# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2014

#######################################################################
#
#                 Cambridge Crystallographic Data Centre
#                                CCDC 
# 
#######################################################################
# 
#  This CIF contains data from an original supplementary publication
#  deposited with the CCDC, and may include chemical, crystal,
#  experimental, refinement, atomic coordinates,
#  anisotropic displacement parameters and molecular geometry data,
#  as required by the journal to which it was submitted.
#
#  This CIF is provided on the understanding that it is used for bona
#  fide research purposes only. It may contain copyright material
#  of the CCDC or of third parties, and may not be copied or further
#  disseminated in any form, whether machine-readable or not,
#  except for the purpose of generating routine backup copies
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#  data retrieval see:
#                         www.ccdc.cam.ac.uk
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#  from this site to visualise CIF-encoded structures and 
#  to carry out CIF format checking respectively.
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data_1

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
;
 ?
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         'C61 H106 Br3 Cl15 P6 Pt3'
_chemical_formula_sum            'C61 H106 Br3 Cl15 P6 Pt3'
_chemical_formula_weight         2382.03

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Br Br -0.2901 2.4595 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           Monoclinic
_symmetry_space_group_name_H-M   Cm

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'x, -y, z'
'x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z'

_cell_length_a                   16.482(5)
_cell_length_b                   29.135(5)
_cell_length_c                   10.874(5)
_cell_angle_alpha                90.000
_cell_angle_beta                 112.156(5)
_cell_angle_gamma                90.000
_cell_volume                     4836(3)
_cell_formula_units_Z            2
_cell_measurement_temperature    100(2)
_cell_measurement_reflns_used    999
_cell_measurement_theta_min      ?
_cell_measurement_theta_max      ?

_exptl_crystal_description       Block
_exptl_crystal_colour            Colorless
_exptl_crystal_size_max          0.18
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.12
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    1.636
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             2312
_exptl_absorpt_coefficient_mu    6.112
_exptl_absorpt_correction_type   Empirical
_exptl_absorpt_correction_T_min  0.4059
_exptl_absorpt_correction_T_max  0.5275
_exptl_absorpt_process_details   Sadabs

_exptl_special_details           
;
 ?
;

_diffrn_ambient_temperature      100(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  ?
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            12376
_diffrn_reflns_av_R_equivalents  0.0556
_diffrn_reflns_av_sigmaI/netI    0.0750
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_k_min       -34
_diffrn_reflns_limit_k_max       32
_diffrn_reflns_limit_l_min       -12
_diffrn_reflns_limit_l_max       12
_diffrn_reflns_theta_min         2.08
_diffrn_reflns_theta_max         25.00
_reflns_number_total             6148
_reflns_number_gt                5790
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    ?
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_special_details          
;
 Refinement of F² against ALL reflections.  The weighted R-factor wR and
 goodness of fit S are based on F², conventional R-factors R are based
 on F, with F set to zero for negative F². The threshold expression of
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is
 not relevant to the choice of reflections for refinement.  R-factors based
 on F² are statistically about twice as large as those based on F, and R-
 factors based on ALL data will be even larger.
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0828P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    mixed
_refine_ls_extinction_method     SHELXL
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.026(12)
_refine_ls_number_reflns         6148
_refine_ls_number_parameters     424
_refine_ls_number_restraints     122
_refine_ls_R_factor_all          0.0526
_refine_ls_R_factor_gt           0.0506
_refine_ls_wR_factor_ref         0.1272
_refine_ls_wR_factor_gt          0.1255
_refine_ls_goodness_of_fit_ref   1.013
_refine_ls_restrained_S_all      1.007
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.2105(11) 1.0000 0.2722(16) 0.015(3) Uani 1 2 d SU . .
H1 H 0.2035 1.0000 0.3551 0.019 Uiso 1 2 calc SR . .
C2 C 0.2873(12) 0.9117(6) 0.5787(16) 0.051(4) Uani 1 1 d U . .
H2A H 0.2431 0.8980 0.4993 0.076 Uiso 1 1 calc R . .
H2B H 0.2814 0.9452 0.5739 0.076 Uiso 1 1 calc R . .
H2C H 0.2785 0.9005 0.6579 0.076 Uiso 1 1 calc R . .
C3 C 0.3801(13) 0.8980(4) 0.5868(15) 0.045(3) Uani 1 1 d U . .
H3A H 0.3854 0.8642 0.5882 0.053 Uiso 1 1 calc R . .
H3B H 0.4246 0.9102 0.6699 0.053 Uiso 1 1 calc R . .
C4 C 0.3163(10) 0.8939(5) 0.2934(13) 0.035(3) Uani 1 1 d U . .
H4A H 0.2576 0.9042 0.2871 0.042 Uiso 1 1 calc R . .
H4B H 0.3248 0.9051 0.2131 0.042 Uiso 1 1 calc R . .
C5 C 0.5025(10) 0.8950(5) 0.4501(15) 0.037(3) Uani 1 1 d U . .
H5A H 0.5509 0.9063 0.5303 0.044 Uiso 1 1 calc R . .
H5B H 0.4984 0.8613 0.4584 0.044 Uiso 1 1 calc R . .
C6 C 0.5232(14) 0.9060(6) 0.326(2) 0.058(5) Uani 1 1 d U . .
H6A H 0.5149 0.9389 0.3061 0.086 Uiso 1 1 calc R . .
H6B H 0.4839 0.8884 0.2498 0.086 Uiso 1 1 calc R . .
H6C H 0.5841 0.8977 0.3425 0.086 Uiso 1 1 calc R . .
C7 C 0.2935(11) 1.0000 0.2688(17) 0.018(3) Uani 1 2 d SU . .
C8 C 0.3060(12) 1.0000 0.1502(18) 0.021(3) Uani 1 2 d SU . .
H8 H 0.3635 1.0000 0.1498 0.025 Uiso 1 2 calc SR . .
C9 C 0.2321(12) 1.0000 0.0294(18) 0.025(3) Uani 1 2 d SU . .
H9 H 0.2402 1.0000 -0.0526 0.029 Uiso 1 2 calc SR . .
C11 C 0.1382(12) 1.0000 0.1560(17) 0.019(3) Uani 1 2 d SU . .
C12 C 0.0451(11) 1.0000 0.1410(16) 0.020(3) Uani 1 2 d SU . .
H12 H 0.0371 1.0000 0.2277 0.023 Uiso 1 2 calc SR . .
C13 C 0.0033(7) 0.9584(4) 0.0536(11) 0.018(2) Uani 1 1 d U . .
C14 C 0.0140(8) 0.9576(4) -0.0699(11) 0.022(2) Uani 1 1 d U . .
C15 C 0.0629(12) 1.0000 -0.0888(18) 0.025(3) Uani 1 2 d SU . .
H15 H 0.0705 1.0000 -0.1758 0.030 Uiso 1 2 calc SR . .
C16 C -0.0185(9) 0.9220(4) -0.1550(12) 0.023(2) Uani 1 1 d U . .
H16 H -0.0128 0.9220 -0.2388 0.028 Uiso 1 1 calc R . .
C17 C -0.0607(9) 0.8851(4) -0.1192(12) 0.025(3) Uani 1 1 d U . .
H17 H -0.0838 0.8606 -0.1801 0.030 Uiso 1 1 calc R . .
C18 C -0.0691(8) 0.8839(4) 0.0029(13) 0.022(2) Uani 1 1 d U . .
C19 C -0.0364(8) 0.9219(4) 0.0896(11) 0.018(2) Uani 1 1 d U . .
H19 H -0.0419 0.9223 0.1735 0.022 Uiso 1 1 calc R . .
C21 C 0.0646(9) 0.7926(4) 0.0357(13) 0.029(3) Uani 1 1 d U . .
H21A H 0.0754 0.8233 0.0060 0.035 Uiso 1 1 calc R . .
H21B H 0.1220 0.7777 0.0822 0.035 Uiso 1 1 calc R . .
C22 C 0.0130(9) 0.7413(4) 0.2250(14) 0.030(3) Uani 1 1 d U . .
H22A H -0.0164 0.7426 0.2892 0.036 Uiso 1 1 calc R . .
H22B H -0.0207 0.7198 0.1534 0.036 Uiso 1 1 calc R . .
C23 C 0.0857(9) 0.8339(4) 0.2895(14) 0.029(3) Uani 1 1 d U . .
H23A H 0.1436 0.8185 0.3237 0.034 Uiso 1 1 calc R . .
H23B H 0.0932 0.8644 0.2552 0.034 Uiso 1 1 calc R . .
C25 C 0.1043(10) 0.7218(5) 0.2953(15) 0.037(3) Uani 1 1 d U . .
H25A H 0.1348 0.7394 0.3765 0.056 Uiso 1 1 calc R . .
H25B H 0.1370 0.7239 0.2366 0.056 Uiso 1 1 calc R . .
H25C H 0.1000 0.6896 0.3181 0.056 Uiso 1 1 calc R . .
C26 C 0.3170(11) 0.8424(5) 0.2917(14) 0.035(3) Uani 1 1 d U . .
H26A H 0.3113 0.8307 0.3726 0.052 Uiso 1 1 calc R . .
H26B H 0.3723 0.8316 0.2878 0.052 Uiso 1 1 calc R . .
H26C H 0.2680 0.8313 0.2138 0.052 Uiso 1 1 calc R . .
C28 C 0.2441(11) 0.8282(5) 0.9055(16) 0.037(3) Uani 1 1 d U . .
H28 H 0.2448 0.8065 0.9772 0.044 Uiso 1 1 calc R . .
C30 C 0.8742(11) 0.7639(5) 0.5066(16) 0.040(3) Uani 1 1 d U . .
H30 H 0.8436 0.7599 0.4085 0.048 Uiso 1 1 calc R . .
C81 C -0.280(2) 0.8884(11) -0.217(2) 0.140(12) Uani 1 1 d DU . .
H81A H -0.3346 0.9062 -0.2526 0.169 Uiso 1 1 calc R . .
H81B H -0.2306 0.9089 -0.2128 0.169 Uiso 1 1 calc R . .
C82A C -0.2842(19) 0.8489(18) -0.307(3) 0.27(3) Uani 1 1 d DU . .
H82A H -0.3429 0.8475 -0.3767 0.401 Uiso 1 1 calc R . .
H82B H -0.2722 0.8203 -0.2557 0.401 Uiso 1 1 calc R . .
H82C H -0.2407 0.8531 -0.3473 0.401 Uiso 1 1 calc R . .
C84 C -0.3569(14) 0.8356(10) -0.063(5) 0.160(15) Uani 1 1 d DU . .
H84A H -0.3555 0.8067 -0.1098 0.192 Uiso 1 1 calc R . .
H84B H -0.3546 0.8273 0.0266 0.192 Uiso 1 1 calc R . .
C84A C -0.4412(14) 0.8583(13) -0.135(3) 0.128(13) Uani 1 1 d DU . .
H84Q H -0.4656 0.8470 -0.2262 0.192 Uiso 1 1 calc R . .
H84W H -0.4323 0.8915 -0.1348 0.192 Uiso 1 1 calc R . .
H84R H -0.4818 0.8514 -0.0906 0.192 Uiso 1 1 calc R . .
C101 C 0.1499(12) 1.0000 0.0297(16) 0.020(3) Uani 1 2 d SU . .
C102 C 0.0549(11) 0.8396(6) 0.3970(15) 0.040(3) Uani 1 1 d U . .
H10A H 0.0510 0.8096 0.4348 0.060 Uiso 1 1 calc R . .
H10B H -0.0031 0.8541 0.3629 0.060 Uiso 1 1 calc R . .
H10C H 0.0959 0.8592 0.4659 0.060 Uiso 1 1 calc R . .
C103 C -0.5272(17) 1.0000 -0.0629(19) 0.044(4) Uani 1 2 d SU . .
H103 H -0.5034 1.0000 -0.1351 0.053 Uiso 1 2 calc SR . .
C203 C -0.2673(18) 0.9007(12) 0.190(2) 0.167(17) Uani 1 1 d DU . .
H20A H -0.2204 0.8790 0.2370 0.251 Uiso 1 1 calc R . .
H20B H -0.3242 0.8862 0.1726 0.251 Uiso 1 1 calc R . .
H20C H -0.2617 0.9280 0.2454 0.251 Uiso 1 1 calc R . .
C501 C -0.261(2) 0.9140(10) 0.064(3) 0.140(11) Uani 1 1 d DU . .
H50A H -0.2059 0.9315 0.0838 0.169 Uiso 1 1 calc R . .
H50B H -0.3102 0.9348 0.0162 0.169 Uiso 1 1 calc R . .
C20A C 0.0118(13) 0.7644(6) -0.0835(16) 0.049(4) Uani 1 1 d U . .
H20D H 0.0438 0.7615 -0.1429 0.074 Uiso 1 1 calc R . .
H20E H -0.0447 0.7794 -0.1306 0.074 Uiso 1 1 calc R . .
H20F H 0.0018 0.7338 -0.0544 0.074 Uiso 1 1 calc R . .
P1 P 0.0080(2) 0.79917(11) 0.1515(3) 0.0237(7) Uani 1 1 d U . .
P3 P 0.3998(3) 0.92157(10) 0.4410(3) 0.0260(7) Uani 1 1 d U . .
P7 P -0.2619(2) 0.86697(11) -0.0440(3) 0.0276(7) Uani 1 1 d U . .
Cl1 Cl 0.2070(3) 0.88179(13) 0.9342(4) 0.0499(10) Uani 1 1 d U . .
Cl2 Cl 0.1734(3) 0.80616(18) 0.7492(4) 0.0635(12) Uani 1 1 d U . .
Cl3 Cl 0.3515(3) 0.83259(14) 0.9055(5) 0.0537(11) Uani 1 1 d U . .
Cl4 Cl 0.8120(3) 0.73580(14) 0.5863(4) 0.0429(9) Uani 1 1 d U . .
Cl5 Cl 0.8846(4) 0.82250(13) 0.5419(5) 0.0551(12) Uani 1 1 d U . .
Cl6 Cl 0.9793(3) 0.73717(12) 0.5567(3) 0.0367(8) Uani 1 1 d U . .
Cl7 Cl -0.4369(4) 1.0000 0.0954(6) 0.0507(14) Uani 1 2 d SU . .
Cl8 Cl -0.5881(4) 0.95021(18) -0.0756(5) 0.0709(15) Uani 1 1 d U . .
Br3 Br 0.53821(13) 1.0000 0.65622(17) 0.0285(4) Uani 1 2 d SU . .
Br4 Br -0.20314(10) 0.76838(4) 0.13809(14) 0.0317(3) Uani 1 1 d U . .
Pt1 Pt 0.40266(5) 1.0000 0.44218(5) 0.01978(17) Uani 1 2 d SU . .
Pt2 Pt -0.1291 0.831522(14) 0.05866(4) 0.02170(15) Uani 1 1 d U . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C11 1.37(2) . ?
C1 C7 1.38(2) . ?
C2 C3 1.55(3) . ?
C3 P3 1.865(14) . ?
C4 C26 1.501(19) . ?
C4 P3 1.858(14) . ?
C5 C6 1.55(2) . ?
C5 P3 1.830(15) . ?
C7 C8 1.38(2) . ?
C7 Pt1 2.058(18) . ?
C8 C9 1.41(3) . ?
C9 C101 1.36(3) . ?
C11 C101 1.46(2) . ?
C11 C12 1.48(2) . ?
C12 C13 1.534(15) . ?
C12 C13 1.534(15) 2_575 ?
C13 C19 1.379(16) . ?
C13 C14 1.419(16) . ?
C14 C16 1.357(17) . ?
C14 C15 1.531(16) . ?
C15 C101 1.52(2) . ?
C15 C14 1.531(16) 2_575 ?
C16 C17 1.412(17) . ?
C17 C18 1.387(16) . ?
C18 C19 1.424(17) . ?
C18 Pt2 2.031(12) . ?
C21 C20A 1.51(2) . ?
C21 P1 1.837(13) . ?
C22 C25 1.52(2) . ?
C22 P1 1.853(12) . ?
C23 C102 1.45(2) . ?
C23 P1 1.861(13) . ?
C28 Cl1 1.747(14) . ?
C28 Cl3 1.773(16) . ?
C28 Cl2 1.779(16) . ?
C30 Cl5 1.745(15) . ?
C30 Cl4 1.772(14) . ?
C30 Cl6 1.786(16) . ?
C81 C82A 1.491(19) . ?
C81 P7 1.90(2) . ?
C84 C84A 1.468(18) . ?
C84 P7 1.76(2) . ?
C103 Cl8 1.740(15) . ?
C103 Cl8 1.740(15) 2_575 ?
C103 Cl7 1.80(2) . ?
C203 C501 1.468(19) . ?
C501 P7 1.80(2) . ?
P1 Pt2 2.302(3) . ?
P3 Pt1 2.285(3) . ?
P7 Pt2 2.294(4) . ?
Br3 Pt1 2.547(2) . ?
Br4 Pt2 2.5323(13) . ?
Pt1 P3 2.285(3) 2_575 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C11 C1 C7 120.0(15) . . ?
C2 C3 P3 110.0(11) . . ?
C26 C4 P3 115.9(11) . . ?
C6 C5 P3 111.7(11) . . ?
C8 C7 C1 121.5(16) . . ?
C8 C7 Pt1 117.9(12) . . ?
C1 C7 Pt1 120.5(12) . . ?
C7 C8 C9 119.2(16) . . ?
C101 C9 C8 120.6(16) . . ?
C1 C11 C101 119.4(15) . . ?
C1 C11 C12 127.3(15) . . ?
C101 C11 C12 113.3(15) . . ?
C11 C12 C13 105.9(9) . . ?
C11 C12 C13 105.9(9) . 2_575 ?
C13 C12 C13 104.4(13) . 2_575 ?
C19 C13 C14 119.8(10) . . ?
C19 C13 C12 125.6(11) . . ?
C14 C13 C12 114.4(10) . . ?
C16 C14 C13 120.0(11) . . ?
C16 C14 C15 128.1(12) . . ?
C13 C14 C15 111.9(11) . . ?
C101 C15 C14 105.2(10) . . ?
C101 C15 C14 105.2(10) . 2_575 ?
C14 C15 C14 107.6(14) . 2_575 ?
C14 C16 C17 120.1(11) . . ?
C18 C17 C16 121.4(11) . . ?
C17 C18 C19 117.6(11) . . ?
C17 C18 Pt2 122.8(9) . . ?
C19 C18 Pt2 119.5(8) . . ?
C13 C19 C18 120.9(10) . . ?
C20A C21 P1 111.6(10) . . ?
C25 C22 P1 115.6(9) . . ?
C102 C23 P1 111.7(10) . . ?
Cl1 C28 Cl3 110.7(8) . . ?
Cl1 C28 Cl2 110.2(9) . . ?
Cl3 C28 Cl2 108.7(8) . . ?
Cl5 C30 Cl4 111.8(7) . . ?
Cl5 C30 Cl6 110.9(9) . . ?
Cl4 C30 Cl6 108.8(9) . . ?
C82A C81 P7 110(2) . . ?
C84A C84 P7 117(2) . . ?
C9 C101 C11 119.3(16) . . ?
C9 C101 C15 128.4(15) . . ?
C11 C101 C15 112.4(15) . . ?
Cl8 C103 Cl8 113.0(15) . 2_575 ?
Cl8 C103 Cl7 108.7(7) . . ?
Cl8 C103 Cl7 108.7(7) 2_575 . ?
C203 C501 P7 115.0(19) . . ?
C21 P1 C22 104.5(6) . . ?
C21 P1 C23 103.7(6) . . ?
C22 P1 C23 104.0(6) . . ?
C21 P1 Pt2 114.2(5) . . ?
C22 P1 Pt2 116.0(5) . . ?
C23 P1 Pt2 113.2(5) . . ?
C5 P3 C4 103.4(7) . . ?
C5 P3 C3 104.6(7) . . ?
C4 P3 C3 105.4(7) . . ?
C5 P3 Pt1 113.9(5) . . ?
C4 P3 Pt1 116.4(5) . . ?
C3 P3 Pt1 111.9(4) . . ?
C84 P7 C501 105(2) . . ?
C84 P7 C81 105(2) . . ?
C501 P7 C81 110.9(14) . . ?
C84 P7 Pt2 117.9(7) . . ?
C501 P7 Pt2 104.6(10) . . ?
C81 P7 Pt2 113.0(10) . . ?
C7 Pt1 P3 89.18(9) . . ?
C7 Pt1 P3 89.18(9) . 2_575 ?
P3 Pt1 P3 177.76(19) . 2_575 ?
C7 Pt1 Br3 179.8(4) . . ?
P3 Pt1 Br3 90.82(9) . . ?
P3 Pt1 Br3 90.82(9) 2_575 . ?
C18 Pt2 P7 90.0(4) . . ?
C18 Pt2 P1 86.0(4) . . ?
P7 Pt2 P1 175.66(11) . . ?
C18 Pt2 Br4 177.3(3) . . ?
P7 Pt2 Br4 89.94(9) . . ?
P1 Pt2 Br4 94.16(8) . . ?

# SQUEEZE RESULTS (APPEND TO CIF)
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
1 0.093 0.000 0.450 325.6 54.7
2 0.593 0.500 0.450 325.6 54.7
_platon_squeeze_details          
; ?
;

_diffrn_measured_fraction_theta_max 0.998
_diffrn_reflns_theta_full        25.00
_diffrn_measured_fraction_theta_full 0.998
_refine_diff_density_max         3.291
_refine_diff_density_min         -1.646
_refine_diff_density_rms         0.226
_database_code_depnum_ccdc_archive 'CCDC 953632'
