# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2014

#######################################################################
#
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#                                CCDC 
# 
#######################################################################
# 
#  This CIF contains data from an original supplementary publication
#  deposited with the CCDC, and may include chemical, crystal,
#  experimental, refinement, atomic coordinates,
#  anisotropic displacement parameters and molecular geometry data,
#  as required by the journal to which it was submitted.
#
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#  fide research purposes only. It may contain copyright material
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data_1

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C50 H26 Dy2 F20 N2 O12'
_chemical_formula_weight         1551.73

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   P21/c

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   9.4512(19)
_cell_length_b                   31.333(6)
_cell_length_c                   20.413(6)
_cell_angle_alpha                90.00
_cell_angle_beta                 117.58(2)
_cell_angle_gamma                90.00
_cell_volume                     5358(2)
_cell_formula_units_Z            4
_cell_measurement_temperature    133(2)
_cell_measurement_reflns_used    12845
_cell_measurement_theta_min      1.7195
_cell_measurement_theta_max      27.9946

_exptl_crystal_description       needle
_exptl_crystal_colour            colorless
_exptl_crystal_size_max          0.26
_exptl_crystal_size_mid          0.09
_exptl_crystal_size_min          0.09
_exptl_crystal_density_meas      none
_exptl_crystal_density_diffrn    1.924
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             2992
_exptl_absorpt_coefficient_mu    2.900
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.6954
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_process_details   'SADABS; Bruker, 2000'

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      133(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'Rigaku Saturn724 CCD'
_diffrn_measurement_method       ω
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            31924
_diffrn_reflns_av_R_equivalents  0.0614
_diffrn_reflns_av_unet/netI      0.0617
_diffrn_reflns_limit_h_min       -11
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_k_min       -37
_diffrn_reflns_limit_k_max       36
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_limit_l_max       24
_diffrn_reflns_theta_min         1.72
_diffrn_reflns_theta_max         25.01
_reflns_number_total             9127
_reflns_number_gt                8665
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'CrystalClear (Rigaku Inc., 2008)'
_computing_cell_refinement       'CrystalClear (Rigaku Inc., 2008)'
_computing_data_reduction        'CrystalClear (Rigaku Inc., 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0539P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    mixed
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         9127
_refine_ls_number_parameters     788
_refine_ls_number_restraints     4
_refine_ls_R_factor_all          0.0454
_refine_ls_R_factor_gt           0.0427
_refine_ls_wR_factor_ref         0.1043
_refine_ls_wR_factor_gt          0.1014
_refine_ls_goodness_of_fit_ref   1.094
_refine_ls_restrained_S_all      1.093
_refine_ls_shift/su_max          0.007
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.34478(4) -0.460040(9) -0.49819(2) 0.03556(9) Uani 1 1 d . . .
Dy2 Dy -0.15768(4) -0.433220(9) -0.38828(2) 0.03546(9) Uani 1 1 d . . .
F14 F 0.0239(9) -0.22545(16) -0.6320(3) 0.0684(15) Uani 1 1 d . . .
F4 F 0.6632(11) -0.5009(3) -0.0068(5) 0.111(3) Uani 1 1 d . . .
F5 F -0.0878(8) -0.33707(16) -0.8271(4) 0.0764(18) Uani 1 1 d . . .
F3 F 0.8026(11) -0.5515(4) -0.0195(5) 0.125(3) Uani 1 1 d . . .
F13 F 0.1844(9) -0.30408(16) -0.6180(4) 0.081(2) Uani 1 1 d . . .
F12 F 0.5552(13) -0.3459(3) -0.8640(5) 0.113(3) Uani 1 1 d . . .
F10 F 0.5371(14) -0.2862(2) -0.8221(5) 0.122(3) Uani 1 1 d . . .
F16 F 0.0902(7) -0.19940(14) -0.5244(3) 0.0604(14) Uani 1 1 d . . .
F19 F 0.4859(10) -0.2729(3) -0.1181(6) 0.124(4) Uani 1 1 d . . .
F7 F -0.2935(10) -0.3600(3) -0.9809(5) 0.128(4) Uani 1 1 d . . .
F6 F -0.0520(10) -0.3454(3) -0.9555(5) 0.111(3) Uani 1 1 d . . .
F15 F 0.2718(8) -0.22206(18) -0.5501(4) 0.0783(19) Uani 1 1 d . . .
F17 F 0.3529(8) -0.28125(19) -0.2777(4) 0.081(2) Uani 1 1 d . . .
F1 F 0.7735(7) -0.48679(19) -0.1187(3) 0.0697(15) Uani 1 1 d . . .
F2 F 0.5803(11) -0.5654(2) -0.0197(4) 0.097(2) Uani 1 1 d . . .
F9 F 0.7804(7) -0.3360(2) -0.7092(4) 0.0760(17) Uani 1 1 d . . .
F20 F 0.7348(9) -0.27694(19) -0.0662(4) 0.087(2) Uani 1 1 d . . .
F18 F 0.6175(14) -0.23623(17) -0.1569(4) 0.112(3) Uani 1 1 d . . .
F11 F 0.3305(11) -0.3206(5) -0.8802(6) 0.195(7) Uani 1 1 d . . .
F8 F -0.1685(15) -0.4033(3) -1.0171(4) 0.136(4) Uani 1 1 d . . .
O1 O 0.1787(6) -0.52650(15) -0.3963(3) 0.0413(11) Uani 1 1 d . . .
O2 O 0.4021(6) -0.49904(15) -0.3907(3) 0.0435(12) Uani 1 1 d . . .
O9 O 0.0597(7) -0.50766(14) -0.6862(3) 0.0403(11) Uani 1 1 d . . .
O11 O 0.1196(7) -0.51386(16) -0.5351(3) 0.0379(11) Uani 1 1 d D . .
O4 O 0.4646(6) -0.40582(15) -0.4028(3) 0.0431(12) Uani 1 1 d . . .
O6 O 0.0466(6) -0.40458(15) -0.4073(3) 0.0405(12) Uani 1 1 d . . .
O5 O 0.1431(7) -0.43058(14) -0.4799(3) 0.0428(13) Uani 1 1 d . . .
O12 O 0.3790(6) -0.51906(15) -0.5603(3) 0.0361(11) Uani 1 1 d D . .
O10 O 0.1425(7) -0.44595(14) -0.6232(3) 0.0418(11) Uani 1 1 d . . .
O8 O 0.7118(7) -0.40668(14) -0.5074(3) 0.0435(11) Uani 1 1 d . . .
O7 O 0.4467(7) -0.41395(17) -0.5542(4) 0.0463(13) Uani 1 1 d . . .
O3 O 0.7081(7) -0.42704(16) -0.3173(3) 0.0414(12) Uani 1 1 d . . .
N2 N 0.0625(8) -0.40354(19) -0.2685(4) 0.0422(14) Uani 1 1 d . . .
N1 N -0.1797(8) -0.35362(19) -0.3676(4) 0.0433(15) Uani 1 1 d . . .
C15 C 0.3963(12) -0.3803(3) -0.6895(6) 0.069(3) Uani 1 1 d . . .
H15 H 0.3089 -0.3905 -0.6849 0.083 Uiso 1 1 calc R . .
C45 C 0.0729(11) -0.3610(2) -0.2536(5) 0.0473(18) Uani 1 1 d . . .
C13 C 0.5033(13) -0.3458(3) -0.7622(5) 0.059(2) Uani 1 1 d . . .
C16 C 0.4818(14) -0.3252(5) -0.8328(7) 0.081(4) Uani 1 1 d . . .
C34 C 0.0987(9) -0.3562(2) -0.4841(4) 0.0405(16) Uani 1 1 d . . .
C41 C 0.1810(10) -0.4283(3) -0.2212(5) 0.0487(19) Uani 1 1 d . . .
H41 H 0.1739 -0.4574 -0.2310 0.058 Uiso 1 1 calc R . .
C11 C 0.6783(10) -0.3689(3) -0.6374(5) 0.0478(19) Uani 1 1 d . . .
H11 H 0.7811 -0.3714 -0.5986 0.057 Uiso 1 1 calc R . .
C30 C -0.0633(11) -0.3792(3) -0.8243(6) 0.057(2) Uani 1 1 d . . .
C17 C 0.3228(10) -0.5147(2) -0.3613(5) 0.0424(18) Uani 1 1 d . . .
C18 C 0.4101(9) -0.5199(2) -0.2785(4) 0.0405(16) Uani 1 1 d . . .
C23 C 0.3405(10) -0.5446(3) -0.2448(5) 0.0472(19) Uani 1 1 d . . .
H23 H 0.2418 -0.5574 -0.2730 0.057 Uiso 1 1 calc R . .
C39 C 0.0614(10) -0.3212(2) -0.4529(5) 0.0448(18) Uani 1 1 d . . .
H39 H 0.0301 -0.3252 -0.4164 0.054 Uiso 1 1 calc R . .
C9 C 0.5689(9) -0.4030(2) -0.5589(5) 0.0398(16) Uani 1 1 d . . .
C10 C 0.5476(10) -0.3835(2) -0.6297(4) 0.0418(17) Uani 1 1 d . . .
C50 C -0.3027(11) -0.3296(2) -0.4165(5) 0.0467(19) Uani 1 1 d . . .
H50 H -0.3847 -0.3432 -0.4567 0.056 Uiso 1 1 calc R . .
C46 C -0.0632(11) -0.3337(2) -0.3096(5) 0.0461(18) Uani 1 1 d . . .
C19 C 0.5557(11) -0.5004(3) -0.2368(5) 0.051(2) Uani 1 1 d . . .
H19 H 0.6030 -0.4839 -0.2591 0.062 Uiso 1 1 calc R . .
C43 C 0.3224(13) -0.3705(3) -0.1437(5) 0.064(2) Uani 1 1 d . . .
H43 H 0.4075 -0.3592 -0.1019 0.076 Uiso 1 1 calc R . .
C12 C 0.6528(11) -0.3507(3) -0.7031(5) 0.051(2) Uani 1 1 d . . .
C25 C 0.0778(10) -0.4670(2) -0.6819(4) 0.0407(16) Uani 1 1 d . . .
C21 C 0.5671(11) -0.5316(3) -0.1264(5) 0.055(2) Uani 1 1 d . . .
C26 C 0.0184(10) -0.4437(2) -0.7546(4) 0.0413(16) Uani 1 1 d . . .
C31 C -0.0092(9) -0.3998(2) -0.7578(5) 0.0477(19) Uani 1 1 d . . .
H31 H 0.0088 -0.3847 -0.7153 0.057 Uiso 1 1 calc R . .
C6 C 0.4700(13) -0.3105(3) -0.2566(6) 0.058(2) Uani 1 1 d . . .
C20 C 0.6297(11) -0.5060(3) -0.1607(5) 0.054(2) Uani 1 1 d . . .
C1 C 0.5832(10) -0.4043(2) -0.3388(5) 0.0416(17) Uani 1 1 d . . .
C40 C 0.1272(13) -0.2296(3) -0.5585(6) 0.060(3) Uani 1 1 d . . .
C33 C 0.0962(9) -0.4007(2) -0.4546(4) 0.0392(16) Uani 1 1 d . . .
C3 C 0.7104(11) -0.3706(2) -0.2122(5) 0.0469(18) Uani 1 1 d . . .
H3 H 0.7920 -0.3907 -0.1976 0.056 Uiso 1 1 calc R . .
C37 C 0.1124(11) -0.2743(3) -0.5321(5) 0.051(2) Uani 1 1 d . . .
C4 C 0.5811(9) -0.3718(2) -0.2851(5) 0.0430(17) Uani 1 1 d . . .
C5 C 0.7145(11) -0.3393(3) -0.1628(5) 0.0496(19) Uani 1 1 d . . .
H5 H 0.7973 -0.3389 -0.1147 0.060 Uiso 1 1 calc R . .
C7 C 0.5939(12) -0.3086(2) -0.1858(5) 0.051(2) Uani 1 1 d . . .
C35 C 0.1370(11) -0.3507(2) -0.5407(5) 0.0491(19) Uani 1 1 d . . .
H35 H 0.1577 -0.3739 -0.5633 0.059 Uiso 1 1 calc R . .
C8 C 0.6041(13) -0.2731(3) -0.1334(6) 0.059(2) Uani 1 1 d . . .
C38 C 0.0712(10) -0.2795(2) -0.4770(5) 0.048(2) Uani 1 1 d . . .
H38 H 0.0498 -0.2559 -0.4555 0.057 Uiso 1 1 calc R . .
C27 C -0.0043(11) -0.4656(3) -0.8173(5) 0.052(2) Uani 1 1 d . . .
H27 H 0.0147 -0.4949 -0.8147 0.062 Uiso 1 1 calc R . .
C36 C 0.1437(12) -0.3091(3) -0.5632(5) 0.052(2) Uani 1 1 d . . .
C14 C 0.4600(11) -0.3415(3) -0.3070(5) 0.053(2) Uani 1 1 d . . .
H14 H 0.3745 -0.3421 -0.3544 0.063 Uiso 1 1 calc R . .
C32 C -0.1491(16) -0.3778(4) -0.9602(8) 0.086(4) Uani 1 1 d . . .
C42 C 0.3150(12) -0.4139(3) -0.1581(6) 0.059(2) Uani 1 1 d . . .
H42 H 0.3950 -0.4324 -0.1273 0.071 Uiso 1 1 calc R . .
C22 C 0.4204(12) -0.5502(3) -0.1674(5) 0.054(2) Uani 1 1 d . . .
H22 H 0.3740 -0.5663 -0.1442 0.065 Uiso 1 1 calc R . .
C47 C -0.0623(13) -0.2896(3) -0.3006(6) 0.061(2) Uani 1 1 d . . .
H47 H 0.0221 -0.2765 -0.2609 0.073 Uiso 1 1 calc R . .
C48 C -0.1873(15) -0.2659(2) -0.3510(6) 0.066(3) Uani 1 1 d . . .
H48 H -0.1878 -0.2364 -0.3457 0.079 Uiso 1 1 calc R . .
C1D C -0.0905(11) -0.4009(3) -0.8892(6) 0.067(3) Uani 1 1 d . . .
C1E C 0.3720(15) -0.3620(4) -0.7574(7) 0.087(4) Uani 1 1 d . . .
H1E H 0.2707 -0.3609 -0.7977 0.104 Uiso 1 1 calc R . .
C24 C 0.6506(14) -0.5382(4) -0.0438(7) 0.081(3) Uani 1 1 d . . .
C49 C -0.3122(13) -0.2858(3) -0.4096(6) 0.060(2) Uani 1 1 d . . .
H49 H -0.3997 -0.2703 -0.4432 0.072 Uiso 1 1 calc R . .
C28 C -0.0551(14) -0.4446(3) -0.8846(6) 0.067(2) Uani 1 1 d . . .
H28 H -0.0655 -0.4594 -0.9261 0.081 Uiso 1 1 calc R . .
C44 C 0.2031(12) -0.3444(3) -0.1918(6) 0.059(2) Uani 1 1 d . . .
H44 H 0.2091 -0.3152 -0.1829 0.071 Uiso 1 1 calc R . .
H12 H 0.381(12) -0.517(3) -0.601(3) 0.05(3) Uiso 1 1 d D . .
H11A H 0.026(4) -0.506(2) -0.551(4) 0.05(3) Uiso 1 1 d D . .
H11B H 0.134(7) -0.522(2) -0.4938(18) 0.025(18) Uiso 1 1 d D . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Dy1 O5 2.298(5) . ?
Dy1 O7 2.311(5) . ?
Dy1 O2 2.346(6) . ?
Dy1 O12 2.348(5) . ?
Dy1 O12 2.405(5) 3_644 ?
Dy1 O10 2.417(5) . ?
Dy1 O4 2.433(5) . ?
Dy1 O11 2.541(5) . ?
Dy1 Dy1 3.8840(8) 3_644 ?
Dy1 Dy2 3.9861(8) 3_544 ?
Dy2 O9 2.302(5) 3_544 ?
Dy2 O8 2.313(6) 1_455 ?
Dy2 O6 2.319(5) . ?
Dy2 O3 2.334(5) 1_455 ?
Dy2 O12 2.383(5) 3_544 ?
Dy2 O11 2.419(5) 3_544 ?
Dy2 N2 2.542(7) . ?
Dy2 N1 2.554(6) . ?
Dy2 Dy1 3.9861(8) 3_544 ?
F14 C40 1.365(13) . ?
F4 C24 1.368(15) . ?
F5 C30 1.337(10) . ?
F3 C24 1.349(15) . ?
F13 C36 1.349(10) . ?
F12 C16 1.311(15) . ?
F10 C16 1.307(16) . ?
F16 C40 1.315(11) . ?
F19 C8 1.291(12) . ?
F7 C32 1.349(16) . ?
F6 C32 1.340(14) . ?
F15 C40 1.317(12) . ?
F17 C6 1.346(11) . ?
F1 C20 1.365(10) . ?
F2 C24 1.307(13) . ?
F9 C12 1.350(10) . ?
F20 C8 1.362(12) . ?
F18 C8 1.280(11) . ?
F11 C16 1.312(14) . ?
F8 C32 1.352(17) . ?
O1 C17 1.265(10) . ?
O2 C17 1.255(9) . ?
O9 C25 1.282(8) . ?
O9 Dy2 2.302(5) 3_544 ?
O11 Dy2 2.419(5) 3_544 ?
O11 H11A 0.83(2) . ?
O11 H11B 0.83(2) . ?
O4 C1 1.268(10) . ?
O6 C33 1.259(9) . ?
O5 C33 1.245(9) . ?
O12 Dy2 2.383(5) 3_544 ?
O12 Dy1 2.405(5) 3_644 ?
O12 H12 0.85(2) . ?
O10 C25 1.253(9) . ?
O8 C9 1.275(10) . ?
O8 Dy2 2.313(6) 1_655 ?
O7 C9 1.251(9) . ?
O3 C1 1.271(10) . ?
O3 Dy2 2.334(5) 1_655 ?
N2 C41 1.336(11) . ?
N2 C45 1.361(10) . ?
N1 C46 1.340(11) . ?
N1 C50 1.356(11) . ?
C15 C10 1.388(12) . ?
C15 C1E 1.419(14) . ?
C15 H15 0.9300 . ?
C45 C44 1.393(13) . ?
C45 C46 1.525(12) . ?
C13 C12 1.378(14) . ?
C13 C1E 1.385(15) . ?
C13 C16 1.505(12) . ?
C34 C35 1.374(11) . ?
C34 C39 1.392(10) . ?
C34 C33 1.525(10) . ?
C41 C42 1.399(13) . ?
C41 H41 0.9300 . ?
C11 C12 1.371(12) . ?
C11 C10 1.392(11) . ?
C11 H11 0.9300 . ?
C30 C31 1.371(12) . ?
C30 C1D 1.401(16) . ?
C17 C18 1.508(11) . ?
C18 C19 1.381(11) . ?
C18 C23 1.388(11) . ?
C23 C22 1.412(13) . ?
C23 H23 0.9300 . ?
C39 C38 1.414(10) . ?
C39 H39 0.9300 . ?
C9 C10 1.495(11) . ?
C50 C49 1.390(11) . ?
C50 H50 0.9300 . ?
C46 C47 1.393(11) . ?
C19 C20 1.388(13) . ?
C19 H19 0.9300 . ?
C43 C44 1.371(15) . ?
C43 C42 1.385(13) . ?
C43 H43 0.9300 . ?
C25 C26 1.509(10) . ?
C21 C20 1.367(13) . ?
C21 C22 1.373(13) . ?
C21 C24 1.510(15) . ?
C26 C27 1.378(12) . ?
C26 C31 1.398(10) . ?
C31 H31 0.9300 . ?
C6 C7 1.376(14) . ?
C6 C14 1.387(12) . ?
C1 C4 1.503(11) . ?
C40 C37 1.530(12) . ?
C3 C5 1.395(11) . ?
C3 C4 1.423(12) . ?
C3 H3 0.9300 . ?
C37 C38 1.358(12) . ?
C37 C36 1.362(12) . ?
C4 C14 1.391(12) . ?
C5 C7 1.396(13) . ?
C5 H5 0.9300 . ?
C7 C8 1.515(11) . ?
C35 C36 1.391(11) . ?
C35 H35 0.9300 . ?
C38 H38 0.9300 . ?
C27 C28 1.394(13) . ?
C27 H27 0.9300 . ?
C14 H14 0.9300 . ?
C32 C1D 1.481(14) . ?
C42 H42 0.9300 . ?
C22 H22 0.9300 . ?
C47 C48 1.373(15) . ?
C47 H47 0.9300 . ?
C48 C49 1.379(15) . ?
C48 H48 0.9300 . ?
C1D C28 1.402(15) . ?
C1E H1E 0.9300 . ?
C49 H49 0.9300 . ?
C28 H28 0.9300 . ?
C44 H44 0.9300 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O5 Dy1 O7 113.35(18) . . ?
O5 Dy1 O2 84.65(19) . . ?
O7 Dy1 O2 145.1(2) . . ?
O5 Dy1 O12 137.39(18) . . ?
O7 Dy1 O12 91.83(19) . . ?
O2 Dy1 O12 93.73(18) . . ?
O5 Dy1 O12 145.1(2) . 3_644 ?
O7 Dy1 O12 79.07(19) . 3_644 ?
O2 Dy1 O12 70.50(18) . 3_644 ?
O12 Dy1 O12 70.4(2) . 3_644 ?
O5 Dy1 O10 77.8(2) . . ?
O7 Dy1 O10 70.8(2) . . ?
O2 Dy1 O10 144.07(18) . . ?
O12 Dy1 O10 79.24(18) . . ?
O12 Dy1 O10 136.08(19) 3_644 . ?
O5 Dy1 O4 72.73(19) . . ?
O7 Dy1 O4 79.3(2) . . ?
O2 Dy1 O4 78.14(19) . . ?
O12 Dy1 O4 148.53(18) . . ?
O12 Dy1 O4 78.27(17) 3_644 . ?
O10 Dy1 O4 124.40(17) . . ?
O5 Dy1 O11 70.78(17) . . ?
O7 Dy1 O11 138.8(2) . . ?
O2 Dy1 O11 74.36(19) . . ?
O12 Dy1 O11 67.87(17) . . ?
O12 Dy1 O11 122.29(17) 3_644 . ?
O10 Dy1 O11 70.35(18) . . ?
O4 Dy1 O11 135.74(18) . . ?
O5 Dy1 Dy1 162.28(12) . 3_644 ?
O7 Dy1 Dy1 84.37(13) . 3_644 ?
O2 Dy1 Dy1 80.37(12) . 3_644 ?
O12 Dy1 Dy1 35.68(13) . 3_644 ?
O12 Dy1 Dy1 34.71(12) 3_644 3_644 ?
O10 Dy1 Dy1 109.46(13) . 3_644 ?
O4 Dy1 Dy1 112.93(13) . 3_644 ?
O11 Dy1 Dy1 95.91(12) . 3_644 ?
O5 Dy1 Dy2 104.68(13) . 3_544 ?
O7 Dy1 Dy2 114.27(16) . 3_544 ?
O2 Dy1 Dy2 87.42(13) . 3_544 ?
O12 Dy1 Dy2 32.86(12) . 3_544 ?
O12 Dy1 Dy2 98.49(12) 3_644 3_544 ?
O10 Dy1 Dy2 67.57(11) . 3_544 ?
O4 Dy1 Dy2 165.48(13) . 3_544 ?
O11 Dy1 Dy2 35.48(12) . 3_544 ?
Dy1 Dy1 Dy2 65.397(19) 3_644 3_544 ?
O9 Dy2 O8 147.10(17) 3_544 1_455 ?
O9 Dy2 O6 108.1(2) 3_544 . ?
O8 Dy2 O6 76.4(2) 1_455 . ?
O9 Dy2 O3 79.91(19) 3_544 1_455 ?
O8 Dy2 O3 116.4(2) 1_455 1_455 ?
O6 Dy2 O3 143.66(19) . 1_455 ?
O9 Dy2 O12 77.80(19) 3_544 3_544 ?
O8 Dy2 O12 80.24(18) 1_455 3_544 ?
O6 Dy2 O12 142.97(18) . 3_544 ?
O3 Dy2 O12 72.96(18) 1_455 3_544 ?
O9 Dy2 O11 74.97(18) 3_544 3_544 ?
O8 Dy2 O11 74.51(18) 1_455 3_544 ?
O6 Dy2 O11 76.84(18) . 3_544 ?
O3 Dy2 O11 138.16(17) 1_455 3_544 ?
O12 Dy2 O11 69.40(18) 3_544 3_544 ?
O9 Dy2 N2 76.06(18) 3_544 . ?
O8 Dy2 N2 132.88(19) 1_455 . ?
O6 Dy2 N2 69.2(2) . . ?
O3 Dy2 N2 79.1(2) 1_455 . ?
O12 Dy2 N2 144.46(19) 3_544 . ?
O11 Dy2 N2 124.9(2) 3_544 . ?
O9 Dy2 N1 135.7(2) 3_544 . ?
O8 Dy2 N1 77.2(2) 1_455 . ?
O6 Dy2 N1 77.73(18) . . ?
O3 Dy2 N1 72.97(19) 1_455 . ?
O12 Dy2 N1 124.30(19) 3_544 . ?
O11 Dy2 N1 145.52(19) 3_544 . ?
N2 Dy2 N1 65.0(2) . . ?
O9 Dy2 Dy1 69.11(13) 3_544 3_544 ?
O8 Dy2 Dy1 79.24(12) 1_455 3_544 ?
O6 Dy2 Dy1 114.03(12) . 3_544 ?
O3 Dy2 Dy1 102.02(13) 1_455 3_544 ?
O12 Dy2 Dy1 32.32(12) 3_544 3_544 ?
O11 Dy2 Dy1 37.58(13) 3_544 3_544 ?
N2 Dy2 Dy1 144.23(14) . 3_544 ?
N1 Dy2 Dy1 150.15(16) . 3_544 ?
C17 O2 Dy1 136.0(5) . . ?
C25 O9 Dy2 138.9(5) . 3_544 ?
Dy2 O11 Dy1 106.9(2) 3_544 . ?
Dy2 O11 H11A 114(6) 3_544 . ?
Dy1 O11 H11A 120(6) . . ?
Dy2 O11 H11B 116(5) 3_544 . ?
Dy1 O11 H11B 101(5) . . ?
H11A O11 H11B 98(3) . . ?
C1 O4 Dy1 135.5(5) . . ?
C33 O6 Dy2 143.1(5) . . ?
C33 O5 Dy1 148.3(5) . . ?
Dy1 O12 Dy2 114.8(2) . 3_544 ?
Dy1 O12 Dy1 109.6(2) . 3_644 ?
Dy2 O12 Dy1 125.3(2) 3_544 3_644 ?
Dy1 O12 H12 123(6) . . ?
Dy2 O12 H12 92(6) 3_544 . ?
Dy1 O12 H12 90(7) 3_644 . ?
C25 O10 Dy1 135.3(4) . . ?
C9 O8 Dy2 138.1(5) . 1_655 ?
C9 O7 Dy1 145.1(5) . . ?
C1 O3 Dy2 121.1(5) . 1_655 ?
C41 N2 C45 117.2(8) . . ?
C41 N2 Dy2 121.5(5) . . ?
C45 N2 Dy2 121.0(6) . . ?
C46 N1 C50 117.8(7) . . ?
C46 N1 Dy2 120.3(5) . . ?
C50 N1 Dy2 121.8(5) . . ?
C10 C15 C1E 121.5(9) . . ?
C10 C15 H15 119.3 . . ?
C1E C15 H15 119.3 . . ?
N2 C45 C44 120.7(8) . . ?
N2 C45 C46 115.6(7) . . ?
C44 C45 C46 123.7(7) . . ?
C12 C13 C1E 119.0(9) . . ?
C12 C13 C16 121.1(9) . . ?
C1E C13 C16 119.8(10) . . ?
F10 C16 F12 106.6(9) . . ?
F10 C16 F11 103.7(12) . . ?
F12 C16 F11 109.7(14) . . ?
F10 C16 C13 111.9(11) . . ?
F12 C16 C13 112.7(10) . . ?
F11 C16 C13 111.7(9) . . ?
C35 C34 C39 120.5(7) . . ?
C35 C34 C33 120.4(7) . . ?
C39 C34 C33 119.2(7) . . ?
N2 C41 C42 125.2(8) . . ?
N2 C41 H41 117.4 . . ?
C42 C41 H41 117.4 . . ?
C12 C11 C10 118.9(8) . . ?
C12 C11 H11 120.6 . . ?
C10 C11 H11 120.6 . . ?
F5 C30 C31 118.9(10) . . ?
F5 C30 C1D 119.1(8) . . ?
C31 C30 C1D 122.0(8) . . ?
O2 C17 O1 124.7(8) . . ?
O2 C17 C18 116.1(7) . . ?
O1 C17 C18 119.3(7) . . ?
C19 C18 C23 120.4(8) . . ?
C19 C18 C17 121.1(7) . . ?
C23 C18 C17 118.5(7) . . ?
C18 C23 C22 119.5(8) . . ?
C18 C23 H23 120.2 . . ?
C22 C23 H23 120.2 . . ?
C34 C39 C38 119.8(7) . . ?
C34 C39 H39 120.1 . . ?
C38 C39 H39 120.1 . . ?
O7 C9 O8 125.1(8) . . ?
O7 C9 C10 118.1(7) . . ?
O8 C9 C10 116.8(7) . . ?
C15 C10 C11 119.0(8) . . ?
C15 C10 C9 120.1(7) . . ?
C11 C10 C9 120.9(7) . . ?
N1 C50 C49 123.2(9) . . ?
N1 C50 H50 118.4 . . ?
C49 C50 H50 118.4 . . ?
N1 C46 C47 122.0(8) . . ?
N1 C46 C45 117.7(7) . . ?
C47 C46 C45 120.3(8) . . ?
C18 C19 C20 118.5(8) . . ?
C18 C19 H19 120.7 . . ?
C20 C19 H19 120.7 . . ?
C44 C43 C42 119.3(9) . . ?
C44 C43 H43 120.3 . . ?
C42 C43 H43 120.3 . . ?
F9 C12 C11 118.2(9) . . ?
F9 C12 C13 118.5(8) . . ?
C11 C12 C13 123.2(8) . . ?
O10 C25 O9 125.4(7) . . ?
O10 C25 C26 118.8(6) . . ?
O9 C25 C26 115.8(7) . . ?
C20 C21 C22 119.5(9) . . ?
C20 C21 C24 121.7(9) . . ?
C22 C21 C24 118.7(9) . . ?
C27 C26 C31 120.1(7) . . ?
C27 C26 C25 120.0(7) . . ?
C31 C26 C25 119.8(7) . . ?
C30 C31 C26 119.0(9) . . ?
C30 C31 H31 120.5 . . ?
C26 C31 H31 120.5 . . ?
F17 C6 C7 118.7(8) . . ?
F17 C6 C14 118.4(9) . . ?
C7 C6 C14 122.8(9) . . ?
F1 C20 C21 118.6(9) . . ?
F1 C20 C19 119.2(8) . . ?
C21 C20 C19 122.2(9) . . ?
O4 C1 O3 124.8(7) . . ?
O4 C1 C4 118.3(7) . . ?
O3 C1 C4 116.8(8) . . ?
F16 C40 F15 108.3(9) . . ?
F16 C40 F14 106.4(8) . . ?
F15 C40 F14 107.3(9) . . ?
F16 C40 C37 112.5(8) . . ?
F15 C40 C37 112.2(8) . . ?
F14 C40 C37 109.9(8) . . ?
O5 C33 O6 125.3(7) . . ?
O5 C33 C34 116.8(7) . . ?
O6 C33 C34 118.0(6) . . ?
C5 C3 C4 119.8(8) . . ?
C5 C3 H3 120.1 . . ?
C4 C3 H3 120.1 . . ?
C38 C37 C36 119.8(7) . . ?
C38 C37 C40 120.6(8) . . ?
C36 C37 C40 119.5(8) . . ?
C14 C4 C3 119.9(8) . . ?
C14 C4 C1 120.9(8) . . ?
C3 C4 C1 119.1(7) . . ?
C3 C5 C7 119.8(9) . . ?
C3 C5 H5 120.1 . . ?
C7 C5 H5 120.1 . . ?
C6 C7 C5 119.2(8) . . ?
C6 C7 C8 121.2(9) . . ?
C5 C7 C8 119.5(9) . . ?
C34 C35 C36 117.7(8) . . ?
C34 C35 H35 121.1 . . ?
C36 C35 H35 121.1 . . ?
F18 C8 F19 109.4(10) . . ?
F18 C8 F20 104.9(9) . . ?
F19 C8 F20 103.9(10) . . ?
F18 C8 C7 112.5(8) . . ?
F19 C8 C7 113.3(8) . . ?
F20 C8 C7 112.2(8) . . ?
C37 C38 C39 119.2(7) . . ?
C37 C38 H38 120.4 . . ?
C39 C38 H38 120.4 . . ?
C26 C27 C28 120.9(8) . . ?
C26 C27 H27 119.5 . . ?
C28 C27 H27 119.5 . . ?
F13 C36 C37 119.9(7) . . ?
F13 C36 C35 117.2(8) . . ?
C37 C36 C35 122.9(8) . . ?
C6 C14 C4 118.4(9) . . ?
C6 C14 H14 120.8 . . ?
C4 C14 H14 120.8 . . ?
F6 C32 F7 105.7(11) . . ?
F6 C32 F8 109.0(12) . . ?
F7 C32 F8 105.1(12) . . ?
F6 C32 C1D 111.5(11) . . ?
F7 C32 C1D 111.9(11) . . ?
F8 C32 C1D 113.1(11) . . ?
C43 C42 C41 116.5(9) . . ?
C43 C42 H42 121.7 . . ?
C41 C42 H42 121.7 . . ?
C21 C22 C23 119.7(8) . . ?
C21 C22 H22 120.2 . . ?
C23 C22 H22 120.2 . . ?
C48 C47 C46 119.3(9) . . ?
C48 C47 H47 120.4 . . ?
C46 C47 H47 120.4 . . ?
C47 C48 C49 119.9(8) . . ?
C47 C48 H48 120.0 . . ?
C49 C48 H48 120.0 . . ?
C30 C1D C28 118.5(9) . . ?
C30 C1D C32 120.7(11) . . ?
C28 C1D C32 120.8(12) . . ?
C13 C1E C15 118.2(11) . . ?
C13 C1E H1E 120.9 . . ?
C15 C1E H1E 120.9 . . ?
F2 C24 F3 107.5(10) . . ?
F2 C24 F4 106.2(11) . . ?
F3 C24 F4 104.7(11) . . ?
F2 C24 C21 114.6(10) . . ?
F3 C24 C21 111.7(11) . . ?
F4 C24 C21 111.5(10) . . ?
C48 C49 C50 117.7(9) . . ?
C48 C49 H49 121.1 . . ?
C50 C49 H49 121.1 . . ?
C27 C28 C1D 119.4(10) . . ?
C27 C28 H28 120.3 . . ?
C1D C28 H28 120.3 . . ?
C43 C44 C45 121.0(8) . . ?
C43 C44 H44 119.5 . . ?
C45 C44 H44 119.5 . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O5 Dy1 O2 C17 33.5(7) . . . . ?
O7 Dy1 O2 C17 157.6(7) . . . . ?
O12 Dy1 O2 C17 -103.8(7) . . . . ?
O12 Dy1 O2 C17 -171.5(8) 3_644 . . . ?
O10 Dy1 O2 C17 -27.0(9) . . . . ?
O4 Dy1 O2 C17 106.9(7) . . . . ?
O11 Dy1 O2 C17 -38.0(7) . . . . ?
Dy1 Dy1 O2 C17 -137.0(7) 3_644 . . . ?
Dy2 Dy1 O2 C17 -71.5(7) 3_544 . . . ?
O5 Dy1 O11 Dy2 162.1(3) . . . 3_544 ?
O7 Dy1 O11 Dy2 58.3(3) . . . 3_544 ?
O2 Dy1 O11 Dy2 -108.2(2) . . . 3_544 ?
O12 Dy1 O11 Dy2 -7.42(19) . . . 3_544 ?
O12 Dy1 O11 Dy2 -54.1(3) 3_644 . . 3_544 ?
O10 Dy1 O11 Dy2 78.6(2) . . . 3_544 ?
O4 Dy1 O11 Dy2 -161.82(19) . . . 3_544 ?
Dy1 Dy1 O11 Dy2 -29.95(19) 3_644 . . 3_544 ?
O5 Dy1 O4 C1 130.3(7) . . . . ?
O7 Dy1 O4 C1 -110.9(7) . . . . ?
O2 Dy1 O4 C1 42.2(7) . . . . ?
O12 Dy1 O4 C1 -35.3(9) . . . . ?
O12 Dy1 O4 C1 -30.0(7) 3_644 . . . ?
O10 Dy1 O4 C1 -168.5(7) . . . . ?
O11 Dy1 O4 C1 94.6(7) . . . . ?
Dy1 Dy1 O4 C1 -31.8(7) 3_644 . . . ?
Dy2 Dy1 O4 C1 48.4(10) 3_544 . . . ?
O9 Dy2 O6 C33 105.9(8) 3_544 . . . ?
O8 Dy2 O6 C33 -40.1(8) 1_455 . . . ?
O3 Dy2 O6 C33 -156.4(7) 1_455 . . . ?
O12 Dy2 O6 C33 12.3(9) 3_544 . . . ?
O11 Dy2 O6 C33 36.8(8) 3_544 . . . ?
N2 Dy2 O6 C33 172.7(8) . . . . ?
N1 Dy2 O6 C33 -119.7(8) . . . . ?
Dy1 Dy2 O6 C33 31.3(8) 3_544 . . . ?
O7 Dy1 O5 C33 -52.9(11) . . . . ?
O2 Dy1 O5 C33 96.0(10) . . . . ?
O12 Dy1 O5 C33 -174.3(9) . . . . ?
O12 Dy1 O5 C33 52.0(11) 3_644 . . . ?
O10 Dy1 O5 C33 -115.5(10) . . . . ?
O4 Dy1 O5 C33 16.8(10) . . . . ?
O11 Dy1 O5 C33 171.3(11) . . . . ?
Dy1 Dy1 O5 C33 128.3(9) 3_644 . . . ?
Dy2 Dy1 O5 C33 -178.1(10) 3_544 . . . ?
O5 Dy1 O12 Dy2 -6.8(4) . . . 3_544 ?
O7 Dy1 O12 Dy2 -135.1(2) . . . 3_544 ?
O2 Dy1 O12 Dy2 79.4(2) . . . 3_544 ?
O12 Dy1 O12 Dy2 147.2(4) 3_644 . . 3_544 ?
O10 Dy1 O12 Dy2 -65.1(2) . . . 3_544 ?
O4 Dy1 O12 Dy2 152.7(3) . . . 3_544 ?
O11 Dy1 O12 Dy2 7.9(2) . . . 3_544 ?
Dy1 Dy1 O12 Dy2 147.2(4) 3_644 . . 3_544 ?
O5 Dy1 O12 Dy1 -153.9(2) . . . 3_644 ?
O7 Dy1 O12 Dy1 77.7(2) . . . 3_644 ?
O2 Dy1 O12 Dy1 -67.8(2) . . . 3_644 ?
O12 Dy1 O12 Dy1 0.0 3_644 . . 3_644 ?
O10 Dy1 O12 Dy1 147.8(2) . . . 3_644 ?
O4 Dy1 O12 Dy1 5.5(5) . . . 3_644 ?
O11 Dy1 O12 Dy1 -139.2(3) . . . 3_644 ?
Dy2 Dy1 O12 Dy1 -147.2(4) 3_544 . . 3_644 ?
O5 Dy1 O10 C25 -130.3(7) . . . . ?
O7 Dy1 O10 C25 109.3(7) . . . . ?
O2 Dy1 O10 C25 -67.9(8) . . . . ?
O12 Dy1 O10 C25 13.5(7) . . . . ?
O12 Dy1 O10 C25 59.9(8) 3_644 . . . ?
O4 Dy1 O10 C25 170.8(7) . . . . ?
O11 Dy1 O10 C25 -56.6(7) . . . . ?
Dy1 Dy1 O10 C25 32.8(7) 3_644 . . . ?
Dy2 Dy1 O10 C25 -18.6(7) 3_544 . . . ?
O5 Dy1 O7 C9 147.5(10) . . . . ?
O2 Dy1 O7 C9 31.4(12) . . . . ?
O12 Dy1 O7 C9 -67.8(10) . . . . ?
O12 Dy1 O7 C9 1.8(10) 3_644 . . . ?
O10 Dy1 O7 C9 -145.8(10) . . . . ?
O4 Dy1 O7 C9 81.8(10) . . . . ?
O11 Dy1 O7 C9 -125.4(10) . . . . ?
Dy1 Dy1 O7 C9 -32.9(10) 3_644 . . . ?
Dy2 Dy1 O7 C9 -92.7(10) 3_544 . . . ?
O9 Dy2 N2 C41 22.6(6) 3_544 . . . ?
O8 Dy2 N2 C41 -139.3(6) 1_455 . . . ?
O6 Dy2 N2 C41 -93.3(7) . . . . ?
O3 Dy2 N2 C41 104.7(7) 1_455 . . . ?
O12 Dy2 N2 C41 66.3(8) 3_544 . . . ?
O11 Dy2 N2 C41 -37.5(7) 3_544 . . . ?
N1 Dy2 N2 C41 -179.1(7) . . . . ?
Dy1 Dy2 N2 C41 9.3(8) 3_544 . . . ?
O9 Dy2 N2 C45 -164.1(6) 3_544 . . . ?
O8 Dy2 N2 C45 34.1(7) 1_455 . . . ?
O6 Dy2 N2 C45 80.0(6) . . . . ?
O3 Dy2 N2 C45 -81.9(6) 1_455 . . . ?
O12 Dy2 N2 C45 -120.4(6) 3_544 . . . ?
O11 Dy2 N2 C45 135.8(6) 3_544 . . . ?
N1 Dy2 N2 C45 -5.8(6) . . . . ?
Dy1 Dy2 N2 C45 -177.4(5) 3_544 . . . ?
O9 Dy2 N1 C46 36.6(7) 3_544 . . . ?
O8 Dy2 N1 C46 -145.4(6) 1_455 . . . ?
O6 Dy2 N1 C46 -66.8(6) . . . . ?
O3 Dy2 N1 C46 91.4(6) 1_455 . . . ?
O12 Dy2 N1 C46 146.0(6) 3_544 . . . ?
O11 Dy2 N1 C46 -110.0(6) 3_544 . . . ?
N2 Dy2 N1 C46 5.8(6) . . . . ?
Dy1 Dy2 N1 C46 175.9(4) 3_544 . . . ?
O9 Dy2 N1 C50 -147.6(5) 3_544 . . . ?
O8 Dy2 N1 C50 30.4(6) 1_455 . . . ?
O6 Dy2 N1 C50 109.0(6) . . . . ?
O3 Dy2 N1 C50 -92.7(6) 1_455 . . . ?
O12 Dy2 N1 C50 -38.2(7) 3_544 . . . ?
O11 Dy2 N1 C50 65.8(7) 3_544 . . . ?
N2 Dy2 N1 C50 -178.4(6) . . . . ?
Dy1 Dy2 N1 C50 -8.2(8) 3_544 . . . ?
C41 N2 C45 C44 0.5(12) . . . . ?
Dy2 N2 C45 C44 -173.1(6) . . . . ?
C41 N2 C45 C46 179.0(7) . . . . ?
Dy2 N2 C45 C46 5.4(9) . . . . ?
C12 C13 C16 F10 -59.6(14) . . . . ?
C1E C13 C16 F10 123.7(13) . . . . ?
C12 C13 C16 F12 60.5(16) . . . . ?
C1E C13 C16 F12 -116.1(13) . . . . ?
C12 C13 C16 F11 -175.4(13) . . . . ?
C1E C13 C16 F11 8(2) . . . . ?
C45 N2 C41 C42 -0.4(14) . . . . ?
Dy2 N2 C41 C42 173.1(7) . . . . ?
Dy1 O2 C17 O1 27.5(11) . . . . ?
Dy1 O2 C17 C18 -153.5(5) . . . . ?
O2 C17 C18 C19 13.2(10) . . . . ?
O1 C17 C18 C19 -167.7(7) . . . . ?
O2 C17 C18 C23 -167.1(7) . . . . ?
O1 C17 C18 C23 12.0(10) . . . . ?
C19 C18 C23 C22 -0.8(12) . . . . ?
C17 C18 C23 C22 179.6(7) . . . . ?
C35 C34 C39 C38 -3.4(13) . . . . ?
C33 C34 C39 C38 176.7(8) . . . . ?
Dy1 O7 C9 O8 -28.5(15) . . . . ?
Dy1 O7 C9 C10 152.5(7) . . . . ?
Dy2 O8 C9 O7 2.7(12) 1_655 . . . ?
Dy2 O8 C9 C10 -178.4(4) 1_655 . . . ?
C1E C15 C10 C11 -1.0(17) . . . . ?
C1E C15 C10 C9 180.0(10) . . . . ?
C12 C11 C10 C15 1.8(13) . . . . ?
C12 C11 C10 C9 -179.2(7) . . . . ?
O7 C9 C10 C15 -4.0(12) . . . . ?
O8 C9 C10 C15 176.9(8) . . . . ?
O7 C9 C10 C11 177.0(7) . . . . ?
O8 C9 C10 C11 -2.0(11) . . . . ?
C46 N1 C50 C49 0.7(12) . . . . ?
Dy2 N1 C50 C49 -175.3(7) . . . . ?
C50 N1 C46 C47 -3.0(12) . . . . ?
Dy2 N1 C46 C47 173.0(7) . . . . ?
C50 N1 C46 C45 178.5(7) . . . . ?
Dy2 N1 C46 C45 -5.5(10) . . . . ?
N2 C45 C46 N1 0.1(11) . . . . ?
C44 C45 C46 N1 178.6(8) . . . . ?
N2 C45 C46 C47 -178.4(8) . . . . ?
C44 C45 C46 C47 0.0(13) . . . . ?
C23 C18 C19 C20 -0.3(12) . . . . ?
C17 C18 C19 C20 179.4(8) . . . . ?
C10 C11 C12 F9 178.8(8) . . . . ?
C10 C11 C12 C13 0.7(14) . . . . ?
C1E C13 C12 F9 177.9(10) . . . . ?
C16 C13 C12 F9 1.2(15) . . . . ?
C1E C13 C12 C11 -4.0(16) . . . . ?
C16 C13 C12 C11 179.3(10) . . . . ?
Dy1 O10 C25 O9 28.1(13) . . . . ?
Dy1 O10 C25 C26 -150.5(6) . . . . ?
Dy2 O9 C25 O10 -16.5(13) 3_544 . . . ?
Dy2 O9 C25 C26 162.2(6) 3_544 . . . ?
O10 C25 C26 C27 158.8(8) . . . . ?
O9 C25 C26 C27 -19.9(11) . . . . ?
O10 C25 C26 C31 -19.3(11) . . . . ?
O9 C25 C26 C31 161.9(7) . . . . ?
F5 C30 C31 C26 -179.2(7) . . . . ?
C1D C30 C31 C26 -0.5(13) . . . . ?
C27 C26 C31 C30 1.9(12) . . . . ?
C25 C26 C31 C30 180.0(8) . . . . ?
C22 C21 C20 F1 178.1(8) . . . . ?
C24 C21 C20 F1 1.6(14) . . . . ?
C22 C21 C20 C19 -4.9(14) . . . . ?
C24 C21 C20 C19 178.6(10) . . . . ?
C18 C19 C20 F1 -179.8(8) . . . . ?
C18 C19 C20 C21 3.2(14) . . . . ?
Dy1 O4 C1 O3 27.9(12) . . . . ?
Dy1 O4 C1 C4 -155.2(5) . . . . ?
Dy2 O3 C1 O4 48.9(9) 1_655 . . . ?
Dy2 O3 C1 C4 -128.0(6) 1_655 . . . ?
Dy1 O5 C33 O6 -121.8(9) . . . . ?
Dy1 O5 C33 C34 58.6(13) . . . . ?
Dy2 O6 C33 O5 -66.2(13) . . . . ?
Dy2 O6 C33 C34 113.5(8) . . . . ?
C35 C34 C33 O5 5.9(12) . . . . ?
C39 C34 C33 O5 -174.2(8) . . . . ?
C35 C34 C33 O6 -173.8(8) . . . . ?
C39 C34 C33 O6 6.1(11) . . . . ?
F16 C40 C37 C38 -2.5(14) . . . . ?
F15 C40 C37 C38 119.9(10) . . . . ?
F14 C40 C37 C38 -120.8(10) . . . . ?
F16 C40 C37 C36 178.7(9) . . . . ?
F15 C40 C37 C36 -58.8(14) . . . . ?
F14 C40 C37 C36 60.5(12) . . . . ?
C5 C3 C4 C14 0.6(12) . . . . ?
C5 C3 C4 C1 176.7(7) . . . . ?
O4 C1 C4 C14 -6.2(11) . . . . ?
O3 C1 C4 C14 170.9(7) . . . . ?
O4 C1 C4 C3 177.8(7) . . . . ?
O3 C1 C4 C3 -5.1(10) . . . . ?
C4 C3 C5 C7 -1.8(13) . . . . ?
F17 C6 C7 C5 178.8(8) . . . . ?
C14 C6 C7 C5 -0.8(15) . . . . ?
F17 C6 C7 C8 -3.0(14) . . . . ?
C14 C6 C7 C8 177.4(9) . . . . ?
C3 C5 C7 C6 1.9(13) . . . . ?
C3 C5 C7 C8 -176.4(8) . . . . ?
C39 C34 C35 C36 2.7(13) . . . . ?
C33 C34 C35 C36 -177.4(8) . . . . ?
C6 C7 C8 F18 -62.2(14) . . . . ?
C5 C7 C8 F18 116.0(11) . . . . ?
C6 C7 C8 F19 62.5(14) . . . . ?
C5 C7 C8 F19 -119.2(12) . . . . ?
C6 C7 C8 F20 179.8(9) . . . . ?
C5 C7 C8 F20 -2.0(13) . . . . ?
C36 C37 C38 C39 -0.1(14) . . . . ?
C40 C37 C38 C39 -178.8(9) . . . . ?
C34 C39 C38 C37 2.0(13) . . . . ?
C31 C26 C27 C28 -0.2(14) . . . . ?
C25 C26 C27 C28 -178.3(9) . . . . ?
C38 C37 C36 F13 179.9(9) . . . . ?
C40 C37 C36 F13 -1.3(15) . . . . ?
C38 C37 C36 C35 -0.5(16) . . . . ?
C40 C37 C36 C35 178.2(10) . . . . ?
C34 C35 C36 F13 178.8(8) . . . . ?
C34 C35 C36 C37 -0.8(15) . . . . ?
F17 C6 C14 C4 -179.9(8) . . . . ?
C7 C6 C14 C4 -0.3(15) . . . . ?
C3 C4 C14 C6 0.4(13) . . . . ?
C1 C4 C14 C6 -175.6(8) . . . . ?
C44 C43 C42 C41 -1.5(15) . . . . ?
N2 C41 C42 C43 0.9(15) . . . . ?
C20 C21 C22 C23 3.7(14) . . . . ?
C24 C21 C22 C23 -179.7(9) . . . . ?
C18 C23 C22 C21 -0.9(13) . . . . ?
N1 C46 C47 C48 2.6(15) . . . . ?
C45 C46 C47 C48 -178.9(9) . . . . ?
C46 C47 C48 C49 0.2(17) . . . . ?
F5 C30 C1D C28 176.2(9) . . . . ?
C31 C30 C1D C28 -2.6(14) . . . . ?
F5 C30 C1D C32 -1.3(14) . . . . ?
C31 C30 C1D C32 179.9(9) . . . . ?
F6 C32 C1D C30 56.5(16) . . . . ?
F7 C32 C1D C30 -61.6(15) . . . . ?
F8 C32 C1D C30 179.8(10) . . . . ?
F6 C32 C1D C28 -120.9(13) . . . . ?
F7 C32 C1D C28 120.9(13) . . . . ?
F8 C32 C1D C28 2.3(17) . . . . ?
C12 C13 C1E C15 4.6(19) . . . . ?
C16 C13 C1E C15 -178.7(12) . . . . ?
C10 C15 C1E C13 -2(2) . . . . ?
C20 C21 C24 F2 -176.5(10) . . . . ?
C22 C21 C24 F2 6.9(16) . . . . ?
C20 C21 C24 F3 -53.9(15) . . . . ?
C22 C21 C24 F3 129.5(11) . . . . ?
C20 C21 C24 F4 62.9(14) . . . . ?
C22 C21 C24 F4 -113.7(11) . . . . ?
C47 C48 C49 C50 -2.4(16) . . . . ?
N1 C50 C49 C48 2.0(15) . . . . ?
C26 C27 C28 C1D -2.8(15) . . . . ?
C30 C1D C28 C27 4.2(15) . . . . ?
C32 C1D C28 C27 -178.3(10) . . . . ?
C42 C43 C44 C45 1.6(16) . . . . ?
N2 C45 C44 C43 -1.1(14) . . . . ?
C46 C45 C44 C43 -179.5(9) . . . . ?

_diffrn_measured_fraction_theta_max 0.966
_diffrn_reflns_theta_full        25.01
_diffrn_measured_fraction_theta_full 0.966
_refine_diff_density_max         1.900
_refine_diff_density_min         -1.281
_refine_diff_density_rms         0.135
_database_code_depnum_ccdc_archive 'CCDC 989712'
#######################################################################
#
#                 Cambridge Crystallographic Data Centre
#                                CCDC 
# 
#######################################################################
# 
#  This CIF contains data from an original supplementary publication
#  deposited with the CCDC, and may include chemical, crystal,
#  experimental, refinement, atomic coordinates,
#  anisotropic displacement parameters and molecular geometry data,
#  as required by the journal to which it was submitted.
#
#  This CIF is provided on the understanding that it is used for bona
#  fide research purposes only. It may contain copyright material
#  of the CCDC or of third parties, and may not be copied or further
#  disseminated in any form, whether machine-readable or not,
#  except for the purpose of generating routine backup copies
#  on your local computer system.
# 
#  For further information on the CCDC, data deposition and
#  data retrieval see:
#                         www.ccdc.cam.ac.uk
#
#  Bona fide researchers may freely download Mercury and enCIFer
#  from this site to visualise CIF-encoded structures and 
#  to carry out CIF format checking respectively.
#
data_2

_audit_creation_method           SHELXL-2013
_chemical_name_systematic        
;
 ?
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         'C196 H94 Dy10 F88 N4 O54'
_chemical_formula_sum            'C196 H94 Dy10 F88 N4 O54'
_chemical_formula_weight         6665.75

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           4
_space_group_name_H-M_alt        'P 21'
_space_group_name_Hall           'P 2yb'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z'

_cell_length_a                   16.0773(6)
_cell_length_b                   32.033(2)
_cell_length_c                   23.3478(9)
_cell_angle_alpha                90
_cell_angle_beta                 107.376(4)
_cell_angle_gamma                90
_cell_volume                     11475.4(10)
_cell_formula_units_Z            2
_cell_measurement_temperature    128(9)
_cell_measurement_reflns_used    4793
_cell_measurement_theta_min      2.11
_cell_measurement_theta_max      25.16

_exptl_crystal_description       rhomb
_exptl_crystal_colour            colorless
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.929
_exptl_crystal_F_000             6364
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          0.24
_exptl_crystal_size_mid          0.22
_exptl_crystal_size_min          0.20
_exptl_absorpt_coefficient_mu    3.358
_shelx_estimated_absorpt_T_min   ?
_shelx_estimated_absorpt_T_max   ?
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.45
_exptl_absorpt_correction_T_max  0.51
_exptl_absorpt_process_details   'SADABS; Bruker, 2000'

_exptl_special_details           
;
 ?
;

_diffrn_ambient_temperature      128(9)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'Bruker Smart Aepex CCD'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            78951
_diffrn_reflns_av_unetI/netI     0.0809
_diffrn_reflns_av_R_equivalents  0.0251
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_k_min       -42
_diffrn_reflns_limit_k_max       40
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_theta_min         2.944
_diffrn_reflns_theta_max         28.000
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measured_fraction_theta_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.980
_diffrn_reflns_point_group_measured_fraction_full 0.996
_reflns_number_total             43895
_reflns_number_gt                37192
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.934
_reflns_Friedel_fraction_max     0.964
_reflns_Friedel_fraction_full    0.994

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

# SQUEEZE RESULTS
# Note: Data are Listed for all Voids in the P1 Unit Cell
# i.e. Centre of Gravity, Solvent Accessible Volume,
# Recovered number of Electrons in the Void and
# Details about the Squeezed Material
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 -0.003 0.417 0.672 13 2 ' '
2 0.002 0.917 0.328 13 2 ' '
3 0.105 0.795 0.065 28 3 ' '
4 0.350 1.016 0.106 422 52 ' '
5 0.119 0.631 0.437 9 1 ' '
6 0.210 0.186 0.289 19 3 ' '
7 0.317 0.320 0.105 42 5 ' '
8 0.650 0.516 0.894 422 52 ' '
9 0.309 0.695 0.665 16 2 ' '
10 0.323 0.130 0.297 8 1 ' '
11 0.365 0.254 0.433 16 3 ' '
12 0.408 0.770 0.952 33 5 ' '
13 0.462 0.851 0.396 22 3 ' '
14 0.537 0.351 0.604 22 3 ' '
15 0.592 0.270 0.048 33 5 ' '
16 0.683 0.820 0.895 42 5 ' '
17 0.635 0.754 0.567 16 3 ' '
18 0.690 0.194 0.335 16 2 ' '
19 0.677 0.630 0.703 7 1 ' '
20 0.790 0.686 0.711 19 3 ' '
21 0.894 0.295 0.935 28 3 ' '
22 0.881 0.131 0.562 9 1 ' '

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    ?
_computing_structure_refinement  'SHELXL-2013 (Sheldrick, 2013)'
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_special_details          
;
 Refined as a 2-component twin.
;
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           fullcycle
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
;
 w=1/[σ²(Fo²)+(0.08P)²+1.88P]
 where P=(Fo²+2Fc²)/3
;
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   mixed
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_abs_structure_details 
;
 Classical Flack method preferred over Parsons because s.u. lower.
;
_refine_ls_abs_structure_Flack   -0.004(6)
_chemical_absolute_configuration ?
_refine_ls_number_reflns         43895
_refine_ls_number_parameters     3170
_refine_ls_number_restraints     4
_refine_ls_R_factor_all          0.0515
_refine_ls_R_factor_gt           0.0507
_refine_ls_wR_factor_ref         0.1218
_refine_ls_wR_factor_gt          0.1216
_refine_ls_goodness_of_fit_ref   1.024
_refine_ls_restrained_S_all      1.024
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.6486(7) -0.0834(4) 0.4927(4) 0.047(2) Uani 1 1 d . . . . .
C2 C 0.5847(6) -0.1011(3) 0.5223(3) 0.0392(18) Uani 1 1 d . . . . .
C3 C 0.5331(6) -0.0714(3) 0.5373(3) 0.042(2) Uani 1 1 d . . . . .
H3 H 0.5382 -0.0434 0.5283 0.050 Uiso 1 1 calc R U . . .
C4 C 0.4737(6) -0.0838(4) 0.5658(4) 0.044(2) Uani 1 1 d . . . . .
C5 C 0.4690(7) -0.1269(3) 0.5847(3) 0.047(2) Uani 1 1 d . . . . .
C6 C 0.5246(7) -0.1540(3) 0.5701(4) 0.0421(19) Uani 1 1 d . . . . .
H6 H 0.5233 -0.1820 0.5802 0.051 Uiso 1 1 calc R U . . .
C7 C 0.5840(7) -0.1411(3) 0.5402(4) 0.043(2) Uani 1 1 d . . . . .
H7 H 0.6230 -0.1602 0.5326 0.051 Uiso 1 1 calc R U . . .
C8 C 0.4079(7) -0.1383(4) 0.6208(4) 0.048(2) Uani 1 1 d . . . . .
C9 C 0.9469(6) -0.1075(3) 0.5090(3) 0.0407(19) Uani 1 1 d . . . . .
C10 C 0.9827(6) -0.1494(3) 0.5110(3) 0.0396(18) Uani 1 1 d . . . . .
C11 C 1.0674(6) -0.1558(3) 0.5442(3) 0.0400(19) Uani 1 1 d . . . . .
H11 H 1.1014 -0.1337 0.5642 0.048 Uiso 1 1 calc R U . . .
C12 C 1.1031(7) -0.1969(3) 0.5478(4) 0.043(2) Uani 1 1 d . . . . .
C13 C 1.0505(6) -0.2293(3) 0.5170(3) 0.042(2) Uani 1 1 d . . . . .
C14 C 0.9635(7) -0.2228(4) 0.4842(4) 0.050(2) Uani 1 1 d . . . . .
H14 H 0.9290 -0.2448 0.4643 0.060 Uiso 1 1 calc R U . . .
C15 C 0.9297(7) -0.1826(3) 0.4818(4) 0.047(2) Uani 1 1 d . . . . .
H15 H 0.8716 -0.1776 0.4607 0.056 Uiso 1 1 calc R U . . .
C16 C 1.0860(7) -0.2738(4) 0.5216(4) 0.045(2) Uani 1 1 d . . . . .
C17 C 0.9362(6) -0.0092(3) 0.4103(3) 0.0416(19) Uani 1 1 d . . . . .
C18 C 0.9757(6) 0.0085(3) 0.3639(3) 0.0378(18) Uani 1 1 d . . . . .
C19 C 0.9330(7) 0.0138(4) 0.3056(4) 0.052(3) Uani 1 1 d . . . . .
H19 H 0.8766 0.0034 0.2912 0.063 Uiso 1 1 calc R U . . .
C20 C 0.9674(7) 0.0335(4) 0.2661(4) 0.054(3) Uani 1 1 d . . . . .
C21 C 1.0496(7) 0.0477(4) 0.2853(3) 0.045(2) Uani 1 1 d . . . . .
C22 C 1.0969(8) 0.0431(4) 0.3454(4) 0.052(3) Uani 1 1 d . . . . .
H22 H 1.1531 0.0539 0.3588 0.062 Uiso 1 1 calc R U . . .
C23 C 1.0620(6) 0.0224(4) 0.3869(4) 0.054(3) Uani 1 1 d . . . . .
H23 H 1.0943 0.0183 0.4268 0.065 Uiso 1 1 calc R U . . .
C24 C 1.0848(7) 0.0726(3) 0.2416(3) 0.045(2) Uani 1 1 d . . . . .
C25 C 0.6819(6) 0.0420(4) 0.4153(4) 0.045(2) Uani 1 1 d . . . . .
C26 C 0.6308(6) 0.0705(3) 0.3743(3) 0.042(2) Uani 1 1 d . . . . .
C27 C 0.6178(6) 0.0652(4) 0.3142(4) 0.051(3) Uani 1 1 d . . . . .
H27 H 0.6424 0.0424 0.3005 0.062 Uiso 1 1 calc R U . . .
C28 C 0.5683(7) 0.0934(3) 0.2738(3) 0.045(2) Uani 1 1 d . . . . .
C29 C 0.5320(8) 0.1279(3) 0.2923(3) 0.053(3) Uani 1 1 d . . . . .
C30 C 0.5425(9) 0.1338(4) 0.3565(4) 0.058(3) Uani 1 1 d . . . . .
H30 H 0.5184 0.1568 0.3702 0.070 Uiso 1 1 calc R U . . .
C31 C 0.5905(8) 0.1034(4) 0.3967(4) 0.054(3) Uani 1 1 d . . . . .
H31 H 0.5955 0.1049 0.4373 0.064 Uiso 1 1 calc R U . . .
C32 C 0.4740(7) 0.1571(4) 0.2486(4) 0.050(2) Uani 1 1 d . . . . .
C33 C 0.5657(6) 0.0479(4) 0.5945(3) 0.044(2) Uani 1 1 d . . . . .
C34 C 0.5001(7) 0.0727(5) 0.5531(4) 0.054(3) Uani 1 1 d . . . . .
C35 C 0.4773(7) 0.1114(4) 0.5731(4) 0.049(2) Uani 1 1 d . . . . .
H35 H 0.5061 0.1207 0.6117 0.059 Uiso 1 1 calc R U . . .
C36 C 0.4146(7) 0.1347(4) 0.5370(3) 0.050(2) Uani 1 1 d . . . . .
H36 H 0.3956 0.1587 0.5518 0.060 Uiso 1 1 calc R U . . .
C37 C 0.3767(8) 0.1231(4) 0.4761(3) 0.051(2) Uani 1 1 d . . . . .
C38 C 0.4014(7) 0.0852(4) 0.4558(3) 0.051(2) Uani 1 1 d . . . . .
C39 C 0.4675(6) 0.0611(4) 0.4952(3) 0.046(2) Uani 1 1 d . . . . .
H39 H 0.4886 0.0373 0.4813 0.055 Uiso 1 1 calc R U . . .
C40 C 0.2980(9) 0.1453(4) 0.4338(3) 0.053(3) Uani 1 1 d . . . . .
C41 C 0.8569(5) -0.0730(3) 0.6264(2) 0.0337(16) Uani 1 1 d . . . . .
C42 C 0.8809(6) -0.1175(3) 0.6294(3) 0.0376(17) Uani 1 1 d . . . . .
C43 C 0.9603(7) -0.1325(4) 0.6626(4) 0.048(2) Uani 1 1 d . . . . .
H43 H 1.0048 -0.1138 0.6802 0.057 Uiso 1 1 calc R U . . .
C44 C 0.9757(5) -0.1753(3) 0.6706(3) 0.0338(16) Uani 1 1 d . . . . .
C45 C 0.9137(7) -0.2035(4) 0.6383(4) 0.048(2) Uani 1 1 d . . . . .
C46 C 0.8335(7) -0.1893(3) 0.6028(4) 0.048(2) Uani 1 1 d . . . . .
H46 H 0.7908 -0.2082 0.5827 0.058 Uiso 1 1 calc R U . . .
C47 C 0.8168(6) -0.1448(3) 0.5971(4) 0.0415(18) Uani 1 1 d . . . . .
H47 H 0.7641 -0.1347 0.5723 0.050 Uiso 1 1 calc R U . . .
C48 C 0.9324(7) -0.2501(4) 0.6409(3) 0.047(2) Uani 1 1 d . . . . .
C49 C 0.7241(6) 0.1101(3) 0.6214(3) 0.0382(17) Uani 1 1 d . . . . .
C50 C 0.6940(6) 0.1501(3) 0.5933(3) 0.0384(18) Uani 1 1 d . . . . .
C51 C 0.6978(6) 0.1590(3) 0.5338(3) 0.0373(17) Uani 1 1 d . . . . .
H51 H 0.7222 0.1398 0.5136 0.045 Uiso 1 1 calc R U . . .
C52 C 0.6656(7) 0.1958(3) 0.5073(3) 0.042(2) Uani 1 1 d . . . . .
C53 C 0.6299(7) 0.2249(3) 0.5355(4) 0.044(2) Uani 1 1 d . . . . .
C54 C 0.6283(7) 0.2182(4) 0.5951(3) 0.046(2) Uani 1 1 d . . . . .
H54 H 0.6059 0.2385 0.6148 0.055 Uiso 1 1 calc R U . . .
C55 C 0.6610(7) 0.1805(4) 0.6244(4) 0.045(2) Uani 1 1 d . . . . .
H55 H 0.6607 0.1757 0.6636 0.054 Uiso 1 1 calc R U . . .
C56 C 0.5976(7) 0.2657(3) 0.5063(4) 0.044(2) Uani 1 1 d . . . . .
C57 C 1.1947(7) -0.0087(4) 0.5594(4) 0.047(2) Uani 1 1 d . . . . .
C58 C 1.2101(7) -0.0292(3) 0.5087(4) 0.0393(18) Uani 1 1 d . . . . .
C59 C 1.2755(6) -0.0176(4) 0.4848(3) 0.046(2) Uani 1 1 d . . . . .
H59 H 1.3097 0.0055 0.5003 0.055 Uiso 1 1 calc R U . . .
C60 C 1.2913(7) -0.0399(3) 0.4379(3) 0.042(2) Uani 1 1 d . . . . .
C61 C 1.2409(9) -0.0745(4) 0.4152(4) 0.054(3) Uani 1 1 d . . . . .
C62 C 1.1739(7) -0.0862(4) 0.4381(4) 0.046(2) Uani 1 1 d . . . . .
H62 H 1.1385 -0.1088 0.4218 0.055 Uiso 1 1 calc R U . . .
C63 C 1.1598(6) -0.0640(4) 0.4856(3) 0.048(2) Uani 1 1 d . . . . .
H63 H 1.1164 -0.0725 0.5019 0.058 Uiso 1 1 calc R U . . .
C64 C 1.2504(7) -0.0973(4) 0.3619(4) 0.0477(19) Uani 1 1 d . U . . .
C65 C 1.0626(6) 0.0831(3) 0.5399(3) 0.0409(19) Uani 1 1 d D . . . .
C66 C 1.0110(6) 0.0987(3) 0.4790(3) 0.0408(19) Uani 1 1 d D . . . .
C67 C 1.0524(7) 0.1215(4) 0.4452(3) 0.046(2) Uani 1 1 d . . . . .
H67 H 1.1123 0.1260 0.4594 0.056 Uiso 1 1 calc R U . . .
C68 C 1.0033(7) 0.1383(4) 0.3883(4) 0.052(3) Uani 1 1 d . . . . .
C69 C 0.9146(7) 0.1317(4) 0.3691(4) 0.046(2) Uani 1 1 d . . . . .
C70 C 0.8743(7) 0.1092(4) 0.4032(3) 0.043(2) Uani 1 1 d . . . . .
H70 H 0.8145 0.1048 0.3891 0.052 Uiso 1 1 calc R U . . .
C71 C 0.9214(7) 0.0928(3) 0.4583(3) 0.0392(18) Uani 1 1 d . . . . .
H71 H 0.8931 0.0781 0.4813 0.047 Uiso 1 1 calc R U . . .
C72 C 0.8653(9) 0.1479(4) 0.3079(4) 0.056(3) Uani 1 1 d . . . . .
C73 C 1.0185(6) 0.1122(3) 0.6783(4) 0.0403(17) Uani 1 1 d . . . . .
C74 C 0.9981(6) 0.1559(3) 0.6830(3) 0.0386(18) Uani 1 1 d . . . . .
C75 C 1.0584(7) 0.1852(4) 0.6733(3) 0.046(2) Uani 1 1 d . . . . .
H75 H 1.1127 0.1766 0.6712 0.055 Uiso 1 1 calc R U . . .
C76 C 1.0334(7) 0.2293(4) 0.6667(4) 0.047(2) Uani 1 1 d . . . . .
C77 C 0.9479(7) 0.2410(3) 0.6691(4) 0.044(2) Uani 1 1 d . . . . .
C78 C 0.8917(7) 0.2104(4) 0.6789(5) 0.051(2) Uani 1 1 d . . . . .
H78 H 0.8374 0.2181 0.6818 0.061 Uiso 1 1 calc R U . . .
C79 C 0.9156(6) 0.1689(4) 0.6845(4) 0.044(2) Uani 1 1 d . . . . .
H79 H 0.8760 0.1490 0.6893 0.052 Uiso 1 1 calc R U . . .
C80 C 0.9197(8) 0.2835(4) 0.6619(4) 0.050(2) Uani 1 1 d . . . . .
C81 C 0.7960(6) 0.1369(3) 0.8129(3) 0.0376(17) Uani 1 1 d . . . . .
C82 C 0.7788(7) 0.1817(4) 0.8013(4) 0.051(3) Uani 1 1 d . . . . .
C83 C 0.6960(7) 0.1958(4) 0.7775(4) 0.050(2) Uani 1 1 d . . . . .
H83 H 0.6509 0.1765 0.7663 0.060 Uiso 1 1 calc R U . . .
C84 C 0.6759(7) 0.2383(4) 0.7691(4) 0.044(2) Uani 1 1 d . . . . .
C85 C 0.7451(7) 0.2673(3) 0.7817(3) 0.0423(19) Uani 1 1 d . . . . .
C86 C 0.8292(8) 0.2536(4) 0.8040(4) 0.052(3) Uani 1 1 d . . . . .
H86 H 0.8747 0.2727 0.8140 0.063 Uiso 1 1 calc R U . . .
C87 C 0.8472(7) 0.2108(4) 0.8119(4) 0.049(2) Uani 1 1 d . . . . .
H87 H 0.9046 0.2016 0.8243 0.059 Uiso 1 1 calc R U . . .
C88 C 0.7142(8) 0.3100(4) 0.7677(4) 0.051(2) Uani 1 1 d . . . . .
C89 C 0.6223(8) -0.0434(4) 0.7499(4) 0.048(2) Uani 1 1 d . . . . .
C90 C 0.6327(8) -0.0902(4) 0.7526(4) 0.046(2) Uani 1 1 d . . . . .
C91 C 0.7127(8) -0.1075(4) 0.7434(4) 0.048(2) Uani 1 1 d . . . . .
H91 H 0.7562 -0.0903 0.7378 0.057 Uiso 1 1 calc R U . . .
C92 C 0.7199(7) -0.1505(4) 0.7433(4) 0.050(2) Uani 1 1 d . . . . .
C93 C 0.6540(8) -0.1756(4) 0.7504(4) 0.051(2) Uani 1 1 d . . . . .
C94 C 0.5805(7) -0.1578(3) 0.7618(4) 0.045(2) Uani 1 1 d . . . . .
H94 H 0.5374 -0.1745 0.7691 0.054 Uiso 1 1 calc R U . . .
C95 C 0.5739(7) -0.1144(4) 0.7618(4) 0.048(2) Uani 1 1 d . . . . .
H95 H 0.5251 -0.1025 0.7688 0.058 Uiso 1 1 calc R U . . .
C96 C 0.6661(6) -0.2223(3) 0.7538(4) 0.0417(19) Uani 1 1 d . . . . .
C97 C 0.2842(6) -0.0359(4) 0.7224(3) 0.043(2) Uani 1 1 d . . . . .
C98 C 0.2900(7) -0.0824(4) 0.7336(4) 0.049(2) Uani 1 1 d . . . . .
C99 C 0.3589(6) -0.0972(3) 0.7807(3) 0.043(2) Uani 1 1 d . . . . .
H99 H 0.3980 -0.0786 0.8054 0.051 Uiso 1 1 calc R U . . .
C100 C 0.3686(6) -0.1396(4) 0.7905(3) 0.042(2) Uani 1 1 d . . . . .
C101 C 0.3047(7) -0.1674(3) 0.7548(3) 0.043(2) Uani 1 1 d . . . . .
C102 C 0.2359(9) -0.1525(4) 0.7075(5) 0.057(3) Uani 1 1 d . . . . .
H102 H 0.1963 -0.1707 0.6823 0.069 Uiso 1 1 calc R U . . .
C103 C 0.2283(7) -0.1082(4) 0.6988(4) 0.049(2) Uani 1 1 d . . . . .
H103 H 0.1810 -0.0972 0.6693 0.058 Uiso 1 1 calc R U . . .
C104 C 0.3058(7) -0.2169(4) 0.7606(4) 0.046(2) Uani 1 1 d . . . . .
C105 C 0.3639(6) 0.1053(3) 0.6961(3) 0.0393(18) Uani 1 1 d . . . . .
C106 C 0.3498(7) 0.1481(3) 0.6735(3) 0.043(2) Uani 1 1 d . . . . .
C107 C 0.2778(8) 0.1612(4) 0.6285(4) 0.059(3) Uani 1 1 d . . . . .
H107 H 0.2326 0.1425 0.6129 0.071 Uiso 1 1 calc R U . . .
C108 C 0.2706(7) 0.2013(4) 0.6060(4) 0.049(2) Uani 1 1 d . . . . .
C109 C 0.3377(7) 0.2292(4) 0.6297(4) 0.052(3) Uani 1 1 d . . . . .
C110 C 0.4126(6) 0.2166(4) 0.6750(3) 0.043(2) Uani 1 1 d . . . . .
H110 H 0.4579 0.2354 0.6906 0.052 Uiso 1 1 calc R U . . .
C111 C 0.4184(6) 0.1762(3) 0.6961(3) 0.044(2) Uani 1 1 d . . . . .
H111 H 0.4683 0.1675 0.7256 0.053 Uiso 1 1 calc R U . . .
C112 C 0.3315(7) 0.2736(4) 0.6038(3) 0.049(2) Uani 1 1 d . . . . .
C113 C 0.4498(6) 0.0793(4) 0.8647(4) 0.045(2) Uani 1 1 d . . . . .
C114 C 0.4359(7) 0.1060(3) 0.9117(3) 0.0405(18) Uani 1 1 d . . . . .
C115 C 0.3567(6) 0.1065(3) 0.9215(3) 0.0411(19) Uani 1 1 d . . . . .
H115 H 0.3141 0.0883 0.8993 0.049 Uiso 1 1 calc R U . . .
C116 C 0.3361(6) 0.1323(3) 0.9622(3) 0.0348(16) Uani 1 1 d . . . . .
C117 C 0.3993(7) 0.1608(3) 0.9951(4) 0.0440(19) Uani 1 1 d . . . . .
C118 C 0.4816(7) 0.1600(4) 0.9861(4) 0.046(2) Uani 1 1 d . . . . .
H118 H 0.5262 0.1769 1.0090 0.055 Uiso 1 1 calc R U . . .
C119 C 0.4961(8) 0.1340(4) 0.9434(4) 0.049(2) Uani 1 1 d . . . . .
H119 H 0.5495 0.1356 0.9357 0.059 Uiso 1 1 calc R U . . .
C120 C 0.3790(7) 0.1884(4) 1.0387(4) 0.050(2) Uani 1 1 d . . . . .
C121 C 0.7091(6) 0.1744(3) 0.9223(4) 0.0399(18) Uani 1 1 d . . . . .
C122 C 0.6719(7) 0.2169(3) 0.9186(3) 0.049(2) Uani 1 1 d . . . . .
C123 C 0.5834(8) 0.2195(4) 0.8894(3) 0.051(2) Uani 1 1 d . . . . .
H123 H 0.5520 0.1954 0.8747 0.061 Uiso 1 1 calc R U . . .
C124 C 0.5418(6) 0.2575(3) 0.8820(3) 0.0394(18) Uani 1 1 d . . . . .
C125 C 0.5875(5) 0.2938(3) 0.9053(3) 0.0345(16) Uani 1 1 d . . . . .
C126 C 0.6789(7) 0.2916(4) 0.9327(4) 0.048(2) Uani 1 1 d . . . . .
H126 H 0.7110 0.3157 0.9461 0.058 Uiso 1 1 calc R U . . .
C127 C 0.7191(7) 0.2535(4) 0.9389(4) 0.045(2) Uani 1 1 d . . . . .
H127 H 0.7789 0.2519 0.9570 0.053 Uiso 1 1 calc R U . . .
C128 C 0.5338(7) 0.3328(4) 0.9031(4) 0.046(2) Uani 1 1 d . . . . .
C129 C 0.6917(6) 0.0837(4) 1.0181(3) 0.044(2) Uani 1 1 d . . . . .
C130 C 0.6831(6) 0.0550(4) 1.0665(3) 0.045(2) Uani 1 1 d . . . . .
C131 C 0.6307(7) 0.0193(4) 1.0511(3) 0.047(2) Uani 1 1 d . . . . .
H131 H 0.5996 0.0138 1.0114 0.056 Uiso 1 1 calc R U . . .
C132 C 0.6265(7) -0.0077(4) 1.0975(4) 0.046(2) Uani 1 1 d . . . . .
C133 C 0.6717(6) 0.0010(3) 1.1555(3) 0.0389(18) Uani 1 1 d . . . . .
C134 C 0.7245(8) 0.0349(4) 1.1704(4) 0.052(3) Uani 1 1 d . . . . .
H134 H 0.7567 0.0398 1.2101 0.063 Uiso 1 1 calc R U . . .
C135 C 0.7293(6) 0.0617(3) 1.1259(3) 0.0390(18) Uani 1 1 d . . . . .
H135 H 0.7647 0.0852 1.1359 0.047 Uiso 1 1 calc R U . . .
C136 C 0.6600(7) -0.0291(4) 1.2053(4) 0.045(2) Uani 1 1 d . . . . .
C137 C 0.5887(6) -0.0222(3) 0.8872(4) 0.0394(17) Uani 1 1 d . . . . .
C138 C 0.6069(6) -0.0565(4) 0.9259(3) 0.047(3) Uani 1 1 d . . . . .
C139 C 0.6942(6) -0.0586(3) 0.9583(3) 0.0408(19) Uani 1 1 d . . . . .
H139 H 0.7326 -0.0378 0.9545 0.049 Uiso 1 1 calc R U . . .
C140 C 0.7235(8) -0.0921(4) 0.9968(5) 0.054(2) Uani 1 1 d . . . . .
C141 C 0.6681(7) -0.1233(4) 1.0009(4) 0.047(2) Uani 1 1 d . . . . .
C142 C 0.5792(7) -0.1224(4) 0.9660(4) 0.053(3) Uani 1 1 d . . . . .
H142 H 0.5422 -0.1442 0.9685 0.064 Uiso 1 1 calc R U . . .
C143 C 0.5470(7) -0.0882(4) 0.9272(4) 0.049(2) Uani 1 1 d . . . . .
H143 H 0.4891 -0.0868 0.9038 0.059 Uiso 1 1 calc R U . . .
C144 C 0.6998(7) -0.1610(4) 1.0394(3) 0.046(2) Uani 1 1 d . . . . .
C145 C 1.0800(6) 0.0128(4) 0.8412(3) 0.0424(19) Uani 1 1 d . . . . .
C146 C 1.1077(7) -0.0309(4) 0.8594(3) 0.046(2) Uani 1 1 d . . . . .
C147 C 1.1088(7) -0.0459(3) 0.9162(4) 0.046(2) Uani 1 1 d . . . . .
H147 H 1.0947 -0.0281 0.9434 0.055 Uiso 1 1 calc R U . . .
C148 C 1.1310(7) -0.0869(4) 0.9318(4) 0.045(2) Uani 1 1 d . . . . .
C149 C 1.1571(7) -0.1120(4) 0.8929(4) 0.048(2) Uani 1 1 d . . . . .
C150 C 1.1576(7) -0.0981(4) 0.8369(3) 0.049(2) Uani 1 1 d . . . . .
H150 H 1.1740 -0.1159 0.8107 0.059 Uiso 1 1 calc R U . . .
C151 C 1.1334(7) -0.0571(4) 0.8203(4) 0.049(2) Uani 1 1 d . . . . .
H151 H 1.1345 -0.0472 0.7830 0.059 Uiso 1 1 calc R U . . .
C152 C 1.1862(7) -0.1571(3) 0.9115(4) 0.046(2) Uani 1 1 d . . . . .
C153 C 1.0019(6) 0.1395(3) 0.9320(3) 0.044(2) Uani 1 1 d . . . . .
C154 C 1.0685(7) 0.1583(3) 0.9051(4) 0.047(2) Uani 1 1 d . . . . .
C155 C 1.0883(7) 0.2012(3) 0.9158(4) 0.047(2) Uani 1 1 d . . . . .
H155 H 1.0604 0.2169 0.9381 0.056 Uiso 1 1 calc R U . . .
C156 C 1.1494(6) 0.2196(3) 0.8929(3) 0.043(2) Uani 1 1 d . . . . .
C157 C 1.1894(7) 0.1963(4) 0.8567(4) 0.049(2) Uani 1 1 d . . . . .
C158 C 1.1644(7) 0.1557(4) 0.8434(3) 0.045(2) Uani 1 1 d . . . . .
H158 H 1.1862 0.1414 0.8163 0.054 Uiso 1 1 calc R U . . .
C159 C 1.1072(8) 0.1346(4) 0.8692(4) 0.052(3) Uani 1 1 d . . . . .
H159 H 1.0955 0.1063 0.8626 0.062 Uiso 1 1 calc R U . . .
C160 C 1.2505(8) 0.2182(4) 0.8293(4) 0.050(2) Uani 1 1 d . . . . .
C161 C 0.9450(6) 0.0203(3) 1.0106(3) 0.045(2) Uani 1 1 d . . . . .
C162 C 0.9441(6) -0.0170(3) 1.0488(3) 0.0403(18) Uani 1 1 d . . . . .
C163 C 0.9184(7) -0.0160(3) 1.1013(4) 0.045(2) Uani 1 1 d . . . . .
H163 H 0.8929 0.0078 1.1115 0.054 Uiso 1 1 calc R U . . .
C164 C 0.9311(7) -0.0494(4) 1.1361(4) 0.051(2) Uani 1 1 d . . . . .
C165 C 0.9731(7) -0.0864(3) 1.1264(3) 0.044(2) Uani 1 1 d . . . . .
C166 C 1.0016(8) -0.0873(4) 1.0739(4) 0.052(3) Uani 1 1 d . . . . .
H166 H 1.0300 -0.1107 1.0652 0.062 Uiso 1 1 calc R U . . .
C167 C 0.9859(7) -0.0521(3) 1.0355(4) 0.044(2) Uani 1 1 d . . . . .
H167 H 1.0037 -0.0525 1.0011 0.053 Uiso 1 1 calc R U . . .
C168 C 0.9848(7) -0.1234(3) 1.1664(4) 0.0434(17) Uani 1 1 d . U . . .
C169 C 0.8974(7) -0.0446(3) 0.8093(3) 0.045(2) Uani 1 1 d . . . . .
C170 C 0.9048(8) -0.0873(4) 0.8363(4) 0.047(2) Uani 1 1 d . . . . .
C171 C 0.9111(8) -0.1260(4) 0.8062(4) 0.047(2) Uani 1 1 d . . . . .
H171 H 0.9094 -0.1261 0.7661 0.056 Uiso 1 1 calc R U . . .
C172 C 0.9195(8) -0.1623(4) 0.8376(5) 0.055(3) Uani 1 1 d . . . . .
C173 C 0.9206(8) -0.1642(4) 0.8959(5) 0.052(2) Uani 1 1 d . . . . .
C174 C 0.9150(8) -0.1260(4) 0.9252(4) 0.050(2) Uani 1 1 d . . . . .
H174 H 0.9175 -0.1263 0.9656 0.060 Uiso 1 1 calc R U . . .
C175 C 0.9063(8) -0.0898(4) 0.8963(4) 0.055(3) Uani 1 1 d . . . . .
H175 H 0.9010 -0.0655 0.9165 0.066 Uiso 1 1 calc R U . . .
C176 C 0.9324(8) -0.2046(4) 0.9307(4) 0.052(2) Uani 1 1 d . . . . .
C177 C 0.8336(6) -0.1260(3) 0.3377(3) 0.0384(18) Uani 1 1 d . . . . .
H177 H 0.8877 -0.1191 0.3641 0.046 Uiso 1 1 calc R U . . .
C178 C 0.8294(8) -0.1533(4) 0.2927(4) 0.054(3) Uani 1 1 d . . . . .
H178 H 0.8802 -0.1647 0.2879 0.065 Uiso 1 1 calc R U . . .
C179 C 0.7467(7) -0.1643(4) 0.2527(4) 0.051(2) Uani 1 1 d . . . . .
H179 H 0.7431 -0.1835 0.2222 0.061 Uiso 1 1 calc R U . . .
C180 C 0.6730(6) -0.1468(4) 0.2592(3) 0.045(2) Uani 1 1 d . . . . .
H180 H 0.6192 -0.1542 0.2328 0.054 Uiso 1 1 d R U . . .
C181 C 0.6773(6) -0.1186(4) 0.3060(3) 0.043(2) Uani 1 1 d . . . . .
C182 C 0.6035(7) -0.1012(4) 0.3139(3) 0.049(2) Uani 1 1 d . . . . .
C183 C 0.5191(7) -0.1117(3) 0.2781(3) 0.0427(19) Uani 1 1 d . . . . .
H183 H 0.5121 -0.1346 0.2526 0.051 Uiso 1 1 d R U . . .
C184 C 0.4490(7) -0.0904(3) 0.2788(3) 0.0393(18) Uani 1 1 d . . . . .
H184 H 0.3952 -0.0969 0.2517 0.047 Uiso 1 1 calc R U . . .
C185 C 0.4553(7) -0.0575(4) 0.3208(4) 0.051(3) Uani 1 1 d . . . . .
H185 H 0.4057 -0.0447 0.3254 0.061 Uiso 1 1 calc R U . . .
C186 C 0.5392(7) -0.0450(3) 0.3552(4) 0.045(2) Uani 1 1 d . . . . .
H186 H 0.5463 -0.0220 0.3805 0.054 Uiso 1 1 calc R U . . .
C187 C 0.8083(7) 0.1858(3) 1.0887(3) 0.0405(18) Uani 1 1 d . . . . .
H187 H 0.7579 0.1755 1.0612 0.049 Uiso 1 1 calc R U . . .
C188 C 0.8044(7) 0.2164(3) 1.1322(3) 0.0387(18) Uani 1 1 d . . . . .
H188 H 0.7509 0.2274 1.1323 0.046 Uiso 1 1 calc R U . . .
C189 C 0.8829(8) 0.2302(4) 1.1757(4) 0.053(3) Uani 1 1 d . . . . .
H189 H 0.8809 0.2492 1.2054 0.063 Uiso 1 1 calc R U . . .
C190 C 0.9629(8) 0.2144(3) 1.1725(3) 0.049(2) Uani 1 1 d . . . . .
H190 H 1.0140 0.2234 1.2004 0.059 Uiso 1 1 calc R U . . .
C191 C 0.9683(7) 0.1853(4) 1.1286(4) 0.051(3) Uani 1 1 d . . . . .
C192 C 1.0466(6) 0.1646(4) 1.1233(3) 0.044(2) Uani 1 1 d . . . . .
C193 C 1.1312(7) 0.1761(4) 1.1580(3) 0.055(3) Uani 1 1 d . . . . .
H193 H 1.1385 0.1977 1.1855 0.066 Uiso 1 1 calc R U . . .
C194 C 1.2032(8) 0.1558(4) 1.1517(4) 0.056(3) Uani 1 1 d . . . . .
H194 H 1.2586 0.1645 1.1740 0.067 Uiso 1 1 calc R U . . .
C195 C 1.1936(7) 0.1215(5) 1.1113(4) 0.053(3) Uani 1 1 d . . . . .
H195 H 1.2424 0.1076 1.1073 0.063 Uiso 1 1 calc R U . . .
C196 C 1.1106(7) 0.1090(3) 1.0780(4) 0.044(2) Uani 1 1 d . . . . .
H196 H 1.1032 0.0863 1.0521 0.053 Uiso 1 1 calc R U . . .
F1 F 0.4190(4) -0.0578(2) 0.5816(2) 0.0453(13) Uani 1 1 d . . . . .
F2 F 0.4048(4) -0.1064(2) 0.6571(2) 0.0477(14) Uani 1 1 d . . . . .
F3 F 0.4489(4) -0.1726(2) 0.6508(2) 0.0469(13) Uani 1 1 d . . . . .
F4 F 0.3303(4) -0.1475(2) 0.5811(2) 0.0483(14) Uani 1 1 d . . . . .
F5 F 1.1856(4) -0.2041(2) 0.5793(2) 0.0428(12) Uani 1 1 d . . . . .
F6 F 1.1307(4) -0.2816(2) 0.5790(2) 0.0451(13) Uani 1 1 d . . . . .
F7 F 1.0228(4) -0.2999(2) 0.5029(2) 0.0493(14) Uani 1 1 d . . . . .
F8 F 1.1434(5) -0.2834(3) 0.4909(3) 0.0557(17) Uani 1 1 d . . . . .
F9 F 0.9169(4) 0.0379(2) 0.2074(2) 0.0503(14) Uani 1 1 d . . . . .
F10 F 1.0313(4) 0.1061(2) 0.2229(2) 0.0464(13) Uani 1 1 d . . . . .
F11 F 1.0793(4) 0.0480(2) 0.1958(2) 0.0453(13) Uani 1 1 d . . . . .
F12 F 1.1642(4) 0.0864(3) 0.2652(2) 0.0507(15) Uani 1 1 d . . . . .
F13 F 0.5573(4) 0.0887(2) 0.2144(2) 0.0487(14) Uani 1 1 d . . . . .
F14 F 0.6547(4) -0.1938(2) 1.0143(2) 0.0476(13) Uani 1 1 d . . . . .
F15 F 0.6930(4) -0.1556(2) 1.0943(2) 0.0478(14) Uani 1 1 d . . . . .
F16 F 0.7846(4) -0.1668(2) 1.0439(2) 0.0494(14) Uani 1 1 d . . . . .
F17 F 0.3676(4) 0.0743(2) 0.3987(2) 0.0504(15) Uani 1 1 d . . . . .
F18 F 0.3276(4) 0.1703(2) 0.3917(2) 0.0456(13) Uani 1 1 d . . . . .
F19 F 0.2719(4) 0.1698(2) 0.4638(2) 0.0507(15) Uani 1 1 d . . . . .
F20 F 0.2427(4) 0.1214(2) 0.3988(2) 0.0456(12) Uani 1 1 d . . . . .
F21 F 1.0541(4) -0.1899(2) 0.7066(2) 0.0503(15) Uani 1 1 d . . . . .
F22 F 0.9359(4) -0.2628(2) 0.6948(2) 0.0485(14) Uani 1 1 d . . . . .
F23 F 1.0110(4) -0.2538(2) 0.6340(2) 0.0445(13) Uani 1 1 d . . . . .
F24 F 0.8763(4) -0.2726(2) 0.5990(2) 0.0468(14) Uani 1 1 d . . . . .
F25 F 0.6673(4) 0.2028(2) 0.4497(2) 0.0474(14) Uani 1 1 d . . . . .
F26 F 0.6581(5) 0.2965(3) 0.5303(2) 0.0541(16) Uani 1 1 d . . . . .
F27 F 0.5249(4) 0.2774(2) 0.5199(2) 0.0501(15) Uani 1 1 d . . . . .
F28 F 0.5836(4) 0.2622(2) 0.4468(2) 0.0516(16) Uani 1 1 d . . . . .
F29 F 1.3551(4) -0.0284(2) 0.4143(2) 0.0463(14) Uani 1 1 d . . . . .
F30 F 0.4424(5) 0.1857(2) 0.2793(2) 0.0518(15) Uani 1 1 d . . . . .
F31 F 0.4095(4) 0.1374(2) 0.2111(2) 0.0435(12) Uani 1 1 d . . . . .
F32 F 0.5220(4) 0.1771(2) 0.2198(2) 0.0490(14) Uani 1 1 d . . . . .
F33 F 1.0275(5) 0.1596(2) 0.3452(2) 0.0535(16) Uani 1 1 d . . . . .
F34 F 0.8996(5) 0.1378(3) 0.2646(2) 0.0550(16) Uani 1 1 d . . . . .
F35 F 0.7844(4) 0.1307(2) 0.2918(2) 0.0457(13) Uani 1 1 d . . . . .
F36 F 0.8526(4) 0.1897(2) 0.3029(2) 0.0489(14) Uani 1 1 d . . . . .
F37 F 1.0868(4) 0.2564(2) 0.6554(2) 0.0434(12) Uani 1 1 d . . . . .
F38 F 0.9359(4) 0.3017(2) 0.6133(2) 0.0450(13) Uani 1 1 d . . . . .
F39 F 0.9580(4) 0.3085(2) 0.7086(2) 0.0496(15) Uani 1 1 d . . . . .
F40 F 0.8323(4) 0.2885(2) 0.6535(2) 0.0508(15) Uani 1 1 d . . . . .
F41 F 0.5982(4) 0.2550(2) 0.7481(2) 0.0445(12) Uani 1 1 d . . . . .
F42 F 0.6291(4) 0.3198(2) 0.7393(2) 0.0487(14) Uani 1 1 d . . . . .
F43 F 0.7377(4) 0.3368(2) 0.8148(2) 0.0489(14) Uani 1 1 d . . . . .
F44 F 0.7614(4) 0.3208(2) 0.7310(2) 0.0470(13) Uani 1 1 d . . . . .
F45 F 0.7945(5) -0.1683(2) 0.7418(2) 0.0503(14) Uani 1 1 d . . . . .
F46 F 0.7486(4) -0.2345(2) 0.7813(2) 0.0458(14) Uani 1 1 d . . . . .
F47 F 0.6470(4) -0.2370(2) 0.6963(2) 0.0504(15) Uani 1 1 d . . . . .
F48 F 0.6208(4) -0.2392(2) 0.7905(2) 0.0468(14) Uani 1 1 d . . . . .
F49 F 0.4333(4) -0.1539(2) 0.8347(2) 0.0496(15) Uani 1 1 d . . . . .
F50 F 0.3756(4) -0.2354(2) 0.7480(2) 0.0462(13) Uani 1 1 d . . . . .
F51 F 0.2327(4) -0.2317(2) 0.7236(2) 0.0503(15) Uani 1 1 d . . . . .
F52 F 0.3110(5) -0.2268(2) 0.8175(2) 0.0519(15) Uani 1 1 d . . . . .
F53 F 0.1956(4) 0.2128(2) 0.5632(2) 0.0449(13) Uani 1 1 d . . . . .
F54 F 0.2627(4) 0.2921(2) 0.6143(2) 0.0469(13) Uani 1 1 d . . . . .
F55 F 0.3176(5) 0.2744(2) 0.5446(2) 0.0515(15) Uani 1 1 d . . . . .
F56 F 0.4006(4) 0.2983(2) 0.6283(2) 0.0484(14) Uani 1 1 d . . . . .
F57 F 0.2588(4) 0.1315(2) 0.9718(2) 0.0494(14) Uani 1 1 d . . . . .
F58 F 0.3761(5) 0.1746(2) 1.0947(2) 0.0519(16) Uani 1 1 d . . . . .
F59 F 0.3005(4) 0.2037(3) 1.0127(2) 0.0530(16) Uani 1 1 d . . . . .
F60 F 0.4351(4) 0.2210(2) 1.0520(2) 0.0490(14) Uani 1 1 d . . . . .
F61 F 0.4550(4) 0.2594(2) 0.8539(2) 0.0503(15) Uani 1 1 d . . . . .
F62 F 0.4962(4) 0.3328(2) 0.9489(2) 0.0488(14) Uani 1 1 d . . . . .
F63 F 0.4679(4) 0.3366(2) 0.8522(2) 0.0490(14) Uani 1 1 d . . . . .
F64 F 0.5815(4) 0.3686(2) 0.9034(2) 0.0475(13) Uani 1 1 d . . . . .
F65 F 0.5699(5) -0.0404(2) 1.0788(2) 0.0502(14) Uani 1 1 d . . . . .
F66 F 0.6589(5) -0.0692(2) 1.1829(2) 0.0547(16) Uani 1 1 d . . . . .
F67 F 0.5878(4) -0.0271(2) 1.2245(3) 0.0512(15) Uani 1 1 d . . . . .
F68 F 0.7291(4) -0.0268(2) 1.2506(2) 0.0421(12) Uani 1 1 d . . . . .
F69 F 0.8077(4) -0.0935(3) 1.0296(3) 0.0551(16) Uani 1 1 d . . . . .
F70 F 1.3213(5) -0.0803(2) 0.3490(3) 0.0512(15) Uani 1 1 d . . . . .
F71 F 1.1822(5) -0.0932(2) 0.3155(2) 0.0533(16) Uani 1 1 d . . . . .
F72 F 1.2700(5) -0.1374(2) 0.3756(2) 0.0549(15) Uani 1 1 d . U . . .
F73 F 1.1352(4) -0.1054(3) 0.9861(2) 0.0513(15) Uani 1 1 d . . . . .
F74 F 1.1428(4) -0.1775(2) 0.9442(2) 0.0484(14) Uani 1 1 d . . . . .
F75 F 1.2692(4) -0.1568(2) 0.9446(2) 0.0542(17) Uani 1 1 d . . . . .
F76 F 1.1819(4) -0.1811(2) 0.8626(2) 0.0455(13) Uani 1 1 d . . . . .
F77 F 1.1722(5) 0.2589(2) 0.9044(2) 0.0489(14) Uani 1 1 d . . . . .
F78 F 1.2727(5) 0.2586(2) 0.8495(2) 0.0498(14) Uani 1 1 d . . . . .
F79 F 1.3275(4) 0.1984(2) 0.8382(2) 0.0487(14) Uani 1 1 d . . . . .
F80 F 1.2107(5) 0.2204(2) 0.7722(2) 0.0526(15) Uani 1 1 d . . . . .
F81 F 0.9027(5) -0.0477(3) 1.1873(2) 0.0544(16) Uani 1 1 d . . . . .
F82 F 0.9123(4) -0.1409(2) 1.1688(2) 0.0480(13) Uani 1 1 d . U . . .
F83 F 1.0374(4) -0.1510(2) 1.1552(2) 0.0492(14) Uani 1 1 d . . . . .
F84 F 1.0251(5) -0.1080(2) 1.2221(2) 0.0516(15) Uani 1 1 d . . . . .
F85 F 0.9444(4) -0.1988(2) 0.8114(2) 0.0488(14) Uani 1 1 d . . . . .
F86 F 1.0056(4) -0.2258(2) 0.9275(2) 0.0462(13) Uani 1 1 d . . . . .
F87 F 0.8643(4) -0.2276(2) 0.9021(2) 0.0448(13) Uani 1 1 d . . . . .
F88 F 0.9374(5) -0.2032(2) 0.9867(2) 0.0479(14) Uani 1 1 d . . . . .
N1 N 0.7572(6) -0.1075(3) 0.3456(3) 0.0435(18) Uani 1 1 d . . . . .
N2 N 0.6112(6) -0.0671(3) 0.3510(3) 0.0450(19) Uani 1 1 d . . . . .
N3 N 0.8935(6) 0.1712(3) 1.0890(3) 0.0412(17) Uani 1 1 d . . . . .
N4 N 1.0378(6) 0.1311(3) 1.0838(3) 0.048(2) Uani 1 1 d . . . . .
Dy1 Dy 0.76077(2) -0.05714(3) 0.42543(2) 0.03209(8) Uani 1 1 d . . . . .
Dy2 Dy 0.74003(3) 0.00880(3) 0.56321(2) 0.04269(10) Uani 1 1 d . . . . .
Dy3 Dy 0.97467(2) -0.00983(3) 0.56170(2) 0.03169(8) Uani 1 1 d . . . . .
Dy4 Dy 1.16748(3) 0.04725(3) 0.65232(2) 0.04000(10) Uani 1 1 d . . . . .
Dy5 Dy 0.93396(2) 0.01604(3) 0.70194(2) 0.03131(8) Uani 1 1 d . . . . .
Dy6 Dy 0.71901(3) 0.04915(3) 0.73087(2) 0.04169(10) Uani 1 1 d . . . . .
Dy7 Dy 0.47172(3) 0.02768(3) 0.76817(2) 0.03713(9) Uani 1 1 d . . . . .
Dy8 Dy 0.67632(2) 0.07620(3) 0.87048(2) 0.03191(8) Uani 1 1 d . . . . .
Dy9 Dy 0.91059(2) 0.05543(3) 0.87017(2) 0.03209(8) Uani 1 1 d . . . . .
Dy10 Dy 0.89291(2) 0.12336(3) 1.00605(2) 0.03187(8) Uani 1 1 d . . . . .
O1 O 0.6605(4) -0.0457(2) 0.4912(2) 0.0367(13) Uani 1 1 d . . . . .
O2 O 0.6882(5) -0.1082(2) 0.4715(3) 0.0407(14) Uani 1 1 d . . . . .
O3 O 0.8707(5) -0.1028(3) 0.4730(3) 0.0450(16) Uani 1 1 d . . . . .
O4 O 0.9890(5) -0.0783(2) 0.5420(2) 0.0378(13) Uani 1 1 d . . . . .
O5 O 0.8896(5) -0.0417(3) 0.4112(3) 0.0474(18) Uani 1 1 d . . . . .
O6 O 0.9742(4) -0.0010(2) 0.4635(2) 0.0360(13) Uani 1 1 d . . . . .
O7 O 0.7124(5) 0.0083(2) 0.3969(2) 0.0412(14) Uani 1 1 d . . . . .
O8 O 0.7000(5) 0.0471(3) 0.4731(2) 0.0424(14) Uani 1 1 d . . . . .
O9 O 0.6052(4) 0.0123(3) 0.5695(2) 0.0455(16) Uani 1 1 d . . . . .
O10 O 0.5923(5) 0.0536(3) 0.6475(2) 0.0467(16) Uani 1 1 d . . . . .
O11 O 0.7801(4) -0.0609(2) 0.6024(2) 0.0394(14) Uani 1 1 d . . . . .
O12 O 0.9211(4) -0.0477(2) 0.6349(2) 0.0343(12) Uani 1 1 d . . . . .
O13 O 0.7337(4) 0.0801(3) 0.5869(2) 0.0404(14) Uani 1 1 d . . . . .
O14 O 0.7383(5) 0.1050(2) 0.6773(2) 0.0417(14) Uani 1 1 d . . . . .
O15 O 1.1180(4) -0.0089(2) 0.5667(2) 0.0385(13) Uani 1 1 d . . . . .
O16 O 1.2518(4) 0.0165(3) 0.5887(3) 0.0419(14) Uani 1 1 d . . . . .
O17 O 1.1434(4) 0.0882(2) 0.5637(2) 0.0387(14) Uani 1 1 d . . . . .
O18 O 1.0178(5) 0.0612(2) 0.5630(2) 0.0403(14) Uani 1 1 d . . . . .
O19 O 1.0823(5) 0.1020(3) 0.6581(2) 0.0426(15) Uani 1 1 d . . . . .
O20 O 0.9724(5) 0.0880(2) 0.6948(2) 0.0413(15) Uani 1 1 d . . . . .
O21 O 0.7310(5) 0.1141(2) 0.7992(2) 0.0400(14) Uani 1 1 d . . . . .
O22 O 0.8744(5) 0.1266(2) 0.8331(2) 0.0396(14) Uani 1 1 d . . . . .
O23 O 0.6872(4) -0.0189(2) 0.7483(2) 0.0381(14) Uani 1 1 d . . . . .
O24 O 0.5485(5) -0.0316(2) 0.7489(3) 0.0445(15) Uani 1 1 d . . . . .
O25 O 0.3480(4) -0.0138(2) 0.7509(2) 0.0384(13) Uani 1 1 d . . . . .
O26 O 0.2226(5) -0.0169(2) 0.6907(3) 0.0413(14) Uani 1 1 d . . . . .
O27 O 0.4378(5) 0.0937(2) 0.7278(3) 0.0412(14) Uani 1 1 d . . . . .
O28 O 0.3048(5) 0.0772(3) 0.6861(3) 0.0448(16) Uani 1 1 d . . . . .
O29 O 0.3883(4) 0.0577(3) 0.8297(2) 0.0448(16) Uani 1 1 d . . . . .
O30 O 0.5242(4) 0.0780(3) 0.8605(2) 0.0413(15) Uani 1 1 d . . . . .
O31 O 0.6669(4) 0.1447(3) 0.8921(2) 0.0400(14) Uani 1 1 d . . . . .
O32 O 0.7859(5) 0.1702(2) 0.9558(2) 0.0397(14) Uani 1 1 d . . . . .
O33 O 0.6638(5) 0.0758(3) 0.9628(2) 0.0454(16) Uani 1 1 d . . . . .
O34 O 0.7336(5) 0.1174(3) 1.0347(2) 0.0427(15) Uani 1 1 d . . . . .
O35 O 0.5093(5) -0.0188(3) 0.8576(2) 0.0450(16) Uani 1 1 d . . . . .
O36 O 0.6395(5) 0.0082(2) 0.8806(3) 0.0418(14) Uani 1 1 d . . . . .
O37 O 1.0616(5) 0.0456(3) 0.8676(3) 0.0493(18) Uani 1 1 d . . . . .
O38 O 1.0805(4) 0.0161(2) 0.7861(2) 0.0401(14) Uani 1 1 d . . . . .
O39 O 0.9827(4) 0.1062(2) 0.9222(2) 0.0383(14) Uani 1 1 d . . . . .
O40 O 0.9781(5) 0.1657(3) 0.9620(2) 0.0446(16) Uani 1 1 d . . . . .
O41 O 0.9381(5) 0.0152(3) 0.9568(2) 0.0442(15) Uani 1 1 d . . . . .
O42 O 0.9439(5) 0.0558(3) 1.0349(2) 0.0422(14) Uani 1 1 d . . . . .
O43 O 0.9138(5) -0.0441(2) 0.7544(2) 0.0411(14) Uani 1 1 d . . . . .
O44 O 0.8995(5) -0.0146(2) 0.8382(3) 0.0412(14) Uani 1 1 d . . . . .
O45 O 0.8318(4) -0.0208(2) 0.5115(2) 0.0397(14) Uani 1 1 d . . . . .
H45 H 0.8296 0.0049 0.4884 0.048 Uiso 1 1 calc R U . . .
O46 O 0.8824(4) 0.0331(2) 0.5989(2) 0.0371(13) Uani 1 1 d . . . . .
H46A H 0.8879 0.0629 0.5910 0.045 Uiso 1 1 calc R U . . .
O47 O 1.0516(4) 0.0059(2) 0.6630(2) 0.0394(14) Uani 1 1 d . . . . .
H47A H 1.0784 -0.0205 0.6804 0.047 Uiso 1 1 calc R U . . .
O48 O 0.7896(4) 0.0111(2) 0.6821(2) 0.0369(13) Uani 1 1 d . . . . .
H48 H 0.7807 -0.0176 0.6936 0.044 Uiso 1 1 calc R U . . .
O49 O 0.8768(5) 0.0539(2) 0.7607(2) 0.0398(13) Uani 1 1 d . . . . .
H49 H 0.8874 0.0827 0.7506 0.048 Uiso 1 1 calc R U . . .
O50 O 0.6003(4) 0.0400(2) 0.7680(2) 0.0370(13) Uani 1 1 d . . . . .
H50 H 0.6204 0.0123 0.7840 0.044 Uiso 1 1 calc R U . . .
O51 O 0.7780(4) 0.0443(2) 0.8547(2) 0.0335(12) Uani 1 1 d . . . . .
H51A H 0.7722 0.0151 0.8653 0.040 Uiso 1 1 calc R U . . .
O52 O 0.8215(4) 0.0882(2) 0.9233(2) 0.0315(11) Uani 1 1 d . . . . .
H52 H 0.8229 0.0627 0.9469 0.038 Uiso 1 1 calc R U . . .
O1W O 0.4260(5) 0.0175(3) 0.6588(2) 0.0432(16) Uani 1 1 d . . . . .
H1X H 0.3649 0.0111 0.6452 0.052 Uiso 1 1 d R U . . .
H1Y H 0.4584 -0.0050 0.6487 0.052 Uiso 1 1 d R U . . .
O2W O 1.2099(5) 0.0530(3) 0.7572(2) 0.0439(15) Uani 1 1 d . . . . .
H2X H 1.2714 0.0583 0.7716 0.053 Uiso 1 1 d R U . . .
H2Y H 1.1971 0.0274 0.7743 0.053 Uiso 1 1 d R U . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 O2 1.214(10) . ?
C1 O1 1.224(11) . ?
C1 C2 1.508(11) . ?
C1 Dy1 2.850(9) . ?
C2 C7 1.350(15) . ?
C2 C3 1.372(14) . ?
C3 C4 1.375(13) . ?
C3 H3 0.9300 . ?
C4 F1 1.341(11) . ?
C4 C5 1.459(16) . ?
C5 C6 1.361(14) . ?
C5 C8 1.518(13) . ?
C6 C7 1.402(11) . ?
C6 H6 0.9300 . ?
C7 H7 0.9300 . ?
C8 F2 1.336(10) . ?
C8 F4 1.346(11) . ?
C8 F3 1.363(13) . ?
C9 O4 1.270(10) . ?
C9 O3 1.272(10) . ?
C9 C10 1.458(13) . ?
C10 C11 1.366(14) . ?
C10 C15 1.404(15) . ?
C11 C12 1.430(14) . ?
C11 H11 0.9300 . ?
C12 F5 1.331(10) . ?
C12 C13 1.395(13) . ?
C13 C14 1.395(13) . ?
C13 C16 1.527(15) . ?
C14 C15 1.395(16) . ?
C14 H14 0.9300 . ?
C15 H15 0.9300 . ?
C16 F7 1.286(11) . ?
C16 F6 1.342(9) . ?
C16 F8 1.362(9) . ?
C17 O6 1.239(8) . ?
C17 O5 1.287(10) . ?
C17 C18 1.519(11) . ?
C18 C19 1.340(12) . ?
C18 C23 1.401(13) . ?
C19 C20 1.363(14) . ?
C19 H19 0.9300 . ?
C20 C21 1.340(16) . ?
C20 F9 1.375(9) . ?
C21 C22 1.390(12) . ?
C21 C24 1.531(12) . ?
C22 C23 1.423(12) . ?
C22 H22 0.9300 . ?
C23 H23 0.9300 . ?
C24 F12 1.306(10) . ?
C24 F11 1.309(10) . ?
C24 F10 1.362(10) . ?
C25 O8 1.302(8) . ?
C25 O7 1.309(11) . ?
C25 C26 1.400(14) . ?
C26 C27 1.367(11) . ?
C26 C31 1.417(15) . ?
C27 C28 1.375(14) . ?
C27 H27 0.9300 . ?
C28 F13 1.355(8) . ?
C28 C29 1.377(16) . ?
C29 C30 1.469(12) . ?
C29 C32 1.489(15) . ?
C30 C31 1.411(16) . ?
C30 H30 0.9300 . ?
C31 H31 0.9300 . ?
C32 F31 1.303(12) . ?
C32 F32 1.328(11) . ?
C32 F30 1.353(11) . ?
C33 O10 1.195(7) . ?
C33 C34 1.437(14) . ?
C33 O9 1.507(11) . ?
C34 C39 1.347(12) . ?
C34 C35 1.414(18) . ?
C35 C36 1.331(15) . ?
C35 H35 0.9300 . ?
C36 C37 1.419(10) . ?
C36 H36 0.9300 . ?
C37 C38 1.404(17) . ?
C37 C40 1.528(15) . ?
C38 F17 1.326(8) . ?
C38 C39 1.410(14) . ?
C39 H39 0.9300 . ?
C40 F19 1.209(13) . ?
C40 F20 1.268(11) . ?
C40 F18 1.454(11) . ?
C41 O11 1.256(8) . ?
C41 O12 1.280(8) . ?
C41 C42 1.471(14) . ?
C42 C43 1.367(13) . ?
C42 C47 1.390(13) . ?
C43 C44 1.395(16) . ?
C43 H43 0.9300 . ?
C44 F21 1.372(9) . ?
C44 C45 1.389(13) . ?
C45 C46 1.385(14) . ?
C45 C48 1.521(16) . ?
C46 C47 1.450(16) . ?
C46 H46 0.9300 . ?
C47 H47 0.9300 . ?
C48 F22 1.306(9) . ?
C48 F23 1.327(11) . ?
C48 F24 1.327(10) . ?
C49 O14 1.266(7) . ?
C49 O13 1.294(9) . ?
C49 C50 1.456(14) . ?
C50 C55 1.410(13) . ?
C50 C51 1.436(11) . ?
C51 C52 1.358(14) . ?
C51 H51 0.9300 . ?
C52 C53 1.362(13) . ?
C52 F25 1.373(8) . ?
C53 C54 1.415(11) . ?
C53 C56 1.496(15) . ?
C54 C55 1.409(15) . ?
C54 H54 0.9300 . ?
C55 H55 0.9300 . ?
C56 F28 1.343(8) . ?
C56 F27 1.352(11) . ?
C56 F26 1.381(11) . ?
C57 O16 1.260(12) . ?
C57 O15 1.295(9) . ?
C57 C58 1.438(11) . ?
C57 Dy4 2.946(9) . ?
C58 C59 1.381(12) . ?
C58 C63 1.388(14) . ?
C59 C60 1.391(12) . ?
C59 H59 0.9300 . ?
C60 F29 1.353(9) . ?
C60 C61 1.383(15) . ?
C61 C62 1.389(14) . ?
C61 C64 1.491(14) . ?
C62 C63 1.390(13) . ?
C62 H62 0.9300 . ?
C63 H63 0.9300 . ?
C64 F71 1.298(9) . ?
C64 F72 1.338(13) . ?
C64 F70 1.375(12) . ?
C65 O18 1.238(11) . ?
C65 O17 1.261(9) . ?
C65 C66 1.5004(13) . ?
C65 Dy4 2.900(7) . ?
C66 C67 1.387(13) . ?
C66 C71 1.388(14) . ?
C67 C68 1.431(13) . ?
C67 H67 0.9300 . ?
C68 F33 1.366(9) . ?
C68 C69 1.377(15) . ?
C69 C70 1.371(14) . ?
C69 C72 1.504(13) . ?
C70 C71 1.386(12) . ?
C70 H70 0.9300 . ?
C71 H71 0.9300 . ?
C72 F34 1.327(12) . ?
C72 F35 1.358(12) . ?
C72 F36 1.357(14) . ?
C73 O20 1.213(10) . ?
C73 O19 1.293(10) . ?
C73 C74 1.450(14) . ?
C74 C79 1.400(13) . ?
C74 C75 1.414(15) . ?
C75 C76 1.465(17) . ?
C75 H75 0.9300 . ?
C76 F37 1.301(11) . ?
C76 C77 1.443(14) . ?
C77 C78 1.399(15) . ?
C77 C80 1.428(17) . ?
C78 C79 1.378(18) . ?
C78 H78 0.9300 . ?
C79 H79 0.9300 . ?
C80 F39 1.343(11) . ?
C80 F40 1.369(12) . ?
C80 F38 1.367(10) . ?
C81 O21 1.237(9) . ?
C81 O22 1.251(9) . ?
C81 C82 1.472(15) . ?
C82 C83 1.357(16) . ?
C82 C87 1.405(16) . ?
C83 C84 1.398(16) . ?
C83 H83 0.9300 . ?
C84 F41 1.312(10) . ?
C84 C85 1.411(15) . ?
C85 C86 1.368(16) . ?
C85 C88 1.460(16) . ?
C86 C87 1.400(18) . ?
C86 H86 0.9300 . ?
C87 H87 0.9300 . ?
C88 F44 1.349(10) . ?
C88 F43 1.358(11) . ?
C88 F42 1.367(12) . ?
C89 O24 1.240(11) . ?
C89 O23 1.316(12) . ?
C89 C90 1.507(16) . ?
C90 C95 1.290(17) . ?
C90 C91 1.473(15) . ?
C91 C92 1.382(16) . ?
C91 H91 0.9300 . ?
C92 F45 1.339(12) . ?
C92 C93 1.379(18) . ?
C93 C94 1.407(15) . ?
C93 C96 1.508(16) . ?
C94 C95 1.393(17) . ?
C94 H94 0.9300 . ?
C95 H95 0.9300 . ?
C96 F46 1.347(10) . ?
C96 F47 1.368(8) . ?
C96 F48 1.388(10) . ?
C97 O26 1.209(10) . ?
C97 O25 1.260(9) . ?
C97 C98 1.510(16) . ?
C98 C103 1.359(10) . ?
C98 C99 1.390(13) . ?
C99 C100 1.379(16) . ?
C99 H99 0.9300 . ?
C100 F49 1.308(9) . ?
C100 C101 1.426(10) . ?
C101 C102 1.394(14) . ?
C101 C104 1.589(16) . ?
C102 C103 1.433(18) . ?
C102 H102 0.9300 . ?
C103 H103 0.9300 . ?
C104 F51 1.323(11) . ?
C104 F52 1.344(9) . ?
C104 F50 1.377(10) . ?
C105 O27 1.255(9) . ?
C105 O28 1.277(10) . ?
C105 C106 1.464(15) . ?
C106 C107 1.376(12) . ?
C106 C111 1.398(14) . ?
C107 C108 1.379(16) . ?
C107 H107 0.9300 . ?
C108 F53 1.366(9) . ?
C108 C109 1.383(16) . ?
C109 C110 1.403(12) . ?
C109 C112 1.540(17) . ?
C110 C111 1.380(15) . ?
C110 H110 0.9300 . ?
C111 H111 0.9300 . ?
C112 F55 1.332(8) . ?
C112 F54 1.341(12) . ?
C112 F56 1.342(10) . ?
C113 O30 1.230(9) . ?
C113 O29 1.280(10) . ?
C113 C114 1.461(11) . ?
C113 Dy7 2.899(9) . ?
C114 C115 1.358(13) . ?
C114 C119 1.365(16) . ?
C115 C116 1.372(10) . ?
C115 H115 0.9300 . ?
C116 F57 1.328(9) . ?
C116 C117 1.411(14) . ?
C117 C118 1.401(14) . ?
C117 C120 1.457(13) . ?
C118 C119 1.370(14) . ?
C118 H118 0.9300 . ?
C119 H119 0.9300 . ?
C120 F59 1.321(12) . ?
C120 F60 1.355(12) . ?
C120 F58 1.393(9) . ?
C121 O32 1.255(9) . ?
C121 O31 1.254(9) . ?
C121 C122 1.481(15) . ?
C122 C123 1.384(14) . ?
C122 C127 1.400(15) . ?
C123 C124 1.375(15) . ?
C123 H123 0.9300 . ?
C124 F61 1.354(9) . ?
C124 C125 1.396(13) . ?
C125 C126 1.418(13) . ?
C125 C128 1.512(14) . ?
C126 C127 1.368(16) . ?
C126 H126 0.9300 . ?
C127 H127 0.9300 . ?
C128 F63 1.341(10) . ?
C128 F64 1.378(12) . ?
C128 F62 1.374(9) . ?
C129 O33 1.261(7) . ?
C129 O34 1.271(11) . ?
C129 C130 1.495(13) . ?
C130 C135 1.381(11) . ?
C130 C131 1.399(16) . ?
C131 C132 1.404(14) . ?
C131 H131 0.9300 . ?
C132 F65 1.370(12) . ?
C132 C133 1.360(12) . ?
C133 C134 1.357(16) . ?
C133 C136 1.567(12) . ?
C134 C135 1.369(12) . ?
C134 H134 0.9300 . ?
C135 H135 0.9300 . ?
C136 F68 1.287(9) . ?
C136 F67 1.365(10) . ?
C136 F66 1.385(12) . ?
C137 O35 1.262(10) . ?
C137 O36 1.311(9) . ?
C137 C138 1.397(11) . ?
C138 C139 1.383(12) . ?
C138 C143 1.405(14) . ?
C139 C140 1.390(14) . ?
C139 H139 0.9300 . ?
C140 F69 1.342(11) . ?
C140 C141 1.360(18) . ?
C141 C142 1.418(15) . ?
C141 C144 1.501(14) . ?
C142 C143 1.417(13) . ?
C142 H142 0.9300 . ?
C143 H143 0.9300 . ?
C144 F14 1.311(11) . ?
C144 F15 1.330(7) . ?
C144 F16 1.349(11) . ?
C145 O38 1.292(8) . ?
C145 O37 1.295(10) . ?
C145 C146 1.493(15) . ?
C146 C151 1.391(14) . ?
C146 C147 1.404(13) . ?
C147 C148 1.382(16) . ?
C147 H147 0.9300 . ?
C148 C149 1.370(13) . ?
C148 F73 1.381(9) . ?
C149 C150 1.384(13) . ?
C149 C152 1.539(16) . ?
C150 C151 1.390(17) . ?
C150 H150 0.9300 . ?
C151 H151 0.9300 . ?
C152 F75 1.328(10) . ?
C152 F74 1.349(12) . ?
C152 F76 1.360(9) . ?
C153 O39 1.114(11) . ?
C153 O40 1.225(10) . ?
C153 C154 1.520(12) . ?
C153 Dy10 2.852(8) . ?
C154 C159 1.408(16) . ?
C154 C155 1.413(16) . ?
C155 C156 1.384(13) . ?
C155 H155 0.9300 . ?
C156 F77 1.316(11) . ?
C156 C157 1.417(16) . ?
C157 C158 1.370(18) . ?
C157 C160 1.496(16) . ?
C158 C159 1.413(14) . ?
C158 H158 0.9300 . ?
C159 H159 0.9300 . ?
C160 F80 1.296(9) . ?
C160 F79 1.350(12) . ?
C160 F78 1.388(12) . ?
C161 O41 1.238(8) . ?
C161 O42 1.272(11) . ?
C161 C162 1.493(14) . ?
C162 C167 1.394(14) . ?
C162 C163 1.407(12) . ?
C163 C164 1.321(15) . ?
C163 H163 0.9300 . ?
C164 F81 1.402(11) . ?
C164 C165 1.412(17) . ?
C165 C166 1.432(15) . ?
C165 C168 1.487(13) . ?
C166 C167 1.415(13) . ?
C166 H166 0.9300 . ?
C167 H167 0.9300 . ?
C168 F82 1.308(12) . ?
C168 F83 1.303(11) . ?
C168 F84 1.360(9) . ?
C169 O44 1.167(10) . ?
C169 O43 1.385(8) . ?
C169 C170 1.498(14) . ?
C170 C175 1.395(13) . ?
C170 C171 1.443(16) . ?
C171 C172 1.359(14) . ?
C171 H171 0.9300 . ?
C172 C173 1.357(15) . ?
C172 F85 1.431(14) . ?
C173 C174 1.419(19) . ?
C173 C176 1.510(15) . ?
C174 C175 1.328(14) . ?
C174 H174 0.9300 . ?
C175 H175 0.9300 . ?
C176 F88 1.288(9) . ?
C176 F87 1.323(12) . ?
C176 F86 1.380(13) . ?
C177 C178 1.353(12) . ?
C177 N1 1.424(9) . ?
C177 H177 0.9300 . ?
C178 C179 1.422(14) . ?
C178 H178 0.9300 . ?
C179 C180 1.360(15) . ?
C179 H179 0.9300 . ?
C180 C181 1.405(13) . ?
C180 H180 0.9300 . ?
C181 N1 1.385(9) . ?
C181 C182 1.373(15) . ?
C182 N2 1.377(11) . ?
C182 C183 1.406(13) . ?
C183 C184 1.322(15) . ?
C183 H183 0.9300 . ?
C184 C185 1.423(12) . ?
C184 H184 0.9300 . ?
C185 C186 1.407(13) . ?
C185 H185 0.9300 . ?
C186 N2 1.384(12) . ?
C186 H186 0.9300 . ?
C187 C188 1.429(11) . ?
C187 N3 1.445(10) . ?
C187 H187 0.9300 . ?
C188 C189 1.433(14) . ?
C188 H188 0.9300 . ?
C189 C190 1.405(17) . ?
C189 H189 0.9300 . ?
C190 C191 1.408(13) . ?
C190 H190 0.9300 . ?
C191 N3 1.357(10) . ?
C191 C192 1.459(16) . ?
C192 N4 1.395(10) . ?
C192 C193 1.409(14) . ?
C193 C194 1.372(18) . ?
C193 H193 0.9300 . ?
C194 C195 1.428(17) . ?
C194 H194 0.9300 . ?
C195 C196 1.386(14) . ?
C195 H195 0.9300 . ?
C196 N4 1.410(11) . ?
C196 H196 0.9300 . ?
N1 Dy1 2.454(7) . ?
N2 Dy1 2.531(8) . ?
N3 Dy10 2.468(7) . ?
N4 Dy10 2.501(8) . ?
Dy1 O5 2.249(7) . ?
Dy1 O7 2.265(8) . ?
Dy1 O45 2.308(6) . ?
Dy1 O3 2.307(8) . ?
Dy1 O2 2.439(7) . ?
Dy1 O1 2.563(5) . ?
Dy1 Dy2 3.9449(5) . ?
Dy2 O9 2.218(7) . ?
Dy2 O46 2.324(7) . ?
Dy2 O8 2.354(6) . ?
Dy2 O13 2.358(8) . ?
Dy2 O45 2.366(6) . ?
Dy2 O11 2.425(8) . ?
Dy2 O1 2.496(7) . ?
Dy2 O48 2.650(5) . ?
Dy2 Dy5 3.7728(6) . ?
Dy2 Dy3 3.8300(6) . ?
Dy3 O4 2.267(7) . ?
Dy3 O15 2.272(7) . ?
Dy3 O45 2.273(6) . ?
Dy3 O6 2.307(5) . ?
Dy3 O46 2.371(6) . ?
Dy3 O47 2.372(5) . ?
Dy3 O18 2.377(8) . ?
Dy3 O12 2.452(6) . ?
Dy3 Dy5 3.6217(4) . ?
Dy3 Dy4 3.6759(6) . ?
Dy4 O19 2.254(7) . ?
Dy4 O26 2.309(8) 1_655 ?
Dy4 O28 2.319(8) 1_655 ?
Dy4 O2W 2.345(5) . ?
Dy4 O47 2.359(7) . ?
Dy4 O17 2.381(7) . ?
Dy4 O16 2.494(6) . ?
Dy4 O15 2.628(6) . ?
Dy4 O18 2.709(7) . ?
Dy5 O49 2.225(6) . ?
Dy5 O48 2.232(7) . ?
Dy5 O43 2.356(7) . ?
Dy5 O47 2.353(6) . ?
Dy5 O46 2.362(5) . ?
Dy5 O20 2.405(8) . ?
Dy5 O12 2.544(6) . ?
Dy5 O38 2.578(6) . ?
Dy5 Dy6 3.8623(6) . ?
Dy6 O48 2.200(6) . ?
Dy6 O14 2.255(7) . ?
Dy6 O23 2.303(7) . ?
Dy6 O50 2.338(7) . ?
Dy6 O10 2.365(7) . ?
Dy6 O49 2.426(7) . ?
Dy6 O21 2.594(7) . ?
Dy6 O51 2.765(5) . ?
Dy6 Dy8 3.6310(5) . ?
Dy6 Dy9 3.7579(6) . ?
Dy7 O50 2.106(7) . ?
Dy7 O27 2.311(7) . ?
Dy7 O25 2.326(7) . ?
Dy7 O24 2.379(8) . ?
Dy7 O29 2.436(6) . ?
Dy7 O1W 2.460(5) . ?
Dy7 O35 2.488(6) . ?
Dy7 O30 2.621(6) . ?
Dy7 Dy8 3.7747(6) . ?
Dy8 O51 2.052(6) . ?
Dy8 O33 2.223(5) . ?
Dy8 O31 2.268(8) . ?
Dy8 O36 2.286(8) . ?
Dy8 O52 2.323(6) . ?
Dy8 O30 2.388(7) . ?
Dy8 O21 2.427(6) . ?
Dy8 O50 2.610(6) . ?
Dy8 Dy9 3.8267(5) . ?
Dy9 O51 2.083(6) . ?
Dy9 O39 2.150(6) . ?
Dy9 O41 2.328(7) . ?
Dy9 O44 2.356(8) . ?
Dy9 O52 2.398(5) . ?
Dy9 O22 2.447(8) . ?
Dy9 O49 2.451(5) . ?
Dy9 O37 2.467(8) . ?
Dy9 Dy10 3.9267(9) . ?
Dy10 O52 2.236(5) . ?
Dy10 O32 2.321(7) . ?
Dy10 O42 2.341(8) . ?
Dy10 O40 2.368(7) . ?
Dy10 O39 2.812(5) . ?
Dy10 O34 2.840(7) . ?
O26 Dy4 2.309(8) 1_455 ?
O28 Dy4 2.319(8) 1_455 ?
O45 H45 0.9800 . ?
O46 H46A 0.9800 . ?
O47 H47A 0.9800 . ?
O48 H48 0.9800 . ?
O49 H49 0.9800 . ?
O50 H50 0.9800 . ?
O51 H51A 0.9800 . ?
O52 H52 0.9800 . ?
O1W H1X 0.9600 . ?
O1W H1Y 0.9599 . ?
O2W H2X 0.9600 . ?
O2W H2Y 0.9600 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O2 C1 O1 121.9(7) . . ?
O2 C1 C2 116.9(9) . . ?
O1 C1 C2 121.2(8) . . ?
O2 C1 Dy1 58.2(4) . . ?
O1 C1 Dy1 64.1(4) . . ?
C2 C1 Dy1 173.0(7) . . ?
C7 C2 C3 121.1(8) . . ?
C7 C2 C1 124.6(9) . . ?
C3 C2 C1 113.8(9) . . ?
C2 C3 C4 118.9(10) . . ?
C2 C3 H3 120.5 . . ?
C4 C3 H3 120.5 . . ?
F1 C4 C3 124.2(10) . . ?
F1 C4 C5 114.0(8) . . ?
C3 C4 C5 121.8(10) . . ?
C6 C5 C4 115.4(9) . . ?
C6 C5 C8 124.8(10) . . ?
C4 C5 C8 119.8(9) . . ?
C5 C6 C7 122.2(10) . . ?
C5 C6 H6 118.9 . . ?
C7 C6 H6 118.9 . . ?
C2 C7 C6 120.3(10) . . ?
C2 C7 H7 119.9 . . ?
C6 C7 H7 119.9 . . ?
F2 C8 F4 113.7(8) . . ?
F2 C8 F3 113.2(7) . . ?
F4 C8 F3 112.6(9) . . ?
F2 C8 C5 108.8(9) . . ?
F4 C8 C5 106.9(7) . . ?
F3 C8 C5 100.6(8) . . ?
O4 C9 O3 123.3(8) . . ?
O4 C9 C10 121.7(8) . . ?
O3 C9 C10 115.0(8) . . ?
C11 C10 C15 121.4(9) . . ?
C11 C10 C9 118.2(9) . . ?
C15 C10 C9 120.3(9) . . ?
C10 C11 C12 119.0(9) . . ?
C10 C11 H11 120.5 . . ?
C12 C11 H11 120.5 . . ?
F5 C12 C13 120.5(9) . . ?
F5 C12 C11 120.5(8) . . ?
C13 C12 C11 119.0(9) . . ?
C14 C13 C12 121.8(10) . . ?
C14 C13 C16 118.0(9) . . ?
C12 C13 C16 120.1(9) . . ?
C13 C14 C15 118.3(11) . . ?
C13 C14 H14 120.8 . . ?
C15 C14 H14 120.8 . . ?
C10 C15 C14 120.5(10) . . ?
C10 C15 H15 119.8 . . ?
C14 C15 H15 119.8 . . ?
F7 C16 F6 110.5(8) . . ?
F7 C16 F8 105.5(6) . . ?
F6 C16 F8 103.8(7) . . ?
F7 C16 C13 109.9(8) . . ?
F6 C16 C13 108.8(6) . . ?
F8 C16 C13 118.1(9) . . ?
O6 C17 O5 105.6(6) . . ?
O6 C17 C18 116.8(7) . . ?
O5 C17 C18 133.2(7) . . ?
C19 C18 C23 119.8(9) . . ?
C19 C18 C17 125.1(9) . . ?
C23 C18 C17 115.0(7) . . ?
C18 C19 C20 123.9(10) . . ?
C18 C19 H19 118.1 . . ?
C20 C19 H19 118.1 . . ?
C21 C20 F9 121.8(8) . . ?
C21 C20 C19 119.3(8) . . ?
F9 C20 C19 118.8(9) . . ?
C20 C21 C22 119.2(9) . . ?
C20 C21 C24 118.6(8) . . ?
C22 C21 C24 121.8(9) . . ?
C21 C22 C23 121.9(10) . . ?
C21 C22 H22 119.0 . . ?
C23 C22 H22 119.0 . . ?
C18 C23 C22 115.7(8) . . ?
C18 C23 H23 122.2 . . ?
C22 C23 H23 122.2 . . ?
F12 C24 F11 111.5(9) . . ?
F12 C24 F10 108.3(7) . . ?
F11 C24 F10 109.3(5) . . ?
F12 C24 C21 113.8(6) . . ?
F11 C24 C21 106.3(7) . . ?
F10 C24 C21 107.5(9) . . ?
O8 C25 O7 117.1(8) . . ?
O8 C25 C26 122.0(9) . . ?
O7 C25 C26 121.0(7) . . ?
C27 C26 C25 120.0(10) . . ?
C27 C26 C31 121.7(10) . . ?
C25 C26 C31 118.2(8) . . ?
C26 C27 C28 120.0(10) . . ?
C26 C27 H27 120.0 . . ?
C28 C27 H27 120.0 . . ?
F13 C28 C29 118.2(8) . . ?
F13 C28 C27 120.0(9) . . ?
C29 C28 C27 121.7(8) . . ?
C28 C29 C30 119.5(10) . . ?
C28 C29 C32 121.7(8) . . ?
C30 C29 C32 118.4(11) . . ?
C31 C30 C29 117.5(11) . . ?
C31 C30 H30 121.2 . . ?
C29 C30 H30 121.2 . . ?
C30 C31 C26 119.2(9) . . ?
C30 C31 H31 120.4 . . ?
C26 C31 H31 120.4 . . ?
F31 C32 F32 111.1(6) . . ?
F31 C32 F30 109.5(7) . . ?
F32 C32 F30 107.9(10) . . ?
F31 C32 C29 111.5(10) . . ?
F32 C32 C29 108.1(8) . . ?
F30 C32 C29 108.6(7) . . ?
O10 C33 C34 125.2(9) . . ?
O10 C33 O9 117.0(8) . . ?
C34 C33 O9 117.8(7) . . ?
C39 C34 C35 120.8(10) . . ?
C39 C34 C33 120.7(11) . . ?
C35 C34 C33 118.2(8) . . ?
C36 C35 C34 120.3(8) . . ?
C36 C35 H35 119.9 . . ?
C34 C35 H35 119.9 . . ?
C35 C36 C37 120.4(11) . . ?
C35 C36 H36 119.8 . . ?
C37 C36 H36 119.8 . . ?
C38 C37 C36 119.0(10) . . ?
C38 C37 C40 116.6(8) . . ?
C36 C37 C40 123.4(11) . . ?
F17 C38 C39 121.1(10) . . ?
F17 C38 C37 119.6(9) . . ?
C39 C38 C37 119.1(8) . . ?
C34 C39 C38 119.8(11) . . ?
C34 C39 H39 120.1 . . ?
C38 C39 H39 120.1 . . ?
F19 C40 F20 117.9(11) . . ?
F19 C40 F18 105.9(8) . . ?
F20 C40 F18 101.8(5) . . ?
F19 C40 C37 106.9(7) . . ?
F20 C40 C37 115.0(9) . . ?
F18 C40 C37 108.6(10) . . ?
O11 C41 O12 120.7(7) . . ?
O11 C41 C42 122.0(7) . . ?
O12 C41 C42 114.8(7) . . ?
C43 C42 C47 120.1(10) . . ?
C43 C42 C41 123.7(9) . . ?
C47 C42 C41 116.2(9) . . ?
C42 C43 C44 121.3(9) . . ?
C42 C43 H43 119.3 . . ?
C44 C43 H43 119.3 . . ?
F21 C44 C43 120.7(7) . . ?
F21 C44 C45 119.4(9) . . ?
C43 C44 C45 119.7(9) . . ?
C46 C45 C44 120.0(11) . . ?
C46 C45 C48 118.9(9) . . ?
C44 C45 C48 121.1(9) . . ?
C45 C46 C47 119.4(10) . . ?
C45 C46 H46 120.3 . . ?
C47 C46 H46 120.3 . . ?
C42 C47 C46 118.8(10) . . ?
C42 C47 H47 120.6 . . ?
C46 C47 H47 120.6 . . ?
F22 C48 F23 108.7(7) . . ?
F22 C48 F24 111.5(9) . . ?
F23 C48 F24 108.9(6) . . ?
F22 C48 C45 107.2(7) . . ?
F23 C48 C45 105.4(9) . . ?
F24 C48 C45 114.9(8) . . ?
O14 C49 O13 121.8(8) . . ?
O14 C49 C50 120.9(8) . . ?
O13 C49 C50 117.3(6) . . ?
C55 C50 C51 119.5(9) . . ?
C55 C50 C49 120.0(7) . . ?
C51 C50 C49 120.5(8) . . ?
C52 C51 C50 119.5(9) . . ?
C52 C51 H51 120.3 . . ?
C50 C51 H51 120.3 . . ?
C53 C52 C51 122.1(8) . . ?
C53 C52 F25 119.7(8) . . ?
C51 C52 F25 118.1(8) . . ?
C52 C53 C54 120.4(10) . . ?
C52 C53 C56 121.2(8) . . ?
C54 C53 C56 118.3(9) . . ?
C53 C54 C55 119.5(9) . . ?
C53 C54 H54 120.2 . . ?
C55 C54 H54 120.2 . . ?
C54 C55 C50 119.0(7) . . ?
C54 C55 H55 120.5 . . ?
C50 C55 H55 120.5 . . ?
F28 C56 F27 112.2(8) . . ?
F28 C56 F26 111.0(7) . . ?
F27 C56 F26 105.2(7) . . ?
F28 C56 C53 109.0(7) . . ?
F27 C56 C53 110.0(8) . . ?
F26 C56 C53 109.4(8) . . ?
O16 C57 O15 120.0(7) . . ?
O16 C57 C58 117.6(8) . . ?
O15 C57 C58 120.8(9) . . ?
O16 C57 Dy4 57.0(3) . . ?
O15 C57 Dy4 63.2(4) . . ?
C58 C57 Dy4 169.7(8) . . ?
C59 C58 C63 118.9(8) . . ?
C59 C58 C57 123.4(9) . . ?
C63 C58 C57 117.6(9) . . ?
C58 C59 C60 121.4(10) . . ?
C58 C59 H59 119.3 . . ?
C60 C59 H59 119.3 . . ?
F29 C60 C59 121.4(9) . . ?
F29 C60 C61 119.4(8) . . ?
C59 C60 C61 119.3(9) . . ?
C62 C61 C60 120.1(10) . . ?
C62 C61 C64 118.4(10) . . ?
C60 C61 C64 121.2(9) . . ?
C61 C62 C63 119.9(10) . . ?
C61 C62 H62 120.0 . . ?
C63 C62 H62 120.0 . . ?
C58 C63 C62 120.4(9) . . ?
C58 C63 H63 119.8 . . ?
C62 C63 H63 119.8 . . ?
F71 C64 F72 112.1(8) . . ?
F71 C64 F70 109.1(7) . . ?
F72 C64 F70 106.3(8) . . ?
F71 C64 C61 112.1(10) . . ?
F72 C64 C61 110.2(8) . . ?
F70 C64 C61 106.7(8) . . ?
O18 C65 O17 122.5(5) . . ?
O18 C65 C66 111.8(8) . . ?
O17 C65 C66 125.4(9) . . ?
O18 C65 Dy4 68.8(3) . . ?
O17 C65 Dy4 53.7(3) . . ?
C66 C65 Dy4 175.0(6) . . ?
C67 C66 C71 119.8(7) . . ?
C67 C66 C65 119.5(9) . . ?
C71 C66 C65 120.6(9) . . ?
C66 C67 C68 120.1(9) . . ?
C66 C67 H67 120.0 . . ?
C68 C67 H67 120.0 . . ?
F33 C68 C69 109.4(8) . . ?
F33 C68 C67 132.1(9) . . ?
C69 C68 C67 118.4(9) . . ?
C70 C69 C68 120.9(9) . . ?
C70 C69 C72 121.7(10) . . ?
C68 C69 C72 117.2(10) . . ?
C69 C70 C71 121.1(10) . . ?
C69 C70 H70 119.5 . . ?
C71 C70 H70 119.5 . . ?
C66 C71 C70 119.7(9) . . ?
C66 C71 H71 120.2 . . ?
C70 C71 H71 120.2 . . ?
F34 C72 F35 105.8(6) . . ?
F34 C72 F36 105.2(7) . . ?
F35 C72 F36 105.6(10) . . ?
F34 C72 C69 114.7(11) . . ?
F35 C72 C69 108.2(8) . . ?
F36 C72 C69 116.4(8) . . ?
O20 C73 O19 125.6(9) . . ?
O20 C73 C74 114.9(8) . . ?
O19 C73 C74 119.5(8) . . ?
C79 C74 C75 120.5(10) . . ?
C79 C74 C73 121.6(9) . . ?
C75 C74 C73 116.6(8) . . ?
C74 C75 C76 118.5(9) . . ?
C74 C75 H75 120.8 . . ?
C76 C75 H75 120.8 . . ?
F37 C76 C77 121.9(10) . . ?
F37 C76 C75 119.2(9) . . ?
C77 C76 C75 118.8(10) . . ?
C78 C77 C76 119.5(11) . . ?
C78 C77 C80 119.4(10) . . ?
C76 C77 C80 121.1(10) . . ?
C79 C78 C77 121.2(10) . . ?
C79 C78 H78 119.4 . . ?
C77 C78 H78 119.4 . . ?
C78 C79 C74 121.5(10) . . ?
C78 C79 H79 119.3 . . ?
C74 C79 H79 119.3 . . ?
F39 C80 F40 104.4(7) . . ?
F39 C80 F38 105.4(8) . . ?
F40 C80 F38 106.0(8) . . ?
F39 C80 C77 114.8(9) . . ?
F40 C80 C77 113.7(9) . . ?
F38 C80 C77 111.7(8) . . ?
O21 C81 O22 128.3(8) . . ?
O21 C81 C82 115.5(8) . . ?
O22 C81 C82 116.1(8) . . ?
C83 C82 C87 118.1(11) . . ?
C83 C82 C81 120.5(10) . . ?
C87 C82 C81 121.3(10) . . ?
C82 C83 C84 122.6(11) . . ?
C82 C83 H83 118.7 . . ?
C84 C83 H83 118.7 . . ?
F41 C84 C83 127.2(10) . . ?
F41 C84 C85 114.4(10) . . ?
C83 C84 C85 118.3(10) . . ?
C86 C85 C84 119.8(11) . . ?
C86 C85 C88 128.2(11) . . ?
C84 C85 C88 112.0(10) . . ?
C85 C86 C87 120.4(11) . . ?
C85 C86 H86 119.8 . . ?
C87 C86 H86 119.8 . . ?
C86 C87 C82 120.3(11) . . ?
C86 C87 H87 119.8 . . ?
C82 C87 H87 119.8 . . ?
F44 C88 F43 106.2(9) . . ?
F44 C88 F42 107.7(6) . . ?
F43 C88 F42 104.1(8) . . ?
F44 C88 C85 99.5(9) . . ?
F43 C88 C85 114.6(7) . . ?
F42 C88 C85 123.4(10) . . ?
O24 C89 O23 125.4(9) . . ?
O24 C89 C90 113.6(10) . . ?
O23 C89 C90 121.1(9) . . ?
C95 C90 C91 120.9(11) . . ?
C95 C90 C89 121.8(11) . . ?
C91 C90 C89 117.3(10) . . ?
C92 C91 C90 116.9(12) . . ?
C92 C91 H91 121.5 . . ?
C90 C91 H91 121.5 . . ?
F45 C92 C93 118.9(10) . . ?
F45 C92 C91 120.1(11) . . ?
C93 C92 C91 120.8(11) . . ?
C92 C93 C94 120.5(11) . . ?
C92 C93 C96 119.5(10) . . ?
C94 C93 C96 119.6(10) . . ?
C95 C94 C93 118.1(11) . . ?
C95 C94 H94 120.9 . . ?
C93 C94 H94 120.9 . . ?
C90 C95 C94 122.7(12) . . ?
C90 C95 H95 118.6 . . ?
C94 C95 H95 118.6 . . ?
F46 C96 F47 105.6(6) . . ?
F46 C96 F48 102.5(6) . . ?
F47 C96 F48 117.7(8) . . ?
F46 C96 C93 114.0(9) . . ?
F47 C96 C93 107.6(7) . . ?
F48 C96 C93 109.6(7) . . ?
O26 C97 O25 115.4(9) . . ?
O26 C97 C98 126.9(8) . . ?
O25 C97 C98 117.6(8) . . ?
C103 C98 C99 122.1(11) . . ?
C103 C98 C97 120.1(8) . . ?
C99 C98 C97 117.8(9) . . ?
C100 C99 C98 119.5(9) . . ?
C100 C99 H99 120.3 . . ?
C98 C99 H99 120.3 . . ?
F49 C100 C99 120.1(8) . . ?
F49 C100 C101 120.4(9) . . ?
C99 C100 C101 119.4(8) . . ?
C102 C101 C100 120.8(10) . . ?
C102 C101 C104 113.3(10) . . ?
C100 C101 C104 125.8(8) . . ?
C101 C102 C103 117.7(10) . . ?
C101 C102 H102 121.1 . . ?
C103 C102 H102 121.1 . . ?
C98 C103 C102 120.2(8) . . ?
C98 C103 H103 119.9 . . ?
C102 C103 H103 119.9 . . ?
F51 C104 F52 110.0(8) . . ?
F51 C104 F50 109.1(7) . . ?
F52 C104 F50 107.2(7) . . ?
F51 C104 C101 108.5(8) . . ?
F52 C104 C101 108.3(7) . . ?
F50 C104 C101 113.7(8) . . ?
O27 C105 O28 114.9(8) . . ?
O27 C105 C106 120.5(9) . . ?
O28 C105 C106 124.6(8) . . ?
C107 C106 C111 118.7(10) . . ?
C107 C106 C105 124.5(10) . . ?
C111 C106 C105 116.5(8) . . ?
C106 C107 C108 122.1(10) . . ?
C106 C107 H107 119.0 . . ?
C108 C107 H107 119.0 . . ?
F53 C108 C107 119.0(9) . . ?
F53 C108 C109 122.1(10) . . ?
C107 C108 C109 118.8(9) . . ?
C108 C109 C110 120.5(11) . . ?
C108 C109 C112 119.3(8) . . ?
C110 C109 C112 120.1(10) . . ?
C111 C110 C109 119.3(10) . . ?
C111 C110 H110 120.3 . . ?
C109 C110 H110 120.3 . . ?
C110 C111 C106 120.5(8) . . ?
C110 C111 H111 119.8 . . ?
C106 C111 H111 119.8 . . ?
F55 C112 F54 106.8(7) . . ?
F55 C112 F56 107.0(8) . . ?
F54 C112 F56 106.6(8) . . ?
F55 C112 C109 113.4(8) . . ?
F54 C112 C109 107.2(9) . . ?
F56 C112 C109 115.3(7) . . ?
O30 C113 O29 121.0(7) . . ?
O30 C113 C114 116.7(9) . . ?
O29 C113 C114 122.3(8) . . ?
O30 C113 Dy7 64.7(4) . . ?
O29 C113 Dy7 56.4(3) . . ?
C114 C113 Dy7 177.9(8) . . ?
C115 C114 C119 116.7(9) . . ?
C115 C114 C113 119.6(9) . . ?
C119 C114 C113 123.4(9) . . ?
C114 C115 C116 123.7(10) . . ?
C114 C115 H115 118.1 . . ?
C116 C115 H115 118.1 . . ?
F57 C116 C115 122.6(8) . . ?
F57 C116 C117 118.5(7) . . ?
C115 C116 C117 118.9(9) . . ?
C118 C117 C116 117.7(9) . . ?
C118 C117 C120 122.3(10) . . ?
C116 C117 C120 119.9(9) . . ?
C119 C118 C117 119.6(11) . . ?
C119 C118 H118 120.2 . . ?
C117 C118 H118 120.2 . . ?
C118 C119 C114 123.1(11) . . ?
C118 C119 H119 118.4 . . ?
C114 C119 H119 118.4 . . ?
F59 C120 F60 107.3(9) . . ?
F59 C120 F58 104.7(7) . . ?
F60 C120 F58 103.7(6) . . ?
F59 C120 C117 106.6(8) . . ?
F60 C120 C117 110.8(8) . . ?
F58 C120 C117 122.7(10) . . ?
O32 C121 O31 122.4(8) . . ?
O32 C121 C122 116.0(7) . . ?
O31 C121 C122 121.5(8) . . ?
C123 C122 C127 119.4(10) . . ?
C123 C122 C121 114.9(9) . . ?
C127 C122 C121 125.6(9) . . ?
C122 C123 C124 120.2(10) . . ?
C122 C123 H123 119.9 . . ?
C124 C123 H123 119.9 . . ?
F61 C124 C123 119.6(9) . . ?
F61 C124 C125 119.8(9) . . ?
C123 C124 C125 120.6(8) . . ?
C124 C125 C126 119.3(9) . . ?
C124 C125 C128 116.6(8) . . ?
C126 C125 C128 124.0(9) . . ?
C127 C126 C125 118.9(10) . . ?
C127 C126 H126 120.5 . . ?
C125 C126 H126 120.5 . . ?
C126 C127 C122 121.3(10) . . ?
C126 C127 H127 119.3 . . ?
C122 C127 H127 119.3 . . ?
F63 C128 F64 102.7(7) . . ?
F63 C128 F62 106.0(7) . . ?
F64 C128 F62 111.6(8) . . ?
F63 C128 C125 113.4(8) . . ?
F64 C128 C125 112.1(8) . . ?
F62 C128 C125 110.7(8) . . ?
O33 C129 O34 118.5(8) . . ?
O33 C129 C130 124.4(9) . . ?
O34 C129 C130 117.0(7) . . ?
C135 C130 C131 119.2(9) . . ?
C135 C130 C129 121.2(10) . . ?
C131 C130 C129 119.5(8) . . ?
C130 C131 C132 118.0(8) . . ?
C130 C131 H131 121.0 . . ?
C132 C131 H131 121.0 . . ?
F65 C132 C133 125.5(9) . . ?
F65 C132 C131 113.9(8) . . ?
C133 C132 C131 120.4(11) . . ?
C134 C133 C132 121.8(9) . . ?
C134 C133 C136 120.4(8) . . ?
C132 C133 C136 117.7(10) . . ?
C133 C134 C135 118.6(9) . . ?
C133 C134 H134 120.7 . . ?
C135 C134 H134 120.7 . . ?
C134 C135 C130 121.9(10) . . ?
C134 C135 H135 119.0 . . ?
C130 C135 H135 119.0 . . ?
F68 C136 F67 109.7(6) . . ?
F68 C136 F66 106.0(7) . . ?
F67 C136 F66 104.6(7) . . ?
F68 C136 C133 108.0(8) . . ?
F67 C136 C133 121.2(8) . . ?
F66 C136 C133 106.3(7) . . ?
O35 C137 O36 115.7(7) . . ?
O35 C137 C138 113.9(7) . . ?
O36 C137 C138 130.1(8) . . ?
C139 C138 C143 123.0(9) . . ?
C139 C138 C137 111.9(8) . . ?
C143 C138 C137 124.7(8) . . ?
C140 C139 C138 118.9(10) . . ?
C140 C139 H139 120.6 . . ?
C138 C139 H139 120.6 . . ?
F69 C140 C141 120.4(10) . . ?
F69 C140 C139 118.9(11) . . ?
C141 C140 C139 120.7(10) . . ?
C140 C141 C142 120.9(10) . . ?
C140 C141 C144 121.4(10) . . ?
C142 C141 C144 117.6(10) . . ?
C143 C142 C141 119.7(10) . . ?
C143 C142 H142 120.2 . . ?
C141 C142 H142 120.2 . . ?
C138 C143 C142 116.8(9) . . ?
C138 C143 H143 121.6 . . ?
C142 C143 H143 121.6 . . ?
F14 C144 F15 110.0(7) . . ?
F14 C144 F16 109.7(7) . . ?
F15 C144 F16 108.3(7) . . ?
F14 C144 C141 109.5(8) . . ?
F15 C144 C141 111.2(8) . . ?
F16 C144 C141 108.1(8) . . ?
O38 C145 O37 118.5(8) . . ?
O38 C145 C146 105.7(7) . . ?
O37 C145 C146 135.6(7) . . ?
C151 C146 C147 119.5(10) . . ?
C151 C146 C145 120.0(8) . . ?
C147 C146 C145 120.6(9) . . ?
C148 C147 C146 120.2(9) . . ?
C148 C147 H147 119.9 . . ?
C146 C147 H147 119.9 . . ?
C149 C148 F73 114.6(9) . . ?
C149 C148 C147 119.3(9) . . ?
F73 C148 C147 126.0(8) . . ?
C148 C149 C150 121.7(11) . . ?
C148 C149 C152 119.4(9) . . ?
C150 C149 C152 118.8(9) . . ?
C151 C150 C149 119.3(9) . . ?
C151 C150 H150 120.4 . . ?
C149 C150 H150 120.4 . . ?
C150 C151 C146 119.9(9) . . ?
C150 C151 H151 120.0 . . ?
C146 C151 H151 120.0 . . ?
F75 C152 F74 105.8(6) . . ?
F75 C152 F76 106.4(8) . . ?
F74 C152 F76 107.2(7) . . ?
F75 C152 C149 109.1(8) . . ?
F74 C152 C149 116.7(9) . . ?
F76 C152 C149 111.1(7) . . ?
O39 C153 O40 131.2(8) . . ?
O39 C153 C154 118.8(9) . . ?
O40 C153 C154 110.0(8) . . ?
O39 C153 Dy10 76.7(4) . . ?
O40 C153 Dy10 54.8(3) . . ?
C154 C153 Dy10 163.5(7) . . ?
C159 C154 C155 120.9(10) . . ?
C159 C154 C153 121.5(10) . . ?
C155 C154 C153 117.6(10) . . ?
C156 C155 C154 119.6(11) . . ?
C156 C155 H155 120.2 . . ?
C154 C155 H155 120.2 . . ?
F77 C156 C155 121.1(10) . . ?
F77 C156 C157 118.5(9) . . ?
C155 C156 C157 120.4(11) . . ?
C158 C157 C156 118.8(10) . . ?
C158 C157 C160 122.2(11) . . ?
C156 C157 C160 118.7(11) . . ?
C157 C158 C159 122.8(10) . . ?
C157 C158 H158 118.6 . . ?
C159 C158 H158 118.6 . . ?
C154 C159 C158 117.1(12) . . ?
C154 C159 H159 121.5 . . ?
C158 C159 H159 121.5 . . ?
F80 C160 F79 109.4(7) . . ?
F80 C160 F78 107.2(8) . . ?
F79 C160 F78 104.7(8) . . ?
F80 C160 C157 106.3(9) . . ?
F79 C160 C157 113.8(9) . . ?
F78 C160 C157 115.2(9) . . ?
O41 C161 O42 124.2(8) . . ?
O41 C161 C162 119.0(9) . . ?
O42 C161 C162 116.4(7) . . ?
C167 C162 C163 119.8(9) . . ?
C167 C162 C161 115.0(8) . . ?
C163 C162 C161 124.2(9) . . ?
C164 C163 C162 119.2(10) . . ?
C164 C163 H163 120.4 . . ?
C162 C163 H163 120.4 . . ?
C163 C164 F81 117.5(10) . . ?
C163 C164 C165 125.0(10) . . ?
F81 C164 C165 117.5(9) . . ?
C164 C165 C166 116.4(9) . . ?
C164 C165 C168 123.0(9) . . ?
C166 C165 C168 120.5(10) . . ?
C167 C166 C165 118.9(10) . . ?
C167 C166 H166 120.5 . . ?
C165 C166 H166 120.5 . . ?
C162 C167 C166 120.6(8) . . ?
C162 C167 H167 119.7 . . ?
C166 C167 H167 119.7 . . ?
F82 C168 F83 111.0(8) . . ?
F82 C168 F84 106.9(7) . . ?
F83 C168 F84 106.6(7) . . ?
F82 C168 C165 114.8(8) . . ?
F83 C168 C165 112.5(9) . . ?
F84 C168 C165 104.3(8) . . ?
O44 C169 O43 123.1(7) . . ?
O44 C169 C170 121.6(7) . . ?
O43 C169 C170 112.7(9) . . ?
C175 C170 C171 117.1(10) . . ?
C175 C170 C169 116.8(10) . . ?
C171 C170 C169 126.1(8) . . ?
C172 C171 C170 118.9(9) . . ?
C172 C171 H171 120.5 . . ?
C170 C171 H171 120.5 . . ?
C171 C172 C173 123.2(13) . . ?
C171 C172 F85 117.6(9) . . ?
C173 C172 F85 118.1(10) . . ?
C172 C173 C174 117.6(11) . . ?
C172 C173 C176 122.7(12) . . ?
C174 C173 C176 119.6(9) . . ?
C175 C174 C173 121.2(10) . . ?
C175 C174 H174 119.4 . . ?
C173 C174 H174 119.4 . . ?
C174 C175 C170 122.0(12) . . ?
C174 C175 H175 119.0 . . ?
C170 C175 H175 119.0 . . ?
F88 C176 F87 108.9(9) . . ?
F88 C176 F86 106.1(7) . . ?
F87 C176 F86 106.8(9) . . ?
F88 C176 C173 118.5(10) . . ?
F87 C176 C173 104.7(8) . . ?
F86 C176 C173 111.4(9) . . ?
C178 C177 N1 121.6(9) . . ?
C178 C177 H177 119.2 . . ?
N1 C177 H177 119.2 . . ?
C177 C178 C179 119.4(10) . . ?
C177 C178 H178 120.3 . . ?
C179 C178 H178 120.3 . . ?
C180 C179 C178 120.0(9) . . ?
C180 C179 H179 120.0 . . ?
C178 C179 H179 120.0 . . ?
C179 C180 C181 120.6(9) . . ?
C179 C180 H180 119.5 . . ?
C181 C180 H180 119.9 . . ?
N1 C181 C182 118.2(8) . . ?
N1 C181 C180 120.3(8) . . ?
C182 C181 C180 121.5(9) . . ?
N2 C182 C181 119.3(9) . . ?
N2 C182 C183 116.9(9) . . ?
C181 C182 C183 122.9(9) . . ?
C184 C183 C182 123.0(10) . . ?
C184 C183 H183 118.3 . . ?
C182 C183 H183 118.7 . . ?
C183 C184 C185 120.3(9) . . ?
C183 C184 H184 119.8 . . ?
C185 C184 H184 119.8 . . ?
C186 C185 C184 117.6(10) . . ?
C186 C185 H185 121.2 . . ?
C184 C185 H185 121.2 . . ?
N2 C186 C185 119.6(9) . . ?
N2 C186 H186 120.2 . . ?
C185 C186 H186 120.2 . . ?
C188 C187 N3 117.5(8) . . ?
C188 C187 H187 121.3 . . ?
N3 C187 H187 121.3 . . ?
C187 C188 C189 120.0(9) . . ?
C187 C188 H188 120.0 . . ?
C189 C188 H188 120.0 . . ?
C190 C189 C188 118.5(8) . . ?
C190 C189 H189 120.8 . . ?
C188 C189 H189 120.8 . . ?
C189 C190 C191 122.3(10) . . ?
C189 C190 H190 118.8 . . ?
C191 C190 H190 118.8 . . ?
N3 C191 C190 118.7(10) . . ?
N3 C191 C192 113.8(7) . . ?
C190 C191 C192 127.2(9) . . ?
N4 C192 C193 118.0(9) . . ?
N4 C192 C191 119.1(7) . . ?
C193 C192 C191 122.9(10) . . ?
C194 C193 C192 121.1(11) . . ?
C194 C193 H193 119.4 . . ?
C192 C193 H193 119.4 . . ?
C193 C194 C195 120.4(11) . . ?
C193 C194 H194 119.8 . . ?
C195 C194 H194 119.8 . . ?
C196 C195 C194 119.3(12) . . ?
C196 C195 H195 120.4 . . ?
C194 C195 H195 120.4 . . ?
C195 C196 N4 119.3(10) . . ?
C195 C196 H196 120.4 . . ?
N4 C196 H196 120.4 . . ?
C181 N1 C177 118.1(6) . . ?
C181 N1 Dy1 118.8(5) . . ?
C177 N1 Dy1 123.1(5) . . ?
C182 N2 C186 122.0(6) . . ?
C182 N2 Dy1 114.8(6) . . ?
C186 N2 Dy1 122.0(5) . . ?
C191 N3 C187 122.9(6) . . ?
C191 N3 Dy10 122.4(5) . . ?
C187 N3 Dy10 114.5(4) . . ?
C192 N4 C196 121.8(6) . . ?
C192 N4 Dy10 116.4(5) . . ?
C196 N4 Dy10 120.1(5) . . ?
O5 Dy1 O7 90.3(3) . . ?
O5 Dy1 O45 77.3(2) . . ?
O7 Dy1 O45 80.0(2) . . ?
O5 Dy1 O3 66.6(3) . . ?
O7 Dy1 O3 151.0(3) . . ?
O45 Dy1 O3 78.0(3) . . ?
O5 Dy1 O2 142.7(3) . . ?
O7 Dy1 O2 125.6(2) . . ?
O45 Dy1 O2 97.6(2) . . ?
O3 Dy1 O2 76.2(3) . . ?
O5 Dy1 N1 81.1(3) . . ?
O7 Dy1 N1 117.2(3) . . ?
O45 Dy1 N1 152.4(3) . . ?
O3 Dy1 N1 77.8(3) . . ?
O2 Dy1 N1 89.3(3) . . ?
O5 Dy1 N2 130.9(2) . . ?
O7 Dy1 N2 75.0(3) . . ?
O45 Dy1 N2 141.5(3) . . ?
O3 Dy1 N2 133.2(3) . . ?
O2 Dy1 N2 74.7(3) . . ?
N1 Dy1 N2 66.1(3) . . ?
O5 Dy1 O1 146.0(2) . . ?
O7 Dy1 O1 79.7(2) . . ?
O45 Dy1 O1 69.1(2) . . ?
O3 Dy1 O1 109.3(2) . . ?
O2 Dy1 O1 50.4(2) . . ?
N1 Dy1 O1 132.3(3) . . ?
N2 Dy1 O1 77.9(2) . . ?
O5 Dy1 C1 155.4(2) . . ?
O7 Dy1 C1 102.5(2) . . ?
O45 Dy1 C1 84.2(2) . . ?
O3 Dy1 C1 93.9(2) . . ?
O2 Dy1 C1 25.0(2) . . ?
N1 Dy1 C1 110.5(2) . . ?
N2 Dy1 C1 73.3(2) . . ?
O1 Dy1 C1 25.4(2) . . ?
O5 Dy1 Dy2 108.01(16) . . ?
O7 Dy1 Dy2 68.84(13) . . ?
O45 Dy1 Dy2 32.89(16) . . ?
O3 Dy1 Dy2 100.75(16) . . ?
O2 Dy1 Dy2 80.30(16) . . ?
N1 Dy1 Dy2 169.5(2) . . ?
N2 Dy1 Dy2 109.4(2) . . ?
O1 Dy1 Dy2 38.15(15) . . ?
C1 Dy1 Dy2 59.1(2) . . ?
O9 Dy2 O46 146.7(2) . . ?
O9 Dy2 O8 91.2(3) . . ?
O46 Dy2 O8 97.1(2) . . ?
O9 Dy2 O13 79.9(3) . . ?
O46 Dy2 O13 72.4(2) . . ?
O8 Dy2 O13 71.7(2) . . ?
O9 Dy2 O45 145.5(2) . . ?
O46 Dy2 O45 67.7(2) . . ?
O8 Dy2 O45 78.4(2) . . ?
O13 Dy2 O45 125.8(2) . . ?
O9 Dy2 O11 100.2(3) . . ?
O46 Dy2 O11 92.9(2) . . ?
O8 Dy2 O11 142.0(2) . . ?
O13 Dy2 O11 145.85(19) . . ?
O45 Dy2 O11 71.8(2) . . ?
O9 Dy2 O1 76.4(2) . . ?
O46 Dy2 O1 136.7(2) . . ?
O8 Dy2 O1 79.3(2) . . ?
O13 Dy2 O1 141.8(2) . . ?
O45 Dy2 O1 69.4(2) . . ?
O11 Dy2 O1 68.6(2) . . ?
O9 Dy2 O48 85.6(2) . . ?
O46 Dy2 O48 70.04(19) . . ?
O8 Dy2 O48 146.9(2) . . ?
O13 Dy2 O48 75.4(2) . . ?
O45 Dy2 O48 120.5(2) . . ?
O11 Dy2 O48 70.6(2) . . ?
O1 Dy2 O48 131.2(2) . . ?
O9 Dy2 Dy5 120.90(15) . . ?
O46 Dy2 Dy5 36.73(14) . . ?
O8 Dy2 Dy5 132.12(18) . . ?
O13 Dy2 Dy5 79.72(16) . . ?
O45 Dy2 Dy5 88.92(14) . . ?
O11 Dy2 Dy5 70.98(14) . . ?
O1 Dy2 Dy5 138.36(16) . . ?
O48 Dy2 Dy5 35.52(14) . . ?
O9 Dy2 Dy3 173.2(2) . . ?
O46 Dy2 Dy3 35.76(16) . . ?
O8 Dy2 Dy3 94.60(18) . . ?
O13 Dy2 Dy3 105.33(17) . . ?
O45 Dy2 Dy3 33.56(15) . . ?
O11 Dy2 Dy3 73.05(15) . . ?
O1 Dy2 Dy3 101.11(15) . . ?
O48 Dy2 Dy3 91.43(14) . . ?
Dy5 Dy2 Dy3 56.890(10) . . ?
O9 Dy2 Dy1 113.76(17) . . ?
O46 Dy2 Dy1 99.11(14) . . ?
O8 Dy2 Dy1 67.50(18) . . ?
O13 Dy2 Dy1 136.84(14) . . ?
O45 Dy2 Dy1 31.99(15) . . ?
O11 Dy2 Dy1 74.77(12) . . ?
O1 Dy2 Dy1 39.37(13) . . ?
O48 Dy2 Dy1 142.83(16) . . ?
Dy5 Dy2 Dy1 118.916(15) . . ?
Dy3 Dy2 Dy1 65.522(10) . . ?
O4 Dy3 O15 82.0(3) . . ?
O4 Dy3 O45 83.9(3) . . ?
O15 Dy3 O45 151.89(18) . . ?
O4 Dy3 O6 83.5(2) . . ?
O15 Dy3 O6 75.7(2) . . ?
O45 Dy3 O6 78.7(2) . . ?
O4 Dy3 O46 138.5(2) . . ?
O15 Dy3 O46 135.2(2) . . ?
O45 Dy3 O46 68.4(2) . . ?
O6 Dy3 O46 118.5(2) . . ?
O4 Dy3 O47 110.7(2) . . ?
O15 Dy3 O47 74.2(2) . . ?
O45 Dy3 O47 133.8(2) . . ?
O6 Dy3 O47 144.1(2) . . ?
O46 Dy3 O47 73.0(2) . . ?
O4 Dy3 O18 151.9(2) . . ?
O15 Dy3 O18 72.5(3) . . ?
O45 Dy3 O18 113.7(3) . . ?
O6 Dy3 O18 79.1(2) . . ?
O46 Dy3 O18 69.6(2) . . ?
O47 Dy3 O18 73.8(2) . . ?
O4 Dy3 O12 75.0(2) . . ?
O15 Dy3 O12 122.2(2) . . ?
O45 Dy3 O12 76.8(2) . . ?
O6 Dy3 O12 148.8(2) . . ?
O46 Dy3 O12 69.1(2) . . ?
O47 Dy3 O12 66.3(2) . . ?
O18 Dy3 O12 128.81(19) . . ?
O4 Dy3 Dy5 117.47(12) . . ?
O15 Dy3 Dy5 113.86(13) . . ?
O45 Dy3 Dy5 94.23(13) . . ?
O6 Dy3 Dy5 157.27(16) . . ?
O46 Dy3 Dy5 39.99(13) . . ?
O47 Dy3 Dy5 39.76(15) . . ?
O18 Dy3 Dy5 84.27(14) . . ?
O12 Dy3 Dy5 44.54(14) . . ?
O4 Dy3 Dy4 118.59(18) . . ?
O15 Dy3 Dy4 45.22(16) . . ?
O45 Dy3 Dy4 157.30(18) . . ?
O6 Dy3 Dy4 105.27(18) . . ?
O46 Dy3 Dy4 90.73(15) . . ?
O47 Dy3 Dy4 38.89(16) . . ?
O18 Dy3 Dy4 47.43(16) . . ?
O12 Dy3 Dy4 104.87(13) . . ?
Dy5 Dy3 Dy4 73.431(10) . . ?
O4 Dy3 Dy2 108.23(18) . . ?
O15 Dy3 Dy2 169.70(19) . . ?
O45 Dy3 Dy2 35.14(14) . . ?
O6 Dy3 Dy2 106.20(17) . . ?
O46 Dy3 Dy2 34.93(16) . . ?
O47 Dy3 Dy2 100.32(15) . . ?
O18 Dy3 Dy2 97.77(17) . . ?
O12 Dy3 Dy2 61.21(16) . . ?
Dy5 Dy3 Dy2 60.760(10) . . ?
Dy4 Dy3 Dy2 125.51(3) . . ?
O19 Dy4 O26 147.0(2) . 1_655 ?
O19 Dy4 O28 101.0(3) . 1_655 ?
O26 Dy4 O28 91.1(3) 1_655 1_655 ?
O19 Dy4 O2W 82.4(2) . . ?
O26 Dy4 O2W 72.9(3) 1_655 . ?
O28 Dy4 O2W 70.2(2) 1_655 . ?
O19 Dy4 O47 85.3(3) . . ?
O26 Dy4 O47 71.5(3) 1_655 . ?
O28 Dy4 O47 153.9(2) 1_655 . ?
O2W Dy4 O47 85.8(2) . . ?
O19 Dy4 O17 71.3(2) . . ?
O26 Dy4 O17 140.4(2) 1_655 . ?
O28 Dy4 O17 87.7(3) 1_655 . ?
O2W Dy4 O17 141.8(3) . . ?
O47 Dy4 O17 118.2(2) . . ?
O19 Dy4 O16 142.3(3) . . ?
O26 Dy4 O16 70.5(3) 1_655 . ?
O28 Dy4 O16 74.6(2) 1_655 . ?
O2W Dy4 O16 127.8(2) . . ?
O47 Dy4 O16 115.4(2) . . ?
O17 Dy4 O16 71.1(3) . . ?
O19 Dy4 O15 121.8(2) . . ?
O26 Dy4 O15 71.4(2) 1_655 . ?
O28 Dy4 O15 125.7(2) 1_655 . ?
O2W Dy4 O15 140.8(3) . . ?
O47 Dy4 O15 68.1(2) . . ?
O17 Dy4 O15 77.4(2) . . ?
O16 Dy4 O15 51.1(2) . . ?
O19 Dy4 O18 60.1(2) . . ?
O26 Dy4 O18 126.5(2) 1_655 . ?
O28 Dy4 O18 136.9(3) 1_655 . ?
O2W Dy4 O18 134.8(2) . . ?
O47 Dy4 O18 68.0(2) . . ?
O17 Dy4 O18 50.5(2) . . ?
O16 Dy4 O18 97.0(2) . . ?
O15 Dy4 O18 62.0(2) . . ?
O19 Dy4 C65 63.02(18) . . ?
O26 Dy4 C65 139.08(17) 1_655 . ?
O28 Dy4 C65 112.4(2) 1_655 . ?
O2W Dy4 C65 145.4(2) . . ?
O47 Dy4 C65 93.1(2) . . ?
O17 Dy4 C65 25.3(2) . . ?
O16 Dy4 C65 83.68(19) . . ?
O15 Dy4 C65 67.73(17) . . ?
O18 Dy4 C65 25.2(2) . . ?
O19 Dy4 C57 138.1(2) . . ?
O26 Dy4 C57 67.7(2) 1_655 . ?
O28 Dy4 C57 99.6(2) 1_655 . ?
O2W Dy4 C57 139.1(2) . . ?
O47 Dy4 C57 91.8(2) . . ?
O17 Dy4 C57 73.5(2) . . ?
O16 Dy4 C57 25.1(2) . . ?
O15 Dy4 C57 26.1(2) . . ?
O18 Dy4 C57 80.0(2) . . ?
C65 Dy4 C57 75.5(3) . . ?
O19 Dy4 Dy3 89.94(18) . . ?
O26 Dy4 Dy3 86.58(16) 1_655 . ?
O28 Dy4 Dy3 162.79(13) 1_655 . ?
O2W Dy4 Dy3 124.9(2) . . ?
O47 Dy4 Dy3 39.15(13) . . ?
O17 Dy4 Dy3 83.30(16) . . ?
O16 Dy4 Dy3 88.61(17) . . ?
O15 Dy4 Dy3 37.85(14) . . ?
O18 Dy4 Dy3 40.25(16) . . ?
C65 Dy4 Dy3 60.9(2) . . ?
C57 Dy4 Dy3 63.8(2) . . ?
O49 Dy5 O48 64.6(2) . . ?
O49 Dy5 O43 88.8(3) . . ?
O48 Dy5 O43 75.8(3) . . ?
O49 Dy5 O47 147.3(3) . . ?
O48 Dy5 O47 144.67(19) . . ?
O43 Dy5 O47 109.8(3) . . ?
O49 Dy5 O46 114.6(2) . . ?
O48 Dy5 O46 77.2(2) . . ?
O43 Dy5 O46 131.1(2) . . ?
O47 Dy5 O46 73.5(2) . . ?
O49 Dy5 O20 71.4(3) . . ?
O48 Dy5 O20 109.0(3) . . ?
O43 Dy5 O20 153.8(2) . . ?
O47 Dy5 O20 81.5(3) . . ?
O46 Dy5 O20 74.1(2) . . ?
O49 Dy5 O12 147.6(2) . . ?
O48 Dy5 O12 85.8(2) . . ?
O43 Dy5 O12 70.4(2) . . ?
O47 Dy5 O12 65.1(2) . . ?
O46 Dy5 O12 67.7(2) . . ?
O20 Dy5 O12 134.60(18) . . ?
O49 Dy5 O38 88.9(2) . . ?
O48 Dy5 O38 144.6(2) . . ?
O43 Dy5 O38 80.8(2) . . ?
O47 Dy5 O38 68.8(2) . . ?
O46 Dy5 O38 137.6(2) . . ?
O20 Dy5 O38 81.8(2) . . ?
O12 Dy5 O38 111.0(2) . . ?
O49 Dy5 Dy3 154.34(18) . . ?
O48 Dy5 Dy3 104.69(13) . . ?
O43 Dy5 Dy3 111.89(17) . . ?
O47 Dy5 Dy3 40.16(14) . . ?
O46 Dy5 Dy3 40.18(16) . . ?
O20 Dy5 Dy3 92.15(13) . . ?
O12 Dy5 Dy3 42.54(13) . . ?
O38 Dy5 Dy3 108.58(14) . . ?
O49 Dy5 Dy2 100.07(17) . . ?
O48 Dy5 Dy2 43.62(13) . . ?
O43 Dy5 Dy2 100.92(17) . . ?
O47 Dy5 Dy2 102.30(14) . . ?
O46 Dy5 Dy2 36.04(17) . . ?
O20 Dy5 Dy2 99.38(15) . . ?
O12 Dy5 Dy2 61.81(15) . . ?
O38 Dy5 Dy2 170.82(14) . . ?
Dy3 Dy5 Dy2 62.350(10) . . ?
O49 Dy5 Dy6 35.56(18) . . ?
O48 Dy5 Dy6 29.15(17) . . ?
O43 Dy5 Dy6 82.23(19) . . ?
O47 Dy5 Dy6 165.88(17) . . ?
O46 Dy5 Dy6 93.09(16) . . ?
O20 Dy5 Dy6 90.59(18) . . ?
O12 Dy5 Dy6 114.55(14) . . ?
O38 Dy5 Dy6 121.88(14) . . ?
Dy3 Dy5 Dy6 129.320(13) . . ?
Dy2 Dy5 Dy6 67.282(11) . . ?
O48 Dy6 O14 88.5(3) . . ?
O48 Dy6 O23 75.1(2) . . ?
O14 Dy6 O23 157.34(19) . . ?
O48 Dy6 O50 136.7(3) . . ?
O14 Dy6 O50 124.5(3) . . ?
O23 Dy6 O50 64.4(2) . . ?
O48 Dy6 O10 93.3(2) . . ?
O14 Dy6 O10 73.9(3) . . ?
O23 Dy6 O10 91.2(3) . . ?
O50 Dy6 O10 73.4(2) . . ?
O48 Dy6 O49 61.7(2) . . ?
O14 Dy6 O49 78.7(3) . . ?
O23 Dy6 O49 106.1(3) . . ?
O50 Dy6 O49 143.20(18) . . ?
O10 Dy6 O49 143.3(2) . . ?
O48 Dy6 O21 143.8(3) . . ?
O14 Dy6 O21 73.0(2) . . ?
O23 Dy6 O21 129.07(18) . . ?
O50 Dy6 O21 77.9(2) . . ?
O10 Dy6 O21 110.2(2) . . ?
O49 Dy6 O21 83.9(2) . . ?
O48 Dy6 O51 116.2(2) . . ?
O14 Dy6 O51 124.2(2) . . ?
O23 Dy6 O51 77.73(18) . . ?
O50 Dy6 O51 70.64(18) . . ?
O10 Dy6 O51 143.8(2) . . ?
O49 Dy6 O51 72.59(18) . . ?
O21 Dy6 O51 57.5(2) . . ?
O48 Dy6 Dy8 149.51(17) . . ?
O14 Dy6 Dy8 113.74(16) . . ?
O23 Dy6 Dy8 87.46(12) . . ?
O50 Dy6 Dy8 45.80(14) . . ?
O10 Dy6 Dy8 112.18(16) . . ?
O49 Dy6 Dy8 100.92(12) . . ?
O21 Dy6 Dy8 41.89(14) . . ?
O51 Dy6 Dy8 34.14(13) . . ?
O48 Dy6 Dy9 93.51(16) . . ?
O14 Dy6 Dy9 102.97(18) . . ?
O23 Dy6 Dy9 93.77(14) . . ?
O50 Dy6 Dy9 103.56(14) . . ?
O10 Dy6 Dy9 172.41(19) . . ?
O49 Dy6 Dy9 39.84(12) . . ?
O21 Dy6 Dy9 62.21(15) . . ?
O51 Dy6 Dy9 33.00(13) . . ?
Dy8 Dy6 Dy9 62.356(10) . . ?
O48 Dy6 Dy5 29.60(18) . . ?
O14 Dy6 Dy5 80.93(19) . . ?
O23 Dy6 Dy5 91.64(16) . . ?
O50 Dy6 Dy5 154.50(17) . . ?
O10 Dy6 Dy5 117.92(16) . . ?
O49 Dy6 Dy5 32.22(14) . . ?
O21 Dy6 Dy5 114.97(16) . . ?
O51 Dy6 Dy5 97.01(13) . . ?
Dy8 Dy6 Dy5 129.896(14) . . ?
Dy9 Dy6 Dy5 67.740(11) . . ?
O50 Dy7 O27 86.5(3) . . ?
O50 Dy7 O25 153.7(2) . . ?
O27 Dy7 O25 111.5(3) . . ?
O50 Dy7 O24 65.5(3) . . ?
O27 Dy7 O24 136.5(2) . . ?
O25 Dy7 O24 88.6(3) . . ?
O50 Dy7 O29 129.8(2) . . ?
O27 Dy7 O29 77.0(2) . . ?
O25 Dy7 O29 74.6(2) . . ?
O24 Dy7 O29 146.5(3) . . ?
O50 Dy7 O1W 90.7(2) . . ?
O27 Dy7 O1W 74.7(3) . . ?
O25 Dy7 O1W 76.7(2) . . ?
O24 Dy7 O1W 73.1(2) . . ?
O29 Dy7 O1W 128.2(2) . . ?
O50 Dy7 O35 97.0(2) . . ?
O27 Dy7 O35 149.0(2) . . ?
O25 Dy7 O35 77.6(2) . . ?
O24 Dy7 O35 70.8(3) . . ?
O29 Dy7 O35 77.2(3) . . ?
O1W Dy7 O35 135.7(3) . . ?
O50 Dy7 O30 79.1(2) . . ?
O27 Dy7 O30 75.6(2) . . ?
O25 Dy7 O30 122.86(19) . . ?
O24 Dy7 O30 126.0(2) . . ?
O29 Dy7 O30 51.0(2) . . ?
O1W Dy7 O30 149.1(3) . . ?
O35 Dy7 O30 74.9(2) . . ?
O50 Dy7 C113 104.0(2) . . ?
O27 Dy7 C113 74.2(2) . . ?
O25 Dy7 C113 99.4(2) . . ?
O24 Dy7 C113 142.4(2) . . ?
O29 Dy7 C113 25.9(2) . . ?
O1W Dy7 C113 144.5(2) . . ?
O35 Dy7 C113 75.1(2) . . ?
O30 Dy7 C113 25.1(2) . . ?
O50 Dy7 Dy8 41.70(14) . . ?
O27 Dy7 Dy8 86.35(19) . . ?
O25 Dy7 Dy8 152.10(13) . . ?
O24 Dy7 Dy8 92.57(15) . . ?
O29 Dy7 Dy8 89.62(17) . . ?
O1W Dy7 Dy8 130.20(19) . . ?
O35 Dy7 Dy8 76.55(16) . . ?
O30 Dy7 Dy8 38.82(15) . . ?
C113 Dy7 Dy8 63.8(2) . . ?
O51 Dy8 O33 118.6(3) . . ?
O51 Dy8 O31 129.1(3) . . ?
O33 Dy8 O31 76.0(3) . . ?
O51 Dy8 O36 77.9(3) . . ?
O33 Dy8 O36 78.1(3) . . ?
O31 Dy8 O36 149.6(2) . . ?
O51 Dy8 O52 56.6(2) . . ?
O33 Dy8 O52 81.6(2) . . ?
O31 Dy8 O52 81.1(2) . . ?
O36 Dy8 O52 110.6(2) . . ?
O51 Dy8 O30 147.4(3) . . ?
O33 Dy8 O30 73.0(2) . . ?
O31 Dy8 O30 82.2(3) . . ?
O36 Dy8 O30 75.2(3) . . ?
O52 Dy8 O30 152.34(17) . . ?
O51 Dy8 O21 69.8(2) . . ?
O33 Dy8 O21 145.5(3) . . ?
O31 Dy8 O21 74.3(2) . . ?
O36 Dy8 O21 134.8(2) . . ?
O52 Dy8 O21 76.7(2) . . ?
O30 Dy8 O21 119.4(2) . . ?
O51 Dy8 O50 78.2(2) . . ?
O33 Dy8 O50 137.1(2) . . ?
O31 Dy8 O50 126.1(2) . . ?
O36 Dy8 O50 66.9(2) . . ?
O52 Dy8 O50 132.91(19) . . ?
O30 Dy8 O50 74.7(2) . . ?
O21 Dy8 O50 76.1(2) . . ?
O51 Dy8 Dy6 49.14(14) . . ?
O33 Dy8 Dy6 164.8(2) . . ?
O31 Dy8 Dy6 118.28(15) . . ?
O36 Dy8 Dy6 89.41(16) . . ?
O52 Dy8 Dy6 94.96(11) . . ?
O30 Dy8 Dy6 112.39(12) . . ?
O21 Dy8 Dy6 45.53(17) . . ?
O50 Dy8 Dy6 39.96(15) . . ?
O51 Dy8 Dy7 105.80(17) . . ?
O33 Dy8 Dy7 107.26(18) . . ?
O31 Dy8 Dy7 115.84(17) . . ?
O36 Dy8 Dy7 57.99(17) . . ?
O52 Dy8 Dy7 162.05(15) . . ?
O30 Dy8 Dy7 43.47(14) . . ?
O21 Dy8 Dy7 101.39(16) . . ?
O50 Dy8 Dy7 32.46(14) . . ?
Dy6 Dy8 Dy7 72.318(12) . . ?
O51 Dy8 Dy9 22.43(18) . . ?
O33 Dy8 Dy9 112.03(19) . . ?
O31 Dy8 Dy9 107.44(17) . . ?
O36 Dy8 Dy9 96.9(2) . . ?
O52 Dy8 Dy9 36.50(13) . . ?
O30 Dy8 Dy9 169.80(17) . . ?
O21 Dy8 Dy9 61.82(17) . . ?
O50 Dy8 Dy9 96.48(14) . . ?
Dy6 Dy8 Dy9 60.449(11) . . ?
Dy7 Dy8 Dy9 126.828(12) . . ?
O51 Dy9 O39 125.3(2) . . ?
O51 Dy9 O41 88.6(2) . . ?
O39 Dy9 O41 89.9(2) . . ?
O51 Dy9 O44 78.8(3) . . ?
O39 Dy9 O44 151.3(3) . . ?
O41 Dy9 O44 74.0(2) . . ?
O51 Dy9 O52 55.0(2) . . ?
O39 Dy9 O52 71.5(2) . . ?
O41 Dy9 O52 77.3(2) . . ?
O44 Dy9 O52 125.5(2) . . ?
O51 Dy9 O22 88.5(2) . . ?
O39 Dy9 O22 61.7(2) . . ?
O41 Dy9 O22 141.9(2) . . ?
O44 Dy9 O22 142.01(19) . . ?
O52 Dy9 O22 70.13(19) . . ?
O51 Dy9 O49 85.4(2) . . ?
O39 Dy9 O49 121.2(2) . . ?
O41 Dy9 O49 145.2(3) . . ?
O44 Dy9 O49 71.2(2) . . ?
O52 Dy9 O49 124.6(2) . . ?
O22 Dy9 O49 72.2(2) . . ?
O51 Dy9 O37 159.6(3) . . ?
O39 Dy9 O37 75.0(3) . . ?
O41 Dy9 O37 91.0(3) . . ?
O44 Dy9 O37 81.5(3) . . ?
O52 Dy9 O37 144.4(2) . . ?
O22 Dy9 O37 104.0(3) . . ?
O49 Dy9 O37 83.4(2) . . ?
O51 Dy9 Dy6 46.31(13) . . ?
O39 Dy9 Dy6 133.92(19) . . ?
O41 Dy9 Dy6 128.05(19) . . ?
O44 Dy9 Dy6 73.12(16) . . ?
O52 Dy9 Dy6 90.52(13) . . ?
O22 Dy9 Dy6 72.33(15) . . ?
O49 Dy9 Dy6 39.36(16) . . ?
O37 Dy9 Dy6 122.02(14) . . ?
O51 Dy9 Dy8 22.08(18) . . ?
O39 Dy9 Dy8 103.45(18) . . ?
O41 Dy9 Dy8 91.49(19) . . ?
O44 Dy9 Dy8 100.66(18) . . ?
O52 Dy9 Dy8 35.18(13) . . ?
O22 Dy9 Dy8 73.05(15) . . ?
O49 Dy9 Dy8 95.38(16) . . ?
O37 Dy9 Dy8 177.1(2) . . ?
Dy6 Dy9 Dy8 57.196(10) . . ?
O51 Dy9 Dy10 85.26(15) . . ?
O39 Dy9 Dy10 44.07(14) . . ?
O41 Dy9 Dy10 69.23(18) . . ?
O44 Dy9 Dy10 140.11(15) . . ?
O52 Dy9 Dy10 30.84(13) . . ?
O22 Dy9 Dy10 72.71(12) . . ?
O49 Dy9 Dy10 143.80(18) . . ?
O37 Dy9 Dy10 113.57(16) . . ?
Dy6 Dy9 Dy10 119.379(14) . . ?
Dy8 Dy9 Dy10 66.009(10) . . ?
O52 Dy10 O32 77.1(2) . . ?
O52 Dy10 O42 80.1(2) . . ?
O32 Dy10 O42 152.5(3) . . ?
O52 Dy10 O40 97.3(2) . . ?
O32 Dy10 O40 81.3(3) . . ?
O42 Dy10 O40 117.1(3) . . ?
O52 Dy10 N3 150.7(3) . . ?
O32 Dy10 N3 79.8(2) . . ?
O42 Dy10 N3 115.4(2) . . ?
O40 Dy10 N3 96.8(3) . . ?
O52 Dy10 N4 143.5(3) . . ?
O32 Dy10 N4 133.8(3) . . ?
O42 Dy10 N4 73.3(3) . . ?
O40 Dy10 N4 74.0(2) . . ?
N3 Dy10 N4 65.4(3) . . ?
O52 Dy10 O39 62.46(19) . . ?
O32 Dy10 O39 103.4(2) . . ?
O42 Dy10 O39 79.1(2) . . ?
O40 Dy10 O39 47.6(2) . . ?
N3 Dy10 O39 141.7(3) . . ?
N4 Dy10 O39 88.0(2) . . ?
O52 Dy10 O34 84.44(19) . . ?
O32 Dy10 O34 65.0(2) . . ?
O42 Dy10 O34 97.7(2) . . ?
O40 Dy10 O34 145.0(3) . . ?
N3 Dy10 O34 69.5(3) . . ?
N4 Dy10 O34 123.1(2) . . ?
O39 Dy10 O34 146.86(18) . . ?
O52 Dy10 C153 79.47(16) . . ?
O32 Dy10 C153 94.2(2) . . ?
O42 Dy10 C153 96.7(3) . . ?
O40 Dy10 C153 25.0(2) . . ?
N3 Dy10 C153 120.3(2) . . ?
N4 Dy10 C153 79.29(17) . . ?
O39 Dy10 C153 22.7(2) . . ?
O34 Dy10 C153 156.2(2) . . ?
O52 Dy10 Dy9 33.35(15) . . ?
O32 Dy10 Dy9 99.89(13) . . ?
O42 Dy10 Dy9 67.48(13) . . ?
O40 Dy10 Dy9 77.03(18) . . ?
N3 Dy10 Dy9 173.7(2) . . ?
N4 Dy10 Dy9 111.4(2) . . ?
O39 Dy10 Dy9 32.12(13) . . ?
O34 Dy10 Dy9 116.17(14) . . ?
C153 Dy10 Dy9 53.47(19) . . ?
C1 O1 Dy2 136.3(5) . . ?
C1 O1 Dy1 90.5(4) . . ?
Dy2 O1 Dy1 102.5(2) . . ?
C1 O2 Dy1 96.8(5) . . ?
C9 O3 Dy1 147.2(6) . . ?
C9 O4 Dy3 140.0(5) . . ?
C17 O5 Dy1 138.3(5) . . ?
C17 O6 Dy3 145.7(5) . . ?
C25 O7 Dy1 142.7(4) . . ?
C25 O8 Dy2 140.9(5) . . ?
C33 O9 Dy2 126.7(5) . . ?
C33 O10 Dy6 142.8(5) . . ?
C41 O11 Dy2 124.7(4) . . ?
C41 O12 Dy3 129.8(3) . . ?
C41 O12 Dy5 121.2(3) . . ?
Dy3 O12 Dy5 92.9(2) . . ?
C49 O13 Dy2 152.5(4) . . ?
C49 O14 Dy6 131.4(5) . . ?
C57 O15 Dy3 169.9(4) . . ?
C57 O15 Dy4 90.8(5) . . ?
Dy3 O15 Dy4 96.9(2) . . ?
C57 O16 Dy4 98.0(4) . . ?
C65 O17 Dy4 101.0(4) . . ?
C65 O18 Dy3 138.0(4) . . ?
C65 O18 Dy4 86.0(3) . . ?
Dy3 O18 Dy4 92.3(2) . . ?
C73 O19 Dy4 141.3(5) . . ?
C73 O20 Dy5 146.0(5) . . ?
C81 O21 Dy8 124.7(3) . . ?
C81 O21 Dy6 122.4(4) . . ?
Dy8 O21 Dy6 92.6(3) . . ?
C81 O22 Dy9 119.1(4) . . ?
C89 O23 Dy6 142.2(5) . . ?
C89 O24 Dy7 142.1(5) . . ?
C97 O25 Dy7 158.7(4) . . ?
C97 O26 Dy4 146.6(5) . 1_455 ?
C105 O27 Dy7 125.3(5) . . ?
C105 O28 Dy4 159.0(6) . 1_455 ?
C113 O29 Dy7 97.7(4) . . ?
C113 O30 Dy8 170.3(4) . . ?
C113 O30 Dy7 90.2(4) . . ?
Dy8 O30 Dy7 97.7(2) . . ?
C121 O31 Dy8 142.9(5) . . ?
C121 O32 Dy10 145.7(5) . . ?
C129 O33 Dy8 152.2(5) . . ?
C129 O34 Dy10 114.7(4) . . ?
C137 O35 Dy7 117.7(4) . . ?
C137 O36 Dy8 155.6(6) . . ?
C145 O37 Dy9 118.8(5) . . ?
C145 O38 Dy5 118.9(4) . . ?
C153 O39 Dy9 155.5(5) . . ?
C153 O39 Dy10 80.7(4) . . ?
Dy9 O39 Dy10 103.8(2) . . ?
C153 O40 Dy10 100.1(4) . . ?
C161 O41 Dy9 138.0(5) . . ?
C161 O42 Dy10 138.3(4) . . ?
C169 O43 Dy5 125.7(5) . . ?
C169 O44 Dy9 162.3(5) . . ?
Dy3 O45 Dy1 133.5(3) . . ?
Dy3 O45 Dy2 111.3(2) . . ?
Dy1 O45 Dy2 115.1(3) . . ?
Dy3 O45 H45 91.0 . . ?
Dy1 O45 H45 91.0 . . ?
Dy2 O45 H45 91.0 . . ?
Dy2 O46 Dy5 107.2(3) . . ?
Dy2 O46 Dy3 109.3(2) . . ?
Dy5 O46 Dy3 99.8(3) . . ?
Dy2 O46 H46A 113.2 . . ?
Dy5 O46 H46A 113.2 . . ?
Dy3 O46 H46A 113.2 . . ?
Dy4 O47 Dy5 135.6(3) . . ?
Dy4 O47 Dy3 102.0(2) . . ?
Dy5 O47 Dy3 100.1(2) . . ?
Dy4 O47 H47A 105.3 . . ?
Dy5 O47 H47A 105.3 . . ?
Dy3 O47 H47A 105.3 . . ?
Dy6 O48 Dy5 121.3(3) . . ?
Dy6 O48 Dy2 121.1(3) . . ?
Dy5 O48 Dy2 100.9(2) . . ?
Dy6 O48 H48 103.7 . . ?
Dy5 O48 H48 103.7 . . ?
Dy2 O48 H48 103.7 . . ?
Dy5 O49 Dy6 112.2(3) . . ?
Dy5 O49 Dy9 130.5(3) . . ?
Dy6 O49 Dy9 100.8(2) . . ?
Dy5 O49 H49 103.4 . . ?
Dy6 O49 H49 103.4 . . ?
Dy9 O49 H49 103.4 . . ?
Dy7 O50 Dy6 159.1(3) . . ?
Dy7 O50 Dy8 105.8(2) . . ?
Dy6 O50 Dy8 94.2(2) . . ?
Dy7 O50 H50 92.4 . . ?
Dy6 O50 H50 92.4 . . ?
Dy8 O50 H50 92.4 . . ?
Dy8 O51 Dy9 135.5(3) . . ?
Dy8 O51 Dy6 96.7(2) . . ?
Dy9 O51 Dy6 100.69(19) . . ?
Dy8 O51 H51A 106.8 . . ?
Dy9 O51 H51A 106.8 . . ?
Dy6 O51 H51A 106.8 . . ?
Dy10 O52 Dy8 135.8(3) . . ?
Dy10 O52 Dy9 115.8(3) . . ?
Dy8 O52 Dy9 108.32(19) . . ?
Dy10 O52 H52 90.7 . . ?
Dy8 O52 H52 90.7 . . ?
Dy9 O52 H52 90.7 . . ?
Dy7 O1W H1X 109.2 . . ?
Dy7 O1W H1Y 109.7 . . ?
H1X O1W H1Y 109.5 . . ?
Dy4 O2W H2X 109.1 . . ?
Dy4 O2W H2Y 109.7 . . ?
H2X O2W H2Y 109.5 . . ?

_refine_diff_density_max         1.299
_refine_diff_density_min         -1.045
_refine_diff_density_rms         0.201

_shelxl_version_number           2013-2

_database_code_depnum_ccdc_archive 'CCDC 989713'
