# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2014

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#                                CCDC 
# 
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# 
#  This CIF contains data from an original supplementary publication
#  deposited with the CCDC, and may include chemical, crystal,
#  experimental, refinement, atomic coordinates,
#  anisotropic displacement parameters and molecular geometry data,
#  as required by the journal to which it was submitted.
#
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#  fide research purposes only. It may contain copyright material
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#  except for the purpose of generating routine backup copies
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data_Mo10N8Cl35AgC32H60
_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C32 H60 Ag Cl35 Mo10 N8'
_chemical_formula_weight         2864.90

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'C 1 2/c 1'

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'

_cell_length_a                   17.057(3)
_cell_length_b                   17.711(4)
_cell_length_c                   29.241(6)
_cell_angle_alpha                90.00
_cell_angle_beta                 104.59(3)
_cell_angle_gamma                90.00
_cell_volume                     8549(3)
_cell_formula_units_Z            4
_cell_measurement_temperature    200(2)
_cell_measurement_reflns_used    2061
_cell_measurement_theta_min      1.84
_cell_measurement_theta_max      29.60

_exptl_crystal_description       ?
_exptl_crystal_colour            red
_exptl_crystal_size_max          0.17
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.06
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    2.226
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             5480
_exptl_absorpt_coefficient_mu    2.763
_exptl_absorpt_correction_type   Numerical
_exptl_absorpt_correction_T_min  0.4626
_exptl_absorpt_correction_T_max  0.7440
_exptl_absorpt_process_details   
'(X-RED, Data Reduction Program, Version 1.14, Stoe & Cie GmbH, Darmstadt 1999.; X-SHAPE, Crystal Optimisation for Numerical Absorption Correction, Version 1.06, Stoe & Cie GmbH, Darmstadt 1999.)'

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      200(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  ?
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            38115
_diffrn_reflns_av_R_equivalents  0.0529
_diffrn_reflns_av_sigmaI/netI    0.0572
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_k_max       23
_diffrn_reflns_limit_l_min       -34
_diffrn_reflns_limit_l_max       38
_diffrn_reflns_theta_min         1.44
_diffrn_reflns_theta_max         28.33
_reflns_number_total             10641
_reflns_number_gt                6913
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'STOE X-AREA'
_computing_cell_refinement       'STOE X-AREA'
_computing_data_reduction        'STOE X-RED'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'DIAMOND, Crystal Impact'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0502P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     SHELXL
_refine_ls_extinction_coef       0.000245(16)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_number_reflns         10641
_refine_ls_number_parameters     395
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0748
_refine_ls_R_factor_gt           0.0409
_refine_ls_wR_factor_ref         0.0939
_refine_ls_wR_factor_gt          0.0849
_refine_ls_goodness_of_fit_ref   0.875
_refine_ls_restrained_S_all      0.875
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Mo1 Mo 0.45713(3) 0.32817(3) 0.393064(16) 0.04153(11) Uani 1 1 d . . .
Mo2 Mo 0.46451(3) -0.09826(3) 0.304365(15) 0.04128(11) Uani 1 1 d . . .
Mo3 Mo 0.43766(3) 0.18358(2) 0.413394(15) 0.04022(11) Uani 1 1 d . . .
Mo4 Mo 0.43383(3) -0.01196(3) 0.369467(15) 0.04087(11) Uani 1 1 d . . .
Mo5 Mo 0.48785(3) 0.44255(2) 0.293148(15) 0.03956(11) Uani 1 1 d . . .
Ag1 Ag 0.5000 0.0000 0.5000 0.0703(2) Uani 1 2 d S . .
Cl1 Cl 0.5000 0.32302(10) 0.2500 0.0432(4) Uani 1 2 d S . .
Cl2 Cl 0.33532(9) 0.09332(7) 0.36709(4) 0.0452(3) Uani 1 1 d . . .
Cl3 Cl 0.47826(10) 0.56353(8) 0.32553(5) 0.0523(3) Uani 1 1 d . . .
Cl4 Cl 0.59577(9) -0.10173(8) 0.28232(4) 0.0472(3) Uani 1 1 d . . .
Cl5 Cl 0.46528(9) 0.22301(7) 0.33892(4) 0.0453(3) Uani 1 1 d . . .
Cl6 Cl 0.57088(9) 0.39001(8) 0.36922(4) 0.0458(3) Uani 1 1 d . . .
Cl7 Cl 0.53407(8) 0.07693(7) 0.41870(4) 0.0434(3) Uani 1 1 d . . .
Cl8 Cl 0.54556(9) -0.10080(8) 0.38543(4) 0.0506(3) Uani 1 1 d . . .
Cl9 Cl 0.37368(9) 0.39972(7) 0.32525(5) 0.0454(3) Uani 1 1 d . . .
Cl10 Cl 0.33081(9) 0.27767(8) 0.40499(5) 0.0494(3) Uani 1 1 d . . .
Cl11 Cl 0.46967(10) 0.04184(7) 0.30024(4) 0.0478(3) Uani 1 1 d . . .
Cl12 Cl 0.55335(10) 0.25874(8) 0.45481(5) 0.0515(3) Uani 1 1 d . . .
Cl13 Cl 0.61683(9) 0.47241(8) 0.27758(4) 0.0475(3) Uani 1 1 d . . .
Cl14 Cl 0.32807(9) -0.08396(8) 0.31572(5) 0.0515(3) Uani 1 1 d . . .
Cl15 Cl 0.39293(10) -0.06621(8) 0.43538(5) 0.0511(3) Uani 1 1 d . . .
Cl16 Cl 0.41214(9) 0.14251(8) 0.48636(4) 0.0507(3) Uani 1 1 d . . .
Cl17 Cl 0.45430(10) -0.23070(8) 0.30918(5) 0.0537(3) Uani 1 1 d . . .
Cl18 Cl 0.45556(10) 0.42679(8) 0.44795(5) 0.0556(4) Uani 1 1 d . . .
N1 N 0.0590(3) 0.1577(3) 0.43599(16) 0.0540(12) Uani 1 1 d . . .
N2 N 0.1628(3) 0.0843(3) 0.44725(16) 0.0508(11) Uani 1 1 d . . .
N3 N 0.8023(3) 0.1893(3) 0.22796(18) 0.0560(12) Uani 1 1 d . . .
N4 N 0.7210(3) 0.1766(3) 0.27332(18) 0.0591(13) Uani 1 1 d . . .
C1 C 0.0843(4) 0.0861(4) 0.44042(19) 0.0557(15) Uani 1 1 d . . .
H1 H 0.0511 0.0441 0.4389 0.067 Uiso 1 1 calc R . .
C2 C 0.1245(5) 0.2034(4) 0.4397(2) 0.0687(19) Uani 1 1 d . . .
H2 H 0.1242 0.2558 0.4378 0.082 Uiso 1 1 calc R . .
C3 C 0.1899(5) 0.1577(4) 0.4467(2) 0.0631(17) Uani 1 1 d . . .
H3 H 0.2434 0.1729 0.4504 0.076 Uiso 1 1 calc R . .
C4 C 0.7803(4) 0.1435(4) 0.2582(2) 0.0610(16) Uani 1 1 d . . .
H4 H 0.8024 0.0962 0.2674 0.073 Uiso 1 1 calc R . .
C5 C 0.7572(4) 0.2536(4) 0.2239(2) 0.0606(16) Uani 1 1 d . . .
H5 H 0.7611 0.2952 0.2051 0.073 Uiso 1 1 calc R . .
C6 C 0.7065(4) 0.2462(4) 0.2518(2) 0.0643(17) Uani 1 1 d . . .
H6 H 0.6685 0.2815 0.2559 0.077 Uiso 1 1 calc R . .
C7 C 0.2197(5) -0.0171(4) 0.5054(3) 0.0693(19) Uani 1 1 d . . .
H7A H 0.1659 -0.0319 0.5075 0.083 Uiso 1 1 calc R . .
H7B H 0.2530 -0.0622 0.5094 0.083 Uiso 1 1 calc R . .
C8 C -0.0257(5) 0.1823(5) 0.4275(2) 0.079(2) Uani 1 1 d . . .
H8A H -0.0508 0.1811 0.3942 0.119 Uiso 1 1 calc R . .
H8B H -0.0275 0.2328 0.4391 0.119 Uiso 1 1 calc R . .
H8C H -0.0543 0.1490 0.4436 0.119 Uiso 1 1 calc R . .
C9 C 0.6821(5) 0.1950(5) 0.3487(3) 0.073(2) Uani 1 1 d . . .
H9A H 0.6557 0.2424 0.3376 0.088 Uiso 1 1 calc R . .
H9B H 0.6514 0.1715 0.3686 0.088 Uiso 1 1 calc R . .
C10 C 0.2140(5) 0.0160(4) 0.4563(3) 0.0677(18) Uani 1 1 d . . .
H10A H 0.2680 0.0285 0.4536 0.081 Uiso 1 1 calc R . .
H10B H 0.1917 -0.0218 0.4326 0.081 Uiso 1 1 calc R . .
C11 C 0.2550(5) 0.0374(4) 0.5450(2) 0.0685(19) Uani 1 1 d . . .
H11A H 0.2219 0.0826 0.5409 0.082 Uiso 1 1 calc R . .
H11B H 0.3089 0.0520 0.5430 0.082 Uiso 1 1 calc R . .
C12 C 0.8658(5) 0.1754(4) 0.2034(3) 0.0689(18) Uani 1 1 d . . .
H12A H 0.9072 0.1442 0.2228 0.103 Uiso 1 1 calc R . .
H12B H 0.8890 0.2226 0.1974 0.103 Uiso 1 1 calc R . .
H12C H 0.8430 0.1502 0.1740 0.103 Uiso 1 1 calc R . .
C13 C 0.6774(5) 0.1447(5) 0.3065(3) 0.075(2) Uani 1 1 d . . .
H13A H 0.7003 0.0957 0.3172 0.089 Uiso 1 1 calc R . .
H13B H 0.6210 0.1372 0.2900 0.089 Uiso 1 1 calc R . .
C14 C 0.7653(5) 0.2119(5) 0.3785(3) 0.077(2) Uani 1 1 d . . .
H14A H 0.7941 0.2414 0.3600 0.092 Uiso 1 1 calc R . .
H14B H 0.7944 0.1647 0.3867 0.092 Uiso 1 1 calc R . .
C15 C 0.2603(5) 0.0043(6) 0.5944(3) 0.092(3) Uani 1 1 d . . .
H15A H 0.2076 -0.0126 0.5962 0.139 Uiso 1 1 calc R . .
H15B H 0.2793 0.0424 0.6180 0.139 Uiso 1 1 calc R . .
H15C H 0.2972 -0.0376 0.6000 0.139 Uiso 1 1 calc R . .
C16 C 0.7656(6) 0.2545(6) 0.4235(3) 0.095(3) Uani 1 1 d . . .
H16A H 0.7346 0.3001 0.4158 0.143 Uiso 1 1 calc R . .
H16B H 0.8203 0.2668 0.4398 0.143 Uiso 1 1 calc R . .
H16C H 0.7419 0.2235 0.4434 0.143 Uiso 1 1 calc R . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Mo1 Cl18 2.3768(14) . ?
Mo1 Cl10 2.4378(15) . ?
Mo1 Cl12 2.4438(17) . ?
Mo1 Cl5 2.4710(14) . ?
Mo1 Cl6 2.4763(15) . ?
Mo1 Cl9 2.4783(16) . ?
Mo1 Mo3 2.6684(8) . ?
Mo2 Cl17 2.3590(15) . ?
Mo2 Cl8 2.4251(16) . ?
Mo2 Cl14 2.4455(16) . ?
Mo2 Cl4 2.4817(15) . ?
Mo2 Cl4 2.4845(15) 2_655 ?
Mo2 Cl11 2.4869(15) . ?
Mo2 Mo4 2.5953(7) . ?
Mo3 Cl16 2.3955(13) . ?
Mo3 Cl12 2.4349(17) . ?
Mo3 Cl10 2.4358(15) . ?
Mo3 Cl5 2.4432(13) . ?
Mo3 Cl7 2.4835(14) . ?
Mo3 Cl2 2.4991(16) . ?
Mo4 Cl15 2.4085(14) . ?
Mo4 Cl8 2.4244(16) . ?
Mo4 Cl14 2.4335(17) . ?
Mo4 Cl11 2.4500(13) . ?
Mo4 Cl7 2.4970(15) . ?
Mo4 Cl2 2.4993(15) . ?
Mo5 Cl3 2.3647(14) . ?
Mo5 Cl13 2.4150(15) . ?
Mo5 Cl13 2.4258(17) 2_655 ?
Mo5 Cl9 2.4839(14) . ?
Mo5 Cl6 2.4965(16) . ?
Mo5 Cl1 2.4996(16) . ?
Mo5 Mo5 2.6583(10) 2_655 ?
Ag1 Cl15 2.5578(17) . ?
Ag1 Cl15 2.5578(17) 5_656 ?
Ag1 Cl16 2.9111(15) . ?
Ag1 Cl16 2.9111(15) 5_656 ?
Ag1 Cl7 2.9226(13) . ?
Ag1 Cl7 2.9226(13) 5_656 ?
Cl1 Mo5 2.4996(16) 2_655 ?
Cl4 Mo2 2.4845(15) 2_655 ?
Cl13 Mo5 2.4258(17) 2_655 ?
N1 C1 1.335(8) . ?
N1 C2 1.362(9) . ?
N1 C8 1.469(9) . ?
N2 C1 1.303(8) . ?
N2 C3 1.381(8) . ?
N2 C10 1.478(8) . ?
N3 C4 1.320(8) . ?
N3 C5 1.363(8) . ?
N3 C12 1.464(8) . ?
N4 C4 1.338(8) . ?
N4 C6 1.378(8) . ?
N4 C13 1.475(8) . ?
C2 C3 1.353(10) . ?
C5 C6 1.336(9) . ?
C7 C11 1.512(10) . ?
C7 C10 1.530(9) . ?
C9 C14 1.497(10) . ?
C9 C13 1.509(10) . ?
C11 C15 1.541(9) . ?
C14 C16 1.516(11) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Cl18 Mo1 Cl10 90.71(6) . . ?
Cl18 Mo1 Cl12 89.46(6) . . ?
Cl10 Mo1 Cl12 99.38(5) . . ?
Cl18 Mo1 Cl5 176.98(6) . . ?
Cl10 Mo1 Cl5 90.55(5) . . ?
Cl12 Mo1 Cl5 87.62(5) . . ?
Cl18 Mo1 Cl6 90.45(5) . . ?
Cl10 Mo1 Cl6 170.41(5) . . ?
Cl12 Mo1 Cl6 90.15(5) . . ?
Cl5 Mo1 Cl6 88.77(5) . . ?
Cl18 Mo1 Cl9 93.59(6) . . ?
Cl10 Mo1 Cl9 87.24(5) . . ?
Cl12 Mo1 Cl9 172.68(5) . . ?
Cl5 Mo1 Cl9 89.22(5) . . ?
Cl6 Mo1 Cl9 83.19(5) . . ?
Cl18 Mo1 Mo3 122.12(4) . . ?
Cl10 Mo1 Mo3 56.77(4) . . ?
Cl12 Mo1 Mo3 56.68(4) . . ?
Cl5 Mo1 Mo3 56.61(3) . . ?
Cl6 Mo1 Mo3 129.61(4) . . ?
Cl9 Mo1 Mo3 126.18(4) . . ?
Cl17 Mo2 Cl8 87.46(5) . . ?
Cl17 Mo2 Cl14 90.44(6) . . ?
Cl8 Mo2 Cl14 101.36(6) . . ?
Cl17 Mo2 Cl4 94.35(5) . . ?
Cl8 Mo2 Cl4 85.64(5) . . ?
Cl14 Mo2 Cl4 171.70(5) . . ?
Cl17 Mo2 Cl4 91.06(5) . 2_655 ?
Cl8 Mo2 Cl4 169.82(5) . 2_655 ?
Cl14 Mo2 Cl4 88.72(6) . 2_655 ?
Cl4 Mo2 Cl4 84.43(6) . 2_655 ?
Cl17 Mo2 Cl11 177.54(6) . . ?
Cl8 Mo2 Cl11 92.72(5) . . ?
Cl14 Mo2 Cl11 87.12(5) . . ?
Cl4 Mo2 Cl11 88.10(5) . . ?
Cl4 Mo2 Cl11 89.19(5) 2_655 . ?
Cl17 Mo2 Mo4 120.68(4) . . ?
Cl8 Mo2 Mo4 57.63(4) . . ?
Cl14 Mo2 Mo4 57.64(4) . . ?
Cl4 Mo2 Mo4 124.53(4) . . ?
Cl4 Mo2 Mo4 130.90(4) 2_655 . ?
Cl11 Mo2 Mo4 57.59(3) . . ?
Cl16 Mo3 Cl12 91.68(6) . . ?
Cl16 Mo3 Cl10 89.91(5) . . ?
Cl12 Mo3 Cl10 99.68(6) . . ?
Cl16 Mo3 Cl5 178.79(5) . . ?
Cl12 Mo3 Cl5 88.45(5) . . ?
Cl10 Mo3 Cl5 91.26(5) . . ?
Cl16 Mo3 Cl7 88.82(5) . . ?
Cl12 Mo3 Cl7 86.77(5) . . ?
Cl10 Mo3 Cl7 173.45(5) . . ?
Cl5 Mo3 Cl7 89.98(5) . . ?
Cl16 Mo3 Cl2 91.69(5) . . ?
Cl12 Mo3 Cl2 170.81(5) . . ?
Cl10 Mo3 Cl2 88.87(5) . . ?
Cl5 Mo3 Cl2 88.00(5) . . ?
Cl7 Mo3 Cl2 84.75(5) . . ?
Cl16 Mo3 Mo1 123.41(4) . . ?
Cl12 Mo3 Mo1 57.00(4) . . ?
Cl10 Mo3 Mo1 56.84(4) . . ?
Cl5 Mo3 Mo1 57.61(3) . . ?
Cl7 Mo3 Mo1 128.77(4) . . ?
Cl2 Mo3 Mo1 127.04(4) . . ?
Cl15 Mo4 Cl8 87.66(5) . . ?
Cl15 Mo4 Cl14 89.47(6) . . ?
Cl8 Mo4 Cl14 101.72(6) . . ?
Cl15 Mo4 Cl11 177.53(6) . . ?
Cl8 Mo4 Cl11 93.66(5) . . ?
Cl14 Mo4 Cl11 88.22(5) . . ?
Cl15 Mo4 Cl7 94.84(5) . . ?
Cl8 Mo4 Cl7 84.68(5) . . ?
Cl14 Mo4 Cl7 172.44(5) . . ?
Cl11 Mo4 Cl7 87.36(5) . . ?
Cl15 Mo4 Cl2 89.52(5) . . ?
Cl8 Mo4 Cl2 168.51(5) . . ?
Cl14 Mo4 Cl2 89.38(5) . . ?
Cl11 Mo4 Cl2 89.59(5) . . ?
Cl7 Mo4 Cl2 84.47(5) . . ?
Cl15 Mo4 Mo2 120.30(4) . . ?
Cl8 Mo4 Mo2 57.66(4) . . ?
Cl14 Mo4 Mo2 58.09(4) . . ?
Cl11 Mo4 Mo2 58.98(4) . . ?
Cl7 Mo4 Mo2 123.98(4) . . ?
Cl2 Mo4 Mo2 132.64(4) . . ?
Cl3 Mo5 Cl13 92.02(5) . . ?
Cl3 Mo5 Cl13 91.92(5) . 2_655 ?
Cl13 Mo5 Cl13 107.54(5) . 2_655 ?
Cl3 Mo5 Cl9 89.17(5) . . ?
Cl13 Mo5 Cl9 167.51(5) . . ?
Cl13 Mo5 Cl9 84.84(5) 2_655 . ?
Cl3 Mo5 Cl6 93.55(5) . . ?
Cl13 Mo5 Cl6 84.85(5) . . ?
Cl13 Mo5 Cl6 166.27(5) 2_655 . ?
Cl9 Mo5 Cl6 82.66(5) . . ?
Cl3 Mo5 Cl1 172.91(4) . . ?
Cl13 Mo5 Cl1 83.97(4) . . ?
Cl13 Mo5 Cl1 83.75(4) 2_655 . ?
Cl9 Mo5 Cl1 96.01(4) . . ?
Cl6 Mo5 Cl1 91.92(4) . . ?
Cl3 Mo5 Mo5 115.03(4) . 2_655 ?
Cl13 Mo5 Mo5 56.89(4) . 2_655 ?
Cl13 Mo5 Mo5 56.50(4) 2_655 2_655 ?
Cl9 Mo5 Mo5 133.10(5) . 2_655 ?
Cl6 Mo5 Mo5 131.05(4) . 2_655 ?
Cl1 Mo5 Mo5 57.88(2) . 2_655 ?
Cl15 Ag1 Cl15 180.00(5) . 5_656 ?
Cl15 Ag1 Cl16 92.82(5) . . ?
Cl15 Ag1 Cl16 87.18(5) 5_656 . ?
Cl15 Ag1 Cl16 87.18(5) . 5_656 ?
Cl15 Ag1 Cl16 92.82(5) 5_656 5_656 ?
Cl16 Ag1 Cl16 180.0 . 5_656 ?
Cl15 Ag1 Cl7 82.19(4) . . ?
Cl15 Ag1 Cl7 97.81(4) 5_656 . ?
Cl16 Ag1 Cl7 71.66(4) . . ?
Cl16 Ag1 Cl7 108.34(4) 5_656 . ?
Cl15 Ag1 Cl7 97.81(4) . 5_656 ?
Cl15 Ag1 Cl7 82.19(4) 5_656 5_656 ?
Cl16 Ag1 Cl7 108.34(4) . 5_656 ?
Cl16 Ag1 Cl7 71.66(4) 5_656 5_656 ?
Cl7 Ag1 Cl7 180.0 . 5_656 ?
Mo5 Cl1 Mo5 64.25(5) 2_655 . ?
Mo3 Cl2 Mo4 95.12(5) . . ?
Mo2 Cl4 Mo2 95.50(6) . 2_655 ?
Mo3 Cl5 Mo1 65.77(4) . . ?
Mo1 Cl6 Mo5 96.13(6) . . ?
Mo3 Cl7 Mo4 95.57(5) . . ?
Mo3 Cl7 Ag1 98.12(4) . . ?
Mo4 Cl7 Ag1 85.84(4) . . ?
Mo4 Cl8 Mo2 64.71(4) . . ?
Mo1 Cl9 Mo5 96.41(5) . . ?
Mo3 Cl10 Mo1 66.40(4) . . ?
Mo4 Cl11 Mo2 63.43(3) . . ?
Mo3 Cl12 Mo1 66.32(5) . . ?
Mo5 Cl13 Mo5 66.62(5) . 2_655 ?
Mo4 Cl14 Mo2 64.27(4) . . ?
Mo4 Cl15 Ag1 96.40(5) . . ?
Mo3 Cl16 Ag1 100.52(5) . . ?
C1 N1 C2 108.5(6) . . ?
C1 N1 C8 125.3(6) . . ?
C2 N1 C8 126.2(6) . . ?
C1 N2 C3 108.1(6) . . ?
C1 N2 C10 125.8(6) . . ?
C3 N2 C10 126.0(6) . . ?
C4 N3 C5 108.8(5) . . ?
C4 N3 C12 126.5(6) . . ?
C5 N3 C12 124.7(6) . . ?
C4 N4 C6 107.7(5) . . ?
C4 N4 C13 126.8(6) . . ?
C6 N4 C13 125.5(6) . . ?
N2 C1 N1 109.4(6) . . ?
C3 C2 N1 106.6(6) . . ?
C2 C3 N2 107.4(6) . . ?
N3 C4 N4 108.6(6) . . ?
C6 C5 N3 107.6(6) . . ?
C5 C6 N4 107.3(6) . . ?
C11 C7 C10 113.1(6) . . ?
C14 C9 C13 116.2(7) . . ?
N2 C10 C7 112.2(5) . . ?
C7 C11 C15 113.1(7) . . ?
N4 C13 C9 112.3(6) . . ?
C9 C14 C16 113.5(7) . . ?

_diffrn_measured_fraction_theta_max 0.997
_diffrn_reflns_theta_full        28.33
_diffrn_measured_fraction_theta_full 0.997
_refine_diff_density_max         1.008
_refine_diff_density_min         -0.620
_refine_diff_density_rms         0.165
_database_code_depnum_ccdc_archive 'CCDC 992336'
