# Electronic Supplementary Material (ESI) for Dalton Transactions # This journal is © The Royal Society of Chemistry 2014 ####################################################################### # # Cambridge Crystallographic Data Centre # CCDC # ####################################################################### # # This CIF contains data from an original supplementary publication # deposited with the CCDC, and may include chemical, crystal, # experimental, refinement, atomic coordinates, # anisotropic displacement parameters and molecular geometry data, # as required by the journal to which it was submitted. # # This CIF is provided on the understanding that it is used for bona # fide research purposes only. It may contain copyright material # of the CCDC or of third parties, and may not be copied or further # disseminated in any form, whether machine-readable or not, # except for the purpose of generating routine backup copies # on your local computer system. # # For further information on the CCDC, data deposition and # data retrieval see: # www.ccdc.cam.ac.uk # # Bona fide researchers may freely download Mercury and enCIFer # from this site to visualise CIF-encoded structures and # to carry out CIF format checking respectively. # data_FINAL _audit_creation_method SHELXL-2013 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C20 H40 Cl Ir N P2, 2(C10 H20 O5), K' _chemical_formula_sum 'C40 H80 Cl Ir K N O10 P2' _chemical_formula_weight 1063.74 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0015 0.0009 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0030 0.0019 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0056 0.0036 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.0667 0.0580 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.0998 0.0984 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' K K 0.1399 0.1562 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ir Ir -0.5977 5.4269 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system orthorhombic _space_group_IT_number 60 _space_group_name_H-M_alt 'P b c n' _space_group_name_Hall '-P 2n 2ab' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' _cell_length_a 20.279(2) _cell_length_b 18.474(2) _cell_length_c 26.694(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 10000.5(18) _cell_formula_units_Z 8 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9861 _cell_measurement_theta_min 2.2595 _cell_measurement_theta_max 19.4255 _exptl_crystal_description block _exptl_crystal_colour red _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.413 _exptl_crystal_F_000 4400 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.103 _exptl_crystal_size_mid 0.103 _exptl_crystal_size_min 0.097 _exptl_absorpt_coefficient_mu 1.586 _shelx_estimated_absorpt_T_min 0.854 _shelx_estimated_absorpt_T_max 0.861 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.6855 _exptl_absorpt_correction_T_max 0.7444 _exptl_absorpt_process_details SADABS-2012/1 _exptl_special_details ; ? ; _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.56086 _diffrn_radiation_type AgK\a _diffrn_source 'INCOATEC Ag Microsource' _diffrn_measurement_device_type 'Bruker Smart APEX II Quazar' _diffrn_measurement_method 'omega and phi scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 156766 _diffrn_reflns_av_unetI/netI 0.0406 _diffrn_reflns_av_R_equivalents 0.0808 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_h_max 24 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_l_min -32 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_theta_min 1.684 _diffrn_reflns_theta_max 19.796 _diffrn_reflns_theta_full 19.665 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 9180 _reflns_number_gt 6741 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'APEX2 v2012.2' _computing_cell_refinement 'SAINT V7.68A' _computing_data_reduction 'SAINT V7.68A' _computing_structure_solution 'SHELXS-2013 (Sheldrick, 2013)' _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_molecular_graphics 'XP Version 5.1' _computing_publication_material 'XP Version 5.1' _refine_special_details ; ? ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0081P)^2^+13.4684P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 9180 _refine_ls_number_parameters 539 _refine_ls_number_restraints 156 _refine_ls_R_factor_all 0.0492 _refine_ls_R_factor_gt 0.0261 _refine_ls_wR_factor_ref 0.0483 _refine_ls_wR_factor_gt 0.0420 _refine_ls_goodness_of_fit_ref 1.000 _refine_ls_restrained_S_all 1.004 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ir1 Ir 0.21974(2) 0.27765(2) 0.37886(2) 0.01669(4) Uani 1 1 d . . . . . K1 K 0.66233(3) 0.50770(3) 0.37257(3) 0.01833(15) Uani 1 1 d . . . . . Cl1 Cl 0.16788(4) 0.16091(4) 0.37911(3) 0.0314(2) Uani 1 1 d . . . . . P1 P 0.12682(4) 0.34590(4) 0.38709(3) 0.01818(19) Uani 1 1 d . . . . . O1 O 0.68954(11) 0.44418(12) 0.46712(8) 0.0294(6) Uani 1 1 d . . . . . O2 O 0.62183(11) 0.58021(12) 0.46160(8) 0.0294(6) Uani 1 1 d . . . . . O3 O 0.51986(11) 0.53530(12) 0.39661(9) 0.0301(6) Uani 1 1 d . . . . . O4 O 0.55711(10) 0.44887(12) 0.31573(8) 0.0254(5) Uani 1 1 d . . . . . O5 O 0.62545(10) 0.36130(11) 0.38967(8) 0.0242(5) Uani 1 1 d . . . . . O7 O 0.77043(11) 0.59824(12) 0.39601(8) 0.0315(6) Uani 1 1 d . . . . . O8 O 0.65153(11) 0.65769(11) 0.35135(8) 0.0284(6) Uani 1 1 d . . . . . O9 O 0.68841(10) 0.56988(11) 0.27232(8) 0.0240(5) Uani 1 1 d . . . . . O10 O 0.71702(10) 0.42396(11) 0.29344(7) 0.0213(5) Uani 1 1 d . . . . . O11 O 0.79287(10) 0.44439(12) 0.38185(9) 0.0309(6) Uani 1 1 d . . . . . N1 N 0.26279(12) 0.37683(12) 0.37710(9) 0.0168(6) Uani 1 1 d . . . . . C1 C 0.15930(16) 0.43560(16) 0.38353(11) 0.0204(7) Uani 1 1 d . . . . . H1 H 0.1323 0.4776 0.3842 0.024 Uiso 1 1 calc R U . . . C2 C 0.22561(15) 0.43860(15) 0.37985(11) 0.0189(7) Uani 1 1 d . . . . . H2 H 0.2469 0.4844 0.3791 0.023 Uiso 1 1 calc R U . . . C3 C 0.32972(15) 0.38368(16) 0.37232(11) 0.0204(7) Uani 1 1 d . . . . . H3 H 0.3487 0.4306 0.3708 0.024 Uiso 1 1 calc R U . . . C4 C 0.36930(15) 0.32501(16) 0.36970(12) 0.0232(8) Uani 1 1 d . . . . . H4 H 0.4159 0.3283 0.3672 0.028 Uiso 1 1 calc R U . . . P2 P 0.32623(4) 0.24028(4) 0.37137(3) 0.0204(2) Uani 1 1 d D U . . . C5 C 0.36265(17) 0.19055(17) 0.42648(13) 0.0308(9) Uani 1 1 d D U . . . C6 C 0.4348(3) 0.1662(7) 0.4191(4) 0.045(2) Uani 0.75(3) 1 d D U P A 1 H6A H 0.4367 0.1291 0.3928 0.068 Uiso 0.75(3) 1 calc R U P A 1 H6B H 0.4517 0.1461 0.4505 0.068 Uiso 0.75(3) 1 calc R U P A 1 H6C H 0.4617 0.2078 0.4092 0.068 Uiso 0.75(3) 1 calc R U P A 1 C7 C 0.3208(4) 0.1226(3) 0.4373(4) 0.0268(18) Uani 0.75(3) 1 d D U P A 1 H7A H 0.2743 0.1364 0.4406 0.040 Uiso 0.75(3) 1 calc R U P A 1 H7B H 0.3358 0.1001 0.4686 0.040 Uiso 0.75(3) 1 calc R U P A 1 H7C H 0.3256 0.0880 0.4097 0.040 Uiso 0.75(3) 1 calc R U P A 1 C8 C 0.3568(6) 0.2412(4) 0.4708(3) 0.045(2) Uani 0.75(3) 1 d D U P A 1 H8A H 0.3671 0.2148 0.5017 0.068 Uiso 0.75(3) 1 calc R U P A 1 H8B H 0.3117 0.2601 0.4727 0.068 Uiso 0.75(3) 1 calc R U P A 1 H8C H 0.3878 0.2815 0.4668 0.068 Uiso 0.75(3) 1 calc R U P A 1 C6A C 0.4373(6) 0.1978(19) 0.4307(11) 0.049(6) Uani 0.25(3) 1 d D U P A 2 H6A1 H 0.4493 0.2492 0.4319 0.073 Uiso 0.25(3) 1 calc R U P A 2 H6A2 H 0.4582 0.1751 0.4016 0.073 Uiso 0.25(3) 1 calc R U P A 2 H6A3 H 0.4524 0.1738 0.4614 0.073 Uiso 0.25(3) 1 calc R U P A 2 C7A C 0.3369(17) 0.1144(9) 0.4318(13) 0.041(6) Uani 0.25(3) 1 d D U P A 2 H7A1 H 0.2890 0.1143 0.4272 0.061 Uiso 0.25(3) 1 calc R U P A 2 H7A2 H 0.3476 0.0961 0.4653 0.061 Uiso 0.25(3) 1 calc R U P A 2 H7A3 H 0.3575 0.0834 0.4065 0.061 Uiso 0.25(3) 1 calc R U P A 2 C8A C 0.3355(17) 0.2355(16) 0.4727(8) 0.045(2) Uani 0.25(3) 1 d D U P A 2 H8A1 H 0.3448 0.2870 0.4676 0.068 Uiso 0.25(3) 1 calc R U P A 2 H8A2 H 0.3573 0.2190 0.5035 0.068 Uiso 0.25(3) 1 calc R U P A 2 H8A3 H 0.2878 0.2282 0.4757 0.068 Uiso 0.25(3) 1 calc R U P A 2 C9 C 0.35139(16) 0.19594(18) 0.31030(13) 0.0261(8) Uani 1 1 d . . . . . C10 C 0.42494(17) 0.1993(2) 0.29779(15) 0.0482(11) Uani 1 1 d . . . . . H10A H 0.4496 0.1692 0.3215 0.072 Uiso 1 1 calc R U . . . H10B H 0.4403 0.2495 0.3001 0.072 Uiso 1 1 calc R U . . . H10C H 0.4321 0.1813 0.2637 0.072 Uiso 1 1 calc R U . . . C11 C 0.32684(19) 0.11822(18) 0.30778(14) 0.0391(10) Uani 1 1 d . . . . . H11A H 0.2806 0.1164 0.3183 0.059 Uiso 1 1 calc R U . . . H11B H 0.3535 0.0878 0.3300 0.059 Uiso 1 1 calc R U . . . H11C H 0.3306 0.1004 0.2733 0.059 Uiso 1 1 calc R U . . . C12 C 0.31529(19) 0.2404(2) 0.27040(13) 0.0396(10) Uani 1 1 d . . . . . H12A H 0.3299 0.2909 0.2721 0.059 Uiso 1 1 calc R U . . . H12B H 0.2677 0.2380 0.2764 0.059 Uiso 1 1 calc R U . . . H12C H 0.3252 0.2207 0.2371 0.059 Uiso 1 1 calc R U . . . C13 C 0.08453(17) 0.34482(18) 0.45012(12) 0.0267(8) Uani 1 1 d . . . . . C14 C 0.1414(2) 0.3514(2) 0.48765(13) 0.0526(12) Uani 1 1 d . . . . . H14A H 0.1238 0.3500 0.5218 0.079 Uiso 1 1 calc R U . . . H14B H 0.1646 0.3972 0.4823 0.079 Uiso 1 1 calc R U . . . H14C H 0.1721 0.3110 0.4829 0.079 Uiso 1 1 calc R U . . . C15 C 0.05010(17) 0.27241(18) 0.45871(13) 0.0324(9) Uani 1 1 d . . . . . H15A H 0.0377 0.2681 0.4941 0.049 Uiso 1 1 calc R U . . . H15B H 0.0801 0.2329 0.4498 0.049 Uiso 1 1 calc R U . . . H15C H 0.0104 0.2698 0.4378 0.049 Uiso 1 1 calc R U . . . C16 C 0.0368(2) 0.4073(2) 0.45910(15) 0.0568(13) Uani 1 1 d . . . . . H16A H 0.0248 0.4090 0.4946 0.085 Uiso 1 1 calc R U . . . H16B H -0.0030 0.4001 0.4389 0.085 Uiso 1 1 calc R U . . . H16C H 0.0580 0.4530 0.4496 0.085 Uiso 1 1 calc R U . . . C17 C 0.06421(15) 0.34264(18) 0.33522(12) 0.0228(8) Uani 1 1 d . . . . . C18 C 0.0269(2) 0.2707(2) 0.33466(14) 0.0489(12) Uani 1 1 d . . . . . H18A H -0.0054 0.2701 0.3619 0.073 Uiso 1 1 calc R U . . . H18B H 0.0581 0.2308 0.3391 0.073 Uiso 1 1 calc R U . . . H18C H 0.0041 0.2652 0.3025 0.073 Uiso 1 1 calc R U . . . C19 C 0.01596(19) 0.4062(2) 0.33430(16) 0.0545(13) Uani 1 1 d . . . . . H19A H 0.0406 0.4518 0.3360 0.082 Uiso 1 1 calc R U . . . H19B H -0.0139 0.4028 0.3631 0.082 Uiso 1 1 calc R U . . . H19C H -0.0097 0.4048 0.3032 0.082 Uiso 1 1 calc R U . . . C20 C 0.10551(17) 0.3464(2) 0.28748(12) 0.0347(9) Uani 1 1 d . . . . . H20A H 0.1386 0.3077 0.2879 0.052 Uiso 1 1 calc R U . . . H20B H 0.1277 0.3935 0.2857 0.052 Uiso 1 1 calc R U . . . H20C H 0.0768 0.3404 0.2583 0.052 Uiso 1 1 calc R U . . . C21 C 0.6585(2) 0.4754(2) 0.50976(13) 0.0422(10) Uani 1 1 d . . . . . H21A H 0.6823 0.4615 0.5407 0.051 Uiso 1 1 calc R U . . . H21B H 0.6124 0.4583 0.5124 0.051 Uiso 1 1 calc R U . . . C22 C 0.6601(2) 0.55670(19) 0.50300(13) 0.0399(10) Uani 1 1 d . . . . . H22A H 0.6434 0.5801 0.5338 0.048 Uiso 1 1 calc R U . . . H22B H 0.7064 0.5724 0.4981 0.048 Uiso 1 1 calc R U . . . C23 C 0.55358(18) 0.5891(2) 0.47243(14) 0.0375(10) Uani 1 1 d . . . . . H23A H 0.5471 0.6312 0.4948 0.045 Uiso 1 1 calc R U . . . H23B H 0.5365 0.5454 0.4896 0.045 Uiso 1 1 calc R U . . . C24 C 0.51750(18) 0.60050(19) 0.42473(15) 0.0372(10) Uani 1 1 d . . . . . H24A H 0.4711 0.6138 0.4317 0.045 Uiso 1 1 calc R U . . . H24B H 0.5381 0.6403 0.4055 0.045 Uiso 1 1 calc R U . . . C25 C 0.48900(17) 0.54225(19) 0.34901(14) 0.0349(10) Uani 1 1 d . . . . . H25A H 0.5130 0.5779 0.3281 0.042 Uiso 1 1 calc R U . . . H25B H 0.4429 0.5590 0.3531 0.042 Uiso 1 1 calc R U . . . C26 C 0.49030(16) 0.4697(2) 0.32481(14) 0.0361(10) Uani 1 1 d . . . . . H26A H 0.4688 0.4337 0.3469 0.043 Uiso 1 1 calc R U . . . H26B H 0.4657 0.4713 0.2928 0.043 Uiso 1 1 calc R U . . . C27 C 0.56572(16) 0.37224(17) 0.31307(13) 0.0273(8) Uani 1 1 d . . . . . H27A H 0.6072 0.3615 0.2950 0.033 Uiso 1 1 calc R U . . . H27B H 0.5289 0.3510 0.2936 0.033 Uiso 1 1 calc R U . . . C28 C 0.56809(16) 0.33725(18) 0.36368(13) 0.0306(9) Uani 1 1 d . . . . . H28A H 0.5281 0.3502 0.3830 0.037 Uiso 1 1 calc R U . . . H28B H 0.5693 0.2840 0.3599 0.037 Uiso 1 1 calc R U . . . C29 C 0.62439(17) 0.34069(18) 0.44071(12) 0.0287(9) Uani 1 1 d . . . . . H29A H 0.6216 0.2873 0.4434 0.034 Uiso 1 1 calc R U . . . H29B H 0.5852 0.3617 0.4573 0.034 Uiso 1 1 calc R U . . . C30 C 0.68581(17) 0.36692(18) 0.46613(13) 0.0303(9) Uani 1 1 d . . . . . H30A H 0.6868 0.3483 0.5009 0.036 Uiso 1 1 calc R U . . . H30B H 0.7248 0.3475 0.4483 0.036 Uiso 1 1 calc R U . . . C31 C 0.76423(18) 0.67225(18) 0.38136(14) 0.0393(10) Uani 1 1 d . . . . . H31A H 0.7791 0.6783 0.3463 0.047 Uiso 1 1 calc R U . . . H31B H 0.7922 0.7030 0.4031 0.047 Uiso 1 1 calc R U . . . C32 C 0.69326(18) 0.69490(18) 0.38603(14) 0.0373(10) Uani 1 1 d . . . . . H32A H 0.6779 0.6851 0.4206 0.045 Uiso 1 1 calc R U . . . H32B H 0.6898 0.7477 0.3801 0.045 Uiso 1 1 calc R U . . . C33 C 0.65572(18) 0.68497(18) 0.30155(13) 0.0318(9) Uani 1 1 d . . . . . H33A H 0.7006 0.7041 0.2953 0.038 Uiso 1 1 calc R U . . . H33B H 0.6238 0.7250 0.2971 0.038 Uiso 1 1 calc R U . . . C34 C 0.64081(17) 0.62544(18) 0.26509(13) 0.0288(9) Uani 1 1 d . . . . . H34A H 0.5959 0.6063 0.2710 0.035 Uiso 1 1 calc R U . . . H34B H 0.6431 0.6440 0.2303 0.035 Uiso 1 1 calc R U . . . C35 C 0.68271(17) 0.51354(18) 0.23600(12) 0.0254(8) Uani 1 1 d . . . . . H35A H 0.6893 0.5334 0.2019 0.031 Uiso 1 1 calc R U . . . H35B H 0.6382 0.4916 0.2376 0.031 Uiso 1 1 calc R U . . . C36 C 0.73390(16) 0.45780(17) 0.24698(12) 0.0244(8) Uani 1 1 d . . . . . H36A H 0.7352 0.4214 0.2198 0.029 Uiso 1 1 calc R U . . . H36B H 0.7779 0.4808 0.2495 0.029 Uiso 1 1 calc R U . . . C37 C 0.76545(15) 0.37444(17) 0.31085(12) 0.0225(8) Uani 1 1 d . . . . . H37A H 0.7839 0.3476 0.2820 0.027 Uiso 1 1 calc R U . . . H37B H 0.7444 0.3389 0.3335 0.027 Uiso 1 1 calc R U . . . C38 C 0.82036(16) 0.41181(19) 0.33815(13) 0.0284(9) Uani 1 1 d . . . . . H38A H 0.8548 0.3764 0.3476 0.034 Uiso 1 1 calc R U . . . H38B H 0.8406 0.4492 0.3165 0.034 Uiso 1 1 calc R U . . . C39 C 0.83577(18) 0.4933(2) 0.40658(14) 0.0396(10) Uani 1 1 d . . . . . H39A H 0.8815 0.4748 0.4042 0.048 Uiso 1 1 calc R U . . . H39B H 0.8238 0.4953 0.4425 0.048 Uiso 1 1 calc R U . . . C40 C 0.83340(18) 0.5685(2) 0.38516(15) 0.0408(10) Uani 1 1 d . . . . . H40A H 0.8684 0.5988 0.4003 0.049 Uiso 1 1 calc R U . . . H40B H 0.8405 0.5670 0.3485 0.049 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ir1 0.01778(7) 0.01589(6) 0.01639(7) 0.00073(6) -0.00184(6) -0.00445(5) K1 0.0184(4) 0.0193(3) 0.0173(4) 0.0003(3) 0.0001(3) -0.0004(3) Cl1 0.0307(5) 0.0223(4) 0.0413(6) -0.0020(4) 0.0043(4) -0.0093(4) P1 0.0193(5) 0.0203(4) 0.0150(5) -0.0009(4) 0.0014(4) -0.0043(4) O1 0.0408(15) 0.0277(14) 0.0197(14) -0.0007(11) 0.0000(11) 0.0021(11) O2 0.0340(15) 0.0299(13) 0.0244(14) -0.0022(11) 0.0026(12) 0.0029(11) O3 0.0262(14) 0.0269(14) 0.0373(16) -0.0008(11) 0.0009(12) 0.0060(11) O4 0.0162(13) 0.0317(13) 0.0284(14) 0.0015(11) -0.0044(10) -0.0010(10) O5 0.0191(13) 0.0292(13) 0.0242(14) 0.0047(11) -0.0016(10) -0.0050(10) O7 0.0316(16) 0.0336(14) 0.0294(14) -0.0030(11) 0.0001(11) -0.0079(12) O8 0.0346(15) 0.0248(13) 0.0259(14) 0.0041(11) 0.0073(11) -0.0005(11) O9 0.0240(13) 0.0258(13) 0.0223(14) 0.0015(11) -0.0029(10) 0.0022(10) O10 0.0217(13) 0.0259(12) 0.0163(12) 0.0026(10) 0.0024(10) -0.0003(11) O11 0.0233(13) 0.0437(14) 0.0257(14) -0.0064(12) -0.0035(11) 0.0043(11) N1 0.0175(15) 0.0180(13) 0.0148(14) 0.0020(12) -0.0007(12) -0.0051(11) C1 0.026(2) 0.0164(16) 0.0189(19) 0.0009(14) 0.0000(16) -0.0008(14) C2 0.0258(19) 0.0168(15) 0.0141(17) 0.0012(14) -0.0008(16) -0.0057(14) C3 0.0235(19) 0.0213(17) 0.0164(19) 0.0029(15) -0.0027(15) -0.0099(14) C4 0.0152(18) 0.0256(18) 0.029(2) 0.0018(16) -0.0057(15) -0.0069(14) P2 0.0207(5) 0.0178(4) 0.0229(5) 0.0013(4) -0.0076(4) -0.0035(3) C5 0.038(2) 0.0221(17) 0.032(2) 0.0056(15) -0.0155(16) -0.0025(15) C6 0.038(3) 0.038(5) 0.059(5) 0.020(4) -0.024(3) -0.003(3) C7 0.034(4) 0.019(3) 0.027(4) -0.001(2) -0.001(3) 0.009(2) C8 0.077(6) 0.031(3) 0.028(2) 0.0001(18) -0.026(3) -0.005(3) C6A 0.049(6) 0.044(13) 0.053(12) 0.007(9) -0.022(5) 0.001(5) C7A 0.068(14) 0.027(6) 0.027(12) 0.006(6) -0.012(10) -0.005(6) C8A 0.077(6) 0.031(3) 0.028(2) 0.0001(18) -0.026(3) -0.005(3) C9 0.021(2) 0.0291(19) 0.029(2) 0.0012(16) -0.0027(16) -0.0018(15) C10 0.027(2) 0.061(3) 0.056(3) -0.020(2) 0.008(2) -0.004(2) C11 0.053(3) 0.034(2) 0.030(2) -0.0106(18) 0.0077(19) -0.0129(19) C12 0.045(3) 0.049(3) 0.025(2) 0.0015(19) -0.0013(18) 0.0033(19) C13 0.036(2) 0.027(2) 0.017(2) -0.0008(16) 0.0073(16) -0.0073(17) C14 0.064(3) 0.075(3) 0.018(2) -0.006(2) 0.003(2) -0.028(3) C15 0.040(2) 0.033(2) 0.024(2) 0.0027(18) 0.0090(17) -0.0059(18) C16 0.088(4) 0.036(2) 0.047(3) 0.005(2) 0.046(3) 0.011(2) C17 0.020(2) 0.0301(19) 0.0180(19) -0.0032(15) 0.0005(15) -0.0020(15) C18 0.053(3) 0.060(3) 0.034(2) 0.009(2) -0.019(2) -0.033(2) C19 0.036(3) 0.068(3) 0.059(3) -0.024(2) -0.022(2) 0.021(2) C20 0.035(2) 0.050(2) 0.019(2) 0.0033(18) -0.0044(17) 0.0013(19) C21 0.066(3) 0.041(2) 0.019(2) 0.0002(18) -0.001(2) 0.012(2) C22 0.058(3) 0.039(2) 0.023(2) -0.0086(18) -0.006(2) 0.007(2) C23 0.042(3) 0.030(2) 0.040(3) -0.0084(18) 0.020(2) 0.0000(18) C24 0.030(2) 0.029(2) 0.052(3) -0.0046(19) 0.018(2) 0.0060(17) C25 0.021(2) 0.039(2) 0.045(3) 0.0118(19) -0.0010(18) 0.0092(17) C26 0.017(2) 0.047(3) 0.044(3) 0.003(2) -0.0062(17) 0.0014(18) C27 0.021(2) 0.029(2) 0.032(2) -0.0020(17) -0.0066(16) -0.0067(16) C28 0.024(2) 0.0296(19) 0.038(2) 0.0061(17) -0.0051(17) -0.0055(16) C29 0.034(2) 0.0258(19) 0.026(2) 0.0085(16) 0.0035(17) 0.0029(17) C30 0.036(2) 0.029(2) 0.026(2) 0.0058(17) -0.0059(17) 0.0064(17) C31 0.045(3) 0.034(2) 0.038(2) -0.0021(19) -0.005(2) -0.0181(18) C32 0.059(3) 0.0224(18) 0.031(2) -0.0037(17) 0.0063(19) -0.0081(18) C33 0.034(2) 0.027(2) 0.034(2) 0.0118(17) 0.0079(18) 0.0039(17) C34 0.026(2) 0.033(2) 0.027(2) 0.0103(17) -0.0018(16) 0.0048(17) C35 0.030(2) 0.0301(19) 0.017(2) 0.0002(16) -0.0026(16) -0.0041(17) C36 0.030(2) 0.0269(19) 0.0162(19) -0.0034(15) 0.0033(15) -0.0034(15) C37 0.023(2) 0.0230(18) 0.0218(19) 0.0026(15) 0.0029(15) 0.0047(15) C38 0.023(2) 0.034(2) 0.028(2) -0.0007(17) 0.0015(17) 0.0059(16) C39 0.025(2) 0.059(3) 0.035(2) -0.013(2) -0.0099(18) 0.0071(19) C40 0.030(2) 0.054(3) 0.038(3) -0.016(2) -0.0023(19) -0.0137(19) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ir1 N1 2.030(2) . ? Ir1 P2 2.2760(9) . ? Ir1 P1 2.2779(9) . ? Ir1 Cl1 2.3995(8) . ? K1 O7 2.828(2) . ? K1 O4 2.835(2) . ? K1 O8 2.837(2) . ? K1 O1 2.838(2) . ? K1 O5 2.843(2) . ? K1 O10 2.843(2) . ? K1 O2 2.849(2) . ? K1 O11 2.905(2) . ? K1 O9 2.960(2) . ? K1 O3 3.003(2) . ? K1 C32 3.533(3) . ? P1 C1 1.786(3) . ? P1 C17 1.879(3) . ? P1 C13 1.889(3) . ? O1 C21 1.423(4) . ? O1 C30 1.430(4) . ? O2 C22 1.419(4) . ? O2 C23 1.423(4) . ? O3 C24 1.420(4) . ? O3 C25 1.422(4) . ? O4 C27 1.428(4) . ? O4 C26 1.429(4) . ? O5 C29 1.415(4) . ? O5 C28 1.425(4) . ? O7 C40 1.420(4) . ? O7 C31 1.428(4) . ? O8 C33 1.424(4) . ? O8 C32 1.430(4) . ? O9 C34 1.422(4) . ? O9 C35 1.427(4) . ? O10 C37 1.420(3) . ? O10 C36 1.430(4) . ? O11 C39 1.417(4) . ? O11 C38 1.426(4) . ? N1 C3 1.369(4) . ? N1 C2 1.370(4) . ? C1 C2 1.349(4) . ? C1 H1 0.9500 . ? C2 H2 0.9500 . ? C3 C4 1.350(4) . ? C3 H3 0.9500 . ? C4 P2 1.793(3) . ? C4 H4 0.9500 . ? P2 C5 1.885(3) . ? P2 C9 1.894(3) . ? C5 C7A 1.507(12) . ? C5 C8 1.513(6) . ? C5 C6A 1.524(12) . ? C5 C6 1.543(6) . ? C5 C7 1.543(6) . ? C5 C8A 1.586(12) . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C6A H6A1 0.9800 . ? C6A H6A2 0.9800 . ? C6A H6A3 0.9800 . ? C7A H7A1 0.9800 . ? C7A H7A2 0.9800 . ? C7A H7A3 0.9800 . ? C8A H8A1 0.9800 . ? C8A H8A2 0.9800 . ? C8A H8A3 0.9800 . ? C9 C11 1.521(4) . ? C9 C10 1.530(5) . ? C9 C12 1.531(5) . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C13 C16 1.525(5) . ? C13 C15 1.526(4) . ? C13 C14 1.532(5) . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 C20 1.526(4) . ? C17 C19 1.529(5) . ? C17 C18 1.529(5) . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 C22 1.513(5) . ? C21 H21A 0.9900 . ? C21 H21B 0.9900 . ? C22 H22A 0.9900 . ? C22 H22B 0.9900 . ? C23 C24 1.484(5) . ? C23 H23A 0.9900 . ? C23 H23B 0.9900 . ? C24 H24A 0.9900 . ? C24 H24B 0.9900 . ? C25 C26 1.489(5) . ? C25 H25A 0.9900 . ? C25 H25B 0.9900 . ? C26 H26A 0.9900 . ? C26 H26B 0.9900 . ? C27 C28 1.498(4) . ? C27 H27A 0.9900 . ? C27 H27B 0.9900 . ? C28 H28A 0.9900 . ? C28 H28B 0.9900 . ? C29 C30 1.499(5) . ? C29 H29A 0.9900 . ? C29 H29B 0.9900 . ? C30 H30A 0.9900 . ? C30 H30B 0.9900 . ? C31 C32 1.504(5) . ? C31 H31A 0.9900 . ? C31 H31B 0.9900 . ? C32 H32A 0.9900 . ? C32 H32B 0.9900 . ? C33 C34 1.499(5) . ? C33 H33A 0.9900 . ? C33 H33B 0.9900 . ? C34 H34A 0.9900 . ? C34 H34B 0.9900 . ? C35 C36 1.491(4) . ? C35 H35A 0.9900 . ? C35 H35B 0.9900 . ? C36 H36A 0.9900 . ? C36 H36B 0.9900 . ? C37 C38 1.499(4) . ? C37 H37A 0.9900 . ? C37 H37B 0.9900 . ? C38 H38A 0.9900 . ? C38 H38B 0.9900 . ? C39 C40 1.504(5) . ? C39 H39A 0.9900 . ? C39 H39B 0.9900 . ? C40 H40A 0.9900 . ? C40 H40B 0.9900 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 Ir1 P2 82.16(7) . . ? N1 Ir1 P1 81.86(7) . . ? P2 Ir1 P1 164.00(3) . . ? N1 Ir1 Cl1 178.72(7) . . ? P2 Ir1 Cl1 98.25(3) . . ? P1 Ir1 Cl1 97.74(3) . . ? O7 K1 O4 158.25(7) . . ? O7 K1 O8 61.72(7) . . ? O4 K1 O8 102.10(7) . . ? O7 K1 O1 84.09(7) . . ? O4 K1 O1 117.64(7) . . ? O8 K1 O1 126.62(7) . . ? O7 K1 O5 136.98(7) . . ? O4 K1 O5 61.52(6) . . ? O8 K1 O5 160.22(7) . . ? O1 K1 O5 60.98(6) . . ? O7 K1 O10 100.59(7) . . ? O4 K1 O10 71.79(6) . . ? O8 K1 O10 114.41(6) . . ? O1 K1 O10 111.09(7) . . ? O5 K1 O10 72.80(6) . . ? O7 K1 O2 76.16(7) . . ? O4 K1 O2 114.19(7) . . ? O8 K1 O2 71.64(6) . . ? O1 K1 O2 60.56(7) . . ? O5 K1 O2 103.74(7) . . ? O10 K1 O2 171.08(7) . . ? O7 K1 O11 60.84(7) . . ? O4 K1 O11 125.26(7) . . ? O8 K1 O11 118.73(7) . . ? O1 K1 O11 65.19(7) . . ? O5 K1 O11 80.97(6) . . ? O10 K1 O11 59.26(6) . . ? O2 K1 O11 112.39(7) . . ? O7 K1 O9 80.33(6) . . ? O4 K1 O9 78.43(6) . . ? O8 K1 O9 56.92(6) . . ? O1 K1 O9 158.43(6) . . ? O5 K1 O9 124.16(6) . . ? O10 K1 O9 57.98(6) . . ? O2 K1 O9 128.55(6) . . ? O11 K1 O9 94.05(6) . . ? O7 K1 O3 126.74(7) . . ? O4 K1 O3 57.00(6) . . ? O8 K1 O3 78.61(6) . . ? O1 K1 O3 93.85(7) . . ? O5 K1 O3 82.77(6) . . ? O10 K1 O3 128.78(7) . . ? O2 K1 O3 57.63(7) . . ? O11 K1 O3 157.96(7) . . ? O9 K1 O3 107.41(6) . . ? O7 K1 C32 42.34(8) . . ? O4 K1 C32 124.29(8) . . ? O8 K1 C32 22.76(7) . . ? O1 K1 C32 106.25(8) . . ? O5 K1 C32 164.06(8) . . ? O10 K1 C32 122.61(8) . . ? O2 K1 C32 60.40(8) . . ? O11 K1 C32 102.93(8) . . ? O9 K1 C32 71.36(7) . . ? O3 K1 C32 89.02(8) . . ? C1 P1 C17 103.88(15) . . ? C1 P1 C13 102.98(15) . . ? C17 P1 C13 110.44(15) . . ? C1 P1 Ir1 101.73(11) . . ? C17 P1 Ir1 118.04(10) . . ? C13 P1 Ir1 117.10(11) . . ? C21 O1 C30 113.4(3) . . ? C21 O1 K1 117.24(19) . . ? C30 O1 K1 112.71(18) . . ? C22 O2 C23 114.2(3) . . ? C22 O2 K1 110.36(19) . . ? C23 O2 K1 120.25(19) . . ? C24 O3 C25 112.4(3) . . ? C24 O3 K1 106.82(19) . . ? C25 O3 K1 104.34(18) . . ? C27 O4 C26 113.0(2) . . ? C27 O4 K1 108.34(17) . . ? C26 O4 K1 121.32(19) . . ? C29 O5 C28 111.9(2) . . ? C29 O5 K1 114.50(18) . . ? C28 O5 K1 115.66(17) . . ? C40 O7 C31 113.2(3) . . ? C40 O7 K1 115.06(19) . . ? C31 O7 K1 115.95(19) . . ? C33 O8 C32 113.5(3) . . ? C33 O8 K1 121.83(18) . . ? C32 O8 K1 107.13(18) . . ? C34 O9 C35 112.3(2) . . ? C34 O9 K1 106.35(18) . . ? C35 O9 K1 108.46(17) . . ? C37 O10 C36 113.6(2) . . ? C37 O10 K1 112.16(17) . . ? C36 O10 K1 119.98(17) . . ? C39 O11 C38 114.2(3) . . ? C39 O11 K1 110.03(19) . . ? C38 O11 K1 117.15(18) . . ? C3 N1 C2 118.3(2) . . ? C3 N1 Ir1 120.79(19) . . ? C2 N1 Ir1 120.92(19) . . ? C2 C1 P1 114.2(2) . . ? C2 C1 H1 122.9 . . ? P1 C1 H1 122.9 . . ? C1 C2 N1 121.2(3) . . ? C1 C2 H2 119.4 . . ? N1 C2 H2 119.4 . . ? C4 C3 N1 121.3(3) . . ? C4 C3 H3 119.3 . . ? N1 C3 H3 119.3 . . ? C3 C4 P2 114.2(2) . . ? C3 C4 H4 122.9 . . ? P2 C4 H4 122.9 . . ? C4 P2 C5 104.72(15) . . ? C4 P2 C9 103.00(15) . . ? C5 P2 C9 110.81(15) . . ? C4 P2 Ir1 101.51(11) . . ? C5 P2 Ir1 116.81(12) . . ? C9 P2 Ir1 117.53(11) . . ? C7A C5 C6A 114.7(12) . . ? C8 C5 C6 110.8(4) . . ? C8 C5 C7 108.2(5) . . ? C6 C5 C7 107.9(4) . . ? C7A C5 C8A 107.1(13) . . ? C6A C5 C8A 103.9(12) . . ? C7A C5 P2 113.2(12) . . ? C8 C5 P2 106.1(4) . . ? C6A C5 P2 113.9(9) . . ? C6 C5 P2 114.4(4) . . ? C7 C5 P2 109.1(4) . . ? C8A C5 P2 102.5(11) . . ? C5 C6 H6A 109.5 . . ? C5 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C5 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C5 C7 H7A 109.5 . . ? C5 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C5 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C5 C8 H8A 109.5 . . ? C5 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C5 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C5 C6A H6A1 109.5 . . ? C5 C6A H6A2 109.5 . . ? H6A1 C6A H6A2 109.5 . . ? C5 C6A H6A3 109.5 . . ? H6A1 C6A H6A3 109.5 . . ? H6A2 C6A H6A3 109.5 . . ? C5 C7A H7A1 109.5 . . ? C5 C7A H7A2 109.5 . . ? H7A1 C7A H7A2 109.5 . . ? C5 C7A H7A3 109.5 . . ? H7A1 C7A H7A3 109.5 . . ? H7A2 C7A H7A3 109.5 . . ? C5 C8A H8A1 109.5 . . ? C5 C8A H8A2 109.5 . . ? H8A1 C8A H8A2 109.5 . . ? C5 C8A H8A3 109.5 . . ? H8A1 C8A H8A3 109.5 . . ? H8A2 C8A H8A3 109.5 . . ? C11 C9 C10 110.3(3) . . ? C11 C9 C12 108.6(3) . . ? C10 C9 C12 107.0(3) . . ? C11 C9 P2 111.0(2) . . ? C10 C9 P2 115.7(2) . . ? C12 C9 P2 103.8(2) . . ? C9 C10 H10A 109.5 . . ? C9 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C9 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C9 C11 H11A 109.5 . . ? C9 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C9 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C9 C12 H12A 109.5 . . ? C9 C12 H12B 109.5 . . ? H12A C12 H12B 109.5 . . ? C9 C12 H12C 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C16 C13 C15 110.5(3) . . ? C16 C13 C14 108.4(3) . . ? C15 C13 C14 108.4(3) . . ? C16 C13 P1 114.8(2) . . ? C15 C13 P1 110.5(2) . . ? C14 C13 P1 103.9(2) . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? C13 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C13 C15 H15A 109.5 . . ? C13 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? C13 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C13 C16 H16A 109.5 . . ? C13 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C13 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C20 C17 C19 107.6(3) . . ? C20 C17 C18 107.6(3) . . ? C19 C17 C18 110.5(3) . . ? C20 C17 P1 104.0(2) . . ? C19 C17 P1 114.8(2) . . ? C18 C17 P1 111.7(2) . . ? C17 C18 H18A 109.5 . . ? C17 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C17 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C17 C19 H19A 109.5 . . ? C17 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C17 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C17 C20 H20A 109.5 . . ? C17 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C17 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? O1 C21 C22 107.3(3) . . ? O1 C21 H21A 110.3 . . ? C22 C21 H21A 110.3 . . ? O1 C21 H21B 110.3 . . ? C22 C21 H21B 110.3 . . ? H21A C21 H21B 108.5 . . ? O2 C22 C21 112.6(3) . . ? O2 C22 H22A 109.1 . . ? C21 C22 H22A 109.1 . . ? O2 C22 H22B 109.1 . . ? C21 C22 H22B 109.1 . . ? H22A C22 H22B 107.8 . . ? O2 C23 C24 108.8(3) . . ? O2 C23 H23A 109.9 . . ? C24 C23 H23A 109.9 . . ? O2 C23 H23B 109.9 . . ? C24 C23 H23B 109.9 . . ? H23A C23 H23B 108.3 . . ? O3 C24 C23 108.4(3) . . ? O3 C24 H24A 110.0 . . ? C23 C24 H24A 110.0 . . ? O3 C24 H24B 110.0 . . ? C23 C24 H24B 110.0 . . ? H24A C24 H24B 108.4 . . ? O3 C25 C26 107.4(3) . . ? O3 C25 H25A 110.2 . . ? C26 C25 H25A 110.2 . . ? O3 C25 H25B 110.2 . . ? C26 C25 H25B 110.2 . . ? H25A C25 H25B 108.5 . . ? O4 C26 C25 109.4(3) . . ? O4 C26 H26A 109.8 . . ? C25 C26 H26A 109.8 . . ? O4 C26 H26B 109.8 . . ? C25 C26 H26B 109.8 . . ? H26A C26 H26B 108.2 . . ? O4 C27 C28 112.8(3) . . ? O4 C27 H27A 109.0 . . ? C28 C27 H27A 109.0 . . ? O4 C27 H27B 109.0 . . ? C28 C27 H27B 109.0 . . ? H27A C27 H27B 107.8 . . ? O5 C28 C27 109.3(3) . . ? O5 C28 H28A 109.8 . . ? C27 C28 H28A 109.8 . . ? O5 C28 H28B 109.8 . . ? C27 C28 H28B 109.8 . . ? H28A C28 H28B 108.3 . . ? O5 C29 C30 109.6(3) . . ? O5 C29 H29A 109.7 . . ? C30 C29 H29A 109.7 . . ? O5 C29 H29B 109.7 . . ? C30 C29 H29B 109.7 . . ? H29A C29 H29B 108.2 . . ? O1 C30 C29 112.0(3) . . ? O1 C30 H30A 109.2 . . ? C29 C30 H30A 109.2 . . ? O1 C30 H30B 109.2 . . ? C29 C30 H30B 109.2 . . ? H30A C30 H30B 107.9 . . ? O7 C31 C32 109.2(3) . . ? O7 C31 H31A 109.8 . . ? C32 C31 H31A 109.8 . . ? O7 C31 H31B 109.8 . . ? C32 C31 H31B 109.8 . . ? H31A C31 H31B 108.3 . . ? O8 C32 C31 112.3(3) . . ? O8 C32 K1 50.11(14) . . ? C31 C32 K1 83.63(19) . . ? O8 C32 H32A 109.2 . . ? C31 C32 H32A 109.2 . . ? K1 C32 H32A 81.9 . . ? O8 C32 H32B 109.2 . . ? C31 C32 H32B 109.2 . . ? K1 C32 H32B 159.2 . . ? H32A C32 H32B 107.9 . . ? O8 C33 C34 109.5(3) . . ? O8 C33 H33A 109.8 . . ? C34 C33 H33A 109.8 . . ? O8 C33 H33B 109.8 . . ? C34 C33 H33B 109.8 . . ? H33A C33 H33B 108.2 . . ? O9 C34 C33 107.7(3) . . ? O9 C34 H34A 110.2 . . ? C33 C34 H34A 110.2 . . ? O9 C34 H34B 110.2 . . ? C33 C34 H34B 110.2 . . ? H34A C34 H34B 108.5 . . ? O9 C35 C36 108.3(3) . . ? O9 C35 H35A 110.0 . . ? C36 C35 H35A 110.0 . . ? O9 C35 H35B 110.0 . . ? C36 C35 H35B 110.0 . . ? H35A C35 H35B 108.4 . . ? O10 C36 C35 107.8(3) . . ? O10 C36 H36A 110.1 . . ? C35 C36 H36A 110.1 . . ? O10 C36 H36B 110.1 . . ? C35 C36 H36B 110.1 . . ? H36A C36 H36B 108.5 . . ? O10 C37 C38 112.1(3) . . ? O10 C37 H37A 109.2 . . ? C38 C37 H37A 109.2 . . ? O10 C37 H37B 109.2 . . ? C38 C37 H37B 109.2 . . ? H37A C37 H37B 107.9 . . ? O11 C38 C37 107.6(3) . . ? O11 C38 H38A 110.2 . . ? C37 C38 H38A 110.2 . . ? O11 C38 H38B 110.2 . . ? C37 C38 H38B 110.2 . . ? H38A C38 H38B 108.5 . . ? O11 C39 C40 113.1(3) . . ? O11 C39 H39A 109.0 . . ? C40 C39 H39A 109.0 . . ? O11 C39 H39B 109.0 . . ? C40 C39 H39B 109.0 . . ? H39A C39 H39B 107.8 . . ? O7 C40 C39 108.0(3) . . ? O7 C40 H40A 110.1 . . ? C39 C40 H40A 110.1 . . ? O7 C40 H40B 110.1 . . ? C39 C40 H40B 110.1 . . ? H40A C40 H40B 108.4 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C17 P1 C1 C2 -126.2(2) . . . . ? C13 P1 C1 C2 118.6(2) . . . . ? Ir1 P1 C1 C2 -3.1(2) . . . . ? P1 C1 C2 N1 2.5(4) . . . . ? C3 N1 C2 C1 178.6(3) . . . . ? Ir1 N1 C2 C1 -0.4(4) . . . . ? C2 N1 C3 C4 179.6(3) . . . . ? Ir1 N1 C3 C4 -1.4(4) . . . . ? N1 C3 C4 P2 1.5(4) . . . . ? C3 C4 P2 C5 -122.9(3) . . . . ? C3 C4 P2 C9 121.1(3) . . . . ? C3 C4 P2 Ir1 -0.9(3) . . . . ? C4 P2 C5 C7A -175.0(16) . . . . ? C9 P2 C5 C7A -64.6(16) . . . . ? Ir1 P2 C5 C7A 73.6(16) . . . . ? C4 P2 C5 C8 53.5(5) . . . . ? C9 P2 C5 C8 163.9(5) . . . . ? Ir1 P2 C5 C8 -57.9(5) . . . . ? C4 P2 C5 C6A -41.6(16) . . . . ? C9 P2 C5 C6A 68.8(16) . . . . ? Ir1 P2 C5 C6A -153.0(16) . . . . ? C4 P2 C5 C6 -69.0(6) . . . . ? C9 P2 C5 C6 41.4(6) . . . . ? Ir1 P2 C5 C6 179.6(6) . . . . ? C4 P2 C5 C7 169.9(4) . . . . ? C9 P2 C5 C7 -79.7(5) . . . . ? Ir1 P2 C5 C7 58.6(5) . . . . ? C4 P2 C5 C8A 70.0(14) . . . . ? C9 P2 C5 C8A -179.6(14) . . . . ? Ir1 P2 C5 C8A -41.4(14) . . . . ? C4 P2 C9 C11 172.4(2) . . . . ? C5 P2 C9 C11 60.9(3) . . . . ? Ir1 P2 C9 C11 -77.0(3) . . . . ? C4 P2 C9 C10 45.7(3) . . . . ? C5 P2 C9 C10 -65.8(3) . . . . ? Ir1 P2 C9 C10 156.3(2) . . . . ? C4 P2 C9 C12 -71.1(2) . . . . ? C5 P2 C9 C12 177.3(2) . . . . ? Ir1 P2 C9 C12 39.4(2) . . . . ? C1 P1 C13 C16 51.2(3) . . . . ? C17 P1 C13 C16 -59.2(3) . . . . ? Ir1 P1 C13 C16 161.8(2) . . . . ? C1 P1 C13 C15 177.0(2) . . . . ? C17 P1 C13 C15 66.6(3) . . . . ? Ir1 P1 C13 C15 -72.4(3) . . . . ? C1 P1 C13 C14 -67.0(3) . . . . ? C17 P1 C13 C14 -177.4(2) . . . . ? Ir1 P1 C13 C14 43.7(3) . . . . ? C1 P1 C17 C20 68.4(2) . . . . ? C13 P1 C17 C20 178.2(2) . . . . ? Ir1 P1 C17 C20 -43.3(2) . . . . ? C1 P1 C17 C19 -49.0(3) . . . . ? C13 P1 C17 C19 60.8(3) . . . . ? Ir1 P1 C17 C19 -160.6(2) . . . . ? C1 P1 C17 C18 -175.8(3) . . . . ? C13 P1 C17 C18 -66.0(3) . . . . ? Ir1 P1 C17 C18 72.5(3) . . . . ? C30 O1 C21 C22 -174.2(3) . . . . ? K1 O1 C21 C22 -40.2(4) . . . . ? C23 O2 C22 C21 83.9(4) . . . . ? K1 O2 C22 C21 -55.1(4) . . . . ? O1 C21 C22 O2 65.1(4) . . . . ? C22 O2 C23 C24 -169.8(3) . . . . ? K1 O2 C23 C24 -35.2(3) . . . . ? C25 O3 C24 C23 -177.3(3) . . . . ? K1 O3 C24 C23 -63.4(3) . . . . ? O2 C23 C24 O3 67.8(4) . . . . ? C24 O3 C25 C26 -176.0(3) . . . . ? K1 O3 C25 C26 68.7(3) . . . . ? C27 O4 C26 C25 155.0(3) . . . . ? K1 O4 C26 C25 23.8(4) . . . . ? O3 C25 C26 O4 -64.4(4) . . . . ? C26 O4 C27 C28 -79.3(3) . . . . ? K1 O4 C27 C28 58.1(3) . . . . ? C29 O5 C28 C27 169.3(3) . . . . ? K1 O5 C28 C27 35.8(3) . . . . ? O4 C27 C28 O5 -65.5(3) . . . . ? C28 O5 C29 C30 179.7(3) . . . . ? K1 O5 C29 C30 -46.2(3) . . . . ? C21 O1 C30 C29 88.4(3) . . . . ? K1 O1 C30 C29 -47.7(3) . . . . ? O5 C29 C30 O1 64.4(4) . . . . ? C40 O7 C31 C32 170.3(3) . . . . ? K1 O7 C31 C32 34.2(3) . . . . ? C33 O8 C32 C31 -77.3(4) . . . . ? K1 O8 C32 C31 60.1(3) . . . . ? C33 O8 C32 K1 -137.4(3) . . . . ? O7 C31 C32 O8 -66.0(4) . . . . ? O7 C31 C32 K1 -24.0(2) . . . . ? C32 O8 C33 C34 151.4(3) . . . . ? K1 O8 C33 C34 21.0(4) . . . . ? C35 O9 C34 C33 -174.2(3) . . . . ? K1 O9 C34 C33 67.4(3) . . . . ? O8 C33 C34 O9 -60.4(3) . . . . ? C34 O9 C35 C36 -179.4(3) . . . . ? K1 O9 C35 C36 -62.2(3) . . . . ? C37 O10 C36 C35 -174.1(2) . . . . ? K1 O10 C36 C35 -37.6(3) . . . . ? O9 C35 C36 O10 67.4(3) . . . . ? C36 O10 C37 C38 82.7(3) . . . . ? K1 O10 C37 C38 -57.3(3) . . . . ? C39 O11 C38 C37 -168.5(3) . . . . ? K1 O11 C38 C37 -37.8(3) . . . . ? O10 C37 C38 O11 63.9(3) . . . . ? C38 O11 C39 C40 85.3(4) . . . . ? K1 O11 C39 C40 -48.9(3) . . . . ? C31 O7 C40 C39 174.8(3) . . . . ? K1 O7 C40 C39 -48.7(3) . . . . ? O11 C39 C40 O7 67.7(4) . . . . ? _refine_diff_density_max 0.645 _refine_diff_density_min -0.677 _refine_diff_density_rms 0.094 _shelxl_version_number 2013-4 _shelx_res_file ; REM Solution 1 R1 0.103, Alpha = 0.0476 in Pbcn REM Formula: C29 N3 O19 Cl3 K Ir TITL pbcn in Pbcn CELL 0.56086 20.279 18.474 26.694 90.000 90.000 90.000 ZERR 8.00 0.002 0.002 0.003 0.0000 0.0000 0.0000 LATT 1 SYMM 1/2-X, 1/2-Y, 1/2+Z SYMM -X, Y, 1/2-Z SYMM 1/2+X, 1/2-Y, -Z SFAC C H N O P CL K IR UNIT 320 640 8 80 16 8 8 8 TEMP -173.000 SIZE 0.097 0.103 0.103 L.S. 10 omit 1 1 1 omit 3 1 0 LIST 4 ACTA CONF BOND $H FMAP 2 PLAN 20 WGHT 0.008100 13.468400 FVAR 0.08053 0.75172 IR1 8 0.219739 0.277651 0.378863 11.00000 0.01778 0.01589 = 0.01639 0.00073 -0.00184 -0.00445 K1 7 0.662330 0.507700 0.372567 11.00000 0.01835 0.01930 = 0.01734 0.00033 0.00013 -0.00040 CL1 6 0.167880 0.160907 0.379110 11.00000 0.03073 0.02232 = 0.04128 -0.00203 0.00428 -0.00927 P1 5 0.126818 0.345905 0.387085 11.00000 0.01926 0.02028 = 0.01501 -0.00087 0.00139 -0.00431 O1 4 0.689538 0.444180 0.467121 11.00000 0.04082 0.02772 = 0.01971 -0.00069 -0.00001 0.00214 O2 4 0.621830 0.580206 0.461600 11.00000 0.03396 0.02992 = 0.02438 -0.00224 0.00263 0.00292 O3 4 0.519861 0.535300 0.396607 11.00000 0.02620 0.02691 = 0.03733 -0.00076 0.00085 0.00604 O4 4 0.557108 0.448865 0.315731 11.00000 0.01618 0.03172 = 0.02839 0.00150 -0.00441 -0.00095 O5 4 0.625447 0.361304 0.389671 11.00000 0.01909 0.02921 = 0.02421 0.00473 -0.00164 -0.00500 O7 4 0.770435 0.598244 0.396012 11.00000 0.03159 0.03360 = 0.02938 -0.00305 0.00006 -0.00793 O8 4 0.651529 0.657692 0.351350 11.00000 0.03459 0.02481 = 0.02592 0.00415 0.00735 -0.00052 O9 4 0.688409 0.569885 0.272315 11.00000 0.02399 0.02577 = 0.02234 0.00149 -0.00292 0.00221 O10 4 0.717022 0.423965 0.293444 11.00000 0.02170 0.02593 = 0.01632 0.00263 0.00239 -0.00033 O11 4 0.792873 0.444387 0.381849 11.00000 0.02329 0.04368 = 0.02567 -0.00636 -0.00348 0.00433 N1 3 0.262795 0.376828 0.377100 11.00000 0.01755 0.01803 = 0.01478 0.00197 -0.00074 -0.00505 C1 1 0.159305 0.435603 0.383532 11.00000 0.02576 0.01637 = 0.01892 0.00093 0.00001 -0.00079 AFIX 43 H1 2 0.132250 0.477574 0.384180 11.00000 -1.20000 AFIX 0 C2 1 0.225613 0.438598 0.379848 11.00000 0.02579 0.01684 = 0.01410 0.00124 -0.00077 -0.00570 AFIX 43 H2 2 0.246900 0.484395 0.379148 11.00000 -1.20000 AFIX 0 C3 1 0.329724 0.383676 0.372322 11.00000 0.02347 0.02133 = 0.01641 0.00294 -0.00268 -0.00990 AFIX 43 H3 2 0.348704 0.430640 0.370822 11.00000 -1.20000 AFIX 0 C4 1 0.369298 0.325013 0.369698 11.00000 0.01516 0.02556 = 0.02882 0.00180 -0.00574 -0.00688 AFIX 43 H4 2 0.415928 0.328347 0.367183 11.00000 -1.20000 AFIX 0 simu c5 > c8a rigu p2 c5 > c8a same p2 c5 c7 c8 c6 same p2 c5 c6a c7a C8a P2 5 0.326231 0.240284 0.371373 11.00000 0.02066 0.01778 = 0.02291 0.00127 -0.00760 -0.00347 C5 1 0.362647 0.190550 0.426477 11.00000 0.03844 0.02212 = 0.03176 0.00560 -0.01547 -0.00251 PART 1 21 C6 1 0.434780 0.166159 0.419072 21.00000 0.03798 0.03848 = 0.05900 0.01964 -0.02442 -0.00288 AFIX 137 H6A 2 0.436712 0.129106 0.392842 21.00000 -1.50000 H6B 2 0.451729 0.146066 0.450515 21.00000 -1.50000 H6C 2 0.461703 0.207818 0.409159 21.00000 -1.50000 AFIX 0 C7 1 0.320782 0.122575 0.437344 21.00000 0.03442 0.01886 = 0.02726 -0.00122 -0.00086 0.00889 AFIX 137 H7A 2 0.274327 0.136409 0.440611 21.00000 -1.50000 H7B 2 0.335800 0.100128 0.468590 21.00000 -1.50000 H7C 2 0.325635 0.088024 0.409732 21.00000 -1.50000 AFIX 0 eadp c8 c8a C8 1 0.356786 0.241198 0.470808 21.00000 0.07675 0.03076 = 0.02785 0.00010 -0.02621 -0.00531 AFIX 137 H8A 2 0.367073 0.214809 0.501681 21.00000 -1.50000 H8B 2 0.311703 0.260111 0.472668 21.00000 -1.50000 H8C 2 0.387788 0.281474 0.466782 21.00000 -1.50000 AFIX 0 PART 2 -21 C6A 1 0.437318 0.197786 0.430722 -21.00000 0.04898 0.04449 = 0.05257 0.00745 -0.02205 0.00078 AFIX 33 H6A1 2 0.449283 0.249151 0.431939 -21.00000 -1.50000 H6A2 2 0.458228 0.175096 0.401587 -21.00000 -1.50000 H6A3 2 0.452447 0.173761 0.461369 -21.00000 -1.50000 AFIX 0 C7A 1 0.336941 0.114413 0.431840 -21.00000 0.06788 0.02692 = 0.02720 0.00575 -0.01182 -0.00452 AFIX 33 H7A1 2 0.289011 0.114279 0.427154 -21.00000 -1.50000 H7A2 2 0.347551 0.096080 0.465334 -21.00000 -1.50000 H7A3 2 0.357544 0.083364 0.406521 -21.00000 -1.50000 AFIX 0 C8A 1 0.335535 0.235474 0.472746 -21.00000 0.07675 0.03076 = 0.02785 0.00010 -0.02621 -0.00531 AFIX 33 H8A1 2 0.344768 0.287015 0.467618 -21.00000 -1.50000 H8A2 2 0.357263 0.218971 0.503486 -21.00000 -1.50000 H8A3 2 0.287828 0.228189 0.475719 -21.00000 -1.50000 AFIX 0 part 0 C9 1 0.351385 0.195941 0.310305 11.00000 0.02055 0.02913 = 0.02871 0.00122 -0.00269 -0.00179 C10 1 0.424939 0.199271 0.297786 11.00000 0.02737 0.06144 = 0.05592 -0.02018 0.00823 -0.00380 AFIX 137 H10A 2 0.449596 0.169219 0.321543 11.00000 -1.50000 H10B 2 0.440261 0.249469 0.300111 11.00000 -1.50000 H10C 2 0.432080 0.181257 0.263684 11.00000 -1.50000 AFIX 0 C11 1 0.326840 0.118217 0.307782 11.00000 0.05345 0.03414 = 0.02978 -0.01057 0.00769 -0.01294 AFIX 137 H11A 2 0.280591 0.116367 0.318350 11.00000 -1.50000 H11B 2 0.353495 0.087833 0.330044 11.00000 -1.50000 H11C 2 0.330623 0.100380 0.273327 11.00000 -1.50000 AFIX 0 C12 1 0.315289 0.240362 0.270401 11.00000 0.04471 0.04903 = 0.02498 0.00147 -0.00125 0.00326 AFIX 137 H12A 2 0.329895 0.290868 0.272115 11.00000 -1.50000 H12B 2 0.267662 0.237961 0.276396 11.00000 -1.50000 H12C 2 0.325204 0.220691 0.237148 11.00000 -1.50000 AFIX 0 C13 1 0.084535 0.344825 0.450116 11.00000 0.03550 0.02749 = 0.01715 -0.00082 0.00731 -0.00729 C14 1 0.141386 0.351357 0.487646 11.00000 0.06443 0.07532 = 0.01819 -0.00581 0.00323 -0.02779 AFIX 137 H14A 2 0.123817 0.350007 0.521834 11.00000 -1.50000 H14B 2 0.164587 0.397234 0.482254 11.00000 -1.50000 H14C 2 0.172119 0.311008 0.482857 11.00000 -1.50000 AFIX 0 C15 1 0.050098 0.272415 0.458709 11.00000 0.03961 0.03327 = 0.02421 0.00270 0.00897 -0.00586 AFIX 137 H15A 2 0.037695 0.268107 0.494067 11.00000 -1.50000 H15B 2 0.080059 0.232852 0.449760 11.00000 -1.50000 H15C 2 0.010431 0.269794 0.437819 11.00000 -1.50000 AFIX 0 C16 1 0.036839 0.407296 0.459104 11.00000 0.08786 0.03557 = 0.04686 0.00549 0.04626 0.01138 AFIX 137 H16A 2 0.024848 0.408951 0.494650 11.00000 -1.50000 H16B 2 -0.002958 0.400122 0.438877 11.00000 -1.50000 H16C 2 0.057971 0.452966 0.449560 11.00000 -1.50000 AFIX 0 C17 1 0.064206 0.342641 0.335221 11.00000 0.02038 0.03010 = 0.01803 -0.00321 0.00054 -0.00203 C18 1 0.026895 0.270712 0.334659 11.00000 0.05283 0.06009 = 0.03384 0.00879 -0.01938 -0.03263 AFIX 137 H18A 2 -0.005427 0.270120 0.361948 11.00000 -1.50000 H18B 2 0.058138 0.230763 0.339137 11.00000 -1.50000 H18C 2 0.004064 0.265158 0.302531 11.00000 -1.50000 AFIX 0 C19 1 0.015960 0.406212 0.334303 11.00000 0.03580 0.06840 = 0.05944 -0.02398 -0.02239 0.02090 AFIX 137 H19A 2 0.040577 0.451793 0.336013 11.00000 -1.50000 H19B 2 -0.013888 0.402803 0.363080 11.00000 -1.50000 H19C 2 -0.009739 0.404791 0.303227 11.00000 -1.50000 AFIX 0 C20 1 0.105509 0.346388 0.287484 11.00000 0.03484 0.05020 = 0.01915 0.00333 -0.00436 0.00133 AFIX 137 H20A 2 0.138584 0.307715 0.287887 11.00000 -1.50000 H20B 2 0.127679 0.393450 0.285665 11.00000 -1.50000 H20C 2 0.076782 0.340403 0.258255 11.00000 -1.50000 AFIX 0 C21 1 0.658511 0.475427 0.509758 11.00000 0.06619 0.04126 = 0.01910 0.00017 -0.00055 0.01198 AFIX 23 H21A 2 0.682313 0.461537 0.540679 11.00000 -1.20000 H21B 2 0.612382 0.458316 0.512440 11.00000 -1.20000 AFIX 0 C22 1 0.660134 0.556696 0.502998 11.00000 0.05838 0.03851 = 0.02289 -0.00855 -0.00583 0.00698 AFIX 23 H22A 2 0.643408 0.580093 0.533849 11.00000 -1.20000 H22B 2 0.706375 0.572373 0.498125 11.00000 -1.20000 AFIX 0 C23 1 0.553575 0.589054 0.472432 11.00000 0.04218 0.03049 = 0.03974 -0.00836 0.02031 -0.00004 AFIX 23 H23A 2 0.547145 0.631192 0.494818 11.00000 -1.20000 H23B 2 0.536486 0.545423 0.489611 11.00000 -1.20000 AFIX 0 C24 1 0.517497 0.600504 0.424725 11.00000 0.03033 0.02918 = 0.05195 -0.00457 0.01789 0.00602 AFIX 23 H24A 2 0.471108 0.613803 0.431713 11.00000 -1.20000 H24B 2 0.538150 0.640332 0.405503 11.00000 -1.20000 AFIX 0 C25 1 0.489001 0.542254 0.349005 11.00000 0.02104 0.03894 = 0.04466 0.01176 -0.00103 0.00924 AFIX 23 H25A 2 0.513021 0.577868 0.328149 11.00000 -1.20000 H25B 2 0.442941 0.559026 0.353051 11.00000 -1.20000 AFIX 0 C26 1 0.490301 0.469660 0.324809 11.00000 0.01709 0.04705 = 0.04411 0.00298 -0.00615 0.00137 AFIX 23 H26A 2 0.468776 0.433681 0.346900 11.00000 -1.20000 H26B 2 0.465745 0.471282 0.292775 11.00000 -1.20000 AFIX 0 C27 1 0.565716 0.372244 0.313071 11.00000 0.02070 0.02907 = 0.03210 -0.00202 -0.00658 -0.00666 AFIX 23 H27A 2 0.607202 0.361534 0.294982 11.00000 -1.20000 H27B 2 0.528909 0.351035 0.293625 11.00000 -1.20000 AFIX 0 C28 1 0.568090 0.337253 0.363680 11.00000 0.02410 0.02959 = 0.03824 0.00606 -0.00508 -0.00545 AFIX 23 H28A 2 0.528127 0.350218 0.383001 11.00000 -1.20000 H28B 2 0.569292 0.283953 0.359943 11.00000 -1.20000 AFIX 0 C29 1 0.624389 0.340693 0.440713 11.00000 0.03388 0.02577 = 0.02641 0.00850 0.00347 0.00288 AFIX 23 H29A 2 0.621553 0.287333 0.443366 11.00000 -1.20000 H29B 2 0.585181 0.361749 0.457323 11.00000 -1.20000 AFIX 0 C30 1 0.685814 0.366917 0.466125 11.00000 0.03627 0.02896 = 0.02580 0.00577 -0.00592 0.00639 AFIX 23 H30A 2 0.686827 0.348267 0.500885 11.00000 -1.20000 H30B 2 0.724797 0.347476 0.448310 11.00000 -1.20000 AFIX 0 C31 1 0.764230 0.672249 0.381364 11.00000 0.04483 0.03449 = 0.03846 -0.00214 -0.00462 -0.01815 AFIX 23 H31A 2 0.779148 0.678263 0.346297 11.00000 -1.20000 H31B 2 0.792182 0.703036 0.403056 11.00000 -1.20000 AFIX 0 C32 1 0.693259 0.694903 0.386034 11.00000 0.05868 0.02243 = 0.03076 -0.00366 0.00632 -0.00806 AFIX 23 H32A 2 0.677859 0.685093 0.420566 11.00000 -1.20000 H32B 2 0.689823 0.747668 0.380105 11.00000 -1.20000 AFIX 0 C33 1 0.655724 0.684975 0.301547 11.00000 0.03386 0.02737 = 0.03430 0.01177 0.00792 0.00394 AFIX 23 H33A 2 0.700577 0.704116 0.295311 11.00000 -1.20000 H33B 2 0.623836 0.725034 0.297070 11.00000 -1.20000 AFIX 0 C34 1 0.640808 0.625438 0.265091 11.00000 0.02628 0.03279 = 0.02735 0.01026 -0.00180 0.00484 AFIX 23 H34A 2 0.595890 0.606261 0.271000 11.00000 -1.20000 H34B 2 0.643121 0.643986 0.230340 11.00000 -1.20000 AFIX 0 C35 1 0.682713 0.513539 0.235996 11.00000 0.02962 0.03008 = 0.01658 0.00017 -0.00264 -0.00409 AFIX 23 H35A 2 0.689312 0.533414 0.201920 11.00000 -1.20000 H35B 2 0.638232 0.491582 0.237627 11.00000 -1.20000 AFIX 0 C36 1 0.733903 0.457800 0.246983 11.00000 0.03020 0.02690 = 0.01624 -0.00339 0.00326 -0.00343 AFIX 23 H36A 2 0.735226 0.421351 0.219814 11.00000 -1.20000 H36B 2 0.777886 0.480772 0.249486 11.00000 -1.20000 AFIX 0 C37 1 0.765448 0.374441 0.310848 11.00000 0.02266 0.02298 = 0.02179 0.00256 0.00292 0.00474 AFIX 23 H37A 2 0.783883 0.347615 0.281957 11.00000 -1.20000 H37B 2 0.744375 0.338899 0.333522 11.00000 -1.20000 AFIX 0 C38 1 0.820359 0.411810 0.338154 11.00000 0.02256 0.03428 = 0.02828 -0.00075 0.00154 0.00590 AFIX 23 H38A 2 0.854847 0.376449 0.347646 11.00000 -1.20000 H38B 2 0.840597 0.449208 0.316492 11.00000 -1.20000 AFIX 0 C39 1 0.835773 0.493284 0.406583 11.00000 0.02519 0.05894 = 0.03463 -0.01272 -0.00994 0.00713 AFIX 23 H39A 2 0.881483 0.474778 0.404216 11.00000 -1.20000 H39B 2 0.823781 0.495341 0.442506 11.00000 -1.20000 AFIX 0 C40 1 0.833402 0.568544 0.385162 11.00000 0.03040 0.05391 = 0.03820 -0.01571 -0.00228 -0.01367 AFIX 23 H40A 2 0.868426 0.598801 0.400296 11.00000 -1.20000 H40B 2 0.840488 0.566950 0.348485 11.00000 -1.20000 AFIX 0 HKLF 4 REM pbcn in Pbcn REM R1 = 0.0261 for 6741 Fo > 4sig(Fo) and 0.0492 for all 9180 data REM 539 parameters refined using 156 restraints END WGHT 0.0081 13.4785 REM Highest difference peak 0.645, deepest hole -0.677, 1-sigma level 0.094 Q1 1 0.2466 0.2383 0.3740 11.00000 0.05 0.65 Q2 1 0.2859 0.2688 0.3915 11.00000 0.05 0.51 Q3 1 0.2126 0.3559 0.3780 11.00000 0.05 0.48 Q4 1 0.3473 0.2781 0.3811 11.00000 0.05 0.47 Q5 1 0.1656 0.2228 0.3909 11.00000 0.05 0.47 Q6 1 0.1399 0.2831 0.3807 11.00000 0.05 0.47 Q7 1 0.1679 0.3209 0.3830 11.00000 0.05 0.41 Q8 1 0.6614 0.3194 0.3764 11.00000 0.05 0.40 Q9 1 0.1978 0.2575 0.4079 11.00000 0.05 0.38 Q10 1 0.6366 0.4608 0.3748 11.00000 0.05 0.36 Q11 1 0.0017 0.2801 0.3112 11.00000 0.05 0.35 Q12 1 0.4632 0.6230 0.3247 11.00000 0.05 0.35 Q13 1 0.4670 0.0544 0.2359 11.00000 0.05 0.35 Q14 1 0.2054 0.1350 0.3462 11.00000 0.05 0.35 Q15 1 0.8472 0.4600 0.3304 11.00000 0.05 0.35 Q16 1 0.5153 0.5992 0.3377 11.00000 0.05 0.34 Q17 1 0.2857 0.1193 0.3720 11.00000 0.05 0.34 Q18 1 0.2715 0.2239 0.3277 11.00000 0.05 0.34 Q19 1 0.1234 0.4623 0.4798 11.00000 0.05 0.33 Q20 1 0.2038 0.3174 0.4050 11.00000 0.05 0.33 ; _shelx_res_checksum 70451 _shelx_hkl_file ; 0 2 0 1189.78 57.29 0 2 0 930.51 56.99 0 2 0 799.52 54.29 0 -2 0 1120.79 57.19 0 -2 0 1177.98 57.29 0 -2 0 1195.28 56.99 0 -2 0 1123.89 54.69 0 2 0 1226.98 54.49 0 2 0 1176.78 56.29 0 -2 0 1185.78 54.09 0 -3 0 -1.20 1.40 0 3 0 1.00 1.90 0 3 0 0.60 2.20 0 -3 0 -0.80 1.30 0 -3 0 1.80 2.30 0 -3 0 0.20 2.00 0 -3 0 1.10 1.90 0 -3 0 -1.70 2.00 0 3 0 1.70 2.20 0 3 0 -0.30 1.70 0 3 0 -2.70 1.90 0 3 0 1.80 1.70 0 3 0 3.10 1.60 0 -4 0 38.20 5.10 0 4 0 26.80 4.80 0 4 0 27.00 4.10 0 4 0 21.50 4.10 0 4 0 22.50 4.50 0 4 0 30.30 4.30 0 -4 0 20.60 4.40 0 -4 0 38.80 4.20 0 -4 0 29.50 5.00 0 4 0 27.00 4.60 0 -4 0 34.00 4.40 0 4 0 34.80 4.20 0 -4 0 37.30 5.20 0 5 0 1.40 3.20 0 -5 0 -3.00 2.80 0 -5 0 0.10 2.80 0 -5 0 0.30 2.30 0 5 0 2.60 3.30 0 5 0 -2.60 2.30 0 5 0 0.80 2.60 0 5 0 -1.60 2.50 0 -5 0 -3.10 2.10 0 -5 0 3.20 3.30 0 5 0 -0.50 2.00 0 -5 0 1.20 2.00 0 5 0 -5.40 2.60 0 -6 0 201.28 14.70 0 6 0 187.98 14.40 0 6 0 159.58 12.70 0 6 0 169.38 13.30 0 -6 0 190.08 13.80 0 6 0 172.68 14.00 0 -6 0 174.48 13.40 0 6 0 179.58 12.20 0 6 0 181.48 12.80 0 6 0 184.78 13.90 0 -6 0 214.18 14.70 0 -6 0 186.78 11.90 0 7 0 0.30 3.10 0 7 0 -3.70 3.50 0 7 0 0.50 2.60 0 -7 0 1.70 3.60 0 -7 0 1.10 3.40 0 -7 0 2.00 4.00 0 7 0 -2.70 2.90 0 7 0 -1.30 3.30 0 7 0 7.00 4.60 0 7 0 2.20 3.90 0 -7 0 6.60 4.40 0 -7 0 -0.70 2.50 0 8 0 63.29 9.40 0 -8 0 51.59 9.30 0 -8 0 51.09 9.00 0 8 0 70.19 9.20 0 8 0 69.99 10.30 0 -8 0 71.59 9.50 0 -8 0 57.39 8.70 0 8 0 71.49 8.50 0 8 0 41.30 8.50 0 8 0 60.19 8.30 0 8 0 61.39 9.90 0 -9 0 -5.20 3.90 0 -9 0 1.90 4.00 0 -9 0 -1.40 4.60 0 9 0 -3.20 5.00 0 9 0 0.60 4.00 0 9 0 -9.50 4.00 0 9 0 -4.60 4.50 0 9 0 2.40 4.30 0 9 0 4.40 4.40 0 -9 0 0.60 4.40 0 9 0 1.60 3.20 0 -10 0 232.18 22.00 0 -10 0 230.48 22.00 0 10 0 227.98 18.50 0 10 0 183.08 19.80 0 -10 0 194.08 18.90 0 10 0 209.58 20.70 0 10 0 233.18 17.70 0 10 0 230.08 22.20 0 10 0 224.08 16.70 0 10 0 259.07 18.00 0 -10 0 244.78 19.00 0 11 0 -2.30 3.80 0 -11 0 -1.60 4.30 0 11 0 0.90 4.70 0 11 0 -3.60 4.40 0 -11 0 -3.20 4.00 0 -11 0 -4.30 3.60 0 11 0 -2.40 3.60 0 -11 0 5.30 6.00 0 -11 0 -6.40 4.10 0 11 0 0.40 4.40 0 12 0 6.60 5.30 0 -12 0 16.40 6.60 0 -12 0 0.80 4.60 0 -12 0 2.50 6.10 0 12 0 1.40 6.00 0 12 0 -4.20 4.30 0 -12 0 0.20 5.10 0 -12 0 -3.00 5.60 0 12 0 0.50 4.50 0 13 0 1.40 4.80 0 13 0 -2.50 4.90 0 13 0 5.70 6.00 0 -13 0 -3.70 5.50 0 -13 0 -2.10 5.30 0 -13 0 -4.40 5.10 0 13 0 2.10 6.00 0 -13 0 -1.50 5.90 0 -13 0 -1.70 4.30 0 -14 0 611.74 41.60 0 14 0 630.54 41.10 0 -14 0 646.64 37.70 0 -14 0 611.64 41.00 0 14 0 600.04 38.40 0 -14 0 607.54 42.90 0 -14 0 566.64 42.20 0 14 0 641.24 40.30 0 14 0 717.83 40.90 0 -15 0 -6.80 5.50 0 -15 0 -10.10 5.00 0 15 0 -1.50 7.00 0 -15 0 -11.80 5.20 0 -15 0 1.40 7.30 0 15 0 -5.50 5.40 0 15 0 0.50 5.40 0 -16 0 495.95 38.00 0 16 0 564.44 37.00 0 -16 0 480.15 35.10 0 -16 0 459.25 35.40 0 16 0 489.55 33.30 0 -16 0 420.66 36.20 0 16 0 464.15 34.30 0 -17 0 5.60 7.20 0 17 0 -8.70 7.90 0 17 0 -0.70 6.00 0 -17 0 -8.20 6.50 0 -17 0 -7.50 7.20 0 -17 0 4.30 9.20 0 17 0 1.80 7.20 0 -18 0 746.53 52.29 0 18 0 694.23 46.40 0 -18 0 738.53 49.99 0 -18 0 635.94 50.39 0 18 0 777.42 49.40 0 18 0 828.22 51.19 0 -18 0 694.13 48.70 0 -19 0 3.80 9.90 0 -19 0 -5.20 7.60 0 19 0 -12.80 7.10 0 19 0 -3.50 5.30 0 20 0 206.78 26.20 0 20 0 216.48 24.80 0 21 0 8.10 8.20 0 21 0 7.60 9.70 0 22 0 93.69 17.30 0 22 0 66.79 16.10 -1 2 0 -1.70 1.00 -1 2 0 0.20 1.30 -1 -2 0 -0.30 0.90 1 -2 0 0.40 1.00 -1 -2 0 -0.70 0.80 -1 -2 0 0.20 0.70 -1 -2 0 -0.10 1.20 1 2 0 -0.20 1.00 1 2 0 -1.10 0.70 -1 2 0 -0.40 0.90 -1 2 0 0.00 1.20 -1 2 0 1.60 1.20 1 2 0 0.10 1.30 1 -2 0 0.50 1.30 -1 -2 0 -1.40 1.20 -1 2 0 0.20 1.10 1 2 0 0.50 1.40 1 2 0 0.70 1.10 1 2 0 -0.40 0.80 -1 -2 0 0.00 1.20 1 -2 0 -0.10 1.10 -1 2 0 -1.40 1.00 1 2 0 0.60 0.70 1 -2 0 1.20 1.20 1 -2 0 1.70 1.40 -1 3 0 872.31 46.20 1 3 0 859.61 42.70 1 -3 0 857.71 45.60 1 -3 0 885.81 46.20 1 -3 0 841.92 45.70 -1 -3 0 859.81 42.80 -1 3 0 855.11 43.60 1 -3 0 893.81 44.00 -1 3 0 837.42 43.90 1 3 0 879.51 43.00 1 3 0 883.61 45.70 -1 3 0 854.11 43.40 -1 -3 0 889.11 45.60 -1 -3 0 893.31 43.30 -1 -3 0 862.81 46.10 1 3 0 821.62 45.20 1 3 0 893.71 46.20 -1 -3 0 859.41 42.50 -1 -3 0 814.42 45.20 -1 3 0 926.01 45.70 1 3 0 896.81 43.50 -1 3 0 887.41 45.90 1 -3 0 889.41 43.40 1 -3 0 830.42 45.20 1 3 0 835.82 45.60 -1 -3 0 854.61 45.70 1 4 0 1.30 2.00 1 4 0 -1.40 2.60 -1 4 0 1.40 2.50 1 4 0 0.20 2.10 1 4 0 -3.70 2.20 1 4 0 -2.20 2.50 1 -4 0 -1.00 1.90 -1 -4 0 -2.30 1.80 1 4 0 -1.40 1.50 1 -4 0 -0.50 2.80 -1 -4 0 0.10 2.70 1 -4 0 -1.30 1.90 -1 -4 0 1.60 1.90 -1 -4 0 -1.20 2.50 1 -4 0 -0.50 2.50 -1 4 0 -3.00 2.20 1 -4 0 0.20 2.30 1 -4 0 0.50 2.60 -1 4 0 0.60 1.90 -1 4 0 -1.10 2.50 -1 -4 0 2.20 1.60 -1 -4 0 -0.50 2.50 -1 -4 0 0.20 1.80 1 4 0 -0.10 1.80 -1 4 0 -0.60 2.70 -1 4 0 -0.20 2.00 1 -5 0 69.19 7.20 1 5 0 68.69 7.80 -1 -5 0 65.49 6.20 1 -5 0 70.79 8.30 -1 -5 0 72.09 6.00 -1 -5 0 58.59 7.40 -1 5 0 63.69 7.00 1 5 0 71.49 7.80 1 -5 0 70.49 8.10 1 5 0 54.29 6.30 -1 5 0 58.39 7.50 1 -5 0 69.69 8.30 1 -5 0 68.99 7.60 -1 5 0 58.89 7.90 -1 -5 0 54.99 6.70 1 5 0 56.49 5.70 1 5 0 55.59 6.20 1 5 0 43.20 6.70 -1 5 0 55.79 7.60 -1 -5 0 52.59 7.40 1 5 0 55.39 7.40 1 -5 0 68.39 6.80 -1 5 0 62.29 7.10 -1 5 0 62.29 7.20 -1 -5 0 53.09 7.40 -1 5 0 66.19 6.80 1 -6 0 1.30 3.50 -1 6 0 -1.40 3.00 1 6 0 -2.90 3.10 1 6 0 1.20 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99.99 14.40 -1 13 0 121.39 15.20 1 13 0 115.49 13.60 1 -13 0 78.49 13.80 1 -13 0 117.79 14.50 -1 -13 0 75.79 12.70 -1 -13 0 105.59 11.80 1 13 0 75.09 12.30 1 -13 0 85.49 14.70 -1 13 0 86.99 12.50 -1 -14 0 -1.40 5.50 -1 14 0 -0.30 6.90 -1 -14 0 3.20 5.00 1 -14 0 4.70 6.40 1 -14 0 -4.90 4.40 -1 14 0 2.50 6.10 -1 -14 0 -5.60 4.50 1 14 0 6.50 5.60 1 -14 0 -2.10 5.20 -1 -14 0 -8.10 6.30 1 14 0 -8.20 6.30 -1 -14 0 4.50 6.00 1 -14 0 8.20 7.20 -1 14 0 -5.80 5.30 1 -14 0 -4.20 6.00 1 14 0 1.10 6.00 1 14 0 -7.40 5.20 -1 14 0 -0.40 4.90 -1 -15 0 15.30 9.00 1 15 0 30.80 9.90 -1 15 0 20.40 9.60 -1 -15 0 17.40 8.10 1 -15 0 10.80 7.90 1 15 0 30.20 9.90 -1 15 0 15.70 8.10 -1 15 0 27.90 8.70 1 -15 0 37.20 11.20 -1 -15 0 31.90 11.40 1 -15 0 40.00 11.50 -1 -15 0 31.70 9.30 1 -15 0 27.80 9.60 1 15 0 22.30 8.20 -1 16 0 5.40 7.30 1 -16 0 6.00 7.10 1 -16 0 -6.30 7.20 1 -16 0 -4.20 6.10 1 16 0 1.20 7.50 -1 -16 0 -13.00 6.80 1 16 0 -6.30 5.40 -1 16 0 0.00 5.60 -1 16 0 -7.80 7.70 1 16 0 -2.80 6.70 1 -16 0 12.20 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6.70 2 10 0 18.90 7.30 -2 -10 0 22.60 7.10 -2 -10 0 24.30 6.50 -2 10 0 10.50 5.40 2 -10 0 3.30 5.60 2 -10 0 20.00 6.50 2 -10 0 12.70 5.70 2 10 0 23.20 6.30 -2 10 0 18.40 7.20 2 10 0 16.50 6.60 -2 10 0 20.60 6.40 2 10 0 16.00 6.90 2 10 0 27.50 6.00 -2 -10 0 26.10 8.10 -2 -10 0 10.40 6.30 2 10 0 23.20 7.50 -2 10 0 22.50 6.70 2 -11 0 1.10 4.90 -2 -11 0 -3.30 4.60 -2 -11 0 -2.40 4.30 -2 11 0 5.90 5.80 -2 11 0 2.40 5.00 -2 -11 0 0.00 4.70 -2 -11 0 -5.90 4.80 -2 11 0 4.20 4.90 -2 11 0 -0.20 4.60 2 11 0 -4.30 4.10 2 11 0 -4.30 3.00 2 -11 0 0.00 4.50 2 -11 0 -2.10 4.60 -2 -11 0 2.60 3.40 -2 11 0 -3.90 3.40 2 -11 0 -1.00 4.60 2 11 0 -2.00 4.40 2 11 0 0.60 5.10 -2 -12 0 79.69 13.10 -2 -12 0 65.39 12.60 2 -12 0 64.99 11.40 -2 -12 0 71.89 9.00 2 -12 0 61.79 12.10 -2 -12 0 56.19 10.70 2 12 0 57.79 8.80 -2 12 0 88.39 12.30 2 12 0 71.19 12.20 -2 12 0 46.70 10.10 2 12 0 50.89 9.80 -2 12 0 59.69 11.70 2 12 0 58.89 10.10 -2 12 0 65.49 11.00 2 -12 0 74.99 12.80 -2 12 0 56.89 9.70 2 -12 0 63.49 10.50 -2 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62.89 12.90 2 16 0 73.59 12.50 2 16 0 81.99 15.00 -2 16 0 69.59 12.70 2 -16 0 69.99 15.00 -2 -16 0 88.89 16.70 -2 -16 0 107.69 15.50 2 -16 0 74.99 13.60 2 -16 0 60.39 14.00 -2 16 0 78.39 14.90 -2 -16 0 80.39 14.70 -2 -17 0 -7.30 7.50 2 17 0 -0.20 9.10 -2 -17 0 -4.30 7.80 2 -17 0 -5.50 7.40 -2 17 0 4.30 7.80 2 17 0 -0.50 6.50 -2 17 0 -8.70 5.50 -2 -17 0 -5.10 7.50 2 -17 0 9.50 8.30 2 -17 0 6.10 7.90 2 17 0 -5.00 6.80 2 -17 0 -5.60 7.70 -2 -17 0 -7.60 5.60 -2 17 0 -1.70 8.00 2 18 0 597.14 41.10 -2 18 0 508.35 36.50 -2 -18 0 516.45 38.40 2 18 0 476.85 36.90 -2 18 0 481.15 37.60 -2 -18 0 519.55 41.30 2 -18 0 407.56 41.30 -2 -18 0 563.04 42.00 2 18 0 476.15 35.10 2 -18 0 537.45 37.70 -2 -18 0 500.55 37.80 2 -18 0 502.25 39.10 2 -18 0 539.45 41.30 2 19 0 3.40 6.50 -2 19 0 1.20 7.20 -2 -19 0 -7.10 6.80 2 -19 0 -4.50 8.30 -2 -19 0 -2.60 8.80 2 19 0 3.50 8.30 -2 19 0 4.50 8.80 -2 -19 0 -2.90 8.40 2 -19 0 2.70 8.80 2 20 0 340.97 30.50 -2 20 0 271.37 28.30 -2 20 0 340.97 33.70 2 20 0 251.17 28.50 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0 775.22 45.40 -3 -11 0 744.03 46.70 3 11 0 792.02 43.90 3 12 0 -3.80 4.30 -3 12 0 -4.90 5.00 -3 -12 0 11.00 5.70 3 -12 0 1.50 5.40 -3 12 0 2.30 5.20 -3 -12 0 -1.40 5.40 3 -12 0 8.50 5.70 -3 -12 0 3.00 6.00 -3 -12 0 2.70 5.70 3 -12 0 4.80 5.50 3 -12 0 -1.70 5.70 3 12 0 2.60 5.20 3 -12 0 8.00 6.70 -3 -12 0 -1.50 3.70 -3 12 0 2.90 4.90 3 12 0 0.90 6.00 -3 12 0 -10.10 5.90 3 12 0 1.10 4.00 -3 12 0 -3.20 5.10 -3 12 0 -7.10 4.80 3 13 0 13.40 6.90 -3 13 0 11.60 7.20 -3 13 0 11.20 6.90 -3 13 0 17.10 6.80 3 -13 0 16.70 7.30 3 13 0 8.10 5.10 -3 13 0 21.80 7.80 -3 -13 0 8.10 7.70 -3 -13 0 18.30 7.70 -3 -13 0 19.10 5.50 3 -13 0 23.40 8.60 -3 -13 0 9.60 6.40 3 -13 0 16.90 8.20 -3 -13 0 1.40 6.20 3 13 0 18.20 8.00 3 -13 0 8.50 5.70 3 13 0 17.70 6.80 -3 13 0 14.60 7.60 3 -13 0 17.90 8.10 3 -14 0 -5.10 5.80 3 -14 0 2.70 6.10 -3 -14 0 -6.60 6.30 3 14 0 -1.20 5.10 -3 -14 0 6.20 7.30 -3 14 0 8.60 6.70 3 -14 0 0.70 5.70 -3 14 0 2.00 5.80 -3 -14 0 -2.20 4.30 3 14 0 1.30 7.00 -3 14 0 -2.20 5.50 3 -14 0 4.80 7.70 3 14 0 -4.60 5.50 -3 14 0 -4.50 4.70 -3 -14 0 4.70 5.70 -3 14 0 1.80 5.90 3 14 0 1.00 4.50 -3 -14 0 1.60 7.30 -3 15 0 198.18 21.10 -3 15 0 177.08 19.30 -3 -15 0 219.78 21.70 -3 -15 0 195.88 23.60 3 -15 0 190.18 22.10 3 -15 0 135.59 20.20 -3 15 0 174.98 20.40 3 -15 0 172.18 19.40 3 15 0 158.18 18.70 -3 -15 0 194.48 21.90 3 -15 0 218.38 24.80 3 15 0 160.98 17.70 -3 -15 0 167.88 21.90 3 15 0 200.98 22.80 -3 -16 0 8.60 8.00 3 -16 0 1.70 6.60 -3 16 0 11.60 7.50 3 -16 0 -6.30 6.20 3 16 0 -1.90 8.30 -3 -16 0 10.20 6.70 -3 -16 0 -3.90 7.10 3 16 0 9.30 7.00 -3 -16 0 1.50 7.70 3 -16 0 -10.00 5.90 3 16 0 -0.70 5.40 -3 16 0 -4.60 6.60 -3 16 0 -6.70 6.70 3 -16 0 4.10 7.60 3 -17 0 -14.20 6.10 3 17 0 -1.50 6.50 -3 17 0 -2.40 7.90 -3 -17 0 -2.40 6.10 3 -17 0 -1.70 8.20 -3 -17 0 -5.50 7.70 3 17 0 -1.20 5.90 3 -17 0 -4.70 7.20 -3 -17 0 -0.80 8.10 3 -17 0 0.20 7.80 -3 17 0 3.90 6.80 3 17 0 1.00 9.20 -3 -17 0 0.60 8.60 -3 17 0 0.80 6.90 3 18 0 -1.80 7.00 -3 -18 0 4.80 8.40 -3 -18 0 -0.50 7.00 -3 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466.55 26.80 5 4 0 1.60 3.50 5 4 0 -4.20 1.80 5 4 0 -0.90 1.70 -5 4 0 2.80 3.10 -5 -4 0 0.00 3.50 5 -4 0 1.40 3.00 -5 -4 0 -0.60 3.20 -5 4 0 -2.30 2.10 -5 -4 0 -1.80 2.60 -5 4 0 -4.90 2.50 5 -4 0 0.50 2.70 5 4 0 -0.60 3.60 -5 -4 0 -1.40 2.30 -5 4 0 -2.80 2.70 5 -4 0 0.30 2.70 5 4 0 -0.80 1.90 -5 4 0 -1.40 2.60 -5 -4 0 -2.90 2.30 5 -4 0 2.60 2.70 5 4 0 4.40 2.70 5 -4 0 2.10 3.10 5 -5 0 81.29 9.10 -5 5 0 74.89 9.00 5 5 0 65.89 8.20 5 -5 0 64.29 9.70 5 5 0 102.69 8.60 5 5 0 97.19 11.70 -5 -5 0 73.29 9.80 5 -5 0 89.99 9.80 -5 5 0 68.39 8.30 -5 -5 0 91.39 8.90 -5 5 0 82.19 9.60 5 -5 0 81.19 9.40 -5 5 0 94.19 11.10 5 -5 0 95.59 9.90 5 5 0 116.59 12.20 -5 5 0 81.09 9.70 5 5 0 91.79 6.70 5 5 0 84.19 7.20 -5 -5 0 94.69 9.50 -5 -5 0 95.69 11.40 5 -5 0 91.99 9.90 -5 -5 0 77.89 8.40 -5 6 0 2.80 4.00 -5 -6 0 -0.30 2.90 5 6 0 -6.40 2.90 -5 6 0 -0.40 3.60 5 -6 0 -3.60 3.30 5 -6 0 -3.80 2.80 -5 -6 0 0.30 3.40 5 6 0 2.80 2.30 -5 6 0 -7.10 2.90 5 6 0 0.00 4.00 -5 6 0 0.60 3.10 -5 -6 0 0.00 4.20 5 6 0 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617.64 35.60 -5 -11 0 592.94 40.10 -5 11 0 581.84 36.90 -5 11 0 599.84 37.50 5 -11 0 640.94 40.60 5 -11 0 577.24 40.30 -5 11 0 625.24 38.60 5 11 0 657.33 40.90 5 11 0 582.94 34.60 -5 12 0 4.80 6.70 5 -12 0 3.20 6.20 -5 12 0 2.00 5.40 5 12 0 -3.30 3.70 -5 12 0 -5.30 4.80 5 12 0 -4.30 3.90 5 -12 0 1.90 5.60 5 12 0 -4.20 3.80 -5 -12 0 5.80 6.20 -5 -12 0 5.60 6.50 -5 12 0 3.90 5.50 -5 -12 0 3.20 5.00 5 -12 0 -3.70 5.00 5 -12 0 -0.10 5.00 -5 -12 0 10.80 7.40 -5 12 0 -0.10 4.40 5 -12 0 5.60 5.60 5 12 0 -13.20 4.90 5 13 0 307.27 22.80 -5 13 0 330.07 24.30 5 -13 0 260.97 27.60 -5 13 0 360.36 25.70 5 -13 0 301.67 29.00 5 13 0 275.07 22.50 -5 13 0 346.87 25.20 -5 -13 0 328.87 30.10 5 13 0 271.37 27.60 5 13 0 290.37 21.70 -5 -13 0 313.67 30.00 -5 -13 0 281.37 23.00 -5 13 0 337.27 25.80 -5 -13 0 322.17 26.60 5 -13 0 311.57 24.30 5 -13 0 347.07 24.90 5 -13 0 334.27 27.10 -5 -14 0 3.20 7.10 -5 14 0 10.50 7.70 -5 14 0 8.50 7.10 5 -14 0 -3.20 6.20 -5 -14 0 7.50 5.80 -5 -14 0 3.70 7.20 5 14 0 20.50 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72.39 7.90 6 4 0 68.49 7.60 6 -4 0 64.49 7.80 -6 -4 0 71.49 9.90 6 4 0 51.99 9.00 -6 4 0 56.99 7.40 6 4 0 57.69 6.70 6 4 0 59.99 6.50 -6 -4 0 61.49 6.80 6 -4 0 49.80 7.20 -6 -5 0 5.40 4.60 6 -5 0 -1.80 3.60 -6 5 0 -0.10 3.60 -6 5 0 -3.40 3.00 6 -5 0 -1.60 3.80 -6 5 0 0.90 3.80 6 5 0 0.50 4.30 6 -5 0 -0.70 3.50 -6 5 0 -3.60 3.90 -6 -5 0 2.30 3.40 -6 5 0 -1.10 2.80 6 5 0 -0.60 2.10 6 5 0 -2.90 2.70 6 5 0 2.30 2.50 6 -5 0 -0.90 3.50 -6 -5 0 -0.80 2.80 6 5 0 0.90 3.90 -6 -5 0 -1.20 2.70 6 5 0 -1.60 2.60 6 -5 0 1.30 3.20 -6 -5 0 -1.10 4.00 6 -6 0 65.69 9.30 6 6 0 64.29 8.80 6 6 0 51.09 6.30 -6 6 0 53.69 8.80 6 6 0 57.39 7.20 6 -6 0 76.19 9.60 -6 6 0 57.69 8.50 -6 -6 0 33.20 8.40 -6 6 0 48.00 7.90 6 -6 0 69.69 8.90 6 6 0 59.59 10.10 -6 -6 0 50.89 7.80 6 6 0 56.39 6.30 6 -6 0 54.39 8.80 -6 -6 0 73.49 8.40 -6 -6 0 63.39 7.90 -6 -6 0 49.70 9.40 6 -6 0 55.29 9.50 -6 6 0 61.49 8.50 -6 6 0 72.69 10.60 6 6 0 60.39 10.00 6 -7 0 -0.30 4.50 -6 7 0 -0.80 4.60 6 -7 0 -4.10 4.40 -6 7 0 -0.20 3.50 6 7 0 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5.30 -6 -9 0 3.40 5.90 -6 10 0 -1.40 5.20 6 -10 0 0.80 4.90 -6 10 0 2.60 4.90 6 10 0 5.90 6.10 6 10 0 -3.10 3.50 -6 -10 0 5.80 6.00 6 -10 0 -2.10 4.80 6 -10 0 -0.20 5.10 -6 -10 0 -3.00 4.90 -6 10 0 -3.00 3.80 6 10 0 -4.20 4.40 6 10 0 1.90 3.60 6 10 0 -4.00 4.20 -6 -10 0 -1.40 4.60 -6 10 0 0.10 4.20 -6 -10 0 -7.40 3.10 -6 10 0 7.00 5.80 6 -10 0 4.60 5.40 6 -11 0 0.50 5.10 -6 -11 0 -0.20 5.00 -6 -11 0 -1.00 5.10 -6 11 0 -0.60 5.20 6 -11 0 -4.30 4.50 6 11 0 3.20 4.50 -6 -11 0 -5.80 4.90 6 11 0 -5.40 5.80 6 -11 0 -3.30 4.70 -6 11 0 0.50 4.60 6 11 0 -4.60 4.20 -6 11 0 -2.40 5.60 6 -11 0 -2.30 5.30 -6 11 0 2.00 5.70 6 11 0 -3.00 3.20 -6 -11 0 4.20 4.50 6 -12 0 195.68 20.60 6 -12 0 194.08 22.70 -6 12 0 216.28 21.00 6 12 0 228.98 23.60 -6 -12 0 206.28 23.00 6 -12 0 204.88 22.30 6 12 0 248.38 18.20 -6 -12 0 223.58 24.20 -6 12 0 214.38 21.00 -6 -12 0 170.38 20.30 6 12 0 220.68 20.00 -6 12 0 230.08 24.60 -6 12 0 253.27 23.70 -6 12 0 247.88 22.40 6 12 0 228.58 16.90 6 -12 0 274.17 26.00 -6 -12 0 235.68 18.50 6 -12 0 210.48 20.80 6 -13 0 -0.70 5.50 -6 13 0 5.70 5.90 -6 -13 0 4.30 6.70 6 -13 0 -0.40 5.80 6 -13 0 -6.00 6.50 -6 13 0 -4.30 5.10 6 13 0 -1.90 4.90 6 13 0 -3.50 3.90 -6 -13 0 -7.40 6.40 6 13 0 3.40 5.40 6 -13 0 -4.00 6.10 6 -13 0 -1.70 5.90 -6 13 0 -6.20 5.20 6 13 0 -0.30 6.70 -6 -13 0 -3.60 4.20 -6 -13 0 -2.60 6.10 -6 14 0 61.39 11.60 -6 -14 0 67.69 10.80 6 14 0 67.49 14.50 6 -14 0 55.19 11.60 6 -14 0 45.60 11.40 6 -14 0 60.19 12.60 -6 -14 0 85.99 15.80 6 -14 0 41.20 11.40 6 -14 0 56.59 13.10 -6 14 0 58.69 12.50 6 14 0 81.09 12.40 -6 -14 0 53.69 12.10 6 14 0 57.29 10.20 -6 -14 0 88.59 15.70 -6 14 0 80.89 13.30 6 -15 0 -2.00 6.30 6 -15 0 -1.90 7.40 -6 15 0 0.10 6.60 6 15 0 2.40 5.70 6 -15 0 1.60 7.70 6 15 0 -1.90 5.20 -6 15 0 -8.80 6.20 -6 -15 0 4.70 7.80 -6 -15 0 -7.70 4.40 -6 -15 0 -11.70 6.80 -6 15 0 -2.60 6.10 -6 -15 0 -5.30 6.30 6 -15 0 -1.80 6.60 6 15 0 -0.70 8.40 6 -16 0 175.28 23.60 -6 16 0 190.08 23.50 6 16 0 186.18 20.70 -6 16 0 213.38 22.90 -6 -16 0 214.88 26.30 6 -16 0 169.78 23.40 6 -16 0 186.88 21.40 -6 -16 0 184.08 20.20 6 -16 0 232.48 26.40 -6 16 0 146.29 19.40 -6 -16 0 187.78 23.60 -6 -16 0 233.98 26.10 6 16 0 179.08 19.00 6 -17 0 0.80 7.10 -6 -17 0 -7.10 8.10 -6 -17 0 -0.70 8.80 6 -17 0 -0.80 8.30 -6 -17 0 1.80 6.10 6 -17 0 7.50 9.70 6 17 0 1.90 6.40 -6 17 0 -8.00 6.70 6 17 0 -5.40 5.80 6 -17 0 8.40 9.50 -6 17 0 -16.20 6.60 -6 -17 0 -2.50 8.40 6 -18 0 39.80 13.80 6 18 0 61.79 11.70 -6 -18 0 48.90 14.60 -6 18 0 45.40 12.20 -6 -18 0 18.30 11.50 6 18 0 41.60 11.70 6 -18 0 25.80 11.60 6 -18 0 37.80 13.60 -6 18 0 33.50 12.90 -6 -18 0 31.60 10.50 -6 -18 0 28.70 11.80 6 19 0 3.00 7.60 -6 19 0 -1.10 8.20 -6 19 0 -11.20 8.90 6 19 0 -2.30 7.80 6 -19 0 7.70 11.50 6 -19 0 8.30 9.40 -6 -19 0 20.80 11.50 -6 -19 0 -3.80 8.90 -6 20 0 130.59 21.50 -6 20 0 150.08 21.50 6 20 0 122.19 18.80 6 -20 0 122.29 21.80 6 20 0 124.09 18.40 6 21 0 -2.90 7.30 -6 21 0 -2.90 9.60 6 21 0 4.70 9.90 -6 21 0 -5.10 7.80 7 0 0 1.20 2.50 -7 0 0 4.10 2.50 7 0 0 3.40 3.10 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377.06 25.60 -7 3 0 375.26 23.00 7 3 0 394.06 22.00 -7 -3 0 413.96 22.10 7 -3 0 381.26 23.40 -7 3 0 410.26 26.00 7 -3 0 390.76 25.70 7 -3 0 403.26 24.20 7 3 0 392.56 24.10 -7 3 0 413.56 23.60 7 4 0 2.50 3.00 7 4 0 1.20 3.60 -7 4 0 0.70 4.10 7 -4 0 -1.70 3.00 7 4 0 3.30 4.60 -7 -4 0 3.90 3.00 7 -4 0 -2.50 3.10 -7 -4 0 -6.20 3.50 7 4 0 -3.20 2.90 7 -4 0 0.10 3.10 -7 -4 0 3.30 4.40 -7 -4 0 3.70 3.30 -7 4 0 2.90 3.30 -7 4 0 -1.40 3.00 7 -4 0 2.20 3.80 7 4 0 0.90 2.50 -7 4 0 1.80 3.70 7 -4 0 -0.80 3.10 -7 4 0 -3.00 3.00 7 4 0 0.10 2.20 7 4 0 5.40 3.00 -7 -5 0 1496.15 78.29 -7 5 0 1573.94 77.29 -7 5 0 1475.25 78.99 -7 5 0 1486.15 78.09 7 5 0 1508.35 78.49 7 5 0 1570.54 83.69 7 5 0 1478.35 74.29 7 -5 0 1491.75 82.39 -7 -5 0 1407.86 82.99 -7 5 0 1561.24 77.19 7 5 0 1550.54 81.09 7 5 0 1450.55 74.19 -7 -5 0 1515.25 81.29 -7 5 0 1446.86 82.19 7 -5 0 1536.35 77.39 -7 -5 0 1497.45 79.19 7 -5 0 1422.96 76.79 7 -5 0 1452.75 77.99 7 -5 0 1462.95 78.99 -7 -5 0 1546.95 79.19 7 5 0 1456.15 75.59 -7 -6 0 3.50 5.40 -7 -6 0 -4.30 3.20 -7 -6 0 0.10 4.60 7 6 0 -4.00 2.30 7 6 0 6.50 3.90 7 6 0 3.40 3.00 -7 6 0 5.20 4.50 -7 -6 0 6.50 3.90 -7 6 0 1.80 4.40 -7 6 0 2.40 4.90 -7 6 0 -2.40 3.30 7 -6 0 -0.90 4.00 7 6 0 0.80 4.40 -7 -6 0 -1.40 3.20 7 -6 0 0.20 3.80 -7 6 0 -0.60 3.80 7 6 0 2.40 3.30 7 -6 0 2.40 4.10 7 6 0 -5.10 4.60 7 -6 0 0.50 4.40 -7 7 0 353.66 23.90 7 7 0 335.27 25.90 -7 7 0 368.36 23.30 7 7 0 346.37 20.20 -7 7 0 331.87 25.50 7 -7 0 280.37 22.40 -7 7 0 321.67 23.00 -7 -7 0 345.97 26.00 -7 7 0 315.87 23.20 -7 -7 0 344.37 22.30 7 -7 0 315.57 23.70 7 7 0 337.57 25.20 -7 -7 0 349.77 23.00 7 7 0 387.26 23.80 7 -7 0 386.46 23.70 7 7 0 373.66 20.70 7 7 0 351.26 21.40 -7 -7 0 297.07 24.60 7 -7 0 351.86 24.00 -7 -7 0 353.96 22.50 7 -7 0 345.37 25.60 -7 -8 0 -2.80 4.70 7 -8 0 -5.00 3.80 -7 -8 0 2.60 3.40 7 8 0 2.40 5.80 -7 -8 0 0.90 5.30 7 8 0 -4.60 3.30 7 -8 0 1.20 4.60 -7 -8 0 -2.70 4.00 -7 8 0 2.70 4.80 -7 8 0 -4.60 4.60 7 8 0 -0.40 2.70 -7 8 0 4.20 5.30 -7 -8 0 0.00 3.70 7 8 0 4.80 3.40 7 8 0 -4.20 4.60 -7 8 0 4.60 5.10 -7 8 0 -3.60 3.70 7 -8 0 -0.60 4.40 7 -8 0 2.20 4.90 7 8 0 -0.60 3.80 7 -9 0 871.81 53.19 -7 9 0 838.02 50.79 7 -9 0 879.11 50.79 7 -9 0 885.31 51.19 -7 9 0 903.81 50.29 7 9 0 847.12 46.00 -7 -9 0 819.42 49.90 -7 -9 0 862.61 48.90 -7 -9 0 759.72 52.29 7 9 0 888.91 50.69 7 -9 0 842.82 49.60 -7 9 0 851.21 48.80 7 9 0 844.12 47.00 -7 9 0 867.91 53.29 7 9 0 870.21 45.70 7 -9 0 888.71 49.40 -7 -9 0 832.32 51.89 -7 9 0 904.11 49.30 7 9 0 832.82 52.99 7 10 0 -1.50 3.10 -7 10 0 7.80 6.70 -7 10 0 -1.80 3.90 7 10 0 -1.00 3.90 7 -10 0 1.00 5.00 7 -10 0 0.80 5.00 7 -10 0 -4.30 4.50 -7 -10 0 -2.50 3.50 7 -10 0 -3.40 5.10 -7 10 0 0.60 5.80 -7 -10 0 4.80 5.90 -7 -10 0 2.50 5.70 7 10 0 -6.70 4.70 -7 -10 0 2.00 4.80 7 10 0 -2.30 3.40 7 -10 0 5.40 5.90 7 10 0 1.00 6.00 -7 10 0 -1.50 4.40 -7 -11 0 600.04 36.40 7 -11 0 518.65 39.50 -7 11 0 586.74 36.90 -7 -11 0 556.34 40.10 -7 -11 0 556.84 39.70 7 11 0 586.04 34.50 7 11 0 639.84 41.20 7 -11 0 569.94 37.60 7 -11 0 611.44 38.10 -7 11 0 560.24 37.70 -7 -11 0 604.54 38.60 -7 11 0 646.44 41.80 7 11 0 606.14 34.00 7 -11 0 532.85 38.50 7 11 0 605.94 38.80 7 11 0 583.54 35.20 -7 12 0 3.00 5.60 -7 -12 0 2.70 4.90 7 12 0 -4.10 6.00 -7 -12 0 1.00 6.40 -7 12 0 -3.80 5.80 -7 -12 0 2.00 6.30 7 -12 0 1.00 6.10 -7 -12 0 3.00 6.40 7 12 0 5.00 5.10 -7 12 0 -0.50 4.50 7 -12 0 -2.00 5.60 7 12 0 1.00 3.90 7 12 0 -1.10 4.20 7 -12 0 4.90 6.50 7 -12 0 -2.80 5.90 7 13 0 433.96 28.50 7 13 0 451.05 34.00 7 13 0 392.96 26.70 -7 -13 0 444.66 32.10 -7 13 0 430.06 31.50 7 -13 0 386.76 29.80 -7 -13 0 417.26 33.00 7 -13 0 422.96 33.20 7 13 0 395.06 27.40 7 -13 0 419.26 32.40 7 -13 0 436.26 30.40 -7 -13 0 387.66 32.20 -7 13 0 399.16 29.50 7 -13 0 413.36 32.20 -7 -13 0 389.76 28.20 -7 14 0 -8.70 5.30 -7 -14 0 2.30 7.40 7 -14 0 -2.60 6.30 -7 -14 0 -1.30 7.00 7 14 0 0.00 5.60 -7 -14 0 2.50 6.60 7 -14 0 5.00 7.60 7 -14 0 -4.30 6.10 7 14 0 -6.40 7.40 7 14 0 1.50 4.90 -7 14 0 1.90 7.30 7 -14 0 -0.80 6.90 7 -14 0 -4.80 6.90 -7 -14 0 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64.69 17.20 7 -20 0 -1.10 9.40 -7 20 0 -9.90 8.20 7 20 0 4.80 7.90 -7 20 0 -1.40 9.90 7 20 0 -9.60 7.50 -7 21 0 94.09 18.50 7 21 0 106.59 17.90 -7 21 0 81.99 18.60 8 0 0 113.79 10.20 -8 0 0 105.19 8.50 8 0 0 118.89 10.30 -8 0 0 109.29 9.60 8 0 0 106.49 10.80 8 0 0 126.19 12.40 8 -1 0 -0.70 3.10 -8 1 0 -1.40 2.50 8 1 0 -1.20 3.30 8 -1 0 -3.60 3.50 8 1 0 -3.30 2.60 -8 -1 0 -0.40 2.00 8 1 0 1.70 2.60 -8 1 0 -0.50 1.60 8 -1 0 -4.80 2.70 8 1 0 1.40 2.80 -8 -1 0 -4.40 2.90 8 1 0 -3.60 3.70 -8 -1 0 -1.00 2.60 8 -1 0 -0.50 1.60 8 -1 0 -1.50 3.00 -8 -1 0 -2.10 2.30 8 1 0 -2.10 3.30 8 2 0 4.00 3.70 -8 -2 0 4.60 2.40 8 -2 0 5.30 4.70 -8 2 0 1.10 2.30 8 -2 0 -1.90 3.10 8 -2 0 9.40 2.70 8 2 0 7.20 2.00 -8 -2 0 4.70 3.70 8 2 0 0.00 4.10 8 2 0 3.40 3.40 8 2 0 0.70 2.50 -8 -2 0 0.20 2.90 8 2 0 4.20 2.00 -8 -2 0 1.00 1.90 8 -2 0 1.00 3.00 -8 2 0 -0.60 3.00 8 2 0 2.30 4.50 8 2 0 3.50 3.00 8 -2 0 1.90 3.80 8 -3 0 6.20 3.00 -8 -3 0 0.40 1.50 8 3 0 -0.80 2.40 -8 -3 0 -2.50 2.80 -8 3 0 0.10 3.50 -8 -3 0 1.30 2.40 8 -3 0 -3.30 3.10 8 3 0 -3.60 3.70 8 3 0 -1.10 2.50 8 3 0 -0.80 2.30 -8 3 0 -9.10 2.90 -8 -3 0 -8.20 3.20 -8 3 0 1.40 3.30 8 3 0 -3.20 4.40 8 -3 0 2.30 3.80 8 -3 0 -2.60 3.50 -8 3 0 -1.80 2.80 8 -3 0 -5.20 3.30 8 3 0 0.10 3.00 8 3 0 2.40 3.40 -8 3 0 3.50 3.70 -8 -4 0 170.98 17.80 8 -4 0 153.68 14.10 -8 4 0 145.19 13.50 -8 -4 0 163.98 11.60 -8 4 0 197.38 15.70 8 4 0 147.29 11.50 -8 4 0 148.19 14.40 8 -4 0 114.39 12.90 8 4 0 196.28 18.00 -8 4 0 143.09 15.60 8 -4 0 181.08 12.70 -8 4 0 144.89 12.30 8 -4 0 169.28 16.70 8 4 0 164.08 13.20 -8 -4 0 169.18 12.80 8 4 0 165.88 11.10 -8 -4 0 171.58 17.50 8 4 0 159.98 17.40 8 4 0 172.58 11.40 8 -4 0 164.18 15.20 8 4 0 151.08 12.00 8 -5 0 -1.80 4.00 -8 -5 0 0.60 5.00 -8 -5 0 -0.50 3.30 8 -5 0 -2.50 3.70 8 -5 0 0.60 4.10 -8 5 0 0.00 3.70 8 5 0 1.40 4.50 -8 5 0 3.20 4.50 -8 -5 0 -1.40 4.50 8 5 0 -4.40 2.20 -8 -5 0 4.70 3.80 8 5 0 -3.50 4.70 8 5 0 6.00 3.30 8 -5 0 -1.90 3.80 -8 5 0 -2.30 3.60 8 5 0 -3.90 3.00 8 5 0 0.00 3.50 8 -5 0 -7.20 2.90 8 5 0 -3.60 3.00 -8 5 0 6.50 4.20 -8 6 0 57.99 8.90 -8 -6 0 70.39 8.60 8 -6 0 48.60 8.60 -8 6 0 64.89 9.40 8 6 0 68.29 11.30 -8 -6 0 66.09 8.40 8 -6 0 62.79 9.60 8 6 0 64.09 7.10 -8 -6 0 61.39 11.20 -8 -6 0 69.09 8.70 -8 6 0 42.80 8.80 8 6 0 60.99 7.20 8 -6 0 60.29 10.70 8 6 0 63.19 8.00 8 6 0 61.69 8.40 -8 -6 0 60.89 10.80 8 -6 0 63.29 9.10 8 6 0 51.19 10.50 -8 6 0 54.49 10.00 8 -7 0 9.10 4.90 8 7 0 -4.80 3.60 8 -7 0 2.70 5.00 8 7 0 -7.80 4.40 -8 -7 0 -0.10 3.30 -8 7 0 -0.60 4.50 8 -7 0 -2.20 3.90 -8 -7 0 -2.20 3.10 -8 7 0 5.00 4.20 -8 -7 0 0.30 3.80 -8 7 0 0.30 4.40 8 -7 0 1.30 4.70 8 7 0 2.40 3.50 -8 -7 0 -2.70 4.50 -8 -7 0 7.30 6.00 -8 7 0 -2.20 4.50 8 7 0 12.20 6.30 8 -7 0 1.70 4.40 8 7 0 -0.30 2.70 8 7 0 2.30 2.90 8 -8 0 3.60 4.80 8 8 0 -2.40 4.20 8 -8 0 1.30 5.10 -8 8 0 -1.50 4.40 -8 -8 0 2.50 3.90 8 8 0 -0.40 2.80 -8 8 0 5.00 5.50 -8 -8 0 0.00 5.90 -8 -8 0 0.60 5.40 8 8 0 6.50 6.10 -8 8 0 -1.70 4.80 -8 8 0 2.20 4.40 8 -8 0 -3.10 3.90 8 -8 0 11.40 5.40 -8 -8 0 5.00 4.40 8 8 0 4.20 3.40 -8 -8 0 4.70 4.20 8 8 0 3.60 3.70 8 9 0 0.00 3.30 8 9 0 5.50 3.70 8 9 0 -3.70 3.70 -8 9 0 4.70 5.40 -8 -9 0 3.10 5.70 -8 -9 0 -1.40 4.30 -8 9 0 5.50 5.70 -8 -9 0 -3.60 3.30 -8 -9 0 4.60 4.50 8 -9 0 -1.20 5.00 -8 9 0 0.70 5.90 8 -9 0 -7.00 4.10 -8 9 0 0.40 4.20 8 -9 0 -1.60 4.50 8 -9 0 -3.00 4.70 8 9 0 1.80 3.90 -8 -9 0 2.90 5.80 8 9 0 -4.60 5.60 8 -10 0 -4.40 4.80 8 10 0 2.40 3.40 -8 10 0 -3.10 4.20 8 -10 0 -2.50 5.10 -8 -10 0 -1.50 5.70 8 -10 0 -0.70 5.50 8 10 0 3.30 5.50 -8 -10 0 -1.10 4.80 8 10 0 -3.30 6.30 -8 10 0 6.70 6.40 -8 10 0 -9.30 5.00 -8 10 0 3.50 5.80 8 10 0 -0.10 4.30 -8 -10 0 2.00 4.20 8 -10 0 -9.30 4.50 -8 -10 0 3.70 5.70 8 -10 0 0.80 4.90 8 10 0 -2.90 3.50 -8 -10 0 14.10 5.80 8 -11 0 0.10 5.80 -8 11 0 -3.10 4.80 8 -11 0 4.50 6.20 -8 11 0 12.30 7.20 8 11 0 -0.50 4.60 -8 -11 0 4.80 5.70 8 -11 0 -2.10 5.80 -8 -11 0 -3.00 5.60 -8 -11 0 -3.50 5.80 8 11 0 -1.10 5.50 8 -11 0 8.00 6.20 8 -11 0 8.30 6.10 8 11 0 -3.20 3.80 -8 11 0 1.00 6.10 -8 -11 0 0.80 4.30 8 11 0 0.60 6.80 8 11 0 -3.30 3.10 8 -12 0 22.20 8.00 -8 -12 0 5.00 7.70 8 12 0 26.60 10.10 -8 12 0 12.30 7.30 -8 -12 0 5.60 4.90 -8 -12 0 3.80 6.60 8 -12 0 18.50 8.60 8 12 0 16.80 5.60 -8 -12 0 10.40 8.00 8 12 0 19.30 7.00 8 12 0 15.10 6.00 8 -12 0 5.50 7.10 -8 12 0 12.30 8.70 8 -12 0 25.10 9.10 -8 12 0 18.30 7.40 8 -13 0 -3.60 6.50 -8 13 0 16.80 8.50 8 -13 0 7.80 7.50 8 13 0 8.10 6.20 8 -13 0 -3.90 6.30 8 13 0 4.60 5.50 -8 -13 0 3.90 5.20 8 -13 0 -8.70 5.90 -8 13 0 8.70 7.00 -8 -13 0 2.50 7.60 -8 -13 0 1.80 7.50 -8 -13 0 -5.30 4.50 8 13 0 -2.60 7.90 8 13 0 0.60 4.40 8 -14 0 -3.80 6.20 -8 -14 0 2.70 6.70 -8 14 0 3.10 6.90 8 14 0 -1.30 4.40 8 14 0 -1.70 5.60 -8 -14 0 -5.50 7.70 8 -14 0 2.90 7.30 8 -14 0 -3.90 7.40 -8 14 0 7.30 6.80 8 -14 0 -0.90 6.30 -8 -14 0 -2.00 4.80 -8 -14 0 -0.10 7.90 -8 15 0 -2.10 6.50 -8 -15 0 -0.10 8.40 -8 -15 0 -4.80 7.30 8 -15 0 0.00 7.40 8 15 0 0.80 4.70 8 15 0 -2.60 5.80 -8 -15 0 0.20 7.20 -8 -15 0 9.20 6.40 -8 15 0 6.10 8.40 8 -15 0 0.00 7.90 8 -15 0 19.90 9.40 8 -15 0 0.00 7.70 -8 -16 0 89.79 17.90 8 16 0 65.39 12.40 -8 16 0 39.10 12.00 -8 -16 0 63.39 11.60 -8 16 0 50.59 12.90 -8 -16 0 73.79 15.50 8 -16 0 58.49 14.40 8 16 0 64.89 11.40 8 -16 0 64.59 13.40 8 -16 0 65.89 15.60 8 -16 0 55.49 14.50 -8 -16 0 58.59 14.10 -8 -17 0 3.70 8.80 8 -17 0 4.10 9.00 8 17 0 -9.90 6.30 8 17 0 -1.30 6.00 8 -17 0 -9.30 7.70 -8 -17 0 9.60 10.00 -8 17 0 -9.50 6.50 -8 -17 0 0.90 6.20 8 -17 0 -6.60 8.00 -8 17 0 -12.80 7.90 -8 -17 0 -2.90 8.70 8 18 0 3.80 6.50 8 -18 0 17.90 11.20 -8 -18 0 4.00 9.20 8 -18 0 1.80 9.20 -8 18 0 -3.80 9.10 -8 18 0 12.20 9.40 8 18 0 -0.50 7.70 8 -18 0 -0.40 9.60 8 19 0 -8.10 6.20 -8 -19 0 -3.10 10.40 -8 19 0 -5.40 7.60 8 19 0 -1.70 7.70 8 -19 0 -8.20 9.30 -8 19 0 -10.80 9.00 8 20 0 7.20 8.20 -8 20 0 6.30 9.60 8 20 0 3.40 9.00 -8 20 0 3.30 10.20 8 -20 0 6.40 10.90 -8 21 0 3.90 10.50 -8 21 0 -2.70 11.10 8 21 0 -9.50 7.10 -9 0 0 4.40 3.60 9 0 0 1.40 4.00 -9 0 0 -0.70 2.30 9 0 0 6.00 4.60 9 0 0 -1.90 2.90 9 0 0 2.10 3.60 9 1 0 304.87 19.00 9 -1 0 323.57 21.40 9 1 0 319.57 21.30 9 -1 0 311.37 16.70 9 1 0 311.57 23.70 9 -1 0 299.07 21.60 9 1 0 267.37 21.90 -9 1 0 305.37 16.70 -9 -1 0 294.87 20.70 9 -1 0 308.57 20.00 9 1 0 313.47 19.20 9 -1 0 307.57 19.70 -9 -1 0 316.77 19.30 9 1 0 301.37 20.20 -9 -1 0 301.47 17.60 9 2 0 0.00 2.80 9 -2 0 1.10 2.30 -9 -2 0 1.50 2.10 9 2 0 0.60 3.40 9 2 0 0.30 1.90 -9 -2 0 5.20 4.00 9 -2 0 1.40 4.50 -9 -2 0 -1.70 2.80 9 2 0 5.80 5.20 9 2 0 0.60 3.20 9 -2 0 0.70 3.60 9 2 0 -2.20 3.30 9 2 0 -0.50 5.30 9 2 0 -0.20 1.80 9 -2 0 -3.40 3.70 -9 2 0 -0.10 2.70 9 -2 0 0.40 3.80 9 -3 0 420.56 26.00 -9 3 0 394.76 23.30 -9 3 0 389.96 25.10 -9 3 0 413.36 24.50 9 -3 0 403.66 25.30 9 -3 0 395.96 26.80 9 -3 0 440.76 27.90 9 -3 0 426.36 23.50 9 3 0 412.06 27.90 9 3 0 395.26 23.00 9 3 0 390.46 22.30 -9 -3 0 381.76 24.90 -9 3 0 378.96 27.00 9 3 0 418.36 24.50 9 3 0 358.96 22.70 9 3 0 397.06 28.90 -9 -3 0 404.46 20.70 9 -3 0 391.66 25.00 -9 -3 0 423.16 28.20 9 3 0 411.96 25.70 9 -4 0 -0.10 3.20 9 4 0 2.50 3.70 -9 4 0 3.40 3.90 9 4 0 -2.10 2.70 -9 4 0 -5.30 3.60 9 4 0 1.70 2.70 -9 -4 0 -4.70 4.40 9 4 0 -4.00 2.70 9 -4 0 -5.30 3.40 9 -4 0 2.40 4.50 -9 -4 0 -1.90 4.40 -9 4 0 -1.90 3.30 9 -4 0 -1.40 3.60 -9 4 0 -0.70 4.30 9 -4 0 2.10 4.70 -9 -4 0 0.90 3.60 9 4 0 1.60 4.90 9 4 0 1.70 3.50 -9 -4 0 -0.40 2.80 9 4 0 1.40 5.20 -9 -5 0 968.00 58.69 9 -5 0 1073.39 56.49 -9 5 0 1027.80 54.79 -9 -5 0 1039.60 55.79 9 5 0 1027.90 52.19 9 5 0 1048.30 56.69 -9 -5 0 1003.80 54.29 9 -5 0 1057.69 55.49 9 5 0 992.60 58.39 -9 -5 0 988.30 60.59 9 5 0 1010.40 53.39 9 -5 0 938.41 58.79 -9 5 0 985.20 59.19 9 -5 0 1001.40 54.99 9 5 0 997.40 52.19 9 5 0 1036.60 54.39 9 -5 0 1022.20 55.39 -9 5 0 1042.60 56.09 -9 5 0 939.91 55.09 9 5 0 1020.10 60.89 -9 6 0 -2.80 3.70 9 6 0 0.80 5.10 9 -6 0 5.30 4.60 -9 6 0 -4.90 4.20 -9 -6 0 6.00 4.00 9 6 0 -2.60 3.10 9 6 0 -0.80 3.30 9 -6 0 -4.60 3.80 -9 -6 0 2.50 3.40 -9 6 0 -1.20 3.70 9 6 0 -2.00 5.60 -9 -6 0 5.10 5.50 9 6 0 2.50 2.90 -9 6 0 -2.70 4.10 9 -6 0 6.90 5.20 -9 -6 0 -3.60 2.90 9 6 0 -3.20 2.40 9 -6 0 0.20 3.80 -9 -6 0 3.40 5.80 -9 7 0 202.08 18.90 9 7 0 196.68 13.70 -9 7 0 203.28 16.50 -9 7 0 178.88 19.50 9 7 0 193.98 14.60 -9 -7 0 153.78 19.50 9 -7 0 204.68 16.50 9 7 0 209.68 15.70 -9 -7 0 197.58 15.10 9 7 0 244.78 23.40 9 -7 0 150.78 18.20 9 -7 0 155.18 16.60 -9 7 0 208.58 18.50 -9 -7 0 220.78 22.00 9 -7 0 163.18 16.70 -9 -7 0 193.48 15.30 -9 -7 0 189.98 14.90 9 7 0 195.88 13.40 -9 8 0 0.90 5.60 -9 -8 0 2.60 3.80 -9 8 0 -6.50 4.00 9 -8 0 1.40 5.20 -9 -8 0 -0.80 3.60 -9 -8 0 -3.20 3.90 -9 8 0 -3.40 4.20 9 -8 0 -2.90 3.90 9 8 0 -3.20 3.60 -9 -8 0 2.80 5.60 9 -8 0 -6.10 3.80 9 8 0 -1.60 3.50 -9 8 0 6.00 4.80 9 8 0 -1.30 2.80 9 8 0 1.00 3.10 -9 -8 0 -5.50 5.30 9 8 0 -2.20 5.40 9 -8 0 -1.10 5.20 -9 -9 0 602.54 37.00 9 -9 0 540.95 39.80 -9 9 0 548.15 36.30 -9 9 0 615.74 38.40 -9 -9 0 669.03 36.60 9 9 0 579.14 33.40 9 -9 0 565.54 36.90 9 -9 0 645.14 39.00 -9 -9 0 613.04 40.30 9 9 0 641.84 34.10 9 9 0 534.15 36.50 -9 9 0 583.14 37.80 9 -9 0 629.44 38.40 -9 9 0 561.54 40.30 -9 -9 0 607.94 35.90 9 9 0 566.54 34.50 9 9 0 601.34 41.30 -9 -9 0 546.45 40.50 9 10 0 5.00 5.60 -9 -10 0 0.90 4.30 9 -10 0 5.90 5.80 -9 -10 0 -3.40 4.80 -9 -10 0 -0.50 3.90 9 10 0 1.60 4.10 -9 -10 0 -2.10 6.30 9 -10 0 1.00 6.00 -9 -10 0 0.50 5.90 -9 10 0 2.40 5.70 -9 10 0 -7.30 5.40 9 -10 0 0.60 5.50 -9 10 0 -1.60 4.40 9 -10 0 5.10 5.90 9 10 0 -2.50 3.30 -9 10 0 -0.80 5.40 9 -10 0 -6.40 4.70 9 10 0 7.10 7.70 9 10 0 -5.90 3.10 -9 11 0 459.05 34.70 9 11 0 446.66 31.60 -9 -11 0 413.56 33.30 9 -11 0 411.66 31.60 -9 -11 0 450.75 31.30 9 11 0 473.25 28.40 9 -11 0 418.46 31.20 9 11 0 445.46 27.40 9 -11 0 459.65 34.40 9 11 0 506.45 35.90 9 -11 0 461.85 31.20 -9 -11 0 450.95 29.70 9 -11 0 448.46 31.60 -9 -11 0 419.46 33.70 -9 11 0 429.96 30.40 -9 -11 0 401.96 28.60 9 11 0 478.85 28.90 -9 11 0 422.36 31.60 -9 -12 0 -3.40 5.90 9 -12 0 -4.20 6.10 -9 12 0 5.60 6.10 9 12 0 0.60 4.40 9 12 0 -7.60 6.60 -9 12 0 0.30 7.30 -9 -12 0 -6.50 5.70 -9 12 0 -0.40 6.50 -9 -12 0 1.50 5.90 9 -12 0 -4.80 5.80 9 -12 0 4.30 6.70 9 12 0 -1.50 4.80 -9 -12 0 1.20 4.40 9 12 0 13.30 6.10 -9 -12 0 5.60 5.60 9 -12 0 8.30 7.50 -9 -13 0 595.74 39.30 -9 -13 0 580.54 42.10 -9 -13 0 550.84 41.20 9 13 0 518.85 34.90 -9 13 0 542.55 38.70 9 -13 0 559.24 38.50 9 -13 0 586.04 38.50 -9 -13 0 520.65 35.40 -9 -13 0 596.64 37.10 -9 13 0 587.24 42.70 9 -13 0 592.54 40.20 -9 13 0 472.85 36.20 9 -13 0 571.54 41.90 9 13 0 561.14 34.10 -9 -14 0 -3.50 5.10 9 14 0 -4.10 4.60 -9 -14 0 3.80 8.50 9 14 0 11.10 7.00 -9 14 0 9.80 8.00 -9 14 0 0.00 6.50 -9 -14 0 -11.10 7.10 -9 -14 0 -7.80 5.70 9 -14 0 1.70 7.60 9 -14 0 2.70 7.20 9 -14 0 -0.30 7.50 9 -15 0 99.29 17.20 -9 15 0 86.59 16.30 -9 -15 0 79.39 15.80 -9 -15 0 104.09 19.00 -9 -15 0 105.49 14.20 -9 -15 0 81.89 16.90 9 15 0 95.79 14.30 9 -15 0 63.89 15.20 -9 15 0 91.69 15.10 9 15 0 97.69 13.00 9 -15 0 105.59 15.90 9 -15 0 113.99 18.80 9 16 0 5.30 6.10 -9 -16 0 -2.50 8.10 9 -16 0 11.80 9.10 -9 -16 0 3.00 9.50 9 16 0 -6.70 6.00 -9 -16 0 -5.00 5.00 -9 16 0 -2.30 7.10 -9 -16 0 -2.30 6.90 -9 16 0 -8.70 8.10 9 -16 0 5.30 8.00 9 -16 0 -13.80 7.60 -9 -17 0 21.50 12.20 -9 17 0 4.00 9.20 9 17 0 12.30 8.70 9 -17 0 10.60 10.60 -9 -17 0 17.70 8.20 -9 -17 0 23.50 12.80 9 -17 0 6.70 10.00 -9 17 0 17.10 10.80 9 -17 0 6.60 10.50 -9 -17 0 12.30 10.10 9 17 0 22.30 8.50 9 18 0 6.70 7.60 -9 -18 0 0.40 9.50 -9 18 0 -11.80 8.20 -9 18 0 8.30 8.80 9 18 0 -9.30 6.50 9 -18 0 -8.00 8.80 9 -18 0 -8.30 8.80 9 -18 0 -12.20 8.00 -9 19 0 169.28 24.70 9 -19 0 239.08 30.40 -9 19 0 188.78 25.10 9 19 0 168.28 20.30 9 19 0 154.48 20.90 9 -20 0 -11.50 9.90 -9 20 0 6.80 8.60 -9 20 0 2.80 10.70 9 20 0 3.50 7.60 9 20 0 -0.80 8.80 10 0 0 161.08 13.00 -10 0 0 180.58 13.60 10 0 0 175.18 16.70 10 0 0 186.38 16.30 10 0 0 144.89 17.20 -10 0 0 148.59 11.70 10 0 0 178.98 13.30 10 1 0 2.20 4.00 10 -1 0 -0.50 4.70 -10 -1 0 -2.10 2.40 10 1 0 -4.20 5.00 10 1 0 -2.40 4.70 10 -1 0 -1.40 1.70 -10 -1 0 4.60 3.80 10 1 0 -4.00 2.90 10 -1 0 0.10 3.80 10 1 0 -1.50 3.10 10 1 0 -1.70 3.50 10 -1 0 -0.80 3.30 -10 1 0 -3.00 1.70 -10 -1 0 -3.00 3.20 10 -1 0 -1.10 3.50 10 -2 0 48.20 8.90 -10 -2 0 41.30 6.60 -10 2 0 41.30 4.90 10 -2 0 36.90 7.20 10 2 0 33.70 6.30 10 2 0 47.50 3.90 10 2 0 45.20 3.80 10 2 0 41.40 7.90 10 2 0 62.29 10.90 -10 -2 0 25.10 6.30 10 2 0 25.60 6.40 10 -2 0 50.19 9.20 10 -2 0 25.00 6.30 10 2 0 54.89 10.20 10 -2 0 47.10 5.10 10 2 0 34.70 6.10 -10 -2 0 47.00 5.20 -10 -3 0 1.10 3.30 10 -3 0 -6.50 3.40 10 3 0 -3.00 3.00 10 3 0 3.80 4.20 10 3 0 0.90 4.90 10 3 0 0.10 3.70 10 3 0 0.20 2.20 10 3 0 -5.60 4.60 -10 -3 0 -1.50 1.80 10 -3 0 -2.10 4.10 10 -3 0 -5.50 3.70 -10 3 0 0.40 4.50 10 -3 0 -6.80 4.20 -10 3 0 -2.30 2.90 -10 3 0 0.90 3.50 10 3 0 -2.00 2.30 10 3 0 -1.20 2.30 -10 3 0 0.90 4.20 -10 -3 0 6.80 4.10 10 -3 0 1.50 2.90 10 4 0 108.79 8.90 -10 4 0 126.89 15.00 10 4 0 128.19 10.90 10 4 0 96.39 13.20 10 -4 0 113.19 12.60 10 -4 0 91.09 12.10 10 4 0 120.59 12.70 10 -4 0 98.99 11.80 -10 -4 0 112.89 11.70 10 -4 0 100.39 10.30 -10 4 0 96.49 10.00 10 -4 0 91.69 13.00 -10 4 0 125.09 12.60 10 4 0 84.39 13.50 -10 4 0 101.59 12.40 -10 -4 0 113.69 15.10 10 4 0 105.89 11.20 -10 -4 0 113.29 9.00 10 4 0 133.49 10.00 -10 5 0 -7.50 3.10 -10 -5 0 -0.10 4.90 -10 -5 0 -6.20 2.90 -10 5 0 -0.40 4.80 10 -5 0 1.10 4.30 10 -5 0 1.40 4.70 -10 -5 0 -3.10 5.10 10 5 0 -2.60 3.90 10 -5 0 -2.20 3.70 10 -5 0 -1.50 3.90 10 5 0 3.20 6.00 10 5 0 -4.80 2.70 -10 -5 0 1.20 3.20 10 5 0 -2.00 4.80 10 5 0 0.10 2.90 -10 5 0 5.20 4.10 10 5 0 -0.70 3.00 -10 5 0 2.30 4.80 10 -5 0 0.90 5.10 10 5 0 1.10 3.70 10 -6 0 325.97 24.70 -10 6 0 301.37 21.30 10 6 0 319.87 20.20 10 6 0 307.97 25.40 -10 6 0 285.37 22.00 10 6 0 295.17 18.80 -10 -6 0 300.97 28.50 10 -6 0 289.87 21.60 -10 -6 0 309.87 20.60 -10 6 0 293.37 24.00 10 6 0 292.67 19.90 10 6 0 336.47 19.30 10 -6 0 301.67 20.90 -10 6 0 280.47 20.60 -10 -6 0 303.47 24.60 10 -6 0 301.37 21.70 10 6 0 288.47 21.40 -10 -6 0 278.77 19.60 10 7 0 -3.90 3.20 10 -7 0 2.10 4.90 -10 -7 0 1.70 3.90 -10 -7 0 -7.50 4.60 10 -7 0 -1.90 4.40 10 -7 0 -8.10 3.90 -10 7 0 -6.70 3.80 -10 7 0 2.50 4.90 10 7 0 3.80 4.20 -10 7 0 -8.70 4.60 -10 -7 0 2.60 5.50 -10 -7 0 0.80 3.90 10 7 0 -0.90 5.80 -10 7 0 3.00 4.50 10 7 0 0.20 3.10 10 -7 0 6.40 5.70 10 7 0 0.80 3.10 -10 -7 0 -3.10 3.30 10 8 0 15.70 5.50 10 8 0 19.60 5.10 -10 -8 0 19.60 7.60 -10 -8 0 22.50 6.70 -10 8 0 18.30 6.90 10 -8 0 18.50 7.00 -10 -8 0 21.10 6.00 10 8 0 13.20 6.20 -10 -8 0 26.70 6.30 10 8 0 -3.10 6.00 10 -8 0 15.50 7.10 -10 8 0 13.10 6.80 -10 8 0 17.20 6.60 10 -8 0 8.80 5.70 -10 8 0 27.70 9.20 -10 -8 0 7.70 7.00 10 8 0 20.80 5.10 10 -9 0 -0.90 5.60 10 -9 0 -4.30 4.90 -10 -9 0 -0.70 4.50 10 9 0 -6.70 3.00 10 -9 0 -3.80 5.40 -10 -9 0 5.30 6.60 10 9 0 5.40 6.10 -10 -9 0 -1.40 4.20 -10 -9 0 -0.40 5.60 -10 -9 0 -2.40 3.40 10 9 0 -6.50 3.40 -10 9 0 -4.60 5.30 -10 9 0 -4.90 5.10 -10 9 0 -4.20 4.20 10 9 0 -4.50 3.90 10 -9 0 -3.70 5.00 -10 9 0 -2.30 5.50 10 9 0 0.30 3.30 10 10 0 -0.10 3.60 10 -10 0 -8.00 4.50 -10 10 0 -0.70 5.80 10 10 0 15.00 5.20 10 -10 0 -1.20 5.60 10 10 0 1.40 4.10 -10 -10 0 -4.20 5.40 -10 10 0 1.10 6.30 10 10 0 4.30 5.50 10 10 0 -2.30 6.10 -10 10 0 1.00 6.70 -10 10 0 3.10 5.30 -10 -10 0 -9.00 5.50 -10 -10 0 1.00 5.20 10 -10 0 -3.30 5.50 -10 -10 0 4.20 4.70 -10 -10 0 2.70 4.40 10 -10 0 -1.00 5.40 10 11 0 4.50 5.80 10 -11 0 -6.60 5.90 10 11 0 4.00 8.10 -10 -11 0 1.10 6.70 -10 -11 0 8.00 8.00 -10 -11 0 -1.00 4.90 10 -11 0 -3.80 5.90 10 -11 0 5.10 6.40 -10 11 0 -10.50 6.20 10 11 0 -1.90 4.10 -10 -11 0 -3.40 3.90 -10 11 0 9.80 7.10 10 -11 0 4.40 6.40 10 11 0 0.60 4.40 10 11 0 1.40 4.30 -10 -11 0 -5.50 4.90 -10 11 0 -8.60 4.30 10 -11 0 -4.00 6.00 -10 12 0 99.19 17.80 -10 12 0 104.69 15.00 10 -12 0 117.69 16.40 -10 -12 0 150.58 20.70 -10 -12 0 112.89 13.40 10 -12 0 100.89 15.40 -10 12 0 122.69 17.50 10 -12 0 116.09 18.20 10 12 0 127.09 13.80 10 12 0 96.39 12.00 -10 -12 0 147.39 15.60 -10 -12 0 91.59 16.50 10 -12 0 74.69 14.20 10 12 0 90.19 12.90 10 -12 0 123.29 16.90 -10 -12 0 108.29 15.70 -10 13 0 -6.00 7.00 10 -13 0 4.70 7.70 -10 -13 0 4.10 6.40 10 -13 0 -6.80 6.40 10 -13 0 -2.00 7.60 -10 13 0 3.40 6.20 10 13 0 1.90 4.60 -10 -13 0 -7.00 4.00 10 -13 0 -2.60 6.90 -10 -13 0 -2.70 6.20 -10 -13 0 3.70 7.90 -10 -13 0 1.80 7.10 10 13 0 0.20 5.50 -10 13 0 -7.10 6.40 -10 -14 0 60.29 15.00 10 14 0 44.20 9.10 10 -14 0 35.50 11.50 -10 -14 0 39.90 9.50 -10 -14 0 52.29 12.30 -10 14 0 32.70 10.50 10 -14 0 42.80 11.80 -10 14 0 39.00 11.80 -10 -14 0 55.09 14.40 10 -14 0 39.00 12.30 10 14 0 53.59 10.90 -10 -15 0 -9.50 7.40 10 -15 0 -5.10 7.60 -10 -15 0 -7.70 5.30 10 -15 0 12.60 10.30 -10 -15 0 -12.30 8.70 10 15 0 -1.30 5.20 -10 15 0 -3.00 7.70 10 15 0 8.40 6.50 -10 15 0 -4.80 6.70 -10 -15 0 1.10 8.40 10 -15 0 -4.80 7.70 10 -16 0 122.09 20.20 -10 -16 0 64.99 12.00 -10 16 0 63.59 15.50 10 16 0 60.29 12.40 -10 16 0 75.89 15.10 -10 -16 0 88.79 16.10 -10 -16 0 95.49 18.20 10 -16 0 70.59 16.50 10 16 0 52.79 11.20 10 -16 0 100.79 18.70 -10 -16 0 63.49 16.70 -10 17 0 5.30 10.00 -10 17 0 -3.60 7.50 10 17 0 4.60 7.80 10 17 0 1.60 6.10 10 -17 0 -1.60 9.60 10 -17 0 -9.60 7.50 -10 -17 0 33.90 13.10 10 -17 0 7.20 9.70 -10 -17 0 -8.80 8.40 10 18 0 7.70 7.60 -10 18 0 12.50 11.40 -10 18 0 -5.00 8.00 10 -18 0 4.00 10.30 -10 -18 0 1.20 9.60 10 -18 0 9.20 10.50 10 18 0 -2.00 6.90 10 19 0 4.10 8.10 10 19 0 -4.90 7.50 -10 19 0 3.40 9.50 -10 19 0 -5.90 9.60 10 -19 0 -7.20 9.60 10 20 0 14.40 10.00 10 -20 0 30.60 14.40 -11 0 0 1.00 2.50 11 0 0 0.80 4.10 11 0 0 -4.30 3.00 11 0 0 -10.30 4.30 11 0 0 1.40 3.60 11 0 0 5.10 5.20 -11 0 0 1.60 3.40 -11 0 0 3.70 4.30 -11 -1 0 120.89 11.60 11 1 0 114.49 11.70 11 1 0 110.59 13.20 11 -1 0 122.29 12.70 11 -1 0 99.29 12.80 11 -1 0 120.79 14.40 11 1 0 110.29 14.90 -11 -1 0 131.39 9.50 11 1 0 119.79 13.30 11 -1 0 141.59 13.30 -11 -1 0 122.69 13.40 11 1 0 94.89 13.90 11 1 0 113.99 11.60 -11 1 0 131.29 11.60 -11 2 0 -0.40 2.20 11 -2 0 -2.10 5.00 -11 -2 0 1.70 3.30 -11 -2 0 2.50 4.10 11 2 0 3.20 5.50 11 2 0 -0.90 3.30 11 2 0 -4.00 3.70 11 2 0 4.60 3.80 11 2 0 0.70 5.40 -11 -2 0 -3.40 2.30 11 2 0 -3.90 3.60 11 -2 0 -3.10 2.10 11 -2 0 4.30 4.90 11 -2 0 1.30 4.40 11 -2 0 6.90 4.80 -11 3 0 192.78 13.60 -11 -3 0 181.18 14.30 11 3 0 189.58 12.30 11 3 0 213.18 14.90 11 3 0 225.78 15.00 -11 -3 0 208.78 16.20 11 3 0 256.17 23.30 11 3 0 190.78 18.00 11 -3 0 199.78 13.70 11 -3 0 215.58 16.90 11 -3 0 221.68 20.80 11 3 0 218.18 16.30 11 3 0 211.48 12.60 -11 3 0 196.08 19.50 -11 3 0 227.08 17.30 -11 -3 0 214.08 12.00 11 3 0 222.68 22.80 11 -3 0 197.28 17.90 11 -3 0 195.38 19.90 -11 4 0 -2.40 4.70 11 -4 0 1.80 3.40 11 -4 0 -4.40 4.00 11 4 0 1.10 3.30 -11 4 0 -1.20 3.60 11 -4 0 0.50 4.10 -11 4 0 -0.20 4.30 -11 -4 0 -3.40 4.80 -11 4 0 -1.70 3.20 11 4 0 -1.30 2.60 11 -4 0 4.50 5.10 11 4 0 5.50 4.40 11 4 0 5.30 6.20 -11 -4 0 -0.60 3.60 11 4 0 4.50 4.60 11 4 0 -1.30 3.00 -11 -4 0 2.80 3.60 11 5 0 760.32 52.09 11 5 0 821.12 43.90 11 -5 0 793.92 46.70 -11 5 0 817.92 45.90 11 5 0 784.22 45.20 11 -5 0 896.81 46.20 -11 5 0 849.32 50.99 11 -5 0 805.22 47.80 11 5 0 814.52 44.60 11 -5 0 825.32 47.00 -11 5 0 808.92 47.30 11 5 0 815.02 43.90 11 -5 0 789.12 50.59 -11 5 0 782.12 46.00 -11 -5 0 843.72 51.39 -11 -5 0 798.72 44.50 -11 -5 0 795.52 46.70 11 5 0 925.71 48.80 -11 6 0 10.70 5.40 -11 -6 0 -2.70 3.40 11 6 0 0.70 3.70 -11 -6 0 0.30 5.70 11 6 0 -0.50 3.70 11 6 0 -1.80 3.00 11 -6 0 0.00 3.90 11 -6 0 -4.00 4.40 11 6 0 2.60 4.20 -11 6 0 6.60 4.90 -11 -6 0 8.60 4.60 -11 6 0 2.20 4.80 -11 6 0 -2.10 5.10 11 6 0 4.20 6.30 -11 -6 0 -3.20 5.50 11 -6 0 -4.10 3.50 11 -6 0 2.70 5.60 11 6 0 0.50 4.20 11 -7 0 471.65 33.70 -11 -7 0 435.16 28.90 -11 7 0 438.66 29.40 -11 -7 0 455.75 28.80 11 7 0 416.46 26.60 11 -7 0 478.05 30.60 -11 -7 0 402.96 33.70 -11 -7 0 498.85 34.40 11 -7 0 401.26 29.40 -11 7 0 466.45 33.40 11 7 0 455.25 28.50 -11 7 0 494.45 31.40 11 7 0 461.75 28.00 11 -7 0 460.15 29.70 11 7 0 454.05 26.70 -11 7 0 473.45 29.80 -11 -7 0 433.16 28.20 11 7 0 488.35 35.20 -11 8 0 3.10 5.20 11 8 0 -1.10 3.80 -11 -8 0 -0.10 6.50 11 8 0 -2.50 3.90 -11 -8 0 -1.80 5.70 11 -8 0 3.90 5.20 -11 -8 0 3.90 4.00 -11 -8 0 -8.70 3.60 -11 8 0 -4.10 5.00 11 -8 0 -2.00 5.00 -11 8 0 3.30 6.40 11 8 0 6.80 3.80 -11 -8 0 2.60 4.60 11 8 0 -1.40 6.70 -11 8 0 1.00 5.20 11 -8 0 5.00 6.40 11 8 0 -1.70 4.20 -11 9 0 488.55 30.20 11 -9 0 395.86 30.20 -11 9 0 431.26 30.30 11 9 0 422.56 28.10 11 -9 0 373.16 28.70 11 -9 0 398.96 28.90 11 9 0 437.26 33.60 -11 9 0 423.56 28.80 -11 -9 0 411.16 27.00 -11 -9 0 390.06 26.80 -11 9 0 415.76 32.50 -11 -9 0 375.56 31.40 -11 -9 0 417.06 33.10 11 9 0 369.76 25.80 11 9 0 424.76 25.50 11 9 0 406.86 25.60 11 -9 0 449.16 32.90 -11 -9 0 386.06 27.60 -11 10 0 -3.40 6.10 -11 -10 0 4.60 4.80 11 -10 0 0.70 6.40 11 10 0 0.70 3.90 -11 -10 0 -6.40 4.40 11 10 0 -3.70 4.80 -11 -10 0 -4.10 4.40 11 10 0 4.40 5.20 -11 10 0 -4.50 5.10 -11 -10 0 4.80 6.90 11 -10 0 0.20 6.10 11 10 0 0.20 4.10 11 -10 0 3.10 6.20 11 -10 0 -6.80 4.60 -11 10 0 -3.90 5.90 -11 -10 0 6.70 7.80 -11 10 0 -10.80 5.90 -11 11 0 402.56 32.80 -11 -11 0 435.16 29.10 11 -11 0 389.36 29.20 -11 -11 0 397.16 36.20 -11 -11 0 400.06 33.20 11 -11 0 292.57 31.80 11 -11 0 406.36 29.80 11 11 0 376.76 24.80 11 11 0 395.96 26.40 11 11 0 358.56 25.20 -11 -11 0 371.56 26.40 -11 11 0 369.46 28.20 -11 11 0 370.36 29.50 11 11 0 439.96 29.30 -11 -11 0 356.86 25.80 11 -11 0 389.26 29.80 -11 -12 0 -1.90 6.10 -11 12 0 0.70 6.50 -11 12 0 2.90 6.70 11 -12 0 11.00 8.30 11 -12 0 -5.80 6.70 -11 12 0 1.40 7.70 11 -12 0 -2.10 5.90 11 12 0 -5.60 4.60 -11 -12 0 -4.00 4.30 11 -12 0 -9.70 6.10 11 -12 0 0.40 6.60 -11 -12 0 -3.00 8.00 -11 -12 0 5.10 5.90 11 12 0 -0.10 4.50 -11 -12 0 -6.40 6.90 11 -13 0 320.37 30.00 11 -13 0 264.97 28.20 11 -13 0 273.07 27.30 11 13 0 283.27 22.00 -11 -13 0 351.86 26.90 -11 -13 0 296.57 31.70 -11 -13 0 292.17 32.60 11 13 0 290.17 23.40 -11 13 0 291.77 31.60 -11 13 0 363.16 32.40 -11 -13 0 283.87 22.70 11 -13 0 318.17 29.10 -11 13 0 366.26 26.90 11 -13 0 313.67 32.90 -11 14 0 -5.90 6.20 -11 -14 0 -7.00 6.10 -11 14 0 -0.30 8.00 11 -14 0 -3.20 7.90 -11 -14 0 -8.70 7.60 11 14 0 1.30 6.10 11 -14 0 8.30 8.80 -11 -14 0 -5.00 8.10 11 14 0 0.90 5.50 -11 -14 0 0.10 5.30 11 -14 0 -0.10 8.00 -11 -15 0 57.09 15.60 11 -15 0 55.49 14.60 11 -15 0 99.89 18.30 11 -15 0 65.19 14.40 -11 -15 0 84.09 12.50 11 15 0 69.49 11.80 -11 15 0 109.19 16.50 11 15 0 90.79 14.10 -11 -15 0 99.09 17.20 -11 15 0 98.69 17.50 11 -16 0 8.40 9.30 11 -16 0 12.40 10.50 -11 -16 0 3.50 10.00 11 16 0 -1.40 5.90 -11 16 0 7.20 8.70 -11 16 0 -10.70 7.60 11 -16 0 -6.80 7.70 -11 -16 0 1.20 6.40 -11 -16 0 -0.70 8.00 11 16 0 -2.40 6.60 11 -17 0 -9.50 7.70 -11 -17 0 3.60 9.20 11 -17 0 -9.30 7.90 -11 17 0 -9.10 8.60 11 -17 0 -15.80 8.60 11 17 0 0.40 6.50 11 17 0 -2.10 7.10 -11 17 0 -10.80 7.60 11 -18 0 -12.20 9.50 11 18 0 3.60 8.10 -11 -18 0 -3.10 9.50 11 18 0 -4.40 6.20 11 19 0 58.59 13.40 11 19 0 63.39 14.20 11 -19 0 77.79 19.30 12 0 0 87.69 10.60 -12 0 0 72.49 9.90 -12 0 0 72.09 10.90 12 0 0 70.19 9.50 12 0 0 74.49 11.20 -12 0 0 78.49 8.50 12 0 0 74.99 11.50 12 0 0 61.59 12.20 12 1 0 -8.90 4.80 -12 1 0 -0.80 2.70 -12 -1 0 7.30 4.80 -12 -1 0 -0.30 3.50 12 -1 0 2.50 4.60 12 1 0 -1.80 3.30 12 1 0 2.00 3.70 -12 -1 0 -2.10 2.50 12 -1 0 -2.30 4.60 12 1 0 2.50 4.70 12 -1 0 -0.60 3.80 12 -1 0 -2.50 3.40 12 1 0 1.00 4.50 12 -2 0 562.34 30.00 12 2 0 586.94 32.90 12 2 0 537.85 32.30 12 -2 0 552.44 33.80 12 2 0 569.94 35.70 12 2 0 543.55 33.70 12 2 0 595.34 39.90 -12 -2 0 583.14 29.90 -12 -2 0 575.94 32.40 -12 -2 0 582.54 35.20 12 -2 0 542.45 35.30 12 -2 0 565.84 36.90 12 -2 0 545.95 33.50 -12 2 0 518.75 29.90 -12 -3 0 -2.90 4.10 12 -3 0 -3.00 2.70 12 -3 0 -1.30 4.20 -12 3 0 -2.60 4.10 12 -3 0 -4.80 4.10 12 -3 0 -3.70 4.70 12 3 0 -2.30 2.00 -12 3 0 -0.30 2.70 12 3 0 -4.60 1.80 12 3 0 0.60 3.50 -12 3 0 0.70 5.00 12 3 0 -5.00 3.60 -12 -3 0 -1.30 2.00 12 -3 0 9.20 5.40 -12 -3 0 5.20 4.00 12 3 0 0.10 3.40 12 3 0 -1.60 4.30 12 3 0 -6.20 5.20 12 -4 0 4.90 5.40 -12 4 0 27.20 7.50 -12 -4 0 29.60 5.90 12 4 0 14.40 5.10 12 4 0 27.10 4.50 12 4 0 36.80 9.90 -12 4 0 21.80 6.10 12 -4 0 21.60 5.10 12 4 0 30.40 6.00 -12 4 0 27.20 8.50 -12 -4 0 27.70 6.60 12 -4 0 19.60 6.80 12 4 0 20.50 4.20 12 4 0 22.20 6.30 12 -4 0 18.60 7.40 -12 4 0 34.60 5.80 12 4 0 24.60 7.20 12 5 0 4.10 4.00 12 5 0 -3.70 2.90 -12 5 0 -2.60 3.90 12 5 0 -1.70 3.00 12 5 0 -0.40 4.00 12 5 0 -5.00 6.00 12 -5 0 7.90 5.40 -12 -5 0 5.10 6.40 -12 -5 0 -2.30 3.60 12 -5 0 0.10 3.90 -12 5 0 -6.70 4.40 -12 5 0 8.10 5.60 12 -5 0 -4.40 4.50 -12 5 0 0.30 4.00 12 5 0 -0.80 4.30 12 -5 0 1.00 4.70 12 -6 0 272.87 20.80 12 -6 0 244.48 18.30 12 6 0 255.37 18.40 -12 -6 0 254.17 17.30 12 -6 0 218.88 23.10 12 6 0 249.97 19.80 -12 6 0 231.18 22.00 -12 -6 0 262.67 26.00 12 6 0 245.48 17.00 12 -6 0 256.27 20.20 12 6 0 236.78 17.20 -12 6 0 278.57 19.00 -12 6 0 259.47 19.60 12 6 0 197.48 23.40 -12 -6 0 214.48 17.70 12 6 0 251.17 17.20 -12 6 0 204.58 22.60 12 7 0 -0.40 3.90 -12 -7 0 9.90 4.60 12 7 0 0.80 4.90 12 7 0 1.50 6.40 12 7 0 -4.10 3.20 -12 -7 0 -5.60 3.60 -12 -7 0 -1.50 6.30 -12 7 0 1.20 5.20 -12 7 0 -0.10 5.70 12 -7 0 2.30 5.90 12 -7 0 2.00 5.90 -12 -7 0 -1.10 6.20 -12 7 0 -1.00 4.70 12 -7 0 3.80 4.80 12 7 0 2.10 3.70 12 7 0 -5.70 3.60 -12 7 0 -3.70 5.00 12 -7 0 -2.40 4.90 12 8 0 67.09 9.20 12 8 0 65.79 14.40 -12 -8 0 73.49 10.30 -12 -8 0 46.80 12.70 12 8 0 56.49 8.30 -12 8 0 52.19 10.00 12 -8 0 52.09 12.20 -12 8 0 68.99 13.70 12 8 0 71.09 10.40 12 -8 0 80.59 11.40 -12 8 0 64.89 10.90 -12 -8 0 59.59 9.40 -12 -8 0 48.30 12.20 12 8 0 69.09 9.70 -12 8 0 85.79 13.70 -12 -8 0 78.29 10.50 12 -8 0 68.79 11.60 -12 -9 0 -2.50 4.90 -12 -9 0 9.30 7.80 12 -9 0 -2.50 4.60 12 9 0 2.20 4.80 -12 -9 0 4.70 7.30 12 -9 0 -8.50 5.90 12 -9 0 5.90 6.50 -12 9 0 -5.60 5.60 -12 9 0 -5.10 5.40 -12 9 0 -0.80 6.40 -12 9 0 2.30 5.80 -12 -9 0 -3.30 3.90 12 9 0 -2.80 4.70 -12 -9 0 -2.20 4.40 12 9 0 0.20 3.60 12 9 0 0.50 4.50 -12 -10 0 1.30 5.60 12 -10 0 1.30 6.70 -12 -10 0 7.20 7.50 -12 10 0 -8.10 5.40 12 -10 0 1.30 6.20 -12 -10 0 -0.80 4.30 12 -10 0 1.80 6.20 -12 -10 0 8.60 8.30 12 10 0 -0.80 4.90 12 10 0 -0.60 5.80 -12 10 0 9.00 7.80 12 10 0 -1.00 4.40 -12 10 0 -1.20 7.10 -12 -10 0 -0.20 4.80 12 10 0 -0.70 4.00 12 -10 0 1.20 6.90 -12 -11 0 0.00 4.60 -12 -11 0 -2.50 7.70 -12 11 0 -7.30 7.00 -12 -11 0 -4.80 7.90 12 -11 0 -3.40 5.80 -12 -11 0 -4.00 5.90 -12 -11 0 1.00 4.80 -12 11 0 -10.40 4.80 12 -11 0 6.20 7.40 12 -11 0 -3.80 6.00 -12 11 0 -3.00 6.10 12 -11 0 -3.00 5.90 12 11 0 2.30 4.40 12 11 0 -5.30 6.10 12 11 0 -1.80 5.00 -12 -12 0 165.18 23.80 -12 -12 0 169.98 23.20 12 -12 0 169.78 20.90 -12 -12 0 150.58 16.60 -12 12 0 168.78 20.30 -12 12 0 153.88 22.70 12 -12 0 187.08 21.20 -12 -12 0 156.88 19.10 12 -12 0 146.39 19.80 12 12 0 143.09 15.70 -12 12 0 135.39 19.80 -12 -12 0 202.58 18.50 12 -12 0 181.78 21.30 12 12 0 173.88 17.70 12 -12 0 211.98 25.60 12 -13 0 -14.30 7.30 -12 -13 0 1.50 7.30 -12 -13 0 6.90 9.20 -12 13 0 5.80 7.10 12 -13 0 -5.70 7.40 -12 -13 0 11.60 9.30 12 -13 0 -2.20 7.60 12 -13 0 2.60 8.60 12 13 0 -1.10 5.50 12 13 0 -1.10 4.70 -12 13 0 -2.40 6.90 12 -13 0 5.90 8.40 -12 -13 0 -0.10 5.40 12 14 0 218.98 21.10 -12 -14 0 256.07 26.40 -12 -14 0 257.97 30.40 12 -14 0 266.77 30.70 12 -14 0 278.77 28.50 -12 14 0 244.28 27.60 12 -14 0 249.97 26.20 -12 -14 0 249.38 20.40 -12 14 0 250.87 26.60 12 14 0 217.48 22.10 -12 -15 0 9.80 10.30 -12 -15 0 -2.20 7.90 -12 15 0 -11.60 7.60 12 -15 0 -7.10 8.20 -12 15 0 8.70 8.70 -12 -15 0 -2.90 5.70 12 15 0 8.20 7.10 12 15 0 3.90 5.90 12 -15 0 -6.10 7.80 12 16 0 287.07 27.60 12 16 0 345.37 25.60 12 -16 0 361.66 34.70 12 -16 0 241.88 31.20 -12 -16 0 352.96 33.30 12 17 0 1.50 6.80 12 17 0 4.40 8.00 12 -17 0 13.50 11.70 -12 -17 0 -11.80 8.60 12 -17 0 -15.60 8.50 12 18 0 68.89 13.60 -12 -18 0 55.99 15.70 12 -18 0 59.79 18.20 12 18 0 55.69 12.30 12 19 0 -2.70 7.10 -13 0 0 -7.30 3.80 -13 0 0 1.30 3.10 13 0 0 2.10 5.30 13 0 0 -2.00 4.30 -13 0 0 -2.60 4.00 13 0 0 -0.60 4.10 13 0 0 -5.00 5.10 13 0 0 1.40 4.20 13 1 0 15.20 6.30 13 1 0 2.60 4.70 13 1 0 -2.30 3.60 13 1 0 5.40 4.40 13 1 0 0.30 6.00 -13 -1 0 10.20 3.90 13 -1 0 14.60 6.10 13 -1 0 -1.80 5.60 -13 -1 0 6.90 5.40 13 -1 0 2.10 4.50 13 -1 0 10.60 5.80 13 -1 0 9.60 6.10 -13 1 0 10.10 4.50 -13 -1 0 5.90 4.50 13 -2 0 0.10 4.10 13 2 0 -2.00 5.70 13 -2 0 1.40 2.10 13 -2 0 -2.40 5.30 13 2 0 -1.10 4.50 13 -2 0 -6.10 3.70 13 2 0 -0.70 3.80 -13 -2 0 0.90 4.10 13 2 0 4.50 4.00 13 -2 0 -1.20 4.60 -13 -2 0 -1.40 2.50 -13 -2 0 -0.50 4.10 13 2 0 -1.00 4.70 -13 2 0 0.30 2.30 -13 3 0 153.08 11.00 -13 -3 0 158.18 15.90 -13 -3 0 144.09 9.60 13 3 0 168.98 16.50 13 -3 0 149.99 18.10 13 -3 0 149.88 16.30 -13 3 0 126.09 16.20 13 -3 0 167.88 18.50 13 3 0 205.78 22.70 13 -3 0 140.09 10.80 13 3 0 161.78 17.00 -13 -3 0 168.58 14.30 13 -3 0 184.38 17.10 13 3 0 146.99 14.30 13 3 0 128.79 13.60 13 -4 0 -9.00 3.90 13 4 0 -0.20 4.40 13 4 0 -1.90 2.70 13 -4 0 -1.50 4.80 -13 4 0 0.90 5.60 -13 4 0 3.10 5.70 13 -4 0 -3.30 4.30 -13 4 0 -3.50 3.80 13 -4 0 0.30 3.50 13 4 0 -5.50 3.20 13 4 0 -4.50 6.00 13 4 0 -1.60 3.30 13 4 0 0.70 2.50 13 4 0 7.00 4.90 -13 -4 0 -0.20 4.50 -13 4 0 -6.00 3.20 13 5 0 56.59 9.40 -13 5 0 53.39 8.00 -13 -5 0 58.79 12.60 13 -5 0 60.59 8.50 13 5 0 51.09 9.70 -13 5 0 71.19 12.90 13 5 0 60.69 8.80 13 -5 0 53.09 10.00 13 5 0 50.89 6.80 13 -5 0 40.70 9.50 -13 5 0 61.59 10.00 13 -5 0 64.49 12.30 -13 5 0 60.39 11.00 13 5 0 57.09 13.10 13 5 0 47.90 7.70 -13 -5 0 64.89 9.80 -13 6 0 1.00 4.80 13 -6 0 -2.60 4.80 -13 6 0 -3.80 5.40 13 6 0 3.80 5.30 -13 6 0 -2.60 4.50 13 6 0 0.40 3.70 13 6 0 -1.10 4.10 13 -6 0 2.80 4.70 13 6 0 6.90 8.00 13 -6 0 1.30 5.10 -13 -6 0 4.50 6.80 -13 6 0 7.30 7.00 -13 -6 0 -3.40 4.10 13 6 0 -4.70 4.20 13 -6 0 2.20 5.50 13 6 0 -0.80 3.50 13 -7 0 657.63 42.00 -13 7 0 652.43 45.70 -13 7 0 688.13 41.50 13 7 0 678.93 38.90 -13 -7 0 715.33 46.90 -13 -7 0 718.03 39.70 13 7 0 643.14 42.20 13 7 0 687.23 40.10 -13 7 0 677.83 42.80 -13 7 0 651.63 40.50 13 -7 0 647.54 45.80 13 7 0 664.03 39.30 13 7 0 673.53 38.50 -13 -7 0 703.23 41.00 13 -7 0 745.73 41.40 13 -8 0 0.00 5.40 -13 8 0 -1.10 5.40 -13 -8 0 -6.90 6.30 -13 8 0 4.40 7.50 13 8 0 -4.10 3.50 -13 8 0 1.10 5.60 -13 -8 0 -5.10 4.80 13 8 0 1.70 4.70 -13 -8 0 6.20 7.60 -13 8 0 9.70 6.50 -13 -8 0 -6.10 4.70 13 -8 0 7.30 6.10 13 8 0 -4.60 3.90 13 -8 0 3.40 7.00 13 8 0 -2.10 4.50 -13 -8 0 -3.60 4.40 13 9 0 210.88 19.50 -13 -9 0 200.88 25.50 13 9 0 227.68 17.00 13 -9 0 219.28 22.90 13 9 0 214.18 17.10 -13 -9 0 167.38 22.80 -13 9 0 205.58 23.10 13 9 0 200.48 19.60 -13 9 0 244.98 26.60 -13 -9 0 238.78 18.70 13 -9 0 239.68 21.90 13 -9 0 253.87 26.90 -13 -9 0 244.08 18.40 -13 -9 0 221.58 18.00 -13 9 0 173.18 19.90 -13 9 0 210.38 21.40 13 10 0 0.30 4.80 -13 -10 0 9.50 5.80 -13 -10 0 -0.10 8.00 -13 10 0 -6.30 6.90 -13 -10 0 10.00 6.30 13 -10 0 -1.10 6.40 -13 10 0 4.30 7.60 -13 -10 0 18.20 9.30 13 10 0 -1.00 5.90 13 -10 0 -4.90 6.30 13 -10 0 2.30 7.50 -13 -10 0 8.70 5.20 -13 10 0 -2.30 6.10 13 10 0 4.30 4.60 13 -10 0 0.60 7.50 -13 11 0 197.18 23.10 -13 -11 0 212.18 18.90 -13 11 0 136.79 18.50 13 11 0 229.08 21.50 -13 -11 0 181.68 18.20 13 -11 0 151.18 19.50 13 -11 0 231.58 26.80 13 11 0 174.48 18.20 -13 -11 0 180.18 25.30 -13 -11 0 213.88 26.20 -13 -11 0 200.58 20.30 13 -11 0 160.28 20.60 13 11 0 172.38 17.00 13 -11 0 225.78 22.40 13 12 0 -9.80 4.50 13 -12 0 -3.00 7.60 -13 12 0 -2.50 6.50 13 -12 0 -4.00 8.00 13 12 0 -3.00 4.40 -13 -12 0 -10.70 7.10 -13 -12 0 -0.40 5.10 -13 -12 0 4.20 8.20 -13 12 0 2.60 7.90 13 -12 0 5.40 7.60 13 -12 0 12.30 8.40 -13 -12 0 2.30 7.20 13 -13 0 79.69 15.20 13 -13 0 45.60 12.80 13 -13 0 68.49 16.30 -13 -13 0 51.09 14.60 -13 -13 0 98.79 15.70 13 13 0 60.89 10.40 -13 -13 0 88.39 12.20 13 13 0 61.69 11.50 13 -13 0 60.79 13.80 13 -13 0 28.20 11.40 -13 -14 0 3.80 6.10 13 14 0 -7.40 5.70 13 -14 0 -10.10 6.80 -13 -14 0 2.80 9.50 13 -14 0 1.60 9.30 13 14 0 7.00 6.00 13 -14 0 -4.40 8.50 -13 -14 0 -7.40 7.20 -13 -15 0 1.70 8.80 13 -15 0 25.60 11.60 13 15 0 1.80 6.20 -13 -15 0 -15.90 7.60 13 -15 0 9.20 9.80 13 15 0 11.60 7.90 -13 -16 0 12.40 10.30 13 -16 0 5.30 10.30 13 16 0 -5.10 5.90 13 16 0 1.90 7.20 13 17 0 2.50 6.80 13 17 0 11.40 8.50 -13 -17 0 7.10 9.80 13 -17 0 8.20 10.80 13 18 0 3.60 8.30 -13 -18 0 -8.50 9.70 13 18 0 -4.60 5.50 14 0 0 577.54 35.30 14 0 0 591.54 38.70 14 0 0 553.94 36.80 -14 0 0 610.74 33.20 14 0 0 633.64 42.60 14 0 0 571.64 35.40 -14 0 0 576.64 35.20 -14 0 0 574.74 38.00 14 -1 0 8.80 5.10 14 1 0 12.40 5.70 -14 -1 0 0.70 3.00 14 1 0 4.80 6.80 -14 1 0 -4.90 2.90 -14 -1 0 3.10 4.80 14 1 0 0.30 5.40 14 -1 0 -3.10 6.40 -14 -1 0 5.80 4.70 14 -1 0 0.40 5.30 14 -1 0 -2.00 4.20 -14 1 0 3.20 5.00 14 1 0 1.10 4.70 14 1 0 2.00 4.20 14 -1 0 -1.60 4.40 14 2 0 579.44 42.20 14 -2 0 603.04 36.30 14 -2 0 487.35 34.80 -14 -2 0 583.44 34.20 14 2 0 593.04 35.00 14 2 0 574.24 34.60 -14 2 0 562.74 33.80 -14 -2 0 568.54 37.10 -14 -2 0 594.54 31.20 14 2 0 612.04 36.70 14 -2 0 584.74 30.60 14 -2 0 603.14 39.50 14 2 0 592.64 38.20 -14 2 0 571.84 30.60 14 -2 0 606.64 38.30 -14 3 0 -2.70 2.80 14 -3 0 1.90 5.90 14 3 0 -2.40 3.50 14 -3 0 3.50 2.90 -14 3 0 -4.00 4.90 14 3 0 -6.50 3.30 14 -3 0 6.90 5.60 14 -3 0 5.60 6.70 -14 -3 0 2.40 4.60 14 3 0 -2.70 4.70 14 3 0 -2.10 4.90 -14 -3 0 3.80 4.70 14 3 0 -1.60 6.10 14 -3 0 2.50 5.40 14 -4 0 221.78 15.30 14 -4 0 250.27 22.20 14 4 0 228.98 13.60 14 -4 0 212.08 22.60 -14 4 0 220.08 23.70 14 4 0 226.08 17.30 14 4 0 210.18 16.60 14 -4 0 232.88 21.20 -14 4 0 207.98 15.20 14 4 0 206.48 19.60 14 4 0 219.48 13.70 14 4 0 201.78 24.90 14 4 0 229.18 21.40 -14 -4 0 229.68 18.60 -14 4 0 244.58 22.30 14 5 0 1.10 3.70 14 5 0 0.70 4.90 14 -5 0 -8.20 3.40 14 5 0 2.70 4.60 14 5 0 -3.50 3.10 -14 -5 0 -3.10 4.10 -14 5 0 -3.80 3.90 -14 5 0 -2.00 5.20 14 -5 0 -3.50 4.80 -14 5 0 -5.80 3.80 14 5 0 -6.90 4.40 14 5 0 2.60 3.00 14 -5 0 -3.40 5.20 14 -5 0 -1.90 5.10 -14 5 0 3.30 6.20 14 6 0 27.80 5.90 14 -6 0 30.90 8.80 -14 -6 0 31.00 10.50 14 -6 0 23.40 9.30 14 6 0 16.90 7.20 14 -6 0 29.90 8.30 14 6 0 9.10 5.90 -14 6 0 35.90 9.80 14 6 0 23.30 6.30 14 6 0 23.70 6.60 -14 -6 0 19.90 6.60 14 -6 0 26.90 6.90 -14 6 0 20.20 9.00 -14 6 0 19.70 7.00 -14 6 0 18.60 6.30 -14 7 0 0.60 5.30 14 -7 0 4.70 5.10 14 7 0 -2.70 4.90 14 7 0 0.60 4.50 -14 7 0 -8.00 4.70 -14 7 0 9.40 7.40 14 7 0 -1.60 4.80 -14 -7 0 -1.00 4.50 -14 7 0 5.30 7.40 14 7 0 -2.40 4.00 14 7 0 -3.00 3.90 -14 -7 0 14.40 8.60 14 -7 0 -3.20 6.20 14 -7 0 8.50 6.50 14 8 0 47.10 8.50 -14 8 0 44.40 12.10 -14 -8 0 49.90 9.40 14 -8 0 43.90 12.30 -14 -8 0 40.20 8.30 14 8 0 36.70 7.70 -14 8 0 34.80 10.10 14 -8 0 39.80 10.00 14 -8 0 39.60 9.30 -14 -8 0 20.30 9.90 -14 8 0 42.40 9.70 -14 -8 0 29.50 7.90 14 8 0 30.80 7.10 -14 8 0 42.20 9.50 14 8 0 37.40 8.50 14 -9 0 -3.60 5.90 -14 -9 0 2.50 4.60 -14 -9 0 -6.90 4.80 -14 -9 0 -4.50 6.80 -14 9 0 -4.70 6.30 14 9 0 -1.00 4.30 14 9 0 -8.10 5.20 -14 -9 0 9.00 9.20 -14 9 0 1.60 6.60 14 -9 0 -8.10 7.00 14 -9 0 4.20 6.70 -14 -9 0 3.20 5.10 -14 9 0 -1.90 6.30 14 9 0 0.00 4.90 14 -10 0 30.90 9.30 14 10 0 20.60 6.70 14 -10 0 12.10 9.30 14 -10 0 26.90 9.80 14 10 0 27.50 7.80 14 -10 0 15.70 10.00 -14 -10 0 31.60 12.40 14 10 0 24.70 8.80 -14 -10 0 19.40 7.30 -14 -10 0 20.10 7.20 -14 -10 0 15.60 7.30 -14 -10 0 35.40 12.50 14 -11 0 4.50 8.90 14 11 0 -10.60 5.20 14 -11 0 -4.50 7.00 -14 -11 0 0.40 8.10 14 11 0 6.80 5.40 -14 -11 0 -1.30 5.90 -14 -11 0 -3.90 8.70 14 11 0 1.30 4.80 14 -11 0 0.40 8.40 14 -11 0 4.00 7.30 -14 -11 0 -2.20 5.20 14 12 0 222.78 19.90 14 12 0 210.18 20.40 -14 -12 0 199.28 19.50 14 -12 0 225.08 24.70 14 -12 0 200.18 26.90 -14 -12 0 186.18 21.60 14 -12 0 190.58 22.90 14 -12 0 220.48 25.10 -14 -12 0 230.98 28.70 -14 -13 0 -0.40 5.50 14 13 0 -3.20 5.30 14 -13 0 -1.90 7.90 14 -13 0 -4.80 7.80 -14 -13 0 5.80 8.20 14 -13 0 1.60 8.90 14 -13 0 -1.00 7.80 14 13 0 2.10 6.50 -14 -13 0 -7.50 8.90 -14 -14 0 287.27 33.30 -14 -14 0 287.27 27.70 14 14 0 206.88 21.30 14 14 0 238.08 23.40 -14 -14 0 257.37 21.10 14 -14 0 269.97 29.00 -14 -15 0 -4.00 8.30 14 -15 0 -11.30 8.70 14 15 0 2.30 6.30 14 15 0 4.20 7.30 14 16 0 271.37 26.50 14 16 0 316.87 24.60 14 -16 0 288.57 31.60 14 17 0 1.50 7.20 14 -17 0 -14.70 9.90 14 17 0 1.20 6.90 14 18 0 195.58 23.00 15 0 0 0.80 4.80 15 0 0 -0.60 6.60 15 0 0 -0.30 4.80 -15 0 0 1.80 4.80 15 0 0 -0.70 5.00 -15 0 0 -0.40 3.60 -15 0 0 4.30 5.40 15 0 0 1.90 5.60 15 1 0 -2.30 5.00 15 1 0 -2.20 4.70 15 1 0 3.20 6.30 -15 -1 0 -0.90 4.90 15 -1 0 0.50 6.00 15 1 0 -5.40 4.00 -15 -1 0 0.30 3.50 -15 -1 0 0.90 4.70 15 -1 0 -7.60 4.20 -15 1 0 -4.30 4.80 15 -1 0 6.60 8.00 15 -1 0 -0.40 5.00 -15 1 0 -3.10 3.80 15 -1 0 -6.20 4.40 -15 2 0 2.90 4.30 -15 -2 0 5.00 5.30 -15 -2 0 3.30 5.40 15 -2 0 -1.90 4.90 15 -2 0 7.40 7.10 15 2 0 -5.00 4.90 -15 -2 0 -1.10 2.90 15 -2 0 -0.20 4.70 15 2 0 3.40 4.90 15 2 0 -0.30 5.60 15 -2 0 2.70 6.20 15 2 0 0.80 4.60 -15 3 0 7.90 3.50 15 -3 0 6.10 3.30 15 3 0 13.60 5.40 15 -3 0 -0.60 5.60 15 3 0 5.40 5.80 -15 -3 0 8.70 5.80 15 -3 0 6.40 7.80 15 -3 0 16.20 6.40 15 3 0 7.60 5.30 15 3 0 3.60 6.00 15 -3 0 5.60 6.10 15 -4 0 -2.40 3.30 15 4 0 1.70 5.00 15 4 0 1.30 5.40 15 4 0 0.00 2.20 -15 4 0 3.70 6.50 15 -4 0 2.40 5.40 15 -4 0 -2.80 5.50 -15 -4 0 3.70 5.50 15 4 0 -0.20 4.20 15 -4 0 0.00 5.70 15 4 0 3.80 5.90 -15 4 0 -0.20 3.70 -15 -5 0 20.80 7.30 15 -5 0 24.40 8.40 15 5 0 8.80 3.80 -15 5 0 18.30 6.50 15 -5 0 20.30 5.60 -15 5 0 -3.90 6.10 -15 5 0 15.50 5.50 15 -5 0 12.30 7.10 15 5 0 17.50 6.10 15 5 0 21.70 6.30 15 5 0 14.30 4.10 15 5 0 10.20 6.20 15 -5 0 12.40 8.20 15 5 0 14.40 6.60 15 6 0 4.20 5.50 -15 -6 0 1.10 6.80 15 -6 0 2.90 6.40 -15 -6 0 0.60 5.10 15 -6 0 -4.70 6.00 15 6 0 0.90 4.60 15 6 0 -5.30 3.70 15 -6 0 1.50 5.10 15 6 0 0.30 5.80 15 6 0 1.00 4.00 15 6 0 0.90 4.80 15 -6 0 -2.20 5.40 -15 6 0 -8.70 4.40 15 -7 0 318.67 22.20 -15 7 0 327.37 22.20 -15 -7 0 230.28 27.70 -15 -7 0 294.77 22.20 15 7 0 309.97 22.40 15 -7 0 251.77 25.40 15 -7 0 275.17 29.30 15 7 0 297.87 20.30 15 7 0 288.77 21.00 15 -8 0 4.10 5.90 15 -8 0 -4.10 6.60 15 8 0 -0.90 4.40 15 -8 0 -6.60 5.70 -15 8 0 -2.60 5.90 15 8 0 -4.10 4.90 -15 -8 0 0.90 5.50 -15 -8 0 -7.30 6.70 -15 -9 0 79.59 11.70 -15 9 0 105.69 14.30 -15 -9 0 73.99 16.20 15 9 0 63.09 10.50 15 -9 0 98.29 17.60 15 -9 0 73.89 12.70 -15 -9 0 100.29 12.50 -15 -9 0 89.89 12.40 15 -9 0 114.69 16.60 15 9 0 83.79 12.30 15 10 0 2.30 5.30 -15 -10 0 2.70 5.40 15 -10 0 1.70 7.00 -15 -10 0 6.90 9.00 15 10 0 -0.50 5.30 15 -10 0 -9.40 6.00 -15 -10 0 -6.20 5.80 -15 -11 0 105.09 13.60 15 11 0 106.09 13.60 15 -11 0 96.39 15.30 -15 -11 0 113.69 20.30 15 -11 0 95.29 16.70 15 -11 0 87.09 17.20 15 11 0 105.49 14.00 15 -12 0 -4.10 7.50 15 12 0 0.40 5.50 15 12 0 2.30 6.30 -15 -12 0 -0.20 5.40 15 -12 0 2.90 8.20 15 -12 0 -10.80 7.00 -15 -12 0 0.60 9.20 15 -13 0 21.40 11.30 -15 -13 0 3.60 6.50 15 13 0 6.80 6.30 -15 -13 0 23.40 12.90 15 13 0 21.40 8.50 15 -13 0 21.60 10.20 15 14 0 -0.60 6.60 15 14 0 -6.60 5.50 15 -14 0 -3.60 9.10 15 15 0 13.90 7.80 15 -15 0 29.10 11.90 15 15 0 11.50 7.90 15 16 0 -3.90 5.70 15 -16 0 -1.30 9.20 15 16 0 -7.40 6.20 15 17 0 25.40 10.20 15 -17 0 41.50 14.40 16 0 0 435.56 33.40 16 0 0 442.46 30.70 16 0 0 541.35 34.00 -16 0 0 461.75 33.20 -16 -1 0 2.20 3.80 16 -1 0 -1.50 5.00 -16 -1 0 4.80 6.00 16 1 0 -4.40 3.80 -16 1 0 -9.40 5.00 16 -1 0 -3.80 6.50 16 1 0 1.30 6.20 16 -1 0 -2.70 5.20 16 1 0 -7.10 5.00 16 -2 0 362.96 28.20 -16 -2 0 343.97 25.90 16 -2 0 334.67 25.20 16 2 0 291.57 28.20 16 2 0 357.96 25.80 16 -2 0 295.37 29.00 16 2 0 341.27 24.20 16 -3 0 5.80 8.00 16 3 0 5.00 6.50 16 3 0 0.90 5.80 -16 -3 0 -5.00 5.00 16 -3 0 4.40 6.10 16 -3 0 0.20 2.70 16 3 0 -3.10 4.20 16 -3 0 8.70 6.40 16 -4 0 732.23 46.40 -16 -4 0 767.62 46.80 16 4 0 768.72 44.20 16 -4 0 747.83 41.50 16 -4 0 758.12 50.39 16 4 0 775.52 45.80 16 -5 0 2.20 4.50 -16 -5 0 5.60 5.60 16 5 0 1.70 4.50 16 -5 0 5.20 7.00 16 5 0 5.30 6.00 16 6 0 117.59 15.30 16 -6 0 112.89 16.50 -16 -6 0 186.78 17.90 16 6 0 140.49 14.90 16 -6 0 147.39 14.40 16 -7 0 0.00 6.50 -16 -7 0 -4.70 7.10 16 7 0 12.60 6.40 16 -7 0 0.50 5.70 16 7 0 7.50 5.50 16 -8 0 11.10 8.20 -16 -8 0 7.10 8.40 16 8 0 9.60 6.40 16 -8 0 0.20 6.70 16 8 0 6.90 5.80 16 -9 0 -3.80 6.20 -16 -9 0 0.20 8.60 16 9 0 -1.10 4.90 16 -9 0 5.00 8.30 16 9 0 3.30 5.70 -16 -9 0 0.40 5.30 16 -10 0 114.29 18.00 -16 -10 0 84.99 18.70 16 10 0 129.59 14.70 16 10 0 85.09 13.50 -16 -10 0 129.19 14.90 16 -10 0 144.49 17.50 16 -11 0 9.30 8.80 16 -11 0 9.10 9.80 16 11 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49.00 11.30 19 -10 0 -7.70 7.50 19 10 0 -1.70 6.70 19 10 0 7.30 6.50 19 -11 0 167.28 22.50 19 11 0 126.09 16.60 19 11 0 134.19 17.50 19 12 0 7.00 6.90 19 12 0 9.10 7.50 19 13 0 -0.50 7.00 19 13 0 -6.90 6.10 19 14 0 0.70 7.40 20 0 0 730.73 48.30 20 0 0 837.92 52.29 20 -1 0 0.40 6.90 20 -1 0 12.10 9.70 20 1 0 -3.10 7.00 20 1 0 0.30 8.50 20 2 0 355.26 32.60 20 -2 0 318.37 33.40 20 2 0 335.37 27.20 20 -2 0 383.86 28.80 20 3 0 -1.10 6.30 20 -3 0 -1.40 9.10 20 3 0 -2.90 7.30 20 -3 0 -5.00 6.50 20 4 0 72.79 14.00 20 4 0 70.69 12.60 20 -4 0 55.89 13.30 20 5 0 2.70 6.60 20 -5 0 -5.00 6.70 20 5 0 -6.90 5.80 20 -6 0 40.60 12.10 20 6 0 63.19 12.90 20 6 0 53.09 11.30 20 -7 0 2.10 7.10 20 7 0 2.00 6.10 20 7 0 3.90 7.70 20 8 0 72.69 12.50 20 -8 0 63.99 14.70 20 8 0 53.79 12.50 20 9 0 -1.10 6.00 20 9 0 -7.90 7.20 20 -9 0 7.30 9.60 20 10 0 -3.20 6.70 20 -10 0 1.60 8.60 20 10 0 2.30 6.80 20 11 0 -0.30 6.90 20 -11 0 1.50 9.00 20 11 0 -6.40 6.20 20 12 0 -0.10 7.30 20 12 0 1.60 6.90 21 0 0 -6.00 6.60 21 0 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18.30 0 9 -1 -4.60 3.60 0 9 -1 3.50 4.10 0 9 -1 2.10 4.80 0 -9 1 -1.70 4.10 0 9 -1 -0.20 4.30 0 -9 -1 -1.50 4.70 0 9 -1 3.00 5.20 0 9 1 7.80 5.70 0 -9 1 -2.10 3.10 0 9 1 4.30 5.40 0 -9 1 4.00 5.20 0 -9 -1 0.60 4.40 0 -9 1 1.60 4.30 0 9 1 -1.60 4.60 0 -9 -1 -7.90 3.60 0 9 1 8.80 4.60 0 -9 -1 5.00 5.20 0 9 1 -4.60 3.10 0 9 1 -4.70 4.50 0 9 1 -2.80 3.90 0 -9 1 6.70 4.30 0 9 -1 -9.20 4.40 0 9 -1 2.00 3.50 0 10 -1 562.44 31.90 0 10 1 559.54 33.50 0 -10 1 520.75 34.20 0 10 -1 516.95 32.60 0 10 1 515.75 35.30 0 10 1 541.75 35.80 0 10 -1 497.15 34.60 0 -10 1 484.95 34.40 0 -10 -1 515.75 34.60 0 10 1 545.95 34.80 0 -10 -1 539.15 34.60 0 -10 -1 543.25 35.50 0 10 -1 594.84 32.90 0 -10 1 564.74 31.30 0 10 -1 504.65 34.50 0 -10 1 547.25 35.70 0 10 1 551.34 35.60 0 -10 1 558.94 33.90 0 10 -1 539.05 35.90 0 10 -1 543.75 33.90 0 10 1 529.35 32.80 0 -10 -1 544.35 35.80 0 10 1 596.34 32.70 0 11 1 1.00 3.70 0 -11 -1 -0.30 4.60 0 11 -1 -2.90 3.80 0 -11 1 -0.50 4.20 0 11 -1 -3.30 4.90 0 -11 -1 2.80 4.90 0 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368.66 22.60 12 5 -3 324.27 23.00 -12 -5 -3 358.86 21.00 12 -5 3 329.77 24.50 12 -5 3 399.76 28.60 -12 -5 -3 327.97 27.40 12 5 -3 362.76 22.10 -12 -5 -3 312.07 30.70 12 5 -3 331.87 20.10 -12 5 3 329.57 26.60 -12 -6 3 154.78 12.00 -12 6 -3 179.58 20.70 12 6 3 156.88 17.70 12 -6 -3 113.99 16.20 12 -6 -3 147.89 16.30 -12 -6 3 153.88 20.00 12 6 3 149.99 12.40 -12 6 -3 145.49 15.80 12 6 3 129.69 15.30 12 6 3 158.58 15.10 12 6 3 148.79 19.70 12 6 3 138.99 15.00 -12 6 -3 137.79 17.40 12 -6 -3 209.28 19.60 12 -6 -3 136.49 14.50 -12 6 -3 183.38 15.90 12 -6 -3 141.99 15.80 -12 -6 -3 122.69 17.60 12 6 -3 132.19 19.30 -12 6 3 211.48 19.30 -12 -6 -3 168.58 11.10 12 6 -3 179.18 15.30 -12 6 3 138.29 18.20 -12 -6 -3 165.18 17.20 12 -6 3 167.18 15.40 -12 -6 -3 165.28 12.70 12 6 -3 165.48 15.00 12 6 -3 171.58 15.50 12 -6 3 129.49 17.50 12 6 -3 152.38 13.70 12 6 -3 152.88 11.20 12 -6 3 139.79 16.20 -12 6 3 122.69 14.20 12 6 -3 144.59 11.00 -12 -6 -3 149.99 20.00 -12 6 3 174.38 16.30 12 7 3 40.30 8.00 12 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13.00 -13 8 -3 110.89 16.30 -13 -8 3 112.89 11.00 13 8 3 123.69 14.20 -13 8 3 105.09 17.20 -13 8 3 89.59 13.00 13 8 -3 111.49 12.00 -13 -8 -3 110.39 18.20 13 8 -3 126.99 11.10 -13 -8 -3 115.99 17.90 13 -8 3 102.69 14.60 13 -8 3 109.69 17.70 13 -8 3 127.19 14.70 -13 8 3 87.39 14.40 13 8 -3 94.89 10.30 -13 -8 -3 110.69 12.70 13 8 -3 118.19 13.70 -13 -8 -3 111.39 14.60 -13 8 3 121.59 15.00 13 -9 -3 1.40 6.60 -13 -9 3 11.40 4.60 13 9 3 2.10 5.50 -13 -9 3 8.70 4.20 -13 9 -3 9.90 8.20 -13 -9 3 17.80 9.30 -13 9 -3 5.60 8.40 -13 9 -3 4.80 6.20 13 9 3 -0.80 5.30 13 -9 -3 17.40 7.70 -13 9 -3 -4.80 6.00 13 -9 -3 20.60 9.90 13 9 3 13.20 6.10 13 -9 -3 1.00 6.50 13 9 -3 6.80 4.70 13 -9 3 -1.20 6.10 -13 -9 -3 7.50 6.90 13 9 -3 -2.00 5.50 13 -9 3 2.80 8.00 -13 9 3 15.10 7.90 13 9 -3 7.60 3.90 13 9 -3 16.70 5.10 -13 9 3 3.50 5.90 -13 -9 -3 5.00 5.50 -13 9 3 10.90 8.70 -13 9 3 2.50 7.00 -13 -9 -3 22.00 10.40 -13 -9 -3 -1.60 7.30 13 -9 3 14.10 7.00 -13 -9 -3 5.60 5.80 13 -10 -3 84.99 13.80 13 10 3 132.09 15.60 13 -10 -3 92.39 14.60 -13 10 -3 101.99 18.50 -13 -10 3 94.69 10.00 13 10 3 105.89 14.50 -13 -10 3 104.49 10.40 -13 -10 3 92.19 18.30 13 -10 -3 166.08 21.60 -13 10 -3 110.59 17.30 -13 10 -3 139.79 17.40 13 10 3 110.89 13.70 13 -10 -3 101.59 17.90 13 -10 3 107.59 17.60 13 -10 3 95.59 14.60 -13 -10 -3 112.59 14.00 13 10 -3 91.59 10.40 -13 10 3 95.09 15.50 13 10 -3 116.89 15.00 13 -10 3 87.69 14.60 13 10 -3 98.39 11.70 -13 -10 -3 104.69 18.70 -13 10 3 95.99 14.80 -13 -10 -3 74.29 12.80 13 10 -3 100.09 10.80 -13 -10 -3 103.89 17.90 13 -11 -3 -0.40 8.20 -13 11 -3 -1.50 6.60 -13 -11 3 4.60 4.20 13 11 3 -5.90 5.90 -13 11 -3 13.10 8.50 -13 -11 3 3.80 9.40 13 -11 -3 -10.00 7.10 -13 -11 3 5.60 6.80 13 -11 -3 -4.50 6.50 -13 -11 3 -1.10 4.10 13 11 3 0.30 6.10 -13 11 -3 1.20 8.70 13 11 3 -5.60 5.20 13 -11 -3 3.70 7.10 13 -11 3 18.30 8.50 13 -11 3 1.70 8.80 -13 -11 -3 -0.10 8.00 -13 -11 -3 1.80 5.80 13 -11 3 -5.90 6.40 -13 -11 -3 1.50 6.40 -13 -11 -3 2.40 8.70 13 -11 3 12.30 9.10 13 11 -3 1.20 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56.79 12.60 14 3 -3 89.49 10.50 14 3 -3 107.39 12.60 14 3 -3 86.59 12.40 14 3 -3 101.69 8.90 -14 3 3 103.69 10.20 -14 3 3 86.59 10.60 14 -3 3 122.69 14.80 -14 -3 -3 91.89 10.10 -14 3 3 143.49 15.20 14 3 -3 103.99 11.10 14 3 -3 94.79 15.90 14 -3 3 101.49 15.60 14 3 -3 94.09 8.90 14 -4 -3 273.07 22.00 14 4 3 300.97 17.30 14 4 3 301.07 23.60 14 -4 -3 301.57 23.00 -14 4 -3 261.97 27.00 -14 -4 3 315.77 21.40 14 -4 -3 316.57 20.60 -14 4 -3 297.47 19.20 14 4 3 310.47 22.30 -14 4 -3 282.27 26.10 14 4 3 326.77 22.90 14 -4 -3 306.07 25.40 -14 4 -3 317.77 22.80 14 -4 -3 324.87 24.30 14 4 3 321.67 25.10 14 4 -3 308.97 21.50 14 -4 3 236.68 23.50 14 4 -3 296.67 19.80 14 4 -3 327.97 23.10 -14 -4 -3 325.37 24.50 -14 4 3 322.97 21.60 14 -4 3 284.87 28.50 14 4 -3 302.17 19.30 -14 -4 -3 297.87 19.10 14 -4 3 320.17 24.10 14 -4 3 378.06 28.10 -14 4 3 306.47 20.40 14 4 -3 318.47 20.30 14 -4 3 314.87 29.00 14 4 -3 293.37 19.30 -14 5 -3 73.99 13.80 14 5 3 76.09 12.90 14 5 3 80.59 12.40 14 -5 -3 83.39 13.80 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3 245.68 19.40 14 6 -3 261.67 17.30 -14 -6 -3 244.28 16.90 14 -6 3 279.17 19.10 -14 -6 -3 251.17 28.30 14 6 -3 262.77 20.10 -14 6 3 260.77 26.90 -14 -6 -3 227.58 26.50 14 -6 3 180.38 23.30 14 6 -3 229.28 18.10 -14 -6 -3 219.08 21.90 -14 7 -3 4.00 5.60 14 7 3 6.90 6.00 -14 -7 3 6.20 4.70 -14 7 -3 0.50 7.00 -14 7 -3 3.90 7.10 14 7 3 15.30 6.00 14 7 3 12.30 5.30 14 -7 -3 6.20 6.60 14 7 3 -1.50 5.80 -14 -7 3 5.40 8.00 -14 7 -3 10.50 6.90 -14 -7 3 9.20 4.70 14 -7 -3 9.40 6.40 14 -7 -3 0.30 5.20 14 -7 -3 15.50 8.40 14 7 -3 9.70 5.90 -14 -7 -3 4.60 8.10 -14 7 3 4.60 5.80 14 -7 3 11.20 6.90 14 -7 3 9.50 8.20 -14 -7 -3 11.50 8.40 -14 -7 -3 -0.90 5.90 14 7 -3 20.20 5.40 -14 -7 -3 10.80 5.10 14 7 -3 9.10 5.60 -14 7 3 14.20 8.90 14 -7 3 22.30 6.90 14 7 -3 11.80 5.60 14 7 -3 10.30 4.60 -14 7 3 11.20 6.10 14 7 -3 14.10 5.70 -14 8 -3 193.88 24.10 -14 -8 3 192.38 24.40 -14 8 -3 217.98 19.80 -14 8 -3 187.28 21.70 14 -8 -3 190.08 20.70 14 -8 -3 170.68 22.70 -14 -8 3 190.88 14.80 -14 -8 3 192.58 14.70 14 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243.18 28.50 -14 -10 3 237.28 17.20 14 -10 -3 226.68 27.20 14 -10 -3 200.98 23.10 14 10 3 261.17 23.90 14 -10 -3 252.17 24.50 -14 -10 3 221.88 27.80 -14 10 -3 246.28 25.90 14 -10 3 269.77 29.90 -14 -10 -3 249.97 30.00 -14 -10 -3 242.08 20.10 14 -10 3 264.27 24.60 14 10 -3 279.77 22.00 14 10 -3 221.88 17.10 -14 -10 -3 252.17 29.00 14 -10 3 292.67 27.30 14 10 -3 233.28 18.60 -14 -10 -3 251.07 23.90 -14 11 -3 8.20 8.00 14 -11 -3 6.30 9.20 14 11 3 11.40 6.70 14 11 3 8.90 7.00 -14 11 -3 0.20 7.80 14 -11 -3 4.00 7.80 14 -11 -3 -0.60 8.00 -14 -11 3 6.70 4.70 -14 -11 3 9.30 10.10 -14 -11 3 20.80 5.60 14 -11 3 6.90 9.60 -14 -11 -3 5.50 7.10 14 -11 3 3.20 7.70 -14 -11 -3 -8.60 4.70 -14 -11 -3 3.40 8.20 14 -11 3 -4.70 7.00 14 11 -3 7.70 5.60 14 -11 3 20.20 9.50 14 11 -3 15.40 5.40 14 -12 -3 250.07 26.40 -14 12 -3 250.87 25.80 -14 -12 3 243.98 17.40 14 -12 -3 206.98 25.00 -14 -12 3 245.38 17.40 14 -12 -3 234.98 27.70 -14 -12 3 255.97 30.70 14 -12 -3 250.17 28.20 14 12 3 241.78 22.70 -14 -12 3 240.48 24.30 14 12 3 261.47 24.80 14 -12 3 298.57 28.10 -14 -12 -3 216.98 23.20 14 12 -3 274.97 19.00 14 -12 3 204.98 27.30 14 -12 3 261.77 26.30 14 -12 3 293.67 29.00 14 12 -3 265.87 20.10 -14 -12 -3 199.78 27.20 -14 -12 -3 259.47 24.70 -14 -13 3 34.90 6.60 -14 -13 3 20.00 5.90 14 -13 -3 32.00 12.00 14 -13 -3 21.90 10.50 14 13 3 20.30 8.30 14 -13 -3 23.20 12.70 14 13 3 65.29 12.30 -14 -13 3 7.80 9.90 -14 -13 3 29.50 10.90 14 -13 -3 22.40 10.30 -14 -13 -3 32.50 13.30 -14 -13 -3 32.00 9.70 14 -13 3 35.90 13.60 14 -13 3 24.40 10.60 14 13 -3 18.60 6.30 -14 -13 -3 24.50 8.70 14 13 -3 31.30 8.30 -14 -14 3 75.99 18.10 14 -14 -3 120.69 19.30 14 -14 -3 100.79 18.40 -14 -14 3 88.29 10.40 14 14 3 77.39 14.30 -14 -14 3 116.49 17.50 14 14 3 95.19 14.40 -14 -14 -3 127.99 22.70 14 -14 3 73.79 16.80 14 14 -3 69.09 11.80 14 14 -3 103.49 12.60 14 -14 3 98.29 17.20 -14 -14 -3 86.29 15.80 -14 -15 3 3.20 8.10 -14 -15 3 -3.00 5.00 14 15 3 10.30 8.60 14 -15 -3 7.90 10.00 14 -15 -3 -2.50 9.20 14 15 3 4.90 7.10 14 15 -3 2.20 6.20 14 -15 3 9.70 11.10 14 -15 3 0.10 8.90 14 15 -3 3.00 6.20 14 -16 -3 43.30 14.30 14 16 3 18.00 10.70 14 16 3 26.50 9.80 -14 -16 3 33.30 12.00 14 16 -3 35.80 9.30 14 -16 3 37.10 14.00 14 16 -3 15.70 7.90 14 17 3 86.09 14.80 14 17 3 52.59 13.20 14 -17 -3 76.09 17.70 14 -17 3 66.29 17.50 14 17 -3 85.19 13.20 14 17 -3 46.10 11.00 14 18 3 9.50 10.00 14 18 -3 11.60 8.00 15 0 3 -0.10 5.80 -15 0 -3 -4.30 3.80 15 0 -3 -2.80 4.00 -15 0 3 -2.50 5.20 15 0 -3 -2.40 5.00 -15 0 3 -0.10 3.00 15 0 3 4.20 6.10 15 0 3 2.90 4.70 15 0 3 -3.80 4.80 15 0 -3 4.00 5.10 -15 0 3 2.90 4.90 15 0 -3 -3.10 5.50 15 0 3 5.70 7.80 15 0 -3 0.80 2.60 15 1 3 21.50 7.70 15 -1 -3 26.20 8.50 15 1 3 14.90 7.70 15 -1 -3 35.90 9.40 15 1 3 24.50 8.00 15 -1 -3 22.70 4.30 15 1 3 7.60 6.00 -15 -1 3 22.10 6.80 15 1 3 20.70 9.50 15 -1 -3 10.20 5.50 15 -1 -3 19.60 6.60 -15 1 -3 20.80 8.40 -15 1 3 22.20 4.50 15 -1 3 23.00 8.90 -15 1 3 14.00 6.60 15 1 -3 8.50 5.30 15 -1 3 33.30 9.00 -15 1 3 34.40 7.80 15 -1 3 15.70 9.20 15 -1 3 28.00 9.40 15 1 -3 33.70 8.60 15 1 -3 19.60 6.50 15 -1 3 16.80 6.70 15 1 -3 17.50 3.50 15 1 -3 21.50 7.70 -15 -1 -3 24.00 6.30 15 1 -3 20.60 3.60 -15 1 3 29.70 5.60 15 2 3 57.19 11.40 15 -2 -3 46.70 9.10 -15 -2 3 57.99 10.00 15 2 3 45.10 9.10 -15 2 -3 43.90 10.00 15 -2 -3 44.90 6.30 15 2 3 35.50 9.70 15 2 3 52.39 9.70 -15 2 -3 48.80 11.40 15 -2 -3 50.79 10.80 15 -2 -3 50.39 9.60 15 -2 3 32.10 8.60 15 2 -3 47.60 5.40 15 -2 3 52.49 12.20 15 2 -3 52.69 5.50 15 -2 3 56.19 12.70 -15 -2 -3 51.49 10.90 15 2 -3 42.10 8.00 15 -2 3 55.59 10.80 -15 2 3 44.00 7.50 15 2 -3 47.90 8.60 15 2 -3 53.19 10.20 15 -2 3 51.39 11.70 -15 2 3 49.90 10.90 -15 -2 -3 49.80 7.70 15 2 -3 51.89 9.80 -15 2 3 48.00 6.30 15 -3 -3 19.90 5.10 -15 -3 3 23.30 6.70 15 -3 -3 6.10 5.90 15 3 3 12.20 6.80 -15 3 -3 19.10 4.00 15 3 3 11.00 6.10 -15 3 -3 18.10 8.40 15 -3 -3 10.50 6.90 -15 3 -3 2.50 5.60 -15 3 -3 21.70 4.00 -15 3 -3 8.40 5.80 15 3 3 25.00 8.00 15 -3 -3 15.20 6.50 15 3 3 10.50 7.00 15 -3 3 16.40 7.40 -15 -3 -3 12.00 6.50 -15 3 3 13.60 5.00 15 -3 3 10.50 6.40 -15 3 3 11.30 5.20 15 3 -3 18.80 4.30 15 -3 3 7.50 7.90 15 -3 3 -2.30 6.40 15 3 -3 5.40 4.90 15 3 -3 11.40 3.60 15 3 -3 9.70 5.10 15 -3 3 20.60 8.90 15 3 -3 13.60 6.30 15 3 -3 11.20 6.30 -15 -3 -3 14.10 5.00 -15 -4 3 56.19 9.70 -15 4 -3 49.20 9.80 15 -4 -3 63.79 11.20 15 4 3 57.79 9.90 15 -4 -3 48.00 11.30 -15 4 -3 70.69 14.00 -15 4 -3 61.69 7.60 15 4 3 68.99 12.00 15 4 3 65.69 11.20 15 -4 -3 66.99 11.60 -15 4 -3 82.39 13.20 15 -4 -3 76.39 9.50 15 4 3 47.50 11.30 15 4 -3 79.09 8.30 15 4 -3 93.49 12.70 15 -4 3 73.69 14.20 15 4 -3 85.29 8.40 15 4 -3 76.69 11.00 15 4 -3 61.99 8.90 15 -4 3 58.19 12.60 15 -4 3 81.89 13.20 15 -4 3 67.89 11.80 15 -4 3 41.30 11.80 -15 -4 -3 69.39 8.40 -15 -4 -3 49.70 10.30 15 4 -3 56.89 8.80 -15 4 3 82.89 9.90 15 5 3 11.40 7.00 -15 5 -3 -6.70 5.00 -15 -5 3 4.50 5.20 15 5 3 12.80 7.30 15 -5 -3 8.10 7.10 15 -5 -3 13.40 6.90 15 5 3 9.70 3.50 -15 5 -3 11.40 5.20 -15 5 -3 9.10 6.00 15 5 3 0.70 4.80 -15 5 -3 7.70 7.60 15 -5 -3 4.20 5.00 -15 5 3 12.40 5.90 15 5 -3 14.40 6.20 -15 -5 -3 1.70 6.00 15 5 -3 18.10 5.60 15 5 -3 12.40 5.00 15 -5 3 2.80 4.30 15 5 -3 14.20 6.20 15 5 -3 12.70 4.80 -15 5 3 11.40 7.40 15 -5 3 19.70 8.30 -15 -5 -3 10.40 4.20 15 -5 3 11.20 8.90 15 -5 3 13.90 8.70 15 5 -3 9.00 4.50 15 -5 3 1.80 5.70 -15 6 -3 221.18 23.50 15 6 3 221.88 16.20 -15 -6 3 256.47 18.30 -15 6 -3 224.18 17.90 15 -6 -3 210.38 24.50 15 6 3 268.97 20.20 -15 6 -3 303.77 22.30 -15 6 -3 189.38 24.10 15 -6 -3 213.28 22.80 15 -6 -3 243.18 19.10 15 6 3 237.38 22.80 15 6 -3 294.47 21.10 -15 -6 -3 236.18 26.50 15 -6 3 307.97 29.70 15 6 -3 235.18 17.50 -15 6 3 229.08 18.90 -15 -6 -3 256.77 23.60 15 6 -3 269.47 17.70 15 6 -3 245.88 18.10 15 -6 3 229.38 18.30 -15 -6 -3 263.27 30.00 15 -6 3 201.98 22.30 -15 -6 -3 265.67 16.80 15 6 -3 246.38 18.00 15 6 -3 240.08 18.80 -15 7 -3 4.40 6.30 15 7 3 18.30 8.10 -15 -7 3 19.00 10.80 15 7 3 11.00 6.30 -15 -7 3 30.00 6.40 15 -7 -3 10.00 8.70 -15 7 -3 17.10 7.90 15 -7 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3 102.29 15.10 -16 -5 3 3.80 5.30 16 5 3 -2.60 6.70 16 -5 -3 8.80 6.70 16 5 3 -0.10 4.90 16 -5 -3 0.50 4.70 16 -5 3 3.10 6.40 16 5 -3 2.70 5.50 16 5 -3 -5.30 4.30 16 -5 3 5.70 7.80 16 5 -3 3.60 4.10 16 -5 3 11.60 9.00 -16 -6 3 315.07 22.30 16 6 3 263.27 25.80 16 6 3 318.17 23.80 16 -6 -3 332.47 23.10 16 -6 -3 294.27 27.20 16 6 -3 291.67 22.70 16 -6 3 367.36 34.00 16 -6 3 336.97 22.20 16 6 -3 336.87 21.80 16 -6 3 295.37 27.50 -16 -6 -3 335.77 33.90 -16 -7 3 60.19 9.00 16 7 3 44.30 9.50 16 -7 -3 50.39 11.60 16 7 3 64.29 11.90 16 -7 -3 63.59 10.80 16 7 -3 40.90 8.80 16 -7 3 51.79 9.60 16 -7 3 46.40 11.10 -16 -7 -3 36.40 12.40 16 7 -3 59.99 9.00 -16 -7 -3 58.49 15.10 16 8 3 506.15 36.20 16 -8 -3 572.64 36.30 -16 -8 3 564.74 33.20 -16 -8 3 556.64 43.10 16 8 3 528.05 35.10 16 -8 -3 486.85 36.90 -16 -8 3 551.24 33.60 16 8 -3 583.14 34.50 16 8 -3 549.85 32.70 16 -8 3 566.94 35.50 -16 -8 -3 520.05 42.40 16 -8 3 572.04 38.60 -16 -9 3 3.20 4.70 16 9 3 5.10 6.00 16 -9 -3 0.60 7.60 -16 -9 3 15.50 10.60 16 -9 -3 0.50 6.40 16 9 3 3.80 6.10 -16 -9 3 0.10 4.60 16 -9 3 15.20 7.90 -16 -9 -3 7.00 6.20 16 9 -3 2.90 4.90 16 -9 3 0.70 7.50 16 9 -3 8.00 6.00 -16 -9 -3 2.50 9.30 16 10 3 201.28 22.40 -16 -10 3 218.38 28.70 16 -10 -3 286.67 25.60 -16 -10 3 265.37 17.60 -16 -10 3 266.97 17.70 16 10 3 215.88 21.70 16 -10 -3 225.58 25.00 16 -10 -3 171.78 24.80 16 -10 3 240.18 25.40 16 10 -3 228.78 20.70 -16 -10 -3 205.48 27.70 -16 -10 -3 199.48 22.20 16 -10 3 249.08 24.10 16 10 -3 245.28 18.20 16 11 3 10.00 7.00 16 -11 -3 16.00 9.10 16 -11 -3 11.80 10.60 16 11 3 9.30 7.70 16 -11 -3 16.50 9.80 -16 -11 3 12.90 5.30 -16 -11 3 -6.80 8.80 -16 -11 3 6.90 4.60 -16 -11 -3 0.90 6.80 16 -11 3 17.60 8.70 16 -11 3 13.10 8.90 -16 -11 -3 8.40 9.60 16 11 -3 7.40 6.20 16 11 -3 16.10 5.50 16 -12 -3 121.79 18.00 -16 -12 3 117.89 11.80 16 12 3 132.69 17.50 16 -12 -3 122.59 21.40 16 -12 -3 92.69 16.80 16 12 3 127.19 16.10 -16 -12 3 115.69 21.30 16 12 -3 101.59 13.70 16 12 -3 105.69 13.00 -16 -12 -3 122.89 21.30 16 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17 4 3 53.99 12.30 17 -4 -3 95.79 14.90 -17 -4 3 85.49 12.20 17 -4 3 64.59 12.80 17 4 -3 71.29 11.90 17 4 -3 78.59 10.90 17 -4 3 73.69 15.40 -17 -5 3 6.40 5.30 17 5 3 14.20 6.90 17 5 3 -0.80 6.40 17 -5 -3 -6.20 5.90 17 5 -3 8.40 5.40 17 5 -3 4.20 6.00 17 -5 3 -0.40 7.00 17 6 3 157.88 19.10 17 -6 -3 134.09 18.00 17 6 3 173.78 18.30 -17 -6 3 172.68 16.20 17 -6 3 158.58 20.40 17 6 -3 171.58 17.50 17 6 -3 138.79 15.00 17 7 3 -3.10 5.60 -17 -7 3 10.90 5.60 17 7 3 1.50 7.20 17 -7 -3 16.60 9.00 17 -7 3 9.10 8.30 17 7 -3 1.30 5.00 -17 -7 -3 8.90 9.30 17 7 -3 13.60 6.60 17 8 3 184.18 21.10 17 8 3 178.08 19.50 17 -8 -3 222.18 24.20 -17 -8 3 222.28 16.90 -17 -8 3 205.98 16.10 17 8 -3 189.48 17.60 17 8 -3 172.58 18.10 -17 -8 -3 208.68 27.40 17 -8 3 189.68 22.60 -17 -9 3 -14.70 7.10 -17 -9 3 3.80 4.70 17 -9 -3 6.40 8.20 17 9 3 -6.40 5.90 17 9 3 2.70 5.90 17 9 -3 -0.60 4.60 17 -9 3 12.00 8.70 -17 -9 -3 -10.20 8.00 17 9 -3 1.10 5.30 17 10 3 238.48 24.20 -17 -10 3 271.17 18.40 -17 -10 3 229.28 30.40 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5.60 6.30 18 -9 3 3.70 8.20 -18 -9 -3 -0.10 9.50 18 9 -3 -1.10 5.30 -18 -10 3 256.27 18.40 18 10 3 269.87 24.50 18 -10 -3 200.18 24.20 18 10 3 220.88 24.30 18 10 -3 276.77 20.10 18 10 -3 186.68 20.50 18 -10 3 239.68 27.60 18 -11 -3 5.10 9.10 18 11 3 8.80 7.50 18 11 3 10.70 7.90 -18 -11 3 12.50 5.90 18 11 -3 3.70 6.40 18 11 -3 4.90 6.30 18 -11 3 -2.50 8.80 18 12 3 54.89 13.10 18 12 3 79.49 14.00 18 -12 -3 96.19 17.20 18 12 -3 66.39 11.90 18 12 -3 71.99 11.40 18 13 3 4.00 7.80 18 13 3 6.10 7.60 18 13 -3 19.20 8.00 18 13 -3 13.20 7.10 18 14 3 -1.20 7.70 18 14 3 21.40 10.00 18 14 -3 17.80 7.80 18 14 -3 7.80 7.10 19 0 -3 -5.40 5.00 19 0 3 -0.30 8.70 19 0 3 0.40 6.70 19 0 -3 -5.50 7.40 19 1 3 96.89 17.30 19 1 3 98.89 15.20 19 -1 -3 110.39 15.20 19 -1 -3 71.59 14.70 19 1 -3 94.49 15.50 19 -1 3 73.79 13.90 19 -1 3 127.99 19.60 19 1 -3 86.59 13.40 19 -2 -3 10.30 7.40 19 2 3 -2.00 6.40 19 2 3 15.10 9.00 19 2 -3 5.40 7.80 19 -2 3 8.40 9.00 19 -2 3 10.10 8.10 19 2 -3 8.30 6.80 19 3 3 22.40 10.20 19 -3 -3 19.20 8.80 19 3 3 6.40 7.60 19 3 -3 4.00 5.80 19 3 -3 22.20 8.60 19 -3 3 0.30 9.60 19 -3 3 13.70 8.10 19 4 3 53.59 13.20 19 4 3 60.69 11.80 19 -4 -3 60.99 12.50 19 -4 3 59.99 15.20 19 4 -3 54.29 10.20 19 4 -3 77.59 13.40 19 -4 3 40.80 10.70 19 -5 -3 31.80 10.40 19 5 3 44.80 10.80 19 5 3 32.90 11.20 19 5 -3 33.50 9.40 19 5 -3 37.00 8.90 19 -5 3 38.90 11.20 19 6 3 118.09 15.80 19 6 3 87.69 15.30 19 -6 -3 100.29 16.40 19 6 -3 88.39 12.50 19 6 -3 87.79 13.50 19 -6 3 111.69 17.40 19 7 3 9.20 7.30 19 7 3 10.50 8.60 19 -7 -3 18.70 9.80 19 7 -3 12.50 6.90 19 7 -3 9.40 5.80 19 -7 3 -1.50 7.50 19 8 3 80.89 13.80 19 8 3 123.69 17.10 19 -8 -3 87.79 15.80 19 -8 3 110.79 17.80 19 8 -3 118.19 14.00 19 8 -3 94.19 14.10 19 -9 -3 5.20 9.00 19 9 3 5.00 7.60 19 9 3 8.60 7.30 19 9 -3 4.10 6.70 19 -9 3 -1.50 7.90 19 9 -3 2.50 5.90 19 10 3 140.39 18.90 19 10 3 111.09 16.60 19 -10 -3 110.69 18.90 19 10 -3 159.98 16.60 19 -10 3 181.28 23.60 19 10 -3 121.79 15.80 19 -11 -3 17.60 10.80 19 11 3 10.00 8.60 19 11 3 16.60 9.60 19 11 -3 24.90 7.80 19 11 -3 23.50 8.30 19 12 3 47.20 12.00 19 12 3 38.10 10.80 19 -12 -3 33.80 12.50 19 12 -3 42.70 9.80 19 12 -3 60.99 11.60 19 13 3 21.10 10.00 19 13 3 18.60 9.40 19 13 -3 14.50 8.00 19 13 -3 12.30 7.50 20 0 -3 5.30 7.70 20 0 3 10.10 7.50 20 0 3 7.30 10.00 20 0 -3 -9.40 7.80 20 -1 -3 125.59 20.10 20 1 3 157.38 19.30 20 1 3 156.88 22.30 20 -1 -3 156.48 19.30 20 -1 3 168.18 20.30 20 1 -3 155.18 18.40 20 -1 3 229.28 26.40 20 1 -3 176.78 21.00 20 -2 -3 20.90 8.80 20 2 3 12.00 7.60 20 2 3 37.60 11.90 20 -2 3 25.90 9.80 20 2 -3 11.50 7.40 20 -2 3 18.10 11.10 20 2 -3 1.90 9.00 20 3 3 3.20 8.20 20 -3 -3 -3.80 6.10 20 3 3 5.50 7.20 20 -3 3 -0.70 10.20 20 3 -3 1.10 6.60 20 -3 3 14.60 8.50 20 3 -3 -1.20 6.80 20 4 3 147.89 18.70 20 4 3 130.49 19.00 20 -4 -3 109.69 16.80 20 -4 3 123.09 17.60 20 4 -3 147.29 18.20 20 -4 3 111.89 20.60 20 4 -3 116.69 15.10 20 5 3 1.60 7.10 20 5 3 23.20 10.40 20 -5 -3 14.40 8.80 20 5 -3 -1.20 6.60 20 5 -3 -3.30 5.20 20 -5 3 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7 4 1883.61 92.89 -5 -7 4 1873.51 93.09 5 -7 -4 1832.92 92.89 5 7 4 1921.31 97.39 5 -7 -4 1915.11 99.69 5 -7 4 1890.51 92.89 5 -7 4 1755.22 94.39 -5 -7 -4 1711.03 99.59 -5 -7 -4 1914.11 91.69 -5 7 4 1775.72 99.29 5 7 -4 1834.92 94.39 -5 7 4 1820.92 97.39 -5 -7 -4 1810.52 97.29 5 7 -4 1791.42 96.79 5 -7 4 1929.31 99.29 -5 -7 -4 1778.72 97.89 -5 7 4 1791.72 94.29 5 -7 4 1701.73 96.59 5 7 -4 1748.23 98.09 -5 7 4 1822.32 99.19 -5 7 4 1862.11 93.19 5 7 -4 1783.02 89.69 5 7 -4 1801.62 96.39 -5 -7 -4 1778.32 96.39 -5 7 4 1842.22 93.19 5 8 4 9.00 6.20 -5 -8 4 4.00 5.20 -5 -8 4 14.90 5.90 -5 8 -4 7.40 4.90 5 8 4 -0.60 4.10 5 8 4 10.20 4.50 5 -8 -4 9.50 6.20 -5 8 -4 -0.70 4.10 -5 8 -4 -0.10 5.00 5 -8 -4 1.70 5.80 5 -8 -4 1.60 5.00 5 8 4 -2.60 4.70 5 -8 -4 0.60 4.90 5 8 4 9.30 5.60 -5 8 -4 11.20 5.70 -5 8 -4 5.70 5.00 5 8 4 -0.50 4.20 5 -8 -4 5.10 4.40 -5 -8 4 1.50 4.80 -5 -8 4 5.90 2.90 -5 8 4 1.40 5.50 -5 -8 -4 6.20 5.90 5 8 -4 3.50 3.00 -5 8 4 5.60 4.60 5 8 -4 3.90 2.00 5 8 -4 6.80 3.90 5 -8 4 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422.96 32.40 -11 5 4 461.35 32.30 11 5 -4 437.16 28.00 -11 -5 -4 453.45 31.10 -11 -5 -4 412.66 33.70 11 5 -4 443.06 34.10 11 5 -4 489.35 28.60 11 -5 4 472.95 30.70 11 5 -4 452.55 28.50 11 -5 4 498.15 32.80 11 -5 4 498.55 28.80 -11 5 4 455.25 29.20 11 5 -4 462.65 26.60 -11 -5 -4 441.46 27.10 11 5 -4 461.75 24.60 11 -5 4 431.96 33.00 11 -5 4 453.45 30.30 11 5 -4 487.75 24.80 11 6 4 6.20 4.80 11 6 4 5.80 4.80 11 -6 -4 4.50 4.90 11 6 4 5.40 7.10 11 -6 -4 3.00 5.00 -11 -6 4 12.80 7.20 -11 6 -4 0.90 5.30 11 6 4 8.50 4.20 11 -6 -4 4.20 5.20 11 -6 -4 12.00 6.70 -11 -6 4 6.60 3.20 11 -6 -4 -2.40 4.60 -11 6 -4 4.80 4.80 -11 -6 4 5.10 3.00 -11 6 -4 5.70 6.20 -11 6 -4 7.70 5.50 11 6 4 4.60 4.50 11 6 -4 9.90 4.30 -11 -6 -4 1.60 4.00 11 6 -4 -5.60 5.90 11 6 -4 6.90 2.50 11 -6 4 2.90 4.40 -11 -6 -4 6.50 5.90 11 6 -4 2.50 2.30 -11 6 4 1.10 4.70 -11 -6 -4 6.90 3.90 -11 6 4 0.00 4.60 -11 6 4 6.20 4.70 11 6 -4 3.20 4.10 -11 6 4 -2.60 4.60 11 -6 4 7.30 5.50 11 6 -4 -1.00 4.10 -11 -6 -4 1.90 5.50 11 -6 4 8.40 6.60 11 6 -4 3.40 3.30 -11 -6 -4 -5.40 4.80 -11 7 -4 391.26 27.30 11 -7 -4 432.46 28.10 11 7 4 399.26 26.40 -11 -7 4 403.16 23.30 11 7 4 379.06 26.00 -11 7 -4 384.26 28.70 -11 -7 4 402.76 23.10 -11 7 -4 415.66 28.10 11 7 4 403.56 27.50 11 -7 -4 436.46 29.30 11 7 4 433.86 32.90 -11 -7 4 405.36 31.20 11 7 4 425.46 27.30 11 -7 -4 395.76 27.80 11 -7 -4 347.87 29.70 -11 7 -4 414.66 31.60 11 -7 -4 364.16 27.60 11 7 -4 407.66 24.00 -11 7 4 390.06 27.80 11 7 -4 373.86 26.50 11 7 -4 442.56 26.00 11 7 -4 421.16 22.00 -11 -7 -4 389.66 32.10 11 7 -4 456.65 33.00 -11 7 4 391.96 27.00 -11 -7 -4 415.26 29.00 -11 7 4 374.16 30.30 11 -7 4 440.16 28.90 -11 -7 -4 437.06 31.70 11 -7 4 479.25 32.70 11 -7 4 412.86 27.40 11 7 -4 419.36 21.80 -11 -7 -4 412.66 23.60 -11 -7 -4 401.36 26.20 -11 7 4 446.76 29.30 -11 -8 4 4.70 6.70 -11 8 -4 -4.70 4.80 11 -8 -4 -0.70 4.70 11 -8 -4 0.00 5.00 11 8 4 -1.40 5.40 -11 -8 4 0.90 2.70 11 8 4 -5.80 3.90 11 -8 -4 -4.40 4.70 -11 8 -4 2.00 5.20 11 8 4 -2.30 5.00 -11 8 -4 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299.47 23.80 -12 -12 4 315.97 19.60 12 -12 -4 345.17 31.40 12 -12 -4 273.47 28.30 12 -12 -4 289.17 28.60 12 -12 -4 249.38 28.80 -12 -12 4 291.57 28.20 12 -12 4 285.67 27.90 -12 -12 -4 331.77 26.20 12 12 -4 314.27 20.10 12 -12 4 310.37 29.70 12 -12 4 414.26 37.00 -12 -12 -4 323.67 33.80 12 -12 4 294.37 25.20 12 12 -4 329.97 22.20 -12 -12 -4 328.37 25.70 12 12 -4 325.87 20.80 -12 -12 -4 306.67 32.00 12 -13 -4 21.00 11.00 -12 -13 4 25.60 5.50 12 -13 -4 14.30 10.40 -12 -13 4 32.80 12.60 12 -13 -4 20.30 10.00 12 13 4 32.70 10.20 -12 -13 4 18.60 5.40 12 13 4 26.00 8.80 -12 13 -4 23.60 9.90 -12 13 -4 8.50 9.10 12 -13 -4 9.00 9.30 -12 -13 4 25.40 10.50 -12 -13 -4 21.80 8.90 12 -13 4 44.10 11.80 12 13 -4 13.00 6.10 -12 -13 -4 20.60 11.00 12 -13 4 26.70 11.90 12 13 -4 23.70 6.00 -12 -13 -4 20.70 9.60 12 -14 -4 130.89 21.10 -12 -14 4 133.49 12.50 -12 -14 4 144.59 23.00 -12 14 -4 127.19 18.50 12 -14 -4 136.09 20.80 12 -14 -4 156.98 24.20 -12 -14 4 151.58 12.10 12 14 4 134.49 17.70 -12 -14 4 111.99 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9 -4 -2.00 3.50 -14 9 4 2.00 6.70 14 9 -4 3.40 6.20 14 9 -4 -1.80 3.60 -14 -9 -4 0.00 8.20 14 -9 4 10.00 7.50 14 9 -4 -8.10 5.30 -14 -9 -4 -4.30 7.80 -14 -9 -4 -4.40 5.20 14 10 4 13.20 8.00 -14 -10 4 7.30 3.80 14 -10 -4 7.50 7.80 14 10 4 12.70 7.00 14 10 4 9.10 6.30 -14 10 -4 11.00 7.50 14 -10 -4 3.90 9.40 -14 10 -4 6.10 8.10 -14 -10 4 12.00 4.10 -14 -10 4 12.70 9.90 14 -10 -4 6.40 7.00 -14 -10 -4 26.00 11.70 14 -10 4 13.60 7.80 -14 -10 -4 14.70 7.60 14 -10 4 21.00 8.90 -14 -10 -4 4.80 6.80 14 10 -4 20.50 7.80 14 10 -4 12.20 5.10 14 10 -4 11.70 4.70 14 10 -4 7.90 5.10 14 -10 4 8.90 9.70 -14 -10 -4 11.20 9.80 14 -11 -4 30.20 9.90 14 -11 -4 31.50 10.90 -14 -11 4 14.90 10.50 14 11 4 25.80 8.60 14 -11 -4 24.70 11.20 14 11 4 27.10 9.30 -14 -11 4 30.00 5.20 -14 11 -4 24.70 10.60 -14 11 -4 16.10 9.00 -14 -11 4 27.30 4.90 -14 -11 -4 23.80 8.50 -14 -11 -4 19.00 10.60 14 11 -4 22.60 6.90 -14 -11 -4 29.20 9.00 14 -11 4 5.40 8.40 14 -11 4 28.70 10.20 14 -11 4 29.20 9.80 14 11 -4 29.20 6.50 14 -11 4 20.40 11.40 -14 -12 4 160.98 11.20 -14 12 -4 153.98 21.30 14 12 4 169.58 18.30 14 12 4 121.39 17.40 14 -12 -4 131.39 19.90 14 -12 -4 214.78 26.10 14 -12 -4 155.38 20.20 14 -12 -4 177.98 21.30 -14 -12 4 144.49 23.20 -14 -12 4 142.79 11.10 -14 12 -4 134.29 18.80 14 -12 4 153.78 23.40 14 -12 4 158.58 20.10 -14 -12 -4 113.39 16.60 -14 -12 -4 134.29 17.70 -14 -12 -4 102.99 20.10 14 12 -4 132.39 14.60 14 12 -4 133.89 13.60 14 13 4 10.60 8.50 -14 -13 4 13.90 11.00 14 -13 -4 3.60 8.90 14 -13 -4 8.20 9.20 14 -13 -4 32.50 11.70 14 -13 -4 -0.70 9.30 14 13 4 7.90 7.00 -14 -13 4 8.90 4.20 -14 -13 4 14.40 4.70 -14 -13 -4 5.30 7.80 14 13 -4 16.00 6.00 14 13 -4 10.10 6.50 14 -13 4 11.20 9.10 14 -13 4 14.40 10.40 -14 -13 -4 16.10 8.30 -14 -13 -4 13.40 10.70 -14 -14 4 260.47 16.80 14 -14 -4 278.77 29.80 -14 -14 4 260.67 16.60 -14 -14 4 286.17 28.20 14 -14 -4 285.77 31.30 -14 -14 4 340.47 36.20 14 14 4 235.48 25.30 14 14 4 233.78 23.90 14 14 -4 203.58 20.50 14 14 -4 262.27 19.60 14 -14 4 182.38 27.40 14 -14 4 270.17 29.20 14 -15 -4 -2.70 10.50 -14 -15 4 0.70 4.10 14 15 4 3.40 7.30 14 -15 -4 -3.70 8.90 -14 -15 4 -4.80 7.90 14 15 4 1.90 7.10 14 -15 4 -7.50 9.50 14 -15 4 -1.10 9.20 14 15 -4 11.00 6.70 14 15 -4 4.90 5.70 -14 -16 4 323.37 32.60 14 16 4 270.27 28.20 14 16 4 265.97 27.40 14 -16 -4 277.87 31.80 14 -16 4 309.97 33.40 14 16 -4 273.27 22.00 14 16 -4 285.47 23.00 14 17 4 0.90 7.80 14 -17 -4 2.80 10.60 14 17 4 -8.70 7.50 14 17 -4 -1.00 6.60 14 -17 4 -9.20 10.00 14 17 -4 -5.00 5.70 14 18 4 300.67 30.10 14 18 -4 240.38 24.30 15 0 4 14.80 7.40 15 0 -4 2.40 6.50 15 0 4 9.60 8.10 15 0 -4 7.60 5.00 -15 0 4 3.30 3.50 15 0 -4 6.20 4.70 15 0 -4 10.90 6.20 15 0 4 13.40 6.50 15 0 -4 8.00 3.40 -15 0 4 14.30 6.50 15 0 4 -0.20 6.10 15 0 4 10.80 7.30 15 -1 -4 17.90 7.70 -15 1 -4 17.40 8.00 15 1 4 16.50 6.90 15 1 4 8.10 8.30 15 -1 -4 38.20 5.60 15 1 4 25.10 9.00 15 1 4 33.40 9.20 15 1 4 19.50 7.60 15 -1 -4 19.20 6.00 -15 -1 4 19.80 6.90 -15 1 -4 14.70 6.80 15 -1 -4 16.50 6.90 15 -1 -4 19.80 6.60 15 -1 4 22.20 9.40 15 1 -4 30.30 6.90 15 -1 4 29.80 8.60 15 -1 4 9.10 7.20 15 1 -4 31.10 6.90 -15 -1 -4 24.70 6.50 -15 1 4 27.60 5.30 15 1 -4 19.70 4.30 -15 1 4 20.80 4.80 15 1 -4 22.50 7.70 15 -1 4 33.70 10.80 -15 1 4 33.10 8.60 15 1 -4 17.90 7.30 15 -1 4 16.30 7.40 15 -2 -4 19.30 7.10 15 2 4 11.00 6.90 -15 -2 4 13.00 6.10 -15 2 -4 27.50 7.70 15 2 4 3.40 6.00 15 2 4 7.80 6.40 -15 2 -4 21.00 8.80 15 -2 -4 20.60 7.40 15 -2 -4 24.30 5.40 15 -2 -4 6.60 6.00 15 2 4 19.60 6.90 15 -2 -4 14.90 6.30 -15 2 -4 24.80 7.10 15 -2 4 20.20 8.20 15 -2 4 22.00 9.10 15 2 -4 31.60 6.50 15 -2 4 12.30 7.40 15 2 -4 20.20 6.90 -15 2 4 19.70 5.40 15 2 -4 21.40 4.30 -15 2 4 17.40 7.60 15 -2 4 26.00 10.10 15 -2 4 17.60 9.00 -15 -2 -4 7.10 5.00 15 2 -4 24.70 4.80 -15 2 4 25.40 5.70 15 2 -4 16.70 5.70 15 2 -4 18.90 7.00 -15 3 -4 3.40 7.10 15 3 4 -0.90 5.00 -15 3 -4 0.50 5.00 15 -3 -4 8.00 4.80 15 -3 -4 -8.80 4.30 15 -3 -4 5.40 5.60 -15 3 -4 -0.40 5.60 15 -3 -4 -7.20 4.50 15 3 4 1.90 5.90 15 3 4 4.10 6.10 -15 3 -4 0.80 3.10 -15 -3 4 1.60 5.00 -15 3 -4 1.00 3.00 15 3 4 -3.80 4.30 -15 -3 -4 -0.30 5.40 15 -3 4 10.10 6.60 -15 3 4 0.10 4.00 -15 3 4 4.70 6.00 15 3 -4 2.20 3.50 15 -3 4 -9.20 5.80 15 -3 4 0.30 5.70 15 -3 4 2.10 7.40 -15 -3 -4 5.00 4.60 15 3 -4 9.70 3.90 15 3 -4 -4.30 3.40 15 3 -4 -0.60 5.00 15 3 -4 -3.50 4.30 -15 3 4 0.20 4.40 15 3 -4 2.40 4.00 15 -3 4 -4.60 5.90 -15 4 -4 8.40 7.40 15 -4 -4 -2.40 5.40 15 4 4 0.50 6.60 -15 4 -4 7.00 6.60 15 -4 -4 -5.30 4.30 -15 4 -4 -5.40 3.70 -15 4 -4 -4.50 3.30 -15 -4 4 -4.30 4.40 15 -4 -4 -1.50 5.20 15 4 4 1.50 5.20 -15 4 -4 2.70 5.30 15 4 4 5.50 6.70 -15 4 4 3.30 4.80 15 4 -4 -2.00 3.60 15 -4 4 8.00 8.00 15 4 -4 -2.80 4.40 15 -4 4 4.00 6.40 15 4 -4 -0.20 3.60 15 4 -4 5.00 4.20 15 4 -4 3.50 4.90 15 4 -4 -2.80 3.60 15 -4 4 5.80 8.00 -15 -4 -4 11.80 6.90 15 -4 4 2.20 6.90 15 -4 4 1.80 6.30 15 -5 -4 33.20 9.30 15 5 4 19.50 8.50 -15 -5 4 12.90 5.50 15 5 4 22.00 8.10 -15 5 -4 19.00 7.30 -15 5 -4 13.70 7.60 15 5 4 12.70 6.10 15 5 4 20.30 4.30 15 -5 -4 15.60 6.30 -15 5 -4 12.20 8.40 15 -5 -4 10.40 7.00 -15 5 -4 12.10 5.30 -15 -5 -4 12.80 7.20 -15 -5 -4 12.00 3.80 15 -5 4 5.30 6.80 15 5 -4 13.60 6.00 15 5 -4 13.40 5.10 -15 -5 -4 27.40 10.50 15 -5 4 23.00 10.60 15 5 -4 14.40 5.40 15 -5 4 17.10 9.20 15 5 -4 13.00 6.30 15 5 -4 13.50 6.10 15 -5 4 22.10 9.60 -15 -5 -4 4.30 8.70 15 5 -4 15.30 5.10 -15 5 4 11.30 5.80 15 -6 -4 9.00 7.00 -15 6 -4 4.10 5.40 15 -6 -4 12.00 6.30 -15 6 -4 0.80 6.50 -15 6 -4 1.70 7.50 15 6 4 3.90 3.90 -15 6 -4 1.10 5.50 15 6 4 0.50 5.40 -15 -6 4 -3.60 3.90 15 6 4 -3.30 5.40 15 -6 -4 -1.30 5.60 15 6 -4 4.90 5.50 -15 -6 -4 -0.40 3.80 15 -6 4 5.50 8.60 -15 -6 -4 4.40 7.70 15 6 -4 1.70 3.80 -15 6 4 -3.90 5.00 15 6 -4 -1.70 4.40 15 -6 4 -5.00 4.80 15 -6 4 1.90 6.80 15 -6 4 15.10 8.60 -15 -6 -4 -4.60 6.80 15 6 -4 -5.90 3.80 15 6 -4 -6.10 4.20 15 6 -4 2.60 4.90 15 7 4 314.77 25.00 -15 7 -4 350.86 30.50 -15 -7 4 322.87 20.90 -15 7 -4 336.77 25.50 -15 -7 4 283.37 20.10 15 7 4 303.77 23.30 15 -7 -4 280.97 26.80 -15 7 -4 332.07 23.10 15 -7 -4 331.37 24.00 -15 -7 -4 248.08 29.20 15 7 -4 295.17 22.30 15 7 -4 336.47 20.50 15 7 -4 308.37 22.40 15 -7 4 312.97 22.70 15 7 -4 307.87 23.20 15 -7 4 387.36 35.10 15 -7 4 328.07 25.90 15 7 -4 273.67 21.00 -15 7 4 288.17 23.10 15 7 -4 303.77 20.10 -15 -7 -4 284.17 32.70 -15 -7 -4 349.07 21.30 -15 -8 4 0.90 3.80 -15 8 -4 3.00 6.40 15 -8 -4 -1.50 6.30 15 8 4 0.90 6.50 15 8 4 0.50 5.10 -15 -8 4 10.70 9.40 -15 -8 4 1.30 3.50 15 -8 -4 -3.00 6.30 15 8 -4 -1.20 4.20 15 8 -4 1.50 4.00 15 8 -4 -0.70 4.50 -15 8 4 9.00 7.20 15 -8 4 -13.40 5.20 15 8 -4 16.70 7.20 -15 -8 -4 1.50 8.70 15 -8 4 4.10 7.20 15 -8 4 5.30 9.20 -15 -8 -4 11.10 9.00 15 8 -4 -2.70 5.30 15 9 4 50.39 10.30 -15 -9 4 54.09 7.20 15 -9 -4 44.10 10.40 15 -9 -4 46.80 11.50 -15 -9 4 51.59 6.80 -15 9 -4 50.19 10.80 15 9 4 45.40 11.00 -15 -9 4 24.60 11.90 15 -9 4 43.10 10.30 -15 9 4 51.19 11.20 -15 -9 -4 39.50 13.40 15 9 -4 36.30 9.30 15 -9 4 59.49 14.80 15 9 -4 39.30 8.10 15 -9 4 43.30 11.70 -15 -9 -4 60.09 12.00 15 9 -4 44.50 7.50 15 -10 -4 2.50 7.40 -15 -10 4 6.50 10.10 -15 -10 4 -0.90 3.40 15 10 4 0.10 5.70 -15 -10 4 3.60 3.90 15 -10 -4 -3.90 8.10 15 -10 -4 -4.50 7.30 15 10 4 12.50 7.90 15 10 -4 6.90 4.70 15 10 -4 0.20 6.10 15 -10 4 11.60 8.80 15 -10 4 3.80 8.50 -15 -10 -4 -3.00 8.70 15 10 -4 -1.30 5.10 -15 -10 -4 7.00 6.70 15 -10 4 -4.70 6.50 -15 -11 4 65.89 16.40 15 -11 -4 99.69 17.80 15 11 4 72.69 13.80 15 -11 -4 93.99 15.70 15 -11 -4 100.39 16.30 -15 -11 4 90.79 8.70 15 11 4 79.29 12.80 -15 -11 4 93.39 8.70 15 -11 4 91.09 18.60 15 11 -4 75.59 11.00 -15 -11 -4 63.89 12.50 15 -11 4 93.39 15.40 15 11 -4 87.99 10.60 -15 -11 -4 69.39 16.70 15 -11 4 118.09 18.00 15 12 4 -0.40 7.50 15 -12 -4 6.90 10.10 -15 -12 4 14.90 11.00 -15 -12 4 7.80 3.80 15 -12 -4 0.30 7.70 15 -12 -4 14.00 9.40 -15 -12 4 0.60 3.70 15 -12 -4 4.00 9.10 15 12 4 18.90 8.20 15 12 -4 10.50 6.00 -15 -12 -4 0.70 7.00 15 12 -4 12.00 5.70 15 -12 4 -1.60 9.00 15 -12 4 -0.70 8.70 -15 -12 -4 4.40 8.90 15 13 4 -3.00 6.10 -15 -13 4 1.40 3.70 15 -13 -4 -4.70 8.60 15 -13 -4 5.30 10.40 15 -13 -4 12.60 10.50 -15 -13 4 4.30 3.60 -15 -13 4 12.50 11.40 15 -13 -4 -7.90 8.00 15 13 4 15.10 7.80 15 -13 4 8.50 9.00 -15 -13 -4 -0.50 9.50 15 13 -4 -0.90 5.50 15 13 -4 -5.40 4.70 15 -14 -4 12.40 10.60 15 14 4 9.90 7.90 -15 -14 4 19.70 4.80 15 -14 -4 -10.00 9.70 15 14 4 24.20 10.40 15 14 -4 8.20 5.80 15 -14 4 4.20 9.70 15 14 -4 9.20 6.70 15 -15 -4 28.10 13.30 15 15 4 15.40 9.80 15 15 4 26.20 10.60 15 -15 -4 31.20 12.90 15 15 -4 30.40 8.10 15 -15 4 42.00 13.60 15 15 -4 36.70 9.60 15 16 4 6.10 7.60 15 16 4 -3.20 8.50 15 -16 -4 -3.50 10.80 15 -16 4 7.50 11.00 15 16 -4 6.10 6.40 15 16 -4 4.30 6.10 15 17 4 12.30 10.60 15 -17 -4 15.30 13.30 15 17 -4 13.40 8.00 15 -17 4 5.50 11.10 15 17 -4 26.10 9.10 16 0 -4 838.62 51.69 16 0 -4 844.12 44.30 16 0 4 827.62 49.80 -16 0 4 783.32 50.29 16 0 -4 792.02 49.70 16 0 -4 862.41 48.00 16 0 4 856.11 52.09 16 0 4 847.02 54.29 16 -1 -4 6.30 3.80 16 -1 -4 1.90 5.00 -16 -1 4 5.40 5.50 16 -1 -4 9.40 7.00 16 1 4 -5.20 4.80 16 1 4 1.00 6.10 16 -1 -4 2.70 6.10 16 1 4 11.20 7.60 -16 1 4 2.10 3.70 16 1 -4 1.60 2.90 16 1 -4 -1.30 4.70 -16 1 4 7.80 6.10 16 1 -4 6.20 5.80 16 -1 4 3.50 6.90 16 1 -4 7.70 3.40 16 -1 4 9.70 7.90 -16 1 4 1.90 3.50 16 1 -4 -1.90 5.40 16 -1 4 5.80 5.90 16 2 4 186.48 21.30 16 -2 -4 208.38 20.20 16 2 4 235.38 22.10 -16 -2 4 242.48 19.20 16 -2 -4 219.08 15.30 16 -2 4 234.58 25.60 16 2 -4 237.68 14.60 16 2 -4 235.38 14.60 16 2 -4 187.18 20.00 -16 2 4 210.38 15.50 16 -2 4 270.47 27.40 16 2 -4 221.58 17.40 16 2 -4 225.38 21.70 16 -2 4 254.77 27.60 16 -2 4 223.08 22.40 -16 -3 4 11.00 6.40 16 -3 -4 5.10 6.20 16 -3 -4 3.90 4.40 16 3 4 12.00 8.00 16 3 4 9.90 6.40 16 -3 4 2.10 7.60 16 3 -4 3.70 6.10 16 -3 4 10.90 7.30 16 3 -4 5.60 3.80 16 -3 4 5.40 8.80 16 3 -4 10.40 6.70 16 3 -4 4.60 4.90 16 -3 4 9.60 8.00 -16 3 4 3.20 4.50 16 3 -4 12.20 5.50 -16 -4 4 740.63 42.10 16 4 4 683.33 42.60 16 -4 -4 711.13 40.40 16 -4 -4 673.23 43.20 16 4 4 720.03 44.90 16 4 -4 695.33 41.60 16 -4 4 743.13 49.00 16 -4 4 676.03 44.00 16 -4 4 649.43 47.60 16 4 -4 714.23 39.90 16 -4 4 701.43 46.90 16 4 -4 703.73 43.80 16 4 -4 744.63 39.40 16 4 -4 629.74 39.40 16 -5 -4 4.40 5.60 16 5 4 -4.50 6.20 16 -5 -4 4.30 6.30 -16 -5 4 3.00 4.90 16 5 4 2.70 5.70 16 -5 4 -3.20 7.90 16 -5 4 -3.10 7.60 16 5 -4 6.50 5.70 16 5 -4 4.40 4.80 16 5 -4 8.30 4.60 16 -5 4 3.20 8.10 16 -5 4 6.30 6.80 16 -6 -4 197.78 21.30 16 6 4 201.18 20.50 16 6 4 182.18 20.80 16 -6 -4 228.48 19.90 -16 -6 4 239.28 16.90 16 -6 4 280.17 28.30 16 -6 4 208.78 22.40 16 -6 4 236.38 26.30 -16 -6 -4 218.78 28.30 -16 -6 -4 152.08 22.90 16 6 -4 217.58 16.40 16 6 -4 207.28 19.10 16 -7 -4 3.20 6.40 -16 -7 4 1.60 4.30 16 7 4 3.40 6.80 16 -7 -4 18.40 8.10 16 7 4 -5.70 5.10 -16 -7 -4 -6.00 7.70 16 -7 4 0.90 7.40 16 -7 4 -7.00 8.00 16 -7 4 15.10 6.70 16 7 -4 6.50 4.90 16 -7 4 8.70 9.90 16 7 -4 2.80 5.30 -16 -8 4 15.30 5.30 16 8 4 19.30 8.50 16 -8 -4 16.80 8.50 -16 -8 4 22.10 5.60 16 -8 -4 29.10 9.10 16 8 4 27.10 8.30 -16 -8 4 37.50 13.20 16 8 -4 13.60 6.40 16 8 -4 33.20 6.90 -16 -8 -4 28.20 11.60 16 -8 4 19.90 8.00 16 -8 4 19.70 9.70 -16 -9 4 14.20 5.00 16 -9 -4 6.20 7.80 -16 -9 4 10.30 4.80 16 9 4 3.60 7.00 16 -9 -4 2.70 7.30 -16 -9 4 6.20 9.70 16 9 4 4.90 6.40 16 9 -4 9.20 6.10 -16 -9 -4 -0.90 8.80 16 -9 4 -2.50 6.50 16 9 -4 3.50 4.60 16 -9 4 -4.80 6.40 -16 -10 4 68.69 8.00 16 -10 -4 64.09 12.90 -16 -10 4 67.49 8.00 16 10 4 68.19 12.00 16 10 4 89.89 14.70 16 -10 -4 78.29 15.00 -16 -10 4 51.89 15.00 16 -10 -4 79.89 17.00 -16 -10 -4 35.30 13.80 16 -10 4 61.69 13.90 16 10 -4 69.69 10.70 16 10 -4 64.89 9.50 16 -10 4 82.79 13.90 -16 -10 -4 72.59 13.50 16 -11 -4 -7.90 7.00 16 11 4 -9.90 5.60 16 11 4 16.80 8.80 16 -11 -4 1.50 8.00 -16 -11 4 -10.80 8.70 16 -11 -4 -6.90 8.20 -16 -11 4 3.80 3.70 -16 -11 4 -3.60 3.50 16 11 -4 1.90 5.30 16 11 -4 7.70 5.30 16 -11 4 -6.00 7.10 -16 -11 -4 -8.70 9.30 -16 -11 -4 -5.00 6.30 16 -12 -4 89.59 17.10 16 12 4 83.69 13.50 -16 -12 4 75.59 7.50 16 -12 -4 85.09 15.40 -16 -12 4 66.39 17.20 -16 -12 4 72.69 7.60 16 -12 -4 47.50 15.20 16 12 4 77.29 14.00 -16 -12 -4 48.10 15.20 16 12 -4 73.89 11.20 16 12 -4 68.89 10.40 16 13 4 -1.60 6.60 16 -13 -4 -8.70 9.20 16 -13 -4 -1.40 8.50 -16 -13 4 5.90 3.70 16 -13 -4 10.10 10.10 16 -13 -4 3.40 10.90 16 13 4 -5.70 6.70 16 13 -4 3.00 4.90 16 13 -4 -0.30 6.00 16 -14 -4 321.47 31.80 16 14 4 303.87 28.10 -16 -14 4 297.97 17.50 16 14 4 285.37 28.10 16 14 -4 276.67 21.40 16 14 -4 242.18 23.00 16 15 4 2.50 8.10 16 15 4 5.10 8.70 16 -15 -4 20.00 11.50 16 15 -4 10.20 6.00 16 15 -4 12.90 7.10 16 -16 -4 100.19 20.00 16 16 4 109.39 17.70 16 16 4 108.59 18.10 16 16 -4 128.89 15.60 16 16 -4 120.39 15.50 17 0 4 57.59 12.80 17 0 -4 53.39 11.90 17 0 -4 49.10 9.80 17 0 4 57.29 11.30 17 1 4 -11.00 6.10 17 1 4 -5.30 5.40 17 -1 -4 -0.60 7.20 17 -1 -4 0.10 5.20 17 -1 4 3.50 6.10 17 -1 4 -9.70 6.10 17 1 -4 -4.20 5.70 17 1 -4 4.30 5.50 17 2 4 -4.00 7.20 -17 -2 4 -5.10 5.10 17 2 4 -4.30 5.20 17 -2 -4 -0.30 5.70 17 2 -4 -6.80 4.20 17 2 -4 2.30 6.30 17 -2 4 -1.30 5.70 17 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9.30 5.00 17 9 4 2.50 7.20 17 -9 -4 26.80 10.10 17 9 -4 9.00 6.10 17 9 -4 3.70 4.70 17 -9 4 -3.10 7.60 -17 -9 -4 16.20 10.50 17 10 4 10.80 7.40 17 -10 -4 12.50 10.30 17 -10 -4 -10.60 6.20 -17 -10 4 5.40 4.40 -17 -10 4 1.20 4.30 -17 -10 4 4.10 10.60 17 10 4 1.70 7.10 -17 -10 -4 3.10 7.40 17 10 -4 1.10 4.70 17 10 -4 0.30 5.50 17 -10 4 5.90 9.10 -17 -10 -4 15.20 10.60 17 11 4 11.40 7.60 17 -11 -4 -5.70 7.20 17 -11 -4 4.40 11.00 -17 -11 4 3.40 3.90 17 11 4 9.50 8.30 -17 -11 4 5.90 4.20 -17 -11 4 -7.40 9.30 17 11 -4 -6.50 5.00 17 11 -4 -2.40 5.60 17 -11 4 15.20 9.80 -17 -11 -4 1.10 9.80 17 12 4 3.90 7.90 17 -12 -4 5.30 9.00 17 12 4 19.60 8.60 -17 -12 4 4.90 3.80 17 12 -4 5.20 5.90 17 12 -4 6.00 5.50 -17 -13 4 10.00 3.90 17 -13 -4 1.60 9.20 17 13 4 3.20 7.50 17 -13 -4 25.10 12.60 17 13 4 14.20 8.80 17 13 -4 20.50 7.60 17 13 -4 12.50 6.50 17 14 4 -6.60 7.50 17 14 4 8.40 7.80 17 14 -4 -0.30 5.80 17 14 -4 2.90 5.80 17 15 4 -2.00 8.40 17 15 4 18.30 9.80 17 15 -4 11.40 7.40 17 15 -4 7.10 7.00 18 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7 -4 10.60 7.30 18 8 4 81.89 14.00 18 -8 -4 65.89 13.80 -18 -8 4 71.19 9.80 18 8 4 68.09 12.50 18 8 -4 76.79 10.60 18 8 -4 57.39 10.60 18 -8 4 69.89 14.40 -18 -8 -4 86.29 19.10 18 -9 -4 2.90 8.20 18 9 4 11.00 8.60 18 9 4 11.00 7.70 -18 -9 4 13.60 5.70 -18 -9 -4 5.10 10.10 18 9 -4 1.20 5.90 18 9 -4 1.90 5.20 18 -9 4 -5.20 7.60 18 10 4 4.90 6.90 18 -10 -4 -3.90 7.80 -18 -10 4 -1.60 4.30 18 10 4 4.60 7.60 18 10 -4 3.50 5.30 18 -10 4 -1.60 8.50 18 10 -4 4.10 6.00 -18 -11 4 6.00 4.30 18 11 4 -1.00 6.80 18 -11 -4 -9.60 7.00 18 11 4 -7.00 6.60 18 11 -4 0.00 5.90 18 11 -4 -3.40 5.20 18 12 4 26.70 9.70 18 -12 -4 -1.70 9.10 18 12 4 6.90 8.20 -18 -12 4 17.90 4.80 18 12 -4 17.50 7.80 18 12 -4 10.00 6.60 18 13 4 23.90 9.50 18 13 4 2.30 8.40 18 -13 -4 5.10 9.60 18 13 -4 -0.90 5.60 18 13 -4 -2.60 5.20 18 14 4 211.48 24.50 18 14 4 235.68 26.00 18 14 -4 221.18 21.00 18 14 -4 257.17 23.10 19 0 4 1.60 7.10 19 0 4 2.30 8.10 19 0 -4 0.70 6.20 19 0 -4 12.00 9.20 19 -1 -4 3.50 6.40 19 1 4 -2.50 6.50 19 1 4 12.00 9.80 19 1 -4 -7.40 7.10 19 -1 4 2.70 6.80 19 1 -4 0.20 6.30 19 -1 4 -0.30 8.40 19 -2 -4 -5.60 5.90 19 2 4 12.00 9.30 19 2 4 1.10 6.70 19 2 -4 -0.70 5.90 19 -2 4 -1.60 8.50 19 2 -4 13.30 8.00 19 -2 4 2.60 7.00 19 -3 -4 25.60 9.30 19 3 4 14.00 9.20 19 3 4 38.70 10.50 19 3 -4 23.30 7.70 19 3 -4 24.30 9.40 19 -3 4 26.30 10.00 19 -3 4 28.70 12.00 19 -4 -4 -2.10 6.80 19 4 4 3.80 8.00 19 4 4 -2.00 6.20 19 4 -4 1.70 6.40 19 -4 4 10.80 10.70 19 -4 4 -7.30 6.60 19 4 -4 13.40 6.60 19 -5 -4 5.00 7.80 19 5 4 3.60 6.90 19 5 4 16.30 9.50 19 -5 4 8.40 10.10 19 -5 4 14.10 9.00 19 5 -4 15.40 7.80 19 5 -4 23.70 7.40 19 -6 -4 -0.60 7.20 19 6 4 13.50 9.40 19 6 4 -5.40 6.30 19 -6 4 2.40 8.00 19 6 -4 6.30 5.30 19 6 -4 -2.70 5.70 19 7 4 155.98 20.60 19 -7 -4 163.18 20.80 19 7 4 171.08 20.00 19 -7 4 188.78 23.20 19 7 -4 224.68 19.30 19 7 -4 185.08 19.10 19 -8 -4 6.40 8.50 19 8 4 -5.00 5.70 19 8 4 -3.90 7.10 -19 -8 4 2.70 5.50 19 8 -4 7.30 6.80 19 8 -4 3.00 5.10 19 -8 4 6.90 8.80 -19 -8 -4 -11.50 8.50 19 9 4 62.89 12.70 -19 -9 4 61.79 9.40 19 -9 -4 54.79 13.70 19 9 4 70.89 14.50 19 9 -4 43.90 10.10 19 -9 4 76.29 15.80 19 9 -4 69.59 10.90 19 10 4 -1.00 7.10 19 10 4 0.00 7.90 19 -10 -4 3.50 9.40 19 10 -4 -1.80 6.20 19 -10 4 1.60 8.80 19 10 -4 6.60 5.90 19 11 4 93.39 15.50 19 11 4 131.19 18.30 19 -11 -4 108.59 18.40 19 11 -4 71.19 12.50 19 11 -4 114.29 13.80 19 12 4 2.30 7.90 19 -12 -4 11.80 11.30 19 12 4 2.60 8.40 19 12 -4 -1.40 5.60 19 12 -4 4.60 6.60 19 13 4 6.70 9.30 19 13 -4 -2.50 6.20 19 13 -4 3.80 6.30 20 0 4 689.53 46.50 20 0 -4 712.83 45.10 20 0 4 734.83 49.80 20 0 -4 759.82 48.30 20 -1 -4 10.60 8.50 20 1 4 0.40 8.90 20 1 4 26.10 9.40 20 -1 4 16.00 11.30 20 1 -4 0.80 6.50 20 -1 4 16.00 8.90 20 1 -4 19.60 10.10 20 2 4 454.15 38.70 20 2 4 402.46 30.80 20 -2 -4 369.86 29.60 20 -2 4 382.96 34.50 20 -2 4 394.26 38.10 20 2 -4 405.76 31.40 20 2 -4 437.66 29.80 20 -3 -4 8.00 8.30 20 3 4 6.40 7.80 20 3 4 -2.50 7.60 20 3 -4 8.50 6.50 20 -3 4 -3.80 9.90 20 3 -4 -2.50 6.50 20 -3 4 9.10 8.10 20 4 4 80.69 15.70 20 4 4 68.89 13.70 20 -4 -4 90.89 15.80 20 4 -4 95.99 14.90 20 -4 4 106.09 19.40 20 4 -4 107.29 14.10 20 -4 4 104.29 17.10 20 5 4 0.40 8.00 20 -5 -4 -1.20 7.40 20 5 4 1.50 6.80 20 -5 4 -4.90 7.10 20 5 -4 10.80 6.60 20 5 -4 -6.20 6.50 20 6 4 57.29 13.50 20 -6 -4 56.69 13.80 20 6 4 49.10 11.80 20 -6 4 40.60 12.30 20 6 -4 60.39 10.80 20 6 -4 57.79 11.60 20 7 4 4.50 8.50 20 -7 -4 20.40 9.70 20 7 4 -3.10 6.70 20 7 -4 12.10 6.60 20 -7 4 7.60 8.40 20 7 -4 9.90 7.10 20 8 4 25.50 10.80 20 8 4 36.60 10.70 20 -8 -4 27.90 11.30 20 8 -4 38.00 9.80 20 8 -4 39.40 8.90 20 -8 4 36.50 12.90 20 -9 -4 -2.60 8.50 20 9 4 8.80 8.20 20 9 4 0.40 8.10 20 9 -4 1.40 6.30 20 -9 4 6.10 9.20 20 9 -4 8.20 6.30 20 -10 -4 25.80 11.70 20 10 4 21.70 9.80 20 10 4 19.80 10.20 20 10 -4 12.40 7.80 20 10 -4 22.60 7.80 20 -10 4 13.10 10.40 20 11 4 5.90 8.60 20 11 4 5.50 8.00 20 -11 -4 -0.70 9.80 20 11 -4 -4.50 6.30 20 11 -4 1.00 5.80 20 12 4 -5.80 8.40 20 -12 -4 3.90 10.10 20 12 -4 -1.20 6.00 20 12 -4 -4.20 5.80 21 0 4 -0.30 9.50 21 0 -4 3.70 10.30 21 0 4 2.60 8.20 21 0 -4 1.20 6.80 21 1 4 9.40 8.40 21 1 4 0.60 9.40 21 -1 -4 2.30 6.50 21 -1 4 2.30 7.70 21 1 -4 -6.10 8.30 21 -1 4 -9.60 8.80 21 1 -4 4.00 7.30 21 2 4 -0.80 8.70 21 -2 -4 11.10 8.00 21 2 4 5.90 8.00 21 2 -4 -5.80 7.90 21 2 -4 0.50 6.60 21 -2 4 0.70 7.50 21 -2 4 -2.10 9.30 21 -3 -4 72.19 14.30 21 3 4 62.69 15.10 21 3 4 63.29 13.60 21 3 -4 71.99 12.80 21 3 -4 106.29 16.30 21 -3 4 84.39 16.30 21 -3 4 77.59 17.60 21 4 4 -4.30 6.70 21 4 4 -1.10 8.30 21 -4 -4 -7.30 7.30 21 -4 4 4.90 10.40 21 4 -4 0.80 6.80 21 4 -4 -2.60 5.50 21 -4 4 5.70 8.30 21 5 4 54.59 13.80 21 5 4 84.49 15.20 21 -5 -4 80.19 14.90 21 5 -4 67.89 13.30 21 5 -4 76.39 12.40 21 -5 4 73.99 15.40 21 6 4 0.00 7.20 21 6 4 0.80 8.40 21 -6 -4 -4.00 7.60 21 6 -4 -0.50 5.90 21 6 -4 -6.10 6.40 21 -6 4 -17.70 6.30 21 7 4 292.87 30.70 21 7 4 345.87 30.60 21 -7 -4 300.17 30.70 21 -7 4 294.27 31.30 21 7 -4 313.07 28.10 21 7 -4 355.96 25.20 21 8 4 -8.80 6.70 21 -8 -4 -14.30 7.50 21 8 4 -8.70 7.20 21 8 -4 4.20 6.80 21 -8 4 -8.20 8.30 21 8 -4 0.10 5.90 21 -9 -4 131.99 20.30 21 9 4 121.29 19.20 21 9 4 125.89 18.30 21 -9 4 172.48 23.50 21 9 -4 139.69 17.50 21 9 -4 158.58 17.40 21 -10 -4 -3.30 8.20 21 10 4 -1.10 6.80 21 10 4 -4.30 8.10 21 10 -4 5.40 7.00 21 10 -4 -1.20 6.10 21 11 4 241.78 26.50 21 -11 -4 220.28 27.80 21 11 -4 210.98 22.30 22 0 -4 3.30 7.90 22 0 -4 15.70 10.60 22 0 4 -0.80 10.40 22 0 4 1.90 7.90 22 1 4 10.80 8.50 22 1 4 16.50 11.70 22 -1 -4 4.00 8.20 22 1 -4 -0.20 6.90 22 -1 4 5.00 8.20 22 1 -4 -2.90 8.40 22 -1 4 0.80 10.00 22 2 4 180.88 22.60 22 -2 -4 200.58 22.40 22 2 4 205.68 25.90 22 2 -4 183.18 22.80 22 2 -4 190.68 21.20 22 -2 4 151.28 24.20 22 -2 4 182.78 22.90 22 3 4 32.90 12.20 22 -3 -4 16.20 9.20 22 3 4 22.90 10.10 22 -3 4 16.70 13.10 22 3 -4 13.00 8.50 22 -3 4 1.40 8.80 22 3 -4 25.60 10.50 22 -4 -4 25.40 11.00 22 4 4 31.10 10.60 22 4 4 16.90 10.50 22 4 -4 30.10 9.80 22 -4 4 19.50 10.70 22 4 -4 29.10 11.10 22 -4 4 16.70 12.50 22 -5 -4 8.90 9.00 22 5 4 -4.60 6.60 22 5 4 -3.10 7.70 22 -5 4 -6.30 8.00 22 5 -4 -1.20 7.20 22 5 -4 -2.40 5.80 22 -6 -4 100.49 17.70 22 6 4 87.49 15.40 22 6 4 81.89 16.50 22 6 -4 76.89 14.10 22 -6 4 77.29 16.50 22 6 -4 92.69 14.00 22 7 4 5.10 8.30 22 -7 -4 0.30 9.70 22 7 4 -3.00 9.30 22 -7 4 4.30 10.00 22 7 -4 6.90 6.70 22 7 -4 6.20 7.00 22 -8 -4 2.60 8.40 22 8 4 2.60 9.00 22 8 4 -6.50 7.40 22 -8 4 -6.80 9.30 22 8 -4 0.90 7.50 22 8 -4 3.20 6.70 22 9 4 -6.30 6.90 22 -9 -4 4.00 9.90 22 -9 4 -6.70 9.70 22 9 -4 -2.40 6.70 23 0 4 4.20 9.00 23 0 -4 -8.10 8.00 23 0 -4 5.90 8.30 23 0 4 10.80 11.20 23 1 4 14.60 12.00 23 -1 -4 -3.70 7.90 23 1 4 14.10 9.20 23 -1 4 12.50 9.70 23 1 -4 -13.00 7.00 23 -1 4 23.60 12.90 23 1 -4 19.00 9.00 23 -2 -4 8.20 9.00 23 2 4 -6.80 9.00 23 2 4 -3.70 7.90 23 2 -4 13.90 8.30 23 -2 4 -3.40 9.80 23 2 -4 -0.50 9.10 23 -2 4 -4.00 8.10 23 -3 -4 75.79 15.20 23 3 4 93.89 16.80 23 3 4 88.09 17.50 23 -3 4 55.99 14.50 23 3 -4 63.19 14.70 23 3 -4 75.59 14.00 23 -3 4 109.79 20.90 23 -4 -4 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5 72.09 14.90 18 12 -5 93.79 12.00 18 12 -5 83.39 12.60 18 -13 -5 -4.30 9.70 18 13 5 2.40 7.60 18 -13 -5 -4.20 10.40 18 13 5 26.50 10.70 18 13 -5 10.00 6.60 18 13 -5 3.50 6.10 18 14 5 4.40 7.60 18 14 5 0.00 8.40 18 14 -5 8.40 7.00 18 14 -5 6.70 6.40 19 0 5 -11.10 5.80 19 0 -5 1.70 6.30 19 0 -5 -2.30 7.60 19 0 5 -5.10 8.20 19 -1 -5 26.90 8.90 19 1 5 36.20 10.80 19 1 5 32.80 11.40 19 -1 5 13.80 10.40 19 1 -5 38.00 9.40 19 1 -5 23.70 9.60 19 -1 5 44.40 11.20 19 2 5 40.80 12.90 19 -2 -5 73.69 12.90 19 2 5 51.39 11.70 19 -2 5 61.19 12.70 19 2 -5 49.00 10.50 19 -2 5 57.99 15.20 19 2 -5 50.59 11.80 19 -3 -5 31.00 9.60 19 3 5 22.30 10.60 19 3 5 18.30 9.20 19 3 -5 1.70 6.60 19 3 -5 19.40 7.50 19 -3 5 24.60 11.60 19 -3 5 8.80 8.50 19 4 5 7.10 8.30 19 -4 -5 26.00 9.30 19 4 5 0.60 6.20 19 -4 5 16.00 9.60 19 -4 5 33.00 12.60 19 4 -5 21.80 8.60 19 4 -5 11.90 6.70 19 5 5 13.00 9.30 19 -5 -5 2.30 6.90 19 5 5 5.60 7.00 19 5 -5 0.40 6.60 19 5 -5 -2.80 4.60 19 -5 5 -0.70 6.90 19 -5 5 -17.00 7.50 19 6 5 140.79 20.00 19 6 5 118.99 17.00 19 -6 -5 140.49 18.40 19 -6 5 126.29 18.30 19 6 -5 89.89 12.70 19 6 -5 132.39 15.70 19 -7 -5 -2.00 7.40 19 7 5 5.10 7.90 19 7 5 -3.00 6.40 19 -7 5 -2.90 7.00 19 7 -5 1.30 6.00 19 7 -5 0.60 5.00 -19 -8 5 231.08 16.20 19 8 5 250.57 24.40 19 8 5 197.78 23.30 19 -8 -5 207.78 24.10 19 8 -5 190.38 19.50 -19 -8 -5 215.18 29.00 19 -8 5 188.38 23.50 19 8 -5 185.68 18.00 19 9 5 3.30 7.10 19 -9 -5 -0.90 8.60 -19 -9 5 1.30 4.20 19 9 5 1.10 7.50 19 -9 5 -1.80 8.50 19 9 -5 -4.30 5.80 19 9 -5 4.00 5.40 19 10 5 165.28 20.70 19 -10 -5 167.28 22.90 19 10 5 125.99 19.50 19 10 -5 185.78 17.30 19 10 -5 162.38 17.70 19 -11 -5 -8.90 8.30 19 11 5 -3.30 7.80 19 11 5 1.40 7.70 19 11 -5 10.40 6.10 19 11 -5 9.00 6.30 19 12 5 98.39 16.30 19 -12 -5 92.29 18.10 19 12 5 76.79 15.50 19 12 -5 83.29 12.40 19 12 -5 105.69 14.40 19 -13 -5 4.60 10.20 19 13 5 12.80 9.80 19 13 -5 13.90 7.60 19 13 -5 -3.10 5.70 20 0 5 -1.30 9.70 20 0 -5 -0.30 7.80 20 0 5 -4.80 6.30 20 0 -5 4.90 7.40 20 1 5 87.79 17.00 20 1 5 71.89 14.30 20 -1 -5 77.19 13.70 20 -1 5 75.19 16.90 20 1 -5 97.89 14.40 20 1 -5 74.79 14.70 20 -1 5 76.69 14.30 20 2 5 45.50 13.30 20 2 5 34.50 11.00 20 -2 -5 37.80 11.10 20 -2 5 64.89 15.60 20 2 -5 41.10 11.10 20 -2 5 55.69 12.80 20 2 -5 33.80 9.50 20 -3 -5 126.89 17.40 20 3 5 120.19 17.70 20 3 5 115.49 18.90 20 -3 5 95.39 18.50 20 -3 5 104.79 17.10 20 3 -5 110.69 14.90 20 3 -5 112.89 16.40 20 -4 -5 61.29 13.00 20 4 5 32.30 10.40 20 4 5 47.90 13.60 20 -4 5 60.49 15.60 20 -4 5 36.10 11.60 20 4 -5 28.00 10.30 20 4 -5 47.60 9.80 20 -5 -5 15.50 8.40 20 5 5 10.90 9.70 20 5 5 14.30 8.50 20 5 -5 10.50 7.40 20 5 -5 4.00 5.70 20 -5 5 7.20 8.90 20 -5 5 3.10 10.80 20 6 5 47.60 12.70 20 -6 -5 37.60 11.70 20 6 5 48.40 10.80 20 -6 5 41.00 12.10 20 6 -5 36.80 9.10 20 6 -5 37.50 9.60 20 7 5 2.40 8.00 20 7 5 -5.10 6.30 20 -7 -5 2.90 7.60 20 7 -5 -2.30 5.20 20 7 -5 -7.90 5.80 20 -7 5 7.10 8.90 20 8 5 64.29 13.40 20 8 5 89.89 15.80 20 -8 -5 80.79 16.10 20 8 -5 71.49 11.40 20 8 -5 85.99 13.30 20 -8 5 59.09 14.70 20 -9 -5 1.30 9.20 20 9 5 -2.00 7.00 20 9 5 10.40 8.90 20 9 -5 10.60 6.50 20 -9 5 10.60 10.30 20 9 -5 9.50 7.10 20 10 5 51.79 13.00 20 -10 -5 55.29 14.20 20 10 5 62.19 13.40 20 10 -5 38.80 9.60 20 10 -5 32.90 8.40 20 11 5 -1.20 7.80 20 11 5 10.20 9.60 20 -11 -5 -6.80 8.20 20 11 -5 -2.80 5.70 20 11 -5 5.20 6.80 20 12 5 37.20 12.70 20 -12 -5 49.70 14.60 20 12 -5 39.40 10.00 20 12 -5 40.30 9.70 21 0 5 -0.50 9.50 21 0 5 5.00 7.40 21 0 -5 5.60 7.00 21 1 5 64.29 13.90 21 -1 -5 84.79 14.60 21 1 5 72.99 16.60 21 -1 5 93.79 16.70 21 1 -5 82.19 15.40 21 -1 5 89.79 18.20 21 1 -5 78.89 13.30 21 2 5 37.80 13.90 21 2 5 34.20 10.90 21 -2 -5 42.10 11.10 21 -2 5 46.60 14.40 21 -2 5 46.10 12.50 21 2 -5 32.20 11.20 21 2 -5 41.80 10.40 21 3 5 38.90 12.70 21 -3 -5 29.40 10.40 21 3 5 37.70 10.90 21 3 -5 28.30 10.70 21 3 -5 34.60 9.70 21 -3 5 48.60 15.90 21 -3 5 37.40 12.10 21 4 5 44.10 11.30 21 4 5 63.89 15.50 21 -4 -5 42.00 12.20 21 -4 5 59.29 13.90 21 4 -5 38.40 11.40 21 -4 5 54.59 16.50 21 4 -5 45.40 10.10 21 5 5 8.80 7.70 21 -5 -5 2.90 8.50 21 5 5 7.10 9.50 21 5 -5 -1.10 6.90 21 -5 5 1.30 8.30 21 5 -5 7.60 6.60 21 -5 5 -6.90 10.20 21 6 5 25.40 10.50 21 -6 -5 40.00 11.90 21 6 5 40.50 12.70 21 -6 5 17.40 10.40 21 6 -5 23.40 9.50 21 6 -5 48.90 10.00 21 7 5 4.00 8.90 21 7 5 -5.80 6.90 21 -7 -5 -11.00 7.60 21 7 -5 0.80 5.30 21 7 -5 9.40 7.20 21 -7 5 -3.60 8.10 21 -8 -5 32.10 12.80 21 8 5 64.29 13.80 21 8 5 44.20 11.80 21 8 -5 55.49 10.80 21 8 -5 40.20 10.30 21 -8 5 57.29 14.40 21 9 5 10.00 8.20 21 9 5 -4.30 8.20 21 -9 -5 -3.50 8.30 21 9 -5 -2.90 6.50 21 -9 5 7.60 10.00 21 9 -5 -5.30 5.90 21 10 5 28.40 10.80 21 10 5 19.00 10.20 21 -10 -5 17.30 11.40 21 10 -5 17.00 7.80 21 10 -5 28.40 9.00 22 0 -5 1.20 7.30 22 0 5 -9.10 9.50 22 0 5 -10.60 6.30 22 1 5 194.08 26.00 22 -1 -5 210.38 23.60 22 1 5 231.58 25.50 22 1 -5 174.18 22.90 22 1 -5 227.08 23.20 22 -1 5 216.28 24.90 22 -1 5 182.88 25.80 22 2 5 2.40 10.10 22 -2 -5 1.90 7.10 22 2 5 -2.00 7.60 22 2 -5 -1.60 7.10 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6.30 0 10 10 4.00 6.50 0 10 -10 -0.40 4.50 0 -10 -10 -4.10 5.90 0 -10 -10 -4.10 4.90 0 10 -10 1.20 3.80 0 10 10 -4.30 5.40 0 10 10 7.50 7.90 0 10 -10 -2.80 3.70 0 10 10 2.40 5.10 0 -10 -10 5.50 6.10 0 -10 -10 9.40 7.10 0 11 -10 1.80 4.40 0 11 10 -1.20 7.00 0 11 -10 -0.70 3.00 0 11 -10 2.10 4.50 0 -11 10 2.80 4.80 0 -11 -10 2.60 6.70 0 11 10 -0.40 5.00 0 11 -10 -4.10 4.50 0 11 10 8.70 6.50 0 -11 -10 -3.40 5.70 0 -11 10 1.60 4.30 0 11 -10 -2.00 3.70 0 -11 -10 -5.00 4.60 0 -11 -10 -3.00 5.80 0 -11 -10 1.20 5.60 0 11 10 -3.50 6.20 0 -12 -10 113.89 17.20 0 -12 -10 64.19 13.60 0 -12 -10 69.59 12.50 0 12 -10 64.59 10.60 0 -12 10 79.39 12.30 0 -12 -10 78.59 15.40 0 12 -10 87.49 13.00 0 12 10 105.29 14.70 0 12 -10 85.29 10.90 0 -12 10 85.19 11.80 0 12 10 96.99 16.80 0 -12 -10 52.99 12.90 0 12 10 80.89 14.90 0 12 -10 93.49 11.60 0 12 10 77.79 13.80 0 12 -10 79.79 9.00 0 -13 -10 7.50 7.70 0 -13 -10 -1.20 6.50 0 -13 10 -6.70 5.60 0 13 10 -2.10 5.70 0 13 -10 -4.20 4.50 0 13 -10 4.50 5.40 0 -13 -10 -5.80 6.80 0 13 10 12.20 8.30 0 -13 -10 8.60 7.50 0 -13 10 12.00 6.60 0 -13 10 3.30 5.30 0 13 -10 1.70 4.70 0 -13 -10 5.40 6.60 0 13 -10 -3.70 3.90 0 -14 -10 33.00 12.00 0 14 -10 32.00 8.30 0 14 10 46.20 12.10 0 14 10 39.30 10.60 0 -14 -10 44.60 12.70 0 -14 10 37.30 8.80 0 14 -10 29.90 8.20 0 -14 10 53.89 12.80 0 -14 -10 38.00 11.70 0 -14 10 48.40 11.20 0 -14 -10 40.90 12.10 0 -15 10 3.10 7.50 0 15 -10 -1.50 5.90 0 -15 -10 -7.70 7.60 0 -15 -10 -0.90 7.70 0 -15 10 4.60 5.80 0 15 10 6.40 8.70 0 15 -10 3.20 5.50 0 -15 -10 -2.70 8.50 0 -15 -10 -5.90 7.50 0 15 10 -1.20 7.10 0 -15 10 1.90 6.60 0 -16 10 13.70 8.50 0 16 -10 -1.10 6.50 0 -16 -10 8.70 9.50 0 16 10 10.10 8.60 0 16 10 5.30 8.60 0 -16 -10 -2.30 8.00 0 16 -10 2.10 6.20 0 -16 10 4.40 8.80 0 -16 -10 0.20 9.60 0 -16 10 19.70 8.00 0 -16 -10 -6.00 8.00 0 17 -10 -0.50 5.70 0 -17 -10 0.20 8.50 0 17 10 -1.20 7.50 0 -17 -10 -6.80 7.20 0 -17 10 -4.20 7.60 0 -17 -10 -1.10 10.80 0 -17 10 -8.90 7.70 0 17 -10 -6.10 6.10 0 -17 10 -9.90 6.00 0 17 10 2.10 9.20 0 -18 10 -4.20 8.80 0 18 10 6.70 11.20 0 -18 -10 7.60 10.40 0 18 -10 17.20 9.30 0 18 10 1.30 8.50 0 18 -10 12.50 7.70 0 -19 -10 -4.40 10.00 0 19 10 -3.20 8.40 0 19 10 2.20 10.20 0 -19 10 -3.20 8.60 0 19 -10 -1.00 6.50 0 19 -10 -2.80 7.60 0 20 10 -5.20 11.00 0 -20 10 8.60 11.60 0 20 -10 19.80 9.50 0 20 10 6.30 10.50 0 20 -10 11.70 8.70 0 -21 10 4.80 11.50 0 21 10 -3.80 9.70 0 21 -10 6.40 8.10 0 21 10 -1.30 10.90 1 0 -10 2029.20 107.09 -1 0 10 1961.90 99.19 1 0 10 1916.41 106.09 1 0 10 2088.39 106.79 -1 0 10 1908.21 98.79 1 0 -10 1924.01 100.09 1 0 -10 2012.80 101.09 -1 0 10 2095.19 100.89 -1 0 -10 2088.79 106.69 -1 0 -10 2074.89 107.29 -1 0 -10 2068.59 106.69 1 0 10 2013.70 100.49 -1 0 -10 1969.00 100.99 1 0 -10 1982.70 99.79 -1 0 -10 2100.49 100.39 -1 0 -10 2001.60 100.49 -1 0 10 1927.01 106.89 -1 0 -10 2072.39 101.89 1 1 10 3.70 3.70 -1 -1 10 8.30 4.70 -1 -1 10 -1.40 2.90 -1 -1 10 16.00 4.80 -1 -1 10 0.00 2.10 -1 1 -10 1.60 3.90 1 1 10 2.70 3.10 1 1 10 1.60 3.30 -1 1 -10 4.40 4.10 1 -1 -10 3.20 3.10 -1 1 -10 2.10 3.00 -1 1 -10 1.30 1.40 -1 1 -10 2.40 4.70 1 -1 -10 -1.30 3.20 1 1 10 8.60 5.30 1 -1 -10 -0.20 3.70 1 -1 -10 -0.20 3.40 -1 -1 10 -1.00 2.30 1 -1 -10 0.20 4.00 1 1 10 4.00 4.30 -1 1 -10 3.30 3.80 -1 1 -10 -4.30 2.70 -1 -1 -10 1.40 3.60 1 1 -10 10.70 3.60 -1 1 10 1.70 3.30 -1 1 10 2.50 4.20 -1 -1 -10 -1.20 2.60 1 -1 10 -0.40 3.80 -1 -1 -10 1.50 4.40 1 1 -10 2.70 2.70 -1 -1 -10 -6.50 2.90 -1 -1 -10 -0.40 3.60 1 -1 10 7.00 3.60 1 1 -10 11.80 4.60 1 1 -10 2.00 3.00 1 -1 10 2.90 4.00 -1 -1 -10 5.10 3.50 -1 1 10 1.00 4.40 1 1 -10 0.60 4.40 1 2 10 2657.03 144.79 -1 -2 10 2668.93 144.79 1 -2 -10 2899.31 145.49 1 -2 -10 2810.82 146.99 1 -2 -10 2628.24 138.89 -1 2 -10 2651.93 144.79 1 2 10 2590.74 137.39 1 -2 -10 2870.31 146.39 1 2 10 2788.32 146.69 1 -2 -10 2859.91 137.79 -1 2 -10 2701.53 137.49 -1 -2 10 2921.11 134.39 1 -2 -10 2696.03 137.99 1 2 10 2747.12 139.19 -1 2 -10 2682.13 138.39 -1 2 -10 2752.12 143.79 -1 -2 10 2848.92 136.99 -1 2 -10 2824.22 136.99 -1 -2 10 2846.42 134.09 -1 2 -10 2794.02 145.19 1 2 10 2818.32 138.29 -1 -2 -10 2746.63 139.99 1 -2 10 2973.90 138.39 1 -2 10 2943.91 144.19 1 -2 10 2798.22 136.09 1 -2 10 2724.83 144.79 1 2 -10 2815.52 136.29 -1 -2 -10 2837.52 146.89 1 -2 10 2871.31 136.69 1 2 -10 2820.22 145.39 -1 -2 -10 2646.14 139.19 -1 2 10 2620.14 144.89 1 2 -10 2954.60 144.39 -1 -2 -10 2726.13 138.59 -1 -2 -10 2746.63 144.89 -1 2 10 2713.73 146.79 -1 2 10 2855.21 137.69 1 2 -10 2729.93 144.59 1 2 -10 2763.92 138.49 -1 -2 -10 2812.32 138.09 1 2 -10 2991.90 137.99 1 2 -10 2820.92 135.79 -1 3 -10 20.80 5.00 -1 3 -10 22.40 5.60 -1 3 -10 24.40 5.40 1 -3 -10 10.30 4.90 1 3 10 27.10 5.60 1 3 10 23.10 5.30 1 3 10 29.20 6.40 -1 3 -10 11.80 4.30 1 -3 -10 26.00 6.10 1 -3 -10 21.60 5.20 -1 3 -10 20.00 4.50 -1 -3 10 29.50 4.90 1 -3 -10 20.60 6.40 1 3 10 26.50 6.90 -1 3 -10 21.80 6.60 1 3 10 20.40 5.90 1 -3 -10 23.70 5.60 -1 -3 10 24.50 6.60 1 -3 -10 23.50 7.40 1 3 10 29.20 7.80 -1 -3 -10 17.10 5.60 -1 -3 -10 16.40 5.90 1 3 -10 25.10 4.10 1 3 -10 21.20 3.60 -1 3 10 21.30 5.80 1 -3 10 29.50 5.50 1 -3 10 16.30 4.10 -1 -3 -10 22.10 5.50 1 3 -10 35.00 7.60 -1 3 10 13.80 5.20 1 -3 10 11.50 5.20 1 3 -10 20.80 5.30 -1 3 10 25.40 7.10 -1 3 10 21.20 6.40 -1 -3 -10 21.30 5.90 -1 -3 -10 22.60 5.30 1 3 -10 30.30 5.60 1 3 -10 23.10 4.60 1 -3 10 17.20 4.50 1 3 -10 21.00 4.10 -1 -3 -10 24.80 7.20 -1 3 10 18.20 4.80 1 -3 10 17.60 5.40 1 -3 10 24.80 4.20 1 4 10 762.52 42.90 1 -4 -10 730.93 46.50 -1 4 -10 762.62 41.20 1 4 10 739.33 46.50 1 -4 -10 837.12 46.20 1 -4 -10 690.03 45.50 1 -4 -10 833.92 43.80 1 4 10 769.82 43.20 1 -4 -10 720.73 43.00 -1 4 -10 757.92 43.90 -1 4 -10 712.53 41.60 -1 -4 10 766.52 40.50 1 4 10 742.33 43.20 -1 4 -10 777.72 45.90 1 -4 -10 831.22 42.90 -1 4 -10 780.12 41.60 1 4 10 725.63 45.20 -1 -4 10 744.13 45.40 -1 4 -10 746.83 40.60 1 -4 -10 756.02 43.00 1 4 10 747.03 42.30 1 -4 10 784.72 45.60 -1 4 10 763.22 43.00 1 -4 10 809.62 41.60 1 4 -10 787.82 40.40 -1 -4 -10 771.72 43.30 -1 4 10 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5 14 49.80 11.90 11 6 14 7.10 7.40 11 -6 -14 2.90 6.70 11 -6 -14 19.20 10.70 11 6 14 11.30 6.80 11 6 14 -4.50 5.30 11 -6 -14 3.90 7.00 -11 6 -14 2.00 6.40 -11 6 -14 -3.00 6.50 11 -6 14 1.10 6.00 11 -6 14 6.90 8.30 11 6 -14 -1.00 2.40 -11 -6 -14 8.50 6.70 11 6 -14 0.90 6.80 -11 -6 -14 -0.80 6.00 -11 -6 -14 -1.60 7.60 11 -6 14 -8.50 6.80 11 -6 14 2.20 5.90 -11 -6 -14 3.40 6.70 11 -7 -14 23.80 12.20 -11 7 -14 23.60 8.90 11 7 14 28.30 9.40 11 -7 -14 23.30 9.50 -11 7 -14 19.20 8.90 11 7 14 18.00 9.30 11 -7 -14 7.60 8.00 -11 -7 -14 29.70 8.70 -11 -7 -14 20.30 10.30 11 -7 14 17.20 10.80 -11 -7 -14 15.10 8.20 11 -7 14 10.40 7.30 11 7 -14 20.30 9.50 11 -8 -14 21.80 9.30 -11 8 -14 9.90 7.70 11 -8 -14 0.30 9.70 -11 8 -14 26.90 9.80 11 8 14 23.90 10.30 11 8 14 6.90 7.20 11 -8 -14 11.10 8.20 11 8 -14 8.80 7.70 -11 -8 -14 -1.90 6.50 -11 -8 -14 0.20 8.20 11 -8 14 20.70 10.90 -11 -8 -14 28.80 9.90 11 9 14 28.40 10.70 11 9 14 26.70 9.40 -11 9 -14 39.20 11.20 11 -9 -14 31.20 11.00 11 -9 -14 20.90 9.50 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20.30 11.30 11 12 -14 10.40 9.80 -11 -13 14 74.39 16.60 11 13 14 70.59 14.70 -11 13 -14 71.69 14.50 -11 13 -14 62.59 15.80 11 13 14 67.79 16.00 11 -13 -14 99.79 18.30 -11 13 -14 82.99 16.80 11 -13 -14 69.49 16.50 -11 -13 -14 86.09 16.40 11 -13 14 67.89 17.20 -11 -13 -14 74.69 16.90 -11 -13 -14 109.09 19.60 11 13 -14 72.99 7.90 11 13 -14 40.50 14.40 11 -14 -14 85.79 18.60 -11 14 -14 111.49 18.60 11 14 14 105.89 17.50 -11 14 -14 58.49 15.80 -11 -14 14 91.29 18.00 11 14 14 103.59 18.90 -11 14 -14 77.69 18.80 11 -14 -14 73.59 17.30 -11 -14 -14 90.49 19.20 11 -14 14 85.19 18.70 11 14 -14 91.69 17.90 11 14 -14 77.19 9.10 -11 -14 -14 123.49 19.70 -11 -14 -14 114.49 20.30 11 15 14 32.40 12.50 -11 -15 14 28.30 13.10 11 15 14 17.60 12.00 -11 15 -14 44.50 14.00 -11 15 -14 38.50 12.80 11 15 -14 33.00 6.70 11 -15 14 15.90 12.90 -11 -15 -14 34.70 13.90 11 15 -14 45.80 14.80 -11 16 -14 24.30 11.80 11 16 14 58.89 17.10 -11 16 -14 34.30 13.70 -11 -16 14 53.79 16.10 11 16 14 48.60 14.90 -11 -16 -14 56.49 16.40 11 16 -14 35.50 7.70 11 16 -14 54.29 6.90 -11 17 -14 6.00 10.20 11 17 14 -6.30 9.80 -11 17 -14 -6.10 8.30 -11 -17 14 2.90 11.10 11 17 14 -4.70 7.90 11 17 -14 -8.90 4.80 11 17 -14 4.60 4.90 12 0 14 229.68 21.40 12 0 14 209.88 23.10 -12 0 -14 203.38 24.30 12 0 -14 205.58 15.60 12 0 -14 186.38 15.00 12 0 14 163.78 19.20 12 0 -14 178.18 17.40 12 0 14 212.38 25.40 12 0 14 175.98 21.60 -12 0 14 185.68 17.70 12 0 -14 217.28 17.60 12 0 -14 157.78 19.90 12 0 14 203.18 19.40 -12 0 -14 198.88 19.30 -12 0 -14 205.68 21.50 -12 0 -14 209.88 22.50 12 -1 -14 42.70 7.90 12 1 14 24.90 10.10 12 1 14 32.90 9.10 12 -1 -14 40.60 10.30 12 1 14 29.40 9.20 12 -1 -14 25.80 6.70 12 1 14 36.70 11.50 12 -1 -14 26.90 7.40 12 -1 -14 32.00 8.50 12 1 14 36.10 8.50 -12 1 -14 39.20 10.00 -12 1 -14 28.30 8.20 -12 1 -14 30.10 10.00 -12 1 -14 15.20 9.70 12 1 14 23.80 10.10 12 -1 14 55.49 11.20 12 1 -14 40.30 6.70 12 -1 14 31.20 10.60 -12 1 14 25.20 7.40 12 1 -14 31.70 9.10 -12 -1 -14 31.60 10.40 12 1 -14 38.40 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23.50 -12 -7 -14 489.85 35.10 12 7 -14 425.16 33.50 12 -8 -14 0.40 7.80 -12 8 -14 1.60 7.30 12 -8 -14 27.50 10.00 12 8 14 5.60 8.40 -12 8 -14 2.60 7.60 12 8 14 10.20 7.70 12 -8 14 -4.30 7.90 12 8 -14 21.50 9.40 -12 -8 -14 19.70 9.80 -12 -8 -14 5.80 7.70 12 9 14 229.38 24.00 -12 9 -14 188.68 22.60 12 -9 -14 184.78 23.30 -12 9 -14 261.67 26.50 12 9 14 202.98 24.50 12 -9 -14 246.48 26.50 -12 -9 -14 230.88 26.80 12 -9 14 248.98 29.00 -12 -9 -14 289.87 26.00 12 9 -14 226.98 25.10 -12 10 -14 -2.00 8.10 12 -10 -14 0.90 8.20 12 10 14 -3.10 6.30 12 10 14 3.60 7.90 12 -10 -14 -0.60 7.70 -12 10 -14 5.20 8.80 -12 -10 -14 -2.30 7.10 -12 -10 -14 6.20 8.40 -12 -10 -14 -13.80 8.00 12 -10 14 -13.60 7.00 12 10 -14 5.40 7.90 12 -11 -14 189.88 24.50 12 11 14 191.78 24.40 -12 -11 14 170.58 24.20 12 -11 -14 173.48 23.80 -12 11 -14 137.49 20.20 -12 11 -14 183.78 23.60 12 11 14 193.78 23.10 -12 11 -14 218.08 25.90 -12 -11 -14 191.88 22.70 -12 -11 -14 235.88 28.00 12 11 -14 204.28 25.10 -12 -11 -14 246.98 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14 9.20 7.50 13 9 14 10.80 9.40 -13 9 -14 9.60 8.80 13 -9 -14 20.90 9.80 13 -9 -14 8.90 9.10 -13 9 -14 10.70 8.40 13 9 -14 19.10 9.60 13 -9 14 8.80 10.10 -13 -9 -14 5.90 8.00 -13 -9 -14 15.10 10.60 13 10 14 78.19 15.00 13 -10 -14 125.59 19.30 -13 10 -14 101.99 17.00 13 -10 -14 86.99 17.00 -13 10 -14 127.79 19.20 13 10 14 107.09 18.10 -13 10 -14 133.99 20.60 -13 -10 -14 111.89 19.60 -13 -10 -14 124.09 20.20 13 -10 14 122.09 21.00 -13 -10 -14 99.19 15.80 13 10 -14 77.89 15.70 13 11 14 -5.80 9.00 -13 11 -14 4.80 10.30 -13 11 -14 2.80 9.40 13 11 14 7.40 8.00 13 -11 -14 4.30 10.00 -13 11 -14 9.10 9.40 -13 -11 14 4.20 9.30 13 -11 -14 -11.90 8.10 -13 -11 -14 17.40 10.70 -13 -11 -14 9.40 8.70 13 11 -14 0.70 8.90 -13 -11 -14 11.60 10.90 13 -11 14 3.10 10.00 -13 12 -14 83.79 17.00 13 -12 -14 84.69 17.50 13 -12 -14 103.19 19.00 -13 12 -14 96.29 18.50 -13 12 -14 86.39 17.20 -13 -12 14 112.39 20.40 13 12 14 81.69 17.20 13 12 14 64.99 14.90 13 12 -14 74.09 16.30 -13 -12 -14 93.79 16.50 -13 -12 -14 106.69 20.10 13 -12 14 95.19 19.60 -13 -12 -14 84.49 18.40 13 13 14 7.30 10.20 -13 -13 14 1.30 10.20 -13 13 -14 10.50 9.90 13 -13 -14 22.80 11.70 13 -13 -14 12.40 9.50 -13 13 -14 14.30 11.70 13 13 14 16.60 10.20 -13 13 -14 17.50 11.40 -13 -13 -14 4.40 10.30 13 13 -14 -9.80 8.00 -13 -13 -14 12.90 11.00 13 -13 14 8.70 11.70 13 14 14 195.08 25.90 13 14 14 190.98 24.20 -13 -14 14 165.78 25.80 13 -14 -14 146.99 23.80 13 -14 -14 228.28 28.30 -13 14 -14 250.47 29.50 -13 14 -14 168.48 23.10 -13 14 -14 173.58 25.00 13 14 -14 139.09 22.90 13 -14 14 177.58 27.30 13 14 -14 143.49 12.60 13 15 14 -3.80 9.00 13 15 14 -14.90 8.80 -13 -15 14 -4.40 11.50 -13 15 -14 -5.20 8.80 -13 15 -14 -11.60 9.80 -13 15 -14 25.70 12.90 13 15 -14 0.20 4.50 13 15 -14 -0.40 10.40 -13 16 -14 137.49 21.50 13 16 14 135.69 23.40 13 16 14 94.69 18.40 -13 16 -14 110.89 21.30 13 16 -14 125.89 9.70 13 16 -14 113.79 11.90 -14 0 -14 42.60 11.00 14 0 -14 44.00 10.50 14 0 14 34.10 11.40 14 0 14 31.60 11.00 -14 0 -14 27.80 7.70 14 0 14 34.80 8.60 14 0 14 18.00 10.50 -14 0 14 27.50 7.60 -14 0 -14 34.60 11.90 14 0 -14 18.50 6.10 14 0 14 37.40 10.20 14 -1 -14 42.20 10.70 14 1 14 34.70 11.00 -14 -1 14 28.60 7.00 14 1 14 36.50 10.60 -14 1 -14 45.50 9.10 14 1 14 47.10 9.30 14 -1 -14 32.10 7.60 -14 1 -14 32.40 11.20 -14 1 -14 20.70 9.10 14 1 14 42.30 12.50 14 1 -14 36.80 8.00 14 -1 14 14.30 10.10 -14 1 14 40.30 9.30 14 -1 14 24.30 9.90 14 -1 14 28.00 11.90 14 -1 14 42.30 11.00 -14 -1 -14 39.20 12.10 -14 -1 -14 39.80 9.10 14 1 -14 53.19 11.20 14 1 -14 22.10 6.30 -14 2 -14 36.20 10.90 14 -2 -14 59.59 11.60 14 2 14 47.10 12.70 -14 2 -14 74.29 14.50 14 2 14 41.70 13.30 14 -2 -14 38.10 8.70 -14 2 -14 55.29 10.50 14 2 14 42.60 11.00 14 2 -14 51.09 9.30 -14 -2 -14 50.69 9.50 14 -2 14 49.60 13.90 14 -2 14 41.90 12.20 14 2 -14 52.89 7.60 -14 -2 -14 62.19 14.40 14 2 -14 47.70 7.40 14 2 -14 67.09 12.80 14 -2 14 57.59 13.80 14 -2 14 60.39 12.70 14 2 -14 54.79 9.00 -14 3 -14 44.80 12.60 -14 3 -14 12.90 8.90 14 -3 -14 20.40 7.50 14 3 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63.09 16.70 14 13 -14 79.29 17.00 14 -13 14 71.29 18.20 14 13 -14 60.79 6.70 14 -14 -14 1.70 10.70 14 -14 -14 10.80 12.30 14 14 14 12.70 10.50 -14 14 -14 10.00 10.10 -14 14 -14 -2.60 10.30 14 14 14 10.50 11.50 -14 -14 14 19.20 12.60 -14 14 -14 48.80 15.40 14 14 -14 -4.60 9.60 14 -14 14 42.90 15.90 14 14 -14 12.60 4.60 -14 15 -14 -9.30 10.30 -14 15 -14 -0.50 9.80 14 15 14 -10.20 9.40 -14 15 -14 18.90 14.00 14 15 14 3.70 10.20 14 15 -14 6.90 12.00 14 15 -14 5.20 4.60 15 0 -14 203.78 23.10 15 0 14 275.17 27.00 15 0 14 243.38 29.00 15 0 14 195.38 25.00 -15 0 14 251.47 19.80 15 0 -14 241.48 18.50 -15 0 -14 250.47 27.60 -15 1 -14 -2.50 8.30 15 -1 -14 9.10 7.80 15 1 14 21.00 10.80 15 -1 -14 29.70 7.50 15 1 14 21.20 9.00 -15 -1 14 14.60 5.70 15 -1 14 27.00 11.20 15 -1 14 4.70 9.10 15 -1 14 32.40 10.30 15 1 -14 12.40 5.60 15 1 -14 21.20 9.70 -15 -1 -14 14.60 9.70 15 -1 14 14.60 10.50 15 2 14 391.96 37.60 15 -2 -14 427.96 28.80 -15 2 -14 440.66 34.70 -15 -2 14 407.66 25.90 15 -2 -14 448.96 32.00 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81.79 17.90 -6 6 -29 1.20 9.40 6 -6 -29 17.10 11.50 6 6 -29 10.50 8.40 6 -7 -29 -3.30 9.20 -6 7 -29 8.60 11.30 6 7 -29 21.80 9.00 6 -8 -29 4.20 10.90 -6 8 -29 -1.90 10.30 -7 0 -29 5.60 10.30 7 0 -29 -4.10 7.90 7 -1 -29 7.20 9.60 -7 1 -29 18.30 11.20 7 1 -29 26.00 10.40 -7 -1 -29 25.20 13.40 7 -2 -29 14.60 10.70 -7 2 -29 34.40 13.30 7 2 -29 -6.50 7.60 -7 -2 -29 7.00 10.80 7 -3 -29 -11.90 8.00 -7 3 -29 6.90 11.00 7 3 -29 4.40 8.50 -7 -3 -29 8.80 11.30 7 -4 -29 17.60 11.70 -7 4 -29 17.10 11.40 -7 -4 -29 2.60 10.70 7 4 -29 18.70 9.90 7 -5 -29 -11.50 9.30 -7 5 -29 -8.90 9.50 7 5 -29 5.10 8.00 -7 6 -29 5.30 10.90 7 -6 -29 7.70 11.00 7 6 -29 5.80 7.40 7 -7 -29 17.50 11.80 -7 7 -29 -12.40 9.60 -8 0 -29 -11.10 9.50 8 0 -29 -12.00 7.10 -8 1 -29 289.67 32.30 8 -1 -29 179.88 23.90 8 1 -29 245.38 26.10 -8 -1 -29 276.77 31.60 -8 2 -29 -4.70 10.30 8 -2 -29 -6.40 8.20 8 2 -29 -1.80 7.40 -8 -2 -29 0.30 10.80 -8 3 -29 292.77 33.00 8 -3 -29 335.27 33.10 8 3 -29 292.47 28.10 -8 -3 -29 321.27 35.60 -8 4 -29 19.20 12.00 8 -4 -29 -1.50 10.00 8 4 -29 1.20 7.70 -8 5 -29 143.59 22.40 8 -5 -29 102.29 19.70 8 5 -29 101.09 15.80 8 -6 -29 12.50 11.60 -8 6 -29 7.50 11.00 9 0 -29 -4.80 8.20 -9 0 -29 -6.70 10.40 9 -1 -29 -3.10 8.50 -9 1 -29 5.60 11.40 -9 -1 -29 -8.10 9.70 9 1 -29 4.60 7.80 9 -2 -29 8.50 9.90 -9 2 -29 19.50 12.80 9 2 -29 19.80 10.10 -9 -2 -29 22.50 13.60 -9 3 -29 63.89 16.50 9 -3 -29 48.90 13.70 9 3 -29 23.60 10.10 9 -4 -29 -2.00 8.90 -9 4 -29 -18.20 8.90 9 -5 -29 0.30 10.10 -9 5 -29 17.20 11.80 -10 0 -29 -3.10 11.10 -10 1 -29 235.18 29.70 -10 2 -29 25.70 14.00 -10 3 -29 238.38 30.90 0 0 -30 73.99 17.20 0 1 -30 -9.20 9.50 0 -1 -30 -2.40 9.80 0 2 -30 121.79 19.80 0 -2 -30 130.99 20.80 0 -3 -30 6.00 10.40 0 3 -30 -4.80 8.60 0 4 -30 11.50 10.00 0 -4 -30 16.70 12.00 0 -5 -30 -9.40 9.40 0 5 -30 -12.20 8.00 0 6 -30 -3.10 8.60 0 -6 -30 7.50 12.40 0 -7 -30 1.00 11.00 0 -8 -30 -6.20 10.50 -1 0 -30 180.78 25.00 1 0 -30 184.88 24.30 -1 1 -30 -1.30 9.70 1 -1 -30 9.20 10.60 1 1 -30 8.50 9.90 -1 -1 -30 23.70 11.80 -1 2 -30 239.08 28.70 1 -2 -30 287.97 31.10 -1 -2 -30 342.57 33.90 1 2 -30 341.77 33.00 -1 3 -30 6.00 9.60 1 -3 -30 10.00 9.90 1 3 -30 -0.10 9.00 -1 -3 -30 -10.00 9.40 1 -4 -30 42.80 15.30 -1 4 -30 71.59 15.40 1 4 -30 33.00 13.00 -1 -4 -30 39.20 14.50 1 -5 -30 -1.10 10.40 -1 5 -30 10.10 10.30 -1 -5 -30 9.90 12.30 1 5 -30 3.60 8.80 -1 6 -30 166.68 23.30 1 -6 -30 159.18 24.30 1 6 -30 178.78 23.10 -1 -6 -30 154.98 24.70 1 -7 -30 -8.20 9.90 -1 7 -30 3.70 9.50 -1 -7 -30 2.30 11.10 1 -8 -30 -14.40 10.10 -1 -8 -30 9.90 12.30 2 0 -30 104.19 18.80 -2 0 -30 91.99 18.00 2 -1 -30 -0.70 8.70 -2 1 -30 -4.40 9.20 -2 -1 -30 1.10 9.70 2 1 -30 -1.80 9.00 2 -2 -30 98.69 18.60 -2 2 -30 106.09 19.20 2 2 -30 98.69 17.80 -2 -2 -30 111.99 20.10 2 -3 -30 26.00 11.60 -2 3 -30 11.90 11.00 -2 -3 -30 -0.10 10.20 2 3 -30 2.80 9.10 -2 4 -30 39.40 12.60 2 -4 -30 57.49 15.30 -2 -4 -30 40.30 15.00 2 4 -30 32.30 12.50 -2 5 -30 45.90 13.60 2 -5 -30 64.29 16.60 2 5 -30 25.60 11.30 -2 -5 -30 38.30 15.40 -2 6 -30 10.90 10.20 2 -6 -30 12.10 12.00 2 6 -30 20.20 10.60 -2 -6 -30 2.60 11.30 2 -7 -30 49.50 16.30 -2 7 -30 22.90 12.60 -2 -7 -30 15.60 13.50 -3 0 -30 250.57 29.90 3 0 -30 241.88 27.70 -3 1 -30 61.39 15.40 3 -1 -30 32.70 12.00 3 1 -30 38.40 12.70 -3 -1 -30 58.09 16.30 -3 2 -30 99.39 18.30 3 -2 -30 111.19 19.40 -3 -2 -30 156.48 22.90 3 2 -30 125.39 20.00 -3 3 -30 -1.20 9.30 3 -3 -30 19.50 12.00 3 3 -30 -2.30 8.50 -3 -3 -30 -5.70 10.00 -3 4 -30 37.30 13.40 3 -4 -30 53.39 15.10 3 4 -30 50.39 13.40 -3 -4 -30 57.99 16.50 -3 5 -30 6.90 10.40 3 -5 -30 24.40 12.90 -3 -5 -30 25.60 13.60 3 5 -30 -0.60 8.50 -3 6 -30 31.80 11.80 3 -6 -30 40.00 14.40 -3 -6 -30 34.90 15.40 3 6 -30 33.90 11.30 3 -7 -30 45.90 15.20 -3 7 -30 22.60 12.00 -3 -7 -30 28.90 15.40 -4 0 -30 71.79 17.20 4 0 -30 61.69 14.80 -4 1 -30 15.00 11.90 4 -1 -30 18.60 11.20 -4 -1 -30 12.00 11.60 4 1 -30 14.60 10.00 4 -2 -30 23.00 11.90 -4 2 -30 39.40 13.20 4 2 -30 67.49 14.70 -4 -2 -30 30.40 13.70 -4 3 -30 -1.70 9.90 4 -3 -30 -6.20 8.50 -4 -3 -30 -0.40 10.40 4 3 -30 -7.40 7.80 -4 4 -30 109.29 20.30 4 -4 -30 88.29 18.20 -4 -4 -30 97.79 19.90 4 4 -30 88.79 16.10 -4 5 -30 106.89 19.30 4 -5 -30 115.49 19.90 4 5 -30 118.89 17.90 -4 -5 -30 92.49 20.00 4 -6 -30 39.40 14.50 -4 6 -30 49.20 15.10 -4 -6 -30 31.00 14.80 -4 7 -30 96.99 18.40 4 -7 -30 66.79 16.90 5 0 -30 108.79 18.20 -5 0 -30 67.59 16.40 5 -1 -30 -12.70 7.70 -5 1 -30 12.10 10.80 -5 -1 -30 6.70 11.50 5 1 -30 1.60 8.50 5 -2 -30 7.30 10.30 -5 2 -30 4.00 11.20 5 2 -30 -10.60 7.90 -5 -2 -30 -3.50 9.70 5 -3 -30 -9.40 8.60 -5 3 -30 -9.00 9.00 -5 -3 -30 2.50 10.20 5 3 -30 4.20 8.50 -5 4 -30 54.49 15.10 5 -4 -30 71.29 17.20 5 4 -30 41.10 11.80 -5 -4 -30 6.20 11.90 -5 5 -30 34.70 13.50 5 -5 -30 37.80 14.70 -5 -5 -30 34.50 14.60 5 -6 -30 -8.10 9.20 -5 6 -30 -2.50 11.00 -5 -6 -30 22.30 13.50 6 0 -30 121.89 19.10 -6 0 -30 85.79 19.30 6 -1 -30 3.40 9.70 -6 1 -30 -1.30 11.70 6 1 -30 13.00 10.10 -6 -1 -30 11.00 13.00 6 -2 -30 -0.90 9.80 -6 2 -30 18.80 12.20 6 2 -30 9.30 9.50 -6 -2 -30 11.70 11.00 6 -3 -30 62.79 15.90 -6 3 -30 55.59 16.60 -6 -3 -30 48.80 16.20 6 3 -30 63.29 13.50 6 -4 -30 36.80 14.50 -6 4 -30 39.20 14.90 -6 -4 -30 45.90 16.00 -6 5 -30 61.39 17.10 6 -5 -30 81.59 17.70 -6 -5 -30 74.69 18.50 6 -6 -30 11.40 11.40 -6 6 -30 20.90 12.00 7 0 -30 4.50 9.30 -7 0 -30 0.00 10.20 7 -1 -30 -2.30 8.10 -7 1 -30 0.80 10.70 7 1 -30 -3.70 8.90 -7 -1 -30 -10.10 9.50 7 -2 -30 7.30 10.00 -7 2 -30 27.00 14.00 -7 -2 -30 49.20 15.90 7 2 -30 7.80 8.70 -7 3 -30 15.80 11.50 7 -3 -30 38.30 13.90 -7 -3 -30 9.50 12.30 -7 4 -30 58.39 15.90 7 -4 -30 45.90 14.50 -7 -4 -30 21.10 12.60 -7 5 -30 104.09 19.80 7 -5 -30 58.79 16.00 -8 0 -30 17.50 13.90 -8 1 -30 -20.00 8.50 -8 -1 -30 12.00 12.30 -8 2 -30 7.80 11.60 -8 -2 -30 -3.90 10.80 -8 3 -30 64.99 17.10 0 0 -31 2.80 10.20 0 -1 -31 -14.80 8.10 0 1 -31 -17.00 7.70 0 -2 -31 79.69 16.80 0 2 -31 28.80 12.40 0 3 -31 9.90 10.40 0 -3 -31 -3.00 10.10 0 4 -31 32.10 12.60 0 -4 -31 52.39 15.80 0 5 -31 4.00 8.80 0 -5 -31 3.60 10.80 0 -6 -31 255.97 32.20 -1 0 -31 -13.60 8.10 1 0 -31 2.30 9.40 -1 1 -31 0.30 10.20 1 -1 -31 -2.30 10.40 -1 -1 -31 28.40 12.00 1 1 -31 -5.30 8.10 -1 2 -31 1.80 9.50 1 -2 -31 9.20 10.80 1 2 -31 18.30 11.90 -1 -2 -31 -2.30 10.70 -1 3 -31 23.00 11.60 1 -3 -31 5.60 10.20 1 3 -31 22.20 11.10 -1 -3 -31 14.80 12.40 -1 4 -31 11.50 11.00 1 -4 -31 10.90 12.00 -1 -4 -31 46.10 15.10 1 4 -31 28.60 12.20 -1 5 -31 -2.10 9.30 1 -5 -31 1.40 10.60 -1 -5 -31 -6.30 10.40 1 -6 -31 2.30 9.50 -1 -6 -31 -2.20 10.80 -2 0 -31 1.80 9.60 2 0 -31 -5.10 8.30 -2 1 -31 44.10 14.80 2 -1 -31 60.39 15.70 -2 -1 -31 56.69 16.00 2 1 -31 31.10 12.90 -2 2 -31 51.49 14.60 2 -2 -31 57.19 15.50 -2 -2 -31 33.80 14.90 2 2 -31 41.90 13.50 2 -3 -31 -7.60 9.00 -2 3 -31 -1.60 9.20 2 3 -31 -3.70 9.00 -2 -3 -31 -7.80 9.10 -2 4 -31 76.59 16.30 2 -4 -31 46.70 15.20 2 4 -31 69.19 15.30 -2 -4 -31 100.89 20.10 2 -5 -31 9.60 11.60 -2 5 -31 4.40 9.70 -2 -5 -31 -8.30 10.80 3 0 -31 -5.10 9.50 -3 0 -31 0.80 10.40 3 -1 -31 102.79 19.30 -3 1 -31 115.99 21.50 -3 -1 -31 149.69 24.40 3 1 -31 131.79 20.90 -3 2 -31 4.10 10.20 3 -2 -31 -0.10 9.50 -3 -2 -31 8.60 10.60 3 2 -31 9.10 10.10 -3 3 -31 17.80 11.40 3 -3 -31 46.50 14.60 -3 -3 -31 41.50 15.50 3 3 -31 48.00 13.50 -3 4 -31 9.10 11.10 3 -4 -31 2.40 10.20 -3 -4 -31 5.10 11.40 -3 5 -31 2.10 10.50 3 -5 -31 0.30 10.30 -3 -5 -31 60.19 16.60 -4 0 -31 -12.60 9.30 4 0 -31 -9.80 8.30 -4 1 -31 14.10 12.20 4 -1 -31 3.90 11.00 4 1 -31 10.50 10.60 -4 -1 -31 4.20 10.30 -4 2 -31 48.60 15.70 4 -2 -31 17.70 12.00 4 2 -31 12.20 10.70 -4 -2 -31 20.10 13.00 -4 3 -31 -10.30 8.70 4 -3 -31 -2.10 9.70 -4 -3 -31 3.80 11.30 4 -4 -31 52.29 16.20 -4 4 -31 54.89 15.40 -4 -4 -31 28.10 13.90 -5 0 -31 -2.10 10.60 5 0 -31 5.90 10.10 5 -1 -31 176.68 24.90 -5 1 -31 225.38 28.90 -5 -1 -31 218.88 28.40 5 -2 -31 33.20 13.10 -5 2 -31 5.60 11.20 -5 -2 -31 22.80 13.40 -5 3 -31 104.99 20.30 5 -3 -31 126.39 21.30 -5 -3 -31 105.79 20.30 5 -4 -31 -6.10 9.10 -5 4 -31 8.20 11.40 -5 -4 -31 18.80 12.70 -6 0 -31 16.30 12.00 -6 1 -31 -0.40 9.30 -6 -1 -31 0.70 10.90 -6 2 -31 6.60 11.10 -6 -2 -31 52.79 15.60 0 0 -32 333.47 35.80 0 -1 -32 13.00 10.60 0 1 -32 14.00 11.50 0 2 -32 73.09 17.30 0 -2 -32 113.59 21.00 -1 0 -32 176.68 25.40 1 0 -32 159.48 23.70 -1 1 -32 -6.90 9.60 1 -1 -32 8.00 11.80 1 1 -32 11.70 11.30 -1 -1 -32 10.20 11.60 -1 2 -32 44.60 15.00 1 -2 -32 40.90 13.70 -1 -2 -32 45.30 16.00 2 0 -32 270.27 29.80 -2 0 -32 205.78 27.30 -2 1 -32 -8.70 8.70 2 -1 -32 5.00 11.20 -2 -1 -32 5.90 11.20 -2 2 -32 92.79 19.00 2 -2 -32 97.19 19.80 -2 -2 -32 119.59 21.60 ; _shelx_hkl_checksum 10405 _database_code_depnum_ccdc_archive 'CCDC 967913' ####################################################################### # # Cambridge Crystallographic Data Centre # CCDC # ####################################################################### # # This CIF contains data from an original supplementary publication # deposited with the CCDC, and may include chemical, crystal, # experimental, refinement, atomic coordinates, # anisotropic displacement parameters and molecular geometry data, # as required by the journal to which it was submitted. # # This CIF is provided on the understanding that it is used for bona # fide research purposes only. It may contain copyright material # of the CCDC or of third parties, and may not be copied or further # disseminated in any form, whether machine-readable or not, # except for the purpose of generating routine backup copies # on your local computer system. # # For further information on the CCDC, data deposition and # data retrieval see: # www.ccdc.cam.ac.uk # # Bona fide researchers may freely download Mercury and enCIFer # from this site to visualise CIF-encoded structures and # to carry out CIF format checking respectively. # data_msb1103 _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety 'C21 H40 Ir N O P2' _chemical_formula_sum 'C21 H40 Ir N O P2' _chemical_formula_weight 576.68 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ir Ir -1.4442 7.9887 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M P2(1)/c _symmetry_space_group_name_Hall -P2ybc loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 7.9010(3) _cell_length_b 26.8610(12) _cell_length_c 11.8140(10) _cell_angle_alpha 90.00 _cell_angle_beta 106.864(5) _cell_angle_gamma 90.00 _cell_volume 2399.4(2) _cell_formula_units_Z 4 _cell_measurement_temperature 150(2) _cell_measurement_reflns_used 81 _cell_measurement_theta_min 6.00 _cell_measurement_theta_max 20.00 _exptl_crystal_description plate _exptl_crystal_colour yellow _exptl_crystal_size_max 0.24 _exptl_crystal_size_mid 0.16 _exptl_crystal_size_min 0.04 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.596 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 1152 _exptl_absorpt_coefficient_mu 5.708 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.612 _exptl_absorpt_correction_T_max 1.0 _exptl_absorpt_process_details 'SADABS, Bruker-AXS, 2002' _exptl_special_details ; ? ; _diffrn_ambient_temperature 150(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker-Nonius KappaCCD' _diffrn_measurement_method ; \f- and \w-rotations with 1.10 \% and 33 sec per frame ; _diffrn_detector_area_resol_mean 9 _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? _diffrn_reflns_number 69417 _diffrn_reflns_av_R_equivalents 0.0524 _diffrn_reflns_av_sigmaI/netI 0.0224 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_k_min -36 _diffrn_reflns_limit_k_max 36 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_theta_min 3.03 _diffrn_reflns_theta_max 28.70 _reflns_number_total 6192 _reflns_number_gt 5581 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'COLLECT (Bruker-Nonius, 2002)' _computing_cell_refinement 'EVALCCD (Duisenberg, 2003)' _computing_data_reduction 'EVALCCD (Duisenberg, 2003)' _computing_structure_solution 'SHELXTL 6.12 (Bruker AXS, 2002)' _computing_structure_refinement 'SHELXTL 6.12 (Bruker AXS, 2002)' _computing_molecular_graphics 'SHELXTL 6.12 (Bruker AXS, 2002)' _computing_publication_material 'SHELXTL 6.12 (Bruker AXS, 2002)' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0095P)^2^+2.8229P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 6192 _refine_ls_number_parameters 247 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0248 _refine_ls_R_factor_gt 0.0199 _refine_ls_wR_factor_ref 0.0413 _refine_ls_wR_factor_gt 0.0400 _refine_ls_goodness_of_fit_ref 1.115 _refine_ls_restrained_S_all 1.115 _refine_ls_shift/su_max 0.004 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Ir1 Ir 0.686014(11) 0.370249(3) 0.116578(7) 0.01352(3) Uani 1 1 d . . . P1 P 0.85122(8) 0.40527(2) 0.29297(5) 0.01539(11) Uani 1 1 d . . . P2 P 0.48671(8) 0.35818(2) -0.06749(5) 0.01629(11) Uani 1 1 d . . . N1 N 0.5398(2) 0.43424(7) 0.11065(17) 0.0164(4) Uani 1 1 d . . . O1 O 0.8853(3) 0.27532(7) 0.12652(18) 0.0328(5) Uani 1 1 d . . . C1 C 0.5829(3) 0.46675(9) 0.2037(2) 0.0201(5) Uani 1 1 d . . . H1A H 0.5116 0.4955 0.2006 0.024 Uiso 1 1 calc R . . C2 C 0.7227(3) 0.45948(9) 0.2995(2) 0.0209(5) Uani 1 1 d . . . H2A H 0.7509 0.4814 0.3654 0.025 Uiso 1 1 calc R . . C3 C 0.3997(3) 0.44397(9) 0.0132(2) 0.0192(5) Uani 1 1 d . . . H3A H 0.3328 0.4735 0.0119 0.023 Uiso 1 1 calc R . . C4 C 0.3536(3) 0.41307(9) -0.0810(2) 0.0211(5) Uani 1 1 d . . . H4A H 0.2578 0.4199 -0.1492 0.025 Uiso 1 1 calc R . . C5 C 1.0731(3) 0.42885(10) 0.2875(2) 0.0232(5) Uani 1 1 d . . . C6 C 1.1839(4) 0.38645(13) 0.2602(4) 0.0463(9) Uani 1 1 d . . . H6A H 1.2912 0.4001 0.2464 0.069 Uiso 1 1 calc R . . H6B H 1.1150 0.3687 0.1894 0.069 Uiso 1 1 calc R . . H6C H 1.2166 0.3634 0.3273 0.069 Uiso 1 1 calc R . . C7 C 1.1776(4) 0.45615(13) 0.3994(3) 0.0410(8) Uani 1 1 d . . . H7A H 1.2805 0.4724 0.3852 0.061 Uiso 1 1 calc R . . H7B H 1.2173 0.4322 0.4644 0.061 Uiso 1 1 calc R . . H7C H 1.1019 0.4813 0.4204 0.061 Uiso 1 1 calc R . . C8 C 1.0324(4) 0.46569(14) 0.1840(3) 0.0468(9) Uani 1 1 d . . . H8A H 1.1435 0.4786 0.1743 0.070 Uiso 1 1 calc R . . H8B H 0.9619 0.4934 0.2001 0.070 Uiso 1 1 calc R . . H8C H 0.9659 0.4487 0.1113 0.070 Uiso 1 1 calc R . . C9 C 0.8635(3) 0.36940(9) 0.4311(2) 0.0216(5) Uani 1 1 d . . . C10 C 0.6757(4) 0.35057(14) 0.4145(3) 0.0407(8) Uani 1 1 d . . . H10A H 0.6730 0.3300 0.4824 0.061 Uiso 1 1 calc R . . H10B H 0.6377 0.3306 0.3420 0.061 Uiso 1 1 calc R . . H10C H 0.5957 0.3790 0.4083 0.061 Uiso 1 1 calc R . . C11 C 0.9896(5) 0.32519(11) 0.4448(3) 0.0415(8) Uani 1 1 d . . . H11A H 0.9802 0.3042 0.5106 0.062 Uiso 1 1 calc R . . H11B H 1.1112 0.3374 0.4610 0.062 Uiso 1 1 calc R . . H11C H 0.9583 0.3056 0.3717 0.062 Uiso 1 1 calc R . . C12 C 0.9172(4) 0.40096(11) 0.5435(2) 0.0314(6) Uani 1 1 d . . . H12A H 0.9117 0.3806 0.6112 0.047 Uiso 1 1 calc R . . H12B H 0.8362 0.4293 0.5351 0.047 Uiso 1 1 calc R . . H12C H 1.0381 0.4132 0.5564 0.047 Uiso 1 1 calc R . . C13 C 0.5886(3) 0.36149(10) -0.1930(2) 0.0243(5) Uani 1 1 d . . . C14 C 0.7337(4) 0.40101(11) -0.1566(2) 0.0311(6) Uani 1 1 d . . . H14A H 0.7838 0.4070 -0.2222 0.047 Uiso 1 1 calc R . . H14B H 0.8270 0.3893 -0.0874 0.047 Uiso 1 1 calc R . . H14C H 0.6833 0.4320 -0.1369 0.047 Uiso 1 1 calc R . . C15 C 0.6734(4) 0.31199(12) -0.2108(3) 0.0349(7) Uani 1 1 d . . . H15A H 0.7418 0.3166 -0.2672 0.052 Uiso 1 1 calc R . . H15B H 0.5807 0.2871 -0.2416 0.052 Uiso 1 1 calc R . . H15C H 0.7520 0.3006 -0.1349 0.052 Uiso 1 1 calc R . . C16 C 0.4560(4) 0.37848(13) -0.3103(2) 0.0395(8) Uani 1 1 d . . . H16A H 0.5181 0.3830 -0.3703 0.059 Uiso 1 1 calc R . . H16B H 0.4020 0.4101 -0.2978 0.059 Uiso 1 1 calc R . . H16C H 0.3636 0.3532 -0.3371 0.059 Uiso 1 1 calc R . . C17 C 0.3292(3) 0.30478(10) -0.0818(2) 0.0245(5) Uani 1 1 d . . . C18 C 0.1938(4) 0.30124(13) -0.2042(3) 0.0441(8) Uani 1 1 d . . . H18A H 0.1043 0.2762 -0.2024 0.066 Uiso 1 1 calc R . . H18B H 0.2539 0.2916 -0.2627 0.066 Uiso 1 1 calc R . . H18C H 0.1366 0.3337 -0.2258 0.066 Uiso 1 1 calc R . . C19 C 0.4298(4) 0.25551(10) -0.0523(3) 0.0359(7) Uani 1 1 d . . . H19A H 0.3459 0.2284 -0.0543 0.054 Uiso 1 1 calc R . . H19B H 0.5142 0.2576 0.0269 0.054 Uiso 1 1 calc R . . H19C H 0.4938 0.2490 -0.1105 0.054 Uiso 1 1 calc R . . C20 C 0.2321(4) 0.31401(12) 0.0108(3) 0.0365(7) Uani 1 1 d . . . H20A H 0.1572 0.2853 0.0139 0.055 Uiso 1 1 calc R . . H20B H 0.1582 0.3438 -0.0106 0.055 Uiso 1 1 calc R . . H20C H 0.3184 0.3189 0.0884 0.055 Uiso 1 1 calc R . . C21 C 0.8101(3) 0.31234(9) 0.1227(2) 0.0199(5) Uani 1 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ir1 0.01403(4) 0.01297(4) 0.01241(4) -0.00014(3) 0.00201(3) 0.00164(3) P1 0.0169(3) 0.0151(3) 0.0133(3) -0.0005(2) 0.0029(2) 0.0000(2) P2 0.0154(3) 0.0183(3) 0.0135(3) -0.0004(2) 0.0015(2) 0.0014(2) N1 0.0176(9) 0.0146(9) 0.0167(9) 0.0021(7) 0.0045(7) 0.0046(7) O1 0.0359(11) 0.0247(10) 0.0334(11) -0.0028(8) 0.0031(8) 0.0142(8) C1 0.0259(12) 0.0138(11) 0.0228(12) -0.0004(9) 0.0103(10) 0.0036(9) C2 0.0265(12) 0.0166(11) 0.0187(11) -0.0042(9) 0.0052(10) 0.0002(9) C3 0.0189(11) 0.0182(11) 0.0206(11) 0.0048(9) 0.0057(9) 0.0056(9) C4 0.0168(11) 0.0233(12) 0.0205(11) 0.0033(9) 0.0008(9) 0.0050(9) C5 0.0201(12) 0.0273(13) 0.0211(12) -0.0028(10) 0.0042(9) -0.0059(10) C6 0.0247(14) 0.0436(18) 0.077(3) -0.0165(18) 0.0247(16) -0.0052(13) C7 0.0370(16) 0.0491(19) 0.0349(16) -0.0164(14) 0.0075(13) -0.0236(14) C8 0.0354(17) 0.062(2) 0.0422(19) 0.0193(16) 0.0103(14) -0.0157(16) C9 0.0297(12) 0.0198(11) 0.0143(11) 0.0017(9) 0.0047(9) 0.0011(10) C10 0.0433(17) 0.055(2) 0.0248(14) 0.0068(13) 0.0106(13) -0.0228(15) C11 0.071(2) 0.0304(16) 0.0249(14) 0.0082(12) 0.0161(14) 0.0211(15) C12 0.0452(16) 0.0332(15) 0.0145(12) 0.0001(10) 0.0064(11) -0.0019(12) C13 0.0246(12) 0.0340(15) 0.0149(11) 0.0010(9) 0.0066(9) 0.0038(10) C14 0.0328(14) 0.0372(16) 0.0269(14) 0.0054(11) 0.0145(11) -0.0020(12) C15 0.0398(16) 0.0406(17) 0.0281(15) -0.0045(12) 0.0156(12) 0.0084(13) C16 0.0388(16) 0.060(2) 0.0167(13) 0.0061(12) 0.0030(11) 0.0083(14) C17 0.0188(12) 0.0227(13) 0.0290(13) -0.0051(10) 0.0023(10) -0.0030(9) C18 0.0359(17) 0.0430(19) 0.0398(18) -0.0059(14) -0.0104(13) -0.0122(14) C19 0.0356(16) 0.0212(14) 0.0490(18) -0.0006(12) 0.0091(13) -0.0026(11) C20 0.0321(15) 0.0320(16) 0.0507(19) -0.0031(13) 0.0203(14) -0.0075(12) C21 0.0212(11) 0.0220(12) 0.0139(10) 0.0000(9) 0.0008(9) 0.0014(9) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ir1 C21 1.829(2) . ? Ir1 N1 2.0608(19) . ? Ir1 P2 2.3080(6) . ? Ir1 P1 2.3137(6) . ? P1 C2 1.790(2) . ? P1 C9 1.873(2) . ? P1 C5 1.882(3) . ? P2 C4 1.791(2) . ? P2 C17 1.874(3) . ? P2 C13 1.884(3) . ? N1 C1 1.367(3) . ? N1 C3 1.371(3) . ? O1 C21 1.153(3) . ? C1 C2 1.347(3) . ? C1 H1A 0.9500 . ? C2 H2A 0.9500 . ? C3 C4 1.351(3) . ? C3 H3A 0.9500 . ? C4 H4A 0.9500 . ? C5 C6 1.527(4) . ? C5 C7 1.528(4) . ? C5 C8 1.533(4) . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 C10 1.526(4) . ? C9 C11 1.528(4) . ? C9 C12 1.529(3) . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C13 C14 1.530(4) . ? C13 C15 1.530(4) . ? C13 C16 1.543(4) . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 C20 1.528(4) . ? C17 C19 1.531(4) . ? C17 C18 1.532(4) . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C21 Ir1 N1 178.20(9) . . ? C21 Ir1 P2 97.42(7) . . ? N1 Ir1 P2 82.11(6) . . ? C21 Ir1 P1 98.88(7) . . ? N1 Ir1 P1 81.70(6) . . ? P2 Ir1 P1 163.37(2) . . ? C2 P1 C9 105.52(11) . . ? C2 P1 C5 105.87(12) . . ? C9 P1 C5 112.94(12) . . ? C2 P1 Ir1 101.00(8) . . ? C9 P1 Ir1 116.65(8) . . ? C5 P1 Ir1 113.16(8) . . ? C4 P2 C17 105.34(12) . . ? C4 P2 C13 105.38(12) . . ? C17 P2 C13 112.91(12) . . ? C4 P2 Ir1 100.99(8) . . ? C17 P2 Ir1 116.51(9) . . ? C13 P2 Ir1 113.86(8) . . ? C1 N1 C3 120.4(2) . . ? C1 N1 Ir1 119.94(15) . . ? C3 N1 Ir1 119.71(16) . . ? C2 C1 N1 122.4(2) . . ? C2 C1 H1A 118.8 . . ? N1 C1 H1A 118.8 . . ? C1 C2 P1 114.76(18) . . ? C1 C2 H2A 122.6 . . ? P1 C2 H2A 122.6 . . ? C4 C3 N1 122.3(2) . . ? C4 C3 H3A 118.9 . . ? N1 C3 H3A 118.9 . . ? C3 C4 P2 114.93(18) . . ? C3 C4 H4A 122.5 . . ? P2 C4 H4A 122.5 . . ? C6 C5 C7 110.0(2) . . ? C6 C5 C8 108.3(3) . . ? C7 C5 C8 108.4(3) . . ? C6 C5 P1 110.68(19) . . ? C7 C5 P1 113.98(19) . . ? C8 C5 P1 105.26(18) . . ? C5 C6 H6A 109.5 . . ? C5 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C5 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C5 C7 H7A 109.5 . . ? C5 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C5 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C5 C8 H8A 109.5 . . ? C5 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C5 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C10 C9 C11 109.6(3) . . ? C10 C9 C12 108.1(2) . . ? C11 C9 C12 109.3(2) . . ? C10 C9 P1 104.83(18) . . ? C11 C9 P1 111.08(18) . . ? C12 C9 P1 113.77(18) . . ? C9 C10 H10A 109.5 . . ? C9 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C9 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C9 C11 H11A 109.5 . . ? C9 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C9 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C9 C12 H12A 109.5 . . ? C9 C12 H12B 109.5 . . ? H12A C12 H12B 109.5 . . ? C9 C12 H12C 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C14 C13 C15 108.6(2) . . ? C14 C13 C16 107.8(2) . . ? C15 C13 C16 110.2(2) . . ? C14 C13 P2 105.53(17) . . ? C15 C13 P2 111.76(19) . . ? C16 C13 P2 112.72(19) . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? C13 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C13 C15 H15A 109.5 . . ? C13 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? C13 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C13 C16 H16A 109.5 . . ? C13 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C13 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C20 C17 C19 108.2(2) . . ? C20 C17 C18 109.1(2) . . ? C19 C17 C18 109.6(2) . . ? C20 C17 P2 105.62(18) . . ? C19 C17 P2 110.70(18) . . ? C18 C17 P2 113.4(2) . . ? C17 C18 H18A 109.5 . . ? C17 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C17 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C17 C19 H19A 109.5 . . ? C17 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C17 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C17 C20 H20A 109.5 . . ? C17 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C17 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? O1 C21 Ir1 178.7(2) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C21 Ir1 P1 C2 -174.37(12) . . . . ? N1 Ir1 P1 C2 3.90(10) . . . . ? P2 Ir1 P1 C2 17.16(12) . . . . ? C21 Ir1 P1 C9 -60.64(12) . . . . ? N1 Ir1 P1 C9 117.64(11) . . . . ? P2 Ir1 P1 C9 130.90(11) . . . . ? C21 Ir1 P1 C5 72.91(12) . . . . ? N1 Ir1 P1 C5 -108.81(11) . . . . ? P2 Ir1 P1 C5 -95.55(12) . . . . ? C21 Ir1 P2 C4 178.76(11) . . . . ? N1 Ir1 P2 C4 0.51(10) . . . . ? P1 Ir1 P2 C4 -12.74(12) . . . . ? C21 Ir1 P2 C17 65.31(12) . . . . ? N1 Ir1 P2 C17 -112.94(11) . . . . ? P1 Ir1 P2 C17 -126.19(11) . . . . ? C21 Ir1 P2 C13 -68.83(12) . . . . ? N1 Ir1 P2 C13 112.92(11) . . . . ? P1 Ir1 P2 C13 99.68(12) . . . . ? P2 Ir1 N1 C1 179.90(18) . . . . ? P1 Ir1 N1 C1 -3.90(17) . . . . ? P2 Ir1 N1 C3 -0.13(17) . . . . ? P1 Ir1 N1 C3 176.07(18) . . . . ? C3 N1 C1 C2 -177.8(2) . . . . ? Ir1 N1 C1 C2 2.1(3) . . . . ? N1 C1 C2 P1 2.0(3) . . . . ? C9 P1 C2 C1 -126.2(2) . . . . ? C5 P1 C2 C1 113.8(2) . . . . ? Ir1 P1 C2 C1 -4.3(2) . . . . ? C1 N1 C3 C4 179.5(2) . . . . ? Ir1 N1 C3 C4 -0.5(3) . . . . ? N1 C3 C4 P2 1.0(3) . . . . ? C17 P2 C4 C3 120.7(2) . . . . ? C13 P2 C4 C3 -119.7(2) . . . . ? Ir1 P2 C4 C3 -0.9(2) . . . . ? C2 P1 C5 C6 -170.2(2) . . . . ? C9 P1 C5 C6 74.8(2) . . . . ? Ir1 P1 C5 C6 -60.5(2) . . . . ? C2 P1 C5 C7 65.3(2) . . . . ? C9 P1 C5 C7 -49.7(2) . . . . ? Ir1 P1 C5 C7 174.97(19) . . . . ? C2 P1 C5 C8 -53.4(2) . . . . ? C9 P1 C5 C8 -168.4(2) . . . . ? Ir1 P1 C5 C8 56.3(2) . . . . ? C2 P1 C9 C10 68.8(2) . . . . ? C5 P1 C9 C10 -176.0(2) . . . . ? Ir1 P1 C9 C10 -42.3(2) . . . . ? C2 P1 C9 C11 -172.8(2) . . . . ? C5 P1 C9 C11 -57.6(2) . . . . ? Ir1 P1 C9 C11 76.0(2) . . . . ? C2 P1 C9 C12 -49.0(2) . . . . ? C5 P1 C9 C12 66.2(2) . . . . ? Ir1 P1 C9 C12 -160.15(17) . . . . ? C4 P2 C13 C14 74.75(19) . . . . ? C17 P2 C13 C14 -170.79(17) . . . . ? Ir1 P2 C13 C14 -35.0(2) . . . . ? C4 P2 C13 C15 -167.37(19) . . . . ? C17 P2 C13 C15 -52.9(2) . . . . ? Ir1 P2 C13 C15 82.9(2) . . . . ? C4 P2 C13 C16 -42.7(2) . . . . ? C17 P2 C13 C16 71.8(2) . . . . ? Ir1 P2 C13 C16 -152.41(19) . . . . ? C4 P2 C17 C20 -54.1(2) . . . . ? C13 P2 C17 C20 -168.54(18) . . . . ? Ir1 P2 C17 C20 56.9(2) . . . . ? C4 P2 C17 C19 -171.0(2) . . . . ? C13 P2 C17 C19 74.6(2) . . . . ? Ir1 P2 C17 C19 -60.0(2) . . . . ? C4 P2 C17 C18 65.4(2) . . . . ? C13 P2 C17 C18 -49.1(2) . . . . ? Ir1 P2 C17 C18 176.33(19) . . . . ? _diffrn_measured_fraction_theta_max 0.999 _diffrn_reflns_theta_full 28.70 _diffrn_measured_fraction_theta_full 0.999 _refine_diff_density_max 0.916 _refine_diff_density_min -0.810 _refine_diff_density_rms 0.106 _database_code_depnum_ccdc_archive 'CCDC 967914' ####################################################################### # # Cambridge Crystallographic Data Centre # CCDC # ####################################################################### # # This CIF contains data from an original supplementary publication # deposited with the CCDC, and may include chemical, crystal, # experimental, refinement, atomic coordinates, # anisotropic displacement parameters and molecular geometry data, # as required by the journal to which it was submitted. # # This CIF is provided on the understanding that it is used for bona # fide research purposes only. It may contain copyright material # of the CCDC or of third parties, and may not be copied or further # disseminated in any form, whether machine-readable or not, # except for the purpose of generating routine backup copies # on your local computer system. # # For further information on the CCDC, data deposition and # data retrieval see: # www.ccdc.cam.ac.uk # # Bona fide researchers may freely download Mercury and enCIFer # from this site to visualise CIF-encoded structures and # to carry out CIF format checking respectively. # data_cw35_0m_a _audit_creation_method SHELXL-2013 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C26 H46 Ir N P2' _chemical_formula_weight 626.78 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0015 0.0009 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0030 0.0019 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.0667 0.0580 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ir Ir -0.5977 5.4269 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/n' _space_group_name_Hall '-P 2yn' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' _cell_length_a 8.896(2) _cell_length_b 29.428(7) _cell_length_c 10.601(2) _cell_angle_alpha 90 _cell_angle_beta 100.058(5) _cell_angle_gamma 90 _cell_volume 2732.5(11) _cell_formula_units_Z 4 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 6148 _cell_measurement_theta_min 2.18 _cell_measurement_theta_max 20.43 _exptl_crystal_description block _exptl_crystal_colour red _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.524 _exptl_crystal_F_000 1264 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.110 _exptl_crystal_size_mid 0.070 _exptl_crystal_size_min 0.060 _exptl_absorpt_coefficient_mu 2.729 _shelx_estimated_absorpt_T_min 0.753 _shelx_estimated_absorpt_T_max 0.853 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.4793 _exptl_absorpt_correction_T_max 0.5599 _exptl_absorpt_process_details SADABS _exptl_special_details ; ? ; _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.56086 _diffrn_radiation_type AgK\a _diffrn_source 'micro source' _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 24583 _diffrn_reflns_av_unetI/netI 0.0476 _diffrn_reflns_av_R_equivalents 0.0561 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -36 _diffrn_reflns_limit_k_max 36 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_theta_min 1.634 _diffrn_reflns_theta_max 20.554 _diffrn_reflns_theta_full 19.665 _diffrn_measured_fraction_theta_max 0.988 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.988 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.988 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 5543 _reflns_number_gt 4733 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Bruker APEX2' _computing_cell_refinement 'Bruker SAINT' _computing_data_reduction 'Bruker SAINT' _computing_structure_solution 'SHELXS-2013 (Sheldrick, 2013)' _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; ? ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens mixed _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 5543 _refine_ls_number_parameters 287 _refine_ls_number_restraints 89 _refine_ls_R_factor_all 0.0615 _refine_ls_R_factor_gt 0.0494 _refine_ls_wR_factor_ref 0.1545 _refine_ls_wR_factor_gt 0.1477 _refine_ls_goodness_of_fit_ref 1.134 _refine_ls_restrained_S_all 1.126 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.6608(9) 0.3094(3) 1.1200(7) 0.0229(17) Uani 1 1 d . U . . . H1 H 0.6326 0.2846 1.1684 0.027 Uiso 1 1 calc R U . . . C2 C 0.7622(11) 0.3407(3) 1.1792(7) 0.028(2) Uani 1 1 d . U . . . H2 H 0.8102 0.3374 1.2661 0.034 Uiso 1 1 calc R U . . . C3 C 0.7055(11) 0.4369(3) 1.1521(7) 0.0294(18) Uani 1 1 d . U . . . C4 C 0.5300(11) 0.4244(4) 1.1238(10) 0.049(3) Uani 1 1 d . U . . . H4A H 0.4953 0.4221 1.0311 0.073 Uiso 1 1 calc R U . . . H4B H 0.4717 0.4481 1.1589 0.073 Uiso 1 1 calc R U . . . H4C H 0.5143 0.3952 1.1641 0.073 Uiso 1 1 calc R U . . . C5 C 0.7287(14) 0.4820(3) 1.0862(8) 0.045(3) Uani 1 1 d . U . . . H5A H 0.7193 0.4770 0.9937 0.068 Uiso 1 1 calc R U . . . H5B H 0.8306 0.4939 1.1202 0.068 Uiso 1 1 calc R U . . . H5C H 0.6512 0.5038 1.1024 0.068 Uiso 1 1 calc R U . . . C6 C 0.7476(12) 0.4432(3) 1.2991(7) 0.037(2) Uani 1 1 d . U . . . H6A H 0.8532 0.4540 1.3212 0.055 Uiso 1 1 calc R U . . . H6B H 0.7374 0.4141 1.3417 0.055 Uiso 1 1 calc R U . . . H6C H 0.6789 0.4656 1.3272 0.055 Uiso 1 1 calc R U . . . C7 C 1.0144(10) 0.3935(3) 1.1121(8) 0.0273(18) Uani 1 1 d . U . . . C8 C 1.0669(12) 0.4380(3) 1.0580(10) 0.046(3) Uani 1 1 d . U . . . H8A H 1.0086 0.4431 0.9718 0.069 Uiso 1 1 calc R U . . . H8B H 1.1758 0.4359 1.0537 0.069 Uiso 1 1 calc R U . . . H8C H 1.0497 0.4633 1.1138 0.069 Uiso 1 1 calc R U . . . C9 C 1.0849(13) 0.3898(4) 1.2570(9) 0.048(3) Uani 1 1 d . U . . . H9A H 1.1965 0.3905 1.2673 0.072 Uiso 1 1 calc R U . . . H9B H 1.0526 0.3612 1.2914 0.072 Uiso 1 1 calc R U . . . H9C H 1.0498 0.4153 1.3035 0.072 Uiso 1 1 calc R U . . . C10 C 1.0733(12) 0.3534(4) 1.0417(11) 0.042(2) Uani 1 1 d . U . . . H10A H 1.0280 0.3547 0.9506 0.064 Uiso 1 1 calc R U . . . H10B H 1.0447 0.3248 1.0784 0.064 Uiso 1 1 calc R U . . . H10C H 1.1847 0.3552 1.0512 0.064 Uiso 1 1 calc R U . . . C11 C 0.5055(8) 0.2795(3) 0.9370(7) 0.0215(17) Uani 1 1 d . U . . . H11 H 0.4766 0.2555 0.9879 0.026 Uiso 1 1 calc R U . . . C12 C 0.4515(8) 0.2795(3) 0.8096(7) 0.0169(15) Uani 1 1 d . U . . . H12 H 0.3851 0.2565 0.7695 0.020 Uiso 1 1 calc R U . . . C13 C 0.3354(10) 0.3579(3) 0.6582(10) 0.030(2) Uani 1 1 d . U . . . C14 C 0.3074(11) 0.3857(3) 0.7744(10) 0.038(2) Uani 1 1 d . U . . . H14A H 0.3962 0.4051 0.8040 0.057 Uiso 1 1 calc R U . . . H14B H 0.2916 0.3651 0.8435 0.057 Uiso 1 1 calc R U . . . H14C H 0.2167 0.4048 0.7497 0.057 Uiso 1 1 calc R U . . . C15 C 0.1920(11) 0.3282(3) 0.6147(11) 0.047(3) Uani 1 1 d . U . . . H15A H 0.1016 0.3478 0.5967 0.071 Uiso 1 1 calc R U . . . H15B H 0.1803 0.3067 0.6828 0.071 Uiso 1 1 calc R U . . . H15C H 0.2034 0.3115 0.5370 0.071 Uiso 1 1 calc R U . . . C16 C 0.3607(13) 0.3911(4) 0.5527(10) 0.052(3) Uani 1 1 d . U . . . H16A H 0.3628 0.3743 0.4732 0.077 Uiso 1 1 calc R U . . . H16B H 0.4581 0.4069 0.5788 0.077 Uiso 1 1 calc R U . . . H16C H 0.2774 0.4133 0.5387 0.077 Uiso 1 1 calc R U . . . C17 C 0.5972(11) 0.2969(3) 0.5903(8) 0.034(2) Uani 1 1 d . U . . . C18 C 0.7143(11) 0.2620(4) 0.6614(10) 0.045(2) Uani 1 1 d . U . . . H18A H 0.7620 0.2454 0.5988 0.067 Uiso 1 1 calc R U . . . H18B H 0.6614 0.2406 0.7094 0.067 Uiso 1 1 calc R U . . . H18C H 0.7930 0.2782 0.7209 0.067 Uiso 1 1 calc R U . . . C19 C 0.6816(14) 0.3310(4) 0.5195(10) 0.058(3) Uani 1 1 d . U . . . H19A H 0.7317 0.3149 0.4574 0.086 Uiso 1 1 calc R U . . . H19B H 0.7585 0.3470 0.5812 0.086 Uiso 1 1 calc R U . . . H19C H 0.6086 0.3530 0.4745 0.086 Uiso 1 1 calc R U . . . C20 C 0.4735(12) 0.2718(4) 0.4952(9) 0.041(2) Uani 1 1 d . U . . . H20A H 0.4006 0.2939 0.4505 0.061 Uiso 1 1 calc R U . . . H20B H 0.4197 0.2503 0.5421 0.061 Uiso 1 1 calc R U . . . H20C H 0.5217 0.2553 0.4326 0.061 Uiso 1 1 calc R U . . . C21 C 0.7382(9) 0.4175(3) 0.7738(7) 0.0182(15) Uani 1 1 d . U . . . C22 C 0.6503(10) 0.4572(3) 0.7426(7) 0.0251(17) Uani 1 1 d . U . . . H22 H 0.5585 0.4607 0.7759 0.030 Uiso 1 1 calc R U . . . C23 C 0.6932(11) 0.4916(3) 0.6644(7) 0.0269(18) Uani 1 1 d . U . . . H23 H 0.6310 0.5179 0.6462 0.032 Uiso 1 1 calc R U . . . C24 C 0.8260(10) 0.4875(3) 0.6138(7) 0.029(2) Uani 1 1 d . U . . . H24 H 0.8537 0.5100 0.5580 0.035 Uiso 1 1 calc R U . . . C25 C 0.9167(10) 0.4501(3) 0.6458(8) 0.030(2) Uani 1 1 d . U . . . H25 H 1.0108 0.4475 0.6156 0.037 Uiso 1 1 calc R U . . . C26 C 0.8722(10) 0.4156(3) 0.7227(8) 0.0270(18) Uani 1 1 d . U . . . H26 H 0.9363 0.3898 0.7409 0.032 Uiso 1 1 calc R U . . . H111 H 0.814(11) 0.340(3) 0.845(9) 0.04(3) Uiso 1 1 d . . . . . N1 N 0.5994(7) 0.3126(2) 0.9947(6) 0.0160(13) Uani 1 1 d . U . . . P1 P 0.7999(3) 0.38806(7) 1.0843(2) 0.0238(5) Uani 1 1 d . U . . . P2 P 0.5133(2) 0.32573(7) 0.72111(18) 0.0166(4) Uani 1 1 d . U . . . Ir1 Ir 0.66893(3) 0.36548(2) 0.88356(3) 0.01605(14) Uani 1 1 d . U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.023(4) 0.026(4) 0.021(4) 0.016(3) 0.005(3) 0.003(3) C2 0.055(6) 0.019(4) 0.008(3) 0.008(3) -0.004(4) -0.005(4) C3 0.050(5) 0.024(4) 0.012(4) -0.001(3) 0.000(4) -0.003(4) C4 0.040(5) 0.057(7) 0.043(6) -0.036(5) -0.011(4) 0.018(4) C5 0.097(8) 0.021(4) 0.020(4) 0.001(4) 0.013(5) 0.012(5) C6 0.056(6) 0.042(6) 0.011(4) 0.000(4) 0.003(4) -0.008(5) C7 0.038(4) 0.027(5) 0.014(4) 0.011(3) -0.005(3) -0.006(3) C8 0.043(5) 0.038(5) 0.049(6) 0.027(5) -0.017(5) -0.020(5) C9 0.057(6) 0.061(7) 0.019(4) 0.012(4) -0.013(4) -0.002(6) C10 0.032(5) 0.044(5) 0.047(6) -0.002(5) -0.004(5) -0.001(4) C11 0.019(4) 0.027(4) 0.021(4) 0.014(3) 0.008(3) -0.006(3) C12 0.011(3) 0.025(4) 0.015(3) 0.003(3) 0.005(3) -0.007(3) C13 0.028(4) 0.023(4) 0.033(5) -0.001(3) -0.016(4) 0.004(3) C14 0.028(5) 0.025(5) 0.059(6) -0.002(4) -0.002(4) 0.006(4) C15 0.028(5) 0.037(6) 0.065(7) -0.001(5) -0.024(5) 0.001(4) C16 0.065(7) 0.038(6) 0.035(5) 0.012(4) -0.038(5) -0.008(5) C17 0.037(5) 0.046(6) 0.023(4) -0.013(4) 0.018(4) -0.013(4) C18 0.033(5) 0.052(6) 0.051(6) -0.023(5) 0.010(4) 0.002(4) C19 0.083(8) 0.069(7) 0.031(5) -0.017(5) 0.041(6) -0.037(6) C20 0.051(6) 0.047(6) 0.027(5) -0.019(4) 0.012(4) -0.010(5) C21 0.027(4) 0.022(4) 0.005(3) 0.004(3) 0.000(3) -0.007(3) C22 0.037(5) 0.021(4) 0.017(4) 0.004(3) 0.004(3) -0.005(3) C23 0.045(5) 0.021(4) 0.013(4) 0.001(3) 0.001(4) -0.007(4) C24 0.040(5) 0.026(5) 0.020(4) 0.009(3) 0.000(4) -0.014(4) C25 0.024(4) 0.045(5) 0.021(4) 0.018(4) 0.002(3) -0.010(4) C26 0.024(4) 0.029(5) 0.027(5) 0.014(3) 0.001(3) -0.005(3) N1 0.017(3) 0.020(3) 0.012(3) 0.009(2) 0.005(2) -0.001(2) P1 0.0384(12) 0.0183(11) 0.0107(9) 0.0051(8) -0.0068(9) -0.0049(9) P2 0.0175(10) 0.0192(10) 0.0128(9) 0.0007(8) 0.0014(8) -0.0043(8) Ir1 0.0221(2) 0.0155(2) 0.00971(19) 0.00459(11) 0.00051(13) -0.00301(12) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 N1 1.348(10) . ? C1 C2 1.362(12) . ? C2 P1 1.786(8) . ? C3 C5 1.530(12) . ? C3 C6 1.549(11) . ? C3 C4 1.581(14) . ? C3 P1 1.870(9) . ? C7 C8 1.535(11) . ? C7 C10 1.535(14) . ? C7 C9 1.559(11) . ? C7 P1 1.886(9) . ? C11 C12 1.352(10) . ? C11 N1 1.357(10) . ? C12 P2 1.792(7) . ? C13 C16 1.532(14) . ? C13 C14 1.535(14) . ? C13 C15 1.547(12) . ? C13 P2 1.864(9) . ? C17 C19 1.526(13) . ? C17 C20 1.545(13) . ? C17 C18 1.559(14) . ? C17 P2 1.887(9) . ? C21 C26 1.393(12) . ? C21 C22 1.413(11) . ? C21 Ir1 2.080(7) . ? C22 C23 1.405(11) . ? C23 C24 1.386(12) . ? C24 C25 1.371(13) . ? C25 C26 1.401(11) . ? N1 Ir1 2.109(6) . ? P1 Ir1 2.337(2) . ? P2 Ir1 2.3276(19) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 C1 C2 121.9(7) . . ? C1 C2 P1 116.3(6) . . ? C5 C3 C6 109.1(7) . . ? C5 C3 C4 108.9(8) . . ? C6 C3 C4 106.0(8) . . ? C5 C3 P1 112.6(6) . . ? C6 C3 P1 115.7(6) . . ? C4 C3 P1 104.1(6) . . ? C8 C7 C10 108.8(8) . . ? C8 C7 C9 109.4(8) . . ? C10 C7 C9 108.2(8) . . ? C8 C7 P1 112.3(6) . . ? C10 C7 P1 106.3(6) . . ? C9 C7 P1 111.7(7) . . ? C12 C11 N1 122.2(7) . . ? C11 C12 P2 115.8(6) . . ? C16 C13 C14 108.0(8) . . ? C16 C13 C15 111.1(8) . . ? C14 C13 C15 107.4(9) . . ? C16 C13 P2 111.2(7) . . ? C14 C13 P2 103.3(6) . . ? C15 C13 P2 115.1(6) . . ? C19 C17 C20 110.4(8) . . ? C19 C17 C18 109.0(9) . . ? C20 C17 C18 109.9(8) . . ? C19 C17 P2 110.9(7) . . ? C20 C17 P2 111.5(6) . . ? C18 C17 P2 104.9(6) . . ? C26 C21 C22 114.7(7) . . ? C26 C21 Ir1 123.1(6) . . ? C22 C21 Ir1 122.2(6) . . ? C23 C22 C21 122.6(8) . . ? C24 C23 C22 120.2(8) . . ? C25 C24 C23 118.7(8) . . ? C24 C25 C26 120.7(8) . . ? C21 C26 C25 123.1(8) . . ? C1 N1 C11 120.3(7) . . ? C1 N1 Ir1 119.6(5) . . ? C11 N1 Ir1 119.7(5) . . ? C2 P1 C3 104.0(4) . . ? C2 P1 C7 105.2(4) . . ? C3 P1 C7 112.7(4) . . ? C2 P1 Ir1 100.3(3) . . ? C3 P1 Ir1 112.5(3) . . ? C7 P1 Ir1 119.7(3) . . ? C12 P2 C13 104.7(4) . . ? C12 P2 C17 103.9(4) . . ? C13 P2 C17 112.7(5) . . ? C12 P2 Ir1 101.0(2) . . ? C13 P2 Ir1 111.6(3) . . ? C17 P2 Ir1 120.6(3) . . ? C21 Ir1 N1 179.8(3) . . ? C21 Ir1 P2 98.7(2) . . ? N1 Ir1 P2 81.26(18) . . ? C21 Ir1 P1 98.7(2) . . ? N1 Ir1 P1 81.33(18) . . ? P2 Ir1 P1 162.58(7) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N1 C1 C2 P1 3.9(12) . . . . ? N1 C11 C12 P2 0.6(11) . . . . ? C26 C21 C22 C23 1.1(11) . . . . ? Ir1 C21 C22 C23 -177.5(6) . . . . ? C21 C22 C23 C24 0.3(12) . . . . ? C22 C23 C24 C25 -2.6(12) . . . . ? C23 C24 C25 C26 3.3(13) . . . . ? C22 C21 C26 C25 -0.4(12) . . . . ? Ir1 C21 C26 C25 178.2(6) . . . . ? C24 C25 C26 C21 -1.9(13) . . . . ? C2 C1 N1 C11 176.2(8) . . . . ? C2 C1 N1 Ir1 3.1(11) . . . . ? C12 C11 N1 C1 -174.4(7) . . . . ? C12 C11 N1 Ir1 -1.3(10) . . . . ? C1 C2 P1 C3 109.0(8) . . . . ? C1 C2 P1 C7 -132.4(7) . . . . ? C1 C2 P1 Ir1 -7.5(8) . . . . ? C5 C3 P1 C2 178.1(7) . . . . ? C6 C3 P1 C2 51.7(8) . . . . ? C4 C3 P1 C2 -64.1(7) . . . . ? C5 C3 P1 C7 64.7(7) . . . . ? C6 C3 P1 C7 -61.7(7) . . . . ? C4 C3 P1 C7 -177.5(6) . . . . ? C5 C3 P1 Ir1 -74.3(7) . . . . ? C6 C3 P1 Ir1 159.3(6) . . . . ? C4 C3 P1 Ir1 43.5(6) . . . . ? C8 C7 P1 C2 -169.2(7) . . . . ? C10 C7 P1 C2 72.0(7) . . . . ? C9 C7 P1 C2 -45.9(8) . . . . ? C8 C7 P1 C3 -56.5(8) . . . . ? C10 C7 P1 C3 -175.3(6) . . . . ? C9 C7 P1 C3 66.8(7) . . . . ? C8 C7 P1 Ir1 79.2(7) . . . . ? C10 C7 P1 Ir1 -39.6(7) . . . . ? C9 C7 P1 Ir1 -157.5(6) . . . . ? C11 C12 P2 C13 -115.7(7) . . . . ? C11 C12 P2 C17 125.9(7) . . . . ? C11 C12 P2 Ir1 0.3(6) . . . . ? C16 C13 P2 C12 -165.4(7) . . . . ? C14 C13 P2 C12 79.0(7) . . . . ? C15 C13 P2 C12 -37.9(9) . . . . ? C16 C13 P2 C17 -53.1(8) . . . . ? C14 C13 P2 C17 -168.8(6) . . . . ? C15 C13 P2 C17 74.4(9) . . . . ? C16 C13 P2 Ir1 86.2(7) . . . . ? C14 C13 P2 Ir1 -29.5(7) . . . . ? C15 C13 P2 Ir1 -146.3(7) . . . . ? C19 C17 P2 C12 -169.8(7) . . . . ? C20 C17 P2 C12 66.6(8) . . . . ? C18 C17 P2 C12 -52.2(7) . . . . ? C19 C17 P2 C13 77.4(8) . . . . ? C20 C17 P2 C13 -46.1(8) . . . . ? C18 C17 P2 C13 -165.0(6) . . . . ? C19 C17 P2 Ir1 -57.8(8) . . . . ? C20 C17 P2 Ir1 178.7(6) . . . . ? C18 C17 P2 Ir1 59.8(7) . . . . ? _refine_diff_density_max 1.428 _refine_diff_density_min -3.398 _refine_diff_density_rms 0.173 _shelxl_version_number 2013-4 _shelx_res_file ; TITL cw35_0m in P2(1)/n CELL 0.56086 8.8957 29.4285 10.6007 90.000 100.058 90.000 ZERR 4.00 0.0020 0.0067 0.0024 0.000 0.005 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H N P IR UNIT 104 184 4 8 4 TEMP -173.000 SIZE 0.06 0.07 0.11 ACTA L.S. 50 BOND LIST 6 FMAP 2 PLAN 5 DELU CONF WGHT 0.100000 FVAR 0.26821 C1 1 0.660831 0.309393 1.119979 11.00000 0.02274 0.02568 = 0.02087 0.01626 0.00549 0.00274 AFIX 43 H1 2 0.632624 0.284618 1.168357 11.00000 -1.20000 AFIX 0 C2 1 0.762213 0.340655 1.179178 11.00000 0.05526 0.01891 = 0.00764 0.00844 -0.00407 -0.00478 AFIX 43 H2 2 0.810177 0.337417 1.266081 11.00000 -1.20000 AFIX 0 C3 1 0.705470 0.436896 1.152076 11.00000 0.05038 0.02429 = 0.01171 -0.00140 0.00029 -0.00295 C4 1 0.530018 0.424372 1.123840 11.00000 0.04017 0.05671 = 0.04307 -0.03578 -0.01098 0.01753 AFIX 137 H4A 2 0.495323 0.422117 1.031089 11.00000 -1.50000 H4B 2 0.471659 0.448057 1.158856 11.00000 -1.50000 H4C 2 0.514287 0.395178 1.164068 11.00000 -1.50000 AFIX 0 C5 1 0.728717 0.481955 1.086164 11.00000 0.09670 0.02102 = 0.01953 0.00104 0.01334 0.01249 AFIX 137 H5A 2 0.719272 0.477009 0.993692 11.00000 -1.50000 H5B 2 0.830563 0.493910 1.120152 11.00000 -1.50000 H5C 2 0.651210 0.503815 1.102419 11.00000 -1.50000 AFIX 0 C6 1 0.747598 0.443237 1.299070 11.00000 0.05599 0.04238 = 0.01090 -0.00012 0.00283 -0.00779 AFIX 137 H6A 2 0.853208 0.453967 1.321230 11.00000 -1.50000 H6B 2 0.737363 0.414141 1.341735 11.00000 -1.50000 H6C 2 0.678878 0.465616 1.327243 11.00000 -1.50000 AFIX 0 C7 1 1.014399 0.393463 1.112056 11.00000 0.03766 0.02672 = 0.01400 0.01100 -0.00515 -0.00593 C8 1 1.066862 0.437958 1.057952 11.00000 0.04266 0.03812 = 0.04864 0.02676 -0.01701 -0.02050 AFIX 137 H8A 2 1.008561 0.443069 0.971790 11.00000 -1.50000 H8B 2 1.175833 0.435944 1.053722 11.00000 -1.50000 H8C 2 1.049696 0.463275 1.113791 11.00000 -1.50000 AFIX 0 C9 1 1.084880 0.389764 1.257000 11.00000 0.05705 0.06071 = 0.01934 0.01247 -0.01290 -0.00249 AFIX 137 H9A 2 1.196497 0.390460 1.267265 11.00000 -1.50000 H9B 2 1.052639 0.361158 1.291398 11.00000 -1.50000 H9C 2 1.049819 0.415346 1.303470 11.00000 -1.50000 AFIX 0 C10 1 1.073281 0.353401 1.041718 11.00000 0.03213 0.04419 = 0.04707 -0.00164 -0.00367 -0.00055 AFIX 137 H10A 2 1.028019 0.354659 0.950612 11.00000 -1.50000 H10B 2 1.044716 0.324770 1.078420 11.00000 -1.50000 H10C 2 1.184697 0.355199 1.051220 11.00000 -1.50000 AFIX 0 C11 1 0.505459 0.279504 0.937047 11.00000 0.01854 0.02695 = 0.02081 0.01386 0.00804 -0.00558 AFIX 43 H11 2 0.476625 0.255530 0.987904 11.00000 -1.20000 AFIX 0 C12 1 0.451546 0.279513 0.809604 11.00000 0.01148 0.02521 = 0.01503 0.00293 0.00519 -0.00658 AFIX 43 H12 2 0.385091 0.256464 0.769500 11.00000 -1.20000 AFIX 0 C13 1 0.335412 0.357858 0.658223 11.00000 0.02781 0.02288 = 0.03262 -0.00149 -0.01603 0.00438 C14 1 0.307445 0.385730 0.774360 11.00000 0.02789 0.02464 = 0.05883 -0.00171 -0.00182 0.00641 AFIX 137 H14A 2 0.396224 0.405091 0.804001 11.00000 -1.50000 H14B 2 0.291584 0.365120 0.843457 11.00000 -1.50000 H14C 2 0.216675 0.404769 0.749749 11.00000 -1.50000 AFIX 0 C15 1 0.192049 0.328226 0.614698 11.00000 0.02816 0.03694 = 0.06494 -0.00132 -0.02442 0.00112 AFIX 137 H15A 2 0.101613 0.347758 0.596701 11.00000 -1.50000 H15B 2 0.180299 0.306682 0.682797 11.00000 -1.50000 H15C 2 0.203435 0.311471 0.537030 11.00000 -1.50000 AFIX 0 C16 1 0.360683 0.391113 0.552717 11.00000 0.06532 0.03755 = 0.03495 0.01236 -0.03831 -0.00782 AFIX 137 H16A 2 0.362760 0.374331 0.473189 11.00000 -1.50000 H16B 2 0.458078 0.406946 0.578755 11.00000 -1.50000 H16C 2 0.277378 0.413333 0.538715 11.00000 -1.50000 AFIX 0 C17 1 0.597228 0.296914 0.590306 11.00000 0.03748 0.04584 = 0.02350 -0.01346 0.01835 -0.01302 C18 1 0.714270 0.262049 0.661435 11.00000 0.03308 0.05157 = 0.05079 -0.02303 0.00972 0.00155 AFIX 137 H18A 2 0.761961 0.245373 0.598779 11.00000 -1.50000 H18B 2 0.661366 0.240634 0.709370 11.00000 -1.50000 H18C 2 0.793048 0.278226 0.720861 11.00000 -1.50000 AFIX 0 C19 1 0.681568 0.331004 0.519500 11.00000 0.08341 0.06928 = 0.03103 -0.01713 0.04089 -0.03712 AFIX 137 H19A 2 0.731748 0.314898 0.457369 11.00000 -1.50000 H19B 2 0.758497 0.346982 0.581161 11.00000 -1.50000 H19C 2 0.608614 0.353023 0.474507 11.00000 -1.50000 AFIX 0 C20 1 0.473492 0.271797 0.495197 11.00000 0.05077 0.04704 = 0.02684 -0.01899 0.01151 -0.01039 AFIX 137 H20A 2 0.400621 0.293906 0.450548 11.00000 -1.50000 H20B 2 0.419671 0.250289 0.542116 11.00000 -1.50000 H20C 2 0.521694 0.255263 0.432595 11.00000 -1.50000 AFIX 0 C21 1 0.738220 0.417459 0.773758 11.00000 0.02670 0.02202 = 0.00486 0.00351 -0.00022 -0.00738 C22 1 0.650257 0.457165 0.742616 11.00000 0.03722 0.02118 = 0.01671 0.00395 0.00403 -0.00470 AFIX 43 H22 2 0.558467 0.460684 0.775891 11.00000 -1.20000 AFIX 0 C23 1 0.693164 0.491636 0.664406 11.00000 0.04527 0.02137 = 0.01253 0.00121 0.00062 -0.00721 AFIX 43 H23 2 0.630977 0.517879 0.646159 11.00000 -1.20000 AFIX 0 C24 1 0.826043 0.487460 0.613768 11.00000 0.03976 0.02559 = 0.01991 0.00854 -0.00049 -0.01369 AFIX 43 H24 2 0.853704 0.510037 0.557984 11.00000 -1.20000 AFIX 0 C25 1 0.916730 0.450090 0.645820 11.00000 0.02449 0.04516 = 0.02073 0.01801 0.00152 -0.01031 AFIX 43 H25 2 1.010796 0.447535 0.615561 11.00000 -1.20000 AFIX 0 C26 1 0.872159 0.415631 0.722721 11.00000 0.02389 0.02906 = 0.02690 0.01357 0.00131 -0.00536 AFIX 43 H26 2 0.936318 0.389796 0.740917 11.00000 -1.20000 AFIX 0 H111 2 0.814195 0.339701 0.844590 11.00000 0.04117 N1 3 0.599387 0.312603 0.994727 11.00000 0.01662 0.01981 = 0.01239 0.00893 0.00489 -0.00091 P1 4 0.799887 0.388059 1.084259 11.00000 0.03841 0.01831 = 0.01074 0.00506 -0.00681 -0.00486 P2 4 0.513318 0.325726 0.721110 11.00000 0.01748 0.01917 = 0.01280 0.00069 0.00138 -0.00426 IR1 5 0.668925 0.365481 0.883563 11.00000 0.02210 0.01553 = 0.00971 0.00459 0.00051 -0.00301 HKLF 4 REM cw35_0m in P2(1)/n REM R1 = 0.0494 for 4733 Fo > 4sig(Fo) and 0.0615 for all 5543 data REM 287 parameters refined using 89 restraints END WGHT 0.0362 10.8683 REM Highest difference peak 1.428, deepest hole -3.398, 1-sigma level 0.173 Q1 1 0.5839 0.3649 0.8382 11.00000 0.05 1.43 Q2 1 0.9833 0.3725 1.4029 11.00000 0.05 1.34 Q3 1 0.6402 0.3628 0.9444 11.00000 0.05 1.32 Q4 1 0.6957 0.3714 0.8224 11.00000 0.05 1.22 Q5 1 0.3488 0.3653 0.4170 11.00000 0.05 1.05 ; _shelx_res_checksum 71476 _shelx_hkl_file ; 1 0 0 -4.90 2.80 -1 0 0 1.10 1.40 -1 0 0 1.40 4.00 1 0 0 -0.60 1.30 -2 0 0 2677.43 90.99 -2 0 0 2705.83 70.89 2 0 0 2687.23 70.89 2 0 0 2695.33 89.89 -3 0 0 -12.60 10.30 3 0 0 11.00 9.20 3 0 0 -14.00 3.50 -3 0 0 -12.10 3.90 -4 0 0 96.59 19.60 4 0 0 104.39 17.90 4 0 0 101.19 9.70 -4 0 0 93.49 10.00 5 0 0 -0.30 13.70 5 0 0 -11.90 5.80 -5 0 0 7.10 6.90 -5 0 0 -14.50 17.10 -6 0 0 3226.08 90.69 6 0 0 3158.68 120.89 -6 0 0 3231.28 132.79 6 0 0 3011.40 90.19 7 0 0 -27.80 17.80 -7 0 0 -25.60 9.30 -7 0 0 -18.40 27.80 8 0 0 531.55 51.99 -8 0 0 474.25 28.40 -9 0 0 7.20 14.10 9 0 0 1.00 26.00 10 0 0 -11.40 28.20 -10 0 0 -47.20 15.10 -1 -1 0 780.92 22.30 1 -1 0 786.32 31.40 1 -1 0 811.52 21.60 -1 -1 0 787.12 28.60 1 1 0 798.62 22.30 1 1 0 801.02 28.60 -1 1 0 809.22 21.60 -1 1 0 838.92 32.60 -2 -1 0 4095.89 130.69 2 -1 0 4014.40 132.59 -2 -1 0 4091.69 105.59 2 -1 0 4036.20 104.69 2 1 0 4171.48 105.59 -2 1 0 4033.80 134.89 -2 1 0 4023.60 104.69 2 1 0 4064.09 130.39 3 -1 0 2457.05 65.69 -3 -1 0 2390.16 86.79 3 -1 0 2347.07 86.99 -3 -1 0 2391.16 66.29 3 1 0 2464.95 66.39 3 1 0 2404.96 85.49 -3 1 0 2412.86 91.49 -3 1 0 2405.46 65.49 4 -1 0 1122.39 34.50 -4 -1 0 1130.39 52.99 4 -1 0 1029.30 50.39 -4 -1 0 1101.29 35.20 -4 1 0 1076.29 56.69 -4 1 0 1080.59 34.40 4 1 0 1074.99 35.10 4 1 0 1067.49 49.50 -5 -1 0 744.83 28.70 5 -1 0 760.12 44.50 5 -1 0 749.33 27.70 -5 -1 0 741.03 48.00 5 1 0 696.33 42.10 5 1 0 743.43 28.40 -5 1 0 850.71 54.89 -5 1 0 727.93 27.80 -6 -1 0 20.90 9.50 6 -1 0 31.10 18.80 6 -1 0 5.50 8.40 -6 -1 0 13.80 22.60 6 1 0 29.10 17.50 -6 1 0 2.50 9.10 -6 1 0 75.59 28.80 6 1 0 23.80 10.00 -7 -1 0 296.87 21.00 -7 -1 0 348.37 49.30 7 -1 0 356.76 40.40 7 1 0 338.67 39.30 -7 1 0 335.17 21.30 -7 1 0 271.37 49.60 8 -1 0 514.65 50.69 -8 -1 0 477.15 30.40 8 1 0 506.15 50.89 -8 1 0 476.05 27.90 -9 -1 0 363.46 29.90 9 -1 0 382.56 51.39 9 1 0 281.97 42.50 -9 1 0 328.67 30.10 -10 -1 0 255.27 29.80 10 -1 0 227.48 42.30 10 1 0 231.78 46.60 -1 -2 0 9347.26 233.48 -1 -2 0 8987.20 281.27 1 -2 0 9397.96 287.77 1 -2 0 9314.07 232.08 1 2 0 9302.07 233.48 1 2 0 9131.99 281.57 -1 2 0 9185.58 232.08 -1 2 0 9506.75 288.27 2 -2 0 404.16 13.60 2 -2 0 422.26 26.80 -2 -2 0 438.56 22.40 -2 -2 0 405.76 14.90 -2 2 0 463.95 30.20 2 2 0 438.66 15.10 -2 2 0 402.06 13.70 2 2 0 411.16 22.10 -3 -2 0 381.16 25.50 -3 -2 0 370.26 16.50 3 -2 0 397.06 28.20 3 -2 0 414.56 15.10 -3 2 0 408.36 33.00 3 2 0 433.46 25.90 3 2 0 415.66 16.60 -3 2 0 412.16 15.40 -4 -2 0 24.30 13.40 4 -2 0 -4.30 11.80 -4 -2 0 -6.90 4.60 4 -2 0 6.40 4.60 -4 2 0 -1.30 16.40 -4 2 0 3.70 5.40 4 2 0 2.30 5.50 4 2 0 20.10 12.00 -5 -2 0 1680.03 52.19 -5 -2 0 1601.04 74.29 5 -2 0 1617.64 72.99 5 -2 0 1698.53 50.69 5 2 0 1642.14 71.49 -5 2 0 1723.93 84.99 5 2 0 1659.53 52.19 -5 2 0 1662.63 50.69 6 -2 0 102.89 23.20 -6 -2 0 113.69 14.10 -6 -2 0 77.59 26.70 6 -2 0 74.49 11.40 -6 2 0 67.09 31.30 6 2 0 92.89 23.20 -6 2 0 90.59 12.10 7 -2 0 1295.77 70.39 -7 -2 0 1213.38 77.99 -7 -2 0 1282.67 46.80 7 2 0 1238.28 67.69 -7 2 0 1175.48 88.59 -7 2 0 1264.47 44.90 -8 -2 0 -9.00 12.50 8 -2 0 29.00 23.20 -8 2 0 -18.70 11.60 8 2 0 -37.90 20.30 9 -2 0 -4.40 27.90 -9 -2 0 -36.80 13.80 9 2 0 6.00 25.50 -9 2 0 -12.40 12.50 -10 -2 0 21.70 16.30 10 -2 0 35.80 35.10 10 2 0 24.30 34.80 -10 2 0 12.70 15.10 0 -3 0 15.70 5.40 0 3 0 14.50 4.90 1 -3 0 3480.55 114.39 1 -3 0 3281.67 84.19 -1 -3 0 3262.27 85.99 -1 -3 0 3325.77 106.89 -1 3 0 3264.47 84.19 1 3 0 3279.87 107.19 -1 3 0 3472.65 114.09 -2 -3 0 655.03 21.60 -2 -3 0 639.34 29.80 2 -3 0 683.83 19.70 2 -3 0 679.13 37.90 2 3 0 647.24 30.20 -2 3 0 667.13 40.10 2 3 0 673.03 21.70 -2 3 0 665.23 19.60 -3 -3 0 2037.40 72.79 3 -3 0 1997.80 53.59 -3 -3 0 1834.32 55.49 3 -3 0 1939.71 78.59 -3 3 0 1944.21 53.59 3 3 0 1942.01 72.29 -3 3 0 1966.20 85.09 3 3 0 1988.90 56.09 -4 -3 0 179.58 22.50 -4 -3 0 166.68 13.10 4 -3 0 206.28 26.20 4 -3 0 173.98 10.20 4 3 0 177.18 13.70 -4 3 0 146.79 10.50 -4 3 0 263.67 37.00 4 3 0 242.48 24.50 -5 -3 0 555.44 40.10 5 -3 0 541.45 39.80 -5 -3 0 512.55 23.60 5 -3 0 551.74 21.70 5 3 0 538.95 24.10 -5 3 0 490.95 21.30 5 3 0 542.45 36.90 -5 3 0 675.23 60.89 6 -3 0 32.00 8.10 6 -3 0 32.00 18.50 -6 -3 0 18.90 10.10 -6 -3 0 39.20 22.80 6 3 0 33.60 18.80 -6 3 0 45.40 10.30 -6 3 0 32.20 31.50 -7 -3 0 566.64 56.09 -7 -3 0 557.64 29.30 7 -3 0 585.54 48.30 7 3 0 562.04 46.60 -7 3 0 749.53 85.89 -7 3 0 585.74 27.90 8 -3 0 456.65 50.19 -8 -3 0 394.56 27.20 -8 3 0 424.76 26.00 8 3 0 415.26 45.20 9 -3 0 540.65 59.19 -9 -3 0 471.55 33.30 9 3 0 596.94 58.19 -9 3 0 508.25 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4 1625.84 77.89 -6 -4 -4 1587.84 58.99 -6 4 -4 1540.25 55.59 -7 -4 -4 93.59 19.80 7 -4 4 115.19 24.20 -7 4 -4 159.58 20.70 -8 -4 -4 557.54 36.80 -8 4 -4 549.54 34.50 -9 -4 -4 44.60 20.20 10 -5 -4 399.86 68.09 -10 -5 4 366.86 32.00 10 5 -4 181.18 52.29 -9 -5 4 133.09 19.70 9 -5 -4 162.88 46.70 -9 5 4 138.09 15.40 9 5 -4 66.29 39.90 8 -5 -4 500.55 64.49 8 -5 -4 477.45 21.70 -8 -5 4 531.35 28.60 8 5 -4 435.96 57.59 -8 5 4 438.56 22.20 7 -5 -4 125.69 35.90 -7 -5 4 155.28 16.60 7 -5 -4 148.99 12.00 -7 5 4 122.99 11.20 7 5 -4 142.69 35.00 -6 -5 4 81.09 11.80 6 -5 -4 91.49 8.70 6 -5 -4 81.89 28.70 -6 5 4 101.49 9.30 6 5 -4 61.49 27.40 5 -5 -4 21.30 19.50 5 -5 -4 18.50 4.40 -5 -5 4 19.50 7.20 5 5 -4 17.40 6.90 -5 5 4 15.60 4.50 5 5 -4 -10.80 18.90 -4 -5 4 2009.90 60.49 -4 -5 4 2135.69 97.29 4 -5 -4 2094.49 54.99 4 -5 -4 1982.10 93.29 4 5 -4 1979.90 93.49 4 5 -4 2069.69 60.79 -4 5 4 2067.59 54.89 -4 5 4 1986.40 54.99 3 -5 -4 123.89 24.90 -3 -5 4 128.29 11.30 -3 -5 4 112.89 24.40 3 5 -4 145.79 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-13 11 53.09 21.10 6 -13 -11 -15.50 56.79 -5 -13 11 265.77 30.80 5 -13 -11 224.98 69.09 5 13 -11 308.17 78.29 -4 -13 11 49.00 18.70 4 13 -11 34.30 58.79 3 -13 -11 1210.98 115.09 -3 -13 11 1190.78 56.19 -3 13 11 1147.39 48.00 3 13 -11 1479.25 140.99 -2 -13 11 41.10 18.40 -1 -13 11 42.50 19.80 1 -13 -11 49.10 17.00 0 -13 11 107.99 23.90 0 -13 -11 110.09 22.20 -1 -13 -11 495.95 39.40 -1 13 -11 534.15 44.20 2 -13 11 28.10 17.90 -2 -13 -11 13.40 21.00 3 -13 11 1058.59 57.49 -6 -14 11 244.48 31.30 6 14 -11 96.89 72.99 5 14 -11 272.07 81.29 -4 -14 11 39.70 20.90 4 -14 -11 45.00 57.19 4 14 -11 65.79 61.39 -3 -14 11 69.59 21.70 -3 14 11 23.70 14.70 3 14 -11 104.89 61.59 -2 -14 11 190.18 28.10 -1 -14 11 754.72 46.00 1 -14 -11 719.23 39.10 0 -14 11 407.96 38.90 0 -14 -11 461.75 36.10 0 14 -11 438.56 40.40 1 -14 11 273.37 32.20 -5 -15 11 16.40 18.80 5 15 -11 42.30 59.09 -4 -15 11 586.54 41.10 4 -15 -11 694.83 98.19 -3 -15 11 42.50 20.10 2 -15 -11 505.45 31.80 -2 -15 11 532.05 38.50 -1 -15 11 62.79 21.40 1 -15 -11 100.79 20.70 0 -15 -11 253.97 28.30 0 15 -11 282.67 33.50 1 -15 11 49.50 20.10 -1 -15 -11 64.89 21.30 -2 -15 -11 765.52 47.80 -2 15 -11 747.23 48.40 -5 -16 11 138.79 26.50 -4 -16 11 165.98 27.50 -3 -16 11 23.90 18.10 -2 -16 11 455.95 39.30 2 -16 -11 378.86 74.59 2 -16 -11 392.16 30.10 1 -16 -11 210.18 26.00 1 -16 -11 180.28 59.19 -1 -16 11 221.88 30.60 0 -16 -11 482.15 35.20 -1 -16 -11 184.78 28.40 -1 16 -11 292.27 34.30 2 -16 11 72.99 23.70 -5 -17 11 339.37 37.20 -4 -17 11 19.10 21.30 -2 -17 11 104.69 23.70 2 -17 -11 38.40 16.80 1 -17 -11 51.89 19.30 0 -17 -11 180.78 25.70 0 -17 11 212.38 31.30 -1 -17 -11 538.45 43.30 -1 17 -11 508.35 45.30 -4 -18 11 23.60 21.30 1 -18 -11 611.24 37.30 0 -18 -11 403.46 35.70 0 -18 11 469.85 43.60 1 -18 11 324.07 37.10 -1 -18 -11 325.57 35.60 -3 -19 11 105.79 26.00 1 -19 -11 50.29 18.60 0 -19 11 122.09 25.20 0 -19 -11 75.49 22.50 1 -20 -11 90.29 20.60 6 0 -12 765.12 107.69 -6 0 12 627.94 39.20 5 0 -12 -14.70 48.90 -5 0 12 30.80 16.10 -4 0 12 715.63 40.50 3 0 -12 6.60 48.40 3 0 -12 4.90 16.30 -3 0 12 5.80 16.20 2 0 -12 92.79 21.90 2 0 -12 11.20 48.50 -2 0 12 135.19 22.90 -1 0 12 38.10 18.00 1 0 -12 46.50 18.80 0 0 12 535.15 36.70 0 0 -12 489.85 36.10 -1 0 -12 -8.60 18.10 -2 0 -12 569.64 47.00 -6 -1 12 113.89 21.60 -6 1 12 79.19 19.50 5 -1 -12 94.09 58.69 -5 -1 12 59.09 18.10 -5 1 12 77.49 18.00 5 1 -12 92.59 53.69 -4 1 12 230.28 26.80 -3 -1 12 249.18 29.50 3 1 -12 186.78 61.79 3 1 -12 233.18 28.20 -3 1 12 287.57 29.10 -2 -1 12 475.65 34.80 2 -1 -12 361.26 71.99 2 -1 -12 391.96 35.50 2 1 -12 462.35 75.29 -2 1 12 434.06 35.90 -1 -1 12 397.66 35.20 -1 1 12 384.76 34.80 1 1 -12 468.55 38.90 0 -1 -12 338.47 32.00 0 -1 12 378.46 34.10 0 1 12 324.27 32.80 0 1 -12 371.26 35.70 -1 -1 -12 45.00 20.20 -1 1 -12 50.39 21.60 -2 -1 -12 256.47 32.30 -2 1 -12 222.68 30.80 -6 -2 12 58.09 19.40 6 2 -12 26.10 57.79 -5 -2 12 971.90 47.00 5 -2 -12 853.11 106.09 -5 2 12 954.20 45.80 -4 -2 12 5.50 15.80 -4 2 12 21.70 15.60 -3 -2 12 344.87 33.50 3 2 -12 340.37 70.29 -2 -2 12 59.49 18.40 2 -2 -12 74.09 19.20 -2 2 12 37.80 16.90 -1 -2 12 59.39 20.20 1 2 -12 64.29 19.90 -1 2 12 71.79 18.90 0 -2 12 42.10 17.90 0 -2 -12 51.49 18.40 0 2 -12 45.10 19.40 0 2 12 34.70 17.20 -1 -2 -12 815.12 49.30 -1 2 -12 934.81 51.39 -2 -2 -12 29.70 21.30 -2 2 -12 34.10 21.40 6 -3 -12 22.10 58.29 -6 -3 12 61.29 19.60 5 -3 -12 99.39 58.69 -5 -3 12 123.29 21.90 -5 3 12 73.79 18.70 5 3 -12 89.69 56.39 4 -3 -12 43.60 53.99 -4 -3 12 67.39 19.60 4 3 -12 167.18 63.09 -4 3 12 41.30 16.70 3 -3 -12 500.15 34.50 -3 -3 12 482.55 35.50 3 3 -12 625.54 90.39 -2 -3 12 541.65 41.50 2 -3 -12 369.66 69.89 -2 3 12 417.16 35.10 -1 -3 12 589.34 39.70 -1 3 12 630.04 39.50 1 3 -12 606.44 41.40 0 -3 -12 254.07 28.20 0 -3 12 202.48 27.20 0 3 -12 182.18 27.10 -1 -3 -12 41.60 20.80 1 -3 12 29.00 18.90 -2 3 -12 40.60 22.10 -6 -4 12 522.55 36.90 -5 -4 12 110.99 22.40 -5 4 12 59.39 17.50 5 4 -12 74.19 61.29 4 -4 -12 767.82 98.79 -4 -4 12 574.14 38.20 4 4 -12 489.45 83.99 -4 4 12 573.04 36.00 -3 -4 12 54.19 19.50 3 4 -12 44.00 50.69 -3 4 12 54.79 16.00 -2 -4 12 54.89 17.90 -2 4 12 103.39 20.60 1 -4 -12 33.40 17.70 -1 -4 12 90.69 20.90 1 4 -12 65.89 20.50 -1 4 12 28.20 17.10 0 -4 -12 680.43 42.40 0 -4 12 617.34 42.30 0 4 -12 539.95 39.60 1 -4 12 156.88 25.60 -1 -4 -12 164.68 27.80 -1 4 -12 128.19 26.70 -2 -4 -12 587.54 47.30 -2 4 -12 576.34 46.00 -6 -5 12 188.78 25.90 6 5 -12 122.49 63.59 -5 -5 12 71.49 19.90 5 -5 -12 178.58 64.29 5 5 -12 37.50 58.79 -5 5 12 73.19 17.40 -4 -5 12 443.96 36.60 -4 5 12 378.66 31.70 4 5 -12 427.16 81.39 -3 -5 12 383.36 35.50 -3 5 12 340.57 30.30 -2 -5 12 770.92 45.60 -1 -5 12 272.87 30.90 -1 5 12 322.47 32.10 0 -5 12 298.07 33.60 0 -5 -12 276.17 31.40 0 5 -12 293.37 33.50 1 -5 12 66.49 19.90 -1 -5 -12 29.80 20.00 -2 -5 -12 285.47 35.00 -2 5 -12 319.97 34.90 -6 -6 12 216.68 28.00 6 6 -12 165.78 70.59 5 -6 -12 723.23 100.29 -5 -6 12 717.73 43.60 5 6 -12 606.54 95.69 -4 -6 12 69.89 20.20 4 -6 -12 -26.20 49.00 -4 6 12 13.70 16.00 -3 6 12 493.95 37.30 2 -6 -12 73.19 18.40 2 -6 -12 61.49 47.90 -2 -6 12 63.99 21.00 -1 -6 12 120.39 23.00 0 -6 12 187.78 27.90 0 -6 -12 133.69 25.50 0 6 -12 156.78 26.40 -1 -6 -12 700.03 44.70 1 -6 12 742.83 44.60 -5 -7 12 57.79 20.70 5 7 -12 64.69 56.09 -4 -7 12 48.90 19.20 4 7 -12 34.30 59.79 -4 7 12 27.00 16.00 3 -7 -12 462.85 35.30 -3 -7 12 492.15 39.70 -3 7 12 423.26 31.90 -2 -7 12 356.46 35.30 -2 7 12 365.06 32.50 -1 -7 12 649.64 43.70 0 -7 12 -15.40 16.40 0 7 -12 12.80 18.70 1 -7 12 32.60 18.60 -1 -7 -12 7.60 17.60 -5 -8 12 290.77 33.30 5 8 -12 170.88 72.49 -4 -8 12 841.12 47.40 4 8 -12 805.22 110.79 -3 -8 12 73.59 21.50 3 -8 -12 49.99 17.50 -2 -8 12 92.19 22.10 -2 8 12 88.19 19.60 1 -8 -12 56.49 19.50 -1 -8 12 75.19 21.50 0 -8 12 213.58 29.40 0 -8 -12 221.38 27.90 0 8 -12 247.78 31.50 1 -8 12 311.07 35.10 -1 -8 -12 344.67 36.30 -1 8 -12 290.57 34.40 2 -8 12 547.65 44.40 -5 -9 12 101.29 24.10 -4 -9 12 180.78 27.40 -3 -9 12 212.98 28.20 -3 9 12 227.38 25.40 -2 -9 12 1007.20 54.29 -2 9 12 1048.20 49.60 -1 -9 12 34.80 20.30 0 -9 12 304.77 34.10 0 -9 -12 345.37 34.00 0 9 -12 277.97 34.00 -1 -9 -12 50.59 21.20 -1 9 -12 62.59 20.60 2 -9 12 95.99 24.40 -5 -10 12 420.76 38.40 5 10 -12 360.76 88.79 4 10 -12 99.79 73.69 -3 -10 12 554.14 43.50 -3 10 12 504.35 33.20 1 -10 -12 89.29 21.50 -1 -10 12 22.60 20.40 0 -10 -12 323.77 33.80 0 10 -12 293.67 34.60 -1 10 -12 419.66 41.30 -3 -11 12 930.31 52.09 3 -11 -12 870.41 43.80 -2 -11 12 29.40 20.60 -1 -11 12 668.73 46.80 1 11 -12 722.53 45.70 0 -11 -12 37.30 19.90 -1 11 -12 59.59 22.90 -3 -12 12 193.68 26.60 -2 -12 12 47.40 20.60 0 -12 -12 205.38 27.10 -1 -12 -12 414.86 39.60 2 -13 -12 1318.57 122.29 1 -13 -12 87.49 20.40 0 -13 -12 442.56 38.20 1 -14 -12 115.19 23.10 -3 -15 12 538.35 45.40 -1 -15 12 592.24 49.20 -4 0 13 5.50 18.70 -3 0 13 723.43 44.50 1 0 -13 282.47 33.50 -1 0 13 319.67 34.90 0 0 13 27.00 19.00 -4 1 13 192.28 27.40 -3 -1 13 28.20 20.40 -3 1 13 31.30 19.40 -2 -1 13 32.70 19.90 2 -1 -13 68.69 22.40 -2 1 13 102.69 22.70 -1 -1 13 416.16 39.30 -1 1 13 392.06 38.20 0 1 13 382.26 38.90 -4 -2 13 576.14 43.40 -4 2 13 503.85 37.30 4 2 -13 502.35 90.99 -3 -2 13 9.30 19.10 -2 -2 13 613.64 43.20 -2 2 13 614.54 41.70 -1 -2 13 44.70 21.00 -1 2 13 21.90 19.80 0 -2 13 80.19 22.60 0 2 13 67.89 24.10 -3 -3 13 56.69 21.30 -3 3 13 49.90 19.80 -2 -3 13 167.98 27.70 -1 -3 13 87.89 23.70 -1 3 13 109.49 23.80 0 -3 13 703.33 47.60 0 3 13 729.03 47.10 -2 -4 13 61.79 22.20 2 4 -13 126.99 26.30 -2 4 13 51.39 19.80 -1 4 13 92.79 23.40 -3 5 13 76.19 20.20 -2 -5 13 42.00 22.40 -2 5 13 84.39 21.70 -1 -5 13 622.74 42.30 -1 5 13 614.44 42.60 1 5 -13 666.03 45.50 -2 -6 13 536.35 45.40 -2 6 13 498.85 40.70 -1 -6 13 118.89 25.20 ; _shelx_hkl_checksum 57994 _database_code_depnum_ccdc_archive 'CCDC 967915' ####################################################################### # # Cambridge Crystallographic Data Centre # CCDC # ####################################################################### # # This CIF contains data from an original supplementary publication # deposited with the CCDC, and may include chemical, crystal, # experimental, refinement, atomic coordinates, # anisotropic displacement parameters and molecular geometry data, # as required by the journal to which it was submitted. # # This CIF is provided on the understanding that it is used for bona # fide research purposes only. It may contain copyright material # of the CCDC or of third parties, and may not be copied or further # disseminated in any form, whether machine-readable or not, # except for the purpose of generating routine backup copies # on your local computer system. # # For further information on the CCDC, data deposition and # data retrieval see: # www.ccdc.cam.ac.uk # # Bona fide researchers may freely download Mercury and enCIFer # from this site to visualise CIF-encoded structures and # to carry out CIF format checking respectively. # data_cw10_MSJA47 _audit_creation_method SHELXL-2013 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H40 Ir N O2 P2' _chemical_formula_weight 580.67 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0015 0.0009 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0030 0.0019 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0056 0.0036 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.0667 0.0580 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ir Ir -0.5977 5.4269 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 12 _space_group_name_H-M_alt 'C 2/m' _space_group_name_Hall '-C 2y' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z' _cell_length_a 13.917(3) _cell_length_b 7.7210(15) _cell_length_c 11.629(2) _cell_angle_alpha 90 _cell_angle_beta 111.39(3) _cell_angle_gamma 90 _cell_volume 1163.5(5) _cell_formula_units_Z 2 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 7685 _cell_measurement_theta_min 2.38 _cell_measurement_theta_max 21.11 _exptl_crystal_description block _exptl_crystal_colour red _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.657 _exptl_crystal_F_000 580 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.090 _exptl_crystal_size_mid 0.080 _exptl_crystal_size_min 0.060 _exptl_absorpt_coefficient_mu 3.203 _shelx_estimated_absorpt_T_min 0.761 _shelx_estimated_absorpt_T_max 0.831 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_min 0.6594 _exptl_absorpt_correction_T_max 0.7459 _exptl_absorpt_process_details SADABS-2012/1 _exptl_special_details ; ? ; _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.56086 _diffrn_radiation_type AgK\a _diffrn_source 'INCOATEC Ag Microsource' _diffrn_measurement_device_type 'Bruker Smart APEX II Quazar' _diffrn_measurement_method 'omega and phi scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 19582 _diffrn_reflns_av_unetI/netI 0.0260 _diffrn_reflns_av_R_equivalents 0.0592 _diffrn_reflns_limit_h_min -19 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_theta_min 2.381 _diffrn_reflns_theta_max 23.612 _diffrn_reflns_theta_full 19.665 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_point_group_measured_fraction_full 0.999 _reflns_number_total 1891 _reflns_number_gt 1891 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'APEX2 v2012.2' _computing_cell_refinement 'SAINT V7.68A' _computing_data_reduction 'SAINT V7.68A' _computing_structure_solution 'SHELXS-2012 (Sheldrick, 2012)' _computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)' _computing_molecular_graphics 'XP Version 5.1' _computing_publication_material 'XP Version 5.1' _refine_special_details ; ? ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0215P)^2^] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 1891 _refine_ls_number_parameters 126 _refine_ls_number_restraints 161 _refine_ls_R_factor_all 0.0168 _refine_ls_R_factor_gt 0.0168 _refine_ls_wR_factor_ref 0.0370 _refine_ls_wR_factor_gt 0.0370 _refine_ls_goodness_of_fit_ref 1.064 _refine_ls_restrained_S_all 1.047 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ir1 Ir 0.0000 0.5000 0.5000 0.01278(5) Uani 1 4 d DS TU P . . P1 P -0.13224(7) 0.45454(10) 0.30783(8) 0.01169(18) Uani 0.5 1 d D U P A -1 C3 C -0.0945(2) 0.5122(15) 0.1736(3) 0.0212(10) Uani 0.5 1 d D U P A -1 C4 C 0.0160(3) 0.4430(6) 0.2082(4) 0.0320(10) Uani 0.5 1 d D U P A -1 H4A H 0.0168 0.3182 0.2241 0.048 Uiso 0.5 1 calc R U P A -1 H4B H 0.0617 0.5023 0.2826 0.048 Uiso 0.5 1 calc R U P A -1 H4C H 0.0400 0.4642 0.1400 0.048 Uiso 0.5 1 calc R U P A -1 C5 C -0.0939(4) 0.7097(6) 0.1578(4) 0.0335(10) Uani 0.5 1 d D U P A -1 H5A H -0.0580 0.7388 0.1019 0.050 Uiso 0.5 1 calc R U P A -1 H5B H -0.0582 0.7640 0.2384 0.050 Uiso 0.5 1 calc R U P A -1 H5C H -0.1651 0.7522 0.1232 0.050 Uiso 0.5 1 calc R U P A -1 C6 C -0.1632(4) 0.4283(7) 0.0517(4) 0.0340(10) Uani 0.5 1 d D U P A -1 H6A H -0.2344 0.4687 0.0301 0.051 Uiso 0.5 1 calc R U P A -1 H6B H -0.1609 0.3021 0.0611 0.051 Uiso 0.5 1 calc R U P A -1 H6C H -0.1381 0.4605 -0.0139 0.051 Uiso 0.5 1 calc R U P A -1 C7 C -0.2629(3) 0.5335(4) 0.2929(3) 0.0156(9) Uani 0.5 1 d D U P A -1 C8 C -0.2615(3) 0.7306(5) 0.3120(4) 0.0280(9) Uani 0.5 1 d D U P A -1 H8A H -0.2588 0.7892 0.2384 0.042 Uiso 0.5 1 calc R U P A -1 H8B H -0.2006 0.7624 0.3839 0.042 Uiso 0.5 1 calc R U P A -1 H8C H -0.3240 0.7659 0.3259 0.042 Uiso 0.5 1 calc R U P A -1 C9 C -0.2860(3) 0.4473(5) 0.3991(4) 0.0230(8) Uani 0.5 1 d D U P A -1 H9A H -0.3511 0.4926 0.4013 0.035 Uiso 0.5 1 calc R U P A -1 H9B H -0.2299 0.4726 0.4775 0.035 Uiso 0.5 1 calc R U P A -1 H9C H -0.2917 0.3217 0.3860 0.035 Uiso 0.5 1 calc R U P A -1 C10 C -0.3487(3) 0.484(3) 0.1704(3) 0.024(2) Uani 0.5 1 d D U P A -1 H10A H -0.3413 0.5525 0.1032 0.036 Uiso 0.5 1 calc R U P A -1 H10B H -0.4161 0.5072 0.1758 0.036 Uiso 0.5 1 calc R U P A -1 H10C H -0.3432 0.3605 0.1541 0.036 Uiso 0.5 1 calc R U P A -1 N1 N 0.0000 0.2390(6) 0.5000 0.0124(9) Uani 0.25 1 d S U P A -1 O1 O 0.0329(3) 0.7346(4) 0.4659(3) 0.0248(7) Uani 0.5 1 d . U P A -1 C1 C -0.0704(2) 0.1431(4) 0.4028(3) 0.0141(6) Uani 0.5 1 d . U P A -1 H1 H -0.0691 0.0202 0.4069 0.017 Uiso 0.5 1 calc R U P A -1 C2 C -0.1398(3) 0.2225(5) 0.3036(3) 0.0157(6) Uani 0.5 1 d . U P A -1 H2 H -0.1886 0.1607 0.2372 0.019 Uiso 0.5 1 calc R U P A -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ir1 0.01223(7) 0.01392(7) 0.01148(7) 0.000 0.00348(5) 0.000 P1 0.0129(4) 0.0103(5) 0.0119(4) -0.0001(2) 0.0046(3) -0.0010(2) C3 0.0200(13) 0.030(3) 0.0140(12) -0.003(2) 0.0073(10) -0.010(3) C4 0.0240(19) 0.050(3) 0.027(2) -0.0045(17) 0.0153(16) -0.0085(16) C5 0.044(3) 0.034(2) 0.021(2) 0.0068(17) 0.0099(19) -0.0117(19) C6 0.032(2) 0.055(3) 0.0162(17) -0.0103(17) 0.0098(16) -0.0182(19) C7 0.0151(13) 0.012(3) 0.0187(14) 0.0020(11) 0.0051(11) 0.0026(10) C8 0.024(2) 0.0175(18) 0.039(2) 0.0002(16) 0.0079(18) 0.0051(15) C9 0.0182(17) 0.031(2) 0.0233(17) 0.0040(13) 0.0121(15) 0.0018(13) C10 0.0177(13) 0.029(6) 0.0211(14) 0.004(2) 0.0016(11) 0.001(2) N1 0.011(2) 0.012(2) 0.013(2) -0.001(5) 0.0043(17) -0.002(6) O1 0.032(2) 0.0136(13) 0.0249(17) 0.0041(12) 0.0059(13) -0.0066(12) C1 0.0128(15) 0.0110(14) 0.0177(16) -0.0028(11) 0.0048(13) -0.0012(11) C2 0.0140(15) 0.0141(15) 0.0175(16) -0.0030(12) 0.0039(13) -0.0024(12) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ir1 O1 1.945(3) . ? Ir1 O1 1.945(3) 2_556 ? Ir1 N1 2.015(5) . ? Ir1 P1 2.3461(13) . ? Ir1 P1 2.3461(13) 2_556 ? P1 C2 1.794(4) . ? P1 C7 1.866(3) . ? P1 C3 1.873(4) . ? C3 C6 1.534(6) . ? C3 C5 1.536(12) . ? C3 C4 1.537(6) . ? C7 C10 1.536(7) . ? C7 C9 1.536(5) . ? C7 C8 1.537(5) . ? N1 C1 1.407(4) . ? O1 O1 1.415(7) 2_556 ? C1 C2 1.352(5) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Ir1 O1 42.7(2) . 2_556 ? O1 Ir1 N1 158.66(11) . . ? O1 Ir1 N1 158.66(11) 2_556 . ? O1 Ir1 P1 96.11(10) . . ? O1 Ir1 P1 99.93(10) 2_556 . ? N1 Ir1 P1 81.40(2) . . ? O1 Ir1 P1 99.93(10) . 2_556 ? O1 Ir1 P1 96.11(10) 2_556 2_556 ? N1 Ir1 P1 81.395(19) . 2_556 ? P1 Ir1 P1 162.79(4) . 2_556 ? C2 P1 C7 106.16(15) . . ? C2 P1 C3 104.2(4) . . ? C7 P1 C3 113.9(2) . . ? C2 P1 Ir1 101.16(12) . . ? C7 P1 Ir1 116.05(11) . . ? C3 P1 Ir1 113.40(14) . . ? C6 C3 C5 109.7(5) . . ? C6 C3 C4 108.7(6) . . ? C5 C3 C4 109.2(5) . . ? C6 C3 P1 113.6(4) . . ? C5 C3 P1 110.5(5) . . ? C4 C3 P1 104.9(4) . . ? C10 C7 C9 108.5(5) . . ? C10 C7 C8 110.2(8) . . ? C9 C7 C8 108.0(3) . . ? C10 C7 P1 113.9(4) . . ? C9 C7 P1 105.4(2) . . ? C8 C7 P1 110.4(3) . . ? C1 N1 Ir1 121.8(2) . . ? O1 O1 Ir1 68.66(11) 2_556 . ? C2 C1 N1 121.2(3) . . ? C1 C2 P1 114.4(3) . . ? _refine_diff_density_max 1.260 _refine_diff_density_min -0.743 _refine_diff_density_rms 0.103 _shelxl_version_number 2013-4 _shelx_res_file ; REM Solution 2 R1 0.050, Alpha = 0.0165 in C2 REM Flack x = 0.499 ( 0.005 ) from Parsons' quotients REM Formula: C22 P2 Ir TITL c2 in C2 CELL 0.56086 13.9170 7.7210 11.6290 90.000 111.392 90.000 ZERR 2.00 0.00278 0.00154 0.00233 0.0000 0.0300 0.0000 LATT 7 SYMM -X, Y, -Z SFAC C H N O P IR UNIT 40 80 2 4 4 2 L.S. 20 TEMP -173 SIZE 0.09 0.08 0.06 BOND SHEL 999 0.7 LIST 4 ACTA EQIV $1 -x,y,1-z BIND O1 O1_$1 BIND Ir1 P1_$1 FMAP 2 PLAN 10 RIGU SAME Ir1 P1 C7 C8 C9 C10 SAME IR1 P1 C3 C5 C6 C4 WGHT 0.021500 FVAR 0.39509 IR1 6 0.000000 0.500000 0.500000 10.25000 0.01223 0.01392 = 0.01148 0.00000 0.00348 0.00000 PART -1 P1 5 -0.132244 0.454537 0.307832 10.50000 0.01290 0.01034 = 0.01193 -0.00011 0.00464 -0.00101 C3 1 -0.094494 0.512241 0.173597 10.50000 0.02002 0.03046 = 0.01400 -0.00309 0.00728 -0.00968 C4 1 0.015993 0.442970 0.208193 10.50000 0.02395 0.04981 = 0.02720 -0.00454 0.01532 -0.00852 AFIX 137 H4A 2 0.016827 0.318227 0.224096 10.50000 -1.50000 H4B 2 0.061655 0.502262 0.282561 10.50000 -1.50000 H4C 2 0.039966 0.464240 0.139989 10.50000 -1.50000 AFIX 0 C5 1 -0.093905 0.709675 0.157831 10.50000 0.04403 0.03414 = 0.02085 0.00684 0.00995 -0.01169 AFIX 137 H5A 2 -0.058016 0.738813 0.101886 10.50000 -1.50000 H5B 2 -0.058243 0.763964 0.238385 10.50000 -1.50000 H5C 2 -0.165082 0.752234 0.123161 10.50000 -1.50000 AFIX 0 C6 1 -0.163156 0.428292 0.051711 10.50000 0.03162 0.05526 = 0.01617 -0.01028 0.00980 -0.01817 AFIX 137 H6A 2 -0.234351 0.468673 0.030089 10.50000 -1.50000 H6B 2 -0.160898 0.302055 0.061104 10.50000 -1.50000 H6C 2 -0.138075 0.460528 -0.013908 10.50000 -1.50000 AFIX 0 C7 1 -0.262937 0.533547 0.292903 10.50000 0.01512 0.01220 = 0.01867 0.00202 0.00511 0.00263 C8 1 -0.261453 0.730621 0.311999 10.50000 0.02412 0.01750 = 0.03926 0.00022 0.00791 0.00510 AFIX 137 H8A 2 -0.258841 0.789163 0.238422 10.50000 -1.50000 H8B 2 -0.200572 0.762438 0.383889 10.50000 -1.50000 H8C 2 -0.323998 0.765936 0.325863 10.50000 -1.50000 AFIX 0 C9 1 -0.286009 0.447298 0.399056 10.50000 0.01819 0.03137 = 0.02326 0.00399 0.01207 0.00183 AFIX 137 H9A 2 -0.351075 0.492560 0.401348 10.50000 -1.50000 H9B 2 -0.229945 0.472572 0.477542 10.50000 -1.50000 H9C 2 -0.291728 0.321738 0.386002 10.50000 -1.50000 AFIX 0 C10 1 -0.348660 0.483962 0.170400 10.50000 0.01769 0.02855 = 0.02110 0.00370 0.00162 0.00090 AFIX 137 H10A 2 -0.341302 0.552548 0.103178 10.50000 -1.50000 H10B 2 -0.416125 0.507178 0.175775 10.50000 -1.50000 H10C 2 -0.343244 0.360525 0.154090 10.50000 -1.50000 AFIX 0 N1 3 10.000000 0.239042 10.500000 10.25000 0.01124 0.01231 = 0.01347 -0.00069 0.00427 -0.00194 O1 4 0.032949 0.734607 0.465859 10.50000 0.03214 0.01361 = 0.02494 0.00410 0.00595 -0.00656 C1 1 -0.070395 0.143112 0.402765 10.50000 0.01281 0.01104 = 0.01775 -0.00282 0.00478 -0.00124 AFIX 43 H1 2 -0.069108 0.020207 0.406882 10.50000 -1.20000 AFIX 0 C2 1 -0.139837 0.222537 0.303580 10.50000 0.01400 0.01408 = 0.01747 -0.00302 0.00390 -0.00244 AFIX 43 H2 2 -0.188583 0.160676 0.237177 10.50000 -1.20000 PART 0 AFIX 0 HKLF 4 REM c2 in C2 REM R1 = 0.0168 for 1891 Fo > 4sig(Fo) and 0.0168 for all 1891 data REM 126 parameters refined using 161 restraints END WGHT 0.0215 0.0000 REM Highest difference peak 1.260, deepest hole -0.743, 1-sigma level 0.103 Q1 1 -0.0278 0.5000 0.4246 10.50000 0.05 1.26 Q2 1 -0.0596 0.5000 0.5067 10.50000 0.05 0.62 Q3 1 -0.3040 0.5000 0.2347 10.50000 0.05 0.57 Q4 1 -0.1477 0.5000 0.4359 10.50000 0.05 0.52 Q5 1 -0.1914 0.5000 0.3004 10.50000 0.05 0.47 Q6 1 -0.2568 0.5000 0.3627 10.50000 0.05 0.44 Q7 1 -0.1264 0.5000 0.1130 10.50000 0.05 0.43 Q8 1 0.1105 0.5000 0.4172 10.50000 0.05 0.41 Q9 1 -0.0438 0.5000 0.5844 10.50000 0.05 0.41 Q10 1 -0.1805 0.5000 0.2581 10.50000 0.05 0.37 ; _shelx_res_checksum 40759 _shelx_hkl_file ; 0 -2 0 5081.49 190.68 0 -2 0 5125.59 166.18 0 -2 0 5292.47 161.68 0 2 0 5188.78 168.98 0 2 0 4991.00 166.28 0 2 0 4946.21 179.18 0 2 0 5214.98 161.68 0 2 0 4923.41 192.38 0 2 0 5160.38 169.08 0 -4 0 6982.20 218.48 0 -4 0 6747.03 264.47 0 -4 0 6973.40 228.18 0 4 0 7082.99 218.38 0 4 0 7140.09 232.98 0 4 0 6766.22 235.08 0 4 0 6734.43 249.97 0 4 0 6645.24 267.37 0 -6 0 813.12 41.70 0 -6 0 866.31 58.49 0 6 0 819.12 57.59 0 6 0 823.32 44.60 0 6 0 919.11 54.99 0 6 0 796.42 58.19 0 -8 0 616.14 40.50 0 -8 0 548.35 56.29 0 8 0 626.64 54.69 0 8 0 620.64 44.90 0 8 0 675.73 61.79 0 8 0 651.93 60.89 0 -10 0 34.90 36.80 0 10 0 96.49 41.70 0 10 0 101.29 51.49 0 10 0 119.99 46.60 0 -12 0 38.30 49.10 0 -12 0 58.69 44.70 0 12 0 59.29 48.90 0 12 0 40.90 44.70 0 12 0 82.79 55.09 0 12 1 376.16 73.39 0 12 1 178.48 64.79 0 12 1 140.29 58.49 0 -12 -1 83.89 47.10 0 -12 -1 124.19 51.19 0 10 1 122.59 46.00 0 10 1 141.29 42.60 0 10 1 181.68 58.59 0 -10 -1 72.39 39.50 0 8 1 739.63 64.49 0 8 1 717.33 58.79 0 8 1 767.32 67.99 0 -8 -1 740.13 48.00 0 -8 -1 697.33 61.39 0 6 1 897.71 60.99 0 6 1 844.62 54.39 0 6 1 870.11 42.50 0 6 1 896.41 58.99 0 6 1 882.11 35.70 0 -6 -1 797.32 34.20 0 -6 -1 869.11 59.29 0 -6 -1 859.41 45.80 0 4 1 2615.94 119.99 0 4 1 2914.41 94.29 0 4 1 2808.62 97.69 0 4 1 2814.72 113.69 0 4 1 2630.84 106.59 0 -4 -1 2675.93 118.69 0 -4 -1 2746.13 101.19 0 -4 -1 2805.62 93.79 0 2 1 1524.25 52.39 0 2 1 1524.15 57.79 0 2 1 1485.65 59.89 0 2 1 1387.76 63.89 0 -2 -1 1486.75 63.39 0 -2 -1 1497.95 52.09 0 -2 -1 1424.36 54.79 0 -2 1 1490.75 47.90 0 -2 1 1459.15 63.09 0 -2 1 1520.65 49.40 0 -2 1 1492.15 63.09 0 2 -1 1527.55 49.50 0 2 -1 1435.96 60.79 0 2 -1 1444.66 63.89 0 2 -1 1462.65 56.99 0 2 -1 1435.86 55.89 0 -4 1 2771.32 96.39 0 -4 1 2759.92 120.09 0 4 -1 2803.22 105.99 0 4 -1 2934.51 108.59 0 4 -1 2637.74 121.09 0 4 -1 2955.80 117.49 0 -6 1 851.81 39.40 0 -6 1 783.12 56.79 0 6 -1 835.02 52.89 0 6 -1 884.41 59.49 0 6 -1 812.22 60.09 0 6 -1 869.91 49.40 0 -8 1 688.73 59.49 0 -8 1 624.44 58.99 0 8 -1 798.52 59.69 0 8 -1 645.14 49.30 0 8 -1 702.13 63.69 0 8 -1 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413.96 55.09 10 -10 -3 244.78 59.09 -10 10 3 212.28 67.19 10 10 -2 83.99 60.99 10 10 -2 173.48 54.69 10 10 -2 111.69 49.00 -10 -10 2 98.99 50.29 10 8 -2 206.58 43.30 10 8 -2 308.87 54.59 10 8 -2 302.47 65.29 -10 -8 2 264.77 42.20 -10 -8 2 247.38 55.19 10 6 -2 572.04 60.89 10 6 -2 592.54 49.80 10 6 -2 495.25 54.69 -10 -6 2 514.85 52.39 -10 -6 2 497.75 42.80 -10 -6 2 484.65 41.30 10 4 -2 1411.76 70.19 10 4 -2 1461.15 86.79 10 4 -2 1417.56 82.59 10 4 -2 1436.66 75.99 10 4 -2 1404.66 74.79 10 4 -2 1516.05 75.49 -10 -4 2 1526.25 74.49 -10 -4 2 1513.65 74.29 10 2 -2 1672.43 82.29 10 2 -2 1608.44 84.09 10 2 -2 1646.84 77.99 10 2 -2 1549.34 78.99 10 2 -2 1720.53 67.59 -10 -2 2 1704.63 77.59 -10 -2 2 1639.54 65.59 -10 -2 2 1330.67 74.79 10 0 -2 1907.11 80.39 10 0 -2 1996.80 93.49 10 0 -2 1853.91 89.89 10 0 -2 1912.81 88.09 -10 0 2 1983.70 70.69 -10 0 2 2021.20 88.19 10 -2 -2 1766.82 83.89 10 -2 -2 1642.04 82.89 10 -2 -2 1625.04 79.79 -10 2 2 1603.44 60.59 -10 2 2 1586.74 82.09 10 -4 -2 1444.16 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