0.13941 -0.01297 -0.01758 0.02788
AFIX 43
H12 2 0.148872 0.009258 0.473173 11.00000 -1.20000
AFIX 0
C13 1 0.222615 0.021424 0.641053 11.00000 0.11386 0.04346 =
0.15217 0.00822 -0.01568 0.03962
AFIX 43
H13 2 0.209288 -0.043013 0.641945 11.00000 -1.20000
AFIX 0
C14 1 0.278307 0.083886 0.739571 11.00000 0.09003 0.05410 =
0.12294 0.03602 0.01812 0.04148
AFIX 43
H14 2 0.305084 0.062791 0.807290 11.00000 -1.20000
AFIX 0
C15 1 0.296216 0.177365 0.742038 11.00000 0.06922 0.05193 =
0.07236 0.01841 0.00936 0.03116
AFIX 43
H15 2 0.334805 0.219843 0.811151 11.00000 -1.20000
AFIX 0
HKLF 4
REM A in P6(3)
REM R1 = 0.0536 for 2764 Fo > 4sig(Fo) and 0.0575 for all 2910 data
REM 162 parameters refined using 1 restraints
END
WGHT 0.0393 1.5259
REM Highest difference peak 0.390, deepest hole -0.223, 1-sigma level 0.052
Q1 1 0.1718 0.1430 0.6410 11.00000 0.05 0.37
Q2 1 0.4032 0.7416 0.6406 11.00000 0.05 0.36
Q3 1 0.2647 0.5890 0.6389 11.00000 0.05 0.35
Q4 1 0.3582 0.6876 0.7376 11.00000 0.05 0.30
Q5 1 0.3702 0.6935 0.5412 11.00000 0.05 0.29
;
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelxl_version_number 2013-3
_database_code_depnum_ccdc_archive 'CCDC 949454'
#######################################################################
#
# Cambridge Crystallographic Data Centre
# CCDC
#
#######################################################################
#
# This CIF contains data from an original supplementary publication
# deposited with the CCDC, and may include chemical, crystal,
# experimental, refinement, atomic coordinates,
# anisotropic displacement parameters and molecular geometry data,
# as required by the journal to which it was submitted.
#
# This CIF is provided on the understanding that it is used for bona
# fide research purposes only. It may contain copyright material
# of the CCDC or of third parties, and may not be copied or further
# disseminated in any form, whether machine-readable or not,
# except for the purpose of generating routine backup copies
# on your local computer system.
#
# For further information on the CCDC, data deposition and
# data retrieval see:
# www.ccdc.cam.ac.uk
#
# Bona fide researchers may freely download Mercury and enCIFer
# from this site to visualise CIF-encoded structures and
# to carry out CIF format checking respectively.
#
data_a
_audit_creation_method SHELXL-97
_chemical_name_systematic
;
?
;
_chemical_name_common ?
_chemical_melting_point ?
_chemical_formula_moiety ?
_chemical_formula_sum 'C45 H57 Er N6'
_chemical_formula_weight 849.23
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Er Er -0.2586 4.9576 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_symmetry_cell_setting Hexagonal
_symmetry_space_group_name_H-M P6(3)
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'-x, -y, z+1/2'
'y, -x+y, z+1/2'
'x-y, x, z+1/2'
_cell_length_a 16.263(2)
_cell_length_b 16.263(2)
_cell_length_c 10.028(2)
_cell_angle_alpha 90.00
_cell_angle_beta 90.00
_cell_angle_gamma 120.00
_cell_volume 2297.0(6)
_cell_formula_units_Z 2
_cell_measurement_temperature 293(2)
_cell_measurement_reflns_used ?
_cell_measurement_theta_min 1.45
_cell_measurement_theta_max 27.50
_exptl_crystal_description ?
_exptl_crystal_colour ?
_exptl_crystal_size_max 0.20
_exptl_crystal_size_mid 0.10
_exptl_crystal_size_min 0.10
_exptl_crystal_density_meas ?
_exptl_crystal_density_diffrn 1.228
_exptl_crystal_density_method 'not measured'
_exptl_crystal_F_000 874
_exptl_absorpt_coefficient_mu 1.861
_exptl_absorpt_correction_type Empirical
_exptl_absorpt_correction_T_min 0.7073
_exptl_absorpt_correction_T_max 0.8358
_exptl_absorpt_process_details
;
HIGASHI, T. (1995). Abscor-Empirical
Absorption Correction based on Fourier
Series Approximation.
Rigaku Corporation,Tokyo,Japan.
;
_diffrn_ambient_temperature 293(2)
_diffrn_radiation_wavelength 0.71073
_diffrn_radiation_type MoK\a
_diffrn_radiation_source 'fine-focus sealed tube'
_diffrn_radiation_monochromator graphite
_diffrn_measurement_device_type 'Rigaku RAXIS RAPID IP'
_diffrn_measurement_method \W
_diffrn_detector_area_resol_mean 10.00
_diffrn_standards_number 0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time 0
_diffrn_standards_decay_% 0
_diffrn_reflns_number 15646
_diffrn_reflns_av_R_equivalents 0.0771
_diffrn_reflns_av_sigmaI/netI 0.1003
_diffrn_reflns_limit_h_min -21
_diffrn_reflns_limit_h_max 21
_diffrn_reflns_limit_k_min -21
_diffrn_reflns_limit_k_max 21
_diffrn_reflns_limit_l_min -13
_diffrn_reflns_limit_l_max 13
_diffrn_reflns_theta_min 1.45
_diffrn_reflns_theta_max 27.50
_reflns_number_total 3523
_reflns_number_gt 2253
_reflns_threshold_expression >2sigma(I)
_computing_data_collection 'Rapid-AUTO (Rigaku,2000)'
_computing_cell_refinement Rapid-AUTO
_computing_data_reduction 'CrystalStructure (Rigaku/MSC,2000)'
_computing_structure_solution SHELXS-97,(Sheldrick,1997)
_computing_structure_refinement SHELXL-97,(Sheldrick,1997)
_computing_molecular_graphics 'Siemens SHELXTL V4.2,(Sheldrick,1990)'
_computing_publication_material SHELXL-97,(Sheldrick,1997)
_refine_special_details
;
Refinement of F^2^ against ALL reflections. The weighted R-factor wR and
goodness of fit S are based on F^2^, conventional R-factors R are based
on F, with F set to zero for negative F^2^. The threshold expression of
F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is
not relevant to the choice of reflections for refinement. R-factors based
on F^2^ are statistically about twice as large as those based on F, and R-
factors based on ALL data will be even larger.
;
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type full
_refine_ls_weighting_scheme calc
_refine_ls_weighting_details
'calc w=1/[\s^2^(Fo^2^)+(0.0500P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_atom_sites_solution_primary direct
_atom_sites_solution_secondary difmap
_atom_sites_solution_hydrogens geom
_refine_ls_hydrogen_treatment none
_refine_ls_extinction_method SHELXL
_refine_ls_extinction_coef 0.0117(11)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack 0.51(3)
_refine_ls_number_reflns 3523
_refine_ls_number_parameters 144
_refine_ls_number_restraints 5
_refine_ls_R_factor_all 0.0878
_refine_ls_R_factor_gt 0.0551
_refine_ls_wR_factor_ref 0.1305
_refine_ls_wR_factor_gt 0.1219
_refine_ls_goodness_of_fit_ref 1.023
_refine_ls_restrained_S_all 1.023
_refine_ls_shift/su_max 0.000
_refine_ls_shift/su_mean 0.000
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Er1 Er 0.3333 0.6667 0.2824(5) 0.0571(2) Uani 1 3 d S . .
N1 N 0.4502(5) 0.6428(6) 0.1834(9) 0.0715(19) Uani 1 1 d . . .
N2 N 0.4822(5) 0.7210(6) 0.3830(9) 0.0734(19) Uani 1 1 d . . .
C1 C 0.5122(5) 0.6887(5) 0.2747(18) 0.067(2) Uani 1 1 d . . .
C2 C 0.6114(5) 0.7075(6) 0.288(2) 0.081(2) Uani 1 1 d . . .
C3 C 0.6900(5) 0.7250(5) 0.273(2) 0.081(2) Uani 1 1 d . . .
C4 C 0.7870(7) 0.7429(7) 0.2867(18) 0.143(3) Uani 1 1 d D . .
C5 C 0.8182(8) 0.7054(10) 0.3820(12) 0.121(4) Uani 1 1 d D . .
H5 H 0.7770 0.6689 0.4497 0.146 Uiso 1 1 calc R . .
C6 C 0.9084(9) 0.7198(11) 0.3809(15) 0.152(6) Uani 1 1 d D . .
H6 H 0.9272 0.6899 0.4430 0.183 Uiso 1 1 calc R . .
C7 C 0.9701(7) 0.7784(8) 0.2874(16) 0.143(3) Uani 1 1 d D . .
H7 H 1.0328 0.7919 0.2909 0.172 Uiso 1 1 calc R . .
C8 C 0.9441(9) 0.8187(8) 0.1881(13) 0.143(3) Uani 1 1 d D . .
H8 H 0.9869 0.8568 0.1228 0.172 Uiso 1 1 calc R . .
C9 C 0.8478(9) 0.7994(10) 0.1893(14) 0.143(3) Uani 1 1 d D . .
H9 H 0.8268 0.8252 0.1241 0.172 Uiso 1 1 calc R . .
C10 C 0.4736(8) 0.5948(8) 0.0842(11) 0.090(3) Uani 1 1 d . . .
H10 H 0.5425 0.6208 0.0828 0.107 Uiso 1 1 calc R . .
C11 C 0.4420(13) 0.6085(12) -0.0463(15) 0.161(7) Uani 1 1 d . . .
H11A H 0.3741 0.5792 -0.0468 0.241 Uiso 1 1 calc R . .
H11B H 0.4616 0.5802 -0.1141 0.241 Uiso 1 1 calc R . .
H11C H 0.4697 0.6752 -0.0637 0.241 Uiso 1 1 calc R . .
C12 C 0.4236(15) 0.4877(11) 0.1202(15) 0.156(6) Uani 1 1 d . . .
H12A H 0.4550 0.4786 0.1951 0.234 Uiso 1 1 calc R . .
H12B H 0.4263 0.4524 0.0452 0.234 Uiso 1 1 calc R . .
H12C H 0.3584 0.4658 0.1425 0.234 Uiso 1 1 calc R . .
C13 C 0.5451(7) 0.7809(7) 0.4918(10) 0.082(3) Uani 1 1 d . . .
H13 H 0.6086 0.7893 0.4784 0.098 Uiso 1 1 calc R . .
C14 C 0.5517(11) 0.8736(8) 0.4890(16) 0.149(6) Uani 1 1 d . . .
H14A H 0.5642 0.8979 0.3996 0.224 Uiso 1 1 calc R . .
H14B H 0.6023 0.9165 0.5464 0.224 Uiso 1 1 calc R . .
H14C H 0.4929 0.8675 0.5193 0.224 Uiso 1 1 calc R . .
C15 C 0.5075(14) 0.7336(12) 0.6231(14) 0.221(12) Uani 1 1 d . . .
H15A H 0.5081 0.7787 0.6853 0.331 Uiso 1 1 calc R . .
H15B H 0.5467 0.7093 0.6564 0.331 Uiso 1 1 calc R . .
H15C H 0.4437 0.6822 0.6121 0.331 Uiso 1 1 calc R . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Er1 0.0541(2) 0.0541(2) 0.0629(3) 0.000 0.000 0.02707(11)
N1 0.054(4) 0.091(6) 0.067(4) -0.032(4) -0.009(4) 0.034(4)
N2 0.063(4) 0.072(5) 0.081(5) -0.019(4) -0.016(4) 0.031(4)
C1 0.063(4) 0.067(4) 0.081(6) 0.020(8) 0.039(8) 0.041(4)
C2 0.068(4) 0.086(5) 0.100(6) 0.009(11) 0.015(11) 0.048(4)
C3 0.070(5) 0.086(5) 0.091(6) 0.008(9) 0.022(8) 0.043(4)
C4 0.077(4) 0.148(6) 0.212(7) 0.056(7) 0.032(6) 0.062(4)
C5 0.087(8) 0.154(11) 0.139(9) -0.025(9) -0.032(7) 0.072(8)
C6 0.096(9) 0.183(15) 0.196(13) 0.023(13) -0.020(10) 0.084(11)
C7 0.077(4) 0.148(6) 0.212(7) 0.056(7) 0.032(6) 0.062(4)
C8 0.077(4) 0.148(6) 0.212(7) 0.056(7) 0.032(6) 0.062(4)
C9 0.077(4) 0.148(6) 0.212(7) 0.056(7) 0.032(6) 0.062(4)
C10 0.093(7) 0.119(9) 0.080(6) -0.031(5) -0.007(5) 0.070(7)
C11 0.237(19) 0.187(17) 0.104(9) -0.063(10) -0.008(11) 0.140(16)
C12 0.25(2) 0.134(12) 0.122(9) -0.042(9) 0.005(11) 0.124(14)
C13 0.069(5) 0.090(7) 0.090(7) -0.038(5) -0.022(5) 0.041(5)
C14 0.175(13) 0.078(8) 0.166(14) -0.046(8) -0.081(11) 0.040(9)
C15 0.26(2) 0.169(16) 0.083(8) -0.003(10) -0.075(12) -0.003(16)
_geom_special_details
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Er1 N1 2.343(6) 2_665 ?
Er1 N1 2.343(6) 3_565 ?
Er1 N1 2.343(6) . ?
Er1 N2 2.350(6) 2_665 ?
Er1 N2 2.350(6) . ?
Er1 N2 2.350(6) 3_565 ?
Er1 C1 2.749(7) 2_665 ?
Er1 C1 2.749(7) 3_565 ?
Er1 C1 2.749(7) . ?
N1 C1 1.289(16) . ?
N1 C10 1.428(11) . ?
N2 C1 1.396(16) . ?
N2 C13 1.479(10) . ?
C1 C2 1.489(10) . ?
C2 C3 1.171(9) . ?
C3 C4 1.460(12) . ?
C4 C5 1.36(2) . ?
C4 C9 1.37(2) . ?
C5 C6 1.365(15) . ?
C5 H5 0.9300 . ?
C6 C7 1.355(9) . ?
C6 H6 0.9300 . ?
C7 C8 1.371(9) . ?
C7 H7 0.9300 . ?
C8 C9 1.435(17) . ?
C8 H8 0.9300 . ?
C9 H9 0.9300 . ?
C10 C11 1.464(16) . ?
C10 C12 1.551(18) . ?
C10 H10 0.9800 . ?
C11 H11A 0.9600 . ?
C11 H11B 0.9600 . ?
C11 H11C 0.9600 . ?
C12 H12A 0.9600 . ?
C12 H12B 0.9600 . ?
C12 H12C 0.9600 . ?
C13 C14 1.458(15) . ?
C13 C15 1.493(16) . ?
C13 H13 0.9800 . ?
C14 H14A 0.9600 . ?
C14 H14B 0.9600 . ?
C14 H14C 0.9600 . ?
C15 H15A 0.9600 . ?
C15 H15B 0.9600 . ?
C15 H15C 0.9600 . ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 Er1 N1 103.3(2) 2_665 3_565 ?
N1 Er1 N1 103.3(2) 2_665 . ?
N1 Er1 N1 103.3(2) 3_565 . ?
N1 Er1 N2 58.4(2) 2_665 2_665 ?
N1 Er1 N2 100.3(3) 3_565 2_665 ?
N1 Er1 N2 153.1(2) . 2_665 ?
N1 Er1 N2 100.3(3) 2_665 . ?
N1 Er1 N2 153.1(2) 3_565 . ?
N1 Er1 N2 58.4(2) . . ?
N2 Er1 N2 102.9(2) 2_665 . ?
N1 Er1 N2 153.1(2) 2_665 3_565 ?
N1 Er1 N2 58.4(2) 3_565 3_565 ?
N1 Er1 N2 100.3(3) . 3_565 ?
N2 Er1 N2 102.9(2) 2_665 3_565 ?
N2 Er1 N2 102.9(2) . 3_565 ?
N1 Er1 C1 27.9(4) 2_665 2_665 ?
N1 Er1 C1 102.3(3) 3_565 2_665 ?
N1 Er1 C1 129.4(4) . 2_665 ?
N2 Er1 C1 30.5(4) 2_665 2_665 ?
N2 Er1 C1 104.6(3) . 2_665 ?
N2 Er1 C1 130.3(4) 3_565 2_665 ?
N1 Er1 C1 129.4(4) 2_665 3_565 ?
N1 Er1 C1 27.9(4) 3_565 3_565 ?
N1 Er1 C1 102.3(3) . 3_565 ?
N2 Er1 C1 104.6(3) 2_665 3_565 ?
N2 Er1 C1 130.3(3) . 3_565 ?
N2 Er1 C1 30.5(4) 3_565 3_565 ?
C1 Er1 C1 119.92(4) 2_665 3_565 ?
N1 Er1 C1 102.3(3) 2_665 . ?
N1 Er1 C1 129.4(4) 3_565 . ?
N1 Er1 C1 27.9(4) . . ?
N2 Er1 C1 130.3(4) 2_665 . ?
N2 Er1 C1 30.5(4) . . ?
N2 Er1 C1 104.6(3) 3_565 . ?
C1 Er1 C1 119.92(4) 2_665 . ?
C1 Er1 C1 119.92(4) 3_565 . ?
C1 N1 C10 117.8(8) . . ?
C1 N1 Er1 93.9(5) . . ?
C10 N1 Er1 147.8(6) . . ?
C1 N2 C13 124.4(8) . . ?
C1 N2 Er1 90.7(6) . . ?
C13 N2 Er1 143.8(6) . . ?
N1 C1 N2 116.8(6) . . ?
N1 C1 C2 129.5(13) . . ?
N2 C1 C2 113.5(14) . . ?
N1 C1 Er1 58.2(4) . . ?
N2 C1 Er1 58.7(4) . . ?
C2 C1 Er1 172.3(13) . . ?
C3 C2 C1 168(2) . . ?
C2 C3 C4 167(2) . . ?
C5 C4 C9 119.8(11) . . ?
C5 C4 C3 125.6(16) . . ?
C9 C4 C3 114.6(16) . . ?
C4 C5 C6 121.8(14) . . ?
C4 C5 H5 119.1 . . ?
C6 C5 H5 119.1 . . ?
C7 C6 C5 118.6(12) . . ?
C7 C6 H6 120.7 . . ?
C5 C6 H6 120.7 . . ?
C6 C7 C8 122.9(11) . . ?
C6 C7 H7 118.6 . . ?
C8 C7 H7 118.6 . . ?
C7 C8 C9 116.9(12) . . ?
C7 C8 H8 121.5 . . ?
C9 C8 H8 121.5 . . ?
C4 C9 C8 119.8(14) . . ?
C4 C9 H9 120.1 . . ?
C8 C9 H9 120.1 . . ?
N1 C10 C11 109.2(9) . . ?
N1 C10 C12 108.5(9) . . ?
C11 C10 C12 110.6(12) . . ?
N1 C10 H10 109.5 . . ?
C11 C10 H10 109.5 . . ?
C12 C10 H10 109.5 . . ?
C10 C11 H11A 109.5 . . ?
C10 C11 H11B 109.5 . . ?
H11A C11 H11B 109.5 . . ?
C10 C11 H11C 109.5 . . ?
H11A C11 H11C 109.5 . . ?
H11B C11 H11C 109.5 . . ?
C10 C12 H12A 109.5 . . ?
C10 C12 H12B 109.5 . . ?
H12A C12 H12B 109.5 . . ?
C10 C12 H12C 109.5 . . ?
H12A C12 H12C 109.5 . . ?
H12B C12 H12C 109.5 . . ?
C14 C13 N2 109.7(9) . . ?
C14 C13 C15 110.4(12) . . ?
N2 C13 C15 109.9(9) . . ?
C14 C13 H13 108.9 . . ?
N2 C13 H13 108.9 . . ?
C15 C13 H13 108.9 . . ?
C13 C14 H14A 109.5 . . ?
C13 C14 H14B 109.5 . . ?
H14A C14 H14B 109.5 . . ?
C13 C14 H14C 109.5 . . ?
H14A C14 H14C 109.5 . . ?
H14B C14 H14C 109.5 . . ?
C13 C15 H15A 109.5 . . ?
C13 C15 H15B 109.5 . . ?
H15A C15 H15B 109.5 . . ?
C13 C15 H15C 109.5 . . ?
H15A C15 H15C 109.5 . . ?
H15B C15 H15C 109.5 . . ?
_diffrn_measured_fraction_theta_max 0.999
_diffrn_reflns_theta_full 27.50
_diffrn_measured_fraction_theta_full 0.999
_refine_diff_density_max 1.186
_refine_diff_density_min -0.680
_refine_diff_density_rms 0.088
_database_code_depnum_ccdc_archive 'CCDC 949453'