# Electronic Supplementary Material (ESI) for Dalton Transactions # This journal is © The Royal Society of Chemistry 2013 ####################################################################### # # Cambridge Crystallographic Data Centre # CCDC # ####################################################################### # # This CIF contains data from an original supplementary publication # deposited with the CCDC, and may include chemical, crystal, # experimental, refinement, atomic coordinates, # anisotropic displacement parameters and molecular geometry data, # as required by the journal to which it was submitted. # # This CIF is provided on the understanding that it is used for bona # fide research purposes only. It may contain copyright material # of the CCDC or of third parties, and may not be copied or further # disseminated in any form, whether machine-readable or not, # except for the purpose of generating routine backup copies # on your local computer system. # # For further information on the CCDC, data deposition and # data retrieval see: # www.ccdc.cam.ac.uk # # Bona fide researchers may freely download Mercury and enCIFer # from this site to visualise CIF-encoded structures and # to carry out CIF format checking respectively. # data_I _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_sum 'C1.17 H2.39 Co O3' _chemical_formula_iupac ? _chemical_formula_weight 123.35 _chemical_melting_point ? _space_group_crystal_system trigonal _space_group_name_H-M_alt 'R -3' _space_group_name_Hall '-R 3' loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' _cell_length_a 11.77382(13) _cell_length_b 11.77382(13) _cell_length_c 11.6202(2) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_volume 1395.02(4) _cell_formula_units_Z 18 _cell_measurement_reflns_used 9949 _cell_measurement_theta_min 2.6576 _cell_measurement_theta_max 31.0482 _cell_measurement_temperature 296.(2) _exptl_crystal_description block _exptl_crystal_colour red _exptl_crystal_size_max 0.060 _exptl_crystal_size_mid 0.040 _exptl_crystal_size_min 0.040 _exptl_crystal_density_diffrn 2.643 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 1087 _exptl_absorpt_coefficient_mu 5.319 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS V2012/1 (Bruker AXS Inc.)' _exptl_absorpt_correction_T_min 0.70 _exptl_absorpt_correction_T_max 0.81 _exptl_special_details ; ; _diffrn_ambient_temperature 296.(2) _diffrn_source ? _diffrn_source_type ? _diffrn_radiation_type ? _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator ? _diffrn_measurement_device_type ? _diffrn_measurement_method ? _diffrn_detector_area_resol_mean 8.3333 _diffrn_reflns_number 21784 _diffrn_reflns_av_R_equivalents 0.0410 _diffrn_reflns_av_unetI/netI 0.0471 _diffrn_reflns_theta_min 3.46 _diffrn_reflns_theta_max 31.05 _diffrn_reflns_theta_full 31.05 _diffrn_measured_fraction_theta_max 0.976 _diffrn_measured_fraction_theta_full 0.976 _diffrn_reflns_limit_h_min -17 _diffrn_reflns_limit_h_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_limit_l_max 16 _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. The Ueq for atom c1 and C2A and O6 are higher as compared to neighbors, so the atomic displacement parameters of these atoms were restrained using SIMU and ISOR. ; _reflns_number_total 976 _reflns_number_gt 877 _reflns_threshold_expression 'I > 2\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_R_factor_all 0.0216 _refine_ls_R_factor_gt 0.0164 _refine_ls_wR_factor_gt 0.0391 _refine_ls_wR_factor_ref 0.0408 _refine_ls_goodness_of_fit_ref 1.026 _refine_ls_restrained_S_all 0.993 _refine_ls_number_reflns 976 _refine_ls_number_parameters 83 _refine_ls_number_restraints 84 _refine_ls_hydrogen_treatment mixed _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0250P)^2^+0.8145P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_diff_density_max 0.428 _refine_diff_density_min -0.267 _refine_ls_extinction_method none _refine_ls_extinction_coef ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _computing_data_collection ? _computing_cell_refinement 'SAINT V8.32B (Bruker AXS Inc., 2013)' _computing_data_reduction 'SAINT V8.32B (Bruker AXS Inc., 2013)' _computing_structure_solution ? _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_molecular_graphics ? _computing_publication_material ? loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_refinement_flags_posn _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co Co1 0.51467(2) 0.12274(2) 0.42008(2) 0.01095(6) Uani d . . D 1.0 . . C C1 0.2356(4) 0.0066(3) 0.3370(3) 0.0170(6) Uani d U P D 0.796(7) A 1 H H1C 0.145(3) -0.062(3) 0.336(2) 0.030(7) Uiso d . P . 0.796(7) A 1 O O1 0.3054(3) 0.0005(4) 0.4134(4) 0.0180(7) Uani d U P D 0.796(7) A 1 C C1A 0.2332(17) 0.0279(15) 0.3539(14) 0.0141(16) Uani d U P D 0.204(7) A 2 O O1A 0.3042(13) 0.0188(15) 0.4280(15) 0.0141(16) Uani d U P D 0.204(7) A 2 C C2A 0.0899(7) -0.0430(8) 0.3756(7) 0.024(2) Uani d U P . 0.204(7) A 2 H H2A1 0.0609 -0.1332 0.3929 0.037 Uiso calc U P R 0.204(7) A 2 H H2A2 0.045 -0.0383 0.3083 0.037 Uiso calc U P R 0.204(7) A 2 H H2A3 0.0709 -0.0035 0.4395 0.037 Uiso calc U P R 0.204(7) A 2 O O2 0.71467(9) 0.20933(9) 0.42529(8) 0.01263(18) Uani d . . . 1.0 . . H H2O 0.724(2) 0.166(2) 0.466(2) 0.034(7) Uiso d . . . 1.0 . . O O3 0.49065(10) 0.06212(10) 0.59485(8) 0.01555(19) Uani d . . . 1.0 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Co1 0.01080(9) 0.01033(9) 0.01197(9) 0.00546(7) 0.00130(5) 0.00205(6) C1 0.0120(8) 0.0158(13) 0.0200(14) 0.0046(9) -0.0006(9) 0.0021(9) O1 0.0159(7) 0.0161(13) 0.0202(13) 0.0066(7) -0.0018(7) 0.0035(9) C1A 0.013(2) 0.014(3) 0.017(3) 0.0078(19) 0.003(2) -0.003(2) O1A 0.015(2) 0.013(3) 0.016(3) 0.0082(17) 0.0008(18) 0.000(2) C2A 0.012(3) 0.027(3) 0.024(3) 0.003(2) 0.002(2) 0.007(3) O2 0.0115(4) 0.0119(4) 0.0129(4) 0.0047(4) -0.0003(3) 0.0016(3) O3 0.0187(5) 0.0142(4) 0.0142(4) 0.0086(4) 0.0031(3) 0.0024(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Co1 O2 3_665 2.0432(9) ? Co1 O2 . 2.0463(9) ? Co1 O2 17 2.1160(9) ? Co1 O3 . 2.1241(9) ? Co1 O1 . 2.145(3) ? Co1 O1A . 2.148(13) ? Co1 O3 10_656 2.1529(10) ? Co1 Co1 17 2.9963(2) ? Co1 Co1 18_545 2.9964(3) ? C1 O1 . 1.236(4) ? C1 O3 8_544 1.264(4) ? C1A O1A . 1.241(14) ? C1A O3 8_544 1.275(17) ? C1A C2A . 1.483(19) ? O2 Co1 2_655 2.0433(9) ? O2 Co1 18_545 2.1160(9) ? O3 C1 6 1.264(4) ? O3 C1A 6 1.275(17) ? O3 Co1 10_656 2.1528(10) ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O2 Co1 O2 3_665 . 100.10(5) ? O2 Co1 O2 3_665 17 84.63(4) ? O2 Co1 O2 . 17 84.55(4) ? O2 Co1 O3 3_665 . 103.19(4) ? O2 Co1 O3 . . 93.78(4) ? O2 Co1 O3 17 . 172.18(4) ? O2 Co1 O1 3_665 . 89.89(12) ? O2 Co1 O1 . . 170.01(12) ? O2 Co1 O1 17 . 96.43(12) ? O3 Co1 O1 . . 83.91(12) ? O2 Co1 O1A 3_665 . 83.8(5) ? O2 Co1 O1A . . 174.2(5) ? O2 Co1 O1A 17 . 100.1(5) ? O3 Co1 O1A . . 81.1(5) ? O2 Co1 O3 3_665 10_656 172.25(4) ? O2 Co1 O3 . 10_656 87.17(4) ? O2 Co1 O3 17 10_656 93.48(4) ? O3 Co1 O3 . 10_656 78.80(4) ? O1 Co1 O3 . 10_656 82.85(12) ? O1A Co1 O3 . 10_656 89.2(4) ? O2 Co1 Co1 3_665 17 44.89(3) ? O2 Co1 Co1 . 17 105.88(3) ? O2 Co1 Co1 17 17 43.04(3) ? O3 Co1 Co1 . 17 144.32(3) ? O1 Co1 Co1 . 17 81.16(13) ? O1A Co1 Co1 . 17 79.9(5) ? O3 Co1 Co1 10_656 17 130.58(3) ? O2 Co1 Co1 3_665 18_545 105.90(3) ? O2 Co1 Co1 . 18_545 44.89(3) ? O2 Co1 Co1 17 18_545 42.95(3) ? O3 Co1 Co1 . 18_545 132.57(3) ? O1 Co1 Co1 . 18_545 132.12(11) ? O1A Co1 Co1 . 18_545 138.3(4) ? O3 Co1 Co1 10_656 18_545 77.35(3) ? Co1 Co1 Co1 17 18_545 79.682(8) ? O1 C1 O3 . 8_544 126.2(3) ? C1 O1 Co1 . . 124.1(3) ? O1A C1A O3 . 8_544 126.5(15) ? O1A C1A C2A . . 117.4(13) ? O3 C1A C2A 8_544 . 116.1(13) ? C1A O1A Co1 . . 123.8(12) ? Co1 O2 Co1 2_655 . 139.70(5) ? Co1 O2 Co1 2_655 18_545 92.16(4) ? Co1 O2 Co1 . 18_545 92.07(4) ? C1 O3 Co1 6 . 123.85(16) ? C1A O3 Co1 6 . 134.5(7) ? C1 O3 Co1 6 10_656 128.47(18) ? C1A O3 Co1 6 10_656 123.1(7) ? Co1 O3 Co1 . 10_656 101.20(4) ? _shelx_res_file ; TITL liu106r in R-3 CELL 0.71073 11.77382 11.77382 11.62020 90.0000 90.0000 120.0000 ZERR 18.00 0.00013 0.00013 0.00022 0.0000 0.0000 0.0000 LATT 3 SYMM -Y, X-Y, Z SYMM -X+Y, -X, Z SFAC C H O Co UNIT 21 43 54 18 omit -1 1 1 L.S. 4 ACTA BOND FMAP 2 PLAN 5 sadi co1 o1 co1 o1a sadi o1 c1 o1a c1a SIZE 0.040 0.040 0.060 DELU 0.01 C1 > C2A SIMU 0.005 C1 > C2A ISOR 0.005 C1 > C2A TEMP 23 WGHT 0.025000 0.814500 FVAR 0.09478 0.79554 CO1 4 0.514670 0.122736 0.420084 11.00000 0.01080 0.01033 = 0.01197 0.00205 0.00130 0.00546 PART 1 21.00 C1 1 0.235575 0.006553 0.337014 21.00000 0.01202 0.01577 = 0.02001 0.00212 -0.00058 0.00455 H1C 2 0.145272 -0.061545 0.335865 21.00000 0.02986 O1 3 0.305435 0.000466 0.413398 21.00000 0.01587 0.01614 = 0.02019 0.00347 -0.00177 0.00664 PART 2 -21.00 C1A 1 0.233227 0.027903 0.353937 -21.00000 0.01302 0.01366 = 0.01704 -0.00261 0.00287 0.00777 O1A 3 0.304217 0.018829 0.427985 -21.00000 0.01487 0.01297 = 0.01606 -0.00027 0.00082 0.00820 C2A 1 0.089884 -0.043014 0.375573 -21.00000 0.01199 0.02743 = 0.02449 0.00726 0.00157 0.00300 AFIX 137 H2A1 2 0.060912 -0.133163 0.392939 -21.00000 -1.50000 H2A2 2 0.045047 -0.038301 0.308329 -21.00000 -1.50000 H2A3 2 0.070906 -0.003482 0.439455 -21.00000 -1.50000 PART 0 AFIX 0 O2 3 0.714672 0.209333 0.425287 11.00000 0.01151 0.01192 = 0.01290 0.00161 -0.00035 0.00470 H2O 2 0.723772 0.166371 0.465927 11.00000 0.03379 O3 3 0.490653 0.062124 0.594851 11.00000 0.01872 0.01424 = 0.01421 0.00238 0.00312 0.00863 HKLF 4 REM liu106r in R-3 REM R1 = 0.0164 for 877 Fo > 4sig(Fo) and 0.0216 for all 976 data REM 83 parameters refined using 84 restraints END WGHT 0.0242 1.0165 REM Highest difference peak 0.428, deepest hole -0.267, 1-sigma level 0.074 Q1 1 0.5651 0.1956 0.3917 11.00000 0.05 0.43 Q2 1 0.4699 0.0564 0.4440 11.00000 0.05 0.42 Q3 1 0.5434 0.0870 0.3778 11.00000 0.05 0.42 Q4 1 0.4870 0.1501 0.4606 11.00000 0.05 0.37 Q5 1 0.5769 0.1389 0.4605 11.00000 0.05 0.36 ; _shelx_res_checksum 40658 _shelx_hkl_file ; 0 -1 1 197.19 7.28 2 1 -2 77.36 3.08 2 1 -2 78.58 3.39 2 1 -2 74.87 3.51 2 1 -2 79.35 2.91 2 1 -2 75.22 3.13 2 1 -2 77.28 3.11 -2 -1 2 77.77 3.03 -2 -1 2 76.30 3.30 -2 -1 2 77.40 3.18 -2 -1 2 76.14 3.10 -2 -1 2 74.26 3.95 -2 0 1 274.59 9.35 -2 0 1 287.71 10.61 -2 0 1 297.58 9.93 -2 0 1 298.31 9.75 2 0 -1 290.23 11.18 2 0 -1 293.55 9.76 2 0 -1 305.17 10.89 2 0 -1 290.39 9.90 2 0 -1 288.74 10.02 -1 1 -2 18.31 0.89 1 -1 2 21.12 1.25 0 -2 2 133.78 4.94 0 -2 2 126.52 4.69 0 -2 2 126.80 5.08 0 -2 2 127.06 4.76 0 -2 2 128.46 6.02 0 -2 2 129.16 5.11 0 2 -2 128.54 4.74 0 2 -2 128.28 4.74 0 2 -2 126.86 4.77 0 2 -2 126.70 4.70 0 2 -2 130.76 5.22 -2 1 0 34.15 1.28 2 -1 0 34.85 1.30 2 -1 0 34.14 1.49 2 -1 0 34.39 1.27 2 -1 0 32.05 1.48 0 -2 -1 275.20 9.55 0 -2 -1 279.48 10.37 0 -2 -1 279.13 9.80 0 -2 -1 280.57 9.40 0 2 1 281.76 9.21 0 2 1 285.88 10.15 0 2 1 290.95 9.80 0 2 1 284.75 9.60 0 2 1 275.39 9.41 0 2 1 244.81 10.55 0 2 1 291.38 10.07 -2 2 -1 273.37 9.82 -2 2 -1 287.99 10.01 -2 2 -1 280.67 9.64 -2 2 -1 287.19 9.54 -2 2 -1 282.17 9.46 2 -2 1 291.78 10.47 2 -2 1 281.25 9.45 2 -2 1 294.38 9.62 2 -2 1 281.85 9.45 2 -2 1 278.21 12.06 2 -2 1 263.06 9.57 2 -2 1 286.93 10.23 -1 -2 1 134.06 4.88 -1 -2 1 130.06 6.31 -1 -2 1 142.17 5.20 -1 -2 1 135.43 5.34 -1 -2 1 131.21 4.95 1 2 -1 142.01 5.00 1 2 -1 137.52 4.92 1 2 -1 133.16 5.36 1 2 -1 134.58 5.55 1 2 -1 131.84 4.97 1 2 -1 138.03 5.95 1 2 -1 138.99 4.54 0 -1 -2 58.48 2.29 0 -1 -2 60.00 2.34 0 -1 -2 57.10 2.34 0 1 2 62.57 2.48 0 1 2 59.24 2.30 0 1 2 60.98 2.36 0 1 2 59.06 2.27 0 1 2 62.80 2.47 -2 -1 -1 412.19 13.88 -2 -1 -1 411.31 17.41 2 1 1 418.04 14.76 2 1 1 421.20 13.68 2 1 1 420.36 13.88 2 1 1 407.37 15.61 2 1 1 394.55 15.12 2 1 1 412.79 15.82 2 1 1 423.37 14.10 2 -2 -2 137.67 4.70 2 -2 -2 130.80 4.92 2 -2 -2 129.58 4.78 2 -2 -2 126.77 4.74 2 -2 -2 129.83 4.94 2 -2 -2 132.35 5.20 2 -2 -2 131.16 4.69 -2 2 2 128.16 4.71 -2 2 2 133.25 4.59 -2 2 2 129.00 5.09 -2 2 2 128.58 4.96 -2 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4 -8 0 33.15 2.41 -8 0 4 40.75 2.40 4 -8 0 26.61 3.16 -8 0 4 43.22 3.16 -8 0 4 38.65 4.09 -8 0 4 41.42 2.64 4 -8 0 31.92 1.89 4 -8 0 32.94 2.16 4 -8 0 33.09 2.36 4 -8 0 32.69 2.29 8 0 -4 41.79 2.37 -4 8 0 33.22 2.40 -4 8 0 32.88 2.32 8 0 -4 43.96 2.71 -4 8 0 31.32 2.41 8 0 -4 42.38 3.38 -4 8 0 31.42 2.53 -4 8 0 36.43 2.95 8 0 -4 41.64 3.25 -1 4 -8 0.14 0.99 -1 4 -8 0.89 1.01 -1 4 -8 0.69 1.25 -1 4 -8 1.50 1.17 -1 4 -8 1.70 1.15 -1 4 -8 1.72 1.54 1 -4 8 1.85 1.35 1 -4 8 1.18 1.15 1 -4 8 1.47 1.88 1 -4 8 2.90 1.67 1 -4 8 2.22 1.56 1 -4 8 0.79 1.20 1 -4 8 2.10 1.16 4 -8 -3 81.48 4.10 4 -8 -3 80.00 3.53 4 -8 -3 81.39 4.09 4 -8 -3 84.96 4.22 4 -8 -3 86.54 4.35 4 -8 -3 86.48 3.81 -4 8 3 79.19 4.21 -4 8 3 82.43 3.98 -4 8 3 80.62 4.21 -4 8 3 84.57 4.86 -4 8 3 81.25 4.03 -4 8 3 79.12 4.10 -4 8 3 81.94 4.07 -4 4 -8 19.11 2.22 -4 4 -8 24.02 2.37 -4 4 -8 22.39 2.06 -4 4 -8 21.64 1.89 -4 4 -8 22.14 2.23 4 -4 8 21.37 2.19 4 -4 8 23.14 2.04 4 -4 8 24.46 2.50 4 -4 8 21.19 2.29 4 -4 8 18.96 2.49 4 -4 8 24.05 2.77 -8 -6 4 24.52 5.36 4 -8 -6 41.18 2.72 4 -8 -6 39.46 3.05 4 -8 -6 39.79 2.99 -8 -6 4 25.74 3.32 4 -8 -6 41.21 2.88 4 -8 -6 39.64 3.03 4 -8 -6 35.61 3.21 -8 -6 4 26.31 3.48 -4 8 6 39.42 2.95 8 6 -4 25.36 3.41 8 6 -4 23.40 3.17 8 6 -4 26.08 4.08 -4 8 6 41.93 2.84 -4 8 6 40.54 3.05 -4 8 6 43.34 3.90 -4 8 6 43.52 2.97 -7 4 -8 16.95 1.85 -7 4 -8 18.62 1.96 -7 4 -8 18.83 2.24 7 -4 8 17.23 2.41 7 -4 8 21.99 2.68 7 -4 8 12.55 2.08 7 -4 8 16.22 1.79 3 -8 8 76.30 5.08 3 -8 8 77.09 4.87 3 -8 8 79.52 4.64 3 -8 8 78.50 6.11 3 -8 8 85.53 4.74 3 -8 8 82.86 5.09 3 -8 8 82.01 4.56 -3 8 -8 78.11 4.57 -3 8 -8 78.12 4.60 -3 8 -8 74.39 4.48 -3 8 -8 79.30 4.39 -3 8 -8 75.86 4.77 -3 8 -8 80.62 4.06 3 -8 5 38.22 2.84 3 -8 5 40.54 3.22 3 -8 5 38.48 2.87 3 -8 5 35.75 2.85 3 -8 5 36.74 2.34 3 -8 5 36.98 4.10 3 -8 5 37.70 3.14 -3 8 -5 36.30 2.49 -3 8 -5 34.95 2.77 -3 8 -5 34.58 2.50 -3 8 -5 36.53 2.99 -3 8 -5 36.65 2.45 -3 8 -5 36.51 2.95 -8 4 3 27.04 1.97 -8 4 3 23.85 2.47 -8 4 3 24.43 2.38 4 3 -8 19.80 2.59 4 3 -8 15.77 2.28 4 3 -8 18.07 1.82 4 3 -8 21.37 2.47 -8 4 3 28.18 1.76 4 3 -8 19.42 2.42 4 3 -8 15.51 2.53 -4 -3 8 18.58 2.51 -4 -3 8 15.45 2.32 8 -4 -3 30.13 2.04 8 -4 -3 24.75 2.46 -4 -3 8 16.89 3.27 -4 -3 8 18.88 2.26 -4 -3 8 18.11 2.75 8 -4 -3 27.12 1.66 -4 -3 8 17.75 2.42 8 -4 -3 28.19 2.13 3 -8 2 84.53 3.96 3 -8 2 87.82 4.16 3 -8 2 85.27 3.98 3 -8 2 78.32 4.35 3 -8 2 84.22 3.83 3 -8 2 81.34 5.50 3 -8 2 83.65 4.09 -3 8 -2 78.51 3.76 -3 8 -2 82.44 3.81 -3 8 -2 80.61 4.09 -3 8 -2 81.35 4.13 -3 8 -2 84.81 4.39 -3 8 -2 83.74 4.29 1 3 -8 130.09 5.51 1 3 -8 127.07 5.81 1 3 -8 128.84 5.60 1 3 -8 127.29 5.88 1 3 -8 125.27 5.88 1 3 -8 125.02 5.38 -1 -3 8 131.32 6.58 -1 -3 8 126.48 5.56 -1 -3 8 127.17 5.85 -1 -3 8 139.23 7.49 -1 -3 8 135.41 6.37 -1 -3 8 127.60 5.87 3 -8 -1 107.87 4.40 3 -8 -1 104.20 4.93 3 -8 -1 108.34 4.30 3 -8 -1 108.18 5.13 3 -8 -1 101.12 6.09 3 -8 -1 106.64 4.75 3 -8 -1 104.61 4.71 -3 8 1 106.56 5.17 -3 8 1 105.28 4.82 -3 8 1 103.29 4.94 -3 8 1 105.58 5.39 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3.85 -8 8 2 66.70 3.49 -8 8 2 67.63 4.21 -8 8 2 70.64 3.45 -8 8 2 66.48 3.54 8 -8 -2 71.27 3.48 8 -8 -2 66.05 3.30 8 -8 -2 66.10 3.56 8 -8 -2 70.47 3.77 8 -8 -2 66.33 3.74 8 -8 -2 65.71 2.99 8 -8 -2 65.68 4.14 2 -8 7 25.64 3.05 2 -8 7 25.54 2.87 2 -8 7 31.10 3.35 2 -8 7 29.24 2.97 2 -8 7 25.52 3.99 2 -8 7 27.58 2.30 2 -8 7 26.09 2.84 -2 8 -7 28.93 3.11 -2 8 -7 30.82 2.76 -2 8 -7 26.61 2.62 -2 8 -7 32.05 2.32 -2 8 -7 30.02 3.09 -2 8 -7 33.36 2.87 6 2 -8 0.70 1.50 6 2 -8 -0.33 1.30 6 2 -8 0.06 1.49 6 2 -8 0.50 1.00 6 2 -8 -0.69 1.49 6 2 -8 -0.71 1.25 -6 -2 8 1.36 1.43 -6 -2 8 0.35 1.34 -6 -2 8 0.04 1.12 -6 -2 8 -2.56 1.90 -6 -2 8 -0.97 1.66 -8 5 2 83.72 3.67 -8 5 2 86.76 3.45 -8 5 2 84.77 3.59 -8 5 2 84.14 4.47 -8 5 2 85.25 4.46 -8 5 2 82.94 3.86 8 -5 -2 85.98 4.04 8 -5 -2 85.95 4.21 8 -5 -2 89.57 3.60 8 -5 -2 80.97 3.71 8 -5 -2 81.09 4.49 2 -8 4 1.07 1.21 2 -8 4 2.02 1.15 2 -8 4 0.14 0.92 2 -8 4 1.21 1.05 2 -8 4 1.02 1.28 2 -8 4 1.41 1.18 2 -8 4 -0.07 1.81 -2 8 -4 0.06 1.13 -2 8 -4 0.36 0.90 -2 8 -4 0.71 0.85 -2 8 -4 1.07 1.18 -2 8 -4 0.17 1.06 3 2 -8 2.57 1.39 3 2 -8 2.20 1.44 3 2 -8 3.04 1.25 3 2 -8 2.43 1.17 3 2 -8 2.00 1.40 3 2 -8 2.51 0.95 3 2 -8 2.38 1.36 -3 -2 8 2.37 1.28 -3 -2 8 2.10 1.42 -3 -2 8 2.58 1.89 -3 -2 8 2.54 1.15 -3 -2 8 1.24 1.23 -8 2 2 2.98 0.83 -8 2 2 2.69 0.68 -8 2 2 3.54 1.24 8 -2 -2 2.15 0.85 8 -2 -2 1.34 1.18 8 -2 -2 2.87 0.79 8 -2 -2 3.20 1.10 2 -8 1 70.70 3.72 2 -8 1 69.85 3.91 2 -8 1 63.29 3.51 2 -8 1 72.80 3.30 2 -8 1 66.82 3.57 2 -8 1 68.37 4.94 -2 8 -1 61.62 3.56 -2 8 -1 65.55 3.74 -2 8 -1 67.16 3.26 -2 8 -1 65.72 3.66 -2 8 -1 69.56 3.54 -2 8 -1 68.19 4.05 0 2 -8 30.10 2.27 0 2 -8 26.26 2.32 0 2 -8 29.19 2.14 0 2 -8 26.44 2.46 0 2 -8 26.55 1.63 0 2 -8 23.71 2.28 0 -2 8 25.73 2.34 0 -2 8 29.48 2.35 0 -2 8 28.25 2.24 0 -2 8 23.03 2.69 0 -2 8 28.84 1.82 0 -2 8 28.93 2.97 0 -2 8 25.45 2.88 -8 -1 2 378.93 13.76 -8 -1 2 391.80 14.75 -8 -1 2 388.93 14.93 -8 -1 2 379.33 18.04 8 1 -2 381.93 13.50 8 1 -2 383.88 16.01 8 1 -2 386.73 15.31 2 -8 -2 2.66 1.12 2 -8 -2 2.81 1.57 2 -8 -2 2.29 1.23 2 -8 -2 3.45 1.32 2 -8 -2 3.52 1.14 2 -8 -2 2.56 1.17 -2 8 2 3.32 1.17 -2 8 2 3.21 1.23 -2 8 2 3.78 1.70 -2 8 2 3.48 1.25 -2 8 2 5.79 1.39 -2 8 2 3.79 0.85 -2 8 2 3.58 1.17 -2 8 2 4.56 1.35 -3 2 -8 1.83 1.14 -3 2 -8 1.21 0.94 -3 2 -8 1.50 0.95 -3 2 -8 2.34 1.13 -3 2 -8 1.08 0.62 3 -2 8 2.18 1.53 3 -2 8 2.06 1.38 3 -2 8 1.31 1.09 3 -2 8 -0.70 1.42 3 -2 8 2.17 0.92 3 -2 8 1.98 1.07 3 -2 8 2.10 0.89 -8 -4 2 15.56 2.12 -8 -4 2 15.72 2.30 -8 -4 2 15.89 3.51 8 4 -2 14.90 2.60 8 4 -2 16.57 2.57 8 4 -2 16.80 2.14 8 4 -2 11.95 2.69 2 -8 -5 70.51 3.96 2 -8 -5 66.27 3.82 2 -8 -5 69.74 4.28 2 -8 -5 67.58 4.06 2 -8 -5 71.29 3.85 -2 8 5 68.76 3.85 -2 8 5 65.94 3.43 -2 8 5 67.01 3.99 -2 8 5 68.43 3.98 -2 8 5 70.21 4.14 -2 8 5 63.54 4.54 -6 2 -8 178.73 7.20 -6 2 -8 181.02 7.14 -6 2 -8 183.68 6.87 -6 2 -8 181.54 7.76 6 -2 8 186.30 7.79 6 -2 8 183.20 7.72 6 -2 8 185.84 8.80 6 -2 8 188.64 7.04 6 -2 8 170.20 8.35 -8 -7 2 11.59 2.43 -8 -7 2 12.45 4.83 -8 -7 2 13.94 2.83 8 7 -2 9.57 2.71 8 7 -2 13.05 2.55 8 7 -2 16.83 3.63 8 1 -8 212.10 9.78 8 1 -8 202.36 8.88 8 1 -8 199.57 10.22 8 1 -8 213.98 9.13 -8 -1 8 189.55 8.96 -8 -1 8 223.90 10.00 -8 -1 8 213.13 11.80 1 -8 6 32.89 3.05 1 -8 6 37.37 2.79 1 -8 6 36.72 3.38 1 -8 6 35.99 4.70 1 -8 6 39.73 2.97 1 -8 6 35.41 3.51 1 -8 6 35.58 3.10 -1 8 -6 37.50 2.96 -1 8 -6 39.68 3.32 -1 8 -6 35.96 3.10 -1 8 -6 36.75 2.42 -1 8 -6 35.54 2.91 -1 8 -6 39.17 4.14 -1 8 -6 36.20 2.94 5 1 -8 40.36 3.11 5 1 -8 39.64 3.08 5 1 -8 40.73 3.25 5 1 -8 42.19 3.54 5 1 -8 44.79 3.31 5 1 -8 44.34 3.16 -5 -1 8 41.43 2.75 -5 -1 8 41.10 3.62 -5 -1 8 43.98 4.27 -5 -1 8 42.91 3.30 -5 -1 8 42.31 3.16 1 -8 3 199.61 8.26 1 -8 3 196.21 10.76 1 -8 3 204.79 8.91 1 -8 3 207.84 8.20 1 -8 3 202.67 8.14 1 -8 3 196.10 8.18 1 -8 3 203.18 7.79 -1 8 -3 206.50 8.35 -1 8 -3 211.03 7.55 -1 8 -3 196.78 8.16 -1 8 -3 200.29 8.34 -1 8 -3 207.23 8.74 2 1 -8 1.61 1.10 2 1 -8 1.35 1.16 2 1 -8 1.52 1.06 2 1 -8 0.99 0.88 2 1 -8 0.99 0.87 2 1 -8 1.57 1.12 -2 -1 8 1.10 0.90 -2 -1 8 0.99 0.98 -2 -1 8 1.93 1.13 -2 -1 8 0.70 1.07 -2 -1 8 1.11 1.45 -2 -1 8 1.17 1.22 1 -8 0 93.45 6.00 1 -8 0 94.64 3.85 1 -8 0 92.46 4.87 1 -8 0 85.95 4.36 1 -8 0 96.23 4.80 1 -8 0 97.90 4.45 -1 8 0 91.90 5.04 -1 8 0 93.81 4.96 -1 8 0 90.68 4.55 -1 8 0 93.33 4.60 -1 8 0 89.42 4.51 -1 8 0 90.12 4.09 -1 8 0 99.03 4.75 -1 1 -8 8.01 1.61 -1 1 -8 8.29 1.15 -1 1 -8 7.12 1.36 -1 1 -8 6.40 1.36 -1 1 -8 7.92 0.87 -1 1 -8 8.52 1.44 1 -1 8 6.57 1.80 1 -1 8 9.01 1.80 1 -1 8 7.23 1.01 1 -1 8 6.73 1.70 1 -1 8 7.48 1.32 1 -1 8 7.64 1.38 1 -1 8 8.24 1.54 1 -1 8 7.41 1.36 1 -8 -3 206.43 8.12 1 -8 -3 207.74 8.29 1 -8 -3 204.74 8.98 1 -8 -3 207.80 10.17 1 -8 -3 202.01 8.68 1 -8 -3 206.86 8.09 -1 8 3 208.97 8.57 -1 8 3 203.00 8.23 -1 8 3 204.47 9.14 -1 8 3 213.13 9.27 -1 8 3 201.92 7.91 -1 8 3 205.62 7.89 -1 8 3 214.40 8.46 -1 8 3 208.60 9.16 -4 1 -8 122.89 5.75 -4 1 -8 125.32 5.14 -4 1 -8 127.47 5.42 -4 1 -8 121.97 5.02 -4 1 -8 127.24 5.42 4 -1 8 130.29 6.48 4 -1 8 126.16 6.33 4 -1 8 127.18 5.31 4 -1 8 129.46 5.73 4 -1 8 131.13 5.23 4 -1 8 125.65 5.79 1 -8 -6 87.18 4.55 1 -8 -6 92.86 5.23 1 -8 -6 85.31 4.73 1 -8 -6 92.72 4.86 1 -8 -6 87.57 5.03 -1 8 6 91.80 4.83 -1 8 6 93.39 4.76 -1 8 6 90.91 4.25 -1 8 6 90.63 5.18 -1 8 6 93.26 5.62 -1 8 6 88.79 4.79 -7 1 -8 105.10 4.84 -7 1 -8 100.98 5.34 -7 1 -8 100.74 4.55 -7 1 -8 105.28 5.04 7 -1 8 106.61 6.09 7 -1 8 106.74 5.40 7 -1 8 110.89 5.93 7 -1 8 107.02 5.17 7 -1 8 105.90 4.47 0 -8 8 88.42 7.51 0 -8 8 84.69 5.50 0 -8 8 94.74 5.41 0 -8 8 91.26 5.20 0 -8 8 90.93 5.90 0 -8 8 88.65 5.33 0 8 -8 97.75 4.22 0 8 -8 93.01 5.54 0 8 -8 92.81 6.46 0 8 -8 90.92 5.36 0 8 -8 90.60 5.38 0 8 -8 88.44 5.18 0 8 -8 96.07 5.08 -8 7 0 91.31 4.20 -8 7 0 91.74 4.13 -8 7 0 90.86 4.24 -8 7 0 96.27 4.00 -8 7 0 90.95 4.60 8 -7 0 92.51 4.47 8 -7 0 90.22 4.02 8 -7 0 91.18 3.65 8 -7 0 93.66 3.90 8 -7 0 86.03 4.65 8 -7 0 91.40 4.68 0 -8 5 110.52 5.99 0 -8 5 113.12 5.67 0 -8 5 110.21 5.55 0 -8 5 110.37 5.48 0 -8 5 121.25 5.18 0 -8 5 118.98 7.96 0 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132.89 6.64 -7 10 -5 152.84 5.90 -7 10 -5 144.86 6.47 -10 4 7 2.18 1.51 -10 4 7 4.64 2.02 -10 4 7 1.56 1.68 10 -4 -7 3.05 1.86 10 -4 -7 1.12 1.25 10 -4 -7 2.54 1.65 10 -4 -7 3.25 1.82 3 7 -10 69.41 5.52 3 7 -10 64.95 5.16 3 7 -10 65.38 4.26 3 7 -10 66.41 5.15 3 7 -10 60.56 4.95 -3 -7 10 62.80 5.12 -3 -7 10 63.30 5.11 -3 -7 10 74.54 5.87 -3 -7 10 61.93 7.59 -3 -7 10 65.74 5.15 -3 -7 10 62.49 5.10 7 -10 2 58.41 4.91 7 -10 2 60.77 3.44 7 -10 2 57.60 3.63 7 -10 2 56.15 3.20 7 -10 2 55.32 3.63 7 -10 2 51.92 3.01 7 -10 2 54.83 3.38 7 -10 2 58.73 3.73 7 -10 2 56.29 3.75 -7 10 -2 62.25 3.81 -7 10 -2 55.56 3.48 -7 10 -2 52.25 3.50 -7 10 -2 55.66 3.42 -7 10 -2 56.34 3.88 -10 1 7 6.74 1.92 -10 1 7 4.30 2.69 -10 1 7 6.08 2.25 -10 1 7 6.94 2.38 10 -1 -7 7.42 2.19 10 -1 -7 6.77 1.94 10 -1 -7 6.36 2.31 0 7 -10 28.90 3.07 0 7 -10 29.29 3.56 0 7 -10 31.55 3.53 0 7 -10 30.28 3.44 0 7 -10 31.56 3.65 0 7 -10 29.91 2.46 0 7 -10 32.34 4.34 0 -7 10 32.25 3.71 0 -7 10 31.28 3.61 0 -7 10 31.64 3.95 0 -7 10 27.71 4.73 0 -7 10 32.10 3.68 0 -7 10 31.33 3.98 0 -7 10 29.89 3.44 0 -7 10 29.07 3.34 7 -10 -1 121.86 4.81 7 -10 -1 128.04 5.84 7 -10 -1 129.45 5.99 7 -10 -1 132.22 5.76 7 -10 -1 124.18 5.63 7 -10 -1 129.87 5.78 7 -10 -1 128.62 6.47 -7 10 1 120.81 5.97 -7 10 1 126.89 5.84 -7 10 1 124.53 5.79 -7 10 1 127.08 6.53 -7 10 1 124.99 5.66 -10 -2 7 8.25 2.24 -10 -2 7 8.13 3.54 -10 -2 7 8.87 2.84 10 2 -7 8.14 2.31 10 2 -7 12.68 3.13 10 2 -7 8.78 2.68 -3 7 -10 104.60 5.78 -3 7 -10 100.88 5.44 -3 7 -10 100.59 6.50 -3 7 -10 100.66 5.88 -3 7 -10 98.56 5.44 -3 7 -10 98.97 5.45 3 -7 10 100.31 6.92 3 -7 10 105.64 5.58 3 -7 10 97.41 6.04 3 -7 10 90.80 5.35 3 -7 10 96.42 6.02 3 -7 10 97.85 5.48 7 -10 -4 139.77 6.38 7 -10 -4 131.06 6.55 7 -10 -4 129.58 5.68 7 -10 -4 133.48 7.06 7 -10 -4 140.48 6.31 7 -10 -4 139.44 6.22 -7 10 4 131.18 6.53 -7 10 4 138.21 6.34 -7 10 4 138.97 6.60 -7 10 4 137.24 6.13 -7 10 4 129.56 7.09 -7 10 4 134.74 6.11 -7 10 4 136.63 6.33 -10 -5 7 1.55 2.23 -10 -5 7 1.62 4.37 10 5 -7 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4.64 -6 10 2 85.59 4.78 -6 10 2 88.96 5.37 -6 10 2 84.11 4.52 -6 10 2 88.53 4.72 -6 10 2 82.29 4.39 -4 6 -10 125.50 6.28 -4 6 -10 123.47 5.93 -4 6 -10 131.23 5.48 -4 6 -10 120.07 6.19 -4 6 -10 127.59 6.15 4 -6 10 126.77 7.30 4 -6 10 113.19 6.61 4 -6 10 135.36 6.07 4 -6 10 126.91 6.13 4 -6 10 118.70 6.84 4 -6 10 123.29 6.13 6 -10 -5 1.02 1.37 6 -10 -5 1.42 1.29 6 -10 -5 1.17 1.05 6 -10 -5 0.73 1.46 6 -10 -5 2.22 1.62 6 -10 -5 2.82 1.32 -6 10 5 0.97 1.24 -6 10 5 1.08 1.48 -6 10 5 2.81 2.00 -6 10 5 1.67 1.22 -6 10 5 2.06 1.49 -6 10 5 1.61 1.34 -6 10 5 -0.08 1.20 -7 6 -10 110.98 5.63 -7 6 -10 114.63 5.76 -7 6 -10 107.29 6.00 7 -6 10 112.74 5.46 7 -6 10 99.03 6.50 7 -6 10 107.49 6.20 7 -6 10 113.86 5.93 6 -10 -8 47.79 4.11 6 -10 -8 53.94 3.54 6 -10 -8 49.48 4.68 6 -10 -8 47.28 4.35 6 -10 -8 51.72 3.95 6 -10 -8 47.48 4.16 6 -10 -8 55.27 3.80 -6 10 8 48.36 3.98 -6 10 8 51.29 4.13 -6 10 8 49.15 4.36 -6 10 8 49.65 3.60 -6 10 8 46.92 4.99 -6 10 8 55.01 4.30 5 -10 9 61.10 5.11 5 -10 9 49.78 4.17 5 -10 9 59.07 4.34 5 -10 9 50.81 4.23 5 -10 9 57.97 4.76 5 -10 9 60.92 5.76 -5 10 -9 56.65 3.89 -5 10 -9 57.54 4.36 -5 10 -9 60.47 4.15 -5 10 -9 58.69 3.91 -5 10 -9 60.11 4.35 -5 10 -9 50.76 4.47 7 5 -10 7.25 2.97 7 5 -10 10.58 3.41 7 5 -10 8.00 2.93 -7 -5 10 12.48 3.00 -7 -5 10 13.59 4.84 -7 -5 10 14.35 3.77 5 -10 6 98.49 5.77 5 -10 6 93.17 5.11 5 -10 6 91.18 6.76 5 -10 6 102.45 5.66 5 -10 6 104.11 5.52 5 -10 6 107.52 5.31 5 -10 6 90.27 5.11 -5 10 -6 96.45 4.78 -5 10 -6 99.29 5.00 -5 10 -6 104.11 4.85 -5 10 -6 93.67 5.23 -5 10 -6 108.93 5.38 -5 10 -6 98.07 5.46 4 5 -10 65.81 3.78 4 5 -10 63.33 4.59 4 5 -10 63.97 5.28 4 5 -10 65.79 4.88 4 5 -10 61.48 4.85 4 5 -10 58.67 4.65 -4 -5 10 67.13 4.86 -4 -5 10 58.63 4.70 -4 -5 10 64.73 5.50 -4 -5 10 58.34 6.73 -4 -5 10 62.89 4.41 -4 -5 10 64.42 4.70 -4 -5 10 64.56 4.96 5 -10 3 132.95 6.15 5 -10 3 127.27 6.58 5 -10 3 134.27 6.11 5 -10 3 136.03 6.14 -10 3 5 137.24 6.07 5 -10 3 132.07 8.05 5 -10 3 126.44 5.61 -10 3 5 138.87 6.85 -10 3 5 141.85 7.08 5 -10 3 127.36 5.98 -5 10 -3 134.41 6.16 -5 10 -3 128.74 6.31 -5 10 -3 128.89 5.79 10 -3 -5 137.05 5.97 10 -3 -5 137.04 7.00 -5 10 -3 129.18 6.22 10 -3 -5 146.31 6.98 -5 10 -3 132.41 6.40 1 5 -10 48.53 4.25 1 5 -10 53.35 3.48 1 5 -10 49.12 3.90 1 5 -10 49.63 4.13 1 5 -10 48.70 4.04 -1 -5 10 49.57 3.70 -1 -5 10 52.33 4.39 -1 -5 10 48.27 4.64 -1 -5 10 49.28 5.60 -1 -5 10 53.04 4.09 -1 -5 10 52.29 4.01 5 -10 0 102.80 5.45 5 -10 0 106.11 4.78 5 -10 0 100.15 5.04 5 -10 0 102.23 6.66 5 -10 0 108.76 5.14 5 -10 0 101.98 5.04 -10 0 5 130.98 7.97 5 -10 0 105.93 4.35 -5 10 0 101.61 5.33 -5 10 0 103.56 5.71 -5 10 0 107.28 5.24 10 0 -5 135.56 6.71 -5 10 0 101.67 4.94 -5 10 0 103.83 5.20 -2 5 -10 32.33 3.07 -2 5 -10 33.78 3.46 -2 5 -10 35.84 3.36 -2 5 -10 34.66 2.71 -2 5 -10 31.62 2.91 -2 5 -10 31.59 3.06 2 -5 10 32.71 3.00 2 -5 10 27.00 3.10 2 -5 10 34.58 3.96 2 -5 10 33.33 3.89 2 -5 10 29.18 2.97 2 -5 10 27.87 3.33 2 -5 10 30.20 3.60 5 -10 -3 197.67 8.51 5 -10 -3 193.94 7.56 5 -10 -3 186.28 7.42 5 -10 -3 196.58 8.06 5 -10 -3 190.24 8.06 5 -10 -3 189.44 8.32 -5 10 3 189.79 8.60 -5 10 3 196.74 8.16 -5 10 3 193.11 8.40 -5 10 3 192.01 8.22 -5 10 3 186.87 9.06 -5 10 3 200.33 8.22 -5 10 3 197.55 7.86 -5 5 -10 4.36 1.67 -5 5 -10 4.35 1.31 -5 5 -10 2.96 1.41 -5 5 -10 3.08 1.77 -5 5 -10 4.62 1.70 5 -5 10 1.96 1.76 5 -5 10 2.10 1.70 5 -5 10 3.39 1.48 5 -5 10 7.11 1.79 5 -5 10 2.93 1.33 5 -5 10 1.17 1.47 5 -10 -6 64.15 4.22 5 -10 -6 70.48 3.72 5 -10 -6 66.42 4.51 -10 -6 5 40.78 7.41 -10 -6 5 46.47 4.89 5 -10 -6 66.37 3.98 5 -10 -6 63.79 4.21 5 -10 -6 69.38 4.16 10 6 -5 43.30 5.87 -5 10 6 65.26 4.04 -5 10 6 58.46 3.89 10 6 -5 46.22 4.87 -5 10 6 66.74 4.30 -5 10 6 64.37 4.45 -5 10 6 66.79 5.24 -5 10 6 68.38 4.01 -8 5 -10 16.30 2.25 -8 5 -10 17.07 2.54 -8 5 -10 23.05 3.10 8 -5 10 18.20 2.19 8 -5 10 19.95 2.82 8 -5 10 18.68 2.97 8 -5 10 13.27 2.59 5 -10 -9 106.35 6.11 5 -10 -9 104.04 5.80 5 -10 -9 98.97 5.86 5 -10 -9 100.50 5.54 5 -10 -9 102.07 6.76 5 -10 -9 98.93 6.36 5 -10 -9 109.49 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99.64 6.15 -6 -4 10 104.67 6.09 -6 -4 10 99.21 8.27 -6 -4 10 91.00 6.03 -6 -4 10 95.92 6.24 -6 -4 10 107.15 7.09 4 -10 5 2.96 1.58 4 -10 5 4.42 1.83 4 -10 5 2.34 1.11 4 -10 5 1.67 1.29 4 -10 5 2.29 1.43 4 -10 5 1.83 2.11 4 -10 5 2.72 1.49 -4 10 -5 2.88 1.55 -4 10 -5 6.01 1.76 -4 10 -5 2.19 1.24 -4 10 -5 3.35 1.59 -4 10 -5 5.23 1.21 -10 4 4 62.13 2.88 -10 4 4 55.27 4.01 -10 4 4 58.06 3.39 -10 4 4 56.17 4.18 10 -4 -4 60.60 4.21 10 -4 -4 54.26 3.73 10 -4 -4 59.99 3.35 3 4 -10 9.37 1.87 3 4 -10 9.96 2.37 3 4 -10 5.43 2.04 3 4 -10 6.39 1.95 3 4 -10 7.21 2.18 3 4 -10 10.84 1.76 -3 -4 10 5.65 1.79 -3 -4 10 5.75 3.06 -3 -4 10 6.70 2.28 -3 -4 10 8.76 2.71 -3 -4 10 10.12 2.26 -3 -4 10 4.43 1.89 4 -10 2 267.87 10.59 4 -10 2 266.21 13.59 4 -10 2 267.94 10.64 4 -10 2 278.36 10.52 4 -10 2 268.13 10.54 4 -10 2 265.43 10.48 4 -10 2 265.24 11.50 -4 10 -2 276.84 10.17 -4 10 -2 270.35 10.83 -4 10 -2 278.72 10.94 -4 10 -2 273.43 10.64 -4 10 -2 276.32 11.26 -10 1 4 0.45 1.17 -10 1 4 0.64 1.58 10 -1 -4 1.59 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3.10 -9 11 4 15.53 2.42 -9 11 4 15.50 2.58 -9 11 4 17.62 2.19 -9 11 4 15.51 2.50 -9 11 4 16.83 2.30 -9 11 4 16.13 2.61 -9 11 4 16.11 2.94 -5 9 -11 4.22 2.19 -5 9 -11 1.29 1.76 -5 9 -11 1.99 2.10 -5 9 -11 3.18 1.97 -5 9 -11 1.44 1.75 -5 9 -11 2.94 2.00 5 -9 11 3.45 2.07 5 -9 11 2.74 2.69 5 -9 11 3.09 2.54 5 -9 11 1.70 2.24 5 -9 11 -0.71 1.68 5 -9 11 1.21 1.68 9 -11 -7 23.32 3.55 9 -11 -7 32.11 3.64 9 -11 -7 30.88 3.23 9 -11 -7 32.62 3.99 9 -11 -7 33.23 3.58 -9 11 7 29.05 3.20 -9 11 7 26.03 3.88 -9 11 7 31.84 3.80 -9 11 7 32.44 3.74 -9 11 7 31.84 3.61 -8 9 -11 11.94 2.82 -8 9 -11 10.07 2.62 -8 9 -11 12.17 2.60 -8 9 -11 11.49 2.43 8 -9 11 10.52 2.40 8 -9 11 10.99 3.07 8 -9 11 10.40 3.06 8 -9 11 10.46 2.67 9 -11 -10 15.61 3.45 9 -11 -10 17.00 3.91 9 -11 -10 16.48 3.53 9 -11 -10 19.52 3.18 9 -11 -10 16.17 3.28 -9 11 10 16.13 3.12 -9 11 10 23.13 3.81 -9 11 10 11.04 3.51 -9 11 10 17.59 3.07 -11 11 8 184.62 10.20 -11 11 8 193.41 9.46 -11 11 8 193.44 8.67 -11 11 8 191.69 9.93 11 -11 -8 189.93 9.16 11 -11 -8 203.67 9.40 11 -11 -8 192.69 8.54 11 -11 -8 190.94 9.66 8 -11 10 83.47 6.22 8 -11 10 78.57 5.30 8 -11 10 90.44 7.02 8 -11 10 74.24 5.95 8 -11 10 80.95 5.59 -8 11 -10 75.12 5.49 -8 11 -10 75.61 5.63 -8 11 -10 82.55 5.36 -11 8 8 13.94 2.59 -11 8 8 13.36 2.22 -11 8 8 10.52 2.64 -11 8 8 11.67 2.65 11 -8 -8 13.77 3.16 11 -8 -8 13.47 2.38 11 -8 -8 11.11 2.35 11 -8 -8 10.63 2.42 8 -11 7 71.21 5.14 8 -11 7 66.08 5.94 8 -11 7 68.96 4.93 8 -11 7 64.86 4.43 8 -11 7 66.60 4.41 -8 11 -7 70.78 4.47 -8 11 -7 65.34 4.62 -8 11 -7 70.90 4.79 -11 5 8 0.83 1.94 -11 5 8 2.60 1.75 -11 5 8 2.07 2.10 11 -5 -8 1.84 1.94 11 -5 -8 3.70 2.03 11 -5 -8 2.90 1.41 11 -5 -8 2.70 2.03 8 -11 4 92.69 4.79 8 -11 4 97.47 5.45 8 -11 4 90.48 5.39 8 -11 4 88.70 4.86 8 -11 4 89.23 5.27 8 -11 4 93.90 4.89 8 -11 4 94.14 4.81 -8 11 -4 89.90 4.98 -8 11 -4 94.92 5.28 -8 11 -4 89.57 4.84 -8 11 -4 92.40 5.11 -8 11 -4 93.27 4.88 3 8 -11 99.59 7.02 3 8 -11 89.59 6.60 3 8 -11 95.61 6.52 3 8 -11 98.53 6.60 -3 -8 11 91.18 6.22 -3 -8 11 88.66 6.52 -3 -8 11 80.57 9.46 -3 -8 11 115.10 7.42 -3 -8 11 86.64 7.50 -3 -8 11 90.55 6.58 -3 -8 11 106.66 6.86 -11 2 8 10.05 3.31 -11 2 8 5.65 2.47 -11 2 8 4.68 2.03 -11 2 8 6.67 2.64 11 -2 -8 9.39 2.76 11 -2 -8 4.87 2.23 11 -2 -8 9.16 2.31 8 -11 1 193.55 7.77 8 -11 1 174.53 7.62 8 -11 1 191.45 8.39 8 -11 1 187.56 7.97 8 -11 1 180.22 7.25 8 -11 1 185.14 8.43 8 -11 1 184.85 7.57 -8 11 -1 183.64 7.79 -8 11 -1 170.23 7.98 -8 11 -1 182.20 7.66 -8 11 -1 188.84 8.04 -8 11 -1 181.72 8.52 0 8 -11 55.05 4.30 0 8 -11 50.88 4.80 0 8 -11 51.29 4.57 0 8 -11 54.24 4.97 0 8 -11 55.81 4.93 0 -8 11 57.39 7.21 0 -8 11 54.62 4.81 0 -8 11 50.34 5.53 0 -8 11 52.60 4.88 0 -8 11 52.28 4.82 0 -8 11 53.52 4.49 -11 -1 8 2.13 2.95 -11 -1 8 1.85 3.43 -11 -1 8 -0.33 1.97 11 1 -8 2.93 2.09 11 1 -8 0.85 2.35 11 1 -8 0.59 2.69 8 -11 -2 93.88 5.12 8 -11 -2 103.88 5.13 8 -11 -2 105.80 5.09 8 -11 -2 90.20 5.64 8 -11 -2 101.39 5.15 8 -11 -2 95.65 4.12 8 -11 -2 103.77 4.98 -8 11 2 98.36 5.12 -8 11 2 96.77 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2.92 -9 8 -11 23.47 3.04 9 -8 11 17.66 3.19 9 -8 11 25.26 3.56 9 -8 11 17.12 2.64 9 -8 11 15.99 3.43 7 -11 6 71.36 4.74 7 -11 6 68.24 4.35 7 -11 6 65.70 4.33 7 -11 6 75.63 5.97 7 -11 6 76.11 4.37 7 -11 6 65.40 4.78 7 -11 6 61.82 4.77 -7 11 -6 70.26 4.37 -7 11 -6 65.42 4.15 -7 11 -6 66.73 4.57 -7 11 -6 70.56 4.57 5 7 -11 0.16 2.65 5 7 -11 0.70 2.19 5 7 -11 0.73 2.55 5 7 -11 1.13 2.51 -5 -7 11 -1.53 2.14 -5 -7 11 0.92 4.23 -5 -7 11 2.38 3.00 -5 -7 11 2.34 2.50 -5 -7 11 0.18 2.58 -5 -7 11 -0.16 2.30 2 7 -11 49.95 4.82 2 7 -11 55.60 4.78 2 7 -11 51.20 5.03 2 7 -11 42.38 4.58 2 7 -11 52.74 4.01 -2 -7 11 51.38 4.87 -2 -7 11 47.28 5.87 -2 -7 11 45.49 6.42 -2 -7 11 49.15 4.42 -2 -7 11 47.33 4.83 -2 -7 11 52.52 5.63 -2 -7 11 47.34 4.75 7 -11 0 68.73 3.94 7 -11 0 65.79 4.19 7 -11 0 68.50 4.55 7 -11 0 67.30 3.83 7 -11 0 70.48 3.98 7 -11 0 71.93 4.08 -7 11 0 69.96 3.98 -7 11 0 67.08 4.23 -7 11 0 69.35 4.11 -7 11 0 64.14 4.06 -7 11 0 67.99 4.77 -1 7 -11 2.17 2.06 -1 7 -11 1.96 1.43 -1 7 -11 2.25 2.49 -1 7 -11 2.77 2.02 -1 7 -11 1.25 1.77 -1 7 -11 3.56 2.15 -1 7 -11 2.13 1.91 1 -7 11 1.62 2.24 1 -7 11 1.22 1.90 1 -7 11 3.13 3.08 1 -7 11 1.41 2.48 1 -7 11 -1.78 1.66 1 -7 11 3.91 2.04 -11 -3 7 21.56 5.39 7 -11 -3 3.83 1.45 7 -11 -3 1.59 1.36 7 -11 -3 1.40 1.67 7 -11 -3 3.04 1.25 7 -11 -3 4.19 1.69 7 -11 -3 1.31 1.43 7 -11 -3 1.75 1.12 -7 11 3 6.02 1.79 -7 11 3 -0.02 1.53 -7 11 3 3.00 1.46 -7 11 3 4.14 1.64 11 3 -7 16.39 3.51 -7 11 3 3.64 1.47 -7 11 3 2.61 1.48 11 3 -7 21.61 4.25 -7 11 3 4.60 2.20 -4 7 -11 25.59 3.12 -4 7 -11 26.26 3.03 -4 7 -11 27.51 3.17 -4 7 -11 26.76 3.30 4 -7 11 23.86 3.16 4 -7 11 26.60 3.67 4 -7 11 28.02 3.99 4 -7 11 23.34 3.09 4 -7 11 30.01 3.24 4 -7 11 28.25 3.93 7 -11 -6 42.30 3.76 7 -11 -6 45.04 3.39 7 -11 -6 45.44 4.43 7 -11 -6 43.82 3.38 7 -11 -6 48.90 4.19 7 -11 -6 44.68 4.00 -7 11 6 48.21 3.41 -7 11 6 45.49 3.90 -7 11 6 46.62 4.20 -7 11 6 43.12 3.56 -7 11 6 45.13 4.79 -7 11 6 45.99 3.73 -7 7 -11 7.10 2.17 -7 7 -11 4.56 1.98 -7 7 -11 6.49 1.97 7 -7 11 7.23 2.01 7 -7 11 6.00 2.29 7 -7 11 5.89 2.64 7 -7 11 3.94 1.92 7 -11 -9 4.64 2.22 7 -11 -9 4.22 2.25 7 -11 -9 6.13 2.80 7 -11 -9 2.35 1.88 7 -11 -9 4.23 2.42 -7 11 9 1.44 2.16 -7 11 9 7.45 2.51 -7 11 9 2.09 2.66 -7 11 9 4.26 2.40 -7 11 9 3.61 2.12 -10 7 -11 -0.50 2.05 -10 7 -11 0.82 1.70 -10 7 -11 -0.03 1.87 10 -7 11 0.64 2.12 10 -7 11 -0.99 1.56 10 -7 11 -0.57 2.01 10 -7 11 -0.19 2.17 6 -11 11 15.69 4.10 6 -11 11 11.56 2.82 6 -11 11 10.45 3.31 6 -11 11 11.36 3.28 6 -11 11 10.76 2.85 -6 11 -11 7.89 2.73 -6 11 -11 11.38 2.59 -6 11 -11 11.54 2.61 -6 11 -11 11.51 3.05 -11 10 6 8.47 2.31 -11 10 6 10.48 2.69 -11 10 6 8.32 2.06 11 -10 -6 7.68 2.26 11 -10 -6 9.65 1.94 11 -10 -6 10.83 2.81 11 -10 -6 6.57 2.07 6 -11 8 2.68 1.81 6 -11 8 1.60 1.79 6 -11 8 3.79 2.39 6 -11 8 2.14 2.52 6 -11 8 1.17 1.84 6 -11 8 2.92 2.06 6 -11 8 3.33 1.80 -6 11 -8 3.79 1.65 -6 11 -8 1.05 1.81 -6 11 -8 3.45 1.99 -6 11 -8 1.07 1.58 -6 11 -8 1.73 1.80 -11 7 6 14.65 2.65 -11 7 6 18.39 2.59 -11 7 6 11.96 2.39 -11 7 6 19.02 2.16 11 -7 -6 19.43 2.48 11 -7 -6 17.76 2.45 11 -7 -6 18.06 2.85 6 -11 5 60.96 4.17 6 -11 5 56.29 4.37 6 -11 5 60.72 4.00 6 -11 5 64.77 4.27 6 -11 5 62.45 4.07 6 -11 5 63.05 4.39 6 -11 5 60.04 5.59 -6 11 -5 60.49 4.09 -6 11 -5 61.69 3.79 -6 11 -5 62.93 4.19 -6 11 -5 67.11 4.44 6 -11 2 0.59 1.71 6 -11 2 0.89 1.31 6 -11 2 1.10 1.19 6 -11 2 -0.50 1.20 6 -11 2 1.06 1.04 6 -11 2 -1.09 1.14 6 -11 2 0.45 1.25 -6 11 -2 1.46 1.33 -6 11 -2 -0.42 1.53 -6 11 -2 1.63 1.35 -6 11 -2 1.14 1.26 -6 11 -2 0.88 1.51 1 6 -11 18.20 1.99 1 6 -11 16.82 2.89 1 6 -11 18.45 3.08 1 6 -11 11.53 2.76 1 6 -11 17.16 2.95 1 6 -11 14.99 2.38 -1 -6 11 15.07 2.61 -1 -6 11 13.91 2.90 -1 -6 11 13.07 2.61 -1 -6 11 14.11 3.61 -1 -6 11 19.09 4.40 -1 -6 11 13.68 2.87 -1 -6 11 17.32 3.55 6 -11 -1 25.90 2.54 6 -11 -1 22.67 1.88 6 -11 -1 24.51 2.74 6 -11 -1 25.59 2.62 6 -11 -1 24.38 2.19 6 -11 -1 19.55 2.33 -6 11 1 23.48 2.59 -6 11 1 24.08 2.77 -6 11 1 21.79 2.62 -6 11 1 27.33 2.75 -6 11 1 21.70 3.05 -6 11 1 25.19 2.69 -2 6 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