# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2014

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#                 Cambridge Crystallographic Data Centre
#                                CCDC 
# 
#######################################################################
# 
#  This CIF contains data from an original supplementary publication
#  deposited with the CCDC, and may include chemical, crystal,
#  experimental, refinement, atomic coordinates,
#  anisotropic displacement parameters and molecular geometry data,
#  as required by the journal to which it was submitted.
#
#  This CIF is provided on the understanding that it is used for bona
#  fide research purposes only. It may contain copyright material
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data_Compoud_2
#TrackingRef 'web_deposit_cif_file_0_Qiao-HuaWei_1365744067.2.cif'


_audit_creation_method           SHELXL-97
_chemical_name_systematic        
;
?
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C96 H78 Ag Cl5 N2 O4 P4 Pt2'
_chemical_formula_weight         2122.78

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           Monoclinic
_symmetry_space_group_name_H-M   P2(1)/c

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   13.4625(14)
_cell_length_b                   25.739(3)
_cell_length_c                   25.325(3)
_cell_angle_alpha                90.00
_cell_angle_beta                 94.556(2)
_cell_angle_gamma                90.00
_cell_volume                     8747.6(16)
_cell_formula_units_Z            4
_cell_measurement_temperature    273(2)
_cell_measurement_reflns_used    5499
_cell_measurement_theta_min      2.26
_cell_measurement_theta_max      22.66

_exptl_crystal_description       prism
_exptl_crystal_colour            yellow
_exptl_crystal_size_max          0.18
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.10
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    1.612
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             4192
_exptl_absorpt_coefficient_mu    3.691
_exptl_absorpt_correction_type   none
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   ?

_exptl_special_details           
;
?
;

_diffrn_ambient_temperature      273(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            62951
_diffrn_reflns_av_R_equivalents  0.1324
_diffrn_reflns_av_sigmaI/netI    0.1411
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_k_min       -30
_diffrn_reflns_limit_k_max       30
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_theta_min         1.13
_diffrn_reflns_theta_max         25.00
_reflns_number_total             15376
_reflns_number_gt                10874
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'Bruker SMART'
_computing_cell_refinement       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'

_refine_special_details          
;
Refinement of F² against ALL reflections. The weighted R-factor wR and
goodness of fit S are based on F², conventional R-factors R are based
on F, with F set to zero for negative F². The threshold expression of
F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is
not relevant to the choice of reflections for refinement. R-factors based
on F² are statistically about twice as large as those based on F, and R-
factors based on ALL data will be even larger.
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0672P)²+70.2096P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    contr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         15376
_refine_ls_number_parameters     929
_refine_ls_number_restraints     3
_refine_ls_R_factor_all          0.1090
_refine_ls_R_factor_gt           0.0748
_refine_ls_wR_factor_ref         0.2017
_refine_ls_wR_factor_gt          0.1830
_refine_ls_goodness_of_fit_ref   1.034
_refine_ls_restrained_S_all      1.034
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.21445(3) 0.321003(18) 0.753207(18) 0.02283(14) Uani 1 1 d . . .
Pt2 Pt 0.18882(3) 0.152366(18) 0.858610(18) 0.02316(15) Uani 1 1 d . . .
Ag3 Ag 0.27132(7) 0.21458(4) 0.77436(4) 0.0314(3) Uani 1 1 d . . .
P1 P 0.3676(2) 0.34680(12) 0.79097(12) 0.0244(7) Uani 1 1 d . . .
P2 P 0.2456(2) 0.20636(12) 0.92653(12) 0.0221(7) Uani 1 1 d . . .
P3 P 0.0603(2) 0.29540(12) 0.71705(13) 0.0241(7) Uani 1 1 d . . .
P4 P 0.1351(2) 0.10192(12) 0.78645(13) 0.0268(7) Uani 1 1 d . . .
Cl1 Cl -0.2723(3) 0.3039(2) 0.07209(17) 0.0619(12) Uani 1 1 d . . .
Cl2 Cl -0.5404(6) 0.4934(3) 0.4181(3) 0.124(3) Uani 1 1 d . . .
Cl3 Cl -0.3929(6) 0.4859(3) 0.3424(3) 0.119(2) Uani 1 1 d . . .
Cl6 Cl 0.3347(9) 0.5290(4) 1.0082(5) 0.100(4) Uani 0.50 1 d PD . .
Cl7 Cl 0.3058(7) 0.5935(4) 1.0932(4) 0.092(4) Uani 0.50 1 d PD . .
Cl8 Cl 0.2113(8) 0.5132(4) 0.4167(4) 0.081(3) Uani 0.50 1 d P . .
Cl9 Cl 0.0672(10) 0.4855(4) 0.4902(4) 0.093(4) Uani 0.50 1 d P . .
O1 O -0.1817(11) 0.3082(11) 0.0550(6) 0.168(11) Uani 1 1 d . . .
O2 O -0.2971(14) 0.3474(8) 0.0990(7) 0.142(8) Uani 1 1 d . . .
O3 O -0.3422(11) 0.2952(8) 0.0294(6) 0.133(8) Uani 1 1 d . . .
O4 O -0.267(2) 0.2642(9) 0.1093(10) 0.189(11) Uani 1 1 d . . .
N1 N 0.0909(7) 0.1932(4) 0.7387(4) 0.021(2) Uani 1 1 d . . .
N2 N 0.3307(7) 0.2760(4) 0.8654(4) 0.024(2) Uani 1 1 d . . .
C01 C -0.4821(17) 0.4534(8) 0.3759(9) 0.090(7) Uani 1 1 d . . .
H01A H -0.5316 0.4387 0.3503 0.108 Uiso 1 1 calc R . .
H01B H -0.4504 0.4251 0.3960 0.108 Uiso 1 1 calc R . .
C02 C 0.285(3) 0.5868(11) 1.0269(8) 0.095(14) Uiso 0.50 1 d PD . .
H02A H 0.3164 0.6153 1.0092 0.114 Uiso 0.50 1 calc PR . .
H02B H 0.2144 0.5876 1.0167 0.114 Uiso 0.50 1 calc PR . .
C03 C 0.094(3) 0.4855(15) 0.4238(12) 0.077(13) Uani 0.50 1 d P . .
H03A H 0.0436 0.5050 0.4029 0.092 Uiso 0.50 1 calc PR . .
H03B H 0.0935 0.4501 0.4107 0.092 Uiso 0.50 1 calc PR . .
C11 C 0.1491(9) 0.3723(5) 0.7985(5) 0.026(3) Uani 1 1 d . . .
C12 C 0.1113(10) 0.4053(5) 0.8223(5) 0.032(3) Uani 1 1 d . . .
C13 C 0.0692(11) 0.4445(5) 0.8544(5) 0.038(3) Uani 1 1 d . . .
C14 C -0.0324(12) 0.4497(7) 0.8535(7) 0.059(5) Uani 1 1 d . . .
H14A H -0.0733 0.4280 0.8320 0.071 Uiso 1 1 calc R . .
C15 C -0.0751(12) 0.4874(7) 0.8845(7) 0.062(5) Uani 1 1 d . . .
H15A H -0.1442 0.4902 0.8827 0.075 Uiso 1 1 calc R . .
C16 C -0.0208(15) 0.5194(6) 0.9165(7) 0.056(5) Uani 1 1 d . . .
C17 C 0.0819(17) 0.5153(8) 0.9162(8) 0.078(6) Uani 1 1 d . . .
H17A H 0.1223 0.5375 0.9375 0.093 Uiso 1 1 calc R . .
C18 C 0.1257(12) 0.4789(6) 0.8850(6) 0.055(4) Uani 1 1 d . . .
H18A H 0.1948 0.4779 0.8849 0.066 Uiso 1 1 calc R . .
C19 C -0.0642(18) 0.5604(8) 0.9505(9) 0.096(8) Uani 1 1 d . . .
H19A H -0.1356 0.5581 0.9469 0.145 Uiso 1 1 calc R . .
H19B H -0.0440 0.5942 0.9393 0.145 Uiso 1 1 calc R . .
H19C H -0.0405 0.5551 0.9868 0.145 Uiso 1 1 calc R . .
C21 C 0.2754(8) 0.2704(4) 0.7050(4) 0.024(3) Uani 1 1 d D . .
C22 C 0.2972(9) 0.2388(5) 0.6726(4) 0.029(3) Uani 1 1 d D . .
C23 C 0.3199(9) 0.2042(5) 0.6293(4) 0.022(3) Uani 1 1 d . . .
C24 C 0.2456(11) 0.1848(6) 0.5956(5) 0.040(4) Uani 1 1 d . . .
H24A H 0.1799 0.1914 0.6025 0.048 Uiso 1 1 calc R . .
C25 C 0.2634(12) 0.1557(6) 0.5514(6) 0.047(4) Uani 1 1 d . . .
H25A H 0.2099 0.1429 0.5298 0.056 Uiso 1 1 calc R . .
C26 C 0.3567(12) 0.1456(6) 0.5391(6) 0.047(4) Uani 1 1 d . . .
C27 C 0.4362(11) 0.1653(6) 0.5746(6) 0.046(4) Uani 1 1 d . . .
H27A H 0.5013 0.1578 0.5674 0.056 Uiso 1 1 calc R . .
C28 C 0.4218(10) 0.1944(6) 0.6181(6) 0.043(4) Uani 1 1 d . . .
H28A H 0.4752 0.2074 0.6397 0.052 Uiso 1 1 calc R . .
C29 C 0.3790(15) 0.1148(8) 0.4909(7) 0.082(7) Uani 1 1 d . . .
H29A H 0.3177 0.1048 0.4717 0.124 Uiso 1 1 calc R . .
H29B H 0.4163 0.0843 0.5017 0.124 Uiso 1 1 calc R . .
H29C H 0.4174 0.1357 0.4686 0.124 Uiso 1 1 calc R . .
C31 C 0.3266(8) 0.1529(5) 0.8346(4) 0.020(3) Uani 1 1 d . . .
C32 C 0.4081(10) 0.1563(5) 0.8176(5) 0.032(3) Uani 1 1 d . . .
C33 C 0.5086(9) 0.1553(5) 0.7991(5) 0.025(3) Uani 1 1 d . . .
C34 C 0.5921(11) 0.1686(6) 0.8320(6) 0.040(3) Uani 1 1 d . . .
H34A H 0.5857 0.1764 0.8675 0.048 Uiso 1 1 calc R . .
C35 C 0.6823(10) 0.1701(7) 0.8126(7) 0.058(5) Uani 1 1 d . . .
H35A H 0.7377 0.1784 0.8354 0.069 Uiso 1 1 calc R . .
C36 C 0.6954(11) 0.1597(6) 0.7600(6) 0.045(4) Uani 1 1 d . . .
C37 C 0.6125(10) 0.1452(6) 0.7269(6) 0.040(4) Uani 1 1 d . . .
H37A H 0.6204 0.1360 0.6919 0.048 Uiso 1 1 calc R . .
C38 C 0.5191(11) 0.1444(5) 0.7452(5) 0.037(3) Uani 1 1 d . . .
H38A H 0.4635 0.1368 0.7224 0.044 Uiso 1 1 calc R . .
C39 C 0.7935(11) 0.1653(8) 0.7367(8) 0.072(6) Uani 1 1 d . . .
H39A H 0.8434 0.1755 0.7639 0.108 Uiso 1 1 calc R . .
H39B H 0.7881 0.1913 0.7094 0.108 Uiso 1 1 calc R . .
H39C H 0.8119 0.1327 0.7218 0.108 Uiso 1 1 calc R . .
C41 C 0.0542(9) 0.1504(5) 0.8867(5) 0.029(3) Uani 1 1 d . . .
C42 C -0.0258(10) 0.1500(6) 0.9059(5) 0.042(4) Uani 1 1 d . . .
C43 C -0.1200(10) 0.1450(6) 0.9282(6) 0.040(3) Uani 1 1 d . . .
C44 C -0.1620(11) 0.0972(7) 0.9331(6) 0.051(4) Uani 1 1 d . . .
H44A H -0.1304 0.0679 0.9208 0.061 Uiso 1 1 calc R . .
C45 C -0.2538(11) 0.0916(7) 0.9567(6) 0.053(4) Uani 1 1 d . . .
H45A H -0.2814 0.0587 0.9596 0.064 Uiso 1 1 calc R . .
C46 C -0.3019(11) 0.1332(8) 0.9752(6) 0.055(4) Uani 1 1 d . . .
C47 C -0.2577(11) 0.1827(7) 0.9704(5) 0.045(4) Uani 1 1 d . . .
H47A H -0.2900 0.2121 0.9817 0.054 Uiso 1 1 calc R . .
C48 C -0.1674(12) 0.1876(7) 0.9492(6) 0.048(4) Uani 1 1 d . . .
H48A H -0.1371 0.2200 0.9488 0.057 Uiso 1 1 calc R . .
C49 C -0.3986(13) 0.1285(8) 1.0024(7) 0.074(6) Uani 1 1 d . . .
H49A H -0.4193 0.0928 1.0025 0.110 Uiso 1 1 calc R . .
H49B H -0.4494 0.1491 0.9837 0.110 Uiso 1 1 calc R . .
H49C H -0.3880 0.1407 1.0383 0.110 Uiso 1 1 calc R . .
C52 C 0.3520(9) 0.2475(4) 0.9100(5) 0.026(3) Uani 1 1 d . . .
C53 C 0.4428(10) 0.2481(5) 0.9389(5) 0.033(3) Uani 1 1 d . . .
H53A H 0.4539 0.2289 0.9699 0.040 Uiso 1 1 calc R . .
C54 C 0.5176(10) 0.2788(5) 0.9197(5) 0.034(3) Uani 1 1 d . . .
H54A H 0.5802 0.2801 0.9381 0.041 Uiso 1 1 calc R . .
C55 C 0.4999(10) 0.3069(5) 0.8744(5) 0.034(3) Uani 1 1 d . . .
H55A H 0.5502 0.3269 0.8613 0.041 Uiso 1 1 calc R . .
C56 C 0.4047(8) 0.3053(5) 0.8478(4) 0.023(3) Uani 1 1 d . . .
C61 C 0.0741(9) 0.1427(5) 0.7327(5) 0.028(3) Uani 1 1 d . . .
C62 C 0.0186(9) 0.1209(5) 0.6896(5) 0.031(3) Uani 1 1 d . . .
H62A H 0.0100 0.0851 0.6866 0.038 Uiso 1 1 calc R . .
C63 C -0.0224(10) 0.1538(5) 0.6523(5) 0.033(3) Uani 1 1 d . . .
H63A H -0.0587 0.1406 0.6225 0.040 Uiso 1 1 calc R . .
C64 C -0.0107(9) 0.2068(5) 0.6581(5) 0.033(3) Uani 1 1 d . . .
H64A H -0.0416 0.2297 0.6336 0.039 Uiso 1 1 calc R . .
C65 C 0.0490(8) 0.2250(5) 0.7019(5) 0.026(3) Uani 1 1 d . . .
C101 C 0.4711(9) 0.3401(5) 0.7497(5) 0.029(3) Uani 1 1 d . . .
C102 C 0.5171(10) 0.2929(5) 0.7429(5) 0.037(3) Uani 1 1 d . . .
H10A H 0.5011 0.2647 0.7636 0.044 Uiso 1 1 calc R . .
C103 C 0.5867(11) 0.2867(6) 0.7060(6) 0.044(4) Uani 1 1 d . . .
H10B H 0.6160 0.2544 0.7019 0.052 Uiso 1 1 calc R . .
C104 C 0.6126(10) 0.3269(6) 0.6758(5) 0.040(4) Uani 1 1 d . . .
H10C H 0.6605 0.3225 0.6516 0.048 Uiso 1 1 calc R . .
C105 C 0.5679(11) 0.3740(7) 0.6808(6) 0.049(4) Uani 1 1 d . . .
H10D H 0.5853 0.4016 0.6596 0.059 Uiso 1 1 calc R . .
C106 C 0.4962(11) 0.3817(5) 0.7173(6) 0.045(4) Uani 1 1 d . . .
H10E H 0.4657 0.4139 0.7201 0.054 Uiso 1 1 calc R . .
C111 C 0.3751(10) 0.4137(5) 0.8153(5) 0.033(3) Uani 1 1 d . . .
C112 C 0.3307(10) 0.4511(5) 0.7838(5) 0.039(3) Uani 1 1 d . . .
H11A H 0.2986 0.4419 0.7512 0.046 Uiso 1 1 calc R . .
C113 C 0.3327(13) 0.5029(6) 0.7995(6) 0.055(4) Uani 1 1 d . . .
H11B H 0.3036 0.5283 0.7771 0.066 Uiso 1 1 calc R . .
C114 C 0.3776(12) 0.5165(6) 0.8480(6) 0.047(4) Uani 1 1 d . . .
H11C H 0.3777 0.5510 0.8591 0.056 Uiso 1 1 calc R . .
C115 C 0.4219(12) 0.4795(6) 0.8797(6) 0.049(4) Uani 1 1 d . . .
H11D H 0.4530 0.4886 0.9125 0.059 Uiso 1 1 calc R . .
C116 C 0.4213(10) 0.4275(5) 0.8633(5) 0.037(3) Uani 1 1 d . . .
H11E H 0.4525 0.4024 0.8851 0.045 Uiso 1 1 calc R . .
C201 C 0.1557(9) 0.2527(5) 0.9499(4) 0.023(3) Uani 1 1 d . . .
C202 C 0.1318(11) 0.2983(6) 0.9237(6) 0.046(4) Uani 1 1 d . . .
H20A H 0.1667 0.3083 0.8951 0.056 Uiso 1 1 calc R . .
C203 C 0.0565(12) 0.3293(6) 0.9396(7) 0.052(4) Uani 1 1 d . . .
H20B H 0.0420 0.3606 0.9223 0.062 Uiso 1 1 calc R . .
C204 C 0.0047(10) 0.3149(5) 0.9792(6) 0.037(3) Uani 1 1 d . . .
H20C H -0.0459 0.3364 0.9894 0.044 Uiso 1 1 calc R . .
C205 C 0.0242(10) 0.2682(6) 1.0062(5) 0.040(3) Uani 1 1 d . . .
H20D H -0.0133 0.2587 1.0339 0.048 Uiso 1 1 calc R . .
C206 C 0.0978(10) 0.2370(6) 0.9917(5) 0.035(3) Uani 1 1 d . . .
H20E H 0.1105 0.2055 1.0089 0.042 Uiso 1 1 calc R . .
C211 C 0.2945(9) 0.1709(5) 0.9852(5) 0.024(3) Uani 1 1 d . . .
C212 C 0.3216(10) 0.1936(5) 1.0330(5) 0.033(3) Uani 1 1 d . . .
H21B H 0.3143 0.2293 1.0365 0.040 Uiso 1 1 calc R . .
C213 C 0.3592(10) 0.1654(5) 1.0758(5) 0.030(3) Uani 1 1 d . . .
H21C H 0.3775 0.1817 1.1078 0.036 Uiso 1 1 calc R . .
C214 C 0.3692(11) 0.1129(6) 1.0705(5) 0.039(3) Uani 1 1 d . . .
H21D H 0.3964 0.0937 1.0992 0.047 Uiso 1 1 calc R . .
C215 C 0.3402(11) 0.0876(5) 1.0237(5) 0.043(4) Uani 1 1 d . . .
H21E H 0.3449 0.0516 1.0214 0.051 Uiso 1 1 calc R . .
C216 C 0.3038(10) 0.1167(6) 0.9800(5) 0.038(3) Uani 1 1 d . . .
H21F H 0.2859 0.1005 0.9479 0.045 Uiso 1 1 calc R . .
C301 C 0.0279(10) 0.3286(5) 0.6544(5) 0.032(3) Uiso 1 1 d . . .
C302 C -0.0698(12) 0.3282(6) 0.6303(6) 0.047(4) Uiso 1 1 d . . .
H30A H -0.1214 0.3118 0.6461 0.057 Uiso 1 1 calc R . .
C303 C -0.0862(16) 0.3541(8) 0.5808(8) 0.073(5) Uiso 1 1 d . . .
H30B H -0.1500 0.3552 0.5638 0.088 Uiso 1 1 calc R . .
C304 C -0.0101(14) 0.3771(8) 0.5581(8) 0.071(5) Uiso 1 1 d . . .
H30C H -0.0228 0.3937 0.5256 0.085 Uiso 1 1 calc R . .
C305 C 0.0850(14) 0.3769(7) 0.5814(7) 0.061(5) Uiso 1 1 d . . .
H30D H 0.1365 0.3926 0.5649 0.074 Uiso 1 1 calc R . .
C306 C 0.1029(11) 0.3529(5) 0.6298(5) 0.040(3) Uiso 1 1 d . . .
H30E H 0.1671 0.3532 0.6463 0.048 Uiso 1 1 calc R . .
C311 C -0.0422(10) 0.3028(5) 0.7603(5) 0.037(3) Uiso 1 1 d . . .
C312 C -0.0374(13) 0.2731(7) 0.8040(6) 0.056(4) Uiso 1 1 d . . .
H31B H 0.0169 0.2513 0.8117 0.067 Uiso 1 1 calc R . .
C313 C -0.1141(16) 0.2750(9) 0.8376(9) 0.084(6) Uiso 1 1 d . . .
H31C H -0.1131 0.2530 0.8668 0.101 Uiso 1 1 calc R . .
C314 C -0.1873(16) 0.3076(8) 0.8282(8) 0.080(6) Uiso 1 1 d . . .
H31D H -0.2378 0.3083 0.8512 0.096 Uiso 1 1 calc R . .
C315 C -0.1930(14) 0.3400(7) 0.7872(7) 0.065(5) Uiso 1 1 d . . .
H31E H -0.2460 0.3630 0.7820 0.078 Uiso 1 1 calc R . .
C316 C -0.1158(13) 0.3389(7) 0.7509(7) 0.060(5) Uiso 1 1 d . . .
H31F H -0.1161 0.3617 0.7224 0.072 Uiso 1 1 calc R . .
C401 C 0.0411(10) 0.0512(5) 0.7940(5) 0.037(3) Uiso 1 1 d . . .
C402 C 0.0567(18) -0.0007(9) 0.7866(9) 0.090(7) Uiso 1 1 d . . .
H40A H 0.1186 -0.0120 0.7774 0.108 Uiso 1 1 calc R . .
C403 C -0.0172(17) -0.0361(10) 0.7925(8) 0.090(7) Uiso 1 1 d . . .
H40B H -0.0063 -0.0711 0.7861 0.108 Uiso 1 1 calc R . .
C404 C -0.1042(16) -0.0204(8) 0.8072(8) 0.078(6) Uiso 1 1 d . . .
H40C H -0.1520 -0.0453 0.8134 0.093 Uiso 1 1 calc R . .
C405 C -0.1271(15) 0.0304(8) 0.8138(7) 0.071(5) Uiso 1 1 d . . .
H40D H -0.1895 0.0406 0.8234 0.085 Uiso 1 1 calc R . .
C406 C -0.0508(13) 0.0678(7) 0.8054(7) 0.061(5) Uiso 1 1 d . . .
H40E H -0.0641 0.1031 0.8078 0.073 Uiso 1 1 calc R . .
C411 C 0.2317(10) 0.0681(6) 0.7538(5) 0.038(3) Uiso 1 1 d . . .
C412 C 0.2917(14) 0.0337(7) 0.7845(8) 0.069(5) Uiso 1 1 d . . .
H41A H 0.2844 0.0297 0.8204 0.083 Uiso 1 1 calc R . .
C413 C 0.3633(16) 0.0054(9) 0.7595(9) 0.086(6) Uiso 1 1 d . . .
H41B H 0.4008 -0.0192 0.7791 0.104 Uiso 1 1 calc R . .
C414 C 0.3803(14) 0.0121(8) 0.7094(7) 0.069(5) Uiso 1 1 d . . .
H41C H 0.4286 -0.0076 0.6942 0.083 Uiso 1 1 calc R . .
C415 C 0.3274(14) 0.0472(7) 0.6808(8) 0.068(5) Uiso 1 1 d . . .
H41D H 0.3405 0.0528 0.6458 0.082 Uiso 1 1 calc R . .
C416 C 0.2514(12) 0.0763(6) 0.7028(6) 0.051(4) Uiso 1 1 d . . .
H41E H 0.2153 0.1009 0.6823 0.061 Uiso 1 1 calc R . .


_geom_special_details            
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C11 1.998(12) . ?
Pt1 C21 2.004(10) . ?
Pt1 P3 2.297(3) . ?
Pt1 P1 2.300(3) . ?
Pt1 Ag3 2.8830(11) . ?
Pt2 C31 1.998(11) . ?
Pt2 C41 2.000(12) . ?
Pt2 P2 2.295(3) . ?
Pt2 P4 2.311(3) . ?
Pt2 Ag3 2.9542(11) . ?
Ag3 C21 2.274(12) . ?
Ag3 C31 2.285(11) . ?
Ag3 C32 2.553(13) . ?
Ag3 N1 2.582(10) . ?
Ag3 C22 2.702(12) . ?
P1 C101 1.816(13) . ?
P1 C111 1.828(14) . ?
P1 C56 1.831(12) . ?
P2 C211 1.820(12) . ?
P2 C201 1.831(11) . ?
P2 C52 1.856(13) . ?
P3 C301 1.823(13) . ?
P3 C311 1.839(14) . ?
P3 C65 1.855(13) . ?
P4 C411 1.819(14) . ?
P4 C401 1.838(14) . ?
P4 C61 1.857(13) . ?
Cl1 O1 1.330(15) . ?
Cl1 O2 1.367(16) . ?
Cl1 O4 1.39(2) . ?
Cl1 O3 1.393(13) . ?
Cl2 C01 1.72(2) . ?
Cl3 C01 1.74(2) . ?
Cl6 C02 1.712(19) . ?
Cl7 C02 1.690(19) . ?
Cl8 C03 1.75(4) . ?
Cl9 C03 1.75(3) . ?
Cl9 Cl9 2.05(3) 3_566 ?
N1 C61 1.326(15) . ?
N1 C65 1.332(15) . ?
N2 C56 1.352(14) . ?
N2 C52 1.357(15) . ?
C01 H01A 0.9700 . ?
C01 H01B 0.9700 . ?
C02 H02A 0.9700 . ?
C02 H02B 0.9700 . ?
C03 H03A 0.9700 . ?
C03 H03B 0.9700 . ?
C11 C12 1.180(17) . ?
C12 C13 1.442(18) . ?
C13 C18 1.37(2) . ?
C13 C14 1.37(2) . ?
C14 C15 1.40(2) . ?
C14 H14A 0.9300 . ?
C15 C16 1.33(2) . ?
C15 H15A 0.9300 . ?
C16 C17 1.39(3) . ?
C16 C19 1.51(2) . ?
C17 C18 1.39(2) . ?
C17 H17A 0.9300 . ?
C18 H18A 0.9300 . ?
C19 H19A 0.9600 . ?
C19 H19B 0.9600 . ?
C19 H19C 0.9600 . ?
C21 C22 1.209(9) . ?
C22 C23 1.464(15) . ?
C23 C24 1.358(18) . ?
C23 C28 1.445(17) . ?
C24 C25 1.38(2) . ?
C24 H24A 0.9300 . ?
C25 C26 1.34(2) . ?
C25 H25A 0.9300 . ?
C26 C27 1.44(2) . ?
C26 C29 1.50(2) . ?
C27 C28 1.358(19) . ?
C27 H27A 0.9300 . ?
C28 H28A 0.9300 . ?
C29 H29A 0.9600 . ?
C29 H29B 0.9600 . ?
C29 H29C 0.9600 . ?
C31 C32 1.214(17) . ?
C32 C33 1.465(18) . ?
C33 C34 1.387(19) . ?
C33 C38 1.412(17) . ?
C34 C35 1.35(2) . ?
C34 H34A 0.9300 . ?
C35 C36 1.38(2) . ?
C35 H35A 0.9300 . ?
C36 C37 1.39(2) . ?
C36 C39 1.496(19) . ?
C37 C38 1.375(18) . ?
C37 H37A 0.9300 . ?
C38 H38A 0.9300 . ?
C39 H39A 0.9600 . ?
C39 H39B 0.9600 . ?
C39 H39C 0.9600 . ?
C41 C42 1.215(18) . ?
C42 C43 1.44(2) . ?
C43 C44 1.36(2) . ?
C43 C48 1.39(2) . ?
C44 C45 1.42(2) . ?
C44 H44A 0.9300 . ?
C45 C46 1.35(2) . ?
C45 H45A 0.9300 . ?
C46 C47 1.42(2) . ?
C46 C49 1.53(2) . ?
C47 C48 1.37(2) . ?
C47 H47A 0.9300 . ?
C48 H48A 0.9300 . ?
C49 H49A 0.9600 . ?
C49 H49B 0.9600 . ?
C49 H49C 0.9600 . ?
C52 C53 1.374(17) . ?
C53 C54 1.397(19) . ?
C53 H53A 0.9300 . ?
C54 C55 1.362(18) . ?
C54 H54A 0.9300 . ?
C55 C56 1.400(17) . ?
C55 H55A 0.9300 . ?
C61 C62 1.392(17) . ?
C62 C63 1.354(18) . ?
C62 H62A 0.9300 . ?
C63 C64 1.379(18) . ?
C63 H63A 0.9300 . ?
C64 C65 1.398(17) . ?
C64 H64A 0.9300 . ?
C101 C102 1.381(18) . ?
C101 C106 1.404(18) . ?
C102 C103 1.386(19) . ?
C102 H10A 0.9300 . ?
C103 C104 1.35(2) . ?
C103 H10B 0.9300 . ?
C104 C105 1.36(2) . ?
C104 H10C 0.9300 . ?
C105 C106 1.40(2) . ?
C105 H10D 0.9300 . ?
C106 H10E 0.9300 . ?
C111 C112 1.359(18) . ?
C111 C116 1.368(18) . ?
C112 C113 1.39(2) . ?
C112 H11A 0.9300 . ?
C113 C114 1.37(2) . ?
C113 H11B 0.9300 . ?
C114 C115 1.35(2) . ?
C114 H11C 0.9300 . ?
C115 C116 1.400(19) . ?
C115 H11D 0.9300 . ?
C116 H11E 0.9300 . ?
C201 C202 1.374(18) . ?
C201 C206 1.422(17) . ?
C202 C203 1.37(2) . ?
C202 H20A 0.9300 . ?
C203 C204 1.32(2) . ?
C203 H20B 0.9300 . ?
C204 C205 1.398(19) . ?
C204 H20C 0.9300 . ?
C205 C206 1.348(18) . ?
C205 H20D 0.9300 . ?
C206 H20E 0.9300 . ?
C211 C212 1.367(17) . ?
C211 C216 1.409(18) . ?
C212 C213 1.366(18) . ?
C212 H21B 0.9300 . ?
C213 C214 1.365(18) . ?
C213 H21C 0.9300 . ?
C214 C215 1.382(19) . ?
C214 H21D 0.9300 . ?
C215 C216 1.392(18) . ?
C215 H21E 0.9300 . ?
C216 H21F 0.9300 . ?
C301 C306 1.379(19) . ?
C301 C302 1.41(2) . ?
C302 C303 1.42(2) . ?
C302 H30A 0.9300 . ?
C303 C304 1.35(3) . ?
C303 H30B 0.9300 . ?
C304 C305 1.37(2) . ?
C304 H30C 0.9300 . ?
C305 C306 1.38(2) . ?
C305 H30D 0.9300 . ?
C306 H30E 0.9300 . ?
C311 C312 1.34(2) . ?
C311 C316 1.36(2) . ?
C312 C313 1.39(3) . ?
C312 H31B 0.9300 . ?
C313 C314 1.30(3) . ?
C313 H31C 0.9300 . ?
C314 C315 1.33(3) . ?
C314 H31D 0.9300 . ?
C315 C316 1.44(2) . ?
C315 H31E 0.9300 . ?
C316 H31F 0.9300 . ?
C401 C406 1.36(2) . ?
C401 C402 1.37(2) . ?
C402 C403 1.37(3) . ?
C402 H40A 0.9300 . ?
C403 C404 1.32(3) . ?
C403 H40B 0.9300 . ?
C404 C405 1.36(3) . ?
C404 H40C 0.9300 . ?
C405 C406 1.43(2) . ?
C405 H40D 0.9300 . ?
C406 H40E 0.9300 . ?
C411 C416 1.355(19) . ?
C411 C412 1.39(2) . ?
C412 C413 1.40(3) . ?
C412 H41A 0.9300 . ?
C413 C414 1.32(3) . ?
C413 H41B 0.9300 . ?
C414 C415 1.33(2) . ?
C414 H41C 0.9300 . ?
C415 C416 1.42(2) . ?
C415 H41D 0.9300 . ?
C416 H41E 0.9300 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C11 Pt1 C21 177.3(5) . . ?
C11 Pt1 P3 89.6(4) . . ?
C21 Pt1 P3 88.4(3) . . ?
C11 Pt1 P1 89.5(4) . . ?
C21 Pt1 P1 92.5(3) . . ?
P3 Pt1 P1 178.90(12) . . ?
C11 Pt1 Ag3 130.1(4) . . ?
C21 Pt1 Ag3 51.7(3) . . ?
P3 Pt1 Ag3 91.13(8) . . ?
P1 Pt1 Ag3 88.92(8) . . ?
C31 Pt2 C41 176.7(5) . . ?
C31 Pt2 P2 87.8(3) . . ?
C41 Pt2 P2 90.4(4) . . ?
C31 Pt2 P4 90.2(3) . . ?
C41 Pt2 P4 91.8(4) . . ?
P2 Pt2 P4 176.31(11) . . ?
C31 Pt2 Ag3 50.6(3) . . ?
C41 Pt2 Ag3 132.4(4) . . ?
P2 Pt2 Ag3 95.23(8) . . ?
P4 Pt2 Ag3 81.11(9) . . ?
C21 Ag3 C31 158.2(4) . . ?
C21 Ag3 C32 129.9(4) . . ?
C31 Ag3 C32 28.4(4) . . ?
C21 Ag3 N1 86.8(4) . . ?
C31 Ag3 N1 109.5(4) . . ?
C32 Ag3 N1 130.6(4) . . ?
C21 Ag3 C22 26.4(2) . . ?
C31 Ag3 C22 137.6(4) . . ?
C32 Ag3 C22 113.7(4) . . ?
N1 Ag3 C22 84.5(3) . . ?
C21 Ag3 Pt1 43.8(3) . . ?
C31 Ag3 Pt1 148.4(3) . . ?
C32 Ag3 Pt1 144.1(3) . . ?
N1 Ag3 Pt1 84.8(2) . . ?
C22 Ag3 Pt1 69.9(2) . . ?
C21 Ag3 Pt2 159.1(3) . . ?
C31 Ag3 Pt2 42.5(3) . . ?
C32 Ag3 Pt2 70.8(3) . . ?
N1 Ag3 Pt2 74.9(2) . . ?
C22 Ag3 Pt2 154.0(3) . . ?
Pt1 Ag3 Pt2 122.66(4) . . ?
C101 P1 C111 105.0(6) . . ?
C101 P1 C56 102.9(6) . . ?
C111 P1 C56 106.3(6) . . ?
C101 P1 Pt1 115.9(4) . . ?
C111 P1 Pt1 115.8(5) . . ?
C56 P1 Pt1 109.8(4) . . ?
C211 P2 C201 105.5(5) . . ?
C211 P2 C52 103.6(6) . . ?
C201 P2 C52 104.1(6) . . ?
C211 P2 Pt2 112.7(4) . . ?
C201 P2 Pt2 116.6(4) . . ?
C52 P2 Pt2 113.2(4) . . ?
C301 P3 C311 109.3(6) . . ?
C301 P3 C65 105.5(6) . . ?
C311 P3 C65 99.8(6) . . ?
C301 P3 Pt1 111.0(4) . . ?
C311 P3 Pt1 115.5(5) . . ?
C65 P3 Pt1 114.8(4) . . ?
C411 P4 C401 103.4(6) . . ?
C411 P4 C61 103.2(6) . . ?
C401 P4 C61 102.1(6) . . ?
C411 P4 Pt2 116.0(5) . . ?
C401 P4 Pt2 119.4(4) . . ?
C61 P4 Pt2 110.7(4) . . ?
O1 Cl1 O2 111.1(15) . . ?
O1 Cl1 O4 106.4(16) . . ?
O2 Cl1 O4 105.5(15) . . ?
O1 Cl1 O3 109.9(11) . . ?
O2 Cl1 O3 110.1(10) . . ?
O4 Cl1 O3 113.8(14) . . ?
C03 Cl9 Cl9 119.1(18) . 3_566 ?
C61 N1 C65 117.6(10) . . ?
C61 N1 Ag3 113.3(8) . . ?
C65 N1 Ag3 116.6(7) . . ?
C56 N2 C52 117.6(10) . . ?
Cl2 C01 Cl3 112.5(12) . . ?
Cl2 C01 H01A 109.1 . . ?
Cl3 C01 H01A 109.1 . . ?
Cl2 C01 H01B 109.1 . . ?
Cl3 C01 H01B 109.1 . . ?
H01A C01 H01B 107.8 . . ?
Cl7 C02 Cl6 109.1(14) . . ?
Cl7 C02 H02A 109.9 . . ?
Cl6 C02 H02A 109.9 . . ?
Cl7 C02 H02B 109.9 . . ?
Cl6 C02 H02B 109.9 . . ?
H02A C02 H02B 108.3 . . ?
Cl9 C03 Cl8 110.9(17) . . ?
Cl9 C03 H03A 109.5 . . ?
Cl8 C03 H03A 109.5 . . ?
Cl9 C03 H03B 109.5 . . ?
Cl8 C03 H03B 109.5 . . ?
H03A C03 H03B 108.0 . . ?
C12 C11 Pt1 175.1(12) . . ?
C11 C12 C13 176.4(14) . . ?
C18 C13 C14 117.1(14) . . ?
C18 C13 C12 123.1(13) . . ?
C14 C13 C12 119.7(14) . . ?
C13 C14 C15 120.8(16) . . ?
C13 C14 H14A 119.6 . . ?
C15 C14 H14A 119.6 . . ?
C16 C15 C14 122.6(16) . . ?
C16 C15 H15A 118.7 . . ?
C14 C15 H15A 118.7 . . ?
C15 C16 C17 116.7(15) . . ?
C15 C16 C19 124.1(19) . . ?
C17 C16 C19 119.2(18) . . ?
C16 C17 C18 121.6(17) . . ?
C16 C17 H17A 119.2 . . ?
C18 C17 H17A 119.2 . . ?
C13 C18 C17 121.1(16) . . ?
C13 C18 H18A 119.5 . . ?
C17 C18 H18A 119.5 . . ?
C16 C19 H19A 109.5 . . ?
C16 C19 H19B 109.5 . . ?
H19A C19 H19B 109.5 . . ?
C16 C19 H19C 109.5 . . ?
H19A C19 H19C 109.5 . . ?
H19B C19 H19C 109.5 . . ?
C22 C21 Pt1 169.8(10) . . ?
C22 C21 Ag3 97.0(9) . . ?
Pt1 C21 Ag3 84.5(4) . . ?
C21 C22 C23 174.3(13) . . ?
C21 C22 Ag3 56.7(8) . . ?
C23 C22 Ag3 128.6(8) . . ?
C24 C23 C28 118.5(11) . . ?
C24 C23 C22 120.4(11) . . ?
C28 C23 C22 120.7(11) . . ?
C23 C24 C25 122.7(13) . . ?
C23 C24 H24A 118.6 . . ?
C25 C24 H24A 118.6 . . ?
C26 C25 C24 121.2(15) . . ?
C26 C25 H25A 119.4 . . ?
C24 C25 H25A 119.4 . . ?
C25 C26 C27 116.7(14) . . ?
C25 C26 C29 122.7(16) . . ?
C27 C26 C29 120.5(15) . . ?
C28 C27 C26 123.8(14) . . ?
C28 C27 H27A 118.1 . . ?
C26 C27 H27A 118.1 . . ?
C27 C28 C23 117.0(13) . . ?
C27 C28 H28A 121.5 . . ?
C23 C28 H28A 121.5 . . ?
C26 C29 H29A 109.5 . . ?
C26 C29 H29B 109.5 . . ?
H29A C29 H29B 109.5 . . ?
C26 C29 H29C 109.5 . . ?
H29A C29 H29C 109.5 . . ?
H29B C29 H29C 109.5 . . ?
C32 C31 Pt2 175.2(11) . . ?
C32 C31 Ag3 88.2(8) . . ?
Pt2 C31 Ag3 87.0(4) . . ?
C31 C32 C33 174.4(13) . . ?
C31 C32 Ag3 63.4(8) . . ?
C33 C32 Ag3 121.7(8) . . ?
C34 C33 C38 119.4(12) . . ?
C34 C33 C32 121.9(12) . . ?
C38 C33 C32 118.5(12) . . ?
C35 C34 C33 120.0(14) . . ?
C35 C34 H34A 120.0 . . ?
C33 C34 H34A 120.0 . . ?
C34 C35 C36 122.2(14) . . ?
C34 C35 H35A 118.9 . . ?
C36 C35 H35A 118.9 . . ?
C35 C36 C37 118.4(13) . . ?
C35 C36 C39 123.0(15) . . ?
C37 C36 C39 118.6(15) . . ?
C38 C37 C36 120.7(13) . . ?
C38 C37 H37A 119.6 . . ?
C36 C37 H37A 119.6 . . ?
C37 C38 C33 119.2(13) . . ?
C37 C38 H38A 120.4 . . ?
C33 C38 H38A 120.4 . . ?
C36 C39 H39A 109.5 . . ?
C36 C39 H39B 109.5 . . ?
H39A C39 H39B 109.5 . . ?
C36 C39 H39C 109.5 . . ?
H39A C39 H39C 109.5 . . ?
H39B C39 H39C 109.5 . . ?
C42 C41 Pt2 177.1(12) . . ?
C41 C42 C43 175.3(17) . . ?
C44 C43 C48 118.0(14) . . ?
C44 C43 C42 120.2(14) . . ?
C48 C43 C42 121.6(14) . . ?
C43 C44 C45 120.6(15) . . ?
C43 C44 H44A 119.7 . . ?
C45 C44 H44A 119.7 . . ?
C46 C45 C44 121.4(16) . . ?
C46 C45 H45A 119.3 . . ?
C44 C45 H45A 119.3 . . ?
C45 C46 C47 117.8(15) . . ?
C45 C46 C49 122.8(17) . . ?
C47 C46 C49 119.3(17) . . ?
C48 C47 C46 120.4(15) . . ?
C48 C47 H47A 119.8 . . ?
C46 C47 H47A 119.8 . . ?
C47 C48 C43 121.6(15) . . ?
C47 C48 H48A 119.2 . . ?
C43 C48 H48A 119.2 . . ?
C46 C49 H49A 109.5 . . ?
C46 C49 H49B 109.5 . . ?
H49A C49 H49B 109.5 . . ?
C46 C49 H49C 109.5 . . ?
H49A C49 H49C 109.5 . . ?
H49B C49 H49C 109.5 . . ?
N2 C52 C53 123.8(12) . . ?
N2 C52 P2 112.4(8) . . ?
C53 C52 P2 123.8(10) . . ?
C52 C53 C54 117.2(12) . . ?
C52 C53 H53A 121.4 . . ?
C54 C53 H53A 121.4 . . ?
C55 C54 C53 120.7(12) . . ?
C55 C54 H54A 119.7 . . ?
C53 C54 H54A 119.7 . . ?
C54 C55 C56 118.8(12) . . ?
C54 C55 H55A 120.6 . . ?
C56 C55 H55A 120.6 . . ?
N2 C56 C55 121.9(11) . . ?
N2 C56 P1 115.0(8) . . ?
C55 C56 P1 122.9(9) . . ?
N1 C61 C62 124.2(12) . . ?
N1 C61 P4 114.2(9) . . ?
C62 C61 P4 121.6(10) . . ?
C63 C62 C61 117.3(12) . . ?
C63 C62 H62A 121.4 . . ?
C61 C62 H62A 121.4 . . ?
C62 C63 C64 120.5(12) . . ?
C62 C63 H63A 119.8 . . ?
C64 C63 H63A 119.8 . . ?
C63 C64 C65 118.1(12) . . ?
C63 C64 H64A 121.0 . . ?
C65 C64 H64A 121.0 . . ?
N1 C65 C64 122.2(12) . . ?
N1 C65 P3 115.6(9) . . ?
C64 C65 P3 121.7(10) . . ?
C102 C101 C106 117.8(13) . . ?
C102 C101 P1 121.8(10) . . ?
C106 C101 P1 119.7(10) . . ?
C101 C102 C103 121.2(13) . . ?
C101 C102 H10A 119.4 . . ?
C103 C102 H10A 119.4 . . ?
C104 C103 C102 121.0(14) . . ?
C104 C103 H10B 119.5 . . ?
C102 C103 H10B 119.5 . . ?
C103 C104 C105 119.6(13) . . ?
C103 C104 H10C 120.2 . . ?
C105 C104 H10C 120.2 . . ?
C104 C105 C106 121.1(14) . . ?
C104 C105 H10D 119.4 . . ?
C106 C105 H10D 119.4 . . ?
C105 C106 C101 119.2(14) . . ?
C105 C106 H10E 120.4 . . ?
C101 C106 H10E 120.4 . . ?
C112 C111 C116 119.0(13) . . ?
C112 C111 P1 117.3(10) . . ?
C116 C111 P1 123.7(10) . . ?
C111 C112 C113 120.9(13) . . ?
C111 C112 H11A 119.5 . . ?
C113 C112 H11A 119.5 . . ?
C114 C113 C112 119.8(14) . . ?
C114 C113 H11B 120.1 . . ?
C112 C113 H11B 120.1 . . ?
C115 C114 C113 119.5(14) . . ?
C115 C114 H11C 120.2 . . ?
C113 C114 H11C 120.2 . . ?
C114 C115 C116 120.4(14) . . ?
C114 C115 H11D 119.8 . . ?
C116 C115 H11D 119.8 . . ?
C111 C116 C115 120.3(13) . . ?
C111 C116 H11E 119.9 . . ?
C115 C116 H11E 119.9 . . ?
C202 C201 C206 118.7(11) . . ?
C202 C201 P2 122.4(10) . . ?
C206 C201 P2 118.2(9) . . ?
C203 C202 C201 120.3(14) . . ?
C203 C202 H20A 119.9 . . ?
C201 C202 H20A 119.9 . . ?
C204 C203 C202 120.4(14) . . ?
C204 C203 H20B 119.8 . . ?
C202 C203 H20B 119.8 . . ?
C203 C204 C205 121.5(13) . . ?
C203 C204 H20C 119.2 . . ?
C205 C204 H20C 119.2 . . ?
C206 C205 C204 119.5(13) . . ?
C206 C205 H20D 120.2 . . ?
C204 C205 H20D 120.2 . . ?
C205 C206 C201 119.5(13) . . ?
C205 C206 H20E 120.3 . . ?
C201 C206 H20E 120.3 . . ?
C212 C211 C216 119.0(11) . . ?
C212 C211 P2 124.2(10) . . ?
C216 C211 P2 116.8(9) . . ?
C213 C212 C211 122.1(12) . . ?
C213 C212 H21B 118.9 . . ?
C211 C212 H21B 118.9 . . ?
C214 C213 C212 118.8(12) . . ?
C214 C213 H21C 120.6 . . ?
C212 C213 H21C 120.6 . . ?
C213 C214 C215 121.8(12) . . ?
C213 C214 H21D 119.1 . . ?
C215 C214 H21D 119.1 . . ?
C214 C215 C216 119.1(13) . . ?
C214 C215 H21E 120.5 . . ?
C216 C215 H21E 120.5 . . ?
C215 C216 C211 119.2(12) . . ?
C215 C216 H21F 120.4 . . ?
C211 C216 H21F 120.4 . . ?
C306 C301 C302 120.0(13) . . ?
C306 C301 P3 118.2(10) . . ?
C302 C301 P3 121.7(11) . . ?
C301 C302 C303 117.1(15) . . ?
C301 C302 H30A 121.5 . . ?
C303 C302 H30A 121.5 . . ?
C304 C303 C302 120.7(19) . . ?
C304 C303 H30B 119.7 . . ?
C302 C303 H30B 119.7 . . ?
C303 C304 C305 122.0(19) . . ?
C303 C304 H30C 119.0 . . ?
C305 C304 H30C 119.0 . . ?
C304 C305 C306 118.6(17) . . ?
C304 C305 H30D 120.7 . . ?
C306 C305 H30D 120.7 . . ?
C305 C306 C301 121.6(14) . . ?
C305 C306 H30E 119.2 . . ?
C301 C306 H30E 119.2 . . ?
C312 C311 C316 121.3(15) . . ?
C312 C311 P3 116.2(12) . . ?
C316 C311 P3 122.4(12) . . ?
C311 C312 C313 119.6(18) . . ?
C311 C312 H31B 120.2 . . ?
C313 C312 H31B 120.2 . . ?
C314 C313 C312 120(2) . . ?
C314 C313 H31C 120.0 . . ?
C312 C313 H31C 120.0 . . ?
C313 C314 C315 123(2) . . ?
C313 C314 H31D 118.6 . . ?
C315 C314 H31D 118.6 . . ?
C314 C315 C316 119.1(19) . . ?
C314 C315 H31E 120.4 . . ?
C316 C315 H31E 120.4 . . ?
C311 C316 C315 116.9(16) . . ?
C311 C316 H31F 121.6 . . ?
C315 C316 H31F 121.6 . . ?
C406 C401 C402 119.1(17) . . ?
C406 C401 P4 116.4(12) . . ?
C402 C401 P4 124.3(14) . . ?
C403 C402 C401 121(2) . . ?
C403 C402 H40A 119.5 . . ?
C401 C402 H40A 119.5 . . ?
C404 C403 C402 120(2) . . ?
C404 C403 H40B 120.1 . . ?
C402 C403 H40B 120.1 . . ?
C403 C404 C405 123(2) . . ?
C403 C404 H40C 118.5 . . ?
C405 C404 H40C 118.5 . . ?
C404 C405 C406 117.1(19) . . ?
C404 C405 H40D 121.4 . . ?
C406 C405 H40D 121.4 . . ?
C401 C406 C405 119.7(17) . . ?
C401 C406 H40E 120.2 . . ?
C405 C406 H40E 120.2 . . ?
C416 C411 C412 118.9(15) . . ?
C416 C411 P4 124.0(12) . . ?
C412 C411 P4 117.0(12) . . ?
C411 C412 C413 117.9(18) . . ?
C411 C412 H41A 121.1 . . ?
C413 C412 H41A 121.1 . . ?
C414 C413 C412 123(2) . . ?
C414 C413 H41B 118.4 . . ?
C412 C413 H41B 118.4 . . ?
C413 C414 C415 119(2) . . ?
C413 C414 H41C 120.5 . . ?
C415 C414 H41C 120.5 . . ?
C414 C415 C416 121.3(18) . . ?
C414 C415 H41D 119.3 . . ?
C416 C415 H41D 119.3 . . ?
C411 C416 C415 119.5(16) . . ?
C411 C416 H41E 120.2 . . ?
C415 C416 H41E 120.2 . . ?

_diffrn_measured_fraction_theta_max 1.000
_diffrn_reflns_theta_full        25.00
_diffrn_measured_fraction_theta_full 1.000
_refine_diff_density_max         2.113
_refine_diff_density_min         -1.730
_refine_diff_density_rms         0.223



#===END


_database_code_depnum_ccdc_archive 'CCDC 933748'
