# Supplementary Material (ESI) for Journal of Materials Chemistry # This journal is (C) The Royal Society of Chemistry 2006 data_global _journal_coden_Cambridge 1145 loop_ _publ_author_name 'Andres Goeta' 'Royston C. B. Copley' 'Judith A. K. Howard' 'Andrew K. Hughes' "Dermot O'Hare" _publ_contact_author_name 'Andres E. Goeta' _publ_contact_author_address ; Department of Chemistry Durham University Durham DH1 3LE UK ; _publ_contact_author_phone '+44 191 3342102' _publ_contact_author_fax '+44 191 3844737' _publ_contact_author_email A.E.Goeta@durham.ac.uk _publ_requested_journal 'Journal of Materials Chemistry' _publ_section_title ; Structural-Magnetic Correlations on the First Dinuclear Spin Crossover d4 System ; #====================================== data_290k _database_code_depnum_ccdc_archive 'CCDC 618747' _audit_creation_method SHELXL-97 _chemical_name_systematic ; \m~2~-\h^5^,\h^5^-cyclopentaphosphole)-bis ((\h^5^-pentamethyl-cyclopentadienyl)-chromium) hexafluoroantimonate ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H30 Cr2 F6 P5 Sb' _chemical_formula_weight 765.04 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting orthorhombic _symmetry_space_group_name_H-M Fddd loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+3/4, -y+3/4, z' '-x+3/4, y, -z+3/4' 'x, -y+3/4, -z+3/4' 'x, y+1/2, z+1/2' '-x+3/4, -y+5/4, z+1/2' '-x+3/4, y+1/2, -z+5/4' 'x, -y+5/4, -z+5/4' 'x+1/2, y, z+1/2' '-x+5/4, -y+3/4, z+1/2' '-x+5/4, y, -z+5/4' 'x+1/2, -y+3/4, -z+5/4' 'x+1/2, y+1/2, z' '-x+5/4, -y+5/4, z' '-x+5/4, y+1/2, -z+3/4' 'x+1/2, -y+5/4, -z+3/4' '-x, -y, -z' 'x-3/4, y-3/4, -z' 'x-3/4, -y, z-3/4' '-x, y-3/4, z-3/4' '-x, -y+1/2, -z+1/2' 'x-3/4, y-1/4, -z+1/2' 'x-3/4, -y+1/2, z-1/4' '-x, y-1/4, z-1/4' '-x+1/2, -y, -z+1/2' 'x-1/4, y-3/4, -z+1/2' 'x-1/4, -y, z-1/4' '-x+1/2, y-3/4, z-1/4' '-x+1/2, -y+1/2, -z' 'x-1/4, y-1/4, -z' 'x-1/4, -y+1/2, z-3/4' '-x+1/2, y-1/4, z-3/4' _cell_length_a 21.5093(5) _cell_length_b 29.6734(8) _cell_length_c 36.0736(9) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_volume 23024.1(10) _cell_formula_units_Z 32 _cell_measurement_temperature 290(2) _cell_measurement_reflns_used 7897 _cell_measurement_theta_min 2.20 _cell_measurement_theta_max 30.38 _exptl_crystal_description 'irregular block' _exptl_crystal_colour 'dark green' _exptl_crystal_size_max 0.60 _exptl_crystal_size_mid 0.52 _exptl_crystal_size_min 0.40 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.766 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 12096 _exptl_absorpt_coefficient_mu 2.000 _exptl_absorpt_correction_type integration _exptl_absorpt_correction_T_min 0.403 _exptl_absorpt_correction_T_max 0.620 _exptl_absorpt_process_details 'XPREP in SHELXTL' _exptl_special_details ; ? ; _diffrn_ambient_temperature 290(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'Bede Microsource X-ray Generator' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEX CCD Diffractometer' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number 0 _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% 0 _diffrn_reflns_number 43650 _diffrn_reflns_av_R_equivalents 0.0216 _diffrn_reflns_av_sigmaI/netI 0.0195 _diffrn_reflns_limit_h_min -30 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_k_min -41 _diffrn_reflns_limit_k_max 41 _diffrn_reflns_limit_l_min -46 _diffrn_reflns_limit_l_max 51 _diffrn_reflns_theta_min 1.30 _diffrn_reflns_theta_max 30.48 _reflns_number_total 8513 _reflns_number_gt 6155 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'SMART V5.625 (Bruker, 2003)' _computing_cell_refinement 'SMART V5.625 (Bruker, 2003)' _computing_data_reduction 'SAINT V6.28A (Bruker, 2003)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'SHELXTL V6.12(Bruker, 2001)' _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0617P)^2^+44.6428P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 8513 _refine_ls_number_parameters 404 _refine_ls_number_restraints 90 _refine_ls_R_factor_all 0.0573 _refine_ls_R_factor_gt 0.0363 _refine_ls_wR_factor_ref 0.1181 _refine_ls_wR_factor_gt 0.0979 _refine_ls_goodness_of_fit_ref 1.055 _refine_ls_restrained_S_all 1.051 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb1 Sb 0.6250 0.1250 0.010693(9) 0.05827(10) Uani 1 2 d S . . F1A F 0.6878(4) 0.1017(4) -0.0144(3) 0.188(4) Uani 0.50 1 d P . 1 F2A F 0.5539(4) 0.1404(4) 0.0338(3) 0.188(4) Uani 0.50 1 d P . 1 F1B F 0.6682(5) 0.1195(3) -0.0336(2) 0.168(4) Uani 0.50 1 d P . 2 F2B F 0.5904(5) 0.1425(3) 0.0548(2) 0.168(4) Uani 0.50 1 d P . 2 F3 F 0.59339(19) 0.06713(11) 0.01075(12) 0.1506(15) Uani 1 1 d . . . Sb2 Sb 0.1250 0.240738(14) 0.1250 0.06947(11) Uani 1 2 d S . . F4 F 0.18389(19) 0.28518(14) 0.12069(13) 0.1705(19) Uani 1 1 d . . . F5 F 0.1176(2) 0.23917(14) 0.07391(8) 0.1460(15) Uani 1 1 d . . . F6 F 0.18577(15) 0.19626(12) 0.12222(9) 0.1239(11) Uani 1 1 d . . . C1 C 0.13985(13) 0.37027(9) 0.01192(8) 0.0455(6) Uani 1 1 d . A . C2 C 0.19756(13) 0.34972(9) 0.00364(8) 0.0485(6) Uani 1 1 d . A . C3 C 0.22727(13) 0.37498(11) -0.02487(8) 0.0529(7) Uani 1 1 d . A . C4 C 0.18761(14) 0.41180(10) -0.03382(7) 0.0497(6) Uani 1 1 d . A . C5 C 0.13398(12) 0.40868(9) -0.01137(7) 0.0439(5) Uani 1 1 d . A . C6 C 0.09176(17) 0.35278(13) 0.03837(10) 0.0715(9) Uani 1 1 d . . . H6A H 0.0661 0.3310 0.0260 0.107 Uiso 1 1 calc R . . H6B H 0.0664 0.3773 0.0469 0.107 Uiso 1 1 calc R . . H6C H 0.1120 0.3388 0.0591 0.107 Uiso 1 1 calc R . . C7 C 0.2216(2) 0.30683(11) 0.02078(11) 0.0798(12) Uani 1 1 d . . . H7A H 0.1984 0.2817 0.0113 0.120 Uiso 1 1 calc R . . H7B H 0.2168 0.3083 0.0472 0.120 Uiso 1 1 calc R . . H7C H 0.2647 0.3032 0.0147 0.120 Uiso 1 1 calc R . . C8 C 0.28783(16) 0.36406(16) -0.04324(11) 0.0843(13) Uani 1 1 d . . . H8A H 0.2805 0.3445 -0.0640 0.126 Uiso 1 1 calc R . . H8B H 0.3147 0.3493 -0.0258 0.126 Uiso 1 1 calc R . . H8C H 0.3071 0.3914 -0.0517 0.126 Uiso 1 1 calc R . . C9 C 0.1974(2) 0.44599(16) -0.06366(10) 0.0847(12) Uani 1 1 d . . . H9A H 0.1752 0.4370 -0.0855 0.127 Uiso 1 1 calc R . . H9B H 0.2409 0.4482 -0.0692 0.127 Uiso 1 1 calc R . . H9C H 0.1823 0.4748 -0.0554 0.127 Uiso 1 1 calc R . . C10 C 0.07820(15) 0.43890(12) -0.01361(11) 0.0682(9) Uani 1 1 d . . . H10A H 0.0530 0.4302 -0.0344 0.102 Uiso 1 1 calc R . . H10B H 0.0915 0.4695 -0.0167 0.102 Uiso 1 1 calc R . . H10C H 0.0544 0.4363 0.0088 0.102 Uiso 1 1 calc R . . Cr1 Cr 0.215812(17) 0.417948(13) 0.024520(11) 0.03613(9) Uani 1 1 d . . . P11 P 0.1831(10) 0.4395(8) 0.0860(5) 0.067(5) Uani 0.25 1 d PU A 1 P21 P 0.2657(10) 0.3981(3) 0.0823(5) 0.060(4) Uani 0.25 1 d PU A 1 P31 P 0.3236(7) 0.4285(8) 0.0406(6) 0.068(6) Uani 0.25 1 d PU A 1 P41 P 0.2804(12) 0.4853(7) 0.0199(4) 0.079(6) Uani 0.25 1 d PU A 1 P51 P 0.1937(8) 0.4934(6) 0.0479(7) 0.074(7) Uani 0.25 1 d PU A 1 P1 P 0.1983(4) 0.4233(4) 0.0910(2) 0.065(3) Uani 0.50 1 d PU A 2 P2 P 0.2886(5) 0.3967(2) 0.0731(2) 0.061(2) Uani 0.50 1 d PU A 2 P3 P 0.3247(5) 0.4408(5) 0.0305(3) 0.067(3) Uani 0.50 1 d PU A 2 P4 P 0.2574(5) 0.4943(3) 0.0210(3) 0.069(3) Uani 0.50 1 d PU A 2 P5 P 0.1795(4) 0.4839(4) 0.0589(3) 0.069(4) Uani 0.50 1 d PU A 2 P12 P 0.2242(11) 0.4072(5) 0.0918(3) 0.072(5) Uani 0.25 1 d PU A 3 P22 P 0.3118(7) 0.4058(5) 0.0597(6) 0.073(4) Uani 0.25 1 d PU A 3 P32 P 0.3128(7) 0.4611(8) 0.0222(3) 0.080(4) Uani 0.25 1 d PU A 3 P42 P 0.2277(11) 0.4993(3) 0.0299(5) 0.082(5) Uani 0.25 1 d PU A 3 P52 P 0.1728(5) 0.4666(7) 0.0727(6) 0.077(5) Uani 0.25 1 d PU A 3 Cr2 Cr 0.283007(17) 0.477769(12) 0.086221(11) 0.03551(9) Uani 1 1 d . . . C11 C 0.29470(13) 0.49106(9) 0.14580(7) 0.0469(6) Uani 1 1 d . A . C12 C 0.35383(13) 0.48031(9) 0.13061(8) 0.0473(6) Uani 1 1 d . A . C13 C 0.36800(11) 0.51377(9) 0.10353(8) 0.0452(6) Uani 1 1 d . A . C14 C 0.31801(12) 0.54483(8) 0.10244(7) 0.0420(5) Uani 1 1 d . A . C15 C 0.27256(12) 0.53084(9) 0.12855(7) 0.0428(5) Uani 1 1 d . A . C16 C 0.2629(2) 0.46600(14) 0.17641(9) 0.0777(11) Uani 1 1 d . . . H16A H 0.2769 0.4773 0.1999 0.117 Uiso 1 1 calc R A . H16B H 0.2726 0.4345 0.1746 0.117 Uiso 1 1 calc R . . H16C H 0.2187 0.4701 0.1744 0.117 Uiso 1 1 calc R . . C17 C 0.3960(2) 0.44276(12) 0.14234(13) 0.0841(13) Uani 1 1 d . . . H17A H 0.4220 0.4528 0.1624 0.126 Uiso 1 1 calc R A . H17B H 0.4216 0.4339 0.1218 0.126 Uiso 1 1 calc R . . H17C H 0.3716 0.4175 0.1504 0.126 Uiso 1 1 calc R . . C18 C 0.42704(15) 0.51752(15) 0.08198(11) 0.0760(11) Uani 1 1 d . . . H18A H 0.4548 0.5379 0.0944 0.114 Uiso 1 1 calc R A . H18B H 0.4181 0.5287 0.0576 0.114 Uiso 1 1 calc R . . H18C H 0.4461 0.4884 0.0801 0.114 Uiso 1 1 calc R . . C19 C 0.31640(19) 0.58646(10) 0.07898(10) 0.0676(9) Uani 1 1 d . . . H19A H 0.3358 0.6108 0.0921 0.101 Uiso 1 1 calc R A . H19B H 0.2740 0.5942 0.0736 0.101 Uiso 1 1 calc R . . H19C H 0.3384 0.5810 0.0562 0.101 Uiso 1 1 calc R . . C20 C 0.21329(14) 0.55513(12) 0.13759(11) 0.0670(9) Uani 1 1 d . . . H20A H 0.2206 0.5760 0.1575 0.101 Uiso 1 1 calc R A . H20B H 0.1822 0.5337 0.1449 0.101 Uiso 1 1 calc R . . H20C H 0.1992 0.5713 0.1161 0.101 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.04758(15) 0.0723(2) 0.05495(18) 0.000 0.000 0.00334(13) F1A 0.126(4) 0.204(7) 0.234(9) -0.028(6) 0.105(5) 0.039(4) F2A 0.126(4) 0.204(7) 0.234(9) -0.028(6) 0.105(5) 0.039(4) F1B 0.278(10) 0.131(4) 0.096(4) -0.018(3) 0.099(5) -0.015(5) F2B 0.278(10) 0.131(4) 0.096(4) -0.018(3) 0.099(5) -0.015(5) F3 0.176(3) 0.092(2) 0.184(4) 0.016(2) -0.050(3) -0.042(2) Sb2 0.05395(17) 0.0857(2) 0.0687(2) 0.000 0.01024(15) 0.000 F4 0.133(3) 0.148(3) 0.230(5) -0.047(3) 0.042(3) -0.072(3) F5 0.203(4) 0.167(3) 0.0683(18) 0.027(2) -0.006(2) -0.042(3) F6 0.098(2) 0.146(3) 0.128(2) -0.040(2) -0.0016(18) 0.0384(19) C1 0.0469(13) 0.0443(13) 0.0453(14) -0.0061(11) -0.0071(11) -0.0046(10) C2 0.0544(15) 0.0407(12) 0.0505(15) -0.0119(11) -0.0149(12) 0.0070(11) C3 0.0428(13) 0.0697(17) 0.0463(15) -0.0238(13) -0.0052(11) 0.0066(12) C4 0.0522(14) 0.0619(16) 0.0350(13) -0.0015(11) -0.0081(11) -0.0024(12) C5 0.0410(12) 0.0461(12) 0.0447(13) -0.0062(11) -0.0123(10) 0.0056(10) C6 0.070(2) 0.078(2) 0.067(2) -0.0032(18) 0.0060(17) -0.0237(18) C7 0.104(3) 0.0429(15) 0.092(3) -0.0066(16) -0.037(2) 0.0199(17) C8 0.0522(18) 0.125(3) 0.075(2) -0.047(2) 0.0060(17) 0.011(2) C9 0.101(3) 0.106(3) 0.0471(18) 0.0272(19) -0.0102(19) -0.012(2) C10 0.0539(17) 0.071(2) 0.079(2) -0.0111(18) -0.0239(16) 0.0215(15) Cr1 0.03600(18) 0.03740(18) 0.03500(19) -0.00235(14) -0.00453(14) 0.00430(14) P11 0.053(9) 0.101(15) 0.047(8) -0.021(9) 0.012(6) -0.028(8) P21 0.095(11) 0.032(3) 0.053(7) 0.003(3) -0.036(7) 0.003(6) P31 0.033(3) 0.106(14) 0.066(11) -0.046(9) 0.010(5) -0.004(6) P41 0.115(16) 0.079(11) 0.043(3) 0.023(6) -0.023(8) -0.043(9) P51 0.066(11) 0.055(7) 0.101(16) -0.030(9) -0.039(9) 0.032(9) P1 0.070(8) 0.083(8) 0.040(2) -0.004(4) 0.007(4) -0.036(4) P2 0.072(5) 0.0440(14) 0.068(6) -0.008(2) -0.032(4) 0.019(3) P3 0.0457(16) 0.103(7) 0.052(5) -0.029(4) 0.018(3) -0.019(3) P4 0.103(8) 0.048(3) 0.056(2) 0.016(2) -0.028(4) -0.017(4) P5 0.041(3) 0.079(7) 0.088(8) -0.039(5) -0.012(4) 0.019(4) P12 0.112(13) 0.062(7) 0.042(3) 0.004(5) -0.012(8) -0.040(6) P22 0.052(6) 0.077(7) 0.090(10) -0.040(6) -0.030(5) 0.031(5) P32 0.078(8) 0.118(11) 0.046(4) -0.007(6) 0.004(4) -0.045(6) P42 0.116(13) 0.042(2) 0.087(11) 0.001(6) -0.059(7) 0.008(8) P52 0.037(2) 0.103(12) 0.091(12) -0.057(8) 0.002(6) 0.002(8) Cr2 0.03548(18) 0.03619(18) 0.03485(19) -0.00295(14) -0.00078(14) -0.00065(14) C11 0.0584(15) 0.0489(13) 0.0334(12) -0.0015(10) -0.0031(11) -0.0169(12) C12 0.0508(14) 0.0441(12) 0.0470(15) -0.0065(11) -0.0149(12) -0.0011(11) C13 0.0378(12) 0.0533(14) 0.0447(14) -0.0127(11) 0.0023(10) -0.0077(10) C14 0.0466(12) 0.0396(11) 0.0396(12) -0.0031(10) 0.0000(10) -0.0084(10) C15 0.0404(12) 0.0460(13) 0.0419(13) -0.0120(10) 0.0028(10) -0.0046(10) C16 0.103(3) 0.086(2) 0.0435(16) 0.0078(16) 0.0006(17) -0.045(2) C17 0.093(3) 0.0606(19) 0.099(3) -0.012(2) -0.051(2) 0.0199(19) C18 0.0433(15) 0.110(3) 0.074(2) -0.026(2) 0.0156(15) -0.0160(17) C19 0.096(3) 0.0452(15) 0.0619(19) 0.0089(13) -0.0044(18) -0.0153(16) C20 0.0490(15) 0.072(2) 0.080(2) -0.0334(18) 0.0097(15) 0.0026(14) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb1 F1A 1.768(7) . ? Sb1 F1A 1.768(7) 14_545 ? Sb1 F2A 1.802(7) . ? Sb1 F2A 1.802(7) 14_545 ? Sb1 F2B 1.831(6) 14_545 ? Sb1 F2B 1.831(6) . ? Sb1 F3 1.847(3) 14_545 ? Sb1 F3 1.847(3) . ? Sb1 F1B 1.857(7) . ? Sb1 F1B 1.857(7) 14_545 ? F1A F2A 1.766(16) 14_545 ? F2A F1A 1.766(16) 14_545 ? Sb2 F4 1.835(3) 11_454 ? Sb2 F4 1.835(3) . ? Sb2 F5 1.850(3) 11_454 ? Sb2 F5 1.850(3) . ? Sb2 F6 1.860(3) 11_454 ? Sb2 F6 1.860(3) . ? C1 C2 1.415(4) . ? C1 C5 1.422(4) . ? C1 C6 1.500(4) . ? C1 Cr1 2.209(3) . ? C2 C3 1.424(5) . ? C2 C7 1.506(4) . ? C2 Cr1 2.195(3) . ? C3 C4 1.423(4) . ? C3 C8 1.497(4) . ? C3 Cr1 2.205(3) . ? C4 C5 1.413(4) . ? C4 C9 1.494(4) . ? C4 Cr1 2.198(3) . ? C5 C10 1.500(4) . ? C5 Cr1 2.202(2) . ? C6 H6A 0.9600 . ? C6 H6B 0.9600 . ? C6 H6C 0.9600 . ? C7 H7A 0.9600 . ? C7 H7B 0.9600 . ? C7 H7C 0.9600 . ? C8 H8A 0.9600 . ? C8 H8B 0.9600 . ? C8 H8C 0.9600 . ? C9 H9A 0.9600 . ? C9 H9B 0.9600 . ? C9 H9C 0.9600 . ? C10 H10A 0.9600 . ? C10 H10B 0.9600 . ? C10 H10C 0.9600 . ? Cr1 P31 2.411(16) . ? Cr1 P11 2.414(19) . ? Cr1 P21 2.417(12) . ? Cr1 P1 2.432(8) . ? Cr1 P2 2.433(6) . ? Cr1 P42 2.435(9) . ? Cr1 P51 2.439(16) . ? P11 P51 2.12(2) . ? P11 P21 2.166(15) . ? P11 Cr2 2.431(19) . ? P21 P31 2.151(16) . ? P21 Cr2 2.399(11) . ? P31 P41 2.07(2) . ? P31 Cr2 2.367(16) . ? P41 P51 2.13(2) . ? P41 Cr2 2.405(15) . ? P51 Cr2 2.411(16) . ? P1 P5 2.176(10) . ? P1 P2 2.193(8) . ? P1 Cr2 2.442(8) . ? P2 P3 2.164(9) . ? P2 Cr2 2.454(7) . ? P3 P4 2.176(13) . ? P3 Cr2 2.460(10) . ? P4 P5 2.185(11) . ? P4 Cr2 2.467(9) . ? P5 Cr2 2.442(8) . ? P12 P52 2.190(13) . ? P12 P22 2.211(13) . ? P12 Cr2 2.454(10) . ? P22 P32 2.127(13) . ? P22 Cr2 2.420(8) . ? P32 P42 2.170(14) . ? P32 Cr2 2.448(10) . ? P42 P52 2.172(15) . ? P42 Cr2 2.438(10) . ? P52 Cr2 2.443(10) . ? Cr2 C11 2.200(3) . ? Cr2 C15 2.205(2) . ? Cr2 C14 2.207(2) . ? Cr2 C13 2.208(2) . ? Cr2 C12 2.211(3) . ? C11 C15 1.417(4) . ? C11 C12 1.421(4) . ? C11 C16 1.497(4) . ? C12 C13 1.426(4) . ? C12 C17 1.498(4) . ? C13 C14 1.417(4) . ? C13 C18 1.493(4) . ? C14 C15 1.420(4) . ? C14 C19 1.498(4) . ? C15 C20 1.500(4) . ? C16 H16A 0.9600 . ? C16 H16B 0.9600 . ? C16 H16C 0.9600 . ? C17 H17A 0.9600 . ? C17 H17B 0.9600 . ? C17 H17C 0.9600 . ? C18 H18A 0.9600 . ? C18 H18B 0.9600 . ? C18 H18C 0.9600 . ? C19 H19A 0.9600 . ? C19 H19B 0.9600 . ? C19 H19C 0.9600 . ? C20 H20A 0.9600 . ? C20 H20B 0.9600 . ? C20 H20C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F1A Sb1 F1A 118.3(9) . 14_545 ? F1A Sb1 F2A 170.3(6) . . ? F1A Sb1 F2A 59.3(6) 14_545 . ? F1A Sb1 F2A 59.3(6) . 14_545 ? F1A Sb1 F2A 170.3(6) 14_545 14_545 ? F2A Sb1 F2A 124.8(9) . 14_545 ? F1A Sb1 F2B 91.4(5) . 14_545 ? F1A Sb1 F2B 150.1(6) 14_545 14_545 ? F2A Sb1 F2B 90.8(6) . 14_545 ? F2A Sb1 F2B 35.0(4) 14_545 14_545 ? F1A Sb1 F2B 150.1(6) . . ? F1A Sb1 F2B 91.4(5) 14_545 . ? F2A Sb1 F2B 35.0(4) . . ? F2A Sb1 F2B 90.8(6) 14_545 . ? F2B Sb1 F2B 59.4(7) 14_545 . ? F1A Sb1 F3 94.7(4) . 14_545 ? F1A Sb1 F3 85.3(4) 14_545 14_545 ? F2A Sb1 F3 94.4(4) . 14_545 ? F2A Sb1 F3 85.6(4) 14_545 14_545 ? F2B Sb1 F3 96.5(3) 14_545 14_545 ? F2B Sb1 F3 83.4(3) . 14_545 ? F1A Sb1 F3 85.3(4) . . ? F1A Sb1 F3 94.7(4) 14_545 . ? F2A Sb1 F3 85.6(4) . . ? F2A Sb1 F3 94.4(4) 14_545 . ? F2B Sb1 F3 83.4(3) 14_545 . ? F2B Sb1 F3 96.5(3) . . ? F3 Sb1 F3 179.9(3) 14_545 . ? F1A Sb1 F1B 30.8(5) . . ? F1A Sb1 F1B 88.6(6) 14_545 . ? F2A Sb1 F1B 147.8(6) . . ? F2A Sb1 F1B 87.2(5) 14_545 . ? F2B Sb1 F1B 121.3(5) 14_545 . ? F2B Sb1 F1B 167.6(4) . . ? F3 Sb1 F1B 84.2(3) 14_545 . ? F3 Sb1 F1B 95.9(3) . . ? F1A Sb1 F1B 88.6(6) . 14_545 ? F1A Sb1 F1B 30.8(5) 14_545 14_545 ? F2A Sb1 F1B 87.2(5) . 14_545 ? F2A Sb1 F1B 147.8(6) 14_545 14_545 ? F2B Sb1 F1B 167.5(4) 14_545 14_545 ? F2B Sb1 F1B 121.3(5) . 14_545 ? F3 Sb1 F1B 95.9(3) 14_545 14_545 ? F3 Sb1 F1B 84.2(3) . 14_545 ? F1B Sb1 F1B 61.1(8) . 14_545 ? F2A F1A Sb1 61.3(4) 14_545 . ? F1A F2A Sb1 59.4(4) 14_545 . ? F4 Sb2 F4 88.1(3) 11_454 . ? F4 Sb2 F5 89.6(2) 11_454 11_454 ? F4 Sb2 F5 92.5(2) . 11_454 ? F4 Sb2 F5 92.5(2) 11_454 . ? F4 Sb2 F5 89.6(2) . . ? F5 Sb2 F5 177.1(3) 11_454 . ? F4 Sb2 F6 91.17(19) 11_454 11_454 ? F4 Sb2 F6 178.0(2) . 11_454 ? F5 Sb2 F6 89.37(18) 11_454 11_454 ? F5 Sb2 F6 88.59(16) . 11_454 ? F4 Sb2 F6 178.0(2) 11_454 . ? F4 Sb2 F6 91.16(19) . . ? F5 Sb2 F6 88.59(16) 11_454 . ? F5 Sb2 F6 89.36(18) . . ? F6 Sb2 F6 89.6(2) 11_454 . ? C2 C1 C5 107.4(2) . . ? C2 C1 C6 126.2(3) . . ? C5 C1 C6 126.3(3) . . ? C2 C1 Cr1 70.76(15) . . ? C5 C1 Cr1 70.96(14) . . ? C6 C1 Cr1 126.9(2) . . ? C1 C2 C3 108.6(2) . . ? C1 C2 C7 125.3(3) . . ? C3 C2 C7 126.0(3) . . ? C1 C2 Cr1 71.76(14) . . ? C3 C2 Cr1 71.46(15) . . ? C7 C2 Cr1 125.2(2) . . ? C4 C3 C2 107.4(2) . . ? C4 C3 C8 126.0(3) . . ? C2 C3 C8 126.6(3) . . ? C4 C3 Cr1 70.88(15) . . ? C2 C3 Cr1 70.77(15) . . ? C8 C3 Cr1 125.5(2) . . ? C5 C4 C3 108.0(3) . . ? C5 C4 C9 124.9(3) . . ? C3 C4 C9 126.9(3) . . ? C5 C4 Cr1 71.45(15) . . ? C3 C4 Cr1 71.40(15) . . ? C9 C4 Cr1 126.5(2) . . ? C4 C5 C1 108.6(2) . . ? C4 C5 C10 125.7(3) . . ? C1 C5 C10 125.6(3) . . ? C4 C5 Cr1 71.10(14) . . ? C1 C5 Cr1 71.43(14) . . ? C10 C5 Cr1 126.6(2) . . ? C1 C6 H6A 109.5 . . ? C1 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C1 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C2 Cr1 C4 62.97(11) . . ? C2 Cr1 C5 62.63(10) . . ? C4 Cr1 C5 37.45(11) . . ? C2 Cr1 C3 37.77(12) . . ? C4 Cr1 C3 37.72(11) . . ? C5 Cr1 C3 62.74(10) . . ? C2 Cr1 C1 37.47(10) . . ? C4 Cr1 C1 62.97(11) . . ? C5 Cr1 C1 37.60(10) . . ? C3 Cr1 C1 62.99(11) . . ? C2 Cr1 P31 112.0(5) . . ? C4 Cr1 P31 120.4(4) . . ? C5 Cr1 P31 157.9(4) . . ? C3 Cr1 P31 99.3(4) . . ? C1 Cr1 P31 147.6(6) . . ? C2 Cr1 P11 120.5(5) . . ? C4 Cr1 P11 145.2(6) . . ? C5 Cr1 P11 109.9(5) . . ? C3 Cr1 P11 158.2(5) . . ? C1 Cr1 P11 98.2(5) . . ? P31 Cr1 P11 91.4(5) . . ? C2 Cr1 P21 98.6(3) . . ? C4 Cr1 P21 158.1(4) . . ? C5 Cr1 P21 146.2(5) . . ? C3 Cr1 P21 120.4(4) . . ? C1 Cr1 P21 110.5(4) . . ? P31 Cr1 P21 52.9(4) . . ? P11 Cr1 P21 53.3(4) . . ? C2 Cr1 P1 111.8(2) . . ? C4 Cr1 P1 155.0(2) . . ? C5 Cr1 P1 117.6(2) . . ? C3 Cr1 P1 148.4(3) . . ? C1 Cr1 P1 97.48(19) . . ? P31 Cr1 P1 84.4(4) . . ? P11 Cr1 P1 14.4(4) . . ? P21 Cr1 P1 40.1(4) . . ? C2 Cr1 P2 97.10(18) . . ? C4 Cr1 P2 147.8(2) . . ? C5 Cr1 P2 154.9(2) . . ? C3 Cr1 P2 111.1(2) . . ? C1 Cr1 P2 117.3(2) . . ? P31 Cr1 P2 40.7(5) . . ? P11 Cr1 P2 66.0(4) . . ? P21 Cr1 P2 14.0(4) . . ? P1 Cr1 P2 53.58(18) . . ? C2 Cr1 P42 163.8(3) . . ? C4 Cr1 P42 100.8(3) . . ? C5 Cr1 P42 104.8(3) . . ? C3 Cr1 P42 128.8(5) . . ? C1 Cr1 P42 136.8(5) . . ? P31 Cr1 P42 75.5(6) . . ? P11 Cr1 P42 72.2(5) . . ? P21 Cr1 P42 97.3(4) . . ? P1 Cr1 P42 82.7(4) . . ? P2 Cr1 P42 97.5(3) . . ? C2 Cr1 P51 158.5(5) . . ? C4 Cr1 P51 110.7(5) . . ? C5 Cr1 P51 99.3(4) . . ? C3 Cr1 P51 146.3(6) . . ? C1 Cr1 P51 121.0(5) . . ? P31 Cr1 P51 89.1(6) . . ? P11 Cr1 P51 51.8(5) . . ? P21 Cr1 P51 90.7(5) . . ? P1 Cr1 P51 64.5(5) . . ? P2 Cr1 P51 96.5(4) . . ? P42 Cr1 P51 23.5(5) . . ? P51 P11 P21 107.4(8) . . ? P51 P11 Cr1 64.7(6) . . ? P21 P11 Cr1 63.4(6) . . ? P51 P11 Cr2 63.5(6) . . ? P21 P11 Cr2 62.6(5) . . ? Cr1 P11 Cr2 82.5(6) . . ? P31 P21 P11 106.3(7) . . ? P31 P21 Cr2 62.4(6) . . ? P11 P21 Cr2 64.1(5) . . ? P31 P21 Cr1 63.4(5) . . ? P11 P21 Cr1 63.3(5) . . ? Cr2 P21 Cr1 83.1(3) . . ? P41 P31 P21 109.6(8) . . ? P41 P31 Cr2 65.3(7) . . ? P21 P31 Cr2 63.9(4) . . ? P41 P31 Cr1 65.5(7) . . ? P21 P31 Cr1 63.7(5) . . ? Cr2 P31 Cr1 83.9(5) . . ? P31 P41 P51 108.2(8) . . ? P31 P41 Cr2 63.4(5) . . ? P51 P41 Cr2 63.8(7) . . ? P31 P41 Cr1 64.1(6) . . ? P51 P41 Cr1 64.0(6) . . ? Cr2 P41 Cr1 82.4(5) . . ? P11 P51 P41 108.5(8) . . ? P11 P51 Cr2 64.5(7) . . ? P41 P51 Cr2 63.6(5) . . ? P11 P51 Cr1 63.5(7) . . ? P41 P51 Cr1 64.1(6) . . ? Cr2 P51 Cr1 82.3(4) . . ? P5 P1 P2 107.8(4) . . ? P5 P1 Cr1 63.8(3) . . ? P2 P1 Cr1 63.2(3) . . ? P5 P1 Cr2 63.6(3) . . ? P2 P1 Cr2 63.7(3) . . ? Cr1 P1 Cr2 81.9(2) . . ? P3 P2 P1 108.0(4) . . ? P3 P2 Cr1 64.0(3) . . ? P1 P2 Cr1 63.2(2) . . ? P3 P2 Cr2 64.0(4) . . ? P1 P2 Cr2 63.1(2) . . ? Cr1 P2 Cr2 81.59(19) . . ? P2 P3 P4 108.3(5) . . ? P2 P3 Cr1 63.3(3) . . ? P4 P3 Cr1 63.4(4) . . ? P2 P3 Cr2 63.7(3) . . ? P4 P3 Cr2 64.0(4) . . ? Cr1 P3 Cr2 81.2(3) . . ? P3 P4 P5 108.0(5) . . ? P3 P4 Cr1 63.8(3) . . ? P5 P4 Cr1 63.5(4) . . ? P3 P4 Cr2 63.6(3) . . ? P5 P4 Cr2 63.0(4) . . ? Cr1 P4 Cr2 81.2(3) . . ? P1 P5 P4 107.9(5) . . ? P1 P5 Cr2 63.5(3) . . ? P4 P5 Cr2 64.1(3) . . ? P1 P5 Cr1 63.2(4) . . ? P4 P5 Cr1 63.3(3) . . ? Cr2 P5 Cr1 81.6(2) . . ? P52 P12 P22 106.4(6) . . ? P52 P12 Cr1 63.2(4) . . ? P22 P12 Cr1 63.2(4) . . ? P52 P12 Cr2 63.2(4) . . ? P22 P12 Cr2 62.2(4) . . ? Cr1 P12 Cr2 81.2(3) . . ? P32 P22 P12 109.0(5) . . ? P32 P22 Cr2 64.8(4) . . ? P12 P22 Cr2 63.8(3) . . ? P32 P22 Cr1 64.2(4) . . ? P12 P22 Cr1 63.2(3) . . ? Cr2 P22 Cr1 81.9(2) . . ? P22 P32 P42 108.2(6) . . ? P22 P32 Cr1 64.3(3) . . ? P42 P32 Cr1 63.3(4) . . ? P22 P32 Cr2 63.4(3) . . ? P42 P32 Cr2 63.4(4) . . ? Cr1 P32 Cr2 81.4(3) . . ? P32 P42 P52 108.5(6) . . ? P32 P42 Cr1 63.9(4) . . ? P52 P42 Cr1 63.7(4) . . ? P32 P42 Cr2 63.9(4) . . ? P52 P42 Cr2 63.7(4) . . ? Cr1 P42 Cr2 81.9(3) . . ? P42 P52 P12 107.9(6) . . ? P42 P52 Cr1 63.4(4) . . ? P12 P52 Cr1 63.7(4) . . ? P42 P52 Cr2 63.5(4) . . ? P12 P52 Cr2 63.7(4) . . ? Cr1 P52 Cr2 81.6(3) . . ? C11 Cr2 C15 37.53(10) . . ? C11 Cr2 C14 62.63(9) . . ? C15 Cr2 C14 37.54(9) . . ? C11 Cr2 C13 62.76(10) . . ? C15 Cr2 C13 62.80(9) . . ? C14 Cr2 C13 37.44(10) . . ? C11 Cr2 C12 37.59(11) . . ? C15 Cr2 C12 62.90(10) . . ? C14 Cr2 C12 62.75(10) . . ? C13 Cr2 C12 37.65(11) . . ? C11 Cr2 P31 138.4(6) . . ? C15 Cr2 P31 163.7(4) . . ? C14 Cr2 P31 127.9(5) . . ? C13 Cr2 P31 100.9(4) . . ? C12 Cr2 P31 105.7(5) . . ? C11 Cr2 P21 104.6(4) . . ? C15 Cr2 P21 136.9(5) . . ? C14 Cr2 P21 163.3(3) . . ? C13 Cr2 P21 128.5(4) . . ? C12 Cr2 P21 100.6(3) . . ? P31 Cr2 P21 53.6(5) . . ? C11 Cr2 P41 163.4(4) . . ? C15 Cr2 P41 128.3(5) . . ? C14 Cr2 P41 100.8(4) . . ? C13 Cr2 P41 104.8(5) . . ? C12 Cr2 P41 137.2(6) . . ? P31 Cr2 P41 51.3(6) . . ? P21 Cr2 P41 91.7(5) . . ? C11 Cr2 P51 128.1(5) . . ? C15 Cr2 P51 100.3(4) . . ? C14 Cr2 P51 104.5(5) . . ? C13 Cr2 P51 136.8(6) . . ? C12 Cr2 P51 163.2(4) . . ? P31 Cr2 P51 90.8(6) . . ? P21 Cr2 P51 91.9(5) . . ? P41 Cr2 P51 52.6(5) . . ? C11 Cr2 P22 121.0(4) . . ? C15 Cr2 P22 158.4(4) . . ? C14 Cr2 P22 144.4(5) . . ? C13 Cr2 P22 109.1(3) . . ? C12 Cr2 P22 98.0(2) . . ? P31 Cr2 P22 24.0(5) . . ? P21 Cr2 P22 31.3(4) . . ? P41 Cr2 P22 72.3(5) . . ? P51 Cr2 P22 98.5(4) . . ? C11 Cr2 P11 100.8(4) . . ? C15 Cr2 P11 104.2(5) . . ? C14 Cr2 P11 136.4(6) . . ? C13 Cr2 P11 163.6(4) . . ? C12 Cr2 P11 128.8(4) . . ? P31 Cr2 P11 92.0(6) . . ? P21 Cr2 P11 53.3(4) . . ? P41 Cr2 P11 91.1(6) . . ? P51 Cr2 P11 52.0(5) . . ? P22 Cr2 P11 79.2(5) . . ? C11 Cr2 P42 145.3(5) . . ? C15 Cr2 P42 109.9(4) . . ? C14 Cr2 P42 98.7(2) . . ? C13 Cr2 P42 120.9(5) . . ? C12 Cr2 P42 158.4(4) . . ? P31 Cr2 P42 76.3(5) . . ? P21 Cr2 P42 97.7(4) . . ? P41 Cr2 P42 30.1(5) . . ? P51 Cr2 P42 23.6(5) . . ? P22 Cr2 P42 91.6(3) . . ? P11 Cr2 P42 71.9(4) . . ? C15 C11 C12 108.6(2) . . ? C15 C11 C16 125.8(3) . . ? C12 C11 C16 125.6(3) . . ? C15 C11 Cr2 71.44(14) . . ? C12 C11 Cr2 71.65(15) . . ? C16 C11 Cr2 125.42(19) . . ? C11 C12 C13 107.4(2) . . ? C11 C12 C17 126.9(3) . . ? C13 C12 C17 125.6(3) . . ? C11 C12 Cr2 70.76(15) . . ? C13 C12 Cr2 71.03(15) . . ? C17 C12 Cr2 126.6(2) . . ? C14 C13 C12 108.0(2) . . ? C14 C13 C18 125.6(3) . . ? C12 C13 C18 126.2(3) . . ? C14 C13 Cr2 71.24(14) . . ? C12 C13 Cr2 71.32(14) . . ? C18 C13 Cr2 126.4(2) . . ? C13 C14 C15 108.3(2) . . ? C13 C14 C19 124.7(3) . . ? C15 C14 C19 126.9(3) . . ? C13 C14 Cr2 71.32(14) . . ? C15 C14 Cr2 71.17(14) . . ? C19 C14 Cr2 125.9(2) . . ? C11 C15 C14 107.7(2) . . ? C11 C15 C20 126.2(3) . . ? C14 C15 C20 126.1(3) . . ? C11 C15 Cr2 71.03(14) . . ? C14 C15 Cr2 71.29(14) . . ? C20 C15 Cr2 125.47(19) . . ? C11 C16 H16A 109.5 . . ? C11 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C11 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag F1A Sb1 F1A F2A 169.2(7) 14_545 . . 14_545 ? F2A Sb1 F1A F2A -118(4) . . . 14_545 ? F2B Sb1 F1A F2A -14.6(7) 14_545 . . 14_545 ? F2B Sb1 F1A F2A -3.0(11) . . . 14_545 ? F3 Sb1 F1A F2A 82.0(5) 14_545 . . 14_545 ? F3 Sb1 F1A F2A -97.9(5) . . . 14_545 ? F1B Sb1 F1A F2A 152.3(14) . . . 14_545 ? F1B Sb1 F1A F2A 177.8(5) 14_545 . . 14_545 ? F1A Sb1 F2A F1A -78(4) . . . 14_545 ? F2A Sb1 F2A F1A 169.6(6) 14_545 . . 14_545 ? F2B Sb1 F2A F1A 178.5(6) 14_545 . . 14_545 ? F2B Sb1 F2A F1A 153.8(12) . . . 14_545 ? F3 Sb1 F2A F1A 81.9(5) 14_545 . . 14_545 ? F3 Sb1 F2A F1A -98.2(5) . . . 14_545 ? F1B Sb1 F2A F1A -4.1(10) . . . 14_545 ? F1B Sb1 F2A F1A -13.8(7) 14_545 . . 14_545 ? C5 C1 C2 C3 -0.5(3) . . . . ? C6 C1 C2 C3 175.4(3) . . . . ? Cr1 C1 C2 C3 -62.34(18) . . . . ? C5 C1 C2 C7 -177.4(3) . . . . ? C6 C1 C2 C7 -1.5(5) . . . . ? Cr1 C1 C2 C7 120.7(3) . . . . ? C5 C1 C2 Cr1 61.88(18) . . . . ? C6 C1 C2 Cr1 -122.2(3) . . . . ? C1 C2 C3 C4 0.8(3) . . . . ? C7 C2 C3 C4 177.6(3) . . . . ? Cr1 C2 C3 C4 -61.78(19) . . . . ? C1 C2 C3 C8 -177.0(3) . . . . ? C7 C2 C3 C8 -0.2(5) . . . . ? Cr1 C2 C3 C8 120.4(3) . . . . ? C1 C2 C3 Cr1 62.53(18) . . . . ? C7 C2 C3 Cr1 -120.6(3) . . . . ? C2 C3 C4 C5 -0.8(3) . . . . ? C8 C3 C4 C5 177.1(3) . . . . ? Cr1 C3 C4 C5 -62.47(19) . . . . ? C2 C3 C4 C9 -176.1(3) . . . . ? C8 C3 C4 C9 1.7(5) . . . . ? Cr1 C3 C4 C9 122.2(3) . . . . ? C2 C3 C4 Cr1 61.71(18) . . . . ? C8 C3 C4 Cr1 -120.5(3) . . . . ? C3 C4 C5 C1 0.5(3) . . . . ? C9 C4 C5 C1 176.0(3) . . . . ? Cr1 C4 C5 C1 -61.95(18) . . . . ? C3 C4 C5 C10 -175.6(3) . . . . ? C9 C4 C5 C10 -0.1(5) . . . . ? Cr1 C4 C5 C10 122.0(3) . . . . ? C3 C4 C5 Cr1 62.43(19) . . . . ? C9 C4 C5 Cr1 -122.1(3) . . . . ? C2 C1 C5 C4 0.0(3) . . . . ? C6 C1 C5 C4 -175.9(3) . . . . ? Cr1 C1 C5 C4 61.74(18) . . . . ? C2 C1 C5 C10 176.0(3) . . . . ? C6 C1 C5 C10 0.1(4) . . . . ? Cr1 C1 C5 C10 -122.2(3) . . . . ? C2 C1 C5 Cr1 -61.75(18) . . . . ? C6 C1 C5 Cr1 122.4(3) . . . . ? C1 C2 Cr1 C4 -80.03(18) . . . . ? C3 C2 Cr1 C4 37.68(16) . . . . ? C7 C2 Cr1 C4 159.1(4) . . . . ? C1 C2 Cr1 C5 -37.72(16) . . . . ? C3 C2 Cr1 C5 79.99(17) . . . . ? C7 C2 Cr1 C5 -158.6(4) . . . . ? C1 C2 Cr1 C3 -117.7(2) . . . . ? C7 C2 Cr1 C3 121.4(4) . . . . ? C3 C2 Cr1 C1 117.7(2) . . . . ? C7 C2 Cr1 C1 -120.8(4) . . . . ? C1 C2 Cr1 P31 165.9(6) . . . . ? C3 C2 Cr1 P31 -76.4(6) . . . . ? C7 C2 Cr1 P31 45.1(7) . . . . ? C1 C2 Cr1 P11 60.3(7) . . . . ? C3 C2 Cr1 P11 178.0(7) . . . . ? C7 C2 Cr1 P11 -60.5(7) . . . . ? C1 C2 Cr1 P21 112.6(6) . . . . ? C3 C2 Cr1 P21 -129.7(6) . . . . ? C7 C2 Cr1 P21 -8.3(7) . . . . ? C1 C2 Cr1 P1 73.1(3) . . . . ? C3 C2 Cr1 P1 -169.2(3) . . . . ? C7 C2 Cr1 P1 -47.7(4) . . . . ? C1 C2 Cr1 P2 126.6(3) . . . . ? C3 C2 Cr1 P2 -115.6(3) . . . . ? C7 C2 Cr1 P2 5.8(4) . . . . ? C1 C2 Cr1 P42 -79(2) . . . . ? C3 C2 Cr1 P42 39(2) . . . . ? C7 C2 Cr1 P42 160(2) . . . . ? C1 C2 Cr1 P51 -2.2(17) . . . . ? C3 C2 Cr1 P51 115.5(17) . . . . ? C7 C2 Cr1 P51 -123.1(17) . . . . ? C5 C4 Cr1 C2 79.47(17) . . . . ? C3 C4 Cr1 C2 -37.72(18) . . . . ? C9 C4 Cr1 C2 -160.3(4) . . . . ? C3 C4 Cr1 C5 -117.2(2) . . . . ? C9 C4 Cr1 C5 120.2(4) . . . . ? C5 C4 Cr1 C3 117.2(2) . . . . ? C9 C4 Cr1 C3 -122.6(4) . . . . ? C5 C4 Cr1 C1 37.19(16) . . . . ? C3 C4 Cr1 C1 -80.00(19) . . . . ? C9 C4 Cr1 C1 157.4(4) . . . . ? C5 C4 Cr1 P31 -179.7(7) . . . . ? C3 C4 Cr1 P31 63.1(7) . . . . ? C9 C4 Cr1 P31 -59.5(8) . . . . ? C5 C4 Cr1 P11 -25.8(9) . . . . ? C3 C4 Cr1 P11 -143.0(9) . . . . ? C9 C4 Cr1 P11 94.3(9) . . . . ? C5 C4 Cr1 P21 114.7(14) . . . . ? C3 C4 Cr1 P21 -2.5(14) . . . . ? C9 C4 Cr1 P21 -125.1(14) . . . . ? C5 C4 Cr1 P1 -4.2(7) . . . . ? C3 C4 Cr1 P1 -121.4(6) . . . . ? C9 C4 Cr1 P1 116.0(7) . . . . ? C5 C4 Cr1 P2 136.2(5) . . . . ? C3 C4 Cr1 P2 19.0(5) . . . . ? C9 C4 Cr1 P2 -103.7(5) . . . . ? C5 C4 Cr1 P42 -100.2(7) . . . . ? C3 C4 Cr1 P42 142.6(7) . . . . ? C9 C4 Cr1 P42 20.0(7) . . . . ? C5 C4 Cr1 P51 -78.0(6) . . . . ? C3 C4 Cr1 P51 164.8(6) . . . . ? C9 C4 Cr1 P51 42.2(7) . . . . ? C4 C5 Cr1 C2 -80.47(18) . . . . ? C1 C5 Cr1 C2 37.59(16) . . . . ? C10 C5 Cr1 C2 158.6(3) . . . . ? C1 C5 Cr1 C4 118.1(2) . . . . ? C10 C5 Cr1 C4 -120.9(4) . . . . ? C4 C5 Cr1 C3 -37.75(18) . . . . ? C1 C5 Cr1 C3 80.31(18) . . . . ? C10 C5 Cr1 C3 -158.7(3) . . . . ? C4 C5 Cr1 C1 -118.1(2) . . . . ? C10 C5 Cr1 C1 121.0(3) . . . . ? C4 C5 Cr1 P31 0.7(16) . . . . ? C1 C5 Cr1 P31 118.8(16) . . . . ? C10 C5 Cr1 P31 -120.2(16) . . . . ? C4 C5 Cr1 P11 164.7(6) . . . . ? C1 C5 Cr1 P11 -77.3(6) . . . . ? C10 C5 Cr1 P11 43.8(6) . . . . ? C4 C5 Cr1 P21 -142.4(7) . . . . ? C1 C5 Cr1 P21 -24.3(7) . . . . ? C10 C5 Cr1 P21 96.7(8) . . . . ? C4 C5 Cr1 P1 178.0(3) . . . . ? C1 C5 Cr1 P1 -64.0(3) . . . . ? C10 C5 Cr1 P1 57.1(4) . . . . ? C4 C5 Cr1 P2 -119.5(6) . . . . ? C1 C5 Cr1 P2 -1.5(6) . . . . ? C10 C5 Cr1 P2 119.6(6) . . . . ? C4 C5 Cr1 P42 88.6(7) . . . . ? C1 C5 Cr1 P42 -153.3(7) . . . . ? C10 C5 Cr1 P42 -32.3(7) . . . . ? C4 C5 Cr1 P51 112.0(7) . . . . ? C1 C5 Cr1 P51 -129.9(7) . . . . ? C10 C5 Cr1 P51 -8.9(7) . . . . ? C4 C3 Cr1 C2 117.1(2) . . . . ? C8 C3 Cr1 C2 -121.8(4) . . . . ? C2 C3 Cr1 C4 -117.1(2) . . . . ? C8 C3 Cr1 C4 121.1(4) . . . . ? C4 C3 Cr1 C5 37.48(17) . . . . ? C2 C3 Cr1 C5 -79.66(17) . . . . ? C8 C3 Cr1 C5 158.6(4) . . . . ? C4 C3 Cr1 C1 79.94(18) . . . . ? C2 C3 Cr1 C1 -37.20(16) . . . . ? C8 C3 Cr1 C1 -159.0(4) . . . . ? C4 C3 Cr1 P31 -128.8(7) . . . . ? C2 C3 Cr1 P31 114.1(7) . . . . ? C8 C3 Cr1 P31 -7.7(8) . . . . ? C4 C3 Cr1 P11 112.6(15) . . . . ? C2 C3 Cr1 P11 -4.6(16) . . . . ? C8 C3 Cr1 P11 -126.4(16) . . . . ? C4 C3 Cr1 P21 178.9(6) . . . . ? C2 C3 Cr1 P21 61.8(6) . . . . ? C8 C3 Cr1 P21 -60.0(7) . . . . ? C4 C3 Cr1 P1 136.6(5) . . . . ? C2 C3 Cr1 P1 19.4(5) . . . . ? C8 C3 Cr1 P1 -102.3(6) . . . . ? C4 C3 Cr1 P2 -169.3(3) . . . . ? C2 C3 Cr1 P2 73.6(3) . . . . ? C8 C3 Cr1 P2 -48.2(5) . . . . ? C4 C3 Cr1 P42 -49.9(7) . . . . ? C2 C3 Cr1 P42 -167.0(6) . . . . ? C8 C3 Cr1 P42 71.2(7) . . . . ? C4 C3 Cr1 P51 -26.2(9) . . . . ? C2 C3 Cr1 P51 -143.3(9) . . . . ? C8 C3 Cr1 P51 94.9(9) . . . . ? C5 C1 Cr1 C2 -117.1(2) . . . . ? C6 C1 Cr1 C2 121.3(3) . . . . ? C2 C1 Cr1 C4 80.04(18) . . . . ? C5 C1 Cr1 C4 -37.04(16) . . . . ? C6 C1 Cr1 C4 -158.7(3) . . . . ? C2 C1 Cr1 C5 117.1(2) . . . . ? C6 C1 Cr1 C5 -121.6(3) . . . . ? C2 C1 Cr1 C3 37.49(17) . . . . ? C5 C1 Cr1 C3 -79.59(17) . . . . ? C6 C1 Cr1 C3 158.8(3) . . . . ? C2 C1 Cr1 P31 -24.9(9) . . . . ? C5 C1 Cr1 P31 -142.0(9) . . . . ? C6 C1 Cr1 P31 96.4(9) . . . . ? C2 C1 Cr1 P11 -130.8(6) . . . . ? C5 C1 Cr1 P11 112.1(6) . . . . ? C6 C1 Cr1 P11 -9.5(7) . . . . ? C2 C1 Cr1 P21 -77.1(5) . . . . ? C5 C1 Cr1 P21 165.9(5) . . . . ? C6 C1 Cr1 P21 44.2(6) . . . . ? C2 C1 Cr1 P1 -116.3(3) . . . . ? C5 C1 Cr1 P1 126.6(3) . . . . ? C6 C1 Cr1 P1 5.0(4) . . . . ? C2 C1 Cr1 P2 -63.6(3) . . . . ? C5 C1 Cr1 P2 179.3(3) . . . . ? C6 C1 Cr1 P2 57.7(4) . . . . ? C2 C1 Cr1 P42 156.4(8) . . . . ? C5 C1 Cr1 P42 39.4(8) . . . . ? C6 C1 Cr1 P42 -82.3(8) . . . . ? C2 C1 Cr1 P51 179.0(7) . . . . ? C5 C1 Cr1 P51 62.0(7) . . . . ? C6 C1 Cr1 P51 -59.6(8) . . . . ? C2 Cr1 P11 P51 -155.5(5) . . . . ? C4 Cr1 P11 P51 -69.9(9) . . . . ? C5 Cr1 P11 P51 -86.3(6) . . . . ? C3 Cr1 P11 P51 -152.3(10) . . . . ? C1 Cr1 P11 P51 -123.3(6) . . . . ? P31 Cr1 P11 P51 87.7(7) . . . . ? P21 Cr1 P11 P51 127.3(7) . . . . ? P1 Cr1 P11 P51 149(3) . . . . ? P2 Cr1 P11 P51 120.5(7) . . . . ? P42 Cr1 P11 P51 13.4(5) . . . . ? C2 Cr1 P11 P21 77.2(6) . . . . ? C4 Cr1 P11 P21 162.8(5) . . . . ? C5 Cr1 P11 P21 146.4(5) . . . . ? C3 Cr1 P11 P21 80.4(13) . . . . ? C1 Cr1 P11 P21 109.5(6) . . . . ? P31 Cr1 P11 P21 -39.5(6) . . . . ? P1 Cr1 P11 P21 21(2) . . . . ? P2 Cr1 P11 P21 -6.8(5) . . . . ? P42 Cr1 P11 P21 -113.9(6) . . . . ? P51 Cr1 P11 P21 -127.3(7) . . . . ? C2 Cr1 P11 Cr2 140.2(3) . . . . ? C4 Cr1 P11 Cr2 -134.1(5) . . . . ? C5 Cr1 P11 Cr2 -150.5(3) . . . . ? C3 Cr1 P11 Cr2 143.5(10) . . . . ? C1 Cr1 P11 Cr2 172.5(4) . . . . ? P31 Cr1 P11 Cr2 23.5(6) . . . . ? P21 Cr1 P11 Cr2 63.1(4) . . . . ? P1 Cr1 P11 Cr2 84(2) . . . . ? P2 Cr1 P11 Cr2 56.2(4) . . . . ? P42 Cr1 P11 Cr2 -50.8(4) . . . . ? P51 Cr1 P11 Cr2 -64.2(5) . . . . ? P51 P11 P21 P31 -0.9(11) . . . . ? Cr1 P11 P21 P31 48.0(7) . . . . ? Cr2 P11 P21 P31 -47.4(7) . . . . ? P51 P11 P21 Cr2 46.5(8) . . . . ? Cr1 P11 P21 Cr2 95.4(4) . . . . ? P51 P11 P21 Cr1 -48.9(8) . . . . ? Cr2 P11 P21 Cr1 -95.4(4) . . . . ? C2 Cr1 P21 P31 111.1(7) . . . . ? C4 Cr1 P21 P31 79.8(12) . . . . ? C5 Cr1 P21 P31 163.5(6) . . . . ? C3 Cr1 P21 P31 78.0(6) . . . . ? C1 Cr1 P21 P31 148.0(6) . . . . ? P11 Cr1 P21 P31 -127.1(8) . . . . ? P1 Cr1 P21 P31 -135.2(7) . . . . ? P2 Cr1 P21 P31 26.4(16) . . . . ? P42 Cr1 P21 P31 -65.7(7) . . . . ? P51 Cr1 P21 P31 -88.3(7) . . . . ? C2 Cr1 P21 P11 -121.8(6) . . . . ? C4 Cr1 P21 P11 -153.1(11) . . . . ? C5 Cr1 P21 P11 -69.4(7) . . . . ? C3 Cr1 P21 P11 -154.9(6) . . . . ? C1 Cr1 P21 P11 -85.0(6) . . . . ? P31 Cr1 P21 P11 127.1(8) . . . . ? P1 Cr1 P21 P11 -8.1(8) . . . . ? P2 Cr1 P21 P11 153.4(18) . . . . ? P42 Cr1 P21 P11 61.4(6) . . . . ? P51 Cr1 P21 P11 38.7(6) . . . . ? C2 Cr1 P21 Cr2 173.7(4) . . . . ? C4 Cr1 P21 Cr2 142.4(8) . . . . ? C5 Cr1 P21 Cr2 -133.9(3) . . . . ? C3 Cr1 P21 Cr2 140.6(3) . . . . ? C1 Cr1 P21 Cr2 -149.4(4) . . . . ? P31 Cr1 P21 Cr2 62.6(6) . . . . ? P11 Cr1 P21 Cr2 -64.5(6) . . . . ? P1 Cr1 P21 Cr2 -72.6(4) . . . . ? P2 Cr1 P21 Cr2 89.0(17) . . . . ? P42 Cr1 P21 Cr2 -3.1(4) . . . . ? P51 Cr1 P21 Cr2 -25.7(5) . . . . ? P11 P21 P31 P41 0.3(12) . . . . ? Cr2 P21 P31 P41 -48.1(8) . . . . ? Cr1 P21 P31 P41 48.2(8) . . . . ? P11 P21 P31 Cr2 48.3(7) . . . . ? Cr1 P21 P31 Cr2 96.3(4) . . . . ? P11 P21 P31 Cr1 -47.9(7) . . . . ? Cr2 P21 P31 Cr1 -96.3(5) . . . . ? C2 Cr1 P31 P41 146.4(7) . . . . ? C4 Cr1 P31 P41 75.7(8) . . . . ? C5 Cr1 P31 P41 75.2(15) . . . . ? C3 Cr1 P31 P41 109.3(8) . . . . ? C1 Cr1 P31 P41 162.4(6) . . . . ? P11 Cr1 P31 P41 -89.7(7) . . . . ? P21 Cr1 P31 P41 -129.5(8) . . . . ? P1 Cr1 P31 P41 -102.4(7) . . . . ? P2 Cr1 P31 P41 -139.0(9) . . . . ? P42 Cr1 P31 P41 -18.5(6) . . . . ? P51 Cr1 P31 P41 -37.9(7) . . . . ? C2 Cr1 P31 P21 -84.1(5) . . . . ? C4 Cr1 P31 P21 -154.8(4) . . . . ? C5 Cr1 P31 P21 -155.3(11) . . . . ? C3 Cr1 P31 P21 -121.2(5) . . . . ? C1 Cr1 P31 P21 -68.1(7) . . . . ? P11 Cr1 P31 P21 39.8(5) . . . . ? P1 Cr1 P31 P21 27.2(4) . . . . ? P2 Cr1 P31 P21 -9.5(5) . . . . ? P42 Cr1 P31 P21 111.0(6) . . . . ? P51 Cr1 P31 P21 91.6(6) . . . . ? C2 Cr1 P31 Cr2 -148.0(4) . . . . ? C4 Cr1 P31 Cr2 141.3(3) . . . . ? C5 Cr1 P31 Cr2 140.8(10) . . . . ? C3 Cr1 P31 Cr2 174.9(5) . . . . ? C1 Cr1 P31 Cr2 -132.0(5) . . . . ? P11 Cr1 P31 Cr2 -24.1(6) . . . . ? P21 Cr1 P31 Cr2 -63.9(4) . . . . ? P1 Cr1 P31 Cr2 -36.7(4) . . . . ? P2 Cr1 P31 Cr2 -73.4(5) . . . . ? P42 Cr1 P31 Cr2 47.1(5) . . . . ? P51 Cr1 P31 Cr2 27.7(6) . . . . ? P21 P31 P41 P51 0.5(13) . . . . ? Cr2 P31 P41 P51 -46.8(8) . . . . ? Cr1 P31 P41 P51 47.7(8) . . . . ? P21 P31 P41 Cr2 47.3(7) . . . . ? Cr1 P31 P41 Cr2 94.6(4) . . . . ? P21 P31 P41 Cr1 -47.2(7) . . . . ? Cr2 P31 P41 Cr1 -94.6(4) . . . . ? C2 Cr1 P41 P31 -68.4(8) . . . . ? C4 Cr1 P41 P31 -122.2(7) . . . . ? C5 Cr1 P41 P31 -154.9(5) . . . . ? C3 Cr1 P41 P31 -84.9(6) . . . . ? C1 Cr1 P41 P31 -153.6(11) . . . . ? P11 Cr1 P41 P31 91.3(6) . . . . ? P21 Cr1 P41 P31 38.0(6) . . . . ? P1 Cr1 P41 P31 77.8(7) . . . . ? P2 Cr1 P41 P31 25.4(6) . . . . ? P42 Cr1 P41 P31 141.9(12) . . . . ? P51 Cr1 P41 P31 128.6(9) . . . . ? C2 Cr1 P41 P51 163.0(6) . . . . ? C4 Cr1 P41 P51 109.2(7) . . . . ? C5 Cr1 P41 P51 76.6(7) . . . . ? C3 Cr1 P41 P51 146.5(6) . . . . ? C1 Cr1 P41 P51 77.8(15) . . . . ? P31 Cr1 P41 P51 -128.6(9) . . . . ? P11 Cr1 P41 P51 -37.3(7) . . . . ? P21 Cr1 P41 P51 -90.6(7) . . . . ? P1 Cr1 P41 P51 -50.8(7) . . . . ? P2 Cr1 P41 P51 -103.1(6) . . . . ? P42 Cr1 P41 P51 13.4(8) . . . . ? C2 Cr1 P41 Cr2 -132.4(4) . . . . ? C4 Cr1 P41 Cr2 173.7(5) . . . . ? C5 Cr1 P41 Cr2 141.1(3) . . . . ? C3 Cr1 P41 Cr2 -149.0(4) . . . . ? C1 Cr1 P41 Cr2 142.4(11) . . . . ? P31 Cr1 P41 Cr2 -64.1(5) . . . . ? P11 Cr1 P41 Cr2 27.2(5) . . . . ? P21 Cr1 P41 Cr2 -26.1(4) . . . . ? P1 Cr1 P41 Cr2 13.7(5) . . . . ? P2 Cr1 P41 Cr2 -38.6(4) . . . . ? P42 Cr1 P41 Cr2 77.9(9) . . . . ? P51 Cr1 P41 Cr2 64.5(7) . . . . ? P21 P11 P51 P41 1.2(13) . . . . ? Cr1 P11 P51 P41 -47.0(8) . . . . ? Cr2 P11 P51 P41 47.2(8) . . . . ? P21 P11 P51 Cr2 -46.0(7) . . . . ? Cr1 P11 P51 Cr2 -94.2(4) . . . . ? P21 P11 P51 Cr1 48.2(7) . . . . ? Cr2 P11 P51 Cr1 94.2(4) . . . . ? P31 P41 P51 P11 -1.1(14) . . . . ? Cr2 P41 P51 P11 -47.7(8) . . . . ? Cr1 P41 P51 P11 46.7(8) . . . . ? P31 P41 P51 Cr2 46.6(8) . . . . ? Cr1 P41 P51 Cr2 94.4(4) . . . . ? P31 P41 P51 Cr1 -47.7(8) . . . . ? Cr2 P41 P51 Cr1 -94.4(4) . . . . ? C2 Cr1 P51 P11 76.5(15) . . . . ? C4 Cr1 P51 P11 145.1(7) . . . . ? C5 Cr1 P51 P11 108.0(7) . . . . ? C3 Cr1 P51 P11 161.9(7) . . . . ? C1 Cr1 P51 P11 74.9(7) . . . . ? P31 Cr1 P51 P11 -92.5(7) . . . . ? P21 Cr1 P51 P11 -39.6(6) . . . . ? P1 Cr1 P51 P11 -8.2(7) . . . . ? P2 Cr1 P51 P11 -52.4(7) . . . . ? P42 Cr1 P51 P11 -146.3(13) . . . . ? C2 Cr1 P51 P41 -153.9(11) . . . . ? C4 Cr1 P51 P41 -85.4(6) . . . . ? C5 Cr1 P51 P41 -122.4(6) . . . . ? C3 Cr1 P51 P41 -68.6(8) . . . . ? C1 Cr1 P51 P41 -155.5(4) . . . . ? P31 Cr1 P51 P41 37.0(6) . . . . ? P11 Cr1 P51 P41 129.5(8) . . . . ? P21 Cr1 P51 P41 89.9(6) . . . . ? P1 Cr1 P51 P41 121.3(6) . . . . ? P2 Cr1 P51 P41 77.1(6) . . . . ? P42 Cr1 P51 P41 -16.8(10) . . . . ? C2 Cr1 P51 Cr2 141.8(11) . . . . ? C4 Cr1 P51 Cr2 -149.6(4) . . . . ? C5 Cr1 P51 Cr2 173.3(5) . . . . ? C3 Cr1 P51 Cr2 -132.9(4) . . . . ? C1 Cr1 P51 Cr2 140.2(3) . . . . ? P31 Cr1 P51 Cr2 -27.2(5) . . . . ? P11 Cr1 P51 Cr2 65.3(7) . . . . ? P21 Cr1 P51 Cr2 25.6(5) . . . . ? P1 Cr1 P51 Cr2 57.0(4) . . . . ? P2 Cr1 P51 Cr2 12.8(5) . . . . ? P42 Cr1 P51 Cr2 -81.1(10) . . . . ? C2 Cr1 P1 P5 -148.4(3) . . . . ? C4 Cr1 P1 P5 -76.0(6) . . . . ? C5 Cr1 P1 P5 -78.9(3) . . . . ? C3 Cr1 P1 P5 -161.1(3) . . . . ? C1 Cr1 P1 P5 -112.4(3) . . . . ? P31 Cr1 P1 P5 100.1(6) . . . . ? P11 Cr1 P1 P5 -18(2) . . . . ? P21 Cr1 P1 P5 134.5(6) . . . . ? P2 Cr1 P1 P5 129.0(4) . . . . ? P42 Cr1 P1 P5 24.0(4) . . . . ? P51 Cr1 P1 P5 8.4(5) . . . . ? C2 Cr1 P1 P2 82.6(3) . . . . ? C4 Cr1 P1 P2 155.0(4) . . . . ? C5 Cr1 P1 P2 152.1(2) . . . . ? C3 Cr1 P1 P2 69.9(4) . . . . ? C1 Cr1 P1 P2 118.5(3) . . . . ? P31 Cr1 P1 P2 -28.9(6) . . . . ? P11 Cr1 P1 P2 -147(2) . . . . ? P21 Cr1 P1 P2 5.5(6) . . . . ? P42 Cr1 P1 P2 -105.0(4) . . . . ? P51 Cr1 P1 P2 -120.6(5) . . . . ? C2 Cr1 P1 Cr2 147.14(18) . . . . ? C4 Cr1 P1 Cr2 -140.4(4) . . . . ? C5 Cr1 P1 Cr2 -143.34(15) . . . . ? C3 Cr1 P1 Cr2 134.5(3) . . . . ? C1 Cr1 P1 Cr2 -176.9(2) . . . . ? P31 Cr1 P1 Cr2 35.6(5) . . . . ? P11 Cr1 P1 Cr2 -83(2) . . . . ? P21 Cr1 P1 Cr2 70.0(5) . . . . ? P2 Cr1 P1 Cr2 64.6(3) . . . . ? P42 Cr1 P1 Cr2 -40.5(4) . . . . ? P51 Cr1 P1 Cr2 -56.0(4) . . . . ? P5 P1 P2 P3 0.1(6) . . . . ? Cr1 P1 P2 P3 47.1(4) . . . . ? Cr2 P1 P2 P3 -47.0(4) . . . . ? P5 P1 P2 Cr1 -47.1(4) . . . . ? Cr2 P1 P2 Cr1 -94.16(18) . . . . ? P5 P1 P2 Cr2 47.1(4) . . . . ? Cr1 P1 P2 Cr2 94.16(18) . . . . ? C2 Cr1 P2 P3 119.0(4) . . . . ? C4 Cr1 P2 P3 70.4(5) . . . . ? C5 Cr1 P2 P3 153.3(5) . . . . ? C3 Cr1 P2 P3 82.7(4) . . . . ? C1 Cr1 P2 P3 152.3(4) . . . . ? P31 Cr1 P2 P3 3.2(10) . . . . ? P11 Cr1 P2 P3 -120.8(6) . . . . ? P21 Cr1 P2 P3 -143.9(17) . . . . ? P1 Cr1 P2 P3 -129.2(5) . . . . ? P42 Cr1 P2 P3 -54.1(6) . . . . ? P51 Cr1 P2 P3 -77.7(6) . . . . ? C2 Cr1 P2 P1 -111.9(3) . . . . ? C4 Cr1 P2 P1 -160.5(3) . . . . ? C5 Cr1 P2 P1 -77.5(4) . . . . ? C3 Cr1 P2 P1 -148.2(3) . . . . ? C1 Cr1 P2 P1 -78.5(3) . . . . ? P31 Cr1 P2 P1 132.4(7) . . . . ? P11 Cr1 P2 P1 8.4(6) . . . . ? P21 Cr1 P2 P1 -14.7(15) . . . . ? P42 Cr1 P2 P1 75.1(5) . . . . ? P51 Cr1 P2 P1 51.4(5) . . . . ? C2 Cr1 P2 Cr2 -175.9(2) . . . . ? C4 Cr1 P2 Cr2 135.5(2) . . . . ? C5 Cr1 P2 Cr2 -141.6(4) . . . . ? C3 Cr1 P2 Cr2 147.79(18) . . . . ? C1 Cr1 P2 Cr2 -142.60(16) . . . . ? P31 Cr1 P2 Cr2 68.3(7) . . . . ? P11 Cr1 P2 Cr2 -55.6(5) . . . . ? P21 Cr1 P2 Cr2 -78.7(16) . . . . ? P1 Cr1 P2 Cr2 -64.1(2) . . . . ? P42 Cr1 P2 Cr2 11.0(5) . . . . ? P51 Cr1 P2 Cr2 -12.6(5) . . . . ? P1 P2 P3 P4 -0.7(7) . . . . ? Cr1 P2 P3 P4 46.0(4) . . . . ? Cr2 P2 P3 P4 -47.2(4) . . . . ? P1 P2 P3 Cr1 -46.7(4) . . . . ? Cr2 P2 P3 Cr1 -93.2(2) . . . . ? P1 P2 P3 Cr2 46.6(4) . . . . ? Cr1 P2 P3 Cr2 93.2(2) . . . . ? C2 Cr1 P3 P2 -77.4(3) . . . . ? C4 Cr1 P3 P2 -147.3(3) . . . . ? C5 Cr1 P3 P2 -158.7(3) . . . . ? C3 Cr1 P3 P2 -111.2(3) . . . . ? C1 Cr1 P3 P2 -74.7(5) . . . . ? P31 Cr1 P3 P2 -10(3) . . . . ? P11 Cr1 P3 P2 52.3(5) . . . . ? P21 Cr1 P3 P2 9.1(4) . . . . ? P1 Cr1 P3 P2 38.6(3) . . . . ? P42 Cr1 P3 P2 119.7(5) . . . . ? P51 Cr1 P3 P2 102.7(6) . . . . ? C2 Cr1 P3 P4 152.4(3) . . . . ? C4 Cr1 P3 P4 82.6(4) . . . . ? C5 Cr1 P3 P4 71.1(7) . . . . ? C3 Cr1 P3 P4 118.6(4) . . . . ? C1 Cr1 P3 P4 155.1(5) . . . . ? P31 Cr1 P3 P4 -140(3) . . . . ? P11 Cr1 P3 P4 -77.9(5) . . . . ? P21 Cr1 P3 P4 -121.0(5) . . . . ? P1 Cr1 P3 P4 -91.5(4) . . . . ? P2 Cr1 P3 P4 -130.2(5) . . . . ? P42 Cr1 P3 P4 -10.5(5) . . . . ? P51 Cr1 P3 P4 -27.5(6) . . . . ? C2 Cr1 P3 Cr2 -142.4(2) . . . . ? C4 Cr1 P3 Cr2 147.8(2) . . . . ? C5 Cr1 P3 Cr2 136.3(3) . . . . ? C3 Cr1 P3 Cr2 -176.2(3) . . . . ? C1 Cr1 P3 Cr2 -139.7(4) . . . . ? P31 Cr1 P3 Cr2 -75(3) . . . . ? P11 Cr1 P3 Cr2 -12.6(5) . . . . ? P21 Cr1 P3 Cr2 -55.8(3) . . . . ? P1 Cr1 P3 Cr2 -26.3(3) . . . . ? P2 Cr1 P3 Cr2 -65.0(2) . . . . ? P42 Cr1 P3 Cr2 54.7(4) . . . . ? P51 Cr1 P3 Cr2 37.7(5) . . . . ? P2 P3 P4 P5 1.0(7) . . . . ? Cr1 P3 P4 P5 47.0(4) . . . . ? Cr2 P3 P4 P5 -46.1(5) . . . . ? P2 P3 P4 Cr1 -46.0(4) . . . . ? Cr2 P3 P4 Cr1 -93.1(2) . . . . ? P2 P3 P4 Cr2 47.1(4) . . . . ? Cr1 P3 P4 Cr2 93.1(2) . . . . ? C2 Cr1 P4 P3 -74.9(5) . . . . ? C4 Cr1 P4 P3 -111.8(3) . . . . ? C5 Cr1 P4 P3 -147.5(3) . . . . ? C3 Cr1 P4 P3 -77.8(3) . . . . ? C1 Cr1 P4 P3 -159.6(3) . . . . ? P31 Cr1 P4 P3 8.8(6) . . . . ? P11 Cr1 P4 P3 103.1(5) . . . . ? P21 Cr1 P4 P3 51.0(5) . . . . ? P1 Cr1 P4 P3 91.1(3) . . . . ? P2 Cr1 P4 P3 37.4(3) . . . . ? P42 Cr1 P4 P3 145.2(14) . . . . ? P51 Cr1 P4 P3 134.7(8) . . . . ? C2 Cr1 P4 P5 156.1(4) . . . . ? C4 Cr1 P4 P5 119.2(4) . . . . ? C5 Cr1 P4 P5 83.5(4) . . . . ? C3 Cr1 P4 P5 153.1(3) . . . . ? C1 Cr1 P4 P5 71.4(6) . . . . ? P31 Cr1 P4 P5 -120.2(6) . . . . ? P11 Cr1 P4 P5 -25.9(5) . . . . ? P21 Cr1 P4 P5 -78.0(5) . . . . ? P1 Cr1 P4 P5 -37.9(4) . . . . ? P2 Cr1 P4 P5 -91.6(3) . . . . ? P42 Cr1 P4 P5 16.2(11) . . . . ? P51 Cr1 P4 P5 5.6(9) . . . . ? C2 Cr1 P4 Cr2 -139.7(4) . . . . ? C4 Cr1 P4 Cr2 -176.7(2) . . . . ? C5 Cr1 P4 Cr2 147.62(17) . . . . ? C3 Cr1 P4 Cr2 -142.70(17) . . . . ? C1 Cr1 P4 Cr2 135.5(3) . . . . ? P31 Cr1 P4 Cr2 -56.1(4) . . . . ? P11 Cr1 P4 Cr2 38.2(5) . . . . ? P21 Cr1 P4 Cr2 -13.9(4) . . . . ? P1 Cr1 P4 Cr2 26.2(2) . . . . ? P2 Cr1 P4 Cr2 -27.4(2) . . . . ? P42 Cr1 P4 Cr2 80.4(13) . . . . ? P51 Cr1 P4 Cr2 69.8(7) . . . . ? P2 P1 P5 P4 0.5(7) . . . . ? Cr1 P1 P5 P4 -46.2(4) . . . . ? Cr2 P1 P5 P4 47.7(4) . . . . ? P2 P1 P5 Cr2 -47.2(3) . . . . ? Cr1 P1 P5 Cr2 -93.93(18) . . . . ? P2 P1 P5 Cr1 46.8(3) . . . . ? Cr2 P1 P5 Cr1 93.93(18) . . . . ? P3 P4 P5 P1 -1.0(7) . . . . ? Cr1 P4 P5 P1 46.1(4) . . . . ? Cr2 P4 P5 P1 -47.4(4) . . . . ? P3 P4 P5 Cr2 46.4(4) . . . . ? Cr1 P4 P5 Cr2 93.5(2) . . . . ? P3 P4 P5 Cr1 -47.1(4) . . . . ? Cr2 P4 P5 Cr1 -93.5(2) . . . . ? C2 Cr1 P5 P1 69.7(6) . . . . ? C4 Cr1 P5 P1 152.5(3) . . . . ? C5 Cr1 P5 P1 118.6(3) . . . . ? C3 Cr1 P5 P1 156.0(5) . . . . ? C1 Cr1 P5 P1 82.3(3) . . . . ? P31 Cr1 P5 P1 -79.5(6) . . . . ? P11 Cr1 P5 P1 7.1(9) . . . . ? P21 Cr1 P5 P1 -27.5(5) . . . . ? P2 Cr1 P5 P1 -38.7(3) . . . . ? P42 Cr1 P5 P1 -137.7(6) . . . . ? P51 Cr1 P5 P1 -146(2) . . . . ? C2 Cr1 P5 P4 -160.5(3) . . . . ? C4 Cr1 P5 P4 -77.8(4) . . . . ? C5 Cr1 P5 P4 -111.7(4) . . . . ? C3 Cr1 P5 P4 -74.2(5) . . . . ? C1 Cr1 P5 P4 -147.9(3) . . . . ? P31 Cr1 P5 P4 50.3(6) . . . . ? P11 Cr1 P5 P4 136.9(8) . . . . ? P21 Cr1 P5 P4 102.2(5) . . . . ? P1 Cr1 P5 P4 129.7(5) . . . . ? P2 Cr1 P5 P4 91.0(3) . . . . ? P42 Cr1 P5 P4 -7.9(5) . . . . ? P51 Cr1 P5 P4 -16(2) . . . . ? C2 Cr1 P5 Cr2 134.3(3) . . . . ? C4 Cr1 P5 Cr2 -143.00(19) . . . . ? C5 Cr1 P5 Cr2 -176.9(2) . . . . ? C3 Cr1 P5 Cr2 -139.5(4) . . . . ? C1 Cr1 P5 Cr2 146.83(18) . . . . ? P31 Cr1 P5 Cr2 -14.9(5) . . . . ? P11 Cr1 P5 Cr2 71.6(7) . . . . ? P21 Cr1 P5 Cr2 37.0(4) . . . . ? P1 Cr1 P5 Cr2 64.5(3) . . . . ? P2 Cr1 P5 Cr2 25.8(2) . . . . ? P42 Cr1 P5 Cr2 -73.2(4) . . . . ? P51 Cr1 P5 Cr2 -81(2) . . . . ? C2 Cr1 P12 P52 -138.4(5) . . . . ? C4 Cr1 P12 P52 -103.1(16) . . . . ? C5 Cr1 P12 P52 -72.9(5) . . . . ? C3 Cr1 P12 P52 -161.7(4) . . . . ? C1 Cr1 P12 P52 -100.3(5) . . . . ? P31 Cr1 P12 P52 112.3(6) . . . . ? P11 Cr1 P12 P52 -10.9(11) . . . . ? P21 Cr1 P12 P52 141.0(10) . . . . ? P1 Cr1 P12 P52 -17.5(6) . . . . ? P2 Cr1 P12 P52 137.5(6) . . . . ? P42 Cr1 P12 P52 38.2(4) . . . . ? P51 Cr1 P12 P52 19.5(6) . . . . ? C2 Cr1 P12 P22 94.0(5) . . . . ? C4 Cr1 P12 P22 129.4(15) . . . . ? C5 Cr1 P12 P22 159.6(3) . . . . ? C3 Cr1 P12 P22 70.8(5) . . . . ? C1 Cr1 P12 P22 132.2(5) . . . . ? P31 Cr1 P12 P22 -15.2(6) . . . . ? P11 Cr1 P12 P22 -138.5(14) . . . . ? P21 Cr1 P12 P22 13.4(9) . . . . ? P1 Cr1 P12 P22 -145.0(9) . . . . ? P2 Cr1 P12 P22 9.9(4) . . . . ? P42 Cr1 P12 P22 -89.3(4) . . . . ? P51 Cr1 P12 P22 -108.0(5) . . . . ? C2 Cr1 P12 Cr2 157.3(4) . . . . ? C4 Cr1 P12 Cr2 -167.4(15) . . . . ? C5 Cr1 P12 Cr2 -137.2(2) . . . . ? C3 Cr1 P12 Cr2 134.0(2) . . . . ? C1 Cr1 P12 Cr2 -164.6(4) . . . . ? P31 Cr1 P12 Cr2 48.0(5) . . . . ? P11 Cr1 P12 Cr2 -75.2(12) . . . . ? P21 Cr1 P12 Cr2 76.6(9) . . . . ? P1 Cr1 P12 Cr2 -81.8(7) . . . . ? P2 Cr1 P12 Cr2 73.2(4) . . . . ? P42 Cr1 P12 Cr2 -26.1(4) . . . . ? P51 Cr1 P12 Cr2 -44.8(4) . . . . ? P52 P12 P22 P32 -1.1(7) . . . . ? Cr1 P12 P22 P32 46.4(4) . . . . ? Cr2 P12 P22 P32 -47.8(4) . . . . ? P52 P12 P22 Cr2 46.7(5) . . . . ? Cr1 P12 P22 Cr2 94.2(2) . . . . ? P52 P12 P22 Cr1 -47.5(4) . . . . ? Cr2 P12 P22 Cr1 -94.2(2) . . . . ? C2 Cr1 P22 P32 130.9(5) . . . . ? C4 Cr1 P22 P32 68.4(5) . . . . ? C5 Cr1 P22 P32 125.6(16) . . . . ? C3 Cr1 P22 P32 92.3(5) . . . . ? C1 Cr1 P22 P32 158.5(4) . . . . ? P31 Cr1 P22 P32 10.7(11) . . . . ? P11 Cr1 P22 P32 -109.9(5) . . . . ? P21 Cr1 P22 P32 -140.9(8) . . . . ? P1 Cr1 P22 P32 -120.0(5) . . . . ? P2 Cr1 P22 P32 -150.9(10) . . . . ? P42 Cr1 P22 P32 -38.2(4) . . . . ? P51 Cr1 P22 P32 -61.0(6) . . . . ? C2 Cr1 P22 P12 -98.6(5) . . . . ? C4 Cr1 P22 P12 -161.1(3) . . . . ? C5 Cr1 P22 P12 -103.9(17) . . . . ? C3 Cr1 P22 P12 -137.2(5) . . . . ? C1 Cr1 P22 P12 -71.0(4) . . . . ? P31 Cr1 P22 P12 141.2(11) . . . . ? P11 Cr1 P22 P12 20.6(6) . . . . ? P21 Cr1 P22 P12 -10.4(6) . . . . ? P1 Cr1 P22 P12 10.6(3) . . . . ? P2 Cr1 P22 P12 -20.4(7) . . . . ? P42 Cr1 P22 P12 92.3(4) . . . . ? P51 Cr1 P22 P12 69.5(6) . . . . ? C2 Cr1 P22 Cr2 -163.3(4) . . . . ? C4 Cr1 P22 Cr2 134.2(2) . . . . ? C5 Cr1 P22 Cr2 -168.6(16) . . . . ? C3 Cr1 P22 Cr2 158.1(4) . . . . ? C1 Cr1 P22 Cr2 -135.7(2) . . . . ? P31 Cr1 P22 Cr2 76.5(11) . . . . ? P11 Cr1 P22 Cr2 -44.1(5) . . . . ? P21 Cr1 P22 Cr2 -75.0(7) . . . . ? P1 Cr1 P22 Cr2 -54.1(3) . . . . ? P2 Cr1 P22 Cr2 -85.1(8) . . . . ? P42 Cr1 P22 Cr2 27.6(4) . . . . ? P51 Cr1 P22 Cr2 4.8(5) . . . . ? P12 P22 P32 P42 1.0(7) . . . . ? Cr2 P22 P32 P42 -46.2(4) . . . . ? Cr1 P22 P32 P42 46.9(4) . . . . ? P12 P22 P32 Cr1 -45.9(4) . . . . ? Cr2 P22 P32 Cr1 -93.2(2) . . . . ? P12 P22 P32 Cr2 47.3(4) . . . . ? Cr1 P22 P32 Cr2 93.2(2) . . . . ? C2 Cr1 P32 P22 -71.4(4) . . . . ? C4 Cr1 P32 P22 -138.0(5) . . . . ? C5 Cr1 P32 P22 -160.6(3) . . . . ? C3 Cr1 P32 P22 -99.6(5) . . . . ? C1 Cr1 P32 P22 -100.0(15) . . . . ? P31 Cr1 P32 P22 -9.0(8) . . . . ? P11 Cr1 P32 P22 68.8(5) . . . . ? P21 Cr1 P32 P22 19.5(4) . . . . ? P1 Cr1 P32 P22 54.3(5) . . . . ? P2 Cr1 P32 P22 9.2(3) . . . . ? P42 Cr1 P32 P22 129.1(5) . . . . ? P51 Cr1 P32 P22 114.4(6) . . . . ? C2 Cr1 P32 P42 159.5(4) . . . . ? C4 Cr1 P32 P42 92.9(5) . . . . ? C5 Cr1 P32 P42 70.4(5) . . . . ? C3 Cr1 P32 P42 131.4(6) . . . . ? C1 Cr1 P32 P42 130.9(15) . . . . ? P31 Cr1 P32 P42 -138.0(11) . . . . ? P11 Cr1 P32 P42 -60.2(5) . . . . ? P21 Cr1 P32 P42 -109.6(4) . . . . ? P1 Cr1 P32 P42 -74.8(5) . . . . ? P2 Cr1 P32 P42 -119.9(5) . . . . ? P51 Cr1 P32 P42 -14.7(5) . . . . ? C2 Cr1 P32 Cr2 -136.0(3) . . . . ? C4 Cr1 P32 Cr2 157.4(4) . . . . ? C5 Cr1 P32 Cr2 134.8(2) . . . . ? C3 Cr1 P32 Cr2 -164.1(4) . . . . ? C1 Cr1 P32 Cr2 -164.6(15) . . . . ? P31 Cr1 P32 Cr2 -73.6(9) . . . . ? P11 Cr1 P32 Cr2 4.2(4) . . . . ? P21 Cr1 P32 Cr2 -45.1(3) . . . . ? P1 Cr1 P32 Cr2 -10.3(4) . . . . ? P2 Cr1 P32 Cr2 -55.4(3) . . . . ? P42 Cr1 P32 Cr2 64.5(4) . . . . ? P51 Cr1 P32 Cr2 49.8(5) . . . . ? P22 P32 P42 P52 -0.5(8) . . . . ? Cr1 P32 P42 P52 46.9(5) . . . . ? Cr2 P32 P42 P52 -46.8(5) . . . . ? P22 P32 P42 Cr1 -47.5(4) . . . . ? Cr2 P32 P42 Cr1 -93.7(3) . . . . ? P22 P32 P42 Cr2 46.2(4) . . . . ? Cr1 P32 P42 Cr2 93.7(3) . . . . ? C2 Cr1 P42 P32 -100.8(18) . . . . ? C4 Cr1 P42 P32 -99.7(5) . . . . ? C5 Cr1 P42 P32 -137.9(5) . . . . ? C3 Cr1 P42 P32 -71.2(4) . . . . ? C1 Cr1 P42 P32 -161.5(3) . . . . ? P31 Cr1 P42 P32 19.2(5) . . . . ? P11 Cr1 P42 P32 115.5(5) . . . . ? P21 Cr1 P42 P32 67.9(5) . . . . ? P1 Cr1 P42 P32 105.3(5) . . . . ? P2 Cr1 P42 P32 53.7(5) . . . . ? P51 Cr1 P42 P32 142.7(12) . . . . ? C2 Cr1 P42 P52 129.8(18) . . . . ? C4 Cr1 P42 P52 130.9(5) . . . . ? C5 Cr1 P42 P52 92.7(5) . . . . ? C3 Cr1 P42 P52 159.4(4) . . . . ? C1 Cr1 P42 P52 69.1(5) . . . . ? P31 Cr1 P42 P52 -110.2(5) . . . . ? P11 Cr1 P42 P52 -13.9(5) . . . . ? P21 Cr1 P42 P52 -61.5(5) . . . . ? P1 Cr1 P42 P52 -24.1(5) . . . . ? P2 Cr1 P42 P52 -75.7(5) . . . . ? P51 Cr1 P42 P52 13.3(12) . . . . ? C2 Cr1 P42 Cr2 -165.6(17) . . . . ? C4 Cr1 P42 Cr2 -164.5(5) . . . . ? C5 Cr1 P42 Cr2 157.3(4) . . . . ? C3 Cr1 P42 Cr2 -136.1(3) . . . . ? C1 Cr1 P42 Cr2 133.7(2) . . . . ? P31 Cr1 P42 Cr2 -45.6(4) . . . . ? P11 Cr1 P42 Cr2 50.7(4) . . . . ? P21 Cr1 P42 Cr2 3.1(4) . . . . ? P1 Cr1 P42 Cr2 40.5(4) . . . . ? P2 Cr1 P42 Cr2 -11.1(5) . . . . ? P51 Cr1 P42 Cr2 77.9(11) . . . . ? P32 P42 P52 P12 -0.2(8) . . . . ? Cr1 P42 P52 P12 46.9(5) . . . . ? Cr2 P42 P52 P12 -47.0(5) . . . . ? P32 P42 P52 Cr1 -47.0(5) . . . . ? Cr2 P42 P52 Cr1 -93.9(3) . . . . ? P32 P42 P52 Cr2 46.9(5) . . . . ? Cr1 P42 P52 Cr2 93.9(3) . . . . ? P22 P12 P52 P42 0.8(8) . . . . ? Cr1 P12 P52 P42 -46.7(5) . . . . ? Cr2 P12 P52 P42 46.9(5) . . . . ? P22 P12 P52 Cr1 47.5(4) . . . . ? Cr2 P12 P52 Cr1 93.6(3) . . . . ? P22 P12 P52 Cr2 -46.1(4) . . . . ? Cr1 P12 P52 Cr2 -93.6(3) . . . . ? C2 Cr1 P52 P42 -162.0(3) . . . . ? C4 Cr1 P52 P42 -72.2(5) . . . . ? C5 Cr1 P52 P42 -100.3(5) . . . . ? C3 Cr1 P52 P42 -102.2(18) . . . . ? C1 Cr1 P52 P42 -138.8(5) . . . . ? P31 Cr1 P52 P42 66.2(6) . . . . ? P11 Cr1 P52 P42 143.9(14) . . . . ? P21 Cr1 P52 P42 113.9(5) . . . . ? P1 Cr1 P52 P42 137.7(6) . . . . ? P2 Cr1 P52 P42 104.7(5) . . . . ? P51 Cr1 P52 P42 -10.5(9) . . . . ? C2 Cr1 P52 P12 68.8(5) . . . . ? C4 Cr1 P52 P12 158.6(4) . . . . ? C5 Cr1 P52 P12 130.5(5) . . . . ? C3 Cr1 P52 P12 128.6(18) . . . . ? C1 Cr1 P52 P12 92.0(5) . . . . ? P31 Cr1 P52 P12 -63.0(6) . . . . ? P11 Cr1 P52 P12 14.7(14) . . . . ? P21 Cr1 P52 P12 -15.3(5) . . . . ? P1 Cr1 P52 P12 8.5(4) . . . . ? P2 Cr1 P52 P12 -24.5(4) . . . . ? P42 Cr1 P52 P12 -129.2(6) . . . . ? P51 Cr1 P52 P12 -139.7(12) . . . . ? C2 Cr1 P52 Cr2 133.6(2) . . . . ? C4 Cr1 P52 Cr2 -136.7(2) . . . . ? C5 Cr1 P52 Cr2 -164.8(5) . . . . ? C3 Cr1 P52 Cr2 -166.6(17) . . . . ? C1 Cr1 P52 Cr2 156.8(4) . . . . ? P31 Cr1 P52 Cr2 1.8(6) . . . . ? P11 Cr1 P52 Cr2 79.5(13) . . . . ? P21 Cr1 P52 Cr2 49.4(4) . . . . ? P1 Cr1 P52 Cr2 73.3(5) . . . . ? P2 Cr1 P52 Cr2 40.3(4) . . . . ? P42 Cr1 P52 Cr2 -64.5(4) . . . . ? P51 Cr1 P52 Cr2 -74.9(10) . . . . ? P41 P31 Cr2 C11 -161.3(6) . . . . ? P21 P31 Cr2 C11 69.1(7) . . . . ? Cr1 P31 Cr2 C11 132.8(4) . . . . ? P41 P31 Cr2 C15 -95(2) . . . . ? P21 P31 Cr2 C15 135.2(19) . . . . ? Cr1 P31 Cr2 C15 -161.1(17) . . . . ? P41 P31 Cr2 C14 -71.4(8) . . . . ? P21 P31 Cr2 C14 159.1(4) . . . . ? Cr1 P31 Cr2 C14 -137.2(3) . . . . ? P41 P31 Cr2 C13 -100.3(7) . . . . ? P21 P31 Cr2 C13 130.1(5) . . . . ? Cr1 P31 Cr2 C13 -166.2(5) . . . . ? P41 P31 Cr2 C12 -138.8(7) . . . . ? P21 P31 Cr2 C12 91.7(5) . . . . ? Cr1 P31 Cr2 C12 155.4(4) . . . . ? P41 P31 Cr2 P21 129.5(8) . . . . ? Cr1 P31 Cr2 P21 63.7(5) . . . . ? P21 P31 Cr2 P41 -129.5(8) . . . . ? Cr1 P31 Cr2 P41 -65.9(7) . . . . ? P41 P31 Cr2 P51 37.8(7) . . . . ? P21 P31 Cr2 P51 -91.7(6) . . . . ? Cr1 P31 Cr2 P51 -28.0(6) . . . . ? P41 P31 Cr2 P22 147.1(13) . . . . ? P21 P31 Cr2 P22 17.6(9) . . . . ? Cr1 P31 Cr2 P22 81.2(9) . . . . ? P41 P31 Cr2 P11 89.8(7) . . . . ? P21 P31 Cr2 P11 -39.7(5) . . . . ? Cr1 P31 Cr2 P11 23.9(5) . . . . ? P41 P31 Cr2 P42 19.0(7) . . . . ? P21 P31 Cr2 P42 -110.5(5) . . . . ? Cr1 P31 Cr2 P42 -46.8(5) . . . . ? P31 P21 Cr2 C11 -140.1(6) . . . . ? P11 P21 Cr2 C11 92.7(6) . . . . ? Cr1 P21 Cr2 C11 156.3(4) . . . . ? P31 P21 Cr2 C15 -163.2(6) . . . . ? P11 P21 Cr2 C15 69.7(6) . . . . ? Cr1 P21 Cr2 C15 133.3(3) . . . . ? P31 P21 Cr2 C14 -101.7(17) . . . . ? P11 P21 Cr2 C14 131.1(17) . . . . ? Cr1 P21 Cr2 C14 -165.3(15) . . . . ? P31 P21 Cr2 C13 -73.5(6) . . . . ? P11 P21 Cr2 C13 159.3(5) . . . . ? Cr1 P21 Cr2 C13 -137.0(2) . . . . ? P31 P21 Cr2 C12 -101.8(7) . . . . ? P11 P21 Cr2 C12 131.1(6) . . . . ? Cr1 P21 Cr2 C12 -165.3(4) . . . . ? P11 P21 Cr2 P31 -127.2(8) . . . . ? Cr1 P21 Cr2 P31 -63.6(6) . . . . ? P31 P21 Cr2 P41 37.0(7) . . . . ? P11 P21 Cr2 P41 -90.2(7) . . . . ? Cr1 P21 Cr2 P41 -26.5(5) . . . . ? P31 P21 Cr2 P51 89.6(7) . . . . ? P11 P21 Cr2 P51 -37.5(6) . . . . ? Cr1 P21 Cr2 P51 26.1(5) . . . . ? P31 P21 Cr2 P22 -13.7(8) . . . . ? P11 P21 Cr2 P22 -140.8(10) . . . . ? Cr1 P21 Cr2 P22 -77.2(8) . . . . ? P31 P21 Cr2 P11 127.2(8) . . . . ? Cr1 P21 Cr2 P11 63.6(6) . . . . ? P31 P21 Cr2 P42 66.7(6) . . . . ? P11 P21 Cr2 P42 -60.5(6) . . . . ? Cr1 P21 Cr2 P42 3.1(4) . . . . ? P31 P41 Cr2 C11 131.8(19) . . . . ? P51 P41 Cr2 C11 -99(2) . . . . ? Cr1 P41 Cr2 C11 -163.5(17) . . . . ? P31 P41 Cr2 C15 159.1(5) . . . . ? P51 P41 Cr2 C15 -71.4(7) . . . . ? Cr1 P41 Cr2 C15 -136.2(3) . . . . ? P31 P41 Cr2 C14 130.5(6) . . . . ? P51 P41 Cr2 C14 -100.1(7) . . . . ? Cr1 P41 Cr2 C14 -164.8(5) . . . . ? P31 P41 Cr2 C13 92.2(6) . . . . ? P51 P41 Cr2 C13 -138.3(7) . . . . ? Cr1 P41 Cr2 C13 157.0(4) . . . . ? P31 P41 Cr2 C12 69.1(8) . . . . ? P51 P41 Cr2 C12 -161.4(6) . . . . ? Cr1 P41 Cr2 C12 133.9(4) . . . . ? P51 P41 Cr2 P31 129.5(9) . . . . ? Cr1 P41 Cr2 P31 64.7(6) . . . . ? P31 P41 Cr2 P21 -38.4(6) . . . . ? P51 P41 Cr2 P21 91.0(7) . . . . ? Cr1 P41 Cr2 P21 26.3(4) . . . . ? P31 P41 Cr2 P51 -129.5(9) . . . . ? Cr1 P41 Cr2 P51 -64.7(6) . . . . ? P31 P41 Cr2 P22 -13.4(5) . . . . ? P51 P41 Cr2 P22 116.0(7) . . . . ? Cr1 P41 Cr2 P22 51.3(3) . . . . ? P31 P41 Cr2 P11 -91.7(7) . . . . ? P51 P41 Cr2 P11 37.7(7) . . . . ? Cr1 P41 Cr2 P11 -27.0(5) . . . . ? P31 P41 Cr2 P42 -140.8(14) . . . . ? P51 P41 Cr2 P42 -11.4(9) . . . . ? Cr1 P41 Cr2 P42 -76.1(10) . . . . ? P11 P51 Cr2 C11 -71.9(8) . . . . ? P41 P51 Cr2 C11 159.0(5) . . . . ? Cr1 P51 Cr2 C11 -136.1(3) . . . . ? P11 P51 Cr2 C15 -100.1(8) . . . . ? P41 P51 Cr2 C15 130.9(7) . . . . ? Cr1 P51 Cr2 C15 -164.3(5) . . . . ? P11 P51 Cr2 C14 -138.3(7) . . . . ? P41 P51 Cr2 C14 92.7(7) . . . . ? Cr1 P51 Cr2 C14 157.5(4) . . . . ? P11 P51 Cr2 C13 -161.1(6) . . . . ? P41 P51 Cr2 C13 69.9(8) . . . . ? Cr1 P51 Cr2 C13 134.8(3) . . . . ? P11 P51 Cr2 C12 -99.5(19) . . . . ? P41 P51 Cr2 C12 131.5(18) . . . . ? Cr1 P51 Cr2 C12 -163.6(16) . . . . ? P11 P51 Cr2 P31 92.0(7) . . . . ? P41 P51 Cr2 P31 -37.0(7) . . . . ? Cr1 P51 Cr2 P31 27.8(6) . . . . ? P11 P51 Cr2 P21 38.3(6) . . . . ? P41 P51 Cr2 P21 -90.7(7) . . . . ? Cr1 P51 Cr2 P21 -25.9(5) . . . . ? P11 P51 Cr2 P41 129.0(9) . . . . ? Cr1 P51 Cr2 P41 64.8(6) . . . . ? P11 P51 Cr2 P22 69.1(7) . . . . ? P41 P51 Cr2 P22 -59.9(7) . . . . ? Cr1 P51 Cr2 P22 4.9(5) . . . . ? P41 P51 Cr2 P11 -129.0(9) . . . . ? Cr1 P51 Cr2 P11 -64.2(7) . . . . ? P11 P51 Cr2 P42 143.3(13) . . . . ? P41 P51 Cr2 P42 14.3(11) . . . . ? Cr1 P51 Cr2 P42 79.1(10) . . . . ? P32 P22 Cr2 C11 -154.9(4) . . . . ? P12 P22 Cr2 C11 75.8(4) . . . . ? Cr1 P22 Cr2 C11 139.8(3) . . . . ? P32 P22 Cr2 C15 -149.7(9) . . . . ? P12 P22 Cr2 C15 81.0(9) . . . . ? Cr1 P22 Cr2 C15 145.0(8) . . . . ? P32 P22 Cr2 C14 -69.7(5) . . . . ? P12 P22 Cr2 C14 161.0(4) . . . . ? Cr1 P22 Cr2 C14 -134.9(2) . . . . ? P32 P22 Cr2 C13 -85.9(5) . . . . ? P12 P22 Cr2 C13 144.8(5) . . . . ? Cr1 P22 Cr2 C13 -151.1(4) . . . . ? P32 P22 Cr2 C12 -123.0(5) . . . . ? P12 P22 Cr2 C12 107.7(6) . . . . ? Cr1 P22 Cr2 C12 171.8(5) . . . . ? P32 P22 Cr2 P31 -12.3(11) . . . . ? P12 P22 Cr2 P31 -141.6(11) . . . . ? Cr1 P22 Cr2 P31 -77.5(10) . . . . ? P32 P22 Cr2 P21 139.9(10) . . . . ? P12 P22 Cr2 P21 10.5(8) . . . . ? Cr1 P22 Cr2 P21 74.6(8) . . . . ? P32 P22 Cr2 P41 14.1(5) . . . . ? P12 P22 Cr2 P41 -115.2(6) . . . . ? Cr1 P22 Cr2 P41 -51.1(5) . . . . ? P32 P22 Cr2 P51 60.3(6) . . . . ? P12 P22 Cr2 P51 -69.0(6) . . . . ? Cr1 P22 Cr2 P51 -4.9(5) . . . . ? P32 P22 Cr2 P11 108.8(5) . . . . ? P12 P22 Cr2 P11 -20.5(6) . . . . ? Cr1 P22 Cr2 P11 43.6(4) . . . . ? P32 P22 Cr2 P42 37.6(4) . . . . ? P12 P22 Cr2 P42 -91.7(4) . . . . ? Cr1 P22 Cr2 P42 -27.6(4) . . . . ? P51 P11 Cr2 C11 130.4(7) . . . . ? P21 P11 Cr2 C11 -100.3(6) . . . . ? Cr1 P11 Cr2 C11 -164.2(4) . . . . ? P51 P11 Cr2 C15 92.0(7) . . . . ? P21 P11 Cr2 C15 -138.6(5) . . . . ? Cr1 P11 Cr2 C15 157.5(4) . . . . ? P51 P11 Cr2 C14 68.9(8) . . . . ? P21 P11 Cr2 C14 -161.7(5) . . . . ? Cr1 P11 Cr2 C14 134.4(4) . . . . ? P51 P11 Cr2 C13 128.2(16) . . . . ? P21 P11 Cr2 C13 -102.4(18) . . . . ? Cr1 P11 Cr2 C13 -166.4(16) . . . . ? P51 P11 Cr2 C12 158.5(5) . . . . ? P21 P11 Cr2 C12 -72.1(6) . . . . ? Cr1 P11 Cr2 C12 -136.1(3) . . . . ? P51 P11 Cr2 P31 -89.4(7) . . . . ? P21 P11 Cr2 P31 39.9(6) . . . . ? Cr1 P11 Cr2 P31 -24.0(6) . . . . ? P51 P11 Cr2 P21 -129.4(8) . . . . ? Cr1 P11 Cr2 P21 -63.9(5) . . . . ? P51 P11 Cr2 P41 -38.1(7) . . . . ? P21 P11 Cr2 P41 91.2(6) . . . . ? Cr1 P11 Cr2 P41 27.3(5) . . . . ? P21 P11 Cr2 P51 129.4(8) . . . . ? Cr1 P11 Cr2 P51 65.4(6) . . . . ? P51 P11 Cr2 P22 -109.8(6) . . . . ? P21 P11 Cr2 P22 19.5(6) . . . . ? Cr1 P11 Cr2 P22 -44.4(3) . . . . ? P51 P11 Cr2 P42 -14.6(5) . . . . ? P21 P11 Cr2 P42 114.8(6) . . . . ? Cr1 P11 Cr2 P42 50.9(3) . . . . ? P32 P42 Cr2 C11 162.1(4) . . . . ? P52 P42 Cr2 C11 -68.4(6) . . . . ? Cr1 P42 Cr2 C11 -133.1(3) . . . . ? P32 P42 Cr2 C15 145.8(5) . . . . ? P52 P42 Cr2 C15 -84.7(5) . . . . ? Cr1 P42 Cr2 C15 -149.3(4) . . . . ? P32 P42 Cr2 C14 108.7(6) . . . . ? P52 P42 Cr2 C14 -121.8(5) . . . . ? Cr1 P42 Cr2 C14 173.6(5) . . . . ? P32 P42 Cr2 C13 76.3(5) . . . . ? P52 P42 Cr2 C13 -154.2(4) . . . . ? Cr1 P42 Cr2 C13 141.2(3) . . . . ? P32 P42 Cr2 C12 79.6(10) . . . . ? P52 P42 Cr2 C12 -150.9(10) . . . . ? Cr1 P42 Cr2 C12 144.5(9) . . . . ? P32 P42 Cr2 P31 -18.4(6) . . . . ? P52 P42 Cr2 P31 111.1(6) . . . . ? Cr1 P42 Cr2 P31 46.5(5) . . . . ? P32 P42 Cr2 P21 -68.0(5) . . . . ? P52 P42 Cr2 P21 61.6(5) . . . . ? Cr1 P42 Cr2 P21 -3.1(4) . . . . ? P32 P42 Cr2 P41 12.1(10) . . . . ? P52 P42 Cr2 P41 141.6(12) . . . . ? Cr1 P42 Cr2 P41 77.0(11) . . . . ? P32 P42 Cr2 P51 -144.9(12) . . . . ? P52 P42 Cr2 P51 -15.4(12) . . . . ? Cr1 P42 Cr2 P51 -80.0(11) . . . . ? P32 P42 Cr2 P22 -37.1(4) . . . . ? P52 P42 Cr2 P22 92.4(4) . . . . ? Cr1 P42 Cr2 P22 27.8(3) . . . . ? P32 P42 Cr2 P11 -115.2(6) . . . . ? P52 P42 Cr2 P11 14.3(5) . . . . ? Cr1 P42 Cr2 P11 -50.3(5) . . . . ? C14 Cr2 C11 C15 37.65(15) . . . . ? C13 Cr2 C11 C15 80.00(16) . . . . ? C12 Cr2 C11 C15 117.7(2) . . . . ? P31 Cr2 C11 C15 155.0(7) . . . . ? P21 Cr2 C11 C15 -153.9(6) . . . . ? P41 Cr2 C11 C15 36(2) . . . . ? P51 Cr2 C11 C15 -49.6(8) . . . . ? P22 Cr2 C11 C15 176.9(6) . . . . ? P11 Cr2 C11 C15 -99.3(6) . . . . ? P42 Cr2 C11 C15 -25.6(9) . . . . ? C15 Cr2 C11 C12 -117.7(2) . . . . ? C14 Cr2 C11 C12 -80.06(16) . . . . ? C13 Cr2 C11 C12 -37.71(16) . . . . ? P31 Cr2 C11 C12 37.3(7) . . . . ? P21 Cr2 C11 C12 88.4(6) . . . . ? P41 Cr2 C11 C12 -82(2) . . . . ? P51 Cr2 C11 C12 -167.3(7) . . . . ? P22 Cr2 C11 C12 59.1(6) . . . . ? P11 Cr2 C11 C12 143.0(6) . . . . ? P42 Cr2 C11 C12 -143.3(9) . . . . ? C15 Cr2 C11 C16 121.2(4) . . . . ? C14 Cr2 C11 C16 158.8(3) . . . . ? C13 Cr2 C11 C16 -158.8(4) . . . . ? C12 Cr2 C11 C16 -121.1(4) . . . . ? P31 Cr2 C11 C16 -83.8(8) . . . . ? P21 Cr2 C11 C16 -32.8(6) . . . . ? P41 Cr2 C11 C16 157(2) . . . . ? P51 Cr2 C11 C16 71.5(8) . . . . ? P22 Cr2 C11 C16 -62.0(7) . . . . ? P11 Cr2 C11 C16 21.9(7) . . . . ? P42 Cr2 C11 C16 95.5(9) . . . . ? C15 C11 C12 C13 -0.3(3) . . . . ? C16 C11 C12 C13 -177.2(3) . . . . ? Cr2 C11 C12 C13 61.94(18) . . . . ? C15 C11 C12 C17 175.8(3) . . . . ? C16 C11 C12 C17 -1.0(5) . . . . ? Cr2 C11 C12 C17 -121.9(3) . . . . ? C15 C11 C12 Cr2 -62.28(18) . . . . ? C16 C11 C12 Cr2 120.9(3) . . . . ? C15 Cr2 C12 C11 37.29(15) . . . . ? C14 Cr2 C12 C11 79.70(16) . . . . ? C13 Cr2 C12 C11 117.1(2) . . . . ? P31 Cr2 C12 C11 -155.3(6) . . . . ? P21 Cr2 C12 C11 -100.3(6) . . . . ? P41 Cr2 C12 C11 155.5(8) . . . . ? P51 Cr2 C12 C11 37(2) . . . . ? P22 Cr2 C12 C11 -132.0(7) . . . . ? P11 Cr2 C12 C11 -49.4(8) . . . . ? P42 Cr2 C12 C11 112.5(15) . . . . ? C11 Cr2 C12 C13 -117.1(2) . . . . ? C15 Cr2 C12 C13 -79.80(16) . . . . ? C14 Cr2 C12 C13 -37.39(15) . . . . ? P31 Cr2 C12 C13 87.6(6) . . . . ? P21 Cr2 C12 C13 142.6(6) . . . . ? P41 Cr2 C12 C13 38.4(8) . . . . ? P51 Cr2 C12 C13 -80(2) . . . . ? P22 Cr2 C12 C13 110.9(7) . . . . ? P11 Cr2 C12 C13 -166.5(8) . . . . ? P42 Cr2 C12 C13 -4.6(15) . . . . ? C11 Cr2 C12 C17 122.2(4) . . . . ? C15 Cr2 C12 C17 159.5(4) . . . . ? C14 Cr2 C12 C17 -158.1(4) . . . . ? C13 Cr2 C12 C17 -120.7(4) . . . . ? P31 Cr2 C12 C17 -33.1(7) . . . . ? P21 Cr2 C12 C17 21.9(7) . . . . ? P41 Cr2 C12 C17 -82.3(8) . . . . ? P51 Cr2 C12 C17 159(2) . . . . ? P22 Cr2 C12 C17 -9.8(7) . . . . ? P11 Cr2 C12 C17 72.8(8) . . . . ? P42 Cr2 C12 C17 -125.4(15) . . . . ? C11 C12 C13 C14 0.4(3) . . . . ? C17 C12 C13 C14 -175.9(3) . . . . ? Cr2 C12 C13 C14 62.15(17) . . . . ? C11 C12 C13 C18 176.3(3) . . . . ? C17 C12 C13 C18 0.1(5) . . . . ? Cr2 C12 C13 C18 -121.9(3) . . . . ? C11 C12 C13 Cr2 -61.76(17) . . . . ? C17 C12 C13 Cr2 122.0(3) . . . . ? C11 Cr2 C13 C14 -79.73(17) . . . . ? C15 Cr2 C13 C14 -37.32(15) . . . . ? C12 Cr2 C13 C14 -117.4(2) . . . . ? P31 Cr2 C13 C14 141.1(7) . . . . ? P21 Cr2 C13 C14 -167.1(7) . . . . ? P41 Cr2 C13 C14 88.5(7) . . . . ? P51 Cr2 C13 C14 38.0(8) . . . . ? P22 Cr2 C13 C14 164.5(6) . . . . ? P11 Cr2 C13 C14 -77(2) . . . . ? P42 Cr2 C13 C14 60.6(6) . . . . ? C11 Cr2 C13 C12 37.65(16) . . . . ? C15 Cr2 C13 C12 80.07(17) . . . . ? C14 Cr2 C13 C12 117.4(2) . . . . ? P31 Cr2 C13 C12 -101.5(7) . . . . ? P21 Cr2 C13 C12 -49.7(7) . . . . ? P41 Cr2 C13 C12 -154.1(7) . . . . ? P51 Cr2 C13 C12 155.4(7) . . . . ? P22 Cr2 C13 C12 -78.1(6) . . . . ? P11 Cr2 C13 C12 40(2) . . . . ? P42 Cr2 C13 C12 178.0(6) . . . . ? C11 Cr2 C13 C18 159.3(3) . . . . ? C15 Cr2 C13 C18 -158.3(3) . . . . ? C14 Cr2 C13 C18 -120.9(4) . . . . ? C12 Cr2 C13 C18 121.7(4) . . . . ? P31 Cr2 C13 C18 20.1(8) . . . . ? P21 Cr2 C13 C18 72.0(7) . . . . ? P41 Cr2 C13 C18 -32.4(7) . . . . ? P51 Cr2 C13 C18 -83.0(8) . . . . ? P22 Cr2 C13 C18 43.6(7) . . . . ? P11 Cr2 C13 C18 162(2) . . . . ? P42 Cr2 C13 C18 -60.3(7) . . . . ? C12 C13 C14 C15 -0.3(3) . . . . ? C18 C13 C14 C15 -176.3(3) . . . . ? Cr2 C13 C14 C15 61.91(17) . . . . ? C12 C13 C14 C19 176.6(3) . . . . ? C18 C13 C14 C19 0.6(4) . . . . ? Cr2 C13 C14 C19 -121.2(3) . . . . ? C12 C13 C14 Cr2 -62.21(18) . . . . ? C18 C13 C14 Cr2 121.8(3) . . . . ? C11 Cr2 C14 C13 80.11(17) . . . . ? C15 Cr2 C14 C13 117.8(2) . . . . ? C12 Cr2 C14 C13 37.59(16) . . . . ? P31 Cr2 C14 C13 -51.5(8) . . . . ? P21 Cr2 C14 C13 38(2) . . . . ? P41 Cr2 C14 C13 -100.3(7) . . . . ? P51 Cr2 C14 C13 -154.2(6) . . . . ? P22 Cr2 C14 C13 -25.7(8) . . . . ? P11 Cr2 C14 C13 156.4(6) . . . . ? P42 Cr2 C14 C13 -130.8(7) . . . . ? C11 Cr2 C14 C15 -37.64(16) . . . . ? C13 Cr2 C14 C15 -117.8(2) . . . . ? C12 Cr2 C14 C15 -80.16(17) . . . . ? P31 Cr2 C14 C15 -169.2(8) . . . . ? P21 Cr2 C14 C15 -80(2) . . . . ? P41 Cr2 C14 C15 141.9(7) . . . . ? P51 Cr2 C14 C15 88.0(6) . . . . ? P22 Cr2 C14 C15 -143.5(8) . . . . ? P11 Cr2 C14 C15 38.7(7) . . . . ? P42 Cr2 C14 C15 111.4(7) . . . . ? C11 Cr2 C14 C19 -160.0(3) . . . . ? C15 Cr2 C14 C19 -122.4(3) . . . . ? C13 Cr2 C14 C19 119.8(3) . . . . ? C12 Cr2 C14 C19 157.4(3) . . . . ? P31 Cr2 C14 C19 68.4(8) . . . . ? P21 Cr2 C14 C19 157(2) . . . . ? P41 Cr2 C14 C19 19.5(7) . . . . ? P51 Cr2 C14 C19 -34.4(7) . . . . ? P22 Cr2 C14 C19 94.1(9) . . . . ? P11 Cr2 C14 C19 -83.7(7) . . . . ? P42 Cr2 C14 C19 -11.0(7) . . . . ? C12 C11 C15 C14 0.2(3) . . . . ? C16 C11 C15 C14 177.0(3) . . . . ? Cr2 C11 C15 C14 -62.26(17) . . . . ? C12 C11 C15 C20 -177.0(3) . . . . ? C16 C11 C15 C20 -0.2(4) . . . . ? Cr2 C11 C15 C20 120.6(3) . . . . ? C12 C11 C15 Cr2 62.42(18) . . . . ? C16 C11 C15 Cr2 -120.8(3) . . . . ? C13 C14 C15 C11 0.1(3) . . . . ? C19 C14 C15 C11 -176.7(3) . . . . ? Cr2 C14 C15 C11 62.09(17) . . . . ? C13 C14 C15 C20 177.2(3) . . . . ? C19 C14 C15 C20 0.5(4) . . . . ? Cr2 C14 C15 C20 -120.7(3) . . . . ? C13 C14 C15 Cr2 -62.01(17) . . . . ? C19 C14 C15 Cr2 121.2(3) . . . . ? C14 Cr2 C15 C11 -117.1(2) . . . . ? C13 Cr2 C15 C11 -79.87(17) . . . . ? C12 Cr2 C15 C11 -37.35(16) . . . . ? P31 Cr2 C15 C11 -85(2) . . . . ? P21 Cr2 C15 C11 38.5(6) . . . . ? P41 Cr2 C15 C11 -167.6(8) . . . . ? P51 Cr2 C15 C11 142.4(7) . . . . ? P22 Cr2 C15 C11 -7.3(15) . . . . ? P11 Cr2 C15 C11 89.3(5) . . . . ? P42 Cr2 C15 C11 164.8(6) . . . . ? C11 Cr2 C15 C14 117.1(2) . . . . ? C13 Cr2 C15 C14 37.22(16) . . . . ? C12 Cr2 C15 C14 79.74(17) . . . . ? P31 Cr2 C15 C14 32(2) . . . . ? P21 Cr2 C15 C14 155.6(6) . . . . ? P41 Cr2 C15 C14 -50.5(8) . . . . ? P51 Cr2 C15 C14 -100.5(7) . . . . ? P22 Cr2 C15 C14 109.8(15) . . . . ? P11 Cr2 C15 C14 -153.6(5) . . . . ? P42 Cr2 C15 C14 -78.1(6) . . . . ? C11 Cr2 C15 C20 -121.4(3) . . . . ? C14 Cr2 C15 C20 121.5(3) . . . . ? C13 Cr2 C15 C20 158.7(3) . . . . ? C12 Cr2 C15 C20 -158.8(3) . . . . ? P31 Cr2 C15 C20 153(2) . . . . ? P21 Cr2 C15 C20 -83.0(7) . . . . ? P41 Cr2 C15 C20 70.9(8) . . . . ? P51 Cr2 C15 C20 21.0(7) . . . . ? P22 Cr2 C15 C20 -128.8(15) . . . . ? P11 Cr2 C15 C20 -32.1(6) . . . . ? P42 Cr2 C15 C20 43.4(7) . . . . ? _diffrn_measured_fraction_theta_max 0.970 _diffrn_reflns_theta_full 30.48 _diffrn_measured_fraction_theta_full 0.970 _refine_diff_density_max 0.924 _refine_diff_density_min -0.453 _refine_diff_density_rms 0.094 #===END data_270k _database_code_depnum_ccdc_archive 'CCDC 618748' _audit_creation_method SHELXL-97 _chemical_name_systematic ; \m~2~-\h^5^,\h^5^-cyclopentaphosphole)-bis ((\h^5^-pentamethyl-cyclopentadienyl)-chromium) hexafluoroantimonate ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H30 Cr2 F6 P5 Sb' _chemical_formula_weight 765.04 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting orthorhombic _symmetry_space_group_name_H-M Fddd loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+3/4, -y+3/4, z' '-x+3/4, y, -z+3/4' 'x, -y+3/4, -z+3/4' 'x, y+1/2, z+1/2' '-x+3/4, -y+5/4, z+1/2' '-x+3/4, y+1/2, -z+5/4' 'x, -y+5/4, -z+5/4' 'x+1/2, y, z+1/2' '-x+5/4, -y+3/4, z+1/2' '-x+5/4, y, -z+5/4' 'x+1/2, -y+3/4, -z+5/4' 'x+1/2, y+1/2, z' '-x+5/4, -y+5/4, z' '-x+5/4, y+1/2, -z+3/4' 'x+1/2, -y+5/4, -z+3/4' '-x, -y, -z' 'x-3/4, y-3/4, -z' 'x-3/4, -y, z-3/4' '-x, y-3/4, z-3/4' '-x, -y+1/2, -z+1/2' 'x-3/4, y-1/4, -z+1/2' 'x-3/4, -y+1/2, z-1/4' '-x, y-1/4, z-1/4' '-x+1/2, -y, -z+1/2' 'x-1/4, y-3/4, -z+1/2' 'x-1/4, -y, z-1/4' '-x+1/2, y-3/4, z-1/4' '-x+1/2, -y+1/2, -z' 'x-1/4, y-1/4, -z' 'x-1/4, -y+1/2, z-3/4' '-x+1/2, y-1/4, z-3/4' _cell_length_a 21.4775(5) _cell_length_b 29.6112(7) _cell_length_c 36.0527(9) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_volume 22928.6(10) _cell_formula_units_Z 32 _cell_measurement_temperature 270(2) _cell_measurement_reflns_used 8350 _cell_measurement_theta_min 2.20 _cell_measurement_theta_max 30.44 _exptl_crystal_description 'irregular block' _exptl_crystal_colour 'dark green' _exptl_crystal_size_max 0.60 _exptl_crystal_size_mid 0.52 _exptl_crystal_size_min 0.40 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.773 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 12096 _exptl_absorpt_coefficient_mu 2.008 _exptl_absorpt_correction_type integration _exptl_absorpt_correction_T_min 0.401 _exptl_absorpt_correction_T_max 0.619 _exptl_absorpt_process_details 'XPREP in SHELXTL' _exptl_special_details ; ? ; _diffrn_ambient_temperature 270(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'Bede Microsource X-ray Generator' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEX CCD Diffractometer' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number 0 _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% 0 _diffrn_reflns_number 43503 _diffrn_reflns_av_R_equivalents 0.0209 _diffrn_reflns_av_sigmaI/netI 0.0186 _diffrn_reflns_limit_h_min -30 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_k_min -41 _diffrn_reflns_limit_k_max 41 _diffrn_reflns_limit_l_min -46 _diffrn_reflns_limit_l_max 51 _diffrn_reflns_theta_min 1.30 _diffrn_reflns_theta_max 30.46 _reflns_number_total 8483 _reflns_number_gt 6364 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'SMART V5.625 (Bruker, 2003)' _computing_cell_refinement 'SMART V5.625 (Bruker, 2003)' _computing_data_reduction 'SAINT V6.28A (Bruker, 2003)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'SHELXTL V6.12(Bruker, 2001)' _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0574P)^2^+44.4574P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 8483 _refine_ls_number_parameters 404 _refine_ls_number_restraints 90 _refine_ls_R_factor_all 0.0527 _refine_ls_R_factor_gt 0.0344 _refine_ls_wR_factor_ref 0.1104 _refine_ls_wR_factor_gt 0.0924 _refine_ls_goodness_of_fit_ref 1.067 _refine_ls_restrained_S_all 1.064 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb1 Sb 0.6250 0.1250 0.010518(8) 0.05441(9) Uani 1 2 d S . . F1A F 0.6881(4) 0.1024(4) -0.0150(3) 0.176(3) Uani 0.50 1 d P A 1 F2A F 0.5532(4) 0.1397(4) 0.0337(3) 0.176(3) Uani 0.50 1 d P A 1 F1B F 0.6686(5) 0.1192(3) -0.0339(2) 0.159(3) Uani 0.50 1 d P A 2 F2B F 0.5894(5) 0.1424(3) 0.05444(19) 0.159(3) Uani 0.50 1 d P A 2 F3 F 0.59361(18) 0.06681(10) 0.01051(11) 0.1394(13) Uani 1 1 d . A . Sb2 Sb 0.1250 0.240479(12) 0.1250 0.06379(10) Uani 1 2 d S . . F4 F 0.18407(17) 0.28529(13) 0.12074(12) 0.1515(15) Uani 1 1 d . . . F5 F 0.11785(18) 0.23902(12) 0.07380(8) 0.1317(13) Uani 1 1 d . . . F6 F 0.18609(13) 0.19606(11) 0.12225(8) 0.1100(10) Uani 1 1 d . . . C1 C 0.13977(12) 0.37022(8) 0.01210(7) 0.0419(5) Uani 1 1 d . B . C2 C 0.19755(12) 0.34961(8) 0.00383(8) 0.0446(6) Uani 1 1 d . B . C3 C 0.22731(12) 0.37493(10) -0.02465(7) 0.0482(6) Uani 1 1 d . B . C4 C 0.18751(13) 0.41182(10) -0.03376(7) 0.0463(6) Uani 1 1 d . B . C5 C 0.13377(11) 0.40875(8) -0.01119(7) 0.0411(5) Uani 1 1 d . B . C6 C 0.09161(16) 0.35272(12) 0.03877(10) 0.0656(8) Uani 1 1 d . . . H6A H 0.0658 0.3309 0.0265 0.098 Uiso 1 1 calc R . . H6B H 0.0663 0.3773 0.0473 0.098 Uiso 1 1 calc R . . H6C H 0.1120 0.3388 0.0595 0.098 Uiso 1 1 calc R . . C7 C 0.22152(18) 0.30664(10) 0.02095(11) 0.0726(10) Uani 1 1 d . . . H7A H 0.1983 0.2814 0.0114 0.109 Uiso 1 1 calc R . . H7B H 0.2167 0.3081 0.0474 0.109 Uiso 1 1 calc R . . H7C H 0.2648 0.3030 0.0149 0.109 Uiso 1 1 calc R . . C8 C 0.28808(15) 0.36396(15) -0.04305(10) 0.0771(11) Uani 1 1 d . . . H8A H 0.2808 0.3444 -0.0638 0.116 Uiso 1 1 calc R . . H8B H 0.3150 0.3491 -0.0256 0.116 Uiso 1 1 calc R . . H8C H 0.3074 0.3913 -0.0515 0.116 Uiso 1 1 calc R . . C9 C 0.1975(2) 0.44607(15) -0.06364(9) 0.0791(11) Uani 1 1 d . . . H9A H 0.1753 0.4371 -0.0855 0.119 Uiso 1 1 calc R . . H9B H 0.2411 0.4482 -0.0692 0.119 Uiso 1 1 calc R . . H9C H 0.1825 0.4749 -0.0554 0.119 Uiso 1 1 calc R . . C10 C 0.07786(14) 0.43888(11) -0.01348(10) 0.0633(8) Uani 1 1 d . . . H10A H 0.0527 0.4301 -0.0343 0.095 Uiso 1 1 calc R . . H10B H 0.0911 0.4696 -0.0165 0.095 Uiso 1 1 calc R . . H10C H 0.0540 0.4362 0.0089 0.095 Uiso 1 1 calc R . . Cr1 Cr 0.215768(16) 0.418004(12) 0.024670(10) 0.03350(9) Uani 1 1 d . . . P11 P 0.1835(11) 0.4396(8) 0.0864(5) 0.069(5) Uani 0.25 1 d PU B 1 P21 P 0.2664(10) 0.3981(3) 0.0822(5) 0.064(5) Uani 0.25 1 d PU B 1 P31 P 0.3236(6) 0.4285(8) 0.0398(6) 0.067(6) Uani 0.25 1 d PU B 1 P41 P 0.2799(11) 0.4858(6) 0.0199(4) 0.072(5) Uani 0.25 1 d PU B 1 P51 P 0.1930(7) 0.4929(6) 0.0480(6) 0.071(6) Uani 0.25 1 d PU B 1 P1 P 0.1981(5) 0.4235(3) 0.0911(2) 0.062(3) Uani 0.50 1 d PU B 2 P2 P 0.2883(4) 0.3965(3) 0.0734(2) 0.061(2) Uani 0.50 1 d PU B 2 P3 P 0.3246(5) 0.4413(4) 0.0307(3) 0.064(3) Uani 0.50 1 d PU B 2 P4 P 0.2572(5) 0.4947(3) 0.0213(2) 0.063(2) Uani 0.50 1 d PU B 2 P5 P 0.1794(4) 0.4843(4) 0.0591(3) 0.066(3) Uani 0.50 1 d PU B 2 P12 P 0.2229(9) 0.4076(5) 0.0920(3) 0.070(4) Uani 0.25 1 d PU B 3 P22 P 0.3113(7) 0.4052(5) 0.0604(5) 0.072(4) Uani 0.25 1 d PU B 3 P32 P 0.3136(6) 0.4608(7) 0.0224(3) 0.076(4) Uani 0.25 1 d PU B 3 P42 P 0.2281(9) 0.4994(3) 0.0295(4) 0.074(4) Uani 0.25 1 d PU B 3 P52 P 0.1728(5) 0.4675(6) 0.0724(5) 0.072(4) Uani 0.25 1 d PU B 3 Cr2 Cr 0.283078(16) 0.477895(12) 0.086296(10) 0.03301(9) Uani 1 1 d . . . C11 C 0.29477(12) 0.49121(9) 0.14589(7) 0.0439(5) Uani 1 1 d . B . C12 C 0.35406(12) 0.48037(8) 0.13071(7) 0.0445(5) Uani 1 1 d . B . C13 C 0.36823(11) 0.51386(9) 0.10370(7) 0.0421(5) Uani 1 1 d . B . C14 C 0.31815(11) 0.54515(8) 0.10247(7) 0.0390(5) Uani 1 1 d . B . C15 C 0.27249(11) 0.53109(8) 0.12866(7) 0.0400(5) Uani 1 1 d . B . C16 C 0.26270(19) 0.46604(12) 0.17657(8) 0.0713(10) Uani 1 1 d . . . H16A H 0.2767 0.4773 0.2001 0.107 Uiso 1 1 calc R B . H16B H 0.2723 0.4345 0.1747 0.107 Uiso 1 1 calc R . . H16C H 0.2185 0.4702 0.1745 0.107 Uiso 1 1 calc R . . C17 C 0.39607(18) 0.44260(11) 0.14267(12) 0.0781(11) Uani 1 1 d . . . H17A H 0.4220 0.4527 0.1627 0.117 Uiso 1 1 calc R B . H17B H 0.4217 0.4335 0.1222 0.117 Uiso 1 1 calc R . . H17C H 0.3714 0.4174 0.1508 0.117 Uiso 1 1 calc R . . C18 C 0.42739(14) 0.51770(14) 0.08205(10) 0.0710(10) Uani 1 1 d . . . H18A H 0.4552 0.5381 0.0945 0.106 Uiso 1 1 calc R B . H18B H 0.4184 0.5290 0.0577 0.106 Uiso 1 1 calc R . . H18C H 0.4466 0.4885 0.0801 0.106 Uiso 1 1 calc R . . C19 C 0.31654(18) 0.58672(10) 0.07901(9) 0.0626(8) Uani 1 1 d . . . H19A H 0.3360 0.6112 0.0921 0.094 Uiso 1 1 calc R B . H19B H 0.2741 0.5944 0.0736 0.094 Uiso 1 1 calc R . . H19C H 0.3385 0.5813 0.0563 0.094 Uiso 1 1 calc R . . C20 C 0.21330(13) 0.55541(11) 0.13766(10) 0.0621(8) Uani 1 1 d . . . H20A H 0.2206 0.5762 0.1576 0.093 Uiso 1 1 calc R B . H20B H 0.1821 0.5339 0.1450 0.093 Uiso 1 1 calc R . . H20C H 0.1992 0.5716 0.1162 0.093 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.04437(14) 0.06746(18) 0.05140(16) 0.000 0.000 0.00354(11) F1A 0.115(4) 0.187(6) 0.226(8) -0.029(5) 0.100(5) 0.034(4) F2A 0.115(4) 0.187(6) 0.226(8) -0.029(5) 0.100(5) 0.034(4) F1B 0.263(9) 0.121(4) 0.092(3) -0.017(3) 0.095(5) -0.014(5) F2B 0.263(9) 0.121(4) 0.092(3) -0.017(3) 0.095(5) -0.014(5) F3 0.163(3) 0.0865(19) 0.169(3) 0.014(2) -0.046(3) -0.039(2) Sb2 0.05010(16) 0.0780(2) 0.06329(19) 0.000 0.00981(13) 0.000 F4 0.120(2) 0.131(3) 0.203(4) -0.040(3) 0.037(2) -0.064(2) F5 0.181(3) 0.151(3) 0.0635(16) 0.0271(17) -0.0043(18) -0.038(2) F6 0.0861(17) 0.131(2) 0.113(2) -0.0336(18) -0.0021(15) 0.0335(16) C1 0.0427(12) 0.0405(11) 0.0424(13) -0.0055(10) -0.0059(10) -0.0027(9) C2 0.0488(13) 0.0386(11) 0.0465(14) -0.0111(10) -0.0134(11) 0.0072(10) C3 0.0393(12) 0.0632(15) 0.0421(13) -0.0212(12) -0.0041(10) 0.0075(11) C4 0.0487(13) 0.0582(15) 0.0319(11) 0.0001(10) -0.0065(10) -0.0019(11) C5 0.0376(11) 0.0434(12) 0.0422(12) -0.0057(10) -0.0114(9) 0.0052(9) C6 0.0634(19) 0.069(2) 0.064(2) -0.0015(16) 0.0065(15) -0.0207(16) C7 0.093(2) 0.0398(14) 0.085(2) -0.0066(15) -0.032(2) 0.0180(15) C8 0.0489(16) 0.114(3) 0.068(2) -0.043(2) 0.0059(15) 0.0103(18) C9 0.092(3) 0.100(3) 0.0454(17) 0.0257(18) -0.0094(17) -0.012(2) C10 0.0512(15) 0.0661(18) 0.073(2) -0.0093(16) -0.0207(15) 0.0204(14) Cr1 0.03351(16) 0.03460(17) 0.03239(18) -0.00209(13) -0.00372(13) 0.00404(13) P11 0.055(9) 0.107(16) 0.045(9) -0.023(9) 0.014(6) -0.036(10) P21 0.105(12) 0.029(2) 0.059(8) 0.002(3) -0.045(8) 0.005(5) P31 0.029(3) 0.096(13) 0.075(12) -0.049(9) 0.006(5) -0.001(5) P41 0.106(13) 0.072(10) 0.040(2) 0.017(5) -0.016(7) -0.040(7) P51 0.061(9) 0.058(6) 0.093(13) -0.034(8) -0.037(8) 0.035(7) P1 0.071(8) 0.078(7) 0.037(2) -0.004(4) 0.007(4) -0.037(5) P2 0.073(5) 0.0413(13) 0.068(5) -0.008(2) -0.034(4) 0.019(3) P3 0.0431(16) 0.094(7) 0.054(5) -0.029(4) 0.018(2) -0.019(3) P4 0.091(7) 0.044(3) 0.054(2) 0.0155(19) -0.026(4) -0.014(4) P5 0.039(3) 0.079(6) 0.079(7) -0.040(4) -0.010(3) 0.020(3) P12 0.114(13) 0.056(6) 0.039(3) 0.005(4) -0.015(7) -0.037(6) P22 0.055(6) 0.070(7) 0.091(9) -0.042(5) -0.038(5) 0.034(4) P32 0.075(8) 0.107(10) 0.045(4) -0.014(6) 0.011(4) -0.042(6) P42 0.100(10) 0.0386(19) 0.084(9) 0.002(5) -0.055(7) 0.007(6) P52 0.0331(19) 0.102(11) 0.081(11) -0.052(7) 0.000(6) 0.002(7) Cr2 0.03291(16) 0.03355(16) 0.03258(18) -0.00256(13) -0.00061(13) -0.00045(13) C11 0.0548(14) 0.0451(12) 0.0318(11) -0.0013(9) -0.0025(10) -0.0150(11) C12 0.0471(12) 0.0411(11) 0.0453(14) -0.0063(10) -0.0148(11) 0.0002(10) C13 0.0344(10) 0.0507(13) 0.0412(12) -0.0115(10) 0.0019(9) -0.0075(9) C14 0.0430(11) 0.0368(11) 0.0370(11) -0.0034(9) 0.0009(9) -0.0080(9) C15 0.0381(11) 0.0429(12) 0.0391(12) -0.0106(9) 0.0038(9) -0.0046(9) C16 0.095(2) 0.079(2) 0.0402(15) 0.0076(14) 0.0002(16) -0.040(2) C17 0.087(2) 0.0555(17) 0.092(3) -0.0127(17) -0.049(2) 0.0194(17) C18 0.0404(13) 0.103(3) 0.070(2) -0.0263(19) 0.0149(14) -0.0155(15) C19 0.088(2) 0.0429(14) 0.0573(18) 0.0098(12) -0.0033(16) -0.0139(14) C20 0.0447(14) 0.0669(18) 0.075(2) -0.0312(16) 0.0094(14) 0.0017(13) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb1 F1A 1.771(6) . ? Sb1 F1A 1.771(6) 14_545 ? Sb1 F2A 1.807(6) 14_545 ? Sb1 F2A 1.808(6) . ? Sb1 F2B 1.833(6) 14_545 ? Sb1 F2B 1.833(6) . ? Sb1 F3 1.850(3) 14_545 ? Sb1 F3 1.850(3) . ? Sb1 F1B 1.862(6) . ? Sb1 F1B 1.862(6) 14_545 ? Sb2 F4 1.842(3) 11_454 ? Sb2 F4 1.842(3) . ? Sb2 F5 1.853(3) 11_454 ? Sb2 F5 1.853(3) . ? Sb2 F6 1.860(3) . ? Sb2 F6 1.860(3) 11_454 ? C1 C2 1.415(4) . ? C1 C5 1.423(4) . ? C1 C6 1.504(4) . ? C1 Cr1 2.207(2) . ? C2 C3 1.423(4) . ? C2 C7 1.505(4) . ? C2 Cr1 2.195(2) . ? C3 C4 1.425(4) . ? C3 C8 1.500(4) . ? C3 Cr1 2.202(2) . ? C4 C5 1.415(4) . ? C4 C9 1.495(4) . ? C4 Cr1 2.200(2) . ? C5 C10 1.498(3) . ? C5 Cr1 2.202(2) . ? C6 H6A 0.9600 . ? C6 H6B 0.9600 . ? C6 H6C 0.9600 . ? C7 H7A 0.9600 . ? C7 H7B 0.9600 . ? C7 H7C 0.9600 . ? C8 H8A 0.9600 . ? C8 H8B 0.9600 . ? C8 H8C 0.9600 . ? C9 H9A 0.9600 . ? C9 H9B 0.9600 . ? C9 H9C 0.9600 . ? C10 H10A 0.9600 . ? C10 H10B 0.9600 . ? C10 H10C 0.9600 . ? Cr1 P31 2.401(14) . ? Cr1 P21 2.413(13) . ? Cr1 P11 2.42(2) . ? Cr1 P51 2.422(14) . ? Cr1 P1 2.430(9) . ? Cr1 P42 2.433(9) . ? Cr1 P2 2.433(7) . ? P11 P51 2.11(2) . ? P11 P21 2.168(17) . ? P11 Cr2 2.42(2) . ? P21 P31 2.157(19) . ? P21 Cr2 2.393(11) . ? P31 P41 2.07(2) . ? P31 Cr2 2.388(16) . ? P41 P51 2.135(18) . ? P41 Cr2 2.408(14) . ? P51 Cr2 2.419(14) . ? P1 P5 2.175(10) . ? P1 P2 2.192(9) . ? P1 Cr2 2.440(8) . ? P2 P3 2.176(10) . ? P2 Cr2 2.456(7) . ? P3 P4 2.170(12) . ? P3 Cr2 2.448(10) . ? P4 P5 2.179(9) . ? P4 Cr2 2.459(8) . ? P5 Cr2 2.440(8) . ? P12 P52 2.193(12) . ? P12 P22 2.216(13) . ? P12 Cr2 2.460(10) . ? P22 P32 2.142(13) . ? P22 Cr2 2.422(8) . ? P32 P42 2.179(13) . ? P32 Cr2 2.448(10) . ? P42 P52 2.166(14) . ? P42 Cr2 2.447(9) . ? P52 Cr2 2.440(10) . ? Cr2 C11 2.199(2) . ? Cr2 C15 2.206(2) . ? Cr2 C13 2.207(2) . ? Cr2 C14 2.208(2) . ? Cr2 C12 2.212(2) . ? C11 C15 1.418(4) . ? C11 C12 1.423(4) . ? C11 C16 1.501(4) . ? C12 C13 1.423(4) . ? C12 C17 1.500(4) . ? C13 C14 1.420(4) . ? C13 C18 1.495(4) . ? C14 C15 1.424(3) . ? C14 C19 1.494(4) . ? C15 C20 1.497(4) . ? C16 H16A 0.9600 . ? C16 H16B 0.9600 . ? C16 H16C 0.9600 . ? C17 H17A 0.9600 . ? C17 H17B 0.9600 . ? C17 H17C 0.9600 . ? C18 H18A 0.9600 . ? C18 H18B 0.9600 . ? C18 H18C 0.9600 . ? C19 H19A 0.9600 . ? C19 H19B 0.9600 . ? C19 H19C 0.9600 . ? C20 H20A 0.9600 . ? C20 H20B 0.9600 . ? C20 H20C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F1A Sb1 F1A 117.3(8) . 14_545 ? F1A Sb1 F2A 59.8(5) . 14_545 ? F1A Sb1 F2A 170.2(5) 14_545 14_545 ? F1A Sb1 F2A 170.2(5) . . ? F1A Sb1 F2A 59.8(5) 14_545 . ? F2A Sb1 F2A 124.8(8) 14_545 . ? F1A Sb1 F2B 91.3(5) . 14_545 ? F1A Sb1 F2B 151.1(6) 14_545 14_545 ? F2A Sb1 F2B 34.5(4) 14_545 14_545 ? F2A Sb1 F2B 91.4(6) . 14_545 ? F1A Sb1 F2B 151.1(6) . . ? F1A Sb1 F2B 91.3(5) 14_545 . ? F2A Sb1 F2B 91.4(6) 14_545 . ? F2A Sb1 F2B 34.5(4) . . ? F2B Sb1 F2B 60.5(7) 14_545 . ? F1A Sb1 F3 94.2(4) . 14_545 ? F1A Sb1 F3 85.8(4) 14_545 14_545 ? F2A Sb1 F3 85.1(4) 14_545 14_545 ? F2A Sb1 F3 94.9(4) . 14_545 ? F2B Sb1 F3 96.3(3) 14_545 14_545 ? F2B Sb1 F3 83.7(3) . 14_545 ? F1A Sb1 F3 85.8(4) . . ? F1A Sb1 F3 94.2(4) 14_545 . ? F2A Sb1 F3 94.9(4) 14_545 . ? F2A Sb1 F3 85.1(4) . . ? F2B Sb1 F3 83.7(3) 14_545 . ? F2B Sb1 F3 96.3(3) . . ? F3 Sb1 F3 180.0(2) 14_545 . ? F1A Sb1 F1B 29.9(4) . . ? F1A Sb1 F1B 88.5(5) 14_545 . ? F2A Sb1 F1B 86.9(5) 14_545 . ? F2A Sb1 F1B 148.2(6) . . ? F2B Sb1 F1B 120.4(5) 14_545 . ? F2B Sb1 F1B 168.1(4) . . ? F3 Sb1 F1B 84.4(3) 14_545 . ? F3 Sb1 F1B 95.6(3) . . ? F1A Sb1 F1B 88.5(5) . 14_545 ? F1A Sb1 F1B 29.9(4) 14_545 14_545 ? F2A Sb1 F1B 148.1(6) 14_545 14_545 ? F2A Sb1 F1B 86.9(5) . 14_545 ? F2B Sb1 F1B 168.1(4) 14_545 14_545 ? F2B Sb1 F1B 120.4(5) . 14_545 ? F3 Sb1 F1B 95.6(3) 14_545 14_545 ? F3 Sb1 F1B 84.4(3) . 14_545 ? F1B Sb1 F1B 61.6(7) . 14_545 ? F4 Sb2 F4 87.8(3) 11_454 . ? F4 Sb2 F5 89.48(17) 11_454 11_454 ? F4 Sb2 F5 92.45(19) . 11_454 ? F4 Sb2 F5 92.44(19) 11_454 . ? F4 Sb2 F5 89.48(17) . . ? F5 Sb2 F5 177.3(2) 11_454 . ? F4 Sb2 F6 177.90(18) 11_454 . ? F4 Sb2 F6 91.10(17) . . ? F5 Sb2 F6 88.75(14) 11_454 . ? F5 Sb2 F6 89.37(16) . . ? F4 Sb2 F6 91.10(17) 11_454 11_454 ? F4 Sb2 F6 177.89(18) . 11_454 ? F5 Sb2 F6 89.37(16) 11_454 11_454 ? F5 Sb2 F6 88.74(14) . 11_454 ? F6 Sb2 F6 90.0(2) . 11_454 ? C2 C1 C5 107.5(2) . . ? C2 C1 C6 126.1(3) . . ? C5 C1 C6 126.2(3) . . ? C2 C1 Cr1 70.80(14) . . ? C5 C1 Cr1 70.97(13) . . ? C6 C1 Cr1 126.74(19) . . ? C1 C2 C3 108.6(2) . . ? C1 C2 C7 125.3(3) . . ? C3 C2 C7 126.0(3) . . ? C1 C2 Cr1 71.72(14) . . ? C3 C2 Cr1 71.39(14) . . ? C7 C2 Cr1 125.35(19) . . ? C2 C3 C4 107.5(2) . . ? C2 C3 C8 126.6(3) . . ? C4 C3 C8 125.9(3) . . ? C2 C3 Cr1 70.85(14) . . ? C4 C3 Cr1 71.01(14) . . ? C8 C3 Cr1 125.5(2) . . ? C5 C4 C3 107.9(2) . . ? C5 C4 C9 125.1(3) . . ? C3 C4 C9 126.9(3) . . ? C5 C4 Cr1 71.32(14) . . ? C3 C4 Cr1 71.20(14) . . ? C9 C4 Cr1 126.4(2) . . ? C4 C5 C1 108.5(2) . . ? C4 C5 C10 125.7(3) . . ? C1 C5 C10 125.6(3) . . ? C4 C5 Cr1 71.18(14) . . ? C1 C5 Cr1 71.38(13) . . ? C10 C5 Cr1 126.81(19) . . ? C1 C6 H6A 109.5 . . ? C1 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C1 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C2 Cr1 C4 63.02(10) . . ? C2 Cr1 C5 62.72(9) . . ? C4 Cr1 C5 37.50(10) . . ? C2 Cr1 C3 37.76(11) . . ? C4 Cr1 C3 37.79(10) . . ? C5 Cr1 C3 62.86(9) . . ? C2 Cr1 C1 37.49(9) . . ? C4 Cr1 C1 63.00(10) . . ? C5 Cr1 C1 37.64(9) . . ? C3 Cr1 C1 63.01(10) . . ? C2 Cr1 P31 111.7(5) . . ? C4 Cr1 P31 119.7(5) . . ? C5 Cr1 P31 157.2(5) . . ? C3 Cr1 P31 98.7(4) . . ? C1 Cr1 P31 147.5(6) . . ? C2 Cr1 P21 98.6(3) . . ? C4 Cr1 P21 157.9(4) . . ? C5 Cr1 P21 146.5(5) . . ? C3 Cr1 P21 120.1(4) . . ? C1 Cr1 P21 110.7(4) . . ? P31 Cr1 P21 53.2(5) . . ? C2 Cr1 P11 120.6(5) . . ? C4 Cr1 P11 145.5(6) . . ? C5 Cr1 P11 110.1(6) . . ? C3 Cr1 P11 158.3(5) . . ? C1 Cr1 P11 98.4(5) . . ? P31 Cr1 P11 91.9(6) . . ? P21 Cr1 P11 53.3(4) . . ? C2 Cr1 P51 158.1(4) . . ? C4 Cr1 P51 110.6(5) . . ? C5 Cr1 P51 99.0(3) . . ? C3 Cr1 P51 146.4(5) . . ? C1 Cr1 P51 120.6(4) . . ? P31 Cr1 P51 89.8(6) . . ? P21 Cr1 P51 90.9(5) . . ? P11 Cr1 P51 51.7(5) . . ? C2 Cr1 P1 111.8(2) . . ? C4 Cr1 P1 155.0(2) . . ? C5 Cr1 P1 117.5(2) . . ? C3 Cr1 P1 148.4(2) . . ? C1 Cr1 P1 97.5(2) . . ? P31 Cr1 P1 85.3(4) . . ? P21 Cr1 P1 40.6(4) . . ? P11 Cr1 P1 14.1(5) . . ? P51 Cr1 P1 64.2(5) . . ? C2 Cr1 P42 163.5(3) . . ? C4 Cr1 P42 100.5(3) . . ? C5 Cr1 P42 104.7(3) . . ? C3 Cr1 P42 128.3(4) . . ? C1 Cr1 P42 137.0(4) . . ? P31 Cr1 P42 75.5(5) . . ? P21 Cr1 P42 97.5(3) . . ? P11 Cr1 P42 72.7(5) . . ? P51 Cr1 P42 24.3(5) . . ? P1 Cr1 P42 83.1(3) . . ? C2 Cr1 P2 96.91(19) . . ? C4 Cr1 P2 147.8(2) . . ? C5 Cr1 P2 154.7(2) . . ? C3 Cr1 P2 111.1(2) . . ? C1 Cr1 P2 117.0(2) . . ? P31 Cr1 P2 41.5(5) . . ? P21 Cr1 P2 13.5(5) . . ? P11 Cr1 P2 65.7(5) . . ? P51 Cr1 P2 96.8(4) . . ? P1 Cr1 P2 53.6(2) . . ? P42 Cr1 P2 97.9(3) . . ? P51 P11 P21 107.3(8) . . ? P51 P11 Cr1 64.3(6) . . ? P21 P11 Cr1 63.2(6) . . ? P51 P11 Cr2 64.1(6) . . ? P21 P11 Cr2 62.6(6) . . ? Cr1 P11 Cr2 82.5(6) . . ? P31 P21 P11 106.4(7) . . ? P31 P21 Cr2 63.1(6) . . ? P11 P21 Cr2 63.9(6) . . ? P31 P21 Cr1 63.1(6) . . ? P11 P21 Cr1 63.4(6) . . ? Cr2 P21 Cr1 83.1(4) . . ? P41 P31 P21 109.3(8) . . ? P41 P31 Cr2 65.0(7) . . ? P21 P31 Cr2 63.3(4) . . ? P41 P31 Cr1 65.7(7) . . ? P21 P31 Cr1 63.7(5) . . ? Cr2 P31 Cr1 83.5(4) . . ? P31 P41 P51 108.2(8) . . ? P31 P41 Cr2 63.9(5) . . ? P51 P41 Cr2 64.0(6) . . ? P31 P41 Cr1 63.7(6) . . ? P51 P41 Cr1 63.5(6) . . ? Cr2 P41 Cr1 82.2(5) . . ? P11 P51 P41 108.8(8) . . ? P11 P51 Cr2 64.2(7) . . ? P41 P51 Cr2 63.5(5) . . ? P11 P51 Cr1 64.0(7) . . ? P41 P51 Cr1 64.4(5) . . ? Cr2 P51 Cr1 82.4(3) . . ? P5 P1 P2 108.1(5) . . ? P5 P1 Cr1 64.1(3) . . ? P2 P1 Cr1 63.3(3) . . ? P5 P1 Cr2 63.5(3) . . ? P2 P1 Cr2 63.8(3) . . ? Cr1 P1 Cr2 81.8(3) . . ? P3 P2 P1 107.5(5) . . ? P3 P2 Cr1 63.9(4) . . ? P1 P2 Cr1 63.1(2) . . ? P3 P2 Cr2 63.5(4) . . ? P1 P2 Cr2 63.0(2) . . ? Cr1 P2 Cr2 81.4(2) . . ? P4 P3 P2 108.4(5) . . ? P4 P3 Cr1 63.5(4) . . ? P2 P3 Cr1 63.2(3) . . ? P4 P3 Cr2 64.0(4) . . ? P2 P3 Cr2 63.9(3) . . ? Cr1 P3 Cr2 81.3(3) . . ? P3 P4 P5 108.2(5) . . ? P3 P4 Cr1 63.8(3) . . ? P5 P4 Cr1 63.8(3) . . ? P3 P4 Cr2 63.5(3) . . ? P5 P4 Cr2 63.1(3) . . ? Cr1 P4 Cr2 81.2(2) . . ? P1 P5 P4 107.8(5) . . ? P1 P5 Cr2 63.5(4) . . ? P4 P5 Cr2 64.0(2) . . ? P1 P5 Cr1 63.0(4) . . ? P4 P5 Cr1 63.3(3) . . ? Cr2 P5 Cr1 81.4(2) . . ? P52 P12 P22 106.2(6) . . ? P52 P12 Cr1 63.1(4) . . ? P22 P12 Cr1 63.1(4) . . ? P52 P12 Cr2 62.9(3) . . ? P22 P12 Cr2 62.1(4) . . ? Cr1 P12 Cr2 81.0(3) . . ? P32 P22 P12 109.0(5) . . ? P32 P22 Cr2 64.5(4) . . ? P12 P22 Cr2 63.9(3) . . ? P32 P22 Cr1 64.2(4) . . ? P12 P22 Cr1 63.1(3) . . ? Cr2 P22 Cr1 81.7(2) . . ? P22 P32 P42 107.9(6) . . ? P22 P32 Cr2 63.3(3) . . ? P42 P32 Cr2 63.6(4) . . ? P22 P32 Cr1 64.0(3) . . ? P42 P32 Cr1 63.0(4) . . ? Cr2 P32 Cr1 81.1(3) . . ? P52 P42 P32 108.5(5) . . ? P52 P42 Cr1 63.8(4) . . ? P32 P42 Cr1 64.1(3) . . ? P52 P42 Cr2 63.5(4) . . ? P32 P42 Cr2 63.6(3) . . ? Cr1 P42 Cr2 81.6(2) . . ? P42 P52 P12 108.3(6) . . ? P42 P52 Cr2 63.9(4) . . ? P12 P52 Cr2 63.9(4) . . ? P42 P52 Cr1 63.4(4) . . ? P12 P52 Cr1 63.6(4) . . ? Cr2 P52 Cr1 81.6(3) . . ? C11 Cr2 C15 37.55(10) . . ? C11 Cr2 C13 62.69(9) . . ? C15 Cr2 C13 62.88(9) . . ? C11 Cr2 C14 62.68(9) . . ? C15 Cr2 C14 37.63(9) . . ? C13 Cr2 C14 37.53(9) . . ? C11 Cr2 C12 37.63(10) . . ? C15 Cr2 C12 63.02(9) . . ? C13 Cr2 C12 37.56(10) . . ? C14 Cr2 C12 62.85(9) . . ? C11 Cr2 P31 138.9(6) . . ? C15 Cr2 P31 163.8(4) . . ? C13 Cr2 P31 101.1(4) . . ? C14 Cr2 P31 127.8(5) . . ? C12 Cr2 P31 106.1(5) . . ? C11 Cr2 P21 104.8(4) . . ? C15 Cr2 P21 137.1(5) . . ? C13 Cr2 P21 128.2(4) . . ? C14 Cr2 P21 163.3(3) . . ? C12 Cr2 P21 100.4(3) . . ? P31 Cr2 P21 53.6(5) . . ? C11 Cr2 P41 163.3(4) . . ? C15 Cr2 P41 128.0(5) . . ? C13 Cr2 P41 105.0(5) . . ? C14 Cr2 P41 100.6(4) . . ? C12 Cr2 P41 137.4(5) . . ? P31 Cr2 P41 51.1(6) . . ? P21 Cr2 P41 91.7(5) . . ? C11 Cr2 P51 128.1(4) . . ? C15 Cr2 P51 100.5(3) . . ? C13 Cr2 P51 137.4(5) . . ? C14 Cr2 P51 104.9(4) . . ? C12 Cr2 P51 163.5(3) . . ? P31 Cr2 P51 90.2(5) . . ? P21 Cr2 P51 91.5(5) . . ? P41 Cr2 P51 52.5(5) . . ? C11 Cr2 P11 100.6(5) . . ? C15 Cr2 P11 104.0(6) . . ? C13 Cr2 P11 163.3(5) . . ? C14 Cr2 P11 136.3(6) . . ? C12 Cr2 P11 128.6(5) . . ? P31 Cr2 P11 92.1(6) . . ? P21 Cr2 P11 53.5(4) . . ? P41 Cr2 P11 91.3(6) . . ? P51 Cr2 P11 51.7(5) . . ? C11 Cr2 P22 120.5(4) . . ? C15 Cr2 P22 158.0(4) . . ? C13 Cr2 P22 109.3(3) . . ? C14 Cr2 P22 144.8(4) . . ? C12 Cr2 P22 97.8(2) . . ? P31 Cr2 P22 25.1(5) . . ? P21 Cr2 P22 30.3(4) . . ? P41 Cr2 P22 73.2(4) . . ? P51 Cr2 P22 98.2(4) . . ? P11 Cr2 P22 78.8(5) . . ? C11 Cr2 P52 109.5(4) . . ? C15 Cr2 P52 97.6(2) . . ? C13 Cr2 P52 157.4(3) . . ? C14 Cr2 P52 119.9(4) . . ? C12 Cr2 P52 145.3(5) . . ? P31 Cr2 P52 97.6(4) . . ? P21 Cr2 P52 73.6(4) . . ? P41 Cr2 P52 77.3(5) . . ? P51 Cr2 P52 29.5(6) . . ? P11 Cr2 P52 23.6(4) . . ? P22 Cr2 P52 93.0(3) . . ? C15 C11 C12 108.8(2) . . ? C15 C11 C16 125.6(3) . . ? C12 C11 C16 125.6(3) . . ? C15 C11 Cr2 71.49(14) . . ? C12 C11 Cr2 71.70(14) . . ? C16 C11 Cr2 125.35(18) . . ? C11 C12 C13 107.3(2) . . ? C11 C12 C17 126.6(3) . . ? C13 C12 C17 126.0(3) . . ? C11 C12 Cr2 70.67(14) . . ? C13 C12 Cr2 71.03(14) . . ? C17 C12 Cr2 126.71(19) . . ? C14 C13 C12 108.3(2) . . ? C14 C13 C18 125.3(3) . . ? C12 C13 C18 126.3(3) . . ? C14 C13 Cr2 71.24(13) . . ? C12 C13 Cr2 71.40(14) . . ? C18 C13 Cr2 126.32(19) . . ? C13 C14 C15 108.1(2) . . ? C13 C14 C19 124.9(2) . . ? C15 C14 C19 126.9(3) . . ? C13 C14 Cr2 71.23(13) . . ? C15 C14 Cr2 71.12(13) . . ? C19 C14 Cr2 125.86(19) . . ? C11 C15 C14 107.6(2) . . ? C11 C15 C20 126.3(3) . . ? C14 C15 C20 126.0(3) . . ? C11 C15 Cr2 70.96(14) . . ? C14 C15 Cr2 71.25(13) . . ? C20 C15 Cr2 125.54(18) . . ? C11 C16 H16A 109.5 . . ? C11 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C11 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 C1 C2 C3 -0.4(3) . . . . ? C6 C1 C2 C3 175.8(3) . . . . ? Cr1 C1 C2 C3 -62.24(17) . . . . ? C5 C1 C2 C7 -177.3(3) . . . . ? C6 C1 C2 C7 -1.2(4) . . . . ? Cr1 C1 C2 C7 120.8(3) . . . . ? C5 C1 C2 Cr1 61.84(17) . . . . ? C6 C1 C2 Cr1 -122.0(3) . . . . ? C1 C2 C3 C4 0.5(3) . . . . ? C7 C2 C3 C4 177.4(3) . . . . ? Cr1 C2 C3 C4 -61.93(18) . . . . ? C1 C2 C3 C8 -177.1(3) . . . . ? C7 C2 C3 C8 -0.2(4) . . . . ? Cr1 C2 C3 C8 120.5(3) . . . . ? C1 C2 C3 Cr1 62.45(17) . . . . ? C7 C2 C3 Cr1 -120.7(3) . . . . ? C2 C3 C4 C5 -0.4(3) . . . . ? C8 C3 C4 C5 177.2(3) . . . . ? Cr1 C3 C4 C5 -62.26(17) . . . . ? C2 C3 C4 C9 -176.2(3) . . . . ? C8 C3 C4 C9 1.4(5) . . . . ? Cr1 C3 C4 C9 121.9(3) . . . . ? C2 C3 C4 Cr1 61.82(17) . . . . ? C8 C3 C4 Cr1 -120.6(3) . . . . ? C3 C4 C5 C1 0.2(3) . . . . ? C9 C4 C5 C1 176.1(3) . . . . ? Cr1 C4 C5 C1 -61.99(17) . . . . ? C3 C4 C5 C10 -175.5(2) . . . . ? C9 C4 C5 C10 0.4(4) . . . . ? Cr1 C4 C5 C10 122.3(3) . . . . ? C3 C4 C5 Cr1 62.18(17) . . . . ? C9 C4 C5 Cr1 -121.9(3) . . . . ? C2 C1 C5 C4 0.1(3) . . . . ? C6 C1 C5 C4 -176.0(3) . . . . ? Cr1 C1 C5 C4 61.85(17) . . . . ? C2 C1 C5 C10 175.8(2) . . . . ? C6 C1 C5 C10 -0.3(4) . . . . ? Cr1 C1 C5 C10 -122.4(3) . . . . ? C2 C1 C5 Cr1 -61.73(17) . . . . ? C6 C1 C5 Cr1 122.1(3) . . . . ? C1 C2 Cr1 C4 -80.03(17) . . . . ? C3 C2 Cr1 C4 37.72(15) . . . . ? C7 C2 Cr1 C4 159.2(3) . . . . ? C1 C2 Cr1 C5 -37.68(15) . . . . ? C3 C2 Cr1 C5 80.07(16) . . . . ? C7 C2 Cr1 C5 -158.5(3) . . . . ? C1 C2 Cr1 C3 -117.7(2) . . . . ? C7 C2 Cr1 C3 121.4(3) . . . . ? C3 C2 Cr1 C1 117.7(2) . . . . ? C7 C2 Cr1 C1 -120.8(4) . . . . ? C1 C2 Cr1 P31 166.7(6) . . . . ? C3 C2 Cr1 P31 -75.6(6) . . . . ? C7 C2 Cr1 P31 45.9(6) . . . . ? C1 C2 Cr1 P21 113.0(6) . . . . ? C3 C2 Cr1 P21 -129.3(6) . . . . ? C7 C2 Cr1 P21 -7.8(7) . . . . ? C1 C2 Cr1 P11 60.7(7) . . . . ? C3 C2 Cr1 P11 178.4(7) . . . . ? C7 C2 Cr1 P11 -60.1(7) . . . . ? C1 C2 Cr1 P51 -1.9(15) . . . . ? C3 C2 Cr1 P51 115.9(14) . . . . ? C7 C2 Cr1 P51 -122.7(15) . . . . ? C1 C2 Cr1 P1 73.0(3) . . . . ? C3 C2 Cr1 P1 -169.2(3) . . . . ? C7 C2 Cr1 P1 -47.8(4) . . . . ? C1 C2 Cr1 P42 -80.1(19) . . . . ? C3 C2 Cr1 P42 37.6(19) . . . . ? C7 C2 Cr1 P42 159.1(19) . . . . ? C1 C2 Cr1 P2 126.5(3) . . . . ? C3 C2 Cr1 P2 -115.8(3) . . . . ? C7 C2 Cr1 P2 5.7(4) . . . . ? C5 C4 Cr1 C2 79.54(16) . . . . ? C3 C4 Cr1 C2 -37.70(16) . . . . ? C9 C4 Cr1 C2 -160.1(3) . . . . ? C3 C4 Cr1 C5 -117.2(2) . . . . ? C9 C4 Cr1 C5 120.3(4) . . . . ? C5 C4 Cr1 C3 117.2(2) . . . . ? C9 C4 Cr1 C3 -122.4(4) . . . . ? C5 C4 Cr1 C1 37.27(14) . . . . ? C3 C4 Cr1 C1 -79.97(18) . . . . ? C9 C4 Cr1 C1 157.6(3) . . . . ? C5 C4 Cr1 P31 -179.6(7) . . . . ? C3 C4 Cr1 P31 63.1(7) . . . . ? C9 C4 Cr1 P31 -59.3(7) . . . . ? C5 C4 Cr1 P21 115.7(14) . . . . ? C3 C4 Cr1 P21 -1.5(14) . . . . ? C9 C4 Cr1 P21 -124.0(14) . . . . ? C5 C4 Cr1 P11 -25.9(9) . . . . ? C3 C4 Cr1 P11 -143.1(9) . . . . ? C9 C4 Cr1 P11 94.4(9) . . . . ? C5 C4 Cr1 P51 -77.5(6) . . . . ? C3 C4 Cr1 P51 165.3(6) . . . . ? C9 C4 Cr1 P51 42.8(6) . . . . ? C5 C4 Cr1 P1 -4.4(6) . . . . ? C3 C4 Cr1 P1 -121.6(6) . . . . ? C9 C4 Cr1 P1 115.9(6) . . . . ? C5 C4 Cr1 P42 -100.5(6) . . . . ? C3 C4 Cr1 P42 142.3(6) . . . . ? C9 C4 Cr1 P42 19.8(6) . . . . ? C5 C4 Cr1 P2 135.8(5) . . . . ? C3 C4 Cr1 P2 18.6(5) . . . . ? C9 C4 Cr1 P2 -103.9(5) . . . . ? C4 C5 Cr1 C2 -80.42(17) . . . . ? C1 C5 Cr1 C2 37.52(15) . . . . ? C10 C5 Cr1 C2 158.6(3) . . . . ? C1 C5 Cr1 C4 117.9(2) . . . . ? C10 C5 Cr1 C4 -121.0(3) . . . . ? C4 C5 Cr1 C3 -37.75(16) . . . . ? C1 C5 Cr1 C3 80.19(17) . . . . ? C10 C5 Cr1 C3 -158.7(3) . . . . ? C4 C5 Cr1 C1 -117.9(2) . . . . ? C10 C5 Cr1 C1 121.1(3) . . . . ? C4 C5 Cr1 P31 0.8(15) . . . . ? C1 C5 Cr1 P31 118.7(15) . . . . ? C10 C5 Cr1 P31 -120.2(15) . . . . ? C4 C5 Cr1 P21 -142.0(7) . . . . ? C1 C5 Cr1 P21 -24.1(7) . . . . ? C10 C5 Cr1 P21 97.0(8) . . . . ? C4 C5 Cr1 P11 164.7(6) . . . . ? C1 C5 Cr1 P11 -77.3(6) . . . . ? C10 C5 Cr1 P11 43.7(6) . . . . ? C4 C5 Cr1 P51 112.3(6) . . . . ? C1 C5 Cr1 P51 -129.7(6) . . . . ? C10 C5 Cr1 P51 -8.7(7) . . . . ? C4 C5 Cr1 P1 177.9(3) . . . . ? C1 C5 Cr1 P1 -64.2(3) . . . . ? C10 C5 Cr1 P1 56.9(4) . . . . ? C4 C5 Cr1 P42 88.1(6) . . . . ? C1 C5 Cr1 P42 -153.9(6) . . . . ? C10 C5 Cr1 P42 -32.9(6) . . . . ? C4 C5 Cr1 P2 -119.8(5) . . . . ? C1 C5 Cr1 P2 -1.8(6) . . . . ? C10 C5 Cr1 P2 119.2(6) . . . . ? C4 C3 Cr1 C2 117.1(2) . . . . ? C8 C3 Cr1 C2 -121.8(4) . . . . ? C2 C3 Cr1 C4 -117.1(2) . . . . ? C8 C3 Cr1 C4 121.0(4) . . . . ? C2 C3 Cr1 C5 -79.67(16) . . . . ? C4 C3 Cr1 C5 37.47(16) . . . . ? C8 C3 Cr1 C5 158.5(3) . . . . ? C2 C3 Cr1 C1 -37.19(14) . . . . ? C4 C3 Cr1 C1 79.95(17) . . . . ? C8 C3 Cr1 C1 -159.0(3) . . . . ? C2 C3 Cr1 P31 114.5(6) . . . . ? C4 C3 Cr1 P31 -128.4(6) . . . . ? C8 C3 Cr1 P31 -7.3(7) . . . . ? C2 C3 Cr1 P21 62.2(6) . . . . ? C4 C3 Cr1 P21 179.3(6) . . . . ? C8 C3 Cr1 P21 -59.6(7) . . . . ? C2 C3 Cr1 P11 -3.7(16) . . . . ? C4 C3 Cr1 P11 113.5(16) . . . . ? C8 C3 Cr1 P11 -125.5(16) . . . . ? C2 C3 Cr1 P51 -142.6(8) . . . . ? C4 C3 Cr1 P51 -25.5(8) . . . . ? C8 C3 Cr1 P51 95.6(8) . . . . ? C2 C3 Cr1 P1 19.4(5) . . . . ? C4 C3 Cr1 P1 136.5(5) . . . . ? C8 C3 Cr1 P1 -102.4(5) . . . . ? C2 C3 Cr1 P42 -167.2(5) . . . . ? C4 C3 Cr1 P42 -50.1(6) . . . . ? C8 C3 Cr1 P42 71.0(6) . . . . ? C2 C3 Cr1 P2 73.3(3) . . . . ? C4 C3 Cr1 P2 -169.5(3) . . . . ? C8 C3 Cr1 P2 -48.5(4) . . . . ? C5 C1 Cr1 C2 -117.2(2) . . . . ? C6 C1 Cr1 C2 121.3(3) . . . . ? C2 C1 Cr1 C4 80.07(17) . . . . ? C5 C1 Cr1 C4 -37.13(15) . . . . ? C6 C1 Cr1 C4 -158.7(3) . . . . ? C2 C1 Cr1 C5 117.2(2) . . . . ? C6 C1 Cr1 C5 -121.5(3) . . . . ? C2 C1 Cr1 C3 37.45(16) . . . . ? C5 C1 Cr1 C3 -79.75(16) . . . . ? C6 C1 Cr1 C3 158.7(3) . . . . ? C2 C1 Cr1 P31 -23.5(9) . . . . ? C5 C1 Cr1 P31 -140.7(9) . . . . ? C6 C1 Cr1 P31 97.8(9) . . . . ? C2 C1 Cr1 P21 -76.7(5) . . . . ? C5 C1 Cr1 P21 166.1(5) . . . . ? C6 C1 Cr1 P21 44.6(6) . . . . ? C2 C1 Cr1 P11 -130.6(6) . . . . ? C5 C1 Cr1 P11 112.2(6) . . . . ? C6 C1 Cr1 P11 -9.4(7) . . . . ? C2 C1 Cr1 P51 179.2(6) . . . . ? C5 C1 Cr1 P51 62.0(6) . . . . ? C6 C1 Cr1 P51 -59.6(7) . . . . ? C2 C1 Cr1 P1 -116.4(3) . . . . ? C5 C1 Cr1 P1 126.4(3) . . . . ? C6 C1 Cr1 P1 4.9(4) . . . . ? C2 C1 Cr1 P42 155.8(7) . . . . ? C5 C1 Cr1 P42 38.6(7) . . . . ? C6 C1 Cr1 P42 -83.0(7) . . . . ? C2 C1 Cr1 P2 -63.7(3) . . . . ? C5 C1 Cr1 P2 179.1(3) . . . . ? C6 C1 Cr1 P2 57.6(4) . . . . ? C2 Cr1 P11 P51 -155.0(5) . . . . ? C4 Cr1 P11 P51 -69.1(9) . . . . ? C5 Cr1 P11 P51 -85.5(6) . . . . ? C3 Cr1 P11 P51 -152.4(11) . . . . ? C1 Cr1 P11 P51 -122.6(6) . . . . ? P31 Cr1 P11 P51 88.3(7) . . . . ? P21 Cr1 P11 P51 127.9(8) . . . . ? P1 Cr1 P11 P51 150(3) . . . . ? P42 Cr1 P11 P51 14.1(5) . . . . ? P2 Cr1 P11 P51 121.5(7) . . . . ? C2 Cr1 P11 P21 77.1(6) . . . . ? C4 Cr1 P11 P21 163.1(5) . . . . ? C5 Cr1 P11 P21 146.6(5) . . . . ? C3 Cr1 P11 P21 79.7(14) . . . . ? C1 Cr1 P11 P21 109.6(6) . . . . ? P31 Cr1 P11 P21 -39.6(6) . . . . ? P51 Cr1 P11 P21 -127.9(8) . . . . ? P1 Cr1 P11 P21 23(2) . . . . ? P42 Cr1 P11 P21 -113.7(6) . . . . ? P2 Cr1 P11 P21 -6.4(6) . . . . ? C2 Cr1 P11 Cr2 140.1(3) . . . . ? C4 Cr1 P11 Cr2 -133.9(5) . . . . ? C5 Cr1 P11 Cr2 -150.4(4) . . . . ? C3 Cr1 P11 Cr2 142.7(11) . . . . ? C1 Cr1 P11 Cr2 172.6(4) . . . . ? P31 Cr1 P11 Cr2 23.5(6) . . . . ? P21 Cr1 P11 Cr2 63.0(5) . . . . ? P51 Cr1 P11 Cr2 -64.8(5) . . . . ? P1 Cr1 P11 Cr2 86(3) . . . . ? P42 Cr1 P11 Cr2 -50.7(3) . . . . ? P2 Cr1 P11 Cr2 56.7(4) . . . . ? P51 P11 P21 P31 -0.6(12) . . . . ? Cr1 P11 P21 P31 47.6(7) . . . . ? Cr2 P11 P21 P31 -47.9(7) . . . . ? P51 P11 P21 Cr2 47.4(8) . . . . ? Cr1 P11 P21 Cr2 95.6(5) . . . . ? P51 P11 P21 Cr1 -48.2(8) . . . . ? Cr2 P11 P21 Cr1 -95.6(5) . . . . ? C2 Cr1 P21 P31 110.7(6) . . . . ? C4 Cr1 P21 P31 78.6(12) . . . . ? C5 Cr1 P21 P31 163.0(6) . . . . ? C3 Cr1 P21 P31 77.5(6) . . . . ? C1 Cr1 P21 P31 147.5(6) . . . . ? P11 Cr1 P21 P31 -127.4(8) . . . . ? P51 Cr1 P21 P31 -89.1(7) . . . . ? P1 Cr1 P21 P31 -135.6(8) . . . . ? P42 Cr1 P21 P31 -65.5(7) . . . . ? P2 Cr1 P21 P31 27.0(18) . . . . ? C2 Cr1 P21 P11 -121.9(6) . . . . ? C4 Cr1 P21 P11 -154.0(11) . . . . ? C5 Cr1 P21 P11 -69.7(7) . . . . ? C3 Cr1 P21 P11 -155.1(6) . . . . ? C1 Cr1 P21 P11 -85.1(6) . . . . ? P31 Cr1 P21 P11 127.4(8) . . . . ? P51 Cr1 P21 P11 38.3(6) . . . . ? P1 Cr1 P21 P11 -8.3(8) . . . . ? P42 Cr1 P21 P11 61.8(6) . . . . ? P2 Cr1 P21 P11 154(2) . . . . ? C2 Cr1 P21 Cr2 173.9(4) . . . . ? C4 Cr1 P21 Cr2 141.8(8) . . . . ? C5 Cr1 P21 Cr2 -133.8(3) . . . . ? C3 Cr1 P21 Cr2 140.7(3) . . . . ? C1 Cr1 P21 Cr2 -149.3(3) . . . . ? P31 Cr1 P21 Cr2 63.2(6) . . . . ? P11 Cr1 P21 Cr2 -64.2(6) . . . . ? P51 Cr1 P21 Cr2 -25.9(5) . . . . ? P1 Cr1 P21 Cr2 -72.4(4) . . . . ? P42 Cr1 P21 Cr2 -2.3(4) . . . . ? P2 Cr1 P21 Cr2 90.2(19) . . . . ? P11 P21 P31 P41 1.0(12) . . . . ? Cr2 P21 P31 P41 -47.4(8) . . . . ? Cr1 P21 P31 P41 48.8(7) . . . . ? P11 P21 P31 Cr2 48.4(7) . . . . ? Cr1 P21 P31 Cr2 96.2(4) . . . . ? P11 P21 P31 Cr1 -47.8(7) . . . . ? Cr2 P21 P31 Cr1 -96.2(4) . . . . ? C2 Cr1 P31 P41 146.8(6) . . . . ? C4 Cr1 P31 P41 76.3(7) . . . . ? C5 Cr1 P31 P41 75.8(14) . . . . ? C3 Cr1 P31 P41 109.9(7) . . . . ? C1 Cr1 P31 P41 161.9(6) . . . . ? P21 Cr1 P31 P41 -128.8(8) . . . . ? P11 Cr1 P31 P41 -89.2(7) . . . . ? P51 Cr1 P31 P41 -37.5(7) . . . . ? P1 Cr1 P31 P41 -101.6(6) . . . . ? P42 Cr1 P31 P41 -17.6(6) . . . . ? P2 Cr1 P31 P41 -138.0(9) . . . . ? C2 Cr1 P31 P21 -84.4(5) . . . . ? C4 Cr1 P31 P21 -154.9(4) . . . . ? C5 Cr1 P31 P21 -155.4(10) . . . . ? C3 Cr1 P31 P21 -121.3(5) . . . . ? C1 Cr1 P31 P21 -69.3(8) . . . . ? P11 Cr1 P31 P21 39.6(5) . . . . ? P51 Cr1 P31 P21 91.3(6) . . . . ? P1 Cr1 P31 P21 27.2(5) . . . . ? P42 Cr1 P31 P21 111.2(5) . . . . ? P2 Cr1 P31 P21 -9.2(5) . . . . ? C2 Cr1 P31 Cr2 -147.8(4) . . . . ? C4 Cr1 P31 Cr2 141.8(3) . . . . ? C5 Cr1 P31 Cr2 141.2(9) . . . . ? C3 Cr1 P31 Cr2 175.3(5) . . . . ? C1 Cr1 P31 Cr2 -132.7(5) . . . . ? P21 Cr1 P31 Cr2 -63.4(4) . . . . ? P11 Cr1 P31 Cr2 -23.7(6) . . . . ? P51 Cr1 P31 Cr2 27.9(6) . . . . ? P1 Cr1 P31 Cr2 -36.2(4) . . . . ? P42 Cr1 P31 Cr2 47.8(5) . . . . ? P2 Cr1 P31 Cr2 -72.6(5) . . . . ? P21 P31 P41 P51 -1.1(12) . . . . ? Cr2 P31 P41 P51 -47.6(7) . . . . ? Cr1 P31 P41 P51 46.6(7) . . . . ? P21 P31 P41 Cr2 46.5(7) . . . . ? Cr1 P31 P41 Cr2 94.2(4) . . . . ? P21 P31 P41 Cr1 -47.7(7) . . . . ? Cr2 P31 P41 Cr1 -94.2(4) . . . . ? C2 Cr1 P41 P31 -67.8(8) . . . . ? C4 Cr1 P41 P31 -121.3(6) . . . . ? C5 Cr1 P41 P31 -154.0(5) . . . . ? C3 Cr1 P41 P31 -84.0(6) . . . . ? C1 Cr1 P41 P31 -153.0(10) . . . . ? P21 Cr1 P41 P31 38.6(6) . . . . ? P11 Cr1 P41 P31 92.0(7) . . . . ? P51 Cr1 P41 P31 129.5(8) . . . . ? P1 Cr1 P41 P31 78.9(6) . . . . ? P42 Cr1 P41 P31 143.3(12) . . . . ? P2 Cr1 P41 P31 26.5(6) . . . . ? C2 Cr1 P41 P51 162.7(5) . . . . ? C4 Cr1 P41 P51 109.2(6) . . . . ? C5 Cr1 P41 P51 76.5(6) . . . . ? C3 Cr1 P41 P51 146.5(6) . . . . ? C1 Cr1 P41 P51 77.5(13) . . . . ? P31 Cr1 P41 P51 -129.5(8) . . . . ? P21 Cr1 P41 P51 -90.9(6) . . . . ? P11 Cr1 P41 P51 -37.5(6) . . . . ? P1 Cr1 P41 P51 -50.6(6) . . . . ? P42 Cr1 P41 P51 13.8(8) . . . . ? P2 Cr1 P41 P51 -103.0(6) . . . . ? C2 Cr1 P41 Cr2 -132.5(4) . . . . ? C4 Cr1 P41 Cr2 174.0(4) . . . . ? C5 Cr1 P41 Cr2 141.2(3) . . . . ? C3 Cr1 P41 Cr2 -148.7(4) . . . . ? C1 Cr1 P41 Cr2 142.3(10) . . . . ? P31 Cr1 P41 Cr2 -64.7(5) . . . . ? P21 Cr1 P41 Cr2 -26.1(4) . . . . ? P11 Cr1 P41 Cr2 27.3(5) . . . . ? P51 Cr1 P41 Cr2 64.8(6) . . . . ? P1 Cr1 P41 Cr2 14.2(4) . . . . ? P42 Cr1 P41 Cr2 78.6(9) . . . . ? P2 Cr1 P41 Cr2 -38.2(3) . . . . ? P21 P11 P51 P41 -0.1(12) . . . . ? Cr1 P11 P51 P41 -47.7(8) . . . . ? Cr2 P11 P51 P41 46.5(8) . . . . ? P21 P11 P51 Cr2 -46.6(7) . . . . ? Cr1 P11 P51 Cr2 -94.2(5) . . . . ? P21 P11 P51 Cr1 47.6(7) . . . . ? Cr2 P11 P51 Cr1 94.2(5) . . . . ? P31 P41 P51 P11 0.7(13) . . . . ? Cr2 P41 P51 P11 -46.8(8) . . . . ? Cr1 P41 P51 P11 47.5(8) . . . . ? P31 P41 P51 Cr2 47.6(8) . . . . ? Cr1 P41 P51 Cr2 94.3(4) . . . . ? P31 P41 P51 Cr1 -46.7(8) . . . . ? Cr2 P41 P51 Cr1 -94.3(4) . . . . ? C2 Cr1 P51 P11 76.9(13) . . . . ? C4 Cr1 P51 P11 145.6(7) . . . . ? C5 Cr1 P51 P11 108.6(7) . . . . ? C3 Cr1 P51 P11 162.0(7) . . . . ? C1 Cr1 P51 P11 75.5(7) . . . . ? P31 Cr1 P51 P11 -92.5(7) . . . . ? P21 Cr1 P51 P11 -39.3(6) . . . . ? P1 Cr1 P51 P11 -7.7(8) . . . . ? P42 Cr1 P51 P11 -145.6(12) . . . . ? P2 Cr1 P51 P11 -51.5(7) . . . . ? C2 Cr1 P51 P41 -154.0(10) . . . . ? C4 Cr1 P51 P41 -85.3(5) . . . . ? C5 Cr1 P51 P41 -122.3(5) . . . . ? C3 Cr1 P51 P41 -68.9(8) . . . . ? C1 Cr1 P51 P41 -155.4(4) . . . . ? P31 Cr1 P51 P41 36.6(6) . . . . ? P21 Cr1 P51 P41 89.8(6) . . . . ? P11 Cr1 P51 P41 129.1(8) . . . . ? P1 Cr1 P51 P41 121.4(6) . . . . ? P42 Cr1 P51 P41 -16.5(9) . . . . ? P2 Cr1 P51 P41 77.6(6) . . . . ? C2 Cr1 P51 Cr2 141.8(9) . . . . ? C4 Cr1 P51 Cr2 -149.5(4) . . . . ? C5 Cr1 P51 Cr2 173.5(4) . . . . ? C3 Cr1 P51 Cr2 -133.1(4) . . . . ? C1 Cr1 P51 Cr2 140.5(3) . . . . ? P31 Cr1 P51 Cr2 -27.6(6) . . . . ? P21 Cr1 P51 Cr2 25.6(5) . . . . ? P11 Cr1 P51 Cr2 64.9(7) . . . . ? P1 Cr1 P51 Cr2 57.2(4) . . . . ? P42 Cr1 P51 Cr2 -80.7(9) . . . . ? P2 Cr1 P51 Cr2 13.4(5) . . . . ? C2 Cr1 P1 P5 -148.5(3) . . . . ? C4 Cr1 P1 P5 -75.9(5) . . . . ? C5 Cr1 P1 P5 -78.9(3) . . . . ? C3 Cr1 P1 P5 -161.2(3) . . . . ? C1 Cr1 P1 P5 -112.6(3) . . . . ? P31 Cr1 P1 P5 100.0(6) . . . . ? P21 Cr1 P1 P5 134.2(7) . . . . ? P11 Cr1 P1 P5 -18(3) . . . . ? P51 Cr1 P1 P5 7.9(5) . . . . ? P42 Cr1 P1 P5 24.1(4) . . . . ? P2 Cr1 P1 P5 129.2(4) . . . . ? C2 Cr1 P1 P2 82.3(3) . . . . ? C4 Cr1 P1 P2 154.9(4) . . . . ? C5 Cr1 P1 P2 151.9(3) . . . . ? C3 Cr1 P1 P2 69.6(5) . . . . ? C1 Cr1 P1 P2 118.2(3) . . . . ? P31 Cr1 P1 P2 -29.2(6) . . . . ? P21 Cr1 P1 P2 5.0(7) . . . . ? P11 Cr1 P1 P2 -147(3) . . . . ? P51 Cr1 P1 P2 -121.3(5) . . . . ? P42 Cr1 P1 P2 -105.1(4) . . . . ? C2 Cr1 P1 Cr2 147.00(16) . . . . ? C4 Cr1 P1 Cr2 -140.4(4) . . . . ? C5 Cr1 P1 Cr2 -143.39(15) . . . . ? C3 Cr1 P1 Cr2 134.4(3) . . . . ? C1 Cr1 P1 Cr2 -177.1(2) . . . . ? P31 Cr1 P1 Cr2 35.5(5) . . . . ? P21 Cr1 P1 Cr2 69.7(6) . . . . ? P11 Cr1 P1 Cr2 -82(3) . . . . ? P51 Cr1 P1 Cr2 -56.6(4) . . . . ? P42 Cr1 P1 Cr2 -40.4(3) . . . . ? P2 Cr1 P1 Cr2 64.7(3) . . . . ? P5 P1 P2 P3 0.2(7) . . . . ? Cr1 P1 P2 P3 47.3(4) . . . . ? Cr2 P1 P2 P3 -46.7(4) . . . . ? P5 P1 P2 Cr1 -47.2(4) . . . . ? Cr2 P1 P2 Cr1 -94.0(2) . . . . ? P5 P1 P2 Cr2 46.9(4) . . . . ? Cr1 P1 P2 Cr2 94.0(2) . . . . ? C2 Cr1 P2 P3 119.3(4) . . . . ? C4 Cr1 P2 P3 71.0(5) . . . . ? C5 Cr1 P2 P3 153.9(4) . . . . ? C3 Cr1 P2 P3 83.1(4) . . . . ? C1 Cr1 P2 P3 152.6(4) . . . . ? P31 Cr1 P2 P3 4.1(9) . . . . ? P21 Cr1 P2 P3 -142.6(19) . . . . ? P11 Cr1 P2 P3 -120.2(7) . . . . ? P51 Cr1 P2 P3 -77.8(6) . . . . ? P1 Cr1 P2 P3 -128.6(5) . . . . ? P42 Cr1 P2 P3 -53.3(5) . . . . ? C2 Cr1 P2 P1 -112.1(3) . . . . ? C4 Cr1 P2 P1 -160.3(3) . . . . ? C5 Cr1 P2 P1 -77.5(4) . . . . ? C3 Cr1 P2 P1 -148.3(3) . . . . ? C1 Cr1 P2 P1 -78.7(3) . . . . ? P31 Cr1 P2 P1 132.8(7) . . . . ? P21 Cr1 P2 P1 -14.0(17) . . . . ? P11 Cr1 P2 P1 8.4(6) . . . . ? P51 Cr1 P2 P1 50.8(5) . . . . ? P42 Cr1 P2 P1 75.3(4) . . . . ? C2 Cr1 P2 Cr2 -176.1(2) . . . . ? C4 Cr1 P2 Cr2 135.6(3) . . . . ? C5 Cr1 P2 Cr2 -141.5(3) . . . . ? C3 Cr1 P2 Cr2 147.68(16) . . . . ? C1 Cr1 P2 Cr2 -142.77(15) . . . . ? P31 Cr1 P2 Cr2 68.7(7) . . . . ? P21 Cr1 P2 Cr2 -78.0(18) . . . . ? P11 Cr1 P2 Cr2 -55.6(5) . . . . ? P51 Cr1 P2 Cr2 -13.2(5) . . . . ? P1 Cr1 P2 Cr2 -64.0(2) . . . . ? P42 Cr1 P2 Cr2 11.3(4) . . . . ? P1 P2 P3 P4 -0.9(7) . . . . ? Cr1 P2 P3 P4 46.1(4) . . . . ? Cr2 P2 P3 P4 -47.4(4) . . . . ? P1 P2 P3 Cr1 -46.9(4) . . . . ? Cr2 P2 P3 Cr1 -93.4(2) . . . . ? P1 P2 P3 Cr2 46.5(4) . . . . ? Cr1 P2 P3 Cr2 93.4(2) . . . . ? C2 Cr1 P3 P4 152.6(3) . . . . ? C4 Cr1 P3 P4 82.6(4) . . . . ? C5 Cr1 P3 P4 70.8(6) . . . . ? C3 Cr1 P3 P4 118.8(3) . . . . ? C1 Cr1 P3 P4 155.3(5) . . . . ? P31 Cr1 P3 P4 -144(3) . . . . ? P21 Cr1 P3 P4 -121.2(5) . . . . ? P11 Cr1 P3 P4 -77.8(5) . . . . ? P51 Cr1 P3 P4 -27.4(5) . . . . ? P1 Cr1 P3 P4 -91.2(3) . . . . ? P42 Cr1 P3 P4 -9.8(4) . . . . ? P2 Cr1 P3 P4 -130.2(5) . . . . ? C2 Cr1 P3 P2 -77.2(3) . . . . ? C4 Cr1 P3 P2 -147.1(3) . . . . ? C5 Cr1 P3 P2 -159.0(3) . . . . ? C3 Cr1 P3 P2 -110.9(3) . . . . ? C1 Cr1 P3 P2 -74.5(6) . . . . ? P31 Cr1 P3 P2 -14(3) . . . . ? P21 Cr1 P3 P2 9.1(4) . . . . ? P11 Cr1 P3 P2 52.5(5) . . . . ? P51 Cr1 P3 P2 102.8(5) . . . . ? P1 Cr1 P3 P2 39.0(3) . . . . ? P42 Cr1 P3 P2 120.4(4) . . . . ? C2 Cr1 P3 Cr2 -142.2(2) . . . . ? C4 Cr1 P3 Cr2 147.83(19) . . . . ? C5 Cr1 P3 Cr2 136.0(3) . . . . ? C3 Cr1 P3 Cr2 -176.0(3) . . . . ? C1 Cr1 P3 Cr2 -139.5(4) . . . . ? P31 Cr1 P3 Cr2 -79(3) . . . . ? P21 Cr1 P3 Cr2 -56.0(3) . . . . ? P11 Cr1 P3 Cr2 -12.6(5) . . . . ? P51 Cr1 P3 Cr2 37.8(5) . . . . ? P1 Cr1 P3 Cr2 -26.0(3) . . . . ? P42 Cr1 P3 Cr2 55.4(4) . . . . ? P2 Cr1 P3 Cr2 -65.0(3) . . . . ? P2 P3 P4 P5 1.3(7) . . . . ? Cr1 P3 P4 P5 47.2(4) . . . . ? Cr2 P3 P4 P5 -46.0(4) . . . . ? P2 P3 P4 Cr1 -45.9(4) . . . . ? Cr2 P3 P4 Cr1 -93.2(2) . . . . ? P2 P3 P4 Cr2 47.3(4) . . . . ? Cr1 P3 P4 Cr2 93.2(2) . . . . ? C2 Cr1 P4 P3 -74.8(5) . . . . ? C4 Cr1 P4 P3 -111.8(3) . . . . ? C5 Cr1 P4 P3 -147.6(3) . . . . ? C3 Cr1 P4 P3 -77.7(3) . . . . ? C1 Cr1 P4 P3 -159.9(3) . . . . ? P31 Cr1 P4 P3 7.9(6) . . . . ? P21 Cr1 P4 P3 50.7(5) . . . . ? P11 Cr1 P4 P3 102.9(6) . . . . ? P51 Cr1 P4 P3 135.0(7) . . . . ? P1 Cr1 P4 P3 91.2(3) . . . . ? P42 Cr1 P4 P3 146.7(11) . . . . ? P2 Cr1 P4 P3 37.6(3) . . . . ? C2 Cr1 P4 P5 156.2(4) . . . . ? C4 Cr1 P4 P5 119.2(3) . . . . ? C5 Cr1 P4 P5 83.3(4) . . . . ? C3 Cr1 P4 P5 153.2(3) . . . . ? C1 Cr1 P4 P5 71.0(5) . . . . ? P31 Cr1 P4 P5 -121.2(6) . . . . ? P21 Cr1 P4 P5 -78.4(5) . . . . ? P11 Cr1 P4 P5 -26.2(5) . . . . ? P51 Cr1 P4 P5 6.0(8) . . . . ? P1 Cr1 P4 P5 -37.8(4) . . . . ? P42 Cr1 P4 P5 17.7(9) . . . . ? P2 Cr1 P4 P5 -91.5(3) . . . . ? C2 Cr1 P4 Cr2 -139.5(3) . . . . ? C4 Cr1 P4 Cr2 -176.5(2) . . . . ? C5 Cr1 P4 Cr2 147.65(15) . . . . ? C3 Cr1 P4 Cr2 -142.47(15) . . . . ? C1 Cr1 P4 Cr2 135.3(3) . . . . ? P31 Cr1 P4 Cr2 -56.9(4) . . . . ? P21 Cr1 P4 Cr2 -14.0(4) . . . . ? P11 Cr1 P4 Cr2 38.1(5) . . . . ? P51 Cr1 P4 Cr2 70.3(6) . . . . ? P1 Cr1 P4 Cr2 26.5(2) . . . . ? P42 Cr1 P4 Cr2 82.0(10) . . . . ? P2 Cr1 P4 Cr2 -27.14(19) . . . . ? P2 P1 P5 P4 0.6(7) . . . . ? Cr1 P1 P5 P4 -46.1(4) . . . . ? Cr2 P1 P5 P4 47.6(4) . . . . ? P2 P1 P5 Cr2 -47.0(4) . . . . ? Cr1 P1 P5 Cr2 -93.75(19) . . . . ? P2 P1 P5 Cr1 46.7(4) . . . . ? Cr2 P1 P5 Cr1 93.75(19) . . . . ? P3 P4 P5 P1 -1.2(7) . . . . ? Cr1 P4 P5 P1 46.0(4) . . . . ? Cr2 P4 P5 P1 -47.4(4) . . . . ? P3 P4 P5 Cr2 46.2(4) . . . . ? Cr1 P4 P5 Cr2 93.3(2) . . . . ? P3 P4 P5 Cr1 -47.2(4) . . . . ? Cr2 P4 P5 Cr1 -93.3(2) . . . . ? C2 Cr1 P5 P1 69.5(6) . . . . ? C4 Cr1 P5 P1 152.4(3) . . . . ? C5 Cr1 P5 P1 118.4(3) . . . . ? C3 Cr1 P5 P1 156.1(5) . . . . ? C1 Cr1 P5 P1 82.2(4) . . . . ? P31 Cr1 P5 P1 -80.2(6) . . . . ? P21 Cr1 P5 P1 -28.0(5) . . . . ? P11 Cr1 P5 P1 6.6(10) . . . . ? P51 Cr1 P5 P1 -147(2) . . . . ? P42 Cr1 P5 P1 -138.1(6) . . . . ? P2 Cr1 P5 P1 -38.6(3) . . . . ? C2 Cr1 P5 P4 -160.7(3) . . . . ? C4 Cr1 P5 P4 -77.8(3) . . . . ? C5 Cr1 P5 P4 -111.7(3) . . . . ? C3 Cr1 P5 P4 -74.1(5) . . . . ? C1 Cr1 P5 P4 -148.0(3) . . . . ? P31 Cr1 P5 P4 49.6(6) . . . . ? P21 Cr1 P5 P4 101.9(5) . . . . ? P11 Cr1 P5 P4 136.4(8) . . . . ? P51 Cr1 P5 P4 -17(2) . . . . ? P1 Cr1 P5 P4 129.8(5) . . . . ? P42 Cr1 P5 P4 -8.3(4) . . . . ? P2 Cr1 P5 P4 91.2(3) . . . . ? C2 Cr1 P5 Cr2 134.1(3) . . . . ? C4 Cr1 P5 Cr2 -142.96(17) . . . . ? C5 Cr1 P5 Cr2 -176.9(2) . . . . ? C3 Cr1 P5 Cr2 -139.3(4) . . . . ? C1 Cr1 P5 Cr2 146.79(17) . . . . ? P31 Cr1 P5 Cr2 -15.6(5) . . . . ? P21 Cr1 P5 Cr2 36.7(4) . . . . ? P11 Cr1 P5 Cr2 71.3(8) . . . . ? P51 Cr1 P5 Cr2 -82(2) . . . . ? P1 Cr1 P5 Cr2 64.6(3) . . . . ? P42 Cr1 P5 Cr2 -73.4(4) . . . . ? P2 Cr1 P5 Cr2 26.0(2) . . . . ? C2 Cr1 P12 P52 -139.0(5) . . . . ? C4 Cr1 P12 P52 -101.9(13) . . . . ? C5 Cr1 P12 P52 -73.3(4) . . . . ? C3 Cr1 P12 P52 -161.9(3) . . . . ? C1 Cr1 P12 P52 -100.9(5) . . . . ? P31 Cr1 P12 P52 111.8(6) . . . . ? P21 Cr1 P12 P52 139.9(10) . . . . ? P11 Cr1 P12 P52 -10.7(12) . . . . ? P51 Cr1 P12 P52 18.5(6) . . . . ? P1 Cr1 P12 P52 -17.3(7) . . . . ? P42 Cr1 P12 P52 37.7(4) . . . . ? P2 Cr1 P12 P52 137.1(6) . . . . ? C2 Cr1 P12 P22 93.6(5) . . . . ? C4 Cr1 P12 P22 130.7(13) . . . . ? C5 Cr1 P12 P22 159.3(3) . . . . ? C3 Cr1 P12 P22 70.7(5) . . . . ? C1 Cr1 P12 P22 131.7(5) . . . . ? P31 Cr1 P12 P22 -15.6(6) . . . . ? P21 Cr1 P12 P22 12.5(8) . . . . ? P11 Cr1 P12 P22 -138.1(15) . . . . ? P51 Cr1 P12 P22 -108.9(5) . . . . ? P1 Cr1 P12 P22 -144.7(9) . . . . ? P42 Cr1 P12 P22 -89.7(4) . . . . ? P2 Cr1 P12 P22 9.7(5) . . . . ? C2 Cr1 P12 Cr2 156.8(3) . . . . ? C4 Cr1 P12 Cr2 -166.1(12) . . . . ? C5 Cr1 P12 Cr2 -137.4(2) . . . . ? C3 Cr1 P12 Cr2 134.0(2) . . . . ? C1 Cr1 P12 Cr2 -165.1(4) . . . . ? P31 Cr1 P12 Cr2 47.7(5) . . . . ? P21 Cr1 P12 Cr2 75.7(9) . . . . ? P11 Cr1 P12 Cr2 -74.9(12) . . . . ? P51 Cr1 P12 Cr2 -45.7(4) . . . . ? P1 Cr1 P12 Cr2 -81.4(7) . . . . ? P42 Cr1 P12 Cr2 -26.4(3) . . . . ? P2 Cr1 P12 Cr2 72.9(4) . . . . ? P52 P12 P22 P32 -1.2(7) . . . . ? Cr1 P12 P22 P32 46.4(4) . . . . ? Cr2 P12 P22 P32 -47.5(4) . . . . ? P52 P12 P22 Cr2 46.4(4) . . . . ? Cr1 P12 P22 Cr2 94.0(2) . . . . ? P52 P12 P22 Cr1 -47.6(4) . . . . ? Cr2 P12 P22 Cr1 -94.0(2) . . . . ? C2 Cr1 P22 P32 130.6(5) . . . . ? C4 Cr1 P22 P32 68.5(4) . . . . ? C5 Cr1 P22 P32 127.4(15) . . . . ? C3 Cr1 P22 P32 92.0(5) . . . . ? C1 Cr1 P22 P32 158.4(3) . . . . ? P31 Cr1 P22 P32 11.6(11) . . . . ? P21 Cr1 P22 P32 -140.8(8) . . . . ? P11 Cr1 P22 P32 -110.1(5) . . . . ? P51 Cr1 P22 P32 -61.8(6) . . . . ? P1 Cr1 P22 P32 -120.1(4) . . . . ? P42 Cr1 P22 P32 -38.1(4) . . . . ? P2 Cr1 P22 P32 -151.0(11) . . . . ? C2 Cr1 P22 P12 -98.9(5) . . . . ? C4 Cr1 P22 P12 -161.0(3) . . . . ? C5 Cr1 P22 P12 -102.1(15) . . . . ? C3 Cr1 P22 P12 -137.5(4) . . . . ? C1 Cr1 P22 P12 -71.1(4) . . . . ? P31 Cr1 P22 P12 142.1(11) . . . . ? P21 Cr1 P22 P12 -10.4(7) . . . . ? P11 Cr1 P22 P12 20.3(6) . . . . ? P51 Cr1 P22 P12 68.7(6) . . . . ? P1 Cr1 P22 P12 10.4(3) . . . . ? P42 Cr1 P22 P12 92.3(4) . . . . ? P2 Cr1 P22 P12 -20.6(8) . . . . ? C2 Cr1 P22 Cr2 -163.8(4) . . . . ? C4 Cr1 P22 Cr2 134.16(19) . . . . ? C5 Cr1 P22 Cr2 -167.0(14) . . . . ? C3 Cr1 P22 Cr2 157.7(4) . . . . ? C1 Cr1 P22 Cr2 -136.0(2) . . . . ? P31 Cr1 P22 Cr2 77.2(11) . . . . ? P21 Cr1 P22 Cr2 -75.2(7) . . . . ? P11 Cr1 P22 Cr2 -44.5(4) . . . . ? P51 Cr1 P22 Cr2 3.8(5) . . . . ? P1 Cr1 P22 Cr2 -54.5(3) . . . . ? P42 Cr1 P22 Cr2 27.5(4) . . . . ? P2 Cr1 P22 Cr2 -85.4(9) . . . . ? P12 P22 P32 P42 0.6(7) . . . . ? Cr2 P22 P32 P42 -46.6(4) . . . . ? Cr1 P22 P32 P42 46.4(4) . . . . ? P12 P22 P32 Cr2 47.2(5) . . . . ? Cr1 P22 P32 Cr2 93.0(2) . . . . ? P12 P22 P32 Cr1 -45.8(4) . . . . ? Cr2 P22 P32 Cr1 -93.0(2) . . . . ? C2 Cr1 P32 P22 -71.5(4) . . . . ? C4 Cr1 P32 P22 -138.3(4) . . . . ? C5 Cr1 P32 P22 -160.7(3) . . . . ? C3 Cr1 P32 P22 -99.8(5) . . . . ? C1 Cr1 P32 P22 -98.9(14) . . . . ? P31 Cr1 P32 P22 -10.5(10) . . . . ? P21 Cr1 P32 P22 19.0(5) . . . . ? P11 Cr1 P32 P22 68.2(5) . . . . ? P51 Cr1 P32 P22 114.1(5) . . . . ? P1 Cr1 P32 P22 53.9(5) . . . . ? P42 Cr1 P32 P22 129.3(5) . . . . ? P2 Cr1 P32 P22 8.9(3) . . . . ? C2 Cr1 P32 P42 159.1(4) . . . . ? C4 Cr1 P32 P42 92.4(5) . . . . ? C5 Cr1 P32 P42 70.0(5) . . . . ? C3 Cr1 P32 P42 130.9(5) . . . . ? C1 Cr1 P32 P42 131.8(13) . . . . ? P31 Cr1 P32 P42 -139.8(12) . . . . ? P21 Cr1 P32 P42 -110.4(4) . . . . ? P11 Cr1 P32 P42 -61.1(5) . . . . ? P51 Cr1 P32 P42 -15.2(5) . . . . ? P1 Cr1 P32 P42 -75.4(5) . . . . ? P2 Cr1 P32 P42 -120.4(4) . . . . ? C2 Cr1 P32 Cr2 -136.1(2) . . . . ? C4 Cr1 P32 Cr2 157.2(3) . . . . ? C5 Cr1 P32 Cr2 134.8(2) . . . . ? C3 Cr1 P32 Cr2 -164.4(4) . . . . ? C1 Cr1 P32 Cr2 -163.5(13) . . . . ? P31 Cr1 P32 Cr2 -75.0(10) . . . . ? P21 Cr1 P32 Cr2 -45.6(3) . . . . ? P11 Cr1 P32 Cr2 3.6(4) . . . . ? P51 Cr1 P32 Cr2 49.5(5) . . . . ? P1 Cr1 P32 Cr2 -10.6(4) . . . . ? P42 Cr1 P32 Cr2 64.8(4) . . . . ? P2 Cr1 P32 Cr2 -55.6(3) . . . . ? P22 P32 P42 P52 0.2(7) . . . . ? Cr2 P32 P42 P52 -46.3(5) . . . . ? Cr1 P32 P42 P52 47.2(5) . . . . ? P22 P32 P42 Cr1 -47.0(4) . . . . ? Cr2 P32 P42 Cr1 -93.5(3) . . . . ? P22 P32 P42 Cr2 46.5(4) . . . . ? Cr1 P32 P42 Cr2 93.5(3) . . . . ? C2 Cr1 P42 P52 130.8(15) . . . . ? C4 Cr1 P42 P52 130.7(5) . . . . ? C5 Cr1 P42 P52 92.5(4) . . . . ? C3 Cr1 P42 P52 159.3(3) . . . . ? C1 Cr1 P42 P52 69.3(5) . . . . ? P31 Cr1 P42 P52 -111.1(5) . . . . ? P21 Cr1 P42 P52 -62.2(5) . . . . ? P11 Cr1 P42 P52 -14.4(6) . . . . ? P51 Cr1 P42 P52 13.2(10) . . . . ? P1 Cr1 P42 P52 -24.2(4) . . . . ? P2 Cr1 P42 P52 -75.9(5) . . . . ? C2 Cr1 P42 P32 -100.0(15) . . . . ? C4 Cr1 P42 P32 -100.1(5) . . . . ? C5 Cr1 P42 P32 -138.3(4) . . . . ? C3 Cr1 P42 P32 -71.6(4) . . . . ? C1 Cr1 P42 P32 -161.5(3) . . . . ? P31 Cr1 P42 P32 18.1(6) . . . . ? P21 Cr1 P42 P32 66.9(5) . . . . ? P11 Cr1 P42 P32 114.7(6) . . . . ? P51 Cr1 P42 P32 142.4(10) . . . . ? P1 Cr1 P42 P32 105.0(5) . . . . ? P2 Cr1 P42 P32 53.3(5) . . . . ? C2 Cr1 P42 Cr2 -164.7(14) . . . . ? C4 Cr1 P42 Cr2 -164.8(4) . . . . ? C5 Cr1 P42 Cr2 157.0(4) . . . . ? C3 Cr1 P42 Cr2 -136.2(2) . . . . ? C1 Cr1 P42 Cr2 133.8(2) . . . . ? P31 Cr1 P42 Cr2 -46.6(4) . . . . ? P21 Cr1 P42 Cr2 2.3(4) . . . . ? P11 Cr1 P42 Cr2 50.1(5) . . . . ? P51 Cr1 P42 Cr2 77.8(9) . . . . ? P1 Cr1 P42 Cr2 40.3(4) . . . . ? P2 Cr1 P42 Cr2 -11.3(4) . . . . ? P32 P42 P52 P12 -0.9(8) . . . . ? Cr1 P42 P52 P12 46.4(5) . . . . ? Cr2 P42 P52 P12 -47.2(5) . . . . ? P32 P42 P52 Cr2 46.3(4) . . . . ? Cr1 P42 P52 Cr2 93.6(2) . . . . ? P32 P42 P52 Cr1 -47.3(4) . . . . ? Cr2 P42 P52 Cr1 -93.6(2) . . . . ? P22 P12 P52 P42 1.3(8) . . . . ? Cr1 P12 P52 P42 -46.3(5) . . . . ? Cr2 P12 P52 P42 47.2(5) . . . . ? P22 P12 P52 Cr2 -46.0(4) . . . . ? Cr1 P12 P52 Cr2 -93.5(3) . . . . ? P22 P12 P52 Cr1 47.6(4) . . . . ? Cr2 P12 P52 Cr1 93.5(3) . . . . ? C2 Cr1 P52 P42 -161.7(3) . . . . ? C4 Cr1 P52 P42 -71.9(4) . . . . ? C5 Cr1 P52 P42 -100.3(4) . . . . ? C3 Cr1 P52 P42 -100.1(16) . . . . ? C1 Cr1 P52 P42 -138.8(4) . . . . ? P31 Cr1 P52 P42 65.6(6) . . . . ? P21 Cr1 P52 P42 113.6(5) . . . . ? P11 Cr1 P52 P42 143.5(15) . . . . ? P51 Cr1 P52 P42 -11.1(8) . . . . ? P1 Cr1 P52 P42 138.0(6) . . . . ? P2 Cr1 P52 P42 104.9(4) . . . . ? C2 Cr1 P52 P12 68.4(5) . . . . ? C4 Cr1 P52 P12 158.2(4) . . . . ? C5 Cr1 P52 P12 129.8(5) . . . . ? C3 Cr1 P52 P12 130.0(15) . . . . ? C1 Cr1 P52 P12 91.4(5) . . . . ? P31 Cr1 P52 P12 -64.3(6) . . . . ? P21 Cr1 P52 P12 -16.3(5) . . . . ? P11 Cr1 P52 P12 13.7(15) . . . . ? P51 Cr1 P52 P12 -141.0(11) . . . . ? P1 Cr1 P52 P12 8.1(4) . . . . ? P42 Cr1 P52 P12 -129.9(5) . . . . ? P2 Cr1 P52 P12 -25.0(4) . . . . ? C2 Cr1 P52 Cr2 133.4(2) . . . . ? C4 Cr1 P52 Cr2 -136.8(2) . . . . ? C5 Cr1 P52 Cr2 -165.2(4) . . . . ? C3 Cr1 P52 Cr2 -165.1(14) . . . . ? C1 Cr1 P52 Cr2 156.3(4) . . . . ? P31 Cr1 P52 Cr2 0.6(6) . . . . ? P21 Cr1 P52 Cr2 48.7(4) . . . . ? P11 Cr1 P52 Cr2 78.6(13) . . . . ? P51 Cr1 P52 Cr2 -76.0(9) . . . . ? P1 Cr1 P52 Cr2 73.1(5) . . . . ? P42 Cr1 P52 Cr2 -64.9(3) . . . . ? P2 Cr1 P52 Cr2 40.0(4) . . . . ? P41 P31 Cr2 C11 -161.3(6) . . . . ? P21 P31 Cr2 C11 68.7(6) . . . . ? Cr1 P31 Cr2 C11 132.5(3) . . . . ? P41 P31 Cr2 C15 -93(2) . . . . ? P21 P31 Cr2 C15 136.6(18) . . . . ? Cr1 P31 Cr2 C15 -159.7(16) . . . . ? P41 P31 Cr2 C13 -100.4(7) . . . . ? P21 P31 Cr2 C13 129.6(5) . . . . ? Cr1 P31 Cr2 C13 -166.6(4) . . . . ? P41 P31 Cr2 C14 -71.0(7) . . . . ? P21 P31 Cr2 C14 159.1(4) . . . . ? Cr1 P31 Cr2 C14 -137.2(3) . . . . ? P41 P31 Cr2 C12 -138.8(6) . . . . ? P21 P31 Cr2 C12 91.3(5) . . . . ? Cr1 P31 Cr2 C12 155.0(4) . . . . ? P41 P31 Cr2 P21 130.0(8) . . . . ? Cr1 P31 Cr2 P21 63.7(5) . . . . ? P21 P31 Cr2 P41 -130.0(8) . . . . ? Cr1 P31 Cr2 P41 -66.2(7) . . . . ? P41 P31 Cr2 P51 38.2(7) . . . . ? P21 P31 Cr2 P51 -91.7(6) . . . . ? Cr1 P31 Cr2 P51 -28.0(6) . . . . ? P41 P31 Cr2 P11 89.9(7) . . . . ? P21 P31 Cr2 P11 -40.0(5) . . . . ? Cr1 P31 Cr2 P11 23.7(6) . . . . ? P41 P31 Cr2 P22 147.5(12) . . . . ? P21 P31 Cr2 P22 17.5(9) . . . . ? Cr1 P31 Cr2 P22 81.3(8) . . . . ? P41 P31 Cr2 P52 66.9(7) . . . . ? P21 P31 Cr2 P52 -63.1(6) . . . . ? Cr1 P31 Cr2 P52 0.6(6) . . . . ? P31 P21 Cr2 C11 -140.7(6) . . . . ? P11 P21 Cr2 C11 92.3(6) . . . . ? Cr1 P21 Cr2 C11 156.1(4) . . . . ? P31 P21 Cr2 C15 -163.7(5) . . . . ? P11 P21 Cr2 C15 69.4(7) . . . . ? Cr1 P21 Cr2 C15 133.1(3) . . . . ? P31 P21 Cr2 C13 -74.0(6) . . . . ? P11 P21 Cr2 C13 159.0(6) . . . . ? Cr1 P21 Cr2 C13 -137.3(2) . . . . ? P31 P21 Cr2 C14 -101.2(17) . . . . ? P11 P21 Cr2 C14 131.9(17) . . . . ? Cr1 P21 Cr2 C14 -164.4(14) . . . . ? P31 P21 Cr2 C12 -102.3(6) . . . . ? P11 P21 Cr2 C12 130.7(6) . . . . ? Cr1 P21 Cr2 C12 -165.6(4) . . . . ? P11 P21 Cr2 P31 -127.0(8) . . . . ? Cr1 P21 Cr2 P31 -63.3(6) . . . . ? P31 P21 Cr2 P41 36.6(6) . . . . ? P11 P21 Cr2 P41 -90.3(7) . . . . ? Cr1 P21 Cr2 P41 -26.6(5) . . . . ? P31 P21 Cr2 P51 89.2(7) . . . . ? P11 P21 Cr2 P51 -37.8(6) . . . . ? Cr1 P21 Cr2 P51 25.9(5) . . . . ? P31 P21 Cr2 P11 127.0(8) . . . . ? Cr1 P21 Cr2 P11 63.7(6) . . . . ? P31 P21 Cr2 P22 -14.7(8) . . . . ? P11 P21 Cr2 P22 -141.6(11) . . . . ? Cr1 P21 Cr2 P22 -77.9(8) . . . . ? P31 P21 Cr2 P52 112.9(6) . . . . ? P11 P21 Cr2 P52 -14.1(6) . . . . ? Cr1 P21 Cr2 P52 49.6(4) . . . . ? P31 P41 Cr2 C11 132.9(16) . . . . ? P51 P41 Cr2 C11 -98.4(17) . . . . ? Cr1 P41 Cr2 C11 -162.6(15) . . . . ? P31 P41 Cr2 C15 159.3(5) . . . . ? P51 P41 Cr2 C15 -72.0(7) . . . . ? Cr1 P41 Cr2 C15 -136.2(3) . . . . ? P31 P41 Cr2 C13 92.3(6) . . . . ? P51 P41 Cr2 C13 -139.0(6) . . . . ? Cr1 P41 Cr2 C13 156.7(4) . . . . ? P31 P41 Cr2 C14 130.5(6) . . . . ? P51 P41 Cr2 C14 -100.8(6) . . . . ? Cr1 P41 Cr2 C14 -165.0(4) . . . . ? P31 P41 Cr2 C12 69.4(7) . . . . ? P51 P41 Cr2 C12 -161.9(5) . . . . ? Cr1 P41 Cr2 C12 133.8(3) . . . . ? P51 P41 Cr2 P31 128.7(8) . . . . ? Cr1 P41 Cr2 P31 64.5(5) . . . . ? P31 P41 Cr2 P21 -38.1(6) . . . . ? P51 P41 Cr2 P21 90.6(6) . . . . ? Cr1 P41 Cr2 P21 26.3(4) . . . . ? P31 P41 Cr2 P51 -128.7(8) . . . . ? Cr1 P41 Cr2 P51 -64.3(6) . . . . ? P31 P41 Cr2 P11 -91.7(7) . . . . ? P51 P41 Cr2 P11 37.0(7) . . . . ? Cr1 P41 Cr2 P11 -27.2(5) . . . . ? P31 P41 Cr2 P22 -13.8(5) . . . . ? P51 P41 Cr2 P22 114.9(6) . . . . ? Cr1 P41 Cr2 P22 50.7(3) . . . . ? P31 P41 Cr2 P52 -110.9(6) . . . . ? P51 P41 Cr2 P52 17.8(6) . . . . ? Cr1 P41 Cr2 P52 -46.4(3) . . . . ? P11 P51 Cr2 C11 -71.3(8) . . . . ? P41 P51 Cr2 C11 158.8(5) . . . . ? Cr1 P51 Cr2 C11 -136.0(2) . . . . ? P11 P51 Cr2 C15 -99.7(8) . . . . ? P41 P51 Cr2 C15 130.4(6) . . . . ? Cr1 P51 Cr2 C15 -164.4(4) . . . . ? P11 P51 Cr2 C13 -160.7(7) . . . . ? P41 P51 Cr2 C13 69.4(7) . . . . ? Cr1 P51 Cr2 C13 134.5(3) . . . . ? P11 P51 Cr2 C14 -138.0(8) . . . . ? P41 P51 Cr2 C14 92.0(6) . . . . ? Cr1 P51 Cr2 C14 157.2(4) . . . . ? P11 P51 Cr2 C12 -97.5(19) . . . . ? P41 P51 Cr2 C12 132.5(17) . . . . ? Cr1 P51 Cr2 C12 -162.3(15) . . . . ? P11 P51 Cr2 P31 92.5(8) . . . . ? P41 P51 Cr2 P31 -37.4(7) . . . . ? Cr1 P51 Cr2 P31 27.8(6) . . . . ? P11 P51 Cr2 P21 38.9(7) . . . . ? P41 P51 Cr2 P21 -91.0(7) . . . . ? Cr1 P51 Cr2 P21 -25.8(5) . . . . ? P11 P51 Cr2 P41 129.9(9) . . . . ? Cr1 P51 Cr2 P41 65.2(6) . . . . ? P41 P51 Cr2 P11 -129.9(9) . . . . ? Cr1 P51 Cr2 P11 -64.8(7) . . . . ? P11 P51 Cr2 P22 68.6(7) . . . . ? P41 P51 Cr2 P22 -61.3(6) . . . . ? Cr1 P51 Cr2 P22 3.9(5) . . . . ? P11 P51 Cr2 P52 -12.8(10) . . . . ? P41 P51 Cr2 P52 -142.7(12) . . . . ? Cr1 P51 Cr2 P52 -77.5(9) . . . . ? P51 P11 Cr2 C11 130.7(6) . . . . ? P21 P11 Cr2 C11 -100.6(6) . . . . ? Cr1 P11 Cr2 C11 -164.3(4) . . . . ? P51 P11 Cr2 C15 92.4(6) . . . . ? P21 P11 Cr2 C15 -139.0(5) . . . . ? Cr1 P11 Cr2 C15 157.4(4) . . . . ? P51 P11 Cr2 C13 129.2(16) . . . . ? P21 P11 Cr2 C13 -102.2(18) . . . . ? Cr1 P11 Cr2 C13 -165.8(15) . . . . ? P51 P11 Cr2 C14 69.4(8) . . . . ? P21 P11 Cr2 C14 -161.9(5) . . . . ? Cr1 P11 Cr2 C14 134.4(4) . . . . ? P51 P11 Cr2 C12 158.8(4) . . . . ? P21 P11 Cr2 C12 -72.5(7) . . . . ? Cr1 P11 Cr2 C12 -136.2(3) . . . . ? P51 P11 Cr2 P31 -88.6(7) . . . . ? P21 P11 Cr2 P31 40.1(6) . . . . ? Cr1 P11 Cr2 P31 -23.6(6) . . . . ? P51 P11 Cr2 P21 -128.7(8) . . . . ? Cr1 P11 Cr2 P21 -63.7(5) . . . . ? P51 P11 Cr2 P41 -37.5(6) . . . . ? P21 P11 Cr2 P41 91.2(6) . . . . ? Cr1 P11 Cr2 P41 27.5(4) . . . . ? P21 P11 Cr2 P51 128.7(8) . . . . ? Cr1 P11 Cr2 P51 65.0(5) . . . . ? P51 P11 Cr2 P22 -110.0(6) . . . . ? P21 P11 Cr2 P22 18.6(6) . . . . ? Cr1 P11 Cr2 P22 -45.0(4) . . . . ? P51 P11 Cr2 P52 15.7(13) . . . . ? P21 P11 Cr2 P52 144.4(17) . . . . ? Cr1 P11 Cr2 P52 80.7(13) . . . . ? P32 P22 Cr2 C11 -154.6(4) . . . . ? P12 P22 Cr2 C11 76.0(4) . . . . ? Cr1 P22 Cr2 C11 140.1(3) . . . . ? P32 P22 Cr2 C15 -150.6(9) . . . . ? P12 P22 Cr2 C15 80.0(9) . . . . ? Cr1 P22 Cr2 C15 144.1(7) . . . . ? P32 P22 Cr2 C13 -85.5(4) . . . . ? P12 P22 Cr2 C13 145.1(4) . . . . ? Cr1 P22 Cr2 C13 -150.9(3) . . . . ? P32 P22 Cr2 C14 -69.7(5) . . . . ? P12 P22 Cr2 C14 161.0(4) . . . . ? Cr1 P22 Cr2 C14 -135.0(2) . . . . ? P32 P22 Cr2 C12 -122.4(5) . . . . ? P12 P22 Cr2 C12 108.2(5) . . . . ? Cr1 P22 Cr2 C12 172.2(4) . . . . ? P32 P22 Cr2 P31 -11.0(10) . . . . ? P12 P22 Cr2 P31 -140.4(10) . . . . ? Cr1 P22 Cr2 P31 -76.4(10) . . . . ? P32 P22 Cr2 P21 140.3(10) . . . . ? P12 P22 Cr2 P21 10.9(8) . . . . ? Cr1 P22 Cr2 P21 74.9(8) . . . . ? P32 P22 Cr2 P41 14.9(5) . . . . ? P12 P22 Cr2 P41 -114.5(5) . . . . ? Cr1 P22 Cr2 P41 -50.5(4) . . . . ? P32 P22 Cr2 P51 61.5(6) . . . . ? P12 P22 Cr2 P51 -67.9(6) . . . . ? Cr1 P22 Cr2 P51 -3.8(5) . . . . ? P32 P22 Cr2 P11 109.7(5) . . . . ? P12 P22 Cr2 P11 -19.7(6) . . . . ? Cr1 P22 Cr2 P11 44.3(4) . . . . ? P32 P22 Cr2 P52 90.7(5) . . . . ? P12 P22 Cr2 P52 -38.7(4) . . . . ? Cr1 P22 Cr2 P52 25.3(4) . . . . ? P42 P52 Cr2 C11 146.2(4) . . . . ? P12 P52 Cr2 C11 -84.7(5) . . . . ? Cr1 P52 Cr2 C11 -149.3(3) . . . . ? P42 P52 Cr2 C15 109.5(5) . . . . ? P12 P52 Cr2 C15 -121.4(5) . . . . ? Cr1 P52 Cr2 C15 173.9(4) . . . . ? P42 P52 Cr2 C13 80.7(10) . . . . ? P12 P52 Cr2 C13 -150.2(9) . . . . ? Cr1 P52 Cr2 C13 145.2(8) . . . . ? P42 P52 Cr2 C14 77.2(4) . . . . ? P12 P52 Cr2 C14 -153.7(4) . . . . ? Cr1 P52 Cr2 C14 141.6(2) . . . . ? P42 P52 Cr2 C12 161.8(3) . . . . ? P12 P52 Cr2 C12 -69.1(6) . . . . ? Cr1 P52 Cr2 C12 -133.8(3) . . . . ? P42 P52 Cr2 P31 -65.1(6) . . . . ? P12 P52 Cr2 P31 64.0(6) . . . . ? Cr1 P52 Cr2 P31 -0.6(6) . . . . ? P42 P52 Cr2 P21 -113.5(5) . . . . ? P12 P52 Cr2 P21 15.6(5) . . . . ? Cr1 P52 Cr2 P21 -49.1(4) . . . . ? P42 P52 Cr2 P41 -17.9(6) . . . . ? P12 P52 Cr2 P41 111.2(5) . . . . ? Cr1 P52 Cr2 P41 46.6(4) . . . . ? P42 P52 Cr2 P51 11.6(8) . . . . ? P12 P52 Cr2 P51 140.7(11) . . . . ? Cr1 P52 Cr2 P51 76.1(9) . . . . ? P42 P52 Cr2 P11 -142.7(15) . . . . ? P12 P52 Cr2 P11 -13.6(16) . . . . ? Cr1 P52 Cr2 P11 -78.3(14) . . . . ? P42 P52 Cr2 P22 -89.9(4) . . . . ? P12 P52 Cr2 P22 39.2(5) . . . . ? Cr1 P52 Cr2 P22 -25.4(4) . . . . ? C13 Cr2 C11 C15 80.21(15) . . . . ? C14 Cr2 C11 C15 37.76(14) . . . . ? C12 Cr2 C11 C15 117.9(2) . . . . ? P31 Cr2 C11 C15 155.0(7) . . . . ? P21 Cr2 C11 C15 -154.1(5) . . . . ? P41 Cr2 C11 C15 35(2) . . . . ? P51 Cr2 C11 C15 -50.2(7) . . . . ? P11 Cr2 C11 C15 -99.3(6) . . . . ? P22 Cr2 C11 C15 177.6(5) . . . . ? P52 Cr2 C11 C15 -76.6(5) . . . . ? C15 Cr2 C11 C12 -117.9(2) . . . . ? C13 Cr2 C11 C12 -37.69(15) . . . . ? C14 Cr2 C11 C12 -80.15(15) . . . . ? P31 Cr2 C11 C12 37.1(7) . . . . ? P21 Cr2 C11 C12 88.0(5) . . . . ? P41 Cr2 C11 C12 -83(2) . . . . ? P51 Cr2 C11 C12 -168.1(7) . . . . ? P11 Cr2 C11 C12 142.8(6) . . . . ? P22 Cr2 C11 C12 59.7(6) . . . . ? P52 Cr2 C11 C12 165.5(5) . . . . ? C15 Cr2 C11 C16 121.0(3) . . . . ? C13 Cr2 C11 C16 -158.8(3) . . . . ? C14 Cr2 C11 C16 158.7(3) . . . . ? C12 Cr2 C11 C16 -121.1(3) . . . . ? P31 Cr2 C11 C16 -84.1(7) . . . . ? P21 Cr2 C11 C16 -33.2(6) . . . . ? P41 Cr2 C11 C16 156(2) . . . . ? P51 Cr2 C11 C16 70.8(7) . . . . ? P11 Cr2 C11 C16 21.7(7) . . . . ? P22 Cr2 C11 C16 -61.5(6) . . . . ? P52 Cr2 C11 C16 44.4(6) . . . . ? C15 C11 C12 C13 -0.3(3) . . . . ? C16 C11 C12 C13 -177.2(2) . . . . ? Cr2 C11 C12 C13 61.97(17) . . . . ? C15 C11 C12 C17 175.8(3) . . . . ? C16 C11 C12 C17 -1.1(4) . . . . ? Cr2 C11 C12 C17 -121.9(3) . . . . ? C15 C11 C12 Cr2 -62.26(17) . . . . ? C16 C11 C12 Cr2 120.8(3) . . . . ? C15 Cr2 C12 C11 37.18(14) . . . . ? C13 Cr2 C12 C11 117.0(2) . . . . ? C14 Cr2 C12 C11 79.66(15) . . . . ? P31 Cr2 C12 C11 -155.7(6) . . . . ? P21 Cr2 C12 C11 -100.7(6) . . . . ? P41 Cr2 C12 C11 155.1(7) . . . . ? P51 Cr2 C12 C11 35(2) . . . . ? P11 Cr2 C12 C11 -49.5(8) . . . . ? P22 Cr2 C12 C11 -131.4(6) . . . . ? P52 Cr2 C12 C11 -24.5(7) . . . . ? C11 Cr2 C12 C13 -117.0(2) . . . . ? C15 Cr2 C12 C13 -79.80(15) . . . . ? C14 Cr2 C12 C13 -37.33(14) . . . . ? P31 Cr2 C12 C13 87.4(6) . . . . ? P21 Cr2 C12 C13 142.3(6) . . . . ? P41 Cr2 C12 C13 38.1(7) . . . . ? P51 Cr2 C12 C13 -82(2) . . . . ? P11 Cr2 C12 C13 -166.5(8) . . . . ? P22 Cr2 C12 C13 111.7(6) . . . . ? P52 Cr2 C12 C13 -141.5(7) . . . . ? C11 Cr2 C12 C17 121.8(4) . . . . ? C15 Cr2 C12 C17 159.0(3) . . . . ? C13 Cr2 C12 C17 -121.2(4) . . . . ? C14 Cr2 C12 C17 -158.6(3) . . . . ? P31 Cr2 C12 C17 -33.9(7) . . . . ? P21 Cr2 C12 C17 21.0(7) . . . . ? P41 Cr2 C12 C17 -83.2(8) . . . . ? P51 Cr2 C12 C17 157(2) . . . . ? P11 Cr2 C12 C17 72.3(9) . . . . ? P22 Cr2 C12 C17 -9.6(7) . . . . ? P52 Cr2 C12 C17 97.3(8) . . . . ? C11 C12 C13 C14 0.3(3) . . . . ? C17 C12 C13 C14 -175.8(2) . . . . ? Cr2 C12 C13 C14 62.05(16) . . . . ? C11 C12 C13 C18 176.4(3) . . . . ? C17 C12 C13 C18 0.2(4) . . . . ? Cr2 C12 C13 C18 -121.9(3) . . . . ? C11 C12 C13 Cr2 -61.73(16) . . . . ? C17 C12 C13 Cr2 122.1(3) . . . . ? C11 Cr2 C13 C14 -79.89(15) . . . . ? C15 Cr2 C13 C14 -37.46(14) . . . . ? C12 Cr2 C13 C14 -117.7(2) . . . . ? P31 Cr2 C13 C14 140.4(7) . . . . ? P21 Cr2 C13 C14 -167.6(7) . . . . ? P41 Cr2 C13 C14 87.9(6) . . . . ? P51 Cr2 C13 C14 37.7(7) . . . . ? P11 Cr2 C13 C14 -78(2) . . . . ? P22 Cr2 C13 C14 165.0(6) . . . . ? P52 Cr2 C13 C14 -5.1(14) . . . . ? C11 Cr2 C13 C12 37.76(15) . . . . ? C15 Cr2 C13 C12 80.19(16) . . . . ? C14 Cr2 C13 C12 117.7(2) . . . . ? P31 Cr2 C13 C12 -102.0(7) . . . . ? P21 Cr2 C13 C12 -49.9(7) . . . . ? P41 Cr2 C13 C12 -154.4(6) . . . . ? P51 Cr2 C13 C12 155.4(6) . . . . ? P11 Cr2 C13 C12 39(2) . . . . ? P22 Cr2 C13 C12 -77.3(6) . . . . ? P52 Cr2 C13 C12 112.6(13) . . . . ? C11 Cr2 C13 C18 159.6(3) . . . . ? C15 Cr2 C13 C18 -158.0(3) . . . . ? C14 Cr2 C13 C18 -120.5(3) . . . . ? C12 Cr2 C13 C18 121.9(3) . . . . ? P31 Cr2 C13 C18 19.9(7) . . . . ? P21 Cr2 C13 C18 71.9(7) . . . . ? P41 Cr2 C13 C18 -32.6(6) . . . . ? P51 Cr2 C13 C18 -82.8(7) . . . . ? P11 Cr2 C13 C18 161(2) . . . . ? P22 Cr2 C13 C18 44.5(6) . . . . ? P52 Cr2 C13 C18 -125.6(14) . . . . ? C12 C13 C14 C15 -0.2(3) . . . . ? C18 C13 C14 C15 -176.3(2) . . . . ? Cr2 C13 C14 C15 61.93(16) . . . . ? C12 C13 C14 C19 176.7(2) . . . . ? C18 C13 C14 C19 0.6(4) . . . . ? Cr2 C13 C14 C19 -121.1(3) . . . . ? C12 C13 C14 Cr2 -62.16(17) . . . . ? C18 C13 C14 Cr2 121.7(3) . . . . ? C11 Cr2 C14 C13 79.90(16) . . . . ? C15 Cr2 C14 C13 117.6(2) . . . . ? C12 Cr2 C14 C13 37.36(15) . . . . ? P31 Cr2 C14 C13 -52.4(7) . . . . ? P21 Cr2 C14 C13 36(2) . . . . ? P41 Cr2 C14 C13 -100.9(6) . . . . ? P51 Cr2 C14 C13 -154.6(6) . . . . ? P11 Cr2 C14 C13 155.9(7) . . . . ? P22 Cr2 C14 C13 -25.1(8) . . . . ? P52 Cr2 C14 C13 177.8(6) . . . . ? C11 Cr2 C14 C15 -37.67(15) . . . . ? C13 Cr2 C14 C15 -117.6(2) . . . . ? C12 Cr2 C14 C15 -80.21(16) . . . . ? P31 Cr2 C14 C15 -170.0(7) . . . . ? P21 Cr2 C14 C15 -81(2) . . . . ? P41 Cr2 C14 C15 141.6(6) . . . . ? P51 Cr2 C14 C15 87.8(6) . . . . ? P11 Cr2 C14 C15 38.3(7) . . . . ? P22 Cr2 C14 C15 -142.6(8) . . . . ? P52 Cr2 C14 C15 60.2(6) . . . . ? C11 Cr2 C14 C19 -160.1(3) . . . . ? C15 Cr2 C14 C19 -122.4(3) . . . . ? C13 Cr2 C14 C19 120.0(3) . . . . ? C12 Cr2 C14 C19 157.4(3) . . . . ? P31 Cr2 C14 C19 67.6(8) . . . . ? P21 Cr2 C14 C19 156(2) . . . . ? P41 Cr2 C14 C19 19.2(6) . . . . ? P51 Cr2 C14 C19 -34.6(6) . . . . ? P11 Cr2 C14 C19 -84.1(7) . . . . ? P22 Cr2 C14 C19 95.0(8) . . . . ? P52 Cr2 C14 C19 -62.2(6) . . . . ? C12 C11 C15 C14 0.2(3) . . . . ? C16 C11 C15 C14 177.1(2) . . . . ? Cr2 C11 C15 C14 -62.24(16) . . . . ? C12 C11 C15 C20 -177.0(2) . . . . ? C16 C11 C15 C20 -0.1(4) . . . . ? Cr2 C11 C15 C20 120.6(3) . . . . ? C12 C11 C15 Cr2 62.39(17) . . . . ? C16 C11 C15 Cr2 -120.7(3) . . . . ? C13 C14 C15 C11 0.1(3) . . . . ? C19 C14 C15 C11 -176.8(2) . . . . ? Cr2 C14 C15 C11 62.05(16) . . . . ? C13 C14 C15 C20 177.2(2) . . . . ? C19 C14 C15 C20 0.3(4) . . . . ? Cr2 C14 C15 C20 -120.8(3) . . . . ? C13 C14 C15 Cr2 -62.00(16) . . . . ? C19 C14 C15 Cr2 121.2(3) . . . . ? C13 Cr2 C15 C11 -79.65(16) . . . . ? C14 Cr2 C15 C11 -117.0(2) . . . . ? C12 Cr2 C15 C11 -37.27(15) . . . . ? P31 Cr2 C15 C11 -87(2) . . . . ? P21 Cr2 C15 C11 38.3(6) . . . . ? P41 Cr2 C15 C11 -167.9(7) . . . . ? P51 Cr2 C15 C11 142.1(6) . . . . ? P11 Cr2 C15 C11 89.2(5) . . . . ? P22 Cr2 C15 C11 -5.6(13) . . . . ? P52 Cr2 C15 C11 112.3(6) . . . . ? C11 Cr2 C15 C14 117.0(2) . . . . ? C13 Cr2 C15 C14 37.35(15) . . . . ? C12 Cr2 C15 C14 79.74(16) . . . . ? P31 Cr2 C15 C14 30(2) . . . . ? P21 Cr2 C15 C14 155.3(6) . . . . ? P41 Cr2 C15 C14 -50.9(7) . . . . ? P51 Cr2 C15 C14 -100.9(6) . . . . ? P11 Cr2 C15 C14 -153.8(5) . . . . ? P22 Cr2 C15 C14 111.4(13) . . . . ? P52 Cr2 C15 C14 -130.7(6) . . . . ? C11 Cr2 C15 C20 -121.6(3) . . . . ? C13 Cr2 C15 C20 158.8(3) . . . . ? C14 Cr2 C15 C20 121.4(3) . . . . ? C12 Cr2 C15 C20 -158.8(3) . . . . ? P31 Cr2 C15 C20 151(2) . . . . ? P21 Cr2 C15 C20 -83.3(7) . . . . ? P41 Cr2 C15 C20 70.6(7) . . . . ? P51 Cr2 C15 C20 20.5(7) . . . . ? P11 Cr2 C15 C20 -32.4(6) . . . . ? P22 Cr2 C15 C20 -127.2(13) . . . . ? P52 Cr2 C15 C20 -9.2(6) . . . . ? _diffrn_measured_fraction_theta_max 0.972 _diffrn_reflns_theta_full 30.46 _diffrn_measured_fraction_theta_full 0.972 _refine_diff_density_max 0.894 _refine_diff_density_min -0.512 _refine_diff_density_rms 0.094 #===END data_250k _database_code_depnum_ccdc_archive 'CCDC 618749' _audit_creation_method SHELXL-97 _chemical_name_systematic ; \m~2~-\h^5^,\h^5^-cyclopentaphosphole)-bis ((\h^5^-pentamethyl-cyclopentadienyl)-chromium) hexafluoroantimonate ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H30 Cr2 F6 P5 Sb' _chemical_formula_weight 765.04 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting orthorhombic _symmetry_space_group_name_H-M Fddd loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+3/4, -y+3/4, z' '-x+3/4, y, -z+3/4' 'x, -y+3/4, -z+3/4' 'x, y+1/2, z+1/2' '-x+3/4, -y+5/4, z+1/2' '-x+3/4, y+1/2, -z+5/4' 'x, -y+5/4, -z+5/4' 'x+1/2, y, z+1/2' '-x+5/4, -y+3/4, z+1/2' '-x+5/4, y, -z+5/4' 'x+1/2, -y+3/4, -z+5/4' 'x+1/2, y+1/2, z' '-x+5/4, -y+5/4, z' '-x+5/4, y+1/2, -z+3/4' 'x+1/2, -y+5/4, -z+3/4' '-x, -y, -z' 'x-3/4, y-3/4, -z' 'x-3/4, -y, z-3/4' '-x, y-3/4, z-3/4' '-x, -y+1/2, -z+1/2' 'x-3/4, y-1/4, -z+1/2' 'x-3/4, -y+1/2, z-1/4' '-x, y-1/4, z-1/4' '-x+1/2, -y, -z+1/2' 'x-1/4, y-3/4, -z+1/2' 'x-1/4, -y, z-1/4' '-x+1/2, y-3/4, z-1/4' '-x+1/2, -y+1/2, -z' 'x-1/4, y-1/4, -z' 'x-1/4, -y+1/2, z-3/4' '-x+1/2, y-1/4, z-3/4' _cell_length_a 21.4468(5) _cell_length_b 29.5529(7) _cell_length_c 36.0359(9) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_volume 22840.1(9) _cell_formula_units_Z 32 _cell_measurement_temperature 250(2) _cell_measurement_reflns_used 8663 _cell_measurement_theta_min 2.21 _cell_measurement_theta_max 30.30 _exptl_crystal_description 'irregular block' _exptl_crystal_colour 'dark green' _exptl_crystal_size_max 0.60 _exptl_crystal_size_mid 0.52 _exptl_crystal_size_min 0.40 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.780 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 12096 _exptl_absorpt_coefficient_mu 2.016 _exptl_absorpt_correction_type integration _exptl_absorpt_correction_T_min 0.400 _exptl_absorpt_correction_T_max 0.618 _exptl_absorpt_process_details 'XPREP in SHELXTL' _exptl_special_details ; ? ; _diffrn_ambient_temperature 250(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'Bede Microsource X-ray Generator' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEX CCD Diffractometer' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number 0 _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% 0 _diffrn_reflns_number 43284 _diffrn_reflns_av_R_equivalents 0.0212 _diffrn_reflns_av_sigmaI/netI 0.0182 _diffrn_reflns_limit_h_min -30 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_k_min -41 _diffrn_reflns_limit_k_max 41 _diffrn_reflns_limit_l_min -46 _diffrn_reflns_limit_l_max 51 _diffrn_reflns_theta_min 1.30 _diffrn_reflns_theta_max 30.47 _reflns_number_total 8445 _reflns_number_gt 6459 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'SMART V5.625 (Bruker, 2003)' _computing_cell_refinement 'SMART V5.625 (Bruker, 2003)' _computing_data_reduction 'SAINT V6.28A (Bruker, 2003)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'SHELXTL V6.12(Bruker, 2001)' _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0545P)^2^+43.1372P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 8445 _refine_ls_number_parameters 404 _refine_ls_number_restraints 90 _refine_ls_R_factor_all 0.0492 _refine_ls_R_factor_gt 0.0327 _refine_ls_wR_factor_ref 0.1045 _refine_ls_wR_factor_gt 0.0878 _refine_ls_goodness_of_fit_ref 1.076 _refine_ls_restrained_S_all 1.072 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb1 Sb 0.6250 0.1250 0.010330(8) 0.05063(8) Uani 1 2 d S . . F1A F 0.6884(4) 0.1032(3) -0.0156(3) 0.167(3) Uani 0.50 1 d P A 1 F2A F 0.5536(4) 0.1398(3) 0.0340(3) 0.167(3) Uani 0.50 1 d P A 1 F1B F 0.6694(5) 0.1189(3) -0.0337(2) 0.154(3) Uani 0.50 1 d P A 2 F2B F 0.5889(5) 0.1424(3) 0.05427(18) 0.154(3) Uani 0.50 1 d P A 2 F3 F 0.59392(17) 0.06648(9) 0.01038(10) 0.1291(12) Uani 1 1 d . A . Sb2 Sb 0.1250 0.240218(11) 0.1250 0.05828(9) Uani 1 2 d S . . F4 F 0.18455(15) 0.28527(11) 0.12087(11) 0.1359(13) Uani 1 1 d . . . F5 F 0.11792(16) 0.23890(11) 0.07355(7) 0.1172(11) Uani 1 1 d . . . F6 F 0.18622(11) 0.19565(10) 0.12242(7) 0.0976(8) Uani 1 1 d . . . C1 C 0.13951(11) 0.37014(8) 0.01236(7) 0.0386(5) Uani 1 1 d . B . C2 C 0.19772(12) 0.34944(8) 0.00406(7) 0.0410(5) Uani 1 1 d . B . C3 C 0.22734(11) 0.37493(9) -0.02446(7) 0.0440(5) Uani 1 1 d . B . C4 C 0.18755(12) 0.41177(9) -0.03362(7) 0.0427(5) Uani 1 1 d . B . C5 C 0.13360(10) 0.40875(8) -0.01099(7) 0.0377(5) Uani 1 1 d . B . C6 C 0.09157(15) 0.35263(11) 0.03899(9) 0.0594(7) Uani 1 1 d . . . H6A H 0.0654 0.3305 0.0266 0.089 Uiso 1 1 calc R . . H6B H 0.0660 0.3775 0.0477 0.089 Uiso 1 1 calc R . . H6C H 0.1123 0.3385 0.0599 0.089 Uiso 1 1 calc R . . C7 C 0.22154(17) 0.30645(9) 0.02114(10) 0.0654(9) Uani 1 1 d . . . H7A H 0.1981 0.2810 0.0115 0.098 Uiso 1 1 calc R . . H7B H 0.2166 0.3079 0.0479 0.098 Uiso 1 1 calc R . . H7C H 0.2653 0.3027 0.0151 0.098 Uiso 1 1 calc R . . C8 C 0.28822(14) 0.36388(14) -0.04290(10) 0.0698(10) Uani 1 1 d . . . H8A H 0.2808 0.3441 -0.0639 0.105 Uiso 1 1 calc R . . H8B H 0.3154 0.3488 -0.0253 0.105 Uiso 1 1 calc R . . H8C H 0.3078 0.3916 -0.0514 0.105 Uiso 1 1 calc R . . C9 C 0.19766(18) 0.44602(13) -0.06349(9) 0.0725(10) Uani 1 1 d . . . H9A H 0.1752 0.4369 -0.0856 0.109 Uiso 1 1 calc R . . H9B H 0.2418 0.4481 -0.0690 0.109 Uiso 1 1 calc R . . H9C H 0.1825 0.4753 -0.0552 0.109 Uiso 1 1 calc R . . C10 C 0.07781(13) 0.43897(10) -0.01338(9) 0.0574(7) Uani 1 1 d . . . H10A H 0.0524 0.4301 -0.0344 0.086 Uiso 1 1 calc R . . H10B H 0.0913 0.4701 -0.0165 0.086 Uiso 1 1 calc R . . H10C H 0.0535 0.4363 0.0092 0.086 Uiso 1 1 calc R . . Cr1 Cr 0.215742(15) 0.418060(11) 0.024835(10) 0.03097(8) Uani 1 1 d . . . P11 P 0.1852(10) 0.4380(8) 0.0866(5) 0.069(6) Uani 0.25 1 d PU B 1 P21 P 0.2683(9) 0.3980(4) 0.0819(5) 0.060(4) Uani 0.25 1 d PU B 1 P31 P 0.3231(6) 0.4295(7) 0.0389(5) 0.063(5) Uani 0.25 1 d PU B 1 P41 P 0.2789(10) 0.4869(6) 0.0201(4) 0.071(5) Uani 0.25 1 d PU B 1 P51 P 0.1922(7) 0.4930(6) 0.0489(6) 0.068(5) Uani 0.25 1 d PU B 1 P1 P 0.1982(5) 0.4232(3) 0.0916(3) 0.062(3) Uani 0.50 1 d PU B 2 P2 P 0.2888(4) 0.3967(3) 0.0732(2) 0.056(2) Uani 0.50 1 d PU B 2 P3 P 0.3251(5) 0.4414(4) 0.0306(3) 0.061(3) Uani 0.50 1 d PU B 2 P4 P 0.2568(4) 0.4948(2) 0.0215(2) 0.059(2) Uani 0.50 1 d PU B 2 P5 P 0.1792(3) 0.4839(3) 0.0594(3) 0.061(3) Uani 0.50 1 d PU B 2 P12 P 0.2236(9) 0.4074(5) 0.0920(3) 0.072(4) Uani 0.25 1 d PU B 3 P22 P 0.3118(6) 0.4053(4) 0.0602(4) 0.070(4) Uani 0.25 1 d PU B 3 P32 P 0.3142(6) 0.4610(6) 0.0229(3) 0.072(3) Uani 0.25 1 d PU B 3 P42 P 0.2282(8) 0.4997(3) 0.0294(4) 0.073(4) Uani 0.25 1 d PU B 3 P52 P 0.1725(4) 0.4673(6) 0.0728(4) 0.070(4) Uani 0.25 1 d PU B 3 Cr2 Cr 0.283148(15) 0.478012(11) 0.086369(9) 0.03059(8) Uani 1 1 d . . . C11 C 0.29482(12) 0.49134(8) 0.14600(6) 0.0404(5) Uani 1 1 d . B . C12 C 0.35408(12) 0.48040(8) 0.13084(7) 0.0416(5) Uani 1 1 d . B . C13 C 0.36855(10) 0.51400(8) 0.10377(7) 0.0396(5) Uani 1 1 d . B . C14 C 0.31828(11) 0.54537(7) 0.10254(6) 0.0360(4) Uani 1 1 d . B . C15 C 0.27256(10) 0.53138(8) 0.12870(6) 0.0367(5) Uani 1 1 d . B . C16 C 0.26270(18) 0.46611(12) 0.17672(8) 0.0664(9) Uani 1 1 d . . . H16A H 0.2769 0.4776 0.2005 0.100 Uiso 1 1 calc R B . H16B H 0.2725 0.4341 0.1748 0.100 Uiso 1 1 calc R . . H16C H 0.2180 0.4703 0.1747 0.100 Uiso 1 1 calc R . . C17 C 0.39608(17) 0.44255(11) 0.14279(11) 0.0728(10) Uani 1 1 d . . . H17A H 0.4223 0.4527 0.1631 0.109 Uiso 1 1 calc R B . H17B H 0.4220 0.4333 0.1221 0.109 Uiso 1 1 calc R . . H17C H 0.3711 0.4171 0.1510 0.109 Uiso 1 1 calc R . . C18 C 0.42770(13) 0.51787(13) 0.08207(9) 0.0661(9) Uani 1 1 d . . . H18A H 0.4559 0.5385 0.0946 0.099 Uiso 1 1 calc R B . H18B H 0.4185 0.5293 0.0574 0.099 Uiso 1 1 calc R . . H18C H 0.4471 0.4883 0.0801 0.099 Uiso 1 1 calc R . . C19 C 0.31690(17) 0.58698(9) 0.07903(8) 0.0576(7) Uani 1 1 d . . . H19A H 0.3366 0.6117 0.0923 0.086 Uiso 1 1 calc R B . H19B H 0.2740 0.5948 0.0735 0.086 Uiso 1 1 calc R . . H19C H 0.3393 0.5814 0.0561 0.086 Uiso 1 1 calc R . . C20 C 0.21323(12) 0.55569(10) 0.13773(9) 0.0563(7) Uani 1 1 d . . . H20A H 0.2206 0.5768 0.1579 0.084 Uiso 1 1 calc R B . H20B H 0.1817 0.5339 0.1451 0.084 Uiso 1 1 calc R . . H20C H 0.1990 0.5721 0.1160 0.084 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.04124(13) 0.06276(16) 0.04789(15) 0.000 0.000 0.00370(11) F1A 0.107(3) 0.175(5) 0.219(8) -0.037(5) 0.097(4) 0.025(3) F2A 0.107(3) 0.175(5) 0.219(8) -0.037(5) 0.097(4) 0.025(3) F1B 0.259(9) 0.115(4) 0.088(3) -0.013(3) 0.096(4) -0.017(4) F2B 0.259(9) 0.115(4) 0.088(3) -0.013(3) 0.096(4) -0.017(4) F3 0.152(3) 0.0798(17) 0.156(3) 0.0137(18) -0.042(2) -0.0346(18) Sb2 0.04634(14) 0.07061(19) 0.05789(18) 0.000 0.00930(12) 0.000 F4 0.109(2) 0.119(2) 0.179(3) -0.038(2) 0.035(2) -0.0572(19) F5 0.158(3) 0.135(2) 0.0590(14) 0.0253(15) -0.0025(15) -0.031(2) F6 0.0752(14) 0.117(2) 0.1010(18) -0.0296(15) 0.0002(13) 0.0275(14) C1 0.0391(11) 0.0371(11) 0.0395(12) -0.0054(9) -0.0053(9) -0.0022(9) C2 0.0457(12) 0.0348(11) 0.0425(12) -0.0105(9) -0.0116(10) 0.0064(9) C3 0.0373(11) 0.0576(14) 0.0370(12) -0.0167(11) -0.0031(9) 0.0064(10) C4 0.0446(12) 0.0535(13) 0.0300(11) 0.0003(10) -0.0062(9) -0.0017(10) C5 0.0352(10) 0.0402(11) 0.0376(11) -0.0036(9) -0.0103(9) 0.0050(8) C6 0.0573(17) 0.0638(18) 0.0570(17) -0.0011(14) 0.0067(14) -0.0178(14) C7 0.084(2) 0.0374(13) 0.075(2) -0.0060(13) -0.0264(18) 0.0172(14) C8 0.0449(14) 0.104(3) 0.0607(19) -0.0377(19) 0.0057(13) 0.0094(16) C9 0.086(2) 0.089(2) 0.0416(16) 0.0230(16) -0.0088(16) -0.011(2) C10 0.0464(14) 0.0594(16) 0.0664(19) -0.0078(14) -0.0196(13) 0.0187(12) Cr1 0.03100(16) 0.03205(16) 0.02987(17) -0.00167(13) -0.00319(13) 0.00390(12) P11 0.060(8) 0.109(16) 0.038(7) -0.018(7) 0.013(5) -0.045(9) P21 0.101(12) 0.028(3) 0.053(7) 0.002(3) -0.038(7) 0.003(5) P31 0.026(2) 0.091(12) 0.072(10) -0.047(9) 0.010(4) -0.006(5) P41 0.103(12) 0.072(10) 0.037(2) 0.015(5) -0.014(7) -0.042(8) P51 0.059(9) 0.051(6) 0.093(13) -0.032(7) -0.040(7) 0.031(7) P1 0.073(6) 0.080(7) 0.032(2) -0.004(3) 0.006(3) -0.042(4) P2 0.069(5) 0.0379(12) 0.062(5) -0.008(2) -0.033(3) 0.018(3) P3 0.0417(15) 0.086(6) 0.055(4) -0.028(4) 0.0200(17) -0.021(2) P4 0.085(6) 0.041(3) 0.050(2) 0.0152(17) -0.025(4) -0.014(3) P5 0.034(3) 0.074(6) 0.075(6) -0.037(4) -0.009(3) 0.017(3) P12 0.122(11) 0.060(6) 0.035(3) 0.004(4) -0.013(7) -0.047(6) P22 0.052(5) 0.069(6) 0.089(9) -0.042(5) -0.035(5) 0.033(4) P32 0.076(7) 0.096(8) 0.043(4) -0.020(5) 0.015(4) -0.043(6) P42 0.098(9) 0.0361(18) 0.085(9) 0.002(5) -0.055(7) 0.006(6) P52 0.0300(17) 0.103(10) 0.076(9) -0.054(6) 0.005(4) -0.002(5) Cr2 0.03052(15) 0.03103(15) 0.03023(17) -0.00214(12) -0.00038(12) -0.00026(12) C11 0.0512(13) 0.0411(11) 0.0288(11) -0.0006(9) -0.0024(10) -0.0136(10) C12 0.0446(12) 0.0387(11) 0.0416(13) -0.0053(9) -0.0134(10) -0.0001(9) C13 0.0320(10) 0.0476(12) 0.0393(12) -0.0108(10) 0.0006(9) -0.0055(9) C14 0.0406(11) 0.0336(10) 0.0338(11) -0.0019(8) 0.0010(9) -0.0069(8) C15 0.0358(10) 0.0389(11) 0.0355(11) -0.0095(9) 0.0037(8) -0.0042(8) C16 0.089(2) 0.073(2) 0.0370(14) 0.0080(13) -0.0014(14) -0.0393(18) C17 0.080(2) 0.0517(16) 0.087(2) -0.0118(16) -0.045(2) 0.0185(15) C18 0.0374(13) 0.096(2) 0.0646(19) -0.0246(18) 0.0132(13) -0.0141(14) C19 0.081(2) 0.0390(12) 0.0532(16) 0.0090(11) -0.0045(15) -0.0127(13) C20 0.0413(12) 0.0598(16) 0.0677(18) -0.0279(14) 0.0093(12) 0.0018(11) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb1 F1A 1.772(6) . ? Sb1 F1A 1.772(6) 14_545 ? Sb1 F2A 1.807(6) . ? Sb1 F2A 1.807(6) 14_545 ? Sb1 F2B 1.836(6) . ? Sb1 F2B 1.836(6) 14_545 ? Sb1 F3 1.854(3) 14_545 ? Sb1 F3 1.854(3) . ? Sb1 F1B 1.860(6) . ? Sb1 F1B 1.860(6) 14_545 ? Sb2 F4 1.851(3) . ? Sb2 F4 1.851(3) 11_454 ? Sb2 F5 1.861(3) . ? Sb2 F5 1.861(3) 11_454 ? Sb2 F6 1.862(2) 11_454 ? Sb2 F6 1.862(2) . ? C1 C2 1.422(3) . ? C1 C5 1.424(3) . ? C1 C6 1.499(4) . ? C1 Cr1 2.209(2) . ? C2 C3 1.424(4) . ? C2 C7 1.501(4) . ? C2 Cr1 2.196(2) . ? C3 C4 1.422(4) . ? C3 C8 1.501(4) . ? C3 Cr1 2.201(2) . ? C4 C5 1.418(4) . ? C4 C9 1.493(4) . ? C4 Cr1 2.199(2) . ? C5 C10 1.495(3) . ? C5 Cr1 2.201(2) . ? C6 H6A 0.9700 . ? C6 H6B 0.9700 . ? C6 H6C 0.9700 . ? C7 H7A 0.9700 . ? C7 H7B 0.9700 . ? C7 H7C 0.9700 . ? C8 H8A 0.9700 . ? C8 H8B 0.9700 . ? C8 H8C 0.9700 . ? C9 H9A 0.9700 . ? C9 H9B 0.9700 . ? C9 H9C 0.9700 . ? C10 H10A 0.9700 . ? C10 H10B 0.9700 . ? C10 H10C 0.9700 . ? Cr1 P31 2.382(13) . ? Cr1 P11 2.39(2) . ? Cr1 P21 2.420(15) . ? Cr1 P2 2.426(7) . ? Cr1 P42 2.433(9) . ? Cr1 P51 2.433(15) . ? Cr1 P4 2.437(7) . ? P11 P51 2.12(2) . ? P11 P21 2.14(2) . ? P11 Cr2 2.411(19) . ? P21 P31 2.157(19) . ? P21 Cr2 2.390(12) . ? P31 P41 2.06(2) . ? P31 Cr2 2.390(16) . ? P41 P51 2.137(18) . ? P41 Cr2 2.405(15) . ? P51 Cr2 2.412(15) . ? P1 P5 2.176(10) . ? P1 P2 2.197(11) . ? P1 Cr2 2.445(9) . ? P2 P3 2.170(10) . ? P2 Cr2 2.453(7) . ? P3 P4 2.178(13) . ? P3 Cr2 2.453(10) . ? P4 P5 2.176(9) . ? P4 Cr2 2.456(8) . ? P5 Cr2 2.437(8) . ? P12 P52 2.193(13) . ? P12 P22 2.212(12) . ? P12 Cr2 2.454(9) . ? P22 P32 2.125(12) . ? P22 Cr2 2.425(7) . ? P32 P42 2.184(12) . ? P32 Cr2 2.436(9) . ? P42 P52 2.188(13) . ? P42 Cr2 2.451(9) . ? P52 Cr2 2.444(9) . ? Cr2 C11 2.199(2) . ? Cr2 C15 2.206(2) . ? Cr2 C14 2.207(2) . ? Cr2 C13 2.209(2) . ? Cr2 C12 2.211(2) . ? C11 C15 1.420(3) . ? C11 C12 1.421(4) . ? C11 C16 1.502(4) . ? C12 C13 1.426(4) . ? C12 C17 1.499(4) . ? C13 C14 1.423(3) . ? C13 C18 1.495(3) . ? C14 C15 1.422(3) . ? C14 C19 1.493(3) . ? C15 C20 1.497(3) . ? C16 H16A 0.9700 . ? C16 H16B 0.9700 . ? C16 H16C 0.9700 . ? C17 H17A 0.9700 . ? C17 H17B 0.9700 . ? C17 H17C 0.9700 . ? C18 H18A 0.9700 . ? C18 H18B 0.9700 . ? C18 H18C 0.9700 . ? C19 H19A 0.9700 . ? C19 H19B 0.9700 . ? C19 H19C 0.9700 . ? C20 H20A 0.9700 . ? C20 H20B 0.9700 . ? C20 H20C 0.9700 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F1A Sb1 F1A 116.4(8) . 14_545 ? F1A Sb1 F2A 171.1(5) . . ? F1A Sb1 F2A 60.6(5) 14_545 . ? F1A Sb1 F2A 60.6(5) . 14_545 ? F1A Sb1 F2A 171.1(5) 14_545 14_545 ? F2A Sb1 F2A 123.7(8) . 14_545 ? F1A Sb1 F2B 151.7(5) . . ? F1A Sb1 F2B 91.7(5) 14_545 . ? F2A Sb1 F2B 33.7(4) . . ? F2A Sb1 F2B 91.1(6) 14_545 . ? F1A Sb1 F2B 91.7(5) . 14_545 ? F1A Sb1 F2B 151.7(5) 14_545 14_545 ? F2A Sb1 F2B 91.1(6) . 14_545 ? F2A Sb1 F2B 33.7(4) 14_545 14_545 ? F2B Sb1 F2B 60.8(6) . 14_545 ? F1A Sb1 F3 93.7(3) . 14_545 ? F1A Sb1 F3 86.4(4) 14_545 14_545 ? F2A Sb1 F3 94.5(3) . 14_545 ? F2A Sb1 F3 85.5(3) 14_545 14_545 ? F2B Sb1 F3 83.7(3) . 14_545 ? F2B Sb1 F3 96.2(3) 14_545 14_545 ? F1A Sb1 F3 86.4(4) . . ? F1A Sb1 F3 93.7(3) 14_545 . ? F2A Sb1 F3 85.5(3) . . ? F2A Sb1 F3 94.5(3) 14_545 . ? F2B Sb1 F3 96.2(3) . . ? F2B Sb1 F3 83.7(3) 14_545 . ? F3 Sb1 F3 179.9(2) 14_545 . ? F1A Sb1 F1B 28.6(4) . . ? F1A Sb1 F1B 88.8(5) 14_545 . ? F2A Sb1 F1B 149.3(5) . . ? F2A Sb1 F1B 86.9(5) 14_545 . ? F2B Sb1 F1B 168.3(4) . . ? F2B Sb1 F1B 119.6(5) 14_545 . ? F3 Sb1 F1B 84.7(3) 14_545 . ? F3 Sb1 F1B 95.4(3) . . ? F1A Sb1 F1B 88.8(5) . 14_545 ? F1A Sb1 F1B 28.6(4) 14_545 14_545 ? F2A Sb1 F1B 86.9(5) . 14_545 ? F2A Sb1 F1B 149.3(5) 14_545 14_545 ? F2B Sb1 F1B 119.5(5) . 14_545 ? F2B Sb1 F1B 168.3(4) 14_545 14_545 ? F3 Sb1 F1B 95.4(3) 14_545 14_545 ? F3 Sb1 F1B 84.7(3) . 14_545 ? F1B Sb1 F1B 62.8(7) . 14_545 ? F4 Sb2 F4 88.0(2) . 11_454 ? F4 Sb2 F5 89.50(15) . . ? F4 Sb2 F5 92.23(16) 11_454 . ? F4 Sb2 F5 92.23(16) . 11_454 ? F4 Sb2 F5 89.49(15) 11_454 11_454 ? F5 Sb2 F5 177.6(2) . 11_454 ? F4 Sb2 F6 177.93(16) . 11_454 ? F4 Sb2 F6 91.04(15) 11_454 11_454 ? F5 Sb2 F6 88.71(13) . 11_454 ? F5 Sb2 F6 89.60(14) 11_454 11_454 ? F4 Sb2 F6 91.05(15) . . ? F4 Sb2 F6 177.93(16) 11_454 . ? F5 Sb2 F6 89.60(14) . . ? F5 Sb2 F6 88.71(12) 11_454 . ? F6 Sb2 F6 89.96(18) 11_454 . ? C2 C1 C5 107.4(2) . . ? C2 C1 C6 126.0(2) . . ? C5 C1 C6 126.5(2) . . ? C2 C1 Cr1 70.67(13) . . ? C5 C1 Cr1 70.88(13) . . ? C6 C1 Cr1 126.78(18) . . ? C1 C2 C3 108.4(2) . . ? C1 C2 C7 125.2(3) . . ? C3 C2 C7 126.3(3) . . ? C1 C2 Cr1 71.67(13) . . ? C3 C2 Cr1 71.28(14) . . ? C7 C2 Cr1 125.58(18) . . ? C4 C3 C2 107.7(2) . . ? C4 C3 C8 125.9(3) . . ? C2 C3 C8 126.3(3) . . ? C4 C3 Cr1 71.10(14) . . ? C2 C3 Cr1 70.93(13) . . ? C8 C3 Cr1 125.56(19) . . ? C5 C4 C3 107.9(2) . . ? C5 C4 C9 125.1(3) . . ? C3 C4 C9 126.8(3) . . ? C5 C4 Cr1 71.28(13) . . ? C3 C4 Cr1 71.19(13) . . ? C9 C4 Cr1 126.4(2) . . ? C4 C5 C1 108.5(2) . . ? C4 C5 C10 125.6(2) . . ? C1 C5 C10 125.7(2) . . ? C4 C5 Cr1 71.12(13) . . ? C1 C5 Cr1 71.47(13) . . ? C10 C5 Cr1 126.83(18) . . ? C1 C6 H6A 109.5 . . ? C1 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C1 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C2 Cr1 C4 63.06(10) . . ? C2 Cr1 C3 37.79(10) . . ? C4 Cr1 C3 37.71(10) . . ? C2 Cr1 C5 62.86(9) . . ? C4 Cr1 C5 37.60(9) . . ? C3 Cr1 C5 62.91(9) . . ? C2 Cr1 C1 37.66(9) . . ? C4 Cr1 C1 63.09(9) . . ? C3 Cr1 C1 63.13(9) . . ? C5 Cr1 C1 37.66(9) . . ? C2 Cr1 P31 112.0(5) . . ? C4 Cr1 P31 118.8(4) . . ? C3 Cr1 P31 98.3(4) . . ? C5 Cr1 P31 156.4(4) . . ? C1 Cr1 P31 148.2(5) . . ? C2 Cr1 P11 119.7(5) . . ? C4 Cr1 P11 146.7(6) . . ? C3 Cr1 P11 157.5(5) . . ? C5 Cr1 P11 110.9(5) . . ? C1 Cr1 P11 98.3(5) . . ? P31 Cr1 P11 91.8(6) . . ? C2 Cr1 P21 98.4(3) . . ? C4 Cr1 P21 157.2(3) . . ? C3 Cr1 P21 119.5(3) . . ? C5 Cr1 P21 147.2(4) . . ? C1 Cr1 P21 111.2(4) . . ? P31 Cr1 P21 53.4(5) . . ? P11 Cr1 P21 52.9(5) . . ? C2 Cr1 P2 96.78(19) . . ? C4 Cr1 P2 147.5(2) . . ? C3 Cr1 P2 110.84(19) . . ? C5 Cr1 P2 154.9(2) . . ? C1 Cr1 P2 117.2(2) . . ? P31 Cr1 P2 42.2(5) . . ? P11 Cr1 P2 64.7(5) . . ? P21 Cr1 P2 12.9(4) . . ? C2 Cr1 P42 163.4(3) . . ? C4 Cr1 P42 100.3(3) . . ? C3 Cr1 P42 128.1(4) . . ? C5 Cr1 P42 104.6(3) . . ? C1 Cr1 P42 137.0(4) . . ? P31 Cr1 P42 74.8(5) . . ? P11 Cr1 P42 73.9(5) . . ? P21 Cr1 P42 97.6(4) . . ? P2 Cr1 P42 97.9(3) . . ? C2 Cr1 P51 157.9(4) . . ? C4 Cr1 P51 111.2(5) . . ? C3 Cr1 P51 147.1(5) . . ? C5 Cr1 P51 99.0(4) . . ? C1 Cr1 P51 120.2(4) . . ? P31 Cr1 P51 89.7(6) . . ? P11 Cr1 P51 52.2(5) . . ? P21 Cr1 P51 90.9(5) . . ? P2 Cr1 P51 96.6(4) . . ? P42 Cr1 P51 25.2(4) . . ? C2 Cr1 P4 155.1(2) . . ? C4 Cr1 P4 97.5(2) . . ? C3 Cr1 P4 117.3(2) . . ? C5 Cr1 P4 112.11(19) . . ? C1 Cr1 P4 148.7(2) . . ? P31 Cr1 P4 61.9(5) . . ? P11 Cr1 P4 85.2(5) . . ? P21 Cr1 P4 95.8(4) . . ? P2 Cr1 P4 92.6(2) . . ? P42 Cr1 P4 16.3(3) . . ? P51 Cr1 P4 40.9(5) . . ? P51 P11 P21 108.3(8) . . ? P51 P11 Cr1 64.9(6) . . ? P21 P11 Cr1 64.2(7) . . ? P51 P11 Cr2 63.9(6) . . ? P21 P11 Cr2 63.0(6) . . ? Cr1 P11 Cr2 83.1(6) . . ? P11 P21 P31 105.8(7) . . ? P11 P21 Cr2 64.0(5) . . ? P31 P21 Cr2 63.2(6) . . ? P11 P21 Cr1 62.9(6) . . ? P31 P21 Cr1 62.4(5) . . ? Cr2 P21 Cr1 82.9(4) . . ? P41 P31 P21 109.9(8) . . ? P41 P31 Cr1 66.5(7) . . ? P21 P31 Cr1 64.2(5) . . ? P41 P31 Cr2 64.9(7) . . ? P21 P31 Cr2 63.2(5) . . ? Cr1 P31 Cr2 83.7(4) . . ? P31 P41 P51 108.1(8) . . ? P31 P41 Cr2 64.2(5) . . ? P51 P41 Cr2 63.8(6) . . ? P31 P41 Cr1 63.1(6) . . ? P51 P41 Cr1 63.6(6) . . ? Cr2 P41 Cr1 82.0(5) . . ? P11 P51 P41 107.9(8) . . ? P11 P51 Cr2 63.9(7) . . ? P41 P51 Cr2 63.5(5) . . ? P11 P51 Cr1 62.9(7) . . ? P41 P51 Cr1 64.4(6) . . ? Cr2 P51 Cr1 82.2(4) . . ? P5 P1 P2 107.3(5) . . ? P5 P1 Cr1 63.5(3) . . ? P2 P1 Cr1 62.8(4) . . ? P5 P1 Cr2 63.4(3) . . ? P2 P1 Cr2 63.5(3) . . ? Cr1 P1 Cr2 81.4(3) . . ? P3 P2 P1 108.3(5) . . ? P3 P2 Cr1 64.2(3) . . ? P1 P2 Cr1 63.5(3) . . ? P3 P2 Cr2 63.8(4) . . ? P1 P2 Cr2 63.2(3) . . ? Cr1 P2 Cr2 81.5(2) . . ? P2 P3 P4 107.9(5) . . ? P2 P3 Cr1 63.0(3) . . ? P4 P3 Cr1 63.2(3) . . ? P2 P3 Cr2 63.7(3) . . ? P4 P3 Cr2 63.7(4) . . ? Cr1 P3 Cr2 81.0(3) . . ? P5 P4 P3 108.2(4) . . ? P5 P4 Cr1 63.6(3) . . ? P3 P4 Cr1 63.9(3) . . ? P5 P4 Cr2 63.2(3) . . ? P3 P4 Cr2 63.6(3) . . ? Cr1 P4 Cr2 81.2(2) . . ? P4 P5 P1 108.3(5) . . ? P4 P5 Cr2 64.0(2) . . ? P1 P5 Cr2 63.7(4) . . ? P4 P5 Cr1 63.4(2) . . ? P1 P5 Cr1 63.5(4) . . ? Cr2 P5 Cr1 81.5(2) . . ? P52 P12 P22 106.7(5) . . ? P52 P12 Cr1 63.3(4) . . ? P22 P12 Cr1 63.3(3) . . ? P52 P12 Cr2 63.2(3) . . ? P22 P12 Cr2 62.4(3) . . ? Cr1 P12 Cr2 81.1(3) . . ? P32 P22 P12 109.1(5) . . ? P32 P22 Cr2 64.4(3) . . ? P12 P22 Cr2 63.7(3) . . ? P32 P22 Cr1 64.7(4) . . ? P12 P22 Cr1 63.0(3) . . ? Cr2 P22 Cr1 81.6(2) . . ? P22 P32 P42 108.4(6) . . ? P22 P32 Cr2 63.8(3) . . ? P42 P32 Cr2 63.8(4) . . ? P22 P32 Cr1 64.0(3) . . ? P42 P32 Cr1 62.8(4) . . ? Cr2 P32 Cr1 81.1(3) . . ? P32 P42 P52 108.1(5) . . ? P32 P42 Cr1 64.3(3) . . ? P52 P42 Cr1 63.6(4) . . ? P32 P42 Cr2 63.1(3) . . ? P52 P42 Cr2 63.3(4) . . ? Cr1 P42 Cr2 81.4(2) . . ? P42 P52 P12 107.7(5) . . ? P42 P52 Cr2 63.6(3) . . ? P12 P52 Cr2 63.6(4) . . ? P42 P52 Cr1 63.1(3) . . ? P12 P52 Cr1 63.4(4) . . ? Cr2 P52 Cr1 81.3(3) . . ? C11 Cr2 C15 37.61(9) . . ? C11 Cr2 C14 62.71(8) . . ? C15 Cr2 C14 37.59(8) . . ? C11 Cr2 C13 62.74(9) . . ? C15 Cr2 C13 62.92(8) . . ? C14 Cr2 C13 37.59(9) . . ? C11 Cr2 C12 37.59(9) . . ? C15 Cr2 C12 63.05(9) . . ? C14 Cr2 C12 62.93(9) . . ? C13 Cr2 C12 37.65(9) . . ? C11 Cr2 P21 104.9(4) . . ? C15 Cr2 P21 137.7(5) . . ? C14 Cr2 P21 162.8(4) . . ? C13 Cr2 P21 127.3(4) . . ? C12 Cr2 P21 99.9(4) . . ? C11 Cr2 P31 140.0(5) . . ? C15 Cr2 P31 163.8(3) . . ? C14 Cr2 P31 127.4(4) . . ? C13 Cr2 P31 101.2(3) . . ? C12 Cr2 P31 106.9(4) . . ? P21 Cr2 P31 53.6(5) . . ? C11 Cr2 P41 162.9(4) . . ? C15 Cr2 P41 127.2(5) . . ? C14 Cr2 P41 100.2(4) . . ? C13 Cr2 P41 105.1(5) . . ? C12 Cr2 P41 138.0(5) . . ? P21 Cr2 P41 92.1(6) . . ? P31 Cr2 P41 50.8(6) . . ? C11 Cr2 P11 100.6(4) . . ? C15 Cr2 P11 105.0(6) . . ? C14 Cr2 P11 137.7(6) . . ? C13 Cr2 P11 163.3(4) . . ? C12 Cr2 P11 127.8(4) . . ? P21 Cr2 P11 53.0(5) . . ? P31 Cr2 P11 91.2(6) . . ? P41 Cr2 P11 91.3(6) . . ? C11 Cr2 P51 127.3(4) . . ? C15 Cr2 P51 99.9(4) . . ? C14 Cr2 P51 104.9(4) . . ? C13 Cr2 P51 137.8(5) . . ? C12 Cr2 P51 162.9(4) . . ? P21 Cr2 P51 92.1(5) . . ? P31 Cr2 P51 90.0(5) . . ? P41 Cr2 P51 52.7(5) . . ? P11 Cr2 P51 52.2(5) . . ? C11 Cr2 P22 120.7(4) . . ? C15 Cr2 P22 158.2(3) . . ? C14 Cr2 P22 144.6(4) . . ? C13 Cr2 P22 109.1(3) . . ? C12 Cr2 P22 97.82(19) . . ? P21 Cr2 P22 29.8(4) . . ? P31 Cr2 P22 25.8(5) . . ? P41 Cr2 P22 73.7(5) . . ? P11 Cr2 P22 77.7(6) . . ? P51 Cr2 P22 98.6(4) . . ? C11 Cr2 P32 157.5(3) . . ? C15 Cr2 P32 145.6(4) . . ? C14 Cr2 P32 109.9(3) . . ? C13 Cr2 P32 98.0(2) . . ? C12 Cr2 P32 120.0(3) . . ? P21 Cr2 P32 76.7(4) . . ? P31 Cr2 P32 26.6(6) . . ? P41 Cr2 P32 25.8(4) . . ? P11 Cr2 P32 98.0(5) . . ? P51 Cr2 P32 74.6(4) . . ? P22 Cr2 P32 51.8(3) . . ? C15 C11 C12 108.8(2) . . ? C15 C11 C16 125.7(3) . . ? C12 C11 C16 125.5(3) . . ? C15 C11 Cr2 71.46(13) . . ? C12 C11 Cr2 71.65(13) . . ? C16 C11 Cr2 125.39(17) . . ? C11 C12 C13 107.4(2) . . ? C11 C12 C17 126.6(3) . . ? C13 C12 C17 125.8(3) . . ? C11 C12 Cr2 70.76(13) . . ? C13 C12 Cr2 71.11(13) . . ? C17 C12 Cr2 126.72(18) . . ? C14 C13 C12 108.1(2) . . ? C14 C13 C18 125.2(3) . . ? C12 C13 C18 126.6(3) . . ? C14 C13 Cr2 71.13(12) . . ? C12 C13 Cr2 71.24(13) . . ? C18 C13 Cr2 126.31(18) . . ? C15 C14 C13 108.2(2) . . ? C15 C14 C19 127.0(2) . . ? C13 C14 C19 124.7(2) . . ? C15 C14 Cr2 71.17(12) . . ? C13 C14 Cr2 71.29(13) . . ? C19 C14 Cr2 125.88(17) . . ? C11 C15 C14 107.6(2) . . ? C11 C15 C20 126.2(2) . . ? C14 C15 C20 126.2(2) . . ? C11 C15 Cr2 70.93(13) . . ? C14 C15 Cr2 71.24(12) . . ? C20 C15 Cr2 125.52(17) . . ? C11 C16 H16A 109.5 . . ? C11 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C11 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 C1 C2 C3 -0.5(3) . . . . ? C6 C1 C2 C3 175.9(2) . . . . ? Cr1 C1 C2 C3 -62.19(16) . . . . ? C5 C1 C2 C7 -177.2(2) . . . . ? C6 C1 C2 C7 -0.9(4) . . . . ? Cr1 C1 C2 C7 121.1(3) . . . . ? C5 C1 C2 Cr1 61.73(16) . . . . ? C6 C1 C2 Cr1 -122.0(3) . . . . ? C1 C2 C3 C4 0.5(3) . . . . ? C7 C2 C3 C4 177.2(2) . . . . ? Cr1 C2 C3 C4 -61.93(17) . . . . ? C1 C2 C3 C8 -176.9(2) . . . . ? C7 C2 C3 C8 -0.2(4) . . . . ? Cr1 C2 C3 C8 120.6(3) . . . . ? C1 C2 C3 Cr1 62.43(16) . . . . ? C7 C2 C3 Cr1 -120.9(3) . . . . ? C2 C3 C4 C5 -0.4(3) . . . . ? C8 C3 C4 C5 177.1(2) . . . . ? Cr1 C3 C4 C5 -62.18(17) . . . . ? C2 C3 C4 C9 -176.3(3) . . . . ? C8 C3 C4 C9 1.1(4) . . . . ? Cr1 C3 C4 C9 121.8(3) . . . . ? C2 C3 C4 Cr1 61.82(16) . . . . ? C8 C3 C4 Cr1 -120.7(3) . . . . ? C3 C4 C5 C1 0.1(3) . . . . ? C9 C4 C5 C1 176.1(3) . . . . ? Cr1 C4 C5 C1 -62.05(16) . . . . ? C3 C4 C5 C10 -175.6(2) . . . . ? C9 C4 C5 C10 0.5(4) . . . . ? Cr1 C4 C5 C10 122.3(2) . . . . ? C3 C4 C5 Cr1 62.12(17) . . . . ? C9 C4 C5 Cr1 -121.8(3) . . . . ? C2 C1 C5 C4 0.2(3) . . . . ? C6 C1 C5 C4 -176.1(2) . . . . ? Cr1 C1 C5 C4 61.83(16) . . . . ? C2 C1 C5 C10 175.9(2) . . . . ? C6 C1 C5 C10 -0.4(4) . . . . ? Cr1 C1 C5 C10 -122.5(2) . . . . ? C2 C1 C5 Cr1 -61.59(16) . . . . ? C6 C1 C5 Cr1 122.1(3) . . . . ? C1 C2 Cr1 C4 -80.07(16) . . . . ? C3 C2 Cr1 C4 37.55(14) . . . . ? C7 C2 Cr1 C4 159.3(3) . . . . ? C1 C2 Cr1 C3 -117.6(2) . . . . ? C7 C2 Cr1 C3 121.7(3) . . . . ? C1 C2 Cr1 C5 -37.64(14) . . . . ? C3 C2 Cr1 C5 79.98(15) . . . . ? C7 C2 Cr1 C5 -158.3(3) . . . . ? C3 C2 Cr1 C1 117.6(2) . . . . ? C7 C2 Cr1 C1 -120.6(3) . . . . ? C1 C2 Cr1 P31 167.7(5) . . . . ? C3 C2 Cr1 P31 -74.7(5) . . . . ? C7 C2 Cr1 P31 47.1(6) . . . . ? C1 C2 Cr1 P11 62.1(7) . . . . ? C3 C2 Cr1 P11 179.7(6) . . . . ? C7 C2 Cr1 P11 -58.6(7) . . . . ? C1 C2 Cr1 P21 113.9(5) . . . . ? C3 C2 Cr1 P21 -128.4(5) . . . . ? C7 C2 Cr1 P21 -6.7(6) . . . . ? C1 C2 Cr1 P2 126.8(3) . . . . ? C3 C2 Cr1 P2 -115.6(3) . . . . ? C7 C2 Cr1 P2 6.2(4) . . . . ? C1 C2 Cr1 P42 -80.9(17) . . . . ? C3 C2 Cr1 P42 36.8(17) . . . . ? C7 C2 Cr1 P42 158.5(17) . . . . ? C1 C2 Cr1 P51 0.1(14) . . . . ? C3 C2 Cr1 P51 117.7(14) . . . . ? C7 C2 Cr1 P51 -120.6(14) . . . . ? C1 C2 Cr1 P4 -122.0(5) . . . . ? C3 C2 Cr1 P4 -4.3(5) . . . . ? C7 C2 Cr1 P4 117.4(5) . . . . ? C5 C4 Cr1 C2 79.70(15) . . . . ? C3 C4 Cr1 C2 -37.63(15) . . . . ? C9 C4 Cr1 C2 -160.0(3) . . . . ? C5 C4 Cr1 C3 117.3(2) . . . . ? C9 C4 Cr1 C3 -122.4(3) . . . . ? C3 C4 Cr1 C5 -117.3(2) . . . . ? C9 C4 Cr1 C5 120.3(3) . . . . ? C5 C4 Cr1 C1 37.25(14) . . . . ? C3 C4 Cr1 C1 -80.08(16) . . . . ? C9 C4 Cr1 C1 157.6(3) . . . . ? C5 C4 Cr1 P31 -178.8(6) . . . . ? C3 C4 Cr1 P31 63.9(6) . . . . ? C9 C4 Cr1 P31 -58.5(7) . . . . ? C5 C4 Cr1 P11 -24.2(9) . . . . ? C3 C4 Cr1 P11 -141.5(9) . . . . ? C9 C4 Cr1 P11 96.2(9) . . . . ? C5 C4 Cr1 P21 117.9(12) . . . . ? C3 C4 Cr1 P21 0.6(12) . . . . ? C9 C4 Cr1 P21 -121.8(12) . . . . ? C5 C4 Cr1 P2 136.3(4) . . . . ? C3 C4 Cr1 P2 19.0(5) . . . . ? C9 C4 Cr1 P2 -103.4(5) . . . . ? C5 C4 Cr1 P42 -100.5(5) . . . . ? C3 C4 Cr1 P42 142.1(5) . . . . ? C9 C4 Cr1 P42 19.8(6) . . . . ? C5 C4 Cr1 P51 -76.8(5) . . . . ? C3 C4 Cr1 P51 165.8(5) . . . . ? C9 C4 Cr1 P51 43.5(6) . . . . ? C5 C4 Cr1 P4 -116.8(3) . . . . ? C3 C4 Cr1 P4 125.9(3) . . . . ? C9 C4 Cr1 P4 3.5(4) . . . . ? C4 C3 Cr1 C2 117.3(2) . . . . ? C8 C3 Cr1 C2 -121.6(3) . . . . ? C2 C3 Cr1 C4 -117.3(2) . . . . ? C8 C3 Cr1 C4 121.1(4) . . . . ? C4 C3 Cr1 C5 37.51(15) . . . . ? C2 C3 Cr1 C5 -79.83(15) . . . . ? C8 C3 Cr1 C5 158.6(3) . . . . ? C4 C3 Cr1 C1 79.97(16) . . . . ? C2 C3 Cr1 C1 -37.37(14) . . . . ? C8 C3 Cr1 C1 -158.9(3) . . . . ? C4 C3 Cr1 P31 -127.3(6) . . . . ? C2 C3 Cr1 P31 115.3(6) . . . . ? C8 C3 Cr1 P31 -6.3(6) . . . . ? C4 C3 Cr1 P11 116.7(15) . . . . ? C2 C3 Cr1 P11 -0.6(15) . . . . ? C8 C3 Cr1 P11 -122.2(15) . . . . ? C4 C3 Cr1 P21 -179.8(5) . . . . ? C2 C3 Cr1 P21 62.9(5) . . . . ? C8 C3 Cr1 P21 -58.7(6) . . . . ? C4 C3 Cr1 P2 -169.2(3) . . . . ? C2 C3 Cr1 P2 73.5(3) . . . . ? C8 C3 Cr1 P2 -48.1(4) . . . . ? C4 C3 Cr1 P42 -50.1(5) . . . . ? C2 C3 Cr1 P42 -167.5(5) . . . . ? C8 C3 Cr1 P42 71.0(5) . . . . ? C4 C3 Cr1 P51 -24.8(8) . . . . ? C2 C3 Cr1 P51 -142.1(8) . . . . ? C8 C3 Cr1 P51 96.3(8) . . . . ? C4 C3 Cr1 P4 -64.7(3) . . . . ? C2 C3 Cr1 P4 177.9(2) . . . . ? C8 C3 Cr1 P4 56.4(4) . . . . ? C4 C5 Cr1 C2 -80.29(16) . . . . ? C1 C5 Cr1 C2 37.65(14) . . . . ? C10 C5 Cr1 C2 158.9(3) . . . . ? C1 C5 Cr1 C4 117.9(2) . . . . ? C10 C5 Cr1 C4 -120.8(3) . . . . ? C4 C5 Cr1 C3 -37.62(15) . . . . ? C1 C5 Cr1 C3 80.32(15) . . . . ? C10 C5 Cr1 C3 -158.5(3) . . . . ? C4 C5 Cr1 C1 -117.9(2) . . . . ? C10 C5 Cr1 C1 121.2(3) . . . . ? C4 C5 Cr1 P31 2.6(13) . . . . ? C1 C5 Cr1 P31 120.5(13) . . . . ? C10 C5 Cr1 P31 -118.2(13) . . . . ? C4 C5 Cr1 P11 166.1(5) . . . . ? C1 C5 Cr1 P11 -76.0(6) . . . . ? C10 C5 Cr1 P11 45.2(6) . . . . ? C4 C5 Cr1 P21 -140.7(7) . . . . ? C1 C5 Cr1 P21 -22.8(7) . . . . ? C10 C5 Cr1 P21 98.4(7) . . . . ? C4 C5 Cr1 P2 -119.0(5) . . . . ? C1 C5 Cr1 P2 -1.1(5) . . . . ? C10 C5 Cr1 P2 120.1(5) . . . . ? C4 C5 Cr1 P42 88.1(5) . . . . ? C1 C5 Cr1 P42 -154.0(5) . . . . ? C10 C5 Cr1 P42 -32.8(5) . . . . ? C4 C5 Cr1 P51 113.2(6) . . . . ? C1 C5 Cr1 P51 -128.9(6) . . . . ? C10 C5 Cr1 P51 -7.6(6) . . . . ? C4 C5 Cr1 P4 72.8(3) . . . . ? C1 C5 Cr1 P4 -169.3(3) . . . . ? C10 C5 Cr1 P4 -48.1(4) . . . . ? C5 C1 Cr1 C2 -117.2(2) . . . . ? C6 C1 Cr1 C2 121.1(3) . . . . ? C2 C1 Cr1 C4 79.98(16) . . . . ? C5 C1 Cr1 C4 -37.20(14) . . . . ? C6 C1 Cr1 C4 -158.9(3) . . . . ? C2 C1 Cr1 C3 37.49(15) . . . . ? C5 C1 Cr1 C3 -79.69(15) . . . . ? C6 C1 Cr1 C3 158.6(3) . . . . ? C2 C1 Cr1 C5 117.2(2) . . . . ? C6 C1 Cr1 C5 -121.7(3) . . . . ? C2 C1 Cr1 P31 -22.0(8) . . . . ? C5 C1 Cr1 P31 -139.1(8) . . . . ? C6 C1 Cr1 P31 99.1(9) . . . . ? C2 C1 Cr1 P11 -129.1(6) . . . . ? C5 C1 Cr1 P11 113.7(6) . . . . ? C6 C1 Cr1 P11 -8.1(6) . . . . ? C2 C1 Cr1 P21 -75.8(5) . . . . ? C5 C1 Cr1 P21 167.0(4) . . . . ? C6 C1 Cr1 P21 45.3(5) . . . . ? C2 C1 Cr1 P2 -63.3(3) . . . . ? C5 C1 Cr1 P2 179.5(3) . . . . ? C6 C1 Cr1 P2 57.7(3) . . . . ? C2 C1 Cr1 P42 155.6(6) . . . . ? C5 C1 Cr1 P42 38.4(6) . . . . ? C6 C1 Cr1 P42 -83.3(6) . . . . ? C2 C1 Cr1 P51 -180.0(6) . . . . ? C5 C1 Cr1 P51 62.8(6) . . . . ? C6 C1 Cr1 P51 -58.9(6) . . . . ? C2 C1 Cr1 P4 136.5(5) . . . . ? C5 C1 Cr1 P4 19.3(5) . . . . ? C6 C1 Cr1 P4 -102.4(5) . . . . ? C2 Cr1 P11 P51 -155.1(5) . . . . ? C4 Cr1 P11 P51 -69.7(9) . . . . ? C3 Cr1 P11 P51 -154.6(10) . . . . ? C5 Cr1 P11 P51 -85.2(6) . . . . ? C1 Cr1 P11 P51 -122.0(6) . . . . ? P31 Cr1 P11 P51 88.2(7) . . . . ? P21 Cr1 P11 P51 127.7(8) . . . . ? P2 Cr1 P11 P51 121.7(7) . . . . ? P42 Cr1 P11 P51 14.6(5) . . . . ? P4 Cr1 P11 P51 26.6(5) . . . . ? C2 Cr1 P11 P21 77.2(6) . . . . ? C4 Cr1 P11 P21 162.6(6) . . . . ? C3 Cr1 P11 P21 77.7(14) . . . . ? C5 Cr1 P11 P21 147.1(5) . . . . ? C1 Cr1 P11 P21 110.3(6) . . . . ? P31 Cr1 P11 P21 -39.4(7) . . . . ? P2 Cr1 P11 P21 -5.9(6) . . . . ? P42 Cr1 P11 P21 -113.1(6) . . . . ? P51 Cr1 P11 P21 -127.7(8) . . . . ? P4 Cr1 P11 P21 -101.1(5) . . . . ? C2 Cr1 P11 Cr2 140.5(3) . . . . ? C4 Cr1 P11 Cr2 -134.1(5) . . . . ? C3 Cr1 P11 Cr2 141.0(10) . . . . ? C5 Cr1 P11 Cr2 -149.6(3) . . . . ? C1 Cr1 P11 Cr2 173.6(4) . . . . ? P31 Cr1 P11 Cr2 23.9(6) . . . . ? P21 Cr1 P11 Cr2 63.3(5) . . . . ? P2 Cr1 P11 Cr2 57.4(4) . . . . ? P42 Cr1 P11 Cr2 -49.8(4) . . . . ? P51 Cr1 P11 Cr2 -64.4(5) . . . . ? P4 Cr1 P11 Cr2 -37.8(4) . . . . ? P51 P11 P21 P31 -2.2(12) . . . . ? Cr1 P11 P21 P31 46.8(7) . . . . ? Cr2 P11 P21 P31 -48.7(7) . . . . ? P51 P11 P21 Cr2 46.5(8) . . . . ? Cr1 P11 P21 Cr2 95.5(4) . . . . ? P51 P11 P21 Cr1 -49.0(8) . . . . ? Cr2 P11 P21 Cr1 -95.5(4) . . . . ? C2 Cr1 P21 P11 -121.1(6) . . . . ? C4 Cr1 P21 P11 -155.0(10) . . . . ? C3 Cr1 P21 P11 -154.6(6) . . . . ? C5 Cr1 P21 P11 -69.6(7) . . . . ? C1 Cr1 P21 P11 -84.3(6) . . . . ? P31 Cr1 P21 P11 127.7(8) . . . . ? P2 Cr1 P21 P11 155(2) . . . . ? P42 Cr1 P21 P11 63.1(6) . . . . ? P51 Cr1 P21 P11 38.7(6) . . . . ? P4 Cr1 P21 P11 79.4(6) . . . . ? C2 Cr1 P21 P31 111.2(6) . . . . ? C4 Cr1 P21 P31 77.3(11) . . . . ? C3 Cr1 P21 P31 77.7(6) . . . . ? C5 Cr1 P21 P31 162.7(6) . . . . ? C1 Cr1 P21 P31 148.0(6) . . . . ? P11 Cr1 P21 P31 -127.7(8) . . . . ? P2 Cr1 P21 P31 28(2) . . . . ? P42 Cr1 P21 P31 -64.6(6) . . . . ? P51 Cr1 P21 P31 -89.0(7) . . . . ? P4 Cr1 P21 P31 -48.3(6) . . . . ? C2 Cr1 P21 Cr2 174.5(4) . . . . ? C4 Cr1 P21 Cr2 140.7(7) . . . . ? C3 Cr1 P21 Cr2 141.1(2) . . . . ? C5 Cr1 P21 Cr2 -134.0(3) . . . . ? C1 Cr1 P21 Cr2 -148.7(3) . . . . ? P31 Cr1 P21 Cr2 63.4(6) . . . . ? P11 Cr1 P21 Cr2 -64.3(6) . . . . ? P2 Cr1 P21 Cr2 91(2) . . . . ? P42 Cr1 P21 Cr2 -1.2(4) . . . . ? P51 Cr1 P21 Cr2 -25.6(5) . . . . ? P4 Cr1 P21 Cr2 15.1(4) . . . . ? P11 P21 P31 P41 2.7(12) . . . . ? Cr2 P21 P31 P41 -46.5(8) . . . . ? Cr1 P21 P31 P41 49.7(8) . . . . ? P11 P21 P31 Cr1 -47.0(8) . . . . ? Cr2 P21 P31 Cr1 -96.2(4) . . . . ? P11 P21 P31 Cr2 49.2(7) . . . . ? Cr1 P21 P31 Cr2 96.2(4) . . . . ? C2 Cr1 P31 P41 147.4(6) . . . . ? C4 Cr1 P31 P41 77.0(7) . . . . ? C3 Cr1 P31 P41 110.7(7) . . . . ? C5 Cr1 P31 P41 75.2(13) . . . . ? C1 Cr1 P31 P41 161.6(7) . . . . ? P11 Cr1 P31 P41 -89.4(7) . . . . ? P21 Cr1 P31 P41 -128.6(8) . . . . ? P2 Cr1 P31 P41 -137.4(9) . . . . ? P42 Cr1 P31 P41 -16.6(7) . . . . ? P51 Cr1 P31 P41 -37.2(7) . . . . ? P4 Cr1 P31 P41 -5.9(7) . . . . ? C2 Cr1 P31 P21 -84.1(5) . . . . ? C4 Cr1 P31 P21 -154.4(4) . . . . ? C3 Cr1 P31 P21 -120.7(5) . . . . ? C5 Cr1 P31 P21 -156.3(9) . . . . ? C1 Cr1 P31 P21 -69.8(8) . . . . ? P11 Cr1 P31 P21 39.1(6) . . . . ? P2 Cr1 P31 P21 -8.8(5) . . . . ? P42 Cr1 P31 P21 111.9(5) . . . . ? P51 Cr1 P31 P21 91.3(6) . . . . ? P4 Cr1 P31 P21 122.7(6) . . . . ? C2 Cr1 P31 Cr2 -147.3(3) . . . . ? C4 Cr1 P31 Cr2 142.4(3) . . . . ? C3 Cr1 P31 Cr2 176.1(4) . . . . ? C5 Cr1 P31 Cr2 140.5(8) . . . . ? C1 Cr1 P31 Cr2 -133.0(5) . . . . ? P11 Cr1 P31 Cr2 -24.0(6) . . . . ? P21 Cr1 P31 Cr2 -63.2(5) . . . . ? P2 Cr1 P31 Cr2 -72.0(5) . . . . ? P42 Cr1 P31 Cr2 48.7(5) . . . . ? P51 Cr1 P31 Cr2 28.1(6) . . . . ? P4 Cr1 P31 Cr2 59.5(4) . . . . ? P21 P31 P41 P51 -2.1(12) . . . . ? Cr1 P31 P41 P51 46.4(8) . . . . ? Cr2 P31 P41 P51 -47.7(8) . . . . ? P21 P31 P41 Cr2 45.6(7) . . . . ? Cr1 P31 P41 Cr2 94.1(4) . . . . ? P21 P31 P41 Cr1 -48.5(7) . . . . ? Cr2 P31 P41 Cr1 -94.1(4) . . . . ? C2 Cr1 P41 P31 -67.2(8) . . . . ? C4 Cr1 P41 P31 -120.2(6) . . . . ? C3 Cr1 P41 P31 -83.1(6) . . . . ? C5 Cr1 P41 P31 -153.3(5) . . . . ? C1 Cr1 P41 P31 -153.7(10) . . . . ? P11 Cr1 P41 P31 91.8(7) . . . . ? P21 Cr1 P41 P31 38.9(6) . . . . ? P2 Cr1 P41 P31 27.2(6) . . . . ? P42 Cr1 P41 P31 144.6(13) . . . . ? P51 Cr1 P41 P31 129.8(8) . . . . ? P4 Cr1 P41 P31 155(3) . . . . ? C2 Cr1 P41 P51 163.0(6) . . . . ? C4 Cr1 P41 P51 110.0(6) . . . . ? C3 Cr1 P41 P51 147.1(6) . . . . ? C5 Cr1 P41 P51 76.9(6) . . . . ? C1 Cr1 P41 P51 76.5(13) . . . . ? P31 Cr1 P41 P51 -129.8(8) . . . . ? P11 Cr1 P41 P51 -38.0(7) . . . . ? P21 Cr1 P41 P51 -90.9(6) . . . . ? P2 Cr1 P41 P51 -102.6(6) . . . . ? P42 Cr1 P41 P51 14.8(9) . . . . ? P4 Cr1 P41 P51 26(2) . . . . ? C2 Cr1 P41 Cr2 -132.3(4) . . . . ? C4 Cr1 P41 Cr2 174.7(4) . . . . ? C3 Cr1 P41 Cr2 -148.2(3) . . . . ? C5 Cr1 P41 Cr2 141.6(2) . . . . ? C1 Cr1 P41 Cr2 141.2(9) . . . . ? P31 Cr1 P41 Cr2 -65.1(5) . . . . ? P11 Cr1 P41 Cr2 26.7(5) . . . . ? P21 Cr1 P41 Cr2 -26.2(4) . . . . ? P2 Cr1 P41 Cr2 -37.9(3) . . . . ? P42 Cr1 P41 Cr2 79.5(10) . . . . ? P51 Cr1 P41 Cr2 64.7(6) . . . . ? P4 Cr1 P41 Cr2 90(3) . . . . ? P21 P11 P51 P41 1.0(13) . . . . ? Cr1 P11 P51 P41 -47.6(8) . . . . ? Cr2 P11 P51 P41 47.1(8) . . . . ? P21 P11 P51 Cr2 -46.0(7) . . . . ? Cr1 P11 P51 Cr2 -94.7(5) . . . . ? P21 P11 P51 Cr1 48.6(8) . . . . ? Cr2 P11 P51 Cr1 94.7(5) . . . . ? P31 P41 P51 P11 0.6(13) . . . . ? Cr2 P41 P51 P11 -47.3(8) . . . . ? Cr1 P41 P51 P11 46.8(8) . . . . ? P31 P41 P51 Cr2 47.9(7) . . . . ? Cr1 P41 P51 Cr2 94.1(4) . . . . ? P31 P41 P51 Cr1 -46.2(8) . . . . ? Cr2 P41 P51 Cr1 -94.1(4) . . . . ? C2 Cr1 P51 P11 76.1(13) . . . . ? C4 Cr1 P51 P11 146.5(6) . . . . ? C3 Cr1 P51 P11 162.5(7) . . . . ? C5 Cr1 P51 P11 109.5(7) . . . . ? C1 Cr1 P51 P11 76.1(7) . . . . ? P31 Cr1 P51 P11 -92.5(7) . . . . ? P21 Cr1 P51 P11 -39.2(7) . . . . ? P2 Cr1 P51 P11 -50.7(7) . . . . ? P42 Cr1 P51 P11 -145.4(12) . . . . ? P4 Cr1 P51 P11 -137.0(9) . . . . ? C2 Cr1 P51 P41 -155.1(10) . . . . ? C4 Cr1 P51 P41 -84.7(5) . . . . ? C3 Cr1 P51 P41 -68.7(8) . . . . ? C5 Cr1 P51 P41 -121.7(5) . . . . ? C1 Cr1 P51 P41 -155.1(4) . . . . ? P31 Cr1 P51 P41 36.3(6) . . . . ? P11 Cr1 P51 P41 128.8(8) . . . . ? P21 Cr1 P51 P41 89.7(6) . . . . ? P2 Cr1 P51 P41 78.1(6) . . . . ? P42 Cr1 P51 P41 -16.6(9) . . . . ? P4 Cr1 P51 P41 -8.2(6) . . . . ? C2 Cr1 P51 Cr2 140.6(9) . . . . ? C4 Cr1 P51 Cr2 -149.0(3) . . . . ? C3 Cr1 P51 Cr2 -133.0(4) . . . . ? C5 Cr1 P51 Cr2 174.1(4) . . . . ? C1 Cr1 P51 Cr2 140.7(3) . . . . ? P31 Cr1 P51 Cr2 -28.0(6) . . . . ? P11 Cr1 P51 Cr2 64.6(7) . . . . ? P21 Cr1 P51 Cr2 25.4(5) . . . . ? P2 Cr1 P51 Cr2 13.8(5) . . . . ? P42 Cr1 P51 Cr2 -80.8(9) . . . . ? P4 Cr1 P51 Cr2 -72.5(5) . . . . ? C2 Cr1 P1 P5 -148.5(3) . . . . ? C4 Cr1 P1 P5 -76.5(6) . . . . ? C3 Cr1 P1 P5 -161.2(3) . . . . ? C5 Cr1 P1 P5 -78.9(3) . . . . ? C1 Cr1 P1 P5 -112.4(3) . . . . ? P31 Cr1 P1 P5 99.4(6) . . . . ? P11 Cr1 P1 P5 -17(3) . . . . ? P21 Cr1 P1 P5 133.6(7) . . . . ? P2 Cr1 P1 P5 129.0(4) . . . . ? P42 Cr1 P1 P5 24.3(3) . . . . ? P51 Cr1 P1 P5 7.8(5) . . . . ? P4 Cr1 P1 P5 37.8(3) . . . . ? C2 Cr1 P1 P2 82.4(3) . . . . ? C4 Cr1 P1 P2 154.5(5) . . . . ? C3 Cr1 P1 P2 69.7(5) . . . . ? C5 Cr1 P1 P2 152.1(3) . . . . ? C1 Cr1 P1 P2 118.6(3) . . . . ? P31 Cr1 P1 P2 -29.6(6) . . . . ? P11 Cr1 P1 P2 -146(3) . . . . ? P21 Cr1 P1 P2 4.6(7) . . . . ? P42 Cr1 P1 P2 -104.8(4) . . . . ? P51 Cr1 P1 P2 -121.3(5) . . . . ? P4 Cr1 P1 P2 -91.2(3) . . . . ? C2 Cr1 P1 Cr2 147.00(16) . . . . ? C4 Cr1 P1 Cr2 -140.9(4) . . . . ? C3 Cr1 P1 Cr2 134.3(3) . . . . ? C5 Cr1 P1 Cr2 -143.32(16) . . . . ? C1 Cr1 P1 Cr2 -176.8(2) . . . . ? P31 Cr1 P1 Cr2 35.0(5) . . . . ? P11 Cr1 P1 Cr2 -81(3) . . . . ? P21 Cr1 P1 Cr2 69.2(6) . . . . ? P2 Cr1 P1 Cr2 64.6(3) . . . . ? P42 Cr1 P1 Cr2 -40.2(3) . . . . ? P51 Cr1 P1 Cr2 -56.7(4) . . . . ? P4 Cr1 P1 Cr2 -26.6(2) . . . . ? P5 P1 P2 P3 0.7(7) . . . . ? Cr1 P1 P2 P3 47.4(4) . . . . ? Cr2 P1 P2 P3 -46.4(4) . . . . ? P5 P1 P2 Cr1 -46.7(4) . . . . ? Cr2 P1 P2 Cr1 -93.9(2) . . . . ? P5 P1 P2 Cr2 47.1(4) . . . . ? Cr1 P1 P2 Cr2 93.9(2) . . . . ? C2 Cr1 P2 P3 119.2(4) . . . . ? C4 Cr1 P2 P3 70.6(5) . . . . ? C3 Cr1 P2 P3 82.9(4) . . . . ? C5 Cr1 P2 P3 153.3(4) . . . . ? C1 Cr1 P2 P3 152.5(4) . . . . ? P31 Cr1 P2 P3 3.8(9) . . . . ? P11 Cr1 P2 P3 -121.1(6) . . . . ? P21 Cr1 P2 P3 -143(2) . . . . ? P42 Cr1 P2 P3 -53.1(5) . . . . ? P51 Cr1 P2 P3 -78.5(5) . . . . ? P4 Cr1 P2 P3 -37.6(4) . . . . ? C2 Cr1 P2 P1 -111.8(3) . . . . ? C4 Cr1 P2 P1 -160.3(3) . . . . ? C3 Cr1 P2 P1 -148.0(3) . . . . ? C5 Cr1 P2 P1 -77.6(4) . . . . ? C1 Cr1 P2 P1 -78.4(3) . . . . ? P31 Cr1 P2 P1 132.8(7) . . . . ? P11 Cr1 P2 P1 8.0(6) . . . . ? P21 Cr1 P2 P1 -13.7(19) . . . . ? P42 Cr1 P2 P1 75.9(4) . . . . ? P51 Cr1 P2 P1 50.5(5) . . . . ? P4 Cr1 P2 P1 91.4(3) . . . . ? C2 Cr1 P2 Cr2 -175.93(19) . . . . ? C4 Cr1 P2 Cr2 135.5(2) . . . . ? C3 Cr1 P2 Cr2 147.81(15) . . . . ? C5 Cr1 P2 Cr2 -141.8(3) . . . . ? C1 Cr1 P2 Cr2 -142.56(15) . . . . ? P31 Cr1 P2 Cr2 68.7(7) . . . . ? P11 Cr1 P2 Cr2 -56.2(5) . . . . ? P21 Cr1 P2 Cr2 -78(2) . . . . ? P42 Cr1 P2 Cr2 11.8(4) . . . . ? P51 Cr1 P2 Cr2 -13.6(4) . . . . ? P4 Cr1 P2 Cr2 27.2(2) . . . . ? P1 P2 P3 P4 -1.2(7) . . . . ? Cr1 P2 P3 P4 45.8(4) . . . . ? Cr2 P2 P3 P4 -47.4(4) . . . . ? P1 P2 P3 Cr1 -47.0(4) . . . . ? Cr2 P2 P3 Cr1 -93.2(2) . . . . ? P1 P2 P3 Cr2 46.1(4) . . . . ? Cr1 P2 P3 Cr2 93.2(2) . . . . ? C2 Cr1 P3 P2 -77.1(3) . . . . ? C4 Cr1 P3 P2 -146.9(3) . . . . ? C3 Cr1 P3 P2 -110.8(3) . . . . ? C5 Cr1 P3 P2 -158.8(3) . . . . ? C1 Cr1 P3 P2 -74.6(6) . . . . ? P31 Cr1 P3 P2 -14(3) . . . . ? P11 Cr1 P3 P2 51.2(5) . . . . ? P21 Cr1 P3 P2 8.7(4) . . . . ? P42 Cr1 P3 P2 120.6(4) . . . . ? P51 Cr1 P3 P2 102.2(5) . . . . ? P4 Cr1 P3 P2 130.1(5) . . . . ? C2 Cr1 P3 P4 152.8(3) . . . . ? C4 Cr1 P3 P4 83.0(4) . . . . ? C3 Cr1 P3 P4 119.1(3) . . . . ? C5 Cr1 P3 P4 71.1(6) . . . . ? C1 Cr1 P3 P4 155.3(5) . . . . ? P31 Cr1 P3 P4 -144(3) . . . . ? P11 Cr1 P3 P4 -78.9(5) . . . . ? P21 Cr1 P3 P4 -121.4(5) . . . . ? P2 Cr1 P3 P4 -130.1(5) . . . . ? P42 Cr1 P3 P4 -9.5(4) . . . . ? P51 Cr1 P3 P4 -27.9(5) . . . . ? C2 Cr1 P3 Cr2 -142.14(19) . . . . ? C4 Cr1 P3 Cr2 148.02(18) . . . . ? C3 Cr1 P3 Cr2 -175.9(2) . . . . ? C5 Cr1 P3 Cr2 136.2(3) . . . . ? C1 Cr1 P3 Cr2 -139.6(4) . . . . ? P31 Cr1 P3 Cr2 -79(3) . . . . ? P11 Cr1 P3 Cr2 -13.8(5) . . . . ? P21 Cr1 P3 Cr2 -56.4(3) . . . . ? P2 Cr1 P3 Cr2 -65.0(3) . . . . ? P42 Cr1 P3 Cr2 55.6(3) . . . . ? P51 Cr1 P3 Cr2 37.2(5) . . . . ? P4 Cr1 P3 Cr2 65.0(4) . . . . ? P2 P3 P4 P5 1.3(7) . . . . ? Cr1 P3 P4 P5 47.0(4) . . . . ? Cr2 P3 P4 P5 -46.1(4) . . . . ? P2 P3 P4 Cr1 -45.7(4) . . . . ? Cr2 P3 P4 Cr1 -93.1(2) . . . . ? P2 P3 P4 Cr2 47.4(4) . . . . ? Cr1 P3 P4 Cr2 93.1(2) . . . . ? C2 Cr1 P4 P5 156.4(4) . . . . ? C4 Cr1 P4 P5 119.5(3) . . . . ? C3 Cr1 P4 P5 153.4(3) . . . . ? C5 Cr1 P4 P5 83.5(3) . . . . ? C1 Cr1 P4 P5 70.9(5) . . . . ? P31 Cr1 P4 P5 -121.8(6) . . . . ? P11 Cr1 P4 P5 -27.2(5) . . . . ? P21 Cr1 P4 P5 -79.1(4) . . . . ? P2 Cr1 P4 P5 -91.5(3) . . . . ? P42 Cr1 P4 P5 18.3(9) . . . . ? P51 Cr1 P4 P5 5.6(8) . . . . ? C2 Cr1 P4 P3 -74.5(5) . . . . ? C4 Cr1 P4 P3 -111.4(3) . . . . ? C3 Cr1 P4 P3 -77.5(3) . . . . ? C5 Cr1 P4 P3 -147.4(3) . . . . ? C1 Cr1 P4 P3 -160.0(3) . . . . ? P31 Cr1 P4 P3 7.3(6) . . . . ? P11 Cr1 P4 P3 102.0(6) . . . . ? P21 Cr1 P4 P3 50.1(5) . . . . ? P2 Cr1 P4 P3 37.6(3) . . . . ? P42 Cr1 P4 P3 147.4(11) . . . . ? P51 Cr1 P4 P3 134.7(7) . . . . ? C2 Cr1 P4 Cr2 -139.3(3) . . . . ? C4 Cr1 P4 Cr2 -176.22(18) . . . . ? C3 Cr1 P4 Cr2 -142.31(15) . . . . ? C5 Cr1 P4 Cr2 147.78(14) . . . . ? C1 Cr1 P4 Cr2 135.2(3) . . . . ? P31 Cr1 P4 Cr2 -57.5(4) . . . . ? P11 Cr1 P4 Cr2 37.2(5) . . . . ? P21 Cr1 P4 Cr2 -14.7(4) . . . . ? P2 Cr1 P4 Cr2 -27.23(19) . . . . ? P42 Cr1 P4 Cr2 82.6(10) . . . . ? P51 Cr1 P4 Cr2 69.9(6) . . . . ? P3 P4 P5 P1 -0.9(7) . . . . ? Cr1 P4 P5 P1 46.3(4) . . . . ? Cr2 P4 P5 P1 -47.2(4) . . . . ? P3 P4 P5 Cr2 46.3(4) . . . . ? Cr1 P4 P5 Cr2 93.48(19) . . . . ? P3 P4 P5 Cr1 -47.2(4) . . . . ? Cr2 P4 P5 Cr1 -93.48(19) . . . . ? P2 P1 P5 P4 0.1(7) . . . . ? Cr1 P1 P5 P4 -46.3(4) . . . . ? Cr2 P1 P5 P4 47.3(4) . . . . ? P2 P1 P5 Cr2 -47.2(4) . . . . ? Cr1 P1 P5 Cr2 -93.6(2) . . . . ? P2 P1 P5 Cr1 46.4(4) . . . . ? Cr2 P1 P5 Cr1 93.6(2) . . . . ? C2 Cr1 P5 P4 -161.0(3) . . . . ? C4 Cr1 P5 P4 -77.6(3) . . . . ? C3 Cr1 P5 P4 -74.3(5) . . . . ? C5 Cr1 P5 P4 -111.6(3) . . . . ? C1 Cr1 P5 P4 -148.0(2) . . . . ? P31 Cr1 P5 P4 48.8(5) . . . . ? P11 Cr1 P5 P4 135.7(8) . . . . ? P21 Cr1 P5 P4 101.3(5) . . . . ? P2 Cr1 P5 P4 91.1(3) . . . . ? P42 Cr1 P5 P4 -8.3(3) . . . . ? P51 Cr1 P5 P4 -17(2) . . . . ? C2 Cr1 P5 P1 69.1(5) . . . . ? C4 Cr1 P5 P1 152.5(3) . . . . ? C3 Cr1 P5 P1 155.8(5) . . . . ? C5 Cr1 P5 P1 118.5(3) . . . . ? C1 Cr1 P5 P1 82.1(4) . . . . ? P31 Cr1 P5 P1 -81.1(6) . . . . ? P11 Cr1 P5 P1 5.8(10) . . . . ? P21 Cr1 P5 P1 -28.6(5) . . . . ? P2 Cr1 P5 P1 -38.8(4) . . . . ? P42 Cr1 P5 P1 -138.2(5) . . . . ? P51 Cr1 P5 P1 -147(2) . . . . ? P4 Cr1 P5 P1 -129.9(4) . . . . ? C2 Cr1 P5 Cr2 133.8(3) . . . . ? C4 Cr1 P5 Cr2 -142.77(15) . . . . ? C3 Cr1 P5 Cr2 -139.5(4) . . . . ? C5 Cr1 P5 Cr2 -176.71(19) . . . . ? C1 Cr1 P5 Cr2 146.91(15) . . . . ? P31 Cr1 P5 Cr2 -16.3(5) . . . . ? P11 Cr1 P5 Cr2 70.6(7) . . . . ? P21 Cr1 P5 Cr2 36.1(4) . . . . ? P2 Cr1 P5 Cr2 26.0(2) . . . . ? P42 Cr1 P5 Cr2 -73.4(4) . . . . ? P51 Cr1 P5 Cr2 -82(2) . . . . ? P4 Cr1 P5 Cr2 -65.1(2) . . . . ? C2 Cr1 P12 P52 -138.8(4) . . . . ? C4 Cr1 P12 P52 -102.9(13) . . . . ? C3 Cr1 P12 P52 -161.7(3) . . . . ? C5 Cr1 P12 P52 -73.0(4) . . . . ? C1 Cr1 P12 P52 -100.5(4) . . . . ? P31 Cr1 P12 P52 111.7(6) . . . . ? P11 Cr1 P12 P52 -10.9(11) . . . . ? P21 Cr1 P12 P52 140.0(10) . . . . ? P2 Cr1 P12 P52 137.4(5) . . . . ? P42 Cr1 P12 P52 38.3(4) . . . . ? P51 Cr1 P12 P52 18.5(6) . . . . ? P4 Cr1 P12 P52 53.8(4) . . . . ? C2 Cr1 P12 P22 93.4(4) . . . . ? C4 Cr1 P12 P22 129.3(12) . . . . ? C3 Cr1 P12 P22 70.5(4) . . . . ? C5 Cr1 P12 P22 159.2(3) . . . . ? C1 Cr1 P12 P22 131.7(4) . . . . ? P31 Cr1 P12 P22 -16.1(6) . . . . ? P11 Cr1 P12 P22 -138.7(13) . . . . ? P21 Cr1 P12 P22 12.1(9) . . . . ? P2 Cr1 P12 P22 9.5(4) . . . . ? P42 Cr1 P12 P22 -89.5(4) . . . . ? P51 Cr1 P12 P22 -109.3(5) . . . . ? P4 Cr1 P12 P22 -74.0(4) . . . . ? C2 Cr1 P12 Cr2 156.9(3) . . . . ? C4 Cr1 P12 Cr2 -167.2(12) . . . . ? C3 Cr1 P12 Cr2 133.91(19) . . . . ? C5 Cr1 P12 Cr2 -137.32(19) . . . . ? C1 Cr1 P12 Cr2 -164.8(3) . . . . ? P31 Cr1 P12 Cr2 47.4(5) . . . . ? P11 Cr1 P12 Cr2 -75.2(12) . . . . ? P21 Cr1 P12 Cr2 75.6(9) . . . . ? P2 Cr1 P12 Cr2 73.0(4) . . . . ? P42 Cr1 P12 Cr2 -26.1(3) . . . . ? P51 Cr1 P12 Cr2 -45.8(4) . . . . ? P4 Cr1 P12 Cr2 -10.6(4) . . . . ? P52 P12 P22 P32 -0.6(7) . . . . ? Cr1 P12 P22 P32 46.9(4) . . . . ? Cr2 P12 P22 P32 -47.0(4) . . . . ? P52 P12 P22 Cr2 46.4(4) . . . . ? Cr1 P12 P22 Cr2 93.9(2) . . . . ? P52 P12 P22 Cr1 -47.5(4) . . . . ? Cr2 P12 P22 Cr1 -93.9(2) . . . . ? C2 Cr1 P22 P32 130.8(4) . . . . ? C4 Cr1 P22 P32 68.8(4) . . . . ? C3 Cr1 P22 P32 92.3(4) . . . . ? C5 Cr1 P22 P32 126.6(13) . . . . ? C1 Cr1 P22 P32 158.6(3) . . . . ? P31 Cr1 P22 P32 11.5(10) . . . . ? P11 Cr1 P22 P32 -110.8(5) . . . . ? P21 Cr1 P22 P32 -140.8(9) . . . . ? P2 Cr1 P22 P32 -150.6(10) . . . . ? P42 Cr1 P22 P32 -37.6(4) . . . . ? P51 Cr1 P22 P32 -62.2(5) . . . . ? P4 Cr1 P22 P32 -24.0(4) . . . . ? C2 Cr1 P22 P12 -98.9(4) . . . . ? C4 Cr1 P22 P12 -160.9(3) . . . . ? C3 Cr1 P22 P12 -137.4(4) . . . . ? C5 Cr1 P22 P12 -103.1(13) . . . . ? C1 Cr1 P22 P12 -71.1(4) . . . . ? P31 Cr1 P22 P12 141.8(11) . . . . ? P11 Cr1 P22 P12 19.5(6) . . . . ? P21 Cr1 P22 P12 -10.5(7) . . . . ? P2 Cr1 P22 P12 -20.3(7) . . . . ? P42 Cr1 P22 P12 92.7(4) . . . . ? P51 Cr1 P22 P12 68.1(5) . . . . ? P4 Cr1 P22 P12 106.2(4) . . . . ? C2 Cr1 P22 Cr2 -163.6(4) . . . . ? C4 Cr1 P22 Cr2 134.35(18) . . . . ? C3 Cr1 P22 Cr2 157.8(3) . . . . ? C5 Cr1 P22 Cr2 -167.8(12) . . . . ? C1 Cr1 P22 Cr2 -135.9(2) . . . . ? P31 Cr1 P22 Cr2 77.1(10) . . . . ? P11 Cr1 P22 Cr2 -45.2(5) . . . . ? P21 Cr1 P22 Cr2 -75.2(7) . . . . ? P2 Cr1 P22 Cr2 -85.0(8) . . . . ? P42 Cr1 P22 Cr2 28.0(3) . . . . ? P51 Cr1 P22 Cr2 3.4(5) . . . . ? P4 Cr1 P22 Cr2 41.5(4) . . . . ? P12 P22 P32 P42 -0.3(7) . . . . ? Cr2 P22 P32 P42 -47.0(4) . . . . ? Cr1 P22 P32 P42 45.7(4) . . . . ? P12 P22 P32 Cr2 46.7(4) . . . . ? Cr1 P22 P32 Cr2 92.7(2) . . . . ? P12 P22 P32 Cr1 -46.0(4) . . . . ? Cr2 P22 P32 Cr1 -92.7(2) . . . . ? C2 Cr1 P32 P22 -70.8(4) . . . . ? C4 Cr1 P32 P22 -137.7(4) . . . . ? C3 Cr1 P32 P22 -99.3(4) . . . . ? C5 Cr1 P32 P22 -160.3(3) . . . . ? C1 Cr1 P32 P22 -97.6(12) . . . . ? P31 Cr1 P32 P22 -11.2(10) . . . . ? P11 Cr1 P32 P22 67.1(5) . . . . ? P21 Cr1 P32 P22 18.7(5) . . . . ? P2 Cr1 P32 P22 9.1(3) . . . . ? P42 Cr1 P32 P22 130.2(5) . . . . ? P51 Cr1 P32 P22 114.0(5) . . . . ? P4 Cr1 P32 P22 138.8(6) . . . . ? C2 Cr1 P32 P42 159.1(3) . . . . ? C4 Cr1 P32 P42 92.1(4) . . . . ? C3 Cr1 P32 P42 130.5(5) . . . . ? C5 Cr1 P32 P42 69.5(4) . . . . ? C1 Cr1 P32 P42 132.3(12) . . . . ? P31 Cr1 P32 P42 -141.4(11) . . . . ? P11 Cr1 P32 P42 -63.0(5) . . . . ? P21 Cr1 P32 P42 -111.5(4) . . . . ? P2 Cr1 P32 P42 -121.1(4) . . . . ? P51 Cr1 P32 P42 -16.2(5) . . . . ? P4 Cr1 P32 P42 8.6(4) . . . . ? C2 Cr1 P32 Cr2 -135.9(2) . . . . ? C4 Cr1 P32 Cr2 157.1(3) . . . . ? C3 Cr1 P32 Cr2 -164.5(3) . . . . ? C5 Cr1 P32 Cr2 134.59(19) . . . . ? C1 Cr1 P32 Cr2 -162.7(11) . . . . ? P31 Cr1 P32 Cr2 -76.3(10) . . . . ? P11 Cr1 P32 Cr2 2.0(5) . . . . ? P21 Cr1 P32 Cr2 -46.4(3) . . . . ? P2 Cr1 P32 Cr2 -56.1(2) . . . . ? P42 Cr1 P32 Cr2 65.0(4) . . . . ? P51 Cr1 P32 Cr2 48.8(5) . . . . ? P4 Cr1 P32 Cr2 73.7(4) . . . . ? P22 P32 P42 P52 1.0(7) . . . . ? Cr2 P32 P42 P52 -45.9(4) . . . . ? Cr1 P32 P42 P52 47.4(4) . . . . ? P22 P32 P42 Cr1 -46.4(4) . . . . ? Cr2 P32 P42 Cr1 -93.4(3) . . . . ? P22 P32 P42 Cr2 47.0(4) . . . . ? Cr1 P32 P42 Cr2 93.4(3) . . . . ? C2 Cr1 P42 P32 -99.8(13) . . . . ? C4 Cr1 P42 P32 -100.5(4) . . . . ? C3 Cr1 P42 P32 -72.0(4) . . . . ? C5 Cr1 P42 P32 -138.8(4) . . . . ? C1 Cr1 P42 P32 -161.9(3) . . . . ? P31 Cr1 P42 P32 16.7(6) . . . . ? P11 Cr1 P42 P32 113.2(6) . . . . ? P21 Cr1 P42 P32 65.4(5) . . . . ? P2 Cr1 P42 P32 52.4(4) . . . . ? P51 Cr1 P42 P32 141.1(11) . . . . ? P4 Cr1 P42 P32 -19.1(8) . . . . ? C2 Cr1 P42 P52 131.6(13) . . . . ? C4 Cr1 P42 P52 130.9(4) . . . . ? C3 Cr1 P42 P52 159.4(3) . . . . ? C5 Cr1 P42 P52 92.6(4) . . . . ? C1 Cr1 P42 P52 69.5(5) . . . . ? P31 Cr1 P42 P52 -111.8(5) . . . . ? P11 Cr1 P42 P52 -15.4(6) . . . . ? P21 Cr1 P42 P52 -63.2(5) . . . . ? P2 Cr1 P42 P52 -76.2(4) . . . . ? P51 Cr1 P42 P52 12.5(11) . . . . ? P4 Cr1 P42 P52 -147.7(11) . . . . ? C2 Cr1 P42 Cr2 -164.0(12) . . . . ? C4 Cr1 P42 Cr2 -164.7(3) . . . . ? C3 Cr1 P42 Cr2 -136.2(2) . . . . ? C5 Cr1 P42 Cr2 157.0(3) . . . . ? C1 Cr1 P42 Cr2 133.86(19) . . . . ? P31 Cr1 P42 Cr2 -47.5(4) . . . . ? P11 Cr1 P42 Cr2 49.0(5) . . . . ? P21 Cr1 P42 Cr2 1.2(4) . . . . ? P2 Cr1 P42 Cr2 -11.8(4) . . . . ? P51 Cr1 P42 Cr2 76.8(10) . . . . ? P4 Cr1 P42 Cr2 -83.4(9) . . . . ? P32 P42 P52 P12 -1.4(7) . . . . ? Cr1 P42 P52 P12 46.4(4) . . . . ? Cr2 P42 P52 P12 -47.3(4) . . . . ? P32 P42 P52 Cr2 45.8(4) . . . . ? Cr1 P42 P52 Cr2 93.6(2) . . . . ? P32 P42 P52 Cr1 -47.8(4) . . . . ? Cr2 P42 P52 Cr1 -93.6(2) . . . . ? P22 P12 P52 P42 1.2(7) . . . . ? Cr1 P12 P52 P42 -46.2(4) . . . . ? Cr2 P12 P52 P42 47.2(4) . . . . ? P22 P12 P52 Cr2 -46.0(4) . . . . ? Cr1 P12 P52 Cr2 -93.5(2) . . . . ? P22 P12 P52 Cr1 47.5(4) . . . . ? Cr2 P12 P52 Cr1 93.5(2) . . . . ? C2 Cr1 P52 P42 -162.0(3) . . . . ? C4 Cr1 P52 P42 -72.1(4) . . . . ? C3 Cr1 P52 P42 -101.2(14) . . . . ? C5 Cr1 P52 P42 -100.3(4) . . . . ? C1 Cr1 P52 P42 -138.8(4) . . . . ? P31 Cr1 P52 P42 64.7(6) . . . . ? P11 Cr1 P52 P42 142.4(13) . . . . ? P21 Cr1 P52 P42 112.9(5) . . . . ? P2 Cr1 P52 P42 104.7(4) . . . . ? P51 Cr1 P52 P42 -10.9(9) . . . . ? P4 Cr1 P52 P42 9.3(3) . . . . ? C2 Cr1 P52 P12 68.5(5) . . . . ? C4 Cr1 P52 P12 158.4(3) . . . . ? C3 Cr1 P52 P12 129.3(13) . . . . ? C5 Cr1 P52 P12 130.2(4) . . . . ? C1 Cr1 P52 P12 91.7(4) . . . . ? P31 Cr1 P52 P12 -64.9(6) . . . . ? P11 Cr1 P52 P12 12.9(13) . . . . ? P21 Cr1 P52 P12 -16.6(5) . . . . ? P2 Cr1 P52 P12 -24.8(4) . . . . ? P42 Cr1 P52 P12 -129.5(5) . . . . ? P51 Cr1 P52 P12 -140.4(12) . . . . ? P4 Cr1 P52 P12 -120.2(4) . . . . ? C2 Cr1 P52 Cr2 133.3(2) . . . . ? C4 Cr1 P52 Cr2 -136.8(2) . . . . ? C3 Cr1 P52 Cr2 -165.9(12) . . . . ? C5 Cr1 P52 Cr2 -165.0(3) . . . . ? C1 Cr1 P52 Cr2 156.5(3) . . . . ? P31 Cr1 P52 Cr2 -0.1(6) . . . . ? P11 Cr1 P52 Cr2 77.7(12) . . . . ? P21 Cr1 P52 Cr2 48.2(4) . . . . ? P2 Cr1 P52 Cr2 40.0(3) . . . . ? P42 Cr1 P52 Cr2 -64.7(3) . . . . ? P51 Cr1 P52 Cr2 -75.6(10) . . . . ? P4 Cr1 P52 Cr2 -55.4(3) . . . . ? P11 P21 Cr2 C11 92.2(6) . . . . ? P31 P21 Cr2 C11 -142.0(5) . . . . ? Cr1 P21 Cr2 C11 155.4(3) . . . . ? P11 P21 Cr2 C15 69.9(7) . . . . ? P31 P21 Cr2 C15 -164.3(5) . . . . ? Cr1 P21 Cr2 C15 133.1(3) . . . . ? P11 P21 Cr2 C14 134.2(14) . . . . ? P31 P21 Cr2 C14 -99.9(15) . . . . ? Cr1 P21 Cr2 C14 -162.5(12) . . . . ? P11 P21 Cr2 C13 159.1(5) . . . . ? P31 P21 Cr2 C13 -75.1(6) . . . . ? Cr1 P21 Cr2 C13 -137.7(2) . . . . ? P11 P21 Cr2 C12 130.4(6) . . . . ? P31 P21 Cr2 C12 -103.8(6) . . . . ? Cr1 P21 Cr2 C12 -166.4(3) . . . . ? P11 P21 Cr2 P31 -125.8(8) . . . . ? Cr1 P21 Cr2 P31 -62.6(5) . . . . ? P11 P21 Cr2 P41 -90.1(7) . . . . ? P31 P21 Cr2 P41 35.7(6) . . . . ? Cr1 P21 Cr2 P41 -26.9(5) . . . . ? P31 P21 Cr2 P11 125.8(8) . . . . ? Cr1 P21 Cr2 P11 63.2(6) . . . . ? P11 P21 Cr2 P51 -37.4(6) . . . . ? P31 P21 Cr2 P51 88.5(6) . . . . ? Cr1 P21 Cr2 P51 25.9(5) . . . . ? P11 P21 Cr2 P22 -141.1(12) . . . . ? P31 P21 Cr2 P22 -15.3(9) . . . . ? Cr1 P21 Cr2 P22 -77.9(9) . . . . ? P11 P21 Cr2 P32 -111.0(6) . . . . ? P31 P21 Cr2 P32 14.9(6) . . . . ? Cr1 P21 Cr2 P32 -47.7(4) . . . . ? P41 P31 Cr2 C11 -161.1(6) . . . . ? P21 P31 Cr2 C11 67.7(6) . . . . ? Cr1 P31 Cr2 C11 131.9(3) . . . . ? P41 P31 Cr2 C15 -89.6(18) . . . . ? P21 P31 Cr2 C15 139.2(16) . . . . ? Cr1 P31 Cr2 C15 -156.6(14) . . . . ? P41 P31 Cr2 C14 -70.4(7) . . . . ? P21 P31 Cr2 C14 158.4(5) . . . . ? Cr1 P31 Cr2 C14 -137.3(2) . . . . ? P41 P31 Cr2 C13 -100.5(7) . . . . ? P21 P31 Cr2 C13 128.4(5) . . . . ? Cr1 P31 Cr2 C13 -167.4(4) . . . . ? P41 P31 Cr2 C12 -138.9(6) . . . . ? P21 P31 Cr2 C12 89.9(5) . . . . ? Cr1 P31 Cr2 C12 154.2(4) . . . . ? P41 P31 Cr2 P21 131.1(8) . . . . ? Cr1 P31 Cr2 P21 64.2(5) . . . . ? P21 P31 Cr2 P41 -131.1(8) . . . . ? Cr1 P31 Cr2 P41 -66.9(7) . . . . ? P41 P31 Cr2 P11 90.8(7) . . . . ? P21 P31 Cr2 P11 -40.4(6) . . . . ? Cr1 P31 Cr2 P11 23.8(6) . . . . ? P41 P31 Cr2 P51 38.5(6) . . . . ? P21 P31 Cr2 P51 -92.6(6) . . . . ? Cr1 P31 Cr2 P51 -28.4(6) . . . . ? P41 P31 Cr2 P22 148.7(11) . . . . ? P21 P31 Cr2 P22 17.5(9) . . . . ? Cr1 P31 Cr2 P22 81.7(8) . . . . ? P41 P31 Cr2 P32 -15.0(9) . . . . ? P21 P31 Cr2 P32 -146.1(11) . . . . ? Cr1 P31 Cr2 P32 -81.9(9) . . . . ? P31 P41 Cr2 C11 135.2(14) . . . . ? P51 P41 Cr2 C11 -96.4(15) . . . . ? Cr1 P41 Cr2 C11 -160.9(13) . . . . ? P31 P41 Cr2 C15 159.5(4) . . . . ? P51 P41 Cr2 C15 -72.1(7) . . . . ? Cr1 P41 Cr2 C15 -136.5(3) . . . . ? P31 P41 Cr2 C14 130.5(5) . . . . ? P51 P41 Cr2 C14 -101.1(6) . . . . ? Cr1 P41 Cr2 C14 -165.6(3) . . . . ? P31 P41 Cr2 C13 92.3(6) . . . . ? P51 P41 Cr2 C13 -139.3(6) . . . . ? Cr1 P41 Cr2 C13 156.2(3) . . . . ? P31 P41 Cr2 C12 69.9(8) . . . . ? P51 P41 Cr2 C12 -161.7(6) . . . . ? Cr1 P41 Cr2 C12 133.8(4) . . . . ? P31 P41 Cr2 P21 -37.4(6) . . . . ? P51 P41 Cr2 P21 91.1(6) . . . . ? Cr1 P41 Cr2 P21 26.6(4) . . . . ? P51 P41 Cr2 P31 128.4(8) . . . . ? Cr1 P41 Cr2 P31 63.9(5) . . . . ? P31 P41 Cr2 P11 -90.4(7) . . . . ? P51 P41 Cr2 P11 38.0(7) . . . . ? Cr1 P41 Cr2 P11 -26.5(6) . . . . ? P31 P41 Cr2 P51 -128.4(8) . . . . ? Cr1 P41 Cr2 P51 -64.5(6) . . . . ? P31 P41 Cr2 P22 -13.6(5) . . . . ? P51 P41 Cr2 P22 114.8(6) . . . . ? Cr1 P41 Cr2 P22 50.3(3) . . . . ? P31 P41 Cr2 P32 15.4(10) . . . . ? P51 P41 Cr2 P32 143.9(13) . . . . ? Cr1 P41 Cr2 P32 79.4(10) . . . . ? P51 P11 Cr2 C11 129.3(6) . . . . ? P21 P11 Cr2 C11 -100.8(6) . . . . ? Cr1 P11 Cr2 C11 -165.3(4) . . . . ? P51 P11 Cr2 C15 91.0(6) . . . . ? P21 P11 Cr2 C15 -139.1(6) . . . . ? Cr1 P11 Cr2 C15 156.4(4) . . . . ? P51 P11 Cr2 C14 68.5(8) . . . . ? P21 P11 Cr2 C14 -161.6(5) . . . . ? Cr1 P11 Cr2 C14 133.8(4) . . . . ? P51 P11 Cr2 C13 132.7(16) . . . . ? P21 P11 Cr2 C13 -97(2) . . . . ? Cr1 P11 Cr2 C13 -161.9(15) . . . . ? P51 P11 Cr2 C12 158.3(5) . . . . ? P21 P11 Cr2 C12 -71.8(8) . . . . ? Cr1 P11 Cr2 C12 -136.3(3) . . . . ? P51 P11 Cr2 P21 -129.9(9) . . . . ? Cr1 P11 Cr2 P21 -64.5(7) . . . . ? P51 P11 Cr2 P31 -89.1(8) . . . . ? P21 P11 Cr2 P31 40.8(7) . . . . ? Cr1 P11 Cr2 P31 -23.8(6) . . . . ? P51 P11 Cr2 P41 -38.3(6) . . . . ? P21 P11 Cr2 P41 91.6(6) . . . . ? Cr1 P11 Cr2 P41 27.1(5) . . . . ? P21 P11 Cr2 P51 129.9(9) . . . . ? Cr1 P11 Cr2 P51 65.4(5) . . . . ? P51 P11 Cr2 P22 -111.3(6) . . . . ? P21 P11 Cr2 P22 18.6(6) . . . . ? Cr1 P11 Cr2 P22 -45.9(4) . . . . ? P51 P11 Cr2 P32 -63.3(7) . . . . ? P21 P11 Cr2 P32 66.6(6) . . . . ? Cr1 P11 Cr2 P32 2.1(5) . . . . ? P11 P51 Cr2 C11 -72.8(8) . . . . ? P41 P51 Cr2 C11 158.4(5) . . . . ? Cr1 P51 Cr2 C11 -136.3(3) . . . . ? P11 P51 Cr2 C15 -101.4(8) . . . . ? P41 P51 Cr2 C15 129.8(6) . . . . ? Cr1 P51 Cr2 C15 -165.0(4) . . . . ? P11 P51 Cr2 C14 -139.6(8) . . . . ? P41 P51 Cr2 C14 91.6(6) . . . . ? Cr1 P51 Cr2 C14 156.8(4) . . . . ? P11 P51 Cr2 C13 -161.7(7) . . . . ? P41 P51 Cr2 C13 69.5(7) . . . . ? Cr1 P51 Cr2 C13 134.7(3) . . . . ? P11 P51 Cr2 C12 -96.9(17) . . . . ? P41 P51 Cr2 C12 134.3(16) . . . . ? Cr1 P51 Cr2 C12 -160.5(14) . . . . ? P11 P51 Cr2 P21 37.8(7) . . . . ? P41 P51 Cr2 P21 -91.0(7) . . . . ? Cr1 P51 Cr2 P21 -25.8(5) . . . . ? P11 P51 Cr2 P31 91.4(8) . . . . ? P41 P51 Cr2 P31 -37.4(7) . . . . ? Cr1 P51 Cr2 P31 27.9(6) . . . . ? P11 P51 Cr2 P41 128.8(9) . . . . ? Cr1 P51 Cr2 P41 65.2(6) . . . . ? P41 P51 Cr2 P11 -128.8(9) . . . . ? Cr1 P51 Cr2 P11 -63.6(8) . . . . ? P11 P51 Cr2 P22 67.0(7) . . . . ? P41 P51 Cr2 P22 -61.8(6) . . . . ? Cr1 P51 Cr2 P22 3.5(5) . . . . ? P11 P51 Cr2 P32 113.4(8) . . . . ? P41 P51 Cr2 P32 -15.5(6) . . . . ? Cr1 P51 Cr2 P32 49.8(4) . . . . ? P32 P22 Cr2 C11 -154.2(3) . . . . ? P12 P22 Cr2 C11 75.9(4) . . . . ? Cr1 P22 Cr2 C11 139.9(2) . . . . ? P32 P22 Cr2 C15 -149.6(8) . . . . ? P12 P22 Cr2 C15 80.5(8) . . . . ? Cr1 P22 Cr2 C15 144.5(7) . . . . ? P32 P22 Cr2 C14 -69.1(5) . . . . ? P12 P22 Cr2 C14 161.0(4) . . . . ? Cr1 P22 Cr2 C14 -135.0(2) . . . . ? P32 P22 Cr2 C13 -85.2(4) . . . . ? P12 P22 Cr2 C13 144.9(4) . . . . ? Cr1 P22 Cr2 C13 -151.1(3) . . . . ? P32 P22 Cr2 C12 -122.2(4) . . . . ? P12 P22 Cr2 C12 107.9(5) . . . . ? Cr1 P22 Cr2 C12 171.8(4) . . . . ? P32 P22 Cr2 P21 141.6(11) . . . . ? P12 P22 Cr2 P21 11.6(9) . . . . ? Cr1 P22 Cr2 P21 75.6(9) . . . . ? P32 P22 Cr2 P31 -9.2(9) . . . . ? P12 P22 Cr2 P31 -139.1(9) . . . . ? Cr1 P22 Cr2 P31 -75.2(9) . . . . ? P32 P22 Cr2 P41 15.6(5) . . . . ? P12 P22 Cr2 P41 -114.3(5) . . . . ? Cr1 P22 Cr2 P41 -50.3(4) . . . . ? P32 P22 Cr2 P11 110.7(5) . . . . ? P12 P22 Cr2 P11 -19.2(6) . . . . ? Cr1 P22 Cr2 P11 44.7(4) . . . . ? P32 P22 Cr2 P51 62.5(5) . . . . ? P12 P22 Cr2 P51 -67.4(5) . . . . ? Cr1 P22 Cr2 P51 -3.4(5) . . . . ? P12 P22 Cr2 P32 -129.9(5) . . . . ? Cr1 P22 Cr2 P32 -65.9(4) . . . . ? P22 P32 Cr2 C11 78.3(8) . . . . ? P42 P32 Cr2 C11 -152.3(7) . . . . ? Cr1 P32 Cr2 C11 143.7(6) . . . . ? P22 P32 Cr2 C15 160.5(3) . . . . ? P42 P32 Cr2 C15 -70.1(5) . . . . ? Cr1 P32 Cr2 C15 -134.1(3) . . . . ? P22 P32 Cr2 C14 144.9(4) . . . . ? P42 P32 Cr2 C14 -85.8(4) . . . . ? Cr1 P32 Cr2 C14 -149.7(3) . . . . ? P22 P32 Cr2 C13 108.0(4) . . . . ? P42 P32 Cr2 C13 -122.6(4) . . . . ? Cr1 P32 Cr2 C13 173.4(3) . . . . ? P22 P32 Cr2 C12 75.3(4) . . . . ? P42 P32 Cr2 C12 -155.3(3) . . . . ? Cr1 P32 Cr2 C12 140.7(2) . . . . ? P22 P32 Cr2 P21 -18.5(5) . . . . ? P42 P32 Cr2 P21 110.9(5) . . . . ? Cr1 P32 Cr2 P21 46.9(4) . . . . ? P22 P32 Cr2 P31 9.0(8) . . . . ? P42 P32 Cr2 P31 138.3(10) . . . . ? Cr1 P32 Cr2 P31 74.4(9) . . . . ? P22 P32 Cr2 P41 -143.6(12) . . . . ? P42 P32 Cr2 P41 -14.3(12) . . . . ? Cr1 P32 Cr2 P41 -78.2(11) . . . . ? P22 P32 Cr2 P11 -67.4(5) . . . . ? P42 P32 Cr2 P11 62.0(5) . . . . ? Cr1 P32 Cr2 P11 -2.0(5) . . . . ? P22 P32 Cr2 P51 -114.5(5) . . . . ? P42 P32 Cr2 P51 14.8(5) . . . . ? Cr1 P32 Cr2 P51 -49.1(5) . . . . ? P42 P32 Cr2 P22 129.4(5) . . . . ? Cr1 P32 Cr2 P22 65.4(3) . . . . ? C14 Cr2 C11 C15 37.69(13) . . . . ? C13 Cr2 C11 C15 80.20(14) . . . . ? C12 Cr2 C11 C15 117.94(19) . . . . ? P21 Cr2 C11 C15 -155.2(5) . . . . ? P31 Cr2 C11 C15 154.3(6) . . . . ? P41 Cr2 C11 C15 32.5(17) . . . . ? P11 Cr2 C11 C15 -100.9(6) . . . . ? P51 Cr2 C11 C15 -50.7(7) . . . . ? P22 Cr2 C11 C15 177.2(5) . . . . ? P32 Cr2 C11 C15 113.7(10) . . . . ? C15 Cr2 C11 C12 -117.94(19) . . . . ? C14 Cr2 C11 C12 -80.25(15) . . . . ? C13 Cr2 C11 C12 -37.74(14) . . . . ? P21 Cr2 C11 C12 86.9(5) . . . . ? P31 Cr2 C11 C12 36.4(7) . . . . ? P41 Cr2 C11 C12 -85.4(17) . . . . ? P11 Cr2 C11 C12 141.2(6) . . . . ? P51 Cr2 C11 C12 -168.6(6) . . . . ? P22 Cr2 C11 C12 59.3(5) . . . . ? P32 Cr2 C11 C12 -4.3(11) . . . . ? C15 Cr2 C11 C16 121.1(3) . . . . ? C14 Cr2 C11 C16 158.8(3) . . . . ? C13 Cr2 C11 C16 -158.7(3) . . . . ? C12 Cr2 C11 C16 -121.0(3) . . . . ? P21 Cr2 C11 C16 -34.1(5) . . . . ? P31 Cr2 C11 C16 -84.6(7) . . . . ? P41 Cr2 C11 C16 153.6(17) . . . . ? P11 Cr2 C11 C16 20.2(7) . . . . ? P51 Cr2 C11 C16 70.4(7) . . . . ? P22 Cr2 C11 C16 -61.7(5) . . . . ? P32 Cr2 C11 C16 -125.3(11) . . . . ? C15 C11 C12 C13 -0.2(3) . . . . ? C16 C11 C12 C13 -177.1(2) . . . . ? Cr2 C11 C12 C13 62.04(16) . . . . ? C15 C11 C12 C17 175.8(2) . . . . ? C16 C11 C12 C17 -1.1(4) . . . . ? Cr2 C11 C12 C17 -122.0(3) . . . . ? C15 C11 C12 Cr2 -62.20(16) . . . . ? C16 C11 C12 Cr2 120.9(2) . . . . ? C15 Cr2 C12 C11 37.22(13) . . . . ? C14 Cr2 C12 C11 79.62(14) . . . . ? C13 Cr2 C12 C11 117.0(2) . . . . ? P21 Cr2 C12 C11 -101.7(5) . . . . ? P31 Cr2 C12 C11 -156.5(5) . . . . ? P41 Cr2 C12 C11 154.0(7) . . . . ? P11 Cr2 C12 C11 -51.3(8) . . . . ? P51 Cr2 C12 C11 32.2(19) . . . . ? P22 Cr2 C12 C11 -131.7(5) . . . . ? P32 Cr2 C12 C11 178.1(5) . . . . ? C11 Cr2 C12 C13 -117.0(2) . . . . ? C15 Cr2 C12 C13 -79.81(14) . . . . ? C14 Cr2 C12 C13 -37.40(13) . . . . ? P21 Cr2 C12 C13 141.3(5) . . . . ? P31 Cr2 C12 C13 86.5(5) . . . . ? P41 Cr2 C12 C13 36.9(7) . . . . ? P11 Cr2 C12 C13 -168.3(8) . . . . ? P51 Cr2 C12 C13 -84.8(19) . . . . ? P22 Cr2 C12 C13 111.2(5) . . . . ? P32 Cr2 C12 C13 61.1(5) . . . . ? C11 Cr2 C12 C17 121.9(3) . . . . ? C15 Cr2 C12 C17 159.1(3) . . . . ? C14 Cr2 C12 C17 -158.5(3) . . . . ? C13 Cr2 C12 C17 -121.1(3) . . . . ? P21 Cr2 C12 C17 20.2(6) . . . . ? P31 Cr2 C12 C17 -34.6(6) . . . . ? P41 Cr2 C12 C17 -84.1(7) . . . . ? P11 Cr2 C12 C17 70.6(8) . . . . ? P51 Cr2 C12 C17 154.1(19) . . . . ? P22 Cr2 C12 C17 -9.8(6) . . . . ? P32 Cr2 C12 C17 -60.0(5) . . . . ? C11 C12 C13 C14 0.1(3) . . . . ? C17 C12 C13 C14 -175.9(2) . . . . ? Cr2 C12 C13 C14 61.95(16) . . . . ? C11 C12 C13 C18 176.4(2) . . . . ? C17 C12 C13 C18 0.4(4) . . . . ? Cr2 C12 C13 C18 -121.8(3) . . . . ? C11 C12 C13 Cr2 -61.81(16) . . . . ? C17 C12 C13 Cr2 122.2(3) . . . . ? C11 Cr2 C13 C14 -79.85(15) . . . . ? C15 Cr2 C13 C14 -37.37(13) . . . . ? C12 Cr2 C13 C14 -117.5(2) . . . . ? P21 Cr2 C13 C14 -168.2(6) . . . . ? P31 Cr2 C13 C14 139.3(6) . . . . ? P41 Cr2 C13 C14 87.1(5) . . . . ? P11 Cr2 C13 C14 -84(2) . . . . ? P51 Cr2 C13 C14 36.6(7) . . . . ? P22 Cr2 C13 C14 164.7(5) . . . . ? P32 Cr2 C13 C14 112.5(5) . . . . ? C11 Cr2 C13 C12 37.68(14) . . . . ? C15 Cr2 C13 C12 80.17(15) . . . . ? C14 Cr2 C13 C12 117.5(2) . . . . ? P21 Cr2 C13 C12 -50.7(6) . . . . ? P31 Cr2 C13 C12 -103.2(6) . . . . ? P41 Cr2 C13 C12 -155.4(5) . . . . ? P11 Cr2 C13 C12 34(2) . . . . ? P51 Cr2 C13 C12 154.1(7) . . . . ? P22 Cr2 C13 C12 -77.7(5) . . . . ? P32 Cr2 C13 C12 -130.0(5) . . . . ? C11 Cr2 C13 C18 159.8(3) . . . . ? C15 Cr2 C13 C18 -157.7(3) . . . . ? C14 Cr2 C13 C18 -120.4(3) . . . . ? C12 Cr2 C13 C18 122.1(3) . . . . ? P21 Cr2 C13 C18 71.4(7) . . . . ? P31 Cr2 C13 C18 18.9(6) . . . . ? P41 Cr2 C13 C18 -33.3(6) . . . . ? P11 Cr2 C13 C18 156(2) . . . . ? P51 Cr2 C13 C18 -83.8(7) . . . . ? P22 Cr2 C13 C18 44.4(6) . . . . ? P32 Cr2 C13 C18 -7.9(5) . . . . ? C12 C13 C14 C15 -0.1(3) . . . . ? C18 C13 C14 C15 -176.4(2) . . . . ? Cr2 C13 C14 C15 61.95(15) . . . . ? C12 C13 C14 C19 176.8(2) . . . . ? C18 C13 C14 C19 0.4(4) . . . . ? Cr2 C13 C14 C19 -121.2(2) . . . . ? C12 C13 C14 Cr2 -62.03(16) . . . . ? C18 C13 C14 Cr2 121.6(3) . . . . ? C11 Cr2 C14 C15 -37.71(14) . . . . ? C13 Cr2 C14 C15 -117.7(2) . . . . ? C12 Cr2 C14 C15 -80.18(15) . . . . ? P21 Cr2 C14 C15 -84.4(17) . . . . ? P31 Cr2 C14 C15 -171.3(6) . . . . ? P41 Cr2 C14 C15 140.7(5) . . . . ? P11 Cr2 C14 C15 37.3(6) . . . . ? P51 Cr2 C14 C15 86.9(5) . . . . ? P22 Cr2 C14 C15 -143.1(7) . . . . ? P32 Cr2 C14 C15 165.6(5) . . . . ? C11 Cr2 C14 C13 79.94(15) . . . . ? C15 Cr2 C14 C13 117.7(2) . . . . ? C12 Cr2 C14 C13 37.47(14) . . . . ? P21 Cr2 C14 C13 33.2(17) . . . . ? P31 Cr2 C14 C13 -53.7(6) . . . . ? P41 Cr2 C14 C13 -101.6(5) . . . . ? P11 Cr2 C14 C13 154.9(6) . . . . ? P51 Cr2 C14 C13 -155.5(5) . . . . ? P22 Cr2 C14 C13 -25.4(7) . . . . ? P32 Cr2 C14 C13 -76.8(5) . . . . ? C11 Cr2 C14 C19 -160.3(3) . . . . ? C15 Cr2 C14 C19 -122.6(3) . . . . ? C13 Cr2 C14 C19 119.8(3) . . . . ? C12 Cr2 C14 C19 157.3(3) . . . . ? P21 Cr2 C14 C19 153.0(17) . . . . ? P31 Cr2 C14 C19 66.1(7) . . . . ? P41 Cr2 C14 C19 18.2(6) . . . . ? P11 Cr2 C14 C19 -85.3(7) . . . . ? P51 Cr2 C14 C19 -35.7(6) . . . . ? P22 Cr2 C14 C19 94.4(7) . . . . ? P32 Cr2 C14 C19 43.0(5) . . . . ? C12 C11 C15 C14 0.1(3) . . . . ? C16 C11 C15 C14 177.1(2) . . . . ? Cr2 C11 C15 C14 -62.21(15) . . . . ? C12 C11 C15 C20 -177.1(2) . . . . ? C16 C11 C15 C20 -0.2(4) . . . . ? Cr2 C11 C15 C20 120.6(2) . . . . ? C12 C11 C15 Cr2 62.32(16) . . . . ? C16 C11 C15 Cr2 -120.7(2) . . . . ? C13 C14 C15 C11 0.0(3) . . . . ? C19 C14 C15 C11 -176.8(2) . . . . ? Cr2 C14 C15 C11 62.01(15) . . . . ? C13 C14 C15 C20 177.2(2) . . . . ? C19 C14 C15 C20 0.4(4) . . . . ? Cr2 C14 C15 C20 -120.8(2) . . . . ? C13 C14 C15 Cr2 -62.03(16) . . . . ? C19 C14 C15 Cr2 121.2(2) . . . . ? C14 Cr2 C15 C11 -117.0(2) . . . . ? C13 Cr2 C15 C11 -79.67(15) . . . . ? C12 Cr2 C15 C11 -37.20(14) . . . . ? P21 Cr2 C15 C11 37.0(6) . . . . ? P31 Cr2 C15 C11 -92(2) . . . . ? P41 Cr2 C15 C11 -168.5(6) . . . . ? P11 Cr2 C15 C11 88.0(5) . . . . ? P51 Cr2 C15 C11 141.3(6) . . . . ? P22 Cr2 C15 C11 -6.5(12) . . . . ? P32 Cr2 C15 C11 -141.6(6) . . . . ? C11 Cr2 C15 C14 117.0(2) . . . . ? C13 Cr2 C15 C14 37.36(14) . . . . ? C12 Cr2 C15 C14 79.84(15) . . . . ? P21 Cr2 C15 C14 154.0(6) . . . . ? P31 Cr2 C15 C14 25(2) . . . . ? P41 Cr2 C15 C14 -51.5(6) . . . . ? P11 Cr2 C15 C14 -155.0(5) . . . . ? P51 Cr2 C15 C14 -101.7(6) . . . . ? P22 Cr2 C15 C14 110.6(12) . . . . ? P32 Cr2 C15 C14 -24.6(7) . . . . ? C11 Cr2 C15 C20 -121.4(3) . . . . ? C14 Cr2 C15 C20 121.6(3) . . . . ? C13 Cr2 C15 C20 158.9(3) . . . . ? C12 Cr2 C15 C20 -158.6(3) . . . . ? P21 Cr2 C15 C20 -84.4(6) . . . . ? P31 Cr2 C15 C20 147(2) . . . . ? P41 Cr2 C15 C20 70.1(7) . . . . ? P11 Cr2 C15 C20 -33.4(5) . . . . ? P51 Cr2 C15 C20 19.9(6) . . . . ? P22 Cr2 C15 C20 -127.9(12) . . . . ? P32 Cr2 C15 C20 97.0(7) . . . . ? _diffrn_measured_fraction_theta_max 0.971 _diffrn_reflns_theta_full 30.47 _diffrn_measured_fraction_theta_full 0.971 _refine_diff_density_max 0.870 _refine_diff_density_min -0.509 _refine_diff_density_rms 0.091 #===END data_230k _database_code_depnum_ccdc_archive 'CCDC 618750' _audit_creation_method SHELXL-97 _chemical_name_systematic ; \m~2~-\h^5^,\h^5^-cyclopentaphosphole)-bis ((\h^5^-pentamethyl-cyclopentadienyl)-chromium) hexafluoroantimonate ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H30 Cr2 F6 P5 Sb' _chemical_formula_weight 765.04 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting orthorhombic _symmetry_space_group_name_H-M Fddd loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+3/4, -y+3/4, z' '-x+3/4, y, -z+3/4' 'x, -y+3/4, -z+3/4' 'x, y+1/2, z+1/2' '-x+3/4, -y+5/4, z+1/2' '-x+3/4, y+1/2, -z+5/4' 'x, -y+5/4, -z+5/4' 'x+1/2, y, z+1/2' '-x+5/4, -y+3/4, z+1/2' '-x+5/4, y, -z+5/4' 'x+1/2, -y+3/4, -z+5/4' 'x+1/2, y+1/2, z' '-x+5/4, -y+5/4, z' '-x+5/4, y+1/2, -z+3/4' 'x+1/2, -y+5/4, -z+3/4' '-x, -y, -z' 'x-3/4, y-3/4, -z' 'x-3/4, -y, z-3/4' '-x, y-3/4, z-3/4' '-x, -y+1/2, -z+1/2' 'x-3/4, y-1/4, -z+1/2' 'x-3/4, -y+1/2, z-1/4' '-x, y-1/4, z-1/4' '-x+1/2, -y, -z+1/2' 'x-1/4, y-3/4, -z+1/2' 'x-1/4, -y, z-1/4' '-x+1/2, y-3/4, z-1/4' '-x+1/2, -y+1/2, -z' 'x-1/4, y-1/4, -z' 'x-1/4, -y+1/2, z-3/4' '-x+1/2, y-1/4, z-3/4' _cell_length_a 21.4191(5) _cell_length_b 29.4937(7) _cell_length_c 36.0191(9) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_volume 22754.3(9) _cell_formula_units_Z 32 _cell_measurement_temperature 230(2) _cell_measurement_reflns_used 9190 _cell_measurement_theta_min 2.21 _cell_measurement_theta_max 30.35 _exptl_crystal_description 'irregular block' _exptl_crystal_colour 'dark green' _exptl_crystal_size_max 0.60 _exptl_crystal_size_mid 0.52 _exptl_crystal_size_min 0.40 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.787 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 12096 _exptl_absorpt_coefficient_mu 2.023 _exptl_absorpt_correction_type integration _exptl_absorpt_correction_T_min 0.398 _exptl_absorpt_correction_T_max 0.617 _exptl_absorpt_process_details 'XPREP in SHELXTL' _exptl_special_details ; ? ; _diffrn_ambient_temperature 230(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'Bede Microsource X-ray Generator' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEX CCD Diffractometer' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number 0 _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% 0 _diffrn_reflns_number 43082 _diffrn_reflns_av_R_equivalents 0.0207 _diffrn_reflns_av_sigmaI/netI 0.0174 _diffrn_reflns_limit_h_min -30 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_k_min -41 _diffrn_reflns_limit_k_max 41 _diffrn_reflns_limit_l_min -46 _diffrn_reflns_limit_l_max 51 _diffrn_reflns_theta_min 1.30 _diffrn_reflns_theta_max 30.47 _reflns_number_total 8405 _reflns_number_gt 6624 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'SMART V5.625 (Bruker, 2003)' _computing_cell_refinement 'SMART V5.625 (Bruker, 2003)' _computing_data_reduction 'SAINT V6.28A (Bruker, 2003)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'SHELXTL V6.12(Bruker, 2001)' _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0521P)^2^+47.3788P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 8405 _refine_ls_number_parameters 404 _refine_ls_number_restraints 90 _refine_ls_R_factor_all 0.0456 _refine_ls_R_factor_gt 0.0318 _refine_ls_wR_factor_ref 0.0996 _refine_ls_wR_factor_gt 0.0848 _refine_ls_goodness_of_fit_ref 1.075 _refine_ls_restrained_S_all 1.071 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb1 Sb 0.6250 0.1250 0.010129(7) 0.04709(8) Uani 1 2 d S . . F1A F 0.6882(4) 0.1035(3) -0.0163(3) 0.154(3) Uani 0.50 1 d P A 1 F2A F 0.5536(3) 0.1393(3) 0.0342(3) 0.154(3) Uani 0.50 1 d P A 1 F1B F 0.6700(5) 0.1188(3) -0.03383(19) 0.147(3) Uani 0.50 1 d P A 2 F2B F 0.5880(5) 0.1424(3) 0.05406(18) 0.147(3) Uani 0.50 1 d P A 2 F3 F 0.59423(16) 0.06621(9) 0.01018(9) 0.1191(10) Uani 1 1 d . A . Sb2 Sb 0.1250 0.239965(11) 0.1250 0.05310(8) Uani 1 2 d S . . F4 F 0.18488(13) 0.28521(10) 0.12100(10) 0.1209(11) Uani 1 1 d . . . F5 F 0.11803(14) 0.23872(10) 0.07344(6) 0.1044(9) Uani 1 1 d . . . F6 F 0.18647(10) 0.19535(9) 0.12241(7) 0.0862(7) Uani 1 1 d . . . C1 C 0.13936(10) 0.37006(7) 0.01251(6) 0.0350(4) Uani 1 1 d . B . C2 C 0.19768(11) 0.34925(7) 0.00428(7) 0.0378(5) Uani 1 1 d . B . C3 C 0.22740(11) 0.37482(9) -0.02431(6) 0.0400(5) Uani 1 1 d . B . C4 C 0.18746(11) 0.41175(9) -0.03349(6) 0.0396(5) Uani 1 1 d . B . C5 C 0.13337(10) 0.40876(8) -0.01086(6) 0.0352(4) Uani 1 1 d . B . C6 C 0.09136(13) 0.35262(10) 0.03929(8) 0.0537(7) Uani 1 1 d . . . H6A H 0.0651 0.3305 0.0269 0.081 Uiso 1 1 calc R . . H6B H 0.0658 0.3776 0.0480 0.081 Uiso 1 1 calc R . . H6C H 0.1121 0.3385 0.0602 0.081 Uiso 1 1 calc R . . C7 C 0.22159(16) 0.30627(9) 0.02134(9) 0.0597(8) Uani 1 1 d . . . H7A H 0.1981 0.2807 0.0117 0.090 Uiso 1 1 calc R . . H7B H 0.2167 0.3077 0.0481 0.090 Uiso 1 1 calc R . . H7C H 0.2654 0.3026 0.0153 0.090 Uiso 1 1 calc R . . C8 C 0.28842(13) 0.36383(13) -0.04269(9) 0.0634(9) Uani 1 1 d . . . H8A H 0.2811 0.3440 -0.0637 0.095 Uiso 1 1 calc R . . H8B H 0.3156 0.3487 -0.0251 0.095 Uiso 1 1 calc R . . H8C H 0.3080 0.3916 -0.0511 0.095 Uiso 1 1 calc R . . C9 C 0.19763(17) 0.44616(13) -0.06331(8) 0.0669(9) Uani 1 1 d . . . H9A H 0.1752 0.4371 -0.0855 0.100 Uiso 1 1 calc R . . H9B H 0.2419 0.4483 -0.0688 0.100 Uiso 1 1 calc R . . H9C H 0.1825 0.4754 -0.0550 0.100 Uiso 1 1 calc R . . C10 C 0.07747(13) 0.43901(10) -0.01330(9) 0.0535(7) Uani 1 1 d . . . H10A H 0.0521 0.4301 -0.0344 0.080 Uiso 1 1 calc R . . H10B H 0.0910 0.4702 -0.0164 0.080 Uiso 1 1 calc R . . H10C H 0.0531 0.4364 0.0093 0.080 Uiso 1 1 calc R . . Cr1 Cr 0.215720(15) 0.418104(11) 0.025003(9) 0.02868(8) Uani 1 1 d . . . P11 P 0.1855(9) 0.4380(7) 0.0868(4) 0.069(5) Uani 0.25 1 d PU B 1 P21 P 0.2696(8) 0.3981(4) 0.0820(5) 0.063(5) Uani 0.25 1 d PU B 1 P31 P 0.3231(5) 0.4301(6) 0.0389(5) 0.059(5) Uani 0.25 1 d PU B 1 P41 P 0.2763(10) 0.4879(6) 0.0181(4) 0.080(6) Uani 0.25 1 d PU B 1 P51 P 0.1913(8) 0.4932(7) 0.0495(6) 0.065(5) Uani 0.25 1 d PU B 1 P1 P 0.1980(5) 0.4233(3) 0.0916(2) 0.058(2) Uani 0.50 1 d PU B 2 P2 P 0.2886(4) 0.3966(3) 0.0732(2) 0.054(2) Uani 0.50 1 d PU B 2 P3 P 0.3249(4) 0.4418(4) 0.0305(3) 0.057(2) Uani 0.50 1 d PU B 2 P4 P 0.2571(4) 0.49501(19) 0.02213(16) 0.055(2) Uani 0.50 1 d PU B 2 P5 P 0.1794(3) 0.4841(3) 0.0596(3) 0.056(3) Uani 0.50 1 d PU B 2 P12 P 0.2223(7) 0.4079(4) 0.0927(2) 0.067(3) Uani 0.25 1 d PU B 3 P22 P 0.3114(5) 0.4049(4) 0.0607(4) 0.067(3) Uani 0.25 1 d PU B 3 P32 P 0.3149(6) 0.4606(5) 0.0227(3) 0.075(4) Uani 0.25 1 d PU B 3 P42 P 0.2293(7) 0.4997(3) 0.0301(3) 0.064(3) Uani 0.25 1 d PU B 3 P52 P 0.1723(4) 0.4682(5) 0.0724(4) 0.063(4) Uani 0.25 1 d PU B 3 Cr2 Cr 0.283203(15) 0.478113(11) 0.086435(9) 0.02833(8) Uani 1 1 d . . . C11 C 0.29481(11) 0.49149(8) 0.14608(6) 0.0377(5) Uani 1 1 d . B . C12 C 0.35427(11) 0.48051(8) 0.13099(7) 0.0390(5) Uani 1 1 d . B . C13 C 0.36869(10) 0.51410(8) 0.10385(7) 0.0369(5) Uani 1 1 d . B . C14 C 0.31847(10) 0.54557(7) 0.10254(6) 0.0336(4) Uani 1 1 d . B . C15 C 0.27256(10) 0.53161(7) 0.12872(6) 0.0339(4) Uani 1 1 d . B . C16 C 0.26241(17) 0.46619(11) 0.17672(7) 0.0617(8) Uani 1 1 d . . . H16A H 0.2766 0.4776 0.2005 0.093 Uiso 1 1 calc R B . H16B H 0.2721 0.4341 0.1748 0.093 Uiso 1 1 calc R . . H16C H 0.2177 0.4705 0.1746 0.093 Uiso 1 1 calc R . . C17 C 0.39610(17) 0.44258(10) 0.14294(11) 0.0681(9) Uani 1 1 d . . . H17A H 0.4224 0.4527 0.1632 0.102 Uiso 1 1 calc R B . H17B H 0.4221 0.4333 0.1222 0.102 Uiso 1 1 calc R . . H17C H 0.3709 0.4171 0.1511 0.102 Uiso 1 1 calc R . . C18 C 0.42809(12) 0.51797(13) 0.08215(9) 0.0620(8) Uani 1 1 d . . . H18A H 0.4563 0.5386 0.0947 0.093 Uiso 1 1 calc R B . H18B H 0.4190 0.5294 0.0575 0.093 Uiso 1 1 calc R . . H18C H 0.4475 0.4883 0.0802 0.093 Uiso 1 1 calc R . . C19 C 0.31701(16) 0.58734(9) 0.07905(8) 0.0532(7) Uani 1 1 d . . . H19A H 0.3367 0.6121 0.0923 0.080 Uiso 1 1 calc R B . H19B H 0.2740 0.5952 0.0735 0.080 Uiso 1 1 calc R . . H19C H 0.3394 0.5818 0.0561 0.080 Uiso 1 1 calc R . . C20 C 0.21309(12) 0.55594(10) 0.13774(9) 0.0524(7) Uani 1 1 d . . . H20A H 0.2204 0.5771 0.1579 0.079 Uiso 1 1 calc R B . H20B H 0.1816 0.5341 0.1451 0.079 Uiso 1 1 calc R . . H20C H 0.1988 0.5724 0.1160 0.079 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.03827(12) 0.05829(15) 0.04471(14) 0.000 0.000 0.00390(10) F1A 0.100(3) 0.158(5) 0.204(7) -0.041(4) 0.091(4) 0.019(3) F2A 0.100(3) 0.158(5) 0.204(7) -0.041(4) 0.091(4) 0.019(3) F1B 0.249(8) 0.107(3) 0.085(3) -0.012(2) 0.096(4) -0.020(4) F2B 0.249(8) 0.107(3) 0.085(3) -0.012(2) 0.096(4) -0.020(4) F3 0.141(3) 0.0721(15) 0.145(3) 0.0128(16) -0.039(2) -0.0311(16) Sb2 0.04278(13) 0.06360(17) 0.05291(16) 0.000 0.00866(11) 0.000 F4 0.0976(19) 0.104(2) 0.161(3) -0.0331(19) 0.0303(18) -0.0487(16) F5 0.139(2) 0.120(2) 0.0539(13) 0.0228(13) -0.0012(13) -0.0261(17) F6 0.0668(13) 0.1023(17) 0.0895(16) -0.0256(13) 0.0001(11) 0.0235(12) C1 0.0355(10) 0.0338(10) 0.0357(11) -0.0055(8) -0.0043(8) -0.0014(8) C2 0.0413(11) 0.0328(10) 0.0394(12) -0.0099(9) -0.0092(9) 0.0067(9) C3 0.0338(10) 0.0529(13) 0.0334(11) -0.0151(10) -0.0024(9) 0.0060(9) C4 0.0410(11) 0.0491(12) 0.0286(10) 0.0006(9) -0.0052(9) -0.0008(10) C5 0.0327(10) 0.0371(10) 0.0359(11) -0.0038(8) -0.0088(8) 0.0053(8) C6 0.0519(15) 0.0565(15) 0.0527(16) -0.0015(13) 0.0068(12) -0.0148(12) C7 0.0754(19) 0.0339(12) 0.070(2) -0.0053(12) -0.0226(16) 0.0165(12) C8 0.0405(13) 0.093(2) 0.0564(18) -0.0317(17) 0.0052(12) 0.0089(14) C9 0.078(2) 0.084(2) 0.0392(15) 0.0226(15) -0.0083(14) -0.0099(18) C10 0.0442(13) 0.0546(15) 0.0618(17) -0.0069(13) -0.0179(12) 0.0179(11) Cr1 0.02850(15) 0.02972(15) 0.02781(16) -0.00128(12) -0.00259(12) 0.00360(12) P11 0.064(8) 0.108(14) 0.035(6) -0.021(7) 0.017(5) -0.052(9) P21 0.112(13) 0.025(2) 0.051(7) 0.001(3) -0.043(7) 0.002(5) P31 0.024(2) 0.086(10) 0.068(10) -0.045(8) 0.010(4) -0.005(4) P41 0.124(13) 0.078(9) 0.039(2) -0.005(4) 0.008(5) -0.057(8) P51 0.062(10) 0.049(6) 0.085(14) -0.030(7) -0.039(8) 0.031(8) P1 0.070(4) 0.074(5) 0.0297(19) 0.000(3) 0.004(2) -0.040(3) P2 0.069(4) 0.0354(12) 0.057(5) -0.008(2) -0.033(3) 0.018(2) P3 0.0382(13) 0.084(5) 0.049(4) -0.027(3) 0.0193(15) -0.023(2) P4 0.089(5) 0.039(2) 0.035(3) 0.012(2) -0.013(3) -0.016(3) P5 0.031(2) 0.068(7) 0.069(7) -0.034(4) -0.008(3) 0.016(3) P12 0.114(9) 0.054(5) 0.032(2) 0.006(3) -0.017(5) -0.042(5) P22 0.053(5) 0.063(6) 0.084(8) -0.041(5) -0.036(4) 0.034(4) P32 0.078(6) 0.103(8) 0.042(4) -0.023(5) 0.017(4) -0.050(6) P42 0.099(9) 0.0328(17) 0.061(7) 0.004(4) -0.043(6) 0.002(6) P52 0.0274(16) 0.090(9) 0.070(8) -0.048(6) 0.006(4) -0.003(5) Cr2 0.02815(15) 0.02876(15) 0.02807(16) -0.00207(12) -0.00019(12) -0.00006(11) C11 0.0469(12) 0.0383(10) 0.0279(10) -0.0005(8) -0.0017(9) -0.0125(9) C12 0.0411(11) 0.0357(10) 0.0402(12) -0.0052(9) -0.0135(9) 0.0005(9) C13 0.0299(9) 0.0444(11) 0.0363(11) -0.0096(9) 0.0015(8) -0.0051(8) C14 0.0370(10) 0.0314(9) 0.0323(10) -0.0021(8) 0.0006(8) -0.0063(8) C15 0.0330(10) 0.0358(10) 0.0329(10) -0.0084(8) 0.0039(8) -0.0047(8) C16 0.085(2) 0.0667(18) 0.0334(13) 0.0066(12) 0.0000(13) -0.0374(17) C17 0.076(2) 0.0482(15) 0.080(2) -0.0114(15) -0.0415(18) 0.0184(14) C18 0.0348(12) 0.091(2) 0.0603(18) -0.0238(16) 0.0123(12) -0.0125(13) C19 0.0744(18) 0.0354(11) 0.0497(15) 0.0081(10) -0.0039(13) -0.0128(12) C20 0.0384(12) 0.0548(15) 0.0640(17) -0.0262(13) 0.0089(12) 0.0018(11) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb1 F1A 1.771(6) 14_545 ? Sb1 F1A 1.771(6) . ? Sb1 F2A 1.808(6) . ? Sb1 F2A 1.808(6) 14_545 ? Sb1 F2B 1.843(6) . ? Sb1 F2B 1.843(6) 14_545 ? Sb1 F3 1.855(2) 14_545 ? Sb1 F3 1.855(2) . ? Sb1 F1B 1.863(6) . ? Sb1 F1B 1.863(6) 14_545 ? Sb2 F4 1.856(2) 11_454 ? Sb2 F4 1.857(2) . ? Sb2 F5 1.863(2) 11_454 ? Sb2 F5 1.864(2) . ? Sb2 F6 1.864(2) 11_454 ? Sb2 F6 1.864(2) . ? C1 C2 1.423(3) . ? C1 C5 1.424(3) . ? C1 C6 1.501(3) . ? C1 Cr1 2.210(2) . ? C2 C3 1.426(4) . ? C2 C7 1.499(3) . ? C2 Cr1 2.198(2) . ? C3 C4 1.424(3) . ? C3 C8 1.501(3) . ? C3 Cr1 2.202(2) . ? C4 C5 1.419(3) . ? C4 C9 1.494(4) . ? C4 Cr1 2.200(2) . ? C5 C10 1.496(3) . ? C5 Cr1 2.204(2) . ? C6 H6A 0.9700 . ? C6 H6B 0.9700 . ? C6 H6C 0.9700 . ? C7 H7A 0.9700 . ? C7 H7B 0.9700 . ? C7 H7C 0.9700 . ? C8 H8A 0.9700 . ? C8 H8B 0.9700 . ? C8 H8C 0.9700 . ? C9 H9A 0.9700 . ? C9 H9B 0.9700 . ? C9 H9C 0.9700 . ? C10 H10A 0.9700 . ? C10 H10B 0.9700 . ? C10 H10C 0.9700 . ? Cr1 P31 2.379(13) . ? Cr1 P11 2.391(17) . ? Cr1 P2 2.420(7) . ? Cr1 P21 2.428(15) . ? Cr1 P42 2.432(9) . ? Cr1 P1 2.433(9) . ? Cr1 P4 2.437(6) . ? P11 P51 2.11(2) . ? P11 P21 2.16(2) . ? P11 Cr2 2.403(16) . ? P21 P31 2.147(18) . ? P21 Cr2 2.384(12) . ? P31 P41 2.11(2) . ? P31 Cr2 2.381(14) . ? P41 P51 2.148(18) . ? P41 Cr2 2.481(15) . ? P51 Cr2 2.417(19) . ? P1 P5 2.168(10) . ? P1 P2 2.196(10) . ? P1 Cr2 2.446(8) . ? P2 P3 2.178(9) . ? P2 Cr2 2.453(7) . ? P3 P4 2.161(12) . ? P3 Cr2 2.449(9) . ? P4 P5 2.167(8) . ? P4 Cr2 2.434(5) . ? P5 Cr2 2.430(8) . ? P12 P52 2.200(12) . ? P12 P22 2.232(11) . ? P12 Cr2 2.457(8) . ? P22 P32 2.138(12) . ? P22 Cr2 2.426(7) . ? P32 P42 2.183(13) . ? P32 Cr2 2.449(9) . ? P42 P52 2.165(11) . ? P42 Cr2 2.421(8) . ? P52 Cr2 2.446(9) . ? Cr2 C11 2.198(2) . ? Cr2 C15 2.205(2) . ? Cr2 C14 2.206(2) . ? Cr2 C13 2.207(2) . ? Cr2 C12 2.213(2) . ? C11 C15 1.421(3) . ? C11 C12 1.422(3) . ? C11 C16 1.502(3) . ? C12 C13 1.426(3) . ? C12 C17 1.497(3) . ? C13 C14 1.422(3) . ? C13 C18 1.498(3) . ? C14 C15 1.423(3) . ? C14 C19 1.495(3) . ? C15 C20 1.498(3) . ? C16 H16A 0.9700 . ? C16 H16B 0.9700 . ? C16 H16C 0.9700 . ? C17 H17A 0.9700 . ? C17 H17B 0.9700 . ? C17 H17C 0.9700 . ? C18 H18A 0.9700 . ? C18 H18B 0.9700 . ? C18 H18C 0.9700 . ? C19 H19A 0.9700 . ? C19 H19B 0.9700 . ? C19 H19C 0.9700 . ? C20 H20A 0.9700 . ? C20 H20B 0.9700 . ? C20 H20C 0.9700 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F1A Sb1 F1A 115.1(7) 14_545 . ? F1A Sb1 F2A 61.8(5) 14_545 . ? F1A Sb1 F2A 170.8(4) . . ? F1A Sb1 F2A 170.8(4) 14_545 14_545 ? F1A Sb1 F2A 61.8(5) . 14_545 ? F2A Sb1 F2A 122.7(7) . 14_545 ? F1A Sb1 F2B 91.9(5) 14_545 . ? F1A Sb1 F2B 152.8(5) . . ? F2A Sb1 F2B 32.8(4) . . ? F2A Sb1 F2B 91.0(5) 14_545 . ? F1A Sb1 F2B 152.8(5) 14_545 14_545 ? F1A Sb1 F2B 91.9(5) . 14_545 ? F2A Sb1 F2B 91.0(5) . 14_545 ? F2A Sb1 F2B 32.8(4) 14_545 14_545 ? F2B Sb1 F2B 61.6(6) . 14_545 ? F1A Sb1 F3 86.5(3) 14_545 14_545 ? F1A Sb1 F3 93.6(3) . 14_545 ? F2A Sb1 F3 94.8(3) . 14_545 ? F2A Sb1 F3 85.2(3) 14_545 14_545 ? F2B Sb1 F3 83.8(3) . 14_545 ? F2B Sb1 F3 96.1(3) 14_545 14_545 ? F1A Sb1 F3 93.6(3) 14_545 . ? F1A Sb1 F3 86.5(3) . . ? F2A Sb1 F3 85.2(3) . . ? F2A Sb1 F3 94.7(3) 14_545 . ? F2B Sb1 F3 96.1(3) . . ? F2B Sb1 F3 83.8(3) 14_545 . ? F3 Sb1 F3 179.9(2) 14_545 . ? F1A Sb1 F1B 88.5(5) 14_545 . ? F1A Sb1 F1B 27.6(4) . . ? F2A Sb1 F1B 150.2(5) . . ? F2A Sb1 F1B 87.0(5) 14_545 . ? F2B Sb1 F1B 168.5(4) . . ? F2B Sb1 F1B 118.7(5) 14_545 . ? F3 Sb1 F1B 84.7(3) 14_545 . ? F3 Sb1 F1B 95.4(3) . . ? F1A Sb1 F1B 27.6(4) 14_545 14_545 ? F1A Sb1 F1B 88.5(5) . 14_545 ? F2A Sb1 F1B 87.0(5) . 14_545 ? F2A Sb1 F1B 150.2(5) 14_545 14_545 ? F2B Sb1 F1B 118.7(5) . 14_545 ? F2B Sb1 F1B 168.5(4) 14_545 14_545 ? F3 Sb1 F1B 95.4(3) 14_545 14_545 ? F3 Sb1 F1B 84.7(3) . 14_545 ? F1B Sb1 F1B 63.5(7) . 14_545 ? F4 Sb2 F4 88.1(2) 11_454 . ? F4 Sb2 F5 89.56(14) 11_454 11_454 ? F4 Sb2 F5 92.07(15) . 11_454 ? F4 Sb2 F5 92.07(15) 11_454 . ? F4 Sb2 F5 89.55(14) . . ? F5 Sb2 F5 177.74(18) 11_454 . ? F4 Sb2 F6 90.90(13) 11_454 11_454 ? F4 Sb2 F6 178.05(14) . 11_454 ? F5 Sb2 F6 89.59(13) 11_454 11_454 ? F5 Sb2 F6 88.82(11) . 11_454 ? F4 Sb2 F6 178.05(14) 11_454 . ? F4 Sb2 F6 90.89(13) . . ? F5 Sb2 F6 88.82(11) 11_454 . ? F5 Sb2 F6 89.59(13) . . ? F6 Sb2 F6 90.17(16) 11_454 . ? C2 C1 C5 107.6(2) . . ? C2 C1 C6 126.0(2) . . ? C5 C1 C6 126.4(2) . . ? C2 C1 Cr1 70.69(12) . . ? C5 C1 Cr1 70.92(12) . . ? C6 C1 Cr1 126.58(17) . . ? C1 C2 C3 108.3(2) . . ? C1 C2 C7 125.4(3) . . ? C3 C2 C7 126.2(2) . . ? C1 C2 Cr1 71.64(12) . . ? C3 C2 Cr1 71.23(13) . . ? C7 C2 Cr1 125.60(17) . . ? C4 C3 C2 107.7(2) . . ? C4 C3 C8 125.9(3) . . ? C2 C3 C8 126.4(3) . . ? C4 C3 Cr1 71.06(13) . . ? C2 C3 Cr1 70.94(12) . . ? C8 C3 Cr1 125.46(18) . . ? C5 C4 C3 108.0(2) . . ? C5 C4 C9 125.0(2) . . ? C3 C4 C9 126.8(3) . . ? C5 C4 Cr1 71.34(13) . . ? C3 C4 Cr1 71.19(13) . . ? C9 C4 Cr1 126.2(2) . . ? C4 C5 C1 108.40(19) . . ? C4 C5 C10 125.6(2) . . ? C1 C5 C10 125.8(2) . . ? C4 C5 Cr1 71.06(12) . . ? C1 C5 Cr1 71.43(12) . . ? C10 C5 Cr1 126.91(17) . . ? C1 C6 H6A 109.5 . . ? C1 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C1 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C2 Cr1 C4 63.11(9) . . ? C2 Cr1 C3 37.83(10) . . ? C4 Cr1 C3 37.75(9) . . ? C2 Cr1 C5 62.91(8) . . ? C4 Cr1 C5 37.60(9) . . ? C3 Cr1 C5 62.97(8) . . ? C2 Cr1 C1 37.66(8) . . ? C4 Cr1 C1 63.05(9) . . ? C3 Cr1 C1 63.13(9) . . ? C5 Cr1 C1 37.65(8) . . ? C2 Cr1 P31 112.2(4) . . ? C4 Cr1 P31 118.7(4) . . ? C3 Cr1 P31 98.4(4) . . ? C5 Cr1 P31 156.2(4) . . ? C1 Cr1 P31 148.6(4) . . ? C2 Cr1 P11 119.7(4) . . ? C4 Cr1 P11 146.9(5) . . ? C3 Cr1 P11 157.6(4) . . ? C5 Cr1 P11 111.1(5) . . ? C1 Cr1 P11 98.5(4) . . ? P31 Cr1 P11 91.7(5) . . ? C2 Cr1 P2 96.62(18) . . ? C4 Cr1 P2 147.41(19) . . ? C3 Cr1 P2 110.73(18) . . ? C5 Cr1 P2 154.8(2) . . ? C1 Cr1 P2 117.1(2) . . ? P31 Cr1 P2 42.7(4) . . ? P11 Cr1 P2 64.6(5) . . ? C2 Cr1 P21 98.4(3) . . ? C4 Cr1 P21 156.9(3) . . ? C3 Cr1 P21 119.1(3) . . ? C5 Cr1 P21 147.8(4) . . ? C1 Cr1 P21 111.6(4) . . ? P31 Cr1 P21 53.0(5) . . ? P11 Cr1 P21 53.2(5) . . ? P2 Cr1 P21 12.2(4) . . ? C2 Cr1 P42 164.0(2) . . ? C4 Cr1 P42 100.9(2) . . ? C3 Cr1 P42 128.4(3) . . ? C5 Cr1 P42 105.3(2) . . ? C1 Cr1 P42 137.6(3) . . ? P31 Cr1 P42 73.8(5) . . ? P11 Cr1 P42 73.7(4) . . ? P2 Cr1 P42 97.4(3) . . ? P21 Cr1 P42 96.9(3) . . ? C2 Cr1 P1 111.4(2) . . ? C4 Cr1 P1 155.0(2) . . ? C3 Cr1 P1 148.1(2) . . ? C5 Cr1 P1 117.4(2) . . ? C1 Cr1 P1 97.2(2) . . ? P31 Cr1 P1 86.2(4) . . ? P11 Cr1 P1 12.8(5) . . ? P2 Cr1 P1 53.8(2) . . ? P21 Cr1 P1 42.0(4) . . ? P42 Cr1 P1 83.3(3) . . ? C2 Cr1 P4 155.43(19) . . ? C4 Cr1 P4 97.97(14) . . ? C3 Cr1 P4 117.66(18) . . ? C5 Cr1 P4 112.48(16) . . ? C1 Cr1 P4 148.97(18) . . ? P31 Cr1 P4 61.3(4) . . ? P11 Cr1 P4 84.8(4) . . ? P2 Cr1 P4 92.3(2) . . ? P21 Cr1 P4 95.1(3) . . ? P42 Cr1 P4 15.9(3) . . ? P1 Cr1 P4 92.3(2) . . ? P51 P11 P21 108.7(8) . . ? P51 P11 Cr1 65.2(6) . . ? P21 P11 Cr1 64.2(6) . . ? P51 P11 Cr2 64.3(6) . . ? P21 P11 Cr2 62.7(6) . . ? Cr1 P11 Cr2 83.1(5) . . ? P31 P21 P11 105.2(7) . . ? P31 P21 Cr2 63.1(5) . . ? P11 P21 Cr2 63.6(5) . . ? P31 P21 Cr1 62.3(5) . . ? P11 P21 Cr1 62.5(5) . . ? Cr2 P21 Cr1 82.8(4) . . ? P41 P31 P21 111.0(7) . . ? P41 P31 Cr1 65.6(6) . . ? P21 P31 Cr1 64.6(5) . . ? P41 P31 Cr2 66.7(6) . . ? P21 P31 Cr2 63.3(4) . . ? Cr1 P31 Cr2 83.9(4) . . ? P31 P41 P51 106.0(8) . . ? P31 P41 Cr1 62.4(5) . . ? P51 P41 Cr1 63.8(6) . . ? P31 P41 Cr2 61.8(6) . . ? P51 P41 Cr2 62.5(6) . . ? Cr1 P41 Cr2 80.4(4) . . ? P11 P51 P41 109.1(8) . . ? P11 P51 Cr2 63.6(7) . . ? P41 P51 Cr2 65.5(6) . . ? P11 P51 Cr1 62.9(7) . . ? P41 P51 Cr1 64.0(6) . . ? Cr2 P51 Cr1 81.8(5) . . ? P5 P1 P2 107.4(4) . . ? P5 P1 Cr1 63.7(3) . . ? P2 P1 Cr1 62.8(3) . . ? P5 P1 Cr2 63.2(3) . . ? P2 P1 Cr2 63.5(3) . . ? Cr1 P1 Cr2 81.4(3) . . ? P3 P2 P1 108.0(4) . . ? P3 P2 Cr1 64.1(3) . . ? P1 P2 Cr1 63.4(2) . . ? P3 P2 Cr2 63.5(3) . . ? P1 P2 Cr2 63.2(2) . . ? Cr1 P2 Cr2 81.5(2) . . ? P4 P3 P2 107.6(4) . . ? P4 P3 Cr1 63.5(3) . . ? P2 P3 Cr1 62.7(2) . . ? P4 P3 Cr2 63.4(3) . . ? P2 P3 Cr2 63.7(3) . . ? Cr1 P3 Cr2 81.0(2) . . ? P3 P4 P5 108.7(4) . . ? P3 P4 Cr2 64.1(3) . . ? P5 P4 Cr2 63.4(3) . . ? P3 P4 Cr1 64.0(2) . . ? P5 P4 Cr1 63.7(3) . . ? Cr2 P4 Cr1 81.53(14) . . ? P4 P5 P1 108.2(5) . . ? P4 P5 Cr2 63.6(2) . . ? P1 P5 Cr2 64.0(4) . . ? P4 P5 Cr1 63.6(2) . . ? P1 P5 Cr1 63.4(4) . . ? Cr2 P5 Cr1 81.6(2) . . ? P52 P12 P22 106.1(5) . . ? P52 P12 Cr2 63.1(3) . . ? P22 P12 Cr2 62.1(3) . . ? P52 P12 Cr1 62.9(3) . . ? P22 P12 Cr1 62.8(3) . . ? Cr2 P12 Cr1 80.6(2) . . ? P32 P22 P12 109.3(5) . . ? P32 P22 Cr2 64.5(3) . . ? P12 P22 Cr2 63.5(3) . . ? P32 P22 Cr1 64.7(4) . . ? P12 P22 Cr1 63.2(3) . . ? Cr2 P22 Cr1 81.4(2) . . ? P22 P32 P42 107.4(5) . . ? P22 P32 Cr2 63.4(3) . . ? P42 P32 Cr2 62.7(3) . . ? P22 P32 Cr1 63.8(3) . . ? P42 P32 Cr1 62.7(4) . . ? Cr2 P32 Cr1 80.6(3) . . ? P52 P42 P32 109.4(5) . . ? P52 P42 Cr2 64.2(4) . . ? P32 P42 Cr2 64.0(3) . . ? P52 P42 Cr1 63.9(4) . . ? P32 P42 Cr1 64.4(3) . . ? Cr2 P42 Cr1 81.9(2) . . ? P42 P52 P12 107.9(5) . . ? P42 P52 Cr1 63.4(3) . . ? P12 P52 Cr1 63.8(4) . . ? P42 P52 Cr2 63.0(3) . . ? P12 P52 Cr2 63.6(4) . . ? Cr1 P52 Cr2 81.2(3) . . ? C11 Cr2 C15 37.64(9) . . ? C11 Cr2 C14 62.77(8) . . ? C15 Cr2 C14 37.65(8) . . ? C11 Cr2 C13 62.75(8) . . ? C15 Cr2 C13 62.96(8) . . ? C14 Cr2 C13 37.58(8) . . ? C11 Cr2 C12 37.61(9) . . ? C15 Cr2 C12 63.08(8) . . ? C14 Cr2 C12 62.93(8) . . ? C13 Cr2 C12 37.63(9) . . ? C11 Cr2 P31 140.3(4) . . ? C15 Cr2 P31 163.7(3) . . ? C14 Cr2 P31 127.1(4) . . ? C13 Cr2 P31 101.1(3) . . ? C12 Cr2 P31 107.1(4) . . ? C11 Cr2 P21 104.9(4) . . ? C15 Cr2 P21 137.9(4) . . ? C14 Cr2 P21 162.3(4) . . ? C13 Cr2 P21 126.6(4) . . ? C12 Cr2 P21 99.5(4) . . ? P31 Cr2 P21 53.6(5) . . ? C11 Cr2 P11 100.4(4) . . ? C15 Cr2 P11 105.0(5) . . ? C14 Cr2 P11 137.8(5) . . ? C13 Cr2 P11 163.2(4) . . ? C12 Cr2 P11 127.6(4) . . ? P31 Cr2 P11 91.4(5) . . ? P21 Cr2 P11 53.6(5) . . ? C11 Cr2 P51 126.7(5) . . ? C15 Cr2 P51 99.5(4) . . ? C14 Cr2 P51 104.9(5) . . ? C13 Cr2 P51 138.0(5) . . ? C12 Cr2 P51 162.5(4) . . ? P31 Cr2 P51 90.3(6) . . ? P21 Cr2 P51 92.6(6) . . ? P11 Cr2 P51 52.0(5) . . ? C11 Cr2 P42 145.7(3) . . ? C15 Cr2 P42 110.0(3) . . ? C14 Cr2 P42 98.4(2) . . ? C13 Cr2 P42 120.5(3) . . ? C12 Cr2 P42 158.1(3) . . ? P31 Cr2 P42 74.0(5) . . ? P21 Cr2 P42 98.4(4) . . ? P11 Cr2 P42 73.7(4) . . ? P51 Cr2 P42 26.0(5) . . ? C11 Cr2 P22 120.3(3) . . ? C15 Cr2 P22 157.9(3) . . ? C14 Cr2 P22 144.9(3) . . ? C13 Cr2 P22 109.2(3) . . ? C12 Cr2 P22 97.71(18) . . ? P31 Cr2 P22 26.7(5) . . ? P21 Cr2 P22 28.8(4) . . ? P11 Cr2 P22 77.4(5) . . ? P51 Cr2 P22 99.0(5) . . ? P42 Cr2 P22 91.9(3) . . ? C11 Cr2 P5 118.6(2) . . ? C15 Cr2 P5 97.3(2) . . ? C14 Cr2 P5 110.6(2) . . ? C13 Cr2 P5 146.8(3) . . ? C12 Cr2 P5 156.2(2) . . ? P31 Cr2 P5 94.9(4) . . ? P21 Cr2 P5 86.2(4) . . ? P11 Cr2 P5 40.6(4) . . ? P51 Cr2 P5 12.3(6) . . ? P42 Cr2 P5 38.0(3) . . ? P22 Cr2 P5 98.1(3) . . ? C15 C11 C12 108.8(2) . . ? C15 C11 C16 125.6(3) . . ? C12 C11 C16 125.6(3) . . ? C15 C11 Cr2 71.42(12) . . ? C12 C11 Cr2 71.75(13) . . ? C16 C11 Cr2 125.22(16) . . ? C11 C12 C13 107.3(2) . . ? C11 C12 C17 126.6(3) . . ? C13 C12 C17 125.9(3) . . ? C11 C12 Cr2 70.63(13) . . ? C13 C12 Cr2 70.98(13) . . ? C17 C12 Cr2 126.62(18) . . ? C14 C13 C12 108.22(19) . . ? C14 C13 C18 125.2(2) . . ? C12 C13 C18 126.5(2) . . ? C14 C13 Cr2 71.15(12) . . ? C12 C13 Cr2 71.40(12) . . ? C18 C13 Cr2 126.37(17) . . ? C13 C14 C15 108.17(19) . . ? C13 C14 C19 124.9(2) . . ? C15 C14 C19 126.8(2) . . ? C13 C14 Cr2 71.27(12) . . ? C15 C14 Cr2 71.13(12) . . ? C19 C14 Cr2 125.97(17) . . ? C11 C15 C14 107.52(19) . . ? C11 C15 C20 126.1(2) . . ? C14 C15 C20 126.3(2) . . ? C11 C15 Cr2 70.94(12) . . ? C14 C15 Cr2 71.22(12) . . ? C20 C15 Cr2 125.50(16) . . ? C11 C16 H16A 109.5 . . ? C11 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C11 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 C1 C2 C3 -0.5(2) . . . . ? C6 C1 C2 C3 176.1(2) . . . . ? Cr1 C1 C2 C3 -62.16(15) . . . . ? C5 C1 C2 C7 -177.2(2) . . . . ? C6 C1 C2 C7 -0.6(4) . . . . ? Cr1 C1 C2 C7 121.1(2) . . . . ? C5 C1 C2 Cr1 61.70(15) . . . . ? C6 C1 C2 Cr1 -121.7(2) . . . . ? C1 C2 C3 C4 0.5(3) . . . . ? C7 C2 C3 C4 177.2(2) . . . . ? Cr1 C2 C3 C4 -61.92(16) . . . . ? C1 C2 C3 C8 -177.1(2) . . . . ? C7 C2 C3 C8 -0.4(4) . . . . ? Cr1 C2 C3 C8 120.5(2) . . . . ? C1 C2 C3 Cr1 62.43(15) . . . . ? C7 C2 C3 Cr1 -120.9(2) . . . . ? C2 C3 C4 C5 -0.4(3) . . . . ? C8 C3 C4 C5 177.2(2) . . . . ? Cr1 C3 C4 C5 -62.20(16) . . . . ? C2 C3 C4 C9 -176.5(3) . . . . ? C8 C3 C4 C9 1.1(4) . . . . ? Cr1 C3 C4 C9 121.6(3) . . . . ? C2 C3 C4 Cr1 61.84(15) . . . . ? C8 C3 C4 Cr1 -120.6(3) . . . . ? C3 C4 C5 C1 0.1(3) . . . . ? C9 C4 C5 C1 176.3(2) . . . . ? Cr1 C4 C5 C1 -62.03(15) . . . . ? C3 C4 C5 C10 -175.5(2) . . . . ? C9 C4 C5 C10 0.7(4) . . . . ? Cr1 C4 C5 C10 122.4(2) . . . . ? C3 C4 C5 Cr1 62.10(16) . . . . ? C9 C4 C5 Cr1 -121.7(3) . . . . ? C2 C1 C5 C4 0.2(2) . . . . ? C6 C1 C5 C4 -176.3(2) . . . . ? Cr1 C1 C5 C4 61.80(16) . . . . ? C2 C1 C5 C10 175.8(2) . . . . ? C6 C1 C5 C10 -0.7(4) . . . . ? Cr1 C1 C5 C10 -122.6(2) . . . . ? C2 C1 C5 Cr1 -61.55(15) . . . . ? C6 C1 C5 Cr1 121.9(2) . . . . ? C1 C2 Cr1 C4 -79.95(15) . . . . ? C3 C2 Cr1 C4 37.59(13) . . . . ? C7 C2 Cr1 C4 159.2(3) . . . . ? C1 C2 Cr1 C3 -117.54(19) . . . . ? C7 C2 Cr1 C3 121.6(3) . . . . ? C1 C2 Cr1 C5 -37.54(13) . . . . ? C3 C2 Cr1 C5 80.00(14) . . . . ? C7 C2 Cr1 C5 -158.4(3) . . . . ? C3 C2 Cr1 C1 117.54(19) . . . . ? C7 C2 Cr1 C1 -120.9(3) . . . . ? C1 C2 Cr1 P31 168.1(5) . . . . ? C3 C2 Cr1 P31 -74.4(5) . . . . ? C7 C2 Cr1 P31 47.2(5) . . . . ? C1 C2 Cr1 P11 62.5(6) . . . . ? C3 C2 Cr1 P11 180.0(6) . . . . ? C7 C2 Cr1 P11 -58.4(6) . . . . ? C1 C2 Cr1 P2 126.9(3) . . . . ? C3 C2 Cr1 P2 -115.6(3) . . . . ? C7 C2 Cr1 P2 6.0(3) . . . . ? C1 C2 Cr1 P21 114.7(5) . . . . ? C3 C2 Cr1 P21 -127.8(5) . . . . ? C7 C2 Cr1 P21 -6.2(5) . . . . ? C1 C2 Cr1 P42 -82.4(15) . . . . ? C3 C2 Cr1 P42 35.1(15) . . . . ? C7 C2 Cr1 P42 156.7(14) . . . . ? C1 C2 Cr1 P1 73.3(3) . . . . ? C3 C2 Cr1 P1 -169.2(3) . . . . ? C7 C2 Cr1 P1 -47.6(4) . . . . ? C1 C2 Cr1 P4 -122.6(4) . . . . ? C3 C2 Cr1 P4 -5.1(5) . . . . ? C7 C2 Cr1 P4 116.5(5) . . . . ? C5 C4 Cr1 C2 79.73(14) . . . . ? C3 C4 Cr1 C2 -37.68(14) . . . . ? C9 C4 Cr1 C2 -160.0(3) . . . . ? C5 C4 Cr1 C3 117.4(2) . . . . ? C9 C4 Cr1 C3 -122.3(3) . . . . ? C3 C4 Cr1 C5 -117.4(2) . . . . ? C9 C4 Cr1 C5 120.2(3) . . . . ? C5 C4 Cr1 C1 37.28(13) . . . . ? C3 C4 Cr1 C1 -80.12(15) . . . . ? C9 C4 Cr1 C1 157.5(3) . . . . ? C5 C4 Cr1 P31 -178.3(5) . . . . ? C3 C4 Cr1 P31 64.2(5) . . . . ? C9 C4 Cr1 P31 -58.1(6) . . . . ? C5 C4 Cr1 P11 -24.2(8) . . . . ? C3 C4 Cr1 P11 -141.6(8) . . . . ? C9 C4 Cr1 P11 96.1(8) . . . . ? C5 C4 Cr1 P2 136.1(4) . . . . ? C3 C4 Cr1 P2 18.7(5) . . . . ? C9 C4 Cr1 P2 -103.6(5) . . . . ? C5 C4 Cr1 P21 119.3(11) . . . . ? C3 C4 Cr1 P21 1.9(11) . . . . ? C9 C4 Cr1 P21 -120.5(11) . . . . ? C5 C4 Cr1 P42 -101.0(4) . . . . ? C3 C4 Cr1 P42 141.6(4) . . . . ? C9 C4 Cr1 P42 19.3(5) . . . . ? C5 C4 Cr1 P1 -3.4(6) . . . . ? C3 C4 Cr1 P1 -120.8(5) . . . . ? C9 C4 Cr1 P1 116.8(6) . . . . ? C5 C4 Cr1 P4 -116.8(2) . . . . ? C3 C4 Cr1 P4 125.8(3) . . . . ? C9 C4 Cr1 P4 3.4(3) . . . . ? C4 C3 Cr1 C2 117.3(2) . . . . ? C8 C3 Cr1 C2 -121.6(3) . . . . ? C2 C3 Cr1 C4 -117.3(2) . . . . ? C8 C3 Cr1 C4 121.1(3) . . . . ? C4 C3 Cr1 C5 37.45(14) . . . . ? C2 C3 Cr1 C5 -79.84(14) . . . . ? C8 C3 Cr1 C5 158.6(3) . . . . ? C4 C3 Cr1 C1 79.90(15) . . . . ? C2 C3 Cr1 C1 -37.40(13) . . . . ? C8 C3 Cr1 C1 -159.0(3) . . . . ? C4 C3 Cr1 P31 -127.0(5) . . . . ? C2 C3 Cr1 P31 115.7(5) . . . . ? C8 C3 Cr1 P31 -5.9(5) . . . . ? C4 C3 Cr1 P11 117.3(14) . . . . ? C2 C3 Cr1 P11 0.0(14) . . . . ? C8 C3 Cr1 P11 -121.6(14) . . . . ? C4 C3 Cr1 P2 -169.3(3) . . . . ? C2 C3 Cr1 P2 73.4(3) . . . . ? C8 C3 Cr1 P2 -48.2(4) . . . . ? C4 C3 Cr1 P21 -179.2(5) . . . . ? C2 C3 Cr1 P21 63.6(5) . . . . ? C8 C3 Cr1 P21 -58.1(6) . . . . ? C4 C3 Cr1 P42 -51.0(4) . . . . ? C2 C3 Cr1 P42 -168.3(4) . . . . ? C8 C3 Cr1 P42 70.1(5) . . . . ? C4 C3 Cr1 P1 136.6(5) . . . . ? C2 C3 Cr1 P1 19.3(5) . . . . ? C8 C3 Cr1 P1 -102.3(5) . . . . ? C4 C3 Cr1 P4 -65.1(2) . . . . ? C2 C3 Cr1 P4 177.6(2) . . . . ? C8 C3 Cr1 P4 56.0(3) . . . . ? C4 C5 Cr1 C2 -80.30(15) . . . . ? C1 C5 Cr1 C2 37.56(13) . . . . ? C10 C5 Cr1 C2 158.8(3) . . . . ? C1 C5 Cr1 C4 117.86(19) . . . . ? C10 C5 Cr1 C4 -120.9(3) . . . . ? C4 C5 Cr1 C3 -37.60(14) . . . . ? C1 C5 Cr1 C3 80.26(15) . . . . ? C10 C5 Cr1 C3 -158.5(3) . . . . ? C4 C5 Cr1 C1 -117.86(19) . . . . ? C10 C5 Cr1 C1 121.3(3) . . . . ? C4 C5 Cr1 P31 3.6(11) . . . . ? C1 C5 Cr1 P31 121.5(11) . . . . ? C10 C5 Cr1 P31 -117.3(11) . . . . ? C4 C5 Cr1 P11 166.2(5) . . . . ? C1 C5 Cr1 P11 -76.0(5) . . . . ? C10 C5 Cr1 P11 45.3(5) . . . . ? C4 C5 Cr1 P2 -119.0(5) . . . . ? C1 C5 Cr1 P2 -1.1(5) . . . . ? C10 C5 Cr1 P2 120.2(5) . . . . ? C4 C5 Cr1 P21 -140.0(6) . . . . ? C1 C5 Cr1 P21 -22.2(6) . . . . ? C10 C5 Cr1 P21 99.1(6) . . . . ? C4 C5 Cr1 P42 88.1(4) . . . . ? C1 C5 Cr1 P42 -154.1(4) . . . . ? C10 C5 Cr1 P42 -32.8(5) . . . . ? C4 C5 Cr1 P1 178.4(3) . . . . ? C1 C5 Cr1 P1 -63.8(3) . . . . ? C10 C5 Cr1 P1 57.5(3) . . . . ? C4 C5 Cr1 P4 73.1(3) . . . . ? C1 C5 Cr1 P4 -169.1(2) . . . . ? C10 C5 Cr1 P4 -47.8(3) . . . . ? C5 C1 Cr1 C2 -117.3(2) . . . . ? C6 C1 Cr1 C2 121.0(3) . . . . ? C2 C1 Cr1 C4 80.11(15) . . . . ? C5 C1 Cr1 C4 -37.24(13) . . . . ? C6 C1 Cr1 C4 -158.9(2) . . . . ? C2 C1 Cr1 C3 37.57(14) . . . . ? C5 C1 Cr1 C3 -79.78(14) . . . . ? C6 C1 Cr1 C3 158.6(2) . . . . ? C2 C1 Cr1 C5 117.3(2) . . . . ? C6 C1 Cr1 C5 -121.6(3) . . . . ? C2 C1 Cr1 P31 -21.5(8) . . . . ? C5 C1 Cr1 P31 -138.8(7) . . . . ? C6 C1 Cr1 P31 99.6(8) . . . . ? C2 C1 Cr1 P11 -128.9(5) . . . . ? C5 C1 Cr1 P11 113.8(5) . . . . ? C6 C1 Cr1 P11 -7.9(6) . . . . ? C2 C1 Cr1 P2 -63.2(3) . . . . ? C5 C1 Cr1 P2 179.5(2) . . . . ? C6 C1 Cr1 P2 57.8(3) . . . . ? C2 C1 Cr1 P21 -75.2(4) . . . . ? C5 C1 Cr1 P21 167.5(4) . . . . ? C6 C1 Cr1 P21 45.8(5) . . . . ? C2 C1 Cr1 P42 156.1(5) . . . . ? C5 C1 Cr1 P42 38.7(5) . . . . ? C6 C1 Cr1 P42 -82.9(6) . . . . ? C2 C1 Cr1 P1 -116.0(3) . . . . ? C5 C1 Cr1 P1 126.6(3) . . . . ? C6 C1 Cr1 P1 5.0(3) . . . . ? C2 C1 Cr1 P4 137.2(4) . . . . ? C5 C1 Cr1 P4 19.9(4) . . . . ? C6 C1 Cr1 P4 -101.8(4) . . . . ? C2 Cr1 P11 P51 -154.7(5) . . . . ? C4 Cr1 P11 P51 -69.1(9) . . . . ? C3 Cr1 P11 P51 -154.7(11) . . . . ? C5 Cr1 P11 P51 -84.6(6) . . . . ? C1 Cr1 P11 P51 -121.5(6) . . . . ? P31 Cr1 P11 P51 88.4(7) . . . . ? P2 Cr1 P11 P51 122.5(7) . . . . ? P21 Cr1 P11 P51 127.9(8) . . . . ? P42 Cr1 P11 P51 15.8(6) . . . . ? P1 Cr1 P11 P51 153(3) . . . . ? P4 Cr1 P11 P51 27.5(6) . . . . ? C2 Cr1 P11 P21 77.5(6) . . . . ? C4 Cr1 P11 P21 163.0(5) . . . . ? C3 Cr1 P11 P21 77.5(13) . . . . ? C5 Cr1 P11 P21 147.5(5) . . . . ? C1 Cr1 P11 P21 110.7(5) . . . . ? P31 Cr1 P11 P21 -39.4(6) . . . . ? P2 Cr1 P11 P21 -5.4(6) . . . . ? P42 Cr1 P11 P21 -112.0(6) . . . . ? P1 Cr1 P11 P21 26(2) . . . . ? P4 Cr1 P11 P21 -100.4(5) . . . . ? C2 Cr1 P11 Cr2 140.5(3) . . . . ? C4 Cr1 P11 Cr2 -134.0(5) . . . . ? C3 Cr1 P11 Cr2 140.5(9) . . . . ? C5 Cr1 P11 Cr2 -149.5(3) . . . . ? C1 Cr1 P11 Cr2 173.7(4) . . . . ? P31 Cr1 P11 Cr2 23.5(6) . . . . ? P2 Cr1 P11 Cr2 57.6(4) . . . . ? P21 Cr1 P11 Cr2 63.0(5) . . . . ? P42 Cr1 P11 Cr2 -49.1(3) . . . . ? P1 Cr1 P11 Cr2 88(3) . . . . ? P4 Cr1 P11 Cr2 -37.4(4) . . . . ? P51 P11 P21 P31 -2.4(12) . . . . ? Cr1 P11 P21 P31 46.8(6) . . . . ? Cr2 P11 P21 P31 -48.9(6) . . . . ? P51 P11 P21 Cr2 46.5(8) . . . . ? Cr1 P11 P21 Cr2 95.7(4) . . . . ? P51 P11 P21 Cr1 -49.2(8) . . . . ? Cr2 P11 P21 Cr1 -95.7(4) . . . . ? C2 Cr1 P21 P31 111.6(5) . . . . ? C4 Cr1 P21 P31 76.6(11) . . . . ? C3 Cr1 P21 P31 77.9(6) . . . . ? C5 Cr1 P21 P31 162.6(6) . . . . ? C1 Cr1 P21 P31 148.3(5) . . . . ? P11 Cr1 P21 P31 -127.4(7) . . . . ? P2 Cr1 P21 P31 29(2) . . . . ? P42 Cr1 P21 P31 -63.7(6) . . . . ? P1 Cr1 P21 P31 -135.6(7) . . . . ? P4 Cr1 P21 P31 -47.8(5) . . . . ? C2 Cr1 P21 P11 -121.0(5) . . . . ? C4 Cr1 P21 P11 -156.1(9) . . . . ? C3 Cr1 P21 P11 -154.7(5) . . . . ? C5 Cr1 P21 P11 -70.0(7) . . . . ? C1 Cr1 P21 P11 -84.4(5) . . . . ? P31 Cr1 P21 P11 127.4(7) . . . . ? P2 Cr1 P21 P11 156(2) . . . . ? P42 Cr1 P21 P11 63.7(6) . . . . ? P1 Cr1 P21 P11 -8.2(7) . . . . ? P4 Cr1 P21 P11 79.5(5) . . . . ? C2 Cr1 P21 Cr2 175.0(3) . . . . ? C4 Cr1 P21 Cr2 140.0(7) . . . . ? C3 Cr1 P21 Cr2 141.3(2) . . . . ? C5 Cr1 P21 Cr2 -134.0(3) . . . . ? C1 Cr1 P21 Cr2 -148.3(3) . . . . ? P31 Cr1 P21 Cr2 63.4(6) . . . . ? P11 Cr1 P21 Cr2 -64.0(5) . . . . ? P2 Cr1 P21 Cr2 92(2) . . . . ? P42 Cr1 P21 Cr2 -0.3(4) . . . . ? P1 Cr1 P21 Cr2 -72.2(4) . . . . ? P4 Cr1 P21 Cr2 15.6(4) . . . . ? P11 P21 P31 P41 1.0(12) . . . . ? Cr2 P21 P31 P41 -48.2(8) . . . . ? Cr1 P21 P31 P41 47.9(7) . . . . ? P11 P21 P31 Cr1 -46.9(7) . . . . ? Cr2 P21 P31 Cr1 -96.1(4) . . . . ? P11 P21 P31 Cr2 49.2(6) . . . . ? Cr1 P21 P31 Cr2 96.1(4) . . . . ? C2 Cr1 P31 P41 145.8(5) . . . . ? C4 Cr1 P31 P41 75.3(6) . . . . ? C3 Cr1 P31 P41 109.2(6) . . . . ? C5 Cr1 P31 P41 72.8(12) . . . . ? C1 Cr1 P31 P41 159.8(6) . . . . ? P11 Cr1 P31 P41 -90.9(6) . . . . ? P2 Cr1 P31 P41 -139.2(8) . . . . ? P21 Cr1 P31 P41 -130.5(7) . . . . ? P42 Cr1 P31 P41 -18.4(6) . . . . ? P1 Cr1 P31 P41 -102.5(6) . . . . ? P4 Cr1 P31 P41 -7.8(6) . . . . ? C2 Cr1 P31 P21 -83.7(5) . . . . ? C4 Cr1 P31 P21 -154.2(4) . . . . ? C3 Cr1 P31 P21 -120.3(4) . . . . ? C5 Cr1 P31 P21 -156.7(8) . . . . ? C1 Cr1 P31 P21 -69.7(7) . . . . ? P11 Cr1 P31 P21 39.6(5) . . . . ? P2 Cr1 P31 P21 -8.7(5) . . . . ? P42 Cr1 P31 P21 112.1(5) . . . . ? P1 Cr1 P31 P21 28.0(4) . . . . ? P4 Cr1 P31 P21 122.7(5) . . . . ? C2 Cr1 P31 Cr2 -147.0(3) . . . . ? C4 Cr1 P31 Cr2 142.5(2) . . . . ? C3 Cr1 P31 Cr2 176.4(4) . . . . ? C5 Cr1 P31 Cr2 140.0(7) . . . . ? C1 Cr1 P31 Cr2 -133.0(4) . . . . ? P11 Cr1 P31 Cr2 -23.7(5) . . . . ? P2 Cr1 P31 Cr2 -72.0(4) . . . . ? P21 Cr1 P31 Cr2 -63.3(4) . . . . ? P42 Cr1 P31 Cr2 48.7(4) . . . . ? P1 Cr1 P31 Cr2 -35.3(4) . . . . ? P4 Cr1 P31 Cr2 59.4(4) . . . . ? P21 P31 P41 P51 0.8(12) . . . . ? Cr1 P31 P41 P51 48.1(8) . . . . ? Cr2 P31 P41 P51 -45.7(8) . . . . ? P21 P31 P41 Cr1 -47.4(7) . . . . ? Cr2 P31 P41 Cr1 -93.8(4) . . . . ? P21 P31 P41 Cr2 46.5(7) . . . . ? Cr1 P31 P41 Cr2 93.8(4) . . . . ? C2 Cr1 P41 P31 -71.4(9) . . . . ? C4 Cr1 P41 P31 -121.2(5) . . . . ? C3 Cr1 P41 P31 -84.8(6) . . . . ? C5 Cr1 P41 P31 -154.1(5) . . . . ? C1 Cr1 P41 P31 -154.0(8) . . . . ? P11 Cr1 P41 P31 90.7(7) . . . . ? P2 Cr1 P41 P31 26.3(5) . . . . ? P21 Cr1 P41 P31 37.5(6) . . . . ? P42 Cr1 P41 P31 138.4(13) . . . . ? P1 Cr1 P41 P31 79.2(6) . . . . ? P4 Cr1 P41 P31 143(2) . . . . ? C2 Cr1 P41 P51 161.5(8) . . . . ? C4 Cr1 P41 P51 111.7(7) . . . . ? C3 Cr1 P41 P51 148.2(7) . . . . ? C5 Cr1 P41 P51 78.8(7) . . . . ? C1 Cr1 P41 P51 78.9(11) . . . . ? P31 Cr1 P41 P51 -127.0(9) . . . . ? P11 Cr1 P41 P51 -36.3(7) . . . . ? P2 Cr1 P41 P51 -100.7(7) . . . . ? P21 Cr1 P41 P51 -89.6(7) . . . . ? P42 Cr1 P41 P51 11.4(11) . . . . ? P1 Cr1 P41 P51 -47.8(7) . . . . ? P4 Cr1 P41 P51 16(2) . . . . ? C2 Cr1 P41 Cr2 -134.5(4) . . . . ? C4 Cr1 P41 Cr2 175.6(4) . . . . ? C3 Cr1 P41 Cr2 -147.9(3) . . . . ? C5 Cr1 P41 Cr2 142.8(3) . . . . ? C1 Cr1 P41 Cr2 142.9(7) . . . . ? P31 Cr1 P41 Cr2 -63.1(6) . . . . ? P11 Cr1 P41 Cr2 27.6(5) . . . . ? P2 Cr1 P41 Cr2 -36.8(4) . . . . ? P21 Cr1 P41 Cr2 -25.7(5) . . . . ? P42 Cr1 P41 Cr2 75.3(10) . . . . ? P1 Cr1 P41 Cr2 16.1(5) . . . . ? P4 Cr1 P41 Cr2 80(2) . . . . ? P21 P11 P51 P41 2.9(13) . . . . ? Cr1 P11 P51 P41 -45.7(8) . . . . ? Cr2 P11 P51 P41 48.6(8) . . . . ? P21 P11 P51 Cr2 -45.7(7) . . . . ? Cr1 P11 P51 Cr2 -94.3(5) . . . . ? P21 P11 P51 Cr1 48.6(7) . . . . ? Cr2 P11 P51 Cr1 94.3(5) . . . . ? P31 P41 P51 P11 -2.2(13) . . . . ? Cr1 P41 P51 P11 45.1(8) . . . . ? Cr2 P41 P51 P11 -47.6(8) . . . . ? P31 P41 P51 Cr2 45.4(8) . . . . ? Cr1 P41 P51 Cr2 92.7(5) . . . . ? P31 P41 P51 Cr1 -47.4(8) . . . . ? Cr2 P41 P51 Cr1 -92.7(5) . . . . ? C2 Cr1 P51 P11 75.8(15) . . . . ? C4 Cr1 P51 P11 146.8(6) . . . . ? C3 Cr1 P51 P11 162.4(7) . . . . ? C5 Cr1 P51 P11 109.9(7) . . . . ? C1 Cr1 P51 P11 76.5(7) . . . . ? P31 Cr1 P51 P11 -92.3(7) . . . . ? P2 Cr1 P51 P11 -50.1(7) . . . . ? P21 Cr1 P51 P11 -39.2(7) . . . . ? P42 Cr1 P51 P11 -143.2(15) . . . . ? P1 Cr1 P51 P11 -6.4(8) . . . . ? P4 Cr1 P51 P11 -135.9(9) . . . . ? C2 Cr1 P51 P41 -153.1(10) . . . . ? C4 Cr1 P51 P41 -82.0(6) . . . . ? C3 Cr1 P51 P41 -66.4(9) . . . . ? C5 Cr1 P51 P41 -118.9(6) . . . . ? C1 Cr1 P51 P41 -152.3(5) . . . . ? P31 Cr1 P51 P41 38.9(7) . . . . ? P11 Cr1 P51 P41 131.2(9) . . . . ? P2 Cr1 P51 P41 81.1(6) . . . . ? P21 Cr1 P51 P41 92.0(7) . . . . ? P42 Cr1 P51 P41 -12.0(11) . . . . ? P1 Cr1 P51 P41 124.8(8) . . . . ? P4 Cr1 P51 P41 -4.7(6) . . . . ? C2 Cr1 P51 Cr2 140.2(10) . . . . ? C4 Cr1 P51 Cr2 -148.7(3) . . . . ? C3 Cr1 P51 Cr2 -133.1(5) . . . . ? C5 Cr1 P51 Cr2 174.4(4) . . . . ? C1 Cr1 P51 Cr2 141.0(3) . . . . ? P31 Cr1 P51 Cr2 -27.8(5) . . . . ? P11 Cr1 P51 Cr2 64.5(7) . . . . ? P2 Cr1 P51 Cr2 14.4(5) . . . . ? P21 Cr1 P51 Cr2 25.3(5) . . . . ? P42 Cr1 P51 Cr2 -78.7(11) . . . . ? P1 Cr1 P51 Cr2 58.1(4) . . . . ? P4 Cr1 P51 Cr2 -71.4(5) . . . . ? C2 Cr1 P1 P5 -148.7(3) . . . . ? C4 Cr1 P1 P5 -76.7(5) . . . . ? C3 Cr1 P1 P5 -161.3(3) . . . . ? C5 Cr1 P1 P5 -79.1(3) . . . . ? C1 Cr1 P1 P5 -112.6(3) . . . . ? P31 Cr1 P1 P5 98.8(5) . . . . ? P11 Cr1 P1 P5 -16(3) . . . . ? P2 Cr1 P1 P5 128.9(4) . . . . ? P21 Cr1 P1 P5 132.9(6) . . . . ? P42 Cr1 P1 P5 24.7(3) . . . . ? P4 Cr1 P1 P5 37.8(3) . . . . ? C2 Cr1 P1 P2 82.3(3) . . . . ? C4 Cr1 P1 P2 154.4(4) . . . . ? C3 Cr1 P1 P2 69.8(5) . . . . ? C5 Cr1 P1 P2 152.0(3) . . . . ? C1 Cr1 P1 P2 118.5(3) . . . . ? P31 Cr1 P1 P2 -30.1(5) . . . . ? P11 Cr1 P1 P2 -145(3) . . . . ? P21 Cr1 P1 P2 4.0(7) . . . . ? P42 Cr1 P1 P2 -104.2(4) . . . . ? P4 Cr1 P1 P2 -91.1(3) . . . . ? C2 Cr1 P1 Cr2 146.92(14) . . . . ? C4 Cr1 P1 Cr2 -141.1(4) . . . . ? C3 Cr1 P1 Cr2 134.3(3) . . . . ? C5 Cr1 P1 Cr2 -143.41(15) . . . . ? C1 Cr1 P1 Cr2 -176.93(19) . . . . ? P31 Cr1 P1 Cr2 34.5(5) . . . . ? P11 Cr1 P1 Cr2 -80(3) . . . . ? P2 Cr1 P1 Cr2 64.6(3) . . . . ? P21 Cr1 P1 Cr2 68.6(6) . . . . ? P42 Cr1 P1 Cr2 -39.6(3) . . . . ? P4 Cr1 P1 Cr2 -26.5(2) . . . . ? P5 P1 P2 P3 0.5(6) . . . . ? Cr1 P1 P2 P3 47.5(4) . . . . ? Cr2 P1 P2 P3 -46.4(4) . . . . ? P5 P1 P2 Cr1 -47.0(4) . . . . ? Cr2 P1 P2 Cr1 -93.88(19) . . . . ? P5 P1 P2 Cr2 46.9(4) . . . . ? Cr1 P1 P2 Cr2 93.88(19) . . . . ? C2 Cr1 P2 P3 119.4(4) . . . . ? C4 Cr1 P2 P3 71.0(5) . . . . ? C3 Cr1 P2 P3 83.1(4) . . . . ? C5 Cr1 P2 P3 153.4(4) . . . . ? C1 Cr1 P2 P3 152.7(3) . . . . ? P31 Cr1 P2 P3 3.5(8) . . . . ? P11 Cr1 P2 P3 -120.8(6) . . . . ? P21 Cr1 P2 P3 -142(2) . . . . ? P42 Cr1 P2 P3 -52.8(4) . . . . ? P1 Cr1 P2 P3 -128.9(4) . . . . ? P4 Cr1 P2 P3 -37.7(4) . . . . ? C2 Cr1 P2 P1 -111.7(3) . . . . ? C4 Cr1 P2 P1 -160.1(3) . . . . ? C3 Cr1 P2 P1 -148.0(3) . . . . ? C5 Cr1 P2 P1 -77.7(4) . . . . ? C1 Cr1 P2 P1 -78.4(3) . . . . ? P31 Cr1 P2 P1 132.4(6) . . . . ? P11 Cr1 P2 P1 8.1(6) . . . . ? P21 Cr1 P2 P1 -13(2) . . . . ? P42 Cr1 P2 P1 76.1(4) . . . . ? P4 Cr1 P2 P1 91.2(3) . . . . ? C2 Cr1 P2 Cr2 -175.97(18) . . . . ? C4 Cr1 P2 Cr2 135.6(2) . . . . ? C3 Cr1 P2 Cr2 147.76(14) . . . . ? C5 Cr1 P2 Cr2 -141.9(3) . . . . ? C1 Cr1 P2 Cr2 -142.68(14) . . . . ? P31 Cr1 P2 Cr2 68.1(6) . . . . ? P11 Cr1 P2 Cr2 -56.1(4) . . . . ? P21 Cr1 P2 Cr2 -77(2) . . . . ? P42 Cr1 P2 Cr2 11.8(3) . . . . ? P1 Cr1 P2 Cr2 -64.2(2) . . . . ? P4 Cr1 P2 Cr2 27.0(2) . . . . ? P1 P2 P3 P4 -0.8(6) . . . . ? Cr1 P2 P3 P4 46.3(4) . . . . ? Cr2 P2 P3 P4 -47.0(4) . . . . ? P1 P2 P3 Cr1 -47.1(4) . . . . ? Cr2 P2 P3 Cr1 -93.3(2) . . . . ? P1 P2 P3 Cr2 46.3(4) . . . . ? Cr1 P2 P3 Cr2 93.3(2) . . . . ? C2 Cr1 P3 P4 153.4(2) . . . . ? C4 Cr1 P3 P4 83.5(3) . . . . ? C3 Cr1 P3 P4 119.7(3) . . . . ? C5 Cr1 P3 P4 71.4(5) . . . . ? C1 Cr1 P3 P4 155.4(4) . . . . ? P31 Cr1 P3 P4 -142(3) . . . . ? P11 Cr1 P3 P4 -78.3(5) . . . . ? P2 Cr1 P3 P4 -129.7(4) . . . . ? P21 Cr1 P3 P4 -121.2(4) . . . . ? P42 Cr1 P3 P4 -9.3(3) . . . . ? P1 Cr1 P3 P4 -90.7(3) . . . . ? C2 Cr1 P3 P2 -77.0(3) . . . . ? C4 Cr1 P3 P2 -146.8(2) . . . . ? C3 Cr1 P3 P2 -110.7(3) . . . . ? C5 Cr1 P3 P2 -158.9(3) . . . . ? C1 Cr1 P3 P2 -75.0(5) . . . . ? P31 Cr1 P3 P2 -13(3) . . . . ? P11 Cr1 P3 P2 51.3(5) . . . . ? P21 Cr1 P3 P2 8.5(4) . . . . ? P42 Cr1 P3 P2 120.3(4) . . . . ? P1 Cr1 P3 P2 39.0(3) . . . . ? P4 Cr1 P3 P2 129.7(4) . . . . ? C2 Cr1 P3 Cr2 -141.97(17) . . . . ? C4 Cr1 P3 Cr2 148.17(16) . . . . ? C3 Cr1 P3 Cr2 -175.7(2) . . . . ? C5 Cr1 P3 Cr2 136.1(3) . . . . ? C1 Cr1 P3 Cr2 -139.9(4) . . . . ? P31 Cr1 P3 Cr2 -78(3) . . . . ? P11 Cr1 P3 Cr2 -13.6(4) . . . . ? P2 Cr1 P3 Cr2 -65.0(2) . . . . ? P21 Cr1 P3 Cr2 -56.5(3) . . . . ? P42 Cr1 P3 Cr2 55.3(3) . . . . ? P1 Cr1 P3 Cr2 -26.0(2) . . . . ? P4 Cr1 P3 Cr2 64.7(3) . . . . ? P2 P3 P4 P5 0.8(7) . . . . ? Cr1 P3 P4 P5 46.7(4) . . . . ? Cr2 P3 P4 P5 -46.4(4) . . . . ? P2 P3 P4 Cr2 47.2(4) . . . . ? Cr1 P3 P4 Cr2 93.11(16) . . . . ? P2 P3 P4 Cr1 -45.9(4) . . . . ? Cr2 P3 P4 Cr1 -93.11(16) . . . . ? C2 Cr1 P4 P3 -73.3(4) . . . . ? C4 Cr1 P4 P3 -110.9(3) . . . . ? C3 Cr1 P4 P3 -76.8(3) . . . . ? C5 Cr1 P4 P3 -147.0(3) . . . . ? C1 Cr1 P4 P3 -160.0(3) . . . . ? P31 Cr1 P4 P3 7.5(6) . . . . ? P11 Cr1 P4 P3 102.3(5) . . . . ? P2 Cr1 P4 P3 38.1(3) . . . . ? P21 Cr1 P4 P3 50.0(4) . . . . ? P42 Cr1 P4 P3 147.2(10) . . . . ? P1 Cr1 P4 P3 91.9(3) . . . . ? C2 Cr1 P4 P5 156.9(4) . . . . ? C4 Cr1 P4 P5 119.3(3) . . . . ? C3 Cr1 P4 P5 153.4(3) . . . . ? C5 Cr1 P4 P5 83.2(3) . . . . ? C1 Cr1 P4 P5 70.2(5) . . . . ? P31 Cr1 P4 P5 -122.3(5) . . . . ? P11 Cr1 P4 P5 -27.5(5) . . . . ? P2 Cr1 P4 P5 -91.7(3) . . . . ? P21 Cr1 P4 P5 -79.8(5) . . . . ? P42 Cr1 P4 P5 17.5(8) . . . . ? P1 Cr1 P4 P5 -37.8(4) . . . . ? C2 Cr1 P4 Cr2 -138.6(3) . . . . ? C4 Cr1 P4 Cr2 -176.18(17) . . . . ? C3 Cr1 P4 Cr2 -142.08(13) . . . . ? C5 Cr1 P4 Cr2 147.71(13) . . . . ? C1 Cr1 P4 Cr2 134.7(2) . . . . ? P31 Cr1 P4 Cr2 -57.8(4) . . . . ? P11 Cr1 P4 Cr2 37.0(5) . . . . ? P2 Cr1 P4 Cr2 -27.2(2) . . . . ? P21 Cr1 P4 Cr2 -15.3(4) . . . . ? P42 Cr1 P4 Cr2 82.0(9) . . . . ? P1 Cr1 P4 Cr2 26.7(3) . . . . ? P3 P4 P5 P1 -0.5(7) . . . . ? Cr2 P4 P5 P1 -47.2(4) . . . . ? Cr1 P4 P5 P1 46.4(4) . . . . ? P3 P4 P5 Cr2 46.8(4) . . . . ? Cr1 P4 P5 Cr2 93.65(19) . . . . ? P3 P4 P5 Cr1 -46.9(4) . . . . ? Cr2 P4 P5 Cr1 -93.65(19) . . . . ? P2 P1 P5 P4 0.0(7) . . . . ? Cr1 P1 P5 P4 -46.5(4) . . . . ? Cr2 P1 P5 P4 47.1(4) . . . . ? P2 P1 P5 Cr2 -47.1(4) . . . . ? Cr1 P1 P5 Cr2 -93.5(2) . . . . ? P2 P1 P5 Cr1 46.5(4) . . . . ? Cr2 P1 P5 Cr1 93.5(2) . . . . ? C2 Cr1 P5 P4 -161.7(3) . . . . ? C4 Cr1 P5 P4 -78.0(3) . . . . ? C3 Cr1 P5 P4 -74.5(5) . . . . ? C5 Cr1 P5 P4 -112.0(3) . . . . ? C1 Cr1 P5 P4 -148.4(2) . . . . ? P31 Cr1 P5 P4 48.1(5) . . . . ? P11 Cr1 P5 P4 135.1(8) . . . . ? P2 Cr1 P5 P4 90.8(3) . . . . ? P21 Cr1 P5 P4 100.3(5) . . . . ? P42 Cr1 P5 P4 -7.7(3) . . . . ? P1 Cr1 P5 P4 129.7(4) . . . . ? C2 Cr1 P5 P1 68.6(6) . . . . ? C4 Cr1 P5 P1 152.2(3) . . . . ? C3 Cr1 P5 P1 155.7(5) . . . . ? C5 Cr1 P5 P1 118.3(3) . . . . ? C1 Cr1 P5 P1 81.9(3) . . . . ? P31 Cr1 P5 P1 -81.7(5) . . . . ? P11 Cr1 P5 P1 5.4(9) . . . . ? P2 Cr1 P5 P1 -39.0(4) . . . . ? P21 Cr1 P5 P1 -29.4(5) . . . . ? P42 Cr1 P5 P1 -137.4(5) . . . . ? P4 Cr1 P5 P1 -129.7(4) . . . . ? C2 Cr1 P5 Cr2 133.6(3) . . . . ? C4 Cr1 P5 Cr2 -142.72(15) . . . . ? C3 Cr1 P5 Cr2 -139.2(4) . . . . ? C5 Cr1 P5 Cr2 -176.67(19) . . . . ? C1 Cr1 P5 Cr2 146.95(15) . . . . ? P31 Cr1 P5 Cr2 -16.6(4) . . . . ? P11 Cr1 P5 Cr2 70.4(7) . . . . ? P2 Cr1 P5 Cr2 26.1(3) . . . . ? P21 Cr1 P5 Cr2 35.6(4) . . . . ? P42 Cr1 P5 Cr2 -72.4(3) . . . . ? P1 Cr1 P5 Cr2 65.1(3) . . . . ? P4 Cr1 P5 Cr2 -64.7(2) . . . . ? C2 Cr1 P12 P52 -139.2(4) . . . . ? C4 Cr1 P12 P52 -101.2(11) . . . . ? C3 Cr1 P12 P52 -161.8(3) . . . . ? C5 Cr1 P12 P52 -73.1(4) . . . . ? C1 Cr1 P12 P52 -100.9(4) . . . . ? P31 Cr1 P12 P52 110.9(5) . . . . ? P11 Cr1 P12 P52 -10.7(10) . . . . ? P2 Cr1 P12 P52 137.2(5) . . . . ? P21 Cr1 P12 P52 139.2(9) . . . . ? P42 Cr1 P12 P52 38.3(4) . . . . ? P1 Cr1 P12 P52 -18.0(8) . . . . ? P4 Cr1 P12 P52 53.3(4) . . . . ? C2 Cr1 P12 P22 93.0(4) . . . . ? C4 Cr1 P12 P22 131.0(10) . . . . ? C3 Cr1 P12 P22 70.4(4) . . . . ? C5 Cr1 P12 P22 159.1(3) . . . . ? C1 Cr1 P12 P22 131.3(4) . . . . ? P31 Cr1 P12 P22 -16.9(5) . . . . ? P11 Cr1 P12 P22 -138.5(12) . . . . ? P2 Cr1 P12 P22 9.4(4) . . . . ? P21 Cr1 P12 P22 11.4(8) . . . . ? P42 Cr1 P12 P22 -89.6(4) . . . . ? P1 Cr1 P12 P22 -145.8(10) . . . . ? P4 Cr1 P12 P22 -74.6(4) . . . . ? C2 Cr1 P12 Cr2 156.4(3) . . . . ? C4 Cr1 P12 Cr2 -165.7(9) . . . . ? C3 Cr1 P12 Cr2 133.77(17) . . . . ? C5 Cr1 P12 Cr2 -137.58(17) . . . . ? C1 Cr1 P12 Cr2 -165.4(3) . . . . ? P31 Cr1 P12 Cr2 46.5(5) . . . . ? P11 Cr1 P12 Cr2 -75.2(10) . . . . ? P2 Cr1 P12 Cr2 72.7(4) . . . . ? P21 Cr1 P12 Cr2 74.8(8) . . . . ? P42 Cr1 P12 Cr2 -26.2(3) . . . . ? P1 Cr1 P12 Cr2 -82.5(9) . . . . ? P4 Cr1 P12 Cr2 -11.2(3) . . . . ? P52 P12 P22 P32 -0.3(6) . . . . ? Cr2 P12 P22 P32 -46.9(4) . . . . ? Cr1 P12 P22 P32 46.8(4) . . . . ? P52 P12 P22 Cr2 46.7(4) . . . . ? Cr1 P12 P22 Cr2 93.7(2) . . . . ? P52 P12 P22 Cr1 -47.0(4) . . . . ? Cr2 P12 P22 Cr1 -93.7(2) . . . . ? C2 Cr1 P22 P32 130.3(4) . . . . ? C4 Cr1 P22 P32 68.5(4) . . . . ? C3 Cr1 P22 P32 91.7(4) . . . . ? C5 Cr1 P22 P32 127.3(12) . . . . ? C1 Cr1 P22 P32 158.1(3) . . . . ? P31 Cr1 P22 P32 10.4(9) . . . . ? P11 Cr1 P22 P32 -111.3(5) . . . . ? P2 Cr1 P22 P32 -151.1(10) . . . . ? P21 Cr1 P22 P32 -141.1(9) . . . . ? P42 Cr1 P22 P32 -38.3(4) . . . . ? P1 Cr1 P22 P32 -120.7(4) . . . . ? P4 Cr1 P22 P32 -25.0(4) . . . . ? C2 Cr1 P22 P12 -99.3(4) . . . . ? C4 Cr1 P22 P12 -161.1(3) . . . . ? C3 Cr1 P22 P12 -137.9(3) . . . . ? C5 Cr1 P22 P12 -102.2(12) . . . . ? C1 Cr1 P22 P12 -71.5(3) . . . . ? P31 Cr1 P22 P12 140.8(10) . . . . ? P11 Cr1 P22 P12 19.1(5) . . . . ? P2 Cr1 P22 P12 -20.7(8) . . . . ? P21 Cr1 P22 P12 -10.7(7) . . . . ? P42 Cr1 P22 P12 92.1(4) . . . . ? P1 Cr1 P22 P12 9.8(3) . . . . ? P4 Cr1 P22 P12 105.4(3) . . . . ? C2 Cr1 P22 Cr2 -163.9(3) . . . . ? C4 Cr1 P22 Cr2 134.35(17) . . . . ? C3 Cr1 P22 Cr2 157.5(3) . . . . ? C5 Cr1 P22 Cr2 -166.8(10) . . . . ? C1 Cr1 P22 Cr2 -136.12(18) . . . . ? P31 Cr1 P22 Cr2 76.2(9) . . . . ? P11 Cr1 P22 Cr2 -45.5(4) . . . . ? P2 Cr1 P22 Cr2 -85.3(9) . . . . ? P21 Cr1 P22 Cr2 -75.3(7) . . . . ? P42 Cr1 P22 Cr2 27.5(3) . . . . ? P1 Cr1 P22 Cr2 -54.8(3) . . . . ? P4 Cr1 P22 Cr2 40.8(3) . . . . ? P12 P22 P32 P42 0.3(7) . . . . ? Cr2 P22 P32 P42 -46.1(4) . . . . ? Cr1 P22 P32 P42 46.4(4) . . . . ? P12 P22 P32 Cr2 46.4(4) . . . . ? Cr1 P22 P32 Cr2 92.4(2) . . . . ? P12 P22 P32 Cr1 -46.0(4) . . . . ? Cr2 P22 P32 Cr1 -92.4(2) . . . . ? C2 Cr1 P32 P22 -71.2(4) . . . . ? C4 Cr1 P32 P22 -138.1(4) . . . . ? C3 Cr1 P32 P22 -99.8(4) . . . . ? C5 Cr1 P32 P22 -160.2(3) . . . . ? C1 Cr1 P32 P22 -97.3(11) . . . . ? P31 Cr1 P32 P22 -10.7(9) . . . . ? P11 Cr1 P32 P22 66.5(5) . . . . ? P2 Cr1 P32 P22 8.7(3) . . . . ? P21 Cr1 P32 P22 18.0(5) . . . . ? P42 Cr1 P32 P22 129.0(5) . . . . ? P1 Cr1 P32 P22 53.5(4) . . . . ? P4 Cr1 P32 P22 137.3(5) . . . . ? C2 Cr1 P32 P42 159.8(3) . . . . ? C4 Cr1 P32 P42 92.9(4) . . . . ? C3 Cr1 P32 P42 131.3(4) . . . . ? C5 Cr1 P32 P42 70.8(4) . . . . ? C1 Cr1 P32 P42 133.7(10) . . . . ? P31 Cr1 P32 P42 -139.6(11) . . . . ? P11 Cr1 P32 P42 -62.5(5) . . . . ? P2 Cr1 P32 P42 -120.3(4) . . . . ? P21 Cr1 P32 P42 -111.0(4) . . . . ? P1 Cr1 P32 P42 -75.4(4) . . . . ? P4 Cr1 P32 P42 8.3(4) . . . . ? C2 Cr1 P32 Cr2 -136.10(19) . . . . ? C4 Cr1 P32 Cr2 157.0(3) . . . . ? C3 Cr1 P32 Cr2 -164.7(3) . . . . ? C5 Cr1 P32 Cr2 134.84(19) . . . . ? C1 Cr1 P32 Cr2 -162.3(10) . . . . ? P31 Cr1 P32 Cr2 -75.6(10) . . . . ? P11 Cr1 P32 Cr2 1.5(5) . . . . ? P2 Cr1 P32 Cr2 -56.2(2) . . . . ? P21 Cr1 P32 Cr2 -46.9(3) . . . . ? P42 Cr1 P32 Cr2 64.1(3) . . . . ? P1 Cr1 P32 Cr2 -11.4(3) . . . . ? P4 Cr1 P32 Cr2 72.4(3) . . . . ? P22 P32 P42 P52 -0.3(7) . . . . ? Cr2 P32 P42 P52 -46.8(4) . . . . ? Cr1 P32 P42 P52 46.7(4) . . . . ? P22 P32 P42 Cr2 46.4(4) . . . . ? Cr1 P32 P42 Cr2 93.4(2) . . . . ? P22 P32 P42 Cr1 -47.0(4) . . . . ? Cr2 P32 P42 Cr1 -93.4(2) . . . . ? C2 Cr1 P42 P52 132.2(12) . . . . ? C4 Cr1 P42 P52 130.0(4) . . . . ? C3 Cr1 P42 P52 159.0(3) . . . . ? C5 Cr1 P42 P52 91.6(4) . . . . ? C1 Cr1 P42 P52 68.3(4) . . . . ? P31 Cr1 P42 P52 -113.1(5) . . . . ? P11 Cr1 P42 P52 -16.4(6) . . . . ? P2 Cr1 P42 P52 -77.1(4) . . . . ? P21 Cr1 P42 P52 -64.8(5) . . . . ? P1 Cr1 P42 P52 -25.1(4) . . . . ? P4 Cr1 P42 P52 -149.2(10) . . . . ? C2 Cr1 P42 P32 -97.6(12) . . . . ? C4 Cr1 P42 P32 -99.9(4) . . . . ? C3 Cr1 P42 P32 -70.9(4) . . . . ? C5 Cr1 P42 P32 -138.3(4) . . . . ? C1 Cr1 P42 P32 -161.6(3) . . . . ? P31 Cr1 P42 P32 17.1(6) . . . . ? P11 Cr1 P42 P32 113.7(6) . . . . ? P2 Cr1 P42 P32 53.0(4) . . . . ? P21 Cr1 P42 P32 65.3(5) . . . . ? P1 Cr1 P42 P32 105.1(4) . . . . ? P4 Cr1 P42 P32 -19.1(8) . . . . ? C2 Cr1 P42 Cr2 -162.6(10) . . . . ? C4 Cr1 P42 Cr2 -164.9(3) . . . . ? C3 Cr1 P42 Cr2 -135.88(19) . . . . ? C5 Cr1 P42 Cr2 156.7(3) . . . . ? C1 Cr1 P42 Cr2 133.40(18) . . . . ? P31 Cr1 P42 Cr2 -47.9(4) . . . . ? P11 Cr1 P42 Cr2 48.7(5) . . . . ? P2 Cr1 P42 Cr2 -12.0(3) . . . . ? P21 Cr1 P42 Cr2 0.3(4) . . . . ? P1 Cr1 P42 Cr2 40.1(3) . . . . ? P4 Cr1 P42 Cr2 -84.1(9) . . . . ? P32 P42 P52 P12 0.2(7) . . . . ? Cr2 P42 P52 P12 -46.5(4) . . . . ? Cr1 P42 P52 P12 47.1(4) . . . . ? P32 P42 P52 Cr1 -46.9(4) . . . . ? Cr2 P42 P52 Cr1 -93.6(2) . . . . ? P32 P42 P52 Cr2 46.7(4) . . . . ? Cr1 P42 P52 Cr2 93.6(2) . . . . ? P22 P12 P52 P42 0.1(7) . . . . ? Cr2 P12 P52 P42 46.2(4) . . . . ? Cr1 P12 P52 P42 -46.9(4) . . . . ? P22 P12 P52 Cr1 47.0(4) . . . . ? Cr2 P12 P52 Cr1 93.1(2) . . . . ? P22 P12 P52 Cr2 -46.1(4) . . . . ? Cr1 P12 P52 Cr2 -93.1(2) . . . . ? C2 Cr1 P52 P42 -162.6(3) . . . . ? C4 Cr1 P52 P42 -72.9(4) . . . . ? C3 Cr1 P52 P42 -100.3(12) . . . . ? C5 Cr1 P52 P42 -101.4(4) . . . . ? C1 Cr1 P52 P42 -139.7(3) . . . . ? P31 Cr1 P52 P42 63.0(5) . . . . ? P11 Cr1 P52 P42 140.9(12) . . . . ? P2 Cr1 P52 P42 103.7(4) . . . . ? P21 Cr1 P52 P42 111.4(5) . . . . ? P1 Cr1 P52 P42 137.0(5) . . . . ? P4 Cr1 P52 P42 8.8(3) . . . . ? C2 Cr1 P52 P12 68.4(5) . . . . ? C4 Cr1 P52 P12 158.1(3) . . . . ? C3 Cr1 P52 P12 130.7(11) . . . . ? C5 Cr1 P52 P12 129.7(4) . . . . ? C1 Cr1 P52 P12 91.3(4) . . . . ? P31 Cr1 P52 P12 -66.0(5) . . . . ? P11 Cr1 P52 P12 12.0(11) . . . . ? P2 Cr1 P52 P12 -25.3(4) . . . . ? P21 Cr1 P52 P12 -17.6(5) . . . . ? P42 Cr1 P52 P12 -129.0(5) . . . . ? P1 Cr1 P52 P12 8.1(4) . . . . ? P4 Cr1 P52 P12 -120.2(4) . . . . ? C2 Cr1 P52 Cr2 133.2(2) . . . . ? C4 Cr1 P52 Cr2 -137.03(19) . . . . ? C3 Cr1 P52 Cr2 -164.4(10) . . . . ? C5 Cr1 P52 Cr2 -165.5(3) . . . . ? C1 Cr1 P52 Cr2 156.1(3) . . . . ? P31 Cr1 P52 Cr2 -1.1(5) . . . . ? P11 Cr1 P52 Cr2 76.8(11) . . . . ? P2 Cr1 P52 Cr2 39.6(3) . . . . ? P21 Cr1 P52 Cr2 47.2(4) . . . . ? P42 Cr1 P52 Cr2 -64.1(3) . . . . ? P1 Cr1 P52 Cr2 72.9(4) . . . . ? P4 Cr1 P52 Cr2 -55.4(2) . . . . ? P41 P31 Cr2 C11 -162.1(6) . . . . ? P21 P31 Cr2 C11 67.2(6) . . . . ? Cr1 P31 Cr2 C11 131.8(3) . . . . ? P41 P31 Cr2 C15 -89.5(16) . . . . ? P21 P31 Cr2 C15 139.8(14) . . . . ? Cr1 P31 Cr2 C15 -155.6(12) . . . . ? P41 P31 Cr2 C14 -71.4(7) . . . . ? P21 P31 Cr2 C14 157.9(5) . . . . ? Cr1 P31 Cr2 C14 -137.5(2) . . . . ? P41 P31 Cr2 C13 -101.7(6) . . . . ? P21 P31 Cr2 C13 127.6(5) . . . . ? Cr1 P31 Cr2 C13 -167.7(3) . . . . ? P41 P31 Cr2 C12 -140.0(6) . . . . ? P21 P31 Cr2 C12 89.2(5) . . . . ? Cr1 P31 Cr2 C12 153.9(3) . . . . ? P41 P31 Cr2 P21 130.7(8) . . . . ? Cr1 P31 Cr2 P21 64.6(5) . . . . ? P41 P31 Cr2 P11 89.7(7) . . . . ? P21 P31 Cr2 P11 -41.0(6) . . . . ? Cr1 P31 Cr2 P11 23.6(5) . . . . ? P41 P31 Cr2 P51 37.7(7) . . . . ? P21 P31 Cr2 P51 -93.0(7) . . . . ? Cr1 P31 Cr2 P51 -28.4(6) . . . . ? P41 P31 Cr2 P42 17.1(7) . . . . ? P21 P31 Cr2 P42 -113.6(6) . . . . ? Cr1 P31 Cr2 P42 -49.0(4) . . . . ? P41 P31 Cr2 P22 147.4(11) . . . . ? P21 P31 Cr2 P22 16.7(9) . . . . ? Cr1 P31 Cr2 P22 81.3(7) . . . . ? P41 P31 Cr2 P5 49.2(6) . . . . ? P21 P31 Cr2 P5 -81.6(6) . . . . ? Cr1 P31 Cr2 P5 -16.9(5) . . . . ? P31 P21 Cr2 C11 -142.5(5) . . . . ? P11 P21 Cr2 C11 92.1(5) . . . . ? Cr1 P21 Cr2 C11 155.0(3) . . . . ? P31 P21 Cr2 C15 -164.3(5) . . . . ? P11 P21 Cr2 C15 70.3(7) . . . . ? Cr1 P21 Cr2 C15 133.1(3) . . . . ? P31 P21 Cr2 C14 -98.8(14) . . . . ? P11 P21 Cr2 C14 135.8(13) . . . . ? Cr1 P21 Cr2 C14 -161.3(11) . . . . ? P31 P21 Cr2 C13 -75.6(6) . . . . ? P11 P21 Cr2 C13 159.0(5) . . . . ? Cr1 P21 Cr2 C13 -138.1(2) . . . . ? P31 P21 Cr2 C12 -104.3(5) . . . . ? P11 P21 Cr2 C12 130.2(5) . . . . ? Cr1 P21 Cr2 C12 -166.9(3) . . . . ? P11 P21 Cr2 P31 -125.4(7) . . . . ? Cr1 P21 Cr2 P31 -62.6(5) . . . . ? P31 P21 Cr2 P11 125.4(7) . . . . ? Cr1 P21 Cr2 P11 62.9(5) . . . . ? P31 P21 Cr2 P51 88.4(6) . . . . ? P11 P21 Cr2 P51 -37.0(6) . . . . ? Cr1 P21 Cr2 P51 25.8(5) . . . . ? P31 P21 Cr2 P42 62.9(6) . . . . ? P11 P21 Cr2 P42 -62.5(6) . . . . ? Cr1 P21 Cr2 P42 0.3(4) . . . . ? P31 P21 Cr2 P22 -15.5(9) . . . . ? P11 P21 Cr2 P22 -140.9(12) . . . . ? Cr1 P21 Cr2 P22 -78.1(10) . . . . ? P31 P21 Cr2 P5 99.0(5) . . . . ? P11 P21 Cr2 P5 -26.5(5) . . . . ? Cr1 P21 Cr2 P5 36.4(3) . . . . ? P51 P11 Cr2 C11 128.8(6) . . . . ? P21 P11 Cr2 C11 -100.9(6) . . . . ? Cr1 P11 Cr2 C11 -165.4(4) . . . . ? P51 P11 Cr2 C15 90.4(6) . . . . ? P21 P11 Cr2 C15 -139.3(5) . . . . ? Cr1 P11 Cr2 C15 156.2(4) . . . . ? P51 P11 Cr2 C14 68.1(8) . . . . ? P21 P11 Cr2 C14 -161.6(5) . . . . ? Cr1 P11 Cr2 C14 133.9(4) . . . . ? P51 P11 Cr2 C13 132.6(15) . . . . ? P21 P11 Cr2 C13 -97.1(18) . . . . ? Cr1 P11 Cr2 C13 -161.6(14) . . . . ? P51 P11 Cr2 C12 157.8(5) . . . . ? P21 P11 Cr2 C12 -71.9(7) . . . . ? Cr1 P11 Cr2 C12 -136.5(2) . . . . ? P51 P11 Cr2 P31 -89.3(7) . . . . ? P21 P11 Cr2 P31 41.0(6) . . . . ? Cr1 P11 Cr2 P31 -23.5(6) . . . . ? P51 P11 Cr2 P21 -130.3(8) . . . . ? Cr1 P11 Cr2 P21 -64.5(6) . . . . ? P21 P11 Cr2 P51 130.3(8) . . . . ? Cr1 P11 Cr2 P51 65.8(6) . . . . ? P51 P11 Cr2 P42 -16.4(6) . . . . ? P21 P11 Cr2 P42 113.9(6) . . . . ? Cr1 P11 Cr2 P42 49.4(3) . . . . ? P51 P11 Cr2 P22 -112.2(7) . . . . ? P21 P11 Cr2 P22 18.1(6) . . . . ? Cr1 P11 Cr2 P22 -46.4(4) . . . . ? P51 P11 Cr2 P5 6.7(8) . . . . ? P21 P11 Cr2 P5 137.0(9) . . . . ? Cr1 P11 Cr2 P5 72.4(5) . . . . ? P11 P51 Cr2 C11 -72.9(8) . . . . ? P41 P51 Cr2 C11 158.3(5) . . . . ? Cr1 P51 Cr2 C11 -136.6(3) . . . . ? P11 P51 Cr2 C15 -101.6(7) . . . . ? P41 P51 Cr2 C15 129.5(6) . . . . ? Cr1 P51 Cr2 C15 -165.3(4) . . . . ? P11 P51 Cr2 C14 -139.8(7) . . . . ? P41 P51 Cr2 C14 91.3(6) . . . . ? Cr1 P51 Cr2 C14 156.5(3) . . . . ? P11 P51 Cr2 C13 -161.4(6) . . . . ? P41 P51 Cr2 C13 69.7(8) . . . . ? Cr1 P51 Cr2 C13 134.9(4) . . . . ? P11 P51 Cr2 C12 -95.8(17) . . . . ? P41 P51 Cr2 C12 135.4(15) . . . . ? Cr1 P51 Cr2 C12 -159.5(13) . . . . ? P11 P51 Cr2 P31 91.5(7) . . . . ? P41 P51 Cr2 P31 -37.4(7) . . . . ? Cr1 P51 Cr2 P31 27.8(5) . . . . ? P11 P51 Cr2 P21 37.9(7) . . . . ? P41 P51 Cr2 P21 -90.9(6) . . . . ? Cr1 P51 Cr2 P21 -25.8(5) . . . . ? P41 P51 Cr2 P11 -128.9(9) . . . . ? Cr1 P51 Cr2 P11 -63.7(7) . . . . ? P11 P51 Cr2 P42 141.8(15) . . . . ? P41 P51 Cr2 P42 13.0(11) . . . . ? Cr1 P51 Cr2 P42 78.1(11) . . . . ? P11 P51 Cr2 P22 66.2(7) . . . . ? P41 P51 Cr2 P22 -62.7(6) . . . . ? Cr1 P51 Cr2 P22 2.5(5) . . . . ? P11 P51 Cr2 P5 -21(3) . . . . ? P41 P51 Cr2 P5 -150(3) . . . . ? Cr1 P51 Cr2 P5 -84(3) . . . . ? P52 P42 Cr2 C11 -68.2(5) . . . . ? P32 P42 Cr2 C11 161.5(3) . . . . ? Cr1 P42 Cr2 C11 -133.1(2) . . . . ? P52 P42 Cr2 C15 -84.0(4) . . . . ? P32 P42 Cr2 C15 145.8(4) . . . . ? Cr1 P42 Cr2 C15 -148.8(2) . . . . ? P52 P42 Cr2 C14 -121.0(4) . . . . ? P32 P42 Cr2 C14 108.7(4) . . . . ? Cr1 P42 Cr2 C14 174.1(3) . . . . ? P52 P42 Cr2 C13 -153.6(3) . . . . ? P32 P42 Cr2 C13 76.1(4) . . . . ? Cr1 P42 Cr2 C13 141.5(2) . . . . ? P52 P42 Cr2 C12 -151.2(7) . . . . ? P32 P42 Cr2 C12 78.6(8) . . . . ? Cr1 P42 Cr2 C12 144.0(6) . . . . ? P52 P42 Cr2 P31 112.7(5) . . . . ? P32 P42 Cr2 P31 -17.6(5) . . . . ? Cr1 P42 Cr2 P31 47.9(4) . . . . ? P52 P42 Cr2 P21 64.5(5) . . . . ? P32 P42 Cr2 P21 -65.7(5) . . . . ? Cr1 P42 Cr2 P21 -0.3(4) . . . . ? P52 P42 Cr2 P11 16.4(6) . . . . ? P32 P42 Cr2 P11 -113.8(6) . . . . ? Cr1 P42 Cr2 P11 -48.4(5) . . . . ? P52 P42 Cr2 P51 -14.1(13) . . . . ? P32 P42 Cr2 P51 -144.3(13) . . . . ? Cr1 P42 Cr2 P51 -78.9(12) . . . . ? P52 P42 Cr2 P22 92.7(4) . . . . ? P32 P42 Cr2 P22 -37.6(4) . . . . ? Cr1 P42 Cr2 P22 27.8(3) . . . . ? P52 P42 Cr2 P5 -8.1(4) . . . . ? P32 P42 Cr2 P5 -138.4(5) . . . . ? Cr1 P42 Cr2 P5 -72.9(4) . . . . ? P32 P22 Cr2 C11 -154.0(3) . . . . ? P12 P22 Cr2 C11 75.8(3) . . . . ? Cr1 P22 Cr2 C11 140.0(2) . . . . ? P32 P22 Cr2 C15 -150.1(7) . . . . ? P12 P22 Cr2 C15 79.7(7) . . . . ? Cr1 P22 Cr2 C15 143.9(6) . . . . ? P32 P22 Cr2 C14 -69.2(5) . . . . ? P12 P22 Cr2 C14 160.6(3) . . . . ? Cr1 P22 Cr2 C14 -135.1(2) . . . . ? P32 P22 Cr2 C13 -85.0(4) . . . . ? P12 P22 Cr2 C13 144.8(3) . . . . ? Cr1 P22 Cr2 C13 -150.9(2) . . . . ? P32 P22 Cr2 C12 -121.9(4) . . . . ? P12 P22 Cr2 C12 107.9(4) . . . . ? Cr1 P22 Cr2 C12 172.1(3) . . . . ? P32 P22 Cr2 P31 -8.8(8) . . . . ? P12 P22 Cr2 P31 -139.0(9) . . . . ? Cr1 P22 Cr2 P31 -74.8(8) . . . . ? P32 P22 Cr2 P21 142.5(11) . . . . ? P12 P22 Cr2 P21 12.3(10) . . . . ? Cr1 P22 Cr2 P21 76.5(10) . . . . ? P32 P22 Cr2 P11 111.1(5) . . . . ? P12 P22 Cr2 P11 -19.1(5) . . . . ? Cr1 P22 Cr2 P11 45.2(4) . . . . ? P32 P22 Cr2 P51 63.5(5) . . . . ? P12 P22 Cr2 P51 -66.7(5) . . . . ? Cr1 P22 Cr2 P51 -2.5(5) . . . . ? P32 P22 Cr2 P42 38.3(4) . . . . ? P12 P22 Cr2 P42 -91.9(4) . . . . ? Cr1 P22 Cr2 P42 -27.6(3) . . . . ? P32 P22 Cr2 P5 75.9(4) . . . . ? P12 P22 Cr2 P5 -54.3(4) . . . . ? Cr1 P22 Cr2 P5 10.0(4) . . . . ? P4 P5 Cr2 C11 154.2(2) . . . . ? P1 P5 Cr2 C11 -76.7(4) . . . . ? Cr1 P5 Cr2 C11 -141.22(14) . . . . ? P4 P5 Cr2 C15 121.2(3) . . . . ? P1 P5 Cr2 C15 -109.7(3) . . . . ? Cr1 P5 Cr2 C15 -174.19(19) . . . . ? P4 P5 Cr2 C14 84.8(3) . . . . ? P1 P5 Cr2 C14 -146.1(3) . . . . ? Cr1 P5 Cr2 C14 149.37(16) . . . . ? P4 P5 Cr2 C13 71.0(4) . . . . ? P1 P5 Cr2 C13 -159.9(4) . . . . ? Cr1 P5 Cr2 C13 135.6(2) . . . . ? P4 P5 Cr2 C12 154.2(4) . . . . ? P1 P5 Cr2 C12 -76.7(7) . . . . ? Cr1 P5 Cr2 C12 -141.2(4) . . . . ? P4 P5 Cr2 P31 -48.0(5) . . . . ? P1 P5 Cr2 P31 81.1(5) . . . . ? Cr1 P5 Cr2 P31 16.6(4) . . . . ? P4 P5 Cr2 P21 -100.9(5) . . . . ? P1 P5 Cr2 P21 28.2(5) . . . . ? Cr1 P5 Cr2 P21 -36.3(4) . . . . ? P4 P5 Cr2 P11 -134.4(8) . . . . ? P1 P5 Cr2 P11 -5.3(9) . . . . ? Cr1 P5 Cr2 P11 -69.7(7) . . . . ? P4 P5 Cr2 P51 20(3) . . . . ? P1 P5 Cr2 P51 149(3) . . . . ? Cr1 P5 Cr2 P51 85(3) . . . . ? P4 P5 Cr2 P42 8.0(4) . . . . ? P1 P5 Cr2 P42 137.1(5) . . . . ? Cr1 P5 Cr2 P42 72.6(4) . . . . ? P4 P5 Cr2 P22 -74.6(4) . . . . ? P1 P5 Cr2 P22 54.4(4) . . . . ? Cr1 P5 Cr2 P22 -10.0(4) . . . . ? C14 Cr2 C11 C15 37.75(12) . . . . ? C13 Cr2 C11 C15 80.23(14) . . . . ? C12 Cr2 C11 C15 117.92(18) . . . . ? P31 Cr2 C11 C15 154.0(6) . . . . ? P21 Cr2 C11 C15 -155.9(4) . . . . ? P11 Cr2 C11 C15 -101.0(6) . . . . ? P51 Cr2 C11 C15 -51.0(7) . . . . ? P42 Cr2 C11 C15 -24.7(6) . . . . ? P22 Cr2 C11 C15 177.6(4) . . . . ? P5 Cr2 C11 C15 -62.1(3) . . . . ? C15 Cr2 C11 C12 -117.92(18) . . . . ? C14 Cr2 C11 C12 -80.18(14) . . . . ? C13 Cr2 C11 C12 -37.69(13) . . . . ? P31 Cr2 C11 C12 36.0(6) . . . . ? P21 Cr2 C11 C12 86.2(5) . . . . ? P11 Cr2 C11 C12 141.1(6) . . . . ? P51 Cr2 C11 C12 -168.9(7) . . . . ? P42 Cr2 C11 C12 -142.6(6) . . . . ? P22 Cr2 C11 C12 59.7(4) . . . . ? P5 Cr2 C11 C12 180.0(3) . . . . ? C15 Cr2 C11 C16 121.0(3) . . . . ? C14 Cr2 C11 C16 158.7(3) . . . . ? C13 Cr2 C11 C16 -158.8(3) . . . . ? C12 Cr2 C11 C16 -121.1(3) . . . . ? P31 Cr2 C11 C16 -85.1(6) . . . . ? P21 Cr2 C11 C16 -34.9(5) . . . . ? P11 Cr2 C11 C16 20.0(6) . . . . ? P51 Cr2 C11 C16 70.0(7) . . . . ? P42 Cr2 C11 C16 96.3(6) . . . . ? P22 Cr2 C11 C16 -61.4(5) . . . . ? P5 Cr2 C11 C16 58.9(4) . . . . ? C15 C11 C12 C13 -0.3(2) . . . . ? C16 C11 C12 C13 -177.4(2) . . . . ? Cr2 C11 C12 C13 61.86(15) . . . . ? C15 C11 C12 C17 176.0(2) . . . . ? C16 C11 C12 C17 -1.1(4) . . . . ? Cr2 C11 C12 C17 -121.8(2) . . . . ? C15 C11 C12 Cr2 -62.20(15) . . . . ? C16 C11 C12 Cr2 120.7(2) . . . . ? C15 Cr2 C12 C11 37.24(13) . . . . ? C14 Cr2 C12 C11 79.71(14) . . . . ? C13 Cr2 C12 C11 117.07(19) . . . . ? P31 Cr2 C12 C11 -156.8(4) . . . . ? P21 Cr2 C12 C11 -102.2(5) . . . . ? P11 Cr2 C12 C11 -51.3(7) . . . . ? P51 Cr2 C12 C11 30.7(18) . . . . ? P42 Cr2 C12 C11 113.6(10) . . . . ? P22 Cr2 C12 C11 -131.3(5) . . . . ? P5 Cr2 C12 C11 0.0(7) . . . . ? C11 Cr2 C12 C13 -117.07(19) . . . . ? C15 Cr2 C12 C13 -79.83(14) . . . . ? C14 Cr2 C12 C13 -37.37(13) . . . . ? P31 Cr2 C12 C13 86.1(5) . . . . ? P21 Cr2 C12 C13 140.7(5) . . . . ? P11 Cr2 C12 C13 -168.4(7) . . . . ? P51 Cr2 C12 C13 -86.3(18) . . . . ? P42 Cr2 C12 C13 -3.4(10) . . . . ? P22 Cr2 C12 C13 111.7(5) . . . . ? P5 Cr2 C12 C13 -117.1(6) . . . . ? C11 Cr2 C12 C17 121.8(3) . . . . ? C15 Cr2 C12 C17 159.0(3) . . . . ? C14 Cr2 C12 C17 -158.5(3) . . . . ? C13 Cr2 C12 C17 -121.2(3) . . . . ? P31 Cr2 C12 C17 -35.1(5) . . . . ? P21 Cr2 C12 C17 19.6(5) . . . . ? P11 Cr2 C12 C17 70.5(7) . . . . ? P51 Cr2 C12 C17 152.5(18) . . . . ? P42 Cr2 C12 C17 -124.6(10) . . . . ? P22 Cr2 C12 C17 -9.5(5) . . . . ? P5 Cr2 C12 C17 121.7(7) . . . . ? C11 C12 C13 C14 0.3(2) . . . . ? C17 C12 C13 C14 -176.1(2) . . . . ? Cr2 C12 C13 C14 61.99(15) . . . . ? C11 C12 C13 C18 176.4(2) . . . . ? C17 C12 C13 C18 0.0(4) . . . . ? Cr2 C12 C13 C18 -122.0(2) . . . . ? C11 C12 C13 Cr2 -61.64(15) . . . . ? C17 C12 C13 Cr2 122.0(2) . . . . ? C11 Cr2 C13 C14 -79.93(14) . . . . ? C15 Cr2 C13 C14 -37.42(13) . . . . ? C12 Cr2 C13 C14 -117.61(19) . . . . ? P31 Cr2 C13 C14 138.8(5) . . . . ? P21 Cr2 C13 C14 -168.7(6) . . . . ? P11 Cr2 C13 C14 -84.1(19) . . . . ? P51 Cr2 C13 C14 35.7(7) . . . . ? P42 Cr2 C13 C14 60.9(4) . . . . ? P22 Cr2 C13 C14 165.1(4) . . . . ? P5 Cr2 C13 C14 21.4(4) . . . . ? C11 Cr2 C13 C12 37.68(14) . . . . ? C15 Cr2 C13 C12 80.19(14) . . . . ? C14 Cr2 C13 C12 117.61(19) . . . . ? P31 Cr2 C13 C12 -103.6(5) . . . . ? P21 Cr2 C13 C12 -51.1(6) . . . . ? P11 Cr2 C13 C12 33.5(19) . . . . ? P51 Cr2 C13 C12 153.3(7) . . . . ? P42 Cr2 C13 C12 178.5(4) . . . . ? P22 Cr2 C13 C12 -77.3(4) . . . . ? P5 Cr2 C13 C12 139.0(4) . . . . ? C11 Cr2 C13 C18 159.8(3) . . . . ? C15 Cr2 C13 C18 -157.7(3) . . . . ? C14 Cr2 C13 C18 -120.3(3) . . . . ? C12 Cr2 C13 C18 122.1(3) . . . . ? P31 Cr2 C13 C18 18.5(5) . . . . ? P21 Cr2 C13 C18 71.1(6) . . . . ? P11 Cr2 C13 C18 155.6(19) . . . . ? P51 Cr2 C13 C18 -84.6(7) . . . . ? P42 Cr2 C13 C18 -59.4(5) . . . . ? P22 Cr2 C13 C18 44.8(5) . . . . ? P5 Cr2 C13 C18 -98.9(5) . . . . ? C12 C13 C14 C15 -0.2(2) . . . . ? C18 C13 C14 C15 -176.4(2) . . . . ? Cr2 C13 C14 C15 61.92(15) . . . . ? C12 C13 C14 C19 176.5(2) . . . . ? C18 C13 C14 C19 0.4(4) . . . . ? Cr2 C13 C14 C19 -121.3(2) . . . . ? C12 C13 C14 Cr2 -62.14(15) . . . . ? C18 C13 C14 Cr2 121.7(2) . . . . ? C11 Cr2 C14 C13 79.89(15) . . . . ? C15 Cr2 C14 C13 117.63(19) . . . . ? C12 Cr2 C14 C13 37.41(14) . . . . ? P31 Cr2 C14 C13 -54.2(6) . . . . ? P21 Cr2 C14 C13 31.3(15) . . . . ? P11 Cr2 C14 C13 154.6(6) . . . . ? P51 Cr2 C14 C13 -156.2(5) . . . . ? P42 Cr2 C14 C13 -130.4(4) . . . . ? P22 Cr2 C14 C13 -24.9(6) . . . . ? P5 Cr2 C14 C13 -167.7(3) . . . . ? C11 Cr2 C14 C15 -37.74(13) . . . . ? C13 Cr2 C14 C15 -117.63(19) . . . . ? C12 Cr2 C14 C15 -80.22(15) . . . . ? P31 Cr2 C14 C15 -171.8(6) . . . . ? P21 Cr2 C14 C15 -86.4(15) . . . . ? P11 Cr2 C14 C15 37.0(6) . . . . ? P51 Cr2 C14 C15 86.2(5) . . . . ? P42 Cr2 C14 C15 111.9(4) . . . . ? P22 Cr2 C14 C15 -142.6(6) . . . . ? P5 Cr2 C14 C15 74.7(3) . . . . ? C11 Cr2 C14 C19 -160.0(3) . . . . ? C15 Cr2 C14 C19 -122.3(3) . . . . ? C13 Cr2 C14 C19 120.1(3) . . . . ? C12 Cr2 C14 C19 157.5(3) . . . . ? P31 Cr2 C14 C19 65.9(6) . . . . ? P21 Cr2 C14 C19 151.3(15) . . . . ? P11 Cr2 C14 C19 -85.3(6) . . . . ? P51 Cr2 C14 C19 -36.1(5) . . . . ? P42 Cr2 C14 C19 -10.3(5) . . . . ? P22 Cr2 C14 C19 95.2(6) . . . . ? P5 Cr2 C14 C19 -47.6(3) . . . . ? C12 C11 C15 C14 0.2(2) . . . . ? C16 C11 C15 C14 177.3(2) . . . . ? Cr2 C11 C15 C14 -62.21(15) . . . . ? C12 C11 C15 C20 -177.0(2) . . . . ? C16 C11 C15 C20 0.0(4) . . . . ? Cr2 C11 C15 C20 120.6(2) . . . . ? C12 C11 C15 Cr2 62.41(15) . . . . ? C16 C11 C15 Cr2 -120.5(2) . . . . ? C13 C14 C15 C11 0.0(2) . . . . ? C19 C14 C15 C11 -176.7(2) . . . . ? Cr2 C14 C15 C11 62.03(15) . . . . ? C13 C14 C15 C20 177.2(2) . . . . ? C19 C14 C15 C20 0.5(4) . . . . ? Cr2 C14 C15 C20 -120.8(2) . . . . ? C13 C14 C15 Cr2 -62.01(15) . . . . ? C19 C14 C15 Cr2 121.3(2) . . . . ? C14 Cr2 C15 C11 -116.99(19) . . . . ? C13 Cr2 C15 C11 -79.64(14) . . . . ? C12 Cr2 C15 C11 -37.21(13) . . . . ? P31 Cr2 C15 C11 -93.1(17) . . . . ? P21 Cr2 C15 C11 36.1(6) . . . . ? P11 Cr2 C15 C11 87.8(5) . . . . ? P51 Cr2 C15 C11 140.8(6) . . . . ? P42 Cr2 C15 C11 165.5(4) . . . . ? P22 Cr2 C15 C11 -5.5(10) . . . . ? P5 Cr2 C15 C11 128.5(3) . . . . ? C11 Cr2 C15 C14 116.99(19) . . . . ? C13 Cr2 C15 C14 37.35(13) . . . . ? C12 Cr2 C15 C14 79.78(14) . . . . ? P31 Cr2 C15 C14 23.9(17) . . . . ? P21 Cr2 C15 C14 153.1(6) . . . . ? P11 Cr2 C15 C14 -155.3(5) . . . . ? P51 Cr2 C15 C14 -102.2(6) . . . . ? P42 Cr2 C15 C14 -77.5(4) . . . . ? P22 Cr2 C15 C14 111.5(10) . . . . ? P5 Cr2 C15 C14 -114.5(3) . . . . ? C11 Cr2 C15 C20 -121.3(3) . . . . ? C14 Cr2 C15 C20 121.8(3) . . . . ? C13 Cr2 C15 C20 159.1(3) . . . . ? C12 Cr2 C15 C20 -158.5(2) . . . . ? P31 Cr2 C15 C20 145.6(17) . . . . ? P21 Cr2 C15 C20 -85.2(6) . . . . ? P11 Cr2 C15 C20 -33.5(5) . . . . ? P51 Cr2 C15 C20 19.6(6) . . . . ? P42 Cr2 C15 C20 44.3(5) . . . . ? P22 Cr2 C15 C20 -126.8(10) . . . . ? P5 Cr2 C15 C20 7.3(3) . . . . ? _diffrn_measured_fraction_theta_max 0.970 _diffrn_reflns_theta_full 30.47 _diffrn_measured_fraction_theta_full 0.970 _refine_diff_density_max 0.896 _refine_diff_density_min -0.525 _refine_diff_density_rms 0.091 #===END data_210k _database_code_depnum_ccdc_archive 'CCDC 618751' _audit_creation_method SHELXL-97 _chemical_name_systematic ; \m~2~-\h^5^,\h^5^-cyclopentaphosphole)-bis ((\h^5^-pentamethyl-cyclopentadienyl)-chromium) hexafluoroantimonate ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H30 Cr2 F6 P5 Sb' _chemical_formula_weight 765.04 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting orthorhombic _symmetry_space_group_name_H-M Fddd loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+3/4, -y+3/4, z' '-x+3/4, y, -z+3/4' 'x, -y+3/4, -z+3/4' 'x, y+1/2, z+1/2' '-x+3/4, -y+5/4, z+1/2' '-x+3/4, y+1/2, -z+5/4' 'x, -y+5/4, -z+5/4' 'x+1/2, y, z+1/2' '-x+5/4, -y+3/4, z+1/2' '-x+5/4, y, -z+5/4' 'x+1/2, -y+3/4, -z+5/4' 'x+1/2, y+1/2, z' '-x+5/4, -y+5/4, z' '-x+5/4, y+1/2, -z+3/4' 'x+1/2, -y+5/4, -z+3/4' '-x, -y, -z' 'x-3/4, y-3/4, -z' 'x-3/4, -y, z-3/4' '-x, y-3/4, z-3/4' '-x, -y+1/2, -z+1/2' 'x-3/4, y-1/4, -z+1/2' 'x-3/4, -y+1/2, z-1/4' '-x, y-1/4, z-1/4' '-x+1/2, -y, -z+1/2' 'x-1/4, y-3/4, -z+1/2' 'x-1/4, -y, z-1/4' '-x+1/2, y-3/4, z-1/4' '-x+1/2, -y+1/2, -z' 'x-1/4, y-1/4, -z' 'x-1/4, -y+1/2, z-3/4' '-x+1/2, y-1/4, z-3/4' _cell_length_a 21.3887(6) _cell_length_b 29.4302(8) _cell_length_c 35.9890(10) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_volume 22654.1(11) _cell_formula_units_Z 32 _cell_measurement_temperature 210(2) _cell_measurement_reflns_used 9763 _cell_measurement_theta_min 2.21 _cell_measurement_theta_max 30.40 _exptl_crystal_description 'irregular block' _exptl_crystal_colour 'dark green' _exptl_crystal_size_max 0.60 _exptl_crystal_size_mid 0.52 _exptl_crystal_size_min 0.40 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.794 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 12096 _exptl_absorpt_coefficient_mu 2.032 _exptl_absorpt_correction_type integration _exptl_absorpt_correction_T_min 0.397 _exptl_absorpt_correction_T_max 0.616 _exptl_absorpt_process_details 'XPREP in SHELXTL' _exptl_special_details ; ? ; _diffrn_ambient_temperature 210(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'Bede Microsource X-ray Generator' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEX CCD Diffractometer' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number 0 _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% 0 _diffrn_reflns_number 42851 _diffrn_reflns_av_R_equivalents 0.0197 _diffrn_reflns_av_sigmaI/netI 0.0165 _diffrn_reflns_limit_h_min -30 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_k_min -41 _diffrn_reflns_limit_k_max 41 _diffrn_reflns_limit_l_min -46 _diffrn_reflns_limit_l_max 51 _diffrn_reflns_theta_min 1.31 _diffrn_reflns_theta_max 30.47 _reflns_number_total 8360 _reflns_number_gt 6772 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'SMART V5.625 (Bruker, 2003)' _computing_cell_refinement 'SMART V5.625 (Bruker, 2003)' _computing_data_reduction 'SAINT V6.28A (Bruker, 2003)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'SHELXTL V6.12(Bruker, 2001)' _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0494P)^2^+51.2065P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 8360 _refine_ls_number_parameters 404 _refine_ls_number_restraints 90 _refine_ls_R_factor_all 0.0418 _refine_ls_R_factor_gt 0.0302 _refine_ls_wR_factor_ref 0.0938 _refine_ls_wR_factor_gt 0.0809 _refine_ls_goodness_of_fit_ref 1.067 _refine_ls_restrained_S_all 1.064 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb1 Sb 0.6250 0.1250 0.009910(7) 0.04355(7) Uani 1 2 d S . . F1A F 0.6885(3) 0.1037(3) -0.0166(3) 0.149(3) Uani 0.50 1 d P A 1 F2A F 0.5536(3) 0.1390(3) 0.0344(3) 0.149(3) Uani 0.50 1 d P A 1 F1B F 0.6710(5) 0.1187(2) -0.03368(19) 0.139(3) Uani 0.50 1 d P A 2 F2B F 0.5874(4) 0.1420(2) 0.05366(17) 0.139(3) Uani 0.50 1 d P A 2 F3 F 0.59484(15) 0.06589(8) 0.01000(9) 0.1098(9) Uani 1 1 d . A . Sb2 Sb 0.1250 0.239723(10) 0.1250 0.04802(7) Uani 1 2 d S . . F4 F 0.18527(12) 0.28502(9) 0.12113(8) 0.1078(9) Uani 1 1 d . . . F5 F 0.11803(13) 0.23863(9) 0.07328(6) 0.0925(8) Uani 1 1 d . . . F6 F 0.18671(9) 0.19499(8) 0.12250(6) 0.0758(6) Uani 1 1 d . . . C1 C 0.13919(10) 0.37001(7) 0.01276(6) 0.0324(4) Uani 1 1 d . B . C2 C 0.19761(10) 0.34911(7) 0.00452(6) 0.0341(4) Uani 1 1 d . B . C3 C 0.22735(10) 0.37469(8) -0.02418(6) 0.0367(5) Uani 1 1 d . B . C4 C 0.18748(11) 0.41175(8) -0.03335(6) 0.0365(4) Uani 1 1 d . B . C5 C 0.13320(9) 0.40876(7) -0.01072(6) 0.0324(4) Uani 1 1 d . B . C6 C 0.09130(13) 0.35252(9) 0.03952(8) 0.0487(6) Uani 1 1 d . . . H6A H 0.0650 0.3303 0.0271 0.073 Uiso 1 1 calc R . . H6B H 0.0658 0.3776 0.0483 0.073 Uiso 1 1 calc R . . H6C H 0.1121 0.3383 0.0604 0.073 Uiso 1 1 calc R . . C7 C 0.22160(14) 0.30608(8) 0.02156(8) 0.0530(7) Uani 1 1 d . . . H7A H 0.1981 0.2805 0.0119 0.079 Uiso 1 1 calc R . . H7B H 0.2168 0.3075 0.0483 0.079 Uiso 1 1 calc R . . H7C H 0.2655 0.3024 0.0154 0.079 Uiso 1 1 calc R . . C8 C 0.28846(12) 0.36362(12) -0.04257(8) 0.0571(7) Uani 1 1 d . . . H8A H 0.2811 0.3438 -0.0636 0.086 Uiso 1 1 calc R . . H8B H 0.3157 0.3485 -0.0249 0.086 Uiso 1 1 calc R . . H8C H 0.3082 0.3914 -0.0510 0.086 Uiso 1 1 calc R . . C9 C 0.19777(16) 0.44612(12) -0.06322(8) 0.0612(8) Uani 1 1 d . . . H9A H 0.1753 0.4371 -0.0854 0.092 Uiso 1 1 calc R . . H9B H 0.2421 0.4482 -0.0687 0.092 Uiso 1 1 calc R . . H9C H 0.1827 0.4755 -0.0549 0.092 Uiso 1 1 calc R . . C10 C 0.07726(12) 0.43910(9) -0.01319(8) 0.0484(6) Uani 1 1 d . . . H10A H 0.0518 0.4302 -0.0343 0.073 Uiso 1 1 calc R . . H10B H 0.0908 0.4703 -0.0163 0.073 Uiso 1 1 calc R . . H10C H 0.0529 0.4365 0.0094 0.073 Uiso 1 1 calc R . . Cr1 Cr 0.215698(14) 0.418159(10) 0.025184(9) 0.02647(7) Uani 1 1 d . . . P11 P 0.1861(12) 0.4359(8) 0.0874(5) 0.072(6) Uani 0.25 1 d PU B 1 P21 P 0.2713(8) 0.3981(4) 0.0815(5) 0.060(5) Uani 0.25 1 d PU B 1 P31 P 0.3230(6) 0.4315(7) 0.0379(5) 0.059(5) Uani 0.25 1 d PU B 1 P41 P 0.2755(9) 0.4892(6) 0.0206(5) 0.068(5) Uani 0.25 1 d PU B 1 P51 P 0.1900(7) 0.4919(6) 0.0509(6) 0.068(6) Uani 0.25 1 d PU B 1 P1 P 0.1987(5) 0.4234(3) 0.0919(3) 0.056(2) Uani 0.50 1 d PU B 2 P2 P 0.2891(4) 0.3967(2) 0.0732(2) 0.051(2) Uani 0.50 1 d PU B 2 P3 P 0.3252(5) 0.4421(4) 0.0307(3) 0.054(2) Uani 0.50 1 d PU B 2 P4 P 0.2559(4) 0.4952(2) 0.0216(2) 0.0523(19) Uani 0.50 1 d PU B 2 P5 P 0.1790(3) 0.4843(4) 0.0597(3) 0.057(3) Uani 0.50 1 d PU B 2 P12 P 0.2223(6) 0.4079(4) 0.0928(2) 0.066(4) Uani 0.25 1 d PU B 3 P22 P 0.3117(5) 0.4047(3) 0.0608(4) 0.067(3) Uani 0.25 1 d PU B 3 P32 P 0.3148(5) 0.4607(4) 0.0228(2) 0.069(3) Uani 0.25 1 d PU B 3 P42 P 0.2289(6) 0.5000(3) 0.0294(3) 0.066(3) Uani 0.25 1 d PU B 3 P52 P 0.1723(4) 0.4687(4) 0.0725(3) 0.064(3) Uani 0.25 1 d PU B 3 Cr2 Cr 0.283271(14) 0.478202(10) 0.086490(9) 0.02626(7) Uani 1 1 d . . . C11 C 0.29480(11) 0.49158(7) 0.14618(6) 0.0350(4) Uani 1 1 d . B . C12 C 0.35437(11) 0.48055(7) 0.13108(6) 0.0362(4) Uani 1 1 d . B . C13 C 0.36888(9) 0.51419(8) 0.10400(6) 0.0346(4) Uani 1 1 d . B . C14 C 0.31860(10) 0.54582(7) 0.10257(6) 0.0308(4) Uani 1 1 d . B . C15 C 0.27253(9) 0.53182(7) 0.12875(6) 0.0313(4) Uani 1 1 d . B . C16 C 0.26235(16) 0.46629(10) 0.17687(7) 0.0578(8) Uani 1 1 d . . . H16A H 0.2766 0.4777 0.2007 0.087 Uiso 1 1 calc R B . H16B H 0.2720 0.4342 0.1750 0.087 Uiso 1 1 calc R . . H16C H 0.2175 0.4707 0.1747 0.087 Uiso 1 1 calc R . . C17 C 0.39605(16) 0.44246(10) 0.14322(10) 0.0645(9) Uani 1 1 d . . . H17A H 0.4223 0.4527 0.1635 0.097 Uiso 1 1 calc R B . H17B H 0.4221 0.4330 0.1226 0.097 Uiso 1 1 calc R . . H17C H 0.3707 0.4170 0.1514 0.097 Uiso 1 1 calc R . . C18 C 0.42840(12) 0.51797(12) 0.08220(8) 0.0577(8) Uani 1 1 d . . . H18A H 0.4567 0.5387 0.0947 0.087 Uiso 1 1 calc R B . H18B H 0.4192 0.5294 0.0575 0.087 Uiso 1 1 calc R . . H18C H 0.4477 0.4883 0.0802 0.087 Uiso 1 1 calc R . . C19 C 0.31733(14) 0.58762(8) 0.07903(8) 0.0492(6) Uani 1 1 d . . . H19A H 0.3370 0.6125 0.0923 0.074 Uiso 1 1 calc R B . H19B H 0.2743 0.5956 0.0734 0.074 Uiso 1 1 calc R . . H19C H 0.3398 0.5820 0.0561 0.074 Uiso 1 1 calc R . . C20 C 0.21318(11) 0.55620(9) 0.13773(8) 0.0478(6) Uani 1 1 d . . . H20A H 0.2205 0.5773 0.1579 0.072 Uiso 1 1 calc R B . H20B H 0.1816 0.5344 0.1451 0.072 Uiso 1 1 calc R . . H20C H 0.1989 0.5727 0.1160 0.072 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.03556(11) 0.05368(14) 0.04142(13) 0.000 0.000 0.00408(9) F1A 0.092(3) 0.148(5) 0.208(7) -0.042(4) 0.091(4) 0.014(3) F2A 0.092(3) 0.148(5) 0.208(7) -0.042(4) 0.091(4) 0.014(3) F1B 0.236(7) 0.097(3) 0.085(3) -0.011(2) 0.098(4) -0.019(4) F2B 0.236(7) 0.097(3) 0.085(3) -0.011(2) 0.098(4) -0.019(4) F3 0.132(2) 0.0656(14) 0.132(2) 0.0136(14) -0.0353(19) -0.0280(15) Sb2 0.03956(12) 0.05683(15) 0.04767(14) 0.000 0.00815(10) 0.000 F4 0.0885(17) 0.0932(17) 0.142(2) -0.0297(16) 0.0271(16) -0.0435(14) F5 0.122(2) 0.1074(18) 0.0482(11) 0.0206(11) -0.0008(12) -0.0219(15) F6 0.0584(11) 0.0899(14) 0.0790(13) -0.0217(11) 0.0009(9) 0.0206(10) C1 0.0325(9) 0.0321(9) 0.0325(10) -0.0043(8) -0.0036(8) -0.0010(7) C2 0.0370(10) 0.0303(9) 0.0351(11) -0.0087(8) -0.0076(8) 0.0064(8) C3 0.0314(9) 0.0484(12) 0.0303(10) -0.0135(9) -0.0022(8) 0.0052(9) C4 0.0378(10) 0.0457(12) 0.0260(10) 0.0007(8) -0.0048(8) -0.0007(9) C5 0.0303(9) 0.0345(9) 0.0323(10) -0.0032(8) -0.0078(8) 0.0046(7) C6 0.0475(13) 0.0506(14) 0.0482(14) -0.0009(11) 0.0071(11) -0.0128(11) C7 0.0675(17) 0.0318(11) 0.0596(17) -0.0049(11) -0.0187(14) 0.0146(11) C8 0.0383(12) 0.083(2) 0.0504(16) -0.0275(15) 0.0050(11) 0.0070(13) C9 0.0717(19) 0.076(2) 0.0360(13) 0.0203(13) -0.0078(13) -0.0093(16) C10 0.0403(12) 0.0509(14) 0.0540(15) -0.0065(12) -0.0153(11) 0.0171(10) Cr1 0.02648(14) 0.02750(14) 0.02544(15) -0.00096(11) -0.00204(11) 0.00353(11) P11 0.056(8) 0.126(16) 0.033(7) -0.024(8) 0.013(6) -0.051(10) P21 0.107(12) 0.023(2) 0.051(7) 0.000(3) -0.043(7) 0.001(5) P31 0.022(2) 0.085(11) 0.070(10) -0.047(8) 0.010(4) -0.007(4) P41 0.097(12) 0.073(9) 0.034(2) 0.016(5) -0.019(6) -0.047(8) P51 0.056(8) 0.053(5) 0.096(12) -0.040(7) -0.044(8) 0.036(6) P1 0.066(6) 0.076(5) 0.027(2) -0.001(3) 0.004(3) -0.041(4) P2 0.066(4) 0.0329(11) 0.055(5) -0.0091(19) -0.034(3) 0.019(2) P3 0.0357(14) 0.081(5) 0.045(3) -0.027(3) 0.0178(15) -0.0209(19) P4 0.076(5) 0.0359(17) 0.0445(18) 0.0147(13) -0.025(3) -0.015(3) P5 0.030(2) 0.074(4) 0.069(5) -0.039(3) -0.008(2) 0.016(2) P12 0.114(10) 0.054(5) 0.031(2) 0.006(3) -0.017(5) -0.046(5) P22 0.051(4) 0.065(6) 0.086(7) -0.045(5) -0.039(4) 0.036(4) P32 0.071(6) 0.104(8) 0.034(3) -0.018(4) 0.012(3) -0.048(5) P42 0.091(8) 0.0302(16) 0.076(7) 0.001(3) -0.054(5) 0.004(4) P52 0.0251(16) 0.099(8) 0.067(7) -0.053(5) 0.002(4) 0.001(5) Cr2 0.02610(14) 0.02664(14) 0.02606(15) -0.00173(11) -0.00012(11) 0.00009(11) C11 0.0441(11) 0.0356(10) 0.0253(9) -0.0002(8) -0.0026(8) -0.0114(9) C12 0.0391(10) 0.0329(10) 0.0365(11) -0.0049(8) -0.0121(9) 0.0006(8) C13 0.0283(9) 0.0407(11) 0.0348(11) -0.0101(9) 0.0011(8) -0.0045(8) C14 0.0337(9) 0.0287(9) 0.0298(9) -0.0016(7) 0.0018(8) -0.0058(7) C15 0.0304(9) 0.0322(9) 0.0312(10) -0.0072(8) 0.0044(8) -0.0039(7) C16 0.081(2) 0.0621(17) 0.0305(12) 0.0069(11) -0.0022(12) -0.0348(15) C17 0.0724(19) 0.0439(14) 0.077(2) -0.0119(14) -0.0411(17) 0.0171(13) C18 0.0324(11) 0.084(2) 0.0569(17) -0.0226(15) 0.0111(11) -0.0118(12) C19 0.0691(17) 0.0338(11) 0.0446(13) 0.0081(10) -0.0033(12) -0.0122(11) C20 0.0356(11) 0.0496(13) 0.0583(15) -0.0233(12) 0.0085(11) 0.0016(10) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb1 F1A 1.775(6) 14_545 ? Sb1 F1A 1.775(6) . ? Sb1 F2A 1.812(5) . ? Sb1 F2A 1.812(5) 14_545 ? Sb1 F2B 1.837(5) 14_545 ? Sb1 F2B 1.837(5) . ? Sb1 F3 1.855(2) . ? Sb1 F3 1.855(2) 14_545 ? Sb1 F1B 1.861(6) . ? Sb1 F1B 1.862(6) 14_545 ? Sb2 F4 1.860(2) 11_454 ? Sb2 F4 1.860(2) . ? Sb2 F6 1.8663(19) 11_454 ? Sb2 F6 1.8664(19) . ? Sb2 F5 1.868(2) 11_454 ? Sb2 F5 1.868(2) . ? C1 C2 1.424(3) . ? C1 C5 1.425(3) . ? C1 C6 1.497(3) . ? C1 Cr1 2.210(2) . ? C2 C3 1.428(3) . ? C2 C7 1.498(3) . ? C2 Cr1 2.198(2) . ? C3 C4 1.423(3) . ? C3 C8 1.501(3) . ? C3 Cr1 2.203(2) . ? C4 C5 1.421(3) . ? C4 C9 1.493(3) . ? C4 Cr1 2.199(2) . ? C5 C10 1.496(3) . ? C5 Cr1 2.204(2) . ? C6 H6A 0.9700 . ? C6 H6B 0.9700 . ? C6 H6C 0.9700 . ? C7 H7A 0.9700 . ? C7 H7B 0.9700 . ? C7 H7C 0.9700 . ? C8 H8A 0.9700 . ? C8 H8B 0.9700 . ? C8 H8C 0.9700 . ? C9 H9A 0.9700 . ? C9 H9B 0.9700 . ? C9 H9C 0.9700 . ? C10 H10A 0.9700 . ? C10 H10B 0.9700 . ? C10 H10C 0.9700 . ? Cr1 P31 2.373(14) . ? Cr1 P11 2.38(2) . ? Cr1 P2 2.418(7) . ? Cr1 P21 2.423(16) . ? Cr1 P51 2.423(13) . ? Cr1 P4 2.427(6) . ? Cr1 P42 2.431(8) . ? P11 P51 2.11(2) . ? P11 P21 2.14(2) . ? P11 Cr2 2.42(2) . ? P21 P31 2.15(2) . ? P21 Cr2 2.377(12) . ? P31 P41 2.07(2) . ? P31 Cr2 2.381(16) . ? P41 P51 2.13(2) . ? P41 Cr2 2.398(16) . ? P51 Cr2 2.405(14) . ? P1 P5 2.176(13) . ? P1 P2 2.192(12) . ? P1 Cr2 2.432(10) . ? P2 P3 2.173(11) . ? P2 Cr2 2.449(7) . ? P3 P4 2.179(13) . ? P3 Cr2 2.444(10) . ? P4 P5 2.167(10) . ? P4 Cr2 2.460(8) . ? P5 Cr2 2.437(8) . ? P12 P52 2.206(12) . ? P12 P22 2.232(12) . ? P12 Cr2 2.455(8) . ? P22 P32 2.143(11) . ? P22 Cr2 2.430(7) . ? P32 P42 2.186(12) . ? P32 Cr2 2.444(9) . ? P42 P52 2.175(12) . ? P42 Cr2 2.448(8) . ? P52 Cr2 2.442(9) . ? Cr2 C11 2.198(2) . ? Cr2 C15 2.204(2) . ? Cr2 C14 2.206(2) . ? Cr2 C13 2.207(2) . ? Cr2 C12 2.212(2) . ? C11 C15 1.422(3) . ? C11 C12 1.423(3) . ? C11 C16 1.502(3) . ? C12 C13 1.423(3) . ? C12 C17 1.498(3) . ? C13 C14 1.423(3) . ? C13 C18 1.500(3) . ? C14 C15 1.424(3) . ? C14 C19 1.494(3) . ? C15 C20 1.493(3) . ? C16 H16A 0.9700 . ? C16 H16B 0.9700 . ? C16 H16C 0.9700 . ? C17 H17A 0.9700 . ? C17 H17B 0.9700 . ? C17 H17C 0.9700 . ? C18 H18A 0.9700 . ? C18 H18B 0.9700 . ? C18 H18C 0.9700 . ? C19 H19A 0.9700 . ? C19 H19B 0.9700 . ? C19 H19C 0.9700 . ? C20 H20A 0.9700 . ? C20 H20B 0.9700 . ? C20 H20C 0.9700 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F1A Sb1 F1A 114.9(7) 14_545 . ? F1A Sb1 F2A 62.4(5) 14_545 . ? F1A Sb1 F2A 171.1(4) . . ? F1A Sb1 F2A 171.1(4) 14_545 14_545 ? F1A Sb1 F2A 62.4(5) . 14_545 ? F2A Sb1 F2A 121.7(7) . 14_545 ? F1A Sb1 F2B 153.2(5) 14_545 14_545 ? F1A Sb1 F2B 91.7(4) . 14_545 ? F2A Sb1 F2B 90.8(5) . 14_545 ? F2A Sb1 F2B 32.0(4) 14_545 14_545 ? F1A Sb1 F2B 91.7(4) 14_545 . ? F1A Sb1 F2B 153.1(5) . . ? F2A Sb1 F2B 32.0(4) . . ? F2A Sb1 F2B 90.8(5) 14_545 . ? F2B Sb1 F2B 62.1(6) 14_545 . ? F1A Sb1 F3 93.8(3) 14_545 . ? F1A Sb1 F3 86.3(3) . . ? F2A Sb1 F3 85.4(3) . . ? F2A Sb1 F3 94.5(3) 14_545 . ? F2B Sb1 F3 84.0(2) 14_545 . ? F2B Sb1 F3 95.8(2) . . ? F1A Sb1 F3 86.3(3) 14_545 14_545 ? F1A Sb1 F3 93.8(3) . 14_545 ? F2A Sb1 F3 94.5(3) . 14_545 ? F2A Sb1 F3 85.4(3) 14_545 14_545 ? F2B Sb1 F3 95.8(2) 14_545 14_545 ? F2B Sb1 F3 84.0(2) . 14_545 ? F3 Sb1 F3 179.80(19) . 14_545 ? F1A Sb1 F1B 89.2(5) 14_545 . ? F1A Sb1 F1B 26.7(4) . . ? F2A Sb1 F1B 151.5(5) . . ? F2A Sb1 F1B 86.7(4) 14_545 . ? F2B Sb1 F1B 117.6(5) 14_545 . ? F2B Sb1 F1B 168.8(4) . . ? F3 Sb1 F1B 95.3(3) . . ? F3 Sb1 F1B 84.9(2) 14_545 . ? F1A Sb1 F1B 26.7(4) 14_545 14_545 ? F1A Sb1 F1B 89.2(5) . 14_545 ? F2A Sb1 F1B 86.7(4) . 14_545 ? F2A Sb1 F1B 151.5(5) 14_545 14_545 ? F2B Sb1 F1B 168.8(4) 14_545 14_545 ? F2B Sb1 F1B 117.6(5) . 14_545 ? F3 Sb1 F1B 84.9(2) . 14_545 ? F3 Sb1 F1B 95.3(3) 14_545 14_545 ? F1B Sb1 F1B 65.1(6) . 14_545 ? F4 Sb2 F4 88.41(18) 11_454 . ? F4 Sb2 F6 90.68(12) 11_454 11_454 ? F4 Sb2 F6 178.14(12) . 11_454 ? F4 Sb2 F6 178.15(13) 11_454 . ? F4 Sb2 F6 90.68(12) . . ? F6 Sb2 F6 90.28(14) 11_454 . ? F4 Sb2 F5 89.60(12) 11_454 11_454 ? F4 Sb2 F5 91.81(13) . 11_454 ? F6 Sb2 F5 89.80(11) 11_454 11_454 ? F6 Sb2 F5 88.82(10) . 11_454 ? F4 Sb2 F5 91.82(13) 11_454 . ? F4 Sb2 F5 89.60(12) . . ? F6 Sb2 F5 88.82(10) 11_454 . ? F6 Sb2 F5 89.79(11) . . ? F5 Sb2 F5 178.03(16) 11_454 . ? C2 C1 C5 107.52(19) . . ? C2 C1 C6 125.9(2) . . ? C5 C1 C6 126.5(2) . . ? C2 C1 Cr1 70.69(12) . . ? C5 C1 Cr1 70.93(12) . . ? C6 C1 Cr1 126.65(16) . . ? C1 C2 C3 108.29(19) . . ? C1 C2 C7 125.5(2) . . ? C3 C2 C7 126.1(2) . . ? C1 C2 Cr1 71.62(11) . . ? C3 C2 Cr1 71.27(12) . . ? C7 C2 Cr1 125.66(16) . . ? C4 C3 C2 107.75(19) . . ? C4 C3 C8 125.9(2) . . ? C2 C3 C8 126.3(2) . . ? C4 C3 Cr1 70.99(12) . . ? C2 C3 Cr1 70.88(12) . . ? C8 C3 Cr1 125.45(16) . . ? C5 C4 C3 108.0(2) . . ? C5 C4 C9 125.1(2) . . ? C3 C4 C9 126.7(2) . . ? C5 C4 Cr1 71.36(12) . . ? C3 C4 Cr1 71.29(12) . . ? C9 C4 Cr1 126.24(18) . . ? C4 C5 C1 108.42(18) . . ? C4 C5 C10 125.6(2) . . ? C1 C5 C10 125.8(2) . . ? C4 C5 Cr1 70.99(12) . . ? C1 C5 Cr1 71.40(11) . . ? C10 C5 Cr1 126.90(16) . . ? C1 C6 H6A 109.5 . . ? C1 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C1 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C2 Cr1 C4 63.15(8) . . ? C2 Cr1 C3 37.85(9) . . ? C4 Cr1 C3 37.72(9) . . ? C2 Cr1 C5 62.93(8) . . ? C4 Cr1 C5 37.64(8) . . ? C3 Cr1 C5 62.94(8) . . ? C2 Cr1 C1 37.69(8) . . ? C4 Cr1 C1 63.14(8) . . ? C3 Cr1 C1 63.15(8) . . ? C5 Cr1 C1 37.67(8) . . ? C2 Cr1 P31 112.8(5) . . ? C4 Cr1 P31 117.7(4) . . ? C3 Cr1 P31 98.2(4) . . ? C5 Cr1 P31 155.3(4) . . ? C1 Cr1 P31 149.4(5) . . ? C2 Cr1 P11 118.3(5) . . ? C4 Cr1 P11 147.7(6) . . ? C3 Cr1 P11 156.1(5) . . ? C5 Cr1 P11 111.4(6) . . ? C1 Cr1 P11 97.7(6) . . ? P31 Cr1 P11 92.2(7) . . ? C2 Cr1 P2 96.57(18) . . ? C4 Cr1 P2 147.14(19) . . ? C3 Cr1 P2 110.55(17) . . ? C5 Cr1 P2 154.9(2) . . ? C1 Cr1 P2 117.2(2) . . ? P31 Cr1 P2 43.7(5) . . ? P11 Cr1 P2 63.8(6) . . ? C2 Cr1 P21 98.3(3) . . ? C4 Cr1 P21 156.2(3) . . ? C3 Cr1 P21 118.5(3) . . ? C5 Cr1 P21 148.5(4) . . ? C1 Cr1 P21 112.1(4) . . ? P31 Cr1 P21 53.4(5) . . ? P11 Cr1 P21 53.0(6) . . ? P2 Cr1 P21 11.5(5) . . ? C2 Cr1 P51 156.5(4) . . ? C4 Cr1 P51 112.4(4) . . ? C3 Cr1 P51 148.6(5) . . ? C5 Cr1 P51 98.9(3) . . ? C1 Cr1 P51 118.9(4) . . ? P31 Cr1 P51 89.9(6) . . ? P11 Cr1 P51 52.0(7) . . ? P2 Cr1 P51 96.2(4) . . ? P21 Cr1 P51 90.6(5) . . ? C2 Cr1 P4 155.1(2) . . ? C4 Cr1 P4 97.2(2) . . ? C3 Cr1 P4 117.3(2) . . ? C5 Cr1 P4 111.67(18) . . ? C1 Cr1 P4 148.21(19) . . ? P31 Cr1 P4 60.9(5) . . ? P11 Cr1 P4 86.6(6) . . ? P2 Cr1 P4 93.0(2) . . ? P21 Cr1 P4 95.6(4) . . ? P51 Cr1 P4 42.7(5) . . ? C2 Cr1 P42 163.3(2) . . ? C4 Cr1 P42 100.1(2) . . ? C3 Cr1 P42 127.8(3) . . ? C5 Cr1 P42 104.7(2) . . ? C1 Cr1 P42 137.2(3) . . ? P31 Cr1 P42 73.3(5) . . ? P11 Cr1 P42 75.8(5) . . ? P2 Cr1 P42 98.0(3) . . ? P21 Cr1 P42 97.6(4) . . ? P51 Cr1 P42 27.7(5) . . ? P4 Cr1 P42 15.6(3) . . ? P51 P11 P21 108.1(10) . . ? P51 P11 Cr1 64.9(6) . . ? P21 P11 Cr1 64.4(8) . . ? P51 P11 Cr2 63.7(6) . . ? P21 P11 Cr2 62.4(7) . . ? Cr1 P11 Cr2 82.7(7) . . ? P11 P21 P31 105.8(8) . . ? P11 P21 Cr2 64.5(6) . . ? P31 P21 Cr2 63.1(6) . . ? P11 P21 Cr1 62.6(6) . . ? P31 P21 Cr1 62.1(6) . . ? Cr2 P21 Cr1 82.8(4) . . ? P41 P31 P21 109.9(8) . . ? P41 P31 Cr1 66.6(7) . . ? P21 P31 Cr1 64.5(5) . . ? P41 P31 Cr2 64.7(7) . . ? P21 P31 Cr2 63.0(5) . . ? Cr1 P31 Cr2 83.8(4) . . ? P31 P41 P51 107.4(8) . . ? P31 P41 Cr2 63.9(6) . . ? P51 P41 Cr2 63.8(6) . . ? P31 P41 Cr1 62.5(6) . . ? P51 P41 Cr1 63.3(6) . . ? Cr2 P41 Cr1 81.7(5) . . ? P11 P51 P41 108.7(8) . . ? P11 P51 Cr2 64.5(8) . . ? P41 P51 Cr2 63.5(5) . . ? P11 P51 Cr1 63.0(8) . . ? P41 P51 Cr1 64.9(6) . . ? Cr2 P51 Cr1 82.2(3) . . ? P5 P1 P2 107.6(5) . . ? P5 P1 Cr2 63.6(3) . . ? P2 P1 Cr2 63.7(4) . . ? P5 P1 Cr1 63.6(3) . . ? P2 P1 Cr1 62.8(4) . . ? Cr2 P1 Cr1 81.5(3) . . ? P3 P2 P1 108.1(4) . . ? P3 P2 Cr1 64.4(3) . . ? P1 P2 Cr1 63.5(3) . . ? P3 P2 Cr2 63.5(4) . . ? P1 P2 Cr2 62.9(3) . . ? Cr1 P2 Cr2 81.4(2) . . ? P2 P3 P4 107.7(4) . . ? P2 P3 Cr2 63.8(3) . . ? P4 P3 Cr2 64.0(4) . . ? P2 P3 Cr1 62.7(3) . . ? P4 P3 Cr1 62.9(3) . . ? Cr2 P3 Cr1 80.8(3) . . ? P5 P4 P3 108.4(4) . . ? P5 P4 Cr1 63.8(3) . . ? P3 P4 Cr1 64.1(3) . . ? P5 P4 Cr2 63.2(4) . . ? P3 P4 Cr2 63.2(3) . . ? Cr1 P4 Cr2 81.0(2) . . ? P4 P5 P1 108.2(5) . . ? P4 P5 Cr2 64.3(3) . . ? P1 P5 Cr2 63.3(4) . . ? P4 P5 Cr1 63.3(2) . . ? P1 P5 Cr1 63.4(4) . . ? Cr2 P5 Cr1 81.3(2) . . ? P52 P12 P22 106.3(5) . . ? P52 P12 Cr1 63.0(3) . . ? P22 P12 Cr1 62.9(3) . . ? P52 P12 Cr2 62.9(3) . . ? P22 P12 Cr2 62.2(3) . . ? Cr1 P12 Cr2 80.6(3) . . ? P32 P22 P12 108.8(5) . . ? P32 P22 Cr2 64.3(3) . . ? P12 P22 Cr2 63.4(3) . . ? P32 P22 Cr1 64.4(4) . . ? P12 P22 Cr1 63.0(3) . . ? Cr2 P22 Cr1 81.1(2) . . ? P22 P32 P42 108.2(5) . . ? P22 P32 Cr2 63.6(3) . . ? P42 P32 Cr2 63.6(4) . . ? P22 P32 Cr1 63.9(3) . . ? P42 P32 Cr1 62.7(3) . . ? Cr2 P32 Cr1 80.6(3) . . ? P52 P42 P32 108.7(5) . . ? P52 P42 Cr1 63.8(3) . . ? P32 P42 Cr1 64.3(3) . . ? P52 P42 Cr2 63.4(3) . . ? P32 P42 Cr2 63.4(3) . . ? Cr1 P42 Cr2 81.2(2) . . ? P42 P52 P12 108.1(5) . . ? P42 P52 Cr2 63.7(3) . . ? P12 P52 Cr2 63.5(3) . . ? P42 P52 Cr1 63.2(3) . . ? P12 P52 Cr1 63.5(4) . . ? Cr2 P52 Cr1 81.0(3) . . ? C11 Cr2 C15 37.71(8) . . ? C11 Cr2 C14 62.85(8) . . ? C15 Cr2 C14 37.69(7) . . ? C11 Cr2 C13 62.74(8) . . ? C15 Cr2 C13 62.98(8) . . ? C14 Cr2 C13 37.63(8) . . ? C11 Cr2 C12 37.64(9) . . ? C15 Cr2 C12 63.16(8) . . ? C14 Cr2 C12 63.00(8) . . ? C13 Cr2 C12 37.58(9) . . ? C11 Cr2 P21 105.3(4) . . ? C15 Cr2 P21 138.7(4) . . ? C14 Cr2 P21 162.0(4) . . ? C13 Cr2 P21 125.9(4) . . ? C12 Cr2 P21 99.2(4) . . ? C11 Cr2 P31 141.3(5) . . ? C15 Cr2 P31 163.2(4) . . ? C14 Cr2 P31 126.3(4) . . ? C13 Cr2 P31 101.0(4) . . ? C12 Cr2 P31 107.8(4) . . ? P21 Cr2 P31 53.9(6) . . ? C11 Cr2 P41 161.8(4) . . ? C15 Cr2 P41 125.4(4) . . ? C14 Cr2 P41 99.3(4) . . ? C13 Cr2 P41 106.0(4) . . ? C12 Cr2 P41 139.5(4) . . ? P21 Cr2 P41 92.9(6) . . ? P31 Cr2 P41 51.4(6) . . ? C11 Cr2 P51 125.7(4) . . ? C15 Cr2 P51 99.3(3) . . ? C14 Cr2 P51 105.8(4) . . ? C13 Cr2 P51 139.4(5) . . ? C12 Cr2 P51 162.1(4) . . ? P21 Cr2 P51 92.1(5) . . ? P31 Cr2 P51 90.1(5) . . ? P41 Cr2 P51 52.7(5) . . ? C11 Cr2 P11 100.1(5) . . ? C15 Cr2 P11 105.6(6) . . ? C14 Cr2 P11 138.9(6) . . ? C13 Cr2 P11 162.6(4) . . ? C12 Cr2 P11 126.6(4) . . ? P21 Cr2 P11 53.1(6) . . ? P31 Cr2 P11 91.1(7) . . ? P41 Cr2 P11 91.3(6) . . ? P51 Cr2 P11 51.8(6) . . ? C11 Cr2 P22 120.2(3) . . ? C15 Cr2 P22 157.8(3) . . ? C14 Cr2 P22 144.8(3) . . ? C13 Cr2 P22 109.2(2) . . ? C12 Cr2 P22 97.58(18) . . ? P21 Cr2 P22 27.8(5) . . ? P31 Cr2 P22 28.0(6) . . ? P41 Cr2 P22 76.2(5) . . ? P51 Cr2 P22 98.9(4) . . ? P11 Cr2 P22 76.2(6) . . ? C11 Cr2 P1 97.1(2) . . ? C15 Cr2 P1 110.0(3) . . ? C14 Cr2 P1 146.3(3) . . ? C13 Cr2 P1 155.9(2) . . ? C12 Cr2 P1 118.3(2) . . ? P21 Cr2 P1 43.0(5) . . ? P31 Cr2 P1 86.6(5) . . ? P41 Cr2 P1 96.7(5) . . ? P51 Cr2 P1 62.4(5) . . ? P11 Cr2 P1 11.5(6) . . ? P22 Cr2 P1 68.0(4) . . ? C15 C11 C12 108.74(19) . . ? C15 C11 C16 125.6(2) . . ? C12 C11 C16 125.6(2) . . ? C15 C11 Cr2 71.37(12) . . ? C12 C11 Cr2 71.71(12) . . ? C16 C11 Cr2 125.33(15) . . ? C11 C12 C13 107.35(19) . . ? C11 C12 C17 126.3(2) . . ? C13 C12 C17 126.2(2) . . ? C11 C12 Cr2 70.64(12) . . ? C13 C12 Cr2 71.04(12) . . ? C17 C12 Cr2 126.70(17) . . ? C14 C13 C12 108.36(18) . . ? C14 C13 C18 125.0(2) . . ? C12 C13 C18 126.5(2) . . ? C14 C13 Cr2 71.14(11) . . ? C12 C13 Cr2 71.39(12) . . ? C18 C13 Cr2 126.19(16) . . ? C13 C14 C15 108.03(18) . . ? C13 C14 C19 125.0(2) . . ? C15 C14 C19 126.9(2) . . ? C13 C14 Cr2 71.23(12) . . ? C15 C14 Cr2 71.07(11) . . ? C19 C14 Cr2 126.02(16) . . ? C11 C15 C14 107.52(18) . . ? C11 C15 C20 126.1(2) . . ? C14 C15 C20 126.3(2) . . ? C11 C15 Cr2 70.92(12) . . ? C14 C15 Cr2 71.24(11) . . ? C20 C15 Cr2 125.58(15) . . ? C11 C16 H16A 109.5 . . ? C11 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C11 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 C1 C2 C3 -0.5(2) . . . . ? C6 C1 C2 C3 176.0(2) . . . . ? Cr1 C1 C2 C3 -62.21(15) . . . . ? C5 C1 C2 C7 -177.1(2) . . . . ? C6 C1 C2 C7 -0.7(4) . . . . ? Cr1 C1 C2 C7 121.2(2) . . . . ? C5 C1 C2 Cr1 61.74(14) . . . . ? C6 C1 C2 Cr1 -121.8(2) . . . . ? C1 C2 C3 C4 0.7(2) . . . . ? C7 C2 C3 C4 177.3(2) . . . . ? Cr1 C2 C3 C4 -61.77(15) . . . . ? C1 C2 C3 C8 -177.1(2) . . . . ? C7 C2 C3 C8 -0.5(4) . . . . ? Cr1 C2 C3 C8 120.5(2) . . . . ? C1 C2 C3 Cr1 62.43(14) . . . . ? C7 C2 C3 Cr1 -121.0(2) . . . . ? C2 C3 C4 C5 -0.6(2) . . . . ? C8 C3 C4 C5 177.2(2) . . . . ? Cr1 C3 C4 C5 -62.30(15) . . . . ? C2 C3 C4 C9 -176.6(2) . . . . ? C8 C3 C4 C9 1.2(4) . . . . ? Cr1 C3 C4 C9 121.7(3) . . . . ? C2 C3 C4 Cr1 61.70(15) . . . . ? C8 C3 C4 Cr1 -120.5(2) . . . . ? C3 C4 C5 C1 0.3(2) . . . . ? C9 C4 C5 C1 176.3(2) . . . . ? Cr1 C4 C5 C1 -61.94(15) . . . . ? C3 C4 C5 C10 -175.5(2) . . . . ? C9 C4 C5 C10 0.6(4) . . . . ? Cr1 C4 C5 C10 122.3(2) . . . . ? C3 C4 C5 Cr1 62.25(15) . . . . ? C9 C4 C5 Cr1 -121.7(3) . . . . ? C2 C1 C5 C4 0.1(2) . . . . ? C6 C1 C5 C4 -176.3(2) . . . . ? Cr1 C1 C5 C4 61.69(15) . . . . ? C2 C1 C5 C10 175.9(2) . . . . ? C6 C1 C5 C10 -0.6(4) . . . . ? Cr1 C1 C5 C10 -122.6(2) . . . . ? C2 C1 C5 Cr1 -61.58(14) . . . . ? C6 C1 C5 Cr1 122.0(2) . . . . ? C1 C2 Cr1 C4 -80.02(14) . . . . ? C3 C2 Cr1 C4 37.49(12) . . . . ? C7 C2 Cr1 C4 159.0(3) . . . . ? C1 C2 Cr1 C3 -117.51(18) . . . . ? C7 C2 Cr1 C3 121.5(3) . . . . ? C1 C2 Cr1 C5 -37.58(13) . . . . ? C3 C2 Cr1 C5 79.93(13) . . . . ? C7 C2 Cr1 C5 -158.6(3) . . . . ? C3 C2 Cr1 C1 117.51(18) . . . . ? C7 C2 Cr1 C1 -121.0(3) . . . . ? C1 C2 Cr1 P31 169.4(5) . . . . ? C3 C2 Cr1 P31 -73.1(5) . . . . ? C7 C2 Cr1 P31 48.4(6) . . . . ? C1 C2 Cr1 P11 63.5(7) . . . . ? C3 C2 Cr1 P11 -179.0(7) . . . . ? C7 C2 Cr1 P11 -57.5(7) . . . . ? C1 C2 Cr1 P2 127.2(3) . . . . ? C3 C2 Cr1 P2 -115.3(3) . . . . ? C7 C2 Cr1 P2 6.2(3) . . . . ? C1 C2 Cr1 P21 115.7(4) . . . . ? C3 C2 Cr1 P21 -126.8(4) . . . . ? C7 C2 Cr1 P21 -5.3(5) . . . . ? C1 C2 Cr1 P51 4.5(12) . . . . ? C3 C2 Cr1 P51 122.0(12) . . . . ? C7 C2 Cr1 P51 -116.5(12) . . . . ? C1 C2 Cr1 P4 -120.9(5) . . . . ? C3 C2 Cr1 P4 -3.4(5) . . . . ? C7 C2 Cr1 P4 118.1(5) . . . . ? C1 C2 Cr1 P42 -82.1(12) . . . . ? C3 C2 Cr1 P42 35.4(12) . . . . ? C7 C2 Cr1 P42 156.9(12) . . . . ? C5 C4 Cr1 C2 79.69(14) . . . . ? C3 C4 Cr1 C2 -37.62(13) . . . . ? C9 C4 Cr1 C2 -159.9(3) . . . . ? C5 C4 Cr1 C3 117.31(19) . . . . ? C9 C4 Cr1 C3 -122.3(3) . . . . ? C3 C4 Cr1 C5 -117.31(19) . . . . ? C9 C4 Cr1 C5 120.4(3) . . . . ? C5 C4 Cr1 C1 37.24(12) . . . . ? C3 C4 Cr1 C1 -80.07(14) . . . . ? C9 C4 Cr1 C1 157.6(3) . . . . ? C5 C4 Cr1 P31 -177.3(6) . . . . ? C3 C4 Cr1 P31 65.4(6) . . . . ? C9 C4 Cr1 P31 -56.9(6) . . . . ? C5 C4 Cr1 P11 -21.4(10) . . . . ? C3 C4 Cr1 P11 -138.7(10) . . . . ? C9 C4 Cr1 P11 99.0(10) . . . . ? C5 C4 Cr1 P2 136.5(4) . . . . ? C3 C4 Cr1 P2 19.2(5) . . . . ? C9 C4 Cr1 P2 -103.1(5) . . . . ? C5 C4 Cr1 P21 121.4(10) . . . . ? C3 C4 Cr1 P21 4.1(10) . . . . ? C9 C4 Cr1 P21 -118.3(10) . . . . ? C5 C4 Cr1 P51 -74.9(5) . . . . ? C3 C4 Cr1 P51 167.8(5) . . . . ? C9 C4 Cr1 P51 45.4(6) . . . . ? C5 C4 Cr1 P4 -116.4(3) . . . . ? C3 C4 Cr1 P4 126.3(3) . . . . ? C9 C4 Cr1 P4 4.0(3) . . . . ? C5 C4 Cr1 P42 -100.9(4) . . . . ? C3 C4 Cr1 P42 141.8(4) . . . . ? C9 C4 Cr1 P42 19.5(4) . . . . ? C4 C3 Cr1 C2 117.44(18) . . . . ? C8 C3 Cr1 C2 -121.5(3) . . . . ? C2 C3 Cr1 C4 -117.44(18) . . . . ? C8 C3 Cr1 C4 121.0(3) . . . . ? C4 C3 Cr1 C5 37.55(13) . . . . ? C2 C3 Cr1 C5 -79.89(13) . . . . ? C8 C3 Cr1 C5 158.6(3) . . . . ? C4 C3 Cr1 C1 80.01(14) . . . . ? C2 C3 Cr1 C1 -37.42(12) . . . . ? C8 C3 Cr1 C1 -159.0(3) . . . . ? C4 C3 Cr1 P31 -125.6(5) . . . . ? C2 C3 Cr1 P31 117.0(5) . . . . ? C8 C3 Cr1 P31 -4.5(6) . . . . ? C4 C3 Cr1 P11 119.5(15) . . . . ? C2 C3 Cr1 P11 2.1(15) . . . . ? C8 C3 Cr1 P11 -119.4(15) . . . . ? C4 C3 Cr1 P2 -169.0(3) . . . . ? C2 C3 Cr1 P2 73.5(3) . . . . ? C8 C3 Cr1 P2 -48.0(4) . . . . ? C4 C3 Cr1 P21 -178.1(5) . . . . ? C2 C3 Cr1 P21 64.4(5) . . . . ? C8 C3 Cr1 P21 -57.1(5) . . . . ? C4 C3 Cr1 P51 -22.1(8) . . . . ? C2 C3 Cr1 P51 -139.6(8) . . . . ? C8 C3 Cr1 P51 98.9(8) . . . . ? C4 C3 Cr1 P4 -64.2(2) . . . . ? C2 C3 Cr1 P4 178.4(2) . . . . ? C8 C3 Cr1 P4 56.9(3) . . . . ? C4 C3 Cr1 P42 -50.4(4) . . . . ? C2 C3 Cr1 P42 -167.8(4) . . . . ? C8 C3 Cr1 P42 70.6(4) . . . . ? C4 C5 Cr1 C2 -80.34(14) . . . . ? C1 C5 Cr1 C2 37.60(12) . . . . ? C10 C5 Cr1 C2 158.9(2) . . . . ? C1 C5 Cr1 C4 117.94(18) . . . . ? C10 C5 Cr1 C4 -120.8(3) . . . . ? C4 C5 Cr1 C3 -37.62(14) . . . . ? C1 C5 Cr1 C3 80.32(14) . . . . ? C10 C5 Cr1 C3 -158.4(2) . . . . ? C4 C5 Cr1 C1 -117.94(18) . . . . ? C10 C5 Cr1 C1 121.3(3) . . . . ? C4 C5 Cr1 P31 5.8(12) . . . . ? C1 C5 Cr1 P31 123.8(12) . . . . ? C10 C5 Cr1 P31 -115.0(12) . . . . ? C4 C5 Cr1 P11 167.9(6) . . . . ? C1 C5 Cr1 P11 -74.1(6) . . . . ? C10 C5 Cr1 P11 47.1(6) . . . . ? C4 C5 Cr1 P2 -118.3(5) . . . . ? C1 C5 Cr1 P2 -0.4(5) . . . . ? C10 C5 Cr1 P2 120.9(5) . . . . ? C4 C5 Cr1 P21 -138.7(6) . . . . ? C1 C5 Cr1 P21 -20.8(6) . . . . ? C10 C5 Cr1 P21 100.5(6) . . . . ? C4 C5 Cr1 P51 115.3(6) . . . . ? C1 C5 Cr1 P51 -126.7(6) . . . . ? C10 C5 Cr1 P51 -5.5(6) . . . . ? C4 C5 Cr1 P4 73.0(3) . . . . ? C1 C5 Cr1 P4 -169.1(3) . . . . ? C10 C5 Cr1 P4 -47.8(3) . . . . ? C4 C5 Cr1 P42 87.6(4) . . . . ? C1 C5 Cr1 P42 -154.4(4) . . . . ? C10 C5 Cr1 P42 -33.2(4) . . . . ? C5 C1 Cr1 C2 -117.29(18) . . . . ? C6 C1 Cr1 C2 120.9(3) . . . . ? C2 C1 Cr1 C4 80.08(14) . . . . ? C5 C1 Cr1 C4 -37.22(13) . . . . ? C6 C1 Cr1 C4 -159.1(2) . . . . ? C2 C1 Cr1 C3 37.59(13) . . . . ? C5 C1 Cr1 C3 -79.70(14) . . . . ? C6 C1 Cr1 C3 158.5(2) . . . . ? C2 C1 Cr1 C5 117.29(18) . . . . ? C6 C1 Cr1 C5 -121.8(3) . . . . ? C2 C1 Cr1 P31 -19.5(9) . . . . ? C5 C1 Cr1 P31 -136.8(9) . . . . ? C6 C1 Cr1 P31 101.3(9) . . . . ? C2 C1 Cr1 P11 -127.3(6) . . . . ? C5 C1 Cr1 P11 115.4(6) . . . . ? C6 C1 Cr1 P11 -6.5(6) . . . . ? C2 C1 Cr1 P2 -62.9(2) . . . . ? C5 C1 Cr1 P2 179.8(2) . . . . ? C6 C1 Cr1 P2 58.0(3) . . . . ? C2 C1 Cr1 P21 -74.3(4) . . . . ? C5 C1 Cr1 P21 168.5(4) . . . . ? C6 C1 Cr1 P21 46.6(4) . . . . ? C2 C1 Cr1 P51 -178.0(6) . . . . ? C5 C1 Cr1 P51 64.8(6) . . . . ? C6 C1 Cr1 P51 -57.1(6) . . . . ? C2 C1 Cr1 P4 136.8(5) . . . . ? C5 C1 Cr1 P4 19.5(5) . . . . ? C6 C1 Cr1 P4 -102.4(5) . . . . ? C2 C1 Cr1 P42 155.2(5) . . . . ? C5 C1 Cr1 P42 37.9(5) . . . . ? C6 C1 Cr1 P42 -83.9(5) . . . . ? C2 Cr1 P11 P51 -154.4(5) . . . . ? C4 Cr1 P11 P51 -70.6(11) . . . . ? C3 Cr1 P11 P51 -155.8(11) . . . . ? C5 Cr1 P11 P51 -84.5(6) . . . . ? C1 Cr1 P11 P51 -120.9(6) . . . . ? P31 Cr1 P11 P51 88.1(8) . . . . ? P2 Cr1 P11 P51 122.5(8) . . . . ? P21 Cr1 P11 P51 127.2(9) . . . . ? P4 Cr1 P11 P51 27.5(6) . . . . ? P42 Cr1 P11 P51 16.0(5) . . . . ? C2 Cr1 P11 P21 78.5(7) . . . . ? C4 Cr1 P11 P21 162.2(6) . . . . ? C3 Cr1 P11 P21 77.0(15) . . . . ? C5 Cr1 P11 P21 148.3(5) . . . . ? C1 Cr1 P11 P21 112.0(6) . . . . ? P31 Cr1 P11 P21 -39.0(7) . . . . ? P2 Cr1 P11 P21 -4.6(6) . . . . ? P51 Cr1 P11 P21 -127.2(9) . . . . ? P4 Cr1 P11 P21 -99.7(6) . . . . ? P42 Cr1 P11 P21 -111.2(6) . . . . ? C2 Cr1 P11 Cr2 141.3(3) . . . . ? C4 Cr1 P11 Cr2 -135.0(6) . . . . ? C3 Cr1 P11 Cr2 139.8(10) . . . . ? C5 Cr1 P11 Cr2 -148.8(3) . . . . ? C1 Cr1 P11 Cr2 174.8(4) . . . . ? P31 Cr1 P11 Cr2 23.8(7) . . . . ? P2 Cr1 P11 Cr2 58.2(5) . . . . ? P21 Cr1 P11 Cr2 62.8(6) . . . . ? P51 Cr1 P11 Cr2 -64.3(6) . . . . ? P4 Cr1 P11 Cr2 -36.9(4) . . . . ? P42 Cr1 P11 Cr2 -48.3(4) . . . . ? P51 P11 P21 P31 -3.4(13) . . . . ? Cr1 P11 P21 P31 46.1(8) . . . . ? Cr2 P11 P21 P31 -49.1(7) . . . . ? P51 P11 P21 Cr2 45.8(9) . . . . ? Cr1 P11 P21 Cr2 95.2(5) . . . . ? P51 P11 P21 Cr1 -49.4(8) . . . . ? Cr2 P11 P21 Cr1 -95.2(5) . . . . ? C2 Cr1 P21 P11 -119.3(7) . . . . ? C4 Cr1 P21 P11 -156.1(10) . . . . ? C3 Cr1 P21 P11 -153.3(7) . . . . ? C5 Cr1 P21 P11 -69.3(8) . . . . ? C1 Cr1 P21 P11 -82.8(7) . . . . ? P31 Cr1 P21 P11 128.4(9) . . . . ? P2 Cr1 P21 P11 159(2) . . . . ? P51 Cr1 P21 P11 38.9(8) . . . . ? P4 Cr1 P21 P11 81.4(7) . . . . ? P42 Cr1 P21 P11 65.8(7) . . . . ? C2 Cr1 P21 P31 112.4(6) . . . . ? C4 Cr1 P21 P31 75.5(11) . . . . ? C3 Cr1 P21 P31 78.4(6) . . . . ? C5 Cr1 P21 P31 162.4(7) . . . . ? C1 Cr1 P21 P31 148.8(6) . . . . ? P11 Cr1 P21 P31 -128.4(9) . . . . ? P2 Cr1 P21 P31 30(2) . . . . ? P51 Cr1 P21 P31 -89.4(7) . . . . ? P4 Cr1 P21 P31 -47.0(6) . . . . ? P42 Cr1 P21 P31 -62.5(7) . . . . ? C2 Cr1 P21 Cr2 175.7(3) . . . . ? C4 Cr1 P21 Cr2 138.9(6) . . . . ? C3 Cr1 P21 Cr2 141.7(2) . . . . ? C5 Cr1 P21 Cr2 -134.2(3) . . . . ? C1 Cr1 P21 Cr2 -147.8(3) . . . . ? P31 Cr1 P21 Cr2 63.4(6) . . . . ? P11 Cr1 P21 Cr2 -65.0(7) . . . . ? P2 Cr1 P21 Cr2 94(2) . . . . ? P51 Cr1 P21 Cr2 -26.1(6) . . . . ? P4 Cr1 P21 Cr2 16.4(4) . . . . ? P42 Cr1 P21 Cr2 0.8(4) . . . . ? P11 P21 P31 P41 3.9(13) . . . . ? Cr2 P21 P31 P41 -46.0(8) . . . . ? Cr1 P21 P31 P41 50.2(8) . . . . ? P11 P21 P31 Cr1 -46.3(8) . . . . ? Cr2 P21 P31 Cr1 -96.3(5) . . . . ? P11 P21 P31 Cr2 49.9(8) . . . . ? Cr1 P21 P31 Cr2 96.3(5) . . . . ? C2 Cr1 P31 P41 148.7(6) . . . . ? C4 Cr1 P31 P41 78.1(7) . . . . ? C3 Cr1 P31 P41 112.3(6) . . . . ? C5 Cr1 P31 P41 74.1(13) . . . . ? C1 Cr1 P31 P41 161.5(7) . . . . ? P11 Cr1 P31 P41 -89.3(8) . . . . ? P2 Cr1 P31 P41 -136.4(9) . . . . ? P21 Cr1 P31 P41 -128.1(8) . . . . ? P51 Cr1 P31 P41 -37.3(7) . . . . ? P4 Cr1 P31 P41 -4.5(8) . . . . ? P42 Cr1 P31 P41 -14.8(6) . . . . ? C2 Cr1 P31 P21 -83.2(5) . . . . ? C4 Cr1 P31 P21 -153.8(4) . . . . ? C3 Cr1 P31 P21 -119.6(4) . . . . ? C5 Cr1 P31 P21 -157.8(9) . . . . ? C1 Cr1 P31 P21 -70.4(9) . . . . ? P11 Cr1 P31 P21 38.8(6) . . . . ? P2 Cr1 P31 P21 -8.4(5) . . . . ? P51 Cr1 P31 P21 90.8(7) . . . . ? P4 Cr1 P31 P21 123.6(6) . . . . ? P42 Cr1 P31 P21 113.3(5) . . . . ? C2 Cr1 P31 Cr2 -146.2(3) . . . . ? C4 Cr1 P31 Cr2 143.2(3) . . . . ? C3 Cr1 P31 Cr2 177.4(4) . . . . ? C5 Cr1 P31 Cr2 139.2(8) . . . . ? C1 Cr1 P31 Cr2 -133.4(5) . . . . ? P11 Cr1 P31 Cr2 -24.2(7) . . . . ? P2 Cr1 P31 Cr2 -71.3(5) . . . . ? P21 Cr1 P31 Cr2 -63.0(5) . . . . ? P51 Cr1 P31 Cr2 27.8(7) . . . . ? P4 Cr1 P31 Cr2 60.6(5) . . . . ? P42 Cr1 P31 Cr2 50.3(5) . . . . ? P21 P31 P41 P51 -2.9(12) . . . . ? Cr1 P31 P41 P51 46.2(8) . . . . ? Cr2 P31 P41 P51 -48.1(7) . . . . ? P21 P31 P41 Cr2 45.2(8) . . . . ? Cr1 P31 P41 Cr2 94.3(5) . . . . ? P21 P31 P41 Cr1 -49.1(7) . . . . ? Cr2 P31 P41 Cr1 -94.3(5) . . . . ? C2 Cr1 P41 P31 -67.7(8) . . . . ? C4 Cr1 P41 P31 -118.8(6) . . . . ? C3 Cr1 P41 P31 -82.1(6) . . . . ? C5 Cr1 P41 P31 -152.6(5) . . . . ? C1 Cr1 P41 P31 -156.0(9) . . . . ? P11 Cr1 P41 P31 92.2(8) . . . . ? P2 Cr1 P41 P31 28.5(6) . . . . ? P21 Cr1 P41 P31 39.2(6) . . . . ? P51 Cr1 P41 P31 129.6(8) . . . . ? P4 Cr1 P41 P31 159(3) . . . . ? P42 Cr1 P41 P31 146.0(13) . . . . ? C2 Cr1 P41 P51 162.7(6) . . . . ? C4 Cr1 P41 P51 111.6(6) . . . . ? C3 Cr1 P41 P51 148.3(5) . . . . ? C5 Cr1 P41 P51 77.8(6) . . . . ? C1 Cr1 P41 P51 74.3(12) . . . . ? P31 Cr1 P41 P51 -129.6(8) . . . . ? P11 Cr1 P41 P51 -37.4(8) . . . . ? P2 Cr1 P41 P51 -101.1(6) . . . . ? P21 Cr1 P41 P51 -90.4(6) . . . . ? P4 Cr1 P41 P51 29(3) . . . . ? P42 Cr1 P41 P51 16.4(10) . . . . ? C2 Cr1 P41 Cr2 -132.5(4) . . . . ? C4 Cr1 P41 Cr2 176.5(3) . . . . ? C3 Cr1 P41 Cr2 -146.9(3) . . . . ? C5 Cr1 P41 Cr2 142.6(2) . . . . ? C1 Cr1 P41 Cr2 139.2(8) . . . . ? P31 Cr1 P41 Cr2 -64.8(6) . . . . ? P11 Cr1 P41 Cr2 27.4(6) . . . . ? P2 Cr1 P41 Cr2 -36.2(3) . . . . ? P21 Cr1 P41 Cr2 -25.6(5) . . . . ? P51 Cr1 P41 Cr2 64.8(6) . . . . ? P4 Cr1 P41 Cr2 94(3) . . . . ? P42 Cr1 P41 Cr2 81.2(11) . . . . ? P21 P11 P51 P41 1.7(14) . . . . ? Cr1 P11 P51 P41 -47.5(8) . . . . ? Cr2 P11 P51 P41 46.8(8) . . . . ? P21 P11 P51 Cr2 -45.1(8) . . . . ? Cr1 P11 P51 Cr2 -94.3(6) . . . . ? P21 P11 P51 Cr1 49.2(8) . . . . ? Cr2 P11 P51 Cr1 94.3(6) . . . . ? P31 P41 P51 P11 0.8(13) . . . . ? Cr2 P41 P51 P11 -47.3(9) . . . . ? Cr1 P41 P51 P11 46.5(8) . . . . ? P31 P41 P51 Cr2 48.1(7) . . . . ? Cr1 P41 P51 Cr2 93.8(4) . . . . ? P31 P41 P51 Cr1 -45.7(8) . . . . ? Cr2 P41 P51 Cr1 -93.8(4) . . . . ? C2 Cr1 P51 P11 73.2(13) . . . . ? C4 Cr1 P51 P11 147.0(8) . . . . ? C3 Cr1 P51 P11 161.4(9) . . . . ? C5 Cr1 P51 P11 110.3(8) . . . . ? C1 Cr1 P51 P11 76.3(8) . . . . ? P31 Cr1 P51 P11 -92.9(9) . . . . ? P2 Cr1 P51 P11 -49.6(8) . . . . ? P21 Cr1 P51 P11 -39.5(8) . . . . ? P4 Cr1 P51 P11 -137.2(9) . . . . ? P42 Cr1 P51 P11 -145.0(12) . . . . ? C2 Cr1 P51 P41 -157.2(9) . . . . ? C4 Cr1 P51 P41 -83.4(5) . . . . ? C3 Cr1 P51 P41 -69.0(8) . . . . ? C5 Cr1 P51 P41 -120.1(5) . . . . ? C1 Cr1 P51 P41 -154.1(4) . . . . ? P31 Cr1 P51 P41 36.7(7) . . . . ? P11 Cr1 P51 P41 129.6(9) . . . . ? P2 Cr1 P51 P41 80.0(6) . . . . ? P21 Cr1 P51 P41 90.1(6) . . . . ? P4 Cr1 P51 P41 -7.6(6) . . . . ? P42 Cr1 P51 P41 -15.4(8) . . . . ? C2 Cr1 P51 Cr2 138.5(8) . . . . ? C4 Cr1 P51 Cr2 -147.7(3) . . . . ? C3 Cr1 P51 Cr2 -133.3(4) . . . . ? C5 Cr1 P51 Cr2 175.6(4) . . . . ? C1 Cr1 P51 Cr2 141.6(3) . . . . ? P31 Cr1 P51 Cr2 -27.6(6) . . . . ? P11 Cr1 P51 Cr2 65.3(8) . . . . ? P2 Cr1 P51 Cr2 15.7(5) . . . . ? P21 Cr1 P51 Cr2 25.8(6) . . . . ? P4 Cr1 P51 Cr2 -71.9(5) . . . . ? P42 Cr1 P51 Cr2 -79.7(8) . . . . ? C2 Cr1 P1 P5 -148.4(3) . . . . ? C4 Cr1 P1 P5 -76.3(6) . . . . ? C3 Cr1 P1 P5 -161.4(3) . . . . ? C5 Cr1 P1 P5 -78.6(3) . . . . ? C1 Cr1 P1 P5 -112.1(3) . . . . ? P31 Cr1 P1 P5 98.3(6) . . . . ? P11 Cr1 P1 P5 -20(4) . . . . ? P2 Cr1 P1 P5 129.4(4) . . . . ? P21 Cr1 P1 P5 133.1(7) . . . . ? P51 Cr1 P1 P5 6.7(6) . . . . ? P4 Cr1 P1 P5 37.7(3) . . . . ? P42 Cr1 P1 P5 24.8(3) . . . . ? C2 Cr1 P1 P2 82.2(3) . . . . ? C4 Cr1 P1 P2 154.3(5) . . . . ? C3 Cr1 P1 P2 69.2(6) . . . . ? C5 Cr1 P1 P2 152.0(3) . . . . ? C1 Cr1 P1 P2 118.5(3) . . . . ? P31 Cr1 P1 P2 -31.1(6) . . . . ? P11 Cr1 P1 P2 -149(4) . . . . ? P21 Cr1 P1 P2 3.7(7) . . . . ? P51 Cr1 P1 P2 -122.7(6) . . . . ? P4 Cr1 P1 P2 -91.7(3) . . . . ? P42 Cr1 P1 P2 -104.6(4) . . . . ? C2 Cr1 P1 Cr2 146.96(16) . . . . ? C4 Cr1 P1 Cr2 -141.0(4) . . . . ? C3 Cr1 P1 Cr2 133.9(3) . . . . ? C5 Cr1 P1 Cr2 -143.26(16) . . . . ? C1 Cr1 P1 Cr2 -176.8(2) . . . . ? P31 Cr1 P1 Cr2 33.7(5) . . . . ? P11 Cr1 P1 Cr2 -85(4) . . . . ? P2 Cr1 P1 Cr2 64.8(3) . . . . ? P21 Cr1 P1 Cr2 68.4(6) . . . . ? P51 Cr1 P1 Cr2 -57.9(4) . . . . ? P4 Cr1 P1 Cr2 -27.0(3) . . . . ? P42 Cr1 P1 Cr2 -39.9(3) . . . . ? P5 P1 P2 P3 1.3(7) . . . . ? Cr2 P1 P2 P3 -46.0(4) . . . . ? Cr1 P1 P2 P3 47.9(4) . . . . ? P5 P1 P2 Cr1 -46.5(4) . . . . ? Cr2 P1 P2 Cr1 -93.9(2) . . . . ? P5 P1 P2 Cr2 47.4(4) . . . . ? Cr1 P1 P2 Cr2 93.9(2) . . . . ? C2 Cr1 P2 P3 119.6(4) . . . . ? C4 Cr1 P2 P3 70.8(5) . . . . ? C3 Cr1 P2 P3 83.2(4) . . . . ? C5 Cr1 P2 P3 153.1(4) . . . . ? C1 Cr1 P2 P3 152.8(3) . . . . ? P31 Cr1 P2 P3 3.1(9) . . . . ? P11 Cr1 P2 P3 -122.1(7) . . . . ? P21 Cr1 P2 P3 -141(2) . . . . ? P51 Cr1 P2 P3 -80.1(6) . . . . ? P4 Cr1 P2 P3 -37.4(4) . . . . ? P42 Cr1 P2 P3 -52.3(4) . . . . ? C2 Cr1 P2 P1 -111.9(3) . . . . ? C4 Cr1 P2 P1 -160.6(3) . . . . ? C3 Cr1 P2 P1 -148.2(3) . . . . ? C5 Cr1 P2 P1 -78.4(4) . . . . ? C1 Cr1 P2 P1 -78.6(3) . . . . ? P31 Cr1 P2 P1 131.7(7) . . . . ? P11 Cr1 P2 P1 6.5(8) . . . . ? P21 Cr1 P2 P1 -12(2) . . . . ? P51 Cr1 P2 P1 48.5(6) . . . . ? P4 Cr1 P2 P1 91.1(4) . . . . ? P42 Cr1 P2 P1 76.3(4) . . . . ? C2 Cr1 P2 Cr2 -175.78(18) . . . . ? C4 Cr1 P2 Cr2 135.5(2) . . . . ? C3 Cr1 P2 Cr2 147.90(14) . . . . ? C5 Cr1 P2 Cr2 -142.3(3) . . . . ? C1 Cr1 P2 Cr2 -142.56(14) . . . . ? P31 Cr1 P2 Cr2 67.8(7) . . . . ? P11 Cr1 P2 Cr2 -57.5(6) . . . . ? P21 Cr1 P2 Cr2 -76(2) . . . . ? P51 Cr1 P2 Cr2 -15.5(5) . . . . ? P4 Cr1 P2 Cr2 27.2(3) . . . . ? P42 Cr1 P2 Cr2 12.4(3) . . . . ? P1 P2 P3 P4 -2.2(7) . . . . ? Cr1 P2 P3 P4 45.2(4) . . . . ? Cr2 P2 P3 P4 -47.9(4) . . . . ? P1 P2 P3 Cr2 45.7(4) . . . . ? Cr1 P2 P3 Cr2 93.1(2) . . . . ? P1 P2 P3 Cr1 -47.4(4) . . . . ? Cr2 P2 P3 Cr1 -93.1(2) . . . . ? C2 Cr1 P3 P2 -76.7(3) . . . . ? C4 Cr1 P3 P2 -146.6(2) . . . . ? C3 Cr1 P3 P2 -110.4(3) . . . . ? C5 Cr1 P3 P2 -158.8(3) . . . . ? C1 Cr1 P3 P2 -74.7(6) . . . . ? P31 Cr1 P3 P2 -13(4) . . . . ? P11 Cr1 P3 P2 49.9(6) . . . . ? P21 Cr1 P3 P2 8.1(4) . . . . ? P51 Cr1 P3 P2 100.9(5) . . . . ? P4 Cr1 P3 P2 130.5(5) . . . . ? P42 Cr1 P3 P2 121.3(4) . . . . ? C2 Cr1 P3 P4 152.7(3) . . . . ? C4 Cr1 P3 P4 82.8(4) . . . . ? C3 Cr1 P3 P4 119.0(3) . . . . ? C5 Cr1 P3 P4 70.7(6) . . . . ? C1 Cr1 P3 P4 154.7(5) . . . . ? P31 Cr1 P3 P4 -144(4) . . . . ? P11 Cr1 P3 P4 -80.6(6) . . . . ? P2 Cr1 P3 P4 -130.5(5) . . . . ? P21 Cr1 P3 P4 -122.4(5) . . . . ? P51 Cr1 P3 P4 -29.6(6) . . . . ? P42 Cr1 P3 P4 -9.2(4) . . . . ? C2 Cr1 P3 Cr2 -141.86(18) . . . . ? C4 Cr1 P3 Cr2 148.24(17) . . . . ? C3 Cr1 P3 Cr2 -175.6(2) . . . . ? C5 Cr1 P3 Cr2 136.1(3) . . . . ? C1 Cr1 P3 Cr2 -139.9(4) . . . . ? P31 Cr1 P3 Cr2 -78(4) . . . . ? P11 Cr1 P3 Cr2 -15.2(5) . . . . ? P2 Cr1 P3 Cr2 -65.1(3) . . . . ? P21 Cr1 P3 Cr2 -57.0(3) . . . . ? P51 Cr1 P3 Cr2 35.8(5) . . . . ? P4 Cr1 P3 Cr2 65.4(4) . . . . ? P42 Cr1 P3 Cr2 56.2(3) . . . . ? P2 P3 P4 P5 2.2(7) . . . . ? Cr2 P3 P4 P5 -45.6(4) . . . . ? Cr1 P3 P4 P5 47.3(4) . . . . ? P2 P3 P4 Cr1 -45.1(4) . . . . ? Cr2 P3 P4 Cr1 -92.9(2) . . . . ? P2 P3 P4 Cr2 47.8(4) . . . . ? Cr1 P3 P4 Cr2 92.9(2) . . . . ? C2 Cr1 P4 P5 155.8(4) . . . . ? C4 Cr1 P4 P5 119.7(3) . . . . ? C3 Cr1 P4 P5 153.4(3) . . . . ? C5 Cr1 P4 P5 83.7(4) . . . . ? C1 Cr1 P4 P5 71.0(5) . . . . ? P31 Cr1 P4 P5 -122.5(6) . . . . ? P11 Cr1 P4 P5 -28.1(6) . . . . ? P2 Cr1 P4 P5 -91.6(3) . . . . ? P21 Cr1 P4 P5 -80.3(5) . . . . ? P51 Cr1 P4 P5 4.4(8) . . . . ? P42 Cr1 P4 P5 17.9(10) . . . . ? C2 Cr1 P4 P3 -75.3(5) . . . . ? C4 Cr1 P4 P3 -111.3(3) . . . . ? C3 Cr1 P4 P3 -77.6(3) . . . . ? C5 Cr1 P4 P3 -147.4(3) . . . . ? C1 Cr1 P4 P3 -160.0(4) . . . . ? P31 Cr1 P4 P3 6.4(7) . . . . ? P11 Cr1 P4 P3 100.9(6) . . . . ? P2 Cr1 P4 P3 37.4(3) . . . . ? P21 Cr1 P4 P3 48.6(5) . . . . ? P51 Cr1 P4 P3 133.3(7) . . . . ? P42 Cr1 P4 P3 146.8(12) . . . . ? C2 Cr1 P4 Cr2 -139.8(3) . . . . ? C4 Cr1 P4 Cr2 -175.83(17) . . . . ? C3 Cr1 P4 Cr2 -142.12(14) . . . . ? C5 Cr1 P4 Cr2 148.11(13) . . . . ? C1 Cr1 P4 Cr2 135.4(3) . . . . ? P31 Cr1 P4 Cr2 -58.1(5) . . . . ? P11 Cr1 P4 Cr2 36.4(6) . . . . ? P2 Cr1 P4 Cr2 -27.1(2) . . . . ? P21 Cr1 P4 Cr2 -15.9(4) . . . . ? P51 Cr1 P4 Cr2 68.8(6) . . . . ? P42 Cr1 P4 Cr2 82.3(11) . . . . ? P3 P4 P5 P1 -1.4(7) . . . . ? Cr1 P4 P5 P1 46.1(4) . . . . ? Cr2 P4 P5 P1 -47.0(4) . . . . ? P3 P4 P5 Cr2 45.6(4) . . . . ? Cr1 P4 P5 Cr2 93.1(2) . . . . ? P3 P4 P5 Cr1 -47.5(4) . . . . ? Cr2 P4 P5 Cr1 -93.1(2) . . . . ? P2 P1 P5 P4 0.1(7) . . . . ? Cr2 P1 P5 P4 47.5(4) . . . . ? Cr1 P1 P5 P4 -46.0(4) . . . . ? P2 P1 P5 Cr2 -47.4(4) . . . . ? Cr1 P1 P5 Cr2 -93.5(3) . . . . ? P2 P1 P5 Cr1 46.1(4) . . . . ? Cr2 P1 P5 Cr1 93.5(3) . . . . ? C2 Cr1 P5 P4 -160.7(3) . . . . ? C4 Cr1 P5 P4 -77.2(3) . . . . ? C3 Cr1 P5 P4 -74.1(5) . . . . ? C5 Cr1 P5 P4 -111.1(3) . . . . ? C1 Cr1 P5 P4 -147.5(2) . . . . ? P31 Cr1 P5 P4 47.6(6) . . . . ? P11 Cr1 P5 P4 135.8(9) . . . . ? P2 Cr1 P5 P4 91.5(3) . . . . ? P21 Cr1 P5 P4 100.3(5) . . . . ? P51 Cr1 P5 P4 -16(3) . . . . ? P42 Cr1 P5 P4 -7.6(3) . . . . ? C2 Cr1 P5 P1 69.3(6) . . . . ? C4 Cr1 P5 P1 152.8(3) . . . . ? C3 Cr1 P5 P1 155.9(5) . . . . ? C5 Cr1 P5 P1 118.9(4) . . . . ? C1 Cr1 P5 P1 82.5(4) . . . . ? P31 Cr1 P5 P1 -82.4(6) . . . . ? P11 Cr1 P5 P1 5.8(11) . . . . ? P2 Cr1 P5 P1 -38.6(4) . . . . ? P21 Cr1 P5 P1 -29.7(5) . . . . ? P51 Cr1 P5 P1 -146(3) . . . . ? P4 Cr1 P5 P1 -130.0(5) . . . . ? P42 Cr1 P5 P1 -137.7(6) . . . . ? C2 Cr1 P5 Cr2 133.8(3) . . . . ? C4 Cr1 P5 Cr2 -142.70(16) . . . . ? C3 Cr1 P5 Cr2 -139.6(4) . . . . ? C5 Cr1 P5 Cr2 -176.6(2) . . . . ? C1 Cr1 P5 Cr2 146.99(15) . . . . ? P31 Cr1 P5 Cr2 -17.9(5) . . . . ? P11 Cr1 P5 Cr2 70.3(9) . . . . ? P2 Cr1 P5 Cr2 25.9(3) . . . . ? P21 Cr1 P5 Cr2 34.8(4) . . . . ? P51 Cr1 P5 Cr2 -82(3) . . . . ? P4 Cr1 P5 Cr2 -65.5(3) . . . . ? P42 Cr1 P5 Cr2 -73.2(4) . . . . ? C2 Cr1 P12 P52 -139.3(4) . . . . ? C4 Cr1 P12 P52 -101.7(10) . . . . ? C3 Cr1 P12 P52 -161.9(3) . . . . ? C5 Cr1 P12 P52 -73.3(4) . . . . ? C1 Cr1 P12 P52 -101.0(4) . . . . ? P31 Cr1 P12 P52 109.9(6) . . . . ? P11 Cr1 P12 P52 -12.6(14) . . . . ? P2 Cr1 P12 P52 136.9(5) . . . . ? P21 Cr1 P12 P52 138.5(9) . . . . ? P51 Cr1 P12 P52 16.5(6) . . . . ? P4 Cr1 P12 P52 52.6(4) . . . . ? P42 Cr1 P12 P52 37.9(4) . . . . ? C2 Cr1 P12 P22 92.8(3) . . . . ? C4 Cr1 P12 P22 130.5(9) . . . . ? C3 Cr1 P12 P22 70.3(4) . . . . ? C5 Cr1 P12 P22 158.8(3) . . . . ? C1 Cr1 P12 P22 131.1(3) . . . . ? P31 Cr1 P12 P22 -17.9(6) . . . . ? P11 Cr1 P12 P22 -140.4(16) . . . . ? P2 Cr1 P12 P22 9.0(4) . . . . ? P21 Cr1 P12 P22 10.7(8) . . . . ? P51 Cr1 P12 P22 -111.3(5) . . . . ? P4 Cr1 P12 P22 -75.3(4) . . . . ? P42 Cr1 P12 P22 -90.0(4) . . . . ? C2 Cr1 P12 Cr2 156.4(2) . . . . ? C4 Cr1 P12 Cr2 -166.0(8) . . . . ? C3 Cr1 P12 Cr2 133.80(17) . . . . ? C5 Cr1 P12 Cr2 -137.66(16) . . . . ? C1 Cr1 P12 Cr2 -165.4(3) . . . . ? P31 Cr1 P12 Cr2 45.6(5) . . . . ? P11 Cr1 P12 Cr2 -76.9(14) . . . . ? P2 Cr1 P12 Cr2 72.5(4) . . . . ? P21 Cr1 P12 Cr2 74.2(8) . . . . ? P51 Cr1 P12 Cr2 -47.8(4) . . . . ? P4 Cr1 P12 Cr2 -11.7(3) . . . . ? P42 Cr1 P12 Cr2 -26.4(3) . . . . ? P52 P12 P22 P32 -0.4(6) . . . . ? Cr1 P12 P22 P32 46.7(4) . . . . ? Cr2 P12 P22 P32 -46.8(4) . . . . ? P52 P12 P22 Cr2 46.4(4) . . . . ? Cr1 P12 P22 Cr2 93.5(2) . . . . ? P52 P12 P22 Cr1 -47.1(4) . . . . ? Cr2 P12 P22 Cr1 -93.5(2) . . . . ? C2 Cr1 P22 P32 130.4(4) . . . . ? C4 Cr1 P22 P32 68.8(4) . . . . ? C3 Cr1 P22 P32 91.9(4) . . . . ? C5 Cr1 P22 P32 127.3(10) . . . . ? C1 Cr1 P22 P32 158.1(3) . . . . ? P31 Cr1 P22 P32 9.9(10) . . . . ? P11 Cr1 P22 P32 -112.7(6) . . . . ? P2 Cr1 P22 P32 -150.5(10) . . . . ? P21 Cr1 P22 P32 -140.9(9) . . . . ? P51 Cr1 P22 P32 -64.9(6) . . . . ? P4 Cr1 P22 P32 -24.6(4) . . . . ? P42 Cr1 P22 P32 -37.7(4) . . . . ? C2 Cr1 P22 P12 -99.3(3) . . . . ? C4 Cr1 P22 P12 -161.0(3) . . . . ? C3 Cr1 P22 P12 -137.9(3) . . . . ? C5 Cr1 P22 P12 -102.4(10) . . . . ? C1 Cr1 P22 P12 -71.6(3) . . . . ? P31 Cr1 P22 P12 140.1(11) . . . . ? P11 Cr1 P22 P12 17.5(7) . . . . ? P2 Cr1 P22 P12 -20.3(8) . . . . ? P21 Cr1 P22 P12 -10.7(7) . . . . ? P51 Cr1 P22 P12 65.4(6) . . . . ? P4 Cr1 P22 P12 105.6(4) . . . . ? P42 Cr1 P22 P12 92.5(4) . . . . ? C2 Cr1 P22 Cr2 -163.9(3) . . . . ? C4 Cr1 P22 Cr2 134.46(17) . . . . ? C3 Cr1 P22 Cr2 157.5(3) . . . . ? C5 Cr1 P22 Cr2 -167.0(9) . . . . ? C1 Cr1 P22 Cr2 -136.22(17) . . . . ? P31 Cr1 P22 Cr2 75.5(10) . . . . ? P11 Cr1 P22 Cr2 -47.1(5) . . . . ? P2 Cr1 P22 Cr2 -84.9(9) . . . . ? P21 Cr1 P22 Cr2 -75.3(8) . . . . ? P51 Cr1 P22 Cr2 0.8(5) . . . . ? P4 Cr1 P22 Cr2 41.0(3) . . . . ? P42 Cr1 P22 Cr2 27.9(3) . . . . ? P12 P22 P32 P42 -0.3(6) . . . . ? Cr2 P22 P32 P42 -46.6(4) . . . . ? Cr1 P22 P32 P42 45.7(4) . . . . ? P12 P22 P32 Cr2 46.4(4) . . . . ? Cr1 P22 P32 Cr2 92.3(2) . . . . ? P12 P22 P32 Cr1 -46.0(4) . . . . ? Cr2 P22 P32 Cr1 -92.3(2) . . . . ? C2 Cr1 P32 P22 -70.9(4) . . . . ? C4 Cr1 P32 P22 -137.8(3) . . . . ? C3 Cr1 P32 P22 -99.5(4) . . . . ? C5 Cr1 P32 P22 -160.0(3) . . . . ? C1 Cr1 P32 P22 -97.2(9) . . . . ? P31 Cr1 P32 P22 -11.2(11) . . . . ? P11 Cr1 P32 P22 65.1(6) . . . . ? P2 Cr1 P32 P22 8.8(3) . . . . ? P21 Cr1 P32 P22 17.6(5) . . . . ? P51 Cr1 P32 P22 112.3(6) . . . . ? P4 Cr1 P32 P22 138.5(6) . . . . ? P42 Cr1 P32 P22 130.1(5) . . . . ? C2 Cr1 P32 P42 159.0(3) . . . . ? C4 Cr1 P32 P42 92.1(4) . . . . ? C3 Cr1 P32 P42 130.4(4) . . . . ? C5 Cr1 P32 P42 69.9(4) . . . . ? C1 Cr1 P32 P42 132.7(9) . . . . ? P31 Cr1 P32 P42 -141.3(12) . . . . ? P11 Cr1 P32 P42 -65.0(6) . . . . ? P2 Cr1 P32 P42 -121.3(4) . . . . ? P21 Cr1 P32 P42 -112.5(4) . . . . ? P51 Cr1 P32 P42 -17.8(5) . . . . ? P4 Cr1 P32 P42 8.4(5) . . . . ? C2 Cr1 P32 Cr2 -136.02(17) . . . . ? C4 Cr1 P32 Cr2 157.1(2) . . . . ? C3 Cr1 P32 Cr2 -164.6(2) . . . . ? C5 Cr1 P32 Cr2 134.92(17) . . . . ? C1 Cr1 P32 Cr2 -162.3(8) . . . . ? P31 Cr1 P32 Cr2 -76.3(11) . . . . ? P11 Cr1 P32 Cr2 0.0(5) . . . . ? P2 Cr1 P32 Cr2 -56.3(2) . . . . ? P21 Cr1 P32 Cr2 -47.5(3) . . . . ? P51 Cr1 P32 Cr2 47.2(5) . . . . ? P4 Cr1 P32 Cr2 73.4(4) . . . . ? P42 Cr1 P32 Cr2 65.0(3) . . . . ? P22 P32 P42 P52 0.9(7) . . . . ? Cr2 P32 P42 P52 -45.8(4) . . . . ? Cr1 P32 P42 P52 47.2(4) . . . . ? P22 P32 P42 Cr1 -46.3(4) . . . . ? Cr2 P32 P42 Cr1 -93.0(2) . . . . ? P22 P32 P42 Cr2 46.7(4) . . . . ? Cr1 P32 P42 Cr2 93.0(2) . . . . ? C2 Cr1 P42 P52 132.3(10) . . . . ? C4 Cr1 P42 P52 130.4(4) . . . . ? C3 Cr1 P42 P52 159.0(3) . . . . ? C5 Cr1 P42 P52 92.1(4) . . . . ? C1 Cr1 P42 P52 69.3(4) . . . . ? P31 Cr1 P42 P52 -113.5(5) . . . . ? P11 Cr1 P42 P52 -16.8(7) . . . . ? P2 Cr1 P42 P52 -77.1(4) . . . . ? P21 Cr1 P42 P52 -65.5(5) . . . . ? P51 Cr1 P42 P52 11.1(9) . . . . ? P4 Cr1 P42 P52 -149.1(12) . . . . ? C2 Cr1 P42 P32 -98.4(10) . . . . ? C4 Cr1 P42 P32 -100.3(3) . . . . ? C3 Cr1 P42 P32 -71.7(4) . . . . ? C5 Cr1 P42 P32 -138.6(3) . . . . ? C1 Cr1 P42 P32 -161.5(3) . . . . ? P31 Cr1 P42 P32 15.8(6) . . . . ? P11 Cr1 P42 P32 112.5(6) . . . . ? P2 Cr1 P42 P32 52.2(4) . . . . ? P21 Cr1 P42 P32 63.8(5) . . . . ? P51 Cr1 P42 P32 140.3(10) . . . . ? P4 Cr1 P42 P32 -19.8(9) . . . . ? C2 Cr1 P42 Cr2 -163.0(9) . . . . ? C4 Cr1 P42 Cr2 -164.9(3) . . . . ? C3 Cr1 P42 Cr2 -136.29(17) . . . . ? C5 Cr1 P42 Cr2 156.8(2) . . . . ? C1 Cr1 P42 Cr2 133.94(18) . . . . ? P31 Cr1 P42 Cr2 -48.8(5) . . . . ? P11 Cr1 P42 Cr2 47.9(6) . . . . ? P2 Cr1 P42 Cr2 -12.4(3) . . . . ? P21 Cr1 P42 Cr2 -0.8(4) . . . . ? P51 Cr1 P42 Cr2 75.7(9) . . . . ? P4 Cr1 P42 Cr2 -84.4(10) . . . . ? P32 P42 P52 P12 -1.1(7) . . . . ? Cr1 P42 P52 P12 46.3(4) . . . . ? Cr2 P42 P52 P12 -46.9(4) . . . . ? P32 P42 P52 Cr2 45.8(4) . . . . ? Cr1 P42 P52 Cr2 93.1(2) . . . . ? P32 P42 P52 Cr1 -47.4(4) . . . . ? Cr2 P42 P52 Cr1 -93.1(2) . . . . ? P22 P12 P52 P42 0.9(7) . . . . ? Cr1 P12 P52 P42 -46.1(4) . . . . ? Cr2 P12 P52 P42 47.0(4) . . . . ? P22 P12 P52 Cr2 -46.0(4) . . . . ? Cr1 P12 P52 Cr2 -93.1(2) . . . . ? P22 P12 P52 Cr1 47.1(4) . . . . ? Cr2 P12 P52 Cr1 93.1(2) . . . . ? C2 Cr1 P52 P42 -161.8(3) . . . . ? C4 Cr1 P52 P42 -72.0(4) . . . . ? C3 Cr1 P52 P42 -99.0(10) . . . . ? C5 Cr1 P52 P42 -100.6(4) . . . . ? C1 Cr1 P52 P42 -139.0(3) . . . . ? P31 Cr1 P52 P42 62.4(6) . . . . ? P11 Cr1 P52 P42 142.4(14) . . . . ? P2 Cr1 P52 P42 104.2(4) . . . . ? P21 Cr1 P52 P42 111.4(5) . . . . ? P51 Cr1 P52 P42 -11.7(9) . . . . ? P4 Cr1 P52 P42 8.6(3) . . . . ? C2 Cr1 P52 P12 68.3(4) . . . . ? C4 Cr1 P52 P12 158.2(3) . . . . ? C3 Cr1 P52 P12 131.2(10) . . . . ? C5 Cr1 P52 P12 129.6(4) . . . . ? C1 Cr1 P52 P12 91.2(4) . . . . ? P31 Cr1 P52 P12 -67.5(6) . . . . ? P11 Cr1 P52 P12 12.6(14) . . . . ? P2 Cr1 P52 P12 -25.6(3) . . . . ? P21 Cr1 P52 P12 -18.4(5) . . . . ? P51 Cr1 P52 P12 -141.5(11) . . . . ? P4 Cr1 P52 P12 -121.2(4) . . . . ? P42 Cr1 P52 P12 -129.8(5) . . . . ? C2 Cr1 P52 Cr2 133.13(19) . . . . ? C4 Cr1 P52 Cr2 -137.01(17) . . . . ? C3 Cr1 P52 Cr2 -164.0(9) . . . . ? C5 Cr1 P52 Cr2 -165.6(2) . . . . ? C1 Cr1 P52 Cr2 156.0(2) . . . . ? P31 Cr1 P52 Cr2 -2.7(6) . . . . ? P11 Cr1 P52 Cr2 77.4(13) . . . . ? P2 Cr1 P52 Cr2 39.2(3) . . . . ? P21 Cr1 P52 Cr2 46.4(4) . . . . ? P51 Cr1 P52 Cr2 -76.7(10) . . . . ? P4 Cr1 P52 Cr2 -56.4(2) . . . . ? P42 Cr1 P52 Cr2 -65.0(3) . . . . ? P11 P21 Cr2 C11 91.3(6) . . . . ? P31 P21 Cr2 C11 -143.4(5) . . . . ? Cr1 P21 Cr2 C11 154.3(3) . . . . ? P11 P21 Cr2 C15 69.9(8) . . . . ? P31 P21 Cr2 C15 -164.8(5) . . . . ? Cr1 P21 Cr2 C15 132.9(4) . . . . ? P11 P21 Cr2 C14 137.6(13) . . . . ? P31 P21 Cr2 C14 -97.0(14) . . . . ? Cr1 P21 Cr2 C14 -159.4(10) . . . . ? P11 P21 Cr2 C13 158.4(6) . . . . ? P31 P21 Cr2 C13 -76.3(6) . . . . ? Cr1 P21 Cr2 C13 -138.6(2) . . . . ? P11 P21 Cr2 C12 129.3(6) . . . . ? P31 P21 Cr2 C12 -105.4(6) . . . . ? Cr1 P21 Cr2 C12 -167.7(3) . . . . ? P11 P21 Cr2 P31 -125.3(8) . . . . ? Cr1 P21 Cr2 P31 -62.3(6) . . . . ? P11 P21 Cr2 P41 -89.4(7) . . . . ? P31 P21 Cr2 P41 35.9(7) . . . . ? Cr1 P21 Cr2 P41 -26.4(5) . . . . ? P11 P21 Cr2 P51 -36.7(7) . . . . ? P31 P21 Cr2 P51 88.6(7) . . . . ? Cr1 P21 Cr2 P51 26.3(6) . . . . ? P31 P21 Cr2 P11 125.3(8) . . . . ? Cr1 P21 Cr2 P11 63.0(6) . . . . ? P11 P21 Cr2 P22 -141.8(13) . . . . ? P31 P21 Cr2 P22 -16.5(10) . . . . ? Cr1 P21 Cr2 P22 -78.9(10) . . . . ? P11 P21 Cr2 P1 7.3(8) . . . . ? P31 P21 Cr2 P1 132.6(8) . . . . ? Cr1 P21 Cr2 P1 70.3(5) . . . . ? P41 P31 Cr2 C11 -161.5(6) . . . . ? P21 P31 Cr2 C11 67.0(7) . . . . ? Cr1 P31 Cr2 C11 131.5(4) . . . . ? P41 P31 Cr2 C15 -85.4(17) . . . . ? P21 P31 Cr2 C15 143.1(15) . . . . ? Cr1 P31 Cr2 C15 -152.5(13) . . . . ? P41 P31 Cr2 C14 -70.8(7) . . . . ? P21 P31 Cr2 C14 157.6(5) . . . . ? Cr1 P31 Cr2 C14 -137.9(2) . . . . ? P41 P31 Cr2 C13 -101.7(6) . . . . ? P21 P31 Cr2 C13 126.7(5) . . . . ? Cr1 P31 Cr2 C13 -168.8(4) . . . . ? P41 P31 Cr2 C12 -140.0(6) . . . . ? P21 P31 Cr2 C12 88.5(5) . . . . ? Cr1 P31 Cr2 C12 153.0(3) . . . . ? P41 P31 Cr2 P21 131.5(8) . . . . ? Cr1 P31 Cr2 P21 64.5(6) . . . . ? P21 P31 Cr2 P41 -131.5(8) . . . . ? Cr1 P31 Cr2 P41 -67.1(7) . . . . ? P41 P31 Cr2 P51 39.0(7) . . . . ? P21 P31 Cr2 P51 -92.5(7) . . . . ? Cr1 P31 Cr2 P51 -28.1(7) . . . . ? P41 P31 Cr2 P11 90.8(7) . . . . ? P21 P31 Cr2 P11 -40.7(6) . . . . ? Cr1 P31 Cr2 P11 23.8(6) . . . . ? P41 P31 Cr2 P22 147.9(11) . . . . ? P21 P31 Cr2 P22 16.4(9) . . . . ? Cr1 P31 Cr2 P22 80.9(8) . . . . ? P41 P31 Cr2 P1 101.4(6) . . . . ? P21 P31 Cr2 P1 -30.2(6) . . . . ? Cr1 P31 Cr2 P1 34.3(5) . . . . ? P31 P41 Cr2 C11 140.6(12) . . . . ? P51 P41 Cr2 C11 -91.7(14) . . . . ? Cr1 P41 Cr2 C11 -156.0(10) . . . . ? P31 P41 Cr2 C15 159.4(5) . . . . ? P51 P41 Cr2 C15 -73.0(7) . . . . ? Cr1 P41 Cr2 C15 -137.2(3) . . . . ? P31 P41 Cr2 C14 129.5(5) . . . . ? P51 P41 Cr2 C14 -102.8(6) . . . . ? Cr1 P41 Cr2 C14 -167.1(3) . . . . ? P31 P41 Cr2 C13 91.5(6) . . . . ? P51 P41 Cr2 C13 -140.9(5) . . . . ? Cr1 P41 Cr2 C13 154.9(3) . . . . ? P31 P41 Cr2 C12 70.6(8) . . . . ? P51 P41 Cr2 C12 -161.7(5) . . . . ? Cr1 P41 Cr2 C12 134.0(4) . . . . ? P31 P41 Cr2 P21 -37.3(6) . . . . ? P51 P41 Cr2 P21 90.4(7) . . . . ? Cr1 P41 Cr2 P21 26.1(5) . . . . ? P51 P41 Cr2 P31 127.7(8) . . . . ? Cr1 P41 Cr2 P31 63.4(6) . . . . ? P31 P41 Cr2 P51 -127.7(8) . . . . ? Cr1 P41 Cr2 P51 -64.3(6) . . . . ? P31 P41 Cr2 P11 -90.3(8) . . . . ? P51 P41 Cr2 P11 37.3(8) . . . . ? Cr1 P41 Cr2 P11 -26.9(6) . . . . ? P31 P41 Cr2 P22 -14.9(6) . . . . ? P51 P41 Cr2 P22 112.8(6) . . . . ? Cr1 P41 Cr2 P22 48.5(3) . . . . ? P31 P41 Cr2 P1 -80.2(6) . . . . ? P51 P41 Cr2 P1 47.5(6) . . . . ? Cr1 P41 Cr2 P1 -16.8(5) . . . . ? P11 P51 Cr2 C11 -73.1(8) . . . . ? P41 P51 Cr2 C11 157.4(5) . . . . ? Cr1 P51 Cr2 C11 -136.9(2) . . . . ? P11 P51 Cr2 C15 -102.7(8) . . . . ? P41 P51 Cr2 C15 127.8(6) . . . . ? Cr1 P51 Cr2 C15 -166.4(4) . . . . ? P11 P51 Cr2 C14 -140.8(8) . . . . ? P41 P51 Cr2 C14 89.7(6) . . . . ? Cr1 P51 Cr2 C14 155.5(3) . . . . ? P11 P51 Cr2 C13 -161.5(8) . . . . ? P41 P51 Cr2 C13 69.0(7) . . . . ? Cr1 P51 Cr2 C13 134.7(3) . . . . ? P11 P51 Cr2 C12 -91.9(17) . . . . ? P41 P51 Cr2 C12 138.6(15) . . . . ? Cr1 P51 Cr2 C12 -155.6(12) . . . . ? P11 P51 Cr2 P21 37.4(8) . . . . ? P41 P51 Cr2 P21 -92.1(7) . . . . ? Cr1 P51 Cr2 P21 -26.3(6) . . . . ? P11 P51 Cr2 P31 91.3(9) . . . . ? P41 P51 Cr2 P31 -38.2(7) . . . . ? Cr1 P51 Cr2 P31 27.5(6) . . . . ? P11 P51 Cr2 P41 129.5(9) . . . . ? Cr1 P51 Cr2 P41 65.8(6) . . . . ? P41 P51 Cr2 P11 -129.5(9) . . . . ? Cr1 P51 Cr2 P11 -63.7(8) . . . . ? P11 P51 Cr2 P22 64.5(8) . . . . ? P41 P51 Cr2 P22 -65.0(6) . . . . ? Cr1 P51 Cr2 P22 0.8(6) . . . . ? P11 P51 Cr2 P1 5.2(10) . . . . ? P41 P51 Cr2 P1 -124.4(7) . . . . ? Cr1 P51 Cr2 P1 -58.6(4) . . . . ? P51 P11 Cr2 C11 127.9(6) . . . . ? P21 P11 Cr2 C11 -101.6(6) . . . . ? Cr1 P11 Cr2 C11 -166.5(4) . . . . ? P51 P11 Cr2 C15 89.6(6) . . . . ? P21 P11 Cr2 C15 -139.9(6) . . . . ? Cr1 P11 Cr2 C15 155.2(4) . . . . ? P51 P11 Cr2 C14 67.9(8) . . . . ? P21 P11 Cr2 C14 -161.5(6) . . . . ? Cr1 P11 Cr2 C14 133.6(5) . . . . ? P51 P11 Cr2 C13 136.3(16) . . . . ? P21 P11 Cr2 C13 -93(2) . . . . ? Cr1 P11 Cr2 C13 -158.1(15) . . . . ? P51 P11 Cr2 C12 157.5(5) . . . . ? P21 P11 Cr2 C12 -72.0(8) . . . . ? Cr1 P11 Cr2 C12 -136.9(3) . . . . ? P51 P11 Cr2 P21 -130.5(9) . . . . ? Cr1 P11 Cr2 P21 -64.9(7) . . . . ? P51 P11 Cr2 P31 -89.3(8) . . . . ? P21 P11 Cr2 P31 41.2(7) . . . . ? Cr1 P11 Cr2 P31 -23.7(7) . . . . ? P51 P11 Cr2 P41 -37.9(7) . . . . ? P21 P11 Cr2 P41 92.7(7) . . . . ? Cr1 P11 Cr2 P41 27.8(6) . . . . ? P21 P11 Cr2 P51 130.5(9) . . . . ? Cr1 P11 Cr2 P51 65.6(5) . . . . ? P51 P11 Cr2 P22 -113.3(7) . . . . ? P21 P11 Cr2 P22 17.3(6) . . . . ? Cr1 P11 Cr2 P22 -47.7(4) . . . . ? P51 P11 Cr2 P1 -156(4) . . . . ? P21 P11 Cr2 P1 -26(4) . . . . ? Cr1 P11 Cr2 P1 -91(4) . . . . ? P32 P22 Cr2 C11 -154.2(3) . . . . ? P12 P22 Cr2 C11 75.8(3) . . . . ? Cr1 P22 Cr2 C11 139.95(18) . . . . ? P32 P22 Cr2 C15 -150.3(6) . . . . ? P12 P22 Cr2 C15 79.7(7) . . . . ? Cr1 P22 Cr2 C15 143.8(5) . . . . ? P32 P22 Cr2 C14 -69.4(5) . . . . ? P12 P22 Cr2 C14 160.6(3) . . . . ? Cr1 P22 Cr2 C14 -135.2(2) . . . . ? P32 P22 Cr2 C13 -85.2(4) . . . . ? P12 P22 Cr2 C13 144.8(3) . . . . ? Cr1 P22 Cr2 C13 -151.1(2) . . . . ? P32 P22 Cr2 C12 -122.1(4) . . . . ? P12 P22 Cr2 C12 107.9(4) . . . . ? Cr1 P22 Cr2 C12 172.1(3) . . . . ? P32 P22 Cr2 P21 142.6(12) . . . . ? P12 P22 Cr2 P21 12.6(10) . . . . ? Cr1 P22 Cr2 P21 76.7(10) . . . . ? P32 P22 Cr2 P31 -8.2(8) . . . . ? P12 P22 Cr2 P31 -138.2(10) . . . . ? Cr1 P22 Cr2 P31 -74.0(9) . . . . ? P32 P22 Cr2 P41 17.1(5) . . . . ? P12 P22 Cr2 P41 -112.9(5) . . . . ? Cr1 P22 Cr2 P41 -48.7(4) . . . . ? P32 P22 Cr2 P51 65.0(6) . . . . ? P12 P22 Cr2 P51 -64.9(6) . . . . ? Cr1 P22 Cr2 P51 -0.8(6) . . . . ? P32 P22 Cr2 P11 112.0(5) . . . . ? P12 P22 Cr2 P11 -18.0(6) . . . . ? Cr1 P22 Cr2 P11 46.2(4) . . . . ? P32 P22 Cr2 P1 120.4(4) . . . . ? P12 P22 Cr2 P1 -9.6(3) . . . . ? Cr1 P22 Cr2 P1 54.6(3) . . . . ? P5 P1 Cr2 C11 120.4(3) . . . . ? P2 P1 Cr2 C11 -111.1(3) . . . . ? Cr1 P1 Cr2 C11 -174.9(2) . . . . ? P5 P1 Cr2 C15 83.8(3) . . . . ? P2 P1 Cr2 C15 -147.7(3) . . . . ? Cr1 P1 Cr2 C15 148.53(18) . . . . ? P5 P1 Cr2 C14 70.4(5) . . . . ? P2 P1 Cr2 C14 -161.1(3) . . . . ? Cr1 P1 Cr2 C14 135.1(3) . . . . ? P5 P1 Cr2 C13 152.2(5) . . . . ? P2 P1 Cr2 C13 -79.4(8) . . . . ? Cr1 P1 Cr2 C13 -143.1(5) . . . . ? P5 P1 Cr2 C12 153.4(3) . . . . ? P2 P1 Cr2 C12 -78.2(3) . . . . ? Cr1 P1 Cr2 C12 -141.93(14) . . . . ? P5 P1 Cr2 P21 -134.8(8) . . . . ? P2 P1 Cr2 P21 -6.3(8) . . . . ? Cr1 P1 Cr2 P21 -70.1(7) . . . . ? P5 P1 Cr2 P31 -98.2(6) . . . . ? P2 P1 Cr2 P31 30.2(5) . . . . ? Cr1 P1 Cr2 P31 -33.5(5) . . . . ? P5 P1 Cr2 P41 -47.7(5) . . . . ? P2 P1 Cr2 P41 80.8(5) . . . . ? Cr1 P1 Cr2 P41 17.0(5) . . . . ? P5 P1 Cr2 P51 -6.3(6) . . . . ? P2 P1 Cr2 P51 122.1(6) . . . . ? Cr1 P1 Cr2 P51 58.4(4) . . . . ? P5 P1 Cr2 P11 14(4) . . . . ? P2 P1 Cr2 P11 143(4) . . . . ? Cr1 P1 Cr2 P11 79(4) . . . . ? P5 P1 Cr2 P22 -119.8(4) . . . . ? P2 P1 Cr2 P22 8.6(3) . . . . ? Cr1 P1 Cr2 P22 -55.1(3) . . . . ? C14 Cr2 C11 C15 37.75(12) . . . . ? C13 Cr2 C11 C15 80.28(13) . . . . ? C12 Cr2 C11 C15 117.93(18) . . . . ? P21 Cr2 C11 C15 -156.8(4) . . . . ? P31 Cr2 C11 C15 152.8(7) . . . . ? P41 Cr2 C11 C15 25.4(15) . . . . ? P51 Cr2 C11 C15 -52.7(6) . . . . ? P11 Cr2 C11 C15 -102.6(6) . . . . ? P22 Cr2 C11 C15 177.6(4) . . . . ? P1 Cr2 C11 C15 -113.7(3) . . . . ? C15 Cr2 C11 C12 -117.93(18) . . . . ? C14 Cr2 C11 C12 -80.18(13) . . . . ? C13 Cr2 C11 C12 -37.66(13) . . . . ? P21 Cr2 C11 C12 85.2(4) . . . . ? P31 Cr2 C11 C12 34.8(7) . . . . ? P41 Cr2 C11 C12 -92.5(15) . . . . ? P51 Cr2 C11 C12 -170.7(6) . . . . ? P11 Cr2 C11 C12 139.5(6) . . . . ? P22 Cr2 C11 C12 59.7(4) . . . . ? P1 Cr2 C11 C12 128.3(3) . . . . ? C15 Cr2 C11 C16 120.9(3) . . . . ? C14 Cr2 C11 C16 158.7(3) . . . . ? C13 Cr2 C11 C16 -158.8(3) . . . . ? C12 Cr2 C11 C16 -121.1(3) . . . . ? P21 Cr2 C11 C16 -35.9(5) . . . . ? P31 Cr2 C11 C16 -86.3(7) . . . . ? P41 Cr2 C11 C16 146.4(14) . . . . ? P51 Cr2 C11 C16 68.2(6) . . . . ? P11 Cr2 C11 C16 18.4(6) . . . . ? P22 Cr2 C11 C16 -61.5(4) . . . . ? P1 Cr2 C11 C16 7.2(4) . . . . ? C15 C11 C12 C13 -0.2(2) . . . . ? C16 C11 C12 C13 -177.3(2) . . . . ? Cr2 C11 C12 C13 61.92(15) . . . . ? C15 C11 C12 C17 176.0(2) . . . . ? C16 C11 C12 C17 -1.0(4) . . . . ? Cr2 C11 C12 C17 -121.9(2) . . . . ? C15 C11 C12 Cr2 -62.14(15) . . . . ? C16 C11 C12 Cr2 120.8(2) . . . . ? C15 Cr2 C12 C11 37.27(12) . . . . ? C14 Cr2 C12 C11 79.75(13) . . . . ? C13 Cr2 C12 C11 117.06(18) . . . . ? P21 Cr2 C12 C11 -103.1(5) . . . . ? P31 Cr2 C12 C11 -158.0(5) . . . . ? P41 Cr2 C12 C11 151.2(7) . . . . ? P51 Cr2 C12 C11 25.3(17) . . . . ? P11 Cr2 C12 C11 -52.8(8) . . . . ? P22 Cr2 C12 C11 -131.2(4) . . . . ? P1 Cr2 C12 C11 -62.1(4) . . . . ? C11 Cr2 C12 C13 -117.06(18) . . . . ? C15 Cr2 C12 C13 -79.79(13) . . . . ? C14 Cr2 C12 C13 -37.31(12) . . . . ? P21 Cr2 C12 C13 139.8(5) . . . . ? P31 Cr2 C12 C13 84.9(5) . . . . ? P41 Cr2 C12 C13 34.2(7) . . . . ? P51 Cr2 C12 C13 -91.7(17) . . . . ? P11 Cr2 C12 C13 -169.8(8) . . . . ? P22 Cr2 C12 C13 111.7(4) . . . . ? P1 Cr2 C12 C13 -179.2(3) . . . . ? C11 Cr2 C12 C17 121.4(3) . . . . ? C15 Cr2 C12 C17 158.7(3) . . . . ? C14 Cr2 C12 C17 -158.8(3) . . . . ? C13 Cr2 C12 C17 -121.5(3) . . . . ? P21 Cr2 C12 C17 18.3(5) . . . . ? P31 Cr2 C12 C17 -36.6(6) . . . . ? P41 Cr2 C12 C17 -87.3(7) . . . . ? P51 Cr2 C12 C17 146.7(17) . . . . ? P11 Cr2 C12 C17 68.6(8) . . . . ? P22 Cr2 C12 C17 -9.8(5) . . . . ? P1 Cr2 C12 C17 59.3(4) . . . . ? C11 C12 C13 C14 0.2(2) . . . . ? C17 C12 C13 C14 -176.0(2) . . . . ? Cr2 C12 C13 C14 61.89(14) . . . . ? C11 C12 C13 C18 176.6(2) . . . . ? C17 C12 C13 C18 0.4(4) . . . . ? Cr2 C12 C13 C18 -121.7(2) . . . . ? C11 C12 C13 Cr2 -61.67(14) . . . . ? C17 C12 C13 Cr2 122.1(2) . . . . ? C11 Cr2 C13 C14 -80.07(13) . . . . ? C15 Cr2 C13 C14 -37.49(12) . . . . ? C12 Cr2 C13 C14 -117.80(18) . . . . ? P21 Cr2 C13 C14 -169.7(6) . . . . ? P31 Cr2 C13 C14 137.3(5) . . . . ? P41 Cr2 C13 C14 84.5(5) . . . . ? P51 Cr2 C13 C14 34.0(7) . . . . ? P11 Cr2 C13 C14 -89(2) . . . . ? P22 Cr2 C13 C14 165.1(4) . . . . ? P1 Cr2 C13 C14 -116.1(7) . . . . ? C11 Cr2 C13 C12 37.72(13) . . . . ? C15 Cr2 C13 C12 80.31(14) . . . . ? C14 Cr2 C13 C12 117.80(18) . . . . ? P21 Cr2 C13 C12 -51.9(6) . . . . ? P31 Cr2 C13 C12 -104.9(5) . . . . ? P41 Cr2 C13 C12 -157.7(5) . . . . ? P51 Cr2 C13 C12 151.7(6) . . . . ? P11 Cr2 C13 C12 28(2) . . . . ? P22 Cr2 C13 C12 -77.1(4) . . . . ? P1 Cr2 C13 C12 1.7(7) . . . . ? C11 Cr2 C13 C18 159.8(3) . . . . ? C15 Cr2 C13 C18 -157.6(3) . . . . ? C14 Cr2 C13 C18 -120.1(3) . . . . ? C12 Cr2 C13 C18 122.1(3) . . . . ? P21 Cr2 C13 C18 70.2(6) . . . . ? P31 Cr2 C13 C18 17.2(6) . . . . ? P41 Cr2 C13 C18 -35.6(5) . . . . ? P51 Cr2 C13 C18 -86.1(7) . . . . ? P11 Cr2 C13 C18 150(2) . . . . ? P22 Cr2 C13 C18 45.0(4) . . . . ? P1 Cr2 C13 C18 123.8(7) . . . . ? C12 C13 C14 C15 -0.1(2) . . . . ? C18 C13 C14 C15 -176.6(2) . . . . ? Cr2 C13 C14 C15 61.91(14) . . . . ? C12 C13 C14 C19 176.6(2) . . . . ? C18 C13 C14 C19 0.2(4) . . . . ? Cr2 C13 C14 C19 -121.3(2) . . . . ? C12 C13 C14 Cr2 -62.04(15) . . . . ? C18 C13 C14 Cr2 121.5(2) . . . . ? C11 Cr2 C14 C13 79.75(14) . . . . ? C15 Cr2 C14 C13 117.52(18) . . . . ? C12 Cr2 C14 C13 37.26(13) . . . . ? P21 Cr2 C14 C13 28.0(15) . . . . ? P31 Cr2 C14 C13 -55.7(6) . . . . ? P41 Cr2 C14 C13 -104.1(5) . . . . ? P51 Cr2 C14 C13 -157.8(5) . . . . ? P11 Cr2 C14 C13 153.0(7) . . . . ? P22 Cr2 C14 C13 -25.0(5) . . . . ? P1 Cr2 C14 C13 138.5(4) . . . . ? C11 Cr2 C14 C15 -37.77(13) . . . . ? C13 Cr2 C14 C15 -117.52(18) . . . . ? C12 Cr2 C14 C15 -80.26(14) . . . . ? P21 Cr2 C14 C15 -89.5(15) . . . . ? P31 Cr2 C14 C15 -173.2(6) . . . . ? P41 Cr2 C14 C15 138.4(5) . . . . ? P51 Cr2 C14 C15 84.7(5) . . . . ? P11 Cr2 C14 C15 35.4(7) . . . . ? P22 Cr2 C14 C15 -142.5(5) . . . . ? P1 Cr2 C14 C15 20.9(4) . . . . ? C11 Cr2 C14 C19 -160.2(2) . . . . ? C15 Cr2 C14 C19 -122.4(3) . . . . ? C13 Cr2 C14 C19 120.1(3) . . . . ? C12 Cr2 C14 C19 157.3(2) . . . . ? P21 Cr2 C14 C19 148.1(15) . . . . ? P31 Cr2 C14 C19 64.4(6) . . . . ? P41 Cr2 C14 C19 15.9(5) . . . . ? P51 Cr2 C14 C19 -37.8(5) . . . . ? P11 Cr2 C14 C19 -87.0(7) . . . . ? P22 Cr2 C14 C19 95.1(6) . . . . ? P1 Cr2 C14 C19 -101.5(4) . . . . ? C12 C11 C15 C14 0.1(2) . . . . ? C16 C11 C15 C14 177.2(2) . . . . ? Cr2 C11 C15 C14 -62.22(14) . . . . ? C12 C11 C15 C20 -177.0(2) . . . . ? C16 C11 C15 C20 0.0(3) . . . . ? Cr2 C11 C15 C20 120.6(2) . . . . ? C12 C11 C15 Cr2 62.35(15) . . . . ? C16 C11 C15 Cr2 -120.6(2) . . . . ? C13 C14 C15 C11 0.0(2) . . . . ? C19 C14 C15 C11 -176.7(2) . . . . ? Cr2 C14 C15 C11 62.01(14) . . . . ? C13 C14 C15 C20 177.1(2) . . . . ? C19 C14 C15 C20 0.5(4) . . . . ? Cr2 C14 C15 C20 -120.9(2) . . . . ? C13 C14 C15 Cr2 -62.01(14) . . . . ? C19 C14 C15 Cr2 121.3(2) . . . . ? C14 Cr2 C15 C11 -116.99(18) . . . . ? C13 Cr2 C15 C11 -79.56(14) . . . . ? C12 Cr2 C15 C11 -37.21(13) . . . . ? P21 Cr2 C15 C11 35.1(6) . . . . ? P31 Cr2 C15 C11 -97.6(18) . . . . ? P41 Cr2 C15 C11 -170.5(5) . . . . ? P51 Cr2 C15 C11 139.1(6) . . . . ? P11 Cr2 C15 C11 86.3(5) . . . . ? P22 Cr2 C15 C11 -5.5(9) . . . . ? P1 Cr2 C15 C11 75.2(3) . . . . ? C11 Cr2 C15 C14 116.99(18) . . . . ? C13 Cr2 C15 C14 37.43(13) . . . . ? C12 Cr2 C15 C14 79.79(14) . . . . ? P21 Cr2 C15 C14 152.1(6) . . . . ? P31 Cr2 C15 C14 19.4(18) . . . . ? P41 Cr2 C15 C14 -53.5(6) . . . . ? P51 Cr2 C15 C14 -103.9(6) . . . . ? P11 Cr2 C15 C14 -156.7(5) . . . . ? P22 Cr2 C15 C14 111.5(9) . . . . ? P1 Cr2 C15 C14 -167.8(3) . . . . ? C11 Cr2 C15 C20 -121.3(3) . . . . ? C14 Cr2 C15 C20 121.7(3) . . . . ? C13 Cr2 C15 C20 159.2(2) . . . . ? C12 Cr2 C15 C20 -158.5(2) . . . . ? P21 Cr2 C15 C20 -86.2(6) . . . . ? P31 Cr2 C15 C20 141.1(18) . . . . ? P41 Cr2 C15 C20 68.2(6) . . . . ? P51 Cr2 C15 C20 17.8(6) . . . . ? P11 Cr2 C15 C20 -35.0(5) . . . . ? P22 Cr2 C15 C20 -126.8(9) . . . . ? P1 Cr2 C15 C20 -46.1(3) . . . . ? _diffrn_measured_fraction_theta_max 0.970 _diffrn_reflns_theta_full 30.47 _diffrn_measured_fraction_theta_full 0.970 _refine_diff_density_max 0.907 _refine_diff_density_min -0.534 _refine_diff_density_rms 0.089 #===END data_190k _database_code_depnum_ccdc_archive 'CCDC 618752' _audit_creation_method SHELXL-97 _chemical_name_systematic ; \m~2~-\h^5^,\h^5^-cyclopentaphosphole)-bis ((\h^5^-pentamethyl-cyclopentadienyl)-chromium) hexafluoroantimonate ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H30 Cr2 F6 P5 Sb' _chemical_formula_weight 765.04 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting orthorhombic _symmetry_space_group_name_H-M Fddd loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+3/4, -y+3/4, z' '-x+3/4, y, -z+3/4' 'x, -y+3/4, -z+3/4' 'x, y+1/2, z+1/2' '-x+3/4, -y+5/4, z+1/2' '-x+3/4, y+1/2, -z+5/4' 'x, -y+5/4, -z+5/4' 'x+1/2, y, z+1/2' '-x+5/4, -y+3/4, z+1/2' '-x+5/4, y, -z+5/4' 'x+1/2, -y+3/4, -z+5/4' 'x+1/2, y+1/2, z' '-x+5/4, -y+5/4, z' '-x+5/4, y+1/2, -z+3/4' 'x+1/2, -y+5/4, -z+3/4' '-x, -y, -z' 'x-3/4, y-3/4, -z' 'x-3/4, -y, z-3/4' '-x, y-3/4, z-3/4' '-x, -y+1/2, -z+1/2' 'x-3/4, y-1/4, -z+1/2' 'x-3/4, -y+1/2, z-1/4' '-x, y-1/4, z-1/4' '-x+1/2, -y, -z+1/2' 'x-1/4, y-3/4, -z+1/2' 'x-1/4, -y, z-1/4' '-x+1/2, y-3/4, z-1/4' '-x+1/2, -y+1/2, -z' 'x-1/4, y-1/4, -z' 'x-1/4, -y+1/2, z-3/4' '-x+1/2, y-1/4, z-3/4' _cell_length_a 21.3664(7) _cell_length_b 29.3735(9) _cell_length_c 35.9750(12) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_volume 22578.1(13) _cell_formula_units_Z 32 _cell_measurement_temperature 190(2) _cell_measurement_reflns_used 6874 _cell_measurement_theta_min 2.35 _cell_measurement_theta_max 30.39 _exptl_crystal_description 'irregular block' _exptl_crystal_colour 'dark green' _exptl_crystal_size_max 0.60 _exptl_crystal_size_mid 0.52 _exptl_crystal_size_min 0.40 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.801 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 12096 _exptl_absorpt_coefficient_mu 2.039 _exptl_absorpt_correction_type integration _exptl_absorpt_correction_T_min 0.395 _exptl_absorpt_correction_T_max 0.615 _exptl_absorpt_process_details 'XPREP in SHELXTL' _exptl_special_details ; ? ; _diffrn_ambient_temperature 190(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'Bede Microsource X-ray Generator' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEX CCD Diffractometer' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number 0 _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% 0 _diffrn_reflns_number 42727 _diffrn_reflns_av_R_equivalents 0.0198 _diffrn_reflns_av_sigmaI/netI 0.0161 _diffrn_reflns_limit_h_min -30 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_k_min -41 _diffrn_reflns_limit_k_max 41 _diffrn_reflns_limit_l_min -46 _diffrn_reflns_limit_l_max 51 _diffrn_reflns_theta_min 1.31 _diffrn_reflns_theta_max 30.46 _reflns_number_total 8331 _reflns_number_gt 6895 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'SMART V5.625 (Bruker, 2003)' _computing_cell_refinement 'SMART V5.625 (Bruker, 2003)' _computing_data_reduction 'SAINT V6.28A (Bruker, 2003)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'SHELXTL V6.12(Bruker, 2001)' _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0458P)^2^+60.7724P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 8331 _refine_ls_number_parameters 404 _refine_ls_number_restraints 90 _refine_ls_R_factor_all 0.0396 _refine_ls_R_factor_gt 0.0296 _refine_ls_wR_factor_ref 0.0902 _refine_ls_wR_factor_gt 0.0787 _refine_ls_goodness_of_fit_ref 1.077 _refine_ls_restrained_S_all 1.074 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb1 Sb 0.6250 0.1250 0.009693(7) 0.04009(7) Uani 1 2 d S . . F1A F 0.6884(3) 0.1039(3) -0.0173(3) 0.139(2) Uani 0.50 1 d P A 1 F2A F 0.5537(3) 0.1384(3) 0.0346(3) 0.139(2) Uani 0.50 1 d P A 1 F1B F 0.6719(5) 0.1185(2) -0.03387(18) 0.131(3) Uani 0.50 1 d P A 2 F2B F 0.5863(4) 0.1418(2) 0.05316(17) 0.131(3) Uani 0.50 1 d P A 2 F3 F 0.59526(14) 0.06561(8) 0.00975(8) 0.1011(9) Uani 1 1 d . A . Sb2 Sb 0.1250 0.239488(9) 0.1250 0.04321(7) Uani 1 2 d S . . F4 F 0.18548(11) 0.28489(8) 0.12130(8) 0.0951(8) Uani 1 1 d . . . F5 F 0.11806(12) 0.23853(8) 0.07317(6) 0.0814(7) Uani 1 1 d . . . F6 F 0.18682(9) 0.19468(7) 0.12254(6) 0.0671(5) Uani 1 1 d . . . C1 C 0.13914(10) 0.36997(7) 0.01296(6) 0.0294(4) Uani 1 1 d . B . C2 C 0.19763(10) 0.34900(7) 0.00469(6) 0.0312(4) Uani 1 1 d . B . C3 C 0.22743(10) 0.37462(8) -0.02399(6) 0.0334(4) Uani 1 1 d . B . C4 C 0.18739(10) 0.41173(8) -0.03324(6) 0.0334(4) Uani 1 1 d . B . C5 C 0.13299(9) 0.40877(7) -0.01048(6) 0.0298(4) Uani 1 1 d . B . C6 C 0.09115(12) 0.35239(9) 0.03988(7) 0.0444(5) Uani 1 1 d . . . H6A H 0.0645 0.3300 0.0274 0.067 Uiso 1 1 calc R . . H6B H 0.0654 0.3777 0.0488 0.067 Uiso 1 1 calc R . . H6C H 0.1123 0.3380 0.0610 0.067 Uiso 1 1 calc R . . C7 C 0.22159(14) 0.30581(8) 0.02188(8) 0.0479(6) Uani 1 1 d . . . H7A H 0.1978 0.2799 0.0121 0.072 Uiso 1 1 calc R . . H7B H 0.2166 0.3073 0.0489 0.072 Uiso 1 1 calc R . . H7C H 0.2660 0.3020 0.0158 0.072 Uiso 1 1 calc R . . C8 C 0.28853(12) 0.36361(11) -0.04241(8) 0.0511(7) Uani 1 1 d . . . H8A H 0.2810 0.3436 -0.0637 0.077 Uiso 1 1 calc R . . H8B H 0.3161 0.3483 -0.0246 0.077 Uiso 1 1 calc R . . H8C H 0.3084 0.3918 -0.0509 0.077 Uiso 1 1 calc R . . C9 C 0.19790(15) 0.44630(11) -0.06307(7) 0.0554(7) Uani 1 1 d . . . H9A H 0.1752 0.4372 -0.0855 0.083 Uiso 1 1 calc R . . H9B H 0.2427 0.4483 -0.0686 0.083 Uiso 1 1 calc R . . H9C H 0.1827 0.4760 -0.0546 0.083 Uiso 1 1 calc R . . C10 C 0.07705(11) 0.43912(9) -0.01312(8) 0.0440(6) Uani 1 1 d . . . H10A H 0.0514 0.4300 -0.0345 0.066 Uiso 1 1 calc R . . H10B H 0.0908 0.4707 -0.0163 0.066 Uiso 1 1 calc R . . H10C H 0.0522 0.4366 0.0097 0.066 Uiso 1 1 calc R . . Cr1 Cr 0.215699(14) 0.418226(10) 0.025363(9) 0.02442(7) Uani 1 1 d . . . P11 P 0.1883(10) 0.4345(7) 0.0877(5) 0.069(6) Uani 0.25 1 d PU B 1 P21 P 0.2730(7) 0.3981(4) 0.0803(5) 0.056(5) Uani 0.25 1 d PU B 1 P31 P 0.3229(6) 0.4326(7) 0.0371(5) 0.053(5) Uani 0.25 1 d PU B 1 P41 P 0.2729(9) 0.4894(6) 0.0209(5) 0.063(5) Uani 0.25 1 d PU B 1 P51 P 0.1888(7) 0.4912(5) 0.0521(5) 0.068(6) Uani 0.25 1 d PU B 1 P1 P 0.1985(6) 0.4231(4) 0.0923(3) 0.054(2) Uani 0.50 1 d PU B 2 P2 P 0.2897(4) 0.3967(3) 0.0733(3) 0.050(2) Uani 0.50 1 d PU B 2 P3 P 0.3253(5) 0.4425(4) 0.0304(3) 0.050(2) Uani 0.50 1 d PU B 2 P4 P 0.2557(5) 0.4958(3) 0.0216(3) 0.0496(18) Uani 0.50 1 d PU B 2 P5 P 0.1787(3) 0.4846(4) 0.0599(3) 0.055(2) Uani 0.50 1 d PU B 2 P12 P 0.2224(5) 0.4078(3) 0.0930(2) 0.062(3) Uani 0.25 1 d PU B 3 P22 P 0.3120(4) 0.4044(3) 0.0612(3) 0.066(3) Uani 0.25 1 d PU B 3 P32 P 0.3150(5) 0.4611(4) 0.0229(2) 0.065(3) Uani 0.25 1 d PU B 3 P42 P 0.2291(5) 0.5005(3) 0.0294(3) 0.061(3) Uani 0.25 1 d PU B 3 P52 P 0.1722(4) 0.4689(3) 0.0726(3) 0.058(3) Uani 0.25 1 d PU B 3 Cr2 Cr 0.283321(14) 0.478264(10) 0.086526(9) 0.02428(7) Uani 1 1 d . . . C11 C 0.29490(11) 0.49166(7) 0.14627(6) 0.0326(4) Uani 1 1 d . B . C12 C 0.35440(11) 0.48056(7) 0.13110(6) 0.0341(4) Uani 1 1 d . B . C13 C 0.36913(9) 0.51424(8) 0.10399(6) 0.0320(4) Uani 1 1 d . B . C14 C 0.31886(9) 0.54603(7) 0.10255(6) 0.0283(4) Uani 1 1 d . B . C15 C 0.27258(9) 0.53203(7) 0.12878(6) 0.0289(4) Uani 1 1 d . B . C16 C 0.26227(16) 0.46639(10) 0.17703(7) 0.0537(7) Uani 1 1 d . . . H16A H 0.2767 0.4780 0.2011 0.081 Uiso 1 1 calc R B . H16B H 0.2719 0.4338 0.1752 0.081 Uiso 1 1 calc R . . H16C H 0.2170 0.4709 0.1749 0.081 Uiso 1 1 calc R . . C17 C 0.39624(15) 0.44239(9) 0.14331(10) 0.0600(8) Uani 1 1 d . . . H17A H 0.4228 0.4528 0.1638 0.090 Uiso 1 1 calc R B . H17B H 0.4226 0.4328 0.1224 0.090 Uiso 1 1 calc R . . H17C H 0.3706 0.4166 0.1516 0.090 Uiso 1 1 calc R . . C18 C 0.42877(12) 0.51804(12) 0.08228(8) 0.0541(7) Uani 1 1 d . . . H18A H 0.4574 0.5390 0.0950 0.081 Uiso 1 1 calc R B . H18B H 0.4196 0.5297 0.0573 0.081 Uiso 1 1 calc R . . H18C H 0.4483 0.4880 0.0803 0.081 Uiso 1 1 calc R . . C19 C 0.31744(14) 0.58786(8) 0.07896(7) 0.0456(6) Uani 1 1 d . . . H19A H 0.3374 0.6131 0.0923 0.068 Uiso 1 1 calc R B . H19B H 0.2739 0.5958 0.0733 0.068 Uiso 1 1 calc R . . H19C H 0.3401 0.5821 0.0557 0.068 Uiso 1 1 calc R . . C20 C 0.21309(11) 0.55646(9) 0.13773(8) 0.0441(6) Uani 1 1 d . . . H20A H 0.2204 0.5779 0.1582 0.066 Uiso 1 1 calc R B . H20B H 0.1811 0.5343 0.1451 0.066 Uiso 1 1 calc R . . H20C H 0.1987 0.5732 0.1158 0.066 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.03287(11) 0.04908(13) 0.03833(12) 0.000 0.000 0.00414(9) F1A 0.087(3) 0.136(4) 0.194(7) -0.039(4) 0.086(4) 0.010(3) F2A 0.087(3) 0.136(4) 0.194(7) -0.039(4) 0.086(4) 0.010(3) F1B 0.227(7) 0.085(3) 0.082(3) -0.010(2) 0.097(4) -0.019(3) F2B 0.227(7) 0.085(3) 0.082(3) -0.010(2) 0.097(4) -0.019(3) F3 0.122(2) 0.0599(13) 0.122(2) 0.0126(13) -0.0332(17) -0.0245(14) Sb2 0.03639(12) 0.05040(14) 0.04283(13) 0.000 0.00741(9) 0.000 F4 0.0789(15) 0.0819(15) 0.125(2) -0.0258(14) 0.0229(14) -0.0366(13) F5 0.1059(17) 0.0949(16) 0.0434(10) 0.0186(10) 0.0000(10) -0.0184(13) F6 0.0518(10) 0.0796(13) 0.0700(12) -0.0187(10) 0.0013(9) 0.0179(9) C1 0.0305(9) 0.0286(9) 0.0290(9) -0.0041(7) -0.0029(8) -0.0004(7) C2 0.0342(10) 0.0280(9) 0.0314(10) -0.0069(8) -0.0060(8) 0.0060(8) C3 0.0287(9) 0.0436(11) 0.0281(10) -0.0118(8) -0.0015(8) 0.0048(8) C4 0.0346(10) 0.0417(11) 0.0240(9) 0.0015(8) -0.0038(8) 0.0003(8) C5 0.0280(9) 0.0311(9) 0.0301(10) -0.0024(8) -0.0071(8) 0.0050(7) C6 0.0426(13) 0.0461(13) 0.0444(13) -0.0003(11) 0.0069(10) -0.0119(10) C7 0.0601(15) 0.0290(10) 0.0546(15) -0.0034(10) -0.0156(13) 0.0136(10) C8 0.0341(11) 0.0751(19) 0.0442(14) -0.0231(13) 0.0056(10) 0.0051(12) C9 0.0647(17) 0.0687(18) 0.0328(13) 0.0186(12) -0.0067(12) -0.0083(15) C10 0.0368(11) 0.0457(13) 0.0495(14) -0.0053(11) -0.0143(10) 0.0143(10) Cr1 0.02448(14) 0.02541(14) 0.02339(15) -0.00044(11) -0.00136(11) 0.00343(11) P11 0.059(7) 0.120(16) 0.027(5) -0.021(7) 0.015(5) -0.058(9) P21 0.095(12) 0.020(2) 0.054(6) 0.003(3) -0.047(8) 0.002(4) P31 0.020(2) 0.078(10) 0.061(9) -0.043(8) 0.011(3) -0.007(4) P41 0.103(13) 0.055(8) 0.030(2) 0.016(4) -0.019(6) -0.041(8) P51 0.052(7) 0.054(5) 0.097(12) -0.044(7) -0.045(8) 0.038(6) P1 0.068(4) 0.072(4) 0.0237(19) 0.000(2) 0.003(2) -0.042(3) P2 0.061(4) 0.0314(12) 0.058(4) -0.0114(16) -0.034(3) 0.0197(19) P3 0.0325(14) 0.074(5) 0.043(3) -0.025(3) 0.0170(14) -0.0211(18) P4 0.074(5) 0.0323(19) 0.0424(18) 0.0128(13) -0.025(2) -0.011(2) P5 0.028(2) 0.073(4) 0.065(4) -0.040(2) -0.007(2) 0.015(2) P12 0.106(8) 0.051(4) 0.028(2) 0.006(2) -0.017(4) -0.043(4) P22 0.048(4) 0.066(5) 0.084(7) -0.048(5) -0.039(4) 0.035(3) P32 0.069(6) 0.092(7) 0.033(3) -0.019(4) 0.013(3) -0.045(5) P42 0.084(6) 0.0285(16) 0.070(6) 0.000(3) -0.048(5) 0.005(4) P52 0.0216(16) 0.090(7) 0.063(6) -0.050(4) 0.002(3) 0.001(4) Cr2 0.02412(14) 0.02456(14) 0.02416(15) -0.00146(11) 0.00006(11) 0.00029(11) C11 0.0405(11) 0.0328(10) 0.0245(9) 0.0003(8) -0.0025(8) -0.0104(8) C12 0.0375(10) 0.0304(9) 0.0344(11) -0.0050(8) -0.0128(9) 0.0016(8) C13 0.0257(9) 0.0383(10) 0.0320(10) -0.0097(8) 0.0013(8) -0.0038(8) C14 0.0312(9) 0.0262(8) 0.0276(9) -0.0012(7) 0.0021(7) -0.0055(7) C15 0.0287(9) 0.0298(9) 0.0282(9) -0.0068(7) 0.0041(7) -0.0036(7) C16 0.0756(19) 0.0567(16) 0.0287(11) 0.0074(11) -0.0026(12) -0.0334(14) C17 0.0676(18) 0.0402(13) 0.072(2) -0.0120(13) -0.0388(16) 0.0163(13) C18 0.0300(11) 0.078(2) 0.0542(16) -0.0241(14) 0.0110(11) -0.0111(12) C19 0.0654(16) 0.0307(10) 0.0408(13) 0.0073(9) -0.0023(12) -0.0115(11) C20 0.0325(10) 0.0458(13) 0.0542(15) -0.0216(11) 0.0068(10) 0.0022(9) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb1 F1A 1.778(5) 14_545 ? Sb1 F1A 1.778(5) . ? Sb1 F2A 1.811(5) 14_545 ? Sb1 F2A 1.811(5) . ? Sb1 F2B 1.836(5) 14_545 ? Sb1 F2B 1.837(5) . ? Sb1 F3 1.857(2) . ? Sb1 F3 1.857(2) 14_545 ? Sb1 F1B 1.870(5) 14_545 ? Sb1 F1B 1.870(5) . ? Sb2 F4 1.862(2) . ? Sb2 F4 1.862(2) 11_454 ? Sb2 F6 1.8668(18) . ? Sb2 F6 1.8668(18) 11_454 ? Sb2 F5 1.871(2) . ? Sb2 F5 1.871(2) 11_454 ? C1 C5 1.424(3) . ? C1 C2 1.425(3) . ? C1 C6 1.502(3) . ? C1 Cr1 2.210(2) . ? C2 C3 1.427(3) . ? C2 C7 1.501(3) . ? C2 Cr1 2.199(2) . ? C3 C4 1.425(3) . ? C3 C8 1.499(3) . ? C3 Cr1 2.204(2) . ? C4 C5 1.424(3) . ? C4 C9 1.494(3) . ? C4 Cr1 2.202(2) . ? C5 C10 1.494(3) . ? C5 Cr1 2.2051(19) . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? Cr1 P31 2.366(15) . ? Cr1 P11 2.367(18) . ? Cr1 P21 2.400(15) . ? Cr1 P51 2.419(12) . ? Cr1 P2 2.424(8) . ? Cr1 P41 2.427(19) . ? Cr1 P4 2.437(9) . ? P11 P51 2.10(3) . ? P11 P21 2.12(3) . ? P11 Cr2 2.404(18) . ? P21 P31 2.14(2) . ? P21 Cr2 2.375(12) . ? P31 P41 2.07(2) . ? P31 Cr2 2.383(16) . ? P41 P51 2.12(2) . ? P41 Cr2 2.393(16) . ? P51 Cr2 2.399(12) . ? P1 P5 2.190(14) . ? P1 P2 2.205(14) . ? P1 Cr2 2.439(10) . ? P2 P3 2.184(12) . ? P2 Cr2 2.446(7) . ? P3 P4 2.181(14) . ? P3 Cr2 2.446(10) . ? P4 P5 2.171(13) . ? P4 Cr2 2.463(9) . ? P5 Cr2 2.439(8) . ? P12 P52 2.216(11) . ? P12 P22 2.233(11) . ? P12 Cr2 2.457(8) . ? P22 P32 2.163(11) . ? P22 Cr2 2.431(7) . ? P32 P42 2.181(11) . ? P32 Cr2 2.440(8) . ? P42 P52 2.181(11) . ? P42 Cr2 2.446(9) . ? P52 Cr2 2.442(9) . ? Cr2 C11 2.199(2) . ? Cr2 C15 2.2040(19) . ? Cr2 C14 2.2070(19) . ? Cr2 C13 2.207(2) . ? Cr2 C12 2.210(2) . ? C11 C12 1.421(3) . ? C11 C15 1.425(3) . ? C11 C16 1.504(3) . ? C12 C13 1.424(3) . ? C12 C17 1.500(3) . ? C13 C14 1.424(3) . ? C13 C18 1.499(3) . ? C14 C15 1.427(3) . ? C14 C19 1.494(3) . ? C15 C20 1.495(3) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F1A Sb1 F1A 113.7(7) 14_545 . ? F1A Sb1 F2A 170.7(4) 14_545 14_545 ? F1A Sb1 F2A 63.5(5) . 14_545 ? F1A Sb1 F2A 63.5(5) 14_545 . ? F1A Sb1 F2A 170.7(4) . . ? F2A Sb1 F2A 120.7(7) 14_545 . ? F1A Sb1 F2B 154.4(5) 14_545 14_545 ? F1A Sb1 F2B 91.7(4) . 14_545 ? F2A Sb1 F2B 30.8(4) 14_545 14_545 ? F2A Sb1 F2B 90.9(5) . 14_545 ? F1A Sb1 F2B 91.6(4) 14_545 . ? F1A Sb1 F2B 154.4(5) . . ? F2A Sb1 F2B 90.9(5) 14_545 . ? F2A Sb1 F2B 30.8(4) . . ? F2B Sb1 F2B 63.3(6) 14_545 . ? F1A Sb1 F3 93.9(3) 14_545 . ? F1A Sb1 F3 86.2(3) . . ? F2A Sb1 F3 94.7(3) 14_545 . ? F2A Sb1 F3 85.2(3) . . ? F2B Sb1 F3 84.3(2) 14_545 . ? F2B Sb1 F3 95.6(2) . . ? F1A Sb1 F3 86.2(3) 14_545 14_545 ? F1A Sb1 F3 93.9(3) . 14_545 ? F2A Sb1 F3 85.2(3) 14_545 14_545 ? F2A Sb1 F3 94.7(3) . 14_545 ? F2B Sb1 F3 95.6(2) 14_545 14_545 ? F2B Sb1 F3 84.3(2) . 14_545 ? F3 Sb1 F3 179.87(18) . 14_545 ? F1A Sb1 F1B 25.6(4) 14_545 14_545 ? F1A Sb1 F1B 89.2(4) . 14_545 ? F2A Sb1 F1B 152.6(5) 14_545 14_545 ? F2A Sb1 F1B 86.6(4) . 14_545 ? F2B Sb1 F1B 169.2(3) 14_545 14_545 ? F2B Sb1 F1B 116.4(5) . 14_545 ? F3 Sb1 F1B 85.1(2) . 14_545 ? F3 Sb1 F1B 95.1(2) 14_545 14_545 ? F1A Sb1 F1B 89.2(4) 14_545 . ? F1A Sb1 F1B 25.6(4) . . ? F2A Sb1 F1B 86.6(4) 14_545 . ? F2A Sb1 F1B 152.6(5) . . ? F2B Sb1 F1B 116.4(5) 14_545 . ? F2B Sb1 F1B 169.2(3) . . ? F3 Sb1 F1B 95.0(2) . . ? F3 Sb1 F1B 85.1(2) 14_545 . ? F1B Sb1 F1B 66.2(6) 14_545 . ? F4 Sb2 F4 88.50(17) . 11_454 ? F4 Sb2 F6 90.61(11) . . ? F4 Sb2 F6 178.30(12) 11_454 . ? F4 Sb2 F6 178.30(12) . 11_454 ? F4 Sb2 F6 90.60(11) 11_454 11_454 ? F6 Sb2 F6 90.33(13) . 11_454 ? F4 Sb2 F5 89.69(11) . . ? F4 Sb2 F5 91.55(12) 11_454 . ? F6 Sb2 F5 89.90(10) . . ? F6 Sb2 F5 88.89(9) 11_454 . ? F4 Sb2 F5 91.55(12) . 11_454 ? F4 Sb2 F5 89.69(11) 11_454 11_454 ? F6 Sb2 F5 88.89(9) . 11_454 ? F6 Sb2 F5 89.89(10) 11_454 11_454 ? F5 Sb2 F5 178.27(15) . 11_454 ? C5 C1 C2 107.66(19) . . ? C5 C1 C6 126.4(2) . . ? C2 C1 C6 125.8(2) . . ? C5 C1 Cr1 71.00(11) . . ? C2 C1 Cr1 70.74(12) . . ? C6 C1 Cr1 126.55(16) . . ? C1 C2 C3 108.32(18) . . ? C1 C2 C7 125.3(2) . . ? C3 C2 C7 126.3(2) . . ? C1 C2 Cr1 71.57(11) . . ? C3 C2 Cr1 71.25(12) . . ? C7 C2 Cr1 125.61(16) . . ? C4 C3 C2 107.72(18) . . ? C4 C3 C8 125.8(2) . . ? C2 C3 C8 126.5(2) . . ? C4 C3 Cr1 71.05(12) . . ? C2 C3 Cr1 70.92(11) . . ? C8 C3 Cr1 125.48(16) . . ? C5 C4 C3 108.00(19) . . ? C5 C4 C9 125.2(2) . . ? C3 C4 C9 126.7(2) . . ? C5 C4 Cr1 71.28(12) . . ? C3 C4 Cr1 71.21(12) . . ? C9 C4 Cr1 125.98(18) . . ? C1 C5 C4 108.30(18) . . ? C1 C5 C10 126.1(2) . . ? C4 C5 C10 125.4(2) . . ? C1 C5 Cr1 71.38(11) . . ? C4 C5 Cr1 71.01(12) . . ? C10 C5 Cr1 127.10(15) . . ? C1 C6 H6A 109.5 . . ? C1 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C1 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C2 Cr1 C4 63.12(8) . . ? C2 Cr1 C3 37.82(9) . . ? C4 Cr1 C3 37.75(8) . . ? C2 Cr1 C5 62.94(8) . . ? C4 Cr1 C5 37.72(8) . . ? C3 Cr1 C5 63.05(8) . . ? C2 Cr1 C1 37.70(7) . . ? C4 Cr1 C1 63.11(8) . . ? C3 Cr1 C1 63.17(8) . . ? C5 Cr1 C1 37.62(8) . . ? C2 Cr1 P31 113.2(5) . . ? C4 Cr1 P31 116.9(4) . . ? C3 Cr1 P31 97.9(4) . . ? C5 Cr1 P31 154.5(4) . . ? C1 Cr1 P31 150.0(5) . . ? C2 Cr1 P11 117.6(5) . . ? C4 Cr1 P11 149.0(5) . . ? C3 Cr1 P11 155.4(5) . . ? C5 Cr1 P11 112.4(5) . . ? C1 Cr1 P11 97.9(4) . . ? P31 Cr1 P11 92.0(6) . . ? C2 Cr1 P21 98.1(3) . . ? C4 Cr1 P21 155.2(3) . . ? C3 Cr1 P21 117.6(3) . . ? C5 Cr1 P21 149.3(4) . . ? C1 Cr1 P21 112.7(4) . . ? P31 Cr1 P21 53.4(6) . . ? P11 Cr1 P21 52.8(6) . . ? C2 Cr1 P51 155.8(4) . . ? C4 Cr1 P51 113.1(4) . . ? C3 Cr1 P51 149.6(5) . . ? C5 Cr1 P51 98.9(3) . . ? C1 Cr1 P51 118.2(4) . . ? P31 Cr1 P51 90.1(6) . . ? P11 Cr1 P51 52.1(7) . . ? P21 Cr1 P51 90.7(5) . . ? C2 Cr1 P2 96.57(19) . . ? C4 Cr1 P2 146.9(2) . . ? C3 Cr1 P2 110.35(19) . . ? C5 Cr1 P2 155.0(2) . . ? C1 Cr1 P2 117.4(2) . . ? P31 Cr1 P2 44.6(5) . . ? P11 Cr1 P2 62.6(6) . . ? P21 Cr1 P2 10.4(5) . . ? P51 Cr1 P2 95.9(4) . . ? C2 Cr1 P41 149.6(5) . . ? C4 Cr1 P41 98.6(4) . . ? C3 Cr1 P41 113.0(5) . . ? C5 Cr1 P41 118.3(4) . . ? C1 Cr1 P41 155.8(4) . . ? P31 Cr1 P41 51.1(6) . . ? P11 Cr1 P41 90.7(6) . . ? P21 Cr1 P41 90.5(5) . . ? P51 Cr1 P41 51.8(6) . . ? P2 Cr1 P41 86.7(4) . . ? C2 Cr1 P4 155.1(3) . . ? C4 Cr1 P4 97.1(2) . . ? C3 Cr1 P4 117.3(3) . . ? C5 Cr1 P4 111.51(19) . . ? C1 Cr1 P4 148.0(2) . . ? P31 Cr1 P4 60.3(5) . . ? P11 Cr1 P4 87.2(5) . . ? P21 Cr1 P4 95.5(4) . . ? P51 Cr1 P4 43.7(6) . . ? P2 Cr1 P4 93.1(3) . . ? P41 Cr1 P4 9.7(6) . . ? P51 P11 P21 108.6(8) . . ? P51 P11 Cr1 65.2(5) . . ? P21 P11 Cr1 64.4(7) . . ? P51 P11 Cr2 63.9(6) . . ? P21 P11 Cr2 63.0(6) . . ? Cr1 P11 Cr2 83.2(5) . . ? P11 P21 P31 106.2(7) . . ? P11 P21 Cr2 64.4(6) . . ? P31 P21 Cr2 63.5(6) . . ? P11 P21 Cr1 62.8(6) . . ? P31 P21 Cr1 62.5(6) . . ? Cr2 P21 Cr1 83.2(4) . . ? P41 P31 P21 109.2(8) . . ? P41 P31 Cr1 66.0(7) . . ? P21 P31 Cr1 64.1(5) . . ? P41 P31 Cr2 64.6(7) . . ? P21 P31 Cr2 63.1(5) . . ? Cr1 P31 Cr2 83.7(4) . . ? P31 P41 P51 108.1(8) . . ? P31 P41 Cr2 64.1(6) . . ? P51 P41 Cr2 63.9(6) . . ? P31 P41 Cr1 63.0(6) . . ? P51 P41 Cr1 63.9(6) . . ? Cr2 P41 Cr1 82.2(5) . . ? P11 P51 P41 107.9(7) . . ? P11 P51 Cr2 64.2(7) . . ? P41 P51 Cr2 63.6(5) . . ? P11 P51 Cr1 62.7(7) . . ? P41 P51 Cr1 64.3(6) . . ? Cr2 P51 Cr1 82.2(3) . . ? P5 P1 P2 107.2(5) . . ? P5 P1 Cr1 63.4(3) . . ? P2 P1 Cr1 62.7(4) . . ? P5 P1 Cr2 63.3(3) . . ? P2 P1 Cr2 63.3(4) . . ? Cr1 P1 Cr2 81.0(3) . . ? P3 P2 P1 108.0(4) . . ? P3 P2 Cr1 64.1(4) . . ? P1 P2 Cr1 63.4(3) . . ? P3 P2 Cr2 63.5(4) . . ? P1 P2 Cr2 63.0(3) . . ? Cr1 P2 Cr2 81.2(2) . . ? P4 P3 P2 107.9(5) . . ? P4 P3 Cr2 64.0(4) . . ? P2 P3 Cr2 63.5(3) . . ? P4 P3 Cr1 63.1(4) . . ? P2 P3 Cr1 62.7(3) . . ? Cr2 P3 Cr1 80.6(3) . . ? P5 P4 P3 108.4(5) . . ? P5 P4 Cr1 63.7(4) . . ? P3 P4 Cr1 63.9(3) . . ? P5 P4 Cr2 63.1(4) . . ? P3 P4 Cr2 63.2(3) . . ? Cr1 P4 Cr2 80.6(3) . . ? P4 P5 P1 108.4(5) . . ? P4 P5 Cr2 64.3(3) . . ? P1 P5 Cr2 63.3(4) . . ? P4 P5 Cr1 63.5(3) . . ? P1 P5 Cr1 63.3(4) . . ? Cr2 P5 Cr1 81.0(2) . . ? P52 P12 P22 106.3(5) . . ? P52 P12 Cr1 62.8(3) . . ? P22 P12 Cr1 63.1(3) . . ? P52 P12 Cr2 62.7(3) . . ? P22 P12 Cr2 62.2(3) . . ? Cr1 P12 Cr2 80.3(3) . . ? P32 P22 P12 108.5(5) . . ? P32 P22 Cr2 63.9(3) . . ? P12 P22 Cr2 63.4(3) . . ? P32 P22 Cr1 64.1(3) . . ? P12 P22 Cr1 62.9(3) . . ? Cr2 P22 Cr1 80.7(2) . . ? P22 P32 P42 108.3(5) . . ? P22 P32 Cr2 63.4(3) . . ? P42 P32 Cr2 63.6(3) . . ? P22 P32 Cr1 63.8(3) . . ? P42 P32 Cr1 62.9(3) . . ? Cr2 P32 Cr1 80.4(3) . . ? P52 P42 P32 108.7(5) . . ? P52 P42 Cr1 63.6(3) . . ? P32 P42 Cr1 64.3(3) . . ? P52 P42 Cr2 63.4(3) . . ? P32 P42 Cr2 63.4(3) . . ? Cr1 P42 Cr2 80.9(2) . . ? P42 P52 P12 108.1(6) . . ? P42 P52 Cr2 63.6(3) . . ? P12 P52 Cr2 63.5(3) . . ? P42 P52 Cr1 63.3(3) . . ? P12 P52 Cr1 63.4(3) . . ? Cr2 P52 Cr1 80.8(3) . . ? C11 Cr2 C15 37.76(8) . . ? C11 Cr2 C14 62.91(8) . . ? C15 Cr2 C14 37.76(7) . . ? C11 Cr2 C13 62.79(8) . . ? C15 Cr2 C13 63.07(7) . . ? C14 Cr2 C13 37.64(8) . . ? C11 Cr2 C12 37.62(9) . . ? C15 Cr2 C12 63.20(8) . . ? C14 Cr2 C12 63.03(8) . . ? C13 Cr2 C12 37.62(9) . . ? C11 Cr2 P21 106.2(4) . . ? C15 Cr2 P21 139.9(4) . . ? C14 Cr2 P21 161.9(4) . . ? C13 Cr2 P21 125.3(4) . . ? C12 Cr2 P21 99.3(4) . . ? C11 Cr2 P31 142.2(5) . . ? C15 Cr2 P31 162.8(4) . . ? C14 Cr2 P31 125.5(4) . . ? C13 Cr2 P31 100.8(4) . . ? C12 Cr2 P31 108.4(4) . . ? P21 Cr2 P31 53.4(6) . . ? C11 Cr2 P41 161.8(4) . . ? C15 Cr2 P41 124.9(4) . . ? C14 Cr2 P41 99.6(5) . . ? C13 Cr2 P41 107.0(5) . . ? C12 Cr2 P41 140.9(5) . . ? P21 Cr2 P41 92.0(6) . . ? P31 Cr2 P41 51.3(7) . . ? C11 Cr2 P51 124.8(4) . . ? C15 Cr2 P51 98.9(3) . . ? C14 Cr2 P51 106.3(4) . . ? C13 Cr2 P51 140.4(5) . . ? C12 Cr2 P51 161.5(3) . . ? P21 Cr2 P51 91.7(5) . . ? P31 Cr2 P51 90.2(6) . . ? P41 Cr2 P51 52.5(6) . . ? C11 Cr2 P11 100.0(4) . . ? C15 Cr2 P11 106.4(5) . . ? C14 Cr2 P11 140.2(6) . . ? C13 Cr2 P11 162.3(4) . . ? C12 Cr2 P11 125.7(4) . . ? P21 Cr2 P11 52.6(7) . . ? P31 Cr2 P11 90.7(6) . . ? P41 Cr2 P11 90.7(6) . . ? P51 Cr2 P11 51.9(7) . . ? C11 Cr2 P22 119.8(2) . . ? C15 Cr2 P22 157.5(2) . . ? C14 Cr2 P22 144.7(2) . . ? C13 Cr2 P22 108.9(2) . . ? C12 Cr2 P22 97.23(17) . . ? P21 Cr2 P22 26.3(5) . . ? P31 Cr2 P22 29.4(6) . . ? P41 Cr2 P22 77.1(5) . . ? P51 Cr2 P22 99.2(3) . . ? P11 Cr2 P22 75.1(6) . . ? C11 Cr2 P5 118.3(2) . . ? C15 Cr2 P5 96.96(19) . . ? C14 Cr2 P5 110.5(3) . . ? C13 Cr2 P5 146.8(3) . . ? C12 Cr2 P5 155.9(2) . . ? P21 Cr2 P5 87.3(4) . . ? P31 Cr2 P5 94.3(5) . . ? P41 Cr2 P5 61.1(5) . . ? P51 Cr2 P5 9.5(7) . . ? P11 Cr2 P5 43.4(5) . . ? P22 Cr2 P5 98.7(3) . . ? C12 C11 C15 108.70(18) . . ? C12 C11 C16 125.7(2) . . ? C15 C11 C16 125.5(2) . . ? C12 C11 Cr2 71.60(12) . . ? C15 C11 Cr2 71.32(12) . . ? C16 C11 Cr2 125.37(15) . . ? C11 C12 C13 107.54(18) . . ? C11 C12 C17 126.3(2) . . ? C13 C12 C17 126.0(2) . . ? C11 C12 Cr2 70.78(12) . . ? C13 C12 Cr2 71.11(12) . . ? C17 C12 Cr2 126.83(16) . . ? C14 C13 C12 108.28(18) . . ? C14 C13 C18 125.0(2) . . ? C12 C13 C18 126.6(2) . . ? C14 C13 Cr2 71.16(11) . . ? C12 C13 Cr2 71.27(12) . . ? C18 C13 Cr2 126.40(16) . . ? C13 C14 C15 108.03(18) . . ? C13 C14 C19 125.1(2) . . ? C15 C14 C19 126.8(2) . . ? C13 C14 Cr2 71.20(11) . . ? C15 C14 Cr2 71.01(11) . . ? C19 C14 Cr2 125.91(16) . . ? C11 C15 C14 107.45(18) . . ? C11 C15 C20 126.1(2) . . ? C14 C15 C20 126.4(2) . . ? C11 C15 Cr2 70.92(12) . . ? C14 C15 Cr2 71.24(11) . . ? C20 C15 Cr2 125.53(15) . . ? C11 C16 H16A 109.5 . . ? C11 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C11 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 C1 C2 C3 -0.4(2) . . . . ? C6 C1 C2 C3 176.1(2) . . . . ? Cr1 C1 C2 C3 -62.15(14) . . . . ? C5 C1 C2 C7 -177.2(2) . . . . ? C6 C1 C2 C7 -0.7(3) . . . . ? Cr1 C1 C2 C7 121.1(2) . . . . ? C5 C1 C2 Cr1 61.75(14) . . . . ? C6 C1 C2 Cr1 -121.7(2) . . . . ? C1 C2 C3 C4 0.5(2) . . . . ? C7 C2 C3 C4 177.2(2) . . . . ? Cr1 C2 C3 C4 -61.88(15) . . . . ? C1 C2 C3 C8 -177.1(2) . . . . ? C7 C2 C3 C8 -0.4(4) . . . . ? Cr1 C2 C3 C8 120.5(2) . . . . ? C1 C2 C3 Cr1 62.35(14) . . . . ? C7 C2 C3 Cr1 -120.9(2) . . . . ? C2 C3 C4 C5 -0.4(2) . . . . ? C8 C3 C4 C5 177.2(2) . . . . ? Cr1 C3 C4 C5 -62.16(15) . . . . ? C2 C3 C4 C9 -176.8(2) . . . . ? C8 C3 C4 C9 0.8(4) . . . . ? Cr1 C3 C4 C9 121.4(2) . . . . ? C2 C3 C4 Cr1 61.80(14) . . . . ? C8 C3 C4 Cr1 -120.6(2) . . . . ? C2 C1 C5 C4 0.2(2) . . . . ? C6 C1 C5 C4 -176.3(2) . . . . ? Cr1 C1 C5 C4 61.76(15) . . . . ? C2 C1 C5 C10 175.6(2) . . . . ? C6 C1 C5 C10 -0.9(4) . . . . ? Cr1 C1 C5 C10 -122.8(2) . . . . ? C2 C1 C5 Cr1 -61.59(14) . . . . ? C6 C1 C5 Cr1 121.9(2) . . . . ? C3 C4 C5 C1 0.1(2) . . . . ? C9 C4 C5 C1 176.7(2) . . . . ? Cr1 C4 C5 C1 -62.00(14) . . . . ? C3 C4 C5 C10 -175.3(2) . . . . ? C9 C4 C5 C10 1.2(4) . . . . ? Cr1 C4 C5 C10 122.5(2) . . . . ? C3 C4 C5 Cr1 62.11(15) . . . . ? C9 C4 C5 Cr1 -121.3(2) . . . . ? C1 C2 Cr1 C4 -80.02(13) . . . . ? C3 C2 Cr1 C4 37.57(12) . . . . ? C7 C2 Cr1 C4 159.2(2) . . . . ? C1 C2 Cr1 C3 -117.58(18) . . . . ? C7 C2 Cr1 C3 121.7(3) . . . . ? C1 C2 Cr1 C5 -37.49(12) . . . . ? C3 C2 Cr1 C5 80.10(13) . . . . ? C7 C2 Cr1 C5 -158.2(2) . . . . ? C3 C2 Cr1 C1 117.58(18) . . . . ? C7 C2 Cr1 C1 -120.7(3) . . . . ? C1 C2 Cr1 P31 170.5(5) . . . . ? C3 C2 Cr1 P31 -71.9(5) . . . . ? C7 C2 Cr1 P31 49.7(6) . . . . ? C1 C2 Cr1 P11 65.0(6) . . . . ? C3 C2 Cr1 P11 -177.4(6) . . . . ? C7 C2 Cr1 P11 -55.8(7) . . . . ? C1 C2 Cr1 P21 117.0(4) . . . . ? C3 C2 Cr1 P21 -125.4(4) . . . . ? C7 C2 Cr1 P21 -3.7(5) . . . . ? C1 C2 Cr1 P51 6.8(11) . . . . ? C3 C2 Cr1 P51 124.4(11) . . . . ? C7 C2 Cr1 P51 -113.9(11) . . . . ? C1 C2 Cr1 P2 127.4(3) . . . . ? C3 C2 Cr1 P2 -115.0(3) . . . . ? C7 C2 Cr1 P2 6.7(3) . . . . ? C1 C2 Cr1 P41 -137.9(7) . . . . ? C3 C2 Cr1 P41 -20.3(7) . . . . ? C7 C2 Cr1 P41 101.4(7) . . . . ? C1 C2 Cr1 P4 -120.5(5) . . . . ? C3 C2 Cr1 P4 -2.9(5) . . . . ? C7 C2 Cr1 P4 118.8(5) . . . . ? C5 C4 Cr1 C2 79.74(13) . . . . ? C3 C4 Cr1 C2 -37.64(13) . . . . ? C9 C4 Cr1 C2 -159.8(3) . . . . ? C5 C4 Cr1 C3 117.38(19) . . . . ? C9 C4 Cr1 C3 -122.2(3) . . . . ? C3 C4 Cr1 C5 -117.38(19) . . . . ? C9 C4 Cr1 C5 120.5(3) . . . . ? C5 C4 Cr1 C1 37.26(12) . . . . ? C3 C4 Cr1 C1 -80.12(14) . . . . ? C9 C4 Cr1 C1 157.7(3) . . . . ? C5 C4 Cr1 P31 -176.4(6) . . . . ? C3 C4 Cr1 P31 66.2(6) . . . . ? C9 C4 Cr1 P31 -56.0(6) . . . . ? C5 C4 Cr1 P11 -19.8(9) . . . . ? C3 C4 Cr1 P11 -137.2(9) . . . . ? C9 C4 Cr1 P11 100.7(9) . . . . ? C5 C4 Cr1 P21 123.5(9) . . . . ? C3 C4 Cr1 P21 6.1(10) . . . . ? C9 C4 Cr1 P21 -116.0(9) . . . . ? C5 C4 Cr1 P51 -73.8(5) . . . . ? C3 C4 Cr1 P51 168.8(5) . . . . ? C9 C4 Cr1 P51 46.6(6) . . . . ? C5 C4 Cr1 P2 136.8(5) . . . . ? C3 C4 Cr1 P2 19.4(5) . . . . ? C9 C4 Cr1 P2 -102.8(5) . . . . ? C5 C4 Cr1 P41 -125.9(5) . . . . ? C3 C4 Cr1 P41 116.7(5) . . . . ? C9 C4 Cr1 P41 -5.5(5) . . . . ? C5 C4 Cr1 P4 -116.2(3) . . . . ? C3 C4 Cr1 P4 126.4(3) . . . . ? C9 C4 Cr1 P4 4.2(3) . . . . ? C4 C3 Cr1 C2 117.34(18) . . . . ? C8 C3 Cr1 C2 -121.7(3) . . . . ? C2 C3 Cr1 C4 -117.34(18) . . . . ? C8 C3 Cr1 C4 121.0(3) . . . . ? C4 C3 Cr1 C5 37.55(13) . . . . ? C2 C3 Cr1 C5 -79.79(13) . . . . ? C8 C3 Cr1 C5 158.5(3) . . . . ? C4 C3 Cr1 C1 79.94(14) . . . . ? C2 C3 Cr1 C1 -37.40(12) . . . . ? C8 C3 Cr1 C1 -159.1(3) . . . . ? C4 C3 Cr1 P31 -124.5(5) . . . . ? C2 C3 Cr1 P31 118.1(5) . . . . ? C8 C3 Cr1 P31 -3.6(6) . . . . ? C4 C3 Cr1 P11 122.8(13) . . . . ? C2 C3 Cr1 P11 5.5(13) . . . . ? C8 C3 Cr1 P11 -116.2(13) . . . . ? C4 C3 Cr1 P21 -177.1(5) . . . . ? C2 C3 Cr1 P21 65.6(5) . . . . ? C8 C3 Cr1 P21 -56.2(5) . . . . ? C4 C3 Cr1 P51 -20.7(8) . . . . ? C2 C3 Cr1 P51 -138.1(8) . . . . ? C8 C3 Cr1 P51 100.2(8) . . . . ? C4 C3 Cr1 P2 -168.9(3) . . . . ? C2 C3 Cr1 P2 73.8(3) . . . . ? C8 C3 Cr1 P2 -47.9(4) . . . . ? C4 C3 Cr1 P41 -73.6(4) . . . . ? C2 C3 Cr1 P41 169.0(4) . . . . ? C8 C3 Cr1 P41 47.3(5) . . . . ? C4 C3 Cr1 P4 -64.0(3) . . . . ? C2 C3 Cr1 P4 178.6(2) . . . . ? C8 C3 Cr1 P4 56.9(3) . . . . ? C1 C5 Cr1 C2 37.56(12) . . . . ? C4 C5 Cr1 C2 -80.24(14) . . . . ? C10 C5 Cr1 C2 159.2(2) . . . . ? C1 C5 Cr1 C4 117.80(18) . . . . ? C10 C5 Cr1 C4 -120.6(3) . . . . ? C1 C5 Cr1 C3 80.23(13) . . . . ? C4 C5 Cr1 C3 -37.58(13) . . . . ? C10 C5 Cr1 C3 -158.1(2) . . . . ? C4 C5 Cr1 C1 -117.80(18) . . . . ? C10 C5 Cr1 C1 121.6(3) . . . . ? C1 C5 Cr1 P31 125.2(11) . . . . ? C4 C5 Cr1 P31 7.4(11) . . . . ? C10 C5 Cr1 P31 -113.1(11) . . . . ? C1 C5 Cr1 P11 -73.1(5) . . . . ? C4 C5 Cr1 P11 169.1(5) . . . . ? C10 C5 Cr1 P11 48.6(6) . . . . ? C1 C5 Cr1 P21 -19.0(7) . . . . ? C4 C5 Cr1 P21 -136.8(7) . . . . ? C10 C5 Cr1 P21 102.6(7) . . . . ? C1 C5 Cr1 P51 -125.6(5) . . . . ? C4 C5 Cr1 P51 116.6(5) . . . . ? C10 C5 Cr1 P51 -3.9(6) . . . . ? C1 C5 Cr1 P2 -0.2(5) . . . . ? C4 C5 Cr1 P2 -118.0(5) . . . . ? C10 C5 Cr1 P2 121.5(5) . . . . ? C1 C5 Cr1 P41 -176.8(6) . . . . ? C4 C5 Cr1 P41 65.4(6) . . . . ? C10 C5 Cr1 P41 -55.2(6) . . . . ? C1 C5 Cr1 P4 -169.1(3) . . . . ? C4 C5 Cr1 P4 73.1(3) . . . . ? C10 C5 Cr1 P4 -47.5(4) . . . . ? C5 C1 Cr1 C2 -117.40(18) . . . . ? C6 C1 Cr1 C2 120.8(2) . . . . ? C5 C1 Cr1 C4 -37.36(12) . . . . ? C2 C1 Cr1 C4 80.04(14) . . . . ? C6 C1 Cr1 C4 -159.1(2) . . . . ? C5 C1 Cr1 C3 -79.88(13) . . . . ? C2 C1 Cr1 C3 37.53(13) . . . . ? C6 C1 Cr1 C3 158.3(2) . . . . ? C2 C1 Cr1 C5 117.40(18) . . . . ? C6 C1 Cr1 C5 -121.8(2) . . . . ? C5 C1 Cr1 P31 -135.1(9) . . . . ? C2 C1 Cr1 P31 -17.7(9) . . . . ? C6 C1 Cr1 P31 103.1(9) . . . . ? C5 C1 Cr1 P11 116.8(6) . . . . ? C2 C1 Cr1 P11 -125.8(6) . . . . ? C6 C1 Cr1 P11 -5.0(6) . . . . ? C5 C1 Cr1 P21 169.6(4) . . . . ? C2 C1 Cr1 P21 -73.0(4) . . . . ? C6 C1 Cr1 P21 47.8(4) . . . . ? C5 C1 Cr1 P51 65.8(6) . . . . ? C2 C1 Cr1 P51 -176.8(6) . . . . ? C6 C1 Cr1 P51 -56.0(6) . . . . ? C5 C1 Cr1 P2 179.9(3) . . . . ? C2 C1 Cr1 P2 -62.7(3) . . . . ? C6 C1 Cr1 P2 58.1(3) . . . . ? C5 C1 Cr1 P41 6.9(12) . . . . ? C2 C1 Cr1 P41 124.3(12) . . . . ? C6 C1 Cr1 P41 -114.9(12) . . . . ? C5 C1 Cr1 P4 19.3(5) . . . . ? C2 C1 Cr1 P4 136.7(5) . . . . ? C6 C1 Cr1 P4 -102.4(6) . . . . ? C2 Cr1 P11 P51 -153.8(5) . . . . ? C4 Cr1 P11 P51 -70.7(10) . . . . ? C3 Cr1 P11 P51 -157.6(10) . . . . ? C5 Cr1 P11 P51 -83.7(6) . . . . ? C1 Cr1 P11 P51 -119.8(5) . . . . ? P31 Cr1 P11 P51 88.5(7) . . . . ? P21 Cr1 P11 P51 127.6(8) . . . . ? P2 Cr1 P11 P51 123.4(7) . . . . ? P41 Cr1 P11 P51 37.5(6) . . . . ? P4 Cr1 P11 P51 28.5(6) . . . . ? C2 Cr1 P11 P21 78.6(6) . . . . ? C4 Cr1 P11 P21 161.7(7) . . . . ? C3 Cr1 P11 P21 74.8(13) . . . . ? C5 Cr1 P11 P21 148.7(5) . . . . ? C1 Cr1 P11 P21 112.6(5) . . . . ? P31 Cr1 P11 P21 -39.1(7) . . . . ? P51 Cr1 P11 P21 -127.6(8) . . . . ? P2 Cr1 P11 P21 -4.2(6) . . . . ? P41 Cr1 P11 P21 -90.1(6) . . . . ? P4 Cr1 P11 P21 -99.1(5) . . . . ? C2 Cr1 P11 Cr2 141.8(3) . . . . ? C4 Cr1 P11 Cr2 -135.1(5) . . . . ? C3 Cr1 P11 Cr2 138.0(8) . . . . ? C5 Cr1 P11 Cr2 -148.0(3) . . . . ? C1 Cr1 P11 Cr2 175.8(4) . . . . ? P31 Cr1 P11 Cr2 24.2(7) . . . . ? P21 Cr1 P11 Cr2 63.2(6) . . . . ? P51 Cr1 P11 Cr2 -64.4(6) . . . . ? P2 Cr1 P11 Cr2 59.0(5) . . . . ? P41 Cr1 P11 Cr2 -26.9(6) . . . . ? P4 Cr1 P11 Cr2 -35.9(5) . . . . ? P51 P11 P21 P31 -2.9(13) . . . . ? Cr1 P11 P21 P31 46.5(8) . . . . ? Cr2 P11 P21 P31 -49.1(7) . . . . ? P51 P11 P21 Cr2 46.2(8) . . . . ? Cr1 P11 P21 Cr2 95.6(4) . . . . ? P51 P11 P21 Cr1 -49.4(8) . . . . ? Cr2 P11 P21 Cr1 -95.6(4) . . . . ? C2 Cr1 P21 P11 -118.7(6) . . . . ? C4 Cr1 P21 P11 -157.2(9) . . . . ? C3 Cr1 P21 P11 -153.0(6) . . . . ? C5 Cr1 P21 P11 -70.0(8) . . . . ? C1 Cr1 P21 P11 -82.5(6) . . . . ? P31 Cr1 P21 P11 128.3(8) . . . . ? P51 Cr1 P21 P11 38.7(7) . . . . ? P2 Cr1 P21 P11 159(3) . . . . ? P41 Cr1 P21 P11 90.5(7) . . . . ? P4 Cr1 P21 P11 82.2(6) . . . . ? C2 Cr1 P21 P31 113.0(6) . . . . ? C4 Cr1 P21 P31 74.5(10) . . . . ? C3 Cr1 P21 P31 78.7(6) . . . . ? C5 Cr1 P21 P31 161.7(7) . . . . ? C1 Cr1 P21 P31 149.2(6) . . . . ? P11 Cr1 P21 P31 -128.3(8) . . . . ? P51 Cr1 P21 P31 -89.6(7) . . . . ? P2 Cr1 P21 P31 31(3) . . . . ? P41 Cr1 P21 P31 -37.8(7) . . . . ? P4 Cr1 P21 P31 -46.1(6) . . . . ? C2 Cr1 P21 Cr2 176.6(3) . . . . ? C4 Cr1 P21 Cr2 138.1(6) . . . . ? C3 Cr1 P21 Cr2 142.3(2) . . . . ? C5 Cr1 P21 Cr2 -134.7(4) . . . . ? C1 Cr1 P21 Cr2 -147.2(2) . . . . ? P31 Cr1 P21 Cr2 63.6(6) . . . . ? P11 Cr1 P21 Cr2 -64.7(6) . . . . ? P51 Cr1 P21 Cr2 -26.0(6) . . . . ? P2 Cr1 P21 Cr2 94(3) . . . . ? P41 Cr1 P21 Cr2 25.8(6) . . . . ? P4 Cr1 P21 Cr2 17.5(5) . . . . ? P11 P21 P31 P41 3.0(13) . . . . ? Cr2 P21 P31 P41 -46.7(8) . . . . ? Cr1 P21 P31 P41 49.6(8) . . . . ? P11 P21 P31 Cr1 -46.6(8) . . . . ? Cr2 P21 P31 Cr1 -96.3(4) . . . . ? P11 P21 P31 Cr2 49.6(8) . . . . ? Cr1 P21 P31 Cr2 96.3(4) . . . . ? C2 Cr1 P31 P41 149.3(6) . . . . ? C4 Cr1 P31 P41 78.9(7) . . . . ? C3 Cr1 P31 P41 113.3(6) . . . . ? C5 Cr1 P31 P41 73.8(12) . . . . ? C1 Cr1 P31 P41 161.0(8) . . . . ? P11 Cr1 P31 P41 -89.3(8) . . . . ? P21 Cr1 P31 P41 -128.1(8) . . . . ? P51 Cr1 P31 P41 -37.3(8) . . . . ? P2 Cr1 P31 P41 -135.6(9) . . . . ? P4 Cr1 P31 P41 -3.7(8) . . . . ? C2 Cr1 P31 P21 -82.6(5) . . . . ? C4 Cr1 P31 P21 -153.1(4) . . . . ? C3 Cr1 P31 P21 -118.7(5) . . . . ? C5 Cr1 P31 P21 -158.2(8) . . . . ? C1 Cr1 P31 P21 -70.9(9) . . . . ? P11 Cr1 P31 P21 38.7(7) . . . . ? P51 Cr1 P31 P21 90.8(7) . . . . ? P2 Cr1 P31 P21 -7.6(6) . . . . ? P41 Cr1 P31 P21 128.1(8) . . . . ? P4 Cr1 P31 P21 124.3(6) . . . . ? C2 Cr1 P31 Cr2 -145.7(3) . . . . ? C4 Cr1 P31 Cr2 143.8(3) . . . . ? C3 Cr1 P31 Cr2 178.3(4) . . . . ? C5 Cr1 P31 Cr2 138.8(7) . . . . ? C1 Cr1 P31 Cr2 -134.0(5) . . . . ? P11 Cr1 P31 Cr2 -24.4(7) . . . . ? P21 Cr1 P31 Cr2 -63.1(5) . . . . ? P51 Cr1 P31 Cr2 27.7(7) . . . . ? P2 Cr1 P31 Cr2 -70.7(5) . . . . ? P41 Cr1 P31 Cr2 65.0(7) . . . . ? P4 Cr1 P31 Cr2 61.2(5) . . . . ? P21 P31 P41 P51 -1.9(13) . . . . ? Cr1 P31 P41 P51 46.7(8) . . . . ? Cr2 P31 P41 P51 -47.8(8) . . . . ? P21 P31 P41 Cr2 45.9(8) . . . . ? Cr1 P31 P41 Cr2 94.5(5) . . . . ? P21 P31 P41 Cr1 -48.6(8) . . . . ? Cr2 P31 P41 Cr1 -94.5(5) . . . . ? C2 Cr1 P41 P31 -67.9(9) . . . . ? C4 Cr1 P41 P31 -117.7(6) . . . . ? C3 Cr1 P41 P31 -81.3(6) . . . . ? C5 Cr1 P41 P31 -152.0(5) . . . . ? C1 Cr1 P41 P31 -156.7(9) . . . . ? P11 Cr1 P41 P31 92.0(8) . . . . ? P21 Cr1 P41 P31 39.2(7) . . . . ? P51 Cr1 P41 P31 129.6(9) . . . . ? P2 Cr1 P41 P31 29.5(6) . . . . ? P4 Cr1 P41 P31 160(4) . . . . ? C2 Cr1 P41 P51 162.5(6) . . . . ? C4 Cr1 P41 P51 112.7(5) . . . . ? C3 Cr1 P41 P51 149.1(5) . . . . ? C5 Cr1 P41 P51 78.4(6) . . . . ? C1 Cr1 P41 P51 73.7(12) . . . . ? P31 Cr1 P41 P51 -129.6(9) . . . . ? P11 Cr1 P41 P51 -37.6(8) . . . . ? P21 Cr1 P41 P51 -90.4(6) . . . . ? P2 Cr1 P41 P51 -100.1(6) . . . . ? P4 Cr1 P41 P51 31(3) . . . . ? C2 Cr1 P41 Cr2 -132.8(5) . . . . ? C4 Cr1 P41 Cr2 177.4(3) . . . . ? C3 Cr1 P41 Cr2 -146.2(3) . . . . ? C5 Cr1 P41 Cr2 143.2(2) . . . . ? C1 Cr1 P41 Cr2 138.4(8) . . . . ? P31 Cr1 P41 Cr2 -64.9(6) . . . . ? P11 Cr1 P41 Cr2 27.1(7) . . . . ? P21 Cr1 P41 Cr2 -25.7(5) . . . . ? P51 Cr1 P41 Cr2 64.7(6) . . . . ? P2 Cr1 P41 Cr2 -35.4(4) . . . . ? P4 Cr1 P41 Cr2 96(4) . . . . ? P21 P11 P51 P41 1.8(13) . . . . ? Cr1 P11 P51 P41 -47.1(8) . . . . ? Cr2 P11 P51 P41 47.5(8) . . . . ? P21 P11 P51 Cr2 -45.7(8) . . . . ? Cr1 P11 P51 Cr2 -94.7(5) . . . . ? P21 P11 P51 Cr1 48.9(8) . . . . ? Cr2 P11 P51 Cr1 94.7(5) . . . . ? P31 P41 P51 P11 0.1(13) . . . . ? Cr2 P41 P51 P11 -47.8(8) . . . . ? Cr1 P41 P51 P11 46.3(8) . . . . ? P31 P41 P51 Cr2 47.9(8) . . . . ? Cr1 P41 P51 Cr2 94.1(4) . . . . ? P31 P41 P51 Cr1 -46.2(8) . . . . ? Cr2 P41 P51 Cr1 -94.1(4) . . . . ? C2 Cr1 P51 P11 72.5(12) . . . . ? C4 Cr1 P51 P11 148.1(6) . . . . ? C3 Cr1 P51 P11 161.7(8) . . . . ? C5 Cr1 P51 P11 111.6(6) . . . . ? C1 Cr1 P51 P11 77.3(7) . . . . ? P31 Cr1 P51 P11 -92.5(8) . . . . ? P21 Cr1 P51 P11 -39.1(7) . . . . ? P2 Cr1 P51 P11 -48.2(7) . . . . ? P41 Cr1 P51 P11 -129.3(8) . . . . ? P4 Cr1 P51 P11 -136.4(8) . . . . ? C2 Cr1 P51 P41 -158.2(9) . . . . ? C4 Cr1 P51 P41 -82.7(5) . . . . ? C3 Cr1 P51 P41 -69.0(8) . . . . ? C5 Cr1 P51 P41 -119.1(5) . . . . ? C1 Cr1 P51 P41 -153.4(5) . . . . ? P31 Cr1 P51 P41 36.8(7) . . . . ? P11 Cr1 P51 P41 129.3(8) . . . . ? P21 Cr1 P51 P41 90.2(7) . . . . ? P2 Cr1 P51 P41 81.1(6) . . . . ? P4 Cr1 P51 P41 -7.2(7) . . . . ? C2 Cr1 P51 Cr2 137.4(7) . . . . ? C4 Cr1 P51 Cr2 -147.1(3) . . . . ? C3 Cr1 P51 Cr2 -133.4(4) . . . . ? C5 Cr1 P51 Cr2 176.5(4) . . . . ? C1 Cr1 P51 Cr2 142.2(3) . . . . ? P31 Cr1 P51 Cr2 -27.6(7) . . . . ? P11 Cr1 P51 Cr2 64.9(7) . . . . ? P21 Cr1 P51 Cr2 25.8(6) . . . . ? P2 Cr1 P51 Cr2 16.7(6) . . . . ? P41 Cr1 P51 Cr2 -64.4(6) . . . . ? P4 Cr1 P51 Cr2 -71.6(5) . . . . ? C2 Cr1 P1 P5 -148.4(3) . . . . ? C4 Cr1 P1 P5 -76.9(6) . . . . ? C3 Cr1 P1 P5 -161.4(4) . . . . ? C5 Cr1 P1 P5 -78.8(3) . . . . ? C1 Cr1 P1 P5 -112.2(3) . . . . ? P31 Cr1 P1 P5 97.5(6) . . . . ? P11 Cr1 P1 P5 -18(4) . . . . ? P21 Cr1 P1 P5 132.3(7) . . . . ? P51 Cr1 P1 P5 6.2(6) . . . . ? P2 Cr1 P1 P5 129.1(4) . . . . ? P41 Cr1 P1 P5 47.0(5) . . . . ? P4 Cr1 P1 P5 37.5(3) . . . . ? C2 Cr1 P1 P2 82.5(3) . . . . ? C4 Cr1 P1 P2 154.0(5) . . . . ? C3 Cr1 P1 P2 69.5(6) . . . . ? C5 Cr1 P1 P2 152.1(3) . . . . ? C1 Cr1 P1 P2 118.7(3) . . . . ? P31 Cr1 P1 P2 -31.6(6) . . . . ? P11 Cr1 P1 P2 -147(4) . . . . ? P21 Cr1 P1 P2 3.2(7) . . . . ? P51 Cr1 P1 P2 -123.0(6) . . . . ? P41 Cr1 P1 P2 -82.1(5) . . . . ? P4 Cr1 P1 P2 -91.6(3) . . . . ? C2 Cr1 P1 Cr2 147.01(17) . . . . ? C4 Cr1 P1 Cr2 -141.5(4) . . . . ? C3 Cr1 P1 Cr2 134.0(3) . . . . ? C5 Cr1 P1 Cr2 -143.34(17) . . . . ? C1 Cr1 P1 Cr2 -176.7(2) . . . . ? P31 Cr1 P1 Cr2 32.9(5) . . . . ? P11 Cr1 P1 Cr2 -82(4) . . . . ? P21 Cr1 P1 Cr2 67.8(5) . . . . ? P51 Cr1 P1 Cr2 -58.4(4) . . . . ? P2 Cr1 P1 Cr2 64.5(3) . . . . ? P41 Cr1 P1 Cr2 -17.6(5) . . . . ? P4 Cr1 P1 Cr2 -27.1(3) . . . . ? P5 P1 P2 P3 0.8(7) . . . . ? Cr1 P1 P2 P3 47.4(4) . . . . ? Cr2 P1 P2 P3 -46.2(4) . . . . ? P5 P1 P2 Cr1 -46.6(4) . . . . ? Cr2 P1 P2 Cr1 -93.6(2) . . . . ? P5 P1 P2 Cr2 47.0(4) . . . . ? Cr1 P1 P2 Cr2 93.6(2) . . . . ? C2 Cr1 P2 P3 119.6(4) . . . . ? C4 Cr1 P2 P3 70.7(5) . . . . ? C3 Cr1 P2 P3 83.2(4) . . . . ? C5 Cr1 P2 P3 152.8(5) . . . . ? C1 Cr1 P2 P3 152.7(3) . . . . ? P31 Cr1 P2 P3 2.9(9) . . . . ? P11 Cr1 P2 P3 -122.6(7) . . . . ? P21 Cr1 P2 P3 -141(3) . . . . ? P51 Cr1 P2 P3 -81.2(6) . . . . ? P41 Cr1 P2 P3 -30.1(6) . . . . ? P4 Cr1 P2 P3 -37.4(4) . . . . ? C2 Cr1 P2 P1 -111.5(3) . . . . ? C4 Cr1 P2 P1 -160.4(4) . . . . ? C3 Cr1 P2 P1 -147.9(3) . . . . ? C5 Cr1 P2 P1 -78.2(5) . . . . ? C1 Cr1 P2 P1 -78.4(3) . . . . ? P31 Cr1 P2 P1 131.8(7) . . . . ? P11 Cr1 P2 P1 6.3(7) . . . . ? P21 Cr1 P2 P1 -12(3) . . . . ? P51 Cr1 P2 P1 47.7(6) . . . . ? P41 Cr1 P2 P1 98.8(6) . . . . ? P4 Cr1 P2 P1 91.5(4) . . . . ? C2 Cr1 P2 Cr2 -175.67(19) . . . . ? C4 Cr1 P2 Cr2 135.5(2) . . . . ? C3 Cr1 P2 Cr2 147.98(15) . . . . ? C5 Cr1 P2 Cr2 -142.4(3) . . . . ? C1 Cr1 P2 Cr2 -142.52(15) . . . . ? P31 Cr1 P2 Cr2 67.7(6) . . . . ? P11 Cr1 P2 Cr2 -57.9(5) . . . . ? P21 Cr1 P2 Cr2 -77(3) . . . . ? P51 Cr1 P2 Cr2 -16.4(5) . . . . ? P41 Cr1 P2 Cr2 34.6(5) . . . . ? P4 Cr1 P2 Cr2 27.3(3) . . . . ? P1 P2 P3 P4 -1.6(7) . . . . ? Cr1 P2 P3 P4 45.5(4) . . . . ? Cr2 P2 P3 P4 -47.5(4) . . . . ? P1 P2 P3 Cr2 45.9(4) . . . . ? Cr1 P2 P3 Cr2 93.0(2) . . . . ? P1 P2 P3 Cr1 -47.0(4) . . . . ? Cr2 P2 P3 Cr1 -93.0(2) . . . . ? C2 Cr1 P3 P4 152.7(3) . . . . ? C4 Cr1 P3 P4 83.0(4) . . . . ? C3 Cr1 P3 P4 119.2(4) . . . . ? C5 Cr1 P3 P4 70.6(6) . . . . ? C1 Cr1 P3 P4 154.0(5) . . . . ? P31 Cr1 P3 P4 -144(4) . . . . ? P11 Cr1 P3 P4 -81.8(6) . . . . ? P21 Cr1 P3 P4 -123.1(6) . . . . ? P51 Cr1 P3 P4 -30.5(6) . . . . ? P2 Cr1 P3 P4 -130.5(5) . . . . ? P41 Cr1 P3 P4 2.8(9) . . . . ? C2 Cr1 P3 P2 -76.8(3) . . . . ? C4 Cr1 P3 P2 -146.5(2) . . . . ? C3 Cr1 P3 P2 -110.3(3) . . . . ? C5 Cr1 P3 P2 -158.9(3) . . . . ? C1 Cr1 P3 P2 -75.5(6) . . . . ? P31 Cr1 P3 P2 -13(4) . . . . ? P11 Cr1 P3 P2 48.8(6) . . . . ? P21 Cr1 P3 P2 7.4(5) . . . . ? P51 Cr1 P3 P2 100.0(5) . . . . ? P41 Cr1 P3 P2 133.3(7) . . . . ? P4 Cr1 P3 P2 130.5(5) . . . . ? C2 Cr1 P3 Cr2 -141.74(17) . . . . ? C4 Cr1 P3 Cr2 148.53(18) . . . . ? C3 Cr1 P3 Cr2 -175.2(2) . . . . ? C5 Cr1 P3 Cr2 136.2(3) . . . . ? C1 Cr1 P3 Cr2 -140.4(4) . . . . ? P31 Cr1 P3 Cr2 -78(4) . . . . ? P11 Cr1 P3 Cr2 -16.2(6) . . . . ? P21 Cr1 P3 Cr2 -57.5(4) . . . . ? P51 Cr1 P3 Cr2 35.1(5) . . . . ? P2 Cr1 P3 Cr2 -64.9(3) . . . . ? P41 Cr1 P3 Cr2 68.4(7) . . . . ? P4 Cr1 P3 Cr2 65.6(4) . . . . ? P2 P3 P4 P5 1.7(7) . . . . ? Cr2 P3 P4 P5 -45.5(4) . . . . ? Cr1 P3 P4 P5 47.0(4) . . . . ? P2 P3 P4 Cr1 -45.2(4) . . . . ? Cr2 P3 P4 Cr1 -92.4(3) . . . . ? P2 P3 P4 Cr2 47.2(4) . . . . ? Cr1 P3 P4 Cr2 92.4(3) . . . . ? C2 Cr1 P4 P5 155.4(4) . . . . ? C4 Cr1 P4 P5 119.7(3) . . . . ? C3 Cr1 P4 P5 153.4(3) . . . . ? C5 Cr1 P4 P5 83.6(4) . . . . ? C1 Cr1 P4 P5 71.0(6) . . . . ? P31 Cr1 P4 P5 -123.3(6) . . . . ? P11 Cr1 P4 P5 -29.4(6) . . . . ? P21 Cr1 P4 P5 -81.6(5) . . . . ? P51 Cr1 P4 P5 3.5(7) . . . . ? P2 Cr1 P4 P5 -91.8(4) . . . . ? P41 Cr1 P4 P5 -141(4) . . . . ? C2 Cr1 P4 P3 -75.3(5) . . . . ? C4 Cr1 P4 P3 -111.0(4) . . . . ? C3 Cr1 P4 P3 -77.3(4) . . . . ? C5 Cr1 P4 P3 -147.1(3) . . . . ? C1 Cr1 P4 P3 -159.7(4) . . . . ? P31 Cr1 P4 P3 6.0(7) . . . . ? P11 Cr1 P4 P3 99.9(6) . . . . ? P21 Cr1 P4 P3 47.7(5) . . . . ? P51 Cr1 P4 P3 132.9(7) . . . . ? P2 Cr1 P4 P3 37.6(4) . . . . ? P41 Cr1 P4 P3 -11(4) . . . . ? C2 Cr1 P4 Cr2 -140.0(3) . . . . ? C4 Cr1 P4 Cr2 -175.67(19) . . . . ? C3 Cr1 P4 Cr2 -141.98(16) . . . . ? C5 Cr1 P4 Cr2 148.19(13) . . . . ? C1 Cr1 P4 Cr2 135.6(3) . . . . ? P31 Cr1 P4 Cr2 -58.7(5) . . . . ? P11 Cr1 P4 Cr2 35.2(6) . . . . ? P21 Cr1 P4 Cr2 -17.0(4) . . . . ? P51 Cr1 P4 Cr2 68.1(6) . . . . ? P2 Cr1 P4 Cr2 -27.2(3) . . . . ? P41 Cr1 P4 Cr2 -76(4) . . . . ? P3 P4 P5 P1 -1.2(7) . . . . ? Cr1 P4 P5 P1 45.9(4) . . . . ? Cr2 P4 P5 P1 -46.7(4) . . . . ? P3 P4 P5 Cr2 45.5(4) . . . . ? Cr1 P4 P5 Cr2 92.6(2) . . . . ? P3 P4 P5 Cr1 -47.1(5) . . . . ? Cr2 P4 P5 Cr1 -92.6(2) . . . . ? P2 P1 P5 P4 0.3(7) . . . . ? Cr1 P1 P5 P4 -46.0(4) . . . . ? Cr2 P1 P5 P4 47.2(4) . . . . ? P2 P1 P5 Cr2 -47.0(4) . . . . ? Cr1 P1 P5 Cr2 -93.2(3) . . . . ? P2 P1 P5 Cr1 46.2(4) . . . . ? Cr2 P1 P5 Cr1 93.2(3) . . . . ? C2 Cr1 P5 P4 -160.4(4) . . . . ? C4 Cr1 P5 P4 -77.1(3) . . . . ? C3 Cr1 P5 P4 -73.9(6) . . . . ? C5 Cr1 P5 P4 -111.0(3) . . . . ? C1 Cr1 P5 P4 -147.3(3) . . . . ? P31 Cr1 P5 P4 46.7(6) . . . . ? P11 Cr1 P5 P4 134.7(8) . . . . ? P21 Cr1 P5 P4 99.5(5) . . . . ? P51 Cr1 P5 P4 -15(3) . . . . ? P2 Cr1 P5 P4 91.4(4) . . . . ? P41 Cr1 P5 P4 7.0(6) . . . . ? C2 Cr1 P5 P1 69.3(6) . . . . ? C4 Cr1 P5 P1 152.6(3) . . . . ? C3 Cr1 P5 P1 155.7(5) . . . . ? C5 Cr1 P5 P1 118.7(4) . . . . ? C1 Cr1 P5 P1 82.4(4) . . . . ? P31 Cr1 P5 P1 -83.6(6) . . . . ? P11 Cr1 P5 P1 4.4(10) . . . . ? P21 Cr1 P5 P1 -30.8(5) . . . . ? P51 Cr1 P5 P1 -145(3) . . . . ? P2 Cr1 P5 P1 -38.9(4) . . . . ? P41 Cr1 P5 P1 -123.3(6) . . . . ? P4 Cr1 P5 P1 -130.3(5) . . . . ? C2 Cr1 P5 Cr2 133.9(3) . . . . ? C4 Cr1 P5 Cr2 -142.75(16) . . . . ? C3 Cr1 P5 Cr2 -139.6(4) . . . . ? C5 Cr1 P5 Cr2 -176.7(2) . . . . ? C1 Cr1 P5 Cr2 147.01(16) . . . . ? P31 Cr1 P5 Cr2 -19.0(6) . . . . ? P11 Cr1 P5 Cr2 69.0(7) . . . . ? P21 Cr1 P5 Cr2 33.8(4) . . . . ? P51 Cr1 P5 Cr2 -81(3) . . . . ? P2 Cr1 P5 Cr2 25.7(3) . . . . ? P41 Cr1 P5 Cr2 -58.7(4) . . . . ? P4 Cr1 P5 Cr2 -65.7(3) . . . . ? C2 Cr1 P12 P52 -139.4(3) . . . . ? C4 Cr1 P12 P52 -102.1(8) . . . . ? C3 Cr1 P12 P52 -162.0(3) . . . . ? C5 Cr1 P12 P52 -73.5(3) . . . . ? C1 Cr1 P12 P52 -101.1(3) . . . . ? P31 Cr1 P12 P52 109.2(6) . . . . ? P11 Cr1 P12 P52 -12.3(12) . . . . ? P21 Cr1 P12 P52 138.0(8) . . . . ? P51 Cr1 P12 P52 15.7(6) . . . . ? P2 Cr1 P12 P52 136.5(5) . . . . ? P41 Cr1 P12 P52 62.1(5) . . . . ? P4 Cr1 P12 P52 52.4(4) . . . . ? C2 Cr1 P12 P22 92.7(3) . . . . ? C4 Cr1 P12 P22 130.0(8) . . . . ? C3 Cr1 P12 P22 70.1(4) . . . . ? C5 Cr1 P12 P22 158.6(3) . . . . ? C1 Cr1 P12 P22 130.9(3) . . . . ? P31 Cr1 P12 P22 -18.7(6) . . . . ? P11 Cr1 P12 P22 -140.2(13) . . . . ? P21 Cr1 P12 P22 10.1(7) . . . . ? P51 Cr1 P12 P22 -112.2(5) . . . . ? P2 Cr1 P12 P22 8.6(4) . . . . ? P41 Cr1 P12 P22 -65.8(5) . . . . ? P4 Cr1 P12 P22 -75.6(4) . . . . ? C2 Cr1 P12 Cr2 156.34(18) . . . . ? C4 Cr1 P12 Cr2 -166.4(7) . . . . ? C3 Cr1 P12 Cr2 133.79(16) . . . . ? C5 Cr1 P12 Cr2 -137.75(14) . . . . ? C1 Cr1 P12 Cr2 -165.4(2) . . . . ? P31 Cr1 P12 Cr2 45.0(5) . . . . ? P11 Cr1 P12 Cr2 -76.5(12) . . . . ? P21 Cr1 P12 Cr2 73.8(7) . . . . ? P51 Cr1 P12 Cr2 -48.5(4) . . . . ? P2 Cr1 P12 Cr2 72.3(4) . . . . ? P41 Cr1 P12 Cr2 -2.1(5) . . . . ? P4 Cr1 P12 Cr2 -11.9(3) . . . . ? P52 P12 P22 P32 -0.5(6) . . . . ? Cr1 P12 P22 P32 46.5(3) . . . . ? Cr2 P12 P22 P32 -46.6(4) . . . . ? P52 P12 P22 Cr2 46.1(3) . . . . ? Cr1 P12 P22 Cr2 93.1(2) . . . . ? P52 P12 P22 Cr1 -47.0(3) . . . . ? Cr2 P12 P22 Cr1 -93.1(2) . . . . ? C2 Cr1 P22 P32 130.5(3) . . . . ? C4 Cr1 P22 P32 69.2(4) . . . . ? C3 Cr1 P22 P32 92.0(3) . . . . ? C5 Cr1 P22 P32 128.2(9) . . . . ? C1 Cr1 P22 P32 158.2(3) . . . . ? P31 Cr1 P22 P32 9.9(9) . . . . ? P11 Cr1 P22 P32 -113.3(6) . . . . ? P21 Cr1 P22 P32 -141.3(10) . . . . ? P51 Cr1 P22 P32 -66.1(6) . . . . ? P2 Cr1 P22 P32 -150.2(11) . . . . ? P41 Cr1 P22 P32 -18.7(6) . . . . ? P4 Cr1 P22 P32 -24.6(4) . . . . ? C2 Cr1 P22 P12 -99.3(3) . . . . ? C4 Cr1 P22 P12 -160.7(2) . . . . ? C3 Cr1 P22 P12 -137.8(3) . . . . ? C5 Cr1 P22 P12 -101.6(9) . . . . ? C1 Cr1 P22 P12 -71.6(3) . . . . ? P31 Cr1 P22 P12 140.1(10) . . . . ? P11 Cr1 P22 P12 16.8(6) . . . . ? P21 Cr1 P22 P12 -11.1(8) . . . . ? P51 Cr1 P22 P12 64.1(6) . . . . ? P2 Cr1 P22 P12 -20.0(8) . . . . ? P41 Cr1 P22 P12 111.5(5) . . . . ? P4 Cr1 P22 P12 105.6(4) . . . . ? C2 Cr1 P22 Cr2 -164.1(2) . . . . ? C4 Cr1 P22 Cr2 134.53(16) . . . . ? C3 Cr1 P22 Cr2 157.4(2) . . . . ? C5 Cr1 P22 Cr2 -166.4(7) . . . . ? C1 Cr1 P22 Cr2 -136.38(15) . . . . ? P31 Cr1 P22 Cr2 75.3(9) . . . . ? P11 Cr1 P22 Cr2 -48.0(5) . . . . ? P21 Cr1 P22 Cr2 -75.9(8) . . . . ? P51 Cr1 P22 Cr2 -0.7(6) . . . . ? P2 Cr1 P22 Cr2 -84.8(9) . . . . ? P41 Cr1 P22 Cr2 46.6(5) . . . . ? P4 Cr1 P22 Cr2 40.8(3) . . . . ? P12 P22 P32 P42 -0.1(6) . . . . ? Cr2 P22 P32 P42 -46.4(4) . . . . ? Cr1 P22 P32 P42 45.8(4) . . . . ? P12 P22 P32 Cr2 46.4(4) . . . . ? Cr1 P22 P32 Cr2 92.2(2) . . . . ? P12 P22 P32 Cr1 -45.8(3) . . . . ? Cr2 P22 P32 Cr1 -92.2(2) . . . . ? C2 Cr1 P32 P22 -71.0(4) . . . . ? C4 Cr1 P32 P22 -137.8(3) . . . . ? C3 Cr1 P32 P22 -99.4(3) . . . . ? C5 Cr1 P32 P22 -160.1(3) . . . . ? C1 Cr1 P32 P22 -97.6(8) . . . . ? P31 Cr1 P32 P22 -12.1(11) . . . . ? P11 Cr1 P32 P22 63.7(6) . . . . ? P21 Cr1 P32 P22 16.6(5) . . . . ? P51 Cr1 P32 P22 111.4(5) . . . . ? P2 Cr1 P32 P22 8.6(3) . . . . ? P41 Cr1 P32 P22 140.1(10) . . . . ? P4 Cr1 P32 P22 138.6(5) . . . . ? C2 Cr1 P32 P42 158.8(3) . . . . ? C4 Cr1 P32 P42 92.0(3) . . . . ? C3 Cr1 P32 P42 130.4(3) . . . . ? C5 Cr1 P32 P42 69.7(4) . . . . ? C1 Cr1 P32 P42 132.2(8) . . . . ? P31 Cr1 P32 P42 -142.3(12) . . . . ? P11 Cr1 P32 P42 -66.5(6) . . . . ? P21 Cr1 P32 P42 -113.6(5) . . . . ? P51 Cr1 P32 P42 -18.8(5) . . . . ? P2 Cr1 P32 P42 -121.6(4) . . . . ? P41 Cr1 P32 P42 9.9(10) . . . . ? P4 Cr1 P32 P42 8.4(5) . . . . ? C2 Cr1 P32 Cr2 -135.96(15) . . . . ? C4 Cr1 P32 Cr2 157.22(18) . . . . ? C3 Cr1 P32 Cr2 -164.4(2) . . . . ? C5 Cr1 P32 Cr2 134.93(17) . . . . ? C1 Cr1 P32 Cr2 -162.6(7) . . . . ? P31 Cr1 P32 Cr2 -77.1(11) . . . . ? P11 Cr1 P32 Cr2 -1.3(6) . . . . ? P21 Cr1 P32 Cr2 -48.4(4) . . . . ? P51 Cr1 P32 Cr2 46.4(5) . . . . ? P2 Cr1 P32 Cr2 -56.4(2) . . . . ? P41 Cr1 P32 Cr2 75.1(10) . . . . ? P4 Cr1 P32 Cr2 73.6(4) . . . . ? P22 P32 P42 P52 0.7(6) . . . . ? Cr2 P32 P42 P52 -45.7(4) . . . . ? Cr1 P32 P42 P52 46.9(4) . . . . ? P22 P32 P42 Cr1 -46.3(4) . . . . ? Cr2 P32 P42 Cr1 -92.6(2) . . . . ? P22 P32 P42 Cr2 46.3(4) . . . . ? Cr1 P32 P42 Cr2 92.6(2) . . . . ? C2 Cr1 P42 P52 132.7(8) . . . . ? C4 Cr1 P42 P52 130.3(3) . . . . ? C3 Cr1 P42 P52 159.0(3) . . . . ? C5 Cr1 P42 P52 91.9(3) . . . . ? C1 Cr1 P42 P52 69.3(4) . . . . ? P31 Cr1 P42 P52 -114.5(6) . . . . ? P11 Cr1 P42 P52 -18.2(6) . . . . ? P21 Cr1 P42 P52 -66.9(5) . . . . ? P51 Cr1 P42 P52 10.3(8) . . . . ? P2 Cr1 P42 P52 -77.5(4) . . . . ? P41 Cr1 P42 P52 -141.0(12) . . . . ? P4 Cr1 P42 P52 -149.7(13) . . . . ? C2 Cr1 P42 P32 -97.8(8) . . . . ? C4 Cr1 P42 P32 -100.2(3) . . . . ? C3 Cr1 P42 P32 -71.5(4) . . . . ? C5 Cr1 P42 P32 -138.6(3) . . . . ? C1 Cr1 P42 P32 -161.3(3) . . . . ? P31 Cr1 P42 P32 14.9(6) . . . . ? P11 Cr1 P42 P32 111.3(6) . . . . ? P21 Cr1 P42 P32 62.5(5) . . . . ? P51 Cr1 P42 P32 139.8(9) . . . . ? P2 Cr1 P42 P32 52.0(4) . . . . ? P41 Cr1 P42 P32 -11.6(11) . . . . ? P4 Cr1 P42 P32 -20.2(10) . . . . ? C2 Cr1 P42 Cr2 -162.5(7) . . . . ? C4 Cr1 P42 Cr2 -165.0(2) . . . . ? C3 Cr1 P42 Cr2 -136.23(16) . . . . ? C5 Cr1 P42 Cr2 156.66(18) . . . . ? C1 Cr1 P42 Cr2 134.00(18) . . . . ? P31 Cr1 P42 Cr2 -49.8(5) . . . . ? P11 Cr1 P42 Cr2 46.6(5) . . . . ? P21 Cr1 P42 Cr2 -2.2(5) . . . . ? P51 Cr1 P42 Cr2 75.1(8) . . . . ? P2 Cr1 P42 Cr2 -12.7(3) . . . . ? P41 Cr1 P42 Cr2 -76.3(11) . . . . ? P4 Cr1 P42 Cr2 -85.0(11) . . . . ? P32 P42 P52 P12 -1.0(6) . . . . ? Cr1 P42 P52 P12 46.3(4) . . . . ? Cr2 P42 P52 P12 -46.7(4) . . . . ? P32 P42 P52 Cr2 45.6(4) . . . . ? Cr1 P42 P52 Cr2 92.9(2) . . . . ? P32 P42 P52 Cr1 -47.3(4) . . . . ? Cr2 P42 P52 Cr1 -92.9(2) . . . . ? P22 P12 P52 P42 1.0(6) . . . . ? Cr1 P12 P52 P42 -46.2(4) . . . . ? Cr2 P12 P52 P42 46.7(4) . . . . ? P22 P12 P52 Cr2 -45.8(3) . . . . ? Cr1 P12 P52 Cr2 -92.9(2) . . . . ? P22 P12 P52 Cr1 47.2(3) . . . . ? Cr2 P12 P52 Cr1 92.9(2) . . . . ? C2 Cr1 P52 P42 -161.9(3) . . . . ? C4 Cr1 P52 P42 -72.1(4) . . . . ? C3 Cr1 P52 P42 -98.8(9) . . . . ? C5 Cr1 P52 P42 -100.8(3) . . . . ? C1 Cr1 P52 P42 -139.1(3) . . . . ? P31 Cr1 P52 P42 61.1(6) . . . . ? P11 Cr1 P52 P42 141.0(12) . . . . ? P21 Cr1 P52 P42 110.5(5) . . . . ? P51 Cr1 P52 P42 -11.9(9) . . . . ? P2 Cr1 P52 P42 103.9(4) . . . . ? P41 Cr1 P52 P42 15.8(5) . . . . ? P4 Cr1 P52 P42 8.3(3) . . . . ? C2 Cr1 P52 P12 68.3(4) . . . . ? C4 Cr1 P52 P12 158.1(3) . . . . ? C3 Cr1 P52 P12 131.3(8) . . . . ? C5 Cr1 P52 P12 129.4(3) . . . . ? C1 Cr1 P52 P12 91.1(3) . . . . ? P31 Cr1 P52 P12 -68.7(6) . . . . ? P11 Cr1 P52 P12 11.2(11) . . . . ? P21 Cr1 P52 P12 -19.3(5) . . . . ? P51 Cr1 P52 P12 -141.7(11) . . . . ? P2 Cr1 P52 P12 -25.9(3) . . . . ? P41 Cr1 P52 P12 -114.0(5) . . . . ? P4 Cr1 P52 P12 -121.5(4) . . . . ? C2 Cr1 P52 Cr2 133.14(18) . . . . ? C4 Cr1 P52 Cr2 -137.10(15) . . . . ? C3 Cr1 P52 Cr2 -163.8(7) . . . . ? C5 Cr1 P52 Cr2 -165.8(2) . . . . ? C1 Cr1 P52 Cr2 155.92(18) . . . . ? P31 Cr1 P52 Cr2 -3.9(6) . . . . ? P11 Cr1 P52 Cr2 76.0(11) . . . . ? P21 Cr1 P52 Cr2 45.5(4) . . . . ? P51 Cr1 P52 Cr2 -76.9(9) . . . . ? P2 Cr1 P52 Cr2 38.9(3) . . . . ? P41 Cr1 P52 Cr2 -49.2(4) . . . . ? P4 Cr1 P52 Cr2 -56.6(2) . . . . ? P11 P21 Cr2 C11 90.3(6) . . . . ? P31 P21 Cr2 C11 -144.0(6) . . . . ? Cr1 P21 Cr2 C11 153.4(3) . . . . ? P11 P21 Cr2 C15 69.2(7) . . . . ? P31 P21 Cr2 C15 -165.0(6) . . . . ? Cr1 P21 Cr2 C15 132.3(4) . . . . ? P11 P21 Cr2 C14 140.8(12) . . . . ? P31 P21 Cr2 C14 -93.4(15) . . . . ? Cr1 P21 Cr2 C14 -156.1(10) . . . . ? P11 P21 Cr2 C13 158.1(5) . . . . ? P31 P21 Cr2 C13 -76.1(7) . . . . ? Cr1 P21 Cr2 C13 -138.8(2) . . . . ? P11 P21 Cr2 C12 128.2(6) . . . . ? P31 P21 Cr2 C12 -106.0(6) . . . . ? Cr1 P21 Cr2 C12 -168.7(3) . . . . ? P11 P21 Cr2 P31 -125.8(8) . . . . ? Cr1 P21 Cr2 P31 -62.7(6) . . . . ? P11 P21 Cr2 P41 -89.4(7) . . . . ? P31 P21 Cr2 P41 36.4(8) . . . . ? Cr1 P21 Cr2 P41 -26.3(6) . . . . ? P11 P21 Cr2 P51 -36.9(7) . . . . ? P31 P21 Cr2 P51 88.9(7) . . . . ? Cr1 P21 Cr2 P51 26.2(6) . . . . ? P31 P21 Cr2 P11 125.8(8) . . . . ? Cr1 P21 Cr2 P11 63.1(6) . . . . ? P11 P21 Cr2 P22 -144.3(13) . . . . ? P31 P21 Cr2 P22 -18.6(10) . . . . ? Cr1 P21 Cr2 P22 -81.2(10) . . . . ? P11 P21 Cr2 P5 -28.4(6) . . . . ? P31 P21 Cr2 P5 97.3(6) . . . . ? Cr1 P21 Cr2 P5 34.7(4) . . . . ? P41 P31 Cr2 C11 -162.3(7) . . . . ? P21 P31 Cr2 C11 67.2(7) . . . . ? Cr1 P31 Cr2 C11 131.3(4) . . . . ? P41 P31 Cr2 C15 -83.7(18) . . . . ? P21 P31 Cr2 C15 145.8(15) . . . . ? Cr1 P31 Cr2 C15 -150.1(12) . . . . ? P41 P31 Cr2 C14 -71.9(8) . . . . ? P21 P31 Cr2 C14 157.6(5) . . . . ? Cr1 P31 Cr2 C14 -138.3(2) . . . . ? P41 P31 Cr2 C13 -103.2(7) . . . . ? P21 P31 Cr2 C13 126.3(5) . . . . ? Cr1 P31 Cr2 C13 -169.6(4) . . . . ? P41 P31 Cr2 C12 -141.4(7) . . . . ? P21 P31 Cr2 C12 88.1(5) . . . . ? Cr1 P31 Cr2 C12 152.2(3) . . . . ? P41 P31 Cr2 P21 130.5(9) . . . . ? Cr1 P31 Cr2 P21 64.1(5) . . . . ? P21 P31 Cr2 P41 -130.5(9) . . . . ? Cr1 P31 Cr2 P41 -66.4(8) . . . . ? P41 P31 Cr2 P51 38.4(8) . . . . ? P21 P31 Cr2 P51 -92.1(7) . . . . ? Cr1 P31 Cr2 P51 -27.9(7) . . . . ? P41 P31 Cr2 P11 90.3(8) . . . . ? P21 P31 Cr2 P11 -40.2(7) . . . . ? Cr1 P31 Cr2 P11 24.0(6) . . . . ? P41 P31 Cr2 P22 147.2(11) . . . . ? P21 P31 Cr2 P22 16.7(8) . . . . ? Cr1 P31 Cr2 P22 80.8(8) . . . . ? P41 P31 Cr2 P5 47.0(7) . . . . ? P21 P31 Cr2 P5 -83.5(6) . . . . ? Cr1 P31 Cr2 P5 -19.3(6) . . . . ? P31 P41 Cr2 C11 143.5(13) . . . . ? P51 P41 Cr2 C11 -88.1(16) . . . . ? Cr1 P41 Cr2 C11 -152.8(12) . . . . ? P31 P41 Cr2 C15 159.0(5) . . . . ? P51 P41 Cr2 C15 -72.6(7) . . . . ? Cr1 P41 Cr2 C15 -137.3(3) . . . . ? P31 P41 Cr2 C14 128.3(6) . . . . ? P51 P41 Cr2 C14 -103.3(6) . . . . ? Cr1 P41 Cr2 C14 -168.0(3) . . . . ? P31 P41 Cr2 C13 90.3(6) . . . . ? P51 P41 Cr2 C13 -141.3(5) . . . . ? Cr1 P41 Cr2 C13 154.0(3) . . . . ? P31 P41 Cr2 C12 69.7(9) . . . . ? P51 P41 Cr2 C12 -161.9(5) . . . . ? Cr1 P41 Cr2 C12 133.4(4) . . . . ? P31 P41 Cr2 P21 -37.7(7) . . . . ? P51 P41 Cr2 P21 90.7(7) . . . . ? Cr1 P41 Cr2 P21 26.0(5) . . . . ? P51 P41 Cr2 P31 128.4(9) . . . . ? Cr1 P41 Cr2 P31 63.7(6) . . . . ? P31 P41 Cr2 P51 -128.4(9) . . . . ? Cr1 P41 Cr2 P51 -64.7(6) . . . . ? P31 P41 Cr2 P11 -90.3(8) . . . . ? P51 P41 Cr2 P11 38.1(8) . . . . ? Cr1 P41 Cr2 P11 -26.6(7) . . . . ? P31 P41 Cr2 P22 -15.8(6) . . . . ? P51 P41 Cr2 P22 112.6(6) . . . . ? Cr1 P41 Cr2 P22 47.9(4) . . . . ? P31 P41 Cr2 P5 -123.5(8) . . . . ? P51 P41 Cr2 P5 4.8(7) . . . . ? Cr1 P41 Cr2 P5 -59.9(5) . . . . ? P11 P51 Cr2 C11 -73.9(7) . . . . ? P41 P51 Cr2 C11 157.6(6) . . . . ? Cr1 P51 Cr2 C11 -137.3(2) . . . . ? P11 P51 Cr2 C15 -104.0(7) . . . . ? P41 P51 Cr2 C15 127.6(6) . . . . ? Cr1 P51 Cr2 C15 -167.3(4) . . . . ? P11 P51 Cr2 C14 -142.0(7) . . . . ? P41 P51 Cr2 C14 89.6(6) . . . . ? Cr1 P51 Cr2 C14 154.7(3) . . . . ? P11 P51 Cr2 C13 -162.0(7) . . . . ? P41 P51 Cr2 C13 69.6(8) . . . . ? Cr1 P51 Cr2 C13 134.7(3) . . . . ? P11 P51 Cr2 C12 -89.7(16) . . . . ? P41 P51 Cr2 C12 141.8(14) . . . . ? Cr1 P51 Cr2 C12 -153.1(11) . . . . ? P11 P51 Cr2 P21 37.3(8) . . . . ? P41 P51 Cr2 P21 -91.1(7) . . . . ? Cr1 P51 Cr2 P21 -26.1(6) . . . . ? P11 P51 Cr2 P31 90.7(8) . . . . ? P41 P51 Cr2 P31 -37.7(7) . . . . ? Cr1 P51 Cr2 P31 27.4(6) . . . . ? P11 P51 Cr2 P41 128.4(9) . . . . ? Cr1 P51 Cr2 P41 65.1(6) . . . . ? P41 P51 Cr2 P11 -128.4(9) . . . . ? Cr1 P51 Cr2 P11 -63.4(8) . . . . ? P11 P51 Cr2 P22 62.7(7) . . . . ? P41 P51 Cr2 P22 -65.8(7) . . . . ? Cr1 P51 Cr2 P22 -0.7(6) . . . . ? P11 P51 Cr2 P5 -25(3) . . . . ? P41 P51 Cr2 P5 -153(3) . . . . ? Cr1 P51 Cr2 P5 -88(3) . . . . ? P51 P11 Cr2 C11 126.8(5) . . . . ? P21 P11 Cr2 C11 -102.9(6) . . . . ? Cr1 P11 Cr2 C11 -167.5(4) . . . . ? P51 P11 Cr2 C15 88.5(5) . . . . ? P21 P11 Cr2 C15 -141.2(6) . . . . ? Cr1 P11 Cr2 C15 154.2(4) . . . . ? P51 P11 Cr2 C14 67.5(8) . . . . ? P21 P11 Cr2 C14 -162.1(6) . . . . ? Cr1 P11 Cr2 C14 133.2(4) . . . . ? P51 P11 Cr2 C13 139.6(15) . . . . ? P21 P11 Cr2 C13 -90.0(19) . . . . ? Cr1 P11 Cr2 C13 -154.7(14) . . . . ? P51 P11 Cr2 C12 157.0(4) . . . . ? P21 P11 Cr2 C12 -72.7(7) . . . . ? Cr1 P11 Cr2 C12 -137.3(3) . . . . ? P51 P11 Cr2 P21 -130.4(8) . . . . ? Cr1 P11 Cr2 P21 -64.7(7) . . . . ? P51 P11 Cr2 P31 -89.7(7) . . . . ? P21 P11 Cr2 P31 40.7(7) . . . . ? Cr1 P11 Cr2 P31 -24.0(7) . . . . ? P51 P11 Cr2 P41 -38.4(7) . . . . ? P21 P11 Cr2 P41 92.0(7) . . . . ? Cr1 P11 Cr2 P41 27.3(6) . . . . ? P21 P11 Cr2 P51 130.4(8) . . . . ? Cr1 P11 Cr2 P51 65.7(6) . . . . ? P51 P11 Cr2 P22 -114.8(6) . . . . ? P21 P11 Cr2 P22 15.5(6) . . . . ? Cr1 P11 Cr2 P22 -49.1(5) . . . . ? P51 P11 Cr2 P5 5.8(7) . . . . ? P21 P11 Cr2 P5 136.2(9) . . . . ? Cr1 P11 Cr2 P5 71.5(5) . . . . ? P32 P22 Cr2 C11 -154.3(3) . . . . ? P12 P22 Cr2 C11 75.9(3) . . . . ? Cr1 P22 Cr2 C11 140.11(15) . . . . ? P32 P22 Cr2 C15 -150.4(6) . . . . ? P12 P22 Cr2 C15 79.8(6) . . . . ? Cr1 P22 Cr2 C15 144.0(4) . . . . ? P32 P22 Cr2 C14 -69.9(5) . . . . ? P12 P22 Cr2 C14 160.2(3) . . . . ? Cr1 P22 Cr2 C14 -135.57(19) . . . . ? P32 P22 Cr2 C13 -85.4(3) . . . . ? P12 P22 Cr2 C13 144.7(3) . . . . ? Cr1 P22 Cr2 C13 -151.02(18) . . . . ? P32 P22 Cr2 C12 -122.2(3) . . . . ? P12 P22 Cr2 C12 107.9(3) . . . . ? Cr1 P22 Cr2 C12 172.2(2) . . . . ? P32 P22 Cr2 P21 141.3(12) . . . . ? P12 P22 Cr2 P21 11.5(10) . . . . ? Cr1 P22 Cr2 P21 75.7(10) . . . . ? P32 P22 Cr2 P31 -7.2(8) . . . . ? P12 P22 Cr2 P31 -137.1(9) . . . . ? Cr1 P22 Cr2 P31 -72.9(9) . . . . ? P32 P22 Cr2 P41 18.4(6) . . . . ? P12 P22 Cr2 P41 -111.4(6) . . . . ? Cr1 P22 Cr2 P41 -47.2(5) . . . . ? P32 P22 Cr2 P51 66.3(6) . . . . ? P12 P22 Cr2 P51 -63.6(6) . . . . ? Cr1 P22 Cr2 P51 0.7(6) . . . . ? P32 P22 Cr2 P11 112.7(5) . . . . ? P12 P22 Cr2 P11 -17.2(6) . . . . ? Cr1 P22 Cr2 P11 47.0(5) . . . . ? P32 P22 Cr2 P5 75.9(4) . . . . ? P12 P22 Cr2 P5 -53.9(4) . . . . ? Cr1 P22 Cr2 P5 10.3(3) . . . . ? P4 P5 Cr2 C11 154.0(3) . . . . ? P1 P5 Cr2 C11 -76.7(4) . . . . ? Cr1 P5 Cr2 C11 -141.20(14) . . . . ? P4 P5 Cr2 C15 121.0(3) . . . . ? P1 P5 Cr2 C15 -109.7(4) . . . . ? Cr1 P5 Cr2 C15 -174.2(2) . . . . ? P4 P5 Cr2 C14 84.5(3) . . . . ? P1 P5 Cr2 C14 -146.1(4) . . . . ? Cr1 P5 Cr2 C14 149.36(17) . . . . ? P4 P5 Cr2 C13 71.2(4) . . . . ? P1 P5 Cr2 C13 -159.4(4) . . . . ? Cr1 P5 Cr2 C13 136.1(2) . . . . ? P4 P5 Cr2 C12 153.9(5) . . . . ? P1 P5 Cr2 C12 -76.7(8) . . . . ? Cr1 P5 Cr2 C12 -141.2(4) . . . . ? P4 P5 Cr2 P21 -99.0(5) . . . . ? P1 P5 Cr2 P21 30.3(6) . . . . ? Cr1 P5 Cr2 P21 -34.2(5) . . . . ? P4 P5 Cr2 P31 -46.0(6) . . . . ? P1 P5 Cr2 P31 83.4(6) . . . . ? Cr1 P5 Cr2 P31 18.8(5) . . . . ? P4 P5 Cr2 P41 -5.3(7) . . . . ? P1 P5 Cr2 P41 124.1(7) . . . . ? Cr1 P5 Cr2 P41 59.5(5) . . . . ? P4 P5 Cr2 P51 19(3) . . . . ? P1 P5 Cr2 P51 148(3) . . . . ? Cr1 P5 Cr2 P51 83(3) . . . . ? P4 P5 Cr2 P11 -132.4(8) . . . . ? P1 P5 Cr2 P11 -3.1(11) . . . . ? Cr1 P5 Cr2 P11 -67.6(7) . . . . ? P4 P5 Cr2 P22 -75.2(4) . . . . ? P1 P5 Cr2 P22 54.1(4) . . . . ? Cr1 P5 Cr2 P22 -10.4(4) . . . . ? C15 Cr2 C11 C12 -117.98(17) . . . . ? C14 Cr2 C11 C12 -80.16(13) . . . . ? C13 Cr2 C11 C12 -37.64(12) . . . . ? P21 Cr2 C11 C12 84.2(4) . . . . ? P31 Cr2 C11 C12 33.8(7) . . . . ? P41 Cr2 C11 C12 -97.0(16) . . . . ? P51 Cr2 C11 C12 -171.9(6) . . . . ? P11 Cr2 C11 C12 138.0(6) . . . . ? P22 Cr2 C11 C12 59.6(3) . . . . ? P5 Cr2 C11 C12 -180.0(3) . . . . ? C14 Cr2 C11 C15 37.82(11) . . . . ? C13 Cr2 C11 C15 80.34(13) . . . . ? C12 Cr2 C11 C15 117.98(17) . . . . ? P21 Cr2 C11 C15 -157.8(4) . . . . ? P31 Cr2 C11 C15 151.7(7) . . . . ? P41 Cr2 C11 C15 21.0(16) . . . . ? P51 Cr2 C11 C15 -53.9(6) . . . . ? P11 Cr2 C11 C15 -104.0(6) . . . . ? P22 Cr2 C11 C15 177.6(3) . . . . ? P5 Cr2 C11 C15 -62.0(3) . . . . ? C15 Cr2 C11 C16 120.8(3) . . . . ? C14 Cr2 C11 C16 158.6(3) . . . . ? C13 Cr2 C11 C16 -158.9(3) . . . . ? C12 Cr2 C11 C16 -121.2(3) . . . . ? P21 Cr2 C11 C16 -37.0(5) . . . . ? P31 Cr2 C11 C16 -87.5(7) . . . . ? P41 Cr2 C11 C16 141.7(16) . . . . ? P51 Cr2 C11 C16 66.9(6) . . . . ? P11 Cr2 C11 C16 16.8(6) . . . . ? P22 Cr2 C11 C16 -61.6(4) . . . . ? P5 Cr2 C11 C16 58.8(4) . . . . ? C15 C11 C12 C13 0.0(2) . . . . ? C16 C11 C12 C13 -177.2(2) . . . . ? Cr2 C11 C12 C13 61.99(14) . . . . ? C15 C11 C12 C17 175.9(2) . . . . ? C16 C11 C12 C17 -1.3(4) . . . . ? Cr2 C11 C12 C17 -122.1(2) . . . . ? C15 C11 C12 Cr2 -62.03(14) . . . . ? C16 C11 C12 Cr2 120.8(2) . . . . ? C15 Cr2 C12 C11 37.29(12) . . . . ? C14 Cr2 C12 C11 79.83(13) . . . . ? C13 Cr2 C12 C11 117.16(18) . . . . ? P21 Cr2 C12 C11 -104.5(4) . . . . ? P31 Cr2 C12 C11 -159.0(5) . . . . ? P41 Cr2 C12 C11 150.6(7) . . . . ? P51 Cr2 C12 C11 21.5(16) . . . . ? P11 Cr2 C12 C11 -54.3(7) . . . . ? P22 Cr2 C12 C11 -131.0(3) . . . . ? P5 Cr2 C12 C11 0.0(7) . . . . ? C11 Cr2 C12 C13 -117.16(18) . . . . ? C15 Cr2 C12 C13 -79.87(13) . . . . ? C14 Cr2 C12 C13 -37.33(12) . . . . ? P21 Cr2 C12 C13 138.3(4) . . . . ? P31 Cr2 C12 C13 83.9(5) . . . . ? P41 Cr2 C12 C13 33.4(7) . . . . ? P51 Cr2 C12 C13 -95.7(16) . . . . ? P11 Cr2 C12 C13 -171.4(7) . . . . ? P22 Cr2 C12 C13 111.8(3) . . . . ? P5 Cr2 C12 C13 -117.1(7) . . . . ? C11 Cr2 C12 C17 121.5(3) . . . . ? C15 Cr2 C12 C17 158.8(3) . . . . ? C14 Cr2 C12 C17 -158.7(3) . . . . ? C13 Cr2 C12 C17 -121.3(3) . . . . ? P21 Cr2 C12 C17 17.0(5) . . . . ? P31 Cr2 C12 C17 -37.5(5) . . . . ? P41 Cr2 C12 C17 -87.9(7) . . . . ? P51 Cr2 C12 C17 143.0(16) . . . . ? P11 Cr2 C12 C17 67.2(7) . . . . ? P22 Cr2 C12 C17 -9.6(4) . . . . ? P5 Cr2 C12 C17 121.5(7) . . . . ? C11 C12 C13 C14 0.1(2) . . . . ? C17 C12 C13 C14 -175.8(2) . . . . ? Cr2 C12 C13 C14 61.89(14) . . . . ? C11 C12 C13 C18 176.3(2) . . . . ? C17 C12 C13 C18 0.4(4) . . . . ? Cr2 C12 C13 C18 -121.9(2) . . . . ? C11 C12 C13 Cr2 -61.77(14) . . . . ? C17 C12 C13 Cr2 122.3(2) . . . . ? C11 Cr2 C13 C14 -80.11(13) . . . . ? C15 Cr2 C13 C14 -37.50(12) . . . . ? C12 Cr2 C13 C14 -117.75(18) . . . . ? P21 Cr2 C13 C14 -171.3(5) . . . . ? P31 Cr2 C13 C14 136.1(5) . . . . ? P41 Cr2 C13 C14 83.6(5) . . . . ? P51 Cr2 C13 C14 32.5(7) . . . . ? P11 Cr2 C13 C14 -94.4(19) . . . . ? P22 Cr2 C13 C14 165.4(3) . . . . ? P5 Cr2 C13 C14 20.7(4) . . . . ? C11 Cr2 C13 C12 37.64(13) . . . . ? C15 Cr2 C13 C12 80.25(13) . . . . ? C14 Cr2 C13 C12 117.75(18) . . . . ? P21 Cr2 C13 C12 -53.6(5) . . . . ? P31 Cr2 C13 C12 -106.1(5) . . . . ? P41 Cr2 C13 C12 -158.7(5) . . . . ? P51 Cr2 C13 C12 150.3(7) . . . . ? P11 Cr2 C13 C12 23.4(19) . . . . ? P22 Cr2 C13 C12 -76.9(3) . . . . ? P5 Cr2 C13 C12 138.4(4) . . . . ? C11 Cr2 C13 C18 159.8(3) . . . . ? C15 Cr2 C13 C18 -157.6(3) . . . . ? C14 Cr2 C13 C18 -120.1(3) . . . . ? C12 Cr2 C13 C18 122.2(3) . . . . ? P21 Cr2 C13 C18 68.6(6) . . . . ? P31 Cr2 C13 C18 16.0(6) . . . . ? P41 Cr2 C13 C18 -36.5(5) . . . . ? P51 Cr2 C13 C18 -87.5(7) . . . . ? P11 Cr2 C13 C18 145.5(19) . . . . ? P22 Cr2 C13 C18 45.3(4) . . . . ? P5 Cr2 C13 C18 -99.4(5) . . . . ? C12 C13 C14 C15 -0.1(2) . . . . ? C18 C13 C14 C15 -176.4(2) . . . . ? Cr2 C13 C14 C15 61.81(14) . . . . ? C12 C13 C14 C19 176.8(2) . . . . ? C18 C13 C14 C19 0.6(3) . . . . ? Cr2 C13 C14 C19 -121.2(2) . . . . ? C12 C13 C14 Cr2 -61.96(14) . . . . ? C18 C13 C14 Cr2 121.8(2) . . . . ? C11 Cr2 C14 C13 79.75(14) . . . . ? C15 Cr2 C14 C13 117.58(18) . . . . ? C12 Cr2 C14 C13 37.31(13) . . . . ? P21 Cr2 C14 C13 23.4(14) . . . . ? P31 Cr2 C14 C13 -56.8(6) . . . . ? P41 Cr2 C14 C13 -105.5(5) . . . . ? P51 Cr2 C14 C13 -159.0(5) . . . . ? P11 Cr2 C14 C13 151.7(7) . . . . ? P22 Cr2 C14 C13 -24.4(5) . . . . ? P5 Cr2 C14 C13 -168.1(3) . . . . ? C11 Cr2 C14 C15 -37.83(13) . . . . ? C13 Cr2 C14 C15 -117.58(18) . . . . ? C12 Cr2 C14 C15 -80.27(14) . . . . ? P21 Cr2 C14 C15 -94.2(14) . . . . ? P31 Cr2 C14 C15 -174.3(6) . . . . ? P41 Cr2 C14 C15 136.9(5) . . . . ? P51 Cr2 C14 C15 83.4(5) . . . . ? P11 Cr2 C14 C15 34.1(7) . . . . ? P22 Cr2 C14 C15 -142.0(4) . . . . ? P5 Cr2 C14 C15 74.3(3) . . . . ? C11 Cr2 C14 C19 -160.0(2) . . . . ? C15 Cr2 C14 C19 -122.2(3) . . . . ? C13 Cr2 C14 C19 120.2(3) . . . . ? C12 Cr2 C14 C19 157.6(2) . . . . ? P21 Cr2 C14 C19 143.6(14) . . . . ? P31 Cr2 C14 C19 63.5(6) . . . . ? P41 Cr2 C14 C19 14.7(5) . . . . ? P51 Cr2 C14 C19 -38.8(5) . . . . ? P11 Cr2 C14 C19 -88.1(7) . . . . ? P22 Cr2 C14 C19 95.9(5) . . . . ? P5 Cr2 C14 C19 -47.8(3) . . . . ? C12 C11 C15 C14 0.0(2) . . . . ? C16 C11 C15 C14 177.1(2) . . . . ? Cr2 C11 C15 C14 -62.26(14) . . . . ? C12 C11 C15 C20 -177.2(2) . . . . ? C16 C11 C15 C20 0.0(3) . . . . ? Cr2 C11 C15 C20 120.6(2) . . . . ? C12 C11 C15 Cr2 62.21(15) . . . . ? C16 C11 C15 Cr2 -120.6(2) . . . . ? C13 C14 C15 C11 0.1(2) . . . . ? C19 C14 C15 C11 -176.8(2) . . . . ? Cr2 C14 C15 C11 62.05(14) . . . . ? C13 C14 C15 C20 177.3(2) . . . . ? C19 C14 C15 C20 0.3(3) . . . . ? Cr2 C14 C15 C20 -120.8(2) . . . . ? C13 C14 C15 Cr2 -61.93(14) . . . . ? C19 C14 C15 Cr2 121.1(2) . . . . ? C14 Cr2 C15 C11 -116.91(17) . . . . ? C13 Cr2 C15 C11 -79.53(13) . . . . ? C12 Cr2 C15 C11 -37.15(13) . . . . ? P21 Cr2 C15 C11 34.3(6) . . . . ? P31 Cr2 C15 C11 -101.2(17) . . . . ? P41 Cr2 C15 C11 -172.2(6) . . . . ? P51 Cr2 C15 C11 137.8(6) . . . . ? P11 Cr2 C15 C11 85.1(5) . . . . ? P22 Cr2 C15 C11 -5.5(7) . . . . ? P5 Cr2 C15 C11 128.4(3) . . . . ? C11 Cr2 C15 C14 116.91(17) . . . . ? C13 Cr2 C15 C14 37.38(12) . . . . ? C12 Cr2 C15 C14 79.76(13) . . . . ? P21 Cr2 C15 C14 151.2(6) . . . . ? P31 Cr2 C15 C14 15.7(17) . . . . ? P41 Cr2 C15 C14 -55.3(6) . . . . ? P51 Cr2 C15 C14 -105.3(6) . . . . ? P11 Cr2 C15 C14 -158.0(5) . . . . ? P22 Cr2 C15 C14 111.4(7) . . . . ? P5 Cr2 C15 C14 -114.7(3) . . . . ? C11 Cr2 C15 C20 -121.2(2) . . . . ? C14 Cr2 C15 C20 121.8(3) . . . . ? C13 Cr2 C15 C20 159.2(2) . . . . ? C12 Cr2 C15 C20 -158.4(2) . . . . ? P21 Cr2 C15 C20 -87.0(6) . . . . ? P31 Cr2 C15 C20 137.6(17) . . . . ? P41 Cr2 C15 C20 66.6(6) . . . . ? P51 Cr2 C15 C20 16.6(6) . . . . ? P11 Cr2 C15 C20 -36.2(5) . . . . ? P22 Cr2 C15 C20 -126.8(7) . . . . ? P5 Cr2 C15 C20 7.2(4) . . . . ? _diffrn_measured_fraction_theta_max 0.970 _diffrn_reflns_theta_full 30.46 _diffrn_measured_fraction_theta_full 0.970 _refine_diff_density_max 0.979 _refine_diff_density_min -0.498 _refine_diff_density_rms 0.088 #===END data_170k _database_code_depnum_ccdc_archive 'CCDC 618753' _audit_creation_method SHELXL-97 _chemical_name_systematic ; \m~2~-\h^5^,\h^5^-cyclopentaphosphole)-bis ((\h^5^-pentamethyl-cyclopentadienyl)-chromium) hexafluoroantimonate ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H30 Cr2 F6 P5 Sb' _chemical_formula_weight 765.04 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting orthorhombic _symmetry_space_group_name_H-M Fddd loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+3/4, -y+3/4, z' '-x+3/4, y, -z+3/4' 'x, -y+3/4, -z+3/4' 'x, y+1/2, z+1/2' '-x+3/4, -y+5/4, z+1/2' '-x+3/4, y+1/2, -z+5/4' 'x, -y+5/4, -z+5/4' 'x+1/2, y, z+1/2' '-x+5/4, -y+3/4, z+1/2' '-x+5/4, y, -z+5/4' 'x+1/2, -y+3/4, -z+5/4' 'x+1/2, y+1/2, z' '-x+5/4, -y+5/4, z' '-x+5/4, y+1/2, -z+3/4' 'x+1/2, -y+5/4, -z+3/4' '-x, -y, -z' 'x-3/4, y-3/4, -z' 'x-3/4, -y, z-3/4' '-x, y-3/4, z-3/4' '-x, -y+1/2, -z+1/2' 'x-3/4, y-1/4, -z+1/2' 'x-3/4, -y+1/2, z-1/4' '-x, y-1/4, z-1/4' '-x+1/2, -y, -z+1/2' 'x-1/4, y-3/4, -z+1/2' 'x-1/4, -y, z-1/4' '-x+1/2, y-3/4, z-1/4' '-x+1/2, -y+1/2, -z' 'x-1/4, y-1/4, -z' 'x-1/4, -y+1/2, z-3/4' '-x+1/2, y-1/4, z-3/4' _cell_length_a 21.3434(6) _cell_length_b 29.3178(9) _cell_length_c 35.9441(11) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_volume 22491.7(12) _cell_formula_units_Z 32 _cell_measurement_temperature 170(2) _cell_measurement_reflns_used 7231 _cell_measurement_theta_min 2.36 _cell_measurement_theta_max 30.42 _exptl_crystal_description 'irregular block' _exptl_crystal_colour 'dark green' _exptl_crystal_size_max 0.60 _exptl_crystal_size_mid 0.52 _exptl_crystal_size_min 0.40 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.807 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 12096 _exptl_absorpt_coefficient_mu 2.047 _exptl_absorpt_correction_type integration _exptl_absorpt_correction_T_min 0.393 _exptl_absorpt_correction_T_max 0.614 _exptl_absorpt_process_details 'XPREP in SHELXTL' _exptl_special_details ; ? ; _diffrn_ambient_temperature 170(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'Bede Microsource X-ray Generator' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEX CCD Diffractometer' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number 0 _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% 0 _diffrn_reflns_number 42596 _diffrn_reflns_av_R_equivalents 0.0194 _diffrn_reflns_av_sigmaI/netI 0.0159 _diffrn_reflns_limit_h_min -30 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_k_min -41 _diffrn_reflns_limit_k_max 41 _diffrn_reflns_limit_l_min -46 _diffrn_reflns_limit_l_max 51 _diffrn_reflns_theta_min 1.31 _diffrn_reflns_theta_max 30.47 _reflns_number_total 8310 _reflns_number_gt 7056 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'SMART V5.625 (Bruker, 2003)' _computing_cell_refinement 'SMART V5.625 (Bruker, 2003)' _computing_data_reduction 'SAINT V6.28A (Bruker, 2003)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'SHELXTL V6.12(Bruker, 2001)' _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0336P)^2^+82.4353P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 8310 _refine_ls_number_parameters 404 _refine_ls_number_restraints 96 _refine_ls_R_factor_all 0.0379 _refine_ls_R_factor_gt 0.0292 _refine_ls_wR_factor_ref 0.0786 _refine_ls_wR_factor_gt 0.0730 _refine_ls_goodness_of_fit_ref 1.074 _refine_ls_restrained_S_all 1.070 _refine_ls_shift/su_max 0.003 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb1 Sb 0.6250 0.1250 0.009472(6) 0.03688(6) Uani 1 2 d S . . F1A F 0.6886(3) 0.1046(3) -0.0185(3) 0.131(2) Uani 0.50 1 d P A 1 F2A F 0.5535(3) 0.1379(3) 0.0346(2) 0.131(2) Uani 0.50 1 d P A 1 F1B F 0.6724(4) 0.1182(2) -0.03392(18) 0.125(2) Uani 0.50 1 d P A 2 F2B F 0.5851(4) 0.1420(2) 0.05268(16) 0.125(2) Uani 0.50 1 d P A 2 F3 F 0.59599(13) 0.06528(7) 0.00942(8) 0.0935(8) Uani 1 1 d . A . Sb2 Sb 0.1250 0.239291(8) 0.1250 0.03904(6) Uani 1 2 d S . . F4 F 0.18581(10) 0.28489(7) 0.12142(7) 0.0838(7) Uani 1 1 d . . . F5 F 0.11807(10) 0.23854(7) 0.07310(5) 0.0726(6) Uani 1 1 d . . . F6 F 0.18693(8) 0.19443(6) 0.12258(5) 0.0590(4) Uani 1 1 d . . . C1 C 0.13911(9) 0.36994(7) 0.01319(6) 0.0271(4) Uani 1 1 d . B . C2 C 0.19771(10) 0.34887(7) 0.00495(6) 0.0287(4) Uani 1 1 d . B . C3 C 0.22749(9) 0.37462(8) -0.02380(6) 0.0307(4) Uani 1 1 d . B . C4 C 0.18742(10) 0.41173(7) -0.03311(6) 0.0308(4) Uani 1 1 d . B . C5 C 0.13284(9) 0.40879(7) -0.01030(6) 0.0277(4) Uani 1 1 d . B . C6 C 0.09120(11) 0.35238(8) 0.04017(7) 0.0402(5) Uani 1 1 d . . . H6A H 0.0644 0.3299 0.0277 0.060 Uiso 1 1 calc R . . H6B H 0.0654 0.3778 0.0491 0.060 Uiso 1 1 calc R . . H6C H 0.1124 0.3380 0.0613 0.060 Uiso 1 1 calc R . . C7 C 0.22160(13) 0.30566(8) 0.02218(7) 0.0431(6) Uani 1 1 d . . . H7A H 0.1978 0.2797 0.0124 0.065 Uiso 1 1 calc R . . H7B H 0.2165 0.3072 0.0492 0.065 Uiso 1 1 calc R . . H7C H 0.2661 0.3019 0.0161 0.065 Uiso 1 1 calc R . . C8 C 0.28867(11) 0.36362(10) -0.04226(7) 0.0468(6) Uani 1 1 d . . . H8A H 0.2812 0.3435 -0.0636 0.070 Uiso 1 1 calc R . . H8B H 0.3163 0.3482 -0.0244 0.070 Uiso 1 1 calc R . . H8C H 0.3085 0.3919 -0.0508 0.070 Uiso 1 1 calc R . . C9 C 0.19796(14) 0.44646(10) -0.06291(7) 0.0501(6) Uani 1 1 d . . . H9A H 0.1753 0.4374 -0.0854 0.075 Uiso 1 1 calc R . . H9B H 0.2428 0.4485 -0.0684 0.075 Uiso 1 1 calc R . . H9C H 0.1827 0.4762 -0.0544 0.075 Uiso 1 1 calc R . . C10 C 0.07687(11) 0.43926(8) -0.01302(7) 0.0400(5) Uani 1 1 d . . . H10A H 0.0513 0.4301 -0.0344 0.060 Uiso 1 1 calc R . . H10B H 0.0907 0.4709 -0.0163 0.060 Uiso 1 1 calc R . . H10C H 0.0520 0.4367 0.0098 0.060 Uiso 1 1 calc R . . Cr1 Cr 0.215735(14) 0.418310(10) 0.025556(8) 0.02283(7) Uani 1 1 d . . . P11 P 0.1899(10) 0.4330(8) 0.0884(5) 0.055(5) Uani 0.25 1 d PU B 1 P21 P 0.2757(10) 0.3984(4) 0.0794(5) 0.054(5) Uani 0.25 1 d PU B 1 P31 P 0.3232(6) 0.4336(8) 0.0363(5) 0.052(5) Uani 0.25 1 d PU B 1 P41 P 0.2688(12) 0.4909(6) 0.0211(5) 0.063(6) Uani 0.25 1 d PU B 1 P51 P 0.1871(7) 0.4916(6) 0.0526(5) 0.046(3) Uani 0.25 1 d PU B 1 P1 P 0.1994(6) 0.4222(4) 0.0925(3) 0.052(3) Uani 0.50 1 d PU B 2 P2 P 0.2899(6) 0.3962(3) 0.0734(3) 0.050(2) Uani 0.50 1 d PU B 2 P3 P 0.3251(4) 0.4428(4) 0.0305(3) 0.048(2) Uani 0.50 1 d PU B 2 P4 P 0.2555(7) 0.4961(3) 0.0216(3) 0.0510(19) Uani 0.50 1 d PU B 2 P5 P 0.1782(3) 0.4831(3) 0.0612(2) 0.047(2) Uani 0.50 1 d PU B 2 P12 P 0.2231(4) 0.4073(3) 0.0934(2) 0.061(3) Uani 0.25 1 d PU B 3 P22 P 0.3116(4) 0.4043(3) 0.0618(3) 0.059(3) Uani 0.25 1 d PU B 3 P32 P 0.3155(4) 0.4609(3) 0.0229(2) 0.062(3) Uani 0.25 1 d PU B 3 P42 P 0.2284(4) 0.5006(3) 0.0303(2) 0.061(3) Uani 0.25 1 d PU B 3 P52 P 0.1718(4) 0.4680(4) 0.0738(3) 0.058(3) Uani 0.25 1 d PU B 3 Cr2 Cr 0.283327(14) 0.478301(10) 0.086529(8) 0.02266(7) Uani 1 1 d . . . C11 C 0.29490(10) 0.49168(7) 0.14634(6) 0.0305(4) Uani 1 1 d . B . C12 C 0.35451(10) 0.48060(7) 0.13112(6) 0.0325(4) Uani 1 1 d . B . C13 C 0.36926(9) 0.51417(7) 0.10405(6) 0.0301(4) Uani 1 1 d . B . C14 C 0.31903(9) 0.54614(7) 0.10254(6) 0.0268(4) Uani 1 1 d . B . C15 C 0.27263(9) 0.53218(6) 0.12873(5) 0.0262(4) Uani 1 1 d . B . C16 C 0.26225(15) 0.46633(10) 0.17716(7) 0.0507(7) Uani 1 1 d . . . H16A H 0.2767 0.4779 0.2013 0.076 Uiso 1 1 calc R B . H16B H 0.2719 0.4337 0.1753 0.076 Uiso 1 1 calc R . . H16C H 0.2169 0.4708 0.1750 0.076 Uiso 1 1 calc R . . C17 C 0.39622(15) 0.44225(9) 0.14346(9) 0.0579(8) Uani 1 1 d . . . H17A H 0.4228 0.4526 0.1640 0.087 Uiso 1 1 calc R B . H17B H 0.4226 0.4325 0.1226 0.087 Uiso 1 1 calc R . . H17C H 0.3704 0.4165 0.1518 0.087 Uiso 1 1 calc R . . C18 C 0.42918(11) 0.51779(11) 0.08229(8) 0.0520(7) Uani 1 1 d . . . H18A H 0.4579 0.5387 0.0950 0.078 Uiso 1 1 calc R B . H18B H 0.4201 0.5294 0.0573 0.078 Uiso 1 1 calc R . . H18C H 0.4487 0.4876 0.0804 0.078 Uiso 1 1 calc R . . C19 C 0.31778(13) 0.58810(8) 0.07891(7) 0.0428(5) Uani 1 1 d . . . H19A H 0.3377 0.6133 0.0923 0.064 Uiso 1 1 calc R B . H19B H 0.2743 0.5961 0.0732 0.064 Uiso 1 1 calc R . . H19C H 0.3405 0.5823 0.0557 0.064 Uiso 1 1 calc R . . C20 C 0.21303(10) 0.55671(8) 0.13770(7) 0.0403(5) Uani 1 1 d . . . H20A H 0.2204 0.5781 0.1582 0.061 Uiso 1 1 calc R B . H20B H 0.1810 0.5346 0.1451 0.061 Uiso 1 1 calc R . . H20C H 0.1987 0.5735 0.1157 0.061 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.03044(10) 0.04469(12) 0.03551(11) 0.000 0.000 0.00423(8) F1A 0.081(3) 0.125(4) 0.187(6) -0.040(3) 0.082(3) 0.007(2) F2A 0.081(3) 0.125(4) 0.187(6) -0.040(3) 0.082(3) 0.007(2) F1B 0.217(6) 0.077(2) 0.081(3) -0.0075(19) 0.096(4) -0.014(3) F2B 0.217(6) 0.077(2) 0.081(3) -0.0075(19) 0.096(4) -0.014(3) F3 0.1114(19) 0.0550(12) 0.114(2) 0.0115(12) -0.0286(16) -0.0226(12) Sb2 0.03380(11) 0.04465(12) 0.03866(12) 0.000 0.00644(9) 0.000 F4 0.0707(13) 0.0716(13) 0.1090(18) -0.0224(12) 0.0203(12) -0.0321(11) F5 0.0936(15) 0.0846(14) 0.0396(9) 0.0174(9) -0.0004(9) -0.0163(11) F6 0.0462(9) 0.0692(11) 0.0615(10) -0.0156(9) 0.0012(8) 0.0155(8) C1 0.0281(9) 0.0266(9) 0.0265(9) -0.0039(7) -0.0021(7) 0.0000(7) C2 0.0310(9) 0.0259(9) 0.0292(10) -0.0064(7) -0.0050(8) 0.0062(7) C3 0.0275(9) 0.0396(10) 0.0251(9) -0.0097(8) -0.0013(7) 0.0045(8) C4 0.0314(9) 0.0379(10) 0.0230(9) 0.0020(8) -0.0034(8) 0.0003(8) C5 0.0260(9) 0.0289(9) 0.0282(9) -0.0018(7) -0.0061(7) 0.0047(7) C6 0.0396(12) 0.0414(12) 0.0395(12) -0.0008(10) 0.0076(10) -0.0103(10) C7 0.0542(14) 0.0266(10) 0.0484(14) -0.0035(9) -0.0131(11) 0.0130(9) C8 0.0318(11) 0.0683(17) 0.0403(13) -0.0208(12) 0.0049(10) 0.0050(11) C9 0.0587(16) 0.0623(16) 0.0294(12) 0.0168(11) -0.0056(11) -0.0077(13) C10 0.0346(11) 0.0405(12) 0.0448(13) -0.0055(10) -0.0120(10) 0.0139(9) Cr1 0.02273(13) 0.02369(13) 0.02207(14) 0.00003(11) -0.00075(11) 0.00334(10) P11 0.052(5) 0.089(13) 0.023(5) -0.013(6) 0.011(4) -0.044(8) P21 0.092(14) 0.016(2) 0.055(7) 0.001(3) -0.049(8) 0.006(4) P31 0.016(2) 0.074(9) 0.066(10) -0.046(8) 0.009(3) -0.006(4) P41 0.110(15) 0.053(8) 0.026(3) 0.015(4) -0.018(5) -0.048(9) P51 0.040(6) 0.038(3) 0.060(7) -0.019(4) -0.023(5) 0.019(4) P1 0.067(4) 0.067(5) 0.0203(17) 0.003(2) 0.001(2) -0.042(4) P2 0.062(4) 0.0297(16) 0.057(4) -0.0118(15) -0.036(3) 0.0180(19) P3 0.0315(15) 0.074(5) 0.039(2) -0.025(3) 0.0156(14) -0.0205(17) P4 0.080(4) 0.0318(18) 0.041(2) 0.0123(13) -0.025(2) -0.013(2) P5 0.024(2) 0.062(6) 0.055(5) -0.033(4) -0.006(2) 0.013(3) P12 0.104(7) 0.047(4) 0.030(2) 0.007(2) -0.020(4) -0.039(4) P22 0.047(4) 0.052(5) 0.077(6) -0.037(4) -0.038(3) 0.030(3) P32 0.064(5) 0.091(6) 0.030(3) -0.017(3) 0.012(3) -0.045(5) P42 0.099(6) 0.0229(16) 0.062(6) 0.003(3) -0.052(5) -0.001(4) P52 0.0219(14) 0.089(8) 0.062(6) -0.050(5) 0.005(3) -0.002(3) Cr2 0.02248(13) 0.02277(13) 0.02272(14) -0.00120(11) 0.00030(11) 0.00053(10) C11 0.0394(11) 0.0292(9) 0.0228(9) 0.0009(7) -0.0022(8) -0.0093(8) C12 0.0353(10) 0.0284(9) 0.0338(11) -0.0052(8) -0.0115(8) 0.0020(8) C13 0.0235(8) 0.0366(10) 0.0303(10) -0.0102(8) 0.0015(7) -0.0039(7) C14 0.0284(9) 0.0253(8) 0.0266(9) -0.0011(7) 0.0018(7) -0.0047(7) C15 0.0262(8) 0.0258(8) 0.0265(9) -0.0059(7) 0.0033(7) -0.0031(7) C16 0.0721(18) 0.0527(15) 0.0272(11) 0.0066(10) -0.0021(11) -0.0327(14) C17 0.0657(17) 0.0369(12) 0.0710(19) -0.0127(13) -0.0393(16) 0.0162(12) C18 0.0285(10) 0.0753(19) 0.0523(15) -0.0260(14) 0.0110(10) -0.0104(11) C19 0.0620(15) 0.0292(10) 0.0373(12) 0.0071(9) -0.0020(11) -0.0114(10) C20 0.0299(10) 0.0417(12) 0.0494(14) -0.0198(10) 0.0069(9) 0.0014(9) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb1 F1A 1.791(5) 14_545 ? Sb1 F1A 1.792(5) . ? Sb1 F2A 1.812(5) . ? Sb1 F2A 1.812(5) 14_545 ? Sb1 F2B 1.840(5) . ? Sb1 F2B 1.840(5) 14_545 ? Sb1 F3 1.857(2) . ? Sb1 F3 1.857(2) 14_545 ? Sb1 F1B 1.870(5) . ? Sb1 F1B 1.870(5) 14_545 ? Sb2 F6 1.8667(16) 11_454 ? Sb2 F6 1.8667(16) . ? Sb2 F4 1.8676(19) 11_454 ? Sb2 F4 1.8676(19) . ? Sb2 F5 1.8716(18) 11_454 ? Sb2 F5 1.8716(18) . ? C1 C5 1.424(3) . ? C1 C2 1.426(3) . ? C1 C6 1.500(3) . ? C1 Cr1 2.2099(19) . ? C2 C3 1.429(3) . ? C2 C7 1.499(3) . ? C2 Cr1 2.2003(19) . ? C3 C4 1.424(3) . ? C3 C8 1.500(3) . ? C3 Cr1 2.203(2) . ? C4 C5 1.427(3) . ? C4 C9 1.495(3) . ? C4 Cr1 2.202(2) . ? C5 C10 1.495(3) . ? C5 Cr1 2.2066(19) . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? Cr1 P51 2.436(19) . ? Cr1 P31 2.368(14) . ? Cr1 P11 2.366(18) . ? Cr1 P21 2.392(16) . ? Cr1 P41 2.417(19) . ? Cr1 P52 2.451(9) . ? Cr1 P2 2.426(9) . ? P11 P51 2.15(2) . ? P11 P21 2.12(3) . ? P11 Cr2 2.396(19) . ? P21 P31 2.12(3) . ? P21 Cr2 2.361(14) . ? P31 P41 2.11(3) . ? P31 Cr2 2.387(15) . ? P41 P51 2.08(3) . ? P41 Cr2 2.401(16) . ? P51 Cr2 2.420(17) . ? P1 P2 2.187(15) . ? P1 P5 2.161(11) . ? P1 Cr2 2.442(10) . ? P2 P3 2.193(16) . ? P2 Cr2 2.455(9) . ? P3 P4 2.178(16) . ? P3 Cr2 2.435(9) . ? P4 P5 2.213(15) . ? P4 Cr2 2.464(10) . ? P5 Cr2 2.427(7) . ? P12 P52 2.204(12) . ? P12 P22 2.206(11) . ? P12 Cr2 2.458(8) . ? P22 P32 2.171(11) . ? P22 Cr2 2.420(9) . ? P32 P42 2.208(12) . ? P32 Cr2 2.442(8) . ? P42 P52 2.196(11) . ? P42 Cr2 2.427(9) . ? P52 Cr2 2.444(9) . ? Cr2 C11 2.199(2) . ? Cr2 C15 2.2018(19) . ? Cr2 C13 2.2059(19) . ? Cr2 C14 2.2063(19) . ? Cr2 C12 2.209(2) . ? C11 C12 1.423(3) . ? C11 C15 1.427(3) . ? C11 C16 1.505(3) . ? C12 C13 1.419(3) . ? C12 C17 1.501(3) . ? C13 C14 1.425(3) . ? C13 C18 1.503(3) . ? C14 C15 1.426(3) . ? C14 C19 1.495(3) . ? C15 C20 1.496(3) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F1A Sb1 F1A 111.7(6) 14_545 . ? F1A Sb1 F2A 64.7(5) 14_545 . ? F1A Sb1 F2A 170.6(4) . . ? F1A Sb1 F2A 170.6(4) 14_545 14_545 ? F1A Sb1 F2A 64.7(5) . 14_545 ? F2A Sb1 F2A 120.3(6) . 14_545 ? F1A Sb1 F2B 91.9(4) 14_545 . ? F1A Sb1 F2B 156.2(4) . . ? F2A Sb1 F2B 30.0(3) . . ? F2A Sb1 F2B 91.5(4) 14_545 . ? F1A Sb1 F2B 156.2(4) 14_545 14_545 ? F1A Sb1 F2B 91.9(4) . 14_545 ? F2A Sb1 F2B 91.5(4) . 14_545 ? F2A Sb1 F2B 30.0(3) 14_545 14_545 ? F2B Sb1 F2B 64.9(5) . 14_545 ? F1A Sb1 F3 93.6(3) 14_545 . ? F1A Sb1 F3 86.4(3) . . ? F2A Sb1 F3 85.2(3) . . ? F2A Sb1 F3 94.9(3) 14_545 . ? F2B Sb1 F3 95.8(2) . . ? F2B Sb1 F3 84.3(2) 14_545 . ? F1A Sb1 F3 86.4(3) 14_545 14_545 ? F1A Sb1 F3 93.6(3) . 14_545 ? F2A Sb1 F3 94.9(3) . 14_545 ? F2A Sb1 F3 85.2(3) 14_545 14_545 ? F2B Sb1 F3 84.3(2) . 14_545 ? F2B Sb1 F3 95.8(2) 14_545 14_545 ? F3 Sb1 F3 179.88(17) . 14_545 ? F1A Sb1 F1B 88.7(4) 14_545 . ? F1A Sb1 F1B 24.0(4) . . ? F2A Sb1 F1B 153.3(5) . . ? F2A Sb1 F1B 86.4(4) 14_545 . ? F2B Sb1 F1B 169.5(3) . . ? F2B Sb1 F1B 115.1(4) 14_545 . ? F3 Sb1 F1B 94.6(2) . . ? F3 Sb1 F1B 85.3(2) 14_545 . ? F1A Sb1 F1B 24.0(4) 14_545 14_545 ? F1A Sb1 F1B 88.7(4) . 14_545 ? F2A Sb1 F1B 86.4(4) . 14_545 ? F2A Sb1 F1B 153.3(5) 14_545 14_545 ? F2B Sb1 F1B 115.1(4) . 14_545 ? F2B Sb1 F1B 169.5(3) 14_545 14_545 ? F3 Sb1 F1B 85.3(2) . 14_545 ? F3 Sb1 F1B 94.6(2) 14_545 14_545 ? F1B Sb1 F1B 67.0(6) . 14_545 ? F6 Sb2 F6 90.40(12) 11_454 . ? F6 Sb2 F4 90.52(10) 11_454 11_454 ? F6 Sb2 F4 178.39(10) . 11_454 ? F6 Sb2 F4 178.39(10) 11_454 . ? F6 Sb2 F4 90.52(10) . . ? F4 Sb2 F4 88.59(15) 11_454 . ? F6 Sb2 F5 90.07(9) 11_454 11_454 ? F6 Sb2 F5 88.98(8) . 11_454 ? F4 Sb2 F5 89.70(10) 11_454 11_454 ? F4 Sb2 F5 91.27(11) . 11_454 ? F6 Sb2 F5 88.98(8) 11_454 . ? F6 Sb2 F5 90.06(9) . . ? F4 Sb2 F5 91.27(11) 11_454 . ? F4 Sb2 F5 89.70(10) . . ? F5 Sb2 F5 178.65(13) 11_454 . ? C5 C1 C2 107.80(18) . . ? C5 C1 C6 126.40(19) . . ? C2 C1 C6 125.69(19) . . ? C5 C1 Cr1 71.06(11) . . ? C2 C1 Cr1 70.77(11) . . ? C6 C1 Cr1 126.48(15) . . ? C1 C2 C3 108.14(17) . . ? C1 C2 C7 125.3(2) . . ? C3 C2 C7 126.4(2) . . ? C1 C2 Cr1 71.50(11) . . ? C3 C2 Cr1 71.14(11) . . ? C7 C2 Cr1 125.68(15) . . ? C4 C3 C2 107.85(18) . . ? C4 C3 C8 125.7(2) . . ? C2 C3 C8 126.4(2) . . ? C4 C3 Cr1 71.13(12) . . ? C2 C3 Cr1 70.97(11) . . ? C8 C3 Cr1 125.49(15) . . ? C3 C4 C5 108.00(18) . . ? C3 C4 C9 126.8(2) . . ? C5 C4 C9 125.2(2) . . ? C3 C4 Cr1 71.15(11) . . ? C5 C4 Cr1 71.28(11) . . ? C9 C4 Cr1 125.82(17) . . ? C1 C5 C4 108.20(17) . . ? C1 C5 C10 126.3(2) . . ? C4 C5 C10 125.3(2) . . ? C1 C5 Cr1 71.31(11) . . ? C4 C5 Cr1 70.94(11) . . ? C10 C5 Cr1 127.11(15) . . ? C1 C6 H6A 109.5 . . ? C1 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C1 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C2 Cr1 C4 63.17(8) . . ? C2 Cr1 C3 37.88(8) . . ? C4 Cr1 C3 37.72(8) . . ? C2 Cr1 C5 63.01(7) . . ? C4 Cr1 C5 37.78(8) . . ? C3 Cr1 C5 63.08(7) . . ? C2 Cr1 C1 37.73(7) . . ? C4 Cr1 C1 63.13(8) . . ? C3 Cr1 C1 63.20(8) . . ? C5 Cr1 C1 37.62(7) . . ? C2 Cr1 P51 155.1(4) . . ? C4 Cr1 P51 113.0(4) . . ? C3 Cr1 P51 149.6(4) . . ? C5 Cr1 P51 98.3(4) . . ? C1 Cr1 P51 117.5(4) . . ? C2 Cr1 P31 113.5(5) . . ? C4 Cr1 P31 116.0(4) . . ? C3 Cr1 P31 97.6(4) . . ? C5 Cr1 P31 153.6(5) . . ? C1 Cr1 P31 150.6(5) . . ? P51 Cr1 P31 90.6(6) . . ? C2 Cr1 P11 116.7(5) . . ? C4 Cr1 P11 150.1(6) . . ? C3 Cr1 P11 154.4(5) . . ? C5 Cr1 P11 113.2(5) . . ? C1 Cr1 P11 97.9(5) . . ? P51 Cr1 P11 53.2(6) . . ? P31 Cr1 P11 92.0(6) . . ? C2 Cr1 P21 98.1(3) . . ? C4 Cr1 P21 154.2(4) . . ? C3 Cr1 P21 116.7(4) . . ? C5 Cr1 P21 150.5(5) . . ? C1 Cr1 P21 113.7(5) . . ? P51 Cr1 P21 91.5(6) . . ? P31 Cr1 P21 52.8(8) . . ? P11 Cr1 P21 52.8(7) . . ? C2 Cr1 P41 151.0(6) . . ? C4 Cr1 P41 98.2(4) . . ? C3 Cr1 P41 113.9(5) . . ? C5 Cr1 P41 116.7(5) . . ? C1 Cr1 P41 154.0(5) . . ? P51 Cr1 P41 50.7(7) . . ? P31 Cr1 P41 52.4(8) . . ? P11 Cr1 P41 90.7(7) . . ? P21 Cr1 P41 91.0(6) . . ? C2 Cr1 P52 136.1(2) . . ? C4 Cr1 P52 128.6(3) . . ? C3 Cr1 P52 163.5(2) . . ? C5 Cr1 P52 100.4(2) . . ? C1 Cr1 P52 103.9(2) . . ? P51 Cr1 P52 25.6(5) . . ? P31 Cr1 P52 98.2(4) . . ? P11 Cr1 P52 29.2(7) . . ? P21 Cr1 P52 77.1(5) . . ? P41 Cr1 P52 72.7(6) . . ? C2 Cr1 P2 96.1(2) . . ? C4 Cr1 P2 146.6(2) . . ? C3 Cr1 P2 110.0(2) . . ? C5 Cr1 P2 154.7(3) . . ? C1 Cr1 P2 117.0(3) . . ? P51 Cr1 P2 96.7(5) . . ? P31 Cr1 P2 45.8(6) . . ? P11 Cr1 P2 61.5(6) . . ? P21 Cr1 P2 9.0(8) . . ? P41 Cr1 P2 88.6(6) . . ? P52 Cr1 P2 84.6(3) . . ? P51 P11 P21 108.3(9) . . ? P51 P11 Cr1 65.1(6) . . ? P21 P11 Cr1 64.2(7) . . ? P51 P11 Cr2 64.1(6) . . ? P21 P11 Cr2 62.7(7) . . ? Cr1 P11 Cr2 83.1(5) . . ? P31 P21 P11 107.1(8) . . ? P31 P21 Cr2 64.1(7) . . ? P11 P21 Cr2 64.5(6) . . ? P31 P21 Cr1 63.0(6) . . ? P11 P21 Cr1 63.0(6) . . ? Cr2 P21 Cr1 83.3(4) . . ? P41 P31 P21 108.3(8) . . ? P41 P31 Cr1 65.0(7) . . ? P21 P31 Cr1 64.2(6) . . ? P41 P31 Cr2 64.2(7) . . ? P21 P31 Cr2 62.9(6) . . ? Cr1 P31 Cr2 83.3(4) . . ? P31 P41 P51 109.1(9) . . ? P31 P41 Cr2 63.5(6) . . ? P51 P41 Cr2 64.9(7) . . ? P31 P41 Cr1 62.6(6) . . ? P51 P41 Cr1 65.1(8) . . ? Cr2 P41 Cr1 81.9(5) . . ? P11 P51 P41 107.2(9) . . ? P11 P51 Cr2 62.9(7) . . ? P41 P51 Cr2 64.0(6) . . ? P11 P51 Cr1 61.7(7) . . ? P41 P51 Cr1 64.1(7) . . ? Cr2 P51 Cr1 81.1(5) . . ? P2 P1 P5 108.0(5) . . ? P2 P1 Cr1 63.0(4) . . ? P5 P1 Cr1 63.5(3) . . ? P2 P1 Cr2 63.8(4) . . ? P5 P1 Cr2 63.3(3) . . ? Cr1 P1 Cr2 80.7(3) . . ? P1 P2 P3 107.9(5) . . ? P1 P2 Cr1 63.5(3) . . ? P3 P2 Cr1 63.8(4) . . ? P1 P2 Cr2 63.2(3) . . ? P3 P2 Cr2 62.9(4) . . ? Cr1 P2 Cr2 80.6(3) . . ? P4 P3 P2 108.4(5) . . ? P4 P3 Cr2 64.3(4) . . ? P2 P3 Cr2 63.8(3) . . ? P4 P3 Cr1 63.2(4) . . ? P2 P3 Cr1 62.7(3) . . ? Cr2 P3 Cr1 80.6(3) . . ? P5 P4 P3 107.0(5) . . ? P5 P4 Cr1 62.8(4) . . ? P3 P4 Cr1 63.8(3) . . ? P5 P4 Cr2 62.2(4) . . ? P3 P4 Cr2 62.9(3) . . ? Cr1 P4 Cr2 80.3(3) . . ? P4 P5 P1 108.7(5) . . ? P4 P5 Cr2 64.0(3) . . ? P1 P5 Cr2 64.0(4) . . ? P4 P5 Cr1 63.1(3) . . ? P1 P5 Cr1 63.8(4) . . ? Cr2 P5 Cr1 81.2(2) . . ? P52 P12 P22 107.0(5) . . ? P52 P12 Cr2 63.0(3) . . ? P22 P12 Cr2 62.3(3) . . ? P52 P12 Cr1 63.0(3) . . ? P22 P12 Cr1 63.2(3) . . ? Cr2 P12 Cr1 79.8(3) . . ? P32 P22 P12 109.5(5) . . ? P32 P22 Cr2 64.0(4) . . ? P12 P22 Cr2 64.0(3) . . ? P32 P22 Cr1 64.1(3) . . ? P12 P22 Cr1 63.5(3) . . ? Cr2 P22 Cr1 80.7(3) . . ? P22 P32 P42 107.0(5) . . ? P22 P32 Cr2 63.0(3) . . ? P42 P32 Cr2 62.7(3) . . ? P22 P32 Cr1 63.6(3) . . ? P42 P32 Cr1 62.4(3) . . ? Cr2 P32 Cr1 80.0(3) . . ? P52 P42 P32 108.6(5) . . ? P52 P42 Cr2 63.6(4) . . ? P32 P42 Cr2 63.4(3) . . ? P52 P42 Cr1 63.7(3) . . ? P32 P42 Cr1 64.1(3) . . ? Cr2 P42 Cr1 81.1(3) . . ? P42 P52 P12 107.8(5) . . ? P42 P52 Cr1 62.9(3) . . ? P12 P52 Cr1 63.7(4) . . ? P42 P52 Cr2 62.8(3) . . ? P12 P52 Cr2 63.6(3) . . ? Cr1 P52 Cr2 80.4(3) . . ? C11 Cr2 C15 37.84(8) . . ? C11 Cr2 C13 62.78(8) . . ? C15 Cr2 C13 63.10(7) . . ? C11 Cr2 C14 62.97(7) . . ? C15 Cr2 C14 37.76(7) . . ? C13 Cr2 C14 37.69(7) . . ? C11 Cr2 C12 37.65(8) . . ? C15 Cr2 C12 63.24(8) . . ? C13 Cr2 C12 37.50(8) . . ? C14 Cr2 C12 62.99(8) . . ? C11 Cr2 P51 124.0(4) . . ? C15 Cr2 P51 98.3(4) . . ? C13 Cr2 P51 140.6(4) . . ? C14 Cr2 P51 106.2(5) . . ? C12 Cr2 P51 160.8(4) . . ? C11 Cr2 P21 106.9(5) . . ? C15 Cr2 P21 141.2(5) . . ? C13 Cr2 P21 124.1(5) . . ? C14 Cr2 P21 161.1(4) . . ? C12 Cr2 P21 99.0(4) . . ? P51 Cr2 P21 92.7(6) . . ? C11 Cr2 P31 142.8(5) . . ? C15 Cr2 P31 162.1(4) . . ? C13 Cr2 P31 100.4(4) . . ? C14 Cr2 P31 124.7(5) . . ? C12 Cr2 P31 108.7(4) . . ? P51 Cr2 P31 90.6(6) . . ? P21 Cr2 P31 53.0(8) . . ? C11 Cr2 P41 160.9(5) . . ? C15 Cr2 P41 123.4(5) . . ? C13 Cr2 P41 108.3(6) . . ? C14 Cr2 P41 99.3(5) . . ? C12 Cr2 P41 142.6(6) . . ? P51 Cr2 P41 51.1(8) . . ? P21 Cr2 P41 92.1(6) . . ? P31 Cr2 P41 52.4(8) . . ? C11 Cr2 P11 99.5(4) . . ? C15 Cr2 P11 107.0(5) . . ? C13 Cr2 P11 161.4(4) . . ? C14 Cr2 P11 141.2(6) . . ? C12 Cr2 P11 124.6(5) . . ? P51 Cr2 P11 53.0(6) . . ? P21 Cr2 P11 52.8(8) . . ? P31 Cr2 P11 90.8(6) . . ? P41 Cr2 P11 90.4(7) . . ? C11 Cr2 P22 119.4(2) . . ? C15 Cr2 P22 157.2(2) . . ? C13 Cr2 P22 109.0(2) . . ? C14 Cr2 P22 144.8(2) . . ? C12 Cr2 P22 97.07(18) . . ? P51 Cr2 P22 99.8(5) . . ? P21 Cr2 P22 24.3(7) . . ? P31 Cr2 P22 30.8(7) . . ? P41 Cr2 P22 79.0(6) . . ? P11 Cr2 P22 73.8(6) . . ? C11 Cr2 P52 108.3(2) . . ? C15 Cr2 P52 96.7(2) . . ? C13 Cr2 P52 157.3(3) . . ? C14 Cr2 P52 119.8(3) . . ? C12 Cr2 P52 144.1(2) . . ? P51 Cr2 P52 25.7(5) . . ? P21 Cr2 P52 77.8(6) . . ? P31 Cr2 P52 97.9(4) . . ? P41 Cr2 P52 73.1(7) . . ? P11 Cr2 P52 29.1(7) . . ? P22 Cr2 P52 93.6(3) . . ? C12 C11 C15 108.50(18) . . ? C12 C11 C16 125.8(2) . . ? C15 C11 C16 125.7(2) . . ? C12 C11 Cr2 71.57(12) . . ? C15 C11 Cr2 71.18(11) . . ? C16 C11 Cr2 125.42(15) . . ? C13 C12 C11 107.67(18) . . ? C13 C12 C17 126.2(2) . . ? C11 C12 C17 126.0(2) . . ? C13 C12 Cr2 71.11(12) . . ? C11 C12 Cr2 70.78(12) . . ? C17 C12 Cr2 126.82(16) . . ? C12 C13 C14 108.39(18) . . ? C12 C13 C18 126.5(2) . . ? C14 C13 C18 125.0(2) . . ? C12 C13 Cr2 71.39(12) . . ? C14 C13 Cr2 71.17(11) . . ? C18 C13 Cr2 126.34(15) . . ? C13 C14 C15 107.95(17) . . ? C13 C14 C19 125.2(2) . . ? C15 C14 C19 126.8(2) . . ? C13 C14 Cr2 71.14(11) . . ? C15 C14 Cr2 70.95(11) . . ? C19 C14 Cr2 125.98(15) . . ? C14 C15 C11 107.49(17) . . ? C14 C15 C20 126.5(2) . . ? C11 C15 C20 125.97(19) . . ? C14 C15 Cr2 71.29(11) . . ? C11 C15 Cr2 70.98(11) . . ? C20 C15 Cr2 125.54(14) . . ? C11 C16 H16A 109.5 . . ? C11 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C11 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 C1 C2 C3 -0.3(2) . . . . ? C6 C1 C2 C3 176.3(2) . . . . ? Cr1 C1 C2 C3 -62.08(14) . . . . ? C5 C1 C2 C7 -177.1(2) . . . . ? C6 C1 C2 C7 -0.5(3) . . . . ? Cr1 C1 C2 C7 121.1(2) . . . . ? C5 C1 C2 Cr1 61.77(14) . . . . ? C6 C1 C2 Cr1 -121.7(2) . . . . ? C1 C2 C3 C4 0.4(2) . . . . ? C7 C2 C3 C4 177.1(2) . . . . ? Cr1 C2 C3 C4 -61.93(14) . . . . ? C1 C2 C3 C8 -177.1(2) . . . . ? C7 C2 C3 C8 -0.3(3) . . . . ? Cr1 C2 C3 C8 120.6(2) . . . . ? C1 C2 C3 Cr1 62.31(14) . . . . ? C7 C2 C3 Cr1 -120.9(2) . . . . ? C2 C3 C4 C5 -0.3(2) . . . . ? C8 C3 C4 C5 177.2(2) . . . . ? Cr1 C3 C4 C5 -62.13(14) . . . . ? C2 C3 C4 C9 -177.0(2) . . . . ? C8 C3 C4 C9 0.5(4) . . . . ? Cr1 C3 C4 C9 121.1(2) . . . . ? C2 C3 C4 Cr1 61.83(14) . . . . ? C8 C3 C4 Cr1 -120.7(2) . . . . ? C2 C1 C5 C4 0.1(2) . . . . ? C6 C1 C5 C4 -176.4(2) . . . . ? Cr1 C1 C5 C4 61.71(14) . . . . ? C2 C1 C5 C10 175.6(2) . . . . ? C6 C1 C5 C10 -0.9(3) . . . . ? Cr1 C1 C5 C10 -122.8(2) . . . . ? C2 C1 C5 Cr1 -61.58(13) . . . . ? C6 C1 C5 Cr1 121.9(2) . . . . ? C3 C4 C5 C1 0.1(2) . . . . ? C9 C4 C5 C1 176.9(2) . . . . ? Cr1 C4 C5 C1 -61.94(14) . . . . ? C3 C4 C5 C10 -175.4(2) . . . . ? C9 C4 C5 C10 1.4(3) . . . . ? Cr1 C4 C5 C10 122.5(2) . . . . ? C3 C4 C5 Cr1 62.05(14) . . . . ? C9 C4 C5 Cr1 -121.1(2) . . . . ? C1 C2 Cr1 C4 -79.99(13) . . . . ? C3 C2 Cr1 C4 37.48(12) . . . . ? C7 C2 Cr1 C4 159.3(2) . . . . ? C1 C2 Cr1 C3 -117.47(17) . . . . ? C7 C2 Cr1 C3 121.8(2) . . . . ? C1 C2 Cr1 C5 -37.41(12) . . . . ? C3 C2 Cr1 C5 80.05(13) . . . . ? C7 C2 Cr1 C5 -158.1(2) . . . . ? C3 C2 Cr1 C1 117.47(17) . . . . ? C7 C2 Cr1 C1 -120.7(3) . . . . ? C1 C2 Cr1 P51 7.1(10) . . . . ? C3 C2 Cr1 P51 124.6(10) . . . . ? C7 C2 Cr1 P51 -113.6(10) . . . . ? C1 C2 Cr1 P31 171.6(6) . . . . ? C3 C2 Cr1 P31 -71.0(6) . . . . ? C7 C2 Cr1 P31 50.9(6) . . . . ? C1 C2 Cr1 P11 66.4(6) . . . . ? C3 C2 Cr1 P11 -176.1(6) . . . . ? C7 C2 Cr1 P11 -54.3(7) . . . . ? C1 C2 Cr1 P21 118.7(6) . . . . ? C3 C2 Cr1 P21 -123.8(6) . . . . ? C7 C2 Cr1 P21 -2.0(6) . . . . ? C1 C2 Cr1 P41 -134.3(10) . . . . ? C3 C2 Cr1 P41 -16.8(10) . . . . ? C7 C2 Cr1 P41 105.0(11) . . . . ? C1 C2 Cr1 P52 38.9(4) . . . . ? C3 C2 Cr1 P52 156.4(4) . . . . ? C7 C2 Cr1 P52 -81.8(4) . . . . ? C1 C2 Cr1 P2 127.5(4) . . . . ? C3 C2 Cr1 P2 -115.0(4) . . . . ? C7 C2 Cr1 P2 6.8(4) . . . . ? C3 C4 Cr1 C2 -37.65(12) . . . . ? C5 C4 Cr1 C2 79.77(13) . . . . ? C9 C4 Cr1 C2 -159.9(2) . . . . ? C5 C4 Cr1 C3 117.41(18) . . . . ? C9 C4 Cr1 C3 -122.2(3) . . . . ? C3 C4 Cr1 C5 -117.41(18) . . . . ? C9 C4 Cr1 C5 120.3(3) . . . . ? C3 C4 Cr1 C1 -80.14(13) . . . . ? C5 C4 Cr1 C1 37.27(11) . . . . ? C9 C4 Cr1 C1 157.6(2) . . . . ? C3 C4 Cr1 P51 169.6(4) . . . . ? C5 C4 Cr1 P51 -73.0(4) . . . . ? C9 C4 Cr1 P51 47.3(4) . . . . ? C3 C4 Cr1 P31 66.9(6) . . . . ? C5 C4 Cr1 P31 -175.7(6) . . . . ? C9 C4 Cr1 P31 -55.3(6) . . . . ? C3 C4 Cr1 P11 -135.1(10) . . . . ? C5 C4 Cr1 P11 -17.7(10) . . . . ? C9 C4 Cr1 P11 102.6(10) . . . . ? C3 C4 Cr1 P21 9.2(12) . . . . ? C5 C4 Cr1 P21 126.6(12) . . . . ? C9 C4 Cr1 P21 -113.1(12) . . . . ? C3 C4 Cr1 P41 118.9(7) . . . . ? C5 C4 Cr1 P41 -123.7(7) . . . . ? C9 C4 Cr1 P41 -3.3(7) . . . . ? C3 C4 Cr1 P52 -166.7(3) . . . . ? C5 C4 Cr1 P52 -49.3(3) . . . . ? C9 C4 Cr1 P52 71.1(4) . . . . ? C3 C4 Cr1 P2 18.9(6) . . . . ? C5 C4 Cr1 P2 136.3(6) . . . . ? C9 C4 Cr1 P2 -103.3(6) . . . . ? C4 C3 Cr1 C2 117.43(17) . . . . ? C8 C3 Cr1 C2 -121.7(3) . . . . ? C2 C3 Cr1 C4 -117.43(17) . . . . ? C8 C3 Cr1 C4 120.9(3) . . . . ? C4 C3 Cr1 C5 37.58(12) . . . . ? C2 C3 Cr1 C5 -79.85(12) . . . . ? C8 C3 Cr1 C5 158.5(2) . . . . ? C4 C3 Cr1 C1 79.96(13) . . . . ? C2 C3 Cr1 C1 -37.47(11) . . . . ? C8 C3 Cr1 C1 -159.1(2) . . . . ? C4 C3 Cr1 P51 -19.2(7) . . . . ? C2 C3 Cr1 P51 -136.7(7) . . . . ? C8 C3 Cr1 P51 101.7(7) . . . . ? C4 C3 Cr1 P31 -123.5(6) . . . . ? C2 C3 Cr1 P31 119.1(6) . . . . ? C8 C3 Cr1 P31 -2.6(6) . . . . ? C4 C3 Cr1 P11 125.5(13) . . . . ? C2 C3 Cr1 P11 8.1(13) . . . . ? C8 C3 Cr1 P11 -113.6(13) . . . . ? C4 C3 Cr1 P21 -175.5(6) . . . . ? C2 C3 Cr1 P21 67.0(6) . . . . ? C8 C3 Cr1 P21 -54.6(6) . . . . ? C4 C3 Cr1 P41 -71.4(6) . . . . ? C2 C3 Cr1 P41 171.2(6) . . . . ? C8 C3 Cr1 P41 49.5(6) . . . . ? C4 C3 Cr1 P52 39.3(10) . . . . ? C2 C3 Cr1 P52 -78.1(10) . . . . ? C8 C3 Cr1 P52 160.2(10) . . . . ? C4 C3 Cr1 P2 -169.1(4) . . . . ? C2 C3 Cr1 P2 73.5(4) . . . . ? C8 C3 Cr1 P2 -48.2(4) . . . . ? C1 C5 Cr1 C2 37.52(11) . . . . ? C4 C5 Cr1 C2 -80.23(13) . . . . ? C10 C5 Cr1 C2 159.4(2) . . . . ? C1 C5 Cr1 C4 117.75(17) . . . . ? C10 C5 Cr1 C4 -120.4(2) . . . . ? C1 C5 Cr1 C3 80.23(13) . . . . ? C4 C5 Cr1 C3 -37.52(12) . . . . ? C10 C5 Cr1 C3 -157.9(2) . . . . ? C4 C5 Cr1 C1 -117.75(17) . . . . ? C10 C5 Cr1 C1 121.8(2) . . . . ? C1 C5 Cr1 P51 -125.1(4) . . . . ? C4 C5 Cr1 P51 117.2(4) . . . . ? C10 C5 Cr1 P51 -3.3(4) . . . . ? C1 C5 Cr1 P31 126.5(12) . . . . ? C4 C5 Cr1 P31 8.7(12) . . . . ? C10 C5 Cr1 P31 -111.7(12) . . . . ? C1 C5 Cr1 P11 -71.7(6) . . . . ? C4 C5 Cr1 P11 170.5(6) . . . . ? C10 C5 Cr1 P11 50.1(6) . . . . ? C1 C5 Cr1 P21 -17.0(9) . . . . ? C4 C5 Cr1 P21 -134.8(9) . . . . ? C10 C5 Cr1 P21 104.8(9) . . . . ? C1 C5 Cr1 P41 -175.1(7) . . . . ? C4 C5 Cr1 P41 67.2(7) . . . . ? C10 C5 Cr1 P41 -53.2(7) . . . . ? C1 C5 Cr1 P52 -99.3(3) . . . . ? C4 C5 Cr1 P52 143.0(3) . . . . ? C10 C5 Cr1 P52 22.6(3) . . . . ? C1 C5 Cr1 P2 0.4(6) . . . . ? C4 C5 Cr1 P2 -117.4(6) . . . . ? C10 C5 Cr1 P2 122.2(6) . . . . ? C5 C1 Cr1 C2 -117.52(17) . . . . ? C6 C1 Cr1 C2 120.7(2) . . . . ? C5 C1 Cr1 C4 -37.42(12) . . . . ? C2 C1 Cr1 C4 80.10(13) . . . . ? C6 C1 Cr1 C4 -159.2(2) . . . . ? C5 C1 Cr1 C3 -79.90(13) . . . . ? C2 C1 Cr1 C3 37.62(12) . . . . ? C6 C1 Cr1 C3 158.3(2) . . . . ? C2 C1 Cr1 C5 117.52(17) . . . . ? C6 C1 Cr1 C5 -121.8(2) . . . . ? C5 C1 Cr1 P51 65.8(5) . . . . ? C2 C1 Cr1 P51 -176.6(5) . . . . ? C6 C1 Cr1 P51 -55.9(5) . . . . ? C5 C1 Cr1 P31 -133.4(9) . . . . ? C2 C1 Cr1 P31 -15.8(10) . . . . ? C6 C1 Cr1 P31 104.9(10) . . . . ? C5 C1 Cr1 P11 118.2(6) . . . . ? C2 C1 Cr1 P11 -124.2(6) . . . . ? C6 C1 Cr1 P11 -3.5(6) . . . . ? C5 C1 Cr1 P21 171.0(5) . . . . ? C2 C1 Cr1 P21 -71.5(5) . . . . ? C6 C1 Cr1 P21 49.2(6) . . . . ? C5 C1 Cr1 P41 10.1(13) . . . . ? C2 C1 Cr1 P41 127.6(13) . . . . ? C6 C1 Cr1 P41 -111.7(13) . . . . ? C5 C1 Cr1 P52 89.1(3) . . . . ? C2 C1 Cr1 P52 -153.4(3) . . . . ? C6 C1 Cr1 P52 -32.7(3) . . . . ? C5 C1 Cr1 P2 -179.8(3) . . . . ? C2 C1 Cr1 P2 -62.3(3) . . . . ? C6 C1 Cr1 P2 58.4(4) . . . . ? C2 Cr1 P11 P51 -153.1(5) . . . . ? C4 Cr1 P11 P51 -71.0(11) . . . . ? C3 Cr1 P11 P51 -158.6(10) . . . . ? C5 Cr1 P11 P51 -82.7(6) . . . . ? C1 Cr1 P11 P51 -118.6(6) . . . . ? P31 Cr1 P11 P51 89.3(8) . . . . ? P21 Cr1 P11 P51 127.5(9) . . . . ? P41 Cr1 P11 P51 36.8(8) . . . . ? P52 Cr1 P11 P51 -14.1(10) . . . . ? P2 Cr1 P11 P51 124.9(8) . . . . ? C2 Cr1 P11 P21 79.4(7) . . . . ? C4 Cr1 P11 P21 161.4(8) . . . . ? C3 Cr1 P11 P21 73.9(13) . . . . ? C5 Cr1 P11 P21 149.7(6) . . . . ? C1 Cr1 P11 P21 113.9(6) . . . . ? P51 Cr1 P11 P21 -127.5(9) . . . . ? P31 Cr1 P11 P21 -38.3(8) . . . . ? P41 Cr1 P11 P21 -90.7(8) . . . . ? P52 Cr1 P11 P21 -141.6(13) . . . . ? P2 Cr1 P11 P21 -2.7(8) . . . . ? C2 Cr1 P11 Cr2 142.4(3) . . . . ? C4 Cr1 P11 Cr2 -135.6(6) . . . . ? C3 Cr1 P11 Cr2 136.9(8) . . . . ? C5 Cr1 P11 Cr2 -147.3(3) . . . . ? C1 Cr1 P11 Cr2 176.9(4) . . . . ? P51 Cr1 P11 Cr2 -64.6(7) . . . . ? P31 Cr1 P11 Cr2 24.7(8) . . . . ? P21 Cr1 P11 Cr2 63.0(7) . . . . ? P41 Cr1 P11 Cr2 -27.7(8) . . . . ? P52 Cr1 P11 Cr2 -78.6(10) . . . . ? P2 Cr1 P11 Cr2 60.3(5) . . . . ? P51 P11 P21 P31 -2.9(14) . . . . ? Cr1 P11 P21 P31 46.4(8) . . . . ? Cr2 P11 P21 P31 -49.3(8) . . . . ? P51 P11 P21 Cr2 46.4(9) . . . . ? Cr1 P11 P21 Cr2 95.7(5) . . . . ? P51 P11 P21 Cr1 -49.3(9) . . . . ? Cr2 P11 P21 Cr1 -95.7(5) . . . . ? C2 Cr1 P21 P31 113.5(6) . . . . ? C4 Cr1 P21 P31 72.4(12) . . . . ? C3 Cr1 P21 P31 78.7(7) . . . . ? C5 Cr1 P21 P31 160.6(8) . . . . ? C1 Cr1 P21 P31 149.4(6) . . . . ? P51 Cr1 P21 P31 -89.6(7) . . . . ? P11 Cr1 P21 P31 -129.0(9) . . . . ? P41 Cr1 P21 P31 -38.9(9) . . . . ? P52 Cr1 P21 P31 -110.9(7) . . . . ? P2 Cr1 P21 P31 36(4) . . . . ? C2 Cr1 P21 P11 -117.5(6) . . . . ? C4 Cr1 P21 P11 -158.6(10) . . . . ? C3 Cr1 P21 P11 -152.3(6) . . . . ? C5 Cr1 P21 P11 -70.4(9) . . . . ? C1 Cr1 P21 P11 -81.6(6) . . . . ? P51 Cr1 P21 P11 39.4(7) . . . . ? P31 Cr1 P21 P11 129.0(9) . . . . ? P41 Cr1 P21 P11 90.1(9) . . . . ? P52 Cr1 P21 P11 18.1(7) . . . . ? P2 Cr1 P21 P11 165(4) . . . . ? C2 Cr1 P21 Cr2 177.8(4) . . . . ? C4 Cr1 P21 Cr2 136.7(6) . . . . ? C3 Cr1 P21 Cr2 143.0(3) . . . . ? C5 Cr1 P21 Cr2 -135.0(5) . . . . ? C1 Cr1 P21 Cr2 -146.3(3) . . . . ? P51 Cr1 P21 Cr2 -25.3(6) . . . . ? P31 Cr1 P21 Cr2 64.3(7) . . . . ? P11 Cr1 P21 Cr2 -64.7(7) . . . . ? P41 Cr1 P21 Cr2 25.5(8) . . . . ? P52 Cr1 P21 Cr2 -46.6(5) . . . . ? P2 Cr1 P21 Cr2 100(4) . . . . ? P11 P21 P31 P41 2.7(13) . . . . ? Cr2 P21 P31 P41 -46.8(9) . . . . ? Cr1 P21 P31 P41 49.1(8) . . . . ? P11 P21 P31 Cr1 -46.4(9) . . . . ? Cr2 P21 P31 Cr1 -95.8(5) . . . . ? P11 P21 P31 Cr2 49.5(8) . . . . ? Cr1 P21 P31 Cr2 95.8(5) . . . . ? C2 Cr1 P31 P41 150.3(6) . . . . ? C4 Cr1 P31 P41 79.8(7) . . . . ? C3 Cr1 P31 P41 114.4(6) . . . . ? C5 Cr1 P31 P41 73.9(12) . . . . ? C1 Cr1 P31 P41 160.8(9) . . . . ? P51 Cr1 P31 P41 -36.2(8) . . . . ? P11 Cr1 P31 P41 -89.4(9) . . . . ? P21 Cr1 P31 P41 -127.7(9) . . . . ? P52 Cr1 P31 P41 -60.7(7) . . . . ? P2 Cr1 P31 P41 -134.9(9) . . . . ? C2 Cr1 P31 P21 -82.1(6) . . . . ? C4 Cr1 P31 P21 -152.5(5) . . . . ? C3 Cr1 P31 P21 -117.9(5) . . . . ? C5 Cr1 P31 P21 -158.5(9) . . . . ? C1 Cr1 P31 P21 -71.6(10) . . . . ? P51 Cr1 P31 P21 91.4(7) . . . . ? P11 Cr1 P31 P21 38.3(7) . . . . ? P41 Cr1 P31 P21 127.7(9) . . . . ? P52 Cr1 P31 P21 66.9(7) . . . . ? P2 Cr1 P31 P21 -7.3(7) . . . . ? C2 Cr1 P31 Cr2 -145.2(3) . . . . ? C4 Cr1 P31 Cr2 144.4(3) . . . . ? C3 Cr1 P31 Cr2 179.0(4) . . . . ? C5 Cr1 P31 Cr2 138.5(7) . . . . ? C1 Cr1 P31 Cr2 -134.7(5) . . . . ? P51 Cr1 P31 Cr2 28.4(6) . . . . ? P11 Cr1 P31 Cr2 -24.8(7) . . . . ? P21 Cr1 P31 Cr2 -63.1(6) . . . . ? P41 Cr1 P31 Cr2 64.6(7) . . . . ? P52 Cr1 P31 Cr2 3.9(6) . . . . ? P2 Cr1 P31 Cr2 -70.4(5) . . . . ? P21 P31 P41 P51 -1.5(14) . . . . ? Cr1 P31 P41 P51 47.1(9) . . . . ? Cr2 P31 P41 P51 -47.6(9) . . . . ? P21 P31 P41 Cr2 46.1(8) . . . . ? Cr1 P31 P41 Cr2 94.7(6) . . . . ? P21 P31 P41 Cr1 -48.6(8) . . . . ? Cr2 P31 P41 Cr1 -94.7(6) . . . . ? C2 Cr1 P41 P31 -69.6(11) . . . . ? C4 Cr1 P41 P31 -116.7(6) . . . . ? C3 Cr1 P41 P31 -80.8(6) . . . . ? C5 Cr1 P41 P31 -151.5(5) . . . . ? C1 Cr1 P41 P31 -158.3(10) . . . . ? P51 Cr1 P41 P31 130.3(9) . . . . ? P11 Cr1 P41 P31 92.0(8) . . . . ? P21 Cr1 P41 P31 39.1(8) . . . . ? P52 Cr1 P41 P31 115.3(7) . . . . ? P2 Cr1 P41 P31 30.5(7) . . . . ? C2 Cr1 P41 P51 160.1(9) . . . . ? C4 Cr1 P41 P51 113.1(6) . . . . ? C3 Cr1 P41 P51 148.9(6) . . . . ? C5 Cr1 P41 P51 78.3(7) . . . . ? C1 Cr1 P41 P51 71.4(13) . . . . ? P31 Cr1 P41 P51 -130.3(9) . . . . ? P11 Cr1 P41 P51 -38.3(8) . . . . ? P21 Cr1 P41 P51 -91.1(8) . . . . ? P52 Cr1 P41 P51 -14.9(7) . . . . ? P2 Cr1 P41 P51 -99.8(7) . . . . ? C2 Cr1 P41 Cr2 -133.8(6) . . . . ? C4 Cr1 P41 Cr2 179.1(5) . . . . ? C3 Cr1 P41 Cr2 -145.0(4) . . . . ? C5 Cr1 P41 Cr2 144.3(3) . . . . ? C1 Cr1 P41 Cr2 137.5(7) . . . . ? P51 Cr1 P41 Cr2 66.0(7) . . . . ? P31 Cr1 P41 Cr2 -64.2(7) . . . . ? P11 Cr1 P41 Cr2 27.7(8) . . . . ? P21 Cr1 P41 Cr2 -25.1(8) . . . . ? P52 Cr1 P41 Cr2 51.1(5) . . . . ? P2 Cr1 P41 Cr2 -33.7(6) . . . . ? P21 P11 P51 P41 1.9(15) . . . . ? Cr1 P11 P51 P41 -46.8(9) . . . . ? Cr2 P11 P51 P41 47.7(9) . . . . ? P21 P11 P51 Cr2 -45.7(8) . . . . ? Cr1 P11 P51 Cr2 -94.5(5) . . . . ? P21 P11 P51 Cr1 48.8(9) . . . . ? Cr2 P11 P51 Cr1 94.5(5) . . . . ? P31 P41 P51 P11 -0.3(15) . . . . ? Cr2 P41 P51 P11 -47.1(9) . . . . ? Cr1 P41 P51 P11 45.6(9) . . . . ? P31 P41 P51 Cr2 46.8(9) . . . . ? Cr1 P41 P51 Cr2 92.7(5) . . . . ? P31 P41 P51 Cr1 -45.8(9) . . . . ? Cr2 P41 P51 Cr1 -92.7(5) . . . . ? C2 Cr1 P51 P11 73.8(12) . . . . ? C4 Cr1 P51 P11 149.2(6) . . . . ? C3 Cr1 P51 P11 161.8(7) . . . . ? C5 Cr1 P51 P11 112.9(7) . . . . ? C1 Cr1 P51 P11 78.7(7) . . . . ? P31 Cr1 P51 P11 -92.0(8) . . . . ? P21 Cr1 P51 P11 -39.2(9) . . . . ? P41 Cr1 P51 P11 -129.2(10) . . . . ? P52 Cr1 P51 P11 16.0(13) . . . . ? P2 Cr1 P51 P11 -46.5(8) . . . . ? C2 Cr1 P51 P41 -157.0(8) . . . . ? C4 Cr1 P51 P41 -81.5(7) . . . . ? C3 Cr1 P51 P41 -68.9(10) . . . . ? C5 Cr1 P51 P41 -117.8(6) . . . . ? C1 Cr1 P51 P41 -152.1(6) . . . . ? P31 Cr1 P51 P41 37.2(8) . . . . ? P11 Cr1 P51 P41 129.2(10) . . . . ? P21 Cr1 P51 P41 90.0(8) . . . . ? P52 Cr1 P51 P41 145.2(16) . . . . ? P2 Cr1 P51 P41 82.7(7) . . . . ? C2 Cr1 P51 Cr2 137.7(7) . . . . ? C4 Cr1 P51 Cr2 -146.9(2) . . . . ? C3 Cr1 P51 Cr2 -134.2(5) . . . . ? C5 Cr1 P51 Cr2 176.9(2) . . . . ? C1 Cr1 P51 Cr2 142.6(2) . . . . ? P31 Cr1 P51 Cr2 -28.1(6) . . . . ? P11 Cr1 P51 Cr2 63.9(7) . . . . ? P21 Cr1 P51 Cr2 24.7(6) . . . . ? P41 Cr1 P51 Cr2 -65.3(6) . . . . ? P52 Cr1 P51 Cr2 79.9(13) . . . . ? P2 Cr1 P51 Cr2 17.4(5) . . . . ? C2 Cr1 P1 P2 82.2(4) . . . . ? C4 Cr1 P1 P2 152.2(6) . . . . ? C3 Cr1 P1 P2 68.8(6) . . . . ? C5 Cr1 P1 P2 151.7(4) . . . . ? C1 Cr1 P1 P2 118.6(4) . . . . ? P51 Cr1 P1 P2 -124.0(6) . . . . ? P31 Cr1 P1 P2 -32.4(7) . . . . ? P11 Cr1 P1 P2 -146(4) . . . . ? P21 Cr1 P1 P2 1.7(9) . . . . ? P41 Cr1 P1 P2 -84.3(7) . . . . ? P52 Cr1 P1 P2 -138.0(6) . . . . ? C2 Cr1 P1 P5 -147.9(2) . . . . ? C4 Cr1 P1 P5 -77.9(7) . . . . ? C3 Cr1 P1 P5 -161.3(3) . . . . ? C5 Cr1 P1 P5 -78.4(3) . . . . ? C1 Cr1 P1 P5 -111.5(3) . . . . ? P51 Cr1 P1 P5 5.9(6) . . . . ? P31 Cr1 P1 P5 97.6(6) . . . . ? P11 Cr1 P1 P5 -16(4) . . . . ? P21 Cr1 P1 P5 131.6(7) . . . . ? P41 Cr1 P1 P5 45.6(7) . . . . ? P52 Cr1 P1 P5 -8.0(3) . . . . ? P2 Cr1 P1 P5 129.9(5) . . . . ? C2 Cr1 P1 Cr2 147.38(19) . . . . ? C4 Cr1 P1 Cr2 -142.6(4) . . . . ? C3 Cr1 P1 Cr2 134.0(3) . . . . ? C5 Cr1 P1 Cr2 -143.09(17) . . . . ? C1 Cr1 P1 Cr2 -176.2(2) . . . . ? P51 Cr1 P1 Cr2 -58.8(5) . . . . ? P31 Cr1 P1 Cr2 32.9(6) . . . . ? P11 Cr1 P1 Cr2 -81(4) . . . . ? P21 Cr1 P1 Cr2 66.9(6) . . . . ? P41 Cr1 P1 Cr2 -19.1(7) . . . . ? P52 Cr1 P1 Cr2 -72.7(4) . . . . ? P2 Cr1 P1 Cr2 65.2(4) . . . . ? P5 P1 P2 P3 1.0(8) . . . . ? Cr1 P1 P2 P3 47.2(5) . . . . ? Cr2 P1 P2 P3 -45.6(5) . . . . ? P5 P1 P2 Cr1 -46.2(4) . . . . ? Cr2 P1 P2 Cr1 -92.8(3) . . . . ? P5 P1 P2 Cr2 46.6(4) . . . . ? Cr1 P1 P2 Cr2 92.8(3) . . . . ? C2 Cr1 P2 P1 -111.1(4) . . . . ? C4 Cr1 P2 P1 -159.6(4) . . . . ? C3 Cr1 P2 P1 -147.4(3) . . . . ? C5 Cr1 P2 P1 -78.3(6) . . . . ? C1 Cr1 P2 P1 -78.1(4) . . . . ? P51 Cr1 P2 P1 47.4(5) . . . . ? P31 Cr1 P2 P1 131.7(7) . . . . ? P11 Cr1 P2 P1 6.0(8) . . . . ? P21 Cr1 P2 P1 -8(4) . . . . ? P41 Cr1 P2 P1 97.6(7) . . . . ? P52 Cr1 P2 P1 24.8(3) . . . . ? C2 Cr1 P2 P3 120.0(4) . . . . ? C4 Cr1 P2 P3 71.5(6) . . . . ? C3 Cr1 P2 P3 83.7(4) . . . . ? C5 Cr1 P2 P3 152.8(5) . . . . ? C1 Cr1 P2 P3 153.0(3) . . . . ? P51 Cr1 P2 P3 -81.5(5) . . . . ? P31 Cr1 P2 P3 2.8(9) . . . . ? P11 Cr1 P2 P3 -122.9(7) . . . . ? P21 Cr1 P2 P3 -137(4) . . . . ? P41 Cr1 P2 P3 -31.3(7) . . . . ? P52 Cr1 P2 P3 -104.1(4) . . . . ? C2 Cr1 P2 Cr2 -175.7(3) . . . . ? C4 Cr1 P2 Cr2 135.8(3) . . . . ? C3 Cr1 P2 Cr2 148.01(18) . . . . ? C5 Cr1 P2 Cr2 -142.9(4) . . . . ? C1 Cr1 P2 Cr2 -142.67(19) . . . . ? P51 Cr1 P2 Cr2 -17.2(4) . . . . ? P31 Cr1 P2 Cr2 67.1(6) . . . . ? P11 Cr1 P2 Cr2 -58.6(6) . . . . ? P21 Cr1 P2 Cr2 -72(4) . . . . ? P41 Cr1 P2 Cr2 33.0(7) . . . . ? P52 Cr1 P2 Cr2 -39.8(3) . . . . ? P1 P2 P3 P4 -1.9(8) . . . . ? Cr1 P2 P3 P4 45.1(5) . . . . ? Cr2 P2 P3 P4 -47.6(5) . . . . ? P1 P2 P3 Cr2 45.7(5) . . . . ? Cr1 P2 P3 Cr2 92.8(3) . . . . ? P1 P2 P3 Cr1 -47.0(5) . . . . ? Cr2 P2 P3 Cr1 -92.8(3) . . . . ? C2 Cr1 P3 P4 152.6(4) . . . . ? C4 Cr1 P3 P4 82.8(4) . . . . ? C3 Cr1 P3 P4 119.0(4) . . . . ? C5 Cr1 P3 P4 70.2(6) . . . . ? C1 Cr1 P3 P4 153.7(6) . . . . ? P51 Cr1 P3 P4 -30.7(5) . . . . ? P31 Cr1 P3 P4 -146(5) . . . . ? P11 Cr1 P3 P4 -83.3(7) . . . . ? P21 Cr1 P3 P4 -124.1(7) . . . . ? P41 Cr1 P3 P4 2.1(10) . . . . ? P52 Cr1 P3 P4 -54.0(5) . . . . ? P2 Cr1 P3 P4 -131.2(5) . . . . ? C2 Cr1 P3 P2 -76.2(3) . . . . ? C4 Cr1 P3 P2 -146.0(3) . . . . ? C3 Cr1 P3 P2 -109.8(3) . . . . ? C5 Cr1 P3 P2 -158.6(4) . . . . ? C1 Cr1 P3 P2 -75.1(7) . . . . ? P51 Cr1 P3 P2 100.4(5) . . . . ? P31 Cr1 P3 P2 -15(4) . . . . ? P11 Cr1 P3 P2 47.9(7) . . . . ? P21 Cr1 P3 P2 7.1(7) . . . . ? P41 Cr1 P3 P2 133.3(8) . . . . ? P52 Cr1 P3 P2 77.2(4) . . . . ? C2 Cr1 P3 Cr2 -141.57(18) . . . . ? C4 Cr1 P3 Cr2 148.65(18) . . . . ? C3 Cr1 P3 Cr2 -175.1(2) . . . . ? C5 Cr1 P3 Cr2 136.1(3) . . . . ? C1 Cr1 P3 Cr2 -140.4(4) . . . . ? P51 Cr1 P3 Cr2 35.1(5) . . . . ? P31 Cr1 P3 Cr2 -80(4) . . . . ? P11 Cr1 P3 Cr2 -17.4(6) . . . . ? P21 Cr1 P3 Cr2 -58.2(5) . . . . ? P41 Cr1 P3 Cr2 68.0(7) . . . . ? P52 Cr1 P3 Cr2 11.9(4) . . . . ? P2 Cr1 P3 Cr2 -65.3(3) . . . . ? P2 P3 P4 P5 2.0(8) . . . . ? Cr2 P3 P4 P5 -45.4(4) . . . . ? Cr1 P3 P4 P5 46.9(4) . . . . ? P2 P3 P4 Cr1 -44.9(5) . . . . ? Cr2 P3 P4 Cr1 -92.3(3) . . . . ? P2 P3 P4 Cr2 47.4(5) . . . . ? Cr1 P3 P4 Cr2 92.3(3) . . . . ? C2 Cr1 P4 P5 156.2(5) . . . . ? C4 Cr1 P4 P5 120.8(3) . . . . ? C3 Cr1 P4 P5 154.4(2) . . . . ? C5 Cr1 P4 P5 84.6(3) . . . . ? C1 Cr1 P4 P5 72.1(6) . . . . ? P51 Cr1 P4 P5 4.9(8) . . . . ? P31 Cr1 P4 P5 -123.1(6) . . . . ? P11 Cr1 P4 P5 -29.6(6) . . . . ? P21 Cr1 P4 P5 -82.1(6) . . . . ? P41 Cr1 P4 P5 -140(5) . . . . ? P52 Cr1 P4 P5 -8.2(3) . . . . ? P2 Cr1 P4 P5 -90.9(4) . . . . ? C2 Cr1 P4 P3 -75.6(6) . . . . ? C4 Cr1 P4 P3 -111.0(4) . . . . ? C3 Cr1 P4 P3 -77.4(4) . . . . ? C5 Cr1 P4 P3 -147.2(3) . . . . ? C1 Cr1 P4 P3 -159.7(4) . . . . ? P51 Cr1 P4 P3 133.1(8) . . . . ? P31 Cr1 P4 P3 5.2(7) . . . . ? P11 Cr1 P4 P3 98.6(7) . . . . ? P21 Cr1 P4 P3 46.2(7) . . . . ? P41 Cr1 P4 P3 -12(5) . . . . ? P52 Cr1 P4 P3 120.0(5) . . . . ? P2 Cr1 P4 P3 37.3(4) . . . . ? C2 Cr1 P4 Cr2 -140.1(4) . . . . ? C4 Cr1 P4 Cr2 -175.5(3) . . . . ? C3 Cr1 P4 Cr2 -141.9(2) . . . . ? C5 Cr1 P4 Cr2 148.29(18) . . . . ? C1 Cr1 P4 Cr2 135.8(3) . . . . ? P51 Cr1 P4 Cr2 68.6(7) . . . . ? P31 Cr1 P4 Cr2 -59.4(5) . . . . ? P11 Cr1 P4 Cr2 34.1(6) . . . . ? P21 Cr1 P4 Cr2 -18.4(6) . . . . ? P41 Cr1 P4 Cr2 -76(5) . . . . ? P52 Cr1 P4 Cr2 55.5(3) . . . . ? P2 Cr1 P4 Cr2 -27.2(4) . . . . ? P3 P4 P5 P1 -1.4(7) . . . . ? Cr1 P4 P5 P1 46.1(4) . . . . ? Cr2 P4 P5 P1 -47.1(4) . . . . ? P3 P4 P5 Cr2 45.7(5) . . . . ? Cr1 P4 P5 Cr2 93.2(2) . . . . ? P3 P4 P5 Cr1 -47.5(5) . . . . ? Cr2 P4 P5 Cr1 -93.2(2) . . . . ? P2 P1 P5 P4 0.2(7) . . . . ? Cr1 P1 P5 P4 -45.7(4) . . . . ? Cr2 P1 P5 P4 47.1(4) . . . . ? P2 P1 P5 Cr2 -46.9(4) . . . . ? Cr1 P1 P5 Cr2 -92.8(2) . . . . ? P2 P1 P5 Cr1 46.0(5) . . . . ? Cr2 P1 P5 Cr1 92.8(2) . . . . ? C2 Cr1 P5 P4 -161.5(3) . . . . ? C4 Cr1 P5 P4 -76.8(3) . . . . ? C3 Cr1 P5 P4 -75.5(5) . . . . ? C5 Cr1 P5 P4 -110.5(3) . . . . ? C1 Cr1 P5 P4 -147.1(3) . . . . ? P51 Cr1 P5 P4 -19(3) . . . . ? P31 Cr1 P5 P4 46.6(6) . . . . ? P11 Cr1 P5 P4 134.3(8) . . . . ? P21 Cr1 P5 P4 98.8(6) . . . . ? P41 Cr1 P5 P4 5.7(8) . . . . ? P52 Cr1 P5 P4 149.8(10) . . . . ? P2 Cr1 P5 P4 92.4(4) . . . . ? C2 Cr1 P5 P1 68.0(5) . . . . ? C4 Cr1 P5 P1 152.7(4) . . . . ? C3 Cr1 P5 P1 154.0(4) . . . . ? C5 Cr1 P5 P1 119.0(4) . . . . ? C1 Cr1 P5 P1 82.4(4) . . . . ? P51 Cr1 P5 P1 -150(3) . . . . ? P31 Cr1 P5 P1 -83.9(7) . . . . ? P11 Cr1 P5 P1 3.8(10) . . . . ? P21 Cr1 P5 P1 -31.7(7) . . . . ? P41 Cr1 P5 P1 -124.8(7) . . . . ? P52 Cr1 P5 P1 19.3(9) . . . . ? P2 Cr1 P5 P1 -38.1(5) . . . . ? C2 Cr1 P5 Cr2 133.3(2) . . . . ? C4 Cr1 P5 Cr2 -142.04(12) . . . . ? C3 Cr1 P5 Cr2 -140.7(3) . . . . ? C5 Cr1 P5 Cr2 -175.66(14) . . . . ? C1 Cr1 P5 Cr2 147.75(12) . . . . ? P51 Cr1 P5 Cr2 -85(3) . . . . ? P31 Cr1 P5 Cr2 -18.6(6) . . . . ? P11 Cr1 P5 Cr2 69.1(7) . . . . ? P21 Cr1 P5 Cr2 33.6(6) . . . . ? P41 Cr1 P5 Cr2 -59.5(5) . . . . ? P52 Cr1 P5 Cr2 84.6(9) . . . . ? P2 Cr1 P5 Cr2 27.2(4) . . . . ? C2 Cr1 P12 P52 -138.7(3) . . . . ? C4 Cr1 P12 P52 -103.0(7) . . . . ? C3 Cr1 P12 P52 -161.4(3) . . . . ? C5 Cr1 P12 P52 -73.0(4) . . . . ? C1 Cr1 P12 P52 -100.4(3) . . . . ? P51 Cr1 P12 P52 15.7(6) . . . . ? P31 Cr1 P12 P52 109.5(6) . . . . ? P11 Cr1 P12 P52 -11.9(13) . . . . ? P21 Cr1 P12 P52 137.5(9) . . . . ? P41 Cr1 P12 P52 60.8(7) . . . . ? P2 Cr1 P12 P52 137.6(6) . . . . ? C2 Cr1 P12 P22 92.6(3) . . . . ? C4 Cr1 P12 P22 128.4(7) . . . . ? C3 Cr1 P12 P22 69.9(4) . . . . ? C5 Cr1 P12 P22 158.3(3) . . . . ? C1 Cr1 P12 P22 130.9(3) . . . . ? P51 Cr1 P12 P22 -113.0(5) . . . . ? P31 Cr1 P12 P22 -19.2(6) . . . . ? P11 Cr1 P12 P22 -140.5(14) . . . . ? P21 Cr1 P12 P22 8.9(7) . . . . ? P41 Cr1 P12 P22 -67.9(7) . . . . ? P52 Cr1 P12 P22 -128.6(5) . . . . ? P2 Cr1 P12 P22 9.0(6) . . . . ? C2 Cr1 P12 Cr2 156.56(16) . . . . ? C4 Cr1 P12 Cr2 -167.7(6) . . . . ? C3 Cr1 P12 Cr2 133.87(16) . . . . ? C5 Cr1 P12 Cr2 -137.73(13) . . . . ? C1 Cr1 P12 Cr2 -165.12(17) . . . . ? P51 Cr1 P12 Cr2 -49.1(4) . . . . ? P31 Cr1 P12 Cr2 44.7(5) . . . . ? P11 Cr1 P12 Cr2 -76.6(13) . . . . ? P21 Cr1 P12 Cr2 72.8(8) . . . . ? P41 Cr1 P12 Cr2 -3.9(7) . . . . ? P52 Cr1 P12 Cr2 -64.7(3) . . . . ? P2 Cr1 P12 Cr2 72.9(4) . . . . ? P52 P12 P22 P32 -0.6(6) . . . . ? Cr2 P12 P22 P32 -46.3(4) . . . . ? Cr1 P12 P22 P32 46.1(4) . . . . ? P52 P12 P22 Cr2 45.7(4) . . . . ? Cr1 P12 P22 Cr2 92.4(2) . . . . ? P52 P12 P22 Cr1 -46.7(4) . . . . ? Cr2 P12 P22 Cr1 -92.4(2) . . . . ? C2 Cr1 P22 P32 130.1(3) . . . . ? C4 Cr1 P22 P32 68.9(4) . . . . ? C3 Cr1 P22 P32 91.6(3) . . . . ? C5 Cr1 P22 P32 129.1(7) . . . . ? C1 Cr1 P22 P32 158.0(3) . . . . ? P51 Cr1 P22 P32 -67.2(5) . . . . ? P31 Cr1 P22 P32 9.8(9) . . . . ? P11 Cr1 P22 P32 -114.8(6) . . . . ? P21 Cr1 P22 P32 -141.9(11) . . . . ? P41 Cr1 P22 P32 -20.4(7) . . . . ? P52 Cr1 P22 P32 -92.2(4) . . . . ? P2 Cr1 P22 P32 -152.2(15) . . . . ? C2 Cr1 P22 P12 -98.9(3) . . . . ? C4 Cr1 P22 P12 -160.1(2) . . . . ? C3 Cr1 P22 P12 -137.4(3) . . . . ? C5 Cr1 P22 P12 -99.9(8) . . . . ? C1 Cr1 P22 P12 -71.0(4) . . . . ? P51 Cr1 P22 P12 63.8(5) . . . . ? P31 Cr1 P22 P12 140.8(10) . . . . ? P11 Cr1 P22 P12 16.2(7) . . . . ? P21 Cr1 P22 P12 -10.9(9) . . . . ? P41 Cr1 P22 P12 110.6(6) . . . . ? P52 Cr1 P22 P12 38.8(3) . . . . ? P2 Cr1 P22 P12 -21.2(12) . . . . ? C2 Cr1 P22 Cr2 -164.38(17) . . . . ? C4 Cr1 P22 Cr2 134.42(18) . . . . ? C3 Cr1 P22 Cr2 157.10(17) . . . . ? C5 Cr1 P22 Cr2 -165.4(6) . . . . ? C1 Cr1 P22 Cr2 -136.48(14) . . . . ? P51 Cr1 P22 Cr2 -1.7(4) . . . . ? P31 Cr1 P22 Cr2 75.3(9) . . . . ? P11 Cr1 P22 Cr2 -49.3(6) . . . . ? P21 Cr1 P22 Cr2 -76.4(9) . . . . ? P41 Cr1 P22 Cr2 45.1(6) . . . . ? P52 Cr1 P22 Cr2 -26.7(3) . . . . ? P2 Cr1 P22 Cr2 -86.7(13) . . . . ? P12 P22 P32 P42 0.3(6) . . . . ? Cr2 P22 P32 P42 -46.0(3) . . . . ? Cr1 P22 P32 P42 46.1(4) . . . . ? P12 P22 P32 Cr2 46.3(4) . . . . ? Cr1 P22 P32 Cr2 92.1(2) . . . . ? P12 P22 P32 Cr1 -45.8(4) . . . . ? Cr2 P22 P32 Cr1 -92.1(2) . . . . ? C2 Cr1 P32 P22 -71.3(4) . . . . ? C4 Cr1 P32 P22 -138.2(3) . . . . ? C3 Cr1 P32 P22 -99.9(4) . . . . ? C5 Cr1 P32 P22 -160.3(3) . . . . ? C1 Cr1 P32 P22 -97.6(7) . . . . ? P51 Cr1 P32 P22 110.9(5) . . . . ? P31 Cr1 P32 P22 -13.0(11) . . . . ? P11 Cr1 P32 P22 61.7(7) . . . . ? P21 Cr1 P32 P22 15.3(6) . . . . ? P41 Cr1 P32 P22 139.2(10) . . . . ? P52 Cr1 P32 P22 90.6(4) . . . . ? P2 Cr1 P32 P22 7.9(3) . . . . ? C2 Cr1 P32 P42 159.7(3) . . . . ? C4 Cr1 P32 P42 92.9(3) . . . . ? C3 Cr1 P32 P42 131.2(3) . . . . ? C5 Cr1 P32 P42 70.8(4) . . . . ? C1 Cr1 P32 P42 133.5(7) . . . . ? P51 Cr1 P32 P42 -18.0(5) . . . . ? P31 Cr1 P32 P42 -142.0(12) . . . . ? P11 Cr1 P32 P42 -67.2(7) . . . . ? P21 Cr1 P32 P42 -113.7(5) . . . . ? P41 Cr1 P32 P42 10.3(8) . . . . ? P52 Cr1 P32 P42 -38.3(4) . . . . ? P2 Cr1 P32 P42 -121.0(4) . . . . ? C2 Cr1 P32 Cr2 -136.02(14) . . . . ? C4 Cr1 P32 Cr2 157.17(15) . . . . ? C3 Cr1 P32 Cr2 -164.55(17) . . . . ? C5 Cr1 P32 Cr2 135.07(16) . . . . ? C1 Cr1 P32 Cr2 -162.2(6) . . . . ? P51 Cr1 P32 Cr2 46.3(4) . . . . ? P31 Cr1 P32 Cr2 -77.7(11) . . . . ? P11 Cr1 P32 Cr2 -3.0(6) . . . . ? P21 Cr1 P32 Cr2 -49.4(5) . . . . ? P41 Cr1 P32 Cr2 74.6(9) . . . . ? P52 Cr1 P32 Cr2 25.9(3) . . . . ? P2 Cr1 P32 Cr2 -56.8(3) . . . . ? P22 P32 P42 P52 0.1(6) . . . . ? Cr2 P32 P42 P52 -46.1(4) . . . . ? Cr1 P32 P42 P52 46.8(4) . . . . ? P22 P32 P42 Cr2 46.1(4) . . . . ? Cr1 P32 P42 Cr2 92.9(2) . . . . ? P22 P32 P42 Cr1 -46.8(4) . . . . ? Cr2 P32 P42 Cr1 -92.9(2) . . . . ? C2 Cr1 P42 P52 131.5(7) . . . . ? C4 Cr1 P42 P52 130.7(3) . . . . ? C3 Cr1 P42 P52 159.3(3) . . . . ? C5 Cr1 P42 P52 92.1(3) . . . . ? C1 Cr1 P42 P52 69.0(4) . . . . ? P51 Cr1 P42 P52 11.9(11) . . . . ? P31 Cr1 P42 P52 -115.2(6) . . . . ? P11 Cr1 P42 P52 -18.9(7) . . . . ? P21 Cr1 P42 P52 -68.1(7) . . . . ? P41 Cr1 P42 P52 -143.4(13) . . . . ? P2 Cr1 P42 P52 -77.1(4) . . . . ? C2 Cr1 P42 P32 -98.9(8) . . . . ? C4 Cr1 P42 P32 -99.8(3) . . . . ? C3 Cr1 P42 P32 -71.1(4) . . . . ? C5 Cr1 P42 P32 -138.3(3) . . . . ? C1 Cr1 P42 P32 -161.5(2) . . . . ? P51 Cr1 P42 P32 141.5(11) . . . . ? P31 Cr1 P42 P32 14.4(6) . . . . ? P11 Cr1 P42 P32 110.7(6) . . . . ? P21 Cr1 P42 P32 61.5(6) . . . . ? P41 Cr1 P42 P32 -13.8(11) . . . . ? P52 Cr1 P42 P32 129.6(5) . . . . ? P2 Cr1 P42 P32 52.5(4) . . . . ? C2 Cr1 P42 Cr2 -163.6(6) . . . . ? C4 Cr1 P42 Cr2 -164.43(16) . . . . ? C3 Cr1 P42 Cr2 -135.81(15) . . . . ? C5 Cr1 P42 Cr2 157.03(15) . . . . ? C1 Cr1 P42 Cr2 133.85(18) . . . . ? P51 Cr1 P42 Cr2 76.8(10) . . . . ? P31 Cr1 P42 Cr2 -50.3(5) . . . . ? P11 Cr1 P42 Cr2 46.0(6) . . . . ? P21 Cr1 P42 Cr2 -3.2(6) . . . . ? P41 Cr1 P42 Cr2 -78.5(12) . . . . ? P52 Cr1 P42 Cr2 64.9(3) . . . . ? P2 Cr1 P42 Cr2 -12.2(3) . . . . ? P32 P42 P52 P12 -0.5(6) . . . . ? Cr2 P42 P52 P12 -46.4(4) . . . . ? Cr1 P42 P52 P12 46.6(4) . . . . ? P32 P42 P52 Cr1 -47.0(4) . . . . ? Cr2 P42 P52 Cr1 -93.0(3) . . . . ? P32 P42 P52 Cr2 45.9(4) . . . . ? Cr1 P42 P52 Cr2 93.0(3) . . . . ? P22 P12 P52 P42 0.7(6) . . . . ? Cr2 P12 P52 P42 46.0(4) . . . . ? Cr1 P12 P52 P42 -46.2(4) . . . . ? P22 P12 P52 Cr1 46.8(4) . . . . ? Cr2 P12 P52 Cr1 92.2(2) . . . . ? P22 P12 P52 Cr2 -45.3(4) . . . . ? Cr1 P12 P52 Cr2 -92.2(2) . . . . ? C2 Cr1 P52 P42 -162.4(3) . . . . ? C4 Cr1 P52 P42 -72.6(4) . . . . ? C3 Cr1 P52 P42 -102.3(9) . . . . ? C5 Cr1 P52 P42 -100.7(3) . . . . ? C1 Cr1 P52 P42 -139.1(3) . . . . ? P51 Cr1 P52 P42 -13.4(12) . . . . ? P31 Cr1 P52 P42 60.5(7) . . . . ? P11 Cr1 P52 P42 139.8(12) . . . . ? P21 Cr1 P52 P42 109.3(6) . . . . ? P41 Cr1 P52 P42 14.1(7) . . . . ? P2 Cr1 P52 P42 104.3(4) . . . . ? C2 Cr1 P52 P12 68.1(4) . . . . ? C4 Cr1 P52 P12 157.9(3) . . . . ? C3 Cr1 P52 P12 128.2(9) . . . . ? C5 Cr1 P52 P12 129.8(3) . . . . ? C1 Cr1 P52 P12 91.4(3) . . . . ? P51 Cr1 P52 P12 -142.9(15) . . . . ? P31 Cr1 P52 P12 -69.0(7) . . . . ? P11 Cr1 P52 P12 10.3(11) . . . . ? P21 Cr1 P52 P12 -20.2(6) . . . . ? P41 Cr1 P52 P12 -115.4(6) . . . . ? P2 Cr1 P52 P12 -25.2(4) . . . . ? C2 Cr1 P52 Cr2 133.28(18) . . . . ? C4 Cr1 P52 Cr2 -136.86(16) . . . . ? C3 Cr1 P52 Cr2 -166.6(7) . . . . ? C5 Cr1 P52 Cr2 -165.03(19) . . . . ? C1 Cr1 P52 Cr2 156.60(18) . . . . ? P51 Cr1 P52 Cr2 -77.7(13) . . . . ? P31 Cr1 P52 Cr2 -3.8(6) . . . . ? P11 Cr1 P52 Cr2 75.5(11) . . . . ? P21 Cr1 P52 Cr2 45.0(5) . . . . ? P41 Cr1 P52 Cr2 -50.2(5) . . . . ? P2 Cr1 P52 Cr2 40.0(4) . . . . ? P11 P51 Cr2 C11 -74.9(8) . . . . ? P41 P51 Cr2 C11 156.9(6) . . . . ? Cr1 P51 Cr2 C11 -137.6(2) . . . . ? P11 P51 Cr2 C15 -105.1(7) . . . . ? P41 P51 Cr2 C15 126.8(6) . . . . ? Cr1 P51 Cr2 C15 -167.8(2) . . . . ? P11 P51 Cr2 C13 -162.1(7) . . . . ? P41 P51 Cr2 C13 69.7(9) . . . . ? Cr1 P51 Cr2 C13 135.1(4) . . . . ? P11 P51 Cr2 C14 -142.9(7) . . . . ? P41 P51 Cr2 C14 88.9(7) . . . . ? Cr1 P51 Cr2 C14 154.4(2) . . . . ? P11 P51 Cr2 C12 -90.0(14) . . . . ? P41 P51 Cr2 C12 141.8(11) . . . . ? Cr1 P51 Cr2 C12 -152.7(9) . . . . ? P11 P51 Cr2 P21 37.6(9) . . . . ? P41 P51 Cr2 P21 -90.6(8) . . . . ? Cr1 P51 Cr2 P21 -25.1(6) . . . . ? P11 P51 Cr2 P31 90.6(9) . . . . ? P41 P51 Cr2 P31 -37.6(8) . . . . ? Cr1 P51 Cr2 P31 27.9(6) . . . . ? P11 P51 Cr2 P41 128.2(10) . . . . ? Cr1 P51 Cr2 P41 65.5(7) . . . . ? P41 P51 Cr2 P11 -128.2(10) . . . . ? Cr1 P51 Cr2 P11 -62.7(7) . . . . ? P11 P51 Cr2 P22 61.0(8) . . . . ? P41 P51 Cr2 P22 -67.2(7) . . . . ? Cr1 P51 Cr2 P22 -1.7(4) . . . . ? P11 P51 Cr2 P52 -16.7(13) . . . . ? P41 P51 Cr2 P52 -144.9(17) . . . . ? Cr1 P51 Cr2 P52 -79.4(14) . . . . ? P31 P21 Cr2 C11 -144.5(5) . . . . ? P11 P21 Cr2 C11 89.1(6) . . . . ? Cr1 P21 Cr2 C11 152.3(4) . . . . ? P31 P21 Cr2 C15 -164.6(6) . . . . ? P11 P21 Cr2 C15 69.0(8) . . . . ? Cr1 P21 Cr2 C15 132.2(4) . . . . ? P31 P21 Cr2 C13 -76.3(7) . . . . ? P11 P21 Cr2 C13 157.3(6) . . . . ? Cr1 P21 Cr2 C13 -139.5(3) . . . . ? P31 P21 Cr2 C14 -89.9(17) . . . . ? P11 P21 Cr2 C14 143.7(15) . . . . ? Cr1 P21 Cr2 C14 -153.1(12) . . . . ? P31 P21 Cr2 C12 -106.6(6) . . . . ? P11 P21 Cr2 C12 127.0(6) . . . . ? Cr1 P21 Cr2 C12 -169.8(4) . . . . ? P31 P21 Cr2 P51 88.7(7) . . . . ? P11 P21 Cr2 P51 -37.7(7) . . . . ? Cr1 P21 Cr2 P51 25.5(6) . . . . ? P11 P21 Cr2 P31 -126.4(9) . . . . ? Cr1 P21 Cr2 P31 -63.2(7) . . . . ? P31 P21 Cr2 P41 37.5(9) . . . . ? P11 P21 Cr2 P41 -88.8(9) . . . . ? Cr1 P21 Cr2 P41 -25.7(8) . . . . ? P31 P21 Cr2 P11 126.4(9) . . . . ? Cr1 P21 Cr2 P11 63.2(7) . . . . ? P31 P21 Cr2 P22 -19.4(10) . . . . ? P11 P21 Cr2 P22 -145.8(13) . . . . ? Cr1 P21 Cr2 P22 -82.6(11) . . . . ? P31 P21 Cr2 P52 109.8(6) . . . . ? P11 P21 Cr2 P52 -16.6(6) . . . . ? Cr1 P21 Cr2 P52 46.6(5) . . . . ? P41 P31 Cr2 C11 -163.3(8) . . . . ? P21 P31 Cr2 C11 66.9(8) . . . . ? Cr1 P31 Cr2 C11 131.3(4) . . . . ? P41 P31 Cr2 C15 -83.0(17) . . . . ? P21 P31 Cr2 C15 147.2(15) . . . . ? Cr1 P31 Cr2 C15 -148.4(11) . . . . ? P41 P31 Cr2 C13 -105.1(7) . . . . ? P21 P31 Cr2 C13 125.1(6) . . . . ? Cr1 P31 Cr2 C13 -170.5(4) . . . . ? P41 P31 Cr2 C14 -73.4(8) . . . . ? P21 P31 Cr2 C14 156.8(5) . . . . ? Cr1 P31 Cr2 C14 -138.8(3) . . . . ? P41 P31 Cr2 C12 -143.0(7) . . . . ? P21 P31 Cr2 C12 87.3(6) . . . . ? Cr1 P31 Cr2 C12 151.6(3) . . . . ? P41 P31 Cr2 P51 36.8(8) . . . . ? P21 P31 Cr2 P51 -92.9(7) . . . . ? Cr1 P31 Cr2 P51 -28.6(6) . . . . ? P41 P31 Cr2 P21 129.8(10) . . . . ? Cr1 P31 Cr2 P21 64.4(7) . . . . ? P21 P31 Cr2 P41 -129.8(10) . . . . ? Cr1 P31 Cr2 P41 -65.4(8) . . . . ? P41 P31 Cr2 P11 89.9(9) . . . . ? P21 P31 Cr2 P11 -39.9(8) . . . . ? Cr1 P31 Cr2 P11 24.5(7) . . . . ? P41 P31 Cr2 P22 145.3(11) . . . . ? P21 P31 Cr2 P22 15.5(8) . . . . ? Cr1 P31 Cr2 P22 79.9(8) . . . . ? P41 P31 Cr2 P52 61.5(8) . . . . ? P21 P31 Cr2 P52 -68.2(7) . . . . ? Cr1 P31 Cr2 P52 -3.9(7) . . . . ? P31 P41 Cr2 C11 148.0(16) . . . . ? P51 P41 Cr2 C11 -82(2) . . . . ? Cr1 P41 Cr2 C11 -148.6(13) . . . . ? P31 P41 Cr2 C15 158.6(5) . . . . ? P51 P41 Cr2 C15 -71.8(8) . . . . ? Cr1 P41 Cr2 C15 -138.1(3) . . . . ? P31 P41 Cr2 C13 89.2(6) . . . . ? P51 P41 Cr2 C13 -141.1(6) . . . . ? Cr1 P41 Cr2 C13 152.6(4) . . . . ? P31 P41 Cr2 C14 127.0(6) . . . . ? P51 P41 Cr2 C14 -103.4(7) . . . . ? Cr1 P41 Cr2 C14 -169.6(5) . . . . ? P31 P41 Cr2 C12 70.0(9) . . . . ? P51 P41 Cr2 C12 -160.4(7) . . . . ? Cr1 P41 Cr2 C12 133.3(4) . . . . ? P31 P41 Cr2 P51 -129.6(10) . . . . ? Cr1 P41 Cr2 P51 -66.3(8) . . . . ? P31 P41 Cr2 P21 -37.9(8) . . . . ? P51 P41 Cr2 P21 91.7(8) . . . . ? Cr1 P41 Cr2 P21 25.5(8) . . . . ? P51 P41 Cr2 P31 129.6(10) . . . . ? Cr1 P41 Cr2 P31 63.4(7) . . . . ? P31 P41 Cr2 P11 -90.7(9) . . . . ? P51 P41 Cr2 P11 38.9(8) . . . . ? Cr1 P41 Cr2 P11 -27.4(8) . . . . ? P31 P41 Cr2 P22 -17.3(6) . . . . ? P51 P41 Cr2 P22 112.3(7) . . . . ? Cr1 P41 Cr2 P22 46.1(5) . . . . ? P31 P41 Cr2 P52 -114.5(7) . . . . ? P51 P41 Cr2 P52 15.1(8) . . . . ? Cr1 P41 Cr2 P52 -51.2(5) . . . . ? P51 P11 Cr2 C11 125.8(6) . . . . ? P21 P11 Cr2 C11 -104.1(6) . . . . ? Cr1 P11 Cr2 C11 -168.6(4) . . . . ? P51 P11 Cr2 C15 87.6(6) . . . . ? P21 P11 Cr2 C15 -142.3(6) . . . . ? Cr1 P11 Cr2 C15 153.2(4) . . . . ? P51 P11 Cr2 C13 142.4(16) . . . . ? P21 P11 Cr2 C13 -87.5(19) . . . . ? Cr1 P11 Cr2 C13 -152.0(13) . . . . ? P51 P11 Cr2 C14 67.7(9) . . . . ? P21 P11 Cr2 C14 -162.2(7) . . . . ? Cr1 P11 Cr2 C14 133.3(4) . . . . ? P51 P11 Cr2 C12 156.4(5) . . . . ? P21 P11 Cr2 C12 -73.5(8) . . . . ? Cr1 P11 Cr2 C12 -138.0(3) . . . . ? P21 P11 Cr2 P51 130.1(9) . . . . ? Cr1 P11 Cr2 P51 65.6(7) . . . . ? P51 P11 Cr2 P21 -130.1(9) . . . . ? Cr1 P11 Cr2 P21 -64.5(7) . . . . ? P51 P11 Cr2 P31 -90.1(8) . . . . ? P21 P11 Cr2 P31 40.0(8) . . . . ? Cr1 P11 Cr2 P31 -24.5(7) . . . . ? P51 P11 Cr2 P41 -37.7(8) . . . . ? P21 P11 Cr2 P41 92.4(8) . . . . ? Cr1 P11 Cr2 P41 27.9(8) . . . . ? P51 P11 Cr2 P22 -116.1(7) . . . . ? P21 P11 Cr2 P22 14.0(6) . . . . ? Cr1 P11 Cr2 P22 -50.5(5) . . . . ? P51 P11 Cr2 P52 14.9(10) . . . . ? P21 P11 Cr2 P52 145.0(13) . . . . ? Cr1 P11 Cr2 P52 80.5(9) . . . . ? P32 P22 Cr2 C11 -154.1(3) . . . . ? P12 P22 Cr2 C11 75.2(3) . . . . ? Cr1 P22 Cr2 C11 140.22(13) . . . . ? P32 P22 Cr2 C15 -150.6(5) . . . . ? P12 P22 Cr2 C15 78.7(5) . . . . ? Cr1 P22 Cr2 C15 143.7(4) . . . . ? P32 P22 Cr2 C13 -85.3(3) . . . . ? P12 P22 Cr2 C13 144.0(3) . . . . ? Cr1 P22 Cr2 C13 -150.97(14) . . . . ? P32 P22 Cr2 C14 -70.1(5) . . . . ? P12 P22 Cr2 C14 159.2(3) . . . . ? Cr1 P22 Cr2 C14 -135.8(2) . . . . ? P32 P22 Cr2 C12 -121.9(3) . . . . ? P12 P22 Cr2 C12 107.4(3) . . . . ? Cr1 P22 Cr2 C12 172.42(18) . . . . ? P32 P22 Cr2 P51 67.4(5) . . . . ? P12 P22 Cr2 P51 -63.3(5) . . . . ? Cr1 P22 Cr2 P51 1.7(4) . . . . ? P32 P22 Cr2 P21 141.9(12) . . . . ? P12 P22 Cr2 P21 11.2(11) . . . . ? Cr1 P22 Cr2 P21 76.2(11) . . . . ? P32 P22 Cr2 P31 -6.9(7) . . . . ? P12 P22 Cr2 P31 -137.6(9) . . . . ? Cr1 P22 Cr2 P31 -72.6(8) . . . . ? P32 P22 Cr2 P41 20.4(7) . . . . ? P12 P22 Cr2 P41 -110.2(7) . . . . ? Cr1 P22 Cr2 P41 -45.3(6) . . . . ? P32 P22 Cr2 P11 114.0(6) . . . . ? P12 P22 Cr2 P11 -16.6(6) . . . . ? Cr1 P22 Cr2 P11 48.4(5) . . . . ? P32 P22 Cr2 P52 92.5(4) . . . . ? P12 P22 Cr2 P52 -38.2(3) . . . . ? Cr1 P22 Cr2 P52 26.8(3) . . . . ? P42 P52 Cr2 C11 146.1(3) . . . . ? P12 P52 Cr2 C11 -84.3(3) . . . . ? Cr1 P52 Cr2 C11 -149.58(17) . . . . ? P42 P52 Cr2 C15 109.1(3) . . . . ? P12 P52 Cr2 C15 -121.3(3) . . . . ? Cr1 P52 Cr2 C15 173.4(2) . . . . ? P42 P52 Cr2 C13 83.2(6) . . . . ? P12 P52 Cr2 C13 -147.1(6) . . . . ? Cr1 P52 Cr2 C13 147.6(4) . . . . ? P42 P52 Cr2 C14 77.3(3) . . . . ? P12 P52 Cr2 C14 -153.1(3) . . . . ? Cr1 P52 Cr2 C14 141.64(16) . . . . ? P42 P52 Cr2 C12 161.5(3) . . . . ? P12 P52 Cr2 C12 -68.9(5) . . . . ? Cr1 P52 Cr2 C12 -134.2(2) . . . . ? P42 P52 Cr2 P51 14.0(13) . . . . ? P12 P52 Cr2 P51 143.6(16) . . . . ? Cr1 P52 Cr2 P51 78.3(14) . . . . ? P42 P52 Cr2 P21 -109.9(6) . . . . ? P12 P52 Cr2 P21 19.7(6) . . . . ? Cr1 P52 Cr2 P21 -45.6(6) . . . . ? P42 P52 Cr2 P31 -60.6(6) . . . . ? P12 P52 Cr2 P31 69.0(7) . . . . ? Cr1 P52 Cr2 P31 3.8(6) . . . . ? P42 P52 Cr2 P41 -13.9(7) . . . . ? P12 P52 Cr2 P41 115.7(6) . . . . ? Cr1 P52 Cr2 P41 50.5(5) . . . . ? P42 P52 Cr2 P11 -137.8(12) . . . . ? P12 P52 Cr2 P11 -8.2(11) . . . . ? Cr1 P52 Cr2 P11 -73.5(11) . . . . ? P42 P52 Cr2 P22 -91.3(4) . . . . ? P12 P52 Cr2 P22 38.4(4) . . . . ? Cr1 P52 Cr2 P22 -26.9(3) . . . . ? C15 Cr2 C11 C12 -117.84(17) . . . . ? C13 Cr2 C11 C12 -37.46(12) . . . . ? C14 Cr2 C11 C12 -80.02(13) . . . . ? P51 Cr2 C11 C12 -171.9(5) . . . . ? P21 Cr2 C11 C12 82.8(6) . . . . ? P31 Cr2 C11 C12 32.6(8) . . . . ? P41 Cr2 C11 C12 -103(2) . . . . ? P11 Cr2 C11 C12 136.6(6) . . . . ? P22 Cr2 C11 C12 60.0(3) . . . . ? P52 Cr2 C11 C12 165.2(3) . . . . ? C13 Cr2 C11 C15 80.37(12) . . . . ? C14 Cr2 C11 C15 37.82(11) . . . . ? C12 Cr2 C11 C15 117.84(17) . . . . ? P51 Cr2 C11 C15 -54.1(5) . . . . ? P21 Cr2 C11 C15 -159.4(6) . . . . ? P31 Cr2 C11 C15 150.4(8) . . . . ? P41 Cr2 C11 C15 14(2) . . . . ? P11 Cr2 C11 C15 -105.5(6) . . . . ? P22 Cr2 C11 C15 177.8(3) . . . . ? P52 Cr2 C11 C15 -76.9(3) . . . . ? C15 Cr2 C11 C16 120.9(3) . . . . ? C13 Cr2 C11 C16 -158.7(3) . . . . ? C14 Cr2 C11 C16 158.7(2) . . . . ? C12 Cr2 C11 C16 -121.3(3) . . . . ? P51 Cr2 C11 C16 66.8(6) . . . . ? P21 Cr2 C11 C16 -38.5(6) . . . . ? P31 Cr2 C11 C16 -88.7(8) . . . . ? P41 Cr2 C11 C16 135.3(19) . . . . ? P11 Cr2 C11 C16 15.4(6) . . . . ? P22 Cr2 C11 C16 -61.3(3) . . . . ? P52 Cr2 C11 C16 44.0(4) . . . . ? C15 C11 C12 C13 0.0(2) . . . . ? C16 C11 C12 C13 -177.2(2) . . . . ? Cr2 C11 C12 C13 61.91(14) . . . . ? C15 C11 C12 C17 176.0(2) . . . . ? C16 C11 C12 C17 -1.2(3) . . . . ? Cr2 C11 C12 C17 -122.1(2) . . . . ? C15 C11 C12 Cr2 -61.96(14) . . . . ? C16 C11 C12 Cr2 120.8(2) . . . . ? C11 Cr2 C12 C13 -117.32(17) . . . . ? C15 Cr2 C12 C13 -79.91(12) . . . . ? C14 Cr2 C12 C13 -37.37(11) . . . . ? P51 Cr2 C12 C13 -96.6(12) . . . . ? P21 Cr2 C12 C13 136.6(6) . . . . ? P31 Cr2 C12 C13 82.8(6) . . . . ? P41 Cr2 C12 C13 31.0(8) . . . . ? P11 Cr2 C12 C13 -172.7(7) . . . . ? P22 Cr2 C12 C13 112.1(3) . . . . ? P52 Cr2 C12 C13 -141.7(5) . . . . ? C15 Cr2 C12 C11 37.41(11) . . . . ? C13 Cr2 C12 C11 117.32(17) . . . . ? C14 Cr2 C12 C11 79.96(12) . . . . ? P51 Cr2 C12 C11 20.7(12) . . . . ? P21 Cr2 C12 C11 -106.0(6) . . . . ? P31 Cr2 C12 C11 -159.9(6) . . . . ? P41 Cr2 C12 C11 148.3(8) . . . . ? P11 Cr2 C12 C11 -55.4(7) . . . . ? P22 Cr2 C12 C11 -130.6(3) . . . . ? P52 Cr2 C12 C11 -24.4(5) . . . . ? C11 Cr2 C12 C17 121.1(3) . . . . ? C15 Cr2 C12 C17 158.5(3) . . . . ? C13 Cr2 C12 C17 -121.6(3) . . . . ? C14 Cr2 C12 C17 -158.9(3) . . . . ? P51 Cr2 C12 C17 141.8(12) . . . . ? P21 Cr2 C12 C17 15.1(6) . . . . ? P31 Cr2 C12 C17 -38.8(6) . . . . ? P41 Cr2 C12 C17 -90.6(9) . . . . ? P11 Cr2 C12 C17 65.7(7) . . . . ? P22 Cr2 C12 C17 -9.4(3) . . . . ? P52 Cr2 C12 C17 96.8(5) . . . . ? C11 C12 C13 C14 0.2(2) . . . . ? C17 C12 C13 C14 -175.8(2) . . . . ? Cr2 C12 C13 C14 61.91(14) . . . . ? C11 C12 C13 C18 176.4(2) . . . . ? C17 C12 C13 C18 0.4(4) . . . . ? Cr2 C12 C13 C18 -121.9(2) . . . . ? C11 C12 C13 Cr2 -61.70(14) . . . . ? C17 C12 C13 Cr2 122.3(2) . . . . ? C11 Cr2 C13 C12 37.61(12) . . . . ? C15 Cr2 C13 C12 80.31(13) . . . . ? C14 Cr2 C13 C12 117.82(17) . . . . ? P51 Cr2 C13 C12 149.0(6) . . . . ? P21 Cr2 C13 C12 -55.0(6) . . . . ? P31 Cr2 C13 C12 -107.1(6) . . . . ? P41 Cr2 C13 C12 -160.8(6) . . . . ? P11 Cr2 C13 C12 19.1(19) . . . . ? P22 Cr2 C13 C12 -76.4(3) . . . . ? P52 Cr2 C13 C12 109.4(7) . . . . ? C11 Cr2 C13 C14 -80.21(13) . . . . ? C15 Cr2 C13 C14 -37.50(11) . . . . ? C12 Cr2 C13 C14 -117.82(17) . . . . ? P51 Cr2 C13 C14 31.2(6) . . . . ? P21 Cr2 C13 C14 -172.8(6) . . . . ? P31 Cr2 C13 C14 135.1(6) . . . . ? P41 Cr2 C13 C14 81.4(6) . . . . ? P11 Cr2 C13 C14 -98.7(19) . . . . ? P22 Cr2 C13 C14 165.7(3) . . . . ? P52 Cr2 C13 C14 -8.5(7) . . . . ? C11 Cr2 C13 C18 159.7(3) . . . . ? C15 Cr2 C13 C18 -157.6(3) . . . . ? C14 Cr2 C13 C18 -120.1(3) . . . . ? C12 Cr2 C13 C18 122.1(3) . . . . ? P51 Cr2 C13 C18 -88.9(6) . . . . ? P21 Cr2 C13 C18 67.0(7) . . . . ? P31 Cr2 C13 C18 14.9(6) . . . . ? P41 Cr2 C13 C18 -38.7(6) . . . . ? P11 Cr2 C13 C18 141.1(19) . . . . ? P22 Cr2 C13 C18 45.6(3) . . . . ? P52 Cr2 C13 C18 -128.6(7) . . . . ? C12 C13 C14 C15 -0.3(2) . . . . ? C18 C13 C14 C15 -176.5(2) . . . . ? Cr2 C13 C14 C15 61.76(13) . . . . ? C12 C13 C14 C19 176.7(2) . . . . ? C18 C13 C14 C19 0.4(3) . . . . ? Cr2 C13 C14 C19 -121.3(2) . . . . ? C12 C13 C14 Cr2 -62.04(14) . . . . ? C18 C13 C14 Cr2 121.7(2) . . . . ? C11 Cr2 C14 C13 79.65(13) . . . . ? C15 Cr2 C14 C13 117.55(17) . . . . ? C12 Cr2 C14 C13 37.18(12) . . . . ? P51 Cr2 C14 C13 -160.0(4) . . . . ? P21 Cr2 C14 C13 18.6(17) . . . . ? P31 Cr2 C14 C13 -57.6(6) . . . . ? P41 Cr2 C14 C13 -107.9(7) . . . . ? P11 Cr2 C14 C13 149.7(7) . . . . ? P22 Cr2 C14 C13 -23.9(4) . . . . ? P52 Cr2 C14 C13 176.3(3) . . . . ? C11 Cr2 C14 C15 -37.90(12) . . . . ? C13 Cr2 C14 C15 -117.55(17) . . . . ? C12 Cr2 C14 C15 -80.37(13) . . . . ? P51 Cr2 C14 C15 82.5(4) . . . . ? P21 Cr2 C14 C15 -99.0(17) . . . . ? P31 Cr2 C14 C15 -175.2(6) . . . . ? P41 Cr2 C14 C15 134.5(7) . . . . ? P11 Cr2 C14 C15 32.2(7) . . . . ? P22 Cr2 C14 C15 -141.4(4) . . . . ? P52 Cr2 C14 C15 58.7(3) . . . . ? C11 Cr2 C14 C19 -160.0(2) . . . . ? C15 Cr2 C14 C19 -122.1(2) . . . . ? C13 Cr2 C14 C19 120.3(2) . . . . ? C12 Cr2 C14 C19 157.5(2) . . . . ? P51 Cr2 C14 C19 -39.6(4) . . . . ? P21 Cr2 C14 C19 138.9(17) . . . . ? P31 Cr2 C14 C19 62.7(6) . . . . ? P41 Cr2 C14 C19 12.4(7) . . . . ? P11 Cr2 C14 C19 -90.0(8) . . . . ? P22 Cr2 C14 C19 96.4(4) . . . . ? P52 Cr2 C14 C19 -63.4(3) . . . . ? C13 C14 C15 C11 0.3(2) . . . . ? C19 C14 C15 C11 -176.7(2) . . . . ? Cr2 C14 C15 C11 62.14(13) . . . . ? C13 C14 C15 C20 177.26(19) . . . . ? C19 C14 C15 C20 0.3(3) . . . . ? Cr2 C14 C15 C20 -120.9(2) . . . . ? C13 C14 C15 Cr2 -61.88(14) . . . . ? C19 C14 C15 Cr2 121.2(2) . . . . ? C12 C11 C15 C14 -0.1(2) . . . . ? C16 C11 C15 C14 177.06(19) . . . . ? Cr2 C11 C15 C14 -62.34(13) . . . . ? C12 C11 C15 C20 -177.16(19) . . . . ? C16 C11 C15 C20 0.0(3) . . . . ? Cr2 C11 C15 C20 120.6(2) . . . . ? C12 C11 C15 Cr2 62.21(14) . . . . ? C16 C11 C15 Cr2 -120.6(2) . . . . ? C11 Cr2 C15 C14 116.89(17) . . . . ? C13 Cr2 C15 C14 37.43(12) . . . . ? C12 Cr2 C15 C14 79.66(13) . . . . ? P51 Cr2 C15 C14 -105.8(4) . . . . ? P21 Cr2 C15 C14 149.4(8) . . . . ? P31 Cr2 C15 C14 13.0(17) . . . . ? P41 Cr2 C15 C14 -57.5(7) . . . . ? P11 Cr2 C15 C14 -159.6(5) . . . . ? P22 Cr2 C15 C14 112.0(6) . . . . ? P52 Cr2 C15 C14 -131.7(3) . . . . ? C13 Cr2 C15 C11 -79.45(13) . . . . ? C14 Cr2 C15 C11 -116.89(17) . . . . ? C12 Cr2 C15 C11 -37.22(12) . . . . ? P51 Cr2 C15 C11 137.3(4) . . . . ? P21 Cr2 C15 C11 32.5(8) . . . . ? P31 Cr2 C15 C11 -103.9(17) . . . . ? P41 Cr2 C15 C11 -174.4(7) . . . . ? P11 Cr2 C15 C11 83.5(5) . . . . ? P22 Cr2 C15 C11 -4.9(6) . . . . ? P52 Cr2 C15 C11 111.4(3) . . . . ? C11 Cr2 C15 C20 -121.2(2) . . . . ? C13 Cr2 C15 C20 159.4(2) . . . . ? C14 Cr2 C15 C20 122.0(2) . . . . ? C12 Cr2 C15 C20 -158.4(2) . . . . ? P51 Cr2 C15 C20 16.1(4) . . . . ? P21 Cr2 C15 C20 -88.7(8) . . . . ? P31 Cr2 C15 C20 134.9(17) . . . . ? P41 Cr2 C15 C20 64.5(8) . . . . ? P11 Cr2 C15 C20 -37.6(6) . . . . ? P22 Cr2 C15 C20 -126.1(6) . . . . ? P52 Cr2 C15 C20 -9.7(3) . . . . ? _diffrn_measured_fraction_theta_max 0.970 _diffrn_reflns_theta_full 30.47 _diffrn_measured_fraction_theta_full 0.970 _refine_diff_density_max 0.888 _refine_diff_density_min -0.510 _refine_diff_density_rms 0.079 #===END data_150k _database_code_depnum_ccdc_archive 'CCDC 618754' _audit_creation_method SHELXL-97 _chemical_name_systematic ; \m~2~-\h^5^,\h^5^-cyclopentaphosphole)-bis ((\h^5^-pentamethyl-cyclopentadienyl)-chromium) hexafluoroantimonate ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H30 Cr2 F6 P5 Sb' _chemical_formula_weight 765.04 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M I2/a loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' _cell_length_a 23.1539(7) _cell_length_b 21.3296(7) _cell_length_c 23.1371(8) _cell_angle_alpha 90.00 _cell_angle_beta 101.5460(10) _cell_angle_gamma 90.00 _cell_volume 11195.3(6) _cell_formula_units_Z 16 _cell_measurement_temperature 150(2) _cell_measurement_reflns_used 8082 _cell_measurement_theta_min 2.22 _cell_measurement_theta_max 30.36 _exptl_crystal_description 'irregular block' _exptl_crystal_colour 'dark green' _exptl_crystal_size_max 0.60 _exptl_crystal_size_mid 0.52 _exptl_crystal_size_min 0.40 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.816 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 6048 _exptl_absorpt_coefficient_mu 2.056 _exptl_absorpt_correction_type integration _exptl_absorpt_correction_T_min 0.392 _exptl_absorpt_correction_T_max 0.613 _exptl_absorpt_process_details 'XPREP in SHELXTL' _exptl_special_details ; ? ; _diffrn_ambient_temperature 150(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'Bede Microsource X-ray Generator' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEX CCD Diffractometer' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number 0 _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% 0 _diffrn_reflns_number 43253 _diffrn_reflns_av_R_equivalents 0.0254 _diffrn_reflns_av_sigmaI/netI 0.0427 _diffrn_reflns_limit_h_min -32 _diffrn_reflns_limit_h_max 32 _diffrn_reflns_limit_k_min -30 _diffrn_reflns_limit_k_max 29 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_limit_l_max 32 _diffrn_reflns_theta_min 1.14 _diffrn_reflns_theta_max 30.47 _reflns_number_total 15902 _reflns_number_gt 14426 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'SMART V5.625 (Bruker, 2003)' _computing_cell_refinement 'SMART V5.625 (Bruker, 2003)' _computing_data_reduction 'SAINT V6.28A (Bruker, 2003)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'SHELXTL V6.12(Bruker, 2001)' _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0299P)^2^+19.4436P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 15902 _refine_ls_number_parameters 704 _refine_ls_number_restraints 90 _refine_ls_R_factor_all 0.0369 _refine_ls_R_factor_gt 0.0309 _refine_ls_wR_factor_ref 0.0879 _refine_ls_wR_factor_gt 0.0791 _refine_ls_goodness_of_fit_ref 1.063 _refine_ls_restrained_S_all 1.064 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb1 Sb 0.137316(12) 0.871963(12) 0.384570(12) 0.03342(5) Uani 1 1 d . . . F1 F 0.09583(15) 0.81125(15) 0.33387(17) 0.0694(9) Uani 1 1 d . . . F2 F 0.08939(19) 0.93353(15) 0.34241(15) 0.0737(10) Uani 1 1 d . . . F3 F 0.08435(14) 0.86450(16) 0.43549(16) 0.0613(8) Uani 1 1 d . . . F4 F 0.18334(12) 0.80932(11) 0.42749(14) 0.0490(6) Uani 1 1 d . . . F5 F 0.19218(16) 0.87885(14) 0.33484(14) 0.0608(8) Uani 1 1 d . . . F6 F 0.17945(15) 0.93319(12) 0.43341(13) 0.0535(7) Uani 1 1 d . . . Sb2 Sb 0.136422(14) 0.126194(12) 0.116984(13) 0.03151(5) Uani 1 1 d . . . F7 F 0.1235(3) 0.05671(18) 0.1583(2) 0.150(3) Uani 1 1 d . . . F8 F 0.07988(16) 0.1681(2) 0.14693(19) 0.1014(14) Uani 1 1 d . . . F9 F 0.08089(17) 0.09757(19) 0.05286(16) 0.0786(10) Uani 1 1 d . . . F10 F 0.19732(18) 0.0888(2) 0.08795(19) 0.1188(19) Uani 1 1 d . . . F11 F 0.19205(15) 0.15379(19) 0.18099(16) 0.0775(11) Uani 1 1 d . . . F12 F 0.14872(19) 0.19764(17) 0.07653(19) 0.0957(14) Uani 1 1 d . . . C1 C -0.11862(16) 0.31292(16) 0.44631(17) 0.0275(7) Uani 1 1 d . A . C2 C -0.14648(16) 0.27142(15) 0.40052(18) 0.0274(6) Uani 1 1 d . A . C3 C -0.14487(14) 0.29983(16) 0.34533(16) 0.0259(7) Uani 1 1 d . A . C4 C -0.11575(15) 0.35898(15) 0.35599(16) 0.0252(6) Uani 1 1 d . A . C5 C -0.09973(16) 0.36692(15) 0.41875(16) 0.0248(6) Uani 1 1 d . A . C6 C -0.1134(2) 0.3042(2) 0.51080(18) 0.0430(10) Uani 1 1 d . . . H6A H -0.1461 0.3255 0.5236 0.065 Uiso 1 1 calc R . . H6B H -0.0759 0.3220 0.5317 0.065 Uiso 1 1 calc R . . H6C H -0.1145 0.2593 0.5197 0.065 Uiso 1 1 calc R . . C7 C -0.17586(18) 0.21007(17) 0.4103(2) 0.0399(9) Uani 1 1 d . . . H7A H -0.2174 0.2176 0.4111 0.060 Uiso 1 1 calc R . . H7B H -0.1561 0.1918 0.4479 0.060 Uiso 1 1 calc R . . H7C H -0.1731 0.1810 0.3781 0.060 Uiso 1 1 calc R . . C8 C -0.17180(17) 0.27436(19) 0.28531(17) 0.0354(8) Uani 1 1 d . . . H8A H -0.2078 0.2978 0.2691 0.053 Uiso 1 1 calc R . . H8B H -0.1815 0.2300 0.2887 0.053 Uiso 1 1 calc R . . H8C H -0.1437 0.2788 0.2591 0.053 Uiso 1 1 calc R . . C9 C -0.10679(18) 0.40543(18) 0.31065(18) 0.0347(8) Uani 1 1 d . . . H9A H -0.1433 0.4290 0.2971 0.052 Uiso 1 1 calc R . . H9B H -0.0960 0.3835 0.2772 0.052 Uiso 1 1 calc R . . H9C H -0.0752 0.4344 0.3278 0.052 Uiso 1 1 calc R . . C10 C -0.07172(18) 0.42366(17) 0.44995(19) 0.0351(8) Uani 1 1 d . . . H10A H -0.1008 0.4465 0.4673 0.053 Uiso 1 1 calc R . . H10B H -0.0572 0.4508 0.4218 0.053 Uiso 1 1 calc R . . H10C H -0.0387 0.4110 0.4813 0.053 Uiso 1 1 calc R . . Cr1 Cr -0.05418(2) 0.28317(2) 0.39296(2) 0.02064(10) Uani 1 1 d . . . P11 P 0.0377(6) 0.2790(8) 0.4642(5) 0.046(4) Uani 0.25 1 d PU A 1 P21 P -0.0076(7) 0.1938(7) 0.4477(8) 0.058(4) Uani 0.25 1 d PU A 1 P31 P -0.0327(7) 0.1813(7) 0.3547(5) 0.051(4) Uani 0.25 1 d PU A 1 P41 P -0.0043(7) 0.2644(6) 0.3122(7) 0.050(4) Uani 0.25 1 d PU A 1 P51 P 0.0390(6) 0.3249(6) 0.3822(5) 0.037(2) Uani 0.25 1 d PU A 1 P1 P 0.0275(3) 0.2595(4) 0.4735(3) 0.046(2) Uani 0.50 1 d PU A 2 P2 P -0.0193(3) 0.1803(3) 0.4287(3) 0.0398(17) Uani 0.50 1 d PU A 2 P3 P -0.0326(3) 0.1955(3) 0.3342(3) 0.0376(17) Uani 0.50 1 d PU A 2 P4 P 0.0061(3) 0.2866(3) 0.3191(3) 0.043(2) Uani 0.50 1 d PU A 2 P5 P 0.0442(3) 0.3256(3) 0.4062(3) 0.0416(18) Uani 0.50 1 d PU A 2 P12 P 0.0142(4) 0.2351(5) 0.4749(4) 0.043(2) Uani 0.25 1 d PU A 3 P22 P -0.0291(4) 0.1728(4) 0.4030(4) 0.032(2) Uani 0.25 1 d PU A 3 P32 P -0.0262(4) 0.2184(4) 0.3183(3) 0.036(2) Uani 0.25 1 d PU A 3 P42 P 0.0211(4) 0.3086(4) 0.3376(5) 0.042(3) Uani 0.25 1 d PU A 3 P52 P 0.0470(4) 0.3180(4) 0.4347(4) 0.038(2) Uani 0.25 1 d PU A 3 Cr2 Cr 0.06534(2) 0.21664(2) 0.39062(2) 0.02052(10) Uani 1 1 d . . . C11 C 0.14868(15) 0.17854(15) 0.44190(15) 0.0245(6) Uani 1 1 d . A . C12 C 0.11858(16) 0.12987(15) 0.40606(18) 0.0275(7) Uani 1 1 d . A . C13 C 0.11291(16) 0.14820(17) 0.34576(16) 0.0282(7) Uani 1 1 d . A . C14 C 0.14001(15) 0.20775(16) 0.34482(16) 0.0270(7) Uani 1 1 d . A . C15 C 0.16194(14) 0.22722(14) 0.40437(16) 0.0238(6) Uani 1 1 d . A . C16 C 0.16594(18) 0.1760(2) 0.50776(17) 0.0363(8) Uani 1 1 d . . . H16A H 0.2029 0.1526 0.5192 0.055 Uiso 1 1 calc R A . H16B H 0.1348 0.1552 0.5237 0.055 Uiso 1 1 calc R . . H16C H 0.1714 0.2188 0.5235 0.055 Uiso 1 1 calc R . . C17 C 0.09924(19) 0.06852(17) 0.4274(2) 0.0450(11) Uani 1 1 d . . . H17A H 0.1322 0.0389 0.4333 0.068 Uiso 1 1 calc R A . H17B H 0.0665 0.0517 0.3980 0.068 Uiso 1 1 calc R . . H17C H 0.0864 0.0749 0.4648 0.068 Uiso 1 1 calc R . . C18 C 0.08783(19) 0.1098(2) 0.2921(2) 0.0456(10) Uani 1 1 d . . . H18A H 0.1194 0.0851 0.2804 0.068 Uiso 1 1 calc R A . H18B H 0.0703 0.1377 0.2596 0.068 Uiso 1 1 calc R . . H18C H 0.0575 0.0815 0.3011 0.068 Uiso 1 1 calc R . . C19 C 0.14659(18) 0.2439(2) 0.29094(18) 0.0397(9) Uani 1 1 d . . . H19A H 0.1870 0.2394 0.2845 0.060 Uiso 1 1 calc R A . H19B H 0.1383 0.2883 0.2965 0.060 Uiso 1 1 calc R . . H19C H 0.1188 0.2277 0.2566 0.060 Uiso 1 1 calc R . . C20 C 0.19559(16) 0.28607(16) 0.42349(19) 0.0329(8) Uani 1 1 d . . . H20A H 0.2371 0.2801 0.4214 0.049 Uiso 1 1 calc R A . H20B H 0.1927 0.2960 0.4642 0.049 Uiso 1 1 calc R . . H20C H 0.1791 0.3206 0.3975 0.049 Uiso 1 1 calc R . . C21 C 0.10704(15) 0.38713(15) 0.13266(15) 0.0227(6) Uani 1 1 d . . . C22 C 0.16983(16) 0.38295(15) 0.14701(16) 0.0251(7) Uani 1 1 d . . . C23 C 0.19327(16) 0.43800(17) 0.12603(17) 0.0280(7) Uani 1 1 d . . . C24 C 0.14602(18) 0.47668(15) 0.09835(16) 0.0279(7) Uani 1 1 d . . . C25 C 0.09236(16) 0.44534(16) 0.10319(15) 0.0260(7) Uani 1 1 d . . . C26 C 0.06370(18) 0.33748(18) 0.14228(19) 0.0354(8) Uani 1 1 d . . . H26A H 0.0659 0.3019 0.1160 0.053 Uiso 1 1 calc R . . H26B H 0.0237 0.3549 0.1338 0.053 Uiso 1 1 calc R . . H26C H 0.0732 0.3233 0.1834 0.053 Uiso 1 1 calc R . . C27 C 0.20527(18) 0.32773(17) 0.17461(17) 0.0343(8) Uani 1 1 d . . . H27A H 0.2246 0.3077 0.1454 0.052 Uiso 1 1 calc R . . H27B H 0.1791 0.2975 0.1883 0.052 Uiso 1 1 calc R . . H27C H 0.2352 0.3420 0.2082 0.052 Uiso 1 1 calc R . . C28 C 0.25785(18) 0.4505(2) 0.1291(2) 0.0442(10) Uani 1 1 d . . . H28A H 0.2691 0.4358 0.0928 0.066 Uiso 1 1 calc R . . H28B H 0.2811 0.4282 0.1630 0.066 Uiso 1 1 calc R . . H28C H 0.2654 0.4956 0.1337 0.066 Uiso 1 1 calc R . . C29 C 0.1515(2) 0.53786(18) 0.06833(19) 0.0424(10) Uani 1 1 d . . . H29A H 0.1539 0.5302 0.0271 0.064 Uiso 1 1 calc R . . H29B H 0.1872 0.5595 0.0884 0.064 Uiso 1 1 calc R . . H29C H 0.1170 0.5639 0.0698 0.064 Uiso 1 1 calc R . . C30 C 0.03078(18) 0.46734(19) 0.07766(17) 0.0372(9) Uani 1 1 d . . . H30A H 0.0178 0.4493 0.0382 0.056 Uiso 1 1 calc R . . H30B H 0.0304 0.5132 0.0749 0.056 Uiso 1 1 calc R . . H30C H 0.0041 0.4538 0.1032 0.056 Uiso 1 1 calc R . . Cr3 Cr 0.14228(2) 0.46484(2) 0.19260(2) 0.02027(10) Uani 1 1 d . . . P6 P 0.08408(7) 0.44544(7) 0.26697(6) 0.0538(4) Uani 1 1 d . . . P7 P 0.17795(7) 0.42946(5) 0.29413(5) 0.0533(4) Uani 1 1 d . . . P8 P 0.22392(5) 0.50831(7) 0.26443(6) 0.0523(3) Uani 1 1 d . . . P9 P 0.15808(7) 0.57448(5) 0.22062(5) 0.0494(3) Uani 1 1 d . . . P10 P 0.07100(6) 0.53545(7) 0.22151(5) 0.0515(4) Uani 1 1 d . . . Cr4 Cr 0.14275(2) 0.53325(2) 0.31412(2) 0.01993(10) Uani 1 1 d . . . C31 C 0.09520(15) 0.54795(17) 0.38626(16) 0.0270(7) Uani 1 1 d . . . C32 C 0.15217(16) 0.52301(14) 0.41054(14) 0.0245(6) Uani 1 1 d . . . C33 C 0.19505(15) 0.56660(15) 0.39872(14) 0.0220(6) Uani 1 1 d . . . C34 C 0.16449(18) 0.61869(14) 0.36771(16) 0.0264(7) Uani 1 1 d . . . C35 C 0.10311(16) 0.60749(16) 0.36054(15) 0.0275(7) Uani 1 1 d . . . C36 C 0.03723(18) 0.5191(2) 0.39037(19) 0.0434(10) Uani 1 1 d . . . H36A H 0.0212 0.5402 0.4214 0.065 Uiso 1 1 calc R . . H36B H 0.0429 0.4745 0.3999 0.065 Uiso 1 1 calc R . . H36C H 0.0097 0.5237 0.3525 0.065 Uiso 1 1 calc R . . C37 C 0.1644(2) 0.46235(17) 0.44366(17) 0.0364(9) Uani 1 1 d . . . H37A H 0.1675 0.4701 0.4859 0.055 Uiso 1 1 calc R . . H37B H 0.2014 0.4445 0.4369 0.055 Uiso 1 1 calc R . . H37C H 0.1321 0.4328 0.4298 0.055 Uiso 1 1 calc R . . C38 C 0.26061(16) 0.5617(2) 0.41808(19) 0.0362(8) Uani 1 1 d . . . H38A H 0.2726 0.5794 0.4577 0.054 Uiso 1 1 calc R . . H38B H 0.2798 0.5848 0.3905 0.054 Uiso 1 1 calc R . . H38C H 0.2723 0.5175 0.4187 0.054 Uiso 1 1 calc R . . C39 C 0.1935(2) 0.67670(17) 0.35038(19) 0.0412(9) Uani 1 1 d . . . H39A H 0.2012 0.7058 0.3838 0.062 Uiso 1 1 calc R . . H39B H 0.1674 0.6968 0.3169 0.062 Uiso 1 1 calc R . . H39C H 0.2307 0.6654 0.3391 0.062 Uiso 1 1 calc R . . C40 C 0.0554(2) 0.6523(2) 0.33328(19) 0.0451(11) Uani 1 1 d . . . H40A H 0.0464 0.6805 0.3638 0.068 Uiso 1 1 calc R . . H40B H 0.0199 0.6288 0.3156 0.068 Uiso 1 1 calc R . . H40C H 0.0688 0.6770 0.3027 0.068 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.03688(15) 0.02858(9) 0.03617(15) -0.00346(10) 0.01062(8) 0.00392(10) F1 0.062(2) 0.0626(18) 0.079(2) -0.0268(17) 0.0038(17) -0.0145(16) F2 0.107(3) 0.0578(17) 0.0495(18) 0.0036(14) 0.0004(17) 0.0399(19) F3 0.0456(16) 0.0793(19) 0.067(2) 0.0100(16) 0.0307(14) 0.0150(15) F4 0.0447(15) 0.0394(12) 0.0658(19) 0.0089(12) 0.0180(13) 0.0129(11) F5 0.070(2) 0.079(2) 0.0415(16) -0.0066(13) 0.0298(15) -0.0094(15) F6 0.080(2) 0.0411(12) 0.0392(14) -0.0103(11) 0.0115(13) -0.0125(13) Sb2 0.03675(16) 0.02644(8) 0.03255(15) 0.00126(8) 0.00984(7) 0.00275(9) F7 0.271(7) 0.063(2) 0.092(3) 0.044(2) -0.023(4) -0.059(3) F8 0.0542(19) 0.155(4) 0.102(3) -0.038(3) 0.0322(19) 0.023(2) F9 0.076(2) 0.090(2) 0.061(2) -0.0138(19) -0.0070(17) -0.019(2) F10 0.084(3) 0.169(4) 0.097(3) -0.075(3) 0.003(2) 0.064(3) F11 0.0573(19) 0.098(3) 0.067(2) -0.0369(19) -0.0127(15) 0.0128(18) F12 0.101(3) 0.081(2) 0.099(3) 0.048(2) 0.005(2) -0.030(2) C1 0.0297(17) 0.0253(14) 0.0295(17) -0.0071(13) 0.0105(13) 0.0005(13) C2 0.0217(15) 0.0249(13) 0.0372(19) -0.0032(14) 0.0099(12) -0.0034(12) C3 0.0167(14) 0.0272(15) 0.0333(18) -0.0070(13) 0.0040(12) -0.0027(12) C4 0.0208(15) 0.0245(13) 0.0311(17) -0.0023(13) 0.0074(12) 0.0005(12) C5 0.0256(16) 0.0222(13) 0.0276(16) -0.0047(13) 0.0074(13) -0.0017(12) C6 0.054(3) 0.051(2) 0.0270(19) 0.0011(16) 0.0156(17) -0.0002(19) C7 0.0306(19) 0.0278(16) 0.065(3) -0.0034(17) 0.0186(18) -0.0079(14) C8 0.0294(18) 0.0439(19) 0.0306(18) -0.0115(15) 0.0002(14) -0.0020(15) C9 0.0334(19) 0.0327(17) 0.038(2) 0.0080(15) 0.0079(15) 0.0022(14) C10 0.036(2) 0.0294(16) 0.041(2) -0.0108(15) 0.0101(15) -0.0049(15) Cr1 0.0202(2) 0.0202(2) 0.0217(3) -0.00291(18) 0.00473(19) -0.00375(18) P11 0.024(4) 0.095(10) 0.017(4) -0.020(5) -0.001(3) 0.022(5) P21 0.034(7) 0.061(9) 0.089(10) 0.039(6) 0.036(6) 0.019(6) P31 0.022(2) 0.038(5) 0.087(11) -0.034(6) -0.006(6) 0.000(3) P41 0.038(6) 0.089(10) 0.026(2) 0.015(7) 0.013(4) 0.041(7) P51 0.017(3) 0.017(3) 0.077(8) -0.010(5) 0.011(5) -0.003(2) P1 0.028(4) 0.094(7) 0.018(2) -0.002(3) 0.0090(17) 0.021(3) P2 0.023(3) 0.027(3) 0.074(6) 0.020(3) 0.022(3) 0.0039(19) P3 0.0209(13) 0.045(5) 0.040(4) -0.028(3) -0.009(3) 0.010(3) P4 0.037(4) 0.054(4) 0.048(5) 0.032(4) 0.029(3) 0.023(3) P5 0.0191(17) 0.0262(16) 0.079(5) -0.030(4) 0.009(4) -0.0069(12) P12 0.026(4) 0.076(6) 0.031(3) 0.026(4) 0.015(3) 0.007(3) P22 0.017(2) 0.0197(18) 0.059(6) -0.003(3) 0.005(3) -0.0041(15) P32 0.038(4) 0.053(6) 0.014(2) -0.004(3) 0.0003(19) 0.027(4) P42 0.030(4) 0.031(4) 0.074(7) 0.025(4) 0.029(4) 0.010(2) P52 0.022(2) 0.050(4) 0.040(4) -0.033(4) 0.003(3) -0.003(2) Cr2 0.0190(2) 0.0200(2) 0.0227(3) -0.00077(18) 0.00462(18) -0.00197(18) C11 0.0243(16) 0.0243(14) 0.0260(16) 0.0081(12) 0.0076(12) 0.0050(12) C12 0.0245(16) 0.0195(13) 0.0409(19) -0.0006(13) 0.0120(14) 0.0009(12) C13 0.0238(15) 0.0335(16) 0.0271(16) -0.0051(12) 0.0043(12) 0.0050(12) C14 0.0194(15) 0.0333(16) 0.0293(17) 0.0030(13) 0.0074(12) 0.0041(13) C15 0.0201(15) 0.0241(13) 0.0275(16) 0.0033(12) 0.0054(12) 0.0015(12) C16 0.0338(19) 0.048(2) 0.0262(17) 0.0066(15) 0.0035(14) 0.0110(16) C17 0.040(2) 0.0248(15) 0.077(3) 0.0092(18) 0.028(2) 0.0029(15) C18 0.033(2) 0.052(2) 0.049(2) -0.0278(19) 0.0023(17) 0.0051(17) C19 0.039(2) 0.052(2) 0.0319(19) 0.0148(16) 0.0180(16) 0.0176(17) C20 0.0239(16) 0.0245(15) 0.049(2) 0.0053(14) 0.0031(14) -0.0025(12) C21 0.0208(15) 0.0247(12) 0.0218(15) -0.0013(11) 0.0026(11) -0.0007(12) C22 0.0249(16) 0.0250(14) 0.0251(16) -0.0018(12) 0.0044(13) 0.0079(12) C23 0.0246(16) 0.0300(16) 0.0330(18) -0.0039(13) 0.0145(13) -0.0026(13) C24 0.042(2) 0.0242(13) 0.0207(15) 0.0023(12) 0.0132(13) 0.0023(14) C25 0.0268(16) 0.0284(15) 0.0224(16) 0.0006(12) 0.0042(12) 0.0048(13) C26 0.0341(19) 0.0330(17) 0.039(2) -0.0017(15) 0.0073(15) -0.0130(15) C27 0.039(2) 0.0317(16) 0.0309(18) 0.0007(14) 0.0041(15) 0.0171(15) C28 0.0290(19) 0.050(2) 0.061(3) -0.015(2) 0.0264(19) -0.0029(17) C29 0.072(3) 0.0256(16) 0.036(2) 0.0053(14) 0.026(2) -0.0039(17) C30 0.0335(19) 0.047(2) 0.0281(18) 0.0048(15) -0.0017(14) 0.0145(16) Cr3 0.0189(2) 0.0203(2) 0.0222(3) 0.00113(18) 0.00568(19) 0.00226(18) P6 0.0648(8) 0.0584(7) 0.0488(7) -0.0276(6) 0.0365(6) -0.0381(7) P7 0.0974(11) 0.0329(5) 0.0270(5) 0.0025(4) 0.0062(6) 0.0286(6) P8 0.0230(5) 0.0859(9) 0.0486(7) -0.0317(7) 0.0087(4) -0.0053(5) P9 0.0963(11) 0.0251(4) 0.0322(6) -0.0021(4) 0.0259(6) -0.0130(5) P10 0.0411(6) 0.0736(8) 0.0341(6) -0.0186(6) -0.0064(5) 0.0323(6) Cr4 0.0196(2) 0.0201(2) 0.0202(2) 0.00002(18) 0.00427(18) -0.00038(17) C31 0.0180(15) 0.0383(17) 0.0261(16) -0.0087(14) 0.0079(12) -0.0070(13) C32 0.0315(17) 0.0236(13) 0.0185(14) 0.0005(11) 0.0058(12) -0.0048(13) C33 0.0212(15) 0.0240(13) 0.0203(14) -0.0008(11) 0.0026(11) -0.0001(11) C34 0.0367(18) 0.0221(14) 0.0215(15) -0.0011(11) 0.0081(13) -0.0044(12) C35 0.0336(18) 0.0274(13) 0.0210(15) -0.0040(12) 0.0038(12) 0.0069(13) C36 0.0302(19) 0.061(3) 0.042(2) -0.0198(19) 0.0158(16) -0.0189(18) C37 0.055(2) 0.0291(16) 0.0228(16) 0.0049(13) 0.0027(15) -0.0041(15) C38 0.0207(16) 0.049(2) 0.0371(19) -0.0051(16) 0.0018(14) -0.0042(14) C39 0.067(3) 0.0249(15) 0.0342(19) 0.0025(14) 0.0151(18) -0.0110(16) C40 0.044(2) 0.051(2) 0.035(2) -0.0096(17) -0.0065(16) 0.0233(18) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb1 F2 1.864(3) . ? Sb1 F4 1.866(2) . ? Sb1 F6 1.869(3) . ? Sb1 F3 1.870(3) . ? Sb1 F1 1.877(3) . ? Sb1 F5 1.883(3) . ? Sb2 F7 1.820(3) . ? Sb2 F8 1.833(3) . ? Sb2 F12 1.840(3) . ? Sb2 F11 1.853(3) . ? Sb2 F10 1.859(3) . ? Sb2 F9 1.861(3) . ? C1 C5 1.427(5) . ? C1 C2 1.431(5) . ? C1 C6 1.484(5) . ? C1 Cr1 2.211(4) . ? C2 C3 1.421(5) . ? C2 C7 1.512(5) . ? C2 Cr1 2.193(3) . ? C3 C4 1.429(4) . ? C3 C8 1.505(5) . ? C3 Cr1 2.196(3) . ? C4 C5 1.435(5) . ? C4 C9 1.487(5) . ? C4 Cr1 2.211(3) . ? C5 C10 1.490(5) . ? C5 Cr1 2.216(3) . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? Cr1 P51 2.394(15) . ? Cr1 P32 2.401(8) . ? Cr1 P5 2.413(6) . ? Cr1 P21 2.419(17) . ? Cr1 P4 2.414(7) . ? Cr1 P11 2.418(14) . ? Cr1 P41 2.419(18) . ? P11 P21 2.094(18) . ? P11 P51 2.142(16) . ? P11 Cr2 2.349(13) . ? P21 P31 2.131(18) . ? P21 Cr2 2.393(19) . ? P31 P41 2.191(17) . ? P31 Cr2 2.378(14) . ? P41 P51 2.155(17) . ? P41 Cr2 2.400(14) . ? P51 Cr2 2.386(13) . ? P1 P2 2.159(9) . ? P1 P5 2.192(8) . ? P1 Cr2 2.441(6) . ? P2 P3 2.172(8) . ? P2 Cr2 2.432(7) . ? P3 P4 2.196(8) . ? P3 Cr2 2.422(6) . ? P4 P5 2.195(9) . ? P4 Cr2 2.437(7) . ? P5 Cr2 2.417(6) . ? P12 P52 2.202(11) . ? P12 P22 2.208(12) . ? P12 Cr2 2.507(10) . ? P22 P32 2.200(11) . ? P22 Cr2 2.448(9) . ? P32 P42 2.216(11) . ? P32 Cr2 2.424(8) . ? P42 P52 2.215(12) . ? P42 Cr2 2.429(8) . ? P52 Cr2 2.463(8) . ? Cr2 C15 2.207(3) . ? Cr2 C11 2.208(3) . ? Cr2 C13 2.209(3) . ? Cr2 C14 2.209(4) . ? Cr2 C12 2.213(3) . ? C11 C12 1.421(5) . ? C11 C15 1.426(4) . ? C11 C16 1.497(5) . ? C12 C13 1.430(5) . ? C12 C17 1.498(5) . ? C13 C14 1.419(5) . ? C13 C18 1.505(5) . ? C14 C15 1.431(5) . ? C14 C19 1.499(5) . ? C15 C20 1.497(5) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 C25 1.425(5) . ? C21 C22 1.428(5) . ? C21 C26 1.506(5) . ? C21 Cr3 2.210(3) . ? C22 C23 1.419(5) . ? C22 C27 1.503(5) . ? C22 Cr3 2.200(3) . ? C23 C24 1.417(5) . ? C23 C28 1.506(5) . ? C23 Cr3 2.196(4) . ? C24 C25 1.435(5) . ? C24 C29 1.495(5) . ? C24 Cr3 2.214(3) . ? C25 C30 1.505(5) . ? C25 Cr3 2.198(3) . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C27 H27C 0.9800 . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? Cr3 P6 2.4241(13) . ? Cr3 P10 2.4251(12) . ? Cr3 P9 2.4347(11) . ? Cr3 P8 2.4367(13) . ? Cr3 P7 2.4482(13) . ? P6 P7 2.165(2) . ? P6 P10 2.181(2) . ? P6 Cr4 2.4392(12) . ? P7 P8 2.174(2) . ? P7 Cr4 2.4352(11) . ? P8 P9 2.174(2) . ? P8 Cr4 2.4498(13) . ? P9 P10 2.185(2) . ? P9 Cr4 2.4262(12) . ? P10 Cr4 2.4347(13) . ? Cr4 C31 2.198(3) . ? Cr4 C33 2.203(3) . ? Cr4 C34 2.205(3) . ? Cr4 C32 2.209(3) . ? Cr4 C35 2.213(3) . ? C31 C32 1.429(5) . ? C31 C35 1.430(5) . ? C31 C36 1.497(5) . ? C32 C33 1.426(5) . ? C32 C37 1.501(5) . ? C33 C34 1.431(5) . ? C33 C38 1.498(5) . ? C34 C35 1.418(5) . ? C34 C39 1.500(5) . ? C35 C40 1.502(5) . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C39 H39A 0.9800 . ? C39 H39B 0.9800 . ? C39 H39C 0.9800 . ? C40 H40A 0.9800 . ? C40 H40B 0.9800 . ? C40 H40C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F2 Sb1 F4 178.29(17) . . ? F2 Sb1 F6 90.47(14) . . ? F4 Sb1 F6 90.30(10) . . ? F2 Sb1 F3 89.59(17) . . ? F4 Sb1 F3 88.88(14) . . ? F6 Sb1 F3 90.42(16) . . ? F2 Sb1 F1 88.99(13) . . ? F4 Sb1 F1 90.28(14) . . ? F6 Sb1 F1 178.51(16) . . ? F3 Sb1 F1 90.96(17) . . ? F2 Sb1 F5 91.66(17) . . ? F4 Sb1 F5 89.88(14) . . ? F6 Sb1 F5 88.89(15) . . ? F3 Sb1 F5 178.57(12) . . ? F1 Sb1 F5 89.74(16) . . ? F7 Sb2 F8 89.7(3) . . ? F7 Sb2 F12 178.6(3) . . ? F8 Sb2 F12 89.0(2) . . ? F7 Sb2 F11 90.0(2) . . ? F8 Sb2 F11 88.72(17) . . ? F12 Sb2 F11 89.42(19) . . ? F7 Sb2 F10 93.2(3) . . ? F8 Sb2 F10 175.8(2) . . ? F12 Sb2 F10 88.0(2) . . ? F11 Sb2 F10 88.22(17) . . ? F7 Sb2 F9 89.5(2) . . ? F8 Sb2 F9 91.71(19) . . ? F12 Sb2 F9 91.07(18) . . ? F11 Sb2 F9 179.4(2) . . ? F10 Sb2 F9 91.38(18) . . ? C5 C1 C2 107.5(3) . . ? C5 C1 C6 125.4(3) . . ? C2 C1 C6 126.9(3) . . ? C5 C1 Cr1 71.4(2) . . ? C2 C1 Cr1 70.4(2) . . ? C6 C1 Cr1 126.6(3) . . ? C3 C2 C1 108.2(3) . . ? C3 C2 C7 126.6(3) . . ? C1 C2 C7 125.1(4) . . ? C3 C2 Cr1 71.23(19) . . ? C1 C2 Cr1 71.7(2) . . ? C7 C2 Cr1 125.8(2) . . ? C2 C3 C4 108.5(3) . . ? C2 C3 C8 126.5(3) . . ? C4 C3 C8 124.9(3) . . ? C2 C3 Cr1 71.0(2) . . ? C4 C3 Cr1 71.67(19) . . ? C8 C3 Cr1 125.6(3) . . ? C3 C4 C5 107.2(3) . . ? C3 C4 C9 126.4(3) . . ? C5 C4 C9 126.2(3) . . ? C3 C4 Cr1 70.51(19) . . ? C5 C4 Cr1 71.3(2) . . ? C9 C4 Cr1 126.1(3) . . ? C1 C5 C4 108.5(3) . . ? C1 C5 C10 125.6(3) . . ? C4 C5 C10 125.8(3) . . ? C1 C5 Cr1 71.01(19) . . ? C4 C5 Cr1 70.91(19) . . ? C10 C5 Cr1 126.9(3) . . ? C1 C6 H6A 109.5 . . ? C1 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C1 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C2 Cr1 C3 37.77(14) . . ? C2 Cr1 C1 37.92(13) . . ? C3 Cr1 C1 63.23(14) . . ? C2 Cr1 C4 63.35(13) . . ? C3 Cr1 C4 37.82(12) . . ? C1 Cr1 C4 63.35(13) . . ? C2 Cr1 C5 63.06(12) . . ? C3 Cr1 C5 63.00(13) . . ? C1 Cr1 C5 37.61(13) . . ? C4 Cr1 C5 37.82(13) . . ? C2 Cr1 P51 164.6(3) . . ? C3 Cr1 P51 132.8(3) . . ? C1 Cr1 P51 132.4(3) . . ? C4 Cr1 P51 102.3(3) . . ? C5 Cr1 P51 102.5(3) . . ? C2 Cr1 P32 113.5(3) . . ? C3 Cr1 P32 95.8(2) . . ? C1 Cr1 P32 151.2(3) . . ? C4 Cr1 P32 112.9(2) . . ? C5 Cr1 P32 150.4(2) . . ? P51 Cr1 P32 76.1(3) . . ? C2 Cr1 P5 160.56(16) . . ? C3 Cr1 P5 141.85(19) . . ? C1 Cr1 P5 123.16(17) . . ? C4 Cr1 P5 107.09(18) . . ? C5 Cr1 P5 98.72(17) . . ? P51 Cr1 P5 13.0(3) . . ? P32 Cr1 P5 85.6(3) . . ? C2 Cr1 P21 102.0(4) . . ? C3 Cr1 P21 132.2(3) . . ? C1 Cr1 P21 102.3(5) . . ? C4 Cr1 P21 164.5(4) . . ? C5 Cr1 P21 132.8(5) . . ? P51 Cr1 P21 91.8(5) . . ? P32 Cr1 P21 76.6(5) . . ? P5 Cr1 P21 85.3(4) . . ? C2 Cr1 P4 140.4(2) . . ? C3 Cr1 P4 105.7(2) . . ? C1 Cr1 P4 159.49(18) . . ? C4 Cr1 P4 97.07(18) . . ? C5 Cr1 P4 122.66(18) . . ? P51 Cr1 P4 41.7(3) . . ? P32 Cr1 P4 39.7(2) . . ? P5 Cr1 P4 54.1(2) . . ? P21 Cr1 P4 97.7(5) . . ? C2 Cr1 P11 132.8(3) . . ? C3 Cr1 P11 166.0(3) . . ? C1 Cr1 P11 103.3(3) . . ? C4 Cr1 P11 134.5(4) . . ? C5 Cr1 P11 104.3(4) . . ? P51 Cr1 P11 52.9(4) . . ? P32 Cr1 P11 98.2(4) . . ? P5 Cr1 P11 41.3(3) . . ? P21 Cr1 P11 51.3(4) . . ? P4 Cr1 P11 86.0(3) . . ? C2 Cr1 P41 131.8(4) . . ? C3 Cr1 P41 101.3(4) . . ? C1 Cr1 P41 163.5(4) . . ? C4 Cr1 P41 101.1(3) . . ? C5 Cr1 P41 131.9(3) . . ? P51 Cr1 P41 53.2(4) . . ? P32 Cr1 P41 27.0(4) . . ? P5 Cr1 P41 64.9(4) . . ? P21 Cr1 P41 92.4(6) . . ? P4 Cr1 P41 12.9(3) . . ? P11 Cr1 P41 91.7(5) . . ? P21 P11 P51 109.3(8) . . ? P21 P11 Cr2 64.9(7) . . ? P51 P11 Cr2 64.0(4) . . ? P21 P11 Cr1 64.4(6) . . ? P51 P11 Cr1 63.0(5) . . ? Cr2 P11 Cr1 81.8(4) . . ? P11 P21 P31 108.6(9) . . ? P11 P21 Cr2 62.7(5) . . ? P31 P21 Cr2 63.1(6) . . ? P11 P21 Cr1 64.3(6) . . ? P31 P21 Cr1 64.3(6) . . ? Cr2 P21 Cr1 80.8(6) . . ? P21 P31 P41 107.9(8) . . ? P21 P31 Cr2 63.8(5) . . ? P41 P31 Cr2 63.2(6) . . ? P21 P31 Cr1 63.6(6) . . ? P41 P31 Cr1 62.8(6) . . ? Cr2 P31 Cr1 80.8(4) . . ? P51 P41 P31 106.4(8) . . ? P51 P41 Cr2 62.9(5) . . ? P31 P41 Cr2 62.2(5) . . ? P51 P41 Cr1 62.8(6) . . ? P31 P41 Cr1 63.5(6) . . ? Cr2 P41 Cr1 80.7(5) . . ? P11 P51 P41 107.8(8) . . ? P11 P51 Cr2 62.2(5) . . ? P41 P51 Cr2 63.6(4) . . ? P11 P51 Cr1 64.2(5) . . ? P41 P51 Cr1 64.0(5) . . ? Cr2 P51 Cr1 81.5(4) . . ? P2 P1 P5 107.8(4) . . ? P2 P1 Cr1 63.6(2) . . ? P5 P1 Cr1 62.7(2) . . ? P2 P1 Cr2 63.5(3) . . ? P5 P1 Cr2 62.61(19) . . ? Cr1 P1 Cr2 79.7(2) . . ? P1 P2 P3 108.8(3) . . ? P1 P2 Cr1 63.6(2) . . ? P3 P2 Cr1 63.3(2) . . ? P1 P2 Cr2 63.9(2) . . ? P3 P2 Cr2 63.2(3) . . ? Cr1 P2 Cr2 79.91(18) . . ? P2 P3 P4 108.2(3) . . ? P2 P3 Cr2 63.65(19) . . ? P4 P3 Cr2 63.5(3) . . ? P2 P3 Cr1 63.5(2) . . ? P4 P3 Cr1 62.8(2) . . ? Cr2 P3 Cr1 80.21(17) . . ? P5 P4 P3 106.9(4) . . ? P5 P4 Cr1 62.9(3) . . ? P3 P4 Cr1 63.2(2) . . ? P5 P4 Cr2 62.6(3) . . ? P3 P4 Cr2 62.76(19) . . ? Cr1 P4 Cr2 80.1(2) . . ? P1 P5 P4 108.3(3) . . ? P1 P5 Cr1 63.4(3) . . ? P4 P5 Cr1 63.0(2) . . ? P1 P5 Cr2 63.7(3) . . ? P4 P5 Cr2 63.6(2) . . ? Cr1 P5 Cr2 80.48(18) . . ? P52 P12 P22 108.0(5) . . ? P52 P12 Cr1 63.9(3) . . ? P22 P12 Cr1 62.7(4) . . ? P52 P12 Cr2 62.7(3) . . ? P22 P12 Cr2 62.2(4) . . ? Cr1 P12 Cr2 78.2(3) . . ? P32 P22 P12 108.3(5) . . ? P32 P22 Cr1 62.3(3) . . ? P12 P22 Cr1 63.3(3) . . ? P32 P22 Cr2 62.6(4) . . ? P12 P22 Cr2 64.9(3) . . ? Cr1 P22 Cr2 79.6(3) . . ? P22 P32 P42 107.8(5) . . ? P22 P32 Cr1 63.4(3) . . ? P42 P32 Cr1 63.1(3) . . ? P22 P32 Cr2 63.7(3) . . ? P42 P32 Cr2 62.9(3) . . ? Cr1 P32 Cr2 80.6(2) . . ? P32 P42 P52 107.8(5) . . ? P32 P42 Cr1 62.2(3) . . ? P52 P42 Cr1 64.0(4) . . ? P32 P42 Cr2 62.7(3) . . ? P52 P42 Cr2 63.9(3) . . ? Cr1 P42 Cr2 80.1(3) . . ? P12 P52 P42 108.0(5) . . ? P12 P52 Cr2 64.7(4) . . ? P42 P52 Cr2 62.3(3) . . ? P12 P52 Cr1 62.7(4) . . ? P42 P52 Cr1 62.1(3) . . ? Cr2 P52 Cr1 78.6(2) . . ? C15 Cr2 C11 37.68(12) . . ? C15 Cr2 C13 63.19(13) . . ? C11 Cr2 C13 62.93(13) . . ? C15 Cr2 C14 37.82(13) . . ? C11 Cr2 C14 62.78(13) . . ? C13 Cr2 C14 37.46(13) . . ? C15 Cr2 C12 63.03(12) . . ? C11 Cr2 C12 37.50(13) . . ? C13 Cr2 C12 37.72(14) . . ? C14 Cr2 C12 62.71(13) . . ? C15 Cr2 P11 104.7(4) . . ? C11 Cr2 P11 98.9(4) . . ? C13 Cr2 P11 161.6(4) . . ? C14 Cr2 P11 138.5(4) . . ? C12 Cr2 P11 125.5(4) . . ? C15 Cr2 P31 162.1(4) . . ? C11 Cr2 P31 137.9(4) . . ? C13 Cr2 P31 99.0(4) . . ? C14 Cr2 P31 126.1(4) . . ? C12 Cr2 P31 104.7(4) . . ? P11 Cr2 P31 93.1(5) . . ? C15 Cr2 P51 98.5(3) . . ? C11 Cr2 P51 125.6(3) . . ? C13 Cr2 P51 138.1(4) . . ? C14 Cr2 P51 104.8(4) . . ? C12 Cr2 P51 161.3(3) . . ? P11 Cr2 P51 53.8(4) . . ? P31 Cr2 P51 93.9(5) . . ? C15 Cr2 P21 138.4(4) . . ? C11 Cr2 P21 105.4(4) . . ? C13 Cr2 P21 126.8(4) . . ? C14 Cr2 P21 162.5(4) . . ? C12 Cr2 P21 99.9(4) . . ? P11 Cr2 P21 52.4(4) . . ? P31 Cr2 P21 53.1(4) . . ? P51 Cr2 P21 92.6(5) . . ? C15 Cr2 P41 125.0(4) . . ? C11 Cr2 P41 160.9(4) . . ? C13 Cr2 P41 104.3(4) . . ? C14 Cr2 P41 98.4(4) . . ? C12 Cr2 P41 138.2(4) . . ? P11 Cr2 P41 93.9(6) . . ? P31 Cr2 P41 54.6(4) . . ? P51 Cr2 P41 53.5(4) . . ? P21 Cr2 P41 93.6(6) . . ? C15 Cr2 P5 96.30(17) . . ? C11 Cr2 P5 117.07(18) . . ? C13 Cr2 P5 147.17(19) . . ? C14 Cr2 P5 110.80(18) . . ? C12 Cr2 P5 154.57(18) . . ? P11 Cr2 P5 41.8(4) . . ? P31 Cr2 P5 98.6(4) . . ? P51 Cr2 P5 13.0(3) . . ? P21 Cr2 P5 85.8(4) . . ? P41 Cr2 P5 65.1(4) . . ? C15 Cr2 P3 155.42(17) . . ? C11 Cr2 P3 147.63(17) . . ? C13 Cr2 P3 97.18(16) . . ? C14 Cr2 P3 117.62(18) . . ? C12 Cr2 P3 111.27(17) . . ? P11 Cr2 P3 97.7(4) . . ? P31 Cr2 P3 13.5(3) . . ? P51 Cr2 P3 86.5(3) . . ? P21 Cr2 P3 64.7(4) . . ? P41 Cr2 P3 41.9(4) . . ? P5 Cr2 P3 93.6(2) . . ? C12 C11 C15 108.5(3) . . ? C12 C11 C16 124.6(3) . . ? C15 C11 C16 126.8(3) . . ? C12 C11 Cr2 71.4(2) . . ? C15 C11 Cr2 71.11(19) . . ? C16 C11 Cr2 125.9(3) . . ? C11 C12 C13 107.9(3) . . ? C11 C12 C17 126.1(4) . . ? C13 C12 C17 125.8(4) . . ? C11 C12 Cr2 71.07(19) . . ? C13 C12 Cr2 71.0(2) . . ? C17 C12 Cr2 126.2(3) . . ? C14 C13 C12 107.8(3) . . ? C14 C13 C18 125.0(4) . . ? C12 C13 C18 127.0(4) . . ? C14 C13 Cr2 71.3(2) . . ? C12 C13 Cr2 71.29(19) . . ? C18 C13 Cr2 127.0(3) . . ? C13 C14 C15 108.5(3) . . ? C13 C14 C19 126.3(4) . . ? C15 C14 C19 125.1(3) . . ? C13 C14 Cr2 71.2(2) . . ? C15 C14 Cr2 71.0(2) . . ? C19 C14 Cr2 125.0(2) . . ? C11 C15 C14 107.3(3) . . ? C11 C15 C20 126.4(3) . . ? C14 C15 C20 126.2(3) . . ? C11 C15 Cr2 71.2(2) . . ? C14 C15 Cr2 71.19(19) . . ? C20 C15 Cr2 125.5(2) . . ? C11 C16 H16A 109.5 . . ? C11 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C11 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C25 C21 C22 107.5(3) . . ? C25 C21 C26 125.5(3) . . ? C22 C21 C26 126.8(3) . . ? C25 C21 Cr3 70.69(19) . . ? C22 C21 Cr3 70.73(18) . . ? C26 C21 Cr3 127.5(3) . . ? C23 C22 C21 108.1(3) . . ? C23 C22 C27 125.5(3) . . ? C21 C22 C27 126.3(3) . . ? C23 C22 Cr3 71.01(19) . . ? C21 C22 Cr3 71.49(18) . . ? C27 C22 Cr3 127.2(3) . . ? C24 C23 C22 108.8(3) . . ? C24 C23 C28 126.0(4) . . ? C22 C23 C28 125.0(4) . . ? C24 C23 Cr3 72.0(2) . . ? C22 C23 Cr3 71.3(2) . . ? C28 C23 Cr3 126.0(3) . . ? C23 C24 C25 107.2(3) . . ? C23 C24 C29 126.1(4) . . ? C25 C24 C29 126.7(4) . . ? C23 C24 Cr3 70.6(2) . . ? C25 C24 Cr3 70.41(19) . . ? C29 C24 Cr3 125.5(3) . . ? C21 C25 C24 108.4(3) . . ? C21 C25 C30 125.2(3) . . ? C24 C25 C30 126.2(3) . . ? C21 C25 Cr3 71.60(19) . . ? C24 C25 Cr3 71.6(2) . . ? C30 C25 Cr3 126.1(3) . . ? C21 C26 H26A 109.5 . . ? C21 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C21 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C22 C27 H27A 109.5 . . ? C22 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? C22 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? C23 C28 H28A 109.5 . . ? C23 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C23 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C24 C29 H29A 109.5 . . ? C24 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C24 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C25 C30 H30A 109.5 . . ? C25 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? C25 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C23 Cr3 C25 62.99(13) . . ? C23 Cr3 C22 37.67(13) . . ? C25 Cr3 C22 63.06(13) . . ? C23 Cr3 C21 63.07(13) . . ? C25 Cr3 C21 37.71(12) . . ? C22 Cr3 C21 37.78(13) . . ? C23 Cr3 C24 37.48(14) . . ? C25 Cr3 C24 37.96(14) . . ? C22 Cr3 C24 63.00(12) . . ? C21 Cr3 C24 63.25(12) . . ? C23 Cr3 P6 155.05(10) . . ? C25 Cr3 P6 111.92(10) . . ? C22 Cr3 P6 117.42(11) . . ? C21 Cr3 P6 97.44(10) . . ? C24 Cr3 P6 148.81(12) . . ? C23 Cr3 P10 147.84(11) . . ? C25 Cr3 P10 96.80(10) . . ? C22 Cr3 P10 154.68(10) . . ? C21 Cr3 P10 116.92(10) . . ? C24 Cr3 P10 111.34(10) . . ? P6 Cr3 P10 53.45(6) . . ? C23 Cr3 P9 111.35(10) . . ? C25 Cr3 P9 117.07(10) . . ? C22 Cr3 P9 147.97(11) . . ? C21 Cr3 P9 154.76(10) . . ? C24 Cr3 P9 96.85(9) . . ? P6 Cr3 P9 92.88(5) . . ? P10 Cr3 P9 53.44(5) . . ? C23 Cr3 P8 97.18(10) . . ? C25 Cr3 P8 154.69(11) . . ? C22 Cr3 P8 111.67(10) . . ? C21 Cr3 P8 148.43(10) . . ? C24 Cr3 P8 116.78(11) . . ? P6 Cr3 P8 92.66(5) . . ? P10 Cr3 P8 93.06(5) . . ? P9 Cr3 P8 53.00(5) . . ? C23 Cr3 P7 117.85(11) . . ? C25 Cr3 P7 149.04(10) . . ? C22 Cr3 P7 98.09(10) . . ? C21 Cr3 P7 112.46(9) . . ? C24 Cr3 P7 155.23(11) . . ? P6 Cr3 P7 52.77(6) . . ? P10 Cr3 P7 92.54(5) . . ? P9 Cr3 P7 92.11(4) . . ? P8 Cr3 P7 52.85(6) . . ? P7 P6 P10 108.24(7) . . ? P7 P6 Cr3 64.19(5) . . ? P10 P6 Cr3 63.30(5) . . ? P7 P6 Cr4 63.53(5) . . ? P10 P6 Cr4 63.31(5) . . ? Cr3 P6 Cr4 81.22(4) . . ? P6 P7 P8 108.24(7) . . ? P6 P7 Cr4 63.72(5) . . ? P8 P7 Cr4 63.92(5) . . ? P6 P7 Cr3 63.05(5) . . ? P8 P7 Cr3 63.30(5) . . ? Cr4 P7 Cr3 80.82(4) . . ? P9 P8 P7 107.92(7) . . ? P9 P8 Cr3 63.45(5) . . ? P7 P8 Cr3 63.85(5) . . ? P9 P8 Cr4 62.97(5) . . ? P7 P8 Cr4 63.23(5) . . ? Cr3 P8 Cr4 80.76(4) . . ? P8 P9 P10 108.09(7) . . ? P8 P9 Cr4 64.08(5) . . ? P10 P9 Cr4 63.48(5) . . ? P8 P9 Cr3 63.54(5) . . ? P10 P9 Cr3 63.05(4) . . ? Cr4 P9 Cr3 81.27(4) . . ? P6 P10 P9 107.49(7) . . ? P6 P10 Cr3 63.25(5) . . ? P9 P10 Cr3 63.50(5) . . ? P6 P10 Cr4 63.53(5) . . ? P9 P10 Cr4 63.09(5) . . ? Cr3 P10 Cr4 81.29(4) . . ? C31 Cr4 C33 63.20(12) . . ? C31 Cr4 C34 63.11(13) . . ? C33 Cr4 C34 37.87(12) . . ? C31 Cr4 C32 37.84(13) . . ? C33 Cr4 C32 37.72(12) . . ? C34 Cr4 C32 63.15(12) . . ? C31 Cr4 C35 37.82(14) . . ? C33 Cr4 C35 62.97(13) . . ? C34 Cr4 C35 37.43(14) . . ? C32 Cr4 C35 63.08(13) . . ? C31 Cr4 P9 144.12(11) . . ? C33 Cr4 P9 121.50(10) . . ? C34 Cr4 P9 98.29(10) . . ? C32 Cr4 P9 159.07(9) . . ? C35 Cr4 P9 108.80(10) . . ? C31 Cr4 P10 107.96(10) . . ? C33 Cr4 P10 158.81(9) . . ? C34 Cr4 P10 121.18(10) . . ? C32 Cr4 P10 143.41(10) . . ? C35 Cr4 P10 97.88(9) . . ? P9 Cr4 P10 53.43(5) . . ? C31 Cr4 P7 120.76(11) . . ? C33 Cr4 P7 108.47(9) . . ? C34 Cr4 P7 144.17(11) . . ? C32 Cr4 P7 97.63(9) . . ? C35 Cr4 P7 158.39(10) . . ? P9 Cr4 P7 92.63(4) . . ? P10 Cr4 P7 92.62(5) . . ? C31 Cr4 P6 97.49(9) . . ? C33 Cr4 P6 143.42(9) . . ? C34 Cr4 P6 158.45(11) . . ? C32 Cr4 P6 108.02(9) . . ? C35 Cr4 P6 121.23(11) . . ? P9 Cr4 P6 92.71(5) . . ? P10 Cr4 P6 53.16(6) . . ? P7 Cr4 P6 52.75(6) . . ? C31 Cr4 P8 159.25(10) . . ? C33 Cr4 P8 98.63(10) . . ? C34 Cr4 P8 109.46(11) . . ? C32 Cr4 P8 121.51(10) . . ? C35 Cr4 P8 144.56(11) . . ? P9 Cr4 P8 52.95(5) . . ? P10 Cr4 P8 92.50(5) . . ? P7 Cr4 P8 52.85(6) . . ? P6 Cr4 P8 91.96(5) . . ? C32 C31 C35 108.0(3) . . ? C32 C31 C36 126.2(4) . . ? C35 C31 C36 125.7(4) . . ? C32 C31 Cr4 71.47(19) . . ? C35 C31 Cr4 71.7(2) . . ? C36 C31 Cr4 125.5(3) . . ? C33 C32 C31 107.8(3) . . ? C33 C32 C37 126.4(3) . . ? C31 C32 C37 125.9(3) . . ? C33 C32 Cr4 70.94(19) . . ? C31 C32 Cr4 70.69(19) . . ? C37 C32 Cr4 124.8(2) . . ? C32 C33 C34 108.0(3) . . ? C32 C33 C38 126.8(3) . . ? C34 C33 C38 125.1(3) . . ? C32 C33 Cr4 71.34(18) . . ? C34 C33 Cr4 71.12(19) . . ? C38 C33 Cr4 125.9(3) . . ? C35 C34 C33 108.1(3) . . ? C35 C34 C39 126.8(3) . . ? C33 C34 C39 124.9(4) . . ? C35 C34 Cr4 71.59(19) . . ? C33 C34 Cr4 71.00(18) . . ? C39 C34 Cr4 126.6(3) . . ? C34 C35 C31 108.1(3) . . ? C34 C35 C40 125.3(4) . . ? C31 C35 C40 126.6(4) . . ? C34 C35 Cr4 70.97(19) . . ? C31 C35 Cr4 70.53(18) . . ? C40 C35 Cr4 126.4(2) . . ? C31 C36 H36A 109.5 . . ? C31 C36 H36B 109.5 . . ? H36A C36 H36B 109.5 . . ? C31 C36 H36C 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C32 C37 H37A 109.5 . . ? C32 C37 H37B 109.5 . . ? H37A C37 H37B 109.5 . . ? C32 C37 H37C 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? C33 C38 H38A 109.5 . . ? C33 C38 H38B 109.5 . . ? H38A C38 H38B 109.5 . . ? C33 C38 H38C 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? C34 C39 H39A 109.5 . . ? C34 C39 H39B 109.5 . . ? H39A C39 H39B 109.5 . . ? C34 C39 H39C 109.5 . . ? H39A C39 H39C 109.5 . . ? H39B C39 H39C 109.5 . . ? C35 C40 H40A 109.5 . . ? C35 C40 H40B 109.5 . . ? H40A C40 H40B 109.5 . . ? C35 C40 H40C 109.5 . . ? H40A C40 H40C 109.5 . . ? H40B C40 H40C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 C1 C2 C3 -0.2(4) . . . . ? C6 C1 C2 C3 176.1(4) . . . . ? Cr1 C1 C2 C3 -62.3(2) . . . . ? C5 C1 C2 C7 -176.5(3) . . . . ? C6 C1 C2 C7 -0.2(6) . . . . ? Cr1 C1 C2 C7 121.4(4) . . . . ? C5 C1 C2 Cr1 62.1(2) . . . . ? C6 C1 C2 Cr1 -121.6(4) . . . . ? C1 C2 C3 C4 0.4(4) . . . . ? C7 C2 C3 C4 176.6(3) . . . . ? Cr1 C2 C3 C4 -62.2(2) . . . . ? C1 C2 C3 C8 -176.7(3) . . . . ? C7 C2 C3 C8 -0.4(6) . . . . ? Cr1 C2 C3 C8 120.8(4) . . . . ? C1 C2 C3 Cr1 62.6(2) . . . . ? C7 C2 C3 Cr1 -121.2(4) . . . . ? C2 C3 C4 C5 -0.4(4) . . . . ? C8 C3 C4 C5 176.7(3) . . . . ? Cr1 C3 C4 C5 -62.2(2) . . . . ? C2 C3 C4 C9 -177.1(3) . . . . ? C8 C3 C4 C9 0.0(6) . . . . ? Cr1 C3 C4 C9 121.1(4) . . . . ? C2 C3 C4 Cr1 61.8(2) . . . . ? C8 C3 C4 Cr1 -121.1(4) . . . . ? C2 C1 C5 C4 -0.1(4) . . . . ? C6 C1 C5 C4 -176.5(4) . . . . ? Cr1 C1 C5 C4 61.3(2) . . . . ? C2 C1 C5 C10 176.2(3) . . . . ? C6 C1 C5 C10 -0.2(6) . . . . ? Cr1 C1 C5 C10 -122.4(4) . . . . ? C2 C1 C5 Cr1 -61.4(2) . . . . ? C6 C1 C5 Cr1 122.2(4) . . . . ? C3 C4 C5 C1 0.3(4) . . . . ? C9 C4 C5 C1 177.0(3) . . . . ? Cr1 C4 C5 C1 -61.4(2) . . . . ? C3 C4 C5 C10 -176.0(3) . . . . ? C9 C4 C5 C10 0.7(6) . . . . ? Cr1 C4 C5 C10 122.3(4) . . . . ? C3 C4 C5 Cr1 61.7(2) . . . . ? C9 C4 C5 Cr1 -121.6(4) . . . . ? C1 C2 Cr1 C3 -117.4(3) . . . . ? C7 C2 Cr1 C3 122.1(4) . . . . ? C3 C2 Cr1 C1 117.4(3) . . . . ? C7 C2 Cr1 C1 -120.5(5) . . . . ? C3 C2 Cr1 C4 37.32(19) . . . . ? C1 C2 Cr1 C4 -80.1(2) . . . . ? C7 C2 Cr1 C4 159.4(4) . . . . ? C3 C2 Cr1 C5 79.9(2) . . . . ? C1 C2 Cr1 C5 -37.5(2) . . . . ? C7 C2 Cr1 C5 -158.0(4) . . . . ? C3 C2 Cr1 P51 59.2(11) . . . . ? C1 C2 Cr1 P51 -58.2(11) . . . . ? C7 C2 Cr1 P51 -178.7(10) . . . . ? C3 C2 Cr1 P32 -67.5(3) . . . . ? C1 C2 Cr1 P32 175.1(3) . . . . ? C7 C2 Cr1 P32 54.6(4) . . . . ? C3 C2 Cr1 P5 101.6(6) . . . . ? C1 C2 Cr1 P5 -15.8(7) . . . . ? C7 C2 Cr1 P5 -136.3(6) . . . . ? C3 C2 Cr1 P21 -147.9(4) . . . . ? C1 C2 Cr1 P21 94.7(5) . . . . ? C7 C2 Cr1 P21 -25.8(5) . . . . ? C3 C2 Cr1 P4 -29.7(3) . . . . ? C1 C2 Cr1 P4 -147.1(3) . . . . ? C7 C2 Cr1 P4 92.4(4) . . . . ? C3 C2 Cr1 P11 164.6(5) . . . . ? C1 C2 Cr1 P11 47.2(6) . . . . ? C7 C2 Cr1 P11 -73.3(6) . . . . ? C3 C2 Cr1 P41 -43.5(5) . . . . ? C1 C2 Cr1 P41 -160.9(4) . . . . ? C7 C2 Cr1 P41 78.6(5) . . . . ? C4 C3 Cr1 C2 117.9(3) . . . . ? C8 C3 Cr1 C2 -121.8(4) . . . . ? C2 C3 Cr1 C1 -37.68(19) . . . . ? C4 C3 Cr1 C1 80.2(2) . . . . ? C8 C3 Cr1 C1 -159.5(4) . . . . ? C2 C3 Cr1 C4 -117.9(3) . . . . ? C8 C3 Cr1 C4 120.3(4) . . . . ? C2 C3 Cr1 C5 -80.0(2) . . . . ? C4 C3 Cr1 C5 37.9(2) . . . . ? C8 C3 Cr1 C5 158.1(4) . . . . ? C2 C3 Cr1 P51 -161.9(4) . . . . ? C4 C3 Cr1 P51 -44.0(4) . . . . ? C8 C3 Cr1 P51 76.2(5) . . . . ? C2 C3 Cr1 P32 121.6(3) . . . . ? C4 C3 Cr1 P32 -120.4(3) . . . . ? C8 C3 Cr1 P32 -0.2(4) . . . . ? C2 C3 Cr1 P5 -148.1(3) . . . . ? C4 C3 Cr1 P5 -30.2(4) . . . . ? C8 C3 Cr1 P5 90.0(4) . . . . ? C2 C3 Cr1 P21 44.6(7) . . . . ? C4 C3 Cr1 P21 162.5(6) . . . . ? C8 C3 Cr1 P21 -77.2(7) . . . . ? C2 C3 Cr1 P4 160.9(2) . . . . ? C4 C3 Cr1 P4 -81.2(3) . . . . ? C8 C3 Cr1 P4 39.0(4) . . . . ? C2 C3 Cr1 P11 -53.8(15) . . . . ? C4 C3 Cr1 P11 64.1(15) . . . . ? C8 C3 Cr1 P11 -175.6(14) . . . . ? C2 C3 Cr1 P41 148.4(4) . . . . ? C4 C3 Cr1 P41 -93.7(4) . . . . ? C8 C3 Cr1 P41 26.6(5) . . . . ? C5 C1 Cr1 C2 -117.3(3) . . . . ? C6 C1 Cr1 C2 121.9(4) . . . . ? C5 C1 Cr1 C3 -79.7(2) . . . . ? C2 C1 Cr1 C3 37.5(2) . . . . ? C6 C1 Cr1 C3 159.5(4) . . . . ? C5 C1 Cr1 C4 -37.2(2) . . . . ? C2 C1 Cr1 C4 80.1(2) . . . . ? C6 C1 Cr1 C4 -158.0(4) . . . . ? C2 C1 Cr1 C5 117.3(3) . . . . ? C6 C1 Cr1 C5 -120.8(4) . . . . ? C5 C1 Cr1 P51 45.0(5) . . . . ? C2 C1 Cr1 P51 162.2(5) . . . . ? C6 C1 Cr1 P51 -75.8(6) . . . . ? C5 C1 Cr1 P32 -126.6(4) . . . . ? C2 C1 Cr1 P32 -9.3(5) . . . . ? C6 C1 Cr1 P32 112.6(5) . . . . ? C5 C1 Cr1 P5 56.5(3) . . . . ? C2 C1 Cr1 P5 173.8(3) . . . . ? C6 C1 Cr1 P5 -64.3(4) . . . . ? C5 C1 Cr1 P21 149.0(4) . . . . ? C2 C1 Cr1 P21 -93.7(4) . . . . ? C6 C1 Cr1 P21 28.2(5) . . . . ? C5 C1 Cr1 P4 -18.8(7) . . . . ? C2 C1 Cr1 P4 98.4(6) . . . . ? C6 C1 Cr1 P4 -139.6(6) . . . . ? C5 C1 Cr1 P11 96.3(4) . . . . ? C2 C1 Cr1 P11 -146.4(4) . . . . ? C6 C1 Cr1 P11 -24.5(5) . . . . ? C5 C1 Cr1 P41 -58.2(13) . . . . ? C2 C1 Cr1 P41 59.0(13) . . . . ? C6 C1 Cr1 P41 -179.0(12) . . . . ? C3 C4 Cr1 C2 -37.3(2) . . . . ? C5 C4 Cr1 C2 79.6(2) . . . . ? C9 C4 Cr1 C2 -158.7(4) . . . . ? C5 C4 Cr1 C3 116.9(3) . . . . ? C9 C4 Cr1 C3 -121.5(4) . . . . ? C3 C4 Cr1 C1 -79.9(2) . . . . ? C5 C4 Cr1 C1 37.0(2) . . . . ? C9 C4 Cr1 C1 158.6(4) . . . . ? C3 C4 Cr1 C5 -116.9(3) . . . . ? C9 C4 Cr1 C5 121.7(4) . . . . ? C3 C4 Cr1 P51 148.5(3) . . . . ? C5 C4 Cr1 P51 -94.6(3) . . . . ? C9 C4 Cr1 P51 27.1(4) . . . . ? C3 C4 Cr1 P32 68.6(3) . . . . ? C5 C4 Cr1 P32 -174.5(3) . . . . ? C9 C4 Cr1 P32 -52.9(4) . . . . ? C3 C4 Cr1 P5 161.0(2) . . . . ? C5 C4 Cr1 P5 -82.1(2) . . . . ? C9 C4 Cr1 P5 39.6(4) . . . . ? C3 C4 Cr1 P21 -56.7(14) . . . . ? C5 C4 Cr1 P21 60.2(14) . . . . ? C9 C4 Cr1 P21 -178.2(13) . . . . ? C3 C4 Cr1 P4 106.5(3) . . . . ? C5 C4 Cr1 P4 -136.6(3) . . . . ? C9 C4 Cr1 P4 -15.0(4) . . . . ? C3 C4 Cr1 P11 -162.2(4) . . . . ? C5 C4 Cr1 P11 -45.3(4) . . . . ? C9 C4 Cr1 P11 76.3(5) . . . . ? C3 C4 Cr1 P41 94.1(4) . . . . ? C5 C4 Cr1 P41 -149.0(4) . . . . ? C9 C4 Cr1 P41 -27.3(5) . . . . ? C1 C5 Cr1 C2 37.8(2) . . . . ? C4 C5 Cr1 C2 -80.5(2) . . . . ? C10 C5 Cr1 C2 158.5(4) . . . . ? C1 C5 Cr1 C3 80.4(2) . . . . ? C4 C5 Cr1 C3 -37.9(2) . . . . ? C10 C5 Cr1 C3 -158.9(4) . . . . ? C4 C5 Cr1 C1 -118.3(3) . . . . ? C10 C5 Cr1 C1 120.7(4) . . . . ? C1 C5 Cr1 C4 118.3(3) . . . . ? C10 C5 Cr1 C4 -121.0(4) . . . . ? C1 C5 Cr1 P51 -147.7(4) . . . . ? C4 C5 Cr1 P51 94.0(3) . . . . ? C10 C5 Cr1 P51 -27.0(5) . . . . ? C1 C5 Cr1 P32 128.5(5) . . . . ? C4 C5 Cr1 P32 10.2(6) . . . . ? C10 C5 Cr1 P32 -110.8(6) . . . . ? C1 C5 Cr1 P5 -135.0(3) . . . . ? C4 C5 Cr1 P5 106.7(3) . . . . ? C10 C5 Cr1 P5 -14.3(4) . . . . ? C1 C5 Cr1 P21 -43.3(5) . . . . ? C4 C5 Cr1 P21 -161.6(5) . . . . ? C10 C5 Cr1 P21 77.4(6) . . . . ? C1 C5 Cr1 P4 172.3(3) . . . . ? C4 C5 Cr1 P4 54.0(3) . . . . ? C10 C5 Cr1 P4 -67.0(4) . . . . ? C1 C5 Cr1 P11 -93.3(4) . . . . ? C4 C5 Cr1 P11 148.5(3) . . . . ? C10 C5 Cr1 P11 27.5(5) . . . . ? C1 C5 Cr1 P41 161.0(5) . . . . ? C4 C5 Cr1 P41 42.8(6) . . . . ? C10 C5 Cr1 P41 -78.2(6) . . . . ? C2 Cr1 P11 P21 67.7(8) . . . . ? C3 Cr1 P11 P21 110.1(15) . . . . ? C1 Cr1 P11 P21 95.3(6) . . . . ? C4 Cr1 P11 P21 160.8(6) . . . . ? C5 Cr1 P11 P21 134.0(6) . . . . ? P51 Cr1 P11 P21 -131.0(8) . . . . ? P32 Cr1 P11 P21 -65.4(6) . . . . ? P5 Cr1 P11 P21 -139.0(8) . . . . ? P4 Cr1 P11 P21 -103.3(6) . . . . ? P41 Cr1 P11 P21 -91.7(7) . . . . ? C2 Cr1 P11 P51 -161.3(4) . . . . ? C3 Cr1 P11 P51 -118.9(13) . . . . ? C1 Cr1 P11 P51 -133.7(4) . . . . ? C4 Cr1 P11 P51 -68.2(5) . . . . ? C5 Cr1 P11 P51 -95.0(4) . . . . ? P32 Cr1 P11 P51 65.6(5) . . . . ? P5 Cr1 P11 P51 -8.0(5) . . . . ? P21 Cr1 P11 P51 131.0(8) . . . . ? P4 Cr1 P11 P51 27.7(4) . . . . ? P41 Cr1 P11 P51 39.2(5) . . . . ? C2 Cr1 P11 Cr2 133.7(2) . . . . ? C3 Cr1 P11 Cr2 176.1(11) . . . . ? C1 Cr1 P11 Cr2 161.3(2) . . . . ? C4 Cr1 P11 Cr2 -133.2(3) . . . . ? C5 Cr1 P11 Cr2 -159.9(3) . . . . ? P51 Cr1 P11 Cr2 -64.9(4) . . . . ? P32 Cr1 P11 Cr2 0.7(4) . . . . ? P5 Cr1 P11 Cr2 -73.0(4) . . . . ? P21 Cr1 P11 Cr2 66.1(7) . . . . ? P4 Cr1 P11 Cr2 -37.2(3) . . . . ? P41 Cr1 P11 Cr2 -25.7(4) . . . . ? P51 P11 P21 P31 2.6(11) . . . . ? Cr2 P11 P21 P31 -44.7(7) . . . . ? Cr1 P11 P21 P31 48.1(7) . . . . ? P51 P11 P21 Cr2 47.4(6) . . . . ? Cr1 P11 P21 Cr2 92.8(4) . . . . ? P51 P11 P21 Cr1 -45.4(7) . . . . ? Cr2 P11 P21 Cr1 -92.8(4) . . . . ? C2 Cr1 P21 P11 -136.1(5) . . . . ? C3 Cr1 P21 P11 -162.1(4) . . . . ? C1 Cr1 P21 P11 -97.2(5) . . . . ? C4 Cr1 P21 P11 -118.4(12) . . . . ? C5 Cr1 P21 P11 -71.8(7) . . . . ? P51 Cr1 P21 P11 37.0(5) . . . . ? P32 Cr1 P21 P11 112.3(6) . . . . ? P5 Cr1 P21 P11 25.7(5) . . . . ? P4 Cr1 P21 P11 78.5(5) . . . . ? P41 Cr1 P21 P11 90.3(6) . . . . ? C2 Cr1 P21 P31 95.4(5) . . . . ? C3 Cr1 P21 P31 69.4(7) . . . . ? C1 Cr1 P21 P31 134.3(5) . . . . ? C4 Cr1 P21 P31 113.1(14) . . . . ? C5 Cr1 P21 P31 159.6(5) . . . . ? P51 Cr1 P21 P31 -91.5(6) . . . . ? P32 Cr1 P21 P31 -16.2(6) . . . . ? P5 Cr1 P21 P31 -102.8(5) . . . . ? P4 Cr1 P21 P31 -50.0(6) . . . . ? P11 Cr1 P21 P31 -128.5(8) . . . . ? P41 Cr1 P21 P31 -38.3(6) . . . . ? C2 Cr1 P21 Cr2 159.9(2) . . . . ? C3 Cr1 P21 Cr2 133.8(3) . . . . ? C1 Cr1 P21 Cr2 -161.3(3) . . . . ? C4 Cr1 P21 Cr2 177.6(10) . . . . ? C5 Cr1 P21 Cr2 -135.9(3) . . . . ? P51 Cr1 P21 Cr2 -27.0(4) . . . . ? P32 Cr1 P21 Cr2 48.3(3) . . . . ? P5 Cr1 P21 Cr2 -38.3(3) . . . . ? P4 Cr1 P21 Cr2 14.4(4) . . . . ? P11 Cr1 P21 Cr2 -64.0(5) . . . . ? P41 Cr1 P21 Cr2 26.2(5) . . . . ? P11 P21 P31 P41 -2.2(11) . . . . ? Cr2 P21 P31 P41 -46.7(7) . . . . ? Cr1 P21 P31 P41 45.9(7) . . . . ? P11 P21 P31 Cr2 44.5(7) . . . . ? Cr1 P21 P31 Cr2 92.6(4) . . . . ? P11 P21 P31 Cr1 -48.1(7) . . . . ? Cr2 P21 P31 Cr1 -92.6(4) . . . . ? C2 Cr1 P31 P21 -96.3(5) . . . . ? C3 Cr1 P31 P21 -134.9(5) . . . . ? C1 Cr1 P31 P21 -70.3(6) . . . . ? C4 Cr1 P31 P21 -160.6(5) . . . . ? C5 Cr1 P31 P21 -114.1(12) . . . . ? P51 Cr1 P31 P21 90.5(6) . . . . ? P32 Cr1 P31 P21 145.2(12) . . . . ? P5 Cr1 P31 P21 78.4(6) . . . . ? P4 Cr1 P31 P21 123.2(6) . . . . ? P11 Cr1 P31 P21 37.6(6) . . . . ? P41 Cr1 P31 P21 129.8(8) . . . . ? C2 Cr1 P31 P41 133.9(5) . . . . ? C3 Cr1 P31 P41 95.3(5) . . . . ? C1 Cr1 P31 P41 159.9(5) . . . . ? C4 Cr1 P31 P41 69.6(7) . . . . ? C5 Cr1 P31 P41 116.1(12) . . . . ? P51 Cr1 P31 P41 -39.4(5) . . . . ? P32 Cr1 P31 P41 15.4(9) . . . . ? P5 Cr1 P31 P41 -51.5(5) . . . . ? P21 Cr1 P31 P41 -129.8(8) . . . . ? P4 Cr1 P31 P41 -6.6(6) . . . . ? P11 Cr1 P31 P41 -92.2(6) . . . . ? C2 Cr1 P31 Cr2 -161.5(3) . . . . ? C3 Cr1 P31 Cr2 159.9(2) . . . . ? C1 Cr1 P31 Cr2 -135.6(3) . . . . ? C4 Cr1 P31 Cr2 134.1(2) . . . . ? C5 Cr1 P31 Cr2 -179.4(9) . . . . ? P51 Cr1 P31 Cr2 25.2(4) . . . . ? P32 Cr1 P31 Cr2 79.9(10) . . . . ? P5 Cr1 P31 Cr2 13.1(3) . . . . ? P21 Cr1 P31 Cr2 -65.3(5) . . . . ? P4 Cr1 P31 Cr2 58.0(3) . . . . ? P11 Cr1 P31 Cr2 -27.6(4) . . . . ? P41 Cr1 P31 Cr2 64.5(5) . . . . ? P21 P31 P41 P51 0.9(10) . . . . ? Cr2 P31 P41 P51 -46.1(6) . . . . ? Cr1 P31 P41 P51 47.2(6) . . . . ? P21 P31 P41 Cr2 47.1(7) . . . . ? Cr1 P31 P41 Cr2 93.3(4) . . . . ? P21 P31 P41 Cr1 -46.3(7) . . . . ? Cr2 P31 P41 Cr1 -93.3(4) . . . . ? C2 Cr1 P41 P51 161.2(4) . . . . ? C3 Cr1 P41 P51 135.7(4) . . . . ? C1 Cr1 P41 P51 116.2(12) . . . . ? C4 Cr1 P41 P51 97.1(5) . . . . ? C5 Cr1 P41 P51 72.0(6) . . . . ? P32 Cr1 P41 P51 -143.8(11) . . . . ? P5 Cr1 P41 P51 -6.7(5) . . . . ? P21 Cr1 P41 P51 -90.4(5) . . . . ? P4 Cr1 P41 P51 24(2) . . . . ? P11 Cr1 P41 P51 -39.0(6) . . . . ? C2 Cr1 P41 P31 -71.1(6) . . . . ? C3 Cr1 P41 P31 -96.6(5) . . . . ? C1 Cr1 P41 P31 -116.1(11) . . . . ? C4 Cr1 P41 P31 -135.2(4) . . . . ? C5 Cr1 P41 P31 -160.3(4) . . . . ? P51 Cr1 P41 P31 127.7(7) . . . . ? P32 Cr1 P41 P31 -16.1(8) . . . . ? P5 Cr1 P41 P31 121.0(5) . . . . ? P21 Cr1 P41 P31 37.3(5) . . . . ? P4 Cr1 P41 P31 152(2) . . . . ? P11 Cr1 P41 P31 88.7(6) . . . . ? C2 Cr1 P41 Cr2 -134.6(3) . . . . ? C3 Cr1 P41 Cr2 -160.1(3) . . . . ? C1 Cr1 P41 Cr2 -179.6(9) . . . . ? C4 Cr1 P41 Cr2 161.3(2) . . . . ? C5 Cr1 P41 Cr2 136.2(2) . . . . ? P51 Cr1 P41 Cr2 64.2(5) . . . . ? P32 Cr1 P41 Cr2 -79.6(8) . . . . ? P5 Cr1 P41 Cr2 57.5(3) . . . . ? P21 Cr1 P41 Cr2 -26.1(4) . . . . ? P4 Cr1 P41 Cr2 89(2) . . . . ? P11 Cr1 P41 Cr2 25.2(5) . . . . ? P21 P11 P51 P41 -2.0(11) . . . . ? Cr2 P11 P51 P41 45.8(6) . . . . ? Cr1 P11 P51 P41 -48.2(6) . . . . ? P21 P11 P51 Cr2 -47.8(7) . . . . ? Cr1 P11 P51 Cr2 -94.0(4) . . . . ? P21 P11 P51 Cr1 46.1(7) . . . . ? Cr2 P11 P51 Cr1 94.0(4) . . . . ? P31 P41 P51 P11 0.7(10) . . . . ? Cr2 P41 P51 P11 -45.1(6) . . . . ? Cr1 P41 P51 P11 48.3(6) . . . . ? P31 P41 P51 Cr2 45.8(6) . . . . ? Cr1 P41 P51 Cr2 93.4(4) . . . . ? P31 P41 P51 Cr1 -47.6(6) . . . . ? Cr2 P41 P51 Cr1 -93.4(4) . . . . ? C2 Cr1 P51 P11 117.5(11) . . . . ? C3 Cr1 P51 P11 163.2(5) . . . . ? C1 Cr1 P51 P11 72.4(6) . . . . ? C4 Cr1 P51 P11 137.4(5) . . . . ? C5 Cr1 P51 P11 98.6(5) . . . . ? P32 Cr1 P51 P11 -111.8(5) . . . . ? P5 Cr1 P51 P11 24.2(18) . . . . ? P21 Cr1 P51 P11 -36.1(6) . . . . ? P4 Cr1 P51 P11 -135.8(7) . . . . ? P41 Cr1 P51 P11 -127.9(7) . . . . ? C2 Cr1 P51 P41 -114.7(10) . . . . ? C3 Cr1 P51 P41 -68.9(6) . . . . ? C1 Cr1 P51 P41 -159.8(4) . . . . ? C4 Cr1 P51 P41 -94.8(4) . . . . ? C5 Cr1 P51 P41 -133.5(4) . . . . ? P32 Cr1 P51 P41 16.1(4) . . . . ? P5 Cr1 P51 P41 152(2) . . . . ? P21 Cr1 P51 P41 91.7(6) . . . . ? P4 Cr1 P51 P41 -7.9(6) . . . . ? P11 Cr1 P51 P41 127.9(7) . . . . ? C2 Cr1 P51 Cr2 -179(35) . . . . ? C3 Cr1 P51 Cr2 -133.6(3) . . . . ? C1 Cr1 P51 Cr2 135.6(2) . . . . ? C4 Cr1 P51 Cr2 -159.5(2) . . . . ? C5 Cr1 P51 Cr2 161.78(19) . . . . ? P32 Cr1 P51 Cr2 -48.6(2) . . . . ? P5 Cr1 P51 Cr2 87(2) . . . . ? P21 Cr1 P51 Cr2 27.1(5) . . . . ? P4 Cr1 P51 Cr2 -72.6(4) . . . . ? P11 Cr1 P51 Cr2 63.2(5) . . . . ? P41 Cr1 P51 Cr2 -64.7(4) . . . . ? C2 Cr1 P1 P2 73.4(3) . . . . ? C3 Cr1 P1 P2 83.6(7) . . . . ? C1 Cr1 P1 P2 104.7(3) . . . . ? C4 Cr1 P1 P2 160.8(3) . . . . ? C5 Cr1 P1 P2 142.1(2) . . . . ? P51 Cr1 P1 P2 -122.0(4) . . . . ? P32 Cr1 P1 P2 -51.8(3) . . . . ? P5 Cr1 P1 P2 -129.8(3) . . . . ? P21 Cr1 P1 P2 5.1(9) . . . . ? P4 Cr1 P1 P2 -91.6(3) . . . . ? P11 Cr1 P1 P2 -140(2) . . . . ? P41 Cr1 P1 P2 -79.1(4) . . . . ? C2 Cr1 P1 P5 -156.83(19) . . . . ? C3 Cr1 P1 P5 -146.6(5) . . . . ? C1 Cr1 P1 P5 -125.5(2) . . . . ? C4 Cr1 P1 P5 -69.5(3) . . . . ? C5 Cr1 P1 P5 -88.1(2) . . . . ? P51 Cr1 P1 P5 7.8(4) . . . . ? P32 Cr1 P1 P5 78.0(3) . . . . ? P21 Cr1 P1 P5 134.9(8) . . . . ? P4 Cr1 P1 P5 38.2(2) . . . . ? P11 Cr1 P1 P5 -11(2) . . . . ? P41 Cr1 P1 P5 50.6(4) . . . . ? C2 Cr1 P1 Cr2 138.79(13) . . . . ? C3 Cr1 P1 Cr2 149.0(5) . . . . ? C1 Cr1 P1 Cr2 170.10(16) . . . . ? C4 Cr1 P1 Cr2 -133.8(2) . . . . ? C5 Cr1 P1 Cr2 -152.49(15) . . . . ? P51 Cr1 P1 Cr2 -56.6(3) . . . . ? P32 Cr1 P1 Cr2 13.6(3) . . . . ? P5 Cr1 P1 Cr2 -64.39(18) . . . . ? P21 Cr1 P1 Cr2 70.5(7) . . . . ? P4 Cr1 P1 Cr2 -26.2(2) . . . . ? P11 Cr1 P1 Cr2 -75(2) . . . . ? P41 Cr1 P1 Cr2 -13.7(3) . . . . ? P5 P1 P2 P3 -0.2(5) . . . . ? Cr1 P1 P2 P3 45.7(3) . . . . ? Cr2 P1 P2 P3 -45.8(3) . . . . ? P5 P1 P2 Cr1 -45.8(3) . . . . ? Cr2 P1 P2 Cr1 -91.43(18) . . . . ? P5 P1 P2 Cr2 45.6(3) . . . . ? Cr1 P1 P2 Cr2 91.43(18) . . . . ? C2 Cr1 P2 P1 -125.3(2) . . . . ? C3 Cr1 P2 P1 -156.0(2) . . . . ? C1 Cr1 P2 P1 -87.6(2) . . . . ? C4 Cr1 P2 P1 -144.4(5) . . . . ? C5 Cr1 P2 P1 -69.7(3) . . . . ? P51 Cr1 P2 P1 50.8(3) . . . . ? P32 Cr1 P2 P1 122.3(3) . . . . ? P5 Cr1 P2 P1 38.4(2) . . . . ? P21 Cr1 P2 P1 -15(2) . . . . ? P4 Cr1 P2 P1 92.6(3) . . . . ? P11 Cr1 P2 P1 9.2(4) . . . . ? P41 Cr1 P2 P1 103.0(4) . . . . ? C2 Cr1 P2 P3 103.9(2) . . . . ? C3 Cr1 P2 P3 73.3(3) . . . . ? C1 Cr1 P2 P3 141.7(2) . . . . ? C4 Cr1 P2 P3 84.9(6) . . . . ? C5 Cr1 P2 P3 159.5(3) . . . . ? P51 Cr1 P2 P3 -79.9(3) . . . . ? P32 Cr1 P2 P3 -8.5(3) . . . . ? P5 Cr1 P2 P3 -92.3(3) . . . . ? P21 Cr1 P2 P3 -146(3) . . . . ? P4 Cr1 P2 P3 -38.1(3) . . . . ? P11 Cr1 P2 P3 -121.6(4) . . . . ? P41 Cr1 P2 P3 -27.7(4) . . . . ? C2 Cr1 P2 Cr2 168.87(15) . . . . ? C3 Cr1 P2 Cr2 138.23(14) . . . . ? C1 Cr1 P2 Cr2 -153.36(14) . . . . ? C4 Cr1 P2 Cr2 149.8(4) . . . . ? C5 Cr1 P2 Cr2 -135.5(2) . . . . ? P51 Cr1 P2 Cr2 -15.0(3) . . . . ? P32 Cr1 P2 Cr2 56.5(3) . . . . ? P5 Cr1 P2 Cr2 -27.4(2) . . . . ? P21 Cr1 P2 Cr2 -81(3) . . . . ? P4 Cr1 P2 Cr2 26.8(2) . . . . ? P11 Cr1 P2 Cr2 -56.6(3) . . . . ? P41 Cr1 P2 Cr2 37.2(4) . . . . ? P1 P2 P3 P4 -0.4(5) . . . . ? Cr1 P2 P3 P4 45.4(3) . . . . ? Cr2 P2 P3 P4 -46.6(3) . . . . ? P1 P2 P3 Cr2 46.2(3) . . . . ? Cr1 P2 P3 Cr2 92.00(16) . . . . ? P1 P2 P3 Cr1 -45.8(3) . . . . ? Cr2 P2 P3 Cr1 -92.00(16) . . . . ? C2 Cr1 P3 P2 -87.8(2) . . . . ? C3 Cr1 P3 P2 -125.5(2) . . . . ? C1 Cr1 P3 P2 -69.5(3) . . . . ? C4 Cr1 P3 P2 -155.9(2) . . . . ? C5 Cr1 P3 P2 -141.6(5) . . . . ? P51 Cr1 P3 P2 101.9(4) . . . . ? P32 Cr1 P3 P2 149.4(9) . . . . ? P5 Cr1 P3 P2 91.1(3) . . . . ? P21 Cr1 P3 P2 8.2(5) . . . . ? P4 Cr1 P3 P2 130.5(3) . . . . ? P11 Cr1 P3 P2 49.8(4) . . . . ? P41 Cr1 P3 P2 135.8(6) . . . . ? C2 Cr1 P3 P4 141.7(3) . . . . ? C3 Cr1 P3 P4 104.1(3) . . . . ? C1 Cr1 P3 P4 160.0(3) . . . . ? C4 Cr1 P3 P4 73.6(3) . . . . ? C5 Cr1 P3 P4 87.9(6) . . . . ? P51 Cr1 P3 P4 -28.6(4) . . . . ? P32 Cr1 P3 P4 18.9(8) . . . . ? P5 Cr1 P3 P4 -39.3(3) . . . . ? P21 Cr1 P3 P4 -122.3(5) . . . . ? P11 Cr1 P3 P4 -80.7(4) . . . . ? P41 Cr1 P3 P4 5.3(7) . . . . ? C2 Cr1 P3 Cr2 -153.15(15) . . . . ? C3 Cr1 P3 Cr2 169.20(15) . . . . ? C1 Cr1 P3 Cr2 -134.8(2) . . . . ? C4 Cr1 P3 Cr2 138.78(13) . . . . ? C5 Cr1 P3 Cr2 153.1(4) . . . . ? P51 Cr1 P3 Cr2 36.5(3) . . . . ? P32 Cr1 P3 Cr2 84.0(8) . . . . ? P5 Cr1 P3 Cr2 25.8(2) . . . . ? P21 Cr1 P3 Cr2 -57.2(4) . . . . ? P4 Cr1 P3 Cr2 65.1(3) . . . . ? P11 Cr1 P3 Cr2 -15.6(3) . . . . ? P41 Cr1 P3 Cr2 70.5(6) . . . . ? P2 P3 P4 P5 0.8(4) . . . . ? Cr2 P3 P4 P5 -45.8(3) . . . . ? Cr1 P3 P4 P5 46.6(3) . . . . ? P2 P3 P4 Cr1 -45.8(3) . . . . ? Cr2 P3 P4 Cr1 -92.44(18) . . . . ? P2 P3 P4 Cr2 46.7(3) . . . . ? Cr1 P3 P4 Cr2 92.44(18) . . . . ? C2 Cr1 P4 P5 162.0(3) . . . . ? C3 Cr1 P4 P5 143.6(2) . . . . ? C1 Cr1 P4 P5 89.5(6) . . . . ? C4 Cr1 P4 P5 106.0(2) . . . . ? C5 Cr1 P4 P5 76.0(3) . . . . ? P51 Cr1 P4 P5 5.5(6) . . . . ? P32 Cr1 P4 P5 -136.4(4) . . . . ? P21 Cr1 P4 P5 -78.5(4) . . . . ? P11 Cr1 P4 P5 -28.4(4) . . . . ? P41 Cr1 P4 P5 -145(2) . . . . ? C2 Cr1 P4 P3 -69.3(3) . . . . ? C3 Cr1 P4 P3 -87.7(2) . . . . ? C1 Cr1 P4 P3 -141.8(5) . . . . ? C4 Cr1 P4 P3 -125.3(2) . . . . ? C5 Cr1 P4 P3 -155.34(19) . . . . ? P51 Cr1 P4 P3 134.1(6) . . . . ? P32 Cr1 P4 P3 -7.7(3) . . . . ? P5 Cr1 P4 P3 128.7(3) . . . . ? P21 Cr1 P4 P3 50.2(4) . . . . ? P11 Cr1 P4 P3 100.2(4) . . . . ? P41 Cr1 P4 P3 -16(2) . . . . ? C2 Cr1 P4 Cr2 -133.73(19) . . . . ? C3 Cr1 P4 Cr2 -152.10(14) . . . . ? C1 Cr1 P4 Cr2 153.8(5) . . . . ? C4 Cr1 P4 Cr2 170.26(15) . . . . ? C5 Cr1 P4 Cr2 140.26(13) . . . . ? P51 Cr1 P4 Cr2 69.7(5) . . . . ? P32 Cr1 P4 Cr2 -72.1(3) . . . . ? P5 Cr1 P4 Cr2 64.3(2) . . . . ? P21 Cr1 P4 Cr2 -14.2(3) . . . . ? P11 Cr1 P4 Cr2 35.8(4) . . . . ? P41 Cr1 P4 Cr2 -81(2) . . . . ? P2 P1 P5 P4 0.7(5) . . . . ? Cr1 P1 P5 P4 -45.6(3) . . . . ? Cr2 P1 P5 P4 46.8(3) . . . . ? P2 P1 P5 Cr1 46.3(3) . . . . ? Cr2 P1 P5 Cr1 92.32(18) . . . . ? P2 P1 P5 Cr2 -46.1(3) . . . . ? Cr1 P1 P5 Cr2 -92.32(18) . . . . ? P3 P4 P5 P1 -0.9(4) . . . . ? Cr1 P4 P5 P1 45.8(3) . . . . ? Cr2 P4 P5 P1 -46.8(3) . . . . ? P3 P4 P5 Cr1 -46.8(3) . . . . ? Cr2 P4 P5 Cr1 -92.63(18) . . . . ? P3 P4 P5 Cr2 45.9(3) . . . . ? Cr1 P4 P5 Cr2 92.63(18) . . . . ? C2 Cr1 P5 P1 85.8(6) . . . . ? C3 Cr1 P5 P1 162.1(3) . . . . ? C1 Cr1 P5 P1 74.3(3) . . . . ? C4 Cr1 P5 P1 143.2(2) . . . . ? C5 Cr1 P5 P1 105.3(3) . . . . ? P51 Cr1 P5 P1 -147(2) . . . . ? P32 Cr1 P5 P1 -104.2(3) . . . . ? P21 Cr1 P5 P1 -27.4(5) . . . . ? P4 Cr1 P5 P1 -130.4(3) . . . . ? P11 Cr1 P5 P1 3.5(7) . . . . ? P41 Cr1 P5 P1 -122.3(4) . . . . ? C2 Cr1 P5 P4 -143.7(5) . . . . ? C3 Cr1 P5 P4 -67.5(3) . . . . ? C1 Cr1 P5 P4 -155.3(2) . . . . ? C4 Cr1 P5 P4 -86.3(2) . . . . ? C5 Cr1 P5 P4 -124.3(2) . . . . ? P51 Cr1 P5 P4 -16.3(19) . . . . ? P32 Cr1 P5 P4 26.2(2) . . . . ? P21 Cr1 P5 P4 103.1(5) . . . . ? P11 Cr1 P5 P4 134.0(6) . . . . ? P41 Cr1 P5 P4 8.2(4) . . . . ? C2 Cr1 P5 Cr2 151.1(5) . . . . ? C3 Cr1 P5 Cr2 -132.6(2) . . . . ? C1 Cr1 P5 Cr2 139.61(14) . . . . ? C4 Cr1 P5 Cr2 -151.48(14) . . . . ? C5 Cr1 P5 Cr2 170.61(15) . . . . ? P51 Cr1 P5 Cr2 -81.5(19) . . . . ? P32 Cr1 P5 Cr2 -38.9(2) . . . . ? P21 Cr1 P5 Cr2 37.9(5) . . . . ? P4 Cr1 P5 Cr2 -65.1(2) . . . . ? P11 Cr1 P5 Cr2 68.8(6) . . . . ? P41 Cr1 P5 Cr2 -57.0(3) . . . . ? C2 Cr1 P12 P52 -149.8(3) . . . . ? C3 Cr1 P12 P52 -156.9(4) . . . . ? C1 Cr1 P12 P52 -114.8(3) . . . . ? C4 Cr1 P12 P52 -74.7(5) . . . . ? C5 Cr1 P12 P52 -80.6(3) . . . . ? P51 Cr1 P12 P52 17.6(4) . . . . ? P32 Cr1 P12 P52 92.1(4) . . . . ? P5 Cr1 P12 P52 9.1(2) . . . . ? P21 Cr1 P12 P52 138.4(12) . . . . ? P4 Cr1 P12 P52 52.4(4) . . . . ? P11 Cr1 P12 P52 -5.7(10) . . . . ? P41 Cr1 P12 P52 65.4(5) . . . . ? C2 Cr1 P12 P22 80.4(4) . . . . ? C3 Cr1 P12 P22 73.3(7) . . . . ? C1 Cr1 P12 P22 115.5(3) . . . . ? C4 Cr1 P12 P22 155.5(4) . . . . ? C5 Cr1 P12 P22 149.6(3) . . . . ? P51 Cr1 P12 P22 -112.2(4) . . . . ? P32 Cr1 P12 P22 -37.7(4) . . . . ? P5 Cr1 P12 P22 -120.7(4) . . . . ? P21 Cr1 P12 P22 8.7(12) . . . . ? P4 Cr1 P12 P22 -77.4(4) . . . . ? P11 Cr1 P12 P22 -135.5(12) . . . . ? P41 Cr1 P12 P22 -64.3(5) . . . . ? C2 Cr1 P12 Cr2 145.02(14) . . . . ? C3 Cr1 P12 Cr2 137.9(4) . . . . ? C1 Cr1 P12 Cr2 -179.94(19) . . . . ? C4 Cr1 P12 Cr2 -139.9(3) . . . . ? C5 Cr1 P12 Cr2 -145.77(17) . . . . ? P51 Cr1 P12 Cr2 -47.6(3) . . . . ? P32 Cr1 P12 Cr2 26.9(3) . . . . ? P5 Cr1 P12 Cr2 -56.06(18) . . . . ? P21 Cr1 P12 Cr2 73.2(11) . . . . ? P4 Cr1 P12 Cr2 -12.8(3) . . . . ? P11 Cr1 P12 Cr2 -70.9(10) . . . . ? P41 Cr1 P12 Cr2 0.3(4) . . . . ? P52 P12 P22 P32 -2.1(7) . . . . ? Cr1 P12 P22 P32 44.4(4) . . . . ? Cr2 P12 P22 P32 -46.3(4) . . . . ? P52 P12 P22 Cr1 -46.5(4) . . . . ? Cr2 P12 P22 Cr1 -90.7(2) . . . . ? P52 P12 P22 Cr2 44.2(4) . . . . ? Cr1 P12 P22 Cr2 90.7(2) . . . . ? C2 Cr1 P22 P32 115.0(3) . . . . ? C3 Cr1 P22 P32 80.1(4) . . . . ? C1 Cr1 P22 P32 149.7(3) . . . . ? C4 Cr1 P22 P32 72.5(6) . . . . ? C5 Cr1 P22 P32 155.6(4) . . . . ? P51 Cr1 P22 P32 -65.0(4) . . . . ? P5 Cr1 P22 P32 -78.2(3) . . . . ? P21 Cr1 P22 P32 -140.0(14) . . . . ? P4 Cr1 P22 P32 -25.3(3) . . . . ? P11 Cr1 P22 P32 -112.2(4) . . . . ? P41 Cr1 P22 P32 -16.7(5) . . . . ? C2 Cr1 P22 P12 -113.6(3) . . . . ? C3 Cr1 P22 P12 -148.5(3) . . . . ? C1 Cr1 P22 P12 -78.9(3) . . . . ? C4 Cr1 P22 P12 -156.1(4) . . . . ? C5 Cr1 P22 P12 -73.0(5) . . . . ? P51 Cr1 P22 P12 66.4(4) . . . . ? P32 Cr1 P22 P12 131.4(5) . . . . ? P5 Cr1 P22 P12 53.2(4) . . . . ? P21 Cr1 P22 P12 -8.6(12) . . . . ? P4 Cr1 P22 P12 106.1(4) . . . . ? P11 Cr1 P22 P12 19.2(5) . . . . ? P41 Cr1 P22 P12 114.7(5) . . . . ? C2 Cr1 P22 Cr2 179.36(18) . . . . ? C3 Cr1 P22 Cr2 144.51(15) . . . . ? C1 Cr1 P22 Cr2 -145.87(16) . . . . ? C4 Cr1 P22 Cr2 136.9(4) . . . . ? C5 Cr1 P22 Cr2 -140.0(3) . . . . ? P51 Cr1 P22 Cr2 -0.7(3) . . . . ? P32 Cr1 P22 Cr2 64.4(3) . . . . ? P5 Cr1 P22 Cr2 -13.8(2) . . . . ? P21 Cr1 P22 Cr2 -75.6(12) . . . . ? P4 Cr1 P22 Cr2 39.0(2) . . . . ? P11 Cr1 P22 Cr2 -47.8(3) . . . . ? P41 Cr1 P22 Cr2 47.7(4) . . . . ? P12 P22 P32 P42 1.3(6) . . . . ? Cr1 P22 P32 P42 46.3(4) . . . . ? Cr2 P22 P32 P42 -46.2(4) . . . . ? P12 P22 P32 Cr1 -44.9(4) . . . . ? Cr2 P22 P32 Cr1 -92.5(2) . . . . ? P12 P22 P32 Cr2 47.6(4) . . . . ? Cr1 P22 P32 Cr2 92.5(2) . . . . ? C2 Cr1 P32 P22 -79.7(3) . . . . ? C3 Cr1 P32 P22 -114.3(3) . . . . ? C1 Cr1 P32 P22 -73.4(5) . . . . ? C4 Cr1 P32 P22 -149.3(3) . . . . ? C5 Cr1 P32 P22 -156.1(4) . . . . ? P51 Cr1 P32 P22 113.0(4) . . . . ? P5 Cr1 P32 P22 104.0(3) . . . . ? P21 Cr1 P32 P22 17.7(5) . . . . ? P4 Cr1 P32 P22 138.0(5) . . . . ? P11 Cr1 P32 P22 64.6(4) . . . . ? P41 Cr1 P32 P22 142.1(10) . . . . ? C2 Cr1 P32 P42 150.8(3) . . . . ? C3 Cr1 P32 P42 116.1(3) . . . . ? C1 Cr1 P32 P42 157.0(4) . . . . ? C4 Cr1 P32 P42 81.1(3) . . . . ? C5 Cr1 P32 P42 74.3(6) . . . . ? P51 Cr1 P32 P42 -16.6(4) . . . . ? P5 Cr1 P32 P42 -25.6(3) . . . . ? P21 Cr1 P32 P42 -111.8(5) . . . . ? P4 Cr1 P32 P42 8.5(3) . . . . ? P11 Cr1 P32 P42 -65.0(4) . . . . ? P41 Cr1 P32 P42 12.6(10) . . . . ? C2 Cr1 P32 Cr2 -144.88(17) . . . . ? C3 Cr1 P32 Cr2 -179.5(2) . . . . ? C1 Cr1 P32 Cr2 -138.7(3) . . . . ? C4 Cr1 P32 Cr2 145.44(15) . . . . ? C5 Cr1 P32 Cr2 138.7(3) . . . . ? P51 Cr1 P32 Cr2 47.8(4) . . . . ? P5 Cr1 P32 Cr2 38.7(2) . . . . ? P21 Cr1 P32 Cr2 -47.5(4) . . . . ? P4 Cr1 P32 Cr2 72.8(4) . . . . ? P11 Cr1 P32 Cr2 -0.6(4) . . . . ? P41 Cr1 P32 Cr2 76.9(9) . . . . ? P22 P32 P42 P52 -0.1(6) . . . . ? Cr1 P32 P42 P52 46.3(4) . . . . ? Cr2 P32 P42 P52 -46.7(4) . . . . ? P22 P32 P42 Cr1 -46.4(4) . . . . ? Cr2 P32 P42 Cr1 -93.0(2) . . . . ? P22 P32 P42 Cr2 46.6(4) . . . . ? Cr1 P32 P42 Cr2 93.0(2) . . . . ? C2 Cr1 P42 P32 -73.0(5) . . . . ? C3 Cr1 P42 P32 -79.2(3) . . . . ? C1 Cr1 P42 P32 -157.7(4) . . . . ? C4 Cr1 P42 P32 -113.7(3) . . . . ? C5 Cr1 P42 P32 -148.8(2) . . . . ? P51 Cr1 P42 P32 141.0(10) . . . . ? P5 Cr1 P42 P32 136.7(4) . . . . ? P21 Cr1 P42 P32 66.2(4) . . . . ? P4 Cr1 P42 P32 -19.7(7) . . . . ? P11 Cr1 P42 P32 111.8(5) . . . . ? P41 Cr1 P42 P32 -11.9(9) . . . . ? C2 Cr1 P42 P52 157.0(4) . . . . ? C3 Cr1 P42 P52 150.9(3) . . . . ? C1 Cr1 P42 P52 72.3(6) . . . . ? C4 Cr1 P42 P52 116.3(3) . . . . ? C5 Cr1 P42 P52 81.2(3) . . . . ? P51 Cr1 P42 P52 11.0(10) . . . . ? P32 Cr1 P42 P52 -130.0(4) . . . . ? P5 Cr1 P42 P52 6.7(3) . . . . ? P21 Cr1 P42 P52 -63.8(5) . . . . ? P4 Cr1 P42 P52 -149.7(9) . . . . ? P11 Cr1 P42 P52 -18.2(5) . . . . ? P41 Cr1 P42 P52 -141.8(11) . . . . ? C2 Cr1 P42 Cr2 -137.3(3) . . . . ? C3 Cr1 P42 Cr2 -143.47(17) . . . . ? C1 Cr1 P42 Cr2 138.0(3) . . . . ? C4 Cr1 P42 Cr2 -178.0(2) . . . . ? C5 Cr1 P42 Cr2 146.86(16) . . . . ? P51 Cr1 P42 Cr2 76.7(9) . . . . ? P32 Cr1 P42 Cr2 -64.3(3) . . . . ? P5 Cr1 P42 Cr2 72.4(3) . . . . ? P21 Cr1 P42 Cr2 1.9(4) . . . . ? P4 Cr1 P42 Cr2 -84.0(8) . . . . ? P11 Cr1 P42 Cr2 47.5(4) . . . . ? P41 Cr1 P42 Cr2 -76.2(9) . . . . ? P22 P12 P52 P42 2.1(7) . . . . ? Cr1 P12 P52 P42 -43.8(4) . . . . ? Cr2 P12 P52 P42 46.0(4) . . . . ? P22 P12 P52 Cr2 -44.0(4) . . . . ? Cr1 P12 P52 Cr2 -89.8(2) . . . . ? P22 P12 P52 Cr1 45.9(4) . . . . ? Cr2 P12 P52 Cr1 89.8(2) . . . . ? P32 P42 P52 P12 -1.2(6) . . . . ? Cr1 P42 P52 P12 44.1(4) . . . . ? Cr2 P42 P52 P12 -47.3(4) . . . . ? P32 P42 P52 Cr2 46.1(4) . . . . ? Cr1 P42 P52 Cr2 91.5(2) . . . . ? P32 P42 P52 Cr1 -45.4(4) . . . . ? Cr2 P42 P52 Cr1 -91.5(2) . . . . ? C2 Cr1 P52 P12 69.8(6) . . . . ? C3 Cr1 P52 P12 154.8(5) . . . . ? C1 Cr1 P52 P12 79.1(4) . . . . ? C4 Cr1 P52 P12 149.1(4) . . . . ? C5 Cr1 P52 P12 114.4(4) . . . . ? P51 Cr1 P52 P12 -141.9(11) . . . . ? P32 Cr1 P52 P12 -92.9(4) . . . . ? P5 Cr1 P52 P12 -147.5(9) . . . . ? P21 Cr1 P52 P12 -18.2(6) . . . . ? P4 Cr1 P52 P12 -123.1(4) . . . . ? P11 Cr1 P52 P12 5.8(10) . . . . ? P41 Cr1 P52 P12 -114.1(5) . . . . ? C2 Cr1 P52 P42 -158.3(4) . . . . ? C3 Cr1 P52 P42 -73.4(5) . . . . ? C1 Cr1 P52 P42 -149.1(3) . . . . ? C4 Cr1 P52 P42 -79.0(3) . . . . ? C5 Cr1 P52 P42 -113.8(3) . . . . ? P51 Cr1 P52 P42 -10.1(9) . . . . ? P32 Cr1 P52 P42 38.9(3) . . . . ? P5 Cr1 P52 P42 -15.7(6) . . . . ? P21 Cr1 P52 P42 113.6(5) . . . . ? P4 Cr1 P52 P42 8.7(2) . . . . ? P11 Cr1 P52 P42 137.7(9) . . . . ? P41 Cr1 P52 P42 17.7(5) . . . . ? C2 Cr1 P52 Cr2 137.1(3) . . . . ? C3 Cr1 P52 Cr2 -137.9(3) . . . . ? C1 Cr1 P52 Cr2 146.35(15) . . . . ? C4 Cr1 P52 Cr2 -143.58(16) . . . . ? C5 Cr1 P52 Cr2 -178.34(19) . . . . ? P51 Cr1 P52 Cr2 -74.6(9) . . . . ? P32 Cr1 P52 Cr2 -25.7(3) . . . . ? P5 Cr1 P52 Cr2 -80.2(7) . . . . ? P21 Cr1 P52 Cr2 49.0(5) . . . . ? P4 Cr1 P52 Cr2 -55.81(19) . . . . ? P11 Cr1 P52 Cr2 73.1(9) . . . . ? P41 Cr1 P52 Cr2 -46.8(3) . . . . ? P21 P11 Cr2 C15 -140.7(5) . . . . ? P51 P11 Cr2 C15 89.9(5) . . . . ? Cr1 P11 Cr2 C15 153.7(2) . . . . ? P21 P11 Cr2 C11 -102.7(6) . . . . ? P51 P11 Cr2 C11 127.9(4) . . . . ? Cr1 P11 Cr2 C11 -168.2(2) . . . . ? P21 P11 Cr2 C13 -94.4(12) . . . . ? P51 P11 Cr2 C13 136.2(10) . . . . ? Cr1 P11 Cr2 C13 -160.0(8) . . . . ? P21 P11 Cr2 C14 -161.2(6) . . . . ? P51 P11 Cr2 C14 69.4(7) . . . . ? Cr1 P11 Cr2 C14 133.3(3) . . . . ? P21 P11 Cr2 C12 -73.7(6) . . . . ? P51 P11 Cr2 C12 156.9(4) . . . . ? Cr1 P11 Cr2 C12 -139.2(2) . . . . ? P21 P11 Cr2 P31 36.8(6) . . . . ? P51 P11 Cr2 P31 -92.6(6) . . . . ? Cr1 P11 Cr2 P31 -28.7(4) . . . . ? P21 P11 Cr2 P51 129.4(8) . . . . ? Cr1 P11 Cr2 P51 63.9(5) . . . . ? P51 P11 Cr2 P21 -129.4(8) . . . . ? Cr1 P11 Cr2 P21 -65.5(6) . . . . ? P21 P11 Cr2 P41 91.5(6) . . . . ? P51 P11 Cr2 P41 -37.9(5) . . . . ? Cr1 P11 Cr2 P41 26.0(5) . . . . ? P21 P11 Cr2 P5 136.3(8) . . . . ? P51 P11 Cr2 P5 6.9(6) . . . . ? Cr1 P11 Cr2 P5 70.8(5) . . . . ? P21 P11 Cr2 P3 49.5(6) . . . . ? P51 P11 Cr2 P3 -79.9(5) . . . . ? Cr1 P11 Cr2 P3 -16.0(4) . . . . ? P21 P31 Cr2 C15 135.8(11) . . . . ? P41 P31 Cr2 C15 -95.1(12) . . . . ? Cr1 P31 Cr2 C15 -159.2(9) . . . . ? P21 P31 Cr2 C11 70.4(7) . . . . ? P41 P31 Cr2 C11 -160.5(6) . . . . ? Cr1 P31 Cr2 C11 135.4(3) . . . . ? P21 P31 Cr2 C13 129.7(5) . . . . ? P41 P31 Cr2 C13 -101.2(6) . . . . ? Cr1 P31 Cr2 C13 -165.3(2) . . . . ? P21 P31 Cr2 C14 158.2(5) . . . . ? P41 P31 Cr2 C14 -72.7(6) . . . . ? Cr1 P31 Cr2 C14 -136.8(2) . . . . ? P21 P31 Cr2 C12 91.5(5) . . . . ? P41 P31 Cr2 C12 -139.4(5) . . . . ? Cr1 P31 Cr2 C12 156.5(2) . . . . ? P21 P31 Cr2 P11 -36.4(6) . . . . ? P41 P31 Cr2 P11 92.7(6) . . . . ? Cr1 P31 Cr2 P11 28.6(4) . . . . ? P21 P31 Cr2 P51 -90.3(6) . . . . ? P41 P31 Cr2 P51 38.8(6) . . . . ? Cr1 P31 Cr2 P51 -25.3(4) . . . . ? P41 P31 Cr2 P21 129.1(8) . . . . ? Cr1 P31 Cr2 P21 65.0(5) . . . . ? P21 P31 Cr2 P41 -129.1(8) . . . . ? Cr1 P31 Cr2 P41 -64.1(6) . . . . ? P21 P31 Cr2 P5 -78.1(5) . . . . ? P41 P31 Cr2 P5 51.0(6) . . . . ? Cr1 P31 Cr2 P5 -13.1(4) . . . . ? P21 P31 Cr2 P3 -147(2) . . . . ? P41 P31 Cr2 P3 -18.2(19) . . . . ? Cr1 P31 Cr2 P3 -82(2) . . . . ? P11 P51 Cr2 C15 -102.0(5) . . . . ? P41 P51 Cr2 C15 127.7(5) . . . . ? Cr1 P51 Cr2 C15 -167.2(2) . . . . ? P11 P51 Cr2 C11 -73.3(6) . . . . ? P41 P51 Cr2 C11 156.4(5) . . . . ? Cr1 P51 Cr2 C11 -138.5(2) . . . . ? P11 P51 Cr2 C13 -160.9(5) . . . . ? P41 P51 Cr2 C13 68.8(7) . . . . ? Cr1 P51 Cr2 C13 133.9(3) . . . . ? P11 P51 Cr2 C14 -140.1(5) . . . . ? P41 P51 Cr2 C14 89.5(6) . . . . ? Cr1 P51 Cr2 C14 154.7(2) . . . . ? P11 P51 Cr2 C12 -94.6(11) . . . . ? P41 P51 Cr2 C12 135.1(10) . . . . ? Cr1 P51 Cr2 C12 -159.8(8) . . . . ? P41 P51 Cr2 P11 -130.3(7) . . . . ? Cr1 P51 Cr2 P11 -65.2(5) . . . . ? P11 P51 Cr2 P31 90.9(6) . . . . ? P41 P51 Cr2 P31 -39.4(6) . . . . ? Cr1 P51 Cr2 P31 25.7(4) . . . . ? P11 P51 Cr2 P21 37.8(6) . . . . ? P41 P51 Cr2 P21 -92.5(6) . . . . ? Cr1 P51 Cr2 P21 -27.4(4) . . . . ? P11 P51 Cr2 P41 130.3(7) . . . . ? Cr1 P51 Cr2 P41 65.1(5) . . . . ? P11 P51 Cr2 P5 -21(2) . . . . ? P41 P51 Cr2 P5 -151(2) . . . . ? Cr1 P51 Cr2 P5 -86(2) . . . . ? P11 P51 Cr2 P3 102.2(5) . . . . ? P41 P51 Cr2 P3 -28.1(5) . . . . ? Cr1 P51 Cr2 P3 37.0(2) . . . . ? P11 P21 Cr2 C15 67.3(7) . . . . ? P31 P21 Cr2 C15 -161.2(5) . . . . ? Cr1 P21 Cr2 C15 133.0(4) . . . . ? P11 P21 Cr2 C11 89.4(5) . . . . ? P31 P21 Cr2 C11 -139.0(5) . . . . ? Cr1 P21 Cr2 C11 155.2(2) . . . . ? P11 P21 Cr2 C13 156.9(5) . . . . ? P31 P21 Cr2 C13 -71.6(6) . . . . ? Cr1 P21 Cr2 C13 -137.4(2) . . . . ? P11 P21 Cr2 C14 134.7(11) . . . . ? P31 P21 Cr2 C14 -93.8(13) . . . . ? Cr1 P21 Cr2 C14 -159.5(10) . . . . ? P11 P21 Cr2 C12 127.5(5) . . . . ? P31 P21 Cr2 C12 -100.9(5) . . . . ? Cr1 P21 Cr2 C12 -166.7(3) . . . . ? P31 P21 Cr2 P11 131.6(8) . . . . ? Cr1 P21 Cr2 P11 65.8(5) . . . . ? P11 P21 Cr2 P31 -131.6(8) . . . . ? Cr1 P21 Cr2 P31 -65.8(5) . . . . ? P11 P21 Cr2 P51 -38.6(6) . . . . ? P31 P21 Cr2 P51 92.9(6) . . . . ? Cr1 P21 Cr2 P51 27.1(4) . . . . ? P11 P21 Cr2 P41 -92.2(6) . . . . ? P31 P21 Cr2 P41 39.3(6) . . . . ? Cr1 P21 Cr2 P41 -26.5(5) . . . . ? P11 P21 Cr2 P5 -27.5(5) . . . . ? P31 P21 Cr2 P5 104.0(5) . . . . ? Cr1 P21 Cr2 P5 38.2(3) . . . . ? P11 P21 Cr2 P3 -123.6(6) . . . . ? P31 P21 Cr2 P3 8.0(6) . . . . ? Cr1 P21 Cr2 P3 -57.8(3) . . . . ? P51 P41 Cr2 C15 -72.9(6) . . . . ? P31 P41 Cr2 C15 158.1(5) . . . . ? Cr1 P41 Cr2 C15 -137.0(3) . . . . ? P51 P41 Cr2 C11 -94.3(12) . . . . ? P31 P41 Cr2 C11 136.7(10) . . . . ? Cr1 P41 Cr2 C11 -158.4(9) . . . . ? P51 P41 Cr2 C13 -140.0(5) . . . . ? P31 P41 Cr2 C13 91.0(5) . . . . ? Cr1 P41 Cr2 C13 155.9(2) . . . . ? P51 P41 Cr2 C14 -102.2(5) . . . . ? P31 P41 Cr2 C14 128.7(5) . . . . ? Cr1 P41 Cr2 C14 -166.3(3) . . . . ? P51 P41 Cr2 C12 -160.2(5) . . . . ? P31 P41 Cr2 C12 70.8(7) . . . . ? Cr1 P41 Cr2 C12 135.7(4) . . . . ? P51 P41 Cr2 P11 38.1(6) . . . . ? P31 P41 Cr2 P11 -90.9(6) . . . . ? Cr1 P41 Cr2 P11 -26.0(4) . . . . ? P51 P41 Cr2 P31 129.0(8) . . . . ? Cr1 P41 Cr2 P31 64.9(5) . . . . ? P31 P41 Cr2 P51 -129.0(8) . . . . ? Cr1 P41 Cr2 P51 -64.1(5) . . . . ? P51 P41 Cr2 P21 90.6(6) . . . . ? P31 P41 Cr2 P21 -38.4(6) . . . . ? Cr1 P41 Cr2 P21 26.5(4) . . . . ? P51 P41 Cr2 P5 6.9(6) . . . . ? P31 P41 Cr2 P5 -122.1(6) . . . . ? Cr1 P41 Cr2 P5 -57.2(3) . . . . ? P51 P41 Cr2 P3 135.3(8) . . . . ? P31 P41 Cr2 P3 6.2(6) . . . . ? Cr1 P41 Cr2 P3 71.1(5) . . . . ? P1 P5 Cr2 C15 -111.7(2) . . . . ? P4 P5 Cr2 C15 118.9(2) . . . . ? Cr1 P5 Cr2 C15 -176.68(16) . . . . ? P1 P5 Cr2 C11 -78.6(3) . . . . ? P4 P5 Cr2 C11 152.0(2) . . . . ? Cr1 P5 Cr2 C11 -143.58(13) . . . . ? P1 P5 Cr2 C13 -159.9(3) . . . . ? P4 P5 Cr2 C13 70.6(4) . . . . ? Cr1 P5 Cr2 C13 135.1(2) . . . . ? P1 P5 Cr2 C14 -147.8(2) . . . . ? P4 P5 Cr2 C14 82.8(2) . . . . ? Cr1 P5 Cr2 C14 147.24(14) . . . . ? P1 P5 Cr2 C12 -77.9(5) . . . . ? P4 P5 Cr2 C12 152.7(4) . . . . ? Cr1 P5 Cr2 C12 -142.8(3) . . . . ? P1 P5 Cr2 P11 -6.7(7) . . . . ? P4 P5 Cr2 P11 -136.1(6) . . . . ? Cr1 P5 Cr2 P11 -71.7(6) . . . . ? P1 P5 Cr2 P31 78.2(4) . . . . ? P4 P5 Cr2 P31 -51.2(4) . . . . ? Cr1 P5 Cr2 P31 13.3(4) . . . . ? P1 P5 Cr2 P51 148(2) . . . . ? P4 P5 Cr2 P51 18(2) . . . . ? Cr1 P5 Cr2 P51 83(2) . . . . ? P1 P5 Cr2 P21 26.6(4) . . . . ? P4 P5 Cr2 P21 -102.9(4) . . . . ? Cr1 P5 Cr2 P21 -38.4(4) . . . . ? P1 P5 Cr2 P41 122.5(5) . . . . ? P4 P5 Cr2 P41 -6.9(6) . . . . ? Cr1 P5 Cr2 P41 57.5(4) . . . . ? P1 P5 Cr2 P3 90.8(3) . . . . ? P4 P5 Cr2 P3 -38.6(2) . . . . ? Cr1 P5 Cr2 P3 25.8(2) . . . . ? P2 P3 Cr2 C15 155.3(3) . . . . ? P4 P3 Cr2 C15 -75.2(5) . . . . ? Cr1 P3 Cr2 C15 -139.6(3) . . . . ? P2 P3 Cr2 C11 71.3(3) . . . . ? P4 P3 Cr2 C11 -159.2(3) . . . . ? Cr1 P3 Cr2 C11 136.5(2) . . . . ? P2 P3 Cr2 C13 120.1(2) . . . . ? P4 P3 Cr2 C13 -110.3(3) . . . . ? Cr1 P3 Cr2 C13 -174.71(15) . . . . ? P2 P3 Cr2 C14 153.3(2) . . . . ? P4 P3 Cr2 C14 -77.1(3) . . . . ? Cr1 P3 Cr2 C14 -141.54(13) . . . . ? P2 P3 Cr2 C12 83.9(2) . . . . ? P4 P3 Cr2 C12 -146.6(2) . . . . ? Cr1 P3 Cr2 C12 149.05(14) . . . . ? P2 P3 Cr2 P11 -49.1(4) . . . . ? P4 P3 Cr2 P11 80.5(4) . . . . ? Cr1 P3 Cr2 P11 16.1(4) . . . . ? P2 P3 Cr2 P31 21(2) . . . . ? P4 P3 Cr2 P31 151(2) . . . . ? Cr1 P3 Cr2 P31 86(2) . . . . ? P2 P3 Cr2 P51 -101.8(4) . . . . ? P4 P3 Cr2 P51 27.7(4) . . . . ? Cr1 P3 Cr2 P51 -36.7(4) . . . . ? P2 P3 Cr2 P21 -7.3(5) . . . . ? P4 P3 Cr2 P21 122.3(5) . . . . ? Cr1 P3 Cr2 P21 57.9(4) . . . . ? P2 P3 Cr2 P41 -136.4(7) . . . . ? P4 P3 Cr2 P41 -6.8(8) . . . . ? Cr1 P3 Cr2 P41 -71.2(7) . . . . ? P2 P3 Cr2 P5 -90.9(3) . . . . ? P4 P3 Cr2 P5 38.6(3) . . . . ? Cr1 P3 Cr2 P5 -25.8(2) . . . . ? C15 Cr2 C11 C12 -117.9(3) . . . . ? C13 Cr2 C11 C12 -37.5(2) . . . . ? C14 Cr2 C11 C12 -79.8(2) . . . . ? P11 Cr2 C11 C12 139.6(4) . . . . ? P31 Cr2 C11 C12 34.9(6) . . . . ? P51 Cr2 C11 C12 -169.0(5) . . . . ? P21 Cr2 C11 C12 86.3(4) . . . . ? P41 Cr2 C11 C12 -88.7(12) . . . . ? P5 Cr2 C11 C12 179.5(3) . . . . ? P3 Cr2 C11 C12 19.5(4) . . . . ? C13 Cr2 C11 C15 80.4(2) . . . . ? C14 Cr2 C11 C15 38.1(2) . . . . ? C12 Cr2 C11 C15 117.9(3) . . . . ? P11 Cr2 C11 C15 -102.5(4) . . . . ? P31 Cr2 C11 C15 152.8(5) . . . . ? P51 Cr2 C11 C15 -51.0(5) . . . . ? P21 Cr2 C11 C15 -155.8(4) . . . . ? P41 Cr2 C11 C15 29.2(12) . . . . ? P5 Cr2 C11 C15 -62.6(3) . . . . ? P3 Cr2 C11 C15 137.4(3) . . . . ? C15 Cr2 C11 C16 122.3(4) . . . . ? C13 Cr2 C11 C16 -157.3(4) . . . . ? C14 Cr2 C11 C16 160.4(4) . . . . ? C12 Cr2 C11 C16 -119.8(4) . . . . ? P11 Cr2 C11 C16 19.8(5) . . . . ? P31 Cr2 C11 C16 -84.8(6) . . . . ? P51 Cr2 C11 C16 71.3(5) . . . . ? P21 Cr2 C11 C16 -33.5(5) . . . . ? P41 Cr2 C11 C16 151.6(12) . . . . ? P5 Cr2 C11 C16 59.7(4) . . . . ? P3 Cr2 C11 C16 -100.3(4) . . . . ? C15 C11 C12 C13 0.0(4) . . . . ? C16 C11 C12 C13 -176.9(3) . . . . ? Cr2 C11 C12 C13 61.8(2) . . . . ? C15 C11 C12 C17 176.7(3) . . . . ? C16 C11 C12 C17 -0.1(6) . . . . ? Cr2 C11 C12 C17 -121.5(4) . . . . ? C15 C11 C12 Cr2 -61.8(2) . . . . ? C16 C11 C12 Cr2 121.3(4) . . . . ? C15 Cr2 C12 C11 37.3(2) . . . . ? C13 Cr2 C12 C11 117.6(3) . . . . ? C14 Cr2 C12 C11 80.0(2) . . . . ? P11 Cr2 C12 C11 -51.9(5) . . . . ? P31 Cr2 C12 C11 -156.6(4) . . . . ? P51 Cr2 C12 C11 29.1(11) . . . . ? P21 Cr2 C12 C11 -102.4(4) . . . . ? P41 Cr2 C12 C11 150.7(6) . . . . ? P5 Cr2 C12 C11 -1.1(5) . . . . ? P3 Cr2 C12 C11 -168.9(2) . . . . ? C15 Cr2 C12 C13 -80.3(2) . . . . ? C11 Cr2 C12 C13 -117.6(3) . . . . ? C14 Cr2 C12 C13 -37.5(2) . . . . ? P11 Cr2 C12 C13 -169.5(5) . . . . ? P31 Cr2 C12 C13 85.8(4) . . . . ? P51 Cr2 C12 C13 -88.4(10) . . . . ? P21 Cr2 C12 C13 140.0(4) . . . . ? P41 Cr2 C12 C13 33.1(6) . . . . ? P5 Cr2 C12 C13 -118.7(5) . . . . ? P3 Cr2 C12 C13 73.5(3) . . . . ? C15 Cr2 C12 C17 158.8(4) . . . . ? C11 Cr2 C12 C17 121.4(5) . . . . ? C13 Cr2 C12 C17 -121.0(5) . . . . ? C14 Cr2 C12 C17 -158.5(4) . . . . ? P11 Cr2 C12 C17 69.6(6) . . . . ? P31 Cr2 C12 C17 -35.2(5) . . . . ? P51 Cr2 C12 C17 150.6(10) . . . . ? P21 Cr2 C12 C17 19.0(5) . . . . ? P41 Cr2 C12 C17 -87.9(7) . . . . ? P5 Cr2 C12 C17 120.4(5) . . . . ? P3 Cr2 C12 C17 -47.5(4) . . . . ? C11 C12 C13 C14 0.5(4) . . . . ? C17 C12 C13 C14 -176.3(3) . . . . ? Cr2 C12 C13 C14 62.3(2) . . . . ? C11 C12 C13 C18 175.5(3) . . . . ? C17 C12 C13 C18 -1.3(6) . . . . ? Cr2 C12 C13 C18 -122.7(4) . . . . ? C11 C12 C13 Cr2 -61.8(2) . . . . ? C17 C12 C13 Cr2 121.4(4) . . . . ? C15 Cr2 C13 C14 -37.3(2) . . . . ? C11 Cr2 C13 C14 -79.8(2) . . . . ? C12 Cr2 C13 C14 -117.1(3) . . . . ? P11 Cr2 C13 C14 -88.9(11) . . . . ? P31 Cr2 C13 C14 140.6(4) . . . . ? P51 Cr2 C13 C14 34.3(5) . . . . ? P21 Cr2 C13 C14 -169.2(5) . . . . ? P41 Cr2 C13 C14 85.0(4) . . . . ? P5 Cr2 C13 C14 18.9(4) . . . . ? P3 Cr2 C13 C14 127.1(3) . . . . ? C15 Cr2 C13 C12 79.8(2) . . . . ? C11 Cr2 C13 C12 37.3(2) . . . . ? C14 Cr2 C13 C12 117.1(3) . . . . ? P11 Cr2 C13 C12 28.2(12) . . . . ? P31 Cr2 C13 C12 -102.3(4) . . . . ? P51 Cr2 C13 C12 151.4(4) . . . . ? P21 Cr2 C13 C12 -52.2(5) . . . . ? P41 Cr2 C13 C12 -157.9(4) . . . . ? P5 Cr2 C13 C12 136.0(3) . . . . ? P3 Cr2 C13 C12 -115.8(3) . . . . ? C15 Cr2 C13 C18 -157.5(4) . . . . ? C11 Cr2 C13 C18 160.0(4) . . . . ? C14 Cr2 C13 C18 -120.2(5) . . . . ? C12 Cr2 C13 C18 122.7(5) . . . . ? P11 Cr2 C13 C18 150.9(11) . . . . ? P31 Cr2 C13 C18 20.4(5) . . . . ? P51 Cr2 C13 C18 -85.9(6) . . . . ? P21 Cr2 C13 C18 70.5(6) . . . . ? P41 Cr2 C13 C18 -35.2(5) . . . . ? P5 Cr2 C13 C18 -101.3(5) . . . . ? P3 Cr2 C13 C18 6.9(4) . . . . ? C12 C13 C14 C15 -0.8(4) . . . . ? C18 C13 C14 C15 -175.9(3) . . . . ? Cr2 C13 C14 C15 61.5(2) . . . . ? C12 C13 C14 C19 177.5(3) . . . . ? C18 C13 C14 C19 2.4(6) . . . . ? Cr2 C13 C14 C19 -120.2(4) . . . . ? C12 C13 C14 Cr2 -62.3(2) . . . . ? C18 C13 C14 Cr2 122.6(4) . . . . ? C15 Cr2 C14 C13 118.2(3) . . . . ? C11 Cr2 C14 C13 80.2(2) . . . . ? C12 Cr2 C14 C13 37.8(2) . . . . ? P11 Cr2 C14 C13 151.6(5) . . . . ? P31 Cr2 C14 C13 -50.8(5) . . . . ? P51 Cr2 C14 C13 -157.1(3) . . . . ? P21 Cr2 C14 C13 29.8(13) . . . . ? P41 Cr2 C14 C13 -102.7(4) . . . . ? P5 Cr2 C14 C13 -169.2(2) . . . . ? P3 Cr2 C14 C13 -63.2(3) . . . . ? C11 Cr2 C14 C15 -37.94(18) . . . . ? C13 Cr2 C14 C15 -118.2(3) . . . . ? C12 Cr2 C14 C15 -80.3(2) . . . . ? P11 Cr2 C14 C15 33.4(6) . . . . ? P31 Cr2 C14 C15 -169.0(5) . . . . ? P51 Cr2 C14 C15 84.8(3) . . . . ? P21 Cr2 C14 C15 -88.3(13) . . . . ? P41 Cr2 C14 C15 139.2(4) . . . . ? P5 Cr2 C14 C15 72.7(2) . . . . ? P3 Cr2 C14 C15 178.7(2) . . . . ? C15 Cr2 C14 C19 -120.1(4) . . . . ? C11 Cr2 C14 C19 -158.1(4) . . . . ? C13 Cr2 C14 C19 121.7(4) . . . . ? C12 Cr2 C14 C19 159.5(4) . . . . ? P11 Cr2 C14 C19 -86.7(6) . . . . ? P31 Cr2 C14 C19 70.9(6) . . . . ? P51 Cr2 C14 C19 -35.3(4) . . . . ? P21 Cr2 C14 C19 151.6(13) . . . . ? P41 Cr2 C14 C19 19.0(5) . . . . ? P5 Cr2 C14 C19 -47.5(4) . . . . ? P3 Cr2 C14 C19 58.5(4) . . . . ? C12 C11 C15 C14 -0.4(4) . . . . ? C16 C11 C15 C14 176.3(3) . . . . ? Cr2 C11 C15 C14 -62.5(2) . . . . ? C12 C11 C15 C20 -177.2(3) . . . . ? C16 C11 C15 C20 -0.4(6) . . . . ? Cr2 C11 C15 C20 120.8(3) . . . . ? C12 C11 C15 Cr2 62.0(2) . . . . ? C16 C11 C15 Cr2 -121.2(4) . . . . ? C13 C14 C15 C11 0.8(4) . . . . ? C19 C14 C15 C11 -177.5(3) . . . . ? Cr2 C14 C15 C11 62.5(2) . . . . ? C13 C14 C15 C20 177.5(3) . . . . ? C19 C14 C15 C20 -0.8(6) . . . . ? Cr2 C14 C15 C20 -120.8(3) . . . . ? C13 C14 C15 Cr2 -61.7(2) . . . . ? C19 C14 C15 Cr2 120.0(3) . . . . ? C13 Cr2 C15 C11 -79.6(2) . . . . ? C14 Cr2 C15 C11 -116.6(3) . . . . ? C12 Cr2 C15 C11 -37.1(2) . . . . ? P11 Cr2 C15 C11 85.6(4) . . . . ? P31 Cr2 C15 C11 -86.4(12) . . . . ? P51 Cr2 C15 C11 140.2(3) . . . . ? P21 Cr2 C15 C11 36.5(6) . . . . ? P41 Cr2 C15 C11 -168.8(5) . . . . ? P5 Cr2 C15 C11 127.3(3) . . . . ? P3 Cr2 C15 C11 -119.4(4) . . . . ? C11 Cr2 C15 C14 116.6(3) . . . . ? C13 Cr2 C15 C14 36.9(2) . . . . ? C12 Cr2 C15 C14 79.4(2) . . . . ? P11 Cr2 C15 C14 -157.9(4) . . . . ? P31 Cr2 C15 C14 30.1(12) . . . . ? P51 Cr2 C15 C14 -103.2(3) . . . . ? P21 Cr2 C15 C14 153.1(6) . . . . ? P41 Cr2 C15 C14 -52.2(5) . . . . ? P5 Cr2 C15 C14 -116.1(2) . . . . ? P3 Cr2 C15 C14 -2.9(5) . . . . ? C11 Cr2 C15 C20 -121.8(4) . . . . ? C13 Cr2 C15 C20 158.5(4) . . . . ? C14 Cr2 C15 C20 121.6(4) . . . . ? C12 Cr2 C15 C20 -159.0(4) . . . . ? P11 Cr2 C15 C20 -36.3(5) . . . . ? P31 Cr2 C15 C20 151.8(11) . . . . ? P51 Cr2 C15 C20 18.4(4) . . . . ? P21 Cr2 C15 C20 -85.3(6) . . . . ? P41 Cr2 C15 C20 69.4(6) . . . . ? P5 Cr2 C15 C20 5.5(4) . . . . ? P3 Cr2 C15 C20 118.7(5) . . . . ? C25 C21 C22 C23 -0.4(4) . . . . ? C26 C21 C22 C23 175.2(3) . . . . ? Cr3 C21 C22 C23 -61.9(2) . . . . ? C25 C21 C22 C27 -175.5(3) . . . . ? C26 C21 C22 C27 0.1(6) . . . . ? Cr3 C21 C22 C27 123.0(4) . . . . ? C25 C21 C22 Cr3 61.5(2) . . . . ? C26 C21 C22 Cr3 -122.9(4) . . . . ? C21 C22 C23 C24 -0.3(4) . . . . ? C27 C22 C23 C24 174.8(3) . . . . ? Cr3 C22 C23 C24 -62.6(2) . . . . ? C21 C22 C23 C28 -176.3(4) . . . . ? C27 C22 C23 C28 -1.2(6) . . . . ? Cr3 C22 C23 C28 121.4(4) . . . . ? C21 C22 C23 Cr3 62.3(2) . . . . ? C27 C22 C23 Cr3 -122.7(4) . . . . ? C22 C23 C24 C25 0.9(4) . . . . ? C28 C23 C24 C25 176.9(4) . . . . ? Cr3 C23 C24 C25 -61.2(2) . . . . ? C22 C23 C24 C29 -177.5(3) . . . . ? C28 C23 C24 C29 -1.6(6) . . . . ? Cr3 C23 C24 C29 120.3(4) . . . . ? C22 C23 C24 Cr3 62.2(3) . . . . ? C28 C23 C24 Cr3 -121.9(4) . . . . ? C22 C21 C25 C24 1.0(4) . . . . ? C26 C21 C25 C24 -174.6(3) . . . . ? Cr3 C21 C25 C24 62.6(2) . . . . ? C22 C21 C25 C30 176.8(3) . . . . ? C26 C21 C25 C30 1.1(6) . . . . ? Cr3 C21 C25 C30 -121.7(4) . . . . ? C22 C21 C25 Cr3 -61.5(2) . . . . ? C26 C21 C25 Cr3 122.8(4) . . . . ? C23 C24 C25 C21 -1.2(4) . . . . ? C29 C24 C25 C21 177.2(3) . . . . ? Cr3 C24 C25 C21 -62.5(2) . . . . ? C23 C24 C25 C30 -176.9(4) . . . . ? C29 C24 C25 C30 1.5(6) . . . . ? Cr3 C24 C25 C30 121.7(4) . . . . ? C23 C24 C25 Cr3 61.3(2) . . . . ? C29 C24 C25 Cr3 -120.2(4) . . . . ? C24 C23 Cr3 C25 37.8(2) . . . . ? C22 C23 Cr3 C25 -80.1(2) . . . . ? C28 C23 Cr3 C25 159.7(4) . . . . ? C24 C23 Cr3 C22 117.9(3) . . . . ? C28 C23 Cr3 C22 -120.2(4) . . . . ? C24 C23 Cr3 C21 80.4(2) . . . . ? C22 C23 Cr3 C21 -37.6(2) . . . . ? C28 C23 Cr3 C21 -157.8(4) . . . . ? C22 C23 Cr3 C24 -117.9(3) . . . . ? C28 C23 Cr3 C24 121.9(4) . . . . ? C24 C23 Cr3 P6 122.0(3) . . . . ? C22 C23 Cr3 P6 4.0(4) . . . . ? C28 C23 Cr3 P6 -116.2(3) . . . . ? C24 C23 Cr3 P10 -18.0(3) . . . . ? C22 C23 Cr3 P10 -136.0(2) . . . . ? C28 C23 Cr3 P10 103.8(4) . . . . ? C24 C23 Cr3 P9 -72.6(2) . . . . ? C22 C23 Cr3 P9 169.47(19) . . . . ? C28 C23 Cr3 P9 49.3(4) . . . . ? C24 C23 Cr3 P8 -125.6(2) . . . . ? C22 C23 Cr3 P8 116.5(2) . . . . ? C28 C23 Cr3 P8 -3.7(4) . . . . ? C24 C23 Cr3 P7 -177.14(17) . . . . ? C22 C23 Cr3 P7 64.9(2) . . . . ? C28 C23 Cr3 P7 -55.3(4) . . . . ? C21 C25 Cr3 C23 80.1(2) . . . . ? C24 C25 Cr3 C23 -37.37(19) . . . . ? C30 C25 Cr3 C23 -159.3(4) . . . . ? C21 C25 Cr3 C22 37.6(2) . . . . ? C24 C25 Cr3 C22 -79.8(2) . . . . ? C30 C25 Cr3 C22 158.2(4) . . . . ? C24 C25 Cr3 C21 -117.5(3) . . . . ? C30 C25 Cr3 C21 120.6(4) . . . . ? C21 C25 Cr3 C24 117.5(3) . . . . ? C30 C25 Cr3 C24 -121.9(4) . . . . ? C21 C25 Cr3 P6 -73.0(2) . . . . ? C24 C25 Cr3 P6 169.53(17) . . . . ? C30 C25 Cr3 P6 47.6(3) . . . . ? C21 C25 Cr3 P10 -126.24(19) . . . . ? C24 C25 Cr3 P10 116.29(18) . . . . ? C30 C25 Cr3 P10 -5.6(3) . . . . ? C21 C25 Cr3 P9 -178.46(17) . . . . ? C24 C25 Cr3 P9 64.1(2) . . . . ? C30 C25 Cr3 P9 -57.8(3) . . . . ? C21 C25 Cr3 P8 121.5(2) . . . . ? C24 C25 Cr3 P8 4.1(3) . . . . ? C30 C25 Cr3 P8 -117.8(3) . . . . ? C21 C25 Cr3 P7 -19.7(3) . . . . ? C24 C25 Cr3 P7 -137.13(19) . . . . ? C30 C25 Cr3 P7 100.9(3) . . . . ? C21 C22 Cr3 C23 -117.5(3) . . . . ? C27 C22 Cr3 C23 120.6(4) . . . . ? C23 C22 Cr3 C25 79.9(2) . . . . ? C21 C22 Cr3 C25 -37.6(2) . . . . ? C27 C22 Cr3 C25 -159.5(4) . . . . ? C23 C22 Cr3 C21 117.5(3) . . . . ? C27 C22 Cr3 C21 -121.9(4) . . . . ? C23 C22 Cr3 C24 37.1(2) . . . . ? C21 C22 Cr3 C24 -80.4(2) . . . . ? C27 C22 Cr3 C24 157.7(4) . . . . ? C23 C22 Cr3 P6 -178.08(19) . . . . ? C21 C22 Cr3 P6 64.5(2) . . . . ? C27 C22 Cr3 P6 -57.5(4) . . . . ? C23 C22 Cr3 P10 120.1(3) . . . . ? C21 C22 Cr3 P10 2.6(4) . . . . ? C27 C22 Cr3 P10 -119.3(3) . . . . ? C23 C22 Cr3 P9 -18.7(3) . . . . ? C21 C22 Cr3 P9 -136.2(2) . . . . ? C27 C22 Cr3 P9 101.9(4) . . . . ? C23 C22 Cr3 P8 -72.9(2) . . . . ? C21 C22 Cr3 P8 169.66(18) . . . . ? C27 C22 Cr3 P8 47.7(4) . . . . ? C23 C22 Cr3 P7 -126.0(2) . . . . ? C21 C22 Cr3 P7 116.52(19) . . . . ? C27 C22 Cr3 P7 -5.4(3) . . . . ? C25 C21 Cr3 C23 -79.9(2) . . . . ? C22 C21 Cr3 C23 37.5(2) . . . . ? C26 C21 Cr3 C23 159.6(4) . . . . ? C22 C21 Cr3 C25 117.3(3) . . . . ? C26 C21 Cr3 C25 -120.5(4) . . . . ? C25 C21 Cr3 C22 -117.3(3) . . . . ? C26 C21 Cr3 C22 122.2(4) . . . . ? C25 C21 Cr3 C24 -37.7(2) . . . . ? C22 C21 Cr3 C24 79.7(2) . . . . ? C26 C21 Cr3 C24 -158.2(4) . . . . ? C25 C21 Cr3 P6 116.5(2) . . . . ? C22 C21 Cr3 P6 -126.1(2) . . . . ? C26 C21 Cr3 P6 -4.0(3) . . . . ? C25 C21 Cr3 P10 63.9(2) . . . . ? C22 C21 Cr3 P10 -178.74(18) . . . . ? C26 C21 Cr3 P10 -56.6(3) . . . . ? C25 C21 Cr3 P9 3.2(4) . . . . ? C22 C21 Cr3 P9 120.6(2) . . . . ? C26 C21 Cr3 P9 -117.3(3) . . . . ? C25 C21 Cr3 P8 -135.9(2) . . . . ? C22 C21 Cr3 P8 -18.6(3) . . . . ? C26 C21 Cr3 P8 103.6(3) . . . . ? C25 C21 Cr3 P7 169.21(18) . . . . ? C22 C21 Cr3 P7 -73.5(2) . . . . ? C26 C21 Cr3 P7 48.7(3) . . . . ? C25 C24 Cr3 C23 117.3(3) . . . . ? C29 C24 Cr3 C23 -121.0(5) . . . . ? C23 C24 Cr3 C25 -117.3(3) . . . . ? C29 C24 Cr3 C25 121.7(4) . . . . ? C23 C24 Cr3 C22 -37.3(2) . . . . ? C25 C24 Cr3 C22 80.0(2) . . . . ? C29 C24 Cr3 C22 -158.3(4) . . . . ? C23 C24 Cr3 C21 -79.9(2) . . . . ? C25 C24 Cr3 C21 37.43(19) . . . . ? C29 C24 Cr3 C21 159.2(4) . . . . ? C23 C24 Cr3 P6 -136.3(2) . . . . ? C25 C24 Cr3 P6 -19.0(3) . . . . ? C29 C24 Cr3 P6 102.7(4) . . . . ? C23 C24 Cr3 P10 169.81(18) . . . . ? C25 C24 Cr3 P10 -72.90(19) . . . . ? C29 C24 Cr3 P10 48.8(4) . . . . ? C23 C24 Cr3 P9 116.47(19) . . . . ? C25 C24 Cr3 P9 -126.24(18) . . . . ? C29 C24 Cr3 P9 -4.5(4) . . . . ? C23 C24 Cr3 P8 64.7(2) . . . . ? C25 C24 Cr3 P8 -178.05(17) . . . . ? C29 C24 Cr3 P8 -56.3(4) . . . . ? C23 C24 Cr3 P7 6.1(4) . . . . ? C25 C24 Cr3 P7 123.3(3) . . . . ? C29 C24 Cr3 P7 -114.9(3) . . . . ? C23 Cr3 P6 P7 76.0(3) . . . . ? C25 Cr3 P6 P7 148.78(11) . . . . ? C22 Cr3 P6 P7 78.75(11) . . . . ? C21 Cr3 P6 P7 112.63(10) . . . . ? C24 Cr3 P6 P7 161.25(17) . . . . ? P10 Cr3 P6 P7 -129.24(6) . . . . ? P9 Cr3 P6 P7 -90.46(6) . . . . ? P8 Cr3 P6 P7 -37.39(6) . . . . ? C23 Cr3 P6 P10 -154.8(3) . . . . ? C25 Cr3 P6 P10 -81.98(11) . . . . ? C22 Cr3 P6 P10 -152.02(11) . . . . ? C21 Cr3 P6 P10 -118.14(10) . . . . ? C24 Cr3 P6 P10 -69.51(18) . . . . ? P9 Cr3 P6 P10 38.78(6) . . . . ? P8 Cr3 P6 P10 91.85(6) . . . . ? P7 Cr3 P6 P10 129.24(6) . . . . ? C23 Cr3 P6 Cr4 140.7(2) . . . . ? C25 Cr3 P6 Cr4 -146.45(10) . . . . ? C22 Cr3 P6 Cr4 143.52(11) . . . . ? C21 Cr3 P6 Cr4 177.40(9) . . . . ? C24 Cr3 P6 Cr4 -133.98(17) . . . . ? P10 Cr3 P6 Cr4 -64.47(5) . . . . ? P9 Cr3 P6 Cr4 -25.69(6) . . . . ? P8 Cr3 P6 Cr4 27.38(6) . . . . ? P7 Cr3 P6 Cr4 64.77(5) . . . . ? P10 P6 P7 P8 -1.05(9) . . . . ? Cr3 P6 P7 P8 45.71(5) . . . . ? Cr4 P6 P7 P8 -47.24(5) . . . . ? P10 P6 P7 Cr4 46.19(5) . . . . ? Cr3 P6 P7 Cr4 92.95(4) . . . . ? P10 P6 P7 Cr3 -46.77(5) . . . . ? Cr4 P6 P7 Cr3 -92.95(4) . . . . ? C23 Cr3 P7 P6 -152.43(11) . . . . ? C25 Cr3 P7 P6 -69.2(2) . . . . ? C22 Cr3 P7 P6 -118.44(11) . . . . ? C21 Cr3 P7 P6 -82.05(11) . . . . ? C24 Cr3 P7 P6 -156.6(2) . . . . ? P10 Cr3 P7 P6 38.53(6) . . . . ? P9 Cr3 P7 P6 92.01(6) . . . . ? P8 Cr3 P7 P6 130.45(6) . . . . ? C23 Cr3 P7 P8 77.12(12) . . . . ? C25 Cr3 P7 P8 160.4(2) . . . . ? C22 Cr3 P7 P8 111.12(11) . . . . ? C21 Cr3 P7 P8 147.50(11) . . . . ? C24 Cr3 P7 P8 73.0(2) . . . . ? P6 Cr3 P7 P8 -130.45(6) . . . . ? P10 Cr3 P7 P8 -91.92(6) . . . . ? P9 Cr3 P7 P8 -38.43(6) . . . . ? C23 Cr3 P7 Cr4 142.47(11) . . . . ? C25 Cr3 P7 Cr4 -134.29(19) . . . . ? C22 Cr3 P7 Cr4 176.46(11) . . . . ? C21 Cr3 P7 Cr4 -147.16(10) . . . . ? C24 Cr3 P7 Cr4 138.3(2) . . . . ? P6 Cr3 P7 Cr4 -65.11(5) . . . . ? P10 Cr3 P7 Cr4 -26.58(6) . . . . ? P9 Cr3 P7 Cr4 26.91(6) . . . . ? P8 Cr3 P7 Cr4 65.34(5) . . . . ? P6 P7 P8 P9 1.41(9) . . . . ? Cr4 P7 P8 P9 -45.72(5) . . . . ? Cr3 P7 P8 P9 46.99(5) . . . . ? P6 P7 P8 Cr3 -45.58(5) . . . . ? Cr4 P7 P8 Cr3 -92.71(4) . . . . ? P6 P7 P8 Cr4 47.14(6) . . . . ? Cr3 P7 P8 Cr4 92.71(4) . . . . ? C23 Cr3 P8 P9 111.37(11) . . . . ? C25 Cr3 P8 P9 74.9(2) . . . . ? C22 Cr3 P8 P9 147.43(11) . . . . ? C21 Cr3 P8 P9 159.55(18) . . . . ? C24 Cr3 P8 P9 77.71(11) . . . . ? P6 Cr3 P8 P9 -91.60(6) . . . . ? P10 Cr3 P8 P9 -38.08(6) . . . . ? P7 Cr3 P8 P9 -128.94(7) . . . . ? C23 Cr3 P8 P7 -119.68(11) . . . . ? C25 Cr3 P8 P7 -156.2(2) . . . . ? C22 Cr3 P8 P7 -83.62(11) . . . . ? C21 Cr3 P8 P7 -71.50(19) . . . . ? C24 Cr3 P8 P7 -153.34(11) . . . . ? P6 Cr3 P8 P7 37.34(6) . . . . ? P10 Cr3 P8 P7 90.86(6) . . . . ? P9 Cr3 P8 P7 128.94(7) . . . . ? C23 Cr3 P8 Cr4 175.69(10) . . . . ? C25 Cr3 P8 Cr4 139.2(2) . . . . ? C22 Cr3 P8 Cr4 -148.25(11) . . . . ? C21 Cr3 P8 Cr4 -136.13(18) . . . . ? C24 Cr3 P8 Cr4 142.03(10) . . . . ? P6 Cr3 P8 Cr4 -27.29(6) . . . . ? P10 Cr3 P8 Cr4 26.24(5) . . . . ? P9 Cr3 P8 Cr4 64.32(5) . . . . ? P7 Cr3 P8 Cr4 -64.63(5) . . . . ? P7 P8 P9 P10 -1.23(9) . . . . ? Cr3 P8 P9 P10 45.97(5) . . . . ? Cr4 P8 P9 P10 -47.09(5) . . . . ? P7 P8 P9 Cr4 45.86(5) . . . . ? Cr3 P8 P9 Cr4 93.06(4) . . . . ? P7 P8 P9 Cr3 -47.20(5) . . . . ? Cr4 P8 P9 Cr3 -93.06(4) . . . . ? C23 Cr3 P9 P8 -82.74(12) . . . . ? C25 Cr3 P9 P8 -152.39(12) . . . . ? C22 Cr3 P9 P8 -70.58(19) . . . . ? C21 Cr3 P9 P8 -154.6(2) . . . . ? C24 Cr3 P9 P8 -118.53(12) . . . . ? P6 Cr3 P9 P8 91.16(6) . . . . ? P10 Cr3 P9 P8 129.94(7) . . . . ? P7 Cr3 P9 P8 38.34(6) . . . . ? C23 Cr3 P9 P10 147.32(12) . . . . ? C25 Cr3 P9 P10 77.67(12) . . . . ? C22 Cr3 P9 P10 159.48(19) . . . . ? C21 Cr3 P9 P10 75.5(2) . . . . ? C24 Cr3 P9 P10 111.53(11) . . . . ? P6 Cr3 P9 P10 -38.78(6) . . . . ? P8 Cr3 P9 P10 -129.94(7) . . . . ? P7 Cr3 P9 P10 -91.60(6) . . . . ? C23 Cr3 P9 Cr4 -148.06(11) . . . . ? C25 Cr3 P9 Cr4 142.29(11) . . . . ? C22 Cr3 P9 Cr4 -135.90(18) . . . . ? C21 Cr3 P9 Cr4 140.1(2) . . . . ? C24 Cr3 P9 Cr4 176.15(11) . . . . ? P6 Cr3 P9 Cr4 25.84(6) . . . . ? P10 Cr3 P9 Cr4 64.62(5) . . . . ? P8 Cr3 P9 Cr4 -65.32(5) . . . . ? P7 Cr3 P9 Cr4 -26.98(6) . . . . ? P7 P6 P10 P9 0.29(9) . . . . ? Cr3 P6 P10 P9 -46.94(5) . . . . ? Cr4 P6 P10 P9 46.59(5) . . . . ? P7 P6 P10 Cr3 47.24(5) . . . . ? Cr4 P6 P10 Cr3 93.54(4) . . . . ? P7 P6 P10 Cr4 -46.30(6) . . . . ? Cr3 P6 P10 Cr4 -93.54(4) . . . . ? P8 P9 P10 P6 0.58(8) . . . . ? Cr4 P9 P10 P6 -46.83(5) . . . . ? Cr3 P9 P10 P6 46.81(5) . . . . ? P8 P9 P10 Cr3 -46.23(5) . . . . ? Cr4 P9 P10 Cr3 -93.64(4) . . . . ? P8 P9 P10 Cr4 47.41(5) . . . . ? Cr3 P9 P10 Cr4 93.64(4) . . . . ? C23 Cr3 P10 P6 160.28(19) . . . . ? C25 Cr3 P10 P6 112.31(11) . . . . ? C22 Cr3 P10 P6 76.9(2) . . . . ? C21 Cr3 P10 P6 78.72(11) . . . . ? C24 Cr3 P10 P6 148.62(11) . . . . ? P9 Cr3 P10 P6 -128.86(7) . . . . ? P8 Cr3 P10 P6 -91.04(6) . . . . ? P7 Cr3 P10 P6 -38.12(6) . . . . ? C23 Cr3 P10 P9 -70.9(2) . . . . ? C25 Cr3 P10 P9 -118.83(11) . . . . ? C22 Cr3 P10 P9 -154.2(2) . . . . ? C21 Cr3 P10 P9 -152.42(11) . . . . ? C24 Cr3 P10 P9 -82.52(11) . . . . ? P6 Cr3 P10 P9 128.86(7) . . . . ? P8 Cr3 P10 P9 37.82(6) . . . . ? P7 Cr3 P10 P9 90.74(6) . . . . ? C23 Cr3 P10 Cr4 -135.05(19) . . . . ? C25 Cr3 P10 Cr4 176.98(10) . . . . ? C22 Cr3 P10 Cr4 141.6(2) . . . . ? C21 Cr3 P10 Cr4 143.39(10) . . . . ? C24 Cr3 P10 Cr4 -146.72(11) . . . . ? P6 Cr3 P10 Cr4 64.67(5) . . . . ? P9 Cr3 P10 Cr4 -64.19(5) . . . . ? P8 Cr3 P10 Cr4 -26.37(6) . . . . ? P7 Cr3 P10 Cr4 26.55(6) . . . . ? P8 P9 Cr4 C31 162.83(16) . . . . ? P10 P9 Cr4 C31 -68.25(16) . . . . ? Cr3 P9 Cr4 C31 -132.42(15) . . . . ? P8 P9 Cr4 C33 75.99(11) . . . . ? P10 P9 Cr4 C33 -155.09(11) . . . . ? Cr3 P9 Cr4 C33 140.74(11) . . . . ? P8 P9 Cr4 C34 108.17(12) . . . . ? P10 P9 Cr4 C34 -122.91(11) . . . . ? Cr3 P9 Cr4 C34 172.92(11) . . . . ? P8 P9 Cr4 C32 81.9(3) . . . . ? P10 P9 Cr4 C32 -149.2(3) . . . . ? Cr3 P9 Cr4 C32 146.6(3) . . . . ? P8 P9 Cr4 C35 145.22(11) . . . . ? P10 P9 Cr4 C35 -85.86(11) . . . . ? Cr3 P9 Cr4 C35 -150.02(11) . . . . ? P8 P9 Cr4 P10 -128.92(6) . . . . ? Cr3 P9 Cr4 P10 -64.17(5) . . . . ? P8 P9 Cr4 P7 -37.61(6) . . . . ? P10 P9 Cr4 P7 91.31(6) . . . . ? Cr3 P9 Cr4 P7 27.15(6) . . . . ? P8 P9 Cr4 P6 -90.41(6) . . . . ? P10 P9 Cr4 P6 38.51(6) . . . . ? Cr3 P9 Cr4 P6 -25.66(6) . . . . ? P10 P9 Cr4 P8 128.92(6) . . . . ? Cr3 P9 Cr4 P8 64.75(5) . . . . ? P6 P10 Cr4 C31 -85.90(11) . . . . ? P9 P10 Cr4 C31 145.09(11) . . . . ? Cr3 P10 Cr4 C31 -150.28(11) . . . . ? P6 P10 Cr4 C33 -147.5(3) . . . . ? P9 P10 Cr4 C33 83.5(3) . . . . ? Cr3 P10 Cr4 C33 148.1(3) . . . . ? P6 P10 Cr4 C34 -154.82(13) . . . . ? P9 P10 Cr4 C34 76.17(12) . . . . ? Cr3 P10 Cr4 C34 140.80(12) . . . . ? P6 P10 Cr4 C32 -68.87(15) . . . . ? P9 P10 Cr4 C32 162.12(15) . . . . ? Cr3 P10 Cr4 C32 -133.24(14) . . . . ? P6 P10 Cr4 C35 -123.39(11) . . . . ? P9 P10 Cr4 C35 107.60(11) . . . . ? Cr3 P10 Cr4 C35 172.23(11) . . . . ? P6 P10 Cr4 P9 129.01(6) . . . . ? Cr3 P10 Cr4 P9 64.63(5) . . . . ? P6 P10 Cr4 P7 37.67(6) . . . . ? P9 P10 Cr4 P7 -91.33(6) . . . . ? Cr3 P10 Cr4 P7 -26.70(6) . . . . ? P9 P10 Cr4 P6 -129.01(6) . . . . ? Cr3 P10 Cr4 P6 -64.38(5) . . . . ? P6 P10 Cr4 P8 90.58(6) . . . . ? P9 P10 Cr4 P8 -38.43(6) . . . . ? Cr3 P10 Cr4 P8 26.20(5) . . . . ? P6 P7 Cr4 C31 74.81(12) . . . . ? P8 P7 Cr4 C31 -156.12(11) . . . . ? Cr3 P7 Cr4 C31 139.20(11) . . . . ? P6 P7 Cr4 C33 144.06(10) . . . . ? P8 P7 Cr4 C33 -86.87(11) . . . . ? Cr3 P7 Cr4 C33 -151.56(10) . . . . ? P6 P7 Cr4 C34 160.52(17) . . . . ? P8 P7 Cr4 C34 -70.41(18) . . . . ? Cr3 P7 Cr4 C34 -135.09(17) . . . . ? P6 P7 Cr4 C32 106.87(10) . . . . ? P8 P7 Cr4 C32 -124.06(10) . . . . ? Cr3 P7 Cr4 C32 171.26(10) . . . . ? P6 P7 Cr4 C35 81.3(3) . . . . ? P8 P7 Cr4 C35 -149.6(3) . . . . ? Cr3 P7 Cr4 C35 145.7(3) . . . . ? P6 P7 Cr4 P9 -91.41(6) . . . . ? P8 P7 Cr4 P9 37.66(6) . . . . ? Cr3 P7 Cr4 P9 -27.02(6) . . . . ? P6 P7 Cr4 P10 -37.92(6) . . . . ? P8 P7 Cr4 P10 91.15(6) . . . . ? Cr3 P7 Cr4 P10 26.47(6) . . . . ? P8 P7 Cr4 P6 129.07(7) . . . . ? Cr3 P7 Cr4 P6 64.39(5) . . . . ? P6 P7 Cr4 P8 -129.07(7) . . . . ? Cr3 P7 Cr4 P8 -64.68(5) . . . . ? P7 P6 Cr4 C31 -123.23(11) . . . . ? P10 P6 Cr4 C31 106.86(11) . . . . ? Cr3 P6 Cr4 C31 171.31(11) . . . . ? P7 P6 Cr4 C33 -69.10(17) . . . . ? P10 P6 Cr4 C33 160.99(16) . . . . ? Cr3 P6 Cr4 C33 -134.56(16) . . . . ? P7 P6 Cr4 C34 -147.9(3) . . . . ? P10 P6 Cr4 C34 82.2(3) . . . . ? Cr3 P6 Cr4 C34 146.6(3) . . . . ? P7 P6 Cr4 C32 -85.87(11) . . . . ? P10 P6 Cr4 C32 144.22(11) . . . . ? Cr3 P6 Cr4 C32 -151.33(10) . . . . ? P7 P6 Cr4 C35 -154.80(12) . . . . ? P10 P6 Cr4 C35 75.29(12) . . . . ? Cr3 P6 Cr4 C35 139.74(11) . . . . ? P7 P6 Cr4 P9 91.24(6) . . . . ? P10 P6 Cr4 P9 -38.67(6) . . . . ? Cr3 P6 Cr4 P9 25.78(6) . . . . ? P7 P6 Cr4 P10 129.91(7) . . . . ? Cr3 P6 Cr4 P10 64.45(5) . . . . ? P10 P6 Cr4 P7 -129.91(7) . . . . ? Cr3 P6 Cr4 P7 -65.46(5) . . . . ? P7 P6 Cr4 P8 38.26(6) . . . . ? P10 P6 Cr4 P8 -91.65(6) . . . . ? Cr3 P6 Cr4 P8 -27.20(6) . . . . ? P9 P8 Cr4 C31 -150.8(3) . . . . ? P7 P8 Cr4 C31 79.1(3) . . . . ? Cr3 P8 Cr4 C31 144.4(3) . . . . ? P9 P8 Cr4 C33 -123.21(10) . . . . ? P7 P8 Cr4 C33 106.68(10) . . . . ? Cr3 P8 Cr4 C33 171.97(9) . . . . ? P9 P8 Cr4 C34 -85.69(11) . . . . ? P7 P8 Cr4 C34 144.20(11) . . . . ? Cr3 P8 Cr4 C34 -150.51(10) . . . . ? P9 P8 Cr4 C32 -155.49(10) . . . . ? P7 P8 Cr4 C32 74.40(11) . . . . ? Cr3 P8 Cr4 C32 139.68(10) . . . . ? P9 P8 Cr4 C35 -68.62(17) . . . . ? P7 P8 Cr4 C35 161.26(17) . . . . ? Cr3 P8 Cr4 C35 -133.45(16) . . . . ? P7 P8 Cr4 P9 -130.11(7) . . . . ? Cr3 P8 Cr4 P9 -64.83(5) . . . . ? P9 P8 Cr4 P10 38.72(6) . . . . ? P7 P8 Cr4 P10 -91.40(6) . . . . ? Cr3 P8 Cr4 P10 -26.11(5) . . . . ? P9 P8 Cr4 P7 130.11(7) . . . . ? Cr3 P8 Cr4 P7 65.28(5) . . . . ? P9 P8 Cr4 P6 91.92(6) . . . . ? P7 P8 Cr4 P6 -38.19(6) . . . . ? Cr3 P8 Cr4 P6 27.09(6) . . . . ? C33 Cr4 C31 C32 -37.41(18) . . . . ? C34 Cr4 C31 C32 -80.1(2) . . . . ? C35 Cr4 C31 C32 -117.1(3) . . . . ? P9 Cr4 C31 C32 -144.90(17) . . . . ? P10 Cr4 C31 C32 163.46(16) . . . . ? P7 Cr4 C31 C32 59.1(2) . . . . ? P6 Cr4 C31 C32 109.84(18) . . . . ? P8 Cr4 C31 C32 -6.6(4) . . . . ? C33 Cr4 C31 C35 79.7(2) . . . . ? C34 Cr4 C31 C35 37.0(2) . . . . ? C32 Cr4 C31 C35 117.1(3) . . . . ? P9 Cr4 C31 C35 -27.8(3) . . . . ? P10 Cr4 C31 C35 -79.5(2) . . . . ? P7 Cr4 C31 C35 176.11(17) . . . . ? P6 Cr4 C31 C35 -133.11(19) . . . . ? P8 Cr4 C31 C35 110.5(3) . . . . ? C33 Cr4 C31 C36 -159.2(4) . . . . ? C34 Cr4 C31 C36 158.2(4) . . . . ? C32 Cr4 C31 C36 -121.8(4) . . . . ? C35 Cr4 C31 C36 121.2(5) . . . . ? P9 Cr4 C31 C36 93.3(4) . . . . ? P10 Cr4 C31 C36 41.7(4) . . . . ? P7 Cr4 C31 C36 -62.7(4) . . . . ? P6 Cr4 C31 C36 -11.9(4) . . . . ? P8 Cr4 C31 C36 -128.3(3) . . . . ? C35 C31 C32 C33 -1.1(4) . . . . ? C36 C31 C32 C33 -177.4(3) . . . . ? Cr4 C31 C32 C33 61.6(2) . . . . ? C35 C31 C32 C37 177.7(3) . . . . ? C36 C31 C32 C37 1.4(6) . . . . ? Cr4 C31 C32 C37 -119.6(3) . . . . ? C35 C31 C32 Cr4 -62.7(2) . . . . ? C36 C31 C32 Cr4 121.0(4) . . . . ? C31 Cr4 C32 C33 -117.6(3) . . . . ? C34 Cr4 C32 C33 -37.7(2) . . . . ? C35 Cr4 C32 C33 -79.8(2) . . . . ? P9 Cr4 C32 C33 -8.2(4) . . . . ? P10 Cr4 C32 C33 -144.61(17) . . . . ? P7 Cr4 C32 C33 110.45(19) . . . . ? P6 Cr4 C32 C33 163.67(17) . . . . ? P8 Cr4 C32 C33 59.7(2) . . . . ? C33 Cr4 C32 C31 117.6(3) . . . . ? C34 Cr4 C32 C31 79.9(2) . . . . ? C35 Cr4 C32 C31 37.8(2) . . . . ? P9 Cr4 C32 C31 109.3(3) . . . . ? P10 Cr4 C32 C31 -27.0(3) . . . . ? P7 Cr4 C32 C31 -131.96(18) . . . . ? P6 Cr4 C32 C31 -78.74(19) . . . . ? P8 Cr4 C32 C31 177.27(17) . . . . ? C31 Cr4 C32 C37 120.8(4) . . . . ? C33 Cr4 C32 C37 -121.6(4) . . . . ? C34 Cr4 C32 C37 -159.2(4) . . . . ? C35 Cr4 C32 C37 158.6(4) . . . . ? P9 Cr4 C32 C37 -129.8(3) . . . . ? P10 Cr4 C32 C37 93.8(3) . . . . ? P7 Cr4 C32 C37 -11.1(3) . . . . ? P6 Cr4 C32 C37 42.1(3) . . . . ? P8 Cr4 C32 C37 -61.9(3) . . . . ? C31 C32 C33 C34 0.6(4) . . . . ? C37 C32 C33 C34 -178.2(3) . . . . ? Cr4 C32 C33 C34 62.0(2) . . . . ? C31 C32 C33 C38 177.2(3) . . . . ? C37 C32 C33 C38 -1.7(6) . . . . ? Cr4 C32 C33 C38 -121.4(4) . . . . ? C31 C32 C33 Cr4 -61.4(2) . . . . ? C37 C32 C33 Cr4 119.7(3) . . . . ? C31 Cr4 C33 C32 37.5(2) . . . . ? C34 Cr4 C33 C32 117.4(3) . . . . ? C35 Cr4 C33 C32 80.1(2) . . . . ? P9 Cr4 C33 C32 176.56(17) . . . . ? P10 Cr4 C33 C32 107.2(3) . . . . ? P7 Cr4 C33 C32 -78.3(2) . . . . ? P6 Cr4 C33 C32 -26.7(3) . . . . ? P8 Cr4 C33 C32 -131.89(19) . . . . ? C31 Cr4 C33 C34 -79.9(2) . . . . ? C32 Cr4 C33 C34 -117.4(3) . . . . ? C35 Cr4 C33 C34 -37.3(2) . . . . ? P9 Cr4 C33 C34 59.2(2) . . . . ? P10 Cr4 C33 C34 -10.2(4) . . . . ? P7 Cr4 C33 C34 164.32(19) . . . . ? P6 Cr4 C33 C34 -144.05(19) . . . . ? P8 Cr4 C33 C34 110.7(2) . . . . ? C31 Cr4 C33 C38 160.0(4) . . . . ? C34 Cr4 C33 C38 -120.1(4) . . . . ? C32 Cr4 C33 C38 122.5(4) . . . . ? C35 Cr4 C33 C38 -157.4(4) . . . . ? P9 Cr4 C33 C38 -61.0(3) . . . . ? P10 Cr4 C33 C38 -130.4(3) . . . . ? P7 Cr4 C33 C38 44.2(3) . . . . ? P6 Cr4 C33 C38 95.8(3) . . . . ? P8 Cr4 C33 C38 -9.4(3) . . . . ? C32 C33 C34 C35 0.2(4) . . . . ? C38 C33 C34 C35 -176.5(3) . . . . ? Cr4 C33 C34 C35 62.3(2) . . . . ? C32 C33 C34 C39 176.0(3) . . . . ? C38 C33 C34 C39 -0.7(6) . . . . ? Cr4 C33 C34 C39 -121.9(4) . . . . ? C32 C33 C34 Cr4 -62.2(2) . . . . ? C38 C33 C34 Cr4 121.2(4) . . . . ? C31 Cr4 C34 C35 -37.4(2) . . . . ? C33 Cr4 C34 C35 -117.5(3) . . . . ? C32 Cr4 C34 C35 -80.0(2) . . . . ? P9 Cr4 C34 C35 110.2(2) . . . . ? P10 Cr4 C34 C35 58.2(2) . . . . ? P7 Cr4 C34 C35 -143.47(19) . . . . ? P6 Cr4 C34 C35 -9.7(4) . . . . ? P8 Cr4 C34 C35 163.75(18) . . . . ? C31 Cr4 C34 C33 80.1(2) . . . . ? C32 Cr4 C34 C33 37.5(2) . . . . ? C35 Cr4 C34 C33 117.5(3) . . . . ? P9 Cr4 C34 C33 -132.29(19) . . . . ? P10 Cr4 C34 C33 175.70(17) . . . . ? P7 Cr4 C34 C33 -26.0(3) . . . . ? P6 Cr4 C34 C33 107.8(3) . . . . ? P8 Cr4 C34 C33 -78.8(2) . . . . ? C31 Cr4 C34 C39 -160.0(4) . . . . ? C33 Cr4 C34 C39 119.9(4) . . . . ? C32 Cr4 C34 C39 157.4(4) . . . . ? C35 Cr4 C34 C39 -122.6(4) . . . . ? P9 Cr4 C34 C39 -12.4(4) . . . . ? P10 Cr4 C34 C39 -64.4(4) . . . . ? P7 Cr4 C34 C39 93.9(4) . . . . ? P6 Cr4 C34 C39 -132.4(3) . . . . ? P8 Cr4 C34 C39 41.1(4) . . . . ? C33 C34 C35 C31 -0.9(4) . . . . ? C39 C34 C35 C31 -176.6(3) . . . . ? Cr4 C34 C35 C31 61.1(2) . . . . ? C33 C34 C35 C40 176.3(3) . . . . ? C39 C34 C35 C40 0.6(6) . . . . ? Cr4 C34 C35 C40 -121.7(4) . . . . ? C33 C34 C35 Cr4 -62.0(2) . . . . ? C39 C34 C35 Cr4 122.3(4) . . . . ? C32 C31 C35 C34 1.2(4) . . . . ? C36 C31 C35 C34 177.6(3) . . . . ? Cr4 C31 C35 C34 -61.4(2) . . . . ? C32 C31 C35 C40 -175.9(3) . . . . ? C36 C31 C35 C40 0.4(6) . . . . ? Cr4 C31 C35 C40 121.5(4) . . . . ? C32 C31 C35 Cr4 62.6(2) . . . . ? C36 C31 C35 Cr4 -121.0(4) . . . . ? C31 Cr4 C35 C34 118.0(3) . . . . ? C33 Cr4 C35 C34 37.7(2) . . . . ? C32 Cr4 C35 C34 80.2(2) . . . . ? P9 Cr4 C35 C34 -78.8(2) . . . . ? P10 Cr4 C35 C34 -132.76(19) . . . . ? P7 Cr4 C35 C34 108.9(3) . . . . ? P6 Cr4 C35 C34 175.84(17) . . . . ? P8 Cr4 C35 C34 -27.1(3) . . . . ? C33 Cr4 C35 C31 -80.3(2) . . . . ? C34 Cr4 C35 C31 -118.0(3) . . . . ? C32 Cr4 C35 C31 -37.8(2) . . . . ? P9 Cr4 C35 C31 163.19(18) . . . . ? P10 Cr4 C35 C31 109.23(19) . . . . ? P7 Cr4 C35 C31 -9.1(4) . . . . ? P6 Cr4 C35 C31 57.8(2) . . . . ? P8 Cr4 C35 C31 -145.08(18) . . . . ? C31 Cr4 C35 C40 -121.7(5) . . . . ? C33 Cr4 C35 C40 158.0(4) . . . . ? C34 Cr4 C35 C40 120.3(5) . . . . ? C32 Cr4 C35 C40 -159.4(4) . . . . ? P9 Cr4 C35 C40 41.5(4) . . . . ? P10 Cr4 C35 C40 -12.4(4) . . . . ? P7 Cr4 C35 C40 -130.8(3) . . . . ? P6 Cr4 C35 C40 -63.8(4) . . . . ? P8 Cr4 C35 C40 93.3(4) . . . . ? _diffrn_measured_fraction_theta_max 0.934 _diffrn_reflns_theta_full 30.47 _diffrn_measured_fraction_theta_full 0.934 _refine_diff_density_max 1.317 _refine_diff_density_min -0.594 _refine_diff_density_rms 0.110 #===END data_130k _database_code_depnum_ccdc_archive 'CCDC 618755' _audit_creation_method SHELXL-97 _chemical_name_systematic ; \m~2~-\h^5^,\h^5^-cyclopentaphosphole)-bis ((\h^5^-pentamethyl-cyclopentadienyl)-chromium) hexafluoroantimonate ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H30 Cr2 F6 P5 Sb' _chemical_formula_weight 765.04 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M I2/a loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' _cell_length_a 23.0935(8) _cell_length_b 21.3176(7) _cell_length_c 23.0731(8) _cell_angle_alpha 90.00 _cell_angle_beta 101.4420(10) _cell_angle_gamma 90.00 _cell_volume 11133.1(7) _cell_formula_units_Z 16 _cell_measurement_temperature 130(2) _cell_measurement_reflns_used 9054 _cell_measurement_theta_min 2.36 _cell_measurement_theta_max 30.36 _exptl_crystal_description 'irregular block' _exptl_crystal_colour 'dark green' _exptl_crystal_size_max 0.60 _exptl_crystal_size_mid 0.52 _exptl_crystal_size_min 0.40 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.826 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 6048 _exptl_absorpt_coefficient_mu 2.068 _exptl_absorpt_correction_type integration _exptl_absorpt_correction_T_min 0.390 _exptl_absorpt_correction_T_max 0.611 _exptl_absorpt_process_details 'XPREP in SHELXTL' _exptl_special_details ; ? ; _diffrn_ambient_temperature 130(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'Bede Microsource X-ray Generator' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEX CCD Diffractometer' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number 0 _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% 0 _diffrn_reflns_number 42244 _diffrn_reflns_av_R_equivalents 0.0301 _diffrn_reflns_av_sigmaI/netI 0.0388 _diffrn_reflns_limit_h_min -32 _diffrn_reflns_limit_h_max 32 _diffrn_reflns_limit_k_min -30 _diffrn_reflns_limit_k_max 29 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_limit_l_max 32 _diffrn_reflns_theta_min 1.14 _diffrn_reflns_theta_max 30.46 _reflns_number_total 15769 _reflns_number_gt 14510 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'SMART V5.625 (Bruker, 2003)' _computing_cell_refinement 'SMART V5.625 (Bruker, 2003)' _computing_data_reduction 'SAINT V6.28A (Bruker, 2003)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'SHELXTL V6.12(Bruker, 2001)' _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0457P)^2^+19.7312P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 15769 _refine_ls_number_parameters 614 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0382 _refine_ls_R_factor_gt 0.0335 _refine_ls_wR_factor_ref 0.0925 _refine_ls_wR_factor_gt 0.0863 _refine_ls_goodness_of_fit_ref 1.041 _refine_ls_restrained_S_all 1.041 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb1 Sb 0.138051(12) 0.870668(11) 0.384209(12) 0.02827(5) Uani 1 1 d . . . F1 F 0.09670(14) 0.81055(14) 0.33278(15) 0.0573(8) Uani 1 1 d . . . F2 F 0.09029(17) 0.93276(13) 0.34196(14) 0.0613(9) Uani 1 1 d . . . F3 F 0.08400(13) 0.86302(15) 0.43463(15) 0.0533(7) Uani 1 1 d . . . F4 F 0.18387(11) 0.80768(11) 0.42741(13) 0.0417(6) Uani 1 1 d . . . F5 F 0.19330(15) 0.87801(13) 0.33505(13) 0.0504(7) Uani 1 1 d . . . F6 F 0.17964(14) 0.93173(11) 0.43365(12) 0.0460(6) Uani 1 1 d . . . Sb2 Sb 0.137112(12) 0.126596(11) 0.117197(12) 0.02629(5) Uani 1 1 d . . . F7 F 0.1254(2) 0.05417(17) 0.15594(19) 0.1055(18) Uani 1 1 d . . . F8 F 0.07718(14) 0.16585(19) 0.14628(17) 0.0743(10) Uani 1 1 d . . . F9 F 0.08341(14) 0.09921(16) 0.05061(14) 0.0606(8) Uani 1 1 d . . . F10 F 0.20003(15) 0.09125(19) 0.08812(16) 0.0784(12) Uani 1 1 d . . . F11 F 0.19092(14) 0.15368(17) 0.18340(14) 0.0620(9) Uani 1 1 d . . . F12 F 0.14888(16) 0.20016(15) 0.07827(16) 0.0672(9) Uani 1 1 d . . . C1 C -0.11697(16) 0.31257(16) 0.44686(16) 0.0240(6) Uani 1 1 d . . . C2 C -0.14510(15) 0.27049(15) 0.40164(17) 0.0239(6) Uani 1 1 d . . . C3 C -0.14395(14) 0.29845(16) 0.34571(16) 0.0227(6) Uani 1 1 d . . . C4 C -0.11457(15) 0.35768(15) 0.35593(16) 0.0232(6) Uani 1 1 d . . . C5 C -0.09837(15) 0.36651(16) 0.41826(16) 0.0222(6) Uani 1 1 d . . . C6 C -0.1109(2) 0.3046(2) 0.51148(17) 0.0357(9) Uani 1 1 d . . . H6A H -0.1436 0.3259 0.5246 0.054 Uiso 1 1 calc R . . H6B H -0.0733 0.3229 0.5317 0.054 Uiso 1 1 calc R . . H6C H -0.1116 0.2598 0.5209 0.054 Uiso 1 1 calc R . . C7 C -0.17409(17) 0.20970(17) 0.4117(2) 0.0340(8) Uani 1 1 d . . . H7A H -0.2158 0.2172 0.4125 0.051 Uiso 1 1 calc R . . H7B H -0.1543 0.1917 0.4495 0.051 Uiso 1 1 calc R . . H7C H -0.1712 0.1805 0.3796 0.051 Uiso 1 1 calc R . . C8 C -0.17064(17) 0.27238(19) 0.28564(17) 0.0309(8) Uani 1 1 d . . . H8A H -0.2067 0.2956 0.2691 0.046 Uiso 1 1 calc R . . H8B H -0.1802 0.2280 0.2894 0.046 Uiso 1 1 calc R . . H8C H -0.1423 0.2766 0.2594 0.046 Uiso 1 1 calc R . . C9 C -0.10602(17) 0.40382(17) 0.30922(17) 0.0295(7) Uani 1 1 d . . . H9A H -0.1427 0.4273 0.2958 0.044 Uiso 1 1 calc R . . H9B H -0.0956 0.3813 0.2757 0.044 Uiso 1 1 calc R . . H9C H -0.0742 0.4330 0.3257 0.044 Uiso 1 1 calc R . . C10 C -0.07039(18) 0.42374(17) 0.44946(18) 0.0308(8) Uani 1 1 d . . . H10A H -0.0997 0.4465 0.4668 0.046 Uiso 1 1 calc R . . H10B H -0.0559 0.4509 0.4212 0.046 Uiso 1 1 calc R . . H10C H -0.0373 0.4113 0.4809 0.046 Uiso 1 1 calc R . . Cr1 Cr -0.05278(2) 0.28229(2) 0.39282(2) 0.01857(10) Uani 1 1 d . . . P1 P 0.03113(6) 0.26508(10) 0.47163(6) 0.0781(6) Uani 1 1 d . . . P2 P -0.01667(7) 0.18201(7) 0.43237(10) 0.0728(6) Uani 1 1 d . . . P3 P -0.03270(5) 0.19187(8) 0.33746(8) 0.0685(5) Uani 1 1 d . . . P4 P 0.00397(7) 0.28117(10) 0.31591(7) 0.0705(6) Uani 1 1 d . . . P5 P 0.04374(5) 0.32620(5) 0.39899(10) 0.0727(6) Uani 1 1 d . . . Cr2 Cr 0.06507(2) 0.21688(2) 0.38994(2) 0.01821(10) Uani 1 1 d . . . C11 C 0.14820(15) 0.17768(15) 0.44122(15) 0.0206(6) Uani 1 1 d . . . C12 C 0.11796(15) 0.12976(15) 0.40394(17) 0.0225(6) Uani 1 1 d . . . C13 C 0.11311(15) 0.14942(16) 0.34417(16) 0.0239(6) Uani 1 1 d . . . C14 C 0.14035(15) 0.20943(16) 0.34416(16) 0.0237(6) Uani 1 1 d . . . C15 C 0.16192(14) 0.22731(14) 0.40459(15) 0.0207(6) Uani 1 1 d . . . C16 C 0.16513(17) 0.17352(19) 0.50702(16) 0.0312(8) Uani 1 1 d . . . H16A H 0.2021 0.1500 0.5180 0.047 Uiso 1 1 calc R . . H16B H 0.1338 0.1520 0.5224 0.047 Uiso 1 1 calc R . . H16C H 0.1705 0.2159 0.5238 0.047 Uiso 1 1 calc R . . C17 C 0.09795(18) 0.06823(16) 0.4240(2) 0.0363(9) Uani 1 1 d . . . H17A H 0.1309 0.0384 0.4300 0.055 Uiso 1 1 calc R . . H17B H 0.0654 0.0519 0.3940 0.055 Uiso 1 1 calc R . . H17C H 0.0844 0.0741 0.4613 0.055 Uiso 1 1 calc R . . C18 C 0.08828(18) 0.1117(2) 0.28932(19) 0.0364(9) Uani 1 1 d . . . H18A H 0.1200 0.0870 0.2778 0.055 Uiso 1 1 calc R . . H18B H 0.0713 0.1402 0.2571 0.055 Uiso 1 1 calc R . . H18C H 0.0575 0.0834 0.2976 0.055 Uiso 1 1 calc R . . C19 C 0.14770(17) 0.24589(19) 0.29115(17) 0.0331(8) Uani 1 1 d . . . H19A H 0.1883 0.2411 0.2850 0.050 Uiso 1 1 calc R . . H19B H 0.1397 0.2903 0.2971 0.050 Uiso 1 1 calc R . . H19C H 0.1200 0.2302 0.2564 0.050 Uiso 1 1 calc R . . C20 C 0.19589(16) 0.28572(16) 0.42509(19) 0.0288(7) Uani 1 1 d . . . H20A H 0.2375 0.2797 0.4230 0.043 Uiso 1 1 calc R . . H20B H 0.1928 0.2947 0.4660 0.043 Uiso 1 1 calc R . . H20C H 0.1796 0.3209 0.3997 0.043 Uiso 1 1 calc R . . C21 C 0.10704(15) 0.38620(14) 0.13251(15) 0.0197(6) Uani 1 1 d . . . C22 C 0.17022(16) 0.38280(15) 0.14606(16) 0.0220(6) Uani 1 1 d . . . C23 C 0.19304(16) 0.43819(17) 0.12487(16) 0.0250(7) Uani 1 1 d . . . C24 C 0.14478(17) 0.47645(15) 0.09758(15) 0.0241(6) Uani 1 1 d . . . C25 C 0.09178(15) 0.44416(16) 0.10271(15) 0.0225(6) Uani 1 1 d . . . C26 C 0.06463(17) 0.33599(17) 0.14245(17) 0.0293(7) Uani 1 1 d . . . H26A H 0.0671 0.3006 0.1159 0.044 Uiso 1 1 calc R . . H26B H 0.0243 0.3528 0.1343 0.044 Uiso 1 1 calc R . . H26C H 0.0747 0.3217 0.1836 0.044 Uiso 1 1 calc R . . C27 C 0.20646(17) 0.32809(17) 0.17381(17) 0.0298(8) Uani 1 1 d . . . H27A H 0.2258 0.3081 0.1444 0.045 Uiso 1 1 calc R . . H27B H 0.1807 0.2976 0.1880 0.045 Uiso 1 1 calc R . . H27C H 0.2365 0.3428 0.2071 0.045 Uiso 1 1 calc R . . C28 C 0.25738(18) 0.4514(2) 0.1269(2) 0.0390(10) Uani 1 1 d . . . H28A H 0.2683 0.4365 0.0903 0.058 Uiso 1 1 calc R . . H28B H 0.2813 0.4297 0.1608 0.058 Uiso 1 1 calc R . . H28C H 0.2645 0.4967 0.1309 0.058 Uiso 1 1 calc R . . C29 C 0.1498(2) 0.53774(17) 0.06688(18) 0.0361(9) Uani 1 1 d . . . H29A H 0.1522 0.5298 0.0256 0.054 Uiso 1 1 calc R . . H29B H 0.1855 0.5598 0.0868 0.054 Uiso 1 1 calc R . . H29C H 0.1151 0.5636 0.0683 0.054 Uiso 1 1 calc R . . C30 C 0.02986(17) 0.46564(19) 0.07735(17) 0.0324(8) Uani 1 1 d . . . H30A H 0.0169 0.4476 0.0378 0.049 Uiso 1 1 calc R . . H30B H 0.0291 0.5115 0.0746 0.049 Uiso 1 1 calc R . . H30C H 0.0033 0.4518 0.1031 0.049 Uiso 1 1 calc R . . Cr3 Cr 0.14227(2) 0.46432(2) 0.19222(2) 0.01801(10) Uani 1 1 d . . . P6 P 0.08530(5) 0.44412(5) 0.26823(5) 0.0369(2) Uani 1 1 d . . . P7 P 0.18009(6) 0.42979(5) 0.29418(4) 0.0369(2) Uani 1 1 d . . . P8 P 0.22431(4) 0.50934(6) 0.26284(5) 0.0374(2) Uani 1 1 d . . . P9 P 0.15676(6) 0.57447(4) 0.21959(5) 0.0361(2) Uani 1 1 d . . . P10 P 0.07016(5) 0.53379(5) 0.22210(5) 0.0359(2) Uani 1 1 d . . . Cr4 Cr 0.14340(2) 0.53324(2) 0.31386(2) 0.01757(10) Uani 1 1 d . . . C31 C 0.09532(14) 0.55004(17) 0.38554(15) 0.0234(6) Uani 1 1 d . . . C32 C 0.15170(16) 0.52330(15) 0.41016(14) 0.0223(6) Uani 1 1 d . . . C33 C 0.19582(15) 0.56573(15) 0.39897(15) 0.0209(6) Uani 1 1 d . . . C34 C 0.16684(17) 0.61849(15) 0.36778(16) 0.0230(7) Uani 1 1 d . . . C35 C 0.10494(16) 0.60903(15) 0.35970(15) 0.0236(6) Uani 1 1 d . . . C36 C 0.03660(17) 0.5223(2) 0.38889(18) 0.0358(9) Uani 1 1 d . . . H36A H 0.0206 0.5435 0.4200 0.054 Uiso 1 1 calc R . . H36B H 0.0413 0.4775 0.3981 0.054 Uiso 1 1 calc R . . H36C H 0.0094 0.5277 0.3508 0.054 Uiso 1 1 calc R . . C37 C 0.16291(19) 0.46264(17) 0.44369(16) 0.0309(8) Uani 1 1 d . . . H37A H 0.1660 0.4707 0.4860 0.046 Uiso 1 1 calc R . . H37B H 0.1999 0.4441 0.4371 0.046 Uiso 1 1 calc R . . H37C H 0.1302 0.4336 0.4299 0.046 Uiso 1 1 calc R . . C38 C 0.26160(15) 0.55935(19) 0.41846(17) 0.0302(7) Uani 1 1 d . . . H38A H 0.2739 0.5771 0.4582 0.045 Uiso 1 1 calc R . . H38B H 0.2813 0.5819 0.3908 0.045 Uiso 1 1 calc R . . H38C H 0.2725 0.5149 0.4191 0.045 Uiso 1 1 calc R . . C39 C 0.19697(19) 0.67590(16) 0.35057(17) 0.0323(8) Uani 1 1 d . . . H39A H 0.2048 0.7051 0.3840 0.048 Uiso 1 1 calc R . . H39B H 0.1714 0.6962 0.3168 0.048 Uiso 1 1 calc R . . H39C H 0.2344 0.6639 0.3397 0.048 Uiso 1 1 calc R . . C40 C 0.05824(18) 0.6547(2) 0.33189(17) 0.0356(9) Uani 1 1 d . . . H40A H 0.0490 0.6830 0.3623 0.053 Uiso 1 1 calc R . . H40B H 0.0225 0.6317 0.3135 0.053 Uiso 1 1 calc R . . H40C H 0.0726 0.6792 0.3017 0.053 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.03186(13) 0.02381(9) 0.03057(13) -0.00284(9) 0.00961(8) 0.00318(9) F1 0.0507(17) 0.0512(16) 0.065(2) -0.0205(15) 0.0001(15) -0.0082(13) F2 0.091(2) 0.0463(15) 0.0417(16) 0.0047(13) 0.0025(15) 0.0302(16) F3 0.0403(15) 0.0679(17) 0.0594(18) 0.0104(15) 0.0285(13) 0.0140(14) F4 0.0359(13) 0.0333(11) 0.0586(17) 0.0100(11) 0.0157(11) 0.0123(10) F5 0.0575(18) 0.0640(19) 0.0360(14) -0.0044(12) 0.0244(13) -0.0074(13) F6 0.0696(19) 0.0338(12) 0.0348(13) -0.0092(10) 0.0107(12) -0.0091(12) Sb2 0.02995(14) 0.02275(9) 0.02699(13) 0.00021(8) 0.00766(8) 0.00164(8) F7 0.180(5) 0.0471(18) 0.077(3) 0.0302(19) -0.005(3) -0.034(2) F8 0.0454(17) 0.109(3) 0.076(2) -0.018(2) 0.0305(16) 0.0148(18) F9 0.0565(19) 0.0689(19) 0.0494(17) -0.0122(15) -0.0061(14) -0.0120(16) F10 0.0579(19) 0.103(3) 0.073(2) -0.042(2) 0.0087(17) 0.0333(19) F11 0.0493(17) 0.080(2) 0.0491(17) -0.0300(16) -0.0088(13) 0.0103(15) F12 0.072(2) 0.0540(17) 0.072(2) 0.0294(16) 0.0051(17) -0.0184(15) C1 0.0265(16) 0.0213(14) 0.0261(16) -0.0058(12) 0.0101(13) -0.0027(12) C2 0.0204(15) 0.0209(13) 0.0313(17) -0.0042(13) 0.0076(12) -0.0028(12) C3 0.0156(14) 0.0252(15) 0.0268(16) -0.0059(12) 0.0030(12) -0.0026(12) C4 0.0203(15) 0.0229(14) 0.0268(17) -0.0009(13) 0.0059(12) -0.0012(12) C5 0.0206(15) 0.0205(13) 0.0265(16) -0.0047(13) 0.0070(12) -0.0011(12) C6 0.046(2) 0.039(2) 0.0239(18) -0.0018(15) 0.0135(16) -0.0029(17) C7 0.0253(17) 0.0259(16) 0.054(2) -0.0030(16) 0.0146(16) -0.0071(14) C8 0.0254(17) 0.0366(19) 0.0282(18) -0.0102(15) -0.0006(13) -0.0027(14) C9 0.0320(19) 0.0270(16) 0.0308(18) 0.0063(14) 0.0091(14) 0.0013(14) C10 0.0336(19) 0.0261(16) 0.0332(19) -0.0097(14) 0.0074(14) -0.0052(14) Cr1 0.0186(2) 0.0182(2) 0.0192(2) -0.00237(18) 0.00452(18) -0.00384(18) P1 0.0472(7) 0.1473(17) 0.0314(6) -0.0358(8) -0.0123(5) 0.0579(9) P2 0.0460(7) 0.0508(7) 0.1392(16) 0.0554(9) 0.0609(9) 0.0278(6) P3 0.0209(5) 0.0754(10) 0.1009(12) -0.0664(9) -0.0080(6) 0.0101(5) P4 0.0509(8) 0.1184(14) 0.0525(8) 0.0489(9) 0.0356(7) 0.0559(9) P5 0.0210(5) 0.0244(5) 0.1765(19) -0.0214(8) 0.0284(8) -0.0044(4) Cr2 0.0174(2) 0.0178(2) 0.0197(2) -0.00085(18) 0.00434(18) -0.00245(18) C11 0.0203(15) 0.0202(14) 0.0221(15) 0.0061(11) 0.0063(11) 0.0022(11) C12 0.0194(14) 0.0168(12) 0.0321(18) -0.0021(12) 0.0073(12) 0.0007(11) C13 0.0212(15) 0.0265(15) 0.0248(15) -0.0015(12) 0.0061(12) 0.0023(12) C14 0.0184(14) 0.0263(15) 0.0271(16) -0.0001(13) 0.0064(12) 0.0013(12) C15 0.0193(14) 0.0196(12) 0.0232(15) 0.0016(12) 0.0045(11) 0.0003(11) C16 0.0331(18) 0.0379(19) 0.0223(16) 0.0053(14) 0.0049(13) 0.0118(15) C17 0.035(2) 0.0204(15) 0.060(3) 0.0040(16) 0.0237(18) 0.0009(14) C18 0.0269(18) 0.042(2) 0.040(2) -0.0183(17) 0.0053(15) 0.0007(15) C19 0.0319(18) 0.042(2) 0.0293(18) 0.0140(16) 0.0144(14) 0.0107(16) C20 0.0198(15) 0.0200(14) 0.045(2) 0.0034(14) 0.0018(14) -0.0034(12) C21 0.0183(14) 0.0203(12) 0.0200(15) -0.0034(11) 0.0027(11) -0.0017(11) C22 0.0221(16) 0.0211(14) 0.0224(15) -0.0008(11) 0.0036(12) 0.0055(11) C23 0.0226(16) 0.0265(16) 0.0282(17) -0.0037(13) 0.0105(13) -0.0012(13) C24 0.0334(18) 0.0228(13) 0.0179(14) 0.0012(12) 0.0092(12) 0.0006(13) C25 0.0246(16) 0.0220(14) 0.0213(15) 0.0008(12) 0.0055(12) 0.0052(12) C26 0.0313(18) 0.0272(16) 0.0302(18) -0.0016(14) 0.0078(14) -0.0085(14) C27 0.0325(18) 0.0275(16) 0.0280(17) 0.0017(13) 0.0023(14) 0.0135(14) C28 0.0258(18) 0.046(2) 0.052(3) -0.0111(19) 0.0245(17) -0.0036(16) C29 0.061(3) 0.0217(15) 0.0311(19) 0.0054(14) 0.0217(18) -0.0016(16) C30 0.0297(18) 0.041(2) 0.0246(17) 0.0053(15) 0.0009(14) 0.0133(15) Cr3 0.0165(2) 0.0177(2) 0.0205(2) 0.00163(18) 0.00517(18) 0.00198(17) P6 0.0430(6) 0.0383(5) 0.0357(5) -0.0148(4) 0.0228(4) -0.0222(4) P7 0.0594(7) 0.0264(4) 0.0232(4) 0.0024(4) 0.0046(4) 0.0172(4) P8 0.0198(4) 0.0570(6) 0.0364(5) -0.0179(5) 0.0079(4) -0.0054(4) P9 0.0671(7) 0.0199(4) 0.0246(4) 0.0002(3) 0.0170(4) -0.0081(4) P10 0.0269(5) 0.0489(6) 0.0284(5) -0.0122(4) -0.0033(4) 0.0188(4) Cr4 0.0172(2) 0.0173(2) 0.0184(2) 0.00042(17) 0.00383(18) -0.00044(17) C31 0.0172(14) 0.0307(16) 0.0238(16) -0.0071(13) 0.0078(12) -0.0075(12) C32 0.0277(17) 0.0217(13) 0.0176(14) 0.0004(11) 0.0049(12) -0.0060(12) C33 0.0198(15) 0.0212(14) 0.0210(15) -0.0016(11) 0.0022(11) -0.0011(11) C34 0.0294(17) 0.0208(14) 0.0206(15) -0.0007(11) 0.0087(12) -0.0049(12) C35 0.0267(16) 0.0240(13) 0.0195(15) -0.0040(12) 0.0030(12) 0.0040(13) C36 0.0277(18) 0.050(2) 0.0330(19) -0.0141(17) 0.0134(15) -0.0111(17) C37 0.044(2) 0.0258(16) 0.0218(16) 0.0053(13) 0.0034(14) -0.0045(14) C38 0.0191(15) 0.0379(19) 0.0318(18) -0.0035(15) 0.0011(13) -0.0016(14) C39 0.048(2) 0.0218(15) 0.0283(17) 0.0011(13) 0.0115(15) -0.0091(15) C40 0.0341(19) 0.039(2) 0.0290(18) -0.0073(15) -0.0049(15) 0.0163(16) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb1 F6 1.866(2) . ? Sb1 F2 1.869(3) . ? Sb1 F4 1.870(2) . ? Sb1 F1 1.874(3) . ? Sb1 F5 1.874(3) . ? Sb1 F3 1.875(3) . ? Sb2 F7 1.831(3) . ? Sb2 F8 1.853(3) . ? Sb2 F12 1.854(3) . ? Sb2 F11 1.860(3) . ? Sb2 F9 1.866(3) . ? Sb2 F10 1.875(3) . ? C1 C2 1.431(5) . ? C1 C5 1.433(5) . ? C1 C6 1.479(5) . ? C1 Cr1 2.214(4) . ? C2 C3 1.426(5) . ? C2 C7 1.498(5) . ? C2 Cr1 2.196(3) . ? C3 C4 1.431(4) . ? C3 C8 1.507(5) . ? C3 Cr1 2.197(3) . ? C4 C5 1.425(5) . ? C4 C9 1.501(5) . ? C4 Cr1 2.205(3) . ? C5 C10 1.497(5) . ? C5 Cr1 2.218(3) . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? Cr1 P5 2.3956(12) . ? Cr1 P4 2.4062(13) . ? Cr1 P2 2.4075(13) . ? Cr1 P3 2.4077(12) . ? Cr1 P1 2.4079(13) . ? P1 P2 2.186(3) . ? P1 P5 2.188(3) . ? P1 Cr2 2.4102(13) . ? P2 P3 2.158(3) . ? P2 Cr2 2.4099(13) . ? P3 P4 2.180(3) . ? P3 Cr2 2.4007(12) . ? P4 P5 2.177(3) . ? P4 Cr2 2.4146(13) . ? P5 Cr2 2.3996(12) . ? Cr2 C15 2.206(3) . ? Cr2 C13 2.209(3) . ? Cr2 C11 2.210(3) . ? Cr2 C12 2.211(3) . ? Cr2 C14 2.212(4) . ? C11 C12 1.426(5) . ? C11 C15 1.428(4) . ? C11 C16 1.493(5) . ? C12 C13 1.424(5) . ? C12 C17 1.495(5) . ? C13 C14 1.426(5) . ? C13 C18 1.513(5) . ? C14 C15 1.436(5) . ? C14 C19 1.487(5) . ? C15 C20 1.497(4) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 C25 1.424(4) . ? C21 C22 1.432(5) . ? C21 C26 1.499(5) . ? C21 Cr3 2.211(3) . ? C22 C23 1.419(5) . ? C22 C27 1.503(4) . ? C22 Cr3 2.201(3) . ? C23 C24 1.423(5) . ? C23 C28 1.504(5) . ? C23 Cr3 2.196(4) . ? C24 C25 1.429(5) . ? C24 C29 1.502(5) . ? C24 Cr3 2.211(3) . ? C25 C30 1.505(5) . ? C25 Cr3 2.203(3) . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C27 H27C 0.9800 . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? Cr3 P10 2.4284(11) . ? Cr3 P6 2.4306(11) . ? Cr3 P9 2.4374(11) . ? Cr3 P8 2.4374(11) . ? Cr3 P7 2.4544(11) . ? P6 P7 2.1733(17) . ? P6 P10 2.1820(17) . ? P6 Cr4 2.4408(11) . ? P7 P8 2.1759(17) . ? P7 Cr4 2.4373(11) . ? P8 P9 2.1769(17) . ? P8 Cr4 2.4513(11) . ? P9 P10 2.1911(17) . ? P9 Cr4 2.4218(11) . ? P10 Cr4 2.4337(11) . ? Cr4 C31 2.197(3) . ? Cr4 C32 2.202(3) . ? Cr4 C33 2.204(3) . ? Cr4 C34 2.208(3) . ? Cr4 C35 2.211(3) . ? C31 C35 1.428(5) . ? C31 C32 1.432(5) . ? C31 C36 1.495(5) . ? C32 C33 1.424(5) . ? C32 C37 1.503(5) . ? C33 C34 1.428(5) . ? C33 C38 1.502(5) . ? C34 C35 1.419(5) . ? C34 C39 1.500(5) . ? C35 C40 1.499(5) . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C39 H39A 0.9800 . ? C39 H39B 0.9800 . ? C39 H39C 0.9800 . ? C40 H40A 0.9800 . ? C40 H40B 0.9800 . ? C40 H40C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F6 Sb1 F2 90.21(13) . . ? F6 Sb1 F4 90.39(11) . . ? F2 Sb1 F4 178.25(15) . . ? F6 Sb1 F1 178.45(14) . . ? F2 Sb1 F1 88.86(13) . . ? F4 Sb1 F1 90.57(13) . . ? F6 Sb1 F5 88.97(14) . . ? F2 Sb1 F5 91.57(16) . . ? F4 Sb1 F5 90.08(13) . . ? F1 Sb1 F5 89.80(14) . . ? F6 Sb1 F3 90.38(15) . . ? F2 Sb1 F3 89.34(16) . . ? F4 Sb1 F3 89.02(13) . . ? F1 Sb1 F3 90.86(16) . . ? F5 Sb1 F3 178.88(12) . . ? F7 Sb2 F8 90.6(2) . . ? F7 Sb2 F12 179.7(2) . . ? F8 Sb2 F12 89.16(18) . . ? F7 Sb2 F11 90.02(18) . . ? F8 Sb2 F11 89.30(15) . . ? F12 Sb2 F11 89.83(16) . . ? F7 Sb2 F9 89.97(18) . . ? F8 Sb2 F9 90.99(16) . . ? F12 Sb2 F9 90.18(16) . . ? F11 Sb2 F9 179.71(16) . . ? F7 Sb2 F10 92.1(2) . . ? F8 Sb2 F10 176.74(18) . . ? F12 Sb2 F10 88.17(19) . . ? F11 Sb2 F10 88.83(14) . . ? F9 Sb2 F10 90.88(15) . . ? C2 C1 C5 107.5(3) . . ? C2 C1 C6 127.0(3) . . ? C5 C1 C6 125.4(3) . . ? C2 C1 Cr1 70.4(2) . . ? C5 C1 Cr1 71.3(2) . . ? C6 C1 Cr1 126.4(3) . . ? C3 C2 C1 108.1(3) . . ? C3 C2 C7 126.2(3) . . ? C1 C2 C7 125.6(4) . . ? C3 C2 Cr1 71.07(19) . . ? C1 C2 Cr1 71.8(2) . . ? C7 C2 Cr1 125.8(2) . . ? C2 C3 C4 108.2(3) . . ? C2 C3 C8 126.9(3) . . ? C4 C3 C8 124.8(3) . . ? C2 C3 Cr1 71.0(2) . . ? C4 C3 Cr1 71.35(19) . . ? C8 C3 Cr1 125.1(2) . . ? C5 C4 C3 107.7(3) . . ? C5 C4 C9 126.3(3) . . ? C3 C4 C9 125.9(3) . . ? C5 C4 Cr1 71.7(2) . . ? C3 C4 Cr1 70.72(19) . . ? C9 C4 Cr1 126.0(2) . . ? C4 C5 C1 108.4(3) . . ? C4 C5 C10 126.5(3) . . ? C1 C5 C10 124.9(3) . . ? C4 C5 Cr1 70.70(19) . . ? C1 C5 Cr1 70.97(19) . . ? C10 C5 Cr1 127.2(3) . . ? C1 C6 H6A 109.5 . . ? C1 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C1 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C2 Cr1 C3 37.90(14) . . ? C2 Cr1 C4 63.48(12) . . ? C3 Cr1 C4 37.94(12) . . ? C2 Cr1 C1 37.86(12) . . ? C3 Cr1 C1 63.25(13) . . ? C4 Cr1 C1 63.30(13) . . ? C2 Cr1 C5 63.11(12) . . ? C3 Cr1 C5 62.96(12) . . ? C4 Cr1 C5 37.58(12) . . ? C1 Cr1 C5 37.74(13) . . ? C2 Cr1 P5 161.49(9) . . ? C3 Cr1 P5 139.23(11) . . ? C4 Cr1 P5 105.15(10) . . ? C1 Cr1 P5 124.87(10) . . ? C5 Cr1 P5 98.80(9) . . ? C2 Cr1 P4 138.42(11) . . ? C3 Cr1 P4 104.21(10) . . ? C4 Cr1 P4 97.35(10) . . ? C1 Cr1 P4 160.34(10) . . ? C5 Cr1 P4 124.03(11) . . ? P5 Cr1 P4 53.93(7) . . ? C2 Cr1 P2 97.63(9) . . ? C3 Cr1 P2 123.55(10) . . ? C4 Cr1 P2 160.48(10) . . ? C1 Cr1 P2 105.41(10) . . ? C5 Cr1 P2 139.93(11) . . ? P5 Cr1 P2 94.37(5) . . ? P4 Cr1 P2 94.14(6) . . ? C2 Cr1 P3 104.49(9) . . ? C3 Cr1 P3 97.44(9) . . ? C4 Cr1 P3 123.83(10) . . ? C1 Cr1 P3 138.86(10) . . ? C5 Cr1 P3 160.00(10) . . ? P5 Cr1 P3 93.98(5) . . ? P4 Cr1 P3 53.87(7) . . ? P2 Cr1 P3 53.24(7) . . ? C2 Cr1 P1 124.28(11) . . ? C3 Cr1 P1 161.15(11) . . ? C4 Cr1 P1 139.89(10) . . ? C1 Cr1 P1 98.48(10) . . ? C5 Cr1 P1 106.06(10) . . ? P5 Cr1 P1 54.18(8) . . ? P4 Cr1 P1 94.64(6) . . ? P2 Cr1 P1 53.99(8) . . ? P3 Cr1 P1 93.89(5) . . ? P2 P1 P5 107.34(8) . . ? P2 P1 Cr1 62.99(6) . . ? P5 P1 Cr1 62.62(5) . . ? P2 P1 Cr2 63.02(6) . . ? P5 P1 Cr2 62.70(6) . . ? Cr1 P1 Cr2 79.18(4) . . ? P3 P2 P1 108.21(8) . . ? P3 P2 Cr1 63.39(5) . . ? P1 P2 Cr1 63.01(6) . . ? P3 P2 Cr2 63.14(5) . . ? P1 P2 Cr2 63.04(6) . . ? Cr1 P2 Cr2 79.19(4) . . ? P2 P3 P4 108.68(8) . . ? P2 P3 Cr2 63.57(5) . . ? P4 P3 Cr2 63.40(5) . . ? P2 P3 Cr1 63.37(5) . . ? P4 P3 Cr1 63.03(6) . . ? Cr2 P3 Cr1 79.37(4) . . ? P5 P4 P3 107.42(8) . . ? P5 P4 Cr1 62.79(6) . . ? P3 P4 Cr1 63.10(5) . . ? P5 P4 Cr2 62.76(6) . . ? P3 P4 Cr2 62.75(5) . . ? Cr1 P4 Cr2 79.13(4) . . ? P4 P5 P1 108.35(8) . . ? P4 P5 Cr1 63.28(5) . . ? P1 P5 Cr1 63.19(6) . . ? P4 P5 Cr2 63.46(5) . . ? P1 P5 Cr2 63.19(6) . . ? Cr1 P5 Cr2 79.63(4) . . ? C15 Cr2 C13 63.18(13) . . ? C15 Cr2 C11 37.75(12) . . ? C13 Cr2 C11 62.90(13) . . ? C15 Cr2 C12 63.15(12) . . ? C13 Cr2 C12 37.60(13) . . ? C11 Cr2 C12 37.63(12) . . ? C15 Cr2 C14 37.94(13) . . ? C13 Cr2 C14 37.63(12) . . ? C11 Cr2 C14 63.06(13) . . ? C12 Cr2 C14 62.98(13) . . ? C15 Cr2 P5 96.21(9) . . ? C13 Cr2 P5 143.62(10) . . ? C11 Cr2 P5 119.49(10) . . ? C12 Cr2 P5 156.93(10) . . ? C14 Cr2 P5 107.80(10) . . ? C15 Cr2 P3 157.40(10) . . ? C13 Cr2 P3 97.22(10) . . ? C11 Cr2 P3 144.72(10) . . ? C12 Cr2 P3 108.92(10) . . ? C14 Cr2 P3 119.53(10) . . ? P5 Cr2 P3 94.06(5) . . ? C15 Cr2 P2 145.18(10) . . ? C13 Cr2 P2 120.11(10) . . ? C11 Cr2 P2 109.46(10) . . ? C12 Cr2 P2 97.82(10) . . ? C14 Cr2 P2 157.69(10) . . ? P5 Cr2 P2 94.20(5) . . ? P3 Cr2 P2 53.29(7) . . ? C15 Cr2 P1 108.32(10) . . ? C13 Cr2 P1 157.45(10) . . ? C11 Cr2 P1 97.19(10) . . ? C12 Cr2 P1 119.98(11) . . ? C14 Cr2 P1 144.34(11) . . ? P5 Cr2 P1 54.11(8) . . ? P3 Cr2 P1 94.01(5) . . ? P2 Cr2 P1 53.94(8) . . ? C15 Cr2 P4 118.93(9) . . ? C13 Cr2 P4 108.05(10) . . ? C11 Cr2 P4 156.52(10) . . ? C12 Cr2 P4 143.95(11) . . ? C14 Cr2 P4 96.16(10) . . ? P5 Cr2 P4 53.78(7) . . ? P3 Cr2 P4 53.85(7) . . ? P2 Cr2 P4 93.87(5) . . ? P1 Cr2 P4 94.37(5) . . ? C12 C11 C15 108.3(3) . . ? C12 C11 C16 124.7(3) . . ? C15 C11 C16 127.0(3) . . ? C12 C11 Cr2 71.23(19) . . ? C15 C11 Cr2 70.98(18) . . ? C16 C11 Cr2 126.2(2) . . ? C13 C12 C11 108.0(3) . . ? C13 C12 C17 126.1(3) . . ? C11 C12 C17 125.9(4) . . ? C13 C12 Cr2 71.12(19) . . ? C11 C12 Cr2 71.14(18) . . ? C17 C12 Cr2 125.9(2) . . ? C12 C13 C14 108.3(3) . . ? C12 C13 C18 126.7(3) . . ? C14 C13 C18 124.8(3) . . ? C12 C13 Cr2 71.28(19) . . ? C14 C13 Cr2 71.30(19) . . ? C18 C13 Cr2 127.1(2) . . ? C13 C14 C15 107.8(3) . . ? C13 C14 C19 126.3(3) . . ? C15 C14 C19 125.8(3) . . ? C13 C14 Cr2 71.08(19) . . ? C15 C14 Cr2 70.8(2) . . ? C19 C14 Cr2 125.7(2) . . ? C11 C15 C14 107.6(3) . . ? C11 C15 C20 126.4(3) . . ? C14 C15 C20 125.9(3) . . ? C11 C15 Cr2 71.27(19) . . ? C14 C15 Cr2 71.25(19) . . ? C20 C15 Cr2 125.7(2) . . ? C11 C16 H16A 109.5 . . ? C11 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C11 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C25 C21 C22 107.0(3) . . ? C25 C21 C26 125.9(3) . . ? C22 C21 C26 126.8(3) . . ? C25 C21 Cr3 70.88(18) . . ? C22 C21 Cr3 70.68(18) . . ? C26 C21 Cr3 127.8(2) . . ? C23 C22 C21 108.3(3) . . ? C23 C22 C27 125.4(3) . . ? C21 C22 C27 126.1(3) . . ? C23 C22 Cr3 70.99(19) . . ? C21 C22 Cr3 71.44(18) . . ? C27 C22 Cr3 126.8(3) . . ? C22 C23 C24 108.5(3) . . ? C22 C23 C28 125.3(3) . . ? C24 C23 C28 126.0(3) . . ? C22 C23 Cr3 71.4(2) . . ? C24 C23 Cr3 71.7(2) . . ? C28 C23 Cr3 126.4(3) . . ? C23 C24 C25 107.2(3) . . ? C23 C24 C29 125.4(4) . . ? C25 C24 C29 127.3(3) . . ? C23 C24 Cr3 70.6(2) . . ? C25 C24 Cr3 70.81(19) . . ? C29 C24 Cr3 126.0(2) . . ? C21 C25 C24 108.9(3) . . ? C21 C25 C30 125.2(3) . . ? C24 C25 C30 125.8(3) . . ? C21 C25 Cr3 71.48(19) . . ? C24 C25 Cr3 71.4(2) . . ? C30 C25 Cr3 126.2(3) . . ? C21 C26 H26A 109.5 . . ? C21 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C21 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C22 C27 H27A 109.5 . . ? C22 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? C22 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? C23 C28 H28A 109.5 . . ? C23 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C23 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C24 C29 H29A 109.5 . . ? C24 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C24 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C25 C30 H30A 109.5 . . ? C25 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? C25 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C23 Cr3 C22 37.65(13) . . ? C23 Cr3 C25 62.93(13) . . ? C22 Cr3 C25 62.86(13) . . ? C23 Cr3 C21 63.27(13) . . ? C22 Cr3 C21 37.88(12) . . ? C25 Cr3 C21 37.64(12) . . ? C23 Cr3 C24 37.68(13) . . ? C22 Cr3 C24 63.05(12) . . ? C25 Cr3 C24 37.79(13) . . ? C21 Cr3 C24 63.34(12) . . ? C23 Cr3 P10 148.00(10) . . ? C22 Cr3 P10 154.47(10) . . ? C25 Cr3 P10 96.88(9) . . ? C21 Cr3 P10 116.61(9) . . ? C24 Cr3 P10 111.27(10) . . ? C23 Cr3 P6 155.10(10) . . ? C22 Cr3 P6 117.52(10) . . ? C25 Cr3 P6 112.35(10) . . ? C21 Cr3 P6 97.54(9) . . ? C24 Cr3 P6 149.02(11) . . ? P10 Cr3 P6 53.37(4) . . ? C23 Cr3 P9 111.26(10) . . ? C22 Cr3 P9 147.97(10) . . ? C25 Cr3 P9 116.79(9) . . ? C21 Cr3 P9 154.39(9) . . ? C24 Cr3 P9 96.55(9) . . ? P10 Cr3 P9 53.53(4) . . ? P6 Cr3 P9 92.85(4) . . ? C23 Cr3 P8 96.87(10) . . ? C22 Cr3 P8 111.77(10) . . ? C25 Cr3 P8 154.18(10) . . ? C21 Cr3 P8 148.69(9) . . ? C24 Cr3 P8 116.43(10) . . ? P10 Cr3 P8 93.20(4) . . ? P6 Cr3 P8 92.72(4) . . ? P9 Cr3 P8 53.05(4) . . ? C23 Cr3 P7 117.63(10) . . ? C22 Cr3 P7 98.30(9) . . ? C25 Cr3 P7 149.49(10) . . ? C21 Cr3 P7 112.85(9) . . ? C24 Cr3 P7 155.19(10) . . ? P10 Cr3 P7 92.54(4) . . ? P6 Cr3 P7 52.83(4) . . ? P9 Cr3 P7 92.07(4) . . ? P8 Cr3 P7 52.82(4) . . ? P7 P6 P10 108.22(6) . . ? P7 P6 Cr3 64.15(4) . . ? P10 P6 Cr3 63.27(4) . . ? P7 P6 Cr4 63.46(4) . . ? P10 P6 Cr4 63.24(4) . . ? Cr3 P6 Cr4 81.00(3) . . ? P6 P7 P8 108.20(6) . . ? P6 P7 Cr4 63.63(4) . . ? P8 P7 Cr4 63.90(4) . . ? P6 P7 Cr3 63.02(4) . . ? P8 P7 Cr3 63.19(4) . . ? Cr4 P7 Cr3 80.59(3) . . ? P7 P8 P9 107.97(6) . . ? P7 P8 Cr3 63.99(4) . . ? P9 P8 Cr3 63.48(4) . . ? P7 P8 Cr4 63.24(4) . . ? P9 P8 Cr4 62.77(4) . . ? Cr3 P8 Cr4 80.65(3) . . ? P8 P9 P10 108.08(6) . . ? P8 P9 Cr4 64.17(4) . . ? P10 P9 Cr4 63.45(4) . . ? P8 P9 Cr3 63.48(4) . . ? P10 P9 Cr3 63.03(4) . . ? Cr4 P9 Cr3 81.24(3) . . ? P6 P10 P9 107.51(6) . . ? P6 P10 Cr3 63.37(4) . . ? P9 P10 Cr3 63.45(4) . . ? P6 P10 Cr4 63.57(4) . . ? P9 P10 Cr4 62.90(4) . . ? Cr3 P10 Cr4 81.18(3) . . ? C31 Cr4 C32 37.99(13) . . ? C31 Cr4 C33 63.15(12) . . ? C32 Cr4 C33 37.71(12) . . ? C31 Cr4 C34 62.98(13) . . ? C32 Cr4 C34 63.14(12) . . ? C33 Cr4 C34 37.77(12) . . ? C31 Cr4 C35 37.80(13) . . ? C32 Cr4 C35 63.30(13) . . ? C33 Cr4 C35 63.00(12) . . ? C34 Cr4 C35 37.45(13) . . ? C31 Cr4 P9 142.24(10) . . ? C32 Cr4 P9 160.06(9) . . ? C33 Cr4 P9 122.74(10) . . ? C34 Cr4 P9 98.44(9) . . ? C35 Cr4 P9 107.41(10) . . ? C31 Cr4 P10 106.64(10) . . ? C32 Cr4 P10 141.68(10) . . ? C33 Cr4 P10 159.66(9) . . ? C34 Cr4 P10 122.45(10) . . ? C35 Cr4 P10 97.86(9) . . ? P9 Cr4 P10 53.65(4) . . ? C31 Cr4 P7 122.29(10) . . ? C32 Cr4 P7 97.88(9) . . ? C33 Cr4 P7 107.49(9) . . ? C34 Cr4 P7 142.59(11) . . ? C35 Cr4 P7 159.66(10) . . ? P9 Cr4 P7 92.87(4) . . ? P10 Cr4 P7 92.84(4) . . ? C31 Cr4 P6 97.75(9) . . ? C32 Cr4 P6 106.90(9) . . ? C33 Cr4 P6 141.88(9) . . ? C34 Cr4 P6 159.38(10) . . ? C35 Cr4 P6 122.43(10) . . ? P9 Cr4 P6 92.99(4) . . ? P10 Cr4 P6 53.18(4) . . ? P7 Cr4 P6 52.91(4) . . ? C31 Cr4 P8 160.52(10) . . ? C32 Cr4 P8 122.85(10) . . ? C33 Cr4 P8 99.03(10) . . ? C34 Cr4 P8 108.46(10) . . ? C35 Cr4 P8 142.96(10) . . ? P9 Cr4 P8 53.06(4) . . ? P10 Cr4 P8 92.73(4) . . ? P7 Cr4 P8 52.86(4) . . ? P6 Cr4 P8 92.13(4) . . ? C35 C31 C32 108.2(3) . . ? C35 C31 C36 126.0(3) . . ? C32 C31 C36 125.8(3) . . ? C35 C31 Cr4 71.66(19) . . ? C32 C31 Cr4 71.21(19) . . ? C36 C31 Cr4 125.0(2) . . ? C33 C32 C31 107.6(3) . . ? C33 C32 C37 125.7(3) . . ? C31 C32 C37 126.7(3) . . ? C33 C32 Cr4 71.22(19) . . ? C31 C32 Cr4 70.80(19) . . ? C37 C32 Cr4 125.0(2) . . ? C32 C33 C34 108.1(3) . . ? C32 C33 C38 127.3(3) . . ? C34 C33 C38 124.5(3) . . ? C32 C33 Cr4 71.07(19) . . ? C34 C33 Cr4 71.27(19) . . ? C38 C33 Cr4 125.6(2) . . ? C35 C34 C33 108.3(3) . . ? C35 C34 C39 126.1(3) . . ? C33 C34 C39 125.5(3) . . ? C35 C34 Cr4 71.40(19) . . ? C33 C34 Cr4 70.96(18) . . ? C39 C34 Cr4 126.7(3) . . ? C34 C35 C31 107.8(3) . . ? C34 C35 C40 125.8(3) . . ? C31 C35 C40 126.3(3) . . ? C34 C35 Cr4 71.15(19) . . ? C31 C35 Cr4 70.54(18) . . ? C40 C35 Cr4 126.3(2) . . ? C31 C36 H36A 109.5 . . ? C31 C36 H36B 109.5 . . ? H36A C36 H36B 109.5 . . ? C31 C36 H36C 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C32 C37 H37A 109.5 . . ? C32 C37 H37B 109.5 . . ? H37A C37 H37B 109.5 . . ? C32 C37 H37C 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? C33 C38 H38A 109.5 . . ? C33 C38 H38B 109.5 . . ? H38A C38 H38B 109.5 . . ? C33 C38 H38C 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? C34 C39 H39A 109.5 . . ? C34 C39 H39B 109.5 . . ? H39A C39 H39B 109.5 . . ? C34 C39 H39C 109.5 . . ? H39A C39 H39C 109.5 . . ? H39B C39 H39C 109.5 . . ? C35 C40 H40A 109.5 . . ? C35 C40 H40B 109.5 . . ? H40A C40 H40B 109.5 . . ? C35 C40 H40C 109.5 . . ? H40A C40 H40C 109.5 . . ? H40B C40 H40C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 C1 C2 C3 -0.2(4) . . . . ? C6 C1 C2 C3 176.5(4) . . . . ? Cr1 C1 C2 C3 -62.2(2) . . . . ? C5 C1 C2 C7 -176.5(3) . . . . ? C6 C1 C2 C7 0.1(6) . . . . ? Cr1 C1 C2 C7 121.5(4) . . . . ? C5 C1 C2 Cr1 62.0(2) . . . . ? C6 C1 C2 Cr1 -121.4(4) . . . . ? C1 C2 C3 C4 0.6(4) . . . . ? C7 C2 C3 C4 176.9(3) . . . . ? Cr1 C2 C3 C4 -62.0(2) . . . . ? C1 C2 C3 C8 -177.3(3) . . . . ? C7 C2 C3 C8 -1.0(6) . . . . ? Cr1 C2 C3 C8 120.1(4) . . . . ? C1 C2 C3 Cr1 62.6(2) . . . . ? C7 C2 C3 Cr1 -121.1(4) . . . . ? C2 C3 C4 C5 -0.8(4) . . . . ? C8 C3 C4 C5 177.2(3) . . . . ? Cr1 C3 C4 C5 -62.6(2) . . . . ? C2 C3 C4 C9 -177.2(3) . . . . ? C8 C3 C4 C9 0.8(6) . . . . ? Cr1 C3 C4 C9 121.0(3) . . . . ? C2 C3 C4 Cr1 61.8(2) . . . . ? C8 C3 C4 Cr1 -120.2(3) . . . . ? C3 C4 C5 C1 0.7(4) . . . . ? C9 C4 C5 C1 177.1(3) . . . . ? Cr1 C4 C5 C1 -61.3(2) . . . . ? C3 C4 C5 C10 -175.5(3) . . . . ? C9 C4 C5 C10 0.9(6) . . . . ? Cr1 C4 C5 C10 122.5(4) . . . . ? C3 C4 C5 Cr1 61.9(2) . . . . ? C9 C4 C5 Cr1 -121.7(4) . . . . ? C2 C1 C5 C4 -0.3(4) . . . . ? C6 C1 C5 C4 -177.0(4) . . . . ? Cr1 C1 C5 C4 61.1(2) . . . . ? C2 C1 C5 C10 176.0(3) . . . . ? C6 C1 C5 C10 -0.8(6) . . . . ? Cr1 C1 C5 C10 -122.6(4) . . . . ? C2 C1 C5 Cr1 -61.4(2) . . . . ? C6 C1 C5 Cr1 121.9(4) . . . . ? C1 C2 Cr1 C3 -117.3(3) . . . . ? C7 C2 Cr1 C3 121.5(4) . . . . ? C3 C2 Cr1 C4 37.46(19) . . . . ? C1 C2 Cr1 C4 -79.8(2) . . . . ? C7 C2 Cr1 C4 159.0(4) . . . . ? C3 C2 Cr1 C1 117.3(3) . . . . ? C7 C2 Cr1 C1 -121.2(4) . . . . ? C3 C2 Cr1 C5 79.7(2) . . . . ? C1 C2 Cr1 C5 -37.6(2) . . . . ? C7 C2 Cr1 C5 -158.8(4) . . . . ? C3 C2 Cr1 P5 92.7(4) . . . . ? C1 C2 Cr1 P5 -24.6(5) . . . . ? C7 C2 Cr1 P5 -145.8(3) . . . . ? C3 C2 Cr1 P4 -32.2(2) . . . . ? C1 C2 Cr1 P4 -149.55(18) . . . . ? C7 C2 Cr1 P4 89.3(4) . . . . ? C3 C2 Cr1 P2 -137.36(18) . . . . ? C1 C2 Cr1 P2 105.3(2) . . . . ? C7 C2 Cr1 P2 -15.9(3) . . . . ? C3 C2 Cr1 P3 -83.45(19) . . . . ? C1 C2 Cr1 P3 159.24(19) . . . . ? C7 C2 Cr1 P3 38.1(4) . . . . ? C3 C2 Cr1 P1 171.43(16) . . . . ? C1 C2 Cr1 P1 54.1(2) . . . . ? C7 C2 Cr1 P1 -67.1(4) . . . . ? C4 C3 Cr1 C2 117.7(3) . . . . ? C8 C3 Cr1 C2 -122.3(4) . . . . ? C2 C3 Cr1 C4 -117.7(3) . . . . ? C8 C3 Cr1 C4 120.0(4) . . . . ? C2 C3 Cr1 C1 -37.64(19) . . . . ? C4 C3 Cr1 C1 80.1(2) . . . . ? C8 C3 Cr1 C1 -159.9(4) . . . . ? C2 C3 Cr1 C5 -80.2(2) . . . . ? C4 C3 Cr1 C5 37.6(2) . . . . ? C8 C3 Cr1 C5 157.5(4) . . . . ? C2 C3 Cr1 P5 -150.95(17) . . . . ? C4 C3 Cr1 P5 -33.2(3) . . . . ? C8 C3 Cr1 P5 86.8(3) . . . . ? C2 C3 Cr1 P4 158.58(17) . . . . ? C4 C3 Cr1 P4 -83.7(2) . . . . ? C8 C3 Cr1 P4 36.3(3) . . . . ? C2 C3 Cr1 P2 53.7(2) . . . . ? C4 C3 Cr1 P2 171.40(17) . . . . ? C8 C3 Cr1 P2 -68.6(3) . . . . ? C2 C3 Cr1 P3 104.05(18) . . . . ? C4 C3 Cr1 P3 -138.21(19) . . . . ? C8 C3 Cr1 P3 -18.2(3) . . . . ? C2 C3 Cr1 P1 -22.4(4) . . . . ? C4 C3 Cr1 P1 95.3(4) . . . . ? C8 C3 Cr1 P1 -144.7(3) . . . . ? C5 C4 Cr1 C2 79.6(2) . . . . ? C3 C4 Cr1 C2 -37.4(2) . . . . ? C9 C4 Cr1 C2 -158.3(3) . . . . ? C5 C4 Cr1 C3 117.0(3) . . . . ? C9 C4 Cr1 C3 -120.9(4) . . . . ? C5 C4 Cr1 C1 37.07(19) . . . . ? C3 C4 Cr1 C1 -80.0(2) . . . . ? C9 C4 Cr1 C1 159.2(3) . . . . ? C3 C4 Cr1 C5 -117.0(3) . . . . ? C9 C4 Cr1 C5 122.1(4) . . . . ? C5 C4 Cr1 P5 -84.7(2) . . . . ? C3 C4 Cr1 P5 158.25(19) . . . . ? C9 C4 Cr1 P5 37.4(3) . . . . ? C5 C4 Cr1 P4 -139.26(19) . . . . ? C3 C4 Cr1 P4 103.7(2) . . . . ? C9 C4 Cr1 P4 -17.1(3) . . . . ? C5 C4 Cr1 P2 95.1(4) . . . . ? C3 C4 Cr1 P2 -21.9(4) . . . . ? C9 C4 Cr1 P2 -142.7(3) . . . . ? C5 C4 Cr1 P3 169.74(17) . . . . ? C3 C4 Cr1 P3 52.7(2) . . . . ? C9 C4 Cr1 P3 -68.2(3) . . . . ? C5 C4 Cr1 P1 -33.0(3) . . . . ? C3 C4 Cr1 P1 -150.04(19) . . . . ? C9 C4 Cr1 P1 89.1(3) . . . . ? C5 C1 Cr1 C2 -117.3(3) . . . . ? C6 C1 Cr1 C2 122.1(4) . . . . ? C2 C1 Cr1 C3 37.7(2) . . . . ? C5 C1 Cr1 C3 -79.6(2) . . . . ? C6 C1 Cr1 C3 159.8(3) . . . . ? C2 C1 Cr1 C4 80.4(2) . . . . ? C5 C1 Cr1 C4 -36.92(19) . . . . ? C6 C1 Cr1 C4 -157.5(3) . . . . ? C2 C1 Cr1 C5 117.3(3) . . . . ? C6 C1 Cr1 C5 -120.6(4) . . . . ? C2 C1 Cr1 P5 170.72(17) . . . . ? C5 C1 Cr1 P5 53.4(2) . . . . ? C6 C1 Cr1 P5 -67.2(3) . . . . ? C2 C1 Cr1 P4 91.2(4) . . . . ? C5 C1 Cr1 P4 -26.0(4) . . . . ? C6 C1 Cr1 P4 -146.7(3) . . . . ? C2 C1 Cr1 P2 -82.5(2) . . . . ? C5 C1 Cr1 P2 160.19(19) . . . . ? C6 C1 Cr1 P2 39.6(3) . . . . ? C2 C1 Cr1 P3 -31.4(3) . . . . ? C5 C1 Cr1 P3 -148.72(17) . . . . ? C6 C1 Cr1 P3 90.7(3) . . . . ? C2 C1 Cr1 P1 -137.4(2) . . . . ? C5 C1 Cr1 P1 105.3(2) . . . . ? C6 C1 Cr1 P1 -15.3(3) . . . . ? C4 C5 Cr1 C2 -80.7(2) . . . . ? C1 C5 Cr1 C2 37.7(2) . . . . ? C10 C5 Cr1 C2 157.6(4) . . . . ? C4 C5 Cr1 C3 -37.94(19) . . . . ? C1 C5 Cr1 C3 80.4(2) . . . . ? C10 C5 Cr1 C3 -159.7(4) . . . . ? C1 C5 Cr1 C4 118.4(3) . . . . ? C10 C5 Cr1 C4 -121.7(4) . . . . ? C4 C5 Cr1 C1 -118.4(3) . . . . ? C10 C5 Cr1 C1 119.9(4) . . . . ? C4 C5 Cr1 P5 103.45(19) . . . . ? C1 C5 Cr1 P5 -138.18(19) . . . . ? C10 C5 Cr1 P5 -18.3(3) . . . . ? C4 C5 Cr1 P4 51.4(2) . . . . ? C1 C5 Cr1 P4 169.73(17) . . . . ? C10 C5 Cr1 P4 -70.4(3) . . . . ? C4 C5 Cr1 P2 -148.87(18) . . . . ? C1 C5 Cr1 P2 -30.5(3) . . . . ? C10 C5 Cr1 P2 89.4(3) . . . . ? C4 C5 Cr1 P3 -25.6(4) . . . . ? C1 C5 Cr1 P3 92.7(4) . . . . ? C10 C5 Cr1 P3 -147.4(3) . . . . ? C4 C5 Cr1 P1 158.59(18) . . . . ? C1 C5 Cr1 P1 -83.0(2) . . . . ? C10 C5 Cr1 P1 36.9(3) . . . . ? C2 Cr1 P1 P2 72.74(12) . . . . ? C3 Cr1 P1 P2 89.2(3) . . . . ? C4 Cr1 P1 P2 161.04(15) . . . . ? C1 Cr1 P1 P2 102.92(10) . . . . ? C5 Cr1 P1 P2 140.82(11) . . . . ? P5 Cr1 P1 P2 -129.84(7) . . . . ? P4 Cr1 P1 P2 -91.75(8) . . . . ? P3 Cr1 P1 P2 -37.73(7) . . . . ? C2 Cr1 P1 P5 -157.42(11) . . . . ? C3 Cr1 P1 P5 -141.0(3) . . . . ? C4 Cr1 P1 P5 -69.12(16) . . . . ? C1 Cr1 P1 P5 -127.24(10) . . . . ? C5 Cr1 P1 P5 -89.34(11) . . . . ? P4 Cr1 P1 P5 38.08(7) . . . . ? P2 Cr1 P1 P5 129.84(7) . . . . ? P3 Cr1 P1 P5 92.11(7) . . . . ? C2 Cr1 P1 Cr2 137.85(11) . . . . ? C3 Cr1 P1 Cr2 154.3(3) . . . . ? C4 Cr1 P1 Cr2 -133.85(14) . . . . ? C1 Cr1 P1 Cr2 168.03(10) . . . . ? C5 Cr1 P1 Cr2 -154.07(10) . . . . ? P5 Cr1 P1 Cr2 -64.73(6) . . . . ? P4 Cr1 P1 Cr2 -26.65(8) . . . . ? P2 Cr1 P1 Cr2 65.11(6) . . . . ? P3 Cr1 P1 Cr2 27.38(7) . . . . ? P5 P1 P2 P3 0.24(9) . . . . ? Cr1 P1 P2 P3 45.83(6) . . . . ? Cr2 P1 P2 P3 -45.49(6) . . . . ? P5 P1 P2 Cr1 -45.59(5) . . . . ? Cr2 P1 P2 Cr1 -91.32(5) . . . . ? P5 P1 P2 Cr2 45.73(6) . . . . ? Cr1 P1 P2 Cr2 91.32(5) . . . . ? C2 Cr1 P2 P3 102.41(11) . . . . ? C3 Cr1 P2 P3 72.46(13) . . . . ? C4 Cr1 P2 P3 88.4(3) . . . . ? C1 Cr1 P2 P3 140.28(11) . . . . ? C5 Cr1 P2 P3 159.08(15) . . . . ? P5 Cr1 P2 P3 -91.71(8) . . . . ? P4 Cr1 P2 P3 -37.62(7) . . . . ? P1 Cr1 P2 P3 -130.35(7) . . . . ? C2 Cr1 P2 P1 -127.24(11) . . . . ? C3 Cr1 P2 P1 -157.19(13) . . . . ? C4 Cr1 P2 P1 -141.2(3) . . . . ? C1 Cr1 P2 P1 -89.37(11) . . . . ? C5 Cr1 P2 P1 -70.57(15) . . . . ? P5 Cr1 P2 P1 38.64(8) . . . . ? P4 Cr1 P2 P1 92.73(8) . . . . ? P3 Cr1 P2 P1 130.35(7) . . . . ? C2 Cr1 P2 Cr2 167.65(11) . . . . ? C3 Cr1 P2 Cr2 137.69(12) . . . . ? C4 Cr1 P2 Cr2 153.7(3) . . . . ? C1 Cr1 P2 Cr2 -154.48(10) . . . . ? C5 Cr1 P2 Cr2 -135.69(14) . . . . ? P5 Cr1 P2 Cr2 -26.48(8) . . . . ? P4 Cr1 P2 Cr2 27.61(7) . . . . ? P3 Cr1 P2 Cr2 65.23(6) . . . . ? P1 Cr1 P2 Cr2 -65.12(6) . . . . ? P1 P2 P3 P4 -0.47(9) . . . . ? Cr1 P2 P3 P4 45.17(6) . . . . ? Cr2 P2 P3 P4 -45.90(5) . . . . ? P1 P2 P3 Cr2 45.44(6) . . . . ? Cr1 P2 P3 Cr2 91.07(5) . . . . ? P1 P2 P3 Cr1 -45.64(6) . . . . ? Cr2 P2 P3 Cr1 -91.07(5) . . . . ? C2 Cr1 P3 P2 -88.75(11) . . . . ? C3 Cr1 P3 P2 -126.74(11) . . . . ? C4 Cr1 P3 P2 -156.29(12) . . . . ? C1 Cr1 P3 P2 -69.45(17) . . . . ? C5 Cr1 P3 P2 -137.8(3) . . . . ? P5 Cr1 P3 P2 92.48(8) . . . . ? P4 Cr1 P3 P2 131.08(7) . . . . ? P1 Cr1 P3 P2 38.16(8) . . . . ? C2 Cr1 P3 P4 140.17(11) . . . . ? C3 Cr1 P3 P4 102.18(11) . . . . ? C4 Cr1 P3 P4 72.63(12) . . . . ? C1 Cr1 P3 P4 159.47(16) . . . . ? C5 Cr1 P3 P4 91.2(3) . . . . ? P5 Cr1 P3 P4 -38.59(7) . . . . ? P2 Cr1 P3 P4 -131.08(7) . . . . ? P1 Cr1 P3 P4 -92.91(8) . . . . ? C2 Cr1 P3 Cr2 -154.39(11) . . . . ? C3 Cr1 P3 Cr2 167.62(11) . . . . ? C4 Cr1 P3 Cr2 138.07(11) . . . . ? C1 Cr1 P3 Cr2 -135.09(15) . . . . ? C5 Cr1 P3 Cr2 156.6(3) . . . . ? P5 Cr1 P3 Cr2 26.85(8) . . . . ? P4 Cr1 P3 Cr2 65.44(6) . . . . ? P2 Cr1 P3 Cr2 -65.64(6) . . . . ? P1 Cr1 P3 Cr2 -27.48(8) . . . . ? P2 P3 P4 P5 0.51(9) . . . . ? Cr2 P3 P4 P5 -45.48(5) . . . . ? Cr1 P3 P4 P5 45.85(6) . . . . ? P2 P3 P4 Cr1 -45.34(6) . . . . ? Cr2 P3 P4 Cr1 -91.34(5) . . . . ? P2 P3 P4 Cr2 45.99(6) . . . . ? Cr1 P3 P4 Cr2 91.34(5) . . . . ? C2 Cr1 P4 P5 161.21(14) . . . . ? C3 Cr1 P4 P5 141.45(10) . . . . ? C4 Cr1 P4 P5 103.42(10) . . . . ? C1 Cr1 P4 P5 93.6(3) . . . . ? C5 Cr1 P4 P5 74.71(12) . . . . ? P2 Cr1 P4 P5 -92.39(8) . . . . ? P3 Cr1 P4 P5 -129.66(7) . . . . ? P1 Cr1 P4 P5 -38.23(7) . . . . ? C2 Cr1 P4 P3 -69.13(14) . . . . ? C3 Cr1 P4 P3 -88.89(10) . . . . ? C4 Cr1 P4 P3 -126.92(10) . . . . ? C1 Cr1 P4 P3 -136.7(3) . . . . ? C5 Cr1 P4 P3 -155.63(12) . . . . ? P5 Cr1 P4 P3 129.66(7) . . . . ? P2 Cr1 P4 P3 37.27(7) . . . . ? P1 Cr1 P4 P3 91.43(8) . . . . ? C2 Cr1 P4 Cr2 -133.96(13) . . . . ? C3 Cr1 P4 Cr2 -153.72(10) . . . . ? C4 Cr1 P4 Cr2 168.25(10) . . . . ? C1 Cr1 P4 Cr2 158.5(3) . . . . ? C5 Cr1 P4 Cr2 139.54(11) . . . . ? P5 Cr1 P4 Cr2 64.83(6) . . . . ? P2 Cr1 P4 Cr2 -27.56(7) . . . . ? P3 Cr1 P4 Cr2 -64.83(5) . . . . ? P1 Cr1 P4 Cr2 26.60(8) . . . . ? P3 P4 P5 P1 -0.36(9) . . . . ? Cr1 P4 P5 P1 45.66(6) . . . . ? Cr2 P4 P5 P1 -45.83(6) . . . . ? P3 P4 P5 Cr1 -46.02(5) . . . . ? Cr2 P4 P5 Cr1 -91.50(5) . . . . ? P3 P4 P5 Cr2 45.48(6) . . . . ? Cr1 P4 P5 Cr2 91.50(5) . . . . ? P2 P1 P5 P4 0.07(9) . . . . ? Cr1 P1 P5 P4 -45.71(5) . . . . ? Cr2 P1 P5 P4 45.97(6) . . . . ? P2 P1 P5 Cr1 45.78(6) . . . . ? Cr2 P1 P5 Cr1 91.68(5) . . . . ? P2 P1 P5 Cr2 -45.90(5) . . . . ? Cr1 P1 P5 Cr2 -91.68(5) . . . . ? C2 Cr1 P5 P4 -137.7(4) . . . . ? C3 Cr1 P5 P4 -67.68(16) . . . . ? C4 Cr1 P5 P4 -88.10(11) . . . . ? C1 Cr1 P5 P4 -155.84(13) . . . . ? C5 Cr1 P5 P4 -126.01(11) . . . . ? P2 Cr1 P5 P4 91.95(8) . . . . ? P3 Cr1 P5 P4 38.56(7) . . . . ? P1 Cr1 P5 P4 130.48(7) . . . . ? C2 Cr1 P5 P1 91.8(4) . . . . ? C3 Cr1 P5 P1 161.84(15) . . . . ? C4 Cr1 P5 P1 141.42(11) . . . . ? C1 Cr1 P5 P1 73.68(13) . . . . ? C5 Cr1 P5 P1 103.51(11) . . . . ? P4 Cr1 P5 P1 -130.48(7) . . . . ? P2 Cr1 P5 P1 -38.53(7) . . . . ? P3 Cr1 P5 P1 -91.92(7) . . . . ? C2 Cr1 P5 Cr2 156.9(3) . . . . ? C3 Cr1 P5 Cr2 -133.07(14) . . . . ? C4 Cr1 P5 Cr2 -153.49(10) . . . . ? C1 Cr1 P5 Cr2 138.76(12) . . . . ? C5 Cr1 P5 Cr2 168.60(10) . . . . ? P4 Cr1 P5 Cr2 -65.39(6) . . . . ? P2 Cr1 P5 Cr2 26.56(8) . . . . ? P3 Cr1 P5 Cr2 -26.84(8) . . . . ? P1 Cr1 P5 Cr2 65.09(6) . . . . ? P4 P5 Cr2 C15 121.56(10) . . . . ? P1 P5 Cr2 C15 -108.15(10) . . . . ? Cr1 P5 Cr2 C15 -173.24(10) . . . . ? P4 P5 Cr2 C13 69.70(17) . . . . ? P1 P5 Cr2 C13 -160.01(17) . . . . ? Cr1 P5 Cr2 C13 134.90(16) . . . . ? P4 P5 Cr2 C11 153.11(11) . . . . ? P1 P5 Cr2 C11 -76.60(11) . . . . ? Cr1 P5 Cr2 C11 -141.69(11) . . . . ? P4 P5 Cr2 C12 146.9(3) . . . . ? P1 P5 Cr2 C12 -82.8(3) . . . . ? Cr1 P5 Cr2 C12 -147.9(3) . . . . ? P4 P5 Cr2 C14 84.53(11) . . . . ? P1 P5 Cr2 C14 -145.19(11) . . . . ? Cr1 P5 Cr2 C14 149.72(10) . . . . ? P4 P5 Cr2 P3 -38.27(7) . . . . ? P1 P5 Cr2 P3 92.01(7) . . . . ? Cr1 P5 Cr2 P3 26.92(8) . . . . ? P4 P5 Cr2 P2 -91.72(8) . . . . ? P1 P5 Cr2 P2 38.57(8) . . . . ? Cr1 P5 Cr2 P2 -26.52(8) . . . . ? P4 P5 Cr2 P1 -130.29(7) . . . . ? Cr1 P5 Cr2 P1 -65.09(6) . . . . ? P1 P5 Cr2 P4 130.29(7) . . . . ? Cr1 P5 Cr2 P4 65.20(5) . . . . ? P2 P3 Cr2 C15 150.9(2) . . . . ? P4 P3 Cr2 C15 -78.7(2) . . . . ? Cr1 P3 Cr2 C15 -143.7(2) . . . . ? P2 P3 Cr2 C13 122.43(10) . . . . ? P4 P3 Cr2 C13 -107.11(11) . . . . ? Cr1 P3 Cr2 C13 -172.15(10) . . . . ? P2 P3 Cr2 C11 70.47(17) . . . . ? P4 P3 Cr2 C11 -159.07(17) . . . . ? Cr1 P3 Cr2 C11 135.89(16) . . . . ? P2 P3 Cr2 C12 85.64(11) . . . . ? P4 P3 Cr2 C12 -143.90(11) . . . . ? Cr1 P3 Cr2 C12 151.06(11) . . . . ? P2 P3 Cr2 C14 154.67(11) . . . . ? P4 P3 Cr2 C14 -74.87(12) . . . . ? Cr1 P3 Cr2 C14 -139.90(11) . . . . ? P2 P3 Cr2 P5 -92.22(8) . . . . ? P4 P3 Cr2 P5 38.23(8) . . . . ? Cr1 P3 Cr2 P5 -26.80(8) . . . . ? P4 P3 Cr2 P2 130.46(7) . . . . ? Cr1 P3 Cr2 P2 65.42(6) . . . . ? P2 P3 Cr2 P1 -37.97(8) . . . . ? P4 P3 Cr2 P1 92.49(8) . . . . ? Cr1 P3 Cr2 P1 27.45(8) . . . . ? P2 P3 Cr2 P4 -130.46(7) . . . . ? Cr1 P3 Cr2 P4 -65.03(6) . . . . ? P3 P2 Cr2 C15 -160.88(16) . . . . ? P1 P2 Cr2 C15 68.53(17) . . . . ? Cr1 P2 Cr2 C15 133.61(15) . . . . ? P3 P2 Cr2 C13 -75.45(12) . . . . ? P1 P2 Cr2 C13 153.95(12) . . . . ? Cr1 P2 Cr2 C13 -140.96(11) . . . . ? P3 P2 Cr2 C11 -144.74(11) . . . . ? P1 P2 Cr2 C11 84.66(11) . . . . ? Cr1 P2 Cr2 C11 149.75(10) . . . . ? P3 P2 Cr2 C12 -107.80(11) . . . . ? P1 P2 Cr2 C12 121.60(11) . . . . ? Cr1 P2 Cr2 C12 -173.31(11) . . . . ? P3 P2 Cr2 C14 -78.6(3) . . . . ? P1 P2 Cr2 C14 150.8(3) . . . . ? Cr1 P2 Cr2 C14 -144.1(3) . . . . ? P3 P2 Cr2 P5 91.93(8) . . . . ? P1 P2 Cr2 P5 -38.67(7) . . . . ? Cr1 P2 Cr2 P5 26.42(8) . . . . ? P1 P2 Cr2 P3 -130.60(7) . . . . ? Cr1 P2 Cr2 P3 -65.51(6) . . . . ? P3 P2 Cr2 P1 130.60(7) . . . . ? Cr1 P2 Cr2 P1 65.09(6) . . . . ? P3 P2 Cr2 P4 38.01(7) . . . . ? P1 P2 Cr2 P4 -92.59(7) . . . . ? Cr1 P2 Cr2 P4 -27.50(8) . . . . ? P2 P1 Cr2 C15 -145.96(10) . . . . ? P5 P1 Cr2 C15 84.32(10) . . . . ? Cr1 P1 Cr2 C15 148.97(9) . . . . ? P2 P1 Cr2 C13 -82.2(3) . . . . ? P5 P1 Cr2 C13 148.1(3) . . . . ? Cr1 P1 Cr2 C13 -147.3(3) . . . . ? P2 P1 Cr2 C11 -108.87(10) . . . . ? P5 P1 Cr2 C11 121.41(10) . . . . ? Cr1 P1 Cr2 C11 -173.95(10) . . . . ? P2 P1 Cr2 C12 -76.95(12) . . . . ? P5 P1 Cr2 C12 153.33(11) . . . . ? Cr1 P1 Cr2 C12 -142.02(11) . . . . ? P2 P1 Cr2 C14 -161.46(17) . . . . ? P5 P1 Cr2 C14 68.82(18) . . . . ? Cr1 P1 Cr2 C14 133.46(16) . . . . ? P2 P1 Cr2 P5 129.72(7) . . . . ? Cr1 P1 Cr2 P5 64.65(6) . . . . ? P2 P1 Cr2 P3 37.61(7) . . . . ? P5 P1 Cr2 P3 -92.11(7) . . . . ? Cr1 P1 Cr2 P3 -27.47(8) . . . . ? P5 P1 Cr2 P2 -129.72(7) . . . . ? Cr1 P1 Cr2 P2 -65.07(6) . . . . ? P2 P1 Cr2 P4 91.61(7) . . . . ? P5 P1 Cr2 P4 -38.11(7) . . . . ? Cr1 P1 Cr2 P4 26.54(8) . . . . ? P5 P4 Cr2 C15 -75.43(11) . . . . ? P3 P4 Cr2 C15 154.50(11) . . . . ? Cr1 P4 Cr2 C15 -140.29(11) . . . . ? P5 P4 Cr2 C13 -144.19(11) . . . . ? P3 P4 Cr2 C13 85.73(11) . . . . ? Cr1 P4 Cr2 C13 150.95(10) . . . . ? P5 P4 Cr2 C11 -81.1(3) . . . . ? P3 P4 Cr2 C11 148.8(3) . . . . ? Cr1 P4 Cr2 C11 -146.0(2) . . . . ? P5 P4 Cr2 C12 -158.67(17) . . . . ? P3 P4 Cr2 C12 71.25(17) . . . . ? Cr1 P4 Cr2 C12 136.47(16) . . . . ? P5 P4 Cr2 C14 -107.58(10) . . . . ? P3 P4 Cr2 C14 122.35(10) . . . . ? Cr1 P4 Cr2 C14 -172.44(10) . . . . ? P3 P4 Cr2 P5 -130.07(7) . . . . ? Cr1 P4 Cr2 P5 -64.86(6) . . . . ? P5 P4 Cr2 P3 130.07(7) . . . . ? Cr1 P4 Cr2 P3 65.21(5) . . . . ? P5 P4 Cr2 P2 92.38(8) . . . . ? P3 P4 Cr2 P2 -37.69(7) . . . . ? Cr1 P4 Cr2 P2 27.52(7) . . . . ? P5 P4 Cr2 P1 38.30(8) . . . . ? P3 P4 Cr2 P1 -91.78(8) . . . . ? Cr1 P4 Cr2 P1 -26.56(8) . . . . ? C15 Cr2 C11 C12 -117.8(3) . . . . ? C13 Cr2 C11 C12 -37.5(2) . . . . ? C14 Cr2 C11 C12 -79.9(2) . . . . ? P5 Cr2 C11 C12 -176.01(18) . . . . ? P3 Cr2 C11 C12 23.9(3) . . . . ? P2 Cr2 C11 C12 77.2(2) . . . . ? P1 Cr2 C11 C12 131.4(2) . . . . ? P4 Cr2 C11 C12 -109.7(3) . . . . ? C13 Cr2 C11 C15 80.4(2) . . . . ? C12 Cr2 C11 C15 117.8(3) . . . . ? C14 Cr2 C11 C15 37.95(19) . . . . ? P5 Cr2 C11 C15 -58.2(2) . . . . ? P3 Cr2 C11 C15 141.76(18) . . . . ? P2 Cr2 C11 C15 -164.97(18) . . . . ? P1 Cr2 C11 C15 -110.8(2) . . . . ? P4 Cr2 C11 C15 8.1(4) . . . . ? C15 Cr2 C11 C16 122.4(4) . . . . ? C13 Cr2 C11 C16 -157.2(3) . . . . ? C12 Cr2 C11 C16 -119.7(4) . . . . ? C14 Cr2 C11 C16 160.4(3) . . . . ? P5 Cr2 C11 C16 64.2(3) . . . . ? P3 Cr2 C11 C16 -95.8(3) . . . . ? P2 Cr2 C11 C16 -42.6(3) . . . . ? P1 Cr2 C11 C16 11.7(3) . . . . ? P4 Cr2 C11 C16 130.5(3) . . . . ? C15 C11 C12 C13 0.3(4) . . . . ? C16 C11 C12 C13 -176.4(3) . . . . ? Cr2 C11 C12 C13 61.9(2) . . . . ? C15 C11 C12 C17 177.1(3) . . . . ? C16 C11 C12 C17 0.4(5) . . . . ? Cr2 C11 C12 C17 -121.2(3) . . . . ? C15 C11 C12 Cr2 -61.7(2) . . . . ? C16 C11 C12 Cr2 121.6(3) . . . . ? C15 Cr2 C12 C13 -80.1(2) . . . . ? C11 Cr2 C12 C13 -117.5(3) . . . . ? C14 Cr2 C12 C13 -37.4(2) . . . . ? P5 Cr2 C12 C13 -108.6(3) . . . . ? P3 Cr2 C12 C13 76.9(2) . . . . ? P2 Cr2 C12 C13 130.65(19) . . . . ? P1 Cr2 C12 C13 -176.70(17) . . . . ? P4 Cr2 C12 C13 22.9(3) . . . . ? C15 Cr2 C12 C11 37.35(19) . . . . ? C13 Cr2 C12 C11 117.5(3) . . . . ? C14 Cr2 C12 C11 80.1(2) . . . . ? P5 Cr2 C12 C11 8.9(4) . . . . ? P3 Cr2 C12 C11 -165.67(18) . . . . ? P2 Cr2 C12 C11 -111.87(19) . . . . ? P1 Cr2 C12 C11 -59.2(2) . . . . ? P4 Cr2 C12 C11 140.40(18) . . . . ? C15 Cr2 C12 C17 158.5(4) . . . . ? C13 Cr2 C12 C17 -121.4(4) . . . . ? C11 Cr2 C12 C17 121.2(4) . . . . ? C14 Cr2 C12 C17 -158.7(4) . . . . ? P5 Cr2 C12 C17 130.0(3) . . . . ? P3 Cr2 C12 C17 -44.5(4) . . . . ? P2 Cr2 C12 C17 9.3(4) . . . . ? P1 Cr2 C12 C17 61.9(4) . . . . ? P4 Cr2 C12 C17 -98.4(4) . . . . ? C11 C12 C13 C14 0.1(4) . . . . ? C17 C12 C13 C14 -176.8(3) . . . . ? Cr2 C12 C13 C14 62.0(2) . . . . ? C11 C12 C13 C18 175.3(3) . . . . ? C17 C12 C13 C18 -1.6(6) . . . . ? Cr2 C12 C13 C18 -122.8(4) . . . . ? C11 C12 C13 Cr2 -62.0(2) . . . . ? C17 C12 C13 Cr2 121.2(4) . . . . ? C15 Cr2 C13 C12 80.0(2) . . . . ? C11 Cr2 C13 C12 37.48(19) . . . . ? C14 Cr2 C13 C12 117.7(3) . . . . ? P5 Cr2 C13 C12 141.22(18) . . . . ? P3 Cr2 C13 C12 -111.79(19) . . . . ? P2 Cr2 C13 C12 -60.3(2) . . . . ? P1 Cr2 C13 C12 7.5(4) . . . . ? P4 Cr2 C13 C12 -166.05(18) . . . . ? C15 Cr2 C13 C14 -37.7(2) . . . . ? C11 Cr2 C13 C14 -80.2(2) . . . . ? C12 Cr2 C13 C14 -117.7(3) . . . . ? P5 Cr2 C13 C14 23.5(3) . . . . ? P3 Cr2 C13 C14 130.5(2) . . . . ? P2 Cr2 C13 C14 -178.03(18) . . . . ? P1 Cr2 C13 C14 -110.2(3) . . . . ? P4 Cr2 C13 C14 76.2(2) . . . . ? C15 Cr2 C13 C18 -157.6(4) . . . . ? C11 Cr2 C13 C18 159.8(4) . . . . ? C12 Cr2 C13 C18 122.3(4) . . . . ? C14 Cr2 C13 C18 -120.0(4) . . . . ? P5 Cr2 C13 C18 -96.5(4) . . . . ? P3 Cr2 C13 C18 10.5(3) . . . . ? P2 Cr2 C13 C18 62.0(4) . . . . ? P1 Cr2 C13 C18 129.8(3) . . . . ? P4 Cr2 C13 C18 -43.7(3) . . . . ? C12 C13 C14 C15 -0.4(4) . . . . ? C18 C13 C14 C15 -175.7(3) . . . . ? Cr2 C13 C14 C15 61.6(2) . . . . ? C12 C13 C14 C19 177.0(3) . . . . ? C18 C13 C14 C19 1.7(6) . . . . ? Cr2 C13 C14 C19 -121.0(3) . . . . ? C12 C13 C14 Cr2 -62.0(2) . . . . ? C18 C13 C14 Cr2 122.7(3) . . . . ? C15 Cr2 C14 C13 117.5(3) . . . . ? C11 Cr2 C14 C13 79.8(2) . . . . ? C12 Cr2 C14 C13 37.3(2) . . . . ? P5 Cr2 C14 C13 -165.61(18) . . . . ? P3 Cr2 C14 C13 -60.1(2) . . . . ? P2 Cr2 C14 C13 4.5(4) . . . . ? P1 Cr2 C14 C13 141.89(19) . . . . ? P4 Cr2 C14 C13 -111.7(2) . . . . ? C13 Cr2 C14 C15 -117.5(3) . . . . ? C11 Cr2 C14 C15 -37.76(18) . . . . ? C12 Cr2 C14 C15 -80.2(2) . . . . ? P5 Cr2 C14 C15 76.87(19) . . . . ? P3 Cr2 C14 C15 -177.62(15) . . . . ? P2 Cr2 C14 C15 -113.0(3) . . . . ? P1 Cr2 C14 C15 24.4(3) . . . . ? P4 Cr2 C14 C15 130.75(18) . . . . ? C15 Cr2 C14 C19 -120.9(4) . . . . ? C13 Cr2 C14 C19 121.6(4) . . . . ? C11 Cr2 C14 C19 -158.7(4) . . . . ? C12 Cr2 C14 C19 158.9(4) . . . . ? P5 Cr2 C14 C19 -44.0(3) . . . . ? P3 Cr2 C14 C19 61.5(3) . . . . ? P2 Cr2 C14 C19 126.1(3) . . . . ? P1 Cr2 C14 C19 -96.5(3) . . . . ? P4 Cr2 C14 C19 9.9(3) . . . . ? C12 C11 C15 C14 -0.5(4) . . . . ? C16 C11 C15 C14 176.1(3) . . . . ? Cr2 C11 C15 C14 -62.4(2) . . . . ? C12 C11 C15 C20 -177.1(3) . . . . ? C16 C11 C15 C20 -0.5(6) . . . . ? Cr2 C11 C15 C20 121.1(3) . . . . ? C12 C11 C15 Cr2 61.8(2) . . . . ? C16 C11 C15 Cr2 -121.6(4) . . . . ? C13 C14 C15 C11 0.6(4) . . . . ? C19 C14 C15 C11 -176.9(3) . . . . ? Cr2 C14 C15 C11 62.4(2) . . . . ? C13 C14 C15 C20 177.2(3) . . . . ? C19 C14 C15 C20 -0.3(6) . . . . ? Cr2 C14 C15 C20 -121.0(3) . . . . ? C13 C14 C15 Cr2 -61.8(2) . . . . ? C19 C14 C15 Cr2 120.8(3) . . . . ? C13 Cr2 C15 C11 -79.6(2) . . . . ? C12 Cr2 C15 C11 -37.2(2) . . . . ? C14 Cr2 C15 C11 -116.9(3) . . . . ? P5 Cr2 C15 C11 131.94(19) . . . . ? P3 Cr2 C15 C11 -111.5(3) . . . . ? P2 Cr2 C15 C11 25.3(3) . . . . ? P1 Cr2 C15 C11 77.8(2) . . . . ? P4 Cr2 C15 C11 -176.31(17) . . . . ? C13 Cr2 C15 C14 37.35(19) . . . . ? C11 Cr2 C15 C14 116.9(3) . . . . ? C12 Cr2 C15 C14 79.7(2) . . . . ? P5 Cr2 C15 C14 -111.14(19) . . . . ? P3 Cr2 C15 C14 5.4(3) . . . . ? P2 Cr2 C15 C14 142.27(19) . . . . ? P1 Cr2 C15 C14 -165.32(17) . . . . ? P4 Cr2 C15 C14 -59.4(2) . . . . ? C13 Cr2 C15 C20 158.6(3) . . . . ? C11 Cr2 C15 C20 -121.8(4) . . . . ? C12 Cr2 C15 C20 -159.1(4) . . . . ? C14 Cr2 C15 C20 121.2(4) . . . . ? P5 Cr2 C15 C20 10.1(3) . . . . ? P3 Cr2 C15 C20 126.6(3) . . . . ? P2 Cr2 C15 C20 -96.5(3) . . . . ? P1 Cr2 C15 C20 -44.1(3) . . . . ? P4 Cr2 C15 C20 61.9(3) . . . . ? C25 C21 C22 C23 0.2(4) . . . . ? C26 C21 C22 C23 174.9(3) . . . . ? Cr3 C21 C22 C23 -61.7(2) . . . . ? C25 C21 C22 C27 -175.6(3) . . . . ? C26 C21 C22 C27 -0.9(6) . . . . ? Cr3 C21 C22 C27 122.5(4) . . . . ? C25 C21 C22 Cr3 61.9(2) . . . . ? C26 C21 C22 Cr3 -123.3(4) . . . . ? C21 C22 C23 C24 -0.5(4) . . . . ? C27 C22 C23 C24 175.4(3) . . . . ? Cr3 C22 C23 C24 -62.5(2) . . . . ? C21 C22 C23 C28 -176.1(3) . . . . ? C27 C22 C23 C28 -0.2(6) . . . . ? Cr3 C22 C23 C28 121.9(4) . . . . ? C21 C22 C23 Cr3 62.0(2) . . . . ? C27 C22 C23 Cr3 -122.1(4) . . . . ? C22 C23 C24 C25 0.5(4) . . . . ? C28 C23 C24 C25 176.1(3) . . . . ? Cr3 C23 C24 C25 -61.7(2) . . . . ? C22 C23 C24 C29 -176.8(3) . . . . ? C28 C23 C24 C29 -1.3(6) . . . . ? Cr3 C23 C24 C29 120.9(4) . . . . ? C22 C23 C24 Cr3 62.3(2) . . . . ? C28 C23 C24 Cr3 -122.2(4) . . . . ? C22 C21 C25 C24 0.2(4) . . . . ? C26 C21 C25 C24 -174.6(3) . . . . ? Cr3 C21 C25 C24 61.9(2) . . . . ? C22 C21 C25 C30 176.5(3) . . . . ? C26 C21 C25 C30 1.7(6) . . . . ? Cr3 C21 C25 C30 -121.7(4) . . . . ? C22 C21 C25 Cr3 -61.8(2) . . . . ? C26 C21 C25 Cr3 123.4(3) . . . . ? C23 C24 C25 C21 -0.4(4) . . . . ? C29 C24 C25 C21 176.9(3) . . . . ? Cr3 C24 C25 C21 -62.0(2) . . . . ? C23 C24 C25 C30 -176.7(3) . . . . ? C29 C24 C25 C30 0.6(6) . . . . ? Cr3 C24 C25 C30 121.7(4) . . . . ? C23 C24 C25 Cr3 61.6(2) . . . . ? C29 C24 C25 Cr3 -121.1(4) . . . . ? C24 C23 Cr3 C22 117.7(3) . . . . ? C28 C23 Cr3 C22 -120.6(4) . . . . ? C22 C23 Cr3 C25 -79.9(2) . . . . ? C24 C23 Cr3 C25 37.8(2) . . . . ? C28 C23 Cr3 C25 159.6(4) . . . . ? C22 C23 Cr3 C21 -37.4(2) . . . . ? C24 C23 Cr3 C21 80.2(2) . . . . ? C28 C23 Cr3 C21 -158.0(4) . . . . ? C22 C23 Cr3 C24 -117.7(3) . . . . ? C28 C23 Cr3 C24 121.8(4) . . . . ? C22 C23 Cr3 P10 -135.5(2) . . . . ? C24 C23 Cr3 P10 -17.9(3) . . . . ? C28 C23 Cr3 P10 103.9(4) . . . . ? C22 C23 Cr3 P6 5.2(4) . . . . ? C24 C23 Cr3 P6 122.8(2) . . . . ? C28 C23 Cr3 P6 -115.4(3) . . . . ? C22 C23 Cr3 P9 170.00(18) . . . . ? C24 C23 Cr3 P9 -72.3(2) . . . . ? C28 C23 Cr3 P9 49.4(4) . . . . ? C22 C23 Cr3 P8 117.08(19) . . . . ? C24 C23 Cr3 P8 -125.26(19) . . . . ? C28 C23 Cr3 P8 -3.5(3) . . . . ? C22 C23 Cr3 P7 65.7(2) . . . . ? C24 C23 Cr3 P7 -176.66(17) . . . . ? C28 C23 Cr3 P7 -54.9(4) . . . . ? C21 C22 Cr3 C23 -117.8(3) . . . . ? C27 C22 Cr3 C23 120.5(4) . . . . ? C23 C22 Cr3 C25 80.0(2) . . . . ? C21 C22 Cr3 C25 -37.79(19) . . . . ? C27 C22 Cr3 C25 -159.5(4) . . . . ? C23 C22 Cr3 C21 117.8(3) . . . . ? C27 C22 Cr3 C21 -121.7(4) . . . . ? C23 C22 Cr3 C24 37.4(2) . . . . ? C21 C22 Cr3 C24 -80.4(2) . . . . ? C27 C22 Cr3 C24 157.9(4) . . . . ? C23 C22 Cr3 P10 120.5(3) . . . . ? C21 C22 Cr3 P10 2.7(4) . . . . ? C27 C22 Cr3 P10 -119.0(3) . . . . ? C23 C22 Cr3 P6 -177.56(18) . . . . ? C21 C22 Cr3 P6 64.6(2) . . . . ? C27 C22 Cr3 P6 -57.1(3) . . . . ? C23 C22 Cr3 P9 -17.8(3) . . . . ? C21 C22 Cr3 P9 -135.59(19) . . . . ? C27 C22 Cr3 P9 102.7(3) . . . . ? C23 C22 Cr3 P8 -72.1(2) . . . . ? C21 C22 Cr3 P8 170.02(17) . . . . ? C27 C22 Cr3 P8 48.3(3) . . . . ? C23 C22 Cr3 P7 -125.3(2) . . . . ? C21 C22 Cr3 P7 116.85(19) . . . . ? C27 C22 Cr3 P7 -4.9(3) . . . . ? C21 C25 Cr3 C23 80.5(2) . . . . ? C24 C25 Cr3 C23 -37.70(19) . . . . ? C30 C25 Cr3 C23 -158.9(4) . . . . ? C21 C25 Cr3 C22 38.0(2) . . . . ? C24 C25 Cr3 C22 -80.2(2) . . . . ? C30 C25 Cr3 C22 158.6(4) . . . . ? C24 C25 Cr3 C21 -118.2(3) . . . . ? C30 C25 Cr3 C21 120.6(4) . . . . ? C21 C25 Cr3 C24 118.2(3) . . . . ? C30 C25 Cr3 C24 -121.2(4) . . . . ? C21 C25 Cr3 P10 -125.61(19) . . . . ? C24 C25 Cr3 P10 116.15(18) . . . . ? C30 C25 Cr3 P10 -5.0(3) . . . . ? C21 C25 Cr3 P6 -72.5(2) . . . . ? C24 C25 Cr3 P6 169.27(17) . . . . ? C30 C25 Cr3 P6 48.1(3) . . . . ? C21 C25 Cr3 P9 -178.03(17) . . . . ? C24 C25 Cr3 P9 63.7(2) . . . . ? C30 C25 Cr3 P9 -57.4(3) . . . . ? C21 C25 Cr3 P8 122.1(2) . . . . ? C24 C25 Cr3 P8 3.9(3) . . . . ? C30 C25 Cr3 P8 -117.3(3) . . . . ? C21 C25 Cr3 P7 -18.6(3) . . . . ? C24 C25 Cr3 P7 -136.82(19) . . . . ? C30 C25 Cr3 P7 102.0(3) . . . . ? C25 C21 Cr3 C23 -79.5(2) . . . . ? C22 C21 Cr3 C23 37.2(2) . . . . ? C26 C21 Cr3 C23 159.3(3) . . . . ? C25 C21 Cr3 C22 -116.8(3) . . . . ? C26 C21 Cr3 C22 122.1(4) . . . . ? C22 C21 Cr3 C25 116.8(3) . . . . ? C26 C21 Cr3 C25 -121.1(4) . . . . ? C25 C21 Cr3 C24 -37.2(2) . . . . ? C22 C21 Cr3 C24 79.6(2) . . . . ? C26 C21 Cr3 C24 -158.3(3) . . . . ? C25 C21 Cr3 P10 64.5(2) . . . . ? C22 C21 Cr3 P10 -178.71(17) . . . . ? C26 C21 Cr3 P10 -56.6(3) . . . . ? C25 C21 Cr3 P6 117.16(19) . . . . ? C22 C21 Cr3 P6 -126.08(19) . . . . ? C26 C21 Cr3 P6 -4.0(3) . . . . ? C25 C21 Cr3 P9 4.1(3) . . . . ? C22 C21 Cr3 P9 120.8(2) . . . . ? C26 C21 Cr3 P9 -117.1(3) . . . . ? C25 C21 Cr3 P8 -134.8(2) . . . . ? C22 C21 Cr3 P8 -18.0(3) . . . . ? C26 C21 Cr3 P8 104.1(3) . . . . ? C25 C21 Cr3 P7 169.89(17) . . . . ? C22 C21 Cr3 P7 -73.3(2) . . . . ? C26 C21 Cr3 P7 48.7(3) . . . . ? C25 C24 Cr3 C23 117.0(3) . . . . ? C29 C24 Cr3 C23 -120.3(4) . . . . ? C23 C24 Cr3 C22 -37.4(2) . . . . ? C25 C24 Cr3 C22 79.7(2) . . . . ? C29 C24 Cr3 C22 -157.6(4) . . . . ? C23 C24 Cr3 C25 -117.0(3) . . . . ? C29 C24 Cr3 C25 122.7(4) . . . . ? C23 C24 Cr3 C21 -80.0(2) . . . . ? C25 C24 Cr3 C21 37.02(19) . . . . ? C29 C24 Cr3 C21 159.7(4) . . . . ? C23 C24 Cr3 P10 169.96(18) . . . . ? C25 C24 Cr3 P10 -73.00(19) . . . . ? C29 C24 Cr3 P10 49.7(4) . . . . ? C23 C24 Cr3 P6 -136.6(2) . . . . ? C25 C24 Cr3 P6 -19.5(3) . . . . ? C29 C24 Cr3 P6 103.2(4) . . . . ? C23 C24 Cr3 P9 116.64(19) . . . . ? C25 C24 Cr3 P9 -126.32(18) . . . . ? C29 C24 Cr3 P9 -3.6(4) . . . . ? C23 C24 Cr3 P8 64.9(2) . . . . ? C25 C24 Cr3 P8 -178.10(16) . . . . ? C29 C24 Cr3 P8 -55.4(4) . . . . ? C23 C24 Cr3 P7 7.1(3) . . . . ? C25 C24 Cr3 P7 124.1(2) . . . . ? C29 C24 Cr3 P7 -113.2(3) . . . . ? C23 Cr3 P6 P7 75.5(2) . . . . ? C22 Cr3 P6 P7 79.00(11) . . . . ? C25 Cr3 P6 P7 149.01(10) . . . . ? C21 Cr3 P6 P7 113.03(9) . . . . ? C24 Cr3 P6 P7 161.81(17) . . . . ? P10 Cr3 P6 P7 -129.28(5) . . . . ? P9 Cr3 P6 P7 -90.43(5) . . . . ? P8 Cr3 P6 P7 -37.32(5) . . . . ? C23 Cr3 P6 P10 -155.3(2) . . . . ? C22 Cr3 P6 P10 -151.71(11) . . . . ? C25 Cr3 P6 P10 -81.71(10) . . . . ? C21 Cr3 P6 P10 -117.69(9) . . . . ? C24 Cr3 P6 P10 -68.90(18) . . . . ? P9 Cr3 P6 P10 38.85(5) . . . . ? P8 Cr3 P6 P10 91.97(5) . . . . ? P7 Cr3 P6 P10 129.28(5) . . . . ? C23 Cr3 P6 Cr4 140.2(2) . . . . ? C22 Cr3 P6 Cr4 143.79(11) . . . . ? C25 Cr3 P6 Cr4 -146.20(10) . . . . ? C21 Cr3 P6 Cr4 177.82(9) . . . . ? C24 Cr3 P6 Cr4 -133.39(17) . . . . ? P10 Cr3 P6 Cr4 -64.49(4) . . . . ? P9 Cr3 P6 Cr4 -25.64(5) . . . . ? P8 Cr3 P6 Cr4 27.47(4) . . . . ? P7 Cr3 P6 Cr4 64.79(4) . . . . ? P10 P6 P7 P8 -1.14(8) . . . . ? Cr3 P6 P7 P8 45.56(5) . . . . ? Cr4 P6 P7 P8 -47.17(5) . . . . ? P10 P6 P7 Cr4 46.03(5) . . . . ? Cr3 P6 P7 Cr4 92.73(3) . . . . ? P10 P6 P7 Cr3 -46.70(5) . . . . ? Cr4 P6 P7 Cr3 -92.73(3) . . . . ? C23 Cr3 P7 P6 -152.61(11) . . . . ? C22 Cr3 P7 P6 -118.38(10) . . . . ? C25 Cr3 P7 P6 -69.71(19) . . . . ? C21 Cr3 P7 P6 -81.90(10) . . . . ? C24 Cr3 P7 P6 -157.5(2) . . . . ? P10 Cr3 P7 P6 38.44(5) . . . . ? P9 Cr3 P7 P6 92.01(5) . . . . ? P8 Cr3 P7 P6 130.53(5) . . . . ? C23 Cr3 P7 P8 76.85(11) . . . . ? C22 Cr3 P7 P8 111.09(10) . . . . ? C25 Cr3 P7 P8 159.76(19) . . . . ? C21 Cr3 P7 P8 147.56(10) . . . . ? C24 Cr3 P7 P8 72.0(2) . . . . ? P10 Cr3 P7 P8 -92.09(5) . . . . ? P6 Cr3 P7 P8 -130.53(5) . . . . ? P9 Cr3 P7 P8 -38.52(5) . . . . ? C23 Cr3 P7 Cr4 142.28(11) . . . . ? C22 Cr3 P7 Cr4 176.51(10) . . . . ? C25 Cr3 P7 Cr4 -134.82(19) . . . . ? C21 Cr3 P7 Cr4 -147.01(10) . . . . ? C24 Cr3 P7 Cr4 137.4(2) . . . . ? P10 Cr3 P7 Cr4 -26.66(4) . . . . ? P6 Cr3 P7 Cr4 -65.11(4) . . . . ? P9 Cr3 P7 Cr4 26.91(4) . . . . ? P8 Cr3 P7 Cr4 65.43(4) . . . . ? P6 P7 P8 P9 1.63(8) . . . . ? Cr4 P7 P8 P9 -45.39(5) . . . . ? Cr3 P7 P8 P9 47.11(5) . . . . ? P6 P7 P8 Cr3 -45.48(5) . . . . ? Cr4 P7 P8 Cr3 -92.50(4) . . . . ? P6 P7 P8 Cr4 47.02(5) . . . . ? Cr3 P7 P8 Cr4 92.50(4) . . . . ? C23 Cr3 P8 P7 -119.66(10) . . . . ? C22 Cr3 P8 P7 -83.81(11) . . . . ? C25 Cr3 P8 P7 -156.2(2) . . . . ? C21 Cr3 P8 P7 -72.00(18) . . . . ? C24 Cr3 P8 P7 -153.54(11) . . . . ? P10 Cr3 P8 P7 90.77(5) . . . . ? P6 Cr3 P8 P7 37.32(5) . . . . ? P9 Cr3 P8 P7 128.85(6) . . . . ? C23 Cr3 P8 P9 111.49(10) . . . . ? C22 Cr3 P8 P9 147.35(11) . . . . ? C25 Cr3 P8 P9 74.9(2) . . . . ? C21 Cr3 P8 P9 159.16(18) . . . . ? C24 Cr3 P8 P9 77.62(11) . . . . ? P10 Cr3 P8 P9 -38.08(5) . . . . ? P6 Cr3 P8 P9 -91.52(5) . . . . ? P7 Cr3 P8 P9 -128.85(6) . . . . ? C23 Cr3 P8 Cr4 175.64(10) . . . . ? C22 Cr3 P8 Cr4 -148.51(10) . . . . ? C25 Cr3 P8 Cr4 139.1(2) . . . . ? C21 Cr3 P8 Cr4 -136.70(18) . . . . ? C24 Cr3 P8 Cr4 141.77(10) . . . . ? P10 Cr3 P8 Cr4 26.07(4) . . . . ? P6 Cr3 P8 Cr4 -27.37(4) . . . . ? P9 Cr3 P8 Cr4 64.15(4) . . . . ? P7 Cr3 P8 Cr4 -64.70(4) . . . . ? P7 P8 P9 P10 -1.50(7) . . . . ? Cr3 P8 P9 P10 45.88(5) . . . . ? Cr4 P8 P9 P10 -47.13(5) . . . . ? P7 P8 P9 Cr4 45.63(5) . . . . ? Cr3 P8 P9 Cr4 93.01(4) . . . . ? P7 P8 P9 Cr3 -47.38(5) . . . . ? Cr4 P8 P9 Cr3 -93.01(4) . . . . ? C23 Cr3 P9 P8 -82.41(11) . . . . ? C22 Cr3 P9 P8 -70.88(18) . . . . ? C25 Cr3 P9 P8 -151.89(11) . . . . ? C21 Cr3 P9 P8 -154.7(2) . . . . ? C24 Cr3 P9 P8 -118.31(11) . . . . ? P10 Cr3 P9 P8 130.02(6) . . . . ? P6 Cr3 P9 P8 91.26(5) . . . . ? P7 Cr3 P9 P8 38.39(5) . . . . ? C23 Cr3 P9 P10 147.56(11) . . . . ? C22 Cr3 P9 P10 159.10(18) . . . . ? C25 Cr3 P9 P10 78.09(11) . . . . ? C21 Cr3 P9 P10 75.3(2) . . . . ? C24 Cr3 P9 P10 111.67(11) . . . . ? P6 Cr3 P9 P10 -38.76(5) . . . . ? P8 Cr3 P9 P10 -130.02(6) . . . . ? P7 Cr3 P9 P10 -91.64(5) . . . . ? C23 Cr3 P9 Cr4 -147.84(11) . . . . ? C22 Cr3 P9 Cr4 -136.31(18) . . . . ? C25 Cr3 P9 Cr4 142.69(11) . . . . ? C21 Cr3 P9 Cr4 139.9(2) . . . . ? C24 Cr3 P9 Cr4 176.27(10) . . . . ? P10 Cr3 P9 Cr4 64.60(4) . . . . ? P6 Cr3 P9 Cr4 25.84(5) . . . . ? P8 Cr3 P9 Cr4 -65.42(4) . . . . ? P7 Cr3 P9 Cr4 -27.04(4) . . . . ? P7 P6 P10 P9 0.21(7) . . . . ? Cr3 P6 P10 P9 -46.96(5) . . . . ? Cr4 P6 P10 P9 46.35(5) . . . . ? P7 P6 P10 Cr3 47.16(5) . . . . ? Cr4 P6 P10 Cr3 93.31(4) . . . . ? P7 P6 P10 Cr4 -46.15(5) . . . . ? Cr3 P6 P10 Cr4 -93.31(4) . . . . ? P8 P9 P10 P6 0.79(7) . . . . ? Cr4 P9 P10 P6 -46.71(5) . . . . ? Cr3 P9 P10 P6 46.91(5) . . . . ? P8 P9 P10 Cr3 -46.12(5) . . . . ? Cr4 P9 P10 Cr3 -93.63(4) . . . . ? P8 P9 P10 Cr4 47.51(5) . . . . ? Cr3 P9 P10 Cr4 93.63(4) . . . . ? C23 Cr3 P10 P6 160.58(19) . . . . ? C22 Cr3 P10 P6 77.2(2) . . . . ? C25 Cr3 P10 P6 112.80(10) . . . . ? C21 Cr3 P10 P6 79.07(11) . . . . ? C24 Cr3 P10 P6 148.98(11) . . . . ? P9 Cr3 P10 P6 -128.82(5) . . . . ? P8 Cr3 P10 P6 -91.01(5) . . . . ? P7 Cr3 P10 P6 -38.12(5) . . . . ? C23 Cr3 P10 P9 -70.61(19) . . . . ? C22 Cr3 P10 P9 -154.0(2) . . . . ? C25 Cr3 P10 P9 -118.38(10) . . . . ? C21 Cr3 P10 P9 -152.12(11) . . . . ? C24 Cr3 P10 P9 -82.21(11) . . . . ? P6 Cr3 P10 P9 128.82(5) . . . . ? P8 Cr3 P10 P9 37.80(5) . . . . ? P7 Cr3 P10 P9 90.69(5) . . . . ? C23 Cr3 P10 Cr4 -134.64(18) . . . . ? C22 Cr3 P10 Cr4 142.0(2) . . . . ? C25 Cr3 P10 Cr4 177.58(10) . . . . ? C21 Cr3 P10 Cr4 143.85(10) . . . . ? C24 Cr3 P10 Cr4 -146.24(10) . . . . ? P6 Cr3 P10 Cr4 64.78(4) . . . . ? P9 Cr3 P10 Cr4 -64.03(4) . . . . ? P8 Cr3 P10 Cr4 -26.23(4) . . . . ? P7 Cr3 P10 Cr4 26.66(4) . . . . ? P8 P9 Cr4 C31 162.84(15) . . . . ? P10 P9 Cr4 C31 -68.31(15) . . . . ? Cr3 P9 Cr4 C31 -132.46(14) . . . . ? P8 P9 Cr4 C32 85.3(3) . . . . ? P10 P9 Cr4 C32 -145.9(3) . . . . ? Cr3 P9 Cr4 C32 150.0(3) . . . . ? P8 P9 Cr4 C33 75.52(11) . . . . ? P10 P9 Cr4 C33 -155.63(11) . . . . ? Cr3 P9 Cr4 C33 140.22(11) . . . . ? P8 P9 Cr4 C34 106.80(11) . . . . ? P10 P9 Cr4 C34 -124.36(11) . . . . ? Cr3 P9 Cr4 C34 171.49(10) . . . . ? P8 P9 Cr4 C35 144.18(10) . . . . ? P10 P9 Cr4 C35 -86.97(10) . . . . ? Cr3 P9 Cr4 C35 -151.12(10) . . . . ? P8 P9 Cr4 P10 -128.85(5) . . . . ? Cr3 P9 Cr4 P10 -64.15(4) . . . . ? P8 P9 Cr4 P7 -37.43(5) . . . . ? P10 P9 Cr4 P7 91.41(5) . . . . ? Cr3 P9 Cr4 P7 27.26(4) . . . . ? P8 P9 Cr4 P6 -90.42(5) . . . . ? P10 P9 Cr4 P6 38.42(5) . . . . ? Cr3 P9 Cr4 P6 -25.73(5) . . . . ? P10 P9 Cr4 P8 128.85(5) . . . . ? Cr3 P9 Cr4 P8 64.70(4) . . . . ? P6 P10 Cr4 C31 -87.26(10) . . . . ? P9 P10 Cr4 C31 143.57(10) . . . . ? Cr3 P10 Cr4 C31 -151.83(10) . . . . ? P6 P10 Cr4 C32 -68.80(15) . . . . ? P9 P10 Cr4 C32 162.02(15) . . . . ? Cr3 P10 Cr4 C32 -133.37(14) . . . . ? P6 P10 Cr4 C33 -143.9(3) . . . . ? P9 P10 Cr4 C33 86.9(3) . . . . ? Cr3 P10 Cr4 C33 151.5(3) . . . . ? P6 P10 Cr4 C34 -155.43(12) . . . . ? P9 P10 Cr4 C34 75.40(12) . . . . ? Cr3 P10 Cr4 C34 140.01(12) . . . . ? P6 P10 Cr4 C35 -124.96(11) . . . . ? P9 P10 Cr4 C35 105.87(10) . . . . ? Cr3 P10 Cr4 C35 170.48(10) . . . . ? P6 P10 Cr4 P9 129.17(5) . . . . ? Cr3 P10 Cr4 P9 64.61(4) . . . . ? P6 P10 Cr4 P7 37.70(5) . . . . ? P9 P10 Cr4 P7 -91.48(5) . . . . ? Cr3 P10 Cr4 P7 -26.87(4) . . . . ? P9 P10 Cr4 P6 -129.17(5) . . . . ? Cr3 P10 Cr4 P6 -64.56(4) . . . . ? P6 P10 Cr4 P8 90.62(5) . . . . ? P9 P10 Cr4 P8 -38.55(5) . . . . ? Cr3 P10 Cr4 P8 26.06(4) . . . . ? P6 P7 Cr4 C31 73.89(11) . . . . ? P8 P7 Cr4 C31 -156.99(11) . . . . ? Cr3 P7 Cr4 C31 138.35(11) . . . . ? P6 P7 Cr4 C32 105.26(10) . . . . ? P8 P7 Cr4 C32 -125.61(10) . . . . ? Cr3 P7 Cr4 C32 169.73(9) . . . . ? P6 P7 Cr4 C33 142.72(10) . . . . ? P8 P7 Cr4 C33 -88.15(10) . . . . ? Cr3 P7 Cr4 C33 -152.81(10) . . . . ? P6 P7 Cr4 C34 160.53(16) . . . . ? P8 P7 Cr4 C34 -70.34(16) . . . . ? Cr3 P7 Cr4 C34 -135.01(16) . . . . ? P6 P7 Cr4 C35 84.0(3) . . . . ? P8 P7 Cr4 C35 -146.9(3) . . . . ? Cr3 P7 Cr4 C35 148.4(3) . . . . ? P6 P7 Cr4 P9 -91.58(5) . . . . ? P8 P7 Cr4 P9 37.55(5) . . . . ? Cr3 P7 Cr4 P9 -27.11(4) . . . . ? P6 P7 Cr4 P10 -37.86(5) . . . . ? P8 P7 Cr4 P10 91.27(5) . . . . ? Cr3 P7 Cr4 P10 26.61(4) . . . . ? P8 P7 Cr4 P6 129.13(6) . . . . ? Cr3 P7 Cr4 P6 64.47(4) . . . . ? P6 P7 Cr4 P8 -129.13(6) . . . . ? Cr3 P7 Cr4 P8 -64.66(4) . . . . ? P7 P6 Cr4 C31 -124.95(11) . . . . ? P10 P6 Cr4 C31 105.01(11) . . . . ? Cr3 P6 Cr4 C31 169.53(10) . . . . ? P7 P6 Cr4 C32 -87.13(11) . . . . ? P10 P6 Cr4 C32 142.83(11) . . . . ? Cr3 P6 Cr4 C32 -152.65(10) . . . . ? P7 P6 Cr4 C33 -69.34(16) . . . . ? P10 P6 Cr4 C33 160.62(16) . . . . ? Cr3 P6 Cr4 C33 -134.86(15) . . . . ? P7 P6 Cr4 C34 -144.9(3) . . . . ? P10 P6 Cr4 C34 85.1(3) . . . . ? Cr3 P6 Cr4 C34 149.6(3) . . . . ? P7 P6 Cr4 C35 -155.82(12) . . . . ? P10 P6 Cr4 C35 74.14(12) . . . . ? Cr3 P6 Cr4 C35 138.66(11) . . . . ? P7 P6 Cr4 P9 91.34(5) . . . . ? P10 P6 Cr4 P9 -38.70(5) . . . . ? Cr3 P6 Cr4 P9 25.82(5) . . . . ? P7 P6 Cr4 P10 130.04(6) . . . . ? Cr3 P6 Cr4 P10 64.52(4) . . . . ? P10 P6 Cr4 P7 -130.04(6) . . . . ? Cr3 P6 Cr4 P7 -65.52(4) . . . . ? P7 P6 Cr4 P8 38.23(5) . . . . ? P10 P6 Cr4 P8 -91.81(5) . . . . ? Cr3 P6 Cr4 P8 -27.29(4) . . . . ? P7 P8 Cr4 C31 82.4(3) . . . . ? P9 P8 Cr4 C31 -147.2(3) . . . . ? Cr3 P8 Cr4 C31 147.9(3) . . . . ? P7 P8 Cr4 C32 73.47(11) . . . . ? P9 P8 Cr4 C32 -156.13(11) . . . . ? Cr3 P8 Cr4 C32 138.97(10) . . . . ? P7 P8 Cr4 C33 105.16(9) . . . . ? P9 P8 Cr4 C33 -124.45(10) . . . . ? Cr3 P8 Cr4 C33 170.66(9) . . . . ? P7 P8 Cr4 C34 142.90(11) . . . . ? P9 P8 Cr4 C34 -86.70(10) . . . . ? Cr3 P8 Cr4 C34 -151.60(10) . . . . ? P7 P8 Cr4 C35 161.62(15) . . . . ? P9 P8 Cr4 C35 -67.98(16) . . . . ? Cr3 P8 Cr4 C35 -132.88(15) . . . . ? P7 P8 Cr4 P9 -130.40(6) . . . . ? Cr3 P8 Cr4 P9 -64.90(4) . . . . ? P7 P8 Cr4 P10 -91.49(5) . . . . ? P9 P8 Cr4 P10 38.90(5) . . . . ? Cr3 P8 Cr4 P10 -26.00(4) . . . . ? P9 P8 Cr4 P7 130.40(6) . . . . ? Cr3 P8 Cr4 P7 65.50(4) . . . . ? P7 P8 Cr4 P6 -38.26(5) . . . . ? P9 P8 Cr4 P6 92.14(5) . . . . ? Cr3 P8 Cr4 P6 27.24(4) . . . . ? C32 Cr4 C31 C35 117.4(3) . . . . ? C33 Cr4 C31 C35 79.8(2) . . . . ? C34 Cr4 C31 C35 37.2(2) . . . . ? P9 Cr4 C31 C35 -29.9(3) . . . . ? P10 Cr4 C31 C35 -81.23(19) . . . . ? P7 Cr4 C31 C35 174.29(16) . . . . ? P6 Cr4 C31 C35 -135.04(18) . . . . ? P8 Cr4 C31 C35 105.1(3) . . . . ? C33 Cr4 C31 C32 -37.58(18) . . . . ? C34 Cr4 C31 C32 -80.2(2) . . . . ? C35 Cr4 C31 C32 -117.4(3) . . . . ? P9 Cr4 C31 C32 -147.24(16) . . . . ? P10 Cr4 C31 C32 161.40(16) . . . . ? P7 Cr4 C31 C32 56.9(2) . . . . ? P6 Cr4 C31 C32 107.59(18) . . . . ? P8 Cr4 C31 C32 -12.2(4) . . . . ? C32 Cr4 C31 C36 -121.1(4) . . . . ? C33 Cr4 C31 C36 -158.6(4) . . . . ? C34 Cr4 C31 C36 158.8(4) . . . . ? C35 Cr4 C31 C36 121.6(4) . . . . ? P9 Cr4 C31 C36 91.7(4) . . . . ? P10 Cr4 C31 C36 40.3(4) . . . . ? P7 Cr4 C31 C36 -64.1(4) . . . . ? P6 Cr4 C31 C36 -13.5(3) . . . . ? P8 Cr4 C31 C36 -133.3(3) . . . . ? C35 C31 C32 C33 -0.4(4) . . . . ? C36 C31 C32 C33 -177.8(3) . . . . ? Cr4 C31 C32 C33 62.1(2) . . . . ? C35 C31 C32 C37 177.6(3) . . . . ? C36 C31 C32 C37 0.2(6) . . . . ? Cr4 C31 C32 C37 -119.9(3) . . . . ? C35 C31 C32 Cr4 -62.5(2) . . . . ? C36 C31 C32 Cr4 120.1(3) . . . . ? C31 Cr4 C32 C33 -117.2(3) . . . . ? C34 Cr4 C32 C33 -37.5(2) . . . . ? C35 Cr4 C32 C33 -79.6(2) . . . . ? P9 Cr4 C32 C33 -13.5(4) . . . . ? P10 Cr4 C32 C33 -146.69(17) . . . . ? P7 Cr4 C32 C33 108.49(19) . . . . ? P6 Cr4 C32 C33 162.04(18) . . . . ? P8 Cr4 C32 C33 58.0(2) . . . . ? C33 Cr4 C32 C31 117.2(3) . . . . ? C34 Cr4 C32 C31 79.7(2) . . . . ? C35 Cr4 C32 C31 37.54(19) . . . . ? P9 Cr4 C32 C31 103.7(3) . . . . ? P10 Cr4 C32 C31 -29.5(3) . . . . ? P7 Cr4 C32 C31 -134.34(18) . . . . ? P6 Cr4 C32 C31 -80.80(19) . . . . ? P8 Cr4 C32 C31 175.17(16) . . . . ? C31 Cr4 C32 C37 121.9(4) . . . . ? C33 Cr4 C32 C37 -121.0(4) . . . . ? C34 Cr4 C32 C37 -158.4(4) . . . . ? C35 Cr4 C32 C37 159.4(4) . . . . ? P9 Cr4 C32 C37 -134.4(3) . . . . ? P10 Cr4 C32 C37 92.3(3) . . . . ? P7 Cr4 C32 C37 -12.5(3) . . . . ? P6 Cr4 C32 C37 41.1(3) . . . . ? P8 Cr4 C32 C37 -63.0(3) . . . . ? C31 C32 C33 C34 0.2(4) . . . . ? C37 C32 C33 C34 -177.8(3) . . . . ? Cr4 C32 C33 C34 62.0(2) . . . . ? C31 C32 C33 C38 177.4(3) . . . . ? C37 C32 C33 C38 -0.7(6) . . . . ? Cr4 C32 C33 C38 -120.8(4) . . . . ? C31 C32 C33 Cr4 -61.8(2) . . . . ? C37 C32 C33 Cr4 120.1(3) . . . . ? C31 Cr4 C33 C32 37.9(2) . . . . ? C34 Cr4 C33 C32 117.6(3) . . . . ? C35 Cr4 C33 C32 80.5(2) . . . . ? P9 Cr4 C33 C32 174.58(17) . . . . ? P10 Cr4 C33 C32 101.6(3) . . . . ? P7 Cr4 C33 C32 -80.1(2) . . . . ? P6 Cr4 C33 C32 -28.6(3) . . . . ? P8 Cr4 C33 C32 -133.83(19) . . . . ? C31 Cr4 C33 C34 -79.7(2) . . . . ? C32 Cr4 C33 C34 -117.6(3) . . . . ? C35 Cr4 C33 C34 -37.1(2) . . . . ? P9 Cr4 C33 C34 57.0(2) . . . . ? P10 Cr4 C33 C34 -16.0(4) . . . . ? P7 Cr4 C33 C34 162.34(18) . . . . ? P6 Cr4 C33 C34 -146.16(18) . . . . ? P8 Cr4 C33 C34 108.6(2) . . . . ? C31 Cr4 C33 C38 160.7(3) . . . . ? C32 Cr4 C33 C38 122.8(4) . . . . ? C34 Cr4 C33 C38 -119.6(4) . . . . ? C35 Cr4 C33 C38 -156.7(3) . . . . ? P9 Cr4 C33 C38 -62.6(3) . . . . ? P10 Cr4 C33 C38 -135.6(3) . . . . ? P7 Cr4 C33 C38 42.8(3) . . . . ? P6 Cr4 C33 C38 94.3(3) . . . . ? P8 Cr4 C33 C38 -11.0(3) . . . . ? C32 C33 C34 C35 0.1(4) . . . . ? C38 C33 C34 C35 -177.1(3) . . . . ? Cr4 C33 C34 C35 62.0(2) . . . . ? C32 C33 C34 C39 176.1(3) . . . . ? C38 C33 C34 C39 -1.1(6) . . . . ? Cr4 C33 C34 C39 -122.0(4) . . . . ? C32 C33 C34 Cr4 -61.9(2) . . . . ? C38 C33 C34 Cr4 120.9(3) . . . . ? C31 Cr4 C34 C35 -37.5(2) . . . . ? C32 Cr4 C34 C35 -80.4(2) . . . . ? C33 Cr4 C34 C35 -117.8(3) . . . . ? P9 Cr4 C34 C35 107.69(19) . . . . ? P10 Cr4 C34 C35 55.7(2) . . . . ? P7 Cr4 C34 C35 -146.22(18) . . . . ? P6 Cr4 C34 C35 -15.2(4) . . . . ? P8 Cr4 C34 C35 161.46(18) . . . . ? C31 Cr4 C34 C33 80.2(2) . . . . ? C32 Cr4 C34 C33 37.4(2) . . . . ? C35 Cr4 C34 C33 117.8(3) . . . . ? P9 Cr4 C34 C33 -134.53(19) . . . . ? P10 Cr4 C34 C33 173.48(17) . . . . ? P7 Cr4 C34 C33 -28.4(3) . . . . ? P6 Cr4 C34 C33 102.5(3) . . . . ? P8 Cr4 C34 C33 -80.8(2) . . . . ? C31 Cr4 C34 C39 -159.2(4) . . . . ? C32 Cr4 C34 C39 158.0(4) . . . . ? C33 Cr4 C34 C39 120.6(4) . . . . ? C35 Cr4 C34 C39 -121.7(4) . . . . ? P9 Cr4 C34 C39 -14.0(3) . . . . ? P10 Cr4 C34 C39 -66.0(4) . . . . ? P7 Cr4 C34 C39 92.1(3) . . . . ? P6 Cr4 C34 C39 -136.9(3) . . . . ? P8 Cr4 C34 C39 39.8(3) . . . . ? C33 C34 C35 C31 -0.4(4) . . . . ? C39 C34 C35 C31 -176.4(3) . . . . ? Cr4 C34 C35 C31 61.3(2) . . . . ? C33 C34 C35 C40 176.5(3) . . . . ? C39 C34 C35 C40 0.6(6) . . . . ? Cr4 C34 C35 C40 -121.7(3) . . . . ? C33 C34 C35 Cr4 -61.7(2) . . . . ? C39 C34 C35 Cr4 122.3(4) . . . . ? C32 C31 C35 C34 0.5(4) . . . . ? C36 C31 C35 C34 177.9(3) . . . . ? Cr4 C31 C35 C34 -61.7(2) . . . . ? C32 C31 C35 C40 -176.4(3) . . . . ? C36 C31 C35 C40 1.0(6) . . . . ? Cr4 C31 C35 C40 121.4(3) . . . . ? C32 C31 C35 Cr4 62.2(2) . . . . ? C36 C31 C35 Cr4 -120.4(3) . . . . ? C31 Cr4 C35 C34 117.6(3) . . . . ? C32 Cr4 C35 C34 79.9(2) . . . . ? C33 Cr4 C35 C34 37.5(2) . . . . ? P9 Cr4 C35 C34 -81.0(2) . . . . ? P10 Cr4 C35 C34 -135.27(19) . . . . ? P7 Cr4 C35 C34 103.7(3) . . . . ? P6 Cr4 C35 C34 173.70(17) . . . . ? P8 Cr4 C35 C34 -30.0(3) . . . . ? C32 Cr4 C35 C31 -37.72(19) . . . . ? C33 Cr4 C35 C31 -80.2(2) . . . . ? C34 Cr4 C35 C31 -117.6(3) . . . . ? P9 Cr4 C35 C31 161.36(17) . . . . ? P10 Cr4 C35 C31 107.08(19) . . . . ? P7 Cr4 C35 C31 -14.0(4) . . . . ? P6 Cr4 C35 C31 56.1(2) . . . . ? P8 Cr4 C35 C31 -147.69(17) . . . . ? C31 Cr4 C35 C40 -121.3(4) . . . . ? C32 Cr4 C35 C40 -159.0(4) . . . . ? C33 Cr4 C35 C40 158.5(4) . . . . ? C34 Cr4 C35 C40 121.0(4) . . . . ? P9 Cr4 C35 C40 40.0(4) . . . . ? P10 Cr4 C35 C40 -14.2(3) . . . . ? P7 Cr4 C35 C40 -135.3(3) . . . . ? P6 Cr4 C35 C40 -65.3(4) . . . . ? P8 Cr4 C35 C40 91.0(4) . . . . ? _diffrn_measured_fraction_theta_max 0.931 _diffrn_reflns_theta_full 30.46 _diffrn_measured_fraction_theta_full 0.931 _refine_diff_density_max 1.535 _refine_diff_density_min -0.628 _refine_diff_density_rms 0.120 #===END data_110k _database_code_depnum_ccdc_archive 'CCDC 618756' _audit_creation_method SHELXL-97 _chemical_name_systematic ; \m~2~-\h^5^,\h^5^-cyclopentaphosphole)-bis ((\h^5^-pentamethyl-cyclopentadienyl)-chromium) hexafluoroantimonate ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H30 Cr2 F6 P5 Sb' _chemical_formula_weight 765.04 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M I2/a loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' _cell_length_a 23.0402(8) _cell_length_b 21.3055(7) _cell_length_c 23.0110(8) _cell_angle_alpha 90.00 _cell_angle_beta 101.3100(10) _cell_angle_gamma 90.00 _cell_volume 11076.3(7) _cell_formula_units_Z 16 _cell_measurement_temperature 110(2) _cell_measurement_reflns_used 9826 _cell_measurement_theta_min 2.62 _cell_measurement_theta_max 30.46 _exptl_crystal_description 'irregular block' _exptl_crystal_colour 'dark green' _exptl_crystal_size_max 0.60 _exptl_crystal_size_mid 0.52 _exptl_crystal_size_min 0.40 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.835 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 6048 _exptl_absorpt_coefficient_mu 2.078 _exptl_absorpt_correction_type integration _exptl_absorpt_correction_T_min 0.389 _exptl_absorpt_correction_T_max 0.609 _exptl_absorpt_process_details 'XPREP in SHELXTL' _exptl_special_details ; ? ; _diffrn_ambient_temperature 110(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'Bede Microsource X-ray Generator' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEX CCD Diffractometer' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number 0 _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% 0 _diffrn_reflns_number 41426 _diffrn_reflns_av_R_equivalents 0.0315 _diffrn_reflns_av_sigmaI/netI 0.0402 _diffrn_reflns_limit_h_min -32 _diffrn_reflns_limit_h_max 32 _diffrn_reflns_limit_k_min -30 _diffrn_reflns_limit_k_max 29 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_limit_l_max 31 _diffrn_reflns_theta_min 1.14 _diffrn_reflns_theta_max 30.47 _reflns_number_total 15598 _reflns_number_gt 14579 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'SMART V5.625 (Bruker, 2003)' _computing_cell_refinement 'SMART V5.625 (Bruker, 2003)' _computing_data_reduction 'SAINT V6.28A (Bruker, 2003)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'SHELXTL V6.12(Bruker, 2001)' _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0396P)^2^+12.1951P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 15598 _refine_ls_number_parameters 614 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0324 _refine_ls_R_factor_gt 0.0290 _refine_ls_wR_factor_ref 0.0810 _refine_ls_wR_factor_gt 0.0751 _refine_ls_goodness_of_fit_ref 1.044 _refine_ls_restrained_S_all 1.044 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb1 Sb 0.138492(10) 0.870055(10) 0.384051(10) 0.02367(5) Uani 1 1 d . . . F1 F 0.09711(11) 0.80977(11) 0.33255(12) 0.0483(6) Uani 1 1 d . . . F2 F 0.09080(13) 0.93239(11) 0.34182(11) 0.0506(7) Uani 1 1 d . . . F3 F 0.08403(11) 0.86224(12) 0.43448(12) 0.0433(5) Uani 1 1 d . . . F4 F 0.18430(9) 0.80682(9) 0.42719(11) 0.0348(5) Uani 1 1 d . . . F5 F 0.19396(12) 0.87754(11) 0.33470(11) 0.0425(6) Uani 1 1 d . . . F6 F 0.17992(12) 0.93113(10) 0.43391(10) 0.0399(5) Uani 1 1 d . . . Sb2 Sb 0.137117(10) 0.126702(10) 0.117247(10) 0.02177(4) Uani 1 1 d . . . F7 F 0.12511(17) 0.05275(13) 0.15480(15) 0.0787(11) Uani 1 1 d . . . F8 F 0.07522(11) 0.16466(15) 0.14521(13) 0.0579(7) Uani 1 1 d . . . F9 F 0.08458(11) 0.10002(13) 0.04916(11) 0.0478(6) Uani 1 1 d . . . F10 F 0.20088(12) 0.09206(14) 0.08853(13) 0.0586(8) Uani 1 1 d . . . F11 F 0.18966(11) 0.15299(13) 0.18501(11) 0.0485(6) Uani 1 1 d . . . F12 F 0.14943(12) 0.20151(12) 0.07964(12) 0.0520(7) Uani 1 1 d . . . C1 C -0.11533(14) 0.31185(14) 0.44728(14) 0.0211(6) Uani 1 1 d . . . C2 C -0.14379(13) 0.26958(13) 0.40218(14) 0.0204(5) Uani 1 1 d . . . C3 C -0.14287(12) 0.29713(14) 0.34607(14) 0.0196(5) Uani 1 1 d . . . C4 C -0.11349(13) 0.35669(13) 0.35572(13) 0.0195(5) Uani 1 1 d . . . C5 C -0.09680(13) 0.36577(14) 0.41815(13) 0.0189(5) Uani 1 1 d . . . C6 C -0.10910(17) 0.30394(17) 0.51196(14) 0.0299(7) Uani 1 1 d . . . H6A H -0.1419 0.3252 0.5253 0.045 Uiso 1 1 calc R . . H6B H -0.0715 0.3222 0.5321 0.045 Uiso 1 1 calc R . . H6C H -0.1098 0.2591 0.5215 0.045 Uiso 1 1 calc R . . C7 C -0.17256(14) 0.20887(14) 0.41311(17) 0.0277(7) Uani 1 1 d . . . H7A H -0.2144 0.2163 0.4140 0.042 Uiso 1 1 calc R . . H7B H -0.1526 0.1914 0.4512 0.042 Uiso 1 1 calc R . . H7C H -0.1695 0.1792 0.3813 0.042 Uiso 1 1 calc R . . C8 C -0.16972(14) 0.27082(15) 0.28637(14) 0.0258(6) Uani 1 1 d . . . H8A H -0.2059 0.2941 0.2698 0.039 Uiso 1 1 calc R . . H8B H -0.1794 0.2265 0.2905 0.039 Uiso 1 1 calc R . . H8C H -0.1414 0.2747 0.2599 0.039 Uiso 1 1 calc R . . C9 C -0.10514(15) 0.40280(15) 0.30883(15) 0.0250(6) Uani 1 1 d . . . H9A H -0.1420 0.4262 0.2955 0.038 Uiso 1 1 calc R . . H9B H -0.0947 0.3803 0.2752 0.038 Uiso 1 1 calc R . . H9C H -0.0733 0.4321 0.3251 0.038 Uiso 1 1 calc R . . C10 C -0.06894(15) 0.42332(15) 0.44928(15) 0.0257(6) Uani 1 1 d . . . H10A H -0.0984 0.4461 0.4666 0.039 Uiso 1 1 calc R . . H10B H -0.0544 0.4505 0.4208 0.039 Uiso 1 1 calc R . . H10C H -0.0358 0.4110 0.4808 0.039 Uiso 1 1 calc R . . Cr1 Cr -0.05122(2) 0.28135(2) 0.39275(2) 0.01607(9) Uani 1 1 d . . . P1 P 0.03297(5) 0.26747(7) 0.47154(5) 0.0527(4) Uani 1 1 d . . . P2 P -0.01526(5) 0.18257(5) 0.43531(7) 0.0496(3) Uani 1 1 d . . . P3 P -0.03305(4) 0.18951(5) 0.33885(6) 0.0474(3) Uani 1 1 d . . . P4 P 0.00302(5) 0.27886(7) 0.31392(5) 0.0474(3) Uani 1 1 d . . . P5 P 0.04401(4) 0.32693(4) 0.39622(7) 0.0488(3) Uani 1 1 d . . . Cr2 Cr 0.06435(2) 0.21739(2) 0.38960(2) 0.01590(9) Uani 1 1 d . . . C11 C 0.14747(13) 0.17735(13) 0.44092(13) 0.0177(5) Uani 1 1 d . . . C12 C 0.11735(13) 0.12989(13) 0.40275(14) 0.0194(5) Uani 1 1 d . . . C13 C 0.11282(13) 0.15042(14) 0.34302(13) 0.0204(5) Uani 1 1 d . . . C14 C 0.14037(13) 0.21052(14) 0.34399(14) 0.0204(5) Uani 1 1 d . . . C15 C 0.16168(13) 0.22760(13) 0.40479(13) 0.0187(5) Uani 1 1 d . . . C16 C 0.16411(15) 0.17253(15) 0.50651(14) 0.0256(6) Uani 1 1 d . . . H16A H 0.2011 0.1489 0.5174 0.038 Uiso 1 1 calc R . . H16B H 0.1327 0.1508 0.5217 0.038 Uiso 1 1 calc R . . H16C H 0.1695 0.2147 0.5237 0.038 Uiso 1 1 calc R . . C17 C 0.09664(15) 0.06801(14) 0.42201(17) 0.0293(7) Uani 1 1 d . . . H17A H 0.1295 0.0380 0.4280 0.044 Uiso 1 1 calc R . . H17B H 0.0643 0.0521 0.3914 0.044 Uiso 1 1 calc R . . H17C H 0.0826 0.0735 0.4592 0.044 Uiso 1 1 calc R . . C18 C 0.08825(15) 0.11335(16) 0.28801(16) 0.0303(7) Uani 1 1 d . . . H18A H 0.1200 0.0886 0.2764 0.045 Uiso 1 1 calc R . . H18B H 0.0716 0.1422 0.2558 0.045 Uiso 1 1 calc R . . H18C H 0.0571 0.0851 0.2960 0.045 Uiso 1 1 calc R . . C19 C 0.14828(14) 0.24786(16) 0.29127(15) 0.0279(7) Uani 1 1 d . . . H19A H 0.1890 0.2430 0.2852 0.042 Uiso 1 1 calc R . . H19B H 0.1405 0.2922 0.2979 0.042 Uiso 1 1 calc R . . H19C H 0.1206 0.2328 0.2561 0.042 Uiso 1 1 calc R . . C20 C 0.19575(13) 0.28576(14) 0.42595(16) 0.0245(6) Uani 1 1 d . . . H20A H 0.2375 0.2798 0.4238 0.037 Uiso 1 1 calc R . . H20B H 0.1925 0.2943 0.4670 0.037 Uiso 1 1 calc R . . H20C H 0.1796 0.3213 0.4008 0.037 Uiso 1 1 calc R . . C21 C 0.10715(13) 0.38555(13) 0.13250(13) 0.0178(5) Uani 1 1 d . . . C22 C 0.17067(13) 0.38243(13) 0.14568(14) 0.0187(6) Uani 1 1 d . . . C23 C 0.19328(13) 0.43805(14) 0.12439(14) 0.0213(6) Uani 1 1 d . . . C24 C 0.14463(15) 0.47608(13) 0.09727(13) 0.0217(6) Uani 1 1 d . . . C25 C 0.09157(13) 0.44377(14) 0.10267(13) 0.0192(5) Uani 1 1 d . . . C26 C 0.06476(14) 0.33553(15) 0.14260(15) 0.0251(6) Uani 1 1 d . . . H26A H 0.0672 0.3001 0.1161 0.038 Uiso 1 1 calc R . . H26B H 0.0244 0.3524 0.1345 0.038 Uiso 1 1 calc R . . H26C H 0.0748 0.3213 0.1839 0.038 Uiso 1 1 calc R . . C27 C 0.20726(14) 0.32795(14) 0.17345(15) 0.0257(6) Uani 1 1 d . . . H27A H 0.2266 0.3080 0.1439 0.038 Uiso 1 1 calc R . . H27B H 0.1817 0.2974 0.1879 0.038 Uiso 1 1 calc R . . H27C H 0.2374 0.3429 0.2067 0.038 Uiso 1 1 calc R . . C28 C 0.25764(15) 0.45143(18) 0.12585(18) 0.0332(8) Uani 1 1 d . . . H28A H 0.2684 0.4364 0.0891 0.050 Uiso 1 1 calc R . . H28B H 0.2818 0.4298 0.1597 0.050 Uiso 1 1 calc R . . H28C H 0.2647 0.4967 0.1297 0.050 Uiso 1 1 calc R . . C29 C 0.14919(18) 0.53745(15) 0.06638(15) 0.0300(7) Uani 1 1 d . . . H29A H 0.1516 0.5296 0.0250 0.045 Uiso 1 1 calc R . . H29B H 0.1848 0.5598 0.0862 0.045 Uiso 1 1 calc R . . H29C H 0.1142 0.5630 0.0679 0.045 Uiso 1 1 calc R . . C30 C 0.02925(14) 0.46500(16) 0.07753(14) 0.0271(7) Uani 1 1 d . . . H30A H 0.0162 0.4469 0.0380 0.041 Uiso 1 1 calc R . . H30B H 0.0282 0.5109 0.0748 0.041 Uiso 1 1 calc R . . H30C H 0.0028 0.4510 0.1035 0.041 Uiso 1 1 calc R . . Cr3 Cr 0.14253(2) 0.46394(2) 0.19216(2) 0.01596(9) Uani 1 1 d . . . P6 P 0.08560(4) 0.44372(4) 0.26871(4) 0.02791(17) Uani 1 1 d . . . P7 P 0.18102(4) 0.42968(4) 0.29445(4) 0.02821(17) Uani 1 1 d . . . P8 P 0.22515(4) 0.50938(5) 0.26221(4) 0.02913(18) Uani 1 1 d . . . P9 P 0.15681(4) 0.57444(4) 0.21908(4) 0.02740(17) Uani 1 1 d . . . P10 P 0.07012(4) 0.53330(4) 0.22231(4) 0.02722(18) Uani 1 1 d . . . Cr4 Cr 0.14410(2) 0.53331(2) 0.31384(2) 0.01539(8) Uani 1 1 d . . . C31 C 0.09565(12) 0.55113(14) 0.38528(13) 0.0194(5) Uani 1 1 d . . . C32 C 0.15188(13) 0.52371(13) 0.41036(12) 0.0190(5) Uani 1 1 d . . . C33 C 0.19656(13) 0.56576(13) 0.39923(13) 0.0180(5) Uani 1 1 d . . . C34 C 0.16841(14) 0.61862(12) 0.36763(14) 0.0190(5) Uani 1 1 d . . . C35 C 0.10582(13) 0.60993(13) 0.35926(13) 0.0194(5) Uani 1 1 d . . . C36 C 0.03625(15) 0.52404(17) 0.38823(15) 0.0294(7) Uani 1 1 d . . . H36A H 0.0202 0.5453 0.4194 0.044 Uiso 1 1 calc R . . H36B H 0.0404 0.4791 0.3972 0.044 Uiso 1 1 calc R . . H36C H 0.0093 0.5300 0.3500 0.044 Uiso 1 1 calc R . . C37 C 0.16205(15) 0.46307(14) 0.44403(14) 0.0249(6) Uani 1 1 d . . . H37A H 0.1651 0.4713 0.4864 0.037 Uiso 1 1 calc R . . H37B H 0.1988 0.4438 0.4375 0.037 Uiso 1 1 calc R . . H37C H 0.1289 0.4345 0.4302 0.037 Uiso 1 1 calc R . . C38 C 0.26247(13) 0.55845(16) 0.41901(15) 0.0256(6) Uani 1 1 d . . . H38A H 0.2748 0.5762 0.4588 0.038 Uiso 1 1 calc R . . H38B H 0.2827 0.5806 0.3913 0.038 Uiso 1 1 calc R . . H38C H 0.2728 0.5138 0.4198 0.038 Uiso 1 1 calc R . . C39 C 0.19934(16) 0.67549(14) 0.35058(15) 0.0278(6) Uani 1 1 d . . . H39A H 0.2072 0.7048 0.3840 0.042 Uiso 1 1 calc R . . H39B H 0.1742 0.6960 0.3166 0.042 Uiso 1 1 calc R . . H39C H 0.2368 0.6630 0.3400 0.042 Uiso 1 1 calc R . . C40 C 0.05963(15) 0.65604(16) 0.33098(15) 0.0292(7) Uani 1 1 d . . . H40A H 0.0503 0.6845 0.3613 0.044 Uiso 1 1 calc R . . H40B H 0.0238 0.6334 0.3123 0.044 Uiso 1 1 calc R . . H40C H 0.0747 0.6803 0.3009 0.044 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.02682(11) 0.01985(8) 0.02567(11) -0.00239(8) 0.00838(7) 0.00239(8) F1 0.0436(14) 0.0425(13) 0.0548(16) -0.0183(11) 0.0000(11) -0.0062(11) F2 0.0754(19) 0.0371(11) 0.0368(13) 0.0054(10) 0.0047(12) 0.0239(12) F3 0.0331(12) 0.0546(13) 0.0484(14) 0.0082(12) 0.0233(10) 0.0106(11) F4 0.0286(10) 0.0298(10) 0.0478(13) 0.0084(9) 0.0120(9) 0.0101(8) F5 0.0476(14) 0.0533(15) 0.0325(12) -0.0042(10) 0.0223(11) -0.0065(11) F6 0.0593(15) 0.0297(10) 0.0314(11) -0.0092(9) 0.0108(10) -0.0098(10) Sb2 0.02400(11) 0.01925(8) 0.02269(11) -0.00005(7) 0.00610(6) 0.00097(7) F7 0.125(3) 0.0374(14) 0.066(2) 0.0257(14) 0.0013(19) -0.0210(17) F8 0.0375(13) 0.083(2) 0.0592(17) -0.0132(15) 0.0238(12) 0.0094(13) F9 0.0422(14) 0.0552(14) 0.0409(13) -0.0115(11) -0.0042(10) -0.0084(11) F10 0.0437(14) 0.0744(19) 0.0573(17) -0.0294(14) 0.0091(12) 0.0220(13) F11 0.0417(13) 0.0615(16) 0.0367(13) -0.0206(11) -0.0059(10) 0.0066(11) F12 0.0538(15) 0.0414(13) 0.0584(16) 0.0232(12) 0.0050(12) -0.0116(11) C1 0.0229(14) 0.0195(12) 0.0224(14) -0.0053(11) 0.0082(11) -0.0037(11) C2 0.0157(12) 0.0196(12) 0.0267(15) -0.0043(11) 0.0062(10) -0.0026(10) C3 0.0124(12) 0.0220(13) 0.0239(14) -0.0042(11) 0.0019(10) -0.0020(10) C4 0.0170(13) 0.0189(12) 0.0230(14) -0.0003(11) 0.0049(10) 0.0009(10) C5 0.0185(13) 0.0180(12) 0.0211(13) -0.0034(11) 0.0061(10) -0.0002(10) C6 0.0389(18) 0.0327(16) 0.0204(15) -0.0013(12) 0.0117(13) -0.0020(14) C7 0.0205(14) 0.0218(13) 0.0430(19) -0.0022(13) 0.0117(13) -0.0057(11) C8 0.0205(13) 0.0306(15) 0.0245(15) -0.0089(12) 0.0001(11) -0.0015(12) C9 0.0276(15) 0.0224(14) 0.0261(15) 0.0050(12) 0.0077(12) 0.0011(12) C10 0.0273(15) 0.0237(14) 0.0265(15) -0.0077(12) 0.0063(12) -0.0064(12) Cr1 0.0161(2) 0.01577(19) 0.0166(2) -0.00198(16) 0.00388(16) -0.00359(16) P1 0.0324(5) 0.0936(9) 0.0270(5) -0.0244(5) -0.0069(4) 0.0333(6) P2 0.0339(5) 0.0398(5) 0.0859(9) 0.0350(6) 0.0381(6) 0.0184(4) P3 0.0169(4) 0.0485(6) 0.0724(8) -0.0417(6) -0.0023(4) 0.0037(4) P4 0.0343(5) 0.0781(8) 0.0352(5) 0.0267(5) 0.0204(4) 0.0328(5) P5 0.0176(4) 0.0196(4) 0.1115(11) -0.0107(5) 0.0182(5) -0.0028(3) Cr2 0.0155(2) 0.01525(19) 0.0172(2) -0.00079(16) 0.00382(15) -0.00245(16) C11 0.0171(12) 0.0170(12) 0.0196(13) 0.0042(10) 0.0048(10) 0.0019(10) C12 0.0167(12) 0.0153(11) 0.0277(15) -0.0017(11) 0.0084(11) 0.0007(10) C13 0.0182(12) 0.0218(12) 0.0217(13) -0.0013(10) 0.0053(10) 0.0017(10) C14 0.0159(12) 0.0230(13) 0.0234(14) -0.0001(11) 0.0062(10) 0.0021(10) C15 0.0169(12) 0.0181(11) 0.0210(13) 0.0029(10) 0.0034(10) 0.0008(10) C16 0.0278(15) 0.0297(15) 0.0190(13) 0.0035(11) 0.0038(11) 0.0090(12) C17 0.0288(16) 0.0166(12) 0.047(2) 0.0019(13) 0.0189(14) -0.0017(12) C18 0.0228(15) 0.0348(17) 0.0327(17) -0.0141(14) 0.0040(13) -0.0004(12) C19 0.0273(15) 0.0350(16) 0.0239(15) 0.0112(13) 0.0109(12) 0.0081(13) C20 0.0172(13) 0.0184(13) 0.0369(17) 0.0020(11) 0.0026(11) -0.0025(10) C21 0.0158(12) 0.0177(11) 0.0198(13) -0.0015(10) 0.0030(10) -0.0016(10) C22 0.0182(13) 0.0187(13) 0.0191(13) -0.0011(10) 0.0035(10) 0.0036(10) C23 0.0177(13) 0.0219(13) 0.0259(14) -0.0027(11) 0.0080(11) 0.0005(11) C24 0.0300(15) 0.0205(12) 0.0161(13) 0.0011(10) 0.0087(11) 0.0011(11) C25 0.0201(13) 0.0189(12) 0.0187(13) 0.0001(10) 0.0040(10) 0.0033(10) C26 0.0261(15) 0.0233(14) 0.0267(15) -0.0002(12) 0.0068(12) -0.0072(12) C27 0.0260(15) 0.0225(13) 0.0275(15) 0.0012(12) 0.0027(12) 0.0103(12) C28 0.0219(15) 0.0378(18) 0.045(2) -0.0084(16) 0.0201(14) -0.0030(13) C29 0.049(2) 0.0200(14) 0.0244(15) 0.0042(11) 0.0154(14) -0.0012(13) C30 0.0243(15) 0.0338(16) 0.0213(14) 0.0056(12) 0.0000(11) 0.0101(12) Cr3 0.0144(2) 0.01539(19) 0.0187(2) 0.00181(16) 0.00477(16) 0.00153(15) P6 0.0313(4) 0.0290(4) 0.0273(4) -0.0088(3) 0.0151(3) -0.0137(3) P7 0.0415(5) 0.0213(3) 0.0207(4) 0.0016(3) 0.0032(3) 0.0108(3) P8 0.0173(3) 0.0412(5) 0.0297(4) -0.0109(4) 0.0067(3) -0.0039(3) P9 0.0458(5) 0.0173(3) 0.0214(4) 0.0003(3) 0.0122(3) -0.0053(3) P10 0.0215(4) 0.0346(4) 0.0234(4) -0.0072(3) -0.0011(3) 0.0121(3) Cr4 0.0147(2) 0.01519(19) 0.0164(2) 0.00067(15) 0.00341(15) -0.00045(15) C31 0.0152(12) 0.0246(13) 0.0199(13) -0.0043(11) 0.0067(10) -0.0059(10) C32 0.0239(14) 0.0184(11) 0.0147(12) 0.0007(10) 0.0041(10) -0.0041(10) C33 0.0167(12) 0.0181(12) 0.0189(13) -0.0008(10) 0.0031(10) -0.0014(10) C34 0.0238(14) 0.0157(12) 0.0186(13) -0.0013(9) 0.0066(10) -0.0035(10) C35 0.0207(13) 0.0202(11) 0.0171(13) -0.0032(10) 0.0027(10) 0.0018(10) C36 0.0242(15) 0.0391(18) 0.0272(16) -0.0083(13) 0.0107(12) -0.0091(13) C37 0.0355(17) 0.0198(13) 0.0188(13) 0.0047(11) 0.0039(12) -0.0042(12) C38 0.0174(13) 0.0303(15) 0.0275(15) -0.0011(12) 0.0005(11) -0.0015(11) C39 0.0379(18) 0.0191(13) 0.0265(15) 0.0008(11) 0.0065(13) -0.0061(12) C40 0.0284(16) 0.0312(16) 0.0247(15) -0.0035(12) -0.0031(12) 0.0129(13) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb1 F6 1.868(2) . ? Sb1 F2 1.870(2) . ? Sb1 F4 1.872(2) . ? Sb1 F5 1.876(2) . ? Sb1 F3 1.876(2) . ? Sb1 F1 1.876(2) . ? Sb2 F7 1.844(3) . ? Sb2 F8 1.861(2) . ? Sb2 F12 1.862(2) . ? Sb2 F11 1.863(2) . ? Sb2 F9 1.871(2) . ? Sb2 F10 1.876(2) . ? C1 C2 1.432(4) . ? C1 C5 1.436(4) . ? C1 C6 1.477(4) . ? C1 Cr1 2.215(3) . ? C2 C3 1.422(4) . ? C2 C7 1.497(4) . ? C2 Cr1 2.200(3) . ? C3 C4 1.435(4) . ? C3 C8 1.500(4) . ? C3 Cr1 2.199(3) . ? C4 C5 1.425(4) . ? C4 C9 1.499(4) . ? C4 Cr1 2.209(3) . ? C5 C10 1.499(4) . ? C5 Cr1 2.218(3) . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? Cr1 P5 2.3864(10) . ? Cr1 P4 2.3967(11) . ? Cr1 P3 2.3971(10) . ? Cr1 P2 2.3993(11) . ? Cr1 P1 2.3996(10) . ? P1 P2 2.200(2) . ? P1 P5 2.201(2) . ? P1 Cr2 2.3982(11) . ? P2 P3 2.182(2) . ? P2 Cr2 2.4039(11) . ? P3 P4 2.1977(19) . ? P3 Cr2 2.3925(10) . ? P4 P5 2.197(2) . ? P4 Cr2 2.4039(10) . ? P5 Cr2 2.3913(10) . ? Cr2 C15 2.211(3) . ? Cr2 C13 2.214(3) . ? Cr2 C11 2.214(3) . ? Cr2 C12 2.216(3) . ? Cr2 C14 2.216(3) . ? C11 C12 1.427(4) . ? C11 C15 1.432(4) . ? C11 C16 1.486(4) . ? C12 C13 1.427(4) . ? C12 C17 1.498(4) . ? C13 C14 1.427(4) . ? C13 C18 1.505(4) . ? C14 C15 1.436(4) . ? C14 C19 1.492(4) . ? C15 C20 1.496(4) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 C25 1.429(4) . ? C21 C22 1.437(4) . ? C21 C26 1.494(4) . ? C21 Cr3 2.214(3) . ? C22 C23 1.420(4) . ? C22 C27 1.502(4) . ? C22 Cr3 2.203(3) . ? C23 C24 1.424(4) . ? C23 C28 1.504(4) . ? C23 Cr3 2.195(3) . ? C24 C25 1.430(4) . ? C24 C29 1.502(4) . ? C24 Cr3 2.209(3) . ? C25 C30 1.508(4) . ? C25 Cr3 2.204(3) . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C27 H27C 0.9800 . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? Cr3 P10 2.4295(9) . ? Cr3 P6 2.4323(9) . ? Cr3 P9 2.4402(9) . ? Cr3 P8 2.4404(9) . ? Cr3 P7 2.4578(9) . ? P6 P10 2.1819(13) . ? P6 P7 2.1826(13) . ? P6 Cr4 2.4473(9) . ? P7 P8 2.1826(13) . ? P7 Cr4 2.4387(9) . ? P8 P9 2.1846(13) . ? P8 Cr4 2.4555(9) . ? P9 P10 2.1959(13) . ? P9 Cr4 2.4206(9) . ? P10 Cr4 2.4360(9) . ? Cr4 C31 2.194(3) . ? Cr4 C32 2.202(3) . ? Cr4 C33 2.206(3) . ? Cr4 C34 2.208(3) . ? Cr4 C35 2.213(3) . ? C31 C35 1.428(4) . ? C31 C32 1.435(4) . ? C31 C36 1.499(4) . ? C32 C33 1.425(4) . ? C32 C37 1.501(4) . ? C33 C34 1.426(4) . ? C33 C38 1.505(4) . ? C34 C35 1.429(4) . ? C34 C39 1.496(4) . ? C35 C40 1.500(4) . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C39 H39A 0.9800 . ? C39 H39B 0.9800 . ? C39 H39C 0.9800 . ? C40 H40A 0.9800 . ? C40 H40B 0.9800 . ? C40 H40C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F6 Sb1 F2 90.10(11) . . ? F6 Sb1 F4 90.49(9) . . ? F2 Sb1 F4 178.32(12) . . ? F6 Sb1 F5 89.19(11) . . ? F2 Sb1 F5 91.46(13) . . ? F4 Sb1 F5 90.12(11) . . ? F6 Sb1 F3 90.30(12) . . ? F2 Sb1 F3 89.34(12) . . ? F4 Sb1 F3 89.09(10) . . ? F5 Sb1 F3 179.05(11) . . ? F6 Sb1 F1 178.75(12) . . ? F2 Sb1 F1 89.08(11) . . ? F4 Sb1 F1 90.35(11) . . ? F5 Sb1 F1 89.88(12) . . ? F3 Sb1 F1 90.64(12) . . ? F7 Sb2 F8 90.78(17) . . ? F7 Sb2 F12 179.75(16) . . ? F8 Sb2 F12 89.18(14) . . ? F7 Sb2 F11 89.85(14) . . ? F8 Sb2 F11 89.78(12) . . ? F12 Sb2 F11 89.91(12) . . ? F7 Sb2 F9 90.05(14) . . ? F8 Sb2 F9 90.45(12) . . ? F12 Sb2 F9 90.19(12) . . ? F11 Sb2 F9 179.75(13) . . ? F7 Sb2 F10 91.65(17) . . ? F8 Sb2 F10 177.40(14) . . ? F12 Sb2 F10 88.39(14) . . ? F11 Sb2 F10 89.30(11) . . ? F9 Sb2 F10 90.47(12) . . ? C2 C1 C5 107.5(3) . . ? C2 C1 C6 126.8(3) . . ? C5 C1 C6 125.6(3) . . ? C2 C1 Cr1 70.52(17) . . ? C5 C1 Cr1 71.22(17) . . ? C6 C1 Cr1 126.4(2) . . ? C3 C2 C1 108.2(3) . . ? C3 C2 C7 126.5(3) . . ? C1 C2 C7 125.2(3) . . ? C3 C2 Cr1 71.10(16) . . ? C1 C2 Cr1 71.63(17) . . ? C7 C2 Cr1 125.8(2) . . ? C2 C3 C4 108.4(3) . . ? C2 C3 C8 126.9(3) . . ? C4 C3 C8 124.7(3) . . ? C2 C3 Cr1 71.17(16) . . ? C4 C3 Cr1 71.40(16) . . ? C8 C3 Cr1 125.0(2) . . ? C5 C4 C3 107.6(3) . . ? C5 C4 C9 126.1(3) . . ? C3 C4 C9 126.2(3) . . ? C5 C4 Cr1 71.55(17) . . ? C3 C4 Cr1 70.62(16) . . ? C9 C4 Cr1 126.0(2) . . ? C4 C5 C1 108.4(3) . . ? C4 C5 C10 126.7(3) . . ? C1 C5 C10 124.7(3) . . ? C4 C5 Cr1 70.88(16) . . ? C1 C5 Cr1 70.96(17) . . ? C10 C5 Cr1 127.5(2) . . ? C1 C6 H6A 109.5 . . ? C1 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C1 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C3 Cr1 C2 37.73(12) . . ? C3 Cr1 C4 37.99(10) . . ? C2 Cr1 C4 63.39(11) . . ? C3 Cr1 C1 63.17(11) . . ? C2 Cr1 C1 37.85(10) . . ? C4 Cr1 C1 63.29(11) . . ? C3 Cr1 C5 62.99(11) . . ? C2 Cr1 C5 63.14(11) . . ? C4 Cr1 C5 37.56(11) . . ? C1 Cr1 C5 37.82(11) . . ? C3 Cr1 P5 137.95(9) . . ? C2 Cr1 P5 161.05(8) . . ? C4 Cr1 P5 103.91(8) . . ? C1 Cr1 P5 124.93(8) . . ? C5 Cr1 P5 98.10(8) . . ? C3 Cr1 P4 103.12(9) . . ? C2 Cr1 P4 137.02(9) . . ? C4 Cr1 P4 96.88(8) . . ? C1 Cr1 P4 160.04(9) . . ? C5 Cr1 P4 124.16(9) . . ? P5 Cr1 P4 54.68(5) . . ? C3 Cr1 P3 96.92(8) . . ? C2 Cr1 P3 103.25(8) . . ? C4 Cr1 P3 124.03(8) . . ? C1 Cr1 P3 137.41(8) . . ? C5 Cr1 P3 159.72(8) . . ? P5 Cr1 P3 95.55(4) . . ? P4 Cr1 P3 54.57(5) . . ? C3 Cr1 P2 123.72(9) . . ? C2 Cr1 P2 97.10(8) . . ? C4 Cr1 P2 160.19(8) . . ? C1 Cr1 P2 103.97(9) . . ? C5 Cr1 P2 138.35(9) . . ? P5 Cr1 P2 95.84(4) . . ? P4 Cr1 P2 95.73(4) . . ? P3 Cr1 P2 54.11(5) . . ? C3 Cr1 P1 160.81(9) . . ? C2 Cr1 P1 124.55(9) . . ? C4 Cr1 P1 138.46(8) . . ? C1 Cr1 P1 97.95(9) . . ? C5 Cr1 P1 104.79(8) . . ? P5 Cr1 P1 54.77(5) . . ? P4 Cr1 P1 96.02(4) . . ? P3 Cr1 P1 95.33(4) . . ? P2 Cr1 P1 54.57(5) . . ? P2 P1 P5 107.62(6) . . ? P2 P1 Cr2 62.87(4) . . ? P5 P1 Cr2 62.48(4) . . ? P2 P1 Cr1 62.71(4) . . ? P5 P1 Cr1 62.31(4) . . ? Cr2 P1 Cr1 77.56(3) . . ? P3 P2 P1 108.05(6) . . ? P3 P2 Cr1 62.89(4) . . ? P1 P2 Cr1 62.72(4) . . ? P3 P2 Cr2 62.68(4) . . ? P1 P2 Cr2 62.61(4) . . ? Cr1 P2 Cr2 77.45(3) . . ? P2 P3 P4 108.61(6) . . ? P2 P3 Cr2 63.21(4) . . ? P4 P3 Cr2 62.99(4) . . ? P2 P3 Cr1 62.99(4) . . ? P4 P3 Cr1 62.70(4) . . ? Cr2 P3 Cr1 77.71(3) . . ? P5 P4 P3 107.43(6) . . ? P5 P4 Cr1 62.42(4) . . ? P3 P4 Cr1 62.72(4) . . ? P5 P4 Cr2 62.44(4) . . ? P3 P4 Cr2 62.47(4) . . ? Cr1 P4 Cr2 77.50(3) . . ? P4 P5 P1 108.29(6) . . ? P4 P5 Cr1 62.90(4) . . ? P1 P5 Cr1 62.92(4) . . ? P4 P5 Cr2 63.03(4) . . ? P1 P5 Cr2 62.80(4) . . ? Cr1 P5 Cr2 77.94(3) . . ? C15 Cr2 C13 63.12(11) . . ? C15 Cr2 C11 37.76(10) . . ? C13 Cr2 C11 62.89(11) . . ? C15 Cr2 C12 63.05(10) . . ? C13 Cr2 C12 37.57(11) . . ? C11 Cr2 C12 37.58(11) . . ? C15 Cr2 C14 37.84(11) . . ? C13 Cr2 C14 37.59(11) . . ? C11 Cr2 C14 62.99(11) . . ? C12 Cr2 C14 62.85(11) . . ? C15 Cr2 P5 95.69(8) . . ? C13 Cr2 P5 141.60(9) . . ? C11 Cr2 P5 120.12(8) . . ? C12 Cr2 P5 157.19(8) . . ? C14 Cr2 P5 106.12(8) . . ? C15 Cr2 P3 157.90(9) . . ? C13 Cr2 P3 96.76(8) . . ? C11 Cr2 P3 142.66(8) . . ? C12 Cr2 P3 107.27(8) . . ? C14 Cr2 P3 120.35(9) . . ? P5 Cr2 P3 95.54(4) . . ? C15 Cr2 P1 106.53(9) . . ? C13 Cr2 P1 157.80(9) . . ? C11 Cr2 P1 96.58(8) . . ? C12 Cr2 P1 120.65(9) . . ? C14 Cr2 P1 142.17(9) . . ? P5 Cr2 P1 54.73(5) . . ? P3 Cr2 P1 95.49(4) . . ? C15 Cr2 P2 142.97(9) . . ? C13 Cr2 P2 120.91(8) . . ? C11 Cr2 P2 107.59(8) . . ? C12 Cr2 P2 97.35(8) . . ? C14 Cr2 P2 158.22(8) . . ? P5 Cr2 P2 95.59(4) . . ? P3 Cr2 P2 54.11(5) . . ? P1 Cr2 P2 54.53(5) . . ? C15 Cr2 P4 119.65(8) . . ? C13 Cr2 P4 106.33(8) . . ? C11 Cr2 P4 156.96(8) . . ? C12 Cr2 P4 141.90(9) . . ? C14 Cr2 P4 95.73(8) . . ? P5 Cr2 P4 54.53(5) . . ? P3 Cr2 P4 54.54(5) . . ? P1 Cr2 P4 95.86(4) . . ? P2 Cr2 P4 95.42(4) . . ? C12 C11 C15 108.1(3) . . ? C12 C11 C16 125.0(3) . . ? C15 C11 C16 126.8(3) . . ? C12 C11 Cr2 71.29(16) . . ? C15 C11 Cr2 71.01(16) . . ? C16 C11 Cr2 126.3(2) . . ? C13 C12 C11 108.1(3) . . ? C13 C12 C17 126.0(3) . . ? C11 C12 C17 125.9(3) . . ? C13 C12 Cr2 71.12(17) . . ? C11 C12 Cr2 71.13(16) . . ? C17 C12 Cr2 125.6(2) . . ? C12 C13 C14 108.2(3) . . ? C12 C13 C18 126.4(3) . . ? C14 C13 C18 125.2(3) . . ? C12 C13 Cr2 71.32(16) . . ? C14 C13 Cr2 71.29(17) . . ? C18 C13 Cr2 127.1(2) . . ? C13 C14 C15 108.0(3) . . ? C13 C14 C19 126.2(3) . . ? C15 C14 C19 125.8(3) . . ? C13 C14 Cr2 71.12(17) . . ? C15 C14 Cr2 70.90(17) . . ? C19 C14 Cr2 125.7(2) . . ? C11 C15 C14 107.6(2) . . ? C11 C15 C20 126.5(3) . . ? C14 C15 C20 125.8(3) . . ? C11 C15 Cr2 71.22(16) . . ? C14 C15 Cr2 71.25(16) . . ? C20 C15 Cr2 125.7(2) . . ? C11 C16 H16A 109.5 . . ? C11 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C11 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C25 C21 C22 106.9(2) . . ? C25 C21 C26 125.7(3) . . ? C22 C21 C26 127.2(3) . . ? C25 C21 Cr3 70.74(16) . . ? C22 C21 Cr3 70.60(16) . . ? C26 C21 Cr3 127.9(2) . . ? C23 C22 C21 108.4(2) . . ? C23 C22 C27 125.3(3) . . ? C21 C22 C27 126.1(3) . . ? C23 C22 Cr3 70.87(16) . . ? C21 C22 Cr3 71.43(16) . . ? C27 C22 Cr3 126.6(2) . . ? C22 C23 C24 108.4(3) . . ? C22 C23 C28 125.3(3) . . ? C24 C23 C28 126.1(3) . . ? C22 C23 Cr3 71.46(18) . . ? C24 C23 Cr3 71.66(17) . . ? C28 C23 Cr3 126.6(2) . . ? C23 C24 C25 107.5(3) . . ? C23 C24 C29 125.5(3) . . ? C25 C24 C29 126.9(3) . . ? C23 C24 Cr3 70.62(18) . . ? C25 C24 Cr3 70.90(17) . . ? C29 C24 Cr3 125.9(2) . . ? C21 C25 C24 108.7(3) . . ? C21 C25 C30 125.1(3) . . ? C24 C25 C30 126.0(3) . . ? C21 C25 Cr3 71.51(16) . . ? C24 C25 Cr3 71.29(17) . . ? C30 C25 Cr3 126.3(2) . . ? C21 C26 H26A 109.5 . . ? C21 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C21 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C22 C27 H27A 109.5 . . ? C22 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? C22 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? C23 C28 H28A 109.5 . . ? C23 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C23 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C24 C29 H29A 109.5 . . ? C24 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C24 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C25 C30 H30A 109.5 . . ? C25 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? C25 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C23 Cr3 C22 37.67(11) . . ? C23 Cr3 C25 63.10(11) . . ? C22 Cr3 C25 63.00(11) . . ? C23 Cr3 C24 37.73(11) . . ? C22 Cr3 C24 63.05(11) . . ? C25 Cr3 C24 37.81(11) . . ? C23 Cr3 C21 63.42(11) . . ? C22 Cr3 C21 37.97(11) . . ? C25 Cr3 C21 37.75(10) . . ? C24 Cr3 C21 63.39(11) . . ? C23 Cr3 P10 147.89(9) . . ? C22 Cr3 P10 154.44(8) . . ? C25 Cr3 P10 96.64(8) . . ? C24 Cr3 P10 111.13(8) . . ? C21 Cr3 P10 116.49(8) . . ? C23 Cr3 P6 155.24(9) . . ? C22 Cr3 P6 117.64(9) . . ? C25 Cr3 P6 112.21(8) . . ? C24 Cr3 P6 148.90(9) . . ? C21 Cr3 P6 97.48(8) . . ? P10 Cr3 P6 53.33(3) . . ? C23 Cr3 P9 111.02(8) . . ? C22 Cr3 P9 147.79(9) . . ? C25 Cr3 P9 116.49(8) . . ? C24 Cr3 P9 96.32(8) . . ? C21 Cr3 P9 154.20(8) . . ? P10 Cr3 P9 53.61(3) . . ? P6 Cr3 P9 92.98(3) . . ? C23 Cr3 P8 96.53(8) . . ? C22 Cr3 P8 111.58(8) . . ? C25 Cr3 P8 153.94(9) . . ? C24 Cr3 P8 116.17(9) . . ? C21 Cr3 P8 148.61(8) . . ? P10 Cr3 P8 93.47(3) . . ? P6 Cr3 P8 93.07(3) . . ? P9 Cr3 P8 53.18(3) . . ? C23 Cr3 P7 117.60(9) . . ? C22 Cr3 P7 98.37(8) . . ? C25 Cr3 P7 149.66(8) . . ? C24 Cr3 P7 155.20(9) . . ? C21 Cr3 P7 112.93(8) . . ? P10 Cr3 P7 92.65(3) . . ? P6 Cr3 P7 53.01(3) . . ? P9 Cr3 P7 92.18(3) . . ? P8 Cr3 P7 52.92(3) . . ? P10 P6 P7 108.18(5) . . ? P10 P6 Cr3 63.27(3) . . ? P7 P6 Cr3 64.09(3) . . ? P10 P6 Cr4 63.19(3) . . ? P7 P6 Cr4 63.26(3) . . ? Cr3 P6 Cr4 80.72(3) . . ? P8 P7 P6 108.22(5) . . ? P8 P7 Cr4 63.91(3) . . ? P6 P7 Cr4 63.67(3) . . ? P8 P7 Cr3 63.13(3) . . ? P6 P7 Cr3 62.89(3) . . ? Cr4 P7 Cr3 80.39(3) . . ? P7 P8 P9 107.81(5) . . ? P7 P8 Cr3 63.95(3) . . ? P9 P8 Cr3 63.40(3) . . ? P7 P8 Cr4 63.12(3) . . ? P9 P8 Cr4 62.57(3) . . ? Cr3 P8 Cr4 80.40(3) . . ? P8 P9 P10 108.10(5) . . ? P8 P9 Cr4 64.20(3) . . ? P10 P9 Cr4 63.48(3) . . ? P8 P9 Cr3 63.42(3) . . ? P10 P9 Cr3 62.95(3) . . ? Cr4 P9 Cr3 81.10(3) . . ? P6 P10 P9 107.65(5) . . ? P6 P10 Cr3 63.40(3) . . ? P9 P10 Cr3 63.44(3) . . ? P6 P10 Cr4 63.73(3) . . ? P9 P10 Cr4 62.76(3) . . ? Cr3 P10 Cr4 81.01(3) . . ? C31 Cr4 C32 38.10(11) . . ? C31 Cr4 C33 63.18(11) . . ? C32 Cr4 C33 37.72(10) . . ? C31 Cr4 C34 63.13(11) . . ? C32 Cr4 C34 63.24(10) . . ? C33 Cr4 C34 37.69(10) . . ? C31 Cr4 C35 37.81(11) . . ? C32 Cr4 C35 63.47(11) . . ? C33 Cr4 C35 63.11(11) . . ? C34 Cr4 C35 37.71(11) . . ? C31 Cr4 P9 141.42(9) . . ? C32 Cr4 P9 160.35(8) . . ? C33 Cr4 P9 123.15(8) . . ? C34 Cr4 P9 98.32(8) . . ? C35 Cr4 P9 106.75(8) . . ? C31 Cr4 P10 105.99(8) . . ? C32 Cr4 P10 140.96(8) . . ? C33 Cr4 P10 159.77(8) . . ? C34 Cr4 P10 122.83(8) . . ? C35 Cr4 P10 97.60(8) . . ? P9 Cr4 P10 53.76(3) . . ? C31 Cr4 P7 122.74(8) . . ? C32 Cr4 P7 97.94(8) . . ? C33 Cr4 P7 107.27(8) . . ? C34 Cr4 P7 142.05(9) . . ? C35 Cr4 P7 160.06(9) . . ? P9 Cr4 P7 93.14(3) . . ? P10 Cr4 P7 92.97(3) . . ? C31 Cr4 P6 97.71(8) . . ? C32 Cr4 P6 106.54(8) . . ? C33 Cr4 P6 141.46(8) . . ? C34 Cr4 P6 159.67(9) . . ? C35 Cr4 P6 122.58(8) . . ? P9 Cr4 P6 93.09(3) . . ? P10 Cr4 P6 53.08(3) . . ? P7 Cr4 P6 53.06(3) . . ? C31 Cr4 P8 161.01(8) . . ? C32 Cr4 P8 123.33(8) . . ? C33 Cr4 P8 99.22(8) . . ? C34 Cr4 P8 107.98(9) . . ? C35 Cr4 P8 142.47(9) . . ? P9 Cr4 P8 53.23(3) . . ? P10 Cr4 P8 92.93(3) . . ? P7 Cr4 P8 52.97(3) . . ? P6 Cr4 P8 92.33(3) . . ? C35 C31 C32 108.4(2) . . ? C35 C31 C36 125.7(3) . . ? C32 C31 C36 125.8(3) . . ? C35 C31 Cr4 71.82(17) . . ? C32 C31 Cr4 71.27(17) . . ? C36 C31 Cr4 124.8(2) . . ? C33 C32 C31 107.4(2) . . ? C33 C32 C37 126.1(3) . . ? C31 C32 C37 126.5(3) . . ? C33 C32 Cr4 71.29(17) . . ? C31 C32 Cr4 70.62(16) . . ? C37 C32 Cr4 125.0(2) . . ? C32 C33 C34 108.4(3) . . ? C32 C33 C38 127.0(3) . . ? C34 C33 C38 124.5(3) . . ? C32 C33 Cr4 70.99(16) . . ? C34 C33 Cr4 71.24(16) . . ? C38 C33 Cr4 125.5(2) . . ? C33 C34 C35 108.2(2) . . ? C33 C34 C39 125.5(3) . . ? C35 C34 C39 126.1(3) . . ? C33 C34 Cr4 71.07(16) . . ? C35 C34 Cr4 71.31(16) . . ? C39 C34 Cr4 126.9(2) . . ? C31 C35 C34 107.6(2) . . ? C31 C35 C40 126.6(3) . . ? C34 C35 C40 125.8(3) . . ? C31 C35 Cr4 70.37(16) . . ? C34 C35 Cr4 70.98(16) . . ? C40 C35 Cr4 126.4(2) . . ? C31 C36 H36A 109.5 . . ? C31 C36 H36B 109.5 . . ? H36A C36 H36B 109.5 . . ? C31 C36 H36C 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C32 C37 H37A 109.5 . . ? C32 C37 H37B 109.5 . . ? H37A C37 H37B 109.5 . . ? C32 C37 H37C 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? C33 C38 H38A 109.5 . . ? C33 C38 H38B 109.5 . . ? H38A C38 H38B 109.5 . . ? C33 C38 H38C 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? C34 C39 H39A 109.5 . . ? C34 C39 H39B 109.5 . . ? H39A C39 H39B 109.5 . . ? C34 C39 H39C 109.5 . . ? H39A C39 H39C 109.5 . . ? H39B C39 H39C 109.5 . . ? C35 C40 H40A 109.5 . . ? C35 C40 H40B 109.5 . . ? H40A C40 H40B 109.5 . . ? C35 C40 H40C 109.5 . . ? H40A C40 H40C 109.5 . . ? H40B C40 H40C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 C1 C2 C3 -0.1(3) . . . . ? C6 C1 C2 C3 176.5(3) . . . . ? Cr1 C1 C2 C3 -62.1(2) . . . . ? C5 C1 C2 C7 -176.7(3) . . . . ? C6 C1 C2 C7 -0.1(5) . . . . ? Cr1 C1 C2 C7 121.3(3) . . . . ? C5 C1 C2 Cr1 62.0(2) . . . . ? C6 C1 C2 Cr1 -121.5(3) . . . . ? C1 C2 C3 C4 0.3(3) . . . . ? C7 C2 C3 C4 176.9(3) . . . . ? Cr1 C2 C3 C4 -62.1(2) . . . . ? C1 C2 C3 C8 -177.4(3) . . . . ? C7 C2 C3 C8 -0.9(5) . . . . ? Cr1 C2 C3 C8 120.2(3) . . . . ? C1 C2 C3 Cr1 62.4(2) . . . . ? C7 C2 C3 Cr1 -121.0(3) . . . . ? C2 C3 C4 C5 -0.5(3) . . . . ? C8 C3 C4 C5 177.3(3) . . . . ? Cr1 C3 C4 C5 -62.4(2) . . . . ? C2 C3 C4 C9 -177.0(3) . . . . ? C8 C3 C4 C9 0.8(5) . . . . ? Cr1 C3 C4 C9 121.0(3) . . . . ? C2 C3 C4 Cr1 61.9(2) . . . . ? C8 C3 C4 Cr1 -120.2(3) . . . . ? C3 C4 C5 C1 0.4(3) . . . . ? C9 C4 C5 C1 177.0(3) . . . . ? Cr1 C4 C5 C1 -61.4(2) . . . . ? C3 C4 C5 C10 -175.2(3) . . . . ? C9 C4 C5 C10 1.4(5) . . . . ? Cr1 C4 C5 C10 123.0(3) . . . . ? C3 C4 C5 Cr1 61.8(2) . . . . ? C9 C4 C5 Cr1 -121.6(3) . . . . ? C2 C1 C5 C4 -0.2(3) . . . . ? C6 C1 C5 C4 -176.8(3) . . . . ? Cr1 C1 C5 C4 61.3(2) . . . . ? C2 C1 C5 C10 175.5(3) . . . . ? C6 C1 C5 C10 -1.1(5) . . . . ? Cr1 C1 C5 C10 -123.0(3) . . . . ? C2 C1 C5 Cr1 -61.5(2) . . . . ? C6 C1 C5 Cr1 121.9(3) . . . . ? C4 C3 Cr1 C2 117.8(2) . . . . ? C8 C3 Cr1 C2 -122.4(3) . . . . ? C2 C3 Cr1 C4 -117.8(2) . . . . ? C8 C3 Cr1 C4 119.9(3) . . . . ? C2 C3 Cr1 C1 -37.60(16) . . . . ? C4 C3 Cr1 C1 80.17(18) . . . . ? C8 C3 Cr1 C1 -160.0(3) . . . . ? C2 C3 Cr1 C5 -80.22(18) . . . . ? C4 C3 Cr1 C5 37.55(17) . . . . ? C8 C3 Cr1 C5 157.4(3) . . . . ? C2 C3 Cr1 P5 -151.01(14) . . . . ? C4 C3 Cr1 P5 -33.2(2) . . . . ? C8 C3 Cr1 P5 86.6(3) . . . . ? C2 C3 Cr1 P4 157.88(15) . . . . ? C4 C3 Cr1 P4 -84.34(17) . . . . ? C8 C3 Cr1 P4 35.5(3) . . . . ? C2 C3 Cr1 P3 102.72(16) . . . . ? C4 C3 Cr1 P3 -139.50(16) . . . . ? C8 C3 Cr1 P3 -19.6(3) . . . . ? C2 C3 Cr1 P2 51.69(19) . . . . ? C4 C3 Cr1 P2 169.47(14) . . . . ? C8 C3 Cr1 P2 -70.7(3) . . . . ? C2 C3 Cr1 P1 -26.6(4) . . . . ? C4 C3 Cr1 P1 91.2(3) . . . . ? C8 C3 Cr1 P1 -149.0(2) . . . . ? C1 C2 Cr1 C3 -117.5(2) . . . . ? C7 C2 Cr1 C3 121.9(3) . . . . ? C3 C2 Cr1 C4 37.52(16) . . . . ? C1 C2 Cr1 C4 -79.94(19) . . . . ? C7 C2 Cr1 C4 159.4(3) . . . . ? C3 C2 Cr1 C1 117.5(2) . . . . ? C7 C2 Cr1 C1 -120.6(4) . . . . ? C3 C2 Cr1 C5 79.78(18) . . . . ? C1 C2 Cr1 C5 -37.68(17) . . . . ? C7 C2 Cr1 C5 -158.3(3) . . . . ? C3 C2 Cr1 P5 88.4(3) . . . . ? C1 C2 Cr1 P5 -29.1(4) . . . . ? C7 C2 Cr1 P5 -149.7(2) . . . . ? C3 C2 Cr1 P4 -32.5(2) . . . . ? C1 C2 Cr1 P4 -150.00(15) . . . . ? C7 C2 Cr1 P4 89.4(3) . . . . ? C3 C2 Cr1 P3 -84.15(16) . . . . ? C1 C2 Cr1 P3 158.38(16) . . . . ? C7 C2 Cr1 P3 37.7(3) . . . . ? C3 C2 Cr1 P2 -138.88(16) . . . . ? C1 C2 Cr1 P2 103.66(17) . . . . ? C7 C2 Cr1 P2 -17.0(3) . . . . ? C3 C2 Cr1 P1 169.70(14) . . . . ? C1 C2 Cr1 P1 52.2(2) . . . . ? C7 C2 Cr1 P1 -68.4(3) . . . . ? C5 C4 Cr1 C3 117.0(2) . . . . ? C9 C4 Cr1 C3 -121.3(3) . . . . ? C5 C4 Cr1 C2 79.78(18) . . . . ? C3 C4 Cr1 C2 -37.27(17) . . . . ? C9 C4 Cr1 C2 -158.5(3) . . . . ? C5 C4 Cr1 C1 37.21(17) . . . . ? C3 C4 Cr1 C1 -79.83(18) . . . . ? C9 C4 Cr1 C1 158.9(3) . . . . ? C3 C4 Cr1 C5 -117.0(2) . . . . ? C9 C4 Cr1 C5 121.7(3) . . . . ? C5 C4 Cr1 P5 -85.18(17) . . . . ? C3 C4 Cr1 P5 157.78(16) . . . . ? C9 C4 Cr1 P5 36.5(3) . . . . ? C5 C4 Cr1 P4 -140.43(16) . . . . ? C3 C4 Cr1 P4 102.53(17) . . . . ? C9 C4 Cr1 P4 -18.7(3) . . . . ? C5 C4 Cr1 P3 168.11(14) . . . . ? C3 C4 Cr1 P3 51.07(19) . . . . ? C9 C4 Cr1 P3 -70.2(3) . . . . ? C5 C4 Cr1 P2 90.4(3) . . . . ? C3 C4 Cr1 P2 -26.7(4) . . . . ? C9 C4 Cr1 P2 -147.9(2) . . . . ? C5 C4 Cr1 P1 -33.2(2) . . . . ? C3 C4 Cr1 P1 -150.29(16) . . . . ? C9 C4 Cr1 P1 88.4(3) . . . . ? C2 C1 Cr1 C3 37.48(17) . . . . ? C5 C1 Cr1 C3 -79.72(18) . . . . ? C6 C1 Cr1 C3 159.4(3) . . . . ? C5 C1 Cr1 C2 -117.2(3) . . . . ? C6 C1 Cr1 C2 121.9(3) . . . . ? C2 C1 Cr1 C4 80.23(19) . . . . ? C5 C1 Cr1 C4 -36.96(16) . . . . ? C6 C1 Cr1 C4 -157.9(3) . . . . ? C2 C1 Cr1 C5 117.2(3) . . . . ? C6 C1 Cr1 C5 -120.9(3) . . . . ? C2 C1 Cr1 P5 168.91(15) . . . . ? C5 C1 Cr1 P5 51.7(2) . . . . ? C6 C1 Cr1 P5 -69.2(3) . . . . ? C2 C1 Cr1 P4 87.1(3) . . . . ? C5 C1 Cr1 P4 -30.1(3) . . . . ? C6 C1 Cr1 P4 -151.0(2) . . . . ? C2 C1 Cr1 P3 -32.0(2) . . . . ? C5 C1 Cr1 P3 -149.20(14) . . . . ? C6 C1 Cr1 P3 89.9(3) . . . . ? C2 C1 Cr1 P2 -83.54(18) . . . . ? C5 C1 Cr1 P2 159.27(16) . . . . ? C6 C1 Cr1 P2 38.4(3) . . . . ? C2 C1 Cr1 P1 -138.89(17) . . . . ? C5 C1 Cr1 P1 103.91(16) . . . . ? C6 C1 Cr1 P1 -17.0(3) . . . . ? C4 C5 Cr1 C3 -37.97(17) . . . . ? C1 C5 Cr1 C3 80.25(19) . . . . ? C10 C5 Cr1 C3 -160.1(3) . . . . ? C4 C5 Cr1 C2 -80.50(18) . . . . ? C1 C5 Cr1 C2 37.72(17) . . . . ? C10 C5 Cr1 C2 157.4(3) . . . . ? C1 C5 Cr1 C4 118.2(2) . . . . ? C10 C5 Cr1 C4 -122.1(3) . . . . ? C4 C5 Cr1 C1 -118.2(2) . . . . ? C10 C5 Cr1 C1 119.7(3) . . . . ? C4 C5 Cr1 P5 102.32(16) . . . . ? C1 C5 Cr1 P5 -139.46(16) . . . . ? C10 C5 Cr1 P5 -19.8(3) . . . . ? C4 C5 Cr1 P4 49.85(19) . . . . ? C1 C5 Cr1 P4 168.07(14) . . . . ? C10 C5 Cr1 P4 -72.3(3) . . . . ? C4 C5 Cr1 P3 -29.5(4) . . . . ? C1 C5 Cr1 P3 88.7(3) . . . . ? C10 C5 Cr1 P3 -151.6(2) . . . . ? C4 C5 Cr1 P2 -149.35(15) . . . . ? C1 C5 Cr1 P2 -31.1(2) . . . . ? C10 C5 Cr1 P2 88.5(3) . . . . ? C4 C5 Cr1 P1 157.91(15) . . . . ? C1 C5 Cr1 P1 -83.87(17) . . . . ? C10 C5 Cr1 P1 35.8(3) . . . . ? C3 Cr1 P1 P2 91.6(3) . . . . ? C2 Cr1 P1 P2 72.19(10) . . . . ? C4 Cr1 P1 P2 159.74(13) . . . . ? C1 Cr1 P1 P2 101.52(9) . . . . ? C5 Cr1 P1 P2 139.52(9) . . . . ? P5 Cr1 P1 P2 -130.95(6) . . . . ? P4 Cr1 P1 P2 -92.77(5) . . . . ? P3 Cr1 P1 P2 -37.91(5) . . . . ? C3 Cr1 P1 P5 -137.4(3) . . . . ? C2 Cr1 P1 P5 -156.86(10) . . . . ? C4 Cr1 P1 P5 -69.31(13) . . . . ? C1 Cr1 P1 P5 -127.53(9) . . . . ? C5 Cr1 P1 P5 -89.54(9) . . . . ? P4 Cr1 P1 P5 38.18(5) . . . . ? P3 Cr1 P1 P5 93.04(5) . . . . ? P2 Cr1 P1 P5 130.95(6) . . . . ? C3 Cr1 P1 Cr2 157.3(3) . . . . ? C2 Cr1 P1 Cr2 137.89(9) . . . . ? C4 Cr1 P1 Cr2 -134.57(12) . . . . ? C1 Cr1 P1 Cr2 167.22(8) . . . . ? C5 Cr1 P1 Cr2 -154.79(9) . . . . ? P5 Cr1 P1 Cr2 -65.25(4) . . . . ? P4 Cr1 P1 Cr2 -27.08(5) . . . . ? P3 Cr1 P1 Cr2 27.78(5) . . . . ? P2 Cr1 P1 Cr2 65.69(4) . . . . ? P5 P1 P2 P3 0.42(7) . . . . ? Cr2 P1 P2 P3 -44.55(4) . . . . ? Cr1 P1 P2 P3 44.99(4) . . . . ? P5 P1 P2 Cr1 -44.57(4) . . . . ? Cr2 P1 P2 Cr1 -89.54(4) . . . . ? P5 P1 P2 Cr2 44.97(4) . . . . ? Cr1 P1 P2 Cr2 89.54(4) . . . . ? C3 Cr1 P2 P3 72.30(11) . . . . ? C2 Cr1 P2 P3 101.24(9) . . . . ? C4 Cr1 P2 P3 91.7(3) . . . . ? C1 Cr1 P2 P3 139.15(9) . . . . ? C5 Cr1 P2 P3 158.21(12) . . . . ? P5 Cr1 P2 P3 -92.64(5) . . . . ? P4 Cr1 P2 P3 -37.65(5) . . . . ? P1 Cr1 P2 P3 -130.97(6) . . . . ? C3 Cr1 P2 P1 -156.73(11) . . . . ? C2 Cr1 P2 P1 -127.79(9) . . . . ? C4 Cr1 P2 P1 -137.3(3) . . . . ? C1 Cr1 P2 P1 -89.88(9) . . . . ? C5 Cr1 P2 P1 -70.82(13) . . . . ? P5 Cr1 P2 P1 38.33(5) . . . . ? P4 Cr1 P2 P1 93.32(5) . . . . ? P3 Cr1 P2 P1 130.97(6) . . . . ? C3 Cr1 P2 Cr2 137.83(10) . . . . ? C2 Cr1 P2 Cr2 166.76(9) . . . . ? C4 Cr1 P2 Cr2 157.2(2) . . . . ? C1 Cr1 P2 Cr2 -155.32(8) . . . . ? C5 Cr1 P2 Cr2 -136.26(12) . . . . ? P5 Cr1 P2 Cr2 -27.11(5) . . . . ? P4 Cr1 P2 Cr2 27.87(5) . . . . ? P3 Cr1 P2 Cr2 65.53(4) . . . . ? P1 Cr1 P2 Cr2 -65.44(4) . . . . ? P1 P2 P3 P4 -0.52(7) . . . . ? Cr1 P2 P3 P4 44.38(4) . . . . ? Cr2 P2 P3 P4 -45.03(4) . . . . ? P1 P2 P3 Cr2 44.51(4) . . . . ? Cr1 P2 P3 Cr2 89.41(4) . . . . ? P1 P2 P3 Cr1 -44.90(4) . . . . ? Cr2 P2 P3 Cr1 -89.41(4) . . . . ? C3 Cr1 P3 P2 -127.04(9) . . . . ? C2 Cr1 P3 P2 -89.22(9) . . . . ? C4 Cr1 P3 P2 -155.88(10) . . . . ? C1 Cr1 P3 P2 -69.70(13) . . . . ? C5 Cr1 P3 P2 -134.6(3) . . . . ? P5 Cr1 P3 P2 93.20(5) . . . . ? P4 Cr1 P3 P2 131.76(5) . . . . ? P1 Cr1 P3 P2 38.16(5) . . . . ? C3 Cr1 P3 P4 101.20(9) . . . . ? C2 Cr1 P3 P4 139.02(9) . . . . ? C4 Cr1 P3 P4 72.36(10) . . . . ? C1 Cr1 P3 P4 158.54(13) . . . . ? C5 Cr1 P3 P4 93.6(3) . . . . ? P5 Cr1 P3 P4 -38.56(5) . . . . ? P2 Cr1 P3 P4 -131.76(5) . . . . ? P1 Cr1 P3 P4 -93.60(5) . . . . ? C3 Cr1 P3 Cr2 166.96(9) . . . . ? C2 Cr1 P3 Cr2 -155.22(9) . . . . ? C4 Cr1 P3 Cr2 138.12(9) . . . . ? C1 Cr1 P3 Cr2 -135.70(13) . . . . ? C5 Cr1 P3 Cr2 159.4(2) . . . . ? P5 Cr1 P3 Cr2 27.20(5) . . . . ? P4 Cr1 P3 Cr2 65.76(4) . . . . ? P2 Cr1 P3 Cr2 -66.00(4) . . . . ? P1 Cr1 P3 Cr2 -27.84(5) . . . . ? P2 P3 P4 P5 0.41(7) . . . . ? Cr2 P3 P4 P5 -44.72(4) . . . . ? Cr1 P3 P4 P5 44.94(4) . . . . ? P2 P3 P4 Cr1 -44.53(4) . . . . ? Cr2 P3 P4 Cr1 -89.67(4) . . . . ? P2 P3 P4 Cr2 45.14(4) . . . . ? Cr1 P3 P4 Cr2 89.67(4) . . . . ? C3 Cr1 P4 P5 140.29(9) . . . . ? C2 Cr1 P4 P5 160.04(12) . . . . ? C4 Cr1 P4 P5 102.20(8) . . . . ? C1 Cr1 P4 P5 96.0(2) . . . . ? C5 Cr1 P4 P5 74.21(10) . . . . ? P3 Cr1 P4 P5 -130.50(5) . . . . ? P2 Cr1 P4 P5 -93.10(5) . . . . ? P1 Cr1 P4 P5 -38.23(5) . . . . ? C3 Cr1 P4 P3 -89.21(9) . . . . ? C2 Cr1 P4 P3 -69.46(12) . . . . ? C4 Cr1 P4 P3 -127.30(8) . . . . ? C1 Cr1 P4 P3 -133.5(2) . . . . ? C5 Cr1 P4 P3 -155.29(10) . . . . ? P5 Cr1 P4 P3 130.50(5) . . . . ? P2 Cr1 P4 P3 37.40(5) . . . . ? P1 Cr1 P4 P3 92.28(5) . . . . ? C3 Cr1 P4 Cr2 -154.47(8) . . . . ? C2 Cr1 P4 Cr2 -134.72(11) . . . . ? C4 Cr1 P4 Cr2 167.44(8) . . . . ? C1 Cr1 P4 Cr2 161.3(2) . . . . ? C5 Cr1 P4 Cr2 139.45(9) . . . . ? P5 Cr1 P4 Cr2 65.24(4) . . . . ? P3 Cr1 P4 Cr2 -65.26(4) . . . . ? P2 Cr1 P4 Cr2 -27.86(5) . . . . ? P1 Cr1 P4 Cr2 27.01(5) . . . . ? P3 P4 P5 P1 -0.15(7) . . . . ? Cr1 P4 P5 P1 44.95(4) . . . . ? Cr2 P4 P5 P1 -44.89(4) . . . . ? P3 P4 P5 Cr1 -45.10(4) . . . . ? Cr2 P4 P5 Cr1 -89.84(4) . . . . ? P3 P4 P5 Cr2 44.74(4) . . . . ? Cr1 P4 P5 Cr2 89.84(4) . . . . ? P2 P1 P5 P4 -0.16(7) . . . . ? Cr2 P1 P5 P4 45.01(4) . . . . ? Cr1 P1 P5 P4 -44.94(4) . . . . ? P2 P1 P5 Cr1 44.77(4) . . . . ? Cr2 P1 P5 Cr1 89.94(4) . . . . ? P2 P1 P5 Cr2 -45.17(4) . . . . ? Cr1 P1 P5 Cr2 -89.94(4) . . . . ? C3 Cr1 P5 P4 -68.27(13) . . . . ? C2 Cr1 P5 P4 -134.2(3) . . . . ? C4 Cr1 P5 P4 -88.61(9) . . . . ? C1 Cr1 P5 P4 -155.54(11) . . . . ? C5 Cr1 P5 P4 -126.46(9) . . . . ? P3 Cr1 P5 P4 38.50(5) . . . . ? P2 Cr1 P5 P4 92.90(5) . . . . ? P1 Cr1 P5 P4 131.12(5) . . . . ? C3 Cr1 P5 P1 160.61(13) . . . . ? C2 Cr1 P5 P1 94.7(3) . . . . ? C4 Cr1 P5 P1 140.27(9) . . . . ? C1 Cr1 P5 P1 73.34(11) . . . . ? C5 Cr1 P5 P1 102.42(9) . . . . ? P4 Cr1 P5 P1 -131.12(5) . . . . ? P3 Cr1 P5 P1 -92.62(5) . . . . ? P2 Cr1 P5 P1 -38.22(5) . . . . ? C3 Cr1 P5 Cr2 -133.96(12) . . . . ? C2 Cr1 P5 Cr2 160.1(3) . . . . ? C4 Cr1 P5 Cr2 -154.30(9) . . . . ? C1 Cr1 P5 Cr2 138.77(10) . . . . ? C5 Cr1 P5 Cr2 167.85(9) . . . . ? P4 Cr1 P5 Cr2 -65.69(4) . . . . ? P3 Cr1 P5 Cr2 -27.19(5) . . . . ? P2 Cr1 P5 Cr2 27.21(5) . . . . ? P1 Cr1 P5 Cr2 65.43(4) . . . . ? P4 P5 Cr2 C15 122.64(9) . . . . ? P1 P5 Cr2 C15 -106.25(9) . . . . ? Cr1 P5 Cr2 C15 -171.82(9) . . . . ? P4 P5 Cr2 C13 69.93(14) . . . . ? P1 P5 Cr2 C13 -158.96(14) . . . . ? Cr1 P5 Cr2 C13 135.47(13) . . . . ? P4 P5 Cr2 C11 153.25(10) . . . . ? P1 P5 Cr2 C11 -75.64(10) . . . . ? Cr1 P5 Cr2 C11 -141.20(9) . . . . ? P4 P5 Cr2 C12 143.0(2) . . . . ? P1 P5 Cr2 C12 -85.9(2) . . . . ? Cr1 P5 Cr2 C12 -151.5(2) . . . . ? P4 P5 Cr2 C14 85.51(9) . . . . ? P1 P5 Cr2 C14 -143.38(9) . . . . ? Cr1 P5 Cr2 C14 151.05(9) . . . . ? P4 P5 Cr2 P3 -38.30(5) . . . . ? P1 P5 Cr2 P3 92.81(5) . . . . ? Cr1 P5 Cr2 P3 27.24(5) . . . . ? P4 P5 Cr2 P1 -131.11(5) . . . . ? Cr1 P5 Cr2 P1 -65.57(4) . . . . ? P4 P5 Cr2 P2 -92.69(5) . . . . ? P1 P5 Cr2 P2 38.42(5) . . . . ? Cr1 P5 Cr2 P2 -27.14(5) . . . . ? P1 P5 Cr2 P4 131.11(5) . . . . ? Cr1 P5 Cr2 P4 65.54(4) . . . . ? P2 P3 Cr2 C15 146.8(2) . . . . ? P4 P3 Cr2 C15 -82.0(2) . . . . ? Cr1 P3 Cr2 C15 -147.4(2) . . . . ? P2 P3 Cr2 C13 123.56(9) . . . . ? P4 P3 Cr2 C13 -105.25(9) . . . . ? Cr1 P3 Cr2 C13 -170.69(9) . . . . ? P2 P3 Cr2 C11 70.51(14) . . . . ? P4 P3 Cr2 C11 -158.30(14) . . . . ? Cr1 P3 Cr2 C11 136.27(13) . . . . ? P2 P3 Cr2 C12 86.59(9) . . . . ? P4 P3 Cr2 C12 -142.22(9) . . . . ? Cr1 P3 Cr2 C12 152.35(9) . . . . ? P2 P3 Cr2 C14 154.77(10) . . . . ? P4 P3 Cr2 C14 -74.04(10) . . . . ? Cr1 P3 Cr2 C14 -139.48(9) . . . . ? P2 P3 Cr2 P5 -92.90(5) . . . . ? P4 P3 Cr2 P5 38.29(5) . . . . ? Cr1 P3 Cr2 P5 -27.14(5) . . . . ? P2 P3 Cr2 P1 -37.89(5) . . . . ? P4 P3 Cr2 P1 93.29(5) . . . . ? Cr1 P3 Cr2 P1 27.86(5) . . . . ? P4 P3 Cr2 P2 131.19(5) . . . . ? Cr1 P3 Cr2 P2 65.76(4) . . . . ? P2 P3 Cr2 P4 -131.19(5) . . . . ? Cr1 P3 Cr2 P4 -65.43(4) . . . . ? P2 P1 Cr2 C15 -144.20(8) . . . . ? P5 P1 Cr2 C15 85.22(8) . . . . ? Cr1 P1 Cr2 C15 150.29(8) . . . . ? P2 P1 Cr2 C13 -85.6(2) . . . . ? P5 P1 Cr2 C13 143.8(2) . . . . ? Cr1 P1 Cr2 C13 -151.1(2) . . . . ? P2 P1 Cr2 C11 -106.93(8) . . . . ? P5 P1 Cr2 C11 122.49(8) . . . . ? Cr1 P1 Cr2 C11 -172.45(8) . . . . ? P2 P1 Cr2 C12 -76.14(10) . . . . ? P5 P1 Cr2 C12 153.28(10) . . . . ? Cr1 P1 Cr2 C12 -141.65(9) . . . . ? P2 P1 Cr2 C14 -160.30(14) . . . . ? P5 P1 Cr2 C14 69.12(14) . . . . ? Cr1 P1 Cr2 C14 134.19(13) . . . . ? P2 P1 Cr2 P5 130.58(5) . . . . ? Cr1 P1 Cr2 P5 65.07(4) . . . . ? P2 P1 Cr2 P3 37.66(5) . . . . ? P5 P1 Cr2 P3 -92.92(5) . . . . ? Cr1 P1 Cr2 P3 -27.85(5) . . . . ? P5 P1 Cr2 P2 -130.58(5) . . . . ? Cr1 P1 Cr2 P2 -65.51(4) . . . . ? P2 P1 Cr2 P4 92.49(5) . . . . ? P5 P1 Cr2 P4 -38.09(5) . . . . ? Cr1 P1 Cr2 P4 26.98(5) . . . . ? P3 P2 Cr2 C15 -160.02(13) . . . . ? P1 P2 Cr2 C15 68.63(14) . . . . ? Cr1 P2 Cr2 C15 134.21(13) . . . . ? P3 P2 Cr2 C13 -74.70(10) . . . . ? P1 P2 Cr2 C13 153.96(10) . . . . ? Cr1 P2 Cr2 C13 -140.46(10) . . . . ? P3 P2 Cr2 C11 -143.14(9) . . . . ? P1 P2 Cr2 C11 85.51(9) . . . . ? Cr1 P2 Cr2 C11 151.09(8) . . . . ? P3 P2 Cr2 C12 -106.02(9) . . . . ? P1 P2 Cr2 C12 122.63(9) . . . . ? Cr1 P2 Cr2 C12 -171.79(9) . . . . ? P3 P2 Cr2 C14 -82.5(2) . . . . ? P1 P2 Cr2 C14 146.1(2) . . . . ? Cr1 P2 Cr2 C14 -148.3(2) . . . . ? P3 P2 Cr2 P5 92.81(5) . . . . ? P1 P2 Cr2 P5 -38.54(5) . . . . ? Cr1 P2 Cr2 P5 27.04(5) . . . . ? P1 P2 Cr2 P3 -131.35(5) . . . . ? Cr1 P2 Cr2 P3 -65.77(4) . . . . ? P3 P2 Cr2 P1 131.35(5) . . . . ? Cr1 P2 Cr2 P1 65.58(4) . . . . ? P3 P2 Cr2 P4 38.00(5) . . . . ? P1 P2 Cr2 P4 -93.34(5) . . . . ? Cr1 P2 Cr2 P4 -27.76(5) . . . . ? P5 P4 Cr2 C15 -74.61(10) . . . . ? P3 P4 Cr2 C15 154.62(10) . . . . ? Cr1 P4 Cr2 C15 -139.83(9) . . . . ? P5 P4 Cr2 C13 -142.56(9) . . . . ? P3 P4 Cr2 C13 86.67(9) . . . . ? Cr1 P4 Cr2 C13 152.23(9) . . . . ? P5 P4 Cr2 C11 -84.2(2) . . . . ? P3 P4 Cr2 C11 145.0(2) . . . . ? Cr1 P4 Cr2 C11 -149.4(2) . . . . ? P5 P4 Cr2 C12 -157.76(13) . . . . ? P3 P4 Cr2 C12 71.47(14) . . . . ? Cr1 P4 Cr2 C12 137.03(13) . . . . ? P5 P4 Cr2 C14 -105.73(9) . . . . ? P3 P4 Cr2 C14 123.50(9) . . . . ? Cr1 P4 Cr2 C14 -170.95(8) . . . . ? P3 P4 Cr2 P5 -130.77(6) . . . . ? Cr1 P4 Cr2 P5 -65.22(4) . . . . ? P5 P4 Cr2 P3 130.77(6) . . . . ? Cr1 P4 Cr2 P3 65.56(4) . . . . ? P5 P4 Cr2 P1 38.19(5) . . . . ? P3 P4 Cr2 P1 -92.58(5) . . . . ? Cr1 P4 Cr2 P1 -27.02(5) . . . . ? P5 P4 Cr2 P2 93.01(5) . . . . ? P3 P4 Cr2 P2 -37.77(5) . . . . ? Cr1 P4 Cr2 P2 27.79(5) . . . . ? C15 Cr2 C11 C12 -117.6(3) . . . . ? C13 Cr2 C11 C12 -37.36(17) . . . . ? C14 Cr2 C11 C12 -79.77(19) . . . . ? P5 Cr2 C11 C12 -173.48(15) . . . . ? P3 Cr2 C11 C12 25.7(2) . . . . ? P1 Cr2 C11 C12 133.76(17) . . . . ? P2 Cr2 C11 C12 78.95(17) . . . . ? P4 Cr2 C11 C12 -104.0(2) . . . . ? C13 Cr2 C11 C15 80.29(19) . . . . ? C12 Cr2 C11 C15 117.6(3) . . . . ? C14 Cr2 C11 C15 37.87(17) . . . . ? P5 Cr2 C11 C15 -55.83(19) . . . . ? P3 Cr2 C11 C15 143.35(15) . . . . ? P1 Cr2 C11 C15 -108.60(17) . . . . ? P2 Cr2 C11 C15 -163.41(16) . . . . ? P4 Cr2 C11 C15 13.7(3) . . . . ? C15 Cr2 C11 C16 122.2(3) . . . . ? C13 Cr2 C11 C16 -157.5(3) . . . . ? C12 Cr2 C11 C16 -120.2(3) . . . . ? C14 Cr2 C11 C16 160.1(3) . . . . ? P5 Cr2 C11 C16 66.3(3) . . . . ? P3 Cr2 C11 C16 -94.5(3) . . . . ? P1 Cr2 C11 C16 13.6(3) . . . . ? P2 Cr2 C11 C16 -41.2(3) . . . . ? P4 Cr2 C11 C16 135.9(2) . . . . ? C15 C11 C12 C13 0.1(3) . . . . ? C16 C11 C12 C13 -176.4(3) . . . . ? Cr2 C11 C12 C13 61.9(2) . . . . ? C15 C11 C12 C17 177.4(3) . . . . ? C16 C11 C12 C17 1.0(5) . . . . ? Cr2 C11 C12 C17 -120.7(3) . . . . ? C15 C11 C12 Cr2 -61.8(2) . . . . ? C16 C11 C12 Cr2 121.7(3) . . . . ? C15 Cr2 C12 C13 -80.15(19) . . . . ? C11 Cr2 C12 C13 -117.6(2) . . . . ? C14 Cr2 C12 C13 -37.45(17) . . . . ? P5 Cr2 C12 C13 -103.0(3) . . . . ? P3 Cr2 C12 C13 78.35(17) . . . . ? P1 Cr2 C12 C13 -174.16(15) . . . . ? P2 Cr2 C12 C13 132.98(16) . . . . ? P4 Cr2 C12 C13 24.4(2) . . . . ? C15 Cr2 C12 C11 37.49(17) . . . . ? C13 Cr2 C12 C11 117.6(2) . . . . ? C14 Cr2 C12 C11 80.19(18) . . . . ? P5 Cr2 C12 C11 14.7(3) . . . . ? P3 Cr2 C12 C11 -164.01(15) . . . . ? P1 Cr2 C12 C11 -56.51(19) . . . . ? P2 Cr2 C12 C11 -109.38(17) . . . . ? P4 Cr2 C12 C11 142.02(15) . . . . ? C15 Cr2 C12 C17 158.6(3) . . . . ? C13 Cr2 C12 C17 -121.2(4) . . . . ? C11 Cr2 C12 C17 121.1(4) . . . . ? C14 Cr2 C12 C17 -158.7(3) . . . . ? P5 Cr2 C12 C17 135.8(3) . . . . ? P3 Cr2 C12 C17 -42.9(3) . . . . ? P1 Cr2 C12 C17 64.6(3) . . . . ? P2 Cr2 C12 C17 11.7(3) . . . . ? P4 Cr2 C12 C17 -96.9(3) . . . . ? C11 C12 C13 C14 0.3(3) . . . . ? C17 C12 C13 C14 -177.1(3) . . . . ? Cr2 C12 C13 C14 62.1(2) . . . . ? C11 C12 C13 C18 175.3(3) . . . . ? C17 C12 C13 C18 -2.1(5) . . . . ? Cr2 C12 C13 C18 -122.8(3) . . . . ? C11 C12 C13 Cr2 -61.9(2) . . . . ? C17 C12 C13 Cr2 120.7(3) . . . . ? C15 Cr2 C13 C12 79.96(18) . . . . ? C11 Cr2 C13 C12 37.37(17) . . . . ? C14 Cr2 C13 C12 117.5(2) . . . . ? P5 Cr2 C13 C12 142.53(15) . . . . ? P3 Cr2 C13 C12 -109.64(16) . . . . ? P1 Cr2 C13 C12 13.4(3) . . . . ? P2 Cr2 C13 C12 -57.75(19) . . . . ? P4 Cr2 C13 C12 -164.61(15) . . . . ? C15 Cr2 C13 C14 -37.55(17) . . . . ? C11 Cr2 C13 C14 -80.14(18) . . . . ? C12 Cr2 C13 C14 -117.5(2) . . . . ? P5 Cr2 C13 C14 25.0(2) . . . . ? P3 Cr2 C13 C14 132.85(16) . . . . ? P1 Cr2 C13 C14 -104.1(3) . . . . ? P2 Cr2 C13 C14 -175.25(15) . . . . ? P4 Cr2 C13 C14 77.88(17) . . . . ? C15 Cr2 C13 C18 -158.0(3) . . . . ? C11 Cr2 C13 C18 159.4(3) . . . . ? C12 Cr2 C13 C18 122.0(4) . . . . ? C14 Cr2 C13 C18 -120.5(4) . . . . ? P5 Cr2 C13 C18 -95.5(3) . . . . ? P3 Cr2 C13 C18 12.4(3) . . . . ? P1 Cr2 C13 C18 135.4(3) . . . . ? P2 Cr2 C13 C18 64.3(3) . . . . ? P4 Cr2 C13 C18 -42.6(3) . . . . ? C12 C13 C14 C15 -0.5(3) . . . . ? C18 C13 C14 C15 -175.6(3) . . . . ? Cr2 C13 C14 C15 61.7(2) . . . . ? C12 C13 C14 C19 176.9(3) . . . . ? C18 C13 C14 C19 1.7(5) . . . . ? Cr2 C13 C14 C19 -121.0(3) . . . . ? C12 C13 C14 Cr2 -62.2(2) . . . . ? C18 C13 C14 Cr2 122.7(3) . . . . ? C15 Cr2 C14 C13 117.6(2) . . . . ? C11 Cr2 C14 C13 79.84(18) . . . . ? C12 Cr2 C14 C13 37.43(17) . . . . ? P5 Cr2 C14 C13 -164.12(16) . . . . ? P3 Cr2 C14 C13 -57.52(19) . . . . ? P1 Cr2 C14 C13 143.31(16) . . . . ? P2 Cr2 C14 C13 11.0(3) . . . . ? P4 Cr2 C14 C13 -109.44(17) . . . . ? C13 Cr2 C14 C15 -117.6(2) . . . . ? C11 Cr2 C14 C15 -37.79(16) . . . . ? C12 Cr2 C14 C15 -80.20(18) . . . . ? P5 Cr2 C14 C15 78.25(16) . . . . ? P3 Cr2 C14 C15 -175.15(13) . . . . ? P1 Cr2 C14 C15 25.7(2) . . . . ? P2 Cr2 C14 C15 -106.6(2) . . . . ? P4 Cr2 C14 C15 132.93(15) . . . . ? C15 Cr2 C14 C19 -120.8(3) . . . . ? C13 Cr2 C14 C19 121.5(3) . . . . ? C11 Cr2 C14 C19 -158.6(3) . . . . ? C12 Cr2 C14 C19 159.0(3) . . . . ? P5 Cr2 C14 C19 -42.6(3) . . . . ? P3 Cr2 C14 C19 64.0(3) . . . . ? P1 Cr2 C14 C19 -95.2(3) . . . . ? P2 Cr2 C14 C19 132.6(3) . . . . ? P4 Cr2 C14 C19 12.1(3) . . . . ? C12 C11 C15 C14 -0.4(3) . . . . ? C16 C11 C15 C14 176.0(3) . . . . ? Cr2 C11 C15 C14 -62.3(2) . . . . ? C12 C11 C15 C20 -177.0(3) . . . . ? C16 C11 C15 C20 -0.6(5) . . . . ? Cr2 C11 C15 C20 121.0(3) . . . . ? C12 C11 C15 Cr2 62.0(2) . . . . ? C16 C11 C15 Cr2 -121.6(3) . . . . ? C13 C14 C15 C11 0.5(3) . . . . ? C19 C14 C15 C11 -176.9(3) . . . . ? Cr2 C14 C15 C11 62.3(2) . . . . ? C13 C14 C15 C20 177.2(3) . . . . ? C19 C14 C15 C20 -0.2(5) . . . . ? Cr2 C14 C15 C20 -121.0(3) . . . . ? C13 C14 C15 Cr2 -61.8(2) . . . . ? C19 C14 C15 Cr2 120.8(3) . . . . ? C13 Cr2 C15 C11 -79.64(18) . . . . ? C12 Cr2 C15 C11 -37.30(17) . . . . ? C14 Cr2 C15 C11 -116.9(2) . . . . ? P5 Cr2 C15 C11 134.01(17) . . . . ? P3 Cr2 C15 C11 -105.8(2) . . . . ? P1 Cr2 C15 C11 79.16(17) . . . . ? P2 Cr2 C15 C11 26.9(2) . . . . ? P4 Cr2 C15 C11 -173.89(15) . . . . ? C13 Cr2 C15 C14 37.29(17) . . . . ? C11 Cr2 C15 C14 116.9(2) . . . . ? C12 Cr2 C15 C14 79.63(18) . . . . ? P5 Cr2 C15 C14 -109.06(16) . . . . ? P3 Cr2 C15 C14 11.2(3) . . . . ? P1 Cr2 C15 C14 -163.90(15) . . . . ? P2 Cr2 C15 C14 143.81(15) . . . . ? P4 Cr2 C15 C14 -56.95(18) . . . . ? C13 Cr2 C15 C20 158.4(3) . . . . ? C11 Cr2 C15 C20 -122.0(3) . . . . ? C12 Cr2 C15 C20 -159.3(3) . . . . ? C14 Cr2 C15 C20 121.1(3) . . . . ? P5 Cr2 C15 C20 12.0(3) . . . . ? P3 Cr2 C15 C20 132.2(2) . . . . ? P1 Cr2 C15 C20 -42.8(3) . . . . ? P2 Cr2 C15 C20 -95.1(3) . . . . ? P4 Cr2 C15 C20 64.1(3) . . . . ? C25 C21 C22 C23 0.2(3) . . . . ? C26 C21 C22 C23 175.1(3) . . . . ? Cr3 C21 C22 C23 -61.6(2) . . . . ? C25 C21 C22 C27 -175.9(3) . . . . ? C26 C21 C22 C27 -1.1(5) . . . . ? Cr3 C21 C22 C27 122.3(3) . . . . ? C25 C21 C22 Cr3 61.8(2) . . . . ? C26 C21 C22 Cr3 -123.4(3) . . . . ? C21 C22 C23 C24 -0.6(3) . . . . ? C27 C22 C23 C24 175.6(3) . . . . ? Cr3 C22 C23 C24 -62.5(2) . . . . ? C21 C22 C23 C28 -175.8(3) . . . . ? C27 C22 C23 C28 0.4(5) . . . . ? Cr3 C22 C23 C28 122.3(3) . . . . ? C21 C22 C23 Cr3 61.9(2) . . . . ? C27 C22 C23 Cr3 -121.9(3) . . . . ? C22 C23 C24 C25 0.7(3) . . . . ? C28 C23 C24 C25 175.9(3) . . . . ? Cr3 C23 C24 C25 -61.7(2) . . . . ? C22 C23 C24 C29 -176.7(3) . . . . ? C28 C23 C24 C29 -1.6(5) . . . . ? Cr3 C23 C24 C29 120.9(3) . . . . ? C22 C23 C24 Cr3 62.4(2) . . . . ? C28 C23 C24 Cr3 -122.4(3) . . . . ? C22 C21 C25 C24 0.2(3) . . . . ? C26 C21 C25 C24 -174.7(3) . . . . ? Cr3 C21 C25 C24 61.9(2) . . . . ? C22 C21 C25 C30 176.4(3) . . . . ? C26 C21 C25 C30 1.5(5) . . . . ? Cr3 C21 C25 C30 -121.9(3) . . . . ? C22 C21 C25 Cr3 -61.7(2) . . . . ? C26 C21 C25 Cr3 123.4(3) . . . . ? C23 C24 C25 C21 -0.6(3) . . . . ? C29 C24 C25 C21 176.8(3) . . . . ? Cr3 C24 C25 C21 -62.1(2) . . . . ? C23 C24 C25 C30 -176.7(3) . . . . ? C29 C24 C25 C30 0.7(5) . . . . ? Cr3 C24 C25 C30 121.8(3) . . . . ? C23 C24 C25 Cr3 61.5(2) . . . . ? C29 C24 C25 Cr3 -121.1(3) . . . . ? C24 C23 Cr3 C22 117.5(3) . . . . ? C28 C23 Cr3 C22 -120.6(4) . . . . ? C22 C23 Cr3 C25 -79.88(18) . . . . ? C24 C23 Cr3 C25 37.63(17) . . . . ? C28 C23 Cr3 C25 159.5(3) . . . . ? C22 C23 Cr3 C24 -117.5(3) . . . . ? C28 C23 Cr3 C24 121.9(4) . . . . ? C22 C23 Cr3 C21 -37.40(17) . . . . ? C24 C23 Cr3 C21 80.11(18) . . . . ? C28 C23 Cr3 C21 -158.0(3) . . . . ? C22 C23 Cr3 P10 -135.50(17) . . . . ? C24 C23 Cr3 P10 -18.0(3) . . . . ? C28 C23 Cr3 P10 103.9(3) . . . . ? C22 C23 Cr3 P6 5.1(3) . . . . ? C24 C23 Cr3 P6 122.6(2) . . . . ? C28 C23 Cr3 P6 -115.6(3) . . . . ? C22 C23 Cr3 P9 170.19(15) . . . . ? C24 C23 Cr3 P9 -72.30(17) . . . . ? C28 C23 Cr3 P9 49.6(3) . . . . ? C22 C23 Cr3 P8 117.22(16) . . . . ? C24 C23 Cr3 P8 -125.27(16) . . . . ? C28 C23 Cr3 P8 -3.4(3) . . . . ? C22 C23 Cr3 P7 65.89(18) . . . . ? C24 C23 Cr3 P7 -176.60(15) . . . . ? C28 C23 Cr3 P7 -54.7(3) . . . . ? C21 C22 Cr3 C23 -118.0(3) . . . . ? C27 C22 Cr3 C23 120.3(3) . . . . ? C23 C22 Cr3 C25 80.15(19) . . . . ? C21 C22 Cr3 C25 -37.86(17) . . . . ? C27 C22 Cr3 C25 -159.5(3) . . . . ? C23 C22 Cr3 C24 37.51(18) . . . . ? C21 C22 Cr3 C24 -80.50(19) . . . . ? C27 C22 Cr3 C24 157.9(3) . . . . ? C23 C22 Cr3 C21 118.0(3) . . . . ? C27 C22 Cr3 C21 -121.7(3) . . . . ? C23 C22 Cr3 P10 120.3(2) . . . . ? C21 C22 Cr3 P10 2.3(3) . . . . ? C27 C22 Cr3 P10 -119.4(3) . . . . ? C23 C22 Cr3 P6 -177.60(15) . . . . ? C21 C22 Cr3 P6 64.39(18) . . . . ? C27 C22 Cr3 P6 -57.3(3) . . . . ? C23 C22 Cr3 P9 -17.4(3) . . . . ? C21 C22 Cr3 P9 -135.36(16) . . . . ? C27 C22 Cr3 P9 103.0(3) . . . . ? C23 C22 Cr3 P8 -71.82(18) . . . . ? C21 C22 Cr3 P8 170.18(15) . . . . ? C27 C22 Cr3 P8 48.5(3) . . . . ? C23 C22 Cr3 P7 -125.15(16) . . . . ? C21 C22 Cr3 P7 116.84(16) . . . . ? C27 C22 Cr3 P7 -4.8(3) . . . . ? C21 C25 Cr3 C23 80.55(18) . . . . ? C24 C25 Cr3 C23 -37.55(17) . . . . ? C30 C25 Cr3 C23 -159.0(3) . . . . ? C21 C25 Cr3 C22 38.08(17) . . . . ? C24 C25 Cr3 C22 -80.02(18) . . . . ? C30 C25 Cr3 C22 158.5(3) . . . . ? C21 C25 Cr3 C24 118.1(2) . . . . ? C30 C25 Cr3 C24 -121.5(3) . . . . ? C24 C25 Cr3 C21 -118.1(2) . . . . ? C30 C25 Cr3 C21 120.4(3) . . . . ? C21 C25 Cr3 P10 -125.67(16) . . . . ? C24 C25 Cr3 P10 116.24(16) . . . . ? C30 C25 Cr3 P10 -5.2(3) . . . . ? C21 C25 Cr3 P6 -72.67(17) . . . . ? C24 C25 Cr3 P6 169.23(15) . . . . ? C30 C25 Cr3 P6 47.8(3) . . . . ? C21 C25 Cr3 P9 -178.12(14) . . . . ? C24 C25 Cr3 P9 63.78(18) . . . . ? C30 C25 Cr3 P9 -57.7(3) . . . . ? C21 C25 Cr3 P8 122.21(19) . . . . ? C24 C25 Cr3 P8 4.1(3) . . . . ? C30 C25 Cr3 P8 -117.3(3) . . . . ? C21 C25 Cr3 P7 -18.7(3) . . . . ? C24 C25 Cr3 P7 -136.85(17) . . . . ? C30 C25 Cr3 P7 101.7(3) . . . . ? C25 C24 Cr3 C23 117.4(2) . . . . ? C29 C24 Cr3 C23 -120.4(4) . . . . ? C23 C24 Cr3 C22 -37.45(17) . . . . ? C25 C24 Cr3 C22 79.90(18) . . . . ? C29 C24 Cr3 C22 -157.8(3) . . . . ? C23 C24 Cr3 C25 -117.4(2) . . . . ? C29 C24 Cr3 C25 122.3(4) . . . . ? C23 C24 Cr3 C21 -80.19(18) . . . . ? C25 C24 Cr3 C21 37.16(16) . . . . ? C29 C24 Cr3 C21 159.4(3) . . . . ? C23 C24 Cr3 P10 169.86(15) . . . . ? C25 C24 Cr3 P10 -72.79(17) . . . . ? C29 C24 Cr3 P10 49.5(3) . . . . ? C23 C24 Cr3 P6 -136.92(17) . . . . ? C25 C24 Cr3 P6 -19.6(3) . . . . ? C29 C24 Cr3 P6 102.7(3) . . . . ? C23 C24 Cr3 P9 116.53(17) . . . . ? C25 C24 Cr3 P9 -126.12(16) . . . . ? C29 C24 Cr3 P9 -3.8(3) . . . . ? C23 C24 Cr3 P8 64.66(18) . . . . ? C25 C24 Cr3 P8 -177.99(14) . . . . ? C29 C24 Cr3 P8 -55.7(3) . . . . ? C23 C24 Cr3 P7 7.2(3) . . . . ? C25 C24 Cr3 P7 124.6(2) . . . . ? C29 C24 Cr3 P7 -113.2(3) . . . . ? C25 C21 Cr3 C23 -79.61(18) . . . . ? C22 C21 Cr3 C23 37.11(17) . . . . ? C26 C21 Cr3 C23 159.6(3) . . . . ? C25 C21 Cr3 C22 -116.7(3) . . . . ? C26 C21 Cr3 C22 122.5(3) . . . . ? C22 C21 Cr3 C25 116.7(3) . . . . ? C26 C21 Cr3 C25 -120.8(3) . . . . ? C25 C21 Cr3 C24 -37.22(17) . . . . ? C22 C21 Cr3 C24 79.51(19) . . . . ? C26 C21 Cr3 C24 -158.0(3) . . . . ? C25 C21 Cr3 P10 64.37(18) . . . . ? C22 C21 Cr3 P10 -178.90(15) . . . . ? C26 C21 Cr3 P10 -56.4(3) . . . . ? C25 C21 Cr3 P6 116.96(16) . . . . ? C22 C21 Cr3 P6 -126.32(16) . . . . ? C26 C21 Cr3 P6 -3.8(3) . . . . ? C25 C21 Cr3 P9 3.9(3) . . . . ? C22 C21 Cr3 P9 120.6(2) . . . . ? C26 C21 Cr3 P9 -116.9(3) . . . . ? C25 C21 Cr3 P8 -134.46(17) . . . . ? C22 C21 Cr3 P8 -17.7(3) . . . . ? C26 C21 Cr3 P8 104.8(3) . . . . ? C25 C21 Cr3 P7 169.85(15) . . . . ? C22 C21 Cr3 P7 -73.43(18) . . . . ? C26 C21 Cr3 P7 49.1(3) . . . . ? C23 Cr3 P6 P10 -155.1(2) . . . . ? C22 Cr3 P6 P10 -151.61(9) . . . . ? C25 Cr3 P6 P10 -81.47(9) . . . . ? C24 Cr3 P6 P10 -68.66(16) . . . . ? C21 Cr3 P6 P10 -117.59(8) . . . . ? P9 Cr3 P6 P10 38.78(4) . . . . ? P8 Cr3 P6 P10 92.04(4) . . . . ? P7 Cr3 P6 P10 129.27(4) . . . . ? C23 Cr3 P6 P7 75.6(2) . . . . ? C22 Cr3 P6 P7 79.12(9) . . . . ? C25 Cr3 P6 P7 149.26(9) . . . . ? C24 Cr3 P6 P7 162.08(15) . . . . ? C21 Cr3 P6 P7 113.15(8) . . . . ? P10 Cr3 P6 P7 -129.27(4) . . . . ? P9 Cr3 P6 P7 -90.49(4) . . . . ? P8 Cr3 P6 P7 -37.23(4) . . . . ? C23 Cr3 P6 Cr4 140.3(2) . . . . ? C22 Cr3 P6 Cr4 143.82(9) . . . . ? C25 Cr3 P6 Cr4 -146.04(8) . . . . ? C24 Cr3 P6 Cr4 -133.23(15) . . . . ? C21 Cr3 P6 Cr4 177.84(8) . . . . ? P10 Cr3 P6 Cr4 -64.57(3) . . . . ? P9 Cr3 P6 Cr4 -25.79(3) . . . . ? P8 Cr3 P6 Cr4 27.47(3) . . . . ? P7 Cr3 P6 Cr4 64.70(3) . . . . ? P10 P6 P7 P8 -1.38(6) . . . . ? Cr3 P6 P7 P8 45.33(4) . . . . ? Cr4 P6 P7 P8 -47.20(4) . . . . ? P10 P6 P7 Cr4 45.82(4) . . . . ? Cr3 P6 P7 Cr4 92.52(3) . . . . ? P10 P6 P7 Cr3 -46.70(4) . . . . ? Cr4 P6 P7 Cr3 -92.52(3) . . . . ? C23 Cr3 P7 P8 76.46(10) . . . . ? C22 Cr3 P7 P8 110.78(9) . . . . ? C25 Cr3 P7 P8 159.70(16) . . . . ? C24 Cr3 P7 P8 71.5(2) . . . . ? C21 Cr3 P7 P8 147.37(9) . . . . ? P10 Cr3 P7 P8 -92.35(4) . . . . ? P6 Cr3 P7 P8 -130.78(4) . . . . ? P9 Cr3 P7 P8 -38.69(4) . . . . ? C23 Cr3 P7 P6 -152.76(10) . . . . ? C22 Cr3 P7 P6 -118.44(9) . . . . ? C25 Cr3 P7 P6 -69.51(17) . . . . ? C24 Cr3 P7 P6 -157.7(2) . . . . ? C21 Cr3 P7 P6 -81.85(9) . . . . ? P10 Cr3 P7 P6 38.44(4) . . . . ? P9 Cr3 P7 P6 92.09(4) . . . . ? P8 Cr3 P7 P6 130.78(4) . . . . ? C23 Cr3 P7 Cr4 141.99(9) . . . . ? C22 Cr3 P7 Cr4 176.31(8) . . . . ? C25 Cr3 P7 Cr4 -134.76(16) . . . . ? C24 Cr3 P7 Cr4 137.02(19) . . . . ? C21 Cr3 P7 Cr4 -147.10(9) . . . . ? P10 Cr3 P7 Cr4 -26.81(3) . . . . ? P6 Cr3 P7 Cr4 -65.25(3) . . . . ? P9 Cr3 P7 Cr4 26.84(3) . . . . ? P8 Cr3 P7 Cr4 65.53(3) . . . . ? P6 P7 P8 P9 1.92(6) . . . . ? Cr4 P7 P8 P9 -45.15(4) . . . . ? Cr3 P7 P8 P9 47.13(4) . . . . ? P6 P7 P8 Cr3 -45.20(4) . . . . ? Cr4 P7 P8 Cr3 -92.27(3) . . . . ? P6 P7 P8 Cr4 47.07(4) . . . . ? Cr3 P7 P8 Cr4 92.27(3) . . . . ? C23 Cr3 P8 P7 -119.87(9) . . . . ? C22 Cr3 P8 P7 -84.10(9) . . . . ? C25 Cr3 P8 P7 -156.50(18) . . . . ? C24 Cr3 P8 P7 -153.69(9) . . . . ? C21 Cr3 P8 P7 -72.47(16) . . . . ? P10 Cr3 P8 P7 90.70(4) . . . . ? P6 Cr3 P8 P7 37.28(4) . . . . ? P9 Cr3 P8 P7 128.71(5) . . . . ? C23 Cr3 P8 P9 111.42(9) . . . . ? C22 Cr3 P8 P9 147.19(9) . . . . ? C25 Cr3 P8 P9 74.79(18) . . . . ? C24 Cr3 P8 P9 77.60(9) . . . . ? C21 Cr3 P8 P9 158.81(16) . . . . ? P10 Cr3 P8 P9 -38.01(4) . . . . ? P6 Cr3 P8 P9 -91.43(4) . . . . ? P7 Cr3 P8 P9 -128.71(5) . . . . ? C23 Cr3 P8 Cr4 175.46(8) . . . . ? C22 Cr3 P8 Cr4 -148.78(9) . . . . ? C25 Cr3 P8 Cr4 138.83(18) . . . . ? C24 Cr3 P8 Cr4 141.63(9) . . . . ? C21 Cr3 P8 Cr4 -137.15(16) . . . . ? P10 Cr3 P8 Cr4 26.02(3) . . . . ? P6 Cr3 P8 Cr4 -27.40(3) . . . . ? P9 Cr3 P8 Cr4 64.03(3) . . . . ? P7 Cr3 P8 Cr4 -64.68(3) . . . . ? P7 P8 P9 P10 -1.73(6) . . . . ? Cr3 P8 P9 P10 45.68(4) . . . . ? Cr4 P8 P9 P10 -47.17(4) . . . . ? P7 P8 P9 Cr4 45.43(4) . . . . ? Cr3 P8 P9 Cr4 92.85(3) . . . . ? P7 P8 P9 Cr3 -47.42(4) . . . . ? Cr4 P8 P9 Cr3 -92.85(3) . . . . ? C23 Cr3 P9 P8 -82.22(9) . . . . ? C22 Cr3 P9 P8 -70.96(16) . . . . ? C25 Cr3 P9 P8 -151.73(9) . . . . ? C24 Cr3 P9 P8 -118.13(9) . . . . ? C21 Cr3 P9 P8 -154.37(19) . . . . ? P10 Cr3 P9 P8 130.22(5) . . . . ? P6 Cr3 P9 P8 91.60(4) . . . . ? P7 Cr3 P9 P8 38.53(4) . . . . ? C23 Cr3 P9 P10 147.56(9) . . . . ? C22 Cr3 P9 P10 158.83(15) . . . . ? C25 Cr3 P9 P10 78.06(9) . . . . ? C24 Cr3 P9 P10 111.65(9) . . . . ? C21 Cr3 P9 P10 75.41(19) . . . . ? P6 Cr3 P9 P10 -38.62(4) . . . . ? P8 Cr3 P9 P10 -130.22(5) . . . . ? P7 Cr3 P9 P10 -91.68(4) . . . . ? C23 Cr3 P9 Cr4 -147.75(9) . . . . ? C22 Cr3 P9 Cr4 -136.49(15) . . . . ? C25 Cr3 P9 Cr4 142.74(9) . . . . ? C24 Cr3 P9 Cr4 176.34(9) . . . . ? C21 Cr3 P9 Cr4 140.10(19) . . . . ? P10 Cr3 P9 Cr4 64.69(3) . . . . ? P6 Cr3 P9 Cr4 26.07(4) . . . . ? P8 Cr3 P9 Cr4 -65.53(3) . . . . ? P7 Cr3 P9 Cr4 -27.00(3) . . . . ? P7 P6 P10 P9 0.30(6) . . . . ? Cr3 P6 P10 P9 -46.84(4) . . . . ? Cr4 P6 P10 P9 46.16(4) . . . . ? P7 P6 P10 Cr3 47.14(4) . . . . ? Cr4 P6 P10 Cr3 92.99(3) . . . . ? P7 P6 P10 Cr4 -45.86(4) . . . . ? Cr3 P6 P10 Cr4 -92.99(3) . . . . ? P8 P9 P10 P6 0.89(6) . . . . ? Cr4 P9 P10 P6 -46.67(4) . . . . ? Cr3 P9 P10 P6 46.81(4) . . . . ? P8 P9 P10 Cr3 -45.93(4) . . . . ? Cr4 P9 P10 Cr3 -93.48(3) . . . . ? P8 P9 P10 Cr4 47.56(4) . . . . ? Cr3 P9 P10 Cr4 93.48(3) . . . . ? C23 Cr3 P10 P6 160.64(16) . . . . ? C22 Cr3 P10 P6 77.5(2) . . . . ? C25 Cr3 P10 P6 112.82(9) . . . . ? C24 Cr3 P10 P6 148.94(9) . . . . ? C21 Cr3 P10 P6 79.06(9) . . . . ? P9 Cr3 P10 P6 -129.01(4) . . . . ? P8 Cr3 P10 P6 -91.24(4) . . . . ? P7 Cr3 P10 P6 -38.25(4) . . . . ? C23 Cr3 P10 P9 -70.36(16) . . . . ? C22 Cr3 P10 P9 -153.5(2) . . . . ? C25 Cr3 P10 P9 -118.17(9) . . . . ? C24 Cr3 P10 P9 -82.05(9) . . . . ? C21 Cr3 P10 P9 -151.93(9) . . . . ? P6 Cr3 P10 P9 129.01(4) . . . . ? P8 Cr3 P10 P9 37.76(4) . . . . ? P7 Cr3 P10 P9 90.76(4) . . . . ? C23 Cr3 P10 Cr4 -134.32(16) . . . . ? C22 Cr3 P10 Cr4 142.54(19) . . . . ? C25 Cr3 P10 Cr4 177.86(8) . . . . ? C24 Cr3 P10 Cr4 -146.01(9) . . . . ? C21 Cr3 P10 Cr4 144.10(9) . . . . ? P6 Cr3 P10 Cr4 65.04(3) . . . . ? P9 Cr3 P10 Cr4 -63.96(3) . . . . ? P8 Cr3 P10 Cr4 -26.20(3) . . . . ? P7 Cr3 P10 Cr4 26.80(3) . . . . ? P8 P9 Cr4 C31 162.96(12) . . . . ? P10 P9 Cr4 C31 -68.21(13) . . . . ? Cr3 P9 Cr4 C31 -132.34(12) . . . . ? P8 P9 Cr4 C32 87.0(3) . . . . ? P10 P9 Cr4 C32 -144.2(3) . . . . ? Cr3 P9 Cr4 C32 151.7(2) . . . . ? P8 P9 Cr4 C33 75.56(10) . . . . ? P10 P9 Cr4 C33 -155.61(10) . . . . ? Cr3 P9 Cr4 C33 140.26(9) . . . . ? P8 P9 Cr4 C34 106.27(9) . . . . ? P10 P9 Cr4 C34 -124.90(9) . . . . ? Cr3 P9 Cr4 C34 170.97(9) . . . . ? P8 P9 Cr4 C35 144.00(9) . . . . ? P10 P9 Cr4 C35 -87.18(9) . . . . ? Cr3 P9 Cr4 C35 -151.31(8) . . . . ? P8 P9 Cr4 P10 -128.83(4) . . . . ? Cr3 P9 Cr4 P10 -64.13(3) . . . . ? P8 P9 Cr4 P7 -37.44(4) . . . . ? P10 P9 Cr4 P7 91.38(4) . . . . ? Cr3 P9 Cr4 P7 27.25(3) . . . . ? P8 P9 Cr4 P6 -90.59(4) . . . . ? P10 P9 Cr4 P6 38.23(4) . . . . ? Cr3 P9 Cr4 P6 -25.90(3) . . . . ? P10 P9 Cr4 P8 128.83(4) . . . . ? Cr3 P9 Cr4 P8 64.70(3) . . . . ? P6 P10 Cr4 C31 -87.66(9) . . . . ? P9 P10 Cr4 C31 142.96(9) . . . . ? Cr3 P10 Cr4 C31 -152.36(8) . . . . ? P6 P10 Cr4 C32 -68.81(13) . . . . ? P9 P10 Cr4 C32 161.81(12) . . . . ? Cr3 P10 Cr4 C32 -133.51(12) . . . . ? P6 P10 Cr4 C33 -142.2(2) . . . . ? P9 P10 Cr4 C33 88.4(2) . . . . ? Cr3 P10 Cr4 C33 153.1(2) . . . . ? P6 P10 Cr4 C34 -155.66(10) . . . . ? P9 P10 Cr4 C34 74.96(10) . . . . ? Cr3 P10 Cr4 C34 139.65(10) . . . . ? P6 P10 Cr4 C35 -125.40(9) . . . . ? P9 P10 Cr4 C35 105.23(9) . . . . ? Cr3 P10 Cr4 C35 169.91(9) . . . . ? P6 P10 Cr4 P9 129.38(4) . . . . ? Cr3 P10 Cr4 P9 64.68(3) . . . . ? P6 P10 Cr4 P7 37.66(4) . . . . ? P9 P10 Cr4 P7 -91.71(4) . . . . ? Cr3 P10 Cr4 P7 -27.03(4) . . . . ? P9 P10 Cr4 P6 -129.38(4) . . . . ? Cr3 P10 Cr4 P6 -64.69(3) . . . . ? P6 P10 Cr4 P8 90.71(4) . . . . ? P9 P10 Cr4 P8 -38.67(4) . . . . ? Cr3 P10 Cr4 P8 26.01(3) . . . . ? P8 P7 Cr4 C31 -157.39(9) . . . . ? P6 P7 Cr4 C31 73.50(10) . . . . ? Cr3 P7 Cr4 C31 137.92(9) . . . . ? P8 P7 Cr4 C32 -126.14(8) . . . . ? P6 P7 Cr4 C32 104.76(8) . . . . ? Cr3 P7 Cr4 C32 169.17(8) . . . . ? P8 P7 Cr4 C33 -88.60(9) . . . . ? P6 P7 Cr4 C33 142.29(9) . . . . ? Cr3 P7 Cr4 C33 -153.29(8) . . . . ? P8 P7 Cr4 C34 -70.21(14) . . . . ? P6 P7 Cr4 C34 160.68(14) . . . . ? Cr3 P7 Cr4 C34 -134.91(13) . . . . ? P8 P7 Cr4 C35 -146.5(2) . . . . ? P6 P7 Cr4 C35 84.4(2) . . . . ? Cr3 P7 Cr4 C35 148.8(2) . . . . ? P8 P7 Cr4 P9 37.59(4) . . . . ? P6 P7 Cr4 P9 -91.51(4) . . . . ? Cr3 P7 Cr4 P9 -27.10(3) . . . . ? P8 P7 Cr4 P10 91.44(4) . . . . ? P6 P7 Cr4 P10 -37.67(4) . . . . ? Cr3 P7 Cr4 P10 26.75(4) . . . . ? P8 P7 Cr4 P6 129.11(5) . . . . ? Cr3 P7 Cr4 P6 64.42(3) . . . . ? P6 P7 Cr4 P8 -129.11(5) . . . . ? Cr3 P7 Cr4 P8 -64.69(3) . . . . ? P10 P6 Cr4 C31 104.24(9) . . . . ? P7 P6 Cr4 C31 -125.53(9) . . . . ? Cr3 P6 Cr4 C31 168.89(9) . . . . ? P10 P6 Cr4 C32 142.22(9) . . . . ? P7 P6 Cr4 C32 -87.54(9) . . . . ? Cr3 P6 Cr4 C32 -153.12(9) . . . . ? P10 P6 Cr4 C33 160.12(13) . . . . ? P7 P6 Cr4 C33 -69.65(13) . . . . ? Cr3 P6 Cr4 C33 -135.23(13) . . . . ? P10 P6 Cr4 C34 85.6(2) . . . . ? P7 P6 Cr4 C34 -144.1(2) . . . . ? Cr3 P6 Cr4 C34 150.3(2) . . . . ? P10 P6 Cr4 C35 73.52(10) . . . . ? P7 P6 Cr4 C35 -156.25(10) . . . . ? Cr3 P6 Cr4 C35 138.17(9) . . . . ? P10 P6 Cr4 P9 -38.64(4) . . . . ? P7 P6 Cr4 P9 91.60(4) . . . . ? Cr3 P6 Cr4 P9 26.02(4) . . . . ? P7 P6 Cr4 P10 130.23(5) . . . . ? Cr3 P6 Cr4 P10 64.65(3) . . . . ? P10 P6 Cr4 P7 -130.23(5) . . . . ? Cr3 P6 Cr4 P7 -65.58(3) . . . . ? P10 P6 Cr4 P8 -91.92(4) . . . . ? P7 P6 Cr4 P8 38.31(4) . . . . ? Cr3 P6 Cr4 P8 -27.27(3) . . . . ? P7 P8 Cr4 C31 83.7(3) . . . . ? P9 P8 Cr4 C31 -145.8(3) . . . . ? Cr3 P8 Cr4 C31 149.2(3) . . . . ? P7 P8 Cr4 C32 73.21(9) . . . . ? P9 P8 Cr4 C32 -156.30(9) . . . . ? Cr3 P8 Cr4 C32 138.77(9) . . . . ? P7 P8 Cr4 C33 104.73(8) . . . . ? P9 P8 Cr4 C33 -124.77(8) . . . . ? Cr3 P8 Cr4 C33 170.30(8) . . . . ? P7 P8 Cr4 C34 142.52(9) . . . . ? P9 P8 Cr4 C34 -86.98(9) . . . . ? Cr3 P8 Cr4 C34 -151.91(8) . . . . ? P7 P8 Cr4 C35 161.98(13) . . . . ? P9 P8 Cr4 C35 -67.52(13) . . . . ? Cr3 P8 Cr4 C35 -132.45(13) . . . . ? P7 P8 Cr4 P9 -130.49(5) . . . . ? Cr3 P8 Cr4 P9 -64.93(3) . . . . ? P7 P8 Cr4 P10 -91.50(4) . . . . ? P9 P8 Cr4 P10 38.99(4) . . . . ? Cr3 P8 Cr4 P10 -25.94(3) . . . . ? P9 P8 Cr4 P7 130.49(5) . . . . ? Cr3 P8 Cr4 P7 65.57(3) . . . . ? P7 P8 Cr4 P6 -38.37(4) . . . . ? P9 P8 Cr4 P6 92.12(4) . . . . ? Cr3 P8 Cr4 P6 27.20(3) . . . . ? C32 Cr4 C31 C35 117.6(2) . . . . ? C33 Cr4 C31 C35 79.91(17) . . . . ? C34 Cr4 C31 C35 37.47(16) . . . . ? P9 Cr4 C31 C35 -30.5(2) . . . . ? P10 Cr4 C31 C35 -81.68(16) . . . . ? P7 Cr4 C31 C35 173.95(14) . . . . ? P6 Cr4 C31 C35 -135.40(15) . . . . ? P8 Cr4 C31 C35 103.3(3) . . . . ? C33 Cr4 C31 C32 -37.66(16) . . . . ? C34 Cr4 C31 C32 -80.10(17) . . . . ? C35 Cr4 C31 C32 -117.6(2) . . . . ? P9 Cr4 C31 C32 -148.08(14) . . . . ? P10 Cr4 C31 C32 160.75(14) . . . . ? P7 Cr4 C31 C32 56.38(17) . . . . ? P6 Cr4 C31 C32 107.03(15) . . . . ? P8 Cr4 C31 C32 -14.2(4) . . . . ? C32 Cr4 C31 C36 -121.1(3) . . . . ? C33 Cr4 C31 C36 -158.8(3) . . . . ? C34 Cr4 C31 C36 158.8(3) . . . . ? C35 Cr4 C31 C36 121.3(3) . . . . ? P9 Cr4 C31 C36 90.8(3) . . . . ? P10 Cr4 C31 C36 39.6(3) . . . . ? P7 Cr4 C31 C36 -64.8(3) . . . . ? P6 Cr4 C31 C36 -14.1(3) . . . . ? P8 Cr4 C31 C36 -135.4(3) . . . . ? C35 C31 C32 C33 -0.4(3) . . . . ? C36 C31 C32 C33 -177.9(3) . . . . ? Cr4 C31 C32 C33 62.2(2) . . . . ? C35 C31 C32 C37 177.6(3) . . . . ? C36 C31 C32 C37 0.1(5) . . . . ? Cr4 C31 C32 C37 -119.8(3) . . . . ? C35 C31 C32 Cr4 -62.6(2) . . . . ? C36 C31 C32 Cr4 119.9(3) . . . . ? C31 Cr4 C32 C33 -117.0(2) . . . . ? C34 Cr4 C32 C33 -37.19(17) . . . . ? C35 Cr4 C32 C33 -79.58(18) . . . . ? P9 Cr4 C32 C33 -15.7(4) . . . . ? P10 Cr4 C32 C33 -147.19(14) . . . . ? P7 Cr4 C32 C33 108.03(16) . . . . ? P6 Cr4 C32 C33 161.77(15) . . . . ? P8 Cr4 C32 C33 57.53(18) . . . . ? C33 Cr4 C32 C31 117.0(2) . . . . ? C34 Cr4 C32 C31 79.79(18) . . . . ? C35 Cr4 C32 C31 37.40(16) . . . . ? P9 Cr4 C32 C31 101.3(3) . . . . ? P10 Cr4 C32 C31 -30.2(2) . . . . ? P7 Cr4 C32 C31 -135.00(15) . . . . ? P6 Cr4 C32 C31 -81.26(16) . . . . ? P8 Cr4 C32 C31 174.50(13) . . . . ? C31 Cr4 C32 C37 121.6(3) . . . . ? C33 Cr4 C32 C37 -121.4(3) . . . . ? C34 Cr4 C32 C37 -158.6(3) . . . . ? C35 Cr4 C32 C37 159.0(3) . . . . ? P9 Cr4 C32 C37 -137.1(2) . . . . ? P10 Cr4 C32 C37 91.4(3) . . . . ? P7 Cr4 C32 C37 -13.4(3) . . . . ? P6 Cr4 C32 C37 40.3(3) . . . . ? P8 Cr4 C32 C37 -63.9(3) . . . . ? C31 C32 C33 C34 0.0(3) . . . . ? C37 C32 C33 C34 -178.0(3) . . . . ? Cr4 C32 C33 C34 61.8(2) . . . . ? C31 C32 C33 C38 177.6(3) . . . . ? C37 C32 C33 C38 -0.4(5) . . . . ? Cr4 C32 C33 C38 -120.6(3) . . . . ? C31 C32 C33 Cr4 -61.8(2) . . . . ? C37 C32 C33 Cr4 120.2(3) . . . . ? C31 Cr4 C33 C32 38.04(17) . . . . ? C34 Cr4 C33 C32 118.0(3) . . . . ? C35 Cr4 C33 C32 80.63(19) . . . . ? P9 Cr4 C33 C32 173.77(14) . . . . ? P10 Cr4 C33 C32 99.4(3) . . . . ? P7 Cr4 C33 C32 -80.48(17) . . . . ? P6 Cr4 C33 C32 -28.8(2) . . . . ? P8 Cr4 C33 C32 -134.43(16) . . . . ? C31 Cr4 C33 C34 -79.98(19) . . . . ? C32 Cr4 C33 C34 -118.0(3) . . . . ? C35 Cr4 C33 C34 -37.39(18) . . . . ? P9 Cr4 C33 C34 55.75(19) . . . . ? P10 Cr4 C33 C34 -18.6(3) . . . . ? P7 Cr4 C33 C34 161.50(16) . . . . ? P6 Cr4 C33 C34 -146.80(15) . . . . ? P8 Cr4 C33 C34 107.55(17) . . . . ? C31 Cr4 C33 C38 160.5(3) . . . . ? C32 Cr4 C33 C38 122.4(3) . . . . ? C34 Cr4 C33 C38 -119.5(3) . . . . ? C35 Cr4 C33 C38 -156.9(3) . . . . ? P9 Cr4 C33 C38 -63.8(3) . . . . ? P10 Cr4 C33 C38 -138.2(2) . . . . ? P7 Cr4 C33 C38 41.9(3) . . . . ? P6 Cr4 C33 C38 93.6(3) . . . . ? P8 Cr4 C33 C38 -12.0(3) . . . . ? C32 C33 C34 C35 0.4(3) . . . . ? C38 C33 C34 C35 -177.3(3) . . . . ? Cr4 C33 C34 C35 62.0(2) . . . . ? C32 C33 C34 C39 176.0(3) . . . . ? C38 C33 C34 C39 -1.7(5) . . . . ? Cr4 C33 C34 C39 -122.4(3) . . . . ? C32 C33 C34 Cr4 -61.6(2) . . . . ? C38 C33 C34 Cr4 120.7(3) . . . . ? C31 Cr4 C34 C33 80.13(19) . . . . ? C32 Cr4 C34 C33 37.22(17) . . . . ? C35 Cr4 C34 C33 117.7(3) . . . . ? P9 Cr4 C34 C33 -135.62(16) . . . . ? P10 Cr4 C34 C33 172.45(14) . . . . ? P7 Cr4 C34 C33 -29.5(2) . . . . ? P6 Cr4 C34 C33 100.9(3) . . . . ? P8 Cr4 C34 C33 -81.68(17) . . . . ? C31 Cr4 C34 C35 -37.57(17) . . . . ? C32 Cr4 C34 C35 -80.47(19) . . . . ? C33 Cr4 C34 C35 -117.7(3) . . . . ? P9 Cr4 C34 C35 106.68(16) . . . . ? P10 Cr4 C34 C35 54.75(19) . . . . ? P7 Cr4 C34 C35 -147.22(15) . . . . ? P6 Cr4 C34 C35 -16.8(3) . . . . ? P8 Cr4 C34 C35 160.62(15) . . . . ? C31 Cr4 C34 C39 -159.2(3) . . . . ? C32 Cr4 C34 C39 157.9(3) . . . . ? C33 Cr4 C34 C39 120.7(4) . . . . ? C35 Cr4 C34 C39 -121.6(3) . . . . ? P9 Cr4 C34 C39 -14.9(3) . . . . ? P10 Cr4 C34 C39 -66.9(3) . . . . ? P7 Cr4 C34 C39 91.2(3) . . . . ? P6 Cr4 C34 C39 -138.4(2) . . . . ? P8 Cr4 C34 C39 39.0(3) . . . . ? C32 C31 C35 C34 0.6(3) . . . . ? C36 C31 C35 C34 178.2(3) . . . . ? Cr4 C31 C35 C34 -61.6(2) . . . . ? C32 C31 C35 C40 -176.5(3) . . . . ? C36 C31 C35 C40 1.1(5) . . . . ? Cr4 C31 C35 C40 121.3(3) . . . . ? C32 C31 C35 Cr4 62.2(2) . . . . ? C36 C31 C35 Cr4 -120.2(3) . . . . ? C33 C34 C35 C31 -0.6(3) . . . . ? C39 C34 C35 C31 -176.2(3) . . . . ? Cr4 C34 C35 C31 61.2(2) . . . . ? C33 C34 C35 C40 176.5(3) . . . . ? C39 C34 C35 C40 0.9(5) . . . . ? Cr4 C34 C35 C40 -121.7(3) . . . . ? C33 C34 C35 Cr4 -61.9(2) . . . . ? C39 C34 C35 Cr4 122.6(3) . . . . ? C32 Cr4 C35 C31 -37.69(16) . . . . ? C33 Cr4 C35 C31 -80.12(18) . . . . ? C34 Cr4 C35 C31 -117.5(2) . . . . ? P9 Cr4 C35 C31 160.69(15) . . . . ? P10 Cr4 C35 C31 106.33(16) . . . . ? P7 Cr4 C35 C31 -15.1(3) . . . . ? P6 Cr4 C35 C31 55.67(18) . . . . ? P8 Cr4 C35 C31 -148.68(14) . . . . ? C31 Cr4 C35 C34 117.5(2) . . . . ? C32 Cr4 C35 C34 79.80(18) . . . . ? C33 Cr4 C35 C34 37.37(17) . . . . ? P9 Cr4 C35 C34 -81.82(17) . . . . ? P10 Cr4 C35 C34 -136.19(16) . . . . ? P7 Cr4 C35 C34 102.4(3) . . . . ? P6 Cr4 C35 C34 173.16(14) . . . . ? P8 Cr4 C35 C34 -31.2(2) . . . . ? C31 Cr4 C35 C40 -121.5(3) . . . . ? C32 Cr4 C35 C40 -159.2(3) . . . . ? C33 Cr4 C35 C40 158.3(3) . . . . ? C34 Cr4 C35 C40 121.0(4) . . . . ? P9 Cr4 C35 C40 39.2(3) . . . . ? P10 Cr4 C35 C40 -15.2(3) . . . . ? P7 Cr4 C35 C40 -136.6(3) . . . . ? P6 Cr4 C35 C40 -65.9(3) . . . . ? P8 Cr4 C35 C40 89.8(3) . . . . ? _diffrn_measured_fraction_theta_max 0.925 _diffrn_reflns_theta_full 30.47 _diffrn_measured_fraction_theta_full 0.925 _refine_diff_density_max 1.476 _refine_diff_density_min -0.537 _refine_diff_density_rms 0.115 #===END data_090k _database_code_depnum_ccdc_archive 'CCDC 618757' _audit_creation_method SHELXL-97 _chemical_name_systematic ; \m~2~-\h^5^,\h^5^-cyclopentaphosphole)-bis ((\h^5^-pentamethyl-cyclopentadienyl)-chromium) hexafluoroantimonate ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H30 Cr2 F6 P5 Sb' _chemical_formula_weight 765.04 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M I2/a loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' _cell_length_a 22.9943(10) _cell_length_b 21.2963(9) _cell_length_c 22.9549(11) _cell_angle_alpha 90.00 _cell_angle_beta 101.218(2) _cell_angle_gamma 90.00 _cell_volume 11026.1(9) _cell_formula_units_Z 16 _cell_measurement_temperature 90(2) _cell_measurement_reflns_used 7844 _cell_measurement_theta_min 2.23 _cell_measurement_theta_max 30.47 _exptl_crystal_description 'irregular block' _exptl_crystal_colour 'dark green' _exptl_crystal_size_max 0.60 _exptl_crystal_size_mid 0.52 _exptl_crystal_size_min 0.40 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.843 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 6048 _exptl_absorpt_coefficient_mu 2.088 _exptl_absorpt_correction_type integration _exptl_absorpt_correction_T_min 0.388 _exptl_absorpt_correction_T_max 0.608 _exptl_absorpt_process_details 'XPREP in SHELXTL' _exptl_special_details ; ? ; _diffrn_ambient_temperature 90(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'Bede Microsource X-ray Generator' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEX CCD Diffractometer' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number 0 _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% 0 _diffrn_reflns_number 40538 _diffrn_reflns_av_R_equivalents 0.0332 _diffrn_reflns_av_sigmaI/netI 0.0419 _diffrn_reflns_limit_h_min -32 _diffrn_reflns_limit_h_max 32 _diffrn_reflns_limit_k_min -30 _diffrn_reflns_limit_k_max 29 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_limit_l_max 31 _diffrn_reflns_theta_min 1.15 _diffrn_reflns_theta_max 30.48 _reflns_number_total 15483 _reflns_number_gt 14625 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'SMART V5.625 (Bruker, 2003)' _computing_cell_refinement 'SMART V5.625 (Bruker, 2003)' _computing_data_reduction 'SAINT V6.28A (Bruker, 2003)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'SHELXTL V6.12(Bruker, 2001)' _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0394P)^2^+7.9276P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 15483 _refine_ls_number_parameters 614 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0298 _refine_ls_R_factor_gt 0.0270 _refine_ls_wR_factor_ref 0.0772 _refine_ls_wR_factor_gt 0.0710 _refine_ls_goodness_of_fit_ref 1.043 _refine_ls_restrained_S_all 1.043 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb1 Sb 0.138751(9) 0.869716(9) 0.383944(9) 0.01950(4) Uani 1 1 d . . . F1 F 0.09727(10) 0.80928(10) 0.33230(11) 0.0392(5) Uani 1 1 d . . . F2 F 0.09100(11) 0.93224(10) 0.34160(10) 0.0414(5) Uani 1 1 d . . . F3 F 0.08400(9) 0.86156(11) 0.43450(10) 0.0349(5) Uani 1 1 d . . . F4 F 0.18461(8) 0.80629(9) 0.42698(10) 0.0292(4) Uani 1 1 d . . . F5 F 0.19452(10) 0.87738(10) 0.33442(10) 0.0350(5) Uani 1 1 d . . . F6 F 0.18017(10) 0.93085(9) 0.43403(9) 0.0329(4) Uani 1 1 d . . . Sb2 Sb 0.136906(9) 0.126756(9) 0.117290(9) 0.01787(4) Uani 1 1 d . . . F7 F 0.12440(14) 0.05177(11) 0.15388(13) 0.0606(8) Uani 1 1 d . . . F8 F 0.07367(10) 0.16406(12) 0.14453(11) 0.0453(6) Uani 1 1 d . . . F9 F 0.08513(9) 0.10058(11) 0.04830(10) 0.0383(5) Uani 1 1 d . . . F10 F 0.20141(10) 0.09238(12) 0.08903(11) 0.0459(6) Uani 1 1 d . . . F11 F 0.18862(9) 0.15266(11) 0.18621(9) 0.0384(5) Uani 1 1 d . . . F12 F 0.14981(10) 0.20232(10) 0.08053(11) 0.0411(5) Uani 1 1 d . . . C1 C -0.11404(12) 0.31121(13) 0.44743(13) 0.0175(5) Uani 1 1 d . . . C2 C -0.14271(11) 0.26864(12) 0.40257(13) 0.0170(5) Uani 1 1 d . . . C3 C -0.14186(11) 0.29612(13) 0.34630(13) 0.0163(5) Uani 1 1 d . . . C4 C -0.11255(12) 0.35599(12) 0.35569(12) 0.0158(5) Uani 1 1 d . . . C5 C -0.09556(12) 0.36505(13) 0.41817(13) 0.0161(5) Uani 1 1 d . . . C6 C -0.10739(14) 0.30325(15) 0.51232(13) 0.0241(6) Uani 1 1 d . . . H6A H -0.1401 0.3245 0.5259 0.036 Uiso 1 1 calc R . . H6B H -0.0696 0.3216 0.5322 0.036 Uiso 1 1 calc R . . H6C H -0.1080 0.2584 0.5218 0.036 Uiso 1 1 calc R . . C7 C -0.17156(13) 0.20800(13) 0.41384(15) 0.0225(6) Uani 1 1 d . . . H7A H -0.2134 0.2155 0.4147 0.034 Uiso 1 1 calc R . . H7B H -0.1516 0.1907 0.4521 0.034 Uiso 1 1 calc R . . H7C H -0.1685 0.1781 0.3821 0.034 Uiso 1 1 calc R . . C8 C -0.16885(13) 0.26973(14) 0.28652(13) 0.0211(6) Uani 1 1 d . . . H8A H -0.2050 0.2931 0.2700 0.032 Uiso 1 1 calc R . . H8B H -0.1786 0.2254 0.2907 0.032 Uiso 1 1 calc R . . H8C H -0.1405 0.2735 0.2599 0.032 Uiso 1 1 calc R . . C9 C -0.10434(13) 0.40193(13) 0.30850(13) 0.0212(5) Uani 1 1 d . . . H9A H -0.1413 0.4253 0.2952 0.032 Uiso 1 1 calc R . . H9B H -0.0940 0.3793 0.2748 0.032 Uiso 1 1 calc R . . H9C H -0.0724 0.4313 0.3246 0.032 Uiso 1 1 calc R . . C10 C -0.06786(13) 0.42282(13) 0.44925(14) 0.0213(5) Uani 1 1 d . . . H10A H -0.0975 0.4455 0.4665 0.032 Uiso 1 1 calc R . . H10B H -0.0534 0.4500 0.4207 0.032 Uiso 1 1 calc R . . H10C H -0.0346 0.4107 0.4808 0.032 Uiso 1 1 calc R . . Cr1 Cr -0.049812(18) 0.280459(19) 0.392697(19) 0.01312(8) Uani 1 1 d . . . P1 P 0.03395(4) 0.26842(5) 0.47166(4) 0.0379(2) Uani 1 1 d . . . P2 P -0.01456(4) 0.18255(4) 0.43662(5) 0.0362(2) Uani 1 1 d . . . P3 P -0.03318(3) 0.18825(4) 0.33929(5) 0.0347(2) Uani 1 1 d . . . P4 P 0.00284(4) 0.27792(5) 0.31286(4) 0.0344(2) Uani 1 1 d . . . P5 P 0.04439(4) 0.32738(4) 0.39500(6) 0.0353(2) Uani 1 1 d . . . Cr2 Cr 0.063574(18) 0.217926(19) 0.38933(2) 0.01313(8) Uani 1 1 d . . . C11 C 0.14676(11) 0.17741(12) 0.44060(12) 0.0149(5) Uani 1 1 d . . . C12 C 0.11646(12) 0.13026(12) 0.40183(13) 0.0161(5) Uani 1 1 d . . . C13 C 0.11247(12) 0.15131(13) 0.34238(13) 0.0173(5) Uani 1 1 d . . . C14 C 0.14015(12) 0.21125(13) 0.34409(13) 0.0173(5) Uani 1 1 d . . . C15 C 0.16128(11) 0.22784(12) 0.40492(12) 0.0155(5) Uani 1 1 d . . . C16 C 0.16332(13) 0.17181(14) 0.50625(13) 0.0214(5) Uani 1 1 d . . . H16A H 0.2004 0.1481 0.5169 0.032 Uiso 1 1 calc R . . H16B H 0.1318 0.1498 0.5212 0.032 Uiso 1 1 calc R . . H16C H 0.1687 0.2138 0.5239 0.032 Uiso 1 1 calc R . . C17 C 0.09567(13) 0.06808(13) 0.42055(15) 0.0243(6) Uani 1 1 d . . . H17A H 0.1287 0.0381 0.4265 0.037 Uiso 1 1 calc R . . H17B H 0.0635 0.0523 0.3896 0.037 Uiso 1 1 calc R . . H17C H 0.0813 0.0731 0.4577 0.037 Uiso 1 1 calc R . . C18 C 0.08795(13) 0.11447(15) 0.28723(15) 0.0247(6) Uani 1 1 d . . . H18A H 0.1197 0.0897 0.2756 0.037 Uiso 1 1 calc R . . H18B H 0.0714 0.1434 0.2551 0.037 Uiso 1 1 calc R . . H18C H 0.0567 0.0863 0.2951 0.037 Uiso 1 1 calc R . . C19 C 0.14842(13) 0.24915(15) 0.29143(14) 0.0230(6) Uani 1 1 d . . . H19A H 0.1892 0.2443 0.2854 0.035 Uiso 1 1 calc R . . H19B H 0.1407 0.2935 0.2984 0.035 Uiso 1 1 calc R . . H19C H 0.1208 0.2345 0.2561 0.035 Uiso 1 1 calc R . . C20 C 0.19549(12) 0.28598(13) 0.42632(14) 0.0209(6) Uani 1 1 d . . . H20A H 0.2373 0.2800 0.4242 0.031 Uiso 1 1 calc R . . H20B H 0.1922 0.2944 0.4675 0.031 Uiso 1 1 calc R . . H20C H 0.1794 0.3216 0.4013 0.031 Uiso 1 1 calc R . . C21 C 0.10724(12) 0.38501(12) 0.13246(13) 0.0157(5) Uani 1 1 d . . . C22 C 0.17093(12) 0.38190(12) 0.14563(13) 0.0165(5) Uani 1 1 d . . . C23 C 0.19362(12) 0.43769(13) 0.12410(13) 0.0183(5) Uani 1 1 d . . . C24 C 0.14474(13) 0.47585(12) 0.09716(13) 0.0181(5) Uani 1 1 d . . . C25 C 0.09140(12) 0.44327(13) 0.10268(12) 0.0165(5) Uani 1 1 d . . . C26 C 0.06465(13) 0.33504(13) 0.14290(14) 0.0213(5) Uani 1 1 d . . . H26A H 0.0670 0.2995 0.1164 0.032 Uiso 1 1 calc R . . H26B H 0.0243 0.3520 0.1349 0.032 Uiso 1 1 calc R . . H26C H 0.0748 0.3209 0.1843 0.032 Uiso 1 1 calc R . . C27 C 0.20777(13) 0.32745(13) 0.17307(14) 0.0220(6) Uani 1 1 d . . . H27A H 0.2270 0.3077 0.1432 0.033 Uiso 1 1 calc R . . H27B H 0.1823 0.2967 0.1877 0.033 Uiso 1 1 calc R . . H27C H 0.2381 0.3424 0.2062 0.033 Uiso 1 1 calc R . . C28 C 0.25804(13) 0.45101(16) 0.12519(16) 0.0274(7) Uani 1 1 d . . . H28A H 0.2686 0.4359 0.0883 0.041 Uiso 1 1 calc R . . H28B H 0.2824 0.4294 0.1591 0.041 Uiso 1 1 calc R . . H28C H 0.2651 0.4963 0.1289 0.041 Uiso 1 1 calc R . . C29 C 0.14920(15) 0.53698(14) 0.06591(14) 0.0253(6) Uani 1 1 d . . . H29A H 0.1516 0.5288 0.0244 0.038 Uiso 1 1 calc R . . H29B H 0.1848 0.5595 0.0855 0.038 Uiso 1 1 calc R . . H29C H 0.1141 0.5626 0.0673 0.038 Uiso 1 1 calc R . . C30 C 0.02896(13) 0.46466(15) 0.07777(13) 0.0232(6) Uani 1 1 d . . . H30A H 0.0158 0.4466 0.0381 0.035 Uiso 1 1 calc R . . H30B H 0.0280 0.5106 0.0751 0.035 Uiso 1 1 calc R . . H30C H 0.0025 0.4507 0.1039 0.035 Uiso 1 1 calc R . . Cr3 Cr 0.142824(19) 0.463613(19) 0.19214(2) 0.01393(8) Uani 1 1 d . . . P6 P 0.08589(3) 0.44351(4) 0.26917(4) 0.02220(15) Uani 1 1 d . . . P7 P 0.18177(4) 0.42960(3) 0.29467(3) 0.02249(15) Uani 1 1 d . . . P8 P 0.22593(3) 0.50929(4) 0.26178(4) 0.02336(15) Uani 1 1 d . . . P9 P 0.15713(4) 0.57435(3) 0.21874(3) 0.02199(15) Uani 1 1 d . . . P10 P 0.07022(3) 0.53312(4) 0.22249(3) 0.02173(15) Uani 1 1 d . . . Cr4 Cr 0.144768(18) 0.533399(19) 0.313913(19) 0.01326(8) Uani 1 1 d . . . C31 C 0.09597(12) 0.55187(13) 0.38526(12) 0.0166(5) Uani 1 1 d . . . C32 C 0.15211(12) 0.52401(12) 0.41048(12) 0.0167(5) Uani 1 1 d . . . C33 C 0.19736(12) 0.56577(12) 0.39938(12) 0.0156(5) Uani 1 1 d . . . C34 C 0.16957(13) 0.61894(12) 0.36785(13) 0.0160(5) Uani 1 1 d . . . C35 C 0.10680(12) 0.61041(12) 0.35908(12) 0.0163(5) Uani 1 1 d . . . C36 C 0.03607(13) 0.52535(15) 0.38793(14) 0.0239(6) Uani 1 1 d . . . H36A H 0.0201 0.5467 0.4192 0.036 Uiso 1 1 calc R . . H36B H 0.0398 0.4803 0.3967 0.036 Uiso 1 1 calc R . . H36C H 0.0093 0.5317 0.3496 0.036 Uiso 1 1 calc R . . C37 C 0.16165(14) 0.46330(13) 0.44427(13) 0.0210(6) Uani 1 1 d . . . H37A H 0.1647 0.4716 0.4867 0.032 Uiso 1 1 calc R . . H37B H 0.1983 0.4436 0.4377 0.032 Uiso 1 1 calc R . . H37C H 0.1281 0.4351 0.4304 0.032 Uiso 1 1 calc R . . C38 C 0.26338(12) 0.55810(14) 0.41935(14) 0.0216(6) Uani 1 1 d . . . H38A H 0.2757 0.5759 0.4592 0.032 Uiso 1 1 calc R . . H38B H 0.2838 0.5800 0.3917 0.032 Uiso 1 1 calc R . . H38C H 0.2735 0.5134 0.4202 0.032 Uiso 1 1 calc R . . C39 C 0.20107(14) 0.67547(13) 0.35056(14) 0.0227(6) Uani 1 1 d . . . H39A H 0.2090 0.7049 0.3840 0.034 Uiso 1 1 calc R . . H39B H 0.1762 0.6960 0.3163 0.034 Uiso 1 1 calc R . . H39C H 0.2386 0.6625 0.3401 0.034 Uiso 1 1 calc R . . C40 C 0.06084(13) 0.65663(14) 0.33041(13) 0.0239(6) Uani 1 1 d . . . H40A H 0.0513 0.6853 0.3606 0.036 Uiso 1 1 calc R . . H40B H 0.0249 0.6341 0.3115 0.036 Uiso 1 1 calc R . . H40C H 0.0762 0.6808 0.3003 0.036 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.02142(9) 0.01654(8) 0.02163(10) -0.00188(7) 0.00688(6) 0.00173(7) F1 0.0350(11) 0.0345(11) 0.0452(13) -0.0151(10) 0.0006(9) -0.0062(9) F2 0.0584(15) 0.0316(10) 0.0322(11) 0.0041(9) 0.0039(10) 0.0192(10) F3 0.0272(10) 0.0433(11) 0.0391(12) 0.0057(10) 0.0182(8) 0.0089(9) F4 0.0228(9) 0.0256(9) 0.0410(11) 0.0071(8) 0.0104(8) 0.0081(7) F5 0.0386(12) 0.0430(12) 0.0283(11) -0.0032(8) 0.0188(9) -0.0053(9) F6 0.0471(12) 0.0255(9) 0.0270(10) -0.0076(8) 0.0092(8) -0.0083(9) Sb2 0.01830(10) 0.01631(7) 0.01942(10) -0.00020(6) 0.00470(6) 0.00058(6) F7 0.090(2) 0.0299(11) 0.0565(16) 0.0209(11) 0.0009(15) -0.0152(13) F8 0.0298(11) 0.0632(16) 0.0468(13) -0.0089(12) 0.0177(9) 0.0058(11) F9 0.0336(11) 0.0445(12) 0.0329(11) -0.0100(10) -0.0029(9) -0.0071(9) F10 0.0339(11) 0.0569(15) 0.0469(14) -0.0217(11) 0.0077(10) 0.0174(10) F11 0.0340(11) 0.0473(13) 0.0296(11) -0.0148(9) -0.0050(8) 0.0049(9) F12 0.0409(12) 0.0320(11) 0.0481(14) 0.0173(10) 0.0031(10) -0.0090(9) C1 0.0176(12) 0.0167(11) 0.0197(13) -0.0041(10) 0.0075(10) -0.0018(10) C2 0.0106(11) 0.0180(11) 0.0234(13) -0.0034(10) 0.0055(9) -0.0018(9) C3 0.0089(10) 0.0179(12) 0.0213(13) -0.0035(10) 0.0007(9) -0.0009(9) C4 0.0136(11) 0.0153(11) 0.0187(13) 0.0000(10) 0.0037(9) 0.0019(9) C5 0.0144(11) 0.0148(11) 0.0196(13) -0.0021(10) 0.0047(9) 0.0005(9) C6 0.0286(15) 0.0278(14) 0.0175(13) -0.0010(11) 0.0087(11) -0.0008(12) C7 0.0162(12) 0.0181(12) 0.0346(16) -0.0015(11) 0.0081(11) -0.0034(10) C8 0.0172(12) 0.0243(13) 0.0208(13) -0.0065(11) 0.0010(10) -0.0024(10) C9 0.0237(14) 0.0179(12) 0.0226(14) 0.0036(11) 0.0061(11) 0.0001(10) C10 0.0210(13) 0.0198(13) 0.0232(14) -0.0047(11) 0.0050(10) -0.0049(10) Cr1 0.01178(18) 0.01308(18) 0.01472(19) -0.00152(15) 0.00310(14) -0.00228(14) P1 0.0233(4) 0.0639(6) 0.0227(4) -0.0168(4) -0.0047(3) 0.0208(4) P2 0.0252(4) 0.0306(4) 0.0597(6) 0.0230(4) 0.0257(4) 0.0126(3) P3 0.0132(3) 0.0343(4) 0.0536(6) -0.0278(4) -0.0007(3) 0.0018(3) P4 0.0247(4) 0.0552(6) 0.0265(4) 0.0165(4) 0.0130(3) 0.0214(4) P5 0.0140(3) 0.0160(3) 0.0772(7) -0.0065(4) 0.0121(4) -0.0018(3) Cr2 0.01160(18) 0.01275(17) 0.01521(19) -0.00077(15) 0.00301(14) -0.00151(14) C11 0.0131(11) 0.0155(11) 0.0160(12) 0.0028(9) 0.0030(9) 0.0021(9) C12 0.0115(11) 0.0135(10) 0.0241(14) -0.0007(10) 0.0060(10) 0.0010(9) C13 0.0141(11) 0.0178(11) 0.0204(12) -0.0011(10) 0.0047(9) 0.0015(9) C14 0.0120(11) 0.0200(12) 0.0208(13) -0.0003(10) 0.0054(9) 0.0015(9) C15 0.0117(11) 0.0157(10) 0.0191(13) 0.0017(10) 0.0034(9) 0.0011(9) C16 0.0207(13) 0.0258(13) 0.0177(12) 0.0021(11) 0.0032(10) 0.0068(11) C17 0.0231(14) 0.0136(11) 0.0397(17) 0.0010(12) 0.0144(12) -0.0021(10) C18 0.0191(13) 0.0283(15) 0.0264(15) -0.0095(12) 0.0036(11) -0.0012(11) C19 0.0201(13) 0.0287(14) 0.0222(14) 0.0103(11) 0.0087(10) 0.0066(11) C20 0.0135(12) 0.0161(12) 0.0324(15) 0.0007(11) 0.0028(10) -0.0023(9) C21 0.0139(12) 0.0152(11) 0.0178(13) -0.0002(9) 0.0028(9) -0.0007(9) C22 0.0147(12) 0.0166(12) 0.0178(13) -0.0012(9) 0.0026(10) 0.0041(9) C23 0.0140(11) 0.0188(12) 0.0232(13) -0.0009(10) 0.0059(10) 0.0013(10) C24 0.0230(13) 0.0174(11) 0.0155(12) 0.0023(10) 0.0073(10) 0.0011(10) C25 0.0174(12) 0.0161(12) 0.0164(12) 0.0009(9) 0.0040(9) 0.0024(10) C26 0.0211(13) 0.0194(13) 0.0238(14) 0.0010(11) 0.0054(11) -0.0063(10) C27 0.0220(13) 0.0180(12) 0.0250(14) 0.0009(11) 0.0023(11) 0.0072(10) C28 0.0179(13) 0.0315(15) 0.0369(18) -0.0059(13) 0.0153(12) -0.0011(12) C29 0.0377(17) 0.0173(12) 0.0235(14) 0.0039(11) 0.0127(12) -0.0004(12) C30 0.0186(13) 0.0297(15) 0.0196(13) 0.0047(11) -0.0006(10) 0.0078(11) Cr3 0.01155(18) 0.01344(18) 0.0173(2) 0.00203(15) 0.00396(15) 0.00129(14) P6 0.0232(4) 0.0229(3) 0.0230(4) -0.0058(3) 0.0106(3) -0.0091(3) P7 0.0300(4) 0.0176(3) 0.0188(3) 0.0011(3) 0.0019(3) 0.0072(3) P8 0.0141(3) 0.0316(4) 0.0251(4) -0.0075(3) 0.0057(3) -0.0029(3) P9 0.0339(4) 0.0148(3) 0.0188(3) 0.0007(3) 0.0089(3) -0.0033(3) P10 0.0173(3) 0.0264(4) 0.0199(3) -0.0048(3) -0.0003(3) 0.0084(3) Cr4 0.01169(18) 0.01295(18) 0.0152(2) 0.00093(15) 0.00274(14) -0.00040(14) C31 0.0125(11) 0.0210(12) 0.0171(12) -0.0030(10) 0.0050(9) -0.0036(9) C32 0.0188(12) 0.0158(11) 0.0153(12) 0.0007(9) 0.0026(9) -0.0036(10) C33 0.0150(11) 0.0143(11) 0.0166(12) -0.0004(9) 0.0011(9) -0.0014(9) C34 0.0166(12) 0.0143(11) 0.0176(12) -0.0014(9) 0.0049(10) -0.0027(9) C35 0.0157(12) 0.0167(10) 0.0161(12) -0.0030(9) 0.0017(9) -0.0001(9) C36 0.0193(13) 0.0305(15) 0.0235(14) -0.0048(12) 0.0079(11) -0.0065(11) C37 0.0278(14) 0.0175(12) 0.0170(12) 0.0040(10) 0.0025(10) -0.0035(10) C38 0.0136(12) 0.0254(14) 0.0242(14) 0.0003(11) -0.0001(10) -0.0004(10) C39 0.0280(14) 0.0158(12) 0.0246(14) 0.0014(10) 0.0053(11) -0.0048(11) C40 0.0222(13) 0.0255(14) 0.0213(13) -0.0021(11) -0.0023(11) 0.0088(11) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb1 F6 1.8702(19) . ? Sb1 F4 1.8728(18) . ? Sb1 F2 1.873(2) . ? Sb1 F5 1.879(2) . ? Sb1 F3 1.879(2) . ? Sb1 F1 1.879(2) . ? Sb2 F7 1.853(2) . ? Sb2 F12 1.867(2) . ? Sb2 F8 1.868(2) . ? Sb2 F11 1.8680(19) . ? Sb2 F9 1.872(2) . ? Sb2 F10 1.879(2) . ? C1 C2 1.433(4) . ? C1 C5 1.434(4) . ? C1 C6 1.477(4) . ? C1 Cr1 2.216(3) . ? C2 C3 1.421(4) . ? C2 C7 1.497(4) . ? C2 Cr1 2.206(3) . ? C3 C4 1.439(4) . ? C3 C8 1.501(4) . ? C3 Cr1 2.202(3) . ? C4 C5 1.424(4) . ? C4 C9 1.498(4) . ? C4 Cr1 2.217(3) . ? C5 C10 1.500(4) . ? C5 Cr1 2.221(3) . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? Cr1 P5 2.3768(9) . ? Cr1 P3 2.3850(9) . ? Cr1 P4 2.3855(10) . ? Cr1 P2 2.3881(9) . ? Cr1 P1 2.3880(9) . ? Cr1 Cr2 2.9420(6) . ? P1 P2 2.2105(16) . ? P1 P5 2.2126(16) . ? P1 Cr2 2.3861(10) . ? P2 P3 2.1949(16) . ? P2 Cr2 2.3944(10) . ? P3 P4 2.2128(15) . ? P3 Cr2 2.3821(9) . ? P4 P5 2.2083(16) . ? P4 Cr2 2.3895(9) . ? P5 Cr2 2.3805(9) . ? Cr2 C15 2.215(3) . ? Cr2 C13 2.216(3) . ? Cr2 C12 2.216(3) . ? Cr2 C14 2.216(3) . ? Cr2 C11 2.216(3) . ? C11 C15 1.429(4) . ? C11 C12 1.430(4) . ? C11 C16 1.486(4) . ? C12 C13 1.422(4) . ? C12 C17 1.499(4) . ? C13 C14 1.423(4) . ? C13 C18 1.503(4) . ? C14 C15 1.431(4) . ? C14 C19 1.496(4) . ? C15 C20 1.498(4) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 C25 1.429(4) . ? C21 C22 1.438(4) . ? C21 C26 1.497(4) . ? C21 Cr3 2.216(3) . ? C22 C23 1.424(4) . ? C22 C27 1.500(4) . ? C22 Cr3 2.203(3) . ? C23 C24 1.427(4) . ? C23 C28 1.504(4) . ? C23 Cr3 2.195(3) . ? C24 C25 1.436(4) . ? C24 C29 1.499(4) . ? C24 Cr3 2.205(3) . ? C25 C30 1.509(4) . ? C25 Cr3 2.204(3) . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C27 H27C 0.9800 . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? Cr3 P10 2.4322(8) . ? Cr3 P6 2.4340(9) . ? Cr3 P9 2.4423(9) . ? Cr3 P8 2.4424(9) . ? Cr3 P7 2.4588(9) . ? P6 P10 2.1840(11) . ? P6 P7 2.1885(11) . ? P6 Cr4 2.4518(8) . ? P7 P8 2.1862(12) . ? P7 Cr4 2.4397(8) . ? P8 P9 2.1888(11) . ? P8 Cr4 2.4591(9) . ? P9 P10 2.1997(12) . ? P9 Cr4 2.4199(9) . ? P10 Cr4 2.4378(8) . ? Cr4 C31 2.193(3) . ? Cr4 C32 2.199(3) . ? Cr4 C33 2.205(3) . ? Cr4 C35 2.209(3) . ? Cr4 C34 2.214(3) . ? C31 C35 1.427(4) . ? C31 C32 1.436(4) . ? C31 C36 1.501(4) . ? C32 C33 1.429(4) . ? C32 C37 1.502(4) . ? C33 C34 1.426(4) . ? C33 C38 1.507(4) . ? C34 C35 1.430(4) . ? C34 C39 1.498(4) . ? C35 C40 1.500(4) . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C39 H39A 0.9800 . ? C39 H39B 0.9800 . ? C39 H39C 0.9800 . ? C40 H40A 0.9800 . ? C40 H40B 0.9800 . ? C40 H40C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F6 Sb1 F4 90.61(9) . . ? F6 Sb1 F2 90.07(10) . . ? F4 Sb1 F2 178.38(11) . . ? F6 Sb1 F5 89.18(10) . . ? F4 Sb1 F5 90.07(9) . . ? F2 Sb1 F5 91.40(11) . . ? F6 Sb1 F3 90.40(10) . . ? F4 Sb1 F3 89.07(9) . . ? F2 Sb1 F3 89.46(11) . . ? F5 Sb1 F3 179.04(9) . . ? F6 Sb1 F1 178.86(10) . . ? F4 Sb1 F1 90.19(10) . . ? F2 Sb1 F1 89.15(10) . . ? F5 Sb1 F1 90.01(10) . . ? F3 Sb1 F1 90.43(11) . . ? F7 Sb2 F12 179.79(13) . . ? F7 Sb2 F8 90.88(14) . . ? F12 Sb2 F8 89.27(11) . . ? F7 Sb2 F11 90.00(12) . . ? F12 Sb2 F11 89.85(10) . . ? F8 Sb2 F11 89.97(10) . . ? F7 Sb2 F9 89.86(11) . . ? F12 Sb2 F9 90.29(10) . . ? F8 Sb2 F9 90.09(10) . . ? F11 Sb2 F9 179.85(12) . . ? F7 Sb2 F10 91.33(14) . . ? F12 Sb2 F10 88.53(11) . . ? F8 Sb2 F10 177.75(12) . . ? F11 Sb2 F10 89.56(10) . . ? F9 Sb2 F10 90.39(10) . . ? C2 C1 C5 107.8(2) . . ? C2 C1 C6 126.5(3) . . ? C5 C1 C6 125.6(3) . . ? C2 C1 Cr1 70.72(16) . . ? C5 C1 Cr1 71.34(16) . . ? C6 C1 Cr1 126.0(2) . . ? C3 C2 C1 107.9(2) . . ? C3 C2 C7 126.7(3) . . ? C1 C2 C7 125.4(3) . . ? C3 C2 Cr1 71.03(15) . . ? C1 C2 Cr1 71.47(15) . . ? C7 C2 Cr1 125.92(19) . . ? C2 C3 C4 108.5(2) . . ? C2 C3 C8 126.9(2) . . ? C4 C3 C8 124.5(3) . . ? C2 C3 Cr1 71.34(15) . . ? C4 C3 Cr1 71.55(14) . . ? C8 C3 Cr1 124.96(19) . . ? C5 C4 C3 107.4(2) . . ? C5 C4 C9 126.2(2) . . ? C3 C4 C9 126.3(3) . . ? C5 C4 Cr1 71.45(15) . . ? C3 C4 Cr1 70.44(14) . . ? C9 C4 Cr1 125.93(19) . . ? C4 C5 C1 108.4(2) . . ? C4 C5 C10 126.7(3) . . ? C1 C5 C10 124.7(3) . . ? C4 C5 Cr1 71.11(15) . . ? C1 C5 Cr1 70.94(15) . . ? C10 C5 Cr1 127.67(19) . . ? C1 C6 H6A 109.5 . . ? C1 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C1 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C3 Cr1 C2 37.63(11) . . ? C3 Cr1 C1 62.97(10) . . ? C2 Cr1 C1 37.81(10) . . ? C3 Cr1 C4 38.01(9) . . ? C2 Cr1 C4 63.33(10) . . ? C1 Cr1 C4 63.06(10) . . ? C3 Cr1 C5 62.90(10) . . ? C2 Cr1 C5 63.12(10) . . ? C1 Cr1 C5 37.72(10) . . ? C4 Cr1 C5 37.44(10) . . ? C3 Cr1 P5 137.16(8) . . ? C2 Cr1 P5 160.44(7) . . ? C1 Cr1 P5 124.62(8) . . ? C4 Cr1 P5 103.05(7) . . ? C5 Cr1 P5 97.44(7) . . ? C3 Cr1 P3 96.39(7) . . ? C2 Cr1 P3 102.37(7) . . ? C1 Cr1 P3 136.55(8) . . ? C4 Cr1 P3 123.92(8) . . ? C5 Cr1 P3 159.18(8) . . ? P5 Cr1 P3 96.95(3) . . ? C3 Cr1 P4 102.45(8) . . ? C2 Cr1 P4 136.27(8) . . ? C1 Cr1 P4 159.41(8) . . ? C4 Cr1 P4 96.42(7) . . ? C5 Cr1 P4 123.90(8) . . ? P5 Cr1 P4 55.25(4) . . ? P3 Cr1 P4 55.27(4) . . ? C3 Cr1 P2 123.49(8) . . ? C2 Cr1 P2 96.48(8) . . ? C1 Cr1 P2 103.16(8) . . ? C4 Cr1 P2 159.64(7) . . ? C5 Cr1 P2 137.41(8) . . ? P5 Cr1 P2 97.16(4) . . ? P3 Cr1 P2 54.75(4) . . ? P4 Cr1 P2 97.08(4) . . ? C3 Cr1 P1 160.19(8) . . ? C2 Cr1 P1 124.33(8) . . ? C1 Cr1 P1 97.44(8) . . ? C4 Cr1 P1 137.52(8) . . ? C5 Cr1 P1 103.92(8) . . ? P5 Cr1 P1 55.34(4) . . ? P3 Cr1 P1 96.63(3) . . ? P4 Cr1 P1 97.23(4) . . ? P2 Cr1 P1 55.14(4) . . ? C3 Cr1 Cr2 146.02(8) . . ? C2 Cr1 Cr2 146.29(7) . . ? C1 Cr1 Cr2 147.19(8) . . ? C4 Cr1 Cr2 146.34(7) . . ? C5 Cr1 Cr2 147.31(7) . . ? P5 Cr1 Cr2 51.86(2) . . ? P3 Cr1 Cr2 51.85(2) . . ? P4 Cr1 Cr2 52.03(2) . . ? P2 Cr1 Cr2 52.13(2) . . ? P1 Cr1 Cr2 51.93(2) . . ? P2 P1 P5 107.77(5) . . ? P2 P1 Cr2 62.65(4) . . ? P5 P1 Cr2 62.21(4) . . ? P2 P1 Cr1 62.43(3) . . ? P5 P1 Cr1 62.07(3) . . ? Cr2 P1 Cr1 76.08(3) . . ? P3 P2 P1 108.02(5) . . ? P3 P2 Cr1 62.55(4) . . ? P1 P2 Cr1 62.43(3) . . ? P3 P2 Cr2 62.36(4) . . ? P1 P2 Cr2 62.27(4) . . ? Cr1 P2 Cr2 75.93(3) . . ? P2 P3 P4 108.51(5) . . ? P2 P3 Cr2 62.93(4) . . ? P4 P3 Cr2 62.54(3) . . ? P2 P3 Cr1 62.70(3) . . ? P4 P3 Cr1 62.38(4) . . ? Cr2 P3 Cr1 76.22(3) . . ? P5 P4 P3 107.48(5) . . ? P5 P4 Cr1 62.17(4) . . ? P3 P4 Cr1 62.35(3) . . ? P5 P4 Cr2 62.22(4) . . ? P3 P4 Cr2 62.20(3) . . ? Cr1 P4 Cr2 76.07(3) . . ? P4 P5 P1 108.21(5) . . ? P4 P5 Cr1 62.57(3) . . ? P1 P5 Cr1 62.59(3) . . ? P4 P5 Cr2 62.63(3) . . ? P1 P5 Cr2 62.47(4) . . ? Cr1 P5 Cr2 76.40(3) . . ? C15 Cr2 C13 62.93(10) . . ? C15 Cr2 C12 62.97(10) . . ? C13 Cr2 C12 37.44(10) . . ? C15 Cr2 C14 37.67(10) . . ? C13 Cr2 C14 37.47(10) . . ? C12 Cr2 C14 62.65(10) . . ? C15 Cr2 C11 37.63(10) . . ? C13 Cr2 C11 62.73(10) . . ? C12 Cr2 C11 37.64(10) . . ? C14 Cr2 C11 62.71(10) . . ? C15 Cr2 P5 95.21(7) . . ? C13 Cr2 P5 140.39(8) . . ? C12 Cr2 P5 157.02(8) . . ? C14 Cr2 P5 105.13(8) . . ? C11 Cr2 P5 120.14(8) . . ? C15 Cr2 P3 157.81(8) . . ? C13 Cr2 P3 96.33(7) . . ? C12 Cr2 P3 106.05(7) . . ? C14 Cr2 P3 120.65(8) . . ? C11 Cr2 P3 141.38(8) . . ? P5 Cr2 P3 96.93(3) . . ? C15 Cr2 P1 105.42(8) . . ? C13 Cr2 P1 157.50(8) . . ? C12 Cr2 P1 120.74(8) . . ? C14 Cr2 P1 140.84(8) . . ? C11 Cr2 P1 96.01(8) . . ? P5 Cr2 P1 55.31(4) . . ? P3 Cr2 P1 96.76(3) . . ? C15 Cr2 P4 119.81(7) . . ? C13 Cr2 P4 105.33(8) . . ? C12 Cr2 P4 140.64(8) . . ? C14 Cr2 P4 95.41(8) . . ? C11 Cr2 P4 156.77(8) . . ? P5 Cr2 P4 55.16(4) . . ? P3 Cr2 P4 55.26(4) . . ? P1 Cr2 P4 97.17(4) . . ? C15 Cr2 P2 141.59(8) . . ? C13 Cr2 P2 121.04(8) . . ? C12 Cr2 P2 96.75(8) . . ? C14 Cr2 P2 157.98(8) . . ? C11 Cr2 P2 106.43(8) . . ? P5 Cr2 P2 96.89(4) . . ? P3 Cr2 P2 54.71(4) . . ? P1 Cr2 P2 55.08(4) . . ? P4 Cr2 P2 96.80(3) . . ? C15 Cr2 Cr1 145.97(7) . . ? C13 Cr2 Cr1 147.01(7) . . ? C12 Cr2 Cr1 147.64(7) . . ? C14 Cr2 Cr1 146.14(7) . . ? C11 Cr2 Cr1 147.13(8) . . ? P5 Cr2 Cr1 51.74(2) . . ? P3 Cr2 Cr1 51.94(2) . . ? P1 Cr2 Cr1 51.99(2) . . ? P4 Cr2 Cr1 51.90(2) . . ? P2 Cr2 Cr1 51.94(2) . . ? C15 C11 C12 108.1(2) . . ? C15 C11 C16 126.8(3) . . ? C12 C11 C16 124.9(3) . . ? C15 C11 Cr2 71.15(14) . . ? C12 C11 Cr2 71.17(15) . . ? C16 C11 Cr2 126.47(19) . . ? C13 C12 C11 108.0(2) . . ? C13 C12 C17 126.1(3) . . ? C11 C12 C17 125.9(3) . . ? C13 C12 Cr2 71.26(15) . . ? C11 C12 Cr2 71.19(15) . . ? C17 C12 Cr2 125.72(19) . . ? C12 C13 C14 108.1(2) . . ? C12 C13 C18 126.0(3) . . ? C14 C13 C18 125.7(3) . . ? C12 C13 Cr2 71.30(15) . . ? C14 C13 Cr2 71.27(16) . . ? C18 C13 Cr2 126.95(19) . . ? C13 C14 C15 108.3(2) . . ? C13 C14 C19 126.0(3) . . ? C15 C14 C19 125.7(3) . . ? C13 C14 Cr2 71.26(16) . . ? C15 C14 Cr2 71.14(16) . . ? C19 C14 Cr2 125.56(19) . . ? C11 C15 C14 107.5(2) . . ? C11 C15 C20 126.8(3) . . ? C14 C15 C20 125.5(3) . . ? C11 C15 Cr2 71.23(15) . . ? C14 C15 Cr2 71.19(15) . . ? C20 C15 Cr2 125.68(18) . . ? C11 C16 H16A 109.5 . . ? C11 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C11 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C25 C21 C22 107.1(2) . . ? C25 C21 C26 125.5(2) . . ? C22 C21 C26 127.2(2) . . ? C25 C21 Cr3 70.67(15) . . ? C22 C21 Cr3 70.51(15) . . ? C26 C21 Cr3 127.8(2) . . ? C23 C22 C21 108.4(2) . . ? C23 C22 C27 125.1(3) . . ? C21 C22 C27 126.3(3) . . ? C23 C22 Cr3 70.79(15) . . ? C21 C22 Cr3 71.51(15) . . ? C27 C22 Cr3 127.0(2) . . ? C22 C23 C24 108.3(2) . . ? C22 C23 C28 125.3(3) . . ? C24 C23 C28 126.2(3) . . ? C22 C23 Cr3 71.42(16) . . ? C24 C23 Cr3 71.45(16) . . ? C28 C23 Cr3 126.8(2) . . ? C23 C24 C25 107.5(2) . . ? C23 C24 C29 125.5(3) . . ? C25 C24 C29 126.9(3) . . ? C23 C24 Cr3 70.71(17) . . ? C25 C24 Cr3 70.97(16) . . ? C29 C24 Cr3 126.3(2) . . ? C21 C25 C24 108.6(2) . . ? C21 C25 C30 125.4(3) . . ? C24 C25 C30 125.9(3) . . ? C21 C25 Cr3 71.60(16) . . ? C24 C25 Cr3 71.01(16) . . ? C30 C25 Cr3 126.3(2) . . ? C21 C26 H26A 109.5 . . ? C21 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C21 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C22 C27 H27A 109.5 . . ? C22 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? C22 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? C23 C28 H28A 109.5 . . ? C23 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C23 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C24 C29 H29A 109.5 . . ? C24 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C24 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C25 C30 H30A 109.5 . . ? C25 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? C25 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C23 Cr3 C22 37.79(11) . . ? C23 Cr3 C25 63.31(10) . . ? C22 Cr3 C25 63.13(10) . . ? C23 Cr3 C24 37.84(10) . . ? C22 Cr3 C24 63.25(10) . . ? C25 Cr3 C24 38.02(10) . . ? C23 Cr3 C21 63.50(10) . . ? C22 Cr3 C21 37.97(10) . . ? C25 Cr3 C21 37.72(10) . . ? C24 Cr3 C21 63.51(10) . . ? C23 Cr3 P10 147.86(8) . . ? C22 Cr3 P10 154.40(8) . . ? C25 Cr3 P10 96.48(8) . . ? C24 Cr3 P10 110.99(8) . . ? C21 Cr3 P10 116.44(8) . . ? C23 Cr3 P6 155.30(8) . . ? C22 Cr3 P6 117.58(8) . . ? C25 Cr3 P6 112.05(8) . . ? C24 Cr3 P6 148.90(8) . . ? C21 Cr3 P6 97.48(8) . . ? P10 Cr3 P6 53.33(3) . . ? C23 Cr3 P9 110.87(8) . . ? C22 Cr3 P9 147.77(8) . . ? C25 Cr3 P9 116.39(8) . . ? C24 Cr3 P9 96.06(7) . . ? C21 Cr3 P9 154.08(8) . . ? P10 Cr3 P9 53.65(3) . . ? P6 Cr3 P9 93.07(3) . . ? C23 Cr3 P8 96.26(8) . . ? C22 Cr3 P8 111.46(8) . . ? C25 Cr3 P8 153.86(8) . . ? C24 Cr3 P8 115.89(8) . . ? C21 Cr3 P8 148.56(8) . . ? P10 Cr3 P8 93.63(3) . . ? P6 Cr3 P8 93.30(3) . . ? P9 Cr3 P8 53.24(3) . . ? C23 Cr3 P7 117.50(8) . . ? C22 Cr3 P7 98.31(8) . . ? C25 Cr3 P7 149.70(8) . . ? C24 Cr3 P7 155.19(8) . . ? C21 Cr3 P7 113.02(7) . . ? P10 Cr3 P7 92.73(3) . . ? P6 Cr3 P7 53.14(3) . . ? P9 Cr3 P7 92.23(3) . . ? P8 Cr3 P7 52.98(3) . . ? P10 P6 P7 108.12(4) . . ? P10 P6 Cr3 63.29(3) . . ? P7 P6 Cr3 64.01(3) . . ? P10 P6 Cr4 63.14(3) . . ? P7 P6 Cr4 63.14(3) . . ? Cr3 P6 Cr4 80.55(3) . . ? P8 P7 P6 108.30(4) . . ? P8 P7 Cr4 63.95(3) . . ? P6 P7 Cr4 63.71(3) . . ? P8 P7 Cr3 63.12(3) . . ? P6 P7 Cr3 62.85(3) . . ? Cr4 P7 Cr3 80.30(3) . . ? P7 P8 P9 107.69(4) . . ? P7 P8 Cr3 63.90(3) . . ? P9 P8 Cr3 63.38(3) . . ? P7 P8 Cr4 63.04(3) . . ? P9 P8 Cr4 62.43(3) . . ? Cr3 P8 Cr4 80.24(3) . . ? P8 P9 P10 108.18(4) . . ? P8 P9 Cr4 64.27(3) . . ? P10 P9 Cr4 63.49(3) . . ? P8 P9 Cr3 63.38(3) . . ? P10 P9 Cr3 62.94(3) . . ? Cr4 P9 Cr3 81.02(3) . . ? P6 P10 P9 107.68(4) . . ? P6 P10 Cr3 63.37(3) . . ? P9 P10 Cr3 63.41(3) . . ? P6 P10 Cr4 63.80(3) . . ? P9 P10 Cr4 62.66(3) . . ? Cr3 P10 Cr4 80.86(3) . . ? C31 Cr4 C32 38.17(10) . . ? C31 Cr4 C33 63.34(10) . . ? C32 Cr4 C33 37.86(10) . . ? C31 Cr4 C35 37.82(10) . . ? C32 Cr4 C35 63.53(10) . . ? C33 Cr4 C35 63.17(10) . . ? C31 Cr4 C34 63.16(10) . . ? C32 Cr4 C34 63.27(10) . . ? C33 Cr4 C34 37.66(10) . . ? C35 Cr4 C34 37.72(10) . . ? C31 Cr4 P9 140.94(8) . . ? C32 Cr4 P9 160.61(7) . . ? C33 Cr4 P9 123.37(8) . . ? C35 Cr4 P9 106.42(8) . . ? C34 Cr4 P9 98.37(8) . . ? C31 Cr4 P10 105.49(7) . . ? C32 Cr4 P10 140.42(8) . . ? C33 Cr4 P10 159.82(7) . . ? C35 Cr4 P10 97.47(7) . . ? C34 Cr4 P10 123.02(8) . . ? P9 Cr4 P10 53.85(3) . . ? C31 Cr4 P7 123.01(8) . . ? C32 Cr4 P7 97.99(7) . . ? C33 Cr4 P7 107.10(7) . . ? C35 Cr4 P7 160.28(8) . . ? C34 Cr4 P7 141.79(8) . . ? P9 Cr4 P7 93.25(3) . . ? P10 Cr4 P7 93.07(3) . . ? C31 Cr4 P6 97.57(7) . . ? C32 Cr4 P6 106.20(7) . . ? C33 Cr4 P6 141.19(7) . . ? C35 Cr4 P6 122.67(8) . . ? C34 Cr4 P6 159.69(8) . . ? P9 Cr4 P6 93.18(3) . . ? P10 Cr4 P6 53.06(3) . . ? P7 Cr4 P6 53.15(3) . . ? C31 Cr4 P8 161.38(8) . . ? C32 Cr4 P8 123.70(8) . . ? C33 Cr4 P8 99.29(8) . . ? C35 Cr4 P8 142.19(8) . . ? C34 Cr4 P8 107.85(8) . . ? P9 Cr4 P8 53.30(3) . . ? P10 Cr4 P8 93.08(3) . . ? P7 Cr4 P8 53.01(3) . . ? P6 Cr4 P8 92.45(3) . . ? C35 C31 C32 108.3(2) . . ? C35 C31 C36 125.6(3) . . ? C32 C31 C36 126.0(3) . . ? C35 C31 Cr4 71.68(16) . . ? C32 C31 Cr4 71.14(16) . . ? C36 C31 Cr4 124.74(19) . . ? C33 C32 C31 107.4(2) . . ? C33 C32 C37 126.1(3) . . ? C31 C32 C37 126.4(3) . . ? C33 C32 Cr4 71.30(16) . . ? C31 C32 Cr4 70.69(15) . . ? C37 C32 Cr4 125.02(19) . . ? C34 C33 C32 108.3(2) . . ? C34 C33 C38 124.5(2) . . ? C32 C33 C38 127.1(2) . . ? C34 C33 Cr4 71.50(15) . . ? C32 C33 Cr4 70.84(15) . . ? C38 C33 Cr4 125.6(2) . . ? C33 C34 C35 108.1(2) . . ? C33 C34 C39 125.5(3) . . ? C35 C34 C39 126.3(2) . . ? C33 C34 Cr4 70.84(15) . . ? C35 C34 Cr4 70.95(15) . . ? C39 C34 Cr4 126.8(2) . . ? C31 C35 C34 107.8(2) . . ? C31 C35 C40 126.3(3) . . ? C34 C35 C40 125.8(3) . . ? C31 C35 Cr4 70.50(15) . . ? C34 C35 Cr4 71.34(15) . . ? C40 C35 Cr4 126.20(19) . . ? C31 C36 H36A 109.5 . . ? C31 C36 H36B 109.5 . . ? H36A C36 H36B 109.5 . . ? C31 C36 H36C 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C32 C37 H37A 109.5 . . ? C32 C37 H37B 109.5 . . ? H37A C37 H37B 109.5 . . ? C32 C37 H37C 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? C33 C38 H38A 109.5 . . ? C33 C38 H38B 109.5 . . ? H38A C38 H38B 109.5 . . ? C33 C38 H38C 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? C34 C39 H39A 109.5 . . ? C34 C39 H39B 109.5 . . ? H39A C39 H39B 109.5 . . ? C34 C39 H39C 109.5 . . ? H39A C39 H39C 109.5 . . ? H39B C39 H39C 109.5 . . ? C35 C40 H40A 109.5 . . ? C35 C40 H40B 109.5 . . ? H40A C40 H40B 109.5 . . ? C35 C40 H40C 109.5 . . ? H40A C40 H40C 109.5 . . ? H40B C40 H40C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 C1 C2 C3 0.0(3) . . . . ? C6 C1 C2 C3 176.8(3) . . . . ? Cr1 C1 C2 C3 -62.08(18) . . . . ? C5 C1 C2 C7 -176.6(3) . . . . ? C6 C1 C2 C7 0.3(5) . . . . ? Cr1 C1 C2 C7 121.4(3) . . . . ? C5 C1 C2 Cr1 62.06(19) . . . . ? C6 C1 C2 Cr1 -121.1(3) . . . . ? C1 C2 C3 C4 0.1(3) . . . . ? C7 C2 C3 C4 176.6(3) . . . . ? Cr1 C2 C3 C4 -62.27(18) . . . . ? C1 C2 C3 C8 -177.4(3) . . . . ? C7 C2 C3 C8 -1.0(4) . . . . ? Cr1 C2 C3 C8 120.2(3) . . . . ? C1 C2 C3 Cr1 62.37(19) . . . . ? C7 C2 C3 Cr1 -121.2(3) . . . . ? C2 C3 C4 C5 -0.1(3) . . . . ? C8 C3 C4 C5 177.5(2) . . . . ? Cr1 C3 C4 C5 -62.27(18) . . . . ? C2 C3 C4 C9 -177.1(3) . . . . ? C8 C3 C4 C9 0.5(4) . . . . ? Cr1 C3 C4 C9 120.8(3) . . . . ? C2 C3 C4 Cr1 62.13(18) . . . . ? C8 C3 C4 Cr1 -120.2(3) . . . . ? C3 C4 C5 C1 0.1(3) . . . . ? C9 C4 C5 C1 177.1(3) . . . . ? Cr1 C4 C5 C1 -61.49(19) . . . . ? C3 C4 C5 C10 -175.0(3) . . . . ? C9 C4 C5 C10 2.0(4) . . . . ? Cr1 C4 C5 C10 123.4(3) . . . . ? C3 C4 C5 Cr1 61.61(18) . . . . ? C9 C4 C5 Cr1 -121.4(3) . . . . ? C2 C1 C5 C4 -0.1(3) . . . . ? C6 C1 C5 C4 -177.0(3) . . . . ? Cr1 C1 C5 C4 61.60(19) . . . . ? C2 C1 C5 C10 175.2(3) . . . . ? C6 C1 C5 C10 -1.7(5) . . . . ? Cr1 C1 C5 C10 -123.2(3) . . . . ? C2 C1 C5 Cr1 -61.66(19) . . . . ? C6 C1 C5 Cr1 121.4(3) . . . . ? C4 C3 Cr1 C2 117.8(2) . . . . ? C8 C3 Cr1 C2 -122.5(3) . . . . ? C2 C3 Cr1 C1 -37.74(15) . . . . ? C4 C3 Cr1 C1 80.04(17) . . . . ? C8 C3 Cr1 C1 -160.2(3) . . . . ? C2 C3 Cr1 C4 -117.8(2) . . . . ? C8 C3 Cr1 C4 119.7(3) . . . . ? C2 C3 Cr1 C5 -80.31(17) . . . . ? C4 C3 Cr1 C5 37.47(16) . . . . ? C8 C3 Cr1 C5 157.2(3) . . . . ? C2 C3 Cr1 P5 -150.56(13) . . . . ? C4 C3 Cr1 P5 -32.8(2) . . . . ? C8 C3 Cr1 P5 87.0(2) . . . . ? C2 C3 Cr1 P3 101.99(15) . . . . ? C4 C3 Cr1 P3 -140.23(15) . . . . ? C8 C3 Cr1 P3 -20.5(2) . . . . ? C2 C3 Cr1 P4 157.77(14) . . . . ? C4 C3 Cr1 P4 -84.45(16) . . . . ? C8 C3 Cr1 P4 35.3(2) . . . . ? C2 C3 Cr1 P2 50.47(17) . . . . ? C4 C3 Cr1 P2 168.25(13) . . . . ? C8 C3 Cr1 P2 -72.0(3) . . . . ? C2 C3 Cr1 P1 -28.8(3) . . . . ? C4 C3 Cr1 P1 88.9(3) . . . . ? C8 C3 Cr1 P1 -151.3(2) . . . . ? C2 C3 Cr1 Cr2 120.88(16) . . . . ? C4 C3 Cr1 Cr2 -121.34(15) . . . . ? C8 C3 Cr1 Cr2 -1.6(3) . . . . ? C1 C2 Cr1 C3 -117.2(2) . . . . ? C7 C2 Cr1 C3 122.0(3) . . . . ? C3 C2 Cr1 C1 117.2(2) . . . . ? C7 C2 Cr1 C1 -120.7(3) . . . . ? C3 C2 Cr1 C4 37.56(15) . . . . ? C1 C2 Cr1 C4 -79.65(17) . . . . ? C7 C2 Cr1 C4 159.6(3) . . . . ? C3 C2 Cr1 C5 79.70(17) . . . . ? C1 C2 Cr1 C5 -37.51(16) . . . . ? C7 C2 Cr1 C5 -158.3(3) . . . . ? C3 C2 Cr1 P5 86.4(3) . . . . ? C1 C2 Cr1 P5 -30.9(3) . . . . ? C7 C2 Cr1 P5 -151.6(2) . . . . ? C3 C2 Cr1 P3 -84.39(15) . . . . ? C1 C2 Cr1 P3 158.40(15) . . . . ? C7 C2 Cr1 P3 37.7(3) . . . . ? C3 C2 Cr1 P4 -32.3(2) . . . . ? C1 C2 Cr1 P4 -149.52(14) . . . . ? C7 C2 Cr1 P4 89.7(3) . . . . ? C3 C2 Cr1 P2 -139.66(14) . . . . ? C1 C2 Cr1 P2 103.13(16) . . . . ? C7 C2 Cr1 P2 -17.6(3) . . . . ? C3 C2 Cr1 P1 168.58(13) . . . . ? C1 C2 Cr1 P1 51.37(18) . . . . ? C7 C2 Cr1 P1 -69.4(3) . . . . ? C3 C2 Cr1 Cr2 -120.19(16) . . . . ? C1 C2 Cr1 Cr2 122.59(16) . . . . ? C7 C2 Cr1 Cr2 1.8(3) . . . . ? C2 C1 Cr1 C3 37.56(16) . . . . ? C5 C1 Cr1 C3 -79.86(17) . . . . ? C6 C1 Cr1 C3 159.2(3) . . . . ? C5 C1 Cr1 C2 -117.4(2) . . . . ? C6 C1 Cr1 C2 121.7(3) . . . . ? C2 C1 Cr1 C4 80.42(17) . . . . ? C5 C1 Cr1 C4 -36.99(15) . . . . ? C6 C1 Cr1 C4 -157.9(3) . . . . ? C2 C1 Cr1 C5 117.4(2) . . . . ? C6 C1 Cr1 C5 -120.9(3) . . . . ? C2 C1 Cr1 P5 167.95(14) . . . . ? C5 C1 Cr1 P5 50.54(18) . . . . ? C6 C1 Cr1 P5 -70.4(3) . . . . ? C2 C1 Cr1 P3 -31.5(2) . . . . ? C5 C1 Cr1 P3 -148.94(13) . . . . ? C6 C1 Cr1 P3 90.1(3) . . . . ? C2 C1 Cr1 P4 85.5(3) . . . . ? C5 C1 Cr1 P4 -31.9(3) . . . . ? C6 C1 Cr1 P4 -152.8(2) . . . . ? C2 C1 Cr1 P2 -83.57(16) . . . . ? C5 C1 Cr1 P2 159.02(14) . . . . ? C6 C1 Cr1 P2 38.1(2) . . . . ? C2 C1 Cr1 P1 -139.41(16) . . . . ? C5 C1 Cr1 P1 103.17(15) . . . . ? C6 C1 Cr1 P1 -17.7(2) . . . . ? C2 C1 Cr1 Cr2 -120.36(16) . . . . ? C5 C1 Cr1 Cr2 122.23(16) . . . . ? C6 C1 Cr1 Cr2 1.3(3) . . . . ? C5 C4 Cr1 C3 117.0(2) . . . . ? C9 C4 Cr1 C3 -121.2(3) . . . . ? C5 C4 Cr1 C2 79.84(17) . . . . ? C3 C4 Cr1 C2 -37.19(16) . . . . ? C9 C4 Cr1 C2 -158.4(3) . . . . ? C5 C4 Cr1 C1 37.27(16) . . . . ? C3 C4 Cr1 C1 -79.76(17) . . . . ? C9 C4 Cr1 C1 159.1(3) . . . . ? C3 C4 Cr1 C5 -117.0(2) . . . . ? C9 C4 Cr1 C5 121.8(3) . . . . ? C5 C4 Cr1 P5 -85.18(15) . . . . ? C3 C4 Cr1 P5 157.80(15) . . . . ? C9 C4 Cr1 P5 36.6(2) . . . . ? C5 C4 Cr1 P3 167.03(13) . . . . ? C3 C4 Cr1 P3 50.00(18) . . . . ? C9 C4 Cr1 P3 -71.2(2) . . . . ? C5 C4 Cr1 P4 -140.94(15) . . . . ? C3 C4 Cr1 P4 102.04(16) . . . . ? C9 C4 Cr1 P4 -19.1(2) . . . . ? C5 C4 Cr1 P2 87.8(3) . . . . ? C3 C4 Cr1 P2 -29.2(3) . . . . ? C9 C4 Cr1 P2 -150.4(2) . . . . ? C5 C4 Cr1 P1 -32.9(2) . . . . ? C3 C4 Cr1 P1 -149.89(14) . . . . ? C9 C4 Cr1 P1 88.9(2) . . . . ? C5 C4 Cr1 Cr2 -122.44(15) . . . . ? C3 C4 Cr1 Cr2 120.53(16) . . . . ? C9 C4 Cr1 Cr2 -0.7(3) . . . . ? C4 C5 Cr1 C3 -38.03(15) . . . . ? C1 C5 Cr1 C3 80.04(17) . . . . ? C10 C5 Cr1 C3 -160.3(3) . . . . ? C4 C5 Cr1 C2 -80.47(17) . . . . ? C1 C5 Cr1 C2 37.60(16) . . . . ? C10 C5 Cr1 C2 157.3(3) . . . . ? C4 C5 Cr1 C1 -118.1(2) . . . . ? C10 C5 Cr1 C1 119.7(3) . . . . ? C1 C5 Cr1 C4 118.1(2) . . . . ? C10 C5 Cr1 C4 -122.3(3) . . . . ? C4 C5 Cr1 P5 101.77(15) . . . . ? C1 C5 Cr1 P5 -140.16(15) . . . . ? C10 C5 Cr1 P5 -20.5(3) . . . . ? C4 C5 Cr1 P3 -31.6(3) . . . . ? C1 C5 Cr1 P3 86.5(3) . . . . ? C10 C5 Cr1 P3 -153.86(19) . . . . ? C4 C5 Cr1 P4 48.99(17) . . . . ? C1 C5 Cr1 P4 167.06(13) . . . . ? C10 C5 Cr1 P4 -73.3(3) . . . . ? C4 C5 Cr1 P2 -149.09(13) . . . . ? C1 C5 Cr1 P2 -31.0(2) . . . . ? C10 C5 Cr1 P2 88.6(3) . . . . ? C4 C5 Cr1 P1 157.82(14) . . . . ? C1 C5 Cr1 P1 -84.11(15) . . . . ? C10 C5 Cr1 P1 35.5(3) . . . . ? C4 C5 Cr1 Cr2 120.00(16) . . . . ? C1 C5 Cr1 Cr2 -121.93(16) . . . . ? C10 C5 Cr1 Cr2 -2.3(4) . . . . ? C3 Cr1 P1 P2 92.9(2) . . . . ? C2 Cr1 P1 P2 72.00(9) . . . . ? C1 Cr1 P1 P2 100.88(8) . . . . ? C4 Cr1 P1 P2 158.61(11) . . . . ? C5 Cr1 P1 P2 138.74(8) . . . . ? P5 Cr1 P1 P2 -131.79(5) . . . . ? P3 Cr1 P1 P2 -37.90(4) . . . . ? P4 Cr1 P1 P2 -93.61(5) . . . . ? Cr2 Cr1 P1 P2 -66.13(4) . . . . ? C3 Cr1 P1 P5 -135.3(2) . . . . ? C2 Cr1 P1 P5 -156.21(9) . . . . ? C1 Cr1 P1 P5 -127.33(8) . . . . ? C4 Cr1 P1 P5 -69.60(11) . . . . ? C5 Cr1 P1 P5 -89.47(8) . . . . ? P3 Cr1 P1 P5 93.88(4) . . . . ? P4 Cr1 P1 P5 38.17(4) . . . . ? P2 Cr1 P1 P5 131.79(5) . . . . ? Cr2 Cr1 P1 P5 65.66(4) . . . . ? C3 Cr1 P1 Cr2 159.0(2) . . . . ? C2 Cr1 P1 Cr2 138.13(9) . . . . ? C1 Cr1 P1 Cr2 167.01(8) . . . . ? C4 Cr1 P1 Cr2 -135.26(11) . . . . ? C5 Cr1 P1 Cr2 -155.13(8) . . . . ? P5 Cr1 P1 Cr2 -65.66(4) . . . . ? P3 Cr1 P1 Cr2 28.23(4) . . . . ? P4 Cr1 P1 Cr2 -27.48(4) . . . . ? P2 Cr1 P1 Cr2 66.13(4) . . . . ? P5 P1 P2 P3 0.44(6) . . . . ? Cr2 P1 P2 P3 -43.76(4) . . . . ? Cr1 P1 P2 P3 44.21(4) . . . . ? P5 P1 P2 Cr1 -43.77(4) . . . . ? Cr2 P1 P2 Cr1 -87.97(3) . . . . ? P5 P1 P2 Cr2 44.20(4) . . . . ? Cr1 P1 P2 Cr2 87.97(3) . . . . ? C3 Cr1 P2 P3 72.29(10) . . . . ? C2 Cr1 P2 P3 100.58(8) . . . . ? C1 Cr1 P2 P3 138.40(8) . . . . ? C4 Cr1 P2 P3 93.4(2) . . . . ? C5 Cr1 P2 P3 157.29(11) . . . . ? P5 Cr1 P2 P3 -93.47(4) . . . . ? P4 Cr1 P2 P3 -37.75(4) . . . . ? P1 Cr1 P2 P3 -131.65(5) . . . . ? Cr2 Cr1 P2 P3 -65.87(3) . . . . ? C3 Cr1 P2 P1 -156.06(10) . . . . ? C2 Cr1 P2 P1 -127.77(8) . . . . ? C1 Cr1 P2 P1 -89.95(8) . . . . ? C4 Cr1 P2 P1 -134.9(2) . . . . ? C5 Cr1 P2 P1 -71.06(11) . . . . ? P5 Cr1 P2 P1 38.18(5) . . . . ? P3 Cr1 P2 P1 131.65(5) . . . . ? P4 Cr1 P2 P1 93.90(4) . . . . ? Cr2 Cr1 P2 P1 65.78(4) . . . . ? C3 Cr1 P2 Cr2 138.16(9) . . . . ? C2 Cr1 P2 Cr2 166.45(8) . . . . ? C1 Cr1 P2 Cr2 -155.73(8) . . . . ? C4 Cr1 P2 Cr2 159.3(2) . . . . ? C5 Cr1 P2 Cr2 -136.84(11) . . . . ? P5 Cr1 P2 Cr2 -27.60(4) . . . . ? P3 Cr1 P2 Cr2 65.87(3) . . . . ? P4 Cr1 P2 Cr2 28.12(4) . . . . ? P1 Cr1 P2 Cr2 -65.78(4) . . . . ? P1 P2 P3 P4 -0.46(6) . . . . ? Cr1 P2 P3 P4 43.69(4) . . . . ? Cr2 P2 P3 P4 -44.17(4) . . . . ? P1 P2 P3 Cr2 43.72(4) . . . . ? Cr1 P2 P3 Cr2 87.87(3) . . . . ? P1 P2 P3 Cr1 -44.15(4) . . . . ? Cr2 P2 P3 Cr1 -87.87(3) . . . . ? C3 Cr1 P3 P2 -126.93(8) . . . . ? C2 Cr1 P3 P2 -89.24(9) . . . . ? C1 Cr1 P3 P2 -70.08(12) . . . . ? C4 Cr1 P3 P2 -155.26(9) . . . . ? C5 Cr1 P3 P2 -132.7(2) . . . . ? P5 Cr1 P3 P2 93.88(4) . . . . ? P4 Cr1 P3 P2 132.33(5) . . . . ? P1 Cr1 P3 P2 38.11(4) . . . . ? Cr2 Cr1 P3 P2 66.38(4) . . . . ? C3 Cr1 P3 P4 100.74(8) . . . . ? C2 Cr1 P3 P4 138.44(9) . . . . ? C1 Cr1 P3 P4 157.59(12) . . . . ? C4 Cr1 P3 P4 72.41(9) . . . . ? C5 Cr1 P3 P4 95.0(2) . . . . ? P5 Cr1 P3 P4 -38.45(4) . . . . ? P2 Cr1 P3 P4 -132.33(5) . . . . ? P1 Cr1 P3 P4 -94.21(4) . . . . ? Cr2 Cr1 P3 P4 -65.95(3) . . . . ? C3 Cr1 P3 Cr2 166.70(8) . . . . ? C2 Cr1 P3 Cr2 -155.61(8) . . . . ? C1 Cr1 P3 Cr2 -136.46(11) . . . . ? C4 Cr1 P3 Cr2 138.36(9) . . . . ? C5 Cr1 P3 Cr2 160.9(2) . . . . ? P5 Cr1 P3 Cr2 27.50(4) . . . . ? P4 Cr1 P3 Cr2 65.95(3) . . . . ? P2 Cr1 P3 Cr2 -66.38(4) . . . . ? P1 Cr1 P3 Cr2 -28.26(4) . . . . ? P2 P3 P4 P5 0.30(6) . . . . ? Cr2 P3 P4 P5 -44.07(4) . . . . ? Cr1 P3 P4 P5 44.15(4) . . . . ? P2 P3 P4 Cr1 -43.85(4) . . . . ? Cr2 P3 P4 Cr1 -88.22(3) . . . . ? P2 P3 P4 Cr2 44.37(4) . . . . ? Cr1 P3 P4 Cr2 88.22(3) . . . . ? C3 Cr1 P4 P5 139.53(8) . . . . ? C2 Cr1 P4 P5 159.05(11) . . . . ? C1 Cr1 P4 P5 96.9(2) . . . . ? C4 Cr1 P4 P5 101.45(8) . . . . ? C5 Cr1 P4 P5 73.96(9) . . . . ? P3 Cr1 P4 P5 -131.30(5) . . . . ? P2 Cr1 P4 P5 -93.83(4) . . . . ? P1 Cr1 P4 P5 -38.22(4) . . . . ? Cr2 Cr1 P4 P5 -65.66(3) . . . . ? C3 Cr1 P4 P3 -89.17(8) . . . . ? C2 Cr1 P4 P3 -69.65(11) . . . . ? C1 Cr1 P4 P3 -131.8(2) . . . . ? C4 Cr1 P4 P3 -127.25(8) . . . . ? C5 Cr1 P4 P3 -154.74(9) . . . . ? P5 Cr1 P4 P3 131.30(5) . . . . ? P2 Cr1 P4 P3 37.47(4) . . . . ? P1 Cr1 P4 P3 93.08(4) . . . . ? Cr2 Cr1 P4 P3 65.64(3) . . . . ? C3 Cr1 P4 Cr2 -154.81(8) . . . . ? C2 Cr1 P4 Cr2 -135.29(11) . . . . ? C1 Cr1 P4 Cr2 162.6(2) . . . . ? C4 Cr1 P4 Cr2 167.11(7) . . . . ? C5 Cr1 P4 Cr2 139.62(9) . . . . ? P5 Cr1 P4 Cr2 65.66(3) . . . . ? P3 Cr1 P4 Cr2 -65.64(3) . . . . ? P2 Cr1 P4 Cr2 -28.16(4) . . . . ? P1 Cr1 P4 Cr2 27.44(4) . . . . ? P3 P4 P5 P1 -0.03(6) . . . . ? Cr1 P4 P5 P1 44.21(4) . . . . ? Cr2 P4 P5 P1 -44.09(4) . . . . ? P3 P4 P5 Cr1 -44.24(4) . . . . ? Cr2 P4 P5 Cr1 -88.30(3) . . . . ? P3 P4 P5 Cr2 44.06(4) . . . . ? Cr1 P4 P5 Cr2 88.30(3) . . . . ? P2 P1 P5 P4 -0.25(6) . . . . ? Cr2 P1 P5 P4 44.17(4) . . . . ? Cr1 P1 P5 P4 -44.21(4) . . . . ? P2 P1 P5 Cr1 43.95(4) . . . . ? Cr2 P1 P5 Cr1 88.37(3) . . . . ? P2 P1 P5 Cr2 -44.42(4) . . . . ? Cr1 P1 P5 Cr2 -88.37(3) . . . . ? C3 Cr1 P5 P4 -68.77(12) . . . . ? C2 Cr1 P5 P4 -132.4(3) . . . . ? C1 Cr1 P5 P4 -154.89(10) . . . . ? C4 Cr1 P5 P4 -88.79(8) . . . . ? C5 Cr1 P5 P4 -126.45(8) . . . . ? P3 Cr1 P5 P4 38.46(4) . . . . ? P2 Cr1 P5 P4 93.67(4) . . . . ? P1 Cr1 P5 P4 131.74(5) . . . . ? Cr2 Cr1 P5 P4 65.96(3) . . . . ? C3 Cr1 P5 P1 159.49(12) . . . . ? C2 Cr1 P5 P1 95.8(3) . . . . ? C1 Cr1 P5 P1 73.37(10) . . . . ? C4 Cr1 P5 P1 139.47(8) . . . . ? C5 Cr1 P5 P1 101.82(8) . . . . ? P3 Cr1 P5 P1 -93.28(4) . . . . ? P4 Cr1 P5 P1 -131.74(5) . . . . ? P2 Cr1 P5 P1 -38.07(4) . . . . ? Cr2 Cr1 P5 P1 -65.78(4) . . . . ? C3 Cr1 P5 Cr2 -134.73(11) . . . . ? C2 Cr1 P5 Cr2 161.6(2) . . . . ? C1 Cr1 P5 Cr2 139.15(10) . . . . ? C4 Cr1 P5 Cr2 -154.75(8) . . . . ? C5 Cr1 P5 Cr2 167.60(8) . . . . ? P3 Cr1 P5 Cr2 -27.50(4) . . . . ? P4 Cr1 P5 Cr2 -65.96(3) . . . . ? P2 Cr1 P5 Cr2 27.71(4) . . . . ? P1 Cr1 P5 Cr2 65.78(4) . . . . ? P4 P5 Cr2 C15 123.01(8) . . . . ? P1 P5 Cr2 C15 -105.17(8) . . . . ? Cr1 P5 Cr2 C15 -171.09(8) . . . . ? P4 P5 Cr2 C13 70.37(12) . . . . ? P1 P5 Cr2 C13 -157.82(12) . . . . ? Cr1 P5 Cr2 C13 136.26(12) . . . . ? P4 P5 Cr2 C12 140.5(2) . . . . ? P1 P5 Cr2 C12 -87.7(2) . . . . ? Cr1 P5 Cr2 C12 -153.6(2) . . . . ? P4 P5 Cr2 C14 86.03(8) . . . . ? P1 P5 Cr2 C14 -142.16(8) . . . . ? Cr1 P5 Cr2 C14 151.92(8) . . . . ? P4 P5 Cr2 C11 152.94(9) . . . . ? P1 P5 Cr2 C11 -75.25(9) . . . . ? Cr1 P5 Cr2 C11 -141.17(9) . . . . ? P4 P5 Cr2 P3 -38.37(4) . . . . ? P1 P5 Cr2 P3 93.45(4) . . . . ? Cr1 P5 Cr2 P3 27.53(4) . . . . ? P4 P5 Cr2 P1 -131.81(5) . . . . ? Cr1 P5 Cr2 P1 -65.92(3) . . . . ? P1 P5 Cr2 P4 131.81(5) . . . . ? Cr1 P5 Cr2 P4 65.90(3) . . . . ? P4 P5 Cr2 P2 -93.51(4) . . . . ? P1 P5 Cr2 P2 38.30(4) . . . . ? Cr1 P5 Cr2 P2 -27.62(4) . . . . ? P4 P5 Cr2 Cr1 -65.90(3) . . . . ? P1 P5 Cr2 Cr1 65.92(3) . . . . ? P2 P3 Cr2 C15 143.8(2) . . . . ? P4 P3 Cr2 C15 -84.4(2) . . . . ? Cr1 P3 Cr2 C15 -150.12(19) . . . . ? P2 P3 Cr2 C13 123.85(8) . . . . ? P4 P3 Cr2 C13 -104.28(8) . . . . ? Cr1 P3 Cr2 C13 -170.05(8) . . . . ? P2 P3 Cr2 C12 86.92(9) . . . . ? P4 P3 Cr2 C12 -141.22(9) . . . . ? Cr1 P3 Cr2 C12 153.02(8) . . . . ? P2 P3 Cr2 C14 154.26(9) . . . . ? P4 P3 Cr2 C14 -73.88(9) . . . . ? Cr1 P3 Cr2 C14 -139.64(9) . . . . ? P2 P3 Cr2 C11 70.69(13) . . . . ? P4 P3 Cr2 C11 -157.45(13) . . . . ? Cr1 P3 Cr2 C11 136.79(12) . . . . ? P2 P3 Cr2 P5 -93.56(5) . . . . ? P4 P3 Cr2 P5 38.31(5) . . . . ? Cr1 P3 Cr2 P5 -27.45(4) . . . . ? P2 P3 Cr2 P1 -37.81(4) . . . . ? P4 P3 Cr2 P1 94.06(4) . . . . ? Cr1 P3 Cr2 P1 28.29(4) . . . . ? P2 P3 Cr2 P4 -131.87(5) . . . . ? Cr1 P3 Cr2 P4 -65.76(4) . . . . ? P4 P3 Cr2 P2 131.87(5) . . . . ? Cr1 P3 Cr2 P2 66.11(3) . . . . ? P2 P3 Cr2 Cr1 -66.11(3) . . . . ? P4 P3 Cr2 Cr1 65.76(4) . . . . ? P2 P1 Cr2 C15 -143.01(8) . . . . ? P5 P1 Cr2 C15 85.61(8) . . . . ? Cr1 P1 Cr2 C15 151.11(7) . . . . ? P2 P1 Cr2 C13 -87.6(2) . . . . ? P5 P1 Cr2 C13 141.0(2) . . . . ? Cr1 P1 Cr2 C13 -153.5(2) . . . . ? P2 P1 Cr2 C12 -75.62(9) . . . . ? P5 P1 Cr2 C12 153.01(9) . . . . ? Cr1 P1 Cr2 C12 -141.50(8) . . . . ? P2 P1 Cr2 C14 -158.94(12) . . . . ? P5 P1 Cr2 C14 69.69(12) . . . . ? Cr1 P1 Cr2 C14 135.18(12) . . . . ? P2 P1 Cr2 C11 -105.87(8) . . . . ? P5 P1 Cr2 C11 122.76(8) . . . . ? Cr1 P1 Cr2 C11 -171.75(7) . . . . ? P2 P1 Cr2 P5 131.37(4) . . . . ? Cr1 P1 Cr2 P5 65.49(3) . . . . ? P2 P1 Cr2 P3 37.61(4) . . . . ? P5 P1 Cr2 P3 -93.76(4) . . . . ? Cr1 P1 Cr2 P3 -28.27(4) . . . . ? P2 P1 Cr2 P4 93.31(4) . . . . ? P5 P1 Cr2 P4 -38.06(4) . . . . ? Cr1 P1 Cr2 P4 27.43(4) . . . . ? P5 P1 Cr2 P2 -131.37(4) . . . . ? Cr1 P1 Cr2 P2 -65.88(3) . . . . ? P2 P1 Cr2 Cr1 65.88(3) . . . . ? P5 P1 Cr2 Cr1 -65.49(3) . . . . ? P5 P4 Cr2 C15 -74.25(9) . . . . ? P3 P4 Cr2 C15 154.33(9) . . . . ? Cr1 P4 Cr2 C15 -139.86(9) . . . . ? P5 P4 Cr2 C13 -141.49(8) . . . . ? P3 P4 Cr2 C13 87.08(8) . . . . ? Cr1 P4 Cr2 C13 152.90(8) . . . . ? P5 P4 Cr2 C12 -156.94(12) . . . . ? P3 P4 Cr2 C12 71.64(12) . . . . ? Cr1 P4 Cr2 C12 137.45(12) . . . . ? P5 P4 Cr2 C14 -104.69(8) . . . . ? P3 P4 Cr2 C14 123.89(8) . . . . ? Cr1 P4 Cr2 C14 -170.30(8) . . . . ? P5 P4 Cr2 C11 -85.9(2) . . . . ? P3 P4 Cr2 C11 142.6(2) . . . . ? Cr1 P4 Cr2 C11 -151.54(19) . . . . ? P3 P4 Cr2 P5 -131.42(5) . . . . ? Cr1 P4 Cr2 P5 -65.61(4) . . . . ? P5 P4 Cr2 P3 131.42(5) . . . . ? Cr1 P4 Cr2 P3 65.81(3) . . . . ? P5 P4 Cr2 P1 38.15(4) . . . . ? P3 P4 Cr2 P1 -93.28(4) . . . . ? Cr1 P4 Cr2 P1 -27.46(4) . . . . ? P5 P4 Cr2 P2 93.68(4) . . . . ? P3 P4 Cr2 P2 -37.75(4) . . . . ? Cr1 P4 Cr2 P2 28.07(4) . . . . ? P5 P4 Cr2 Cr1 65.61(4) . . . . ? P3 P4 Cr2 Cr1 -65.81(3) . . . . ? P3 P2 Cr2 C15 -158.94(12) . . . . ? P1 P2 Cr2 C15 69.00(12) . . . . ? Cr1 P2 Cr2 C15 134.96(12) . . . . ? P3 P2 Cr2 C13 -74.45(9) . . . . ? P1 P2 Cr2 C13 153.49(9) . . . . ? Cr1 P2 Cr2 C13 -140.54(9) . . . . ? P3 P2 Cr2 C12 -104.91(8) . . . . ? P1 P2 Cr2 C12 123.03(8) . . . . ? Cr1 P2 Cr2 C12 -171.01(8) . . . . ? P3 P2 Cr2 C14 -85.2(2) . . . . ? P1 P2 Cr2 C14 142.8(2) . . . . ? Cr1 P2 Cr2 C14 -151.3(2) . . . . ? P3 P2 Cr2 C11 -142.12(8) . . . . ? P1 P2 Cr2 C11 85.83(8) . . . . ? Cr1 P2 Cr2 C11 151.79(8) . . . . ? P3 P2 Cr2 P5 93.63(4) . . . . ? P1 P2 Cr2 P5 -38.43(4) . . . . ? Cr1 P2 Cr2 P5 27.53(4) . . . . ? P1 P2 Cr2 P3 -132.06(5) . . . . ? Cr1 P2 Cr2 P3 -66.10(3) . . . . ? P3 P2 Cr2 P1 132.06(5) . . . . ? Cr1 P2 Cr2 P1 65.96(3) . . . . ? P3 P2 Cr2 P4 38.04(4) . . . . ? P1 P2 Cr2 P4 -94.02(4) . . . . ? Cr1 P2 Cr2 P4 -28.05(4) . . . . ? P3 P2 Cr2 Cr1 66.10(3) . . . . ? P1 P2 Cr2 Cr1 -65.96(3) . . . . ? C3 Cr1 Cr2 C15 136.20(19) . . . . ? C2 Cr1 Cr2 C15 -153.03(19) . . . . ? C1 Cr1 Cr2 C15 -80.62(19) . . . . ? C4 Cr1 Cr2 C15 64.58(19) . . . . ? C5 Cr1 Cr2 C15 -7.2(2) . . . . ? P5 Cr1 Cr2 C15 16.00(14) . . . . ? P3 Cr1 Cr2 C15 160.35(14) . . . . ? P4 Cr1 Cr2 C15 88.16(14) . . . . ? P2 Cr1 Cr2 C15 -128.24(14) . . . . ? P1 Cr1 Cr2 C15 -56.34(14) . . . . ? C3 Cr1 Cr2 C13 -5.8(2) . . . . ? C2 Cr1 Cr2 C13 65.0(2) . . . . ? C1 Cr1 Cr2 C13 137.43(19) . . . . ? C4 Cr1 Cr2 C13 -77.37(19) . . . . ? C5 Cr1 Cr2 C13 -149.2(2) . . . . ? P5 Cr1 Cr2 C13 -125.96(14) . . . . ? P3 Cr1 Cr2 C13 18.39(14) . . . . ? P4 Cr1 Cr2 C13 -53.80(14) . . . . ? P2 Cr1 Cr2 C13 89.81(14) . . . . ? P1 Cr1 Cr2 C13 161.71(14) . . . . ? C3 Cr1 Cr2 C12 -78.7(2) . . . . ? C2 Cr1 Cr2 C12 -7.9(2) . . . . ? C1 Cr1 Cr2 C12 64.5(2) . . . . ? C4 Cr1 Cr2 C12 -150.32(19) . . . . ? C5 Cr1 Cr2 C12 137.9(2) . . . . ? P5 Cr1 Cr2 C12 161.10(15) . . . . ? P3 Cr1 Cr2 C12 -54.55(15) . . . . ? P4 Cr1 Cr2 C12 -126.74(15) . . . . ? P2 Cr1 Cr2 C12 16.86(15) . . . . ? P1 Cr1 Cr2 C12 88.77(15) . . . . ? C3 Cr1 Cr2 C14 65.56(19) . . . . ? C2 Cr1 Cr2 C14 136.33(19) . . . . ? C1 Cr1 Cr2 C14 -151.25(19) . . . . ? C4 Cr1 Cr2 C14 -6.05(19) . . . . ? C5 Cr1 Cr2 C14 -77.9(2) . . . . ? P5 Cr1 Cr2 C14 -54.64(14) . . . . ? P3 Cr1 Cr2 C14 89.71(14) . . . . ? P4 Cr1 Cr2 C14 17.52(14) . . . . ? P2 Cr1 Cr2 C14 161.13(14) . . . . ? P1 Cr1 Cr2 C14 -126.97(14) . . . . ? C3 Cr1 Cr2 C11 -152.22(19) . . . . ? C2 Cr1 Cr2 C11 -81.45(19) . . . . ? C1 Cr1 Cr2 C11 -9.04(19) . . . . ? C4 Cr1 Cr2 C11 136.16(18) . . . . ? C5 Cr1 Cr2 C11 64.4(2) . . . . ? P5 Cr1 Cr2 C11 87.58(14) . . . . ? P3 Cr1 Cr2 C11 -128.07(14) . . . . ? P4 Cr1 Cr2 C11 159.74(14) . . . . ? P2 Cr1 Cr2 C11 -56.66(14) . . . . ? P1 Cr1 Cr2 C11 15.24(14) . . . . ? C3 Cr1 Cr2 P5 120.20(14) . . . . ? C2 Cr1 Cr2 P5 -169.03(15) . . . . ? C1 Cr1 Cr2 P5 -96.62(14) . . . . ? C4 Cr1 Cr2 P5 48.59(13) . . . . ? C5 Cr1 Cr2 P5 -23.23(15) . . . . ? P3 Cr1 Cr2 P5 144.35(6) . . . . ? P4 Cr1 Cr2 P5 72.16(5) . . . . ? P2 Cr1 Cr2 P5 -144.24(6) . . . . ? P1 Cr1 Cr2 P5 -72.33(5) . . . . ? C3 Cr1 Cr2 P3 -24.15(14) . . . . ? C2 Cr1 Cr2 P3 46.62(15) . . . . ? C1 Cr1 Cr2 P3 119.03(14) . . . . ? C4 Cr1 Cr2 P3 -95.77(13) . . . . ? C5 Cr1 Cr2 P3 -167.58(15) . . . . ? P5 Cr1 Cr2 P3 -144.35(6) . . . . ? P4 Cr1 Cr2 P3 -72.19(5) . . . . ? P2 Cr1 Cr2 P3 71.41(5) . . . . ? P1 Cr1 Cr2 P3 143.31(6) . . . . ? C3 Cr1 Cr2 P1 -167.46(14) . . . . ? C2 Cr1 Cr2 P1 -96.70(15) . . . . ? C1 Cr1 Cr2 P1 -24.28(14) . . . . ? C4 Cr1 Cr2 P1 120.92(14) . . . . ? C5 Cr1 Cr2 P1 49.11(15) . . . . ? P5 Cr1 Cr2 P1 72.33(5) . . . . ? P3 Cr1 Cr2 P1 -143.31(6) . . . . ? P4 Cr1 Cr2 P1 144.49(6) . . . . ? P2 Cr1 Cr2 P1 -71.90(6) . . . . ? C3 Cr1 Cr2 P4 48.04(14) . . . . ? C2 Cr1 Cr2 P4 118.81(15) . . . . ? C1 Cr1 Cr2 P4 -168.78(14) . . . . ? C4 Cr1 Cr2 P4 -23.58(13) . . . . ? C5 Cr1 Cr2 P4 -95.39(15) . . . . ? P5 Cr1 Cr2 P4 -72.16(5) . . . . ? P3 Cr1 Cr2 P4 72.19(5) . . . . ? P2 Cr1 Cr2 P4 143.60(6) . . . . ? P1 Cr1 Cr2 P4 -144.49(6) . . . . ? C3 Cr1 Cr2 P2 -95.56(14) . . . . ? C2 Cr1 Cr2 P2 -24.80(15) . . . . ? C1 Cr1 Cr2 P2 47.62(14) . . . . ? C4 Cr1 Cr2 P2 -167.18(14) . . . . ? C5 Cr1 Cr2 P2 121.01(15) . . . . ? P5 Cr1 Cr2 P2 144.24(6) . . . . ? P3 Cr1 Cr2 P2 -71.41(5) . . . . ? P4 Cr1 Cr2 P2 -143.60(6) . . . . ? P1 Cr1 Cr2 P2 71.90(6) . . . . ? C13 Cr2 C11 C15 80.21(17) . . . . ? C12 Cr2 C11 C15 117.6(2) . . . . ? C14 Cr2 C11 C15 37.84(16) . . . . ? P5 Cr2 C11 C15 -54.46(18) . . . . ? P3 Cr2 C11 C15 143.70(14) . . . . ? P1 Cr2 C11 C15 -107.55(15) . . . . ? P4 Cr2 C11 C15 16.7(3) . . . . ? P2 Cr2 C11 C15 -162.87(14) . . . . ? Cr1 Cr2 C11 C15 -119.57(16) . . . . ? C15 Cr2 C11 C12 -117.6(2) . . . . ? C13 Cr2 C11 C12 -37.40(16) . . . . ? C14 Cr2 C11 C12 -79.77(17) . . . . ? P5 Cr2 C11 C12 -172.07(14) . . . . ? P3 Cr2 C11 C12 26.1(2) . . . . ? P1 Cr2 C11 C12 134.84(16) . . . . ? P4 Cr2 C11 C12 -100.9(2) . . . . ? P2 Cr2 C11 C12 79.52(16) . . . . ? Cr1 Cr2 C11 C12 122.82(16) . . . . ? C15 Cr2 C11 C16 122.4(3) . . . . ? C13 Cr2 C11 C16 -157.4(3) . . . . ? C12 Cr2 C11 C16 -120.0(3) . . . . ? C14 Cr2 C11 C16 160.2(3) . . . . ? P5 Cr2 C11 C16 67.9(3) . . . . ? P3 Cr2 C11 C16 -93.9(3) . . . . ? P1 Cr2 C11 C16 14.8(2) . . . . ? P4 Cr2 C11 C16 139.1(2) . . . . ? P2 Cr2 C11 C16 -40.5(3) . . . . ? Cr1 Cr2 C11 C16 2.8(3) . . . . ? C15 C11 C12 C13 0.2(3) . . . . ? C16 C11 C12 C13 -176.0(3) . . . . ? Cr2 C11 C12 C13 62.15(19) . . . . ? C15 C11 C12 C17 177.1(3) . . . . ? C16 C11 C12 C17 0.9(4) . . . . ? Cr2 C11 C12 C17 -121.0(3) . . . . ? C15 C11 C12 Cr2 -61.92(18) . . . . ? C16 C11 C12 Cr2 121.9(3) . . . . ? C15 Cr2 C12 C13 -79.97(17) . . . . ? C14 Cr2 C12 C13 -37.41(15) . . . . ? C11 Cr2 C12 C13 -117.4(2) . . . . ? P5 Cr2 C12 C13 -99.6(2) . . . . ? P3 Cr2 C12 C13 79.23(15) . . . . ? P1 Cr2 C12 C13 -172.49(13) . . . . ? P4 Cr2 C12 C13 25.0(2) . . . . ? P2 Cr2 C12 C13 134.39(15) . . . . ? Cr1 Cr2 C12 C13 121.10(16) . . . . ? C15 Cr2 C12 C11 37.39(16) . . . . ? C13 Cr2 C12 C11 117.4(2) . . . . ? C14 Cr2 C12 C11 79.95(17) . . . . ? P5 Cr2 C12 C11 17.8(3) . . . . ? P3 Cr2 C12 C11 -163.40(14) . . . . ? P1 Cr2 C12 C11 -55.13(17) . . . . ? P4 Cr2 C12 C11 142.35(14) . . . . ? P2 Cr2 C12 C11 -108.24(15) . . . . ? Cr1 Cr2 C12 C11 -121.54(16) . . . . ? C15 Cr2 C12 C17 158.6(3) . . . . ? C13 Cr2 C12 C17 -121.5(3) . . . . ? C14 Cr2 C12 C17 -158.9(3) . . . . ? C11 Cr2 C12 C17 121.2(3) . . . . ? P5 Cr2 C12 C17 139.0(2) . . . . ? P3 Cr2 C12 C17 -42.2(3) . . . . ? P1 Cr2 C12 C17 66.0(3) . . . . ? P4 Cr2 C12 C17 -96.5(3) . . . . ? P2 Cr2 C12 C17 12.9(3) . . . . ? Cr1 Cr2 C12 C17 -0.4(4) . . . . ? C11 C12 C13 C14 0.0(3) . . . . ? C17 C12 C13 C14 -176.8(3) . . . . ? Cr2 C12 C13 C14 62.13(19) . . . . ? C11 C12 C13 C18 175.3(3) . . . . ? C17 C12 C13 C18 -1.5(4) . . . . ? Cr2 C12 C13 C18 -122.6(3) . . . . ? C11 C12 C13 Cr2 -62.10(18) . . . . ? C17 C12 C13 Cr2 121.0(3) . . . . ? C15 Cr2 C13 C12 80.10(17) . . . . ? C14 Cr2 C13 C12 117.5(2) . . . . ? C11 Cr2 C13 C12 37.60(15) . . . . ? P5 Cr2 C13 C12 142.86(14) . . . . ? P3 Cr2 C13 C12 -108.21(15) . . . . ? P1 Cr2 C13 C12 17.1(3) . . . . ? P4 Cr2 C13 C12 -163.87(14) . . . . ? P2 Cr2 C13 C12 -55.91(17) . . . . ? Cr1 Cr2 C13 C12 -122.68(16) . . . . ? C15 Cr2 C13 C14 -37.39(16) . . . . ? C12 Cr2 C13 C14 -117.5(2) . . . . ? C11 Cr2 C13 C14 -79.90(17) . . . . ? P5 Cr2 C13 C14 25.4(2) . . . . ? P3 Cr2 C13 C14 134.29(15) . . . . ? P1 Cr2 C13 C14 -100.4(2) . . . . ? P4 Cr2 C13 C14 78.63(16) . . . . ? P2 Cr2 C13 C14 -173.41(13) . . . . ? Cr1 Cr2 C13 C14 119.82(16) . . . . ? C15 Cr2 C13 C18 -158.5(3) . . . . ? C12 Cr2 C13 C18 121.4(3) . . . . ? C14 Cr2 C13 C18 -121.1(3) . . . . ? C11 Cr2 C13 C18 159.0(3) . . . . ? P5 Cr2 C13 C18 -95.7(3) . . . . ? P3 Cr2 C13 C18 13.2(3) . . . . ? P1 Cr2 C13 C18 138.5(2) . . . . ? P4 Cr2 C13 C18 -42.5(3) . . . . ? P2 Cr2 C13 C18 65.5(3) . . . . ? Cr1 Cr2 C13 C18 -1.3(3) . . . . ? C12 C13 C14 C15 -0.3(3) . . . . ? C18 C13 C14 C15 -175.6(3) . . . . ? Cr2 C13 C14 C15 61.87(19) . . . . ? C12 C13 C14 C19 177.0(3) . . . . ? C18 C13 C14 C19 1.7(4) . . . . ? Cr2 C13 C14 C19 -120.8(3) . . . . ? C12 C13 C14 Cr2 -62.14(18) . . . . ? C18 C13 C14 Cr2 122.6(3) . . . . ? C15 Cr2 C14 C13 117.8(2) . . . . ? C12 Cr2 C14 C13 37.38(16) . . . . ? C11 Cr2 C14 C13 79.96(17) . . . . ? P5 Cr2 C14 C13 -163.57(15) . . . . ? P3 Cr2 C14 C13 -55.78(17) . . . . ? P1 Cr2 C14 C13 143.41(14) . . . . ? P4 Cr2 C14 C13 -108.24(15) . . . . ? P2 Cr2 C14 C13 15.2(3) . . . . ? Cr1 Cr2 C14 C13 -122.01(16) . . . . ? C13 Cr2 C14 C15 -117.8(2) . . . . ? C12 Cr2 C14 C15 -80.38(17) . . . . ? C11 Cr2 C14 C15 -37.80(15) . . . . ? P5 Cr2 C14 C15 78.67(15) . . . . ? P3 Cr2 C14 C15 -173.54(12) . . . . ? P1 Cr2 C14 C15 25.7(2) . . . . ? P4 Cr2 C14 C15 134.00(14) . . . . ? P2 Cr2 C14 C15 -102.6(2) . . . . ? Cr1 Cr2 C14 C15 120.23(15) . . . . ? C15 Cr2 C14 C19 -120.9(3) . . . . ? C13 Cr2 C14 C19 121.4(3) . . . . ? C12 Cr2 C14 C19 158.7(3) . . . . ? C11 Cr2 C14 C19 -158.7(3) . . . . ? P5 Cr2 C14 C19 -42.2(3) . . . . ? P3 Cr2 C14 C19 65.6(3) . . . . ? P1 Cr2 C14 C19 -95.2(3) . . . . ? P4 Cr2 C14 C19 13.1(2) . . . . ? P2 Cr2 C14 C19 136.6(2) . . . . ? Cr1 Cr2 C14 C19 -0.6(3) . . . . ? C12 C11 C15 C14 -0.4(3) . . . . ? C16 C11 C15 C14 175.7(3) . . . . ? Cr2 C11 C15 C14 -62.33(18) . . . . ? C12 C11 C15 C20 -177.1(3) . . . . ? C16 C11 C15 C20 -0.9(5) . . . . ? Cr2 C11 C15 C20 121.0(3) . . . . ? C12 C11 C15 Cr2 61.94(18) . . . . ? C16 C11 C15 Cr2 -121.9(3) . . . . ? C13 C14 C15 C11 0.4(3) . . . . ? C19 C14 C15 C11 -176.9(3) . . . . ? Cr2 C14 C15 C11 62.35(18) . . . . ? C13 C14 C15 C20 177.1(2) . . . . ? C19 C14 C15 C20 -0.2(4) . . . . ? Cr2 C14 C15 C20 -120.9(3) . . . . ? C13 C14 C15 Cr2 -61.94(18) . . . . ? C19 C14 C15 Cr2 120.7(3) . . . . ? C13 Cr2 C15 C11 -79.65(17) . . . . ? C12 Cr2 C15 C11 -37.41(16) . . . . ? C14 Cr2 C15 C11 -116.8(2) . . . . ? P5 Cr2 C15 C11 135.04(15) . . . . ? P3 Cr2 C15 C11 -102.0(2) . . . . ? P1 Cr2 C15 C11 79.62(16) . . . . ? P4 Cr2 C15 C11 -172.48(14) . . . . ? P2 Cr2 C15 C11 27.1(2) . . . . ? Cr1 Cr2 C15 C11 122.49(15) . . . . ? C13 Cr2 C15 C14 37.20(15) . . . . ? C12 Cr2 C15 C14 79.44(17) . . . . ? C11 Cr2 C15 C14 116.8(2) . . . . ? P5 Cr2 C15 C14 -108.11(15) . . . . ? P3 Cr2 C15 C14 14.8(3) . . . . ? P1 Cr2 C15 C14 -163.53(14) . . . . ? P4 Cr2 C15 C14 -55.63(16) . . . . ? P2 Cr2 C15 C14 143.90(14) . . . . ? Cr1 Cr2 C15 C14 -120.66(16) . . . . ? C13 Cr2 C15 C20 158.0(3) . . . . ? C12 Cr2 C15 C20 -159.8(3) . . . . ? C14 Cr2 C15 C20 120.8(3) . . . . ? C11 Cr2 C15 C20 -122.4(3) . . . . ? P5 Cr2 C15 C20 12.6(2) . . . . ? P3 Cr2 C15 C20 135.6(2) . . . . ? P1 Cr2 C15 C20 -42.8(3) . . . . ? P4 Cr2 C15 C20 65.1(3) . . . . ? P2 Cr2 C15 C20 -95.3(2) . . . . ? Cr1 Cr2 C15 C20 0.1(3) . . . . ? C25 C21 C22 C23 0.0(3) . . . . ? C26 C21 C22 C23 175.3(3) . . . . ? Cr3 C21 C22 C23 -61.5(2) . . . . ? C25 C21 C22 C27 -175.6(3) . . . . ? C26 C21 C22 C27 -0.3(5) . . . . ? Cr3 C21 C22 C27 122.8(3) . . . . ? C25 C21 C22 Cr3 61.54(19) . . . . ? C26 C21 C22 Cr3 -123.2(3) . . . . ? C21 C22 C23 C24 -0.3(3) . . . . ? C27 C22 C23 C24 175.4(3) . . . . ? Cr3 C22 C23 C24 -62.3(2) . . . . ? C21 C22 C23 C28 -175.5(3) . . . . ? C27 C22 C23 C28 0.2(5) . . . . ? Cr3 C22 C23 C28 122.5(3) . . . . ? C21 C22 C23 Cr3 62.0(2) . . . . ? C27 C22 C23 Cr3 -122.3(3) . . . . ? C22 C23 C24 C25 0.5(3) . . . . ? C28 C23 C24 C25 175.6(3) . . . . ? Cr3 C23 C24 C25 -61.79(19) . . . . ? C22 C23 C24 C29 -176.3(3) . . . . ? C28 C23 C24 C29 -1.2(5) . . . . ? Cr3 C23 C24 C29 121.4(3) . . . . ? C22 C23 C24 Cr3 62.3(2) . . . . ? C28 C23 C24 Cr3 -122.6(3) . . . . ? C22 C21 C25 C24 0.3(3) . . . . ? C26 C21 C25 C24 -175.1(3) . . . . ? Cr3 C21 C25 C24 61.7(2) . . . . ? C22 C21 C25 C30 176.6(3) . . . . ? C26 C21 C25 C30 1.2(5) . . . . ? Cr3 C21 C25 C30 -121.9(3) . . . . ? C22 C21 C25 Cr3 -61.4(2) . . . . ? C26 C21 C25 Cr3 123.2(3) . . . . ? C23 C24 C25 C21 -0.5(3) . . . . ? C29 C24 C25 C21 176.3(3) . . . . ? Cr3 C24 C25 C21 -62.1(2) . . . . ? C23 C24 C25 C30 -176.8(3) . . . . ? C29 C24 C25 C30 0.0(5) . . . . ? Cr3 C24 C25 C30 121.6(3) . . . . ? C23 C24 C25 Cr3 61.6(2) . . . . ? C29 C24 C25 Cr3 -121.6(3) . . . . ? C24 C23 Cr3 C22 117.6(2) . . . . ? C28 C23 Cr3 C22 -120.6(3) . . . . ? C22 C23 Cr3 C25 -79.79(17) . . . . ? C24 C23 Cr3 C25 37.79(16) . . . . ? C28 C23 Cr3 C25 159.6(3) . . . . ? C22 C23 Cr3 C24 -117.6(2) . . . . ? C28 C23 Cr3 C24 121.8(3) . . . . ? C22 C23 Cr3 C21 -37.40(16) . . . . ? C24 C23 Cr3 C21 80.18(17) . . . . ? C28 C23 Cr3 C21 -158.0(3) . . . . ? C22 C23 Cr3 P10 -135.55(15) . . . . ? C24 C23 Cr3 P10 -18.0(2) . . . . ? C28 C23 Cr3 P10 103.8(3) . . . . ? C22 C23 Cr3 P6 5.2(3) . . . . ? C24 C23 Cr3 P6 122.78(19) . . . . ? C28 C23 Cr3 P6 -115.4(3) . . . . ? C22 C23 Cr3 P9 170.29(14) . . . . ? C24 C23 Cr3 P9 -72.13(16) . . . . ? C28 C23 Cr3 P9 49.6(3) . . . . ? C22 C23 Cr3 P8 117.34(15) . . . . ? C24 C23 Cr3 P8 -125.08(15) . . . . ? C28 C23 Cr3 P8 -3.3(3) . . . . ? C22 C23 Cr3 P7 66.08(17) . . . . ? C24 C23 Cr3 P7 -176.34(13) . . . . ? C28 C23 Cr3 P7 -54.6(3) . . . . ? C21 C22 Cr3 C23 -118.0(2) . . . . ? C27 C22 Cr3 C23 120.0(3) . . . . ? C23 C22 Cr3 C25 80.32(17) . . . . ? C21 C22 Cr3 C25 -37.63(16) . . . . ? C27 C22 Cr3 C25 -159.7(3) . . . . ? C23 C22 Cr3 C24 37.51(16) . . . . ? C21 C22 Cr3 C24 -80.44(18) . . . . ? C27 C22 Cr3 C24 157.5(3) . . . . ? C23 C22 Cr3 C21 118.0(2) . . . . ? C27 C22 Cr3 C21 -122.0(3) . . . . ? C23 C22 Cr3 P10 120.4(2) . . . . ? C21 C22 Cr3 P10 2.5(3) . . . . ? C27 C22 Cr3 P10 -119.6(2) . . . . ? C23 C22 Cr3 P6 -177.55(14) . . . . ? C21 C22 Cr3 P6 64.50(17) . . . . ? C27 C22 Cr3 P6 -57.5(3) . . . . ? C23 C22 Cr3 P9 -17.2(2) . . . . ? C21 C22 Cr3 P9 -135.14(15) . . . . ? C27 C22 Cr3 P9 102.8(3) . . . . ? C23 C22 Cr3 P8 -71.59(16) . . . . ? C21 C22 Cr3 P8 170.46(14) . . . . ? C27 C22 Cr3 P8 48.4(3) . . . . ? C23 C22 Cr3 P7 -124.98(15) . . . . ? C21 C22 Cr3 P7 117.07(15) . . . . ? C27 C22 Cr3 P7 -5.0(3) . . . . ? C21 C25 Cr3 C23 80.42(17) . . . . ? C24 C25 Cr3 C23 -37.62(16) . . . . ? C30 C25 Cr3 C23 -158.8(3) . . . . ? C21 C25 Cr3 C22 37.88(16) . . . . ? C24 C25 Cr3 C22 -80.15(17) . . . . ? C30 C25 Cr3 C22 158.7(3) . . . . ? C21 C25 Cr3 C24 118.0(2) . . . . ? C30 C25 Cr3 C24 -121.1(3) . . . . ? C24 C25 Cr3 C21 -118.0(2) . . . . ? C30 C25 Cr3 C21 120.8(3) . . . . ? C21 C25 Cr3 P10 -125.85(15) . . . . ? C24 C25 Cr3 P10 116.11(15) . . . . ? C30 C25 Cr3 P10 -5.0(2) . . . . ? C21 C25 Cr3 P6 -72.90(16) . . . . ? C24 C25 Cr3 P6 169.07(13) . . . . ? C30 C25 Cr3 P6 47.9(3) . . . . ? C21 C25 Cr3 P9 -178.29(14) . . . . ? C24 C25 Cr3 P9 63.67(16) . . . . ? C30 C25 Cr3 P9 -57.5(3) . . . . ? C21 C25 Cr3 P8 122.05(18) . . . . ? C24 C25 Cr3 P8 4.0(3) . . . . ? C30 C25 Cr3 P8 -117.1(2) . . . . ? C21 C25 Cr3 P7 -19.0(3) . . . . ? C24 C25 Cr3 P7 -137.07(15) . . . . ? C30 C25 Cr3 P7 101.8(3) . . . . ? C25 C24 Cr3 C23 117.3(2) . . . . ? C29 C24 Cr3 C23 -120.4(3) . . . . ? C23 C24 Cr3 C22 -37.46(16) . . . . ? C25 C24 Cr3 C22 79.79(17) . . . . ? C29 C24 Cr3 C22 -157.9(3) . . . . ? C23 C24 Cr3 C25 -117.3(2) . . . . ? C29 C24 Cr3 C25 122.4(3) . . . . ? C23 C24 Cr3 C21 -80.15(17) . . . . ? C25 C24 Cr3 C21 37.11(15) . . . . ? C29 C24 Cr3 C21 159.5(3) . . . . ? C23 C24 Cr3 P10 169.87(14) . . . . ? C25 C24 Cr3 P10 -72.87(15) . . . . ? C29 C24 Cr3 P10 49.5(3) . . . . ? C23 C24 Cr3 P6 -137.15(16) . . . . ? C25 C24 Cr3 P6 -19.9(2) . . . . ? C29 C24 Cr3 P6 102.5(3) . . . . ? C23 C24 Cr3 P9 116.58(15) . . . . ? C25 C24 Cr3 P9 -126.16(15) . . . . ? C29 C24 Cr3 P9 -3.8(3) . . . . ? C23 C24 Cr3 P8 64.71(17) . . . . ? C25 C24 Cr3 P8 -178.03(13) . . . . ? C29 C24 Cr3 P8 -55.7(3) . . . . ? C23 C24 Cr3 P7 7.7(3) . . . . ? C25 C24 Cr3 P7 125.00(19) . . . . ? C29 C24 Cr3 P7 -112.6(3) . . . . ? C25 C21 Cr3 C23 -79.88(17) . . . . ? C22 C21 Cr3 C23 37.22(16) . . . . ? C26 C21 Cr3 C23 159.7(3) . . . . ? C25 C21 Cr3 C22 -117.1(2) . . . . ? C26 C21 Cr3 C22 122.5(3) . . . . ? C22 C21 Cr3 C25 117.1(2) . . . . ? C26 C21 Cr3 C25 -120.4(3) . . . . ? C25 C21 Cr3 C24 -37.40(16) . . . . ? C22 C21 Cr3 C24 79.70(18) . . . . ? C26 C21 Cr3 C24 -157.8(3) . . . . ? C25 C21 Cr3 P10 64.09(17) . . . . ? C22 C21 Cr3 P10 -178.81(14) . . . . ? C26 C21 Cr3 P10 -56.3(3) . . . . ? C25 C21 Cr3 P6 116.69(15) . . . . ? C22 C21 Cr3 P6 -126.21(16) . . . . ? C26 C21 Cr3 P6 -3.7(2) . . . . ? C25 C21 Cr3 P9 3.5(3) . . . . ? C22 C21 Cr3 P9 120.60(19) . . . . ? C26 C21 Cr3 P9 -116.9(2) . . . . ? C25 C21 Cr3 P8 -134.29(16) . . . . ? C22 C21 Cr3 P8 -17.2(3) . . . . ? C26 C21 Cr3 P8 105.3(2) . . . . ? C25 C21 Cr3 P7 169.70(14) . . . . ? C22 C21 Cr3 P7 -73.20(17) . . . . ? C26 C21 Cr3 P7 49.3(3) . . . . ? C23 Cr3 P6 P10 -155.18(19) . . . . ? C22 Cr3 P6 P10 -151.59(9) . . . . ? C25 Cr3 P6 P10 -81.39(8) . . . . ? C24 Cr3 P6 P10 -68.32(14) . . . . ? C21 Cr3 P6 P10 -117.53(8) . . . . ? P9 Cr3 P6 P10 38.75(3) . . . . ? P8 Cr3 P6 P10 92.08(3) . . . . ? P7 Cr3 P6 P10 129.23(4) . . . . ? C23 Cr3 P6 P7 75.58(19) . . . . ? C22 Cr3 P6 P7 79.17(9) . . . . ? C25 Cr3 P6 P7 149.38(8) . . . . ? C24 Cr3 P6 P7 162.45(14) . . . . ? C21 Cr3 P6 P7 113.24(8) . . . . ? P10 Cr3 P6 P7 -129.23(4) . . . . ? P9 Cr3 P6 P7 -90.49(3) . . . . ? P8 Cr3 P6 P7 -37.16(3) . . . . ? C23 Cr3 P6 Cr4 140.22(18) . . . . ? C22 Cr3 P6 Cr4 143.81(8) . . . . ? C25 Cr3 P6 Cr4 -145.99(8) . . . . ? C24 Cr3 P6 Cr4 -132.92(14) . . . . ? C21 Cr3 P6 Cr4 177.87(7) . . . . ? P10 Cr3 P6 Cr4 -64.60(3) . . . . ? P9 Cr3 P6 Cr4 -25.85(3) . . . . ? P8 Cr3 P6 Cr4 27.48(3) . . . . ? P7 Cr3 P6 Cr4 64.63(3) . . . . ? P10 P6 P7 P8 -1.52(6) . . . . ? Cr3 P6 P7 P8 45.20(4) . . . . ? Cr4 P6 P7 P8 -47.21(4) . . . . ? P10 P6 P7 Cr4 45.69(4) . . . . ? Cr3 P6 P7 Cr4 92.41(3) . . . . ? P10 P6 P7 Cr3 -46.72(4) . . . . ? Cr4 P6 P7 Cr3 -92.41(3) . . . . ? C23 Cr3 P7 P8 76.19(9) . . . . ? C22 Cr3 P7 P8 110.67(8) . . . . ? C25 Cr3 P7 P8 159.72(15) . . . . ? C24 Cr3 P7 P8 70.84(18) . . . . ? C21 Cr3 P7 P8 147.20(8) . . . . ? P10 Cr3 P7 P8 -92.49(3) . . . . ? P6 Cr3 P7 P8 -130.96(4) . . . . ? P9 Cr3 P7 P8 -38.79(3) . . . . ? C23 Cr3 P7 P6 -152.86(9) . . . . ? C22 Cr3 P7 P6 -118.38(8) . . . . ? C25 Cr3 P7 P6 -69.32(16) . . . . ? C24 Cr3 P7 P6 -158.21(18) . . . . ? C21 Cr3 P7 P6 -81.84(8) . . . . ? P10 Cr3 P7 P6 38.46(3) . . . . ? P9 Cr3 P7 P6 92.17(4) . . . . ? P8 Cr3 P7 P6 130.96(4) . . . . ? C23 Cr3 P7 Cr4 141.81(9) . . . . ? C22 Cr3 P7 Cr4 176.29(8) . . . . ? C25 Cr3 P7 Cr4 -134.66(15) . . . . ? C24 Cr3 P7 Cr4 136.46(18) . . . . ? C21 Cr3 P7 Cr4 -147.18(8) . . . . ? P10 Cr3 P7 Cr4 -26.87(3) . . . . ? P6 Cr3 P7 Cr4 -65.33(3) . . . . ? P9 Cr3 P7 Cr4 26.83(3) . . . . ? P8 Cr3 P7 Cr4 65.62(3) . . . . ? P6 P7 P8 P9 2.09(6) . . . . ? Cr4 P7 P8 P9 -44.99(4) . . . . ? Cr3 P7 P8 P9 47.15(4) . . . . ? P6 P7 P8 Cr3 -45.06(4) . . . . ? Cr4 P7 P8 Cr3 -92.14(3) . . . . ? P6 P7 P8 Cr4 47.08(4) . . . . ? Cr3 P7 P8 Cr4 92.14(3) . . . . ? C23 Cr3 P8 P7 -119.95(8) . . . . ? C22 Cr3 P8 P7 -84.15(9) . . . . ? C25 Cr3 P8 P7 -156.61(17) . . . . ? C24 Cr3 P8 P7 -153.86(8) . . . . ? C21 Cr3 P8 P7 -72.88(15) . . . . ? P10 Cr3 P8 P7 90.68(4) . . . . ? P6 Cr3 P8 P7 37.24(3) . . . . ? P9 Cr3 P8 P7 128.62(4) . . . . ? C23 Cr3 P8 P9 111.44(8) . . . . ? C22 Cr3 P8 P9 147.23(9) . . . . ? C25 Cr3 P8 P9 74.77(17) . . . . ? C24 Cr3 P8 P9 77.52(8) . . . . ? C21 Cr3 P8 P9 158.50(15) . . . . ? P10 Cr3 P8 P9 -37.93(3) . . . . ? P6 Cr3 P8 P9 -91.37(4) . . . . ? P7 Cr3 P8 P9 -128.62(4) . . . . ? C23 Cr3 P8 Cr4 175.39(8) . . . . ? C22 Cr3 P8 Cr4 -148.81(8) . . . . ? C25 Cr3 P8 Cr4 138.73(17) . . . . ? C24 Cr3 P8 Cr4 141.48(8) . . . . ? C21 Cr3 P8 Cr4 -137.54(15) . . . . ? P10 Cr3 P8 Cr4 26.02(3) . . . . ? P6 Cr3 P8 Cr4 -27.42(3) . . . . ? P9 Cr3 P8 Cr4 63.96(3) . . . . ? P7 Cr3 P8 Cr4 -64.66(3) . . . . ? P7 P8 P9 P10 -1.87(6) . . . . ? Cr3 P8 P9 P10 45.56(4) . . . . ? Cr4 P8 P9 P10 -47.17(4) . . . . ? P7 P8 P9 Cr4 45.30(4) . . . . ? Cr3 P8 P9 Cr4 92.74(3) . . . . ? P7 P8 P9 Cr3 -47.43(4) . . . . ? Cr4 P8 P9 Cr3 -92.74(3) . . . . ? C23 Cr3 P9 P8 -82.00(8) . . . . ? C22 Cr3 P9 P8 -70.82(15) . . . . ? C25 Cr3 P9 P8 -151.67(9) . . . . ? C24 Cr3 P9 P8 -117.95(8) . . . . ? C21 Cr3 P9 P8 -154.06(18) . . . . ? P10 Cr3 P9 P8 130.38(4) . . . . ? P6 Cr3 P9 P8 91.82(4) . . . . ? P7 Cr3 P9 P8 38.63(3) . . . . ? C23 Cr3 P9 P10 147.62(8) . . . . ? C22 Cr3 P9 P10 158.79(14) . . . . ? C25 Cr3 P9 P10 77.95(9) . . . . ? C24 Cr3 P9 P10 111.66(8) . . . . ? C21 Cr3 P9 P10 75.56(18) . . . . ? P6 Cr3 P9 P10 -38.56(3) . . . . ? P8 Cr3 P9 P10 -130.38(4) . . . . ? P7 Cr3 P9 P10 -91.75(3) . . . . ? C23 Cr3 P9 Cr4 -147.64(8) . . . . ? C22 Cr3 P9 Cr4 -136.46(14) . . . . ? C25 Cr3 P9 Cr4 142.69(9) . . . . ? C24 Cr3 P9 Cr4 176.41(8) . . . . ? C21 Cr3 P9 Cr4 140.30(18) . . . . ? P10 Cr3 P9 Cr4 64.74(3) . . . . ? P6 Cr3 P9 Cr4 26.18(3) . . . . ? P8 Cr3 P9 Cr4 -65.64(3) . . . . ? P7 Cr3 P9 Cr4 -27.01(3) . . . . ? P7 P6 P10 P9 0.36(6) . . . . ? Cr3 P6 P10 P9 -46.74(4) . . . . ? Cr4 P6 P10 P9 46.05(4) . . . . ? P7 P6 P10 Cr3 47.10(4) . . . . ? Cr4 P6 P10 Cr3 92.79(3) . . . . ? P7 P6 P10 Cr4 -45.69(4) . . . . ? Cr3 P6 P10 Cr4 -92.79(3) . . . . ? P8 P9 P10 P6 0.93(6) . . . . ? Cr4 P9 P10 P6 -46.65(4) . . . . ? Cr3 P9 P10 P6 46.72(4) . . . . ? P8 P9 P10 Cr3 -45.79(4) . . . . ? Cr4 P9 P10 Cr3 -93.38(3) . . . . ? P8 P9 P10 Cr4 47.59(4) . . . . ? Cr3 P9 P10 Cr4 93.38(3) . . . . ? C23 Cr3 P10 P6 160.76(15) . . . . ? C22 Cr3 P10 P6 77.42(19) . . . . ? C25 Cr3 P10 P6 112.74(8) . . . . ? C24 Cr3 P10 P6 149.06(8) . . . . ? C21 Cr3 P10 P6 79.11(9) . . . . ? P9 Cr3 P10 P6 -129.11(4) . . . . ? P8 Cr3 P10 P6 -91.41(4) . . . . ? P7 Cr3 P10 P6 -38.35(3) . . . . ? C23 Cr3 P10 P9 -70.14(15) . . . . ? C22 Cr3 P10 P9 -153.48(19) . . . . ? C25 Cr3 P10 P9 -118.16(8) . . . . ? C24 Cr3 P10 P9 -81.83(8) . . . . ? C21 Cr3 P10 P9 -151.79(9) . . . . ? P6 Cr3 P10 P9 129.11(4) . . . . ? P8 Cr3 P10 P9 37.70(3) . . . . ? P7 Cr3 P10 P9 90.76(3) . . . . ? C23 Cr3 P10 Cr4 -134.05(14) . . . . ? C22 Cr3 P10 Cr4 142.61(18) . . . . ? C25 Cr3 P10 Cr4 177.93(8) . . . . ? C24 Cr3 P10 Cr4 -145.75(8) . . . . ? C21 Cr3 P10 Cr4 144.30(8) . . . . ? P6 Cr3 P10 Cr4 65.19(3) . . . . ? P9 Cr3 P10 Cr4 -63.92(3) . . . . ? P8 Cr3 P10 Cr4 -26.22(3) . . . . ? P7 Cr3 P10 Cr4 26.84(3) . . . . ? P8 P9 Cr4 C31 163.18(12) . . . . ? P10 P9 Cr4 C31 -67.96(12) . . . . ? Cr3 P9 Cr4 C31 -132.12(11) . . . . ? P8 P9 Cr4 C32 88.1(2) . . . . ? P10 P9 Cr4 C32 -143.1(2) . . . . ? Cr3 P9 Cr4 C32 152.8(2) . . . . ? P8 P9 Cr4 C33 75.53(9) . . . . ? P10 P9 Cr4 C33 -155.61(9) . . . . ? Cr3 P9 Cr4 C33 140.23(9) . . . . ? P8 P9 Cr4 C35 143.86(8) . . . . ? P10 P9 Cr4 C35 -87.27(8) . . . . ? Cr3 P9 Cr4 C35 -151.44(7) . . . . ? P8 P9 Cr4 C34 106.07(8) . . . . ? P10 P9 Cr4 C34 -125.07(8) . . . . ? Cr3 P9 Cr4 C34 170.77(8) . . . . ? P8 P9 Cr4 P10 -128.86(4) . . . . ? Cr3 P9 Cr4 P10 -64.16(3) . . . . ? P8 P9 Cr4 P7 -37.44(3) . . . . ? P10 P9 Cr4 P7 91.43(3) . . . . ? Cr3 P9 Cr4 P7 27.26(3) . . . . ? P8 P9 Cr4 P6 -90.68(3) . . . . ? P10 P9 Cr4 P6 38.18(3) . . . . ? Cr3 P9 Cr4 P6 -25.98(3) . . . . ? P10 P9 Cr4 P8 128.86(4) . . . . ? Cr3 P9 Cr4 P8 64.70(3) . . . . ? P6 P10 Cr4 C31 -87.86(8) . . . . ? P9 P10 Cr4 C31 142.69(8) . . . . ? Cr3 P10 Cr4 C31 -152.60(8) . . . . ? P6 P10 Cr4 C32 -68.80(12) . . . . ? P9 P10 Cr4 C32 161.75(12) . . . . ? Cr3 P10 Cr4 C32 -133.54(11) . . . . ? P6 P10 Cr4 C33 -141.3(2) . . . . ? P9 P10 Cr4 C33 89.3(2) . . . . ? Cr3 P10 Cr4 C33 154.0(2) . . . . ? P6 P10 Cr4 C35 -125.64(8) . . . . ? P9 P10 Cr4 C35 104.92(8) . . . . ? Cr3 P10 Cr4 C35 169.62(8) . . . . ? P6 P10 Cr4 C34 -155.61(10) . . . . ? P9 P10 Cr4 C34 74.95(10) . . . . ? Cr3 P10 Cr4 C34 139.66(9) . . . . ? P6 P10 Cr4 P9 129.45(4) . . . . ? Cr3 P10 Cr4 P9 64.71(3) . . . . ? P6 P10 Cr4 P7 37.66(3) . . . . ? P9 P10 Cr4 P7 -91.79(4) . . . . ? Cr3 P10 Cr4 P7 -27.08(3) . . . . ? P9 P10 Cr4 P6 -129.45(4) . . . . ? Cr3 P10 Cr4 P6 -64.74(3) . . . . ? P6 P10 Cr4 P8 90.75(4) . . . . ? P9 P10 Cr4 P8 -38.70(3) . . . . ? Cr3 P10 Cr4 P8 26.01(3) . . . . ? P8 P7 Cr4 C31 -157.74(9) . . . . ? P6 P7 Cr4 C31 73.12(9) . . . . ? Cr3 P7 Cr4 C31 137.53(9) . . . . ? P8 P7 Cr4 C32 -126.56(8) . . . . ? P6 P7 Cr4 C32 104.30(8) . . . . ? Cr3 P7 Cr4 C32 168.71(7) . . . . ? P8 P7 Cr4 C33 -88.84(8) . . . . ? P6 P7 Cr4 C33 142.02(8) . . . . ? Cr3 P7 Cr4 C33 -153.56(8) . . . . ? P8 P7 Cr4 C35 -146.1(2) . . . . ? P6 P7 Cr4 C35 84.8(2) . . . . ? Cr3 P7 Cr4 C35 149.2(2) . . . . ? P8 P7 Cr4 C34 -70.34(13) . . . . ? P6 P7 Cr4 C34 160.52(13) . . . . ? Cr3 P7 Cr4 C34 -135.07(13) . . . . ? P8 P7 Cr4 P9 37.60(3) . . . . ? P6 P7 Cr4 P9 -91.54(4) . . . . ? Cr3 P7 Cr4 P9 -27.12(3) . . . . ? P8 P7 Cr4 P10 91.54(4) . . . . ? P6 P7 Cr4 P10 -37.60(4) . . . . ? Cr3 P7 Cr4 P10 26.81(3) . . . . ? P8 P7 Cr4 P6 129.14(4) . . . . ? Cr3 P7 Cr4 P6 64.41(3) . . . . ? P6 P7 Cr4 P8 -129.14(4) . . . . ? Cr3 P7 Cr4 P8 -64.73(3) . . . . ? P10 P6 Cr4 C31 103.72(8) . . . . ? P7 P6 Cr4 C31 -125.95(8) . . . . ? Cr3 P6 Cr4 C31 168.48(8) . . . . ? P10 P6 Cr4 C32 141.78(8) . . . . ? P7 P6 Cr4 C32 -87.89(8) . . . . ? Cr3 P6 Cr4 C32 -153.46(8) . . . . ? P10 P6 Cr4 C33 159.87(12) . . . . ? P7 P6 Cr4 C33 -69.80(13) . . . . ? Cr3 P6 Cr4 C33 -135.37(12) . . . . ? P10 P6 Cr4 C35 73.20(9) . . . . ? P7 P6 Cr4 C35 -156.47(9) . . . . ? Cr3 P6 Cr4 C35 137.96(9) . . . . ? P10 P6 Cr4 C34 86.1(2) . . . . ? P7 P6 Cr4 C34 -143.5(2) . . . . ? Cr3 P6 Cr4 C34 150.9(2) . . . . ? P10 P6 Cr4 P9 -38.65(3) . . . . ? P7 P6 Cr4 P9 91.68(4) . . . . ? Cr3 P6 Cr4 P9 26.11(3) . . . . ? P7 P6 Cr4 P10 130.33(4) . . . . ? Cr3 P6 Cr4 P10 64.76(3) . . . . ? P10 P6 Cr4 P7 -130.33(4) . . . . ? Cr3 P6 Cr4 P7 -65.57(3) . . . . ? P10 P6 Cr4 P8 -92.01(4) . . . . ? P7 P6 Cr4 P8 38.32(3) . . . . ? Cr3 P6 Cr4 P8 -27.25(3) . . . . ? P7 P8 Cr4 C31 84.3(2) . . . . ? P9 P8 Cr4 C31 -145.2(2) . . . . ? Cr3 P8 Cr4 C31 149.9(2) . . . . ? P7 P8 Cr4 C32 72.95(9) . . . . ? P9 P8 Cr4 C32 -156.50(9) . . . . ? Cr3 P8 Cr4 C32 138.54(8) . . . . ? P7 P8 Cr4 C33 104.47(8) . . . . ? P9 P8 Cr4 C33 -124.98(8) . . . . ? Cr3 P8 Cr4 C33 170.05(7) . . . . ? P7 P8 Cr4 C35 162.12(12) . . . . ? P9 P8 Cr4 C35 -67.33(12) . . . . ? Cr3 P8 Cr4 C35 -132.30(12) . . . . ? P7 P8 Cr4 C34 142.27(8) . . . . ? P9 P8 Cr4 C34 -87.18(8) . . . . ? Cr3 P8 Cr4 C34 -152.14(8) . . . . ? P7 P8 Cr4 P9 -130.55(4) . . . . ? Cr3 P8 Cr4 P9 -64.97(3) . . . . ? P7 P8 Cr4 P10 -91.53(3) . . . . ? P9 P8 Cr4 P10 39.02(3) . . . . ? Cr3 P8 Cr4 P10 -25.94(3) . . . . ? P9 P8 Cr4 P7 130.55(4) . . . . ? Cr3 P8 Cr4 P7 65.58(3) . . . . ? P7 P8 Cr4 P6 -38.40(3) . . . . ? P9 P8 Cr4 P6 92.15(3) . . . . ? Cr3 P8 Cr4 P6 27.18(3) . . . . ? C32 Cr4 C31 C35 117.6(2) . . . . ? C33 Cr4 C31 C35 79.82(16) . . . . ? C34 Cr4 C31 C35 37.45(15) . . . . ? P9 Cr4 C31 C35 -31.2(2) . . . . ? P10 Cr4 C31 C35 -82.12(15) . . . . ? P7 Cr4 C31 C35 173.62(12) . . . . ? P6 Cr4 C31 C35 -135.80(14) . . . . ? P8 Cr4 C31 C35 102.2(3) . . . . ? C33 Cr4 C31 C32 -37.73(15) . . . . ? C35 Cr4 C31 C32 -117.6(2) . . . . ? C34 Cr4 C31 C32 -80.11(16) . . . . ? P9 Cr4 C31 C32 -148.72(13) . . . . ? P10 Cr4 C31 C32 160.32(13) . . . . ? P7 Cr4 C31 C32 56.07(16) . . . . ? P6 Cr4 C31 C32 106.64(14) . . . . ? P8 Cr4 C31 C32 -15.3(3) . . . . ? C32 Cr4 C31 C36 -121.3(3) . . . . ? C33 Cr4 C31 C36 -159.0(3) . . . . ? C35 Cr4 C31 C36 121.2(3) . . . . ? C34 Cr4 C31 C36 158.6(3) . . . . ? P9 Cr4 C31 C36 90.0(3) . . . . ? P10 Cr4 C31 C36 39.0(3) . . . . ? P7 Cr4 C31 C36 -65.2(3) . . . . ? P6 Cr4 C31 C36 -14.6(3) . . . . ? P8 Cr4 C31 C36 -136.6(2) . . . . ? C35 C31 C32 C33 -0.2(3) . . . . ? C36 C31 C32 C33 -178.0(3) . . . . ? Cr4 C31 C32 C33 62.23(19) . . . . ? C35 C31 C32 C37 177.8(3) . . . . ? C36 C31 C32 C37 -0.1(5) . . . . ? Cr4 C31 C32 C37 -119.8(3) . . . . ? C35 C31 C32 Cr4 -62.43(19) . . . . ? C36 C31 C32 Cr4 119.7(3) . . . . ? C31 Cr4 C32 C33 -117.0(2) . . . . ? C35 Cr4 C32 C33 -79.58(17) . . . . ? C34 Cr4 C32 C33 -37.20(16) . . . . ? P9 Cr4 C32 C33 -17.2(3) . . . . ? P10 Cr4 C32 C33 -147.59(13) . . . . ? P7 Cr4 C32 C33 107.66(15) . . . . ? P6 Cr4 C32 C33 161.52(14) . . . . ? P8 Cr4 C32 C33 57.20(17) . . . . ? C33 Cr4 C32 C31 117.0(2) . . . . ? C35 Cr4 C32 C31 37.39(15) . . . . ? C34 Cr4 C32 C31 79.77(17) . . . . ? P9 Cr4 C32 C31 99.8(3) . . . . ? P10 Cr4 C32 C31 -30.6(2) . . . . ? P7 Cr4 C32 C31 -135.37(14) . . . . ? P6 Cr4 C32 C31 -81.51(15) . . . . ? P8 Cr4 C32 C31 174.18(13) . . . . ? C31 Cr4 C32 C37 121.5(3) . . . . ? C33 Cr4 C32 C37 -121.5(3) . . . . ? C35 Cr4 C32 C37 158.9(3) . . . . ? C34 Cr4 C32 C37 -158.7(3) . . . . ? P9 Cr4 C32 C37 -138.7(2) . . . . ? P10 Cr4 C32 C37 90.9(3) . . . . ? P7 Cr4 C32 C37 -13.9(2) . . . . ? P6 Cr4 C32 C37 40.0(2) . . . . ? P8 Cr4 C32 C37 -64.3(2) . . . . ? C31 C32 C33 C34 0.2(3) . . . . ? C37 C32 C33 C34 -177.8(3) . . . . ? Cr4 C32 C33 C34 62.0(2) . . . . ? C31 C32 C33 C38 177.5(3) . . . . ? C37 C32 C33 C38 -0.5(5) . . . . ? Cr4 C32 C33 C38 -120.7(3) . . . . ? C31 C32 C33 Cr4 -61.83(19) . . . . ? C37 C32 C33 Cr4 120.2(3) . . . . ? C31 Cr4 C33 C34 -79.84(18) . . . . ? C32 Cr4 C33 C34 -117.9(2) . . . . ? C35 Cr4 C33 C34 -37.28(16) . . . . ? P9 Cr4 C33 C34 55.37(18) . . . . ? P10 Cr4 C33 C34 -19.8(3) . . . . ? P7 Cr4 C33 C34 161.26(15) . . . . ? P6 Cr4 C33 C34 -146.94(14) . . . . ? P8 Cr4 C33 C34 107.25(16) . . . . ? C31 Cr4 C33 C32 38.04(16) . . . . ? C35 Cr4 C33 C32 80.60(17) . . . . ? C34 Cr4 C33 C32 117.9(2) . . . . ? P9 Cr4 C33 C32 173.25(13) . . . . ? P10 Cr4 C33 C32 98.1(2) . . . . ? P7 Cr4 C33 C32 -80.86(16) . . . . ? P6 Cr4 C33 C32 -29.1(2) . . . . ? P8 Cr4 C33 C32 -134.87(15) . . . . ? C31 Cr4 C33 C38 160.5(3) . . . . ? C32 Cr4 C33 C38 122.5(3) . . . . ? C35 Cr4 C33 C38 -156.9(3) . . . . ? C34 Cr4 C33 C38 -119.6(3) . . . . ? P9 Cr4 C33 C38 -64.3(2) . . . . ? P10 Cr4 C33 C38 -139.5(2) . . . . ? P7 Cr4 C33 C38 41.6(2) . . . . ? P6 Cr4 C33 C38 93.4(2) . . . . ? P8 Cr4 C33 C38 -12.4(2) . . . . ? C32 C33 C34 C35 -0.1(3) . . . . ? C38 C33 C34 C35 -177.5(3) . . . . ? Cr4 C33 C34 C35 61.5(2) . . . . ? C32 C33 C34 C39 176.4(3) . . . . ? C38 C33 C34 C39 -1.0(5) . . . . ? Cr4 C33 C34 C39 -122.0(3) . . . . ? C32 C33 C34 Cr4 -61.6(2) . . . . ? C38 C33 C34 Cr4 121.0(3) . . . . ? C31 Cr4 C34 C33 80.37(17) . . . . ? C32 Cr4 C34 C33 37.40(16) . . . . ? C35 Cr4 C34 C33 117.9(2) . . . . ? P9 Cr4 C34 C33 -136.01(15) . . . . ? P10 Cr4 C34 C33 171.98(13) . . . . ? P7 Cr4 C34 C33 -29.8(2) . . . . ? P6 Cr4 C34 C33 100.0(2) . . . . ? P8 Cr4 C34 C33 -81.97(16) . . . . ? C31 Cr4 C34 C35 -37.55(16) . . . . ? C32 Cr4 C34 C35 -80.52(17) . . . . ? C33 Cr4 C34 C35 -117.9(2) . . . . ? P9 Cr4 C34 C35 106.07(15) . . . . ? P10 Cr4 C34 C35 54.06(18) . . . . ? P7 Cr4 C34 C35 -147.68(14) . . . . ? P6 Cr4 C34 C35 -17.9(3) . . . . ? P8 Cr4 C34 C35 160.11(14) . . . . ? C31 Cr4 C34 C39 -159.1(3) . . . . ? C32 Cr4 C34 C39 157.9(3) . . . . ? C33 Cr4 C34 C39 120.5(3) . . . . ? C35 Cr4 C34 C39 -121.6(3) . . . . ? P9 Cr4 C34 C39 -15.5(2) . . . . ? P10 Cr4 C34 C39 -67.5(3) . . . . ? P7 Cr4 C34 C39 90.7(3) . . . . ? P6 Cr4 C34 C39 -139.5(2) . . . . ? P8 Cr4 C34 C39 38.5(3) . . . . ? C32 C31 C35 C34 0.1(3) . . . . ? C36 C31 C35 C34 178.0(3) . . . . ? Cr4 C31 C35 C34 -61.9(2) . . . . ? C32 C31 C35 C40 -176.8(3) . . . . ? C36 C31 C35 C40 1.1(5) . . . . ? Cr4 C31 C35 C40 121.1(3) . . . . ? C32 C31 C35 Cr4 62.08(19) . . . . ? C36 C31 C35 Cr4 -120.1(3) . . . . ? C33 C34 C35 C31 0.0(3) . . . . ? C39 C34 C35 C31 -176.5(3) . . . . ? Cr4 C34 C35 C31 61.41(19) . . . . ? C33 C34 C35 C40 176.9(3) . . . . ? C39 C34 C35 C40 0.5(5) . . . . ? Cr4 C34 C35 C40 -121.7(3) . . . . ? C33 C34 C35 Cr4 -61.4(2) . . . . ? C39 C34 C35 Cr4 122.1(3) . . . . ? C32 Cr4 C35 C31 -37.74(15) . . . . ? C33 Cr4 C35 C31 -80.30(16) . . . . ? C34 Cr4 C35 C31 -117.5(2) . . . . ? P9 Cr4 C35 C31 160.12(14) . . . . ? P10 Cr4 C35 C31 105.69(14) . . . . ? P7 Cr4 C35 C31 -16.0(3) . . . . ? P6 Cr4 C35 C31 55.18(17) . . . . ? P8 Cr4 C35 C31 -149.40(13) . . . . ? C31 Cr4 C35 C34 117.5(2) . . . . ? C32 Cr4 C35 C34 79.78(17) . . . . ? C33 Cr4 C35 C34 37.22(16) . . . . ? P9 Cr4 C35 C34 -82.35(16) . . . . ? P10 Cr4 C35 C34 -136.79(15) . . . . ? P7 Cr4 C35 C34 101.5(3) . . . . ? P6 Cr4 C35 C34 172.71(13) . . . . ? P8 Cr4 C35 C34 -31.9(2) . . . . ? C31 Cr4 C35 C40 -121.3(3) . . . . ? C32 Cr4 C35 C40 -159.1(3) . . . . ? C33 Cr4 C35 C40 158.4(3) . . . . ? C34 Cr4 C35 C40 121.1(3) . . . . ? P9 Cr4 C35 C40 38.8(3) . . . . ? P10 Cr4 C35 C40 -15.6(3) . . . . ? P7 Cr4 C35 C40 -137.4(2) . . . . ? P6 Cr4 C35 C40 -66.1(3) . . . . ? P8 Cr4 C35 C40 89.3(3) . . . . ? _diffrn_measured_fraction_theta_max 0.921 _diffrn_reflns_theta_full 30.48 _diffrn_measured_fraction_theta_full 0.921 _refine_diff_density_max 1.601 _refine_diff_density_min -0.600 _refine_diff_density_rms 0.118 #===END data_070k _database_code_depnum_ccdc_archive 'CCDC 618758' _audit_creation_method SHELXL-97 _chemical_name_systematic ; \m~2~-\h^5^,\h^5^-cyclopentaphosphole)-bis ((\h^5^-pentamethyl-cyclopentadienyl)-chromium) hexafluoroantimonate ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H30 Cr2 F6 P5 Sb' _chemical_formula_weight 765.04 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M I2/a loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' _cell_length_a 22.9383(11) _cell_length_b 21.2836(10) _cell_length_c 22.9242(12) _cell_angle_alpha 90.00 _cell_angle_beta 101.227(2) _cell_angle_gamma 90.00 _cell_volume 10977.6(9) _cell_formula_units_Z 16 _cell_measurement_temperature 70(2) _cell_measurement_reflns_used 7726 _cell_measurement_theta_min 2.091 _cell_measurement_theta_max 30.522 _exptl_crystal_description 'irregular block' _exptl_crystal_colour 'dark green' _exptl_crystal_size_max 0.60 _exptl_crystal_size_mid 0.52 _exptl_crystal_size_min 0.40 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.852 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 6048 _exptl_absorpt_coefficient_mu 2.097 _exptl_absorpt_correction_type integration _exptl_absorpt_correction_T_min 0.398 _exptl_absorpt_correction_T_max 0.600 _exptl_absorpt_process_details 'XPREP in SHELXTL' _exptl_special_details ; ? ; _diffrn_ambient_temperature 70(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'Bede Microsource X-ray Generator' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEX CCD Diffractometer' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number 0 _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% 0 _diffrn_reflns_number 39446 _diffrn_reflns_av_R_equivalents 0.0393 _diffrn_reflns_av_sigmaI/netI 0.0483 _diffrn_reflns_limit_h_min -32 _diffrn_reflns_limit_h_max 32 _diffrn_reflns_limit_k_min -30 _diffrn_reflns_limit_k_max 27 _diffrn_reflns_limit_l_min -31 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_theta_min 1.15 _diffrn_reflns_theta_max 30.54 _reflns_number_total 15342 _reflns_number_gt 14235 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'SMART V5.625 (Bruker, 2003)' _computing_cell_refinement 'SMART V5.625 (Bruker, 2003)' _computing_data_reduction 'SAINT V6.28A (Bruker, 2003)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'SHELXTL V6.12(Bruker, 2001)' _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0799P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 15342 _refine_ls_number_parameters 614 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0448 _refine_ls_R_factor_gt 0.0406 _refine_ls_wR_factor_ref 0.1132 _refine_ls_wR_factor_gt 0.1082 _refine_ls_goodness_of_fit_ref 1.042 _refine_ls_restrained_S_all 1.042 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb1 Sb 0.138864(12) 0.869403(12) 0.383967(12) 0.01728(6) Uani 1 1 d . . . F1 F 0.09735(13) 0.80890(13) 0.33226(13) 0.0329(6) Uani 1 1 d . . . F2 F 0.09083(14) 0.93195(13) 0.34148(12) 0.0338(6) Uani 1 1 d . . . F3 F 0.08372(12) 0.86116(13) 0.43451(13) 0.0292(5) Uani 1 1 d . . . F4 F 0.18479(11) 0.80612(11) 0.42697(12) 0.0256(5) Uani 1 1 d . . . F5 F 0.19455(14) 0.87719(12) 0.33430(13) 0.0297(6) Uani 1 1 d . . . F6 F 0.18025(13) 0.93083(12) 0.43398(12) 0.0286(5) Uani 1 1 d . . . Sb2 Sb 0.136629(12) 0.126852(11) 0.117256(12) 0.01589(6) Uani 1 1 d . . . F7 F 0.12386(17) 0.05122(14) 0.15331(15) 0.0468(9) Uani 1 1 d . . . F8 F 0.07251(12) 0.16387(15) 0.14401(14) 0.0364(7) Uani 1 1 d . . . F9 F 0.08538(12) 0.10093(14) 0.04778(12) 0.0314(6) Uani 1 1 d . . . F10 F 0.20180(13) 0.09255(15) 0.08951(13) 0.0357(7) Uani 1 1 d . . . F11 F 0.18761(12) 0.15228(14) 0.18705(12) 0.0308(6) Uani 1 1 d . . . F12 F 0.15011(13) 0.20300(13) 0.08117(14) 0.0334(6) Uani 1 1 d . . . C1 C -0.11324(16) 0.31088(17) 0.44735(17) 0.0154(6) Uani 1 1 d . . . C2 C -0.14221(16) 0.26812(16) 0.40251(17) 0.0150(6) Uani 1 1 d . . . C3 C -0.14131(15) 0.29581(16) 0.34624(17) 0.0152(7) Uani 1 1 d . . . C4 C -0.11221(16) 0.35568(16) 0.35523(16) 0.0138(6) Uani 1 1 d . . . C5 C -0.09488(16) 0.36475(17) 0.41792(17) 0.0150(6) Uani 1 1 d . . . C6 C -0.10617(19) 0.30292(19) 0.51282(17) 0.0214(7) Uani 1 1 d . . . H6A H -0.1389 0.3241 0.5266 0.032 Uiso 1 1 calc R . . H6B H -0.0683 0.3213 0.5326 0.032 Uiso 1 1 calc R . . H6C H -0.1067 0.2581 0.5224 0.032 Uiso 1 1 calc R . . C7 C -0.17081(17) 0.20753(17) 0.4143(2) 0.0204(7) Uani 1 1 d . . . H7A H -0.2128 0.2149 0.4151 0.031 Uiso 1 1 calc R . . H7B H -0.1507 0.1906 0.4527 0.031 Uiso 1 1 calc R . . H7C H -0.1677 0.1774 0.3827 0.031 Uiso 1 1 calc R . . C8 C -0.16850(17) 0.26933(18) 0.28636(17) 0.0192(7) Uani 1 1 d . . . H8A H -0.2047 0.2927 0.2698 0.029 Uiso 1 1 calc R . . H8B H -0.1784 0.2250 0.2906 0.029 Uiso 1 1 calc R . . H8C H -0.1401 0.2730 0.2596 0.029 Uiso 1 1 calc R . . C9 C -0.10413(18) 0.40151(18) 0.30847(18) 0.0198(7) Uani 1 1 d . . . H9A H -0.1412 0.4249 0.2953 0.030 Uiso 1 1 calc R . . H9B H -0.0937 0.3790 0.2746 0.030 Uiso 1 1 calc R . . H9C H -0.0722 0.4309 0.3247 0.030 Uiso 1 1 calc R . . C10 C -0.06734(17) 0.42277(17) 0.44886(17) 0.0184(7) Uani 1 1 d . . . H10A H -0.0971 0.4454 0.4661 0.028 Uiso 1 1 calc R . . H10B H -0.0530 0.4499 0.4201 0.028 Uiso 1 1 calc R . . H10C H -0.0340 0.4109 0.4805 0.028 Uiso 1 1 calc R . . Cr1 Cr -0.04904(3) 0.28001(3) 0.39251(3) 0.01201(11) Uani 1 1 d . . . P1 P 0.03457(5) 0.26885(6) 0.47170(5) 0.0293(3) Uani 1 1 d . . . P2 P -0.01403(5) 0.18240(5) 0.43719(6) 0.0286(2) Uani 1 1 d . . . P3 P -0.03324(5) 0.18772(5) 0.33909(6) 0.0270(2) Uani 1 1 d . . . P4 P 0.00287(5) 0.27772(6) 0.31211(5) 0.0268(2) Uani 1 1 d . . . P5 P 0.04485(5) 0.32775(5) 0.39427(7) 0.0285(3) Uani 1 1 d . . . Cr2 Cr 0.06322(2) 0.21824(3) 0.38909(3) 0.01205(11) Uani 1 1 d . . . C11 C 0.14647(16) 0.17709(16) 0.44036(16) 0.0139(6) Uani 1 1 d . . . C12 C 0.11602(17) 0.13034(16) 0.40166(18) 0.0159(7) Uani 1 1 d . . . C13 C 0.11236(16) 0.15179(17) 0.34175(17) 0.0155(6) Uani 1 1 d . . . C14 C 0.14015(16) 0.21179(17) 0.34396(17) 0.0155(6) Uani 1 1 d . . . C15 C 0.16133(16) 0.22811(16) 0.40468(17) 0.0147(6) Uani 1 1 d . . . C16 C 0.16300(17) 0.17137(19) 0.50633(17) 0.0192(7) Uani 1 1 d . . . H16A H 0.2002 0.1477 0.5170 0.029 Uiso 1 1 calc R . . H16B H 0.1314 0.1493 0.5212 0.029 Uiso 1 1 calc R . . H16C H 0.1683 0.2134 0.5241 0.029 Uiso 1 1 calc R . . C17 C 0.09532(18) 0.06784(17) 0.41954(19) 0.0218(7) Uani 1 1 d . . . H17A H 0.1285 0.0381 0.4254 0.033 Uiso 1 1 calc R . . H17B H 0.0633 0.0522 0.3882 0.033 Uiso 1 1 calc R . . H17C H 0.0806 0.0723 0.4567 0.033 Uiso 1 1 calc R . . C18 C 0.08813(18) 0.11525(19) 0.28656(19) 0.0221(8) Uani 1 1 d . . . H18A H 0.1201 0.0905 0.2750 0.033 Uiso 1 1 calc R . . H18B H 0.0717 0.1443 0.2544 0.033 Uiso 1 1 calc R . . H18C H 0.0567 0.0870 0.2942 0.033 Uiso 1 1 calc R . . C19 C 0.14892(18) 0.25019(19) 0.29124(18) 0.0210(7) Uani 1 1 d . . . H19A H 0.1898 0.2452 0.2853 0.031 Uiso 1 1 calc R . . H19B H 0.1414 0.2946 0.2984 0.031 Uiso 1 1 calc R . . H19C H 0.1213 0.2358 0.2556 0.031 Uiso 1 1 calc R . . C20 C 0.19584(17) 0.28592(17) 0.42655(19) 0.0194(7) Uani 1 1 d . . . H20A H 0.2377 0.2798 0.4244 0.029 Uiso 1 1 calc R . . H20B H 0.1925 0.2940 0.4679 0.029 Uiso 1 1 calc R . . H20C H 0.1799 0.3218 0.4017 0.029 Uiso 1 1 calc R . . C21 C 0.10738(18) 0.38464(16) 0.13243(18) 0.0162(7) Uani 1 1 d . . . C22 C 0.17096(18) 0.38141(16) 0.14525(18) 0.0165(7) Uani 1 1 d . . . C23 C 0.19384(17) 0.43738(18) 0.12370(18) 0.0174(7) Uani 1 1 d . . . C24 C 0.14464(18) 0.47579(16) 0.09744(17) 0.0165(6) Uani 1 1 d . . . C25 C 0.09106(17) 0.44285(17) 0.10280(16) 0.0160(7) Uani 1 1 d . . . C26 C 0.06453(18) 0.33450(18) 0.14359(19) 0.0204(7) Uani 1 1 d . . . H26A H 0.0667 0.2987 0.1172 0.031 Uiso 1 1 calc R . . H26B H 0.0241 0.3515 0.1358 0.031 Uiso 1 1 calc R . . H26C H 0.0750 0.3206 0.1851 0.031 Uiso 1 1 calc R . . C27 C 0.20803(17) 0.32688(18) 0.17292(18) 0.0194(7) Uani 1 1 d . . . H27A H 0.2273 0.3070 0.1431 0.029 Uiso 1 1 calc R . . H27B H 0.1825 0.2961 0.1876 0.029 Uiso 1 1 calc R . . H27C H 0.2384 0.3419 0.2061 0.029 Uiso 1 1 calc R . . C28 C 0.25846(18) 0.4511(2) 0.1250(2) 0.0244(8) Uani 1 1 d . . . H28A H 0.2693 0.4360 0.0881 0.037 Uiso 1 1 calc R . . H28B H 0.2829 0.4296 0.1590 0.037 Uiso 1 1 calc R . . H28C H 0.2653 0.4964 0.1287 0.037 Uiso 1 1 calc R . . C29 C 0.1491(2) 0.53650(18) 0.06579(19) 0.0230(8) Uani 1 1 d . . . H29A H 0.1515 0.5280 0.0243 0.035 Uiso 1 1 calc R . . H29B H 0.1848 0.5591 0.0853 0.035 Uiso 1 1 calc R . . H29C H 0.1139 0.5622 0.0670 0.035 Uiso 1 1 calc R . . C30 C 0.02856(18) 0.46425(19) 0.07798(18) 0.0214(8) Uani 1 1 d . . . H30A H 0.0153 0.4462 0.0383 0.032 Uiso 1 1 calc R . . H30B H 0.0276 0.5102 0.0753 0.032 Uiso 1 1 calc R . . H30C H 0.0021 0.4502 0.1042 0.032 Uiso 1 1 calc R . . Cr3 Cr 0.14294(3) 0.46341(3) 0.19222(3) 0.01356(11) Uani 1 1 d . . . P6 P 0.08603(5) 0.44327(5) 0.26941(5) 0.01993(19) Uani 1 1 d . . . P7 P 0.18222(5) 0.42944(5) 0.29477(4) 0.01969(19) Uani 1 1 d . . . P8 P 0.22637(4) 0.50918(5) 0.26154(5) 0.02053(19) Uani 1 1 d . . . P9 P 0.15730(5) 0.57441(5) 0.21852(5) 0.01950(19) Uani 1 1 d . . . P10 P 0.07023(5) 0.53311(5) 0.22261(5) 0.01916(19) Uani 1 1 d . . . Cr4 Cr 0.14512(3) 0.53342(3) 0.31400(3) 0.01281(11) Uani 1 1 d . . . C31 C 0.09622(17) 0.55237(18) 0.38505(17) 0.0165(7) Uani 1 1 d . . . C32 C 0.15255(17) 0.52409(17) 0.41053(16) 0.0158(6) Uani 1 1 d . . . C33 C 0.19808(16) 0.56579(17) 0.39951(17) 0.0151(6) Uani 1 1 d . . . C34 C 0.17049(17) 0.61873(16) 0.36796(17) 0.0152(7) Uani 1 1 d . . . C35 C 0.10737(17) 0.61085(17) 0.35913(17) 0.0155(6) Uani 1 1 d . . . C36 C 0.03603(18) 0.52592(19) 0.38779(18) 0.0214(7) Uani 1 1 d . . . H36A H 0.0201 0.5474 0.4191 0.032 Uiso 1 1 calc R . . H36B H 0.0397 0.4809 0.3966 0.032 Uiso 1 1 calc R . . H36C H 0.0091 0.5323 0.3494 0.032 Uiso 1 1 calc R . . C37 C 0.16107(18) 0.46362(17) 0.44458(17) 0.0193(7) Uani 1 1 d . . . H37A H 0.1641 0.4723 0.4871 0.029 Uiso 1 1 calc R . . H37B H 0.1976 0.4432 0.4383 0.029 Uiso 1 1 calc R . . H37C H 0.1271 0.4359 0.4307 0.029 Uiso 1 1 calc R . . C38 C 0.26395(16) 0.55796(19) 0.41945(18) 0.0200(7) Uani 1 1 d . . . H38A H 0.2763 0.5758 0.4594 0.030 Uiso 1 1 calc R . . H38B H 0.2845 0.5798 0.3917 0.030 Uiso 1 1 calc R . . H38C H 0.2740 0.5132 0.4203 0.030 Uiso 1 1 calc R . . C39 C 0.20186(18) 0.67541(18) 0.35042(18) 0.0204(7) Uani 1 1 d . . . H39A H 0.2099 0.7050 0.3838 0.031 Uiso 1 1 calc R . . H39B H 0.1768 0.6958 0.3162 0.031 Uiso 1 1 calc R . . H39C H 0.2395 0.6625 0.3398 0.031 Uiso 1 1 calc R . . C40 C 0.06161(17) 0.65695(19) 0.33003(18) 0.0209(7) Uani 1 1 d . . . H40A H 0.0519 0.6858 0.3601 0.031 Uiso 1 1 calc R . . H40B H 0.0257 0.6344 0.3110 0.031 Uiso 1 1 calc R . . H40C H 0.0773 0.6809 0.3000 0.031 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.02016(13) 0.01202(10) 0.02058(14) -0.00130(8) 0.00625(8) 0.00119(8) F1 0.0320(14) 0.0248(13) 0.0397(16) -0.0109(11) 0.0017(12) -0.0046(11) F2 0.0491(18) 0.0249(13) 0.0265(13) 0.0055(11) 0.0053(11) 0.0141(12) F3 0.0254(13) 0.0304(13) 0.0353(15) 0.0045(11) 0.0141(11) 0.0067(11) F4 0.0221(12) 0.0186(11) 0.0372(14) 0.0038(10) 0.0085(10) 0.0055(9) F5 0.0374(16) 0.0298(15) 0.0265(14) -0.0007(10) 0.0177(12) -0.0049(11) F6 0.0423(16) 0.0192(11) 0.0243(13) -0.0053(10) 0.0063(10) -0.0067(11) Sb2 0.01761(13) 0.01172(10) 0.01880(14) -0.00023(8) 0.00466(8) 0.00037(8) F7 0.069(2) 0.0216(14) 0.0471(19) 0.0154(13) 0.0047(16) -0.0114(14) F8 0.0244(14) 0.0452(18) 0.0425(16) -0.0055(13) 0.0143(11) 0.0066(12) F9 0.0301(14) 0.0296(14) 0.0317(14) -0.0074(11) -0.0008(11) -0.0059(11) F10 0.0311(15) 0.0374(16) 0.0391(16) -0.0130(12) 0.0078(12) 0.0126(12) F11 0.0326(14) 0.0323(14) 0.0247(13) -0.0094(11) -0.0010(10) 0.0020(11) F12 0.0321(14) 0.0225(13) 0.0446(17) 0.0135(11) 0.0047(12) -0.0062(11) C1 0.0165(16) 0.0112(15) 0.0199(17) -0.0007(12) 0.0074(12) 0.0016(12) C2 0.0111(15) 0.0132(14) 0.0216(17) -0.0014(13) 0.0058(12) -0.0015(12) C3 0.0106(15) 0.0106(15) 0.0236(18) -0.0022(13) 0.0017(12) 0.0000(12) C4 0.0120(15) 0.0109(14) 0.0194(17) -0.0004(12) 0.0054(12) 0.0023(12) C5 0.0141(15) 0.0094(14) 0.0218(18) -0.0014(13) 0.0040(12) -0.0001(12) C6 0.026(2) 0.0204(18) 0.0195(18) -0.0011(14) 0.0089(14) 0.0026(15) C7 0.0158(17) 0.0125(15) 0.034(2) -0.0015(14) 0.0083(14) -0.0043(13) C8 0.0173(17) 0.0179(17) 0.0217(18) -0.0040(14) 0.0024(13) 0.0000(13) C9 0.0235(19) 0.0145(16) 0.0221(18) 0.0032(13) 0.0061(14) -0.0016(13) C10 0.0185(17) 0.0143(16) 0.0225(18) -0.0056(13) 0.0042(13) -0.0026(13) Cr1 0.0118(3) 0.0091(2) 0.0154(3) -0.00153(19) 0.00333(19) -0.00076(18) P1 0.0213(5) 0.0421(7) 0.0225(5) -0.0114(5) -0.0009(4) 0.0126(4) P2 0.0218(5) 0.0220(5) 0.0464(7) 0.0147(5) 0.0178(5) 0.0078(4) P3 0.0133(5) 0.0232(5) 0.0426(6) -0.0184(5) 0.0010(4) 0.0011(4) P4 0.0218(5) 0.0367(6) 0.0241(5) 0.0106(4) 0.0100(4) 0.0136(4) P5 0.0144(5) 0.0118(4) 0.0603(8) -0.0037(4) 0.0100(5) -0.0019(3) Cr2 0.0116(3) 0.0089(2) 0.0160(3) -0.00076(19) 0.00333(18) -0.00075(18) C11 0.0125(15) 0.0124(15) 0.0176(16) 0.0015(12) 0.0045(12) 0.0026(11) C12 0.0161(16) 0.0089(14) 0.0242(19) -0.0015(13) 0.0076(13) 0.0018(12) C13 0.0131(15) 0.0132(15) 0.0210(17) -0.0016(12) 0.0051(12) 0.0013(12) C14 0.0123(15) 0.0148(16) 0.0205(17) -0.0008(13) 0.0057(12) 0.0010(12) C15 0.0125(15) 0.0120(14) 0.0200(17) 0.0013(12) 0.0039(12) 0.0005(11) C16 0.0178(17) 0.0187(17) 0.0206(17) 0.0019(13) 0.0024(13) 0.0047(13) C17 0.0229(19) 0.0099(15) 0.035(2) 0.0002(14) 0.0127(15) -0.0022(13) C18 0.0186(19) 0.0211(18) 0.027(2) -0.0085(14) 0.0047(15) -0.0008(13) C19 0.0211(18) 0.0212(18) 0.0227(18) 0.0090(14) 0.0092(14) 0.0082(14) C20 0.0152(17) 0.0120(16) 0.031(2) 0.0002(13) 0.0032(14) -0.0042(12) C21 0.0179(18) 0.0107(14) 0.0202(18) 0.0024(12) 0.0043(13) -0.0006(12) C22 0.0179(18) 0.0117(16) 0.0199(18) 0.0009(12) 0.0037(13) 0.0038(12) C23 0.0158(17) 0.0135(16) 0.0235(18) -0.0003(13) 0.0056(13) 0.0025(12) C24 0.0211(18) 0.0125(14) 0.0172(16) 0.0009(13) 0.0074(13) 0.0030(13) C25 0.0187(17) 0.0122(15) 0.0174(16) 0.0010(12) 0.0044(13) 0.0027(12) C26 0.0209(18) 0.0149(17) 0.0263(19) 0.0030(14) 0.0069(14) -0.0063(13) C27 0.0202(18) 0.0151(16) 0.0226(18) 0.0002(13) 0.0035(14) 0.0063(13) C28 0.0146(17) 0.027(2) 0.034(2) -0.0051(16) 0.0120(15) -0.0009(14) C29 0.035(2) 0.0134(17) 0.0224(19) 0.0038(13) 0.0104(16) 0.0001(15) C30 0.0186(18) 0.0236(19) 0.0211(18) 0.0043(14) 0.0019(14) 0.0058(14) Cr3 0.0125(3) 0.0101(2) 0.0187(3) 0.00255(19) 0.0044(2) 0.00118(18) P6 0.0220(5) 0.0163(4) 0.0234(5) -0.0043(3) 0.0090(4) -0.0065(3) P7 0.0267(5) 0.0130(4) 0.0187(4) 0.0011(3) 0.0029(4) 0.0051(4) P8 0.0156(4) 0.0216(5) 0.0252(5) -0.0050(4) 0.0058(3) -0.0023(3) P9 0.0296(5) 0.0108(4) 0.0195(5) 0.0008(3) 0.0080(4) -0.0020(3) P10 0.0175(4) 0.0186(5) 0.0205(5) -0.0034(3) 0.0015(3) 0.0064(3) Cr4 0.0127(3) 0.0093(2) 0.0166(3) 0.00111(19) 0.00318(19) -0.00037(18) C31 0.0165(17) 0.0164(16) 0.0178(17) 0.0005(13) 0.0067(13) -0.0031(13) C32 0.0200(17) 0.0123(14) 0.0149(16) -0.0010(12) 0.0031(12) -0.0022(12) C33 0.0141(16) 0.0109(14) 0.0194(17) 0.0008(12) 0.0009(12) -0.0006(12) C34 0.0174(17) 0.0107(15) 0.0176(17) -0.0008(11) 0.0033(13) -0.0022(11) C35 0.0159(17) 0.0128(14) 0.0170(17) -0.0004(12) 0.0013(12) 0.0005(12) C36 0.0197(18) 0.0200(18) 0.0250(19) -0.0029(14) 0.0057(14) -0.0056(14) C37 0.027(2) 0.0114(15) 0.0198(17) 0.0033(12) 0.0049(14) -0.0028(13) C38 0.0129(16) 0.0190(17) 0.0274(19) 0.0010(14) 0.0025(13) 0.0003(13) C39 0.0257(19) 0.0122(15) 0.0240(19) 0.0026(13) 0.0071(14) -0.0039(13) C40 0.0197(18) 0.0200(18) 0.0212(17) -0.0017(14) -0.0006(14) 0.0061(14) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb1 F4 1.869(2) . ? Sb1 F6 1.871(2) . ? Sb1 F2 1.875(3) . ? Sb1 F5 1.877(3) . ? Sb1 F1 1.879(3) . ? Sb1 F3 1.883(3) . ? Sb2 F7 1.859(3) . ? Sb2 F11 1.869(3) . ? Sb2 F9 1.869(3) . ? Sb2 F12 1.873(3) . ? Sb2 F8 1.874(3) . ? Sb2 F10 1.882(3) . ? C1 C5 1.435(5) . ? C1 C2 1.436(5) . ? C1 C6 1.487(5) . ? C1 Cr1 2.214(4) . ? C2 C3 1.422(5) . ? C2 C7 1.495(5) . ? C2 Cr1 2.208(4) . ? C3 C4 1.435(5) . ? C3 C8 1.503(5) . ? C3 Cr1 2.201(3) . ? C4 C5 1.428(5) . ? C4 C9 1.487(5) . ? C4 Cr1 2.223(3) . ? C5 C10 1.501(5) . ? C5 Cr1 2.222(4) . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? Cr1 P5 2.3745(12) . ? Cr1 P3 2.3795(12) . ? Cr1 P4 2.3815(12) . ? Cr1 P1 2.3820(12) . ? Cr1 P2 2.3854(12) . ? Cr1 Cr2 2.9057(8) . ? P1 P2 2.2161(19) . ? P1 P5 2.2229(19) . ? P1 Cr2 2.3797(12) . ? P2 P3 2.2087(19) . ? P2 Cr2 2.3869(12) . ? P3 P4 2.2221(18) . ? P3 Cr2 2.3757(12) . ? P4 P5 2.2141(19) . ? P4 Cr2 2.3838(12) . ? P5 Cr2 2.3757(12) . ? Cr2 C12 2.217(4) . ? Cr2 C14 2.217(4) . ? Cr2 C11 2.218(4) . ? Cr2 C15 2.219(4) . ? Cr2 C13 2.219(4) . ? C11 C12 1.423(5) . ? C11 C15 1.440(5) . ? C11 C16 1.491(5) . ? C12 C13 1.434(5) . ? C12 C17 1.496(5) . ? C13 C14 1.424(5) . ? C13 C18 1.497(5) . ? C14 C15 1.425(5) . ? C14 C19 1.505(5) . ? C15 C20 1.496(5) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 C25 1.428(5) . ? C21 C22 1.432(6) . ? C21 C26 1.506(5) . ? C21 Cr3 2.218(4) . ? C22 C23 1.428(5) . ? C22 C27 1.504(5) . ? C22 Cr3 2.211(4) . ? C23 C24 1.428(5) . ? C23 C28 1.505(5) . ? C23 Cr3 2.203(4) . ? C24 C25 1.441(5) . ? C24 C29 1.495(5) . ? C24 Cr3 2.197(4) . ? C25 C30 1.506(5) . ? C25 Cr3 2.205(4) . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C27 H27C 0.9800 . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? Cr3 P6 2.4327(12) . ? Cr3 P10 2.4330(11) . ? Cr3 P8 2.4399(12) . ? Cr3 P9 2.4446(11) . ? Cr3 P7 2.4569(12) . ? P6 P10 2.1879(15) . ? P6 P7 2.1894(15) . ? P6 Cr4 2.4543(11) . ? P7 P8 2.1877(15) . ? P7 Cr4 2.4418(11) . ? P8 P9 2.1915(15) . ? P8 Cr4 2.4615(12) . ? P9 P10 2.2006(15) . ? P9 Cr4 2.4224(12) . ? P10 Cr4 2.4370(12) . ? Cr4 C31 2.187(4) . ? Cr4 C32 2.195(4) . ? Cr4 C33 2.206(4) . ? Cr4 C35 2.210(4) . ? Cr4 C34 2.210(4) . ? C31 C35 1.424(5) . ? C31 C32 1.442(5) . ? C31 C36 1.504(5) . ? C32 C33 1.430(5) . ? C32 C37 1.498(5) . ? C33 C34 1.419(5) . ? C33 C38 1.500(5) . ? C34 C35 1.432(5) . ? C34 C39 1.499(5) . ? C35 C40 1.496(5) . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C39 H39A 0.9800 . ? C39 H39B 0.9800 . ? C39 H39C 0.9800 . ? C40 H40A 0.9800 . ? C40 H40B 0.9800 . ? C40 H40C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F4 Sb1 F6 90.79(11) . . ? F4 Sb1 F2 178.35(13) . . ? F6 Sb1 F2 89.94(12) . . ? F4 Sb1 F5 90.19(12) . . ? F6 Sb1 F5 89.20(13) . . ? F2 Sb1 F5 91.30(13) . . ? F4 Sb1 F1 90.19(12) . . ? F6 Sb1 F1 178.70(13) . . ? F2 Sb1 F1 89.11(13) . . ? F5 Sb1 F1 89.94(13) . . ? F4 Sb1 F3 89.16(12) . . ? F6 Sb1 F3 90.54(13) . . ? F2 Sb1 F3 89.35(13) . . ? F5 Sb1 F3 179.30(13) . . ? F1 Sb1 F3 90.33(13) . . ? F7 Sb2 F11 89.81(14) . . ? F7 Sb2 F9 89.76(14) . . ? F11 Sb2 F9 179.55(14) . . ? F7 Sb2 F12 179.57(15) . . ? F11 Sb2 F12 89.88(13) . . ? F9 Sb2 F12 90.55(13) . . ? F7 Sb2 F8 90.97(16) . . ? F11 Sb2 F8 89.90(13) . . ? F9 Sb2 F8 89.97(13) . . ? F12 Sb2 F8 89.33(14) . . ? F7 Sb2 F10 91.07(16) . . ? F11 Sb2 F10 89.76(12) . . ? F9 Sb2 F10 90.39(13) . . ? F12 Sb2 F10 88.63(14) . . ? F8 Sb2 F10 177.93(14) . . ? C5 C1 C2 107.9(3) . . ? C5 C1 C6 125.5(3) . . ? C2 C1 C6 126.5(3) . . ? C5 C1 Cr1 71.4(2) . . ? C2 C1 Cr1 70.8(2) . . ? C6 C1 Cr1 125.8(3) . . ? C3 C2 C1 107.5(3) . . ? C3 C2 C7 127.3(3) . . ? C1 C2 C7 125.2(4) . . ? C3 C2 Cr1 70.9(2) . . ? C1 C2 Cr1 71.3(2) . . ? C7 C2 Cr1 125.8(3) . . ? C2 C3 C4 109.0(3) . . ? C2 C3 C8 126.6(3) . . ? C4 C3 C8 124.3(3) . . ? C2 C3 Cr1 71.5(2) . . ? C4 C3 Cr1 71.9(2) . . ? C8 C3 Cr1 124.9(3) . . ? C5 C4 C3 107.2(3) . . ? C5 C4 C9 126.0(3) . . ? C3 C4 C9 126.8(3) . . ? C5 C4 Cr1 71.2(2) . . ? C3 C4 Cr1 70.24(19) . . ? C9 C4 Cr1 126.1(2) . . ? C4 C5 C1 108.4(3) . . ? C4 C5 C10 126.6(3) . . ? C1 C5 C10 124.8(3) . . ? C4 C5 Cr1 71.3(2) . . ? C1 C5 Cr1 70.8(2) . . ? C10 C5 Cr1 127.9(3) . . ? C1 C6 H6A 109.5 . . ? C1 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C1 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C3 Cr1 C2 37.63(14) . . ? C3 Cr1 C1 62.92(14) . . ? C2 Cr1 C1 37.89(13) . . ? C3 Cr1 C5 62.77(13) . . ? C2 Cr1 C5 63.18(13) . . ? C1 Cr1 C5 37.74(13) . . ? C3 Cr1 C4 37.84(12) . . ? C2 Cr1 C4 63.34(13) . . ? C1 Cr1 C4 63.09(13) . . ? C5 Cr1 C4 37.47(13) . . ? C3 Cr1 P5 136.61(11) . . ? C2 Cr1 P5 160.11(10) . . ? C1 Cr1 P5 124.39(10) . . ? C5 Cr1 P5 97.02(10) . . ? C4 Cr1 P5 102.57(10) . . ? C3 Cr1 P3 96.12(10) . . ? C2 Cr1 P3 101.90(10) . . ? C1 Cr1 P3 136.21(10) . . ? C5 Cr1 P3 158.79(10) . . ? C4 Cr1 P3 123.60(10) . . ? P5 Cr1 P3 97.67(4) . . ? C3 Cr1 P4 102.06(11) . . ? C2 Cr1 P4 135.88(11) . . ? C1 Cr1 P4 159.00(10) . . ? C5 Cr1 P4 123.57(11) . . ? C4 Cr1 P4 95.97(10) . . ? P5 Cr1 P4 55.49(5) . . ? P3 Cr1 P4 55.64(5) . . ? C3 Cr1 P1 159.81(11) . . ? C2 Cr1 P1 124.15(11) . . ? C1 Cr1 P1 97.05(10) . . ? C5 Cr1 P1 103.48(10) . . ? C4 Cr1 P1 137.14(10) . . ? P5 Cr1 P1 55.72(5) . . ? P3 Cr1 P1 97.43(4) . . ? P4 Cr1 P1 97.94(5) . . ? C3 Cr1 P2 123.49(10) . . ? C2 Cr1 P2 96.16(10) . . ? C1 Cr1 P2 102.72(10) . . ? C5 Cr1 P2 137.01(11) . . ? C4 Cr1 P2 159.37(10) . . ? P5 Cr1 P2 97.88(5) . . ? P3 Cr1 P2 55.23(5) . . ? P4 Cr1 P2 97.89(4) . . ? P1 Cr1 P2 55.40(5) . . ? C3 Cr1 Cr2 146.12(10) . . ? C2 Cr1 Cr2 146.27(10) . . ? C1 Cr1 Cr2 147.19(10) . . ? C5 Cr1 Cr2 147.30(10) . . ? C4 Cr1 Cr2 146.32(9) . . ? P5 Cr1 Cr2 52.31(3) . . ? P3 Cr1 Cr2 52.27(3) . . ? P4 Cr1 Cr2 52.46(3) . . ? P1 Cr1 Cr2 52.36(3) . . ? P2 Cr1 Cr2 52.52(3) . . ? P2 P1 P5 107.90(6) . . ? P2 P1 Cr2 62.46(4) . . ? P5 P1 Cr2 62.04(4) . . ? P2 P1 Cr1 62.38(4) . . ? P5 P1 Cr1 61.97(4) . . ? Cr2 P1 Cr1 75.21(4) . . ? P3 P2 P1 107.92(6) . . ? P3 P2 Cr1 62.25(4) . . ? P1 P2 Cr1 62.22(4) . . ? P3 P2 Cr2 62.11(4) . . ? P1 P2 Cr2 62.13(5) . . ? Cr1 P2 Cr2 75.02(4) . . ? P2 P3 P4 108.44(6) . . ? P2 P3 Cr2 62.63(4) . . ? P4 P3 Cr2 62.35(4) . . ? P2 P3 Cr1 62.52(4) . . ? P4 P3 Cr1 62.22(4) . . ? Cr2 P3 Cr1 75.33(4) . . ? P5 P4 P3 107.57(6) . . ? P5 P4 Cr1 62.10(4) . . ? P3 P4 Cr1 62.13(4) . . ? P5 P4 Cr2 62.09(4) . . ? P3 P4 Cr2 61.98(4) . . ? Cr1 P4 Cr2 75.15(4) . . ? P4 P5 P1 108.17(6) . . ? P4 P5 Cr1 62.42(4) . . ? P1 P5 Cr1 62.31(4) . . ? P4 P5 Cr2 62.46(4) . . ? P1 P5 Cr2 62.22(4) . . ? Cr1 P5 Cr2 75.42(4) . . ? C12 Cr2 C14 62.87(14) . . ? C12 Cr2 C11 37.42(13) . . ? C14 Cr2 C11 62.71(13) . . ? C12 Cr2 C15 63.10(13) . . ? C14 Cr2 C15 37.48(13) . . ? C11 Cr2 C15 37.87(13) . . ? C12 Cr2 C13 37.72(14) . . ? C14 Cr2 C13 37.44(13) . . ? C11 Cr2 C13 62.65(13) . . ? C15 Cr2 C13 62.82(13) . . ? C12 Cr2 P3 105.42(11) . . ? C14 Cr2 P3 120.60(10) . . ? C11 Cr2 P3 140.58(10) . . ? C15 Cr2 P3 157.48(10) . . ? C13 Cr2 P3 95.96(10) . . ? C12 Cr2 P5 156.82(11) . . ? C14 Cr2 P5 104.42(10) . . ? C11 Cr2 P5 120.24(10) . . ? C15 Cr2 P5 94.77(9) . . ? C13 Cr2 P5 139.60(10) . . ? P3 Cr2 P5 97.75(4) . . ? C12 Cr2 P1 120.48(11) . . ? C14 Cr2 P1 140.15(10) . . ? C11 Cr2 P1 95.72(10) . . ? C15 Cr2 P1 104.93(10) . . ? C13 Cr2 P1 157.35(11) . . ? P3 Cr2 P1 97.60(4) . . ? P5 Cr2 P1 55.74(5) . . ? C12 Cr2 P4 140.20(11) . . ? C14 Cr2 P4 95.03(10) . . ? C11 Cr2 P4 156.61(10) . . ? C15 Cr2 P4 119.57(10) . . ? C13 Cr2 P4 104.68(10) . . ? P3 Cr2 P4 55.66(5) . . ? P5 Cr2 P4 55.44(5) . . ? P1 Cr2 P4 97.94(4) . . ? C12 Cr2 P2 96.10(11) . . ? C14 Cr2 P2 157.78(10) . . ? C11 Cr2 P2 105.60(10) . . ? C15 Cr2 P2 140.96(10) . . ? C13 Cr2 P2 121.04(10) . . ? P3 Cr2 P2 55.26(5) . . ? P5 Cr2 P2 97.80(4) . . ? P1 Cr2 P2 55.41(5) . . ? P4 Cr2 P2 97.78(4) . . ? C12 Cr2 Cr1 147.46(10) . . ? C14 Cr2 Cr1 146.17(10) . . ? C11 Cr2 Cr1 147.17(10) . . ? C15 Cr2 Cr1 146.01(9) . . ? C13 Cr2 Cr1 147.00(10) . . ? P3 Cr2 Cr1 52.39(3) . . ? P5 Cr2 Cr1 52.27(3) . . ? P1 Cr2 Cr1 52.43(3) . . ? P4 Cr2 Cr1 52.39(3) . . ? P2 Cr2 Cr1 52.47(3) . . ? C12 C11 C15 108.4(3) . . ? C12 C11 C16 124.9(3) . . ? C15 C11 C16 126.6(3) . . ? C12 C11 Cr2 71.2(2) . . ? C15 C11 Cr2 71.1(2) . . ? C16 C11 Cr2 126.3(3) . . ? C11 C12 C13 107.7(3) . . ? C11 C12 C17 126.5(4) . . ? C13 C12 C17 125.7(3) . . ? C11 C12 Cr2 71.4(2) . . ? C13 C12 Cr2 71.2(2) . . ? C17 C12 Cr2 126.3(3) . . ? C14 C13 C12 108.0(3) . . ? C14 C13 C18 125.9(3) . . ? C12 C13 C18 125.9(3) . . ? C14 C13 Cr2 71.2(2) . . ? C12 C13 Cr2 71.0(2) . . ? C18 C13 Cr2 127.2(3) . . ? C13 C14 C15 108.6(3) . . ? C13 C14 C19 126.0(4) . . ? C15 C14 C19 125.4(3) . . ? C13 C14 Cr2 71.4(2) . . ? C15 C14 Cr2 71.3(2) . . ? C19 C14 Cr2 125.8(3) . . ? C14 C15 C11 107.3(3) . . ? C14 C15 C20 125.8(3) . . ? C11 C15 C20 126.7(3) . . ? C14 C15 Cr2 71.2(2) . . ? C11 C15 Cr2 71.0(2) . . ? C20 C15 Cr2 125.9(3) . . ? C11 C16 H16A 109.5 . . ? C11 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C11 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C25 C21 C22 107.6(3) . . ? C25 C21 C26 125.2(4) . . ? C22 C21 C26 127.1(3) . . ? C25 C21 Cr3 70.7(2) . . ? C22 C21 Cr3 70.9(2) . . ? C26 C21 Cr3 127.2(3) . . ? C23 C22 C21 108.5(3) . . ? C23 C22 C27 125.0(4) . . ? C21 C22 C27 126.4(3) . . ? C23 C22 Cr3 70.8(2) . . ? C21 C22 Cr3 71.4(2) . . ? C27 C22 Cr3 126.7(3) . . ? C22 C23 C24 108.1(3) . . ? C22 C23 C28 125.5(3) . . ? C24 C23 C28 126.3(4) . . ? C22 C23 Cr3 71.4(2) . . ? C24 C23 Cr3 70.8(2) . . ? C28 C23 Cr3 126.5(3) . . ? C23 C24 C25 107.6(3) . . ? C23 C24 C29 125.2(4) . . ? C25 C24 C29 127.0(4) . . ? C23 C24 Cr3 71.3(2) . . ? C25 C24 Cr3 71.2(2) . . ? C29 C24 Cr3 126.9(3) . . ? C21 C25 C24 108.3(3) . . ? C21 C25 C30 125.8(4) . . ? C24 C25 C30 125.9(3) . . ? C21 C25 Cr3 71.7(2) . . ? C24 C25 Cr3 70.6(2) . . ? C30 C25 Cr3 126.4(3) . . ? C21 C26 H26A 109.5 . . ? C21 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C21 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C22 C27 H27A 109.5 . . ? C22 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? C22 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? C23 C28 H28A 109.5 . . ? C23 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C23 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C24 C29 H29A 109.5 . . ? C24 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C24 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C25 C30 H30A 109.5 . . ? C25 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? C25 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C24 Cr3 C23 37.89(13) . . ? C24 Cr3 C25 38.22(14) . . ? C23 Cr3 C25 63.39(14) . . ? C24 Cr3 C22 63.26(14) . . ? C23 Cr3 C22 37.76(14) . . ? C25 Cr3 C22 63.00(14) . . ? C24 Cr3 C21 63.55(14) . . ? C23 Cr3 C21 63.35(14) . . ? C25 Cr3 C21 37.66(13) . . ? C22 Cr3 C21 37.73(14) . . ? C24 Cr3 P6 148.88(11) . . ? C23 Cr3 P6 155.28(10) . . ? C25 Cr3 P6 111.87(11) . . ? C22 Cr3 P6 117.59(11) . . ? C21 Cr3 P6 97.55(11) . . ? C24 Cr3 P10 110.81(10) . . ? C23 Cr3 P10 147.74(10) . . ? C25 Cr3 P10 96.39(10) . . ? C22 Cr3 P10 154.32(11) . . ? C21 Cr3 P10 116.60(11) . . ? P6 Cr3 P10 53.44(4) . . ? C24 Cr3 P8 115.70(11) . . ? C23 Cr3 P8 96.17(11) . . ? C25 Cr3 P8 153.88(11) . . ? C22 Cr3 P8 111.52(11) . . ? C21 Cr3 P8 148.40(11) . . ? P6 Cr3 P8 93.47(4) . . ? P10 Cr3 P8 93.70(4) . . ? C24 Cr3 P9 95.77(10) . . ? C23 Cr3 P9 110.75(10) . . ? C25 Cr3 P9 116.33(10) . . ? C22 Cr3 P9 147.68(11) . . ? C21 Cr3 P9 153.98(10) . . ? P6 Cr3 P9 93.24(4) . . ? P10 Cr3 P9 53.64(4) . . ? P8 Cr3 P9 53.32(4) . . ? C24 Cr3 P7 155.22(11) . . ? C23 Cr3 P7 117.50(10) . . ? C25 Cr3 P7 149.58(10) . . ? C22 Cr3 P7 98.42(11) . . ? C21 Cr3 P7 113.02(10) . . ? P6 Cr3 P7 53.20(4) . . ? P10 Cr3 P7 92.84(4) . . ? P8 Cr3 P7 53.07(4) . . ? P9 Cr3 P7 92.39(4) . . ? P10 P6 P7 108.05(6) . . ? P10 P6 Cr3 63.28(4) . . ? P7 P6 Cr3 63.97(4) . . ? P10 P6 Cr4 63.02(4) . . ? P7 P6 Cr4 63.15(4) . . ? Cr3 P6 Cr4 80.46(4) . . ? P8 P7 P6 108.31(6) . . ? P8 P7 Cr4 63.96(4) . . ? P6 P7 Cr4 63.73(4) . . ? P8 P7 Cr3 63.07(4) . . ? P6 P7 Cr3 62.84(4) . . ? Cr4 P7 Cr3 80.23(3) . . ? P7 P8 P9 107.76(6) . . ? P7 P8 Cr3 63.86(4) . . ? P9 P8 Cr3 63.45(4) . . ? P7 P8 Cr4 63.04(4) . . ? P9 P8 Cr4 62.43(4) . . ? Cr3 P8 Cr4 80.17(4) . . ? P8 P9 P10 108.08(5) . . ? P8 P9 Cr4 64.26(4) . . ? P10 P9 Cr4 63.41(4) . . ? P8 P9 Cr3 63.23(4) . . ? P10 P9 Cr3 62.91(4) . . ? Cr4 P9 Cr3 80.86(4) . . ? P6 P10 P9 107.75(6) . . ? P6 P10 Cr3 63.27(4) . . ? P9 P10 Cr3 63.45(4) . . ? P6 P10 Cr4 63.84(4) . . ? P9 P10 Cr4 62.74(4) . . ? Cr3 P10 Cr4 80.80(4) . . ? C31 Cr4 C32 38.42(14) . . ? C31 Cr4 C33 63.53(14) . . ? C32 Cr4 C33 37.93(13) . . ? C31 Cr4 C35 37.77(14) . . ? C32 Cr4 C35 63.65(14) . . ? C33 Cr4 C35 63.21(13) . . ? C31 Cr4 C34 63.20(14) . . ? C32 Cr4 C34 63.25(13) . . ? C33 Cr4 C34 37.50(13) . . ? C35 Cr4 C34 37.81(14) . . ? C31 Cr4 P9 140.57(11) . . ? C32 Cr4 P9 160.64(10) . . ? C33 Cr4 P9 123.37(10) . . ? C35 Cr4 P9 106.20(10) . . ? C34 Cr4 P9 98.38(10) . . ? C31 Cr4 P10 105.24(11) . . ? C32 Cr4 P10 140.34(11) . . ? C33 Cr4 P10 159.87(10) . . ? C35 Cr4 P10 97.45(10) . . ? C34 Cr4 P10 123.24(10) . . ? P9 Cr4 P10 53.85(4) . . ? C31 Cr4 P7 123.29(11) . . ? C32 Cr4 P7 97.97(10) . . ? C33 Cr4 P7 107.01(10) . . ? C35 Cr4 P7 160.46(11) . . ? C34 Cr4 P7 141.49(11) . . ? P9 Cr4 P7 93.31(4) . . ? P10 Cr4 P7 93.12(4) . . ? C31 Cr4 P6 97.62(10) . . ? C32 Cr4 P6 106.10(10) . . ? C33 Cr4 P6 141.10(10) . . ? C35 Cr4 P6 122.89(10) . . ? C34 Cr4 P6 159.91(11) . . ? P9 Cr4 P6 93.25(4) . . ? P10 Cr4 P6 53.14(4) . . ? P7 Cr4 P6 53.12(4) . . ? C31 Cr4 P8 161.66(11) . . ? C32 Cr4 P8 123.78(11) . . ? C33 Cr4 P8 99.28(10) . . ? C35 Cr4 P8 141.99(11) . . ? C34 Cr4 P8 107.68(11) . . ? P9 Cr4 P8 53.32(4) . . ? P10 Cr4 P8 93.06(4) . . ? P7 Cr4 P8 52.99(4) . . ? P6 Cr4 P8 92.40(4) . . ? C35 C31 C32 108.3(3) . . ? C35 C31 C36 125.9(4) . . ? C32 C31 C36 125.8(3) . . ? C35 C31 Cr4 72.0(2) . . ? C32 C31 Cr4 71.1(2) . . ? C36 C31 Cr4 124.8(3) . . ? C33 C32 C31 107.3(3) . . ? C33 C32 C37 126.8(3) . . ? C31 C32 C37 125.8(3) . . ? C33 C32 Cr4 71.4(2) . . ? C31 C32 Cr4 70.5(2) . . ? C37 C32 Cr4 125.4(3) . . ? C34 C33 C32 108.3(3) . . ? C34 C33 C38 124.5(3) . . ? C32 C33 C38 127.2(3) . . ? C34 C33 Cr4 71.4(2) . . ? C32 C33 Cr4 70.6(2) . . ? C38 C33 Cr4 125.7(3) . . ? C33 C34 C35 108.5(3) . . ? C33 C34 C39 125.9(4) . . ? C35 C34 C39 125.5(3) . . ? C33 C34 Cr4 71.1(2) . . ? C35 C34 Cr4 71.1(2) . . ? C39 C34 Cr4 126.8(3) . . ? C31 C35 C34 107.6(3) . . ? C31 C35 C40 126.3(4) . . ? C34 C35 C40 126.1(3) . . ? C31 C35 Cr4 70.2(2) . . ? C34 C35 Cr4 71.1(2) . . ? C40 C35 Cr4 125.8(3) . . ? C31 C36 H36A 109.5 . . ? C31 C36 H36B 109.5 . . ? H36A C36 H36B 109.5 . . ? C31 C36 H36C 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C32 C37 H37A 109.5 . . ? C32 C37 H37B 109.5 . . ? H37A C37 H37B 109.5 . . ? C32 C37 H37C 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? C33 C38 H38A 109.5 . . ? C33 C38 H38B 109.5 . . ? H38A C38 H38B 109.5 . . ? C33 C38 H38C 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? C34 C39 H39A 109.5 . . ? C34 C39 H39B 109.5 . . ? H39A C39 H39B 109.5 . . ? C34 C39 H39C 109.5 . . ? H39A C39 H39C 109.5 . . ? H39B C39 H39C 109.5 . . ? C35 C40 H40A 109.5 . . ? C35 C40 H40B 109.5 . . ? H40A C40 H40B 109.5 . . ? C35 C40 H40C 109.5 . . ? H40A C40 H40C 109.5 . . ? H40B C40 H40C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 C1 C2 C3 0.1(4) . . . . ? C6 C1 C2 C3 177.1(4) . . . . ? Cr1 C1 C2 C3 -62.1(2) . . . . ? C5 C1 C2 C7 -176.7(3) . . . . ? C6 C1 C2 C7 0.3(6) . . . . ? Cr1 C1 C2 C7 121.2(4) . . . . ? C5 C1 C2 Cr1 62.2(2) . . . . ? C6 C1 C2 Cr1 -120.9(4) . . . . ? C1 C2 C3 C4 -0.2(4) . . . . ? C7 C2 C3 C4 176.5(3) . . . . ? Cr1 C2 C3 C4 -62.5(2) . . . . ? C1 C2 C3 C8 -177.5(3) . . . . ? C7 C2 C3 C8 -0.8(6) . . . . ? Cr1 C2 C3 C8 120.2(4) . . . . ? C1 C2 C3 Cr1 62.3(2) . . . . ? C7 C2 C3 Cr1 -121.0(4) . . . . ? C2 C3 C4 C5 0.2(4) . . . . ? C8 C3 C4 C5 177.6(3) . . . . ? Cr1 C3 C4 C5 -62.0(2) . . . . ? C2 C3 C4 C9 -177.0(3) . . . . ? C8 C3 C4 C9 0.5(6) . . . . ? Cr1 C3 C4 C9 120.8(4) . . . . ? C2 C3 C4 Cr1 62.2(2) . . . . ? C8 C3 C4 Cr1 -120.4(4) . . . . ? C3 C4 C5 C1 -0.1(4) . . . . ? C9 C4 C5 C1 177.1(3) . . . . ? Cr1 C4 C5 C1 -61.5(2) . . . . ? C3 C4 C5 C10 -174.8(3) . . . . ? C9 C4 C5 C10 2.4(6) . . . . ? Cr1 C4 C5 C10 123.9(4) . . . . ? C3 C4 C5 Cr1 61.4(2) . . . . ? C9 C4 C5 Cr1 -121.4(4) . . . . ? C2 C1 C5 C4 0.0(4) . . . . ? C6 C1 C5 C4 -177.0(4) . . . . ? Cr1 C1 C5 C4 61.8(2) . . . . ? C2 C1 C5 C10 174.8(3) . . . . ? C6 C1 C5 C10 -2.2(6) . . . . ? Cr1 C1 C5 C10 -123.4(4) . . . . ? C2 C1 C5 Cr1 -61.8(2) . . . . ? C6 C1 C5 Cr1 121.2(4) . . . . ? C4 C3 Cr1 C2 118.1(3) . . . . ? C8 C3 Cr1 C2 -122.2(4) . . . . ? C2 C3 Cr1 C1 -38.0(2) . . . . ? C4 C3 Cr1 C1 80.2(2) . . . . ? C8 C3 Cr1 C1 -160.2(4) . . . . ? C2 C3 Cr1 C5 -80.6(2) . . . . ? C4 C3 Cr1 C5 37.6(2) . . . . ? C8 C3 Cr1 C5 157.2(4) . . . . ? C2 C3 Cr1 C4 -118.1(3) . . . . ? C8 C3 Cr1 C4 119.6(4) . . . . ? C2 C3 Cr1 P5 -150.44(17) . . . . ? C4 C3 Cr1 P5 -32.3(3) . . . . ? C8 C3 Cr1 P5 87.4(3) . . . . ? C2 C3 Cr1 P3 101.58(19) . . . . ? C4 C3 Cr1 P3 -140.3(2) . . . . ? C8 C3 Cr1 P3 -20.6(3) . . . . ? C2 C3 Cr1 P4 157.69(18) . . . . ? C4 C3 Cr1 P4 -84.2(2) . . . . ? C8 C3 Cr1 P4 35.5(3) . . . . ? C2 C3 Cr1 P1 -30.4(4) . . . . ? C4 C3 Cr1 P1 87.8(4) . . . . ? C8 C3 Cr1 P1 -152.6(3) . . . . ? C2 C3 Cr1 P2 49.7(2) . . . . ? C4 C3 Cr1 P2 167.80(17) . . . . ? C8 C3 Cr1 P2 -72.5(3) . . . . ? C2 C3 Cr1 Cr2 120.8(2) . . . . ? C4 C3 Cr1 Cr2 -121.1(2) . . . . ? C8 C3 Cr1 Cr2 -1.4(4) . . . . ? C1 C2 Cr1 C3 -116.9(3) . . . . ? C7 C2 Cr1 C3 122.7(4) . . . . ? C3 C2 Cr1 C1 116.9(3) . . . . ? C7 C2 Cr1 C1 -120.4(4) . . . . ? C3 C2 Cr1 C5 79.4(2) . . . . ? C1 C2 Cr1 C5 -37.5(2) . . . . ? C7 C2 Cr1 C5 -157.9(4) . . . . ? C3 C2 Cr1 C4 37.3(2) . . . . ? C1 C2 Cr1 C4 -79.7(2) . . . . ? C7 C2 Cr1 C4 160.0(4) . . . . ? C3 C2 Cr1 P5 85.0(4) . . . . ? C1 C2 Cr1 P5 -31.9(4) . . . . ? C7 C2 Cr1 P5 -152.3(3) . . . . ? C3 C2 Cr1 P3 -84.5(2) . . . . ? C1 C2 Cr1 P3 158.53(19) . . . . ? C7 C2 Cr1 P3 38.2(3) . . . . ? C3 C2 Cr1 P4 -32.2(3) . . . . ? C1 C2 Cr1 P4 -149.14(18) . . . . ? C7 C2 Cr1 P4 90.5(3) . . . . ? C3 C2 Cr1 P1 167.83(17) . . . . ? C1 C2 Cr1 P1 50.9(2) . . . . ? C7 C2 Cr1 P1 -69.4(4) . . . . ? C3 C2 Cr1 P2 -140.26(19) . . . . ? C1 C2 Cr1 P2 102.8(2) . . . . ? C7 C2 Cr1 P2 -17.5(3) . . . . ? C3 C2 Cr1 Cr2 -120.4(2) . . . . ? C1 C2 Cr1 Cr2 122.7(2) . . . . ? C7 C2 Cr1 Cr2 2.3(5) . . . . ? C5 C1 Cr1 C3 -79.7(2) . . . . ? C2 C1 Cr1 C3 37.7(2) . . . . ? C6 C1 Cr1 C3 159.4(4) . . . . ? C5 C1 Cr1 C2 -117.4(3) . . . . ? C6 C1 Cr1 C2 121.7(4) . . . . ? C2 C1 Cr1 C5 117.4(3) . . . . ? C6 C1 Cr1 C5 -120.9(4) . . . . ? C5 C1 Cr1 C4 -37.0(2) . . . . ? C2 C1 Cr1 C4 80.4(2) . . . . ? C6 C1 Cr1 C4 -157.9(4) . . . . ? C5 C1 Cr1 P5 50.0(2) . . . . ? C2 C1 Cr1 P5 167.42(18) . . . . ? C6 C1 Cr1 P5 -70.9(3) . . . . ? C5 C1 Cr1 P3 -148.56(18) . . . . ? C2 C1 Cr1 P3 -31.2(3) . . . . ? C6 C1 Cr1 P3 90.5(3) . . . . ? C5 C1 Cr1 P4 -32.3(4) . . . . ? C2 C1 Cr1 P4 85.1(4) . . . . ? C6 C1 Cr1 P4 -153.2(3) . . . . ? C5 C1 Cr1 P1 102.9(2) . . . . ? C2 C1 Cr1 P1 -139.7(2) . . . . ? C6 C1 Cr1 P1 -18.0(3) . . . . ? C5 C1 Cr1 P2 158.98(19) . . . . ? C2 C1 Cr1 P2 -83.6(2) . . . . ? C6 C1 Cr1 P2 38.1(3) . . . . ? C5 C1 Cr1 Cr2 122.2(2) . . . . ? C2 C1 Cr1 Cr2 -120.4(2) . . . . ? C6 C1 Cr1 Cr2 1.3(4) . . . . ? C4 C5 Cr1 C3 -37.9(2) . . . . ? C1 C5 Cr1 C3 80.1(2) . . . . ? C10 C5 Cr1 C3 -160.2(4) . . . . ? C4 C5 Cr1 C2 -80.4(2) . . . . ? C1 C5 Cr1 C2 37.7(2) . . . . ? C10 C5 Cr1 C2 157.3(4) . . . . ? C4 C5 Cr1 C1 -118.1(3) . . . . ? C10 C5 Cr1 C1 119.7(4) . . . . ? C1 C5 Cr1 C4 118.1(3) . . . . ? C10 C5 Cr1 C4 -122.3(4) . . . . ? C4 C5 Cr1 P5 101.5(2) . . . . ? C1 C5 Cr1 P5 -140.4(2) . . . . ? C10 C5 Cr1 P5 -20.8(3) . . . . ? C4 C5 Cr1 P3 -32.0(4) . . . . ? C1 C5 Cr1 P3 86.0(4) . . . . ? C10 C5 Cr1 P3 -154.3(2) . . . . ? C4 C5 Cr1 P4 48.6(2) . . . . ? C1 C5 Cr1 P4 166.70(18) . . . . ? C10 C5 Cr1 P4 -73.6(4) . . . . ? C4 C5 Cr1 P1 157.88(18) . . . . ? C1 C5 Cr1 P1 -84.1(2) . . . . ? C10 C5 Cr1 P1 35.6(3) . . . . ? C4 C5 Cr1 P2 -148.93(17) . . . . ? C1 C5 Cr1 P2 -30.9(3) . . . . ? C10 C5 Cr1 P2 88.8(3) . . . . ? C4 C5 Cr1 Cr2 120.0(2) . . . . ? C1 C5 Cr1 Cr2 -122.0(2) . . . . ? C10 C5 Cr1 Cr2 -2.3(5) . . . . ? C5 C4 Cr1 C3 117.0(3) . . . . ? C9 C4 Cr1 C3 -121.7(4) . . . . ? C5 C4 Cr1 C2 79.9(2) . . . . ? C3 C4 Cr1 C2 -37.0(2) . . . . ? C9 C4 Cr1 C2 -158.7(4) . . . . ? C5 C4 Cr1 C1 37.3(2) . . . . ? C3 C4 Cr1 C1 -79.7(2) . . . . ? C9 C4 Cr1 C1 158.6(4) . . . . ? C3 C4 Cr1 C5 -117.0(3) . . . . ? C9 C4 Cr1 C5 121.3(4) . . . . ? C5 C4 Cr1 P5 -85.1(2) . . . . ? C3 C4 Cr1 P5 157.9(2) . . . . ? C9 C4 Cr1 P5 36.2(3) . . . . ? C5 C4 Cr1 P3 166.68(17) . . . . ? C3 C4 Cr1 P3 49.7(2) . . . . ? C9 C4 Cr1 P3 -72.0(3) . . . . ? C5 C4 Cr1 P4 -141.04(19) . . . . ? C3 C4 Cr1 P4 102.0(2) . . . . ? C9 C4 Cr1 P4 -19.7(3) . . . . ? C5 C4 Cr1 P1 -32.6(3) . . . . ? C3 C4 Cr1 P1 -149.53(19) . . . . ? C9 C4 Cr1 P1 88.8(3) . . . . ? C5 C4 Cr1 P2 87.0(3) . . . . ? C3 C4 Cr1 P2 -30.0(4) . . . . ? C9 C4 Cr1 P2 -151.7(2) . . . . ? C5 C4 Cr1 Cr2 -122.5(2) . . . . ? C3 C4 Cr1 Cr2 120.6(2) . . . . ? C9 C4 Cr1 Cr2 -1.1(4) . . . . ? C3 Cr1 P1 P2 93.8(3) . . . . ? C2 Cr1 P1 P2 71.92(12) . . . . ? C1 Cr1 P1 P2 100.62(10) . . . . ? C5 Cr1 P1 P2 138.45(11) . . . . ? C4 Cr1 P1 P2 158.13(14) . . . . ? P5 Cr1 P1 P2 -132.19(6) . . . . ? P3 Cr1 P1 P2 -37.94(5) . . . . ? P4 Cr1 P1 P2 -94.13(5) . . . . ? Cr2 Cr1 P1 P2 -66.32(4) . . . . ? C3 Cr1 P1 P5 -134.0(3) . . . . ? C2 Cr1 P1 P5 -155.89(12) . . . . ? C1 Cr1 P1 P5 -127.19(10) . . . . ? C5 Cr1 P1 P5 -89.35(11) . . . . ? C4 Cr1 P1 P5 -69.67(14) . . . . ? P3 Cr1 P1 P5 94.25(5) . . . . ? P4 Cr1 P1 P5 38.06(5) . . . . ? P2 Cr1 P1 P5 132.19(6) . . . . ? Cr2 Cr1 P1 P5 65.87(4) . . . . ? C3 Cr1 P1 Cr2 160.1(3) . . . . ? C2 Cr1 P1 Cr2 138.24(12) . . . . ? C1 Cr1 P1 Cr2 166.94(10) . . . . ? C5 Cr1 P1 Cr2 -155.22(10) . . . . ? C4 Cr1 P1 Cr2 -135.55(14) . . . . ? P5 Cr1 P1 Cr2 -65.87(4) . . . . ? P3 Cr1 P1 Cr2 28.38(5) . . . . ? P4 Cr1 P1 Cr2 -27.81(5) . . . . ? P2 Cr1 P1 Cr2 66.32(4) . . . . ? P5 P1 P2 P3 0.25(8) . . . . ? Cr2 P1 P2 P3 -43.36(5) . . . . ? Cr1 P1 P2 P3 43.66(5) . . . . ? P5 P1 P2 Cr1 -43.41(5) . . . . ? Cr2 P1 P2 Cr1 -87.02(4) . . . . ? P5 P1 P2 Cr2 43.61(5) . . . . ? Cr1 P1 P2 Cr2 87.02(4) . . . . ? C3 Cr1 P2 P3 72.31(13) . . . . ? C2 Cr1 P2 P3 100.22(11) . . . . ? C1 Cr1 P2 P3 138.09(11) . . . . ? C5 Cr1 P2 P3 156.87(15) . . . . ? C4 Cr1 P2 P3 93.9(3) . . . . ? P5 Cr1 P2 P3 -93.90(5) . . . . ? P4 Cr1 P2 P3 -37.84(5) . . . . ? P1 Cr1 P2 P3 -132.08(6) . . . . ? Cr2 Cr1 P2 P3 -66.03(4) . . . . ? C3 Cr1 P2 P1 -155.61(13) . . . . ? C2 Cr1 P2 P1 -127.70(11) . . . . ? C1 Cr1 P2 P1 -89.83(11) . . . . ? C5 Cr1 P2 P1 -71.05(15) . . . . ? C4 Cr1 P2 P1 -134.0(3) . . . . ? P5 Cr1 P2 P1 38.17(6) . . . . ? P3 Cr1 P2 P1 132.08(6) . . . . ? P4 Cr1 P2 P1 94.24(6) . . . . ? Cr2 Cr1 P2 P1 66.05(5) . . . . ? C3 Cr1 P2 Cr2 138.34(13) . . . . ? C2 Cr1 P2 Cr2 166.25(10) . . . . ? C1 Cr1 P2 Cr2 -155.88(10) . . . . ? C5 Cr1 P2 Cr2 -137.10(14) . . . . ? C4 Cr1 P2 Cr2 159.9(3) . . . . ? P5 Cr1 P2 Cr2 -27.88(5) . . . . ? P3 Cr1 P2 Cr2 66.03(4) . . . . ? P4 Cr1 P2 Cr2 28.19(5) . . . . ? P1 Cr1 P2 Cr2 -66.05(5) . . . . ? P1 P2 P3 P4 -0.29(8) . . . . ? Cr1 P2 P3 P4 43.35(5) . . . . ? Cr2 P2 P3 P4 -43.66(5) . . . . ? P1 P2 P3 Cr2 43.37(5) . . . . ? Cr1 P2 P3 Cr2 87.01(4) . . . . ? P1 P2 P3 Cr1 -43.65(5) . . . . ? Cr2 P2 P3 Cr1 -87.01(4) . . . . ? C3 Cr1 P3 P2 -126.96(11) . . . . ? C2 Cr1 P3 P2 -89.27(11) . . . . ? C1 Cr1 P3 P2 -70.32(15) . . . . ? C5 Cr1 P3 P2 -132.2(3) . . . . ? C4 Cr1 P3 P2 -155.03(12) . . . . ? P5 Cr1 P3 P2 94.29(6) . . . . ? P4 Cr1 P3 P2 132.60(6) . . . . ? P1 Cr1 P3 P2 38.04(5) . . . . ? Cr2 Cr1 P3 P2 66.45(4) . . . . ? C3 Cr1 P3 P4 100.44(11) . . . . ? C2 Cr1 P3 P4 138.12(11) . . . . ? C1 Cr1 P3 P4 157.08(15) . . . . ? C5 Cr1 P3 P4 95.2(3) . . . . ? C4 Cr1 P3 P4 72.36(12) . . . . ? P5 Cr1 P3 P4 -38.31(5) . . . . ? P1 Cr1 P3 P4 -94.57(6) . . . . ? P2 Cr1 P3 P4 -132.60(6) . . . . ? Cr2 Cr1 P3 P4 -66.15(4) . . . . ? C3 Cr1 P3 Cr2 166.59(11) . . . . ? C2 Cr1 P3 Cr2 -155.72(11) . . . . ? C1 Cr1 P3 Cr2 -136.77(15) . . . . ? C5 Cr1 P3 Cr2 161.3(3) . . . . ? C4 Cr1 P3 Cr2 138.52(11) . . . . ? P5 Cr1 P3 Cr2 27.84(5) . . . . ? P4 Cr1 P3 Cr2 66.15(4) . . . . ? P1 Cr1 P3 Cr2 -28.41(5) . . . . ? P2 Cr1 P3 Cr2 -66.45(4) . . . . ? P2 P3 P4 P5 0.22(8) . . . . ? Cr2 P3 P4 P5 -43.57(5) . . . . ? Cr1 P3 P4 P5 43.72(5) . . . . ? P2 P3 P4 Cr1 -43.50(5) . . . . ? Cr2 P3 P4 Cr1 -87.30(4) . . . . ? P2 P3 P4 Cr2 43.80(5) . . . . ? Cr1 P3 P4 Cr2 87.30(4) . . . . ? C3 Cr1 P4 P5 139.02(10) . . . . ? C2 Cr1 P4 P5 158.47(14) . . . . ? C1 Cr1 P4 P5 97.0(3) . . . . ? C5 Cr1 P4 P5 73.84(12) . . . . ? C4 Cr1 P4 P5 101.17(10) . . . . ? P3 Cr1 P4 P5 -131.78(6) . . . . ? P1 Cr1 P4 P5 -38.19(5) . . . . ? P2 Cr1 P4 P5 -94.17(5) . . . . ? Cr2 Cr1 P4 P5 -65.96(4) . . . . ? C3 Cr1 P4 P3 -89.20(10) . . . . ? C2 Cr1 P4 P3 -69.75(14) . . . . ? C1 Cr1 P4 P3 -131.2(3) . . . . ? C5 Cr1 P4 P3 -154.38(12) . . . . ? C4 Cr1 P4 P3 -127.05(10) . . . . ? P5 Cr1 P4 P3 131.78(6) . . . . ? P1 Cr1 P4 P3 93.60(5) . . . . ? P2 Cr1 P4 P3 37.62(5) . . . . ? Cr2 Cr1 P4 P3 65.83(4) . . . . ? C3 Cr1 P4 Cr2 -155.03(10) . . . . ? C2 Cr1 P4 Cr2 -135.58(14) . . . . ? C1 Cr1 P4 Cr2 162.9(3) . . . . ? C5 Cr1 P4 Cr2 139.79(12) . . . . ? C4 Cr1 P4 Cr2 167.12(10) . . . . ? P5 Cr1 P4 Cr2 65.96(4) . . . . ? P3 Cr1 P4 Cr2 -65.83(4) . . . . ? P1 Cr1 P4 Cr2 27.77(5) . . . . ? P2 Cr1 P4 Cr2 -28.21(5) . . . . ? P3 P4 P5 P1 -0.07(8) . . . . ? Cr1 P4 P5 P1 43.67(5) . . . . ? Cr2 P4 P5 P1 -43.59(5) . . . . ? P3 P4 P5 Cr1 -43.74(5) . . . . ? Cr2 P4 P5 Cr1 -87.26(4) . . . . ? P3 P4 P5 Cr2 43.52(5) . . . . ? Cr1 P4 P5 Cr2 87.26(4) . . . . ? P2 P1 P5 P4 -0.11(8) . . . . ? Cr2 P1 P5 P4 43.71(5) . . . . ? Cr1 P1 P5 P4 -43.73(5) . . . . ? P2 P1 P5 Cr1 43.62(5) . . . . ? Cr2 P1 P5 Cr1 87.43(4) . . . . ? P2 P1 P5 Cr2 -43.82(5) . . . . ? Cr1 P1 P5 Cr2 -87.43(4) . . . . ? C3 Cr1 P5 P4 -69.00(15) . . . . ? C2 Cr1 P5 P4 -131.3(3) . . . . ? C1 Cr1 P5 P4 -154.46(13) . . . . ? C5 Cr1 P5 P4 -126.26(11) . . . . ? C4 Cr1 P5 P4 -88.62(10) . . . . ? P3 Cr1 P5 P4 38.40(5) . . . . ? P1 Cr1 P5 P4 132.19(6) . . . . ? P2 Cr1 P5 P4 94.19(5) . . . . ? Cr2 Cr1 P5 P4 66.23(4) . . . . ? C3 Cr1 P5 P1 158.81(15) . . . . ? C2 Cr1 P5 P1 96.5(3) . . . . ? C1 Cr1 P5 P1 73.35(13) . . . . ? C5 Cr1 P5 P1 101.55(11) . . . . ? C4 Cr1 P5 P1 139.19(10) . . . . ? P3 Cr1 P5 P1 -93.79(6) . . . . ? P4 Cr1 P5 P1 -132.19(6) . . . . ? P2 Cr1 P5 P1 -38.00(5) . . . . ? Cr2 Cr1 P5 P1 -65.96(4) . . . . ? C3 Cr1 P5 Cr2 -135.23(15) . . . . ? C2 Cr1 P5 Cr2 162.5(3) . . . . ? C1 Cr1 P5 Cr2 139.31(12) . . . . ? C5 Cr1 P5 Cr2 167.51(11) . . . . ? C4 Cr1 P5 Cr2 -154.85(10) . . . . ? P3 Cr1 P5 Cr2 -27.83(5) . . . . ? P4 Cr1 P5 Cr2 -66.23(4) . . . . ? P1 Cr1 P5 Cr2 65.96(4) . . . . ? P2 Cr1 P5 Cr2 27.96(5) . . . . ? P2 P3 Cr2 C12 86.72(12) . . . . ? P4 P3 Cr2 C12 -140.96(12) . . . . ? Cr1 P3 Cr2 C12 153.04(11) . . . . ? P2 P3 Cr2 C14 153.98(12) . . . . ? P4 P3 Cr2 C14 -73.69(12) . . . . ? Cr1 P3 Cr2 C14 -139.70(11) . . . . ? P2 P3 Cr2 C11 70.84(16) . . . . ? P4 P3 Cr2 C11 -156.84(16) . . . . ? Cr1 P3 Cr2 C11 137.16(16) . . . . ? P2 P3 Cr2 C15 142.7(3) . . . . ? P4 P3 Cr2 C15 -85.0(3) . . . . ? Cr1 P3 Cr2 C15 -151.0(3) . . . . ? P2 P3 Cr2 C13 123.95(11) . . . . ? P4 P3 Cr2 C13 -103.73(11) . . . . ? Cr1 P3 Cr2 C13 -169.73(10) . . . . ? P2 P3 Cr2 P5 -94.15(6) . . . . ? P4 P3 Cr2 P5 38.17(5) . . . . ? Cr1 P3 Cr2 P5 -27.83(5) . . . . ? P2 P3 Cr2 P1 -37.87(5) . . . . ? P4 P3 Cr2 P1 94.46(5) . . . . ? Cr1 P3 Cr2 P1 28.45(5) . . . . ? P2 P3 Cr2 P4 -132.32(6) . . . . ? Cr1 P3 Cr2 P4 -66.00(4) . . . . ? P4 P3 Cr2 P2 132.32(6) . . . . ? Cr1 P3 Cr2 P2 66.32(4) . . . . ? P2 P3 Cr2 Cr1 -66.32(4) . . . . ? P4 P3 Cr2 Cr1 66.00(4) . . . . ? P4 P5 Cr2 C12 139.6(3) . . . . ? P1 P5 Cr2 C12 -88.2(3) . . . . ? Cr1 P5 Cr2 C12 -154.2(3) . . . . ? P4 P5 Cr2 C14 86.14(11) . . . . ? P1 P5 Cr2 C14 -141.62(11) . . . . ? Cr1 P5 Cr2 C14 152.32(11) . . . . ? P4 P5 Cr2 C11 152.68(12) . . . . ? P1 P5 Cr2 C11 -75.08(12) . . . . ? Cr1 P5 Cr2 C11 -141.15(11) . . . . ? P4 P5 Cr2 C15 122.94(11) . . . . ? P1 P5 Cr2 C15 -104.83(11) . . . . ? Cr1 P5 Cr2 C15 -170.89(10) . . . . ? P4 P5 Cr2 C13 70.47(16) . . . . ? P1 P5 Cr2 C13 -157.30(16) . . . . ? Cr1 P5 Cr2 C13 136.64(16) . . . . ? P4 P5 Cr2 P3 -38.29(5) . . . . ? P1 P5 Cr2 P3 93.94(5) . . . . ? Cr1 P5 Cr2 P3 27.88(5) . . . . ? P4 P5 Cr2 P1 -132.23(6) . . . . ? Cr1 P5 Cr2 P1 -66.06(4) . . . . ? P1 P5 Cr2 P4 132.23(6) . . . . ? Cr1 P5 Cr2 P4 66.17(4) . . . . ? P4 P5 Cr2 P2 -94.11(6) . . . . ? P1 P5 Cr2 P2 38.13(5) . . . . ? Cr1 P5 Cr2 P2 -27.94(5) . . . . ? P4 P5 Cr2 Cr1 -66.17(4) . . . . ? P1 P5 Cr2 Cr1 66.06(4) . . . . ? P2 P1 Cr2 C12 -75.16(12) . . . . ? P5 P1 Cr2 C12 152.83(12) . . . . ? Cr1 P1 Cr2 C12 -141.38(12) . . . . ? P2 P1 Cr2 C14 -158.22(16) . . . . ? P5 P1 Cr2 C14 69.77(16) . . . . ? Cr1 P1 Cr2 C14 135.55(16) . . . . ? P2 P1 Cr2 C11 -105.02(10) . . . . ? P5 P1 Cr2 C11 122.97(10) . . . . ? Cr1 P1 Cr2 C11 -171.25(10) . . . . ? P2 P1 Cr2 C15 -142.43(10) . . . . ? P5 P1 Cr2 C15 85.56(10) . . . . ? Cr1 P1 Cr2 C15 151.35(10) . . . . ? P2 P1 Cr2 C13 -88.5(3) . . . . ? P5 P1 Cr2 C13 139.5(3) . . . . ? Cr1 P1 Cr2 C13 -154.7(3) . . . . ? P2 P1 Cr2 P3 37.79(5) . . . . ? P5 P1 Cr2 P3 -94.23(5) . . . . ? Cr1 P1 Cr2 P3 -28.44(5) . . . . ? P2 P1 Cr2 P5 132.01(6) . . . . ? Cr1 P1 Cr2 P5 65.79(4) . . . . ? P2 P1 Cr2 P4 94.01(5) . . . . ? P5 P1 Cr2 P4 -38.00(5) . . . . ? Cr1 P1 Cr2 P4 27.78(5) . . . . ? P5 P1 Cr2 P2 -132.01(6) . . . . ? Cr1 P1 Cr2 P2 -66.23(4) . . . . ? P2 P1 Cr2 Cr1 66.23(4) . . . . ? P5 P1 Cr2 Cr1 -65.79(4) . . . . ? P5 P4 Cr2 C12 -156.50(17) . . . . ? P3 P4 Cr2 C12 71.54(17) . . . . ? Cr1 P4 Cr2 C12 137.54(16) . . . . ? P5 P4 Cr2 C14 -104.06(10) . . . . ? P3 P4 Cr2 C14 123.98(10) . . . . ? Cr1 P4 Cr2 C14 -170.02(10) . . . . ? P5 P4 Cr2 C11 -87.0(3) . . . . ? P3 P4 Cr2 C11 141.0(3) . . . . ? Cr1 P4 Cr2 C11 -153.0(3) . . . . ? P5 P4 Cr2 C15 -74.06(12) . . . . ? P3 P4 Cr2 C15 153.97(12) . . . . ? Cr1 P4 Cr2 C15 -140.02(11) . . . . ? P5 P4 Cr2 C13 -140.84(11) . . . . ? P3 P4 Cr2 C13 87.20(11) . . . . ? Cr1 P4 Cr2 C13 153.20(10) . . . . ? P5 P4 Cr2 P3 131.96(6) . . . . ? Cr1 P4 Cr2 P3 66.00(4) . . . . ? P3 P4 Cr2 P5 -131.96(6) . . . . ? Cr1 P4 Cr2 P5 -65.96(4) . . . . ? P5 P4 Cr2 P1 38.16(5) . . . . ? P3 P4 Cr2 P1 -93.80(5) . . . . ? Cr1 P4 Cr2 P1 -27.80(5) . . . . ? P5 P4 Cr2 P2 94.14(5) . . . . ? P3 P4 Cr2 P2 -37.82(5) . . . . ? Cr1 P4 Cr2 P2 28.18(5) . . . . ? P5 P4 Cr2 Cr1 65.96(4) . . . . ? P3 P4 Cr2 Cr1 -66.00(4) . . . . ? P3 P2 Cr2 C12 -104.56(11) . . . . ? P1 P2 Cr2 C12 123.09(11) . . . . ? Cr1 P2 Cr2 C12 -170.75(11) . . . . ? P3 P2 Cr2 C14 -86.6(3) . . . . ? P1 P2 Cr2 C14 141.1(3) . . . . ? Cr1 P2 Cr2 C14 -152.8(3) . . . . ? P3 P2 Cr2 C11 -141.48(11) . . . . ? P1 P2 Cr2 C11 86.17(11) . . . . ? Cr1 P2 Cr2 C11 152.33(10) . . . . ? P3 P2 Cr2 C15 -158.36(16) . . . . ? P1 P2 Cr2 C15 69.29(16) . . . . ? Cr1 P2 Cr2 C15 135.45(15) . . . . ? P3 P2 Cr2 C13 -74.35(12) . . . . ? P1 P2 Cr2 C13 153.31(12) . . . . ? Cr1 P2 Cr2 C13 -140.54(12) . . . . ? P1 P2 Cr2 P3 -132.35(6) . . . . ? Cr1 P2 Cr2 P3 -66.19(4) . . . . ? P3 P2 Cr2 P5 94.04(5) . . . . ? P1 P2 Cr2 P5 -38.30(5) . . . . ? Cr1 P2 Cr2 P5 27.85(5) . . . . ? P3 P2 Cr2 P1 132.35(6) . . . . ? Cr1 P2 Cr2 P1 66.16(4) . . . . ? P3 P2 Cr2 P4 38.04(5) . . . . ? P1 P2 Cr2 P4 -94.31(5) . . . . ? Cr1 P2 Cr2 P4 -28.15(5) . . . . ? P3 P2 Cr2 Cr1 66.19(4) . . . . ? P1 P2 Cr2 Cr1 -66.16(4) . . . . ? C3 Cr1 Cr2 C12 -78.8(3) . . . . ? C2 Cr1 Cr2 C12 -7.9(3) . . . . ? C1 Cr1 Cr2 C12 64.6(3) . . . . ? C5 Cr1 Cr2 C12 138.1(3) . . . . ? C4 Cr1 Cr2 C12 -150.1(3) . . . . ? P5 Cr1 Cr2 C12 161.5(2) . . . . ? P3 Cr1 Cr2 C12 -54.3(2) . . . . ? P4 Cr1 Cr2 C12 -126.6(2) . . . . ? P1 Cr1 Cr2 C12 89.1(2) . . . . ? P2 Cr1 Cr2 C12 17.3(2) . . . . ? C3 Cr1 Cr2 C14 65.9(3) . . . . ? C2 Cr1 Cr2 C14 136.7(3) . . . . ? C1 Cr1 Cr2 C14 -150.7(3) . . . . ? C5 Cr1 Cr2 C14 -77.3(3) . . . . ? C4 Cr1 Cr2 C14 -5.5(3) . . . . ? P5 Cr1 Cr2 C14 -53.92(18) . . . . ? P3 Cr1 Cr2 C14 90.28(18) . . . . ? P4 Cr1 Cr2 C14 18.07(18) . . . . ? P1 Cr1 Cr2 C14 -126.29(18) . . . . ? P2 Cr1 Cr2 C14 161.90(18) . . . . ? C3 Cr1 Cr2 C11 -151.6(3) . . . . ? C2 Cr1 Cr2 C11 -80.8(3) . . . . ? C1 Cr1 Cr2 C11 -8.2(3) . . . . ? C5 Cr1 Cr2 C11 65.2(3) . . . . ? C4 Cr1 Cr2 C11 137.0(2) . . . . ? P5 Cr1 Cr2 C11 88.59(18) . . . . ? P3 Cr1 Cr2 C11 -127.21(18) . . . . ? P4 Cr1 Cr2 C11 160.57(18) . . . . ? P1 Cr1 Cr2 C11 16.22(18) . . . . ? P2 Cr1 Cr2 C11 -55.59(18) . . . . ? C3 Cr1 Cr2 C15 136.2(2) . . . . ? C2 Cr1 Cr2 C15 -153.0(3) . . . . ? C1 Cr1 Cr2 C15 -80.4(3) . . . . ? C5 Cr1 Cr2 C15 -7.0(3) . . . . ? C4 Cr1 Cr2 C15 64.8(3) . . . . ? P5 Cr1 Cr2 C15 16.40(18) . . . . ? P3 Cr1 Cr2 C15 160.60(19) . . . . ? P4 Cr1 Cr2 C15 88.38(18) . . . . ? P1 Cr1 Cr2 C15 -55.97(18) . . . . ? P2 Cr1 Cr2 C15 -127.78(19) . . . . ? C3 Cr1 Cr2 C13 -5.4(3) . . . . ? C2 Cr1 Cr2 C13 65.4(3) . . . . ? C1 Cr1 Cr2 C13 138.0(3) . . . . ? C5 Cr1 Cr2 C13 -148.6(3) . . . . ? C4 Cr1 Cr2 C13 -76.8(3) . . . . ? P5 Cr1 Cr2 C13 -125.20(19) . . . . ? P3 Cr1 Cr2 C13 19.00(19) . . . . ? P4 Cr1 Cr2 C13 -53.21(19) . . . . ? P1 Cr1 Cr2 C13 162.43(19) . . . . ? P2 Cr1 Cr2 C13 90.62(19) . . . . ? C3 Cr1 Cr2 P3 -24.43(18) . . . . ? C2 Cr1 Cr2 P3 46.43(19) . . . . ? C1 Cr1 Cr2 P3 118.98(19) . . . . ? C5 Cr1 Cr2 P3 -167.6(2) . . . . ? C4 Cr1 Cr2 P3 -95.78(18) . . . . ? P5 Cr1 Cr2 P3 -144.20(7) . . . . ? P4 Cr1 Cr2 P3 -72.22(6) . . . . ? P1 Cr1 Cr2 P3 143.43(7) . . . . ? P2 Cr1 Cr2 P3 71.62(6) . . . . ? C3 Cr1 Cr2 P5 119.78(19) . . . . ? C2 Cr1 Cr2 P5 -169.36(19) . . . . ? C1 Cr1 Cr2 P5 -96.81(19) . . . . ? C5 Cr1 Cr2 P5 -23.40(19) . . . . ? C4 Cr1 Cr2 P5 48.43(18) . . . . ? P3 Cr1 Cr2 P5 144.20(7) . . . . ? P4 Cr1 Cr2 P5 71.99(6) . . . . ? P1 Cr1 Cr2 P5 -72.37(6) . . . . ? P2 Cr1 Cr2 P5 -144.18(7) . . . . ? C3 Cr1 Cr2 P1 -167.85(19) . . . . ? C2 Cr1 Cr2 P1 -96.99(19) . . . . ? C1 Cr1 Cr2 P1 -24.44(19) . . . . ? C5 Cr1 Cr2 P1 48.97(19) . . . . ? C4 Cr1 Cr2 P1 120.80(18) . . . . ? P5 Cr1 Cr2 P1 72.37(6) . . . . ? P3 Cr1 Cr2 P1 -143.43(7) . . . . ? P4 Cr1 Cr2 P1 144.36(7) . . . . ? P2 Cr1 Cr2 P1 -71.81(6) . . . . ? C3 Cr1 Cr2 P4 47.79(19) . . . . ? C2 Cr1 Cr2 P4 118.65(19) . . . . ? C1 Cr1 Cr2 P4 -168.80(19) . . . . ? C5 Cr1 Cr2 P4 -95.4(2) . . . . ? C4 Cr1 Cr2 P4 -23.56(18) . . . . ? P5 Cr1 Cr2 P4 -71.99(6) . . . . ? P3 Cr1 Cr2 P4 72.22(6) . . . . ? P1 Cr1 Cr2 P4 -144.36(7) . . . . ? P2 Cr1 Cr2 P4 143.84(7) . . . . ? C3 Cr1 Cr2 P2 -96.05(19) . . . . ? C2 Cr1 Cr2 P2 -25.18(19) . . . . ? C1 Cr1 Cr2 P2 47.36(18) . . . . ? C5 Cr1 Cr2 P2 120.8(2) . . . . ? C4 Cr1 Cr2 P2 -167.40(18) . . . . ? P5 Cr1 Cr2 P2 144.18(7) . . . . ? P3 Cr1 Cr2 P2 -71.62(6) . . . . ? P4 Cr1 Cr2 P2 -143.84(7) . . . . ? P1 Cr1 Cr2 P2 71.81(6) . . . . ? C14 Cr2 C11 C12 -80.2(2) . . . . ? C15 Cr2 C11 C12 -117.9(3) . . . . ? C13 Cr2 C11 C12 -37.9(2) . . . . ? P3 Cr2 C11 C12 25.7(3) . . . . ? P5 Cr2 C11 C12 -171.55(19) . . . . ? P1 Cr2 C11 C12 135.1(2) . . . . ? P4 Cr2 C11 C12 -99.4(3) . . . . ? P2 Cr2 C11 C12 79.4(2) . . . . ? Cr1 Cr2 C11 C12 122.2(2) . . . . ? C12 Cr2 C11 C15 117.9(3) . . . . ? C14 Cr2 C11 C15 37.7(2) . . . . ? C13 Cr2 C11 C15 80.1(2) . . . . ? P3 Cr2 C11 C15 143.63(18) . . . . ? P5 Cr2 C11 C15 -53.6(2) . . . . ? P1 Cr2 C11 C15 -107.0(2) . . . . ? P4 Cr2 C11 C15 18.5(4) . . . . ? P2 Cr2 C11 C15 -162.67(19) . . . . ? Cr1 Cr2 C11 C15 -119.9(2) . . . . ? C12 Cr2 C11 C16 -120.1(4) . . . . ? C14 Cr2 C11 C16 159.7(4) . . . . ? C15 Cr2 C11 C16 122.0(4) . . . . ? C13 Cr2 C11 C16 -157.9(4) . . . . ? P3 Cr2 C11 C16 -94.3(3) . . . . ? P5 Cr2 C11 C16 68.4(3) . . . . ? P1 Cr2 C11 C16 15.0(3) . . . . ? P4 Cr2 C11 C16 140.6(3) . . . . ? P2 Cr2 C11 C16 -40.6(3) . . . . ? Cr1 Cr2 C11 C16 2.2(4) . . . . ? C15 C11 C12 C13 0.6(4) . . . . ? C16 C11 C12 C13 -176.0(3) . . . . ? Cr2 C11 C12 C13 62.3(3) . . . . ? C15 C11 C12 C17 176.5(3) . . . . ? C16 C11 C12 C17 -0.1(6) . . . . ? Cr2 C11 C12 C17 -121.8(4) . . . . ? C15 C11 C12 Cr2 -61.7(2) . . . . ? C16 C11 C12 Cr2 121.7(4) . . . . ? C14 Cr2 C12 C11 79.7(2) . . . . ? C15 Cr2 C12 C11 37.5(2) . . . . ? C13 Cr2 C12 C11 117.0(3) . . . . ? P3 Cr2 C12 C11 -163.38(19) . . . . ? P5 Cr2 C12 C11 18.8(4) . . . . ? P1 Cr2 C12 C11 -54.6(2) . . . . ? P4 Cr2 C12 C11 142.27(19) . . . . ? P2 Cr2 C12 C11 -107.8(2) . . . . ? Cr1 Cr2 C12 C11 -121.5(2) . . . . ? C14 Cr2 C12 C13 -37.3(2) . . . . ? C11 Cr2 C12 C13 -117.0(3) . . . . ? C15 Cr2 C12 C13 -79.6(2) . . . . ? P3 Cr2 C12 C13 79.6(2) . . . . ? P5 Cr2 C12 C13 -98.2(3) . . . . ? P1 Cr2 C12 C13 -171.65(18) . . . . ? P4 Cr2 C12 C13 25.3(3) . . . . ? P2 Cr2 C12 C13 135.2(2) . . . . ? Cr1 Cr2 C12 C13 121.5(2) . . . . ? C14 Cr2 C12 C17 -158.2(4) . . . . ? C11 Cr2 C12 C17 122.0(4) . . . . ? C15 Cr2 C12 C17 159.5(4) . . . . ? C13 Cr2 C12 C17 -120.9(4) . . . . ? P3 Cr2 C12 C17 -41.3(4) . . . . ? P5 Cr2 C12 C17 140.8(3) . . . . ? P1 Cr2 C12 C17 67.4(4) . . . . ? P4 Cr2 C12 C17 -95.7(4) . . . . ? P2 Cr2 C12 C17 14.2(4) . . . . ? Cr1 Cr2 C12 C17 0.5(5) . . . . ? C11 C12 C13 C14 -0.4(4) . . . . ? C17 C12 C13 C14 -176.4(3) . . . . ? Cr2 C12 C13 C14 62.0(2) . . . . ? C11 C12 C13 C18 174.9(3) . . . . ? C17 C12 C13 C18 -1.0(6) . . . . ? Cr2 C12 C13 C18 -122.7(4) . . . . ? C11 C12 C13 Cr2 -62.4(2) . . . . ? C17 C12 C13 Cr2 121.7(4) . . . . ? C12 Cr2 C13 C14 -117.5(3) . . . . ? C11 Cr2 C13 C14 -80.0(2) . . . . ? C15 Cr2 C13 C14 -37.2(2) . . . . ? P3 Cr2 C13 C14 134.9(2) . . . . ? P5 Cr2 C13 C14 25.5(3) . . . . ? P1 Cr2 C13 C14 -98.6(3) . . . . ? P4 Cr2 C13 C14 78.9(2) . . . . ? P2 Cr2 C13 C14 -172.41(18) . . . . ? Cr1 Cr2 C13 C14 119.8(2) . . . . ? C14 Cr2 C13 C12 117.5(3) . . . . ? C11 Cr2 C13 C12 37.5(2) . . . . ? C15 Cr2 C13 C12 80.4(2) . . . . ? P3 Cr2 C13 C12 -107.6(2) . . . . ? P5 Cr2 C13 C12 143.04(19) . . . . ? P1 Cr2 C13 C12 19.0(4) . . . . ? P4 Cr2 C13 C12 -163.60(19) . . . . ? P2 Cr2 C13 C12 -54.9(2) . . . . ? Cr1 Cr2 C13 C12 -122.6(2) . . . . ? C12 Cr2 C13 C18 121.2(4) . . . . ? C14 Cr2 C13 C18 -121.2(4) . . . . ? C11 Cr2 C13 C18 158.8(4) . . . . ? C15 Cr2 C13 C18 -158.4(4) . . . . ? P3 Cr2 C13 C18 13.6(3) . . . . ? P5 Cr2 C13 C18 -95.7(3) . . . . ? P1 Cr2 C13 C18 140.2(3) . . . . ? P4 Cr2 C13 C18 -42.4(3) . . . . ? P2 Cr2 C13 C18 66.3(4) . . . . ? Cr1 Cr2 C13 C18 -1.4(5) . . . . ? C12 C13 C14 C15 0.1(4) . . . . ? C18 C13 C14 C15 -175.2(3) . . . . ? Cr2 C13 C14 C15 62.0(3) . . . . ? C12 C13 C14 C19 177.0(3) . . . . ? C18 C13 C14 C19 1.6(6) . . . . ? Cr2 C13 C14 C19 -121.1(4) . . . . ? C12 C13 C14 Cr2 -61.9(2) . . . . ? C18 C13 C14 Cr2 122.8(4) . . . . ? C12 Cr2 C14 C13 37.6(2) . . . . ? C11 Cr2 C14 C13 79.8(2) . . . . ? C15 Cr2 C14 C13 117.9(3) . . . . ? P3 Cr2 C14 C13 -55.0(2) . . . . ? P5 Cr2 C14 C13 -163.3(2) . . . . ? P1 Cr2 C14 C13 143.55(19) . . . . ? P4 Cr2 C14 C13 -107.7(2) . . . . ? P2 Cr2 C14 C13 17.4(4) . . . . ? Cr1 Cr2 C14 C13 -122.0(2) . . . . ? C12 Cr2 C14 C15 -80.4(2) . . . . ? C11 Cr2 C14 C15 -38.1(2) . . . . ? C13 Cr2 C14 C15 -117.9(3) . . . . ? P3 Cr2 C14 C15 -172.91(17) . . . . ? P5 Cr2 C14 C15 78.8(2) . . . . ? P1 Cr2 C14 C15 25.6(3) . . . . ? P4 Cr2 C14 C15 134.38(19) . . . . ? P2 Cr2 C14 C15 -100.5(3) . . . . ? Cr1 Cr2 C14 C15 120.1(2) . . . . ? C12 Cr2 C14 C19 159.0(4) . . . . ? C11 Cr2 C14 C19 -158.7(4) . . . . ? C15 Cr2 C14 C19 -120.6(4) . . . . ? C13 Cr2 C14 C19 121.4(4) . . . . ? P3 Cr2 C14 C19 66.5(3) . . . . ? P5 Cr2 C14 C19 -41.8(3) . . . . ? P1 Cr2 C14 C19 -95.0(3) . . . . ? P4 Cr2 C14 C19 13.8(3) . . . . ? P2 Cr2 C14 C19 138.8(3) . . . . ? Cr1 Cr2 C14 C19 -0.5(4) . . . . ? C13 C14 C15 C11 0.2(4) . . . . ? C19 C14 C15 C11 -176.7(3) . . . . ? Cr2 C14 C15 C11 62.2(2) . . . . ? C13 C14 C15 C20 176.8(3) . . . . ? C19 C14 C15 C20 0.0(6) . . . . ? Cr2 C14 C15 C20 -121.2(4) . . . . ? C13 C14 C15 Cr2 -62.0(2) . . . . ? C19 C14 C15 Cr2 121.1(4) . . . . ? C12 C11 C15 C14 -0.5(4) . . . . ? C16 C11 C15 C14 176.0(3) . . . . ? Cr2 C11 C15 C14 -62.3(2) . . . . ? C12 C11 C15 C20 -177.1(3) . . . . ? C16 C11 C15 C20 -0.6(6) . . . . ? Cr2 C11 C15 C20 121.1(4) . . . . ? C12 C11 C15 Cr2 61.8(3) . . . . ? C16 C11 C15 Cr2 -121.7(4) . . . . ? C12 Cr2 C15 C14 79.7(2) . . . . ? C11 Cr2 C15 C14 116.7(3) . . . . ? C13 Cr2 C15 C14 37.1(2) . . . . ? P3 Cr2 C15 C14 16.1(4) . . . . ? P5 Cr2 C15 C14 -107.6(2) . . . . ? P1 Cr2 C15 C14 -163.34(19) . . . . ? P4 Cr2 C15 C14 -54.9(2) . . . . ? P2 Cr2 C15 C14 143.82(18) . . . . ? Cr1 Cr2 C15 C14 -120.5(2) . . . . ? C12 Cr2 C15 C11 -37.0(2) . . . . ? C14 Cr2 C15 C11 -116.7(3) . . . . ? C13 Cr2 C15 C11 -79.6(2) . . . . ? P3 Cr2 C15 C11 -100.6(3) . . . . ? P5 Cr2 C15 C11 135.7(2) . . . . ? P1 Cr2 C15 C11 79.9(2) . . . . ? P4 Cr2 C15 C11 -171.66(18) . . . . ? P2 Cr2 C15 C11 27.1(3) . . . . ? Cr1 Cr2 C15 C11 122.8(2) . . . . ? C12 Cr2 C15 C20 -159.2(4) . . . . ? C14 Cr2 C15 C20 121.1(4) . . . . ? C11 Cr2 C15 C20 -122.2(4) . . . . ? C13 Cr2 C15 C20 158.3(4) . . . . ? P3 Cr2 C15 C20 137.2(3) . . . . ? P5 Cr2 C15 C20 13.6(3) . . . . ? P1 Cr2 C15 C20 -42.2(3) . . . . ? P4 Cr2 C15 C20 66.2(3) . . . . ? P2 Cr2 C15 C20 -95.1(3) . . . . ? Cr1 Cr2 C15 C20 0.6(4) . . . . ? C25 C21 C22 C23 0.1(5) . . . . ? C26 C21 C22 C23 175.9(4) . . . . ? Cr3 C21 C22 C23 -61.4(3) . . . . ? C25 C21 C22 C27 -176.1(4) . . . . ? C26 C21 C22 C27 -0.3(7) . . . . ? Cr3 C21 C22 C27 122.4(4) . . . . ? C25 C21 C22 Cr3 61.5(3) . . . . ? C26 C21 C22 Cr3 -122.6(4) . . . . ? C21 C22 C23 C24 0.1(4) . . . . ? C27 C22 C23 C24 176.3(4) . . . . ? Cr3 C22 C23 C24 -61.7(3) . . . . ? C21 C22 C23 C28 -176.2(4) . . . . ? C27 C22 C23 C28 0.1(6) . . . . ? Cr3 C22 C23 C28 122.0(4) . . . . ? C21 C22 C23 Cr3 61.8(3) . . . . ? C27 C22 C23 Cr3 -122.0(4) . . . . ? C22 C23 C24 C25 -0.2(4) . . . . ? C28 C23 C24 C25 176.0(4) . . . . ? Cr3 C23 C24 C25 -62.3(3) . . . . ? C22 C23 C24 C29 -175.5(4) . . . . ? C28 C23 C24 C29 0.7(6) . . . . ? Cr3 C23 C24 C29 122.4(4) . . . . ? C22 C23 C24 Cr3 62.1(3) . . . . ? C28 C23 C24 Cr3 -121.7(4) . . . . ? C22 C21 C25 C24 -0.2(4) . . . . ? C26 C21 C25 C24 -176.1(4) . . . . ? Cr3 C21 C25 C24 61.4(3) . . . . ? C22 C21 C25 C30 176.3(4) . . . . ? C26 C21 C25 C30 0.3(6) . . . . ? Cr3 C21 C25 C30 -122.1(4) . . . . ? C22 C21 C25 Cr3 -61.6(3) . . . . ? C26 C21 C25 Cr3 122.4(4) . . . . ? C23 C24 C25 C21 0.2(4) . . . . ? C29 C24 C25 C21 175.4(4) . . . . ? Cr3 C24 C25 C21 -62.1(3) . . . . ? C23 C24 C25 C30 -176.2(4) . . . . ? C29 C24 C25 C30 -1.0(6) . . . . ? Cr3 C24 C25 C30 121.4(4) . . . . ? C23 C24 C25 Cr3 62.4(3) . . . . ? C29 C24 C25 Cr3 -122.5(4) . . . . ? C25 C24 Cr3 C23 116.9(3) . . . . ? C29 C24 Cr3 C23 -120.4(5) . . . . ? C23 C24 Cr3 C25 -116.9(3) . . . . ? C29 C24 Cr3 C25 122.6(4) . . . . ? C23 C24 Cr3 C22 -37.4(2) . . . . ? C25 C24 Cr3 C22 79.5(2) . . . . ? C29 C24 Cr3 C22 -157.9(4) . . . . ? C23 C24 Cr3 C21 -79.8(2) . . . . ? C25 C24 Cr3 C21 37.1(2) . . . . ? C29 C24 Cr3 C21 159.7(4) . . . . ? C23 C24 Cr3 P6 -137.2(2) . . . . ? C25 C24 Cr3 P6 -20.2(3) . . . . ? C29 C24 Cr3 P6 102.4(4) . . . . ? C23 C24 Cr3 P10 169.94(19) . . . . ? C25 C24 Cr3 P10 -73.1(2) . . . . ? C29 C24 Cr3 P10 49.5(4) . . . . ? C23 C24 Cr3 P8 64.9(2) . . . . ? C25 C24 Cr3 P8 -178.17(17) . . . . ? C29 C24 Cr3 P8 -55.5(4) . . . . ? C23 C24 Cr3 P9 116.7(2) . . . . ? C25 C24 Cr3 P9 -126.31(19) . . . . ? C29 C24 Cr3 P9 -3.7(4) . . . . ? C23 C24 Cr3 P7 8.1(4) . . . . ? C25 C24 Cr3 P7 125.1(3) . . . . ? C29 C24 Cr3 P7 -112.3(3) . . . . ? C22 C23 Cr3 C24 -117.6(3) . . . . ? C28 C23 Cr3 C24 121.5(4) . . . . ? C22 C23 Cr3 C25 -79.5(2) . . . . ? C24 C23 Cr3 C25 38.1(2) . . . . ? C28 C23 Cr3 C25 159.6(4) . . . . ? C24 C23 Cr3 C22 117.6(3) . . . . ? C28 C23 Cr3 C22 -121.0(4) . . . . ? C22 C23 Cr3 C21 -37.2(2) . . . . ? C24 C23 Cr3 C21 80.4(2) . . . . ? C28 C23 Cr3 C21 -158.1(4) . . . . ? C22 C23 Cr3 P6 5.2(4) . . . . ? C24 C23 Cr3 P6 122.8(3) . . . . ? C28 C23 Cr3 P6 -115.7(3) . . . . ? C22 C23 Cr3 P10 -135.4(2) . . . . ? C24 C23 Cr3 P10 -17.8(3) . . . . ? C28 C23 Cr3 P10 103.7(3) . . . . ? C22 C23 Cr3 P8 117.6(2) . . . . ? C24 C23 Cr3 P8 -124.8(2) . . . . ? C28 C23 Cr3 P8 -3.4(3) . . . . ? C22 C23 Cr3 P9 170.6(2) . . . . ? C24 C23 Cr3 P9 -71.8(2) . . . . ? C28 C23 Cr3 P9 49.6(3) . . . . ? C22 C23 Cr3 P7 66.3(2) . . . . ? C24 C23 Cr3 P7 -176.16(18) . . . . ? C28 C23 Cr3 P7 -54.7(4) . . . . ? C21 C25 Cr3 C24 117.8(3) . . . . ? C30 C25 Cr3 C24 -120.8(4) . . . . ? C21 C25 Cr3 C23 80.1(2) . . . . ? C24 C25 Cr3 C23 -37.8(2) . . . . ? C30 C25 Cr3 C23 -158.5(4) . . . . ? C21 C25 Cr3 C22 37.6(2) . . . . ? C24 C25 Cr3 C22 -80.3(2) . . . . ? C30 C25 Cr3 C22 158.9(4) . . . . ? C24 C25 Cr3 C21 -117.8(3) . . . . ? C30 C25 Cr3 C21 121.4(4) . . . . ? C21 C25 Cr3 P6 -73.3(2) . . . . ? C24 C25 Cr3 P6 168.90(18) . . . . ? C30 C25 Cr3 P6 48.1(3) . . . . ? C21 C25 Cr3 P10 -126.3(2) . . . . ? C24 C25 Cr3 P10 115.83(19) . . . . ? C30 C25 Cr3 P10 -5.0(3) . . . . ? C21 C25 Cr3 P8 121.6(2) . . . . ? C24 C25 Cr3 P8 3.8(4) . . . . ? C30 C25 Cr3 P8 -117.0(3) . . . . ? C21 C25 Cr3 P9 -178.71(19) . . . . ? C24 C25 Cr3 P9 63.4(2) . . . . ? C30 C25 Cr3 P9 -57.3(4) . . . . ? C21 C25 Cr3 P7 -19.5(3) . . . . ? C24 C25 Cr3 P7 -137.4(2) . . . . ? C30 C25 Cr3 P7 101.9(3) . . . . ? C23 C22 Cr3 C24 37.6(2) . . . . ? C21 C22 Cr3 C24 -80.6(2) . . . . ? C27 C22 Cr3 C24 157.4(4) . . . . ? C21 C22 Cr3 C23 -118.1(3) . . . . ? C27 C22 Cr3 C23 119.9(4) . . . . ? C23 C22 Cr3 C25 80.6(2) . . . . ? C21 C22 Cr3 C25 -37.5(2) . . . . ? C27 C22 Cr3 C25 -159.5(4) . . . . ? C23 C22 Cr3 C21 118.1(3) . . . . ? C27 C22 Cr3 C21 -122.0(4) . . . . ? C23 C22 Cr3 P6 -177.53(19) . . . . ? C21 C22 Cr3 P6 64.3(2) . . . . ? C27 C22 Cr3 P6 -57.6(4) . . . . ? C23 C22 Cr3 P10 120.1(3) . . . . ? C21 C22 Cr3 P10 2.0(4) . . . . ? C27 C22 Cr3 P10 -120.0(3) . . . . ? C23 C22 Cr3 P8 -71.3(2) . . . . ? C21 C22 Cr3 P8 170.57(19) . . . . ? C27 C22 Cr3 P8 48.6(4) . . . . ? C23 C22 Cr3 P9 -16.6(3) . . . . ? C21 C22 Cr3 P9 -134.7(2) . . . . ? C27 C22 Cr3 P9 103.3(3) . . . . ? C23 C22 Cr3 P7 -124.8(2) . . . . ? C21 C22 Cr3 P7 117.0(2) . . . . ? C27 C22 Cr3 P7 -4.9(3) . . . . ? C25 C21 Cr3 C24 -37.7(2) . . . . ? C22 C21 Cr3 C24 79.7(2) . . . . ? C26 C21 Cr3 C24 -157.7(4) . . . . ? C25 C21 Cr3 C23 -80.2(2) . . . . ? C22 C21 Cr3 C23 37.2(2) . . . . ? C26 C21 Cr3 C23 159.7(4) . . . . ? C22 C21 Cr3 C25 117.4(3) . . . . ? C26 C21 Cr3 C25 -120.0(4) . . . . ? C25 C21 Cr3 C22 -117.4(3) . . . . ? C26 C21 Cr3 C22 122.6(4) . . . . ? C25 C21 Cr3 P6 116.3(2) . . . . ? C22 C21 Cr3 P6 -126.3(2) . . . . ? C26 C21 Cr3 P6 -3.7(3) . . . . ? C25 C21 Cr3 P10 63.6(2) . . . . ? C22 C21 Cr3 P10 -179.04(19) . . . . ? C26 C21 Cr3 P10 -56.5(3) . . . . ? C25 C21 Cr3 P8 -134.3(2) . . . . ? C22 C21 Cr3 P8 -16.9(3) . . . . ? C26 C21 Cr3 P8 105.7(3) . . . . ? C25 C21 Cr3 P9 2.6(4) . . . . ? C22 C21 Cr3 P9 120.0(3) . . . . ? C26 C21 Cr3 P9 -117.4(3) . . . . ? C25 C21 Cr3 P7 169.41(19) . . . . ? C22 C21 Cr3 P7 -73.2(2) . . . . ? C26 C21 Cr3 P7 49.4(4) . . . . ? C24 Cr3 P6 P10 -68.15(19) . . . . ? C23 Cr3 P6 P10 -155.1(3) . . . . ? C25 Cr3 P6 P10 -81.47(11) . . . . ? C22 Cr3 P6 P10 -151.45(12) . . . . ? C21 Cr3 P6 P10 -117.64(11) . . . . ? P8 Cr3 P6 P10 92.04(5) . . . . ? P9 Cr3 P6 P10 38.63(4) . . . . ? P7 Cr3 P6 P10 129.19(5) . . . . ? C24 Cr3 P6 P7 162.66(19) . . . . ? C23 Cr3 P6 P7 75.7(3) . . . . ? C25 Cr3 P6 P7 149.34(11) . . . . ? C22 Cr3 P6 P7 79.36(12) . . . . ? C21 Cr3 P6 P7 113.17(11) . . . . ? P10 Cr3 P6 P7 -129.19(5) . . . . ? P8 Cr3 P6 P7 -37.15(4) . . . . ? P9 Cr3 P6 P7 -90.56(5) . . . . ? C24 Cr3 P6 Cr4 -132.66(19) . . . . ? C23 Cr3 P6 Cr4 140.4(3) . . . . ? C25 Cr3 P6 Cr4 -145.98(11) . . . . ? C22 Cr3 P6 Cr4 144.04(12) . . . . ? C21 Cr3 P6 Cr4 177.85(10) . . . . ? P10 Cr3 P6 Cr4 -64.51(4) . . . . ? P8 Cr3 P6 Cr4 27.53(4) . . . . ? P9 Cr3 P6 Cr4 -25.88(4) . . . . ? P7 Cr3 P6 Cr4 64.68(4) . . . . ? P10 P6 P7 P8 -1.65(8) . . . . ? Cr3 P6 P7 P8 45.08(5) . . . . ? Cr4 P6 P7 P8 -47.24(5) . . . . ? P10 P6 P7 Cr4 45.59(5) . . . . ? Cr3 P6 P7 Cr4 92.32(3) . . . . ? P10 P6 P7 Cr3 -46.73(5) . . . . ? Cr4 P6 P7 Cr3 -92.32(3) . . . . ? C24 Cr3 P7 P8 70.5(2) . . . . ? C23 Cr3 P7 P8 76.13(12) . . . . ? C25 Cr3 P7 P8 159.8(2) . . . . ? C22 Cr3 P7 P8 110.65(11) . . . . ? C21 Cr3 P7 P8 146.96(12) . . . . ? P6 Cr3 P7 P8 -131.06(5) . . . . ? P10 Cr3 P7 P8 -92.49(5) . . . . ? P9 Cr3 P7 P8 -38.80(4) . . . . ? C24 Cr3 P7 P6 -158.4(2) . . . . ? C23 Cr3 P7 P6 -152.81(12) . . . . ? C25 Cr3 P7 P6 -69.2(2) . . . . ? C22 Cr3 P7 P6 -118.30(11) . . . . ? C21 Cr3 P7 P6 -81.98(12) . . . . ? P10 Cr3 P7 P6 38.56(4) . . . . ? P8 Cr3 P7 P6 131.06(5) . . . . ? P9 Cr3 P7 P6 92.26(5) . . . . ? C24 Cr3 P7 Cr4 136.2(2) . . . . ? C23 Cr3 P7 Cr4 141.80(12) . . . . ? C25 Cr3 P7 Cr4 -134.6(2) . . . . ? C22 Cr3 P7 Cr4 176.31(11) . . . . ? C21 Cr3 P7 Cr4 -147.37(12) . . . . ? P6 Cr3 P7 Cr4 -65.39(4) . . . . ? P10 Cr3 P7 Cr4 -26.83(4) . . . . ? P8 Cr3 P7 Cr4 65.66(4) . . . . ? P9 Cr3 P7 Cr4 26.86(4) . . . . ? P6 P7 P8 P9 2.20(7) . . . . ? Cr4 P7 P8 P9 -44.92(5) . . . . ? Cr3 P7 P8 P9 47.16(5) . . . . ? P6 P7 P8 Cr3 -44.96(5) . . . . ? Cr4 P7 P8 Cr3 -92.08(4) . . . . ? P6 P7 P8 Cr4 47.12(5) . . . . ? Cr3 P7 P8 Cr4 92.08(4) . . . . ? C24 Cr3 P8 P7 -153.99(11) . . . . ? C23 Cr3 P8 P7 -119.98(11) . . . . ? C25 Cr3 P8 P7 -156.6(2) . . . . ? C22 Cr3 P8 P7 -84.29(12) . . . . ? C21 Cr3 P8 P7 -73.3(2) . . . . ? P6 Cr3 P8 P7 37.22(4) . . . . ? P10 Cr3 P8 P7 90.78(5) . . . . ? P9 Cr3 P8 P7 128.68(5) . . . . ? C24 Cr3 P8 P9 77.33(11) . . . . ? C23 Cr3 P8 P9 111.34(11) . . . . ? C25 Cr3 P8 P9 74.8(2) . . . . ? C22 Cr3 P8 P9 147.03(12) . . . . ? C21 Cr3 P8 P9 158.1(2) . . . . ? P6 Cr3 P8 P9 -91.46(5) . . . . ? P10 Cr3 P8 P9 -37.90(4) . . . . ? P7 Cr3 P8 P9 -128.68(5) . . . . ? C24 Cr3 P8 Cr4 141.32(11) . . . . ? C23 Cr3 P8 Cr4 175.33(10) . . . . ? C25 Cr3 P8 Cr4 138.7(2) . . . . ? C22 Cr3 P8 Cr4 -148.98(11) . . . . ? C21 Cr3 P8 Cr4 -137.9(2) . . . . ? P6 Cr3 P8 Cr4 -27.47(4) . . . . ? P10 Cr3 P8 Cr4 26.09(4) . . . . ? P9 Cr3 P8 Cr4 63.99(4) . . . . ? P7 Cr3 P8 Cr4 -64.69(4) . . . . ? P7 P8 P9 P10 -1.91(7) . . . . ? Cr3 P8 P9 P10 45.48(5) . . . . ? Cr4 P8 P9 P10 -47.14(5) . . . . ? P7 P8 P9 Cr4 45.23(5) . . . . ? Cr3 P8 P9 Cr4 92.62(3) . . . . ? P7 P8 P9 Cr3 -47.39(5) . . . . ? Cr4 P8 P9 Cr3 -92.62(3) . . . . ? C24 Cr3 P9 P8 -117.92(11) . . . . ? C23 Cr3 P9 P8 -82.01(11) . . . . ? C25 Cr3 P9 P8 -151.71(12) . . . . ? C22 Cr3 P9 P8 -71.2(2) . . . . ? C21 Cr3 P9 P8 -153.5(2) . . . . ? P6 Cr3 P9 P8 91.91(5) . . . . ? P10 Cr3 P9 P8 130.43(5) . . . . ? P7 Cr3 P9 P8 38.65(5) . . . . ? C24 Cr3 P9 P10 111.66(11) . . . . ? C23 Cr3 P9 P10 147.57(11) . . . . ? C25 Cr3 P9 P10 77.86(12) . . . . ? C22 Cr3 P9 P10 158.4(2) . . . . ? C21 Cr3 P9 P10 76.1(3) . . . . ? P6 Cr3 P9 P10 -38.51(5) . . . . ? P8 Cr3 P9 P10 -130.43(5) . . . . ? P7 Cr3 P9 P10 -91.77(5) . . . . ? C24 Cr3 P9 Cr4 176.39(11) . . . . ? C23 Cr3 P9 Cr4 -147.70(11) . . . . ? C25 Cr3 P9 Cr4 142.59(11) . . . . ? C22 Cr3 P9 Cr4 -136.9(2) . . . . ? C21 Cr3 P9 Cr4 140.8(2) . . . . ? P6 Cr3 P9 Cr4 26.22(4) . . . . ? P10 Cr3 P9 Cr4 64.73(4) . . . . ? P8 Cr3 P9 Cr4 -65.70(4) . . . . ? P7 Cr3 P9 Cr4 -27.04(4) . . . . ? P7 P6 P10 P9 0.46(7) . . . . ? Cr3 P6 P10 P9 -46.63(5) . . . . ? Cr4 P6 P10 P9 46.12(5) . . . . ? P7 P6 P10 Cr3 47.09(5) . . . . ? Cr4 P6 P10 Cr3 92.75(4) . . . . ? P7 P6 P10 Cr4 -45.65(5) . . . . ? Cr3 P6 P10 Cr4 -92.75(4) . . . . ? P8 P9 P10 P6 0.90(7) . . . . ? Cr4 P9 P10 P6 -46.70(5) . . . . ? Cr3 P9 P10 P6 46.54(5) . . . . ? P8 P9 P10 Cr3 -45.64(5) . . . . ? Cr4 P9 P10 Cr3 -93.23(3) . . . . ? P8 P9 P10 Cr4 47.59(5) . . . . ? Cr3 P9 P10 Cr4 93.23(3) . . . . ? C24 Cr3 P10 P6 149.12(12) . . . . ? C23 Cr3 P10 P6 160.7(2) . . . . ? C25 Cr3 P10 P6 112.55(11) . . . . ? C22 Cr3 P10 P6 77.8(2) . . . . ? C21 Cr3 P10 P6 79.15(12) . . . . ? P8 Cr3 P10 P6 -91.57(5) . . . . ? P9 Cr3 P10 P6 -129.29(5) . . . . ? P7 Cr3 P10 P6 -38.42(4) . . . . ? C24 Cr3 P10 P9 -81.59(12) . . . . ? C23 Cr3 P10 P9 -70.0(2) . . . . ? C25 Cr3 P10 P9 -118.16(11) . . . . ? C22 Cr3 P10 P9 -152.9(2) . . . . ? C21 Cr3 P10 P9 -151.56(12) . . . . ? P6 Cr3 P10 P9 129.29(5) . . . . ? P8 Cr3 P10 P9 37.72(4) . . . . ? P7 Cr3 P10 P9 90.87(5) . . . . ? C24 Cr3 P10 Cr4 -145.62(11) . . . . ? C23 Cr3 P10 Cr4 -134.0(2) . . . . ? C25 Cr3 P10 Cr4 177.81(10) . . . . ? C22 Cr3 P10 Cr4 143.0(2) . . . . ? C21 Cr3 P10 Cr4 144.41(11) . . . . ? P6 Cr3 P10 Cr4 65.26(4) . . . . ? P8 Cr3 P10 Cr4 -26.32(4) . . . . ? P9 Cr3 P10 Cr4 -64.03(4) . . . . ? P7 Cr3 P10 Cr4 26.84(4) . . . . ? P8 P9 Cr4 C31 163.27(16) . . . . ? P10 P9 Cr4 C31 -67.92(16) . . . . ? Cr3 P9 Cr4 C31 -132.12(16) . . . . ? P8 P9 Cr4 C32 88.3(3) . . . . ? P10 P9 Cr4 C32 -142.8(3) . . . . ? Cr3 P9 Cr4 C32 153.0(3) . . . . ? P8 P9 Cr4 C33 75.53(12) . . . . ? P10 P9 Cr4 C33 -155.66(12) . . . . ? Cr3 P9 Cr4 C33 140.13(12) . . . . ? P8 P9 Cr4 C35 143.77(11) . . . . ? P10 P9 Cr4 C35 -87.42(11) . . . . ? Cr3 P9 Cr4 C35 -151.62(10) . . . . ? P8 P9 Cr4 C34 105.85(11) . . . . ? P10 P9 Cr4 C34 -125.34(11) . . . . ? Cr3 P9 Cr4 C34 170.45(11) . . . . ? P8 P9 Cr4 P10 -128.81(5) . . . . ? Cr3 P9 Cr4 P10 -64.20(4) . . . . ? P8 P9 Cr4 P7 -37.36(4) . . . . ? P10 P9 Cr4 P7 91.45(4) . . . . ? Cr3 P9 Cr4 P7 27.25(4) . . . . ? P8 P9 Cr4 P6 -90.58(5) . . . . ? P10 P9 Cr4 P6 38.23(4) . . . . ? Cr3 P9 Cr4 P6 -25.97(4) . . . . ? P10 P9 Cr4 P8 128.81(5) . . . . ? Cr3 P9 Cr4 P8 64.61(4) . . . . ? P6 P10 Cr4 C31 -88.14(11) . . . . ? P9 P10 Cr4 C31 142.41(11) . . . . ? Cr3 P10 Cr4 C31 -152.80(11) . . . . ? P6 P10 Cr4 C32 -68.83(16) . . . . ? P9 P10 Cr4 C32 161.72(16) . . . . ? Cr3 P10 Cr4 C32 -133.49(15) . . . . ? P6 P10 Cr4 C33 -141.3(3) . . . . ? P9 P10 Cr4 C33 89.2(3) . . . . ? Cr3 P10 Cr4 C33 154.0(3) . . . . ? P6 P10 Cr4 C35 -125.90(11) . . . . ? P9 P10 Cr4 C35 104.65(11) . . . . ? Cr3 P10 Cr4 C35 169.44(11) . . . . ? P6 P10 Cr4 C34 -155.80(13) . . . . ? P9 P10 Cr4 C34 74.75(13) . . . . ? Cr3 P10 Cr4 C34 139.55(13) . . . . ? P6 P10 Cr4 P9 129.45(5) . . . . ? Cr3 P10 Cr4 P9 64.79(4) . . . . ? P6 P10 Cr4 P7 37.63(5) . . . . ? P9 P10 Cr4 P7 -91.82(5) . . . . ? Cr3 P10 Cr4 P7 -27.03(4) . . . . ? P9 P10 Cr4 P6 -129.45(5) . . . . ? Cr3 P10 Cr4 P6 -64.66(4) . . . . ? P6 P10 Cr4 P8 90.71(5) . . . . ? P9 P10 Cr4 P8 -38.74(4) . . . . ? Cr3 P10 Cr4 P8 26.05(4) . . . . ? P8 P7 Cr4 C31 -157.98(13) . . . . ? P6 P7 Cr4 C31 72.89(13) . . . . ? Cr3 P7 Cr4 C31 137.32(12) . . . . ? P8 P7 Cr4 C32 -126.69(11) . . . . ? P6 P7 Cr4 C32 104.18(11) . . . . ? Cr3 P7 Cr4 C32 168.61(10) . . . . ? P8 P7 Cr4 C33 -88.88(11) . . . . ? P6 P7 Cr4 C33 141.99(11) . . . . ? Cr3 P7 Cr4 C33 -153.58(11) . . . . ? P8 P7 Cr4 C35 -145.7(3) . . . . ? P6 P7 Cr4 C35 85.2(3) . . . . ? Cr3 P7 Cr4 C35 149.6(3) . . . . ? P8 P7 Cr4 C34 -70.34(17) . . . . ? P6 P7 Cr4 C34 160.54(17) . . . . ? Cr3 P7 Cr4 C34 -135.03(17) . . . . ? P8 P7 Cr4 P9 37.54(5) . . . . ? P6 P7 Cr4 P9 -91.58(5) . . . . ? Cr3 P7 Cr4 P9 -27.15(4) . . . . ? P8 P7 Cr4 P10 91.49(5) . . . . ? P6 P7 Cr4 P10 -37.64(5) . . . . ? Cr3 P7 Cr4 P10 26.79(4) . . . . ? P8 P7 Cr4 P6 129.13(5) . . . . ? Cr3 P7 Cr4 P6 64.43(4) . . . . ? P6 P7 Cr4 P8 -129.13(5) . . . . ? Cr3 P7 Cr4 P8 -64.70(4) . . . . ? P10 P6 Cr4 C31 103.36(11) . . . . ? P7 P6 Cr4 C31 -126.29(11) . . . . ? Cr3 P6 Cr4 C31 168.15(11) . . . . ? P10 P6 Cr4 C32 141.72(11) . . . . ? P7 P6 Cr4 C32 -87.93(11) . . . . ? Cr3 P6 Cr4 C32 -153.49(11) . . . . ? P10 P6 Cr4 C33 159.98(17) . . . . ? P7 P6 Cr4 C33 -69.68(17) . . . . ? Cr3 P6 Cr4 C33 -135.24(16) . . . . ? P10 P6 Cr4 C35 73.04(12) . . . . ? P7 P6 Cr4 C35 -156.61(12) . . . . ? Cr3 P6 Cr4 C35 137.82(12) . . . . ? P10 P6 Cr4 C34 86.8(3) . . . . ? P7 P6 Cr4 C34 -142.8(3) . . . . ? Cr3 P6 Cr4 C34 151.6(3) . . . . ? P10 P6 Cr4 P9 -38.65(4) . . . . ? P7 P6 Cr4 P9 91.70(5) . . . . ? Cr3 P6 Cr4 P9 26.14(4) . . . . ? P7 P6 Cr4 P10 130.35(6) . . . . ? Cr3 P6 Cr4 P10 64.79(4) . . . . ? P10 P6 Cr4 P7 -130.35(6) . . . . ? Cr3 P6 Cr4 P7 -65.56(4) . . . . ? P10 P6 Cr4 P8 -92.03(5) . . . . ? P7 P6 Cr4 P8 38.32(4) . . . . ? Cr3 P6 Cr4 P8 -27.24(4) . . . . ? P7 P8 Cr4 C31 84.9(3) . . . . ? P9 P8 Cr4 C31 -144.5(3) . . . . ? Cr3 P8 Cr4 C31 150.4(3) . . . . ? P7 P8 Cr4 C32 72.83(12) . . . . ? P9 P8 Cr4 C32 -156.51(12) . . . . ? Cr3 P8 Cr4 C32 138.40(12) . . . . ? P7 P8 Cr4 C33 104.36(10) . . . . ? P9 P8 Cr4 C33 -124.98(10) . . . . ? Cr3 P8 Cr4 C33 169.94(10) . . . . ? P7 P8 Cr4 C35 162.18(16) . . . . ? P9 P8 Cr4 C35 -67.16(17) . . . . ? Cr3 P8 Cr4 C35 -132.25(16) . . . . ? P7 P8 Cr4 C34 142.02(11) . . . . ? P9 P8 Cr4 C34 -87.32(11) . . . . ? Cr3 P8 Cr4 C34 -152.40(11) . . . . ? P7 P8 Cr4 P9 -130.66(5) . . . . ? Cr3 P8 Cr4 P9 -65.08(4) . . . . ? P7 P8 Cr4 P10 -91.60(5) . . . . ? P9 P8 Cr4 P10 39.06(4) . . . . ? Cr3 P8 Cr4 P10 -26.02(4) . . . . ? P9 P8 Cr4 P7 130.66(5) . . . . ? Cr3 P8 Cr4 P7 65.58(4) . . . . ? P7 P8 Cr4 P6 -38.40(4) . . . . ? P9 P8 Cr4 P6 92.26(5) . . . . ? Cr3 P8 Cr4 P6 27.18(4) . . . . ? C32 Cr4 C31 C35 117.4(3) . . . . ? C33 Cr4 C31 C35 79.7(2) . . . . ? C34 Cr4 C31 C35 37.5(2) . . . . ? P9 Cr4 C31 C35 -31.6(3) . . . . ? P10 Cr4 C31 C35 -82.4(2) . . . . ? P7 Cr4 C31 C35 173.33(17) . . . . ? P6 Cr4 C31 C35 -136.2(2) . . . . ? P8 Cr4 C31 C35 101.3(4) . . . . ? C33 Cr4 C31 C32 -37.8(2) . . . . ? C35 Cr4 C31 C32 -117.4(3) . . . . ? C34 Cr4 C31 C32 -79.9(2) . . . . ? P9 Cr4 C31 C32 -149.00(17) . . . . ? P10 Cr4 C31 C32 160.14(18) . . . . ? P7 Cr4 C31 C32 55.9(2) . . . . ? P6 Cr4 C31 C32 106.36(19) . . . . ? P8 Cr4 C31 C32 -16.2(5) . . . . ? C32 Cr4 C31 C36 -120.9(4) . . . . ? C33 Cr4 C31 C36 -158.7(4) . . . . ? C35 Cr4 C31 C36 121.6(4) . . . . ? C34 Cr4 C31 C36 159.1(4) . . . . ? P9 Cr4 C31 C36 90.1(3) . . . . ? P10 Cr4 C31 C36 39.2(3) . . . . ? P7 Cr4 C31 C36 -65.1(4) . . . . ? P6 Cr4 C31 C36 -14.6(3) . . . . ? P8 Cr4 C31 C36 -137.1(3) . . . . ? C35 C31 C32 C33 -0.4(4) . . . . ? C36 C31 C32 C33 -177.9(4) . . . . ? Cr4 C31 C32 C33 62.4(3) . . . . ? C35 C31 C32 C37 177.1(3) . . . . ? C36 C31 C32 C37 -0.4(6) . . . . ? Cr4 C31 C32 C37 -120.2(4) . . . . ? C35 C31 C32 Cr4 -62.7(3) . . . . ? C36 C31 C32 Cr4 119.7(4) . . . . ? C31 Cr4 C32 C33 -116.8(3) . . . . ? C35 Cr4 C32 C33 -79.5(2) . . . . ? C34 Cr4 C32 C33 -37.0(2) . . . . ? P9 Cr4 C32 C33 -17.5(5) . . . . ? P10 Cr4 C32 C33 -147.72(18) . . . . ? P7 Cr4 C32 C33 107.5(2) . . . . ? P6 Cr4 C32 C33 161.33(19) . . . . ? P8 Cr4 C32 C33 57.1(2) . . . . ? C33 Cr4 C32 C31 116.8(3) . . . . ? C35 Cr4 C32 C31 37.3(2) . . . . ? C34 Cr4 C32 C31 79.8(2) . . . . ? P9 Cr4 C32 C31 99.3(4) . . . . ? P10 Cr4 C32 C31 -30.9(3) . . . . ? P7 Cr4 C32 C31 -135.67(19) . . . . ? P6 Cr4 C32 C31 -81.8(2) . . . . ? P8 Cr4 C32 C31 173.94(17) . . . . ? C31 Cr4 C32 C37 120.7(4) . . . . ? C33 Cr4 C32 C37 -122.5(4) . . . . ? C35 Cr4 C32 C37 158.0(4) . . . . ? C34 Cr4 C32 C37 -159.5(4) . . . . ? P9 Cr4 C32 C37 -140.0(3) . . . . ? P10 Cr4 C32 C37 89.8(3) . . . . ? P7 Cr4 C32 C37 -15.0(3) . . . . ? P6 Cr4 C32 C37 38.8(3) . . . . ? P8 Cr4 C32 C37 -65.4(3) . . . . ? C31 C32 C33 C34 0.1(4) . . . . ? C37 C32 C33 C34 -177.3(4) . . . . ? Cr4 C32 C33 C34 61.8(3) . . . . ? C31 C32 C33 C38 177.6(4) . . . . ? C37 C32 C33 C38 0.2(6) . . . . ? Cr4 C32 C33 C38 -120.7(4) . . . . ? C31 C32 C33 Cr4 -61.8(3) . . . . ? C37 C32 C33 Cr4 120.8(4) . . . . ? C31 Cr4 C33 C34 -79.7(2) . . . . ? C32 Cr4 C33 C34 -118.0(3) . . . . ? C35 Cr4 C33 C34 -37.3(2) . . . . ? P9 Cr4 C33 C34 55.1(2) . . . . ? P10 Cr4 C33 C34 -20.1(4) . . . . ? P7 Cr4 C33 C34 161.0(2) . . . . ? P6 Cr4 C33 C34 -147.32(19) . . . . ? P8 Cr4 C33 C34 107.0(2) . . . . ? C31 Cr4 C33 C32 38.3(2) . . . . ? C35 Cr4 C33 C32 80.7(2) . . . . ? C34 Cr4 C33 C32 118.0(3) . . . . ? P9 Cr4 C33 C32 173.13(18) . . . . ? P10 Cr4 C33 C32 97.9(3) . . . . ? P7 Cr4 C33 C32 -81.0(2) . . . . ? P6 Cr4 C33 C32 -29.3(3) . . . . ? P8 Cr4 C33 C32 -135.0(2) . . . . ? C31 Cr4 C33 C38 160.7(4) . . . . ? C32 Cr4 C33 C38 122.4(4) . . . . ? C35 Cr4 C33 C38 -156.9(4) . . . . ? C34 Cr4 C33 C38 -119.6(4) . . . . ? P9 Cr4 C33 C38 -64.5(3) . . . . ? P10 Cr4 C33 C38 -139.7(3) . . . . ? P7 Cr4 C33 C38 41.4(3) . . . . ? P6 Cr4 C33 C38 93.1(3) . . . . ? P8 Cr4 C33 C38 -12.6(3) . . . . ? C32 C33 C34 C35 0.3(4) . . . . ? C38 C33 C34 C35 -177.3(4) . . . . ? Cr4 C33 C34 C35 61.6(3) . . . . ? C32 C33 C34 C39 176.4(4) . . . . ? C38 C33 C34 C39 -1.2(6) . . . . ? Cr4 C33 C34 C39 -122.2(4) . . . . ? C32 C33 C34 Cr4 -61.3(3) . . . . ? C38 C33 C34 Cr4 121.1(4) . . . . ? C31 Cr4 C34 C33 80.7(2) . . . . ? C32 Cr4 C34 C33 37.4(2) . . . . ? C35 Cr4 C34 C33 118.2(3) . . . . ? P9 Cr4 C34 C33 -136.2(2) . . . . ? P10 Cr4 C34 C33 171.88(18) . . . . ? P7 Cr4 C34 C33 -30.0(3) . . . . ? P6 Cr4 C34 C33 99.1(3) . . . . ? P8 Cr4 C34 C33 -82.1(2) . . . . ? C31 Cr4 C34 C35 -37.5(2) . . . . ? C32 Cr4 C34 C35 -80.7(2) . . . . ? C33 Cr4 C34 C35 -118.2(3) . . . . ? P9 Cr4 C34 C35 105.7(2) . . . . ? P10 Cr4 C34 C35 53.7(2) . . . . ? P7 Cr4 C34 C35 -148.13(19) . . . . ? P6 Cr4 C34 C35 -19.0(4) . . . . ? P8 Cr4 C34 C35 159.75(19) . . . . ? C31 Cr4 C34 C39 -158.2(4) . . . . ? C32 Cr4 C34 C39 158.5(4) . . . . ? C33 Cr4 C34 C39 121.1(4) . . . . ? C35 Cr4 C34 C39 -120.7(4) . . . . ? P9 Cr4 C34 C39 -15.0(3) . . . . ? P10 Cr4 C34 C39 -67.0(4) . . . . ? P7 Cr4 C34 C39 91.1(3) . . . . ? P6 Cr4 C34 C39 -139.8(3) . . . . ? P8 Cr4 C34 C39 39.0(3) . . . . ? C32 C31 C35 C34 0.5(4) . . . . ? C36 C31 C35 C34 178.0(4) . . . . ? Cr4 C31 C35 C34 -61.6(3) . . . . ? C32 C31 C35 C40 -177.3(4) . . . . ? C36 C31 C35 C40 0.2(6) . . . . ? Cr4 C31 C35 C40 120.5(4) . . . . ? C32 C31 C35 Cr4 62.2(3) . . . . ? C36 C31 C35 Cr4 -120.3(4) . . . . ? C33 C34 C35 C31 -0.5(4) . . . . ? C39 C34 C35 C31 -176.7(4) . . . . ? Cr4 C34 C35 C31 61.1(3) . . . . ? C33 C34 C35 C40 177.4(4) . . . . ? C39 C34 C35 C40 1.2(6) . . . . ? Cr4 C34 C35 C40 -121.1(4) . . . . ? C33 C34 C35 Cr4 -61.6(3) . . . . ? C39 C34 C35 Cr4 122.2(4) . . . . ? C32 Cr4 C35 C31 -38.0(2) . . . . ? C33 Cr4 C35 C31 -80.6(2) . . . . ? C34 Cr4 C35 C31 -117.5(3) . . . . ? P9 Cr4 C35 C31 159.75(19) . . . . ? P10 Cr4 C35 C31 105.3(2) . . . . ? P7 Cr4 C35 C31 -16.9(4) . . . . ? P6 Cr4 C35 C31 54.8(2) . . . . ? P8 Cr4 C35 C31 -149.93(19) . . . . ? C31 Cr4 C35 C34 117.5(3) . . . . ? C32 Cr4 C35 C34 79.6(2) . . . . ? C33 Cr4 C35 C34 37.0(2) . . . . ? P9 Cr4 C35 C34 -82.7(2) . . . . ? P10 Cr4 C35 C34 -137.1(2) . . . . ? P7 Cr4 C35 C34 100.7(3) . . . . ? P6 Cr4 C35 C34 172.33(18) . . . . ? P8 Cr4 C35 C34 -32.4(3) . . . . ? C31 Cr4 C35 C40 -121.1(4) . . . . ? C32 Cr4 C35 C40 -159.1(4) . . . . ? C33 Cr4 C35 C40 158.3(4) . . . . ? C34 Cr4 C35 C40 121.3(4) . . . . ? P9 Cr4 C35 C40 38.6(3) . . . . ? P10 Cr4 C35 C40 -15.8(3) . . . . ? P7 Cr4 C35 C40 -138.0(3) . . . . ? P6 Cr4 C35 C40 -66.3(4) . . . . ? P8 Cr4 C35 C40 89.0(3) . . . . ? _diffrn_measured_fraction_theta_max 0.912 _diffrn_reflns_theta_full 30.54 _diffrn_measured_fraction_theta_full 0.912 _refine_diff_density_max 3.699 _refine_diff_density_min -2.608 _refine_diff_density_rms 0.195 #===END data_050k _database_code_depnum_ccdc_archive 'CCDC 618759' _audit_creation_method SHELXL-97 _chemical_name_systematic ; \m~2~-\h^5^,\h^5^-cyclopentaphosphole)-bis ((\h^5^-pentamethyl-cyclopentadienyl)-chromium) hexafluoroantimonate ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H30 Cr2 F6 P5 Sb' _chemical_formula_weight 765.04 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M 'I 2/a' loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' _cell_length_a 22.9096(11) _cell_length_b 21.2711(10) _cell_length_c 22.8969(12) _cell_angle_alpha 90.00 _cell_angle_beta 101.206(2) _cell_angle_gamma 90.00 _cell_volume 10945.2(9) _cell_formula_units_Z 16 _cell_measurement_temperature 50(2) _cell_measurement_reflns_used 7945 _cell_measurement_theta_min 2.094 _cell_measurement_theta_max 30.491 _exptl_crystal_description 'irregular block' _exptl_crystal_colour 'dark green' _exptl_crystal_size_max 0.60 _exptl_crystal_size_mid 0.52 _exptl_crystal_size_min 0.40 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.857 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 6048 _exptl_absorpt_coefficient_mu 2.103 _exptl_absorpt_correction_type integration _exptl_absorpt_correction_T_min 0.397 _exptl_absorpt_correction_T_max 0.599 _exptl_absorpt_process_details 'XPREP in SHELXTL' _exptl_special_details ; ? ; _diffrn_ambient_temperature 50(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'Bede Microsource X-ray Generator' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEX CCD Diffractometer' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number 0 _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% 0 _diffrn_reflns_number 38702 _diffrn_reflns_av_R_equivalents 0.0394 _diffrn_reflns_av_sigmaI/netI 0.0491 _diffrn_reflns_limit_h_min -32 _diffrn_reflns_limit_h_max 32 _diffrn_reflns_limit_k_min -30 _diffrn_reflns_limit_k_max 27 _diffrn_reflns_limit_l_min -31 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_theta_min 1.15 _diffrn_reflns_theta_max 30.57 _reflns_number_total 15276 _reflns_number_gt 14294 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'SMART V5.625 (Bruker, 2003)' _computing_cell_refinement 'SMART V5.625 (Bruker, 2003)' _computing_data_reduction 'SAINT V6.28A (Bruker, 2003)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'SHELXTL V6.12(Bruker, 2001)' _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0792P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 15276 _refine_ls_number_parameters 614 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0439 _refine_ls_R_factor_gt 0.0403 _refine_ls_wR_factor_ref 0.1122 _refine_ls_wR_factor_gt 0.1077 _refine_ls_goodness_of_fit_ref 1.053 _refine_ls_restrained_S_all 1.053 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb1 Sb 0.138891(11) 0.869062(11) 0.384012(12) 0.01403(6) Uani 1 1 d . . . F1 F 0.09757(12) 0.80834(12) 0.33217(12) 0.0258(5) Uani 1 1 d . . . F2 F 0.09079(13) 0.93166(12) 0.34138(12) 0.0268(5) Uani 1 1 d . . . F3 F 0.08361(12) 0.86066(13) 0.43462(12) 0.0236(5) Uani 1 1 d . . . F4 F 0.18508(11) 0.80562(11) 0.42710(12) 0.0209(5) Uani 1 1 d . . . F5 F 0.19482(13) 0.87703(11) 0.33444(12) 0.0239(6) Uani 1 1 d . . . F6 F 0.18026(12) 0.93057(11) 0.43417(11) 0.0228(5) Uani 1 1 d . . . Sb2 Sb 0.136506(12) 0.127045(11) 0.117175(12) 0.01309(6) Uani 1 1 d . . . F7 F 0.12368(15) 0.05091(13) 0.15271(14) 0.0360(7) Uani 1 1 d . . . F8 F 0.07171(12) 0.16376(14) 0.14359(13) 0.0282(6) Uani 1 1 d . . . F9 F 0.08563(12) 0.10124(13) 0.04720(11) 0.0251(5) Uani 1 1 d . . . F10 F 0.20194(12) 0.09288(13) 0.08955(12) 0.0281(6) Uani 1 1 d . . . F11 F 0.18718(12) 0.15238(13) 0.18745(11) 0.0244(5) Uani 1 1 d . . . F12 F 0.15018(12) 0.20364(12) 0.08152(13) 0.0266(6) Uani 1 1 d . . . C1 C -0.11308(16) 0.31080(16) 0.44741(17) 0.0131(6) Uani 1 1 d . . . C2 C -0.14193(16) 0.26799(16) 0.40253(17) 0.0130(6) Uani 1 1 d . . . C3 C -0.14119(15) 0.29555(16) 0.34609(17) 0.0133(6) Uani 1 1 d . . . C4 C -0.11185(16) 0.35566(16) 0.35520(17) 0.0124(6) Uani 1 1 d . . . C5 C -0.09462(16) 0.36479(16) 0.41783(17) 0.0127(6) Uani 1 1 d . . . C6 C -0.10578(18) 0.30297(19) 0.51277(17) 0.0178(7) Uani 1 1 d . . . H6A H -0.1385 0.3242 0.5267 0.027 Uiso 1 1 calc R . . H6B H -0.0678 0.3215 0.5324 0.027 Uiso 1 1 calc R . . H6C H -0.1062 0.2581 0.5224 0.027 Uiso 1 1 calc R . . C7 C -0.17067(17) 0.20746(17) 0.41446(19) 0.0175(7) Uani 1 1 d . . . H7A H -0.2127 0.2149 0.4153 0.026 Uiso 1 1 calc R . . H7B H -0.1506 0.1906 0.4530 0.026 Uiso 1 1 calc R . . H7C H -0.1676 0.1772 0.3829 0.026 Uiso 1 1 calc R . . C8 C -0.16838(16) 0.26906(18) 0.28643(17) 0.0158(7) Uani 1 1 d . . . H8A H -0.2047 0.2925 0.2698 0.024 Uiso 1 1 calc R . . H8B H -0.1783 0.2247 0.2908 0.024 Uiso 1 1 calc R . . H8C H -0.1400 0.2727 0.2596 0.024 Uiso 1 1 calc R . . C9 C -0.10399(17) 0.40136(18) 0.30822(17) 0.0167(7) Uani 1 1 d . . . H9A H -0.1411 0.4247 0.2951 0.025 Uiso 1 1 calc R . . H9B H -0.0937 0.3787 0.2743 0.025 Uiso 1 1 calc R . . H9C H -0.0720 0.4308 0.3243 0.025 Uiso 1 1 calc R . . C10 C -0.06701(17) 0.42283(17) 0.44883(17) 0.0155(7) Uani 1 1 d . . . H10A H -0.0968 0.4455 0.4661 0.023 Uiso 1 1 calc R . . H10B H -0.0526 0.4500 0.4201 0.023 Uiso 1 1 calc R . . H10C H -0.0336 0.4109 0.4805 0.023 Uiso 1 1 calc R . . Cr1 Cr -0.04874(3) 0.27986(3) 0.39234(3) 0.01026(11) Uani 1 1 d . . . P1 P 0.03490(5) 0.26910(6) 0.47163(5) 0.0229(2) Uani 1 1 d . . . P2 P -0.01384(5) 0.18229(5) 0.43729(6) 0.0222(2) Uani 1 1 d . . . P3 P -0.03320(4) 0.18745(5) 0.33891(5) 0.0208(2) Uani 1 1 d . . . P4 P 0.00292(5) 0.27757(5) 0.31159(5) 0.0211(2) Uani 1 1 d . . . P5 P 0.04498(5) 0.32796(5) 0.39378(6) 0.0223(2) Uani 1 1 d . . . Cr2 Cr 0.06321(3) 0.21826(3) 0.38888(3) 0.01031(11) Uani 1 1 d . . . C11 C 0.14640(16) 0.17706(16) 0.44015(16) 0.0121(6) Uani 1 1 d . . . C12 C 0.11586(17) 0.13023(16) 0.40119(18) 0.0141(7) Uani 1 1 d . . . C13 C 0.11249(16) 0.15196(17) 0.34115(17) 0.0134(6) Uani 1 1 d . . . C14 C 0.14040(16) 0.21196(17) 0.34386(17) 0.0133(6) Uani 1 1 d . . . C15 C 0.16150(16) 0.22807(16) 0.40481(17) 0.0130(6) Uani 1 1 d . . . C16 C 0.16309(17) 0.17084(18) 0.50610(17) 0.0168(7) Uani 1 1 d . . . H16A H 0.2003 0.1471 0.5166 0.025 Uiso 1 1 calc R . . H16B H 0.1314 0.1486 0.5210 0.025 Uiso 1 1 calc R . . H16C H 0.1685 0.2127 0.5242 0.025 Uiso 1 1 calc R . . C17 C 0.09521(18) 0.06762(17) 0.41880(19) 0.0188(7) Uani 1 1 d . . . H17A H 0.1285 0.0379 0.4247 0.028 Uiso 1 1 calc R . . H17B H 0.0633 0.0520 0.3873 0.028 Uiso 1 1 calc R . . H17C H 0.0803 0.0719 0.4559 0.028 Uiso 1 1 calc R . . C18 C 0.08827(18) 0.11567(18) 0.28600(19) 0.0194(8) Uani 1 1 d . . . H18A H 0.1202 0.0909 0.2744 0.029 Uiso 1 1 calc R . . H18B H 0.0719 0.1448 0.2538 0.029 Uiso 1 1 calc R . . H18C H 0.0567 0.0875 0.2936 0.029 Uiso 1 1 calc R . . C19 C 0.14909(17) 0.25080(18) 0.29126(18) 0.0175(7) Uani 1 1 d . . . H19A H 0.1900 0.2459 0.2852 0.026 Uiso 1 1 calc R . . H19B H 0.1416 0.2952 0.2987 0.026 Uiso 1 1 calc R . . H19C H 0.1213 0.2367 0.2556 0.026 Uiso 1 1 calc R . . C20 C 0.19585(16) 0.28597(17) 0.42693(18) 0.0162(7) Uani 1 1 d . . . H20A H 0.2378 0.2800 0.4248 0.024 Uiso 1 1 calc R . . H20B H 0.1924 0.2939 0.4683 0.024 Uiso 1 1 calc R . . H20C H 0.1798 0.3219 0.4022 0.024 Uiso 1 1 calc R . . C21 C 0.10744(18) 0.38458(17) 0.13242(18) 0.0147(7) Uani 1 1 d . . . C22 C 0.17101(18) 0.38151(16) 0.14511(19) 0.0151(7) Uani 1 1 d . . . C23 C 0.19375(16) 0.43750(17) 0.12353(17) 0.0148(7) Uani 1 1 d . . . C24 C 0.14451(18) 0.47596(17) 0.09743(17) 0.0152(7) Uani 1 1 d . . . C25 C 0.09085(17) 0.44264(17) 0.10293(17) 0.0141(7) Uani 1 1 d . . . C26 C 0.06459(17) 0.33396(18) 0.14354(19) 0.0180(7) Uani 1 1 d . . . H26A H 0.0669 0.2982 0.1170 0.027 Uiso 1 1 calc R . . H26B H 0.0240 0.3508 0.1357 0.027 Uiso 1 1 calc R . . H26C H 0.0751 0.3200 0.1851 0.027 Uiso 1 1 calc R . . C27 C 0.20832(17) 0.32693(17) 0.17282(18) 0.0168(7) Uani 1 1 d . . . H27A H 0.2276 0.3071 0.1429 0.025 Uiso 1 1 calc R . . H27B H 0.1829 0.2961 0.1876 0.025 Uiso 1 1 calc R . . H27C H 0.2388 0.3420 0.2060 0.025 Uiso 1 1 calc R . . C28 C 0.25847(17) 0.4514(2) 0.12482(19) 0.0204(8) Uani 1 1 d . . . H28A H 0.2694 0.4364 0.0879 0.031 Uiso 1 1 calc R . . H28B H 0.2830 0.4300 0.1589 0.031 Uiso 1 1 calc R . . H28C H 0.2652 0.4969 0.1285 0.031 Uiso 1 1 calc R . . C29 C 0.1485(2) 0.53667(18) 0.06538(19) 0.0198(8) Uani 1 1 d . . . H29A H 0.1509 0.5280 0.0239 0.030 Uiso 1 1 calc R . . H29B H 0.1841 0.5596 0.0847 0.030 Uiso 1 1 calc R . . H29C H 0.1131 0.5621 0.0666 0.030 Uiso 1 1 calc R . . C30 C 0.02839(17) 0.46400(19) 0.07798(18) 0.0182(7) Uani 1 1 d . . . H30A H 0.0152 0.4459 0.0382 0.027 Uiso 1 1 calc R . . H30B H 0.0274 0.5100 0.0752 0.027 Uiso 1 1 calc R . . H30C H 0.0018 0.4500 0.1042 0.027 Uiso 1 1 calc R . . Cr3 Cr 0.14293(3) 0.46343(3) 0.19229(3) 0.01210(11) Uani 1 1 d . . . P6 P 0.08602(5) 0.44314(5) 0.26954(5) 0.01652(18) Uani 1 1 d . . . P7 P 0.18249(5) 0.42935(4) 0.29488(4) 0.01637(18) Uani 1 1 d . . . P8 P 0.22654(4) 0.50919(5) 0.26137(5) 0.01707(18) Uani 1 1 d . . . P9 P 0.15735(5) 0.57448(4) 0.21844(4) 0.01631(18) Uani 1 1 d . . . P10 P 0.07009(4) 0.53309(5) 0.22267(4) 0.01598(18) Uani 1 1 d . . . Cr4 Cr 0.14528(3) 0.53332(3) 0.31396(3) 0.01141(11) Uani 1 1 d . . . C31 C 0.09631(17) 0.55253(17) 0.38529(17) 0.0140(6) Uani 1 1 d . . . C32 C 0.15251(17) 0.52405(17) 0.41059(16) 0.0142(6) Uani 1 1 d . . . C33 C 0.19832(16) 0.56572(17) 0.39951(17) 0.0139(6) Uani 1 1 d . . . C34 C 0.17095(17) 0.61863(16) 0.36793(18) 0.0132(7) Uani 1 1 d . . . C35 C 0.10769(17) 0.61089(16) 0.35906(17) 0.0130(6) Uani 1 1 d . . . C36 C 0.03592(18) 0.52621(19) 0.38778(18) 0.0183(7) Uani 1 1 d . . . H36A H 0.0199 0.5476 0.4191 0.027 Uiso 1 1 calc R . . H36B H 0.0394 0.4811 0.3965 0.027 Uiso 1 1 calc R . . H36C H 0.0091 0.5327 0.3493 0.027 Uiso 1 1 calc R . . C37 C 0.16098(18) 0.46366(17) 0.44460(17) 0.0162(7) Uani 1 1 d . . . H37A H 0.1640 0.4723 0.4871 0.024 Uiso 1 1 calc R . . H37B H 0.1976 0.4432 0.4383 0.024 Uiso 1 1 calc R . . H37C H 0.1269 0.4359 0.4307 0.024 Uiso 1 1 calc R . . C38 C 0.26420(17) 0.55754(18) 0.41962(19) 0.0178(7) Uani 1 1 d . . . H38A H 0.2766 0.5754 0.4596 0.027 Uiso 1 1 calc R . . H38B H 0.2850 0.5792 0.3919 0.027 Uiso 1 1 calc R . . H38C H 0.2741 0.5127 0.4205 0.027 Uiso 1 1 calc R . . C39 C 0.20234(18) 0.67538(18) 0.35048(18) 0.0177(7) Uani 1 1 d . . . H39A H 0.2103 0.7049 0.3840 0.026 Uiso 1 1 calc R . . H39B H 0.1772 0.6958 0.3162 0.026 Uiso 1 1 calc R . . H39C H 0.2400 0.6626 0.3399 0.026 Uiso 1 1 calc R . . C40 C 0.06192(17) 0.65702(18) 0.32994(18) 0.0175(7) Uani 1 1 d . . . H40A H 0.0522 0.6859 0.3600 0.026 Uiso 1 1 calc R . . H40B H 0.0260 0.6345 0.3109 0.026 Uiso 1 1 calc R . . H40C H 0.0776 0.6810 0.2998 0.026 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.01581(13) 0.00947(10) 0.01743(13) -0.00095(8) 0.00477(8) 0.00076(8) F1 0.0262(13) 0.0178(11) 0.0318(14) -0.0083(10) 0.0017(10) -0.0036(10) F2 0.0382(15) 0.0197(11) 0.0219(13) 0.0040(10) 0.0043(10) 0.0101(11) F3 0.0203(12) 0.0239(12) 0.0289(13) 0.0039(10) 0.0104(10) 0.0051(10) F4 0.0178(11) 0.0147(10) 0.0306(13) 0.0035(9) 0.0055(9) 0.0045(8) F5 0.0305(14) 0.0219(13) 0.0230(13) -0.0004(9) 0.0140(11) -0.0026(10) F6 0.0326(14) 0.0152(10) 0.0206(12) -0.0037(9) 0.0050(10) -0.0048(10) Sb2 0.01392(13) 0.00929(10) 0.01633(14) -0.00033(8) 0.00358(8) 0.00012(8) F7 0.0509(19) 0.0169(12) 0.0379(16) 0.0123(11) 0.0032(14) -0.0073(12) F8 0.0197(12) 0.0331(15) 0.0340(14) -0.0037(11) 0.0103(10) 0.0049(11) F9 0.0254(13) 0.0228(12) 0.0253(13) -0.0072(10) 0.0000(10) -0.0042(10) F10 0.0237(13) 0.0288(14) 0.0316(14) -0.0094(11) 0.0050(10) 0.0088(10) F11 0.0267(13) 0.0249(13) 0.0194(12) -0.0068(10) -0.0009(9) 0.0002(10) F12 0.0255(13) 0.0174(12) 0.0362(15) 0.0106(10) 0.0039(11) -0.0045(10) C1 0.0128(16) 0.0081(14) 0.0198(17) -0.0008(12) 0.0065(12) 0.0009(11) C2 0.0090(15) 0.0110(14) 0.0193(17) -0.0014(13) 0.0036(12) -0.0002(11) C3 0.0089(15) 0.0088(15) 0.0210(18) -0.0018(12) 0.0001(12) -0.0002(12) C4 0.0097(15) 0.0094(14) 0.0183(17) 0.0000(12) 0.0031(12) 0.0030(12) C5 0.0116(15) 0.0075(14) 0.0191(17) -0.0006(12) 0.0033(12) 0.0008(12) C6 0.0219(19) 0.0157(17) 0.0167(17) -0.0005(13) 0.0062(14) 0.0016(14) C7 0.0141(17) 0.0107(15) 0.029(2) -0.0012(14) 0.0068(14) -0.0022(13) C8 0.0134(16) 0.0150(17) 0.0185(17) -0.0028(13) 0.0023(13) -0.0003(12) C9 0.0193(18) 0.0125(16) 0.0188(17) 0.0024(13) 0.0046(13) -0.0011(13) C10 0.0145(17) 0.0117(16) 0.0200(18) -0.0041(13) 0.0029(13) -0.0025(12) Cr1 0.0096(3) 0.0073(2) 0.0140(3) -0.00120(19) 0.00262(19) -0.00021(18) P1 0.0179(5) 0.0299(6) 0.0196(5) -0.0079(4) 0.0003(4) 0.0081(4) P2 0.0176(5) 0.0165(5) 0.0354(6) 0.0097(4) 0.0121(4) 0.0052(4) P3 0.0115(4) 0.0170(5) 0.0327(6) -0.0124(4) 0.0011(4) 0.0006(3) P4 0.0178(5) 0.0263(5) 0.0205(5) 0.0070(4) 0.0072(4) 0.0090(4) P5 0.0123(4) 0.0103(4) 0.0449(7) -0.0028(4) 0.0069(4) -0.0016(3) Cr2 0.0093(3) 0.0071(2) 0.0146(3) -0.00065(19) 0.00250(18) -0.00034(18) C11 0.0100(15) 0.0107(15) 0.0160(16) 0.0017(12) 0.0032(12) 0.0011(11) C12 0.0140(16) 0.0075(14) 0.0217(19) -0.0027(12) 0.0057(13) 0.0020(12) C13 0.0110(15) 0.0111(15) 0.0188(17) -0.0007(12) 0.0049(12) 0.0007(11) C14 0.0094(15) 0.0130(16) 0.0180(17) -0.0007(12) 0.0038(12) 0.0018(12) C15 0.0119(16) 0.0097(14) 0.0173(17) 0.0009(12) 0.0026(12) 0.0016(11) C16 0.0158(17) 0.0159(16) 0.0182(17) 0.0007(13) 0.0020(13) 0.0039(13) C17 0.0193(18) 0.0083(15) 0.031(2) -0.0002(14) 0.0096(15) -0.0023(13) C18 0.0173(19) 0.0173(18) 0.023(2) -0.0071(14) 0.0030(14) -0.0019(13) C19 0.0180(17) 0.0161(17) 0.0198(18) 0.0067(13) 0.0075(13) 0.0062(13) C20 0.0122(16) 0.0101(15) 0.0256(19) 0.0006(13) 0.0021(13) -0.0026(12) C21 0.0146(17) 0.0113(15) 0.0182(18) 0.0030(12) 0.0033(13) -0.0009(12) C22 0.0147(17) 0.0101(16) 0.0207(19) 0.0017(12) 0.0043(14) 0.0025(12) C23 0.0116(16) 0.0124(16) 0.0209(18) -0.0005(13) 0.0042(13) 0.0027(12) C24 0.0181(18) 0.0127(15) 0.0159(17) 0.0018(13) 0.0061(13) 0.0036(13) C25 0.0159(17) 0.0111(15) 0.0155(16) 0.0015(12) 0.0035(13) 0.0023(12) C26 0.0169(18) 0.0133(16) 0.0243(19) 0.0038(14) 0.0053(14) -0.0041(13) C27 0.0162(17) 0.0127(16) 0.0207(18) 0.0001(13) 0.0021(13) 0.0050(13) C28 0.0131(17) 0.0211(19) 0.029(2) -0.0029(15) 0.0084(15) -0.0008(14) C29 0.029(2) 0.0103(16) 0.0213(19) 0.0037(13) 0.0080(15) 0.0007(14) C30 0.0147(17) 0.0201(18) 0.0188(18) 0.0041(14) 0.0008(13) 0.0034(13) Cr3 0.0106(3) 0.0087(2) 0.0174(3) 0.0028(2) 0.0036(2) 0.00111(18) P6 0.0180(5) 0.0128(4) 0.0200(5) -0.0032(3) 0.0068(3) -0.0044(3) P7 0.0210(5) 0.0106(4) 0.0170(4) 0.0005(3) 0.0022(3) 0.0035(3) P8 0.0132(4) 0.0167(4) 0.0218(5) -0.0031(4) 0.0046(3) -0.0021(3) P9 0.0234(5) 0.0092(4) 0.0170(4) 0.0009(3) 0.0055(3) -0.0012(3) P10 0.0147(4) 0.0143(4) 0.0182(5) -0.0027(3) 0.0014(3) 0.0045(3) Cr4 0.0105(3) 0.0079(2) 0.0157(3) 0.00129(19) 0.00229(19) -0.00042(18) C31 0.0148(17) 0.0119(16) 0.0162(17) 0.0009(12) 0.0048(13) -0.0024(12) C32 0.0176(17) 0.0112(14) 0.0137(16) 0.0004(12) 0.0028(12) -0.0009(12) C33 0.0113(16) 0.0096(15) 0.0195(17) 0.0004(12) -0.0001(12) -0.0009(12) C34 0.0138(17) 0.0092(15) 0.0157(17) -0.0007(11) 0.0008(13) -0.0018(11) C35 0.0127(16) 0.0099(13) 0.0154(17) 0.0016(12) 0.0001(12) 0.0001(12) C36 0.0183(18) 0.0158(17) 0.0216(19) -0.0021(14) 0.0060(14) -0.0048(13) C37 0.0219(19) 0.0091(15) 0.0177(17) 0.0026(12) 0.0038(13) -0.0022(13) C38 0.0124(16) 0.0155(17) 0.0249(19) 0.0013(14) 0.0017(13) 0.0005(13) C39 0.0208(18) 0.0106(15) 0.0220(18) 0.0034(13) 0.0052(14) -0.0046(13) C40 0.0144(17) 0.0160(17) 0.0204(17) -0.0013(13) -0.0009(13) 0.0041(13) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb1 F6 1.872(2) . ? Sb1 F4 1.873(2) . ? Sb1 F2 1.877(2) . ? Sb1 F5 1.877(3) . ? Sb1 F1 1.881(2) . ? Sb1 F3 1.884(2) . ? Sb2 F7 1.861(3) . ? Sb2 F9 1.871(2) . ? Sb2 F11 1.871(2) . ? Sb2 F12 1.876(2) . ? Sb2 F8 1.878(3) . ? Sb2 F10 1.883(3) . ? C1 C2 1.435(5) . ? C1 C5 1.438(5) . ? C1 C6 1.482(5) . ? C1 Cr1 2.218(4) . ? C2 C3 1.422(5) . ? C2 C7 1.495(5) . ? C2 Cr1 2.207(4) . ? C3 C4 1.441(5) . ? C3 C8 1.497(5) . ? C3 Cr1 2.202(3) . ? C4 C5 1.425(5) . ? C4 C9 1.487(5) . ? C4 Cr1 2.222(3) . ? C5 C10 1.501(5) . ? C5 Cr1 2.224(4) . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? Cr1 P5 2.3727(12) . ? Cr1 P3 2.3784(12) . ? Cr1 P1 2.3807(12) . ? Cr1 P4 2.3815(12) . ? Cr1 P2 2.3845(12) . ? Cr1 Cr2 2.8948(8) . ? P1 P2 2.2212(17) . ? P1 P5 2.2266(17) . ? P1 Cr2 2.3786(12) . ? P2 P3 2.2123(17) . ? P2 Cr2 2.3855(12) . ? P3 P4 2.2254(16) . ? P3 Cr2 2.3737(12) . ? P4 P5 2.2168(17) . ? P4 Cr2 2.3835(12) . ? P5 Cr2 2.3771(12) . ? Cr2 C12 2.215(4) . ? Cr2 C11 2.216(4) . ? Cr2 C14 2.217(4) . ? Cr2 C15 2.220(4) . ? Cr2 C13 2.222(4) . ? C11 C12 1.426(5) . ? C11 C15 1.435(5) . ? C11 C16 1.490(5) . ? C12 C13 1.438(5) . ? C12 C17 1.495(5) . ? C13 C14 1.423(5) . ? C13 C18 1.492(5) . ? C14 C15 1.427(5) . ? C14 C19 1.505(5) . ? C15 C20 1.496(5) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 C25 1.423(5) . ? C21 C22 1.430(6) . ? C21 C26 1.512(5) . ? C21 Cr3 2.218(4) . ? C22 C23 1.426(5) . ? C22 C27 1.507(5) . ? C22 Cr3 2.211(4) . ? C23 C24 1.427(5) . ? C23 C28 1.507(5) . ? C23 Cr3 2.203(4) . ? C24 C25 1.446(5) . ? C24 C29 1.497(5) . ? C24 Cr3 2.196(4) . ? C25 C30 1.504(5) . ? C25 Cr3 2.204(4) . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C27 H27C 0.9800 . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? Cr3 P6 2.4313(12) . ? Cr3 P10 2.4322(11) . ? Cr3 P8 2.4374(12) . ? Cr3 P9 2.4435(11) . ? Cr3 P7 2.4571(12) . ? P6 P10 2.1895(14) . ? P6 P7 2.1929(14) . ? P6 Cr4 2.4536(11) . ? P7 P8 2.1892(14) . ? P7 Cr4 2.4401(11) . ? P8 P9 2.1914(14) . ? P8 Cr4 2.4598(11) . ? P9 P10 2.2036(15) . ? P9 Cr4 2.4210(12) . ? P10 Cr4 2.4366(12) . ? Cr4 C31 2.192(4) . ? Cr4 C32 2.195(4) . ? Cr4 C33 2.205(4) . ? Cr4 C35 2.208(4) . ? Cr4 C34 2.210(4) . ? C31 C35 1.425(5) . ? C31 C32 1.439(5) . ? C31 C36 1.504(5) . ? C32 C33 1.433(5) . ? C32 C37 1.495(5) . ? C33 C34 1.416(5) . ? C33 C38 1.500(5) . ? C34 C35 1.433(5) . ? C34 C39 1.499(5) . ? C35 C40 1.495(5) . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C39 H39A 0.9800 . ? C39 H39B 0.9800 . ? C39 H39C 0.9800 . ? C40 H40A 0.9800 . ? C40 H40B 0.9800 . ? C40 H40C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F6 Sb1 F4 90.77(11) . . ? F6 Sb1 F2 89.97(12) . . ? F4 Sb1 F2 178.46(12) . . ? F6 Sb1 F5 89.09(12) . . ? F4 Sb1 F5 90.08(12) . . ? F2 Sb1 F5 91.28(12) . . ? F6 Sb1 F1 178.74(12) . . ? F4 Sb1 F1 90.07(12) . . ? F2 Sb1 F1 89.22(12) . . ? F5 Sb1 F1 89.96(12) . . ? F6 Sb1 F3 90.55(12) . . ? F4 Sb1 F3 89.21(11) . . ? F2 Sb1 F3 89.44(12) . . ? F5 Sb1 F3 179.20(12) . . ? F1 Sb1 F3 90.40(12) . . ? F7 Sb2 F9 89.66(13) . . ? F7 Sb2 F11 89.94(13) . . ? F9 Sb2 F11 179.59(13) . . ? F7 Sb2 F12 179.48(14) . . ? F9 Sb2 F12 90.63(12) . . ? F11 Sb2 F12 89.76(12) . . ? F7 Sb2 F8 91.10(14) . . ? F9 Sb2 F8 89.88(12) . . ? F11 Sb2 F8 90.02(12) . . ? F12 Sb2 F8 89.33(13) . . ? F7 Sb2 F10 90.84(14) . . ? F9 Sb2 F10 90.18(12) . . ? F11 Sb2 F10 89.92(12) . . ? F12 Sb2 F10 88.73(12) . . ? F8 Sb2 F10 178.06(13) . . ? C2 C1 C5 107.8(3) . . ? C2 C1 C6 126.7(3) . . ? C5 C1 C6 125.4(3) . . ? C2 C1 Cr1 70.7(2) . . ? C5 C1 Cr1 71.4(2) . . ? C6 C1 Cr1 125.7(3) . . ? C3 C2 C1 107.7(3) . . ? C3 C2 C7 127.2(3) . . ? C1 C2 C7 125.0(3) . . ? C3 C2 Cr1 71.0(2) . . ? C1 C2 Cr1 71.5(2) . . ? C7 C2 Cr1 126.0(2) . . ? C2 C3 C4 108.8(3) . . ? C2 C3 C8 126.7(3) . . ? C4 C3 C8 124.5(3) . . ? C2 C3 Cr1 71.4(2) . . ? C4 C3 Cr1 71.7(2) . . ? C8 C3 Cr1 124.9(3) . . ? C5 C4 C3 107.3(3) . . ? C5 C4 C9 126.2(3) . . ? C3 C4 C9 126.5(3) . . ? C5 C4 Cr1 71.4(2) . . ? C3 C4 Cr1 70.24(19) . . ? C9 C4 Cr1 126.2(2) . . ? C4 C5 C1 108.4(3) . . ? C4 C5 C10 126.6(3) . . ? C1 C5 C10 124.7(3) . . ? C4 C5 Cr1 71.2(2) . . ? C1 C5 Cr1 70.9(2) . . ? C10 C5 Cr1 127.9(3) . . ? C1 C6 H6A 109.5 . . ? C1 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C1 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C3 Cr1 C2 37.64(14) . . ? C3 Cr1 C1 62.93(14) . . ? C2 Cr1 C1 37.84(13) . . ? C3 Cr1 C4 38.01(13) . . ? C2 Cr1 C4 63.41(13) . . ? C1 Cr1 C4 63.08(13) . . ? C3 Cr1 C5 62.85(13) . . ? C2 Cr1 C5 63.19(13) . . ? C1 Cr1 C5 37.78(13) . . ? C4 Cr1 C5 37.38(13) . . ? C3 Cr1 P5 136.44(10) . . ? C2 Cr1 P5 159.93(10) . . ? C1 Cr1 P5 124.31(10) . . ? C4 Cr1 P5 102.25(10) . . ? C5 Cr1 P5 96.81(10) . . ? C3 Cr1 P3 95.97(10) . . ? C2 Cr1 P3 101.79(10) . . ? C1 Cr1 P3 136.07(10) . . ? C4 Cr1 P3 123.66(10) . . ? C5 Cr1 P3 158.72(10) . . ? P5 Cr1 P3 97.94(4) . . ? C3 Cr1 P1 159.70(11) . . ? C2 Cr1 P1 124.07(11) . . ? C1 Cr1 P1 96.91(10) . . ? C4 Cr1 P1 136.82(10) . . ? C5 Cr1 P1 103.26(10) . . ? P5 Cr1 P1 55.86(5) . . ? P3 Cr1 P1 97.70(4) . . ? C3 Cr1 P4 101.91(11) . . ? C2 Cr1 P4 135.78(11) . . ? C1 Cr1 P4 158.90(10) . . ? C4 Cr1 P4 95.87(10) . . ? C5 Cr1 P4 123.49(10) . . ? P5 Cr1 P4 55.59(4) . . ? P3 Cr1 P4 55.75(4) . . ? P1 Cr1 P4 98.18(4) . . ? C3 Cr1 P2 123.37(10) . . ? C2 Cr1 P2 96.02(10) . . ? C1 Cr1 P2 102.53(10) . . ? C4 Cr1 P2 159.32(10) . . ? C5 Cr1 P2 136.85(10) . . ? P5 Cr1 P2 98.21(4) . . ? P3 Cr1 P2 55.35(4) . . ? P1 Cr1 P2 55.57(4) . . ? P4 Cr1 P2 98.15(4) . . ? C3 Cr1 Cr2 146.11(10) . . ? C2 Cr1 Cr2 146.26(9) . . ? C1 Cr1 Cr2 147.16(10) . . ? C4 Cr1 Cr2 146.33(9) . . ? C5 Cr1 Cr2 147.27(10) . . ? P5 Cr1 Cr2 52.52(3) . . ? P3 Cr1 Cr2 52.40(3) . . ? P1 Cr1 Cr2 52.50(3) . . ? P4 Cr1 Cr2 52.62(3) . . ? P2 Cr1 Cr2 52.65(3) . . ? P2 P1 P5 107.90(6) . . ? P2 P1 Cr2 62.37(4) . . ? P5 P1 Cr2 62.05(4) . . ? P2 P1 Cr1 62.30(4) . . ? P5 P1 Cr1 61.89(4) . . ? Cr2 P1 Cr1 74.92(4) . . ? P3 P2 P1 107.86(6) . . ? P3 P2 Cr1 62.18(4) . . ? P1 P2 Cr1 62.13(4) . . ? P3 P2 Cr2 62.03(4) . . ? P1 P2 Cr2 62.05(4) . . ? Cr1 P2 Cr2 74.73(4) . . ? P2 P3 P4 108.48(6) . . ? P2 P3 Cr2 62.57(4) . . ? P4 P3 Cr2 62.33(4) . . ? P2 P3 Cr1 62.46(4) . . ? P4 P3 Cr1 62.20(4) . . ? Cr2 P3 Cr1 75.06(4) . . ? P5 P4 P3 107.57(6) . . ? P5 P4 Cr1 62.00(4) . . ? P3 P4 Cr1 62.05(4) . . ? P5 P4 Cr2 62.10(4) . . ? P3 P4 Cr2 61.89(4) . . ? Cr1 P4 Cr2 74.82(4) . . ? P4 P5 P1 108.19(6) . . ? P4 P5 Cr1 62.41(4) . . ? P1 P5 Cr1 62.25(4) . . ? P4 P5 Cr2 62.39(4) . . ? P1 P5 Cr2 62.12(4) . . ? Cr1 P5 Cr2 75.10(4) . . ? C12 Cr2 C11 37.56(13) . . ? C12 Cr2 C14 62.90(14) . . ? C11 Cr2 C14 62.66(13) . . ? C12 Cr2 C15 63.17(13) . . ? C11 Cr2 C15 37.77(13) . . ? C14 Cr2 C15 37.52(13) . . ? C12 Cr2 C13 37.82(14) . . ? C11 Cr2 C13 62.78(14) . . ? C14 Cr2 C13 37.40(13) . . ? C15 Cr2 C13 62.89(13) . . ? C12 Cr2 P3 105.10(10) . . ? C11 Cr2 P3 140.37(10) . . ? C14 Cr2 P3 120.71(10) . . ? C15 Cr2 P3 157.56(10) . . ? C13 Cr2 P3 95.85(10) . . ? C12 Cr2 P5 156.92(11) . . ? C11 Cr2 P5 120.28(10) . . ? C14 Cr2 P5 104.16(10) . . ? C15 Cr2 P5 94.70(9) . . ? C13 Cr2 P5 139.20(10) . . ? P3 Cr2 P5 97.95(4) . . ? C12 Cr2 P1 120.59(11) . . ? C11 Cr2 P1 95.59(10) . . ? C14 Cr2 P1 139.76(10) . . ? C15 Cr2 P1 104.55(10) . . ? C13 Cr2 P1 157.45(11) . . ? P3 Cr2 P1 97.89(4) . . ? P5 Cr2 P1 55.83(4) . . ? C12 Cr2 P4 139.86(11) . . ? C11 Cr2 P4 156.56(10) . . ? C14 Cr2 P4 94.95(10) . . ? C15 Cr2 P4 119.69(10) . . ? C13 Cr2 P4 104.32(10) . . ? P3 Cr2 P4 55.78(4) . . ? P5 Cr2 P4 55.51(4) . . ? P1 Cr2 P4 98.19(4) . . ? C12 Cr2 P2 95.94(11) . . ? C11 Cr2 P2 105.36(10) . . ? C14 Cr2 P2 157.78(10) . . ? C15 Cr2 P2 140.57(10) . . ? C13 Cr2 P2 121.17(10) . . ? P3 Cr2 P2 55.40(4) . . ? P5 Cr2 P2 98.06(4) . . ? P1 Cr2 P2 55.58(4) . . ? P4 Cr2 P2 98.07(4) . . ? C12 Cr2 Cr1 147.40(10) . . ? C11 Cr2 Cr1 147.14(10) . . ? C14 Cr2 Cr1 146.20(10) . . ? C15 Cr2 Cr1 145.97(9) . . ? C13 Cr2 Cr1 146.96(10) . . ? P3 Cr2 Cr1 52.54(3) . . ? P5 Cr2 Cr1 52.38(3) . . ? P1 Cr2 Cr1 52.57(3) . . ? P4 Cr2 Cr1 52.56(3) . . ? P2 Cr2 Cr1 52.62(3) . . ? C12 C11 C15 108.5(3) . . ? C12 C11 C16 124.7(3) . . ? C15 C11 C16 126.6(3) . . ? C12 C11 Cr2 71.2(2) . . ? C15 C11 Cr2 71.3(2) . . ? C16 C11 Cr2 126.7(3) . . ? C11 C12 C13 107.6(3) . . ? C11 C12 C17 126.6(4) . . ? C13 C12 C17 125.7(3) . . ? C11 C12 Cr2 71.2(2) . . ? C13 C12 Cr2 71.3(2) . . ? C17 C12 Cr2 126.5(3) . . ? C14 C13 C12 107.8(3) . . ? C14 C13 C18 126.2(3) . . ? C12 C13 C18 125.8(3) . . ? C14 C13 Cr2 71.1(2) . . ? C12 C13 Cr2 70.8(2) . . ? C18 C13 Cr2 127.1(3) . . ? C13 C14 C15 108.8(3) . . ? C13 C14 C19 125.8(3) . . ? C15 C14 C19 125.3(3) . . ? C13 C14 Cr2 71.5(2) . . ? C15 C14 Cr2 71.3(2) . . ? C19 C14 Cr2 125.5(2) . . ? C14 C15 C11 107.3(3) . . ? C14 C15 C20 125.8(3) . . ? C11 C15 C20 126.9(3) . . ? C14 C15 Cr2 71.1(2) . . ? C11 C15 Cr2 71.0(2) . . ? C20 C15 Cr2 125.7(2) . . ? C11 C16 H16A 109.5 . . ? C11 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C11 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C25 C21 C22 107.7(3) . . ? C25 C21 C26 125.1(4) . . ? C22 C21 C26 127.0(3) . . ? C25 C21 Cr3 70.7(2) . . ? C22 C21 Cr3 70.9(2) . . ? C26 C21 Cr3 127.3(3) . . ? C23 C22 C21 108.5(3) . . ? C23 C22 C27 125.0(3) . . ? C21 C22 C27 126.3(3) . . ? C23 C22 Cr3 70.8(2) . . ? C21 C22 Cr3 71.4(2) . . ? C27 C22 Cr3 126.6(3) . . ? C22 C23 C24 108.2(3) . . ? C22 C23 C28 125.6(3) . . ? C24 C23 C28 126.2(3) . . ? C22 C23 Cr3 71.5(2) . . ? C24 C23 Cr3 70.8(2) . . ? C28 C23 Cr3 126.3(3) . . ? C23 C24 C25 107.4(3) . . ? C23 C24 C29 125.5(4) . . ? C25 C24 C29 126.8(4) . . ? C23 C24 Cr3 71.3(2) . . ? C25 C24 Cr3 71.1(2) . . ? C29 C24 Cr3 127.2(3) . . ? C21 C25 C24 108.3(3) . . ? C21 C25 C30 126.1(3) . . ? C24 C25 C30 125.5(3) . . ? C21 C25 Cr3 71.8(2) . . ? C24 C25 Cr3 70.5(2) . . ? C30 C25 Cr3 126.5(3) . . ? C21 C26 H26A 109.5 . . ? C21 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C21 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C22 C27 H27A 109.5 . . ? C22 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? C22 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? C23 C28 H28A 109.5 . . ? C23 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C23 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C24 C29 H29A 109.5 . . ? C24 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C24 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C25 C30 H30A 109.5 . . ? C25 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? C25 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C24 Cr3 C23 37.87(13) . . ? C24 Cr3 C25 38.37(14) . . ? C23 Cr3 C25 63.39(14) . . ? C24 Cr3 C22 63.25(14) . . ? C23 Cr3 C22 37.70(14) . . ? C25 Cr3 C22 62.91(14) . . ? C24 Cr3 C21 63.57(14) . . ? C23 Cr3 C21 63.26(14) . . ? C25 Cr3 C21 37.55(13) . . ? C22 Cr3 C21 37.68(14) . . ? C24 Cr3 P6 148.82(11) . . ? C23 Cr3 P6 155.27(10) . . ? C25 Cr3 P6 111.69(10) . . ? C22 Cr3 P6 117.63(11) . . ? C21 Cr3 P6 97.55(11) . . ? C24 Cr3 P10 110.68(10) . . ? C23 Cr3 P10 147.61(10) . . ? C25 Cr3 P10 96.31(10) . . ? C22 Cr3 P10 154.28(11) . . ? C21 Cr3 P10 116.61(11) . . ? P6 Cr3 P10 53.51(4) . . ? C24 Cr3 P8 115.57(11) . . ? C23 Cr3 P8 96.09(10) . . ? C25 Cr3 P8 153.91(11) . . ? C22 Cr3 P8 111.43(11) . . ? C21 Cr3 P8 148.27(11) . . ? P6 Cr3 P8 93.65(4) . . ? P10 Cr3 P8 93.87(4) . . ? C24 Cr3 P9 95.60(10) . . ? C23 Cr3 P9 110.63(10) . . ? C25 Cr3 P9 116.39(10) . . ? C22 Cr3 P9 147.50(11) . . ? C21 Cr3 P9 153.93(10) . . ? P6 Cr3 P9 93.40(4) . . ? P10 Cr3 P9 53.74(4) . . ? P8 Cr3 P9 53.36(4) . . ? C24 Cr3 P7 155.18(11) . . ? C23 Cr3 P7 117.48(10) . . ? C25 Cr3 P7 149.42(10) . . ? C22 Cr3 P7 98.42(11) . . ? C21 Cr3 P7 112.99(10) . . ? P6 Cr3 P7 53.30(4) . . ? P10 Cr3 P7 93.01(4) . . ? P8 Cr3 P7 53.14(4) . . ? P9 Cr3 P7 92.51(4) . . ? P10 P6 P7 108.06(6) . . ? P10 P6 Cr3 63.26(4) . . ? P7 P6 Cr3 63.95(4) . . ? P10 P6 Cr4 63.00(4) . . ? P7 P6 Cr4 63.06(4) . . ? Cr3 P6 Cr4 80.27(4) . . ? P8 P7 P6 108.24(5) . . ? P8 P7 Cr4 63.93(4) . . ? P6 P7 Cr4 63.69(4) . . ? P8 P7 Cr3 62.97(4) . . ? P6 P7 Cr3 62.75(4) . . ? Cr4 P7 Cr3 80.03(3) . . ? P7 P8 P9 107.84(6) . . ? P7 P8 Cr3 63.89(4) . . ? P9 P8 Cr3 63.47(4) . . ? P7 P8 Cr4 63.00(4) . . ? P9 P8 Cr4 62.42(4) . . ? Cr3 P8 Cr4 80.03(4) . . ? P8 P9 P10 108.09(5) . . ? P8 P9 Cr4 64.23(4) . . ? P10 P9 Cr4 63.38(4) . . ? P8 P9 Cr3 63.18(4) . . ? P10 P9 Cr3 62.87(4) . . ? Cr4 P9 Cr3 80.68(4) . . ? P6 P10 P9 107.72(5) . . ? P6 P10 Cr3 63.22(4) . . ? P9 P10 Cr3 63.39(4) . . ? P6 P10 Cr4 63.80(4) . . ? P9 P10 Cr4 62.66(4) . . ? Cr3 P10 Cr4 80.60(4) . . ? C31 Cr4 C32 38.29(14) . . ? C31 Cr4 C33 63.47(14) . . ? C32 Cr4 C33 38.02(13) . . ? C31 Cr4 C35 37.79(13) . . ? C32 Cr4 C35 63.62(13) . . ? C33 Cr4 C35 63.17(13) . . ? C31 Cr4 C34 63.22(14) . . ? C32 Cr4 C34 63.28(14) . . ? C33 Cr4 C34 37.42(13) . . ? C35 Cr4 C34 37.86(14) . . ? C31 Cr4 P9 140.40(10) . . ? C32 Cr4 P9 160.64(10) . . ? C33 Cr4 P9 123.33(10) . . ? C35 Cr4 P9 106.00(10) . . ? C34 Cr4 P9 98.26(10) . . ? C31 Cr4 P10 105.12(10) . . ? C32 Cr4 P10 140.07(11) . . ? C33 Cr4 P10 159.76(10) . . ? C35 Cr4 P10 97.34(10) . . ? C34 Cr4 P10 123.26(10) . . ? P9 Cr4 P10 53.95(4) . . ? C31 Cr4 P7 123.33(10) . . ? C32 Cr4 P7 97.95(10) . . ? C33 Cr4 P7 106.91(10) . . ? C35 Cr4 P7 160.49(10) . . ? C34 Cr4 P7 141.27(11) . . ? P9 Cr4 P7 93.49(4) . . ? P10 Cr4 P7 93.32(4) . . ? C31 Cr4 P6 97.62(10) . . ? C32 Cr4 P6 105.95(10) . . ? C33 Cr4 P6 141.03(10) . . ? C35 Cr4 P6 122.91(10) . . ? C34 Cr4 P6 159.96(11) . . ? P9 Cr4 P6 93.41(4) . . ? P10 Cr4 P6 53.20(4) . . ? P7 Cr4 P6 53.24(4) . . ? C31 Cr4 P8 161.66(11) . . ? C32 Cr4 P8 123.95(11) . . ? C33 Cr4 P8 99.28(10) . . ? C35 Cr4 P8 141.80(10) . . ? C34 Cr4 P8 107.49(11) . . ? P9 Cr4 P8 53.35(4) . . ? P10 Cr4 P8 93.20(4) . . ? P7 Cr4 P8 53.07(4) . . ? P6 Cr4 P8 92.54(4) . . ? C35 C31 C32 108.3(3) . . ? C35 C31 C36 125.8(3) . . ? C32 C31 C36 125.9(3) . . ? C35 C31 Cr4 71.7(2) . . ? C32 C31 Cr4 71.0(2) . . ? C36 C31 Cr4 124.5(3) . . ? C33 C32 C31 107.3(3) . . ? C33 C32 C37 126.7(3) . . ? C31 C32 C37 125.9(3) . . ? C33 C32 Cr4 71.4(2) . . ? C31 C32 Cr4 70.7(2) . . ? C37 C32 Cr4 125.4(3) . . ? C34 C33 C32 108.4(3) . . ? C34 C33 C38 124.6(3) . . ? C32 C33 C38 127.0(3) . . ? C34 C33 Cr4 71.5(2) . . ? C32 C33 Cr4 70.6(2) . . ? C38 C33 Cr4 125.7(3) . . ? C33 C34 C35 108.4(3) . . ? C33 C34 C39 126.0(3) . . ? C35 C34 C39 125.4(3) . . ? C33 C34 Cr4 71.1(2) . . ? C35 C34 Cr4 71.0(2) . . ? C39 C34 Cr4 127.0(3) . . ? C31 C35 C34 107.6(3) . . ? C31 C35 C40 126.2(3) . . ? C34 C35 C40 126.2(3) . . ? C31 C35 Cr4 70.5(2) . . ? C34 C35 Cr4 71.1(2) . . ? C40 C35 Cr4 125.8(3) . . ? C31 C36 H36A 109.5 . . ? C31 C36 H36B 109.5 . . ? H36A C36 H36B 109.5 . . ? C31 C36 H36C 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C32 C37 H37A 109.5 . . ? C32 C37 H37B 109.5 . . ? H37A C37 H37B 109.5 . . ? C32 C37 H37C 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? C33 C38 H38A 109.5 . . ? C33 C38 H38B 109.5 . . ? H38A C38 H38B 109.5 . . ? C33 C38 H38C 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? C34 C39 H39A 109.5 . . ? C34 C39 H39B 109.5 . . ? H39A C39 H39B 109.5 . . ? C34 C39 H39C 109.5 . . ? H39A C39 H39C 109.5 . . ? H39B C39 H39C 109.5 . . ? C35 C40 H40A 109.5 . . ? C35 C40 H40B 109.5 . . ? H40A C40 H40B 109.5 . . ? C35 C40 H40C 109.5 . . ? H40A C40 H40C 109.5 . . ? H40B C40 H40C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 C1 C2 C3 -0.1(4) . . . . ? C6 C1 C2 C3 177.2(4) . . . . ? Cr1 C1 C2 C3 -62.1(2) . . . . ? C5 C1 C2 C7 -176.5(3) . . . . ? C6 C1 C2 C7 0.8(6) . . . . ? Cr1 C1 C2 C7 121.4(4) . . . . ? C5 C1 C2 Cr1 62.0(2) . . . . ? C6 C1 C2 Cr1 -120.6(4) . . . . ? C1 C2 C3 C4 0.1(4) . . . . ? C7 C2 C3 C4 176.4(3) . . . . ? Cr1 C2 C3 C4 -62.4(2) . . . . ? C1 C2 C3 C8 -177.4(3) . . . . ? C7 C2 C3 C8 -1.0(6) . . . . ? Cr1 C2 C3 C8 120.2(4) . . . . ? C1 C2 C3 Cr1 62.5(2) . . . . ? C7 C2 C3 Cr1 -121.2(4) . . . . ? C2 C3 C4 C5 -0.1(4) . . . . ? C8 C3 C4 C5 177.5(3) . . . . ? Cr1 C3 C4 C5 -62.2(2) . . . . ? C2 C3 C4 C9 -176.9(3) . . . . ? C8 C3 C4 C9 0.6(6) . . . . ? Cr1 C3 C4 C9 121.0(4) . . . . ? C2 C3 C4 Cr1 62.1(2) . . . . ? C8 C3 C4 Cr1 -120.3(3) . . . . ? C3 C4 C5 C1 0.0(4) . . . . ? C9 C4 C5 C1 176.9(3) . . . . ? Cr1 C4 C5 C1 -61.4(2) . . . . ? C3 C4 C5 C10 -174.8(3) . . . . ? C9 C4 C5 C10 2.1(6) . . . . ? Cr1 C4 C5 C10 123.8(4) . . . . ? C3 C4 C5 Cr1 61.4(2) . . . . ? C9 C4 C5 Cr1 -121.7(4) . . . . ? C2 C1 C5 C4 0.0(4) . . . . ? C6 C1 C5 C4 -177.3(3) . . . . ? Cr1 C1 C5 C4 61.6(2) . . . . ? C2 C1 C5 C10 174.9(3) . . . . ? C6 C1 C5 C10 -2.4(6) . . . . ? Cr1 C1 C5 C10 -123.5(3) . . . . ? C2 C1 C5 Cr1 -61.6(2) . . . . ? C6 C1 C5 Cr1 121.0(4) . . . . ? C4 C3 Cr1 C2 118.0(3) . . . . ? C8 C3 Cr1 C2 -122.3(4) . . . . ? C2 C3 Cr1 C1 -37.9(2) . . . . ? C4 C3 Cr1 C1 80.1(2) . . . . ? C8 C3 Cr1 C1 -160.1(4) . . . . ? C2 C3 Cr1 C4 -118.0(3) . . . . ? C8 C3 Cr1 C4 119.8(4) . . . . ? C2 C3 Cr1 C5 -80.5(2) . . . . ? C4 C3 Cr1 C5 37.5(2) . . . . ? C8 C3 Cr1 C5 157.2(4) . . . . ? C2 C3 Cr1 P5 -150.26(17) . . . . ? C4 C3 Cr1 P5 -32.3(3) . . . . ? C8 C3 Cr1 P5 87.5(3) . . . . ? C2 C3 Cr1 P3 101.59(19) . . . . ? C4 C3 Cr1 P3 -140.5(2) . . . . ? C8 C3 Cr1 P3 -20.7(3) . . . . ? C2 C3 Cr1 P1 -30.6(4) . . . . ? C4 C3 Cr1 P1 87.4(3) . . . . ? C8 C3 Cr1 P1 -152.8(2) . . . . ? C2 C3 Cr1 P4 157.79(18) . . . . ? C4 C3 Cr1 P4 -84.3(2) . . . . ? C8 C3 Cr1 P4 35.5(3) . . . . ? C2 C3 Cr1 P2 49.6(2) . . . . ? C4 C3 Cr1 P2 167.54(17) . . . . ? C8 C3 Cr1 P2 -72.7(3) . . . . ? C2 C3 Cr1 Cr2 120.8(2) . . . . ? C4 C3 Cr1 Cr2 -121.3(2) . . . . ? C8 C3 Cr1 Cr2 -1.5(4) . . . . ? C1 C2 Cr1 C3 -117.0(3) . . . . ? C7 C2 Cr1 C3 122.7(4) . . . . ? C3 C2 Cr1 C1 117.0(3) . . . . ? C7 C2 Cr1 C1 -120.3(4) . . . . ? C3 C2 Cr1 C4 37.5(2) . . . . ? C1 C2 Cr1 C4 -79.6(2) . . . . ? C7 C2 Cr1 C4 160.1(4) . . . . ? C3 C2 Cr1 C5 79.5(2) . . . . ? C1 C2 Cr1 C5 -37.5(2) . . . . ? C7 C2 Cr1 C5 -157.8(4) . . . . ? C3 C2 Cr1 P5 84.8(4) . . . . ? C1 C2 Cr1 P5 -32.3(4) . . . . ? C7 C2 Cr1 P5 -152.6(3) . . . . ? C3 C2 Cr1 P3 -84.45(19) . . . . ? C1 C2 Cr1 P3 158.52(19) . . . . ? C7 C2 Cr1 P3 38.2(3) . . . . ? C3 C2 Cr1 P1 167.70(17) . . . . ? C1 C2 Cr1 P1 50.7(2) . . . . ? C7 C2 Cr1 P1 -69.6(3) . . . . ? C3 C2 Cr1 P4 -32.0(3) . . . . ? C1 C2 Cr1 P4 -149.07(18) . . . . ? C7 C2 Cr1 P4 90.6(3) . . . . ? C3 C2 Cr1 P2 -140.26(19) . . . . ? C1 C2 Cr1 P2 102.7(2) . . . . ? C7 C2 Cr1 P2 -17.6(3) . . . . ? C3 C2 Cr1 Cr2 -120.4(2) . . . . ? C1 C2 Cr1 Cr2 122.6(2) . . . . ? C7 C2 Cr1 Cr2 2.3(5) . . . . ? C2 C1 Cr1 C3 37.7(2) . . . . ? C5 C1 Cr1 C3 -79.8(2) . . . . ? C6 C1 Cr1 C3 159.5(4) . . . . ? C5 C1 Cr1 C2 -117.4(3) . . . . ? C6 C1 Cr1 C2 121.9(4) . . . . ? C2 C1 Cr1 C4 80.5(2) . . . . ? C5 C1 Cr1 C4 -36.9(2) . . . . ? C6 C1 Cr1 C4 -157.6(4) . . . . ? C2 C1 Cr1 C5 117.4(3) . . . . ? C6 C1 Cr1 C5 -120.7(4) . . . . ? C2 C1 Cr1 P5 167.18(17) . . . . ? C5 C1 Cr1 P5 49.7(2) . . . . ? C6 C1 Cr1 P5 -71.0(3) . . . . ? C2 C1 Cr1 P3 -31.1(3) . . . . ? C5 C1 Cr1 P3 -148.56(18) . . . . ? C6 C1 Cr1 P3 90.7(3) . . . . ? C2 C1 Cr1 P1 -139.8(2) . . . . ? C5 C1 Cr1 P1 102.7(2) . . . . ? C6 C1 Cr1 P1 -17.9(3) . . . . ? C2 C1 Cr1 P4 84.8(3) . . . . ? C5 C1 Cr1 P4 -32.7(4) . . . . ? C6 C1 Cr1 P4 -153.4(2) . . . . ? C2 C1 Cr1 P2 -83.6(2) . . . . ? C5 C1 Cr1 P2 158.93(19) . . . . ? C6 C1 Cr1 P2 38.2(3) . . . . ? C2 C1 Cr1 Cr2 -120.3(2) . . . . ? C5 C1 Cr1 Cr2 122.2(2) . . . . ? C6 C1 Cr1 Cr2 1.5(4) . . . . ? C5 C4 Cr1 C3 117.0(3) . . . . ? C9 C4 Cr1 C3 -121.3(4) . . . . ? C5 C4 Cr1 C2 79.9(2) . . . . ? C3 C4 Cr1 C2 -37.1(2) . . . . ? C9 C4 Cr1 C2 -158.4(4) . . . . ? C5 C4 Cr1 C1 37.3(2) . . . . ? C3 C4 Cr1 C1 -79.7(2) . . . . ? C9 C4 Cr1 C1 159.0(4) . . . . ? C3 C4 Cr1 C5 -117.0(3) . . . . ? C9 C4 Cr1 C5 121.7(4) . . . . ? C5 C4 Cr1 P5 -85.2(2) . . . . ? C3 C4 Cr1 P5 157.9(2) . . . . ? C9 C4 Cr1 P5 36.6(3) . . . . ? C5 C4 Cr1 P3 166.51(17) . . . . ? C3 C4 Cr1 P3 49.5(2) . . . . ? C9 C4 Cr1 P3 -71.8(3) . . . . ? C5 C4 Cr1 P1 -32.6(3) . . . . ? C3 C4 Cr1 P1 -149.57(19) . . . . ? C9 C4 Cr1 P1 89.1(3) . . . . ? C5 C4 Cr1 P4 -141.17(19) . . . . ? C3 C4 Cr1 P4 101.9(2) . . . . ? C9 C4 Cr1 P4 -19.5(3) . . . . ? C5 C4 Cr1 P2 86.3(3) . . . . ? C3 C4 Cr1 P2 -30.7(4) . . . . ? C9 C4 Cr1 P2 -152.0(2) . . . . ? C5 C4 Cr1 Cr2 -122.3(2) . . . . ? C3 C4 Cr1 Cr2 120.7(2) . . . . ? C9 C4 Cr1 Cr2 -0.6(4) . . . . ? C4 C5 Cr1 C3 -38.1(2) . . . . ? C1 C5 Cr1 C3 80.0(2) . . . . ? C10 C5 Cr1 C3 -160.4(4) . . . . ? C4 C5 Cr1 C2 -80.5(2) . . . . ? C1 C5 Cr1 C2 37.6(2) . . . . ? C10 C5 Cr1 C2 157.2(4) . . . . ? C4 C5 Cr1 C1 -118.1(3) . . . . ? C10 C5 Cr1 C1 119.6(4) . . . . ? C1 C5 Cr1 C4 118.1(3) . . . . ? C10 C5 Cr1 C4 -122.3(4) . . . . ? C4 C5 Cr1 P5 101.3(2) . . . . ? C1 C5 Cr1 P5 -140.6(2) . . . . ? C10 C5 Cr1 P5 -21.0(3) . . . . ? C4 C5 Cr1 P3 -32.3(4) . . . . ? C1 C5 Cr1 P3 85.8(3) . . . . ? C10 C5 Cr1 P3 -154.6(2) . . . . ? C4 C5 Cr1 P1 157.75(19) . . . . ? C1 C5 Cr1 P1 -84.1(2) . . . . ? C10 C5 Cr1 P1 35.5(3) . . . . ? C4 C5 Cr1 P4 48.4(2) . . . . ? C1 C5 Cr1 P4 166.52(18) . . . . ? C10 C5 Cr1 P4 -73.9(3) . . . . ? C4 C5 Cr1 P2 -148.98(17) . . . . ? C1 C5 Cr1 P2 -30.9(3) . . . . ? C10 C5 Cr1 P2 88.7(3) . . . . ? C4 C5 Cr1 Cr2 119.9(2) . . . . ? C1 C5 Cr1 Cr2 -122.0(2) . . . . ? C10 C5 Cr1 Cr2 -2.4(5) . . . . ? C3 Cr1 P1 P2 93.9(3) . . . . ? C2 Cr1 P1 P2 71.93(12) . . . . ? C1 Cr1 P1 P2 100.48(10) . . . . ? C4 Cr1 P1 P2 157.98(14) . . . . ? C5 Cr1 P1 P2 138.35(11) . . . . ? P5 Cr1 P1 P2 -132.37(6) . . . . ? P3 Cr1 P1 P2 -37.97(5) . . . . ? P4 Cr1 P1 P2 -94.31(5) . . . . ? Cr2 Cr1 P1 P2 -66.35(4) . . . . ? C3 Cr1 P1 P5 -133.7(3) . . . . ? C2 Cr1 P1 P5 -155.70(12) . . . . ? C1 Cr1 P1 P5 -127.15(10) . . . . ? C4 Cr1 P1 P5 -69.65(14) . . . . ? C5 Cr1 P1 P5 -89.28(11) . . . . ? P3 Cr1 P1 P5 94.40(5) . . . . ? P4 Cr1 P1 P5 38.06(5) . . . . ? P2 Cr1 P1 P5 132.37(6) . . . . ? Cr2 Cr1 P1 P5 66.02(4) . . . . ? C3 Cr1 P1 Cr2 160.3(3) . . . . ? C2 Cr1 P1 Cr2 138.28(11) . . . . ? C1 Cr1 P1 Cr2 166.83(10) . . . . ? C4 Cr1 P1 Cr2 -135.67(14) . . . . ? C5 Cr1 P1 Cr2 -155.30(10) . . . . ? P5 Cr1 P1 Cr2 -66.02(4) . . . . ? P3 Cr1 P1 Cr2 28.38(4) . . . . ? P4 Cr1 P1 Cr2 -27.95(4) . . . . ? P2 Cr1 P1 Cr2 66.35(4) . . . . ? P5 P1 P2 P3 0.31(8) . . . . ? Cr2 P1 P2 P3 -43.22(5) . . . . ? Cr1 P1 P2 P3 43.53(5) . . . . ? P5 P1 P2 Cr1 -43.22(5) . . . . ? Cr2 P1 P2 Cr1 -86.74(4) . . . . ? P5 P1 P2 Cr2 43.53(5) . . . . ? Cr1 P1 P2 Cr2 86.74(4) . . . . ? C3 Cr1 P2 P3 72.32(13) . . . . ? C2 Cr1 P2 P3 100.19(10) . . . . ? C1 Cr1 P2 P3 138.00(11) . . . . ? C4 Cr1 P2 P3 94.4(3) . . . . ? C5 Cr1 P2 P3 156.78(15) . . . . ? P5 Cr1 P2 P3 -94.01(5) . . . . ? P1 Cr1 P2 P3 -132.17(6) . . . . ? P4 Cr1 P2 P3 -37.80(5) . . . . ? Cr2 Cr1 P2 P3 -66.07(4) . . . . ? C3 Cr1 P2 P1 -155.51(13) . . . . ? C2 Cr1 P2 P1 -127.64(11) . . . . ? C1 Cr1 P2 P1 -89.83(11) . . . . ? C4 Cr1 P2 P1 -133.4(3) . . . . ? C5 Cr1 P2 P1 -71.05(15) . . . . ? P5 Cr1 P2 P1 38.16(5) . . . . ? P3 Cr1 P2 P1 132.17(6) . . . . ? P4 Cr1 P2 P1 94.37(5) . . . . ? Cr2 Cr1 P2 P1 66.10(4) . . . . ? C3 Cr1 P2 Cr2 138.39(13) . . . . ? C2 Cr1 P2 Cr2 166.26(10) . . . . ? C1 Cr1 P2 Cr2 -155.93(10) . . . . ? C4 Cr1 P2 Cr2 160.5(3) . . . . ? C5 Cr1 P2 Cr2 -137.15(14) . . . . ? P5 Cr1 P2 Cr2 -27.94(5) . . . . ? P3 Cr1 P2 Cr2 66.07(4) . . . . ? P1 Cr1 P2 Cr2 -66.10(4) . . . . ? P4 Cr1 P2 Cr2 28.27(4) . . . . ? P1 P2 P3 P4 -0.30(8) . . . . ? Cr1 P2 P3 P4 43.21(5) . . . . ? Cr2 P2 P3 P4 -43.52(5) . . . . ? P1 P2 P3 Cr2 43.23(5) . . . . ? Cr1 P2 P3 Cr2 86.73(4) . . . . ? P1 P2 P3 Cr1 -43.50(5) . . . . ? Cr2 P2 P3 Cr1 -86.73(4) . . . . ? C3 Cr1 P3 P2 -126.87(11) . . . . ? C2 Cr1 P3 P2 -89.19(11) . . . . ? C1 Cr1 P3 P2 -70.30(15) . . . . ? C4 Cr1 P3 P2 -154.97(12) . . . . ? C5 Cr1 P3 P2 -132.0(3) . . . . ? P5 Cr1 P3 P2 94.52(5) . . . . ? P1 Cr1 P3 P2 38.09(5) . . . . ? P4 Cr1 P3 P2 132.77(6) . . . . ? Cr2 Cr1 P3 P2 66.51(4) . . . . ? C3 Cr1 P3 P4 100.36(11) . . . . ? C2 Cr1 P3 P4 138.03(11) . . . . ? C1 Cr1 P3 P4 156.93(15) . . . . ? C4 Cr1 P3 P4 72.26(12) . . . . ? C5 Cr1 P3 P4 95.2(3) . . . . ? P5 Cr1 P3 P4 -38.25(5) . . . . ? P1 Cr1 P3 P4 -94.68(5) . . . . ? P2 Cr1 P3 P4 -132.77(6) . . . . ? Cr2 Cr1 P3 P4 -66.26(4) . . . . ? C3 Cr1 P3 Cr2 166.62(11) . . . . ? C2 Cr1 P3 Cr2 -155.71(11) . . . . ? C1 Cr1 P3 Cr2 -136.81(15) . . . . ? C4 Cr1 P3 Cr2 138.52(11) . . . . ? C5 Cr1 P3 Cr2 161.5(3) . . . . ? P5 Cr1 P3 Cr2 28.01(5) . . . . ? P1 Cr1 P3 Cr2 -28.42(5) . . . . ? P4 Cr1 P3 Cr2 66.26(4) . . . . ? P2 Cr1 P3 Cr2 -66.51(4) . . . . ? P2 P3 P4 P5 0.16(8) . . . . ? Cr2 P3 P4 P5 -43.48(5) . . . . ? Cr1 P3 P4 P5 43.50(5) . . . . ? P2 P3 P4 Cr1 -43.34(5) . . . . ? Cr2 P3 P4 Cr1 -86.98(4) . . . . ? P2 P3 P4 Cr2 43.64(5) . . . . ? Cr1 P3 P4 Cr2 86.98(4) . . . . ? C3 Cr1 P4 P5 138.87(10) . . . . ? C2 Cr1 P4 P5 158.20(14) . . . . ? C1 Cr1 P4 P5 97.1(3) . . . . ? C4 Cr1 P4 P5 100.84(10) . . . . ? C5 Cr1 P4 P5 73.69(12) . . . . ? P3 Cr1 P4 P5 -131.99(6) . . . . ? P1 Cr1 P4 P5 -38.21(5) . . . . ? P2 Cr1 P4 P5 -94.40(5) . . . . ? Cr2 Cr1 P4 P5 -66.12(4) . . . . ? C3 Cr1 P4 P3 -89.14(10) . . . . ? C2 Cr1 P4 P3 -69.81(14) . . . . ? C1 Cr1 P4 P3 -131.0(3) . . . . ? C4 Cr1 P4 P3 -127.16(10) . . . . ? C5 Cr1 P4 P3 -154.32(12) . . . . ? P5 Cr1 P4 P3 131.99(6) . . . . ? P1 Cr1 P4 P3 93.78(5) . . . . ? P2 Cr1 P4 P3 37.59(5) . . . . ? Cr2 Cr1 P4 P3 65.87(4) . . . . ? C3 Cr1 P4 Cr2 -155.01(10) . . . . ? C2 Cr1 P4 Cr2 -135.68(14) . . . . ? C1 Cr1 P4 Cr2 163.2(3) . . . . ? C4 Cr1 P4 Cr2 166.96(10) . . . . ? C5 Cr1 P4 Cr2 139.80(12) . . . . ? P5 Cr1 P4 Cr2 66.12(4) . . . . ? P3 Cr1 P4 Cr2 -65.87(4) . . . . ? P1 Cr1 P4 Cr2 27.91(4) . . . . ? P2 Cr1 P4 Cr2 -28.28(4) . . . . ? P3 P4 P5 P1 0.03(8) . . . . ? Cr1 P4 P5 P1 43.56(5) . . . . ? Cr2 P4 P5 P1 -43.34(5) . . . . ? P3 P4 P5 Cr1 -43.53(5) . . . . ? Cr2 P4 P5 Cr1 -86.90(4) . . . . ? P3 P4 P5 Cr2 43.37(5) . . . . ? Cr1 P4 P5 Cr2 86.90(4) . . . . ? P2 P1 P5 P4 -0.21(8) . . . . ? Cr2 P1 P5 P4 43.48(5) . . . . ? Cr1 P1 P5 P4 -43.64(5) . . . . ? P2 P1 P5 Cr1 43.42(5) . . . . ? Cr2 P1 P5 Cr1 87.11(4) . . . . ? P2 P1 P5 Cr2 -43.69(5) . . . . ? Cr1 P1 P5 Cr2 -87.11(4) . . . . ? C3 Cr1 P5 P4 -69.06(15) . . . . ? C2 Cr1 P5 P4 -131.0(3) . . . . ? C1 Cr1 P5 P4 -154.37(12) . . . . ? C4 Cr1 P5 P4 -88.75(10) . . . . ? C5 Cr1 P5 P4 -126.28(11) . . . . ? P3 Cr1 P5 P4 38.34(5) . . . . ? P1 Cr1 P5 P4 132.29(6) . . . . ? P2 Cr1 P5 P4 94.29(5) . . . . ? Cr2 Cr1 P5 P4 66.30(4) . . . . ? C3 Cr1 P5 P1 158.64(15) . . . . ? C2 Cr1 P5 P1 96.7(3) . . . . ? C1 Cr1 P5 P1 73.34(13) . . . . ? C4 Cr1 P5 P1 138.96(10) . . . . ? C5 Cr1 P5 P1 101.42(11) . . . . ? P3 Cr1 P5 P1 -93.95(5) . . . . ? P4 Cr1 P5 P1 -132.29(6) . . . . ? P2 Cr1 P5 P1 -38.00(5) . . . . ? Cr2 Cr1 P5 P1 -65.99(4) . . . . ? C3 Cr1 P5 Cr2 -135.36(15) . . . . ? C2 Cr1 P5 Cr2 162.7(3) . . . . ? C1 Cr1 P5 Cr2 139.33(12) . . . . ? C4 Cr1 P5 Cr2 -155.04(10) . . . . ? C5 Cr1 P5 Cr2 167.42(10) . . . . ? P3 Cr1 P5 Cr2 -27.96(5) . . . . ? P1 Cr1 P5 Cr2 65.99(4) . . . . ? P4 Cr1 P5 Cr2 -66.30(4) . . . . ? P2 Cr1 P5 Cr2 28.00(5) . . . . ? P2 P3 Cr2 C12 86.80(12) . . . . ? P4 P3 Cr2 C12 -140.72(12) . . . . ? Cr1 P3 Cr2 C12 153.18(11) . . . . ? P2 P3 Cr2 C11 70.83(16) . . . . ? P4 P3 Cr2 C11 -156.69(16) . . . . ? Cr1 P3 Cr2 C11 137.21(16) . . . . ? P2 P3 Cr2 C14 153.93(12) . . . . ? P4 P3 Cr2 C14 -73.58(12) . . . . ? Cr1 P3 Cr2 C14 -139.68(11) . . . . ? P2 P3 Cr2 C15 142.0(3) . . . . ? P4 P3 Cr2 C15 -85.5(3) . . . . ? Cr1 P3 Cr2 C15 -151.6(3) . . . . ? P2 P3 Cr2 C13 124.16(10) . . . . ? P4 P3 Cr2 C13 -103.36(10) . . . . ? Cr1 P3 Cr2 C13 -169.46(10) . . . . ? P2 P3 Cr2 P5 -94.34(5) . . . . ? P4 P3 Cr2 P5 38.15(5) . . . . ? Cr1 P3 Cr2 P5 -27.95(5) . . . . ? P2 P3 Cr2 P1 -37.92(5) . . . . ? P4 P3 Cr2 P1 94.57(5) . . . . ? Cr1 P3 Cr2 P1 28.47(5) . . . . ? P2 P3 Cr2 P4 -132.49(5) . . . . ? Cr1 P3 Cr2 P4 -66.10(4) . . . . ? P4 P3 Cr2 P2 132.49(5) . . . . ? Cr1 P3 Cr2 P2 66.39(4) . . . . ? P2 P3 Cr2 Cr1 -66.39(4) . . . . ? P4 P3 Cr2 Cr1 66.10(4) . . . . ? P4 P5 Cr2 C12 138.9(3) . . . . ? P1 P5 Cr2 C12 -88.6(3) . . . . ? Cr1 P5 Cr2 C12 -154.8(3) . . . . ? P4 P5 Cr2 C11 152.61(12) . . . . ? P1 P5 Cr2 C11 -74.93(12) . . . . ? Cr1 P5 Cr2 C11 -141.08(11) . . . . ? P4 P5 Cr2 C14 86.25(11) . . . . ? P1 P5 Cr2 C14 -141.28(11) . . . . ? Cr1 P5 Cr2 C14 152.57(10) . . . . ? P4 P5 Cr2 C15 123.12(11) . . . . ? P1 P5 Cr2 C15 -104.41(11) . . . . ? Cr1 P5 Cr2 C15 -170.56(10) . . . . ? P4 P5 Cr2 C13 70.32(16) . . . . ? P1 P5 Cr2 C13 -157.22(16) . . . . ? Cr1 P5 Cr2 C13 136.63(16) . . . . ? P4 P5 Cr2 P3 -38.29(5) . . . . ? P1 P5 Cr2 P3 94.17(5) . . . . ? Cr1 P5 Cr2 P3 28.02(5) . . . . ? P4 P5 Cr2 P1 -132.47(6) . . . . ? Cr1 P5 Cr2 P1 -66.15(4) . . . . ? P1 P5 Cr2 P4 132.47(6) . . . . ? Cr1 P5 Cr2 P4 66.31(4) . . . . ? P4 P5 Cr2 P2 -94.29(5) . . . . ? P1 P5 Cr2 P2 38.18(5) . . . . ? Cr1 P5 Cr2 P2 -27.97(5) . . . . ? P4 P5 Cr2 Cr1 -66.31(4) . . . . ? P1 P5 Cr2 Cr1 66.15(4) . . . . ? P2 P1 Cr2 C12 -74.97(12) . . . . ? P5 P1 Cr2 C12 152.92(12) . . . . ? Cr1 P1 Cr2 C12 -141.25(12) . . . . ? P2 P1 Cr2 C11 -104.81(10) . . . . ? P5 P1 Cr2 C11 123.09(10) . . . . ? Cr1 P1 Cr2 C11 -171.09(10) . . . . ? P2 P1 Cr2 C14 -158.04(16) . . . . ? P5 P1 Cr2 C14 69.86(16) . . . . ? Cr1 P1 Cr2 C14 135.68(15) . . . . ? P2 P1 Cr2 C15 -142.13(10) . . . . ? P5 P1 Cr2 C15 85.76(10) . . . . ? Cr1 P1 Cr2 C15 151.59(10) . . . . ? P2 P1 Cr2 C13 -89.2(3) . . . . ? P5 P1 Cr2 C13 138.7(3) . . . . ? Cr1 P1 Cr2 C13 -155.5(3) . . . . ? P2 P1 Cr2 P3 37.82(5) . . . . ? P5 P1 Cr2 P3 -94.28(5) . . . . ? Cr1 P1 Cr2 P3 -28.45(4) . . . . ? P2 P1 Cr2 P5 132.10(6) . . . . ? Cr1 P1 Cr2 P5 65.82(4) . . . . ? P2 P1 Cr2 P4 94.21(5) . . . . ? P5 P1 Cr2 P4 -37.90(5) . . . . ? Cr1 P1 Cr2 P4 27.93(4) . . . . ? P5 P1 Cr2 P2 -132.10(6) . . . . ? Cr1 P1 Cr2 P2 -66.28(4) . . . . ? P2 P1 Cr2 Cr1 66.28(4) . . . . ? P5 P1 Cr2 Cr1 -65.82(4) . . . . ? P5 P4 Cr2 C12 -156.45(17) . . . . ? P3 P4 Cr2 C12 71.48(17) . . . . ? Cr1 P4 Cr2 C12 137.55(16) . . . . ? P5 P4 Cr2 C11 -87.3(3) . . . . ? P3 P4 Cr2 C11 140.6(3) . . . . ? Cr1 P4 Cr2 C11 -153.3(3) . . . . ? P5 P4 Cr2 C14 -103.79(10) . . . . ? P3 P4 Cr2 C14 124.13(10) . . . . ? Cr1 P4 Cr2 C14 -169.80(10) . . . . ? P5 P4 Cr2 C15 -73.90(12) . . . . ? P3 P4 Cr2 C15 154.02(12) . . . . ? Cr1 P4 Cr2 C15 -139.91(11) . . . . ? P5 P4 Cr2 C13 -140.58(10) . . . . ? P3 P4 Cr2 C13 87.34(10) . . . . ? Cr1 P4 Cr2 C13 153.41(10) . . . . ? P5 P4 Cr2 P3 132.08(6) . . . . ? Cr1 P4 Cr2 P3 66.07(4) . . . . ? P3 P4 Cr2 P5 -132.08(6) . . . . ? Cr1 P4 Cr2 P5 -66.00(4) . . . . ? P5 P4 Cr2 P1 38.07(5) . . . . ? P3 P4 Cr2 P1 -94.01(5) . . . . ? Cr1 P4 Cr2 P1 -27.93(4) . . . . ? P5 P4 Cr2 P2 94.27(5) . . . . ? P3 P4 Cr2 P2 -37.81(5) . . . . ? Cr1 P4 Cr2 P2 28.26(4) . . . . ? P5 P4 Cr2 Cr1 66.00(4) . . . . ? P3 P4 Cr2 Cr1 -66.07(4) . . . . ? P3 P2 Cr2 C12 -104.27(11) . . . . ? P1 P2 Cr2 C12 123.29(11) . . . . ? Cr1 P2 Cr2 C12 -170.52(11) . . . . ? P3 P2 Cr2 C11 -141.33(11) . . . . ? P1 P2 Cr2 C11 86.22(11) . . . . ? Cr1 P2 Cr2 C11 152.42(10) . . . . ? P3 P2 Cr2 C14 -87.3(3) . . . . ? P1 P2 Cr2 C14 140.3(3) . . . . ? Cr1 P2 Cr2 C14 -153.5(3) . . . . ? P3 P2 Cr2 C15 -158.27(15) . . . . ? P1 P2 Cr2 C15 69.29(16) . . . . ? Cr1 P2 Cr2 C15 135.48(15) . . . . ? P3 P2 Cr2 C13 -74.18(12) . . . . ? P1 P2 Cr2 C13 153.38(12) . . . . ? Cr1 P2 Cr2 C13 -140.43(12) . . . . ? P1 P2 Cr2 P3 -132.44(6) . . . . ? Cr1 P2 Cr2 P3 -66.25(4) . . . . ? P3 P2 Cr2 P5 94.13(5) . . . . ? P1 P2 Cr2 P5 -38.32(5) . . . . ? Cr1 P2 Cr2 P5 27.87(5) . . . . ? P3 P2 Cr2 P1 132.44(6) . . . . ? Cr1 P2 Cr2 P1 66.19(4) . . . . ? P3 P2 Cr2 P4 38.02(5) . . . . ? P1 P2 Cr2 P4 -94.43(5) . . . . ? Cr1 P2 Cr2 P4 -28.24(4) . . . . ? P3 P2 Cr2 Cr1 66.25(4) . . . . ? P1 P2 Cr2 Cr1 -66.19(4) . . . . ? C3 Cr1 Cr2 C12 -78.3(3) . . . . ? C2 Cr1 Cr2 C12 -7.5(3) . . . . ? C1 Cr1 Cr2 C12 64.9(3) . . . . ? C4 Cr1 Cr2 C12 -150.0(3) . . . . ? C5 Cr1 Cr2 C12 138.4(3) . . . . ? P5 Cr1 Cr2 C12 161.9(2) . . . . ? P3 Cr1 Cr2 C12 -53.9(2) . . . . ? P1 Cr1 Cr2 C12 89.6(2) . . . . ? P4 Cr1 Cr2 C12 -126.1(2) . . . . ? P2 Cr1 Cr2 C12 17.7(2) . . . . ? C3 Cr1 Cr2 C11 -151.4(3) . . . . ? C2 Cr1 Cr2 C11 -80.5(3) . . . . ? C1 Cr1 Cr2 C11 -8.1(3) . . . . ? C4 Cr1 Cr2 C11 136.9(2) . . . . ? C5 Cr1 Cr2 C11 65.3(3) . . . . ? P5 Cr1 Cr2 C11 88.87(18) . . . . ? P3 Cr1 Cr2 C11 -127.02(18) . . . . ? P1 Cr1 Cr2 C11 16.51(18) . . . . ? P4 Cr1 Cr2 C11 160.78(18) . . . . ? P2 Cr1 Cr2 C11 -55.37(18) . . . . ? C3 Cr1 Cr2 C14 66.3(3) . . . . ? C2 Cr1 Cr2 C14 137.2(3) . . . . ? C1 Cr1 Cr2 C14 -150.4(2) . . . . ? C4 Cr1 Cr2 C14 -5.4(3) . . . . ? C5 Cr1 Cr2 C14 -77.0(3) . . . . ? P5 Cr1 Cr2 C14 -53.42(18) . . . . ? P3 Cr1 Cr2 C14 90.70(18) . . . . ? P1 Cr1 Cr2 C14 -125.78(18) . . . . ? P4 Cr1 Cr2 C14 18.50(18) . . . . ? P2 Cr1 Cr2 C14 162.34(18) . . . . ? C3 Cr1 Cr2 C15 136.7(2) . . . . ? C2 Cr1 Cr2 C15 -152.4(3) . . . . ? C1 Cr1 Cr2 C15 -80.0(3) . . . . ? C4 Cr1 Cr2 C15 65.0(3) . . . . ? C5 Cr1 Cr2 C15 -6.6(3) . . . . ? P5 Cr1 Cr2 C15 16.98(18) . . . . ? P3 Cr1 Cr2 C15 161.10(18) . . . . ? P1 Cr1 Cr2 C15 -55.38(18) . . . . ? P4 Cr1 Cr2 C15 88.89(18) . . . . ? P2 Cr1 Cr2 C15 -127.26(18) . . . . ? C3 Cr1 Cr2 C13 -4.9(3) . . . . ? C2 Cr1 Cr2 C13 66.0(3) . . . . ? C1 Cr1 Cr2 C13 138.4(2) . . . . ? C4 Cr1 Cr2 C13 -76.6(3) . . . . ? C5 Cr1 Cr2 C13 -148.2(3) . . . . ? P5 Cr1 Cr2 C13 -124.62(18) . . . . ? P3 Cr1 Cr2 C13 19.50(18) . . . . ? P1 Cr1 Cr2 C13 163.02(18) . . . . ? P4 Cr1 Cr2 C13 -52.70(18) . . . . ? P2 Cr1 Cr2 C13 91.15(18) . . . . ? C3 Cr1 Cr2 P3 -24.37(18) . . . . ? C2 Cr1 Cr2 P3 46.48(19) . . . . ? C1 Cr1 Cr2 P3 118.88(18) . . . . ? C4 Cr1 Cr2 P3 -96.08(18) . . . . ? C5 Cr1 Cr2 P3 -167.70(19) . . . . ? P5 Cr1 Cr2 P3 -144.12(6) . . . . ? P1 Cr1 Cr2 P3 143.52(6) . . . . ? P4 Cr1 Cr2 P3 -72.20(6) . . . . ? P2 Cr1 Cr2 P3 71.64(6) . . . . ? C3 Cr1 Cr2 P5 119.75(18) . . . . ? C2 Cr1 Cr2 P5 -169.40(19) . . . . ? C1 Cr1 Cr2 P5 -97.00(18) . . . . ? C4 Cr1 Cr2 P5 48.04(18) . . . . ? C5 Cr1 Cr2 P5 -23.58(19) . . . . ? P3 Cr1 Cr2 P5 144.12(6) . . . . ? P1 Cr1 Cr2 P5 -72.36(6) . . . . ? P4 Cr1 Cr2 P5 71.92(6) . . . . ? P2 Cr1 Cr2 P5 -144.24(6) . . . . ? C3 Cr1 Cr2 P1 -167.89(19) . . . . ? C2 Cr1 Cr2 P1 -97.04(19) . . . . ? C1 Cr1 Cr2 P1 -24.64(18) . . . . ? C4 Cr1 Cr2 P1 120.40(18) . . . . ? C5 Cr1 Cr2 P1 48.78(19) . . . . ? P5 Cr1 Cr2 P1 72.36(6) . . . . ? P3 Cr1 Cr2 P1 -143.52(6) . . . . ? P4 Cr1 Cr2 P1 144.28(6) . . . . ? P2 Cr1 Cr2 P1 -71.88(6) . . . . ? C3 Cr1 Cr2 P4 47.83(18) . . . . ? C2 Cr1 Cr2 P4 118.68(19) . . . . ? C1 Cr1 Cr2 P4 -168.92(18) . . . . ? C4 Cr1 Cr2 P4 -23.88(18) . . . . ? C5 Cr1 Cr2 P4 -95.49(19) . . . . ? P5 Cr1 Cr2 P4 -71.92(6) . . . . ? P3 Cr1 Cr2 P4 72.20(6) . . . . ? P1 Cr1 Cr2 P4 -144.28(6) . . . . ? P2 Cr1 Cr2 P4 143.85(6) . . . . ? C3 Cr1 Cr2 P2 -96.02(18) . . . . ? C2 Cr1 Cr2 P2 -25.16(19) . . . . ? C1 Cr1 Cr2 P2 47.24(18) . . . . ? C4 Cr1 Cr2 P2 -167.72(18) . . . . ? C5 Cr1 Cr2 P2 120.66(19) . . . . ? P5 Cr1 Cr2 P2 144.24(6) . . . . ? P3 Cr1 Cr2 P2 -71.64(6) . . . . ? P1 Cr1 Cr2 P2 71.88(6) . . . . ? P4 Cr1 Cr2 P2 -143.85(6) . . . . ? C14 Cr2 C11 C12 -80.3(2) . . . . ? C15 Cr2 C11 C12 -118.0(3) . . . . ? C13 Cr2 C11 C12 -38.0(2) . . . . ? P3 Cr2 C11 C12 25.8(3) . . . . ? P5 Cr2 C11 C12 -171.24(19) . . . . ? P1 Cr2 C11 C12 135.4(2) . . . . ? P4 Cr2 C11 C12 -98.8(3) . . . . ? P2 Cr2 C11 C12 79.6(2) . . . . ? Cr1 Cr2 C11 C12 122.3(2) . . . . ? C12 Cr2 C11 C15 118.0(3) . . . . ? C14 Cr2 C11 C15 37.8(2) . . . . ? C13 Cr2 C11 C15 80.1(2) . . . . ? P3 Cr2 C11 C15 143.85(18) . . . . ? P5 Cr2 C11 C15 -53.2(2) . . . . ? P1 Cr2 C11 C15 -106.6(2) . . . . ? P4 Cr2 C11 C15 19.2(4) . . . . ? P2 Cr2 C11 C15 -162.41(19) . . . . ? Cr1 Cr2 C11 C15 -119.7(2) . . . . ? C12 Cr2 C11 C16 -119.8(4) . . . . ? C14 Cr2 C11 C16 159.9(4) . . . . ? C15 Cr2 C11 C16 122.2(4) . . . . ? C13 Cr2 C11 C16 -157.8(4) . . . . ? P3 Cr2 C11 C16 -94.0(3) . . . . ? P5 Cr2 C11 C16 68.9(3) . . . . ? P1 Cr2 C11 C16 15.5(3) . . . . ? P4 Cr2 C11 C16 141.4(3) . . . . ? P2 Cr2 C11 C16 -40.3(3) . . . . ? Cr1 Cr2 C11 C16 2.4(4) . . . . ? C15 C11 C12 C13 0.6(4) . . . . ? C16 C11 C12 C13 -175.4(3) . . . . ? Cr2 C11 C12 C13 62.5(3) . . . . ? C15 C11 C12 C17 176.2(3) . . . . ? C16 C11 C12 C17 0.1(6) . . . . ? Cr2 C11 C12 C17 -122.0(4) . . . . ? C15 C11 C12 Cr2 -61.9(2) . . . . ? C16 C11 C12 Cr2 122.1(4) . . . . ? C14 Cr2 C12 C11 79.6(2) . . . . ? C15 Cr2 C12 C11 37.3(2) . . . . ? C13 Cr2 C12 C11 116.8(3) . . . . ? P3 Cr2 C12 C11 -163.27(19) . . . . ? P5 Cr2 C12 C11 19.6(4) . . . . ? P1 Cr2 C12 C11 -54.3(2) . . . . ? P4 Cr2 C12 C11 142.43(18) . . . . ? P2 Cr2 C12 C11 -107.6(2) . . . . ? Cr1 Cr2 C12 C11 -121.6(2) . . . . ? C11 Cr2 C12 C13 -116.8(3) . . . . ? C14 Cr2 C12 C13 -37.3(2) . . . . ? C15 Cr2 C12 C13 -79.6(2) . . . . ? P3 Cr2 C12 C13 79.9(2) . . . . ? P5 Cr2 C12 C13 -97.2(3) . . . . ? P1 Cr2 C12 C13 -171.16(18) . . . . ? P4 Cr2 C12 C13 25.6(3) . . . . ? P2 Cr2 C12 C13 135.6(2) . . . . ? Cr1 Cr2 C12 C13 121.5(2) . . . . ? C11 Cr2 C12 C17 122.1(4) . . . . ? C14 Cr2 C12 C17 -158.3(4) . . . . ? C15 Cr2 C12 C17 159.4(4) . . . . ? C13 Cr2 C12 C17 -121.1(4) . . . . ? P3 Cr2 C12 C17 -41.2(4) . . . . ? P5 Cr2 C12 C17 141.7(3) . . . . ? P1 Cr2 C12 C17 67.8(4) . . . . ? P4 Cr2 C12 C17 -95.5(4) . . . . ? P2 Cr2 C12 C17 14.6(3) . . . . ? Cr1 Cr2 C12 C17 0.5(5) . . . . ? C11 C12 C13 C14 -0.5(4) . . . . ? C17 C12 C13 C14 -176.1(3) . . . . ? Cr2 C12 C13 C14 61.9(2) . . . . ? C11 C12 C13 C18 175.1(3) . . . . ? C17 C12 C13 C18 -0.5(6) . . . . ? Cr2 C12 C13 C18 -122.5(4) . . . . ? C11 C12 C13 Cr2 -62.4(2) . . . . ? C17 C12 C13 Cr2 122.0(4) . . . . ? C12 Cr2 C13 C14 -117.5(3) . . . . ? C11 Cr2 C13 C14 -79.8(2) . . . . ? C15 Cr2 C13 C14 -37.1(2) . . . . ? P3 Cr2 C13 C14 135.3(2) . . . . ? P5 Cr2 C13 C14 26.0(3) . . . . ? P1 Cr2 C13 C14 -97.3(3) . . . . ? P4 Cr2 C13 C14 79.2(2) . . . . ? P2 Cr2 C13 C14 -171.90(18) . . . . ? Cr1 Cr2 C13 C14 119.9(2) . . . . ? C11 Cr2 C13 C12 37.7(2) . . . . ? C14 Cr2 C13 C12 117.5(3) . . . . ? C15 Cr2 C13 C12 80.4(2) . . . . ? P3 Cr2 C13 C12 -107.2(2) . . . . ? P5 Cr2 C13 C12 143.48(19) . . . . ? P1 Cr2 C13 C12 20.2(4) . . . . ? P4 Cr2 C13 C12 -163.30(19) . . . . ? P2 Cr2 C13 C12 -54.4(2) . . . . ? Cr1 Cr2 C13 C12 -122.6(2) . . . . ? C12 Cr2 C13 C18 120.9(4) . . . . ? C11 Cr2 C13 C18 158.6(4) . . . . ? C14 Cr2 C13 C18 -121.6(4) . . . . ? C15 Cr2 C13 C18 -158.7(4) . . . . ? P3 Cr2 C13 C18 13.7(3) . . . . ? P5 Cr2 C13 C18 -95.6(3) . . . . ? P1 Cr2 C13 C18 141.1(3) . . . . ? P4 Cr2 C13 C18 -42.4(3) . . . . ? P2 Cr2 C13 C18 66.5(3) . . . . ? Cr1 Cr2 C13 C18 -1.7(4) . . . . ? C12 C13 C14 C15 0.3(4) . . . . ? C18 C13 C14 C15 -175.4(3) . . . . ? Cr2 C13 C14 C15 61.9(2) . . . . ? C12 C13 C14 C19 177.5(3) . . . . ? C18 C13 C14 C19 1.9(6) . . . . ? Cr2 C13 C14 C19 -120.9(4) . . . . ? C12 C13 C14 Cr2 -61.7(2) . . . . ? C18 C13 C14 Cr2 122.7(4) . . . . ? C12 Cr2 C14 C13 37.7(2) . . . . ? C11 Cr2 C14 C13 80.1(2) . . . . ? C15 Cr2 C14 C13 118.1(3) . . . . ? P3 Cr2 C14 C13 -54.4(2) . . . . ? P5 Cr2 C14 C13 -162.8(2) . . . . ? P1 Cr2 C14 C13 143.94(19) . . . . ? P4 Cr2 C14 C13 -107.2(2) . . . . ? P2 Cr2 C14 C13 18.6(4) . . . . ? Cr1 Cr2 C14 C13 -121.8(2) . . . . ? C12 Cr2 C14 C15 -80.5(2) . . . . ? C11 Cr2 C14 C15 -38.0(2) . . . . ? C13 Cr2 C14 C15 -118.1(3) . . . . ? P3 Cr2 C14 C15 -172.54(17) . . . . ? P5 Cr2 C14 C15 79.1(2) . . . . ? P1 Cr2 C14 C15 25.8(3) . . . . ? P4 Cr2 C14 C15 134.70(19) . . . . ? P2 Cr2 C14 C15 -99.5(3) . . . . ? Cr1 Cr2 C14 C15 120.1(2) . . . . ? C12 Cr2 C14 C19 159.0(4) . . . . ? C11 Cr2 C14 C19 -158.6(4) . . . . ? C15 Cr2 C14 C19 -120.6(4) . . . . ? C13 Cr2 C14 C19 121.3(4) . . . . ? P3 Cr2 C14 C19 66.9(3) . . . . ? P5 Cr2 C14 C19 -41.5(3) . . . . ? P1 Cr2 C14 C19 -94.8(3) . . . . ? P4 Cr2 C14 C19 14.1(3) . . . . ? P2 Cr2 C14 C19 139.9(3) . . . . ? Cr1 Cr2 C14 C19 -0.5(4) . . . . ? C13 C14 C15 C11 0.1(4) . . . . ? C19 C14 C15 C11 -177.1(3) . . . . ? Cr2 C14 C15 C11 62.1(2) . . . . ? C13 C14 C15 C20 177.1(3) . . . . ? C19 C14 C15 C20 -0.1(6) . . . . ? Cr2 C14 C15 C20 -120.9(4) . . . . ? C13 C14 C15 Cr2 -62.0(2) . . . . ? C19 C14 C15 Cr2 120.7(4) . . . . ? C12 C11 C15 C14 -0.4(4) . . . . ? C16 C11 C15 C14 175.5(3) . . . . ? Cr2 C11 C15 C14 -62.3(2) . . . . ? C12 C11 C15 C20 -177.4(3) . . . . ? C16 C11 C15 C20 -1.4(6) . . . . ? Cr2 C11 C15 C20 120.8(4) . . . . ? C12 C11 C15 Cr2 61.8(3) . . . . ? C16 C11 C15 Cr2 -122.2(4) . . . . ? C12 Cr2 C15 C14 79.6(2) . . . . ? C11 Cr2 C15 C14 116.7(3) . . . . ? C13 Cr2 C15 C14 37.0(2) . . . . ? P3 Cr2 C15 C14 17.0(4) . . . . ? P5 Cr2 C15 C14 -107.21(19) . . . . ? P1 Cr2 C15 C14 -163.10(18) . . . . ? P4 Cr2 C15 C14 -54.6(2) . . . . ? P2 Cr2 C15 C14 144.04(18) . . . . ? Cr1 Cr2 C15 C14 -120.6(2) . . . . ? C12 Cr2 C15 C11 -37.1(2) . . . . ? C14 Cr2 C15 C11 -116.7(3) . . . . ? C13 Cr2 C15 C11 -79.7(2) . . . . ? P3 Cr2 C15 C11 -99.7(3) . . . . ? P5 Cr2 C15 C11 136.1(2) . . . . ? P1 Cr2 C15 C11 80.2(2) . . . . ? P4 Cr2 C15 C11 -171.33(18) . . . . ? P2 Cr2 C15 C11 27.3(3) . . . . ? Cr1 Cr2 C15 C11 122.6(2) . . . . ? C12 Cr2 C15 C20 -159.3(4) . . . . ? C11 Cr2 C15 C20 -122.3(4) . . . . ? C14 Cr2 C15 C20 121.0(4) . . . . ? C13 Cr2 C15 C20 158.0(4) . . . . ? P3 Cr2 C15 C20 138.0(3) . . . . ? P5 Cr2 C15 C20 13.8(3) . . . . ? P1 Cr2 C15 C20 -42.1(3) . . . . ? P4 Cr2 C15 C20 66.4(3) . . . . ? P2 Cr2 C15 C20 -94.9(3) . . . . ? Cr1 Cr2 C15 C20 0.4(4) . . . . ? C25 C21 C22 C23 0.0(5) . . . . ? C26 C21 C22 C23 175.7(4) . . . . ? Cr3 C21 C22 C23 -61.5(3) . . . . ? C25 C21 C22 C27 -176.2(4) . . . . ? C26 C21 C22 C27 -0.5(7) . . . . ? Cr3 C21 C22 C27 122.3(4) . . . . ? C25 C21 C22 Cr3 61.4(3) . . . . ? C26 C21 C22 Cr3 -122.9(4) . . . . ? C21 C22 C23 C24 0.2(5) . . . . ? C27 C22 C23 C24 176.5(4) . . . . ? Cr3 C22 C23 C24 -61.6(3) . . . . ? C21 C22 C23 C28 -176.3(4) . . . . ? C27 C22 C23 C28 0.0(6) . . . . ? Cr3 C22 C23 C28 121.8(4) . . . . ? C21 C22 C23 Cr3 61.9(3) . . . . ? C27 C22 C23 Cr3 -121.9(4) . . . . ? C22 C23 C24 C25 -0.3(4) . . . . ? C28 C23 C24 C25 176.2(4) . . . . ? Cr3 C23 C24 C25 -62.4(3) . . . . ? C22 C23 C24 C29 -175.1(4) . . . . ? C28 C23 C24 C29 1.4(6) . . . . ? Cr3 C23 C24 C29 122.8(4) . . . . ? C22 C23 C24 Cr3 62.1(3) . . . . ? C28 C23 C24 Cr3 -121.4(4) . . . . ? C22 C21 C25 C24 -0.2(5) . . . . ? C26 C21 C25 C24 -176.0(4) . . . . ? Cr3 C21 C25 C24 61.4(3) . . . . ? C22 C21 C25 C30 176.0(4) . . . . ? C26 C21 C25 C30 0.2(6) . . . . ? Cr3 C21 C25 C30 -122.4(4) . . . . ? C22 C21 C25 Cr3 -61.6(3) . . . . ? C26 C21 C25 Cr3 122.6(4) . . . . ? C23 C24 C25 C21 0.3(4) . . . . ? C29 C24 C25 C21 175.0(4) . . . . ? Cr3 C24 C25 C21 -62.2(3) . . . . ? C23 C24 C25 C30 -175.9(4) . . . . ? C29 C24 C25 C30 -1.2(6) . . . . ? Cr3 C24 C25 C30 121.6(4) . . . . ? C23 C24 C25 Cr3 62.5(3) . . . . ? C29 C24 C25 Cr3 -122.8(4) . . . . ? C25 C24 Cr3 C23 116.7(3) . . . . ? C29 C24 Cr3 C23 -120.9(5) . . . . ? C23 C24 Cr3 C25 -116.7(3) . . . . ? C29 C24 Cr3 C25 122.4(4) . . . . ? C23 C24 Cr3 C22 -37.3(2) . . . . ? C25 C24 Cr3 C22 79.3(2) . . . . ? C29 C24 Cr3 C22 -158.2(4) . . . . ? C23 C24 Cr3 C21 -79.7(2) . . . . ? C25 C24 Cr3 C21 37.0(2) . . . . ? C29 C24 Cr3 C21 159.4(4) . . . . ? C23 C24 Cr3 P6 -137.1(2) . . . . ? C25 C24 Cr3 P6 -20.5(3) . . . . ? C29 C24 Cr3 P6 102.0(4) . . . . ? C23 C24 Cr3 P10 170.03(19) . . . . ? C25 C24 Cr3 P10 -73.3(2) . . . . ? C29 C24 Cr3 P10 49.1(4) . . . . ? C23 C24 Cr3 P8 64.9(2) . . . . ? C25 C24 Cr3 P8 -178.40(17) . . . . ? C29 C24 Cr3 P8 -56.0(4) . . . . ? C23 C24 Cr3 P9 116.8(2) . . . . ? C25 C24 Cr3 P9 -126.56(19) . . . . ? C29 C24 Cr3 P9 -4.1(4) . . . . ? C23 C24 Cr3 P7 8.3(4) . . . . ? C25 C24 Cr3 P7 125.0(3) . . . . ? C29 C24 Cr3 P7 -112.6(3) . . . . ? C22 C23 Cr3 C24 -117.7(3) . . . . ? C28 C23 Cr3 C24 121.3(4) . . . . ? C22 C23 Cr3 C25 -79.4(2) . . . . ? C24 C23 Cr3 C25 38.3(2) . . . . ? C28 C23 Cr3 C25 159.7(4) . . . . ? C24 C23 Cr3 C22 117.7(3) . . . . ? C28 C23 Cr3 C22 -121.0(4) . . . . ? C22 C23 Cr3 C21 -37.1(2) . . . . ? C24 C23 Cr3 C21 80.6(2) . . . . ? C28 C23 Cr3 C21 -158.1(4) . . . . ? C22 C23 Cr3 P6 4.9(4) . . . . ? C24 C23 Cr3 P6 122.6(3) . . . . ? C28 C23 Cr3 P6 -116.0(3) . . . . ? C22 C23 Cr3 P10 -135.3(2) . . . . ? C24 C23 Cr3 P10 -17.6(3) . . . . ? C28 C23 Cr3 P10 103.7(3) . . . . ? C22 C23 Cr3 P8 117.6(2) . . . . ? C24 C23 Cr3 P8 -124.7(2) . . . . ? C28 C23 Cr3 P8 -3.4(3) . . . . ? C22 C23 Cr3 P9 170.6(2) . . . . ? C24 C23 Cr3 P9 -71.7(2) . . . . ? C28 C23 Cr3 P9 49.6(3) . . . . ? C22 C23 Cr3 P7 66.2(2) . . . . ? C24 C23 Cr3 P7 -176.09(18) . . . . ? C28 C23 Cr3 P7 -54.8(3) . . . . ? C21 C25 Cr3 C24 117.8(3) . . . . ? C30 C25 Cr3 C24 -120.3(4) . . . . ? C21 C25 Cr3 C23 80.0(2) . . . . ? C24 C25 Cr3 C23 -37.8(2) . . . . ? C30 C25 Cr3 C23 -158.2(4) . . . . ? C21 C25 Cr3 C22 37.5(2) . . . . ? C24 C25 Cr3 C22 -80.3(2) . . . . ? C30 C25 Cr3 C22 159.4(4) . . . . ? C24 C25 Cr3 C21 -117.8(3) . . . . ? C30 C25 Cr3 C21 121.9(4) . . . . ? C21 C25 Cr3 P6 -73.4(2) . . . . ? C24 C25 Cr3 P6 168.77(18) . . . . ? C30 C25 Cr3 P6 48.4(3) . . . . ? C21 C25 Cr3 P10 -126.6(2) . . . . ? C24 C25 Cr3 P10 115.63(19) . . . . ? C30 C25 Cr3 P10 -4.7(3) . . . . ? C21 C25 Cr3 P8 121.1(3) . . . . ? C24 C25 Cr3 P8 3.3(4) . . . . ? C30 C25 Cr3 P8 -117.0(3) . . . . ? C21 C25 Cr3 P9 -179.00(19) . . . . ? C24 C25 Cr3 P9 63.2(2) . . . . ? C30 C25 Cr3 P9 -57.1(3) . . . . ? C21 C25 Cr3 P7 -19.6(3) . . . . ? C24 C25 Cr3 P7 -137.5(2) . . . . ? C30 C25 Cr3 P7 102.2(3) . . . . ? C23 C22 Cr3 C24 37.5(2) . . . . ? C21 C22 Cr3 C24 -80.6(2) . . . . ? C27 C22 Cr3 C24 157.4(4) . . . . ? C21 C22 Cr3 C23 -118.1(3) . . . . ? C27 C22 Cr3 C23 119.9(4) . . . . ? C23 C22 Cr3 C25 80.7(2) . . . . ? C21 C22 Cr3 C25 -37.4(2) . . . . ? C27 C22 Cr3 C25 -159.4(4) . . . . ? C23 C22 Cr3 C21 118.1(3) . . . . ? C27 C22 Cr3 C21 -122.0(4) . . . . ? C23 C22 Cr3 P6 -177.67(19) . . . . ? C21 C22 Cr3 P6 64.2(2) . . . . ? C27 C22 Cr3 P6 -57.8(4) . . . . ? C23 C22 Cr3 P10 119.7(3) . . . . ? C21 C22 Cr3 P10 1.6(4) . . . . ? C27 C22 Cr3 P10 -120.4(3) . . . . ? C23 C22 Cr3 P8 -71.3(2) . . . . ? C21 C22 Cr3 P8 170.62(19) . . . . ? C27 C22 Cr3 P8 48.7(3) . . . . ? C23 C22 Cr3 P9 -16.5(3) . . . . ? C21 C22 Cr3 P9 -134.6(2) . . . . ? C27 C22 Cr3 P9 103.4(3) . . . . ? C23 C22 Cr3 P7 -124.9(2) . . . . ? C21 C22 Cr3 P7 117.0(2) . . . . ? C27 C22 Cr3 P7 -4.9(3) . . . . ? C25 C21 Cr3 C24 -37.8(2) . . . . ? C22 C21 Cr3 C24 79.7(2) . . . . ? C26 C21 Cr3 C24 -157.8(4) . . . . ? C25 C21 Cr3 C23 -80.4(2) . . . . ? C22 C21 Cr3 C23 37.2(2) . . . . ? C26 C21 Cr3 C23 159.7(4) . . . . ? C22 C21 Cr3 C25 117.5(3) . . . . ? C26 C21 Cr3 C25 -120.0(4) . . . . ? C25 C21 Cr3 C22 -117.5(3) . . . . ? C26 C21 Cr3 C22 122.5(4) . . . . ? C25 C21 Cr3 P6 116.1(2) . . . . ? C22 C21 Cr3 P6 -126.4(2) . . . . ? C26 C21 Cr3 P6 -3.9(3) . . . . ? C25 C21 Cr3 P10 63.3(2) . . . . ? C22 C21 Cr3 P10 -179.22(19) . . . . ? C26 C21 Cr3 P10 -56.7(3) . . . . ? C25 C21 Cr3 P8 -134.3(2) . . . . ? C22 C21 Cr3 P8 -16.8(3) . . . . ? C26 C21 Cr3 P8 105.7(3) . . . . ? C25 C21 Cr3 P9 2.0(4) . . . . ? C22 C21 Cr3 P9 119.6(3) . . . . ? C26 C21 Cr3 P9 -117.9(3) . . . . ? C25 C21 Cr3 P7 169.30(19) . . . . ? C22 C21 Cr3 P7 -73.2(2) . . . . ? C26 C21 Cr3 P7 49.3(4) . . . . ? C24 Cr3 P6 P10 -68.04(19) . . . . ? C23 Cr3 P6 P10 -154.8(3) . . . . ? C25 Cr3 P6 P10 -81.54(11) . . . . ? C22 Cr3 P6 P10 -151.36(13) . . . . ? C21 Cr3 P6 P10 -117.64(11) . . . . ? P8 Cr3 P6 P10 92.11(4) . . . . ? P9 Cr3 P6 P10 38.65(4) . . . . ? P7 Cr3 P6 P10 129.24(5) . . . . ? C24 Cr3 P6 P7 162.71(19) . . . . ? C23 Cr3 P6 P7 76.0(3) . . . . ? C25 Cr3 P6 P7 149.21(11) . . . . ? C22 Cr3 P6 P7 79.39(13) . . . . ? C21 Cr3 P6 P7 113.11(11) . . . . ? P10 Cr3 P6 P7 -129.24(5) . . . . ? P8 Cr3 P6 P7 -37.13(4) . . . . ? P9 Cr3 P6 P7 -90.60(4) . . . . ? C24 Cr3 P6 Cr4 -132.62(19) . . . . ? C23 Cr3 P6 Cr4 140.6(2) . . . . ? C25 Cr3 P6 Cr4 -146.12(11) . . . . ? C22 Cr3 P6 Cr4 144.06(12) . . . . ? C21 Cr3 P6 Cr4 177.78(10) . . . . ? P10 Cr3 P6 Cr4 -64.57(4) . . . . ? P8 Cr3 P6 Cr4 27.54(4) . . . . ? P9 Cr3 P6 Cr4 -25.93(4) . . . . ? P7 Cr3 P6 Cr4 64.67(4) . . . . ? P10 P6 P7 P8 -1.75(7) . . . . ? Cr3 P6 P7 P8 44.93(5) . . . . ? Cr4 P6 P7 P8 -47.22(5) . . . . ? P10 P6 P7 Cr4 45.47(5) . . . . ? Cr3 P6 P7 Cr4 92.15(3) . . . . ? P10 P6 P7 Cr3 -46.68(5) . . . . ? Cr4 P6 P7 Cr3 -92.15(3) . . . . ? C24 Cr3 P7 P8 70.3(3) . . . . ? C23 Cr3 P7 P8 76.07(12) . . . . ? C25 Cr3 P7 P8 159.6(2) . . . . ? C22 Cr3 P7 P8 110.53(11) . . . . ? C21 Cr3 P7 P8 146.79(12) . . . . ? P6 Cr3 P7 P8 -131.15(5) . . . . ? P10 Cr3 P7 P8 -92.58(4) . . . . ? P9 Cr3 P7 P8 -38.78(4) . . . . ? C24 Cr3 P7 P6 -158.5(2) . . . . ? C23 Cr3 P7 P6 -152.77(12) . . . . ? C25 Cr3 P7 P6 -69.2(2) . . . . ? C22 Cr3 P7 P6 -118.32(11) . . . . ? C21 Cr3 P7 P6 -82.06(12) . . . . ? P10 Cr3 P7 P6 38.57(4) . . . . ? P8 Cr3 P7 P6 131.15(5) . . . . ? P9 Cr3 P7 P6 92.37(4) . . . . ? C24 Cr3 P7 Cr4 136.1(2) . . . . ? C23 Cr3 P7 Cr4 141.79(12) . . . . ? C25 Cr3 P7 Cr4 -134.6(2) . . . . ? C22 Cr3 P7 Cr4 176.24(11) . . . . ? C21 Cr3 P7 Cr4 -147.50(12) . . . . ? P6 Cr3 P7 Cr4 -65.44(4) . . . . ? P10 Cr3 P7 Cr4 -26.87(4) . . . . ? P8 Cr3 P7 Cr4 65.71(4) . . . . ? P9 Cr3 P7 Cr4 26.93(4) . . . . ? P6 P7 P8 P9 2.32(7) . . . . ? Cr4 P7 P8 P9 -44.78(5) . . . . ? Cr3 P7 P8 P9 47.13(5) . . . . ? P6 P7 P8 Cr3 -44.81(5) . . . . ? Cr4 P7 P8 Cr3 -91.91(4) . . . . ? P6 P7 P8 Cr4 47.10(5) . . . . ? Cr3 P7 P8 Cr4 91.91(4) . . . . ? C24 Cr3 P8 P7 -154.01(11) . . . . ? C23 Cr3 P8 P7 -120.01(10) . . . . ? C25 Cr3 P8 P7 -156.3(2) . . . . ? C22 Cr3 P8 P7 -84.39(12) . . . . ? C21 Cr3 P8 P7 -73.5(2) . . . . ? P6 Cr3 P8 P7 37.23(4) . . . . ? P10 Cr3 P8 P7 90.86(4) . . . . ? P9 Cr3 P8 P7 128.76(5) . . . . ? C24 Cr3 P8 P9 77.23(11) . . . . ? C23 Cr3 P8 P9 111.24(11) . . . . ? C25 Cr3 P8 P9 75.0(2) . . . . ? C22 Cr3 P8 P9 146.86(12) . . . . ? C21 Cr3 P8 P9 157.8(2) . . . . ? P6 Cr3 P8 P9 -91.53(5) . . . . ? P10 Cr3 P8 P9 -37.89(4) . . . . ? P7 Cr3 P8 P9 -128.76(5) . . . . ? C24 Cr3 P8 Cr4 141.28(11) . . . . ? C23 Cr3 P8 Cr4 175.28(10) . . . . ? C25 Cr3 P8 Cr4 139.0(2) . . . . ? C22 Cr3 P8 Cr4 -149.10(11) . . . . ? C21 Cr3 P8 Cr4 -138.2(2) . . . . ? P6 Cr3 P8 Cr4 -27.48(4) . . . . ? P10 Cr3 P8 Cr4 26.15(4) . . . . ? P9 Cr3 P8 Cr4 64.04(4) . . . . ? P7 Cr3 P8 Cr4 -64.71(4) . . . . ? P7 P8 P9 P10 -2.00(7) . . . . ? Cr3 P8 P9 P10 45.36(5) . . . . ? Cr4 P8 P9 P10 -47.08(5) . . . . ? P7 P8 P9 Cr4 45.08(5) . . . . ? Cr3 P8 P9 Cr4 92.44(3) . . . . ? P7 P8 P9 Cr3 -47.36(5) . . . . ? Cr4 P8 P9 Cr3 -92.44(3) . . . . ? C24 Cr3 P9 P8 -117.87(11) . . . . ? C23 Cr3 P9 P8 -82.02(11) . . . . ? C25 Cr3 P9 P8 -151.69(12) . . . . ? C22 Cr3 P9 P8 -71.3(2) . . . . ? C21 Cr3 P9 P8 -153.1(2) . . . . ? P6 Cr3 P9 P8 92.02(5) . . . . ? P10 Cr3 P9 P8 130.54(5) . . . . ? P7 Cr3 P9 P8 38.65(4) . . . . ? C24 Cr3 P9 P10 111.59(11) . . . . ? C23 Cr3 P9 P10 147.44(11) . . . . ? C25 Cr3 P9 P10 77.77(12) . . . . ? C22 Cr3 P9 P10 158.1(2) . . . . ? C21 Cr3 P9 P10 76.4(2) . . . . ? P6 Cr3 P9 P10 -38.52(4) . . . . ? P8 Cr3 P9 P10 -130.54(5) . . . . ? P7 Cr3 P9 P10 -91.89(4) . . . . ? C24 Cr3 P9 Cr4 176.38(11) . . . . ? C23 Cr3 P9 Cr4 -147.78(11) . . . . ? C25 Cr3 P9 Cr4 142.56(11) . . . . ? C22 Cr3 P9 Cr4 -137.1(2) . . . . ? C21 Cr3 P9 Cr4 141.2(2) . . . . ? P6 Cr3 P9 Cr4 26.27(4) . . . . ? P10 Cr3 P9 Cr4 64.78(4) . . . . ? P8 Cr3 P9 Cr4 -65.75(4) . . . . ? P7 Cr3 P9 Cr4 -27.11(4) . . . . ? P7 P6 P10 P9 0.51(7) . . . . ? Cr3 P6 P10 P9 -46.53(5) . . . . ? Cr4 P6 P10 P9 46.01(5) . . . . ? P7 P6 P10 Cr3 47.04(5) . . . . ? Cr4 P6 P10 Cr3 92.54(4) . . . . ? P7 P6 P10 Cr4 -45.50(5) . . . . ? Cr3 P6 P10 Cr4 -92.54(4) . . . . ? P8 P9 P10 P6 0.92(7) . . . . ? Cr4 P9 P10 P6 -46.61(5) . . . . ? Cr3 P9 P10 P6 46.44(5) . . . . ? P8 P9 P10 Cr3 -45.52(5) . . . . ? Cr4 P9 P10 Cr3 -93.05(3) . . . . ? P8 P9 P10 Cr4 47.53(5) . . . . ? Cr3 P9 P10 Cr4 93.05(3) . . . . ? C24 Cr3 P10 P6 149.12(12) . . . . ? C23 Cr3 P10 P6 160.6(2) . . . . ? C25 Cr3 P10 P6 112.38(11) . . . . ? C22 Cr3 P10 P6 78.1(3) . . . . ? C21 Cr3 P10 P6 79.18(12) . . . . ? P8 Cr3 P10 P6 -91.68(5) . . . . ? P9 Cr3 P10 P6 -129.36(5) . . . . ? P7 Cr3 P10 P6 -38.45(4) . . . . ? C24 Cr3 P10 P9 -81.52(12) . . . . ? C23 Cr3 P10 P9 -70.1(2) . . . . ? C25 Cr3 P10 P9 -118.26(11) . . . . ? C22 Cr3 P10 P9 -152.6(3) . . . . ? C21 Cr3 P10 P9 -151.46(12) . . . . ? P6 Cr3 P10 P9 129.36(5) . . . . ? P8 Cr3 P10 P9 37.67(4) . . . . ? P7 Cr3 P10 P9 90.91(4) . . . . ? C24 Cr3 P10 Cr4 -145.57(11) . . . . ? C23 Cr3 P10 Cr4 -134.1(2) . . . . ? C25 Cr3 P10 Cr4 177.69(10) . . . . ? C22 Cr3 P10 Cr4 143.4(2) . . . . ? C21 Cr3 P10 Cr4 144.49(11) . . . . ? P6 Cr3 P10 Cr4 65.31(4) . . . . ? P8 Cr3 P10 Cr4 -26.37(4) . . . . ? P9 Cr3 P10 Cr4 -64.05(4) . . . . ? P7 Cr3 P10 Cr4 26.86(4) . . . . ? P8 P9 Cr4 C31 163.09(16) . . . . ? P10 P9 Cr4 C31 -68.05(16) . . . . ? Cr3 P9 Cr4 C31 -132.29(16) . . . . ? P8 P9 Cr4 C32 89.0(3) . . . . ? P10 P9 Cr4 C32 -142.1(3) . . . . ? Cr3 P9 Cr4 C32 153.6(3) . . . . ? P8 P9 Cr4 C33 75.59(12) . . . . ? P10 P9 Cr4 C33 -155.54(12) . . . . ? Cr3 P9 Cr4 C33 140.22(12) . . . . ? P8 P9 Cr4 C35 143.67(11) . . . . ? P10 P9 Cr4 C35 -87.46(11) . . . . ? Cr3 P9 Cr4 C35 -151.70(10) . . . . ? P8 P9 Cr4 C34 105.70(11) . . . . ? P10 P9 Cr4 C34 -125.43(11) . . . . ? Cr3 P9 Cr4 C34 170.33(11) . . . . ? P8 P9 Cr4 P10 -128.86(5) . . . . ? Cr3 P9 Cr4 P10 -64.24(4) . . . . ? P8 P9 Cr4 P7 -37.29(4) . . . . ? P10 P9 Cr4 P7 91.57(4) . . . . ? Cr3 P9 Cr4 P7 27.34(4) . . . . ? P8 P9 Cr4 P6 -90.64(4) . . . . ? P10 P9 Cr4 P6 38.23(4) . . . . ? Cr3 P9 Cr4 P6 -26.01(4) . . . . ? P10 P9 Cr4 P8 128.86(5) . . . . ? Cr3 P9 Cr4 P8 64.63(4) . . . . ? P6 P10 Cr4 C31 -88.24(11) . . . . ? P9 P10 Cr4 C31 142.24(11) . . . . ? Cr3 P10 Cr4 C31 -152.94(10) . . . . ? P6 P10 Cr4 C32 -68.96(16) . . . . ? P9 P10 Cr4 C32 161.53(15) . . . . ? Cr3 P10 Cr4 C32 -133.65(15) . . . . ? P6 P10 Cr4 C33 -141.0(3) . . . . ? P9 P10 Cr4 C33 89.5(3) . . . . ? Cr3 P10 Cr4 C33 154.3(3) . . . . ? P6 P10 Cr4 C35 -126.00(11) . . . . ? P9 P10 Cr4 C35 104.48(11) . . . . ? Cr3 P10 Cr4 C35 169.30(10) . . . . ? P6 P10 Cr4 C34 -155.85(13) . . . . ? P9 P10 Cr4 C34 74.64(13) . . . . ? Cr3 P10 Cr4 C34 139.46(13) . . . . ? P6 P10 Cr4 P9 129.52(5) . . . . ? Cr3 P10 Cr4 P9 64.82(4) . . . . ? P6 P10 Cr4 P7 37.62(4) . . . . ? P9 P10 Cr4 P7 -91.90(4) . . . . ? Cr3 P10 Cr4 P7 -27.07(4) . . . . ? P9 P10 Cr4 P6 -129.52(5) . . . . ? Cr3 P10 Cr4 P6 -64.69(4) . . . . ? P6 P10 Cr4 P8 90.79(4) . . . . ? P9 P10 Cr4 P8 -38.73(4) . . . . ? Cr3 P10 Cr4 P8 26.09(4) . . . . ? P8 P7 Cr4 C31 -157.96(13) . . . . ? P6 P7 Cr4 C31 72.95(13) . . . . ? Cr3 P7 Cr4 C31 137.37(12) . . . . ? P8 P7 Cr4 C32 -126.90(11) . . . . ? P6 P7 Cr4 C32 104.00(11) . . . . ? Cr3 P7 Cr4 C32 168.42(10) . . . . ? P8 P7 Cr4 C33 -88.99(11) . . . . ? P6 P7 Cr4 C33 141.92(11) . . . . ? Cr3 P7 Cr4 C33 -153.66(11) . . . . ? P8 P7 Cr4 C35 -145.3(3) . . . . ? P6 P7 Cr4 C35 85.6(3) . . . . ? Cr3 P7 Cr4 C35 150.0(3) . . . . ? P8 P7 Cr4 C34 -70.36(17) . . . . ? P6 P7 Cr4 C34 160.54(17) . . . . ? Cr3 P7 Cr4 C34 -135.04(17) . . . . ? P8 P7 Cr4 P9 37.45(4) . . . . ? P6 P7 Cr4 P9 -91.65(5) . . . . ? Cr3 P7 Cr4 P9 -27.23(4) . . . . ? P8 P7 Cr4 P10 91.50(5) . . . . ? P6 P7 Cr4 P10 -37.59(4) . . . . ? Cr3 P7 Cr4 P10 26.83(4) . . . . ? P8 P7 Cr4 P6 129.10(5) . . . . ? Cr3 P7 Cr4 P6 64.42(4) . . . . ? P6 P7 Cr4 P8 -129.10(5) . . . . ? Cr3 P7 Cr4 P8 -64.68(4) . . . . ? P10 P6 Cr4 C31 103.21(11) . . . . ? P7 P6 Cr4 C31 -126.31(11) . . . . ? Cr3 P6 Cr4 C31 168.07(10) . . . . ? P10 P6 Cr4 C32 141.46(11) . . . . ? P7 P6 Cr4 C32 -88.06(11) . . . . ? Cr3 P6 Cr4 C32 -153.69(11) . . . . ? P10 P6 Cr4 C33 159.76(17) . . . . ? P7 P6 Cr4 C33 -69.76(17) . . . . ? Cr3 P6 Cr4 C33 -135.38(16) . . . . ? P10 P6 Cr4 C35 72.89(12) . . . . ? P7 P6 Cr4 C35 -156.63(12) . . . . ? Cr3 P6 Cr4 C35 137.75(12) . . . . ? P10 P6 Cr4 C34 87.0(3) . . . . ? P7 P6 Cr4 C34 -142.5(3) . . . . ? Cr3 P6 Cr4 C34 151.8(3) . . . . ? P10 P6 Cr4 P9 -38.67(4) . . . . ? P7 P6 Cr4 P9 91.81(5) . . . . ? Cr3 P6 Cr4 P9 26.18(4) . . . . ? P7 P6 Cr4 P10 130.48(5) . . . . ? Cr3 P6 Cr4 P10 64.85(4) . . . . ? P10 P6 Cr4 P7 -130.48(5) . . . . ? Cr3 P6 Cr4 P7 -65.63(4) . . . . ? P10 P6 Cr4 P8 -92.09(5) . . . . ? P7 P6 Cr4 P8 38.39(4) . . . . ? Cr3 P6 Cr4 P8 -27.24(4) . . . . ? P7 P8 Cr4 C31 85.3(3) . . . . ? P9 P8 Cr4 C31 -143.9(3) . . . . ? Cr3 P8 Cr4 C31 150.9(3) . . . . ? P7 P8 Cr4 C32 72.70(12) . . . . ? P9 P8 Cr4 C32 -156.45(12) . . . . ? Cr3 P8 Cr4 C32 138.38(12) . . . . ? P7 P8 Cr4 C33 104.23(10) . . . . ? P9 P8 Cr4 C33 -124.92(10) . . . . ? Cr3 P8 Cr4 C33 169.91(10) . . . . ? P7 P8 Cr4 C35 162.10(16) . . . . ? P9 P8 Cr4 C35 -67.05(16) . . . . ? Cr3 P8 Cr4 C35 -132.22(16) . . . . ? P7 P8 Cr4 C34 141.84(11) . . . . ? P9 P8 Cr4 C34 -87.31(11) . . . . ? Cr3 P8 Cr4 C34 -152.48(11) . . . . ? P7 P8 Cr4 P9 -130.85(5) . . . . ? Cr3 P8 Cr4 P9 -65.17(4) . . . . ? P7 P8 Cr4 P10 -91.76(4) . . . . ? P9 P8 Cr4 P10 39.09(4) . . . . ? Cr3 P8 Cr4 P10 -26.08(4) . . . . ? P9 P8 Cr4 P7 130.85(5) . . . . ? Cr3 P8 Cr4 P7 65.68(4) . . . . ? P7 P8 Cr4 P6 -38.49(4) . . . . ? P9 P8 Cr4 P6 92.35(5) . . . . ? Cr3 P8 Cr4 P6 27.18(4) . . . . ? C32 Cr4 C31 C35 117.6(3) . . . . ? C33 Cr4 C31 C35 79.7(2) . . . . ? C34 Cr4 C31 C35 37.6(2) . . . . ? P9 Cr4 C31 C35 -31.4(3) . . . . ? P10 Cr4 C31 C35 -82.4(2) . . . . ? P7 Cr4 C31 C35 173.15(17) . . . . ? P6 Cr4 C31 C35 -136.2(2) . . . . ? P8 Cr4 C31 C35 100.7(4) . . . . ? C33 Cr4 C31 C32 -37.9(2) . . . . ? C35 Cr4 C31 C32 -117.6(3) . . . . ? C34 Cr4 C31 C32 -80.0(2) . . . . ? P9 Cr4 C31 C32 -149.04(18) . . . . ? P10 Cr4 C31 C32 159.99(18) . . . . ? P7 Cr4 C31 C32 55.5(2) . . . . ? P6 Cr4 C31 C32 106.15(19) . . . . ? P8 Cr4 C31 C32 -16.9(4) . . . . ? C32 Cr4 C31 C36 -121.0(4) . . . . ? C33 Cr4 C31 C36 -158.9(4) . . . . ? C35 Cr4 C31 C36 121.4(4) . . . . ? C34 Cr4 C31 C36 159.0(4) . . . . ? P9 Cr4 C31 C36 90.0(3) . . . . ? P10 Cr4 C31 C36 39.0(3) . . . . ? P7 Cr4 C31 C36 -65.5(3) . . . . ? P6 Cr4 C31 C36 -14.9(3) . . . . ? P8 Cr4 C31 C36 -137.9(3) . . . . ? C35 C31 C32 C33 0.0(4) . . . . ? C36 C31 C32 C33 -178.2(4) . . . . ? Cr4 C31 C32 C33 62.4(3) . . . . ? C35 C31 C32 C37 177.3(4) . . . . ? C36 C31 C32 C37 -0.9(6) . . . . ? Cr4 C31 C32 C37 -120.3(4) . . . . ? C35 C31 C32 Cr4 -62.4(3) . . . . ? C36 C31 C32 Cr4 119.4(4) . . . . ? C31 Cr4 C32 C33 -116.7(3) . . . . ? C35 Cr4 C32 C33 -79.4(2) . . . . ? C34 Cr4 C32 C33 -36.9(2) . . . . ? P9 Cr4 C32 C33 -18.3(4) . . . . ? P10 Cr4 C32 C33 -147.70(18) . . . . ? P7 Cr4 C32 C33 107.3(2) . . . . ? P6 Cr4 C32 C33 161.30(19) . . . . ? P8 Cr4 C32 C33 56.9(2) . . . . ? C33 Cr4 C32 C31 116.7(3) . . . . ? C35 Cr4 C32 C31 37.3(2) . . . . ? C34 Cr4 C32 C31 79.8(2) . . . . ? P9 Cr4 C32 C31 98.4(4) . . . . ? P10 Cr4 C32 C31 -31.0(3) . . . . ? P7 Cr4 C32 C31 -135.93(19) . . . . ? P6 Cr4 C32 C31 -82.0(2) . . . . ? P8 Cr4 C32 C31 173.66(17) . . . . ? C31 Cr4 C32 C37 120.9(4) . . . . ? C33 Cr4 C32 C37 -122.3(4) . . . . ? C35 Cr4 C32 C37 158.2(4) . . . . ? C34 Cr4 C32 C37 -159.2(4) . . . . ? P9 Cr4 C32 C37 -140.6(3) . . . . ? P10 Cr4 C32 C37 90.0(3) . . . . ? P7 Cr4 C32 C37 -15.0(3) . . . . ? P6 Cr4 C32 C37 39.0(3) . . . . ? P8 Cr4 C32 C37 -65.4(3) . . . . ? C31 C32 C33 C34 -0.2(4) . . . . ? C37 C32 C33 C34 -177.5(4) . . . . ? Cr4 C32 C33 C34 61.8(3) . . . . ? C31 C32 C33 C38 177.3(4) . . . . ? C37 C32 C33 C38 0.0(6) . . . . ? Cr4 C32 C33 C38 -120.7(4) . . . . ? C31 C32 C33 Cr4 -62.0(3) . . . . ? C37 C32 C33 Cr4 120.7(4) . . . . ? C31 Cr4 C33 C34 -79.8(2) . . . . ? C32 Cr4 C33 C34 -118.1(3) . . . . ? C35 Cr4 C33 C34 -37.4(2) . . . . ? P9 Cr4 C33 C34 54.8(2) . . . . ? P10 Cr4 C33 C34 -20.6(4) . . . . ? P7 Cr4 C33 C34 160.8(2) . . . . ? P6 Cr4 C33 C34 -147.41(19) . . . . ? P8 Cr4 C33 C34 106.7(2) . . . . ? C31 Cr4 C33 C32 38.2(2) . . . . ? C35 Cr4 C33 C32 80.7(2) . . . . ? C34 Cr4 C33 C32 118.1(3) . . . . ? P9 Cr4 C33 C32 172.84(17) . . . . ? P10 Cr4 C33 C32 97.5(3) . . . . ? P7 Cr4 C33 C32 -81.1(2) . . . . ? P6 Cr4 C33 C32 -29.4(3) . . . . ? P8 Cr4 C33 C32 -135.2(2) . . . . ? C31 Cr4 C33 C38 160.4(4) . . . . ? C32 Cr4 C33 C38 122.2(4) . . . . ? C35 Cr4 C33 C38 -157.1(4) . . . . ? C34 Cr4 C33 C38 -119.8(4) . . . . ? P9 Cr4 C33 C38 -65.0(3) . . . . ? P10 Cr4 C33 C38 -140.4(3) . . . . ? P7 Cr4 C33 C38 41.0(3) . . . . ? P6 Cr4 C33 C38 92.8(3) . . . . ? P8 Cr4 C33 C38 -13.1(3) . . . . ? C32 C33 C34 C35 0.2(4) . . . . ? C38 C33 C34 C35 -177.3(4) . . . . ? Cr4 C33 C34 C35 61.5(3) . . . . ? C32 C33 C34 C39 176.2(4) . . . . ? C38 C33 C34 C39 -1.4(6) . . . . ? Cr4 C33 C34 C39 -122.5(4) . . . . ? C32 C33 C34 Cr4 -61.3(3) . . . . ? C38 C33 C34 Cr4 121.1(4) . . . . ? C31 Cr4 C34 C33 80.6(2) . . . . ? C32 Cr4 C34 C33 37.5(2) . . . . ? C35 Cr4 C34 C33 118.1(3) . . . . ? P9 Cr4 C34 C33 -136.4(2) . . . . ? P10 Cr4 C34 C33 171.63(18) . . . . ? P7 Cr4 C34 C33 -30.2(3) . . . . ? P6 Cr4 C34 C33 98.7(3) . . . . ? P8 Cr4 C34 C33 -82.3(2) . . . . ? C31 Cr4 C34 C35 -37.5(2) . . . . ? C32 Cr4 C34 C35 -80.6(2) . . . . ? C33 Cr4 C34 C35 -118.1(3) . . . . ? P9 Cr4 C34 C35 105.5(2) . . . . ? P10 Cr4 C34 C35 53.5(2) . . . . ? P7 Cr4 C34 C35 -148.29(18) . . . . ? P6 Cr4 C34 C35 -19.5(4) . . . . ? P8 Cr4 C34 C35 159.58(19) . . . . ? C31 Cr4 C34 C39 -158.0(4) . . . . ? C32 Cr4 C34 C39 158.9(4) . . . . ? C33 Cr4 C34 C39 121.4(4) . . . . ? C35 Cr4 C34 C39 -120.5(4) . . . . ? P9 Cr4 C34 C39 -15.0(3) . . . . ? P10 Cr4 C34 C39 -67.0(4) . . . . ? P7 Cr4 C34 C39 91.2(3) . . . . ? P6 Cr4 C34 C39 -139.9(3) . . . . ? P8 Cr4 C34 C39 39.1(3) . . . . ? C32 C31 C35 C34 0.1(4) . . . . ? C36 C31 C35 C34 178.4(4) . . . . ? Cr4 C31 C35 C34 -61.8(3) . . . . ? C32 C31 C35 C40 -177.4(4) . . . . ? C36 C31 C35 C40 0.8(6) . . . . ? Cr4 C31 C35 C40 120.7(4) . . . . ? C32 C31 C35 Cr4 61.9(3) . . . . ? C36 C31 C35 Cr4 -119.8(4) . . . . ? C33 C34 C35 C31 -0.2(4) . . . . ? C39 C34 C35 C31 -176.2(4) . . . . ? Cr4 C34 C35 C31 61.4(3) . . . . ? C33 C34 C35 C40 177.3(4) . . . . ? C39 C34 C35 C40 1.3(6) . . . . ? Cr4 C34 C35 C40 -121.1(4) . . . . ? C33 C34 C35 Cr4 -61.6(3) . . . . ? C39 C34 C35 Cr4 122.4(4) . . . . ? C32 Cr4 C35 C31 -37.8(2) . . . . ? C33 Cr4 C35 C31 -80.5(2) . . . . ? C34 Cr4 C35 C31 -117.4(3) . . . . ? P9 Cr4 C35 C31 159.77(19) . . . . ? P10 Cr4 C35 C31 105.2(2) . . . . ? P7 Cr4 C35 C31 -17.3(4) . . . . ? P6 Cr4 C35 C31 54.7(2) . . . . ? P8 Cr4 C35 C31 -150.00(18) . . . . ? C31 Cr4 C35 C34 117.4(3) . . . . ? C32 Cr4 C35 C34 79.6(2) . . . . ? C33 Cr4 C35 C34 36.9(2) . . . . ? P9 Cr4 C35 C34 -82.8(2) . . . . ? P10 Cr4 C35 C34 -137.3(2) . . . . ? P7 Cr4 C35 C34 100.1(3) . . . . ? P6 Cr4 C35 C34 172.19(18) . . . . ? P8 Cr4 C35 C34 -32.6(3) . . . . ? C31 Cr4 C35 C40 -121.1(4) . . . . ? C32 Cr4 C35 C40 -158.9(4) . . . . ? C33 Cr4 C35 C40 158.4(4) . . . . ? C34 Cr4 C35 C40 121.5(4) . . . . ? P9 Cr4 C35 C40 38.7(3) . . . . ? P10 Cr4 C35 C40 -15.8(3) . . . . ? P7 Cr4 C35 C40 -138.4(3) . . . . ? P6 Cr4 C35 C40 -66.3(3) . . . . ? P8 Cr4 C35 C40 88.9(3) . . . . ? _diffrn_measured_fraction_theta_max 0.908 _diffrn_reflns_theta_full 30.57 _diffrn_measured_fraction_theta_full 0.908 _refine_diff_density_max 3.853 _refine_diff_density_min -2.652 _refine_diff_density_rms 0.200 #===END data_030k _database_code_depnum_ccdc_archive 'CCDC 618760' _audit_creation_method SHELXL-97 _chemical_name_systematic ; \m~2~-\h^5^,\h^5^-cyclopentaphosphole)-bis ((\h^5^-pentamethyl-cyclopentadienyl)-chromium) hexafluoroantimonate ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H30 Cr2 F6 P5 Sb' _chemical_formula_weight 765.04 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M 'I 2/a' loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' _cell_length_a 22.8945(11) _cell_length_b 21.2571(10) _cell_length_c 22.8707(12) _cell_angle_alpha 90.00 _cell_angle_beta 101.148(2) _cell_angle_gamma 90.00 _cell_volume 10920.5(9) _cell_formula_units_Z 16 _cell_measurement_temperature 30(2) _cell_measurement_reflns_used 8157 _cell_measurement_theta_min 2.096 _cell_measurement_theta_max 30.551 _exptl_crystal_description 'irregular block' _exptl_crystal_colour 'dark green' _exptl_crystal_size_max 0.60 _exptl_crystal_size_mid 0.52 _exptl_crystal_size_min 0.40 _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 1.861 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 6048 _exptl_absorpt_coefficient_mu 2.108 _exptl_absorpt_correction_type integration _exptl_absorpt_correction_T_min 0.397 _exptl_absorpt_correction_T_max 0.598 _exptl_absorpt_process_details 'XPREP in SHELXTL' _exptl_special_details ; ? ; _diffrn_ambient_temperature 30(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'Bede Microsource X-ray Generator' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker APEX CCD Diffractometer' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number 0 _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% 0 _diffrn_reflns_number 38557 _diffrn_reflns_av_R_equivalents 0.0387 _diffrn_reflns_av_sigmaI/netI 0.0480 _diffrn_reflns_limit_h_min -32 _diffrn_reflns_limit_h_max 32 _diffrn_reflns_limit_k_min -30 _diffrn_reflns_limit_k_max 27 _diffrn_reflns_limit_l_min -31 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_theta_min 1.15 _diffrn_reflns_theta_max 30.57 _reflns_number_total 15213 _reflns_number_gt 14392 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'SMART V5.625 (Bruker, 2003)' _computing_cell_refinement 'SMART V5.625 (Bruker, 2003)' _computing_data_reduction 'SAINT V6.28A (Bruker, 2003)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'SHELXTL V6.12(Bruker, 2001)' _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0811P)^2^+3.8728P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 15213 _refine_ls_number_parameters 614 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0437 _refine_ls_R_factor_gt 0.0408 _refine_ls_wR_factor_ref 0.1122 _refine_ls_wR_factor_gt 0.1096 _refine_ls_goodness_of_fit_ref 1.041 _refine_ls_restrained_S_all 1.041 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb1 Sb 0.138867(11) 0.868753(11) 0.384011(11) 0.01098(6) Uani 1 1 d . . . F1 F 0.09763(11) 0.80781(11) 0.33212(12) 0.0195(5) Uani 1 1 d . . . F2 F 0.09065(12) 0.93148(11) 0.34133(11) 0.0201(5) Uani 1 1 d . . . F3 F 0.08337(11) 0.86008(12) 0.43460(11) 0.0182(5) Uani 1 1 d . . . F4 F 0.18516(10) 0.80538(11) 0.42725(11) 0.0168(4) Uani 1 1 d . . . F5 F 0.19488(12) 0.87696(11) 0.33433(12) 0.0183(5) Uani 1 1 d . . . F6 F 0.18001(11) 0.93044(11) 0.43431(11) 0.0178(5) Uani 1 1 d . . . Sb2 Sb 0.136435(12) 0.127257(11) 0.117079(12) 0.01047(6) Uani 1 1 d . . . F7 F 0.12353(13) 0.05056(12) 0.15230(13) 0.0266(6) Uani 1 1 d . . . F8 F 0.07128(11) 0.16362(12) 0.14341(12) 0.0214(5) Uani 1 1 d . . . F9 F 0.08577(11) 0.10161(12) 0.04668(11) 0.0197(5) Uani 1 1 d . . . F10 F 0.20230(11) 0.09323(12) 0.08956(11) 0.0208(5) Uani 1 1 d . . . F11 F 0.18686(11) 0.15254(12) 0.18755(11) 0.0186(5) Uani 1 1 d . . . F12 F 0.15019(11) 0.20413(11) 0.08151(12) 0.0202(5) Uani 1 1 d . . . C1 C -0.11292(16) 0.31090(16) 0.44741(16) 0.0107(6) Uani 1 1 d . . . C2 C -0.14180(16) 0.26792(16) 0.40252(17) 0.0112(6) Uani 1 1 d . . . C3 C -0.14118(15) 0.29552(16) 0.34595(17) 0.0109(6) Uani 1 1 d . . . C4 C -0.11186(16) 0.35553(16) 0.35498(17) 0.0108(6) Uani 1 1 d . . . C5 C -0.09453(16) 0.36481(17) 0.41765(17) 0.0107(6) Uani 1 1 d . . . C6 C -0.10566(18) 0.30316(18) 0.51286(17) 0.0149(7) Uani 1 1 d . . . H6A H -0.1384 0.3244 0.5268 0.022 Uiso 1 1 calc R . . H6B H -0.0677 0.3217 0.5324 0.022 Uiso 1 1 calc R . . H6C H -0.1060 0.2583 0.5226 0.022 Uiso 1 1 calc R . . C7 C -0.17057(17) 0.20746(17) 0.41454(19) 0.0146(7) Uani 1 1 d . . . H7A H -0.2126 0.2150 0.4154 0.022 Uiso 1 1 calc R . . H7B H -0.1505 0.1906 0.4531 0.022 Uiso 1 1 calc R . . H7C H -0.1675 0.1771 0.3830 0.022 Uiso 1 1 calc R . . C8 C -0.16818(17) 0.26886(18) 0.28625(17) 0.0140(7) Uani 1 1 d . . . H8A H -0.2045 0.2922 0.2695 0.021 Uiso 1 1 calc R . . H8B H -0.1780 0.2245 0.2907 0.021 Uiso 1 1 calc R . . H8C H -0.1397 0.2725 0.2595 0.021 Uiso 1 1 calc R . . C9 C -0.10388(17) 0.40123(18) 0.30766(17) 0.0148(7) Uani 1 1 d . . . H9A H -0.1410 0.4246 0.2944 0.022 Uiso 1 1 calc R . . H9B H -0.0936 0.3784 0.2738 0.022 Uiso 1 1 calc R . . H9C H -0.0718 0.4307 0.3236 0.022 Uiso 1 1 calc R . . C10 C -0.06693(17) 0.42294(17) 0.44872(17) 0.0129(6) Uani 1 1 d . . . H10A H -0.0968 0.4456 0.4660 0.019 Uiso 1 1 calc R . . H10B H -0.0525 0.4501 0.4200 0.019 Uiso 1 1 calc R . . H10C H -0.0336 0.4110 0.4804 0.019 Uiso 1 1 calc R . . Cr1 Cr -0.04860(3) 0.27978(3) 0.39228(3) 0.00895(11) Uani 1 1 d . . . P1 P 0.03509(5) 0.26920(5) 0.47165(5) 0.0178(2) Uani 1 1 d . . . P2 P -0.01370(5) 0.18225(5) 0.43748(5) 0.0173(2) Uani 1 1 d . . . P3 P -0.03321(4) 0.18720(5) 0.33884(5) 0.01642(19) Uani 1 1 d . . . P4 P 0.00294(5) 0.27742(5) 0.31127(5) 0.01648(19) Uani 1 1 d . . . P5 P 0.04518(5) 0.32804(5) 0.39359(5) 0.0174(2) Uani 1 1 d . . . Cr2 Cr 0.06326(3) 0.21816(3) 0.38875(3) 0.00911(11) Uani 1 1 d . . . C11 C 0.14657(16) 0.17694(17) 0.44011(17) 0.0112(6) Uani 1 1 d . . . C12 C 0.11594(17) 0.13002(17) 0.40092(18) 0.0122(7) Uani 1 1 d . . . C13 C 0.11274(16) 0.15194(17) 0.34092(17) 0.0118(6) Uani 1 1 d . . . C14 C 0.14060(16) 0.21204(17) 0.34368(17) 0.0119(6) Uani 1 1 d . . . C15 C 0.16172(16) 0.22798(16) 0.40485(16) 0.0111(6) Uani 1 1 d . . . C16 C 0.16286(17) 0.17031(18) 0.50602(17) 0.0143(7) Uani 1 1 d . . . H16A H 0.2001 0.1465 0.5165 0.021 Uiso 1 1 calc R . . H16B H 0.1311 0.1479 0.5206 0.021 Uiso 1 1 calc R . . H16C H 0.1681 0.2121 0.5243 0.021 Uiso 1 1 calc R . . C17 C 0.09513(18) 0.06734(17) 0.41824(19) 0.0165(7) Uani 1 1 d . . . H17A H 0.1284 0.0376 0.4241 0.025 Uiso 1 1 calc R . . H17B H 0.0633 0.0519 0.3866 0.025 Uiso 1 1 calc R . . H17C H 0.0801 0.0715 0.4554 0.025 Uiso 1 1 calc R . . C18 C 0.08837(18) 0.11584(18) 0.28560(19) 0.0166(7) Uani 1 1 d . . . H18A H 0.1203 0.0910 0.2739 0.025 Uiso 1 1 calc R . . H18B H 0.0721 0.1452 0.2535 0.025 Uiso 1 1 calc R . . H18C H 0.0567 0.0877 0.2931 0.025 Uiso 1 1 calc R . . C19 C 0.14959(17) 0.25121(18) 0.29152(17) 0.0148(7) Uani 1 1 d . . . H19A H 0.1906 0.2462 0.2855 0.022 Uiso 1 1 calc R . . H19B H 0.1422 0.2955 0.2993 0.022 Uiso 1 1 calc R . . H19C H 0.1219 0.2374 0.2556 0.022 Uiso 1 1 calc R . . C20 C 0.19587(16) 0.28585(17) 0.42725(18) 0.0140(7) Uani 1 1 d . . . H20A H 0.2379 0.2800 0.4252 0.021 Uiso 1 1 calc R . . H20B H 0.1923 0.2936 0.4687 0.021 Uiso 1 1 calc R . . H20C H 0.1798 0.3219 0.4026 0.021 Uiso 1 1 calc R . . C21 C 0.10746(18) 0.38472(17) 0.13264(19) 0.0137(7) Uani 1 1 d . . . C22 C 0.17118(18) 0.38168(17) 0.14541(19) 0.0137(7) Uani 1 1 d . . . C23 C 0.19374(17) 0.43767(17) 0.12368(18) 0.0136(7) Uani 1 1 d . . . C24 C 0.14421(18) 0.47603(17) 0.09750(17) 0.0128(6) Uani 1 1 d . . . C25 C 0.09080(17) 0.44289(18) 0.10301(17) 0.0127(7) Uani 1 1 d . . . C26 C 0.06477(17) 0.33392(18) 0.14394(19) 0.0155(7) Uani 1 1 d . . . H26A H 0.0671 0.2982 0.1174 0.023 Uiso 1 1 calc R . . H26B H 0.0241 0.3506 0.1363 0.023 Uiso 1 1 calc R . . H26C H 0.0754 0.3200 0.1855 0.023 Uiso 1 1 calc R . . C27 C 0.20868(17) 0.32714(18) 0.17275(18) 0.0146(7) Uani 1 1 d . . . H27A H 0.2279 0.3075 0.1426 0.022 Uiso 1 1 calc R . . H27B H 0.1834 0.2962 0.1876 0.022 Uiso 1 1 calc R . . H27C H 0.2392 0.3422 0.2059 0.022 Uiso 1 1 calc R . . C28 C 0.25852(17) 0.45156(19) 0.12456(19) 0.0172(7) Uani 1 1 d . . . H28A H 0.2692 0.4364 0.0875 0.026 Uiso 1 1 calc R . . H28B H 0.2832 0.4302 0.1586 0.026 Uiso 1 1 calc R . . H28C H 0.2653 0.4970 0.1281 0.026 Uiso 1 1 calc R . . C29 C 0.14811(19) 0.53680(18) 0.06549(19) 0.0173(7) Uani 1 1 d . . . H29A H 0.1505 0.5282 0.0239 0.026 Uiso 1 1 calc R . . H29B H 0.1837 0.5598 0.0848 0.026 Uiso 1 1 calc R . . H29C H 0.1127 0.5622 0.0668 0.026 Uiso 1 1 calc R . . C30 C 0.02813(17) 0.46378(19) 0.07827(18) 0.0157(7) Uani 1 1 d . . . H30A H 0.0150 0.4457 0.0385 0.024 Uiso 1 1 calc R . . H30B H 0.0268 0.5098 0.0756 0.024 Uiso 1 1 calc R . . H30C H 0.0018 0.4495 0.1046 0.024 Uiso 1 1 calc R . . Cr3 Cr 0.14292(3) 0.46358(3) 0.19253(3) 0.01088(11) Uani 1 1 d . . . P6 P 0.08601(4) 0.44299(5) 0.26970(5) 0.01379(18) Uani 1 1 d . . . P7 P 0.18269(5) 0.42926(4) 0.29495(4) 0.01343(17) Uani 1 1 d . . . P8 P 0.22674(4) 0.50925(5) 0.26122(5) 0.01408(18) Uani 1 1 d . . . P9 P 0.15728(5) 0.57465(4) 0.21834(4) 0.01345(18) Uani 1 1 d . . . P10 P 0.06989(4) 0.53300(4) 0.22272(4) 0.01327(18) Uani 1 1 d . . . Cr4 Cr 0.14531(3) 0.53317(3) 0.31371(3) 0.01018(11) Uani 1 1 d . . . C31 C 0.09632(17) 0.55245(18) 0.38495(17) 0.0129(7) Uani 1 1 d . . . C32 C 0.15252(17) 0.52396(17) 0.41047(17) 0.0128(6) Uani 1 1 d . . . C33 C 0.19839(16) 0.56561(17) 0.39946(17) 0.0122(6) Uani 1 1 d . . . C34 C 0.17114(18) 0.61864(16) 0.36788(18) 0.0125(7) Uani 1 1 d . . . C35 C 0.10778(17) 0.61079(17) 0.35876(17) 0.0114(6) Uani 1 1 d . . . C36 C 0.03584(17) 0.52616(18) 0.38784(18) 0.0153(7) Uani 1 1 d . . . H36A H 0.0199 0.5477 0.4193 0.023 Uiso 1 1 calc R . . H36B H 0.0393 0.4811 0.3967 0.023 Uiso 1 1 calc R . . H36C H 0.0089 0.5326 0.3495 0.023 Uiso 1 1 calc R . . C37 C 0.16078(17) 0.46334(17) 0.44455(17) 0.0142(7) Uani 1 1 d . . . H37A H 0.1638 0.4720 0.4871 0.021 Uiso 1 1 calc R . . H37B H 0.1973 0.4427 0.4382 0.021 Uiso 1 1 calc R . . H37C H 0.1266 0.4357 0.4306 0.021 Uiso 1 1 calc R . . C38 C 0.26448(16) 0.55731(18) 0.41946(18) 0.0150(7) Uani 1 1 d . . . H38A H 0.2770 0.5751 0.4594 0.023 Uiso 1 1 calc R . . H38B H 0.2852 0.5790 0.3916 0.023 Uiso 1 1 calc R . . H38C H 0.2743 0.5124 0.4203 0.023 Uiso 1 1 calc R . . C39 C 0.20291(17) 0.67523(18) 0.35040(18) 0.0150(7) Uani 1 1 d . . . H39A H 0.2109 0.7048 0.3839 0.023 Uiso 1 1 calc R . . H39B H 0.1780 0.6957 0.3160 0.023 Uiso 1 1 calc R . . H39C H 0.2406 0.6622 0.3399 0.023 Uiso 1 1 calc R . . C40 C 0.06214(17) 0.65713(18) 0.32972(18) 0.0156(7) Uani 1 1 d . . . H40A H 0.0525 0.6860 0.3599 0.023 Uiso 1 1 calc R . . H40B H 0.0261 0.6347 0.3106 0.023 Uiso 1 1 calc R . . H40C H 0.0780 0.6811 0.2996 0.023 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.01228(12) 0.00687(10) 0.01429(13) -0.00051(8) 0.00387(8) 0.00038(8) F1 0.0208(12) 0.0120(10) 0.0243(12) -0.0055(9) 0.0010(9) -0.0028(9) F2 0.0276(13) 0.0147(10) 0.0173(12) 0.0035(9) 0.0026(9) 0.0066(9) F3 0.0166(11) 0.0176(11) 0.0220(12) 0.0027(9) 0.0077(9) 0.0029(9) F4 0.0144(11) 0.0109(10) 0.0249(12) 0.0022(9) 0.0035(9) 0.0034(8) F5 0.0228(13) 0.0165(12) 0.0184(12) 0.0002(8) 0.0111(10) -0.0025(9) F6 0.0238(12) 0.0118(10) 0.0174(11) -0.0026(8) 0.0030(9) -0.0030(9) Sb2 0.01117(13) 0.00679(10) 0.01380(13) -0.00045(8) 0.00328(8) -0.00009(8) F7 0.0367(15) 0.0121(11) 0.0303(14) 0.0073(10) 0.0049(11) -0.0051(10) F8 0.0158(11) 0.0233(13) 0.0269(13) -0.0025(10) 0.0085(9) 0.0036(9) F9 0.0197(12) 0.0168(11) 0.0212(12) -0.0059(9) 0.0007(9) -0.0033(9) F10 0.0179(12) 0.0199(12) 0.0248(13) -0.0062(10) 0.0049(9) 0.0057(9) F11 0.0212(12) 0.0173(11) 0.0161(11) -0.0052(9) 0.0002(9) -0.0006(9) F12 0.0204(12) 0.0119(11) 0.0278(13) 0.0078(9) 0.0032(10) -0.0034(9) C1 0.0127(16) 0.0054(14) 0.0151(16) 0.0011(12) 0.0054(12) 0.0019(11) C2 0.0077(15) 0.0088(14) 0.0175(17) -0.0007(13) 0.0035(12) -0.0001(11) C3 0.0081(15) 0.0062(14) 0.0178(17) -0.0009(12) 0.0008(12) -0.0004(11) C4 0.0093(15) 0.0073(14) 0.0168(17) -0.0002(12) 0.0047(12) 0.0012(12) C5 0.0098(15) 0.0055(14) 0.0169(17) 0.0003(12) 0.0030(12) 0.0003(12) C6 0.0184(18) 0.0119(16) 0.0151(17) 0.0004(13) 0.0052(13) 0.0025(13) C7 0.0122(16) 0.0073(14) 0.025(2) -0.0012(13) 0.0064(13) -0.0030(12) C8 0.0133(16) 0.0122(16) 0.0163(17) -0.0023(13) 0.0025(13) 0.0006(12) C9 0.0168(18) 0.0104(16) 0.0175(17) 0.0015(13) 0.0044(13) -0.0023(13) C10 0.0127(16) 0.0096(16) 0.0164(17) -0.0016(12) 0.0029(12) -0.0020(12) Cr1 0.0085(3) 0.0058(2) 0.0128(3) -0.00109(19) 0.00258(19) -0.00008(18) P1 0.0145(5) 0.0208(5) 0.0171(5) -0.0052(4) 0.0010(3) 0.0045(4) P2 0.0146(4) 0.0127(4) 0.0262(5) 0.0056(4) 0.0082(4) 0.0029(3) P3 0.0104(4) 0.0126(4) 0.0255(5) -0.0081(4) 0.0016(3) 0.0002(3) P4 0.0144(4) 0.0181(5) 0.0178(5) 0.0043(4) 0.0054(3) 0.0052(4) P5 0.0111(4) 0.0087(4) 0.0328(6) -0.0019(4) 0.0052(4) -0.0014(3) Cr2 0.0083(3) 0.0058(2) 0.0133(3) -0.00051(19) 0.00234(18) -0.00027(18) C11 0.0086(15) 0.0091(15) 0.0161(17) 0.0008(12) 0.0034(12) 0.0009(11) C12 0.0123(16) 0.0050(14) 0.0201(19) -0.0022(12) 0.0052(13) 0.0018(12) C13 0.0099(15) 0.0084(14) 0.0180(17) -0.0005(12) 0.0045(12) 0.0004(11) C14 0.0092(15) 0.0106(16) 0.0163(17) -0.0027(12) 0.0038(12) 0.0009(12) C15 0.0104(15) 0.0087(14) 0.0141(16) 0.0013(12) 0.0023(12) 0.0020(11) C16 0.0129(16) 0.0126(16) 0.0167(17) 0.0001(13) 0.0011(12) 0.0032(12) C17 0.0168(18) 0.0070(15) 0.027(2) -0.0005(14) 0.0071(14) -0.0035(13) C18 0.0150(18) 0.0130(17) 0.0215(19) -0.0047(13) 0.0028(14) -0.0029(13) C19 0.0159(17) 0.0128(16) 0.0170(17) 0.0054(13) 0.0062(13) 0.0059(13) C20 0.0105(16) 0.0082(15) 0.0229(19) 0.0005(13) 0.0024(13) -0.0016(12) C21 0.0129(17) 0.0092(15) 0.0196(19) 0.0032(13) 0.0047(14) -0.0010(12) C22 0.0133(17) 0.0091(16) 0.0191(19) 0.0030(12) 0.0041(14) 0.0020(12) C23 0.0118(16) 0.0087(15) 0.0205(18) 0.0011(13) 0.0035(13) 0.0027(12) C24 0.0165(17) 0.0097(14) 0.0134(16) 0.0020(13) 0.0057(13) 0.0038(13) C25 0.0146(17) 0.0085(15) 0.0152(17) 0.0006(12) 0.0035(13) 0.0021(12) C26 0.0140(17) 0.0110(16) 0.0217(19) 0.0039(13) 0.0041(13) -0.0029(13) C27 0.0137(17) 0.0101(16) 0.0202(18) 0.0016(13) 0.0034(13) 0.0038(12) C28 0.0102(16) 0.0168(18) 0.026(2) -0.0013(15) 0.0077(14) -0.0014(13) C29 0.023(2) 0.0089(16) 0.0213(19) 0.0040(13) 0.0077(14) 0.0011(13) C30 0.0136(17) 0.0169(18) 0.0164(17) 0.0048(14) 0.0022(13) 0.0041(13) Cr3 0.0093(3) 0.0073(2) 0.0165(3) 0.0032(2) 0.0036(2) 0.00099(19) P6 0.0147(4) 0.0101(4) 0.0175(5) -0.0022(3) 0.0054(3) -0.0031(3) P7 0.0168(4) 0.0084(4) 0.0149(4) 0.0005(3) 0.0026(3) 0.0021(3) P8 0.0115(4) 0.0125(4) 0.0187(5) -0.0017(3) 0.0041(3) -0.0014(3) P9 0.0181(5) 0.0075(4) 0.0153(4) 0.0008(3) 0.0046(3) -0.0008(3) P10 0.0124(4) 0.0107(4) 0.0163(4) -0.0016(3) 0.0019(3) 0.0032(3) Cr4 0.0091(3) 0.0066(2) 0.0148(3) 0.00164(19) 0.00235(19) -0.00013(18) C31 0.0139(17) 0.0100(16) 0.0155(17) 0.0016(12) 0.0047(13) -0.0020(12) C32 0.0159(17) 0.0096(14) 0.0132(16) 0.0003(12) 0.0035(12) -0.0002(12) C33 0.0099(15) 0.0075(15) 0.0184(17) 0.0006(13) 0.0009(12) -0.0008(12) C34 0.0124(17) 0.0085(16) 0.0160(18) -0.0001(12) 0.0014(13) -0.0016(11) C35 0.0113(16) 0.0088(14) 0.0135(17) 0.0023(12) 0.0006(12) -0.0003(12) C36 0.0143(17) 0.0116(16) 0.0202(18) -0.0006(13) 0.0041(13) -0.0034(13) C37 0.0177(18) 0.0073(15) 0.0175(17) 0.0031(12) 0.0030(13) -0.0011(12) C38 0.0098(16) 0.0127(16) 0.0220(18) 0.0018(13) 0.0016(13) 0.0001(12) C39 0.0168(18) 0.0085(15) 0.0203(18) 0.0035(13) 0.0049(13) -0.0037(13) C40 0.0140(17) 0.0132(16) 0.0183(17) 0.0000(13) 0.0002(13) 0.0033(13) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb1 F4 1.874(2) . ? Sb1 F6 1.874(2) . ? Sb1 F5 1.879(3) . ? Sb1 F2 1.880(2) . ? Sb1 F1 1.883(2) . ? Sb1 F3 1.886(2) . ? Sb2 F7 1.867(3) . ? Sb2 F11 1.871(2) . ? Sb2 F9 1.874(2) . ? Sb2 F12 1.879(2) . ? Sb2 F8 1.880(2) . ? Sb2 F10 1.887(2) . ? C1 C2 1.437(5) . ? C1 C5 1.437(5) . ? C1 C6 1.483(5) . ? C1 Cr1 2.217(4) . ? C2 C3 1.423(5) . ? C2 C7 1.494(5) . ? C2 Cr1 2.206(4) . ? C3 C4 1.438(5) . ? C3 C8 1.497(5) . ? C3 Cr1 2.204(3) . ? C4 C5 1.425(5) . ? C4 C9 1.492(5) . ? C4 Cr1 2.223(4) . ? C5 C10 1.502(5) . ? C5 Cr1 2.224(4) . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? Cr1 P5 2.3746(12) . ? Cr1 P3 2.3786(12) . ? Cr1 P1 2.3816(12) . ? Cr1 P4 2.3817(12) . ? Cr1 P2 2.3845(12) . ? Cr1 Cr2 2.8915(8) . ? P1 P2 2.2221(16) . ? P1 P5 2.2281(16) . ? P1 Cr2 2.3791(12) . ? P2 P3 2.2160(16) . ? P2 Cr2 2.3851(12) . ? P3 P4 2.2276(15) . ? P3 Cr2 2.3748(12) . ? P4 P5 2.2210(16) . ? P4 Cr2 2.3848(12) . ? P5 Cr2 2.3783(12) . ? Cr2 C12 2.217(4) . ? Cr2 C11 2.218(4) . ? Cr2 C14 2.218(4) . ? Cr2 C15 2.222(4) . ? Cr2 C13 2.223(4) . ? C11 C12 1.431(5) . ? C11 C15 1.434(5) . ? C11 C16 1.488(5) . ? C12 C13 1.438(5) . ? C12 C17 1.494(5) . ? C13 C14 1.424(5) . ? C13 C18 1.493(5) . ? C14 C15 1.430(5) . ? C14 C19 1.501(5) . ? C15 C20 1.494(5) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 C25 1.426(5) . ? C21 C22 1.433(6) . ? C21 C26 1.512(5) . ? C21 Cr3 2.217(4) . ? C22 C23 1.424(5) . ? C22 C27 1.505(5) . ? C22 Cr3 2.209(4) . ? C23 C24 1.431(5) . ? C23 C28 1.509(5) . ? C23 Cr3 2.201(4) . ? C24 C25 1.438(5) . ? C24 C29 1.496(5) . ? C24 Cr3 2.196(4) . ? C25 C30 1.504(5) . ? C25 Cr3 2.206(4) . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C27 H27C 0.9800 . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? Cr3 P6 2.4276(12) . ? Cr3 P10 2.4282(11) . ? Cr3 P8 2.4347(12) . ? Cr3 P9 2.4405(11) . ? Cr3 P7 2.4542(12) . ? P6 P10 2.1905(14) . ? P6 P7 2.1963(14) . ? P6 Cr4 2.4499(11) . ? P7 P8 2.1918(14) . ? P7 Cr4 2.4366(11) . ? P8 P9 2.1956(14) . ? P8 Cr4 2.4579(11) . ? P9 P10 2.2077(14) . ? P9 Cr4 2.4170(12) . ? P10 Cr4 2.4335(12) . ? Cr4 C31 2.188(4) . ? Cr4 C32 2.196(4) . ? Cr4 C35 2.206(4) . ? Cr4 C33 2.208(4) . ? Cr4 C34 2.214(4) . ? C31 C35 1.424(5) . ? C31 C32 1.440(5) . ? C31 C36 1.507(5) . ? C32 C33 1.433(5) . ? C32 C37 1.499(5) . ? C33 C34 1.417(5) . ? C33 C38 1.504(5) . ? C34 C35 1.435(5) . ? C34 C39 1.500(5) . ? C35 C40 1.495(5) . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C39 H39A 0.9800 . ? C39 H39B 0.9800 . ? C39 H39C 0.9800 . ? C40 H40A 0.9800 . ? C40 H40B 0.9800 . ? C40 H40C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F4 Sb1 F6 90.76(10) . . ? F4 Sb1 F5 90.19(11) . . ? F6 Sb1 F5 89.17(11) . . ? F4 Sb1 F2 178.48(12) . . ? F6 Sb1 F2 89.86(11) . . ? F5 Sb1 F2 91.21(12) . . ? F4 Sb1 F1 90.09(11) . . ? F6 Sb1 F1 178.83(11) . . ? F5 Sb1 F1 90.02(11) . . ? F2 Sb1 F1 89.32(11) . . ? F4 Sb1 F3 89.16(11) . . ? F6 Sb1 F3 90.58(11) . . ? F5 Sb1 F3 179.30(11) . . ? F2 Sb1 F3 89.44(11) . . ? F1 Sb1 F3 90.25(12) . . ? F7 Sb2 F11 90.11(12) . . ? F7 Sb2 F9 89.62(12) . . ? F11 Sb2 F9 179.72(13) . . ? F7 Sb2 F12 179.41(13) . . ? F11 Sb2 F12 89.77(11) . . ? F9 Sb2 F12 90.50(11) . . ? F7 Sb2 F8 91.10(12) . . ? F11 Sb2 F8 90.09(11) . . ? F9 Sb2 F8 89.84(11) . . ? F12 Sb2 F8 89.48(12) . . ? F7 Sb2 F10 90.72(13) . . ? F11 Sb2 F10 89.87(11) . . ? F9 Sb2 F10 90.21(11) . . ? F12 Sb2 F10 88.70(11) . . ? F8 Sb2 F10 178.18(12) . . ? C2 C1 C5 107.8(3) . . ? C2 C1 C6 126.7(3) . . ? C5 C1 C6 125.5(3) . . ? C2 C1 Cr1 70.6(2) . . ? C5 C1 Cr1 71.4(2) . . ? C6 C1 Cr1 125.7(3) . . ? C3 C2 C1 107.7(3) . . ? C3 C2 C7 127.2(3) . . ? C1 C2 C7 125.0(3) . . ? C3 C2 Cr1 71.1(2) . . ? C1 C2 Cr1 71.5(2) . . ? C7 C2 Cr1 126.0(2) . . ? C2 C3 C4 108.8(3) . . ? C2 C3 C8 126.7(3) . . ? C4 C3 C8 124.5(3) . . ? C2 C3 Cr1 71.2(2) . . ? C4 C3 Cr1 71.7(2) . . ? C8 C3 Cr1 124.8(3) . . ? C5 C4 C3 107.4(3) . . ? C5 C4 C9 126.2(3) . . ? C3 C4 C9 126.4(3) . . ? C5 C4 Cr1 71.4(2) . . ? C3 C4 Cr1 70.36(19) . . ? C9 C4 Cr1 126.0(2) . . ? C4 C5 C1 108.4(3) . . ? C4 C5 C10 126.8(3) . . ? C1 C5 C10 124.5(3) . . ? C4 C5 Cr1 71.3(2) . . ? C1 C5 Cr1 70.9(2) . . ? C10 C5 Cr1 128.0(3) . . ? C1 C6 H6A 109.5 . . ? C1 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C1 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C3 Cr1 C2 37.66(14) . . ? C3 Cr1 C1 62.96(14) . . ? C2 Cr1 C1 37.91(13) . . ? C3 Cr1 C4 37.90(12) . . ? C2 Cr1 C4 63.36(13) . . ? C1 Cr1 C4 63.05(13) . . ? C3 Cr1 C5 62.79(13) . . ? C2 Cr1 C5 63.21(13) . . ? C1 Cr1 C5 37.75(13) . . ? C4 Cr1 C5 37.38(13) . . ? C3 Cr1 P5 136.35(10) . . ? C2 Cr1 P5 159.89(10) . . ? C1 Cr1 P5 124.22(10) . . ? C4 Cr1 P5 102.26(10) . . ? C5 Cr1 P5 96.75(10) . . ? C3 Cr1 P3 95.90(10) . . ? C2 Cr1 P3 101.68(10) . . ? C1 Cr1 P3 136.05(10) . . ? C4 Cr1 P3 123.54(10) . . ? C5 Cr1 P3 158.60(10) . . ? P5 Cr1 P3 98.08(4) . . ? C3 Cr1 P1 159.70(11) . . ? C2 Cr1 P1 124.10(11) . . ? C1 Cr1 P1 96.88(10) . . ? C4 Cr1 P1 136.84(10) . . ? C5 Cr1 P1 103.25(10) . . ? P5 Cr1 P1 55.87(4) . . ? P3 Cr1 P1 97.83(4) . . ? C3 Cr1 P4 101.78(11) . . ? C2 Cr1 P4 135.65(11) . . ? C1 Cr1 P4 158.78(10) . . ? C4 Cr1 P4 95.79(10) . . ? C5 Cr1 P4 123.40(10) . . ? P5 Cr1 P4 55.67(4) . . ? P3 Cr1 P4 55.80(4) . . ? P1 Cr1 P4 98.29(4) . . ? C3 Cr1 P2 123.43(10) . . ? C2 Cr1 P2 96.00(10) . . ? C1 Cr1 P2 102.51(10) . . ? C4 Cr1 P2 159.24(10) . . ? C5 Cr1 P2 136.83(10) . . ? P5 Cr1 P2 98.27(4) . . ? P3 Cr1 P2 55.45(4) . . ? P1 Cr1 P2 55.58(4) . . ? P4 Cr1 P2 98.28(4) . . ? C3 Cr1 Cr2 146.09(10) . . ? C2 Cr1 Cr2 146.25(10) . . ? C1 Cr1 Cr2 147.19(10) . . ? C4 Cr1 Cr2 146.35(9) . . ? C5 Cr1 Cr2 147.30(10) . . ? P5 Cr1 Cr2 52.59(3) . . ? P3 Cr1 Cr2 52.47(3) . . ? P1 Cr1 Cr2 52.56(3) . . ? P4 Cr1 Cr2 52.70(3) . . ? P2 Cr1 Cr2 52.69(3) . . ? P2 P1 P5 107.95(6) . . ? P2 P1 Cr2 62.34(4) . . ? P5 P1 Cr2 62.06(4) . . ? P2 P1 Cr1 62.28(4) . . ? P5 P1 Cr1 61.91(4) . . ? Cr2 P1 Cr1 74.80(4) . . ? P3 P2 P1 107.89(6) . . ? P3 P2 Cr1 62.14(4) . . ? P1 P2 Cr1 62.14(4) . . ? P3 P2 Cr2 62.02(4) . . ? P1 P2 Cr2 62.06(4) . . ? Cr1 P2 Cr2 74.63(4) . . ? P2 P3 P4 108.43(6) . . ? P2 P3 Cr2 62.49(4) . . ? P4 P3 Cr2 62.32(4) . . ? P2 P3 Cr1 62.41(4) . . ? P4 P3 Cr1 62.17(4) . . ? Cr2 P3 Cr1 74.93(4) . . ? P5 P4 P3 107.58(6) . . ? P5 P4 Cr1 62.00(4) . . ? P3 P4 Cr1 62.03(4) . . ? P5 P4 Cr2 62.06(4) . . ? P3 P4 Cr2 61.87(4) . . ? Cr1 P4 Cr2 74.69(4) . . ? P4 P5 P1 108.15(6) . . ? P4 P5 Cr1 62.33(4) . . ? P1 P5 Cr1 62.22(4) . . ? P4 P5 Cr2 62.35(4) . . ? P1 P5 Cr2 62.09(4) . . ? Cr1 P5 Cr2 74.94(4) . . ? C12 Cr2 C11 37.65(13) . . ? C12 Cr2 C14 62.93(14) . . ? C11 Cr2 C14 62.68(14) . . ? C12 Cr2 C15 63.18(13) . . ? C11 Cr2 C15 37.68(13) . . ? C14 Cr2 C15 37.56(13) . . ? C12 Cr2 C13 37.79(14) . . ? C11 Cr2 C13 62.78(14) . . ? C14 Cr2 C13 37.40(13) . . ? C15 Cr2 C13 62.87(13) . . ? C12 Cr2 P3 105.01(10) . . ? C11 Cr2 P3 140.33(10) . . ? C14 Cr2 P3 120.80(10) . . ? C15 Cr2 P3 157.65(10) . . ? C13 Cr2 P3 95.91(10) . . ? C12 Cr2 P5 156.88(11) . . ? C11 Cr2 P5 120.19(10) . . ? C14 Cr2 P5 103.94(10) . . ? C15 Cr2 P5 94.59(9) . . ? C13 Cr2 P5 138.99(10) . . ? P3 Cr2 P5 98.08(4) . . ? C12 Cr2 P1 120.68(11) . . ? C11 Cr2 P1 95.51(10) . . ? C14 Cr2 P1 139.54(10) . . ? C15 Cr2 P1 104.34(10) . . ? C13 Cr2 P1 157.44(11) . . ? P3 Cr2 P1 98.01(4) . . ? P5 Cr2 P1 55.85(4) . . ? C12 Cr2 P4 139.70(11) . . ? C11 Cr2 P4 156.54(10) . . ? C14 Cr2 P4 94.89(10) . . ? C15 Cr2 P4 119.77(10) . . ? C13 Cr2 P4 104.23(10) . . ? P3 Cr2 P4 55.81(4) . . ? P5 Cr2 P4 55.59(4) . . ? P1 Cr2 P4 98.28(4) . . ? C12 Cr2 P2 95.97(11) . . ? C11 Cr2 P2 105.27(10) . . ? C14 Cr2 P2 157.90(10) . . ? C15 Cr2 P2 140.35(10) . . ? C13 Cr2 P2 121.34(10) . . ? P3 Cr2 P2 55.49(4) . . ? P5 Cr2 P2 98.15(4) . . ? P1 Cr2 P2 55.60(4) . . ? P4 Cr2 P2 98.18(4) . . ? C12 Cr2 Cr1 147.44(11) . . ? C11 Cr2 Cr1 147.12(10) . . ? C14 Cr2 Cr1 146.14(10) . . ? C15 Cr2 Cr1 145.92(9) . . ? C13 Cr2 Cr1 147.04(10) . . ? P3 Cr2 Cr1 52.59(3) . . ? P5 Cr2 Cr1 52.47(3) . . ? P1 Cr2 Cr1 52.64(3) . . ? P4 Cr2 Cr1 52.61(3) . . ? P2 Cr2 Cr1 52.67(3) . . ? C12 C11 C15 108.5(3) . . ? C12 C11 C16 124.4(3) . . ? C15 C11 C16 126.9(3) . . ? C12 C11 Cr2 71.1(2) . . ? C15 C11 Cr2 71.3(2) . . ? C16 C11 Cr2 126.5(3) . . ? C11 C12 C13 107.5(3) . . ? C11 C12 C17 126.7(4) . . ? C13 C12 C17 125.6(3) . . ? C11 C12 Cr2 71.2(2) . . ? C13 C12 Cr2 71.3(2) . . ? C17 C12 Cr2 126.4(3) . . ? C14 C13 C12 108.0(3) . . ? C14 C13 C18 126.1(3) . . ? C12 C13 C18 125.7(3) . . ? C14 C13 Cr2 71.1(2) . . ? C12 C13 Cr2 70.9(2) . . ? C18 C13 Cr2 126.9(3) . . ? C13 C14 C15 108.7(3) . . ? C13 C14 C19 126.3(3) . . ? C15 C14 C19 125.0(3) . . ? C13 C14 Cr2 71.5(2) . . ? C15 C14 Cr2 71.4(2) . . ? C19 C14 Cr2 125.5(3) . . ? C14 C15 C11 107.3(3) . . ? C14 C15 C20 125.9(3) . . ? C11 C15 C20 126.7(3) . . ? C14 C15 Cr2 71.1(2) . . ? C11 C15 Cr2 71.0(2) . . ? C20 C15 Cr2 125.5(2) . . ? C11 C16 H16A 109.5 . . ? C11 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C11 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C25 C21 C22 107.7(3) . . ? C25 C21 C26 125.3(4) . . ? C22 C21 C26 126.8(3) . . ? C25 C21 Cr3 70.8(2) . . ? C22 C21 Cr3 70.8(2) . . ? C26 C21 Cr3 127.3(3) . . ? C23 C22 C21 108.4(3) . . ? C23 C22 C27 124.9(4) . . ? C21 C22 C27 126.6(3) . . ? C23 C22 Cr3 70.9(2) . . ? C21 C22 Cr3 71.4(2) . . ? C27 C22 Cr3 127.0(3) . . ? C22 C23 C24 108.1(3) . . ? C22 C23 C28 125.5(3) . . ? C24 C23 C28 126.3(3) . . ? C22 C23 Cr3 71.5(2) . . ? C24 C23 Cr3 70.8(2) . . ? C28 C23 Cr3 126.6(3) . . ? C23 C24 C25 107.6(3) . . ? C23 C24 C29 125.4(4) . . ? C25 C24 C29 126.7(3) . . ? C23 C24 Cr3 71.2(2) . . ? C25 C24 Cr3 71.3(2) . . ? C29 C24 Cr3 127.0(3) . . ? C21 C25 C24 108.2(3) . . ? C21 C25 C30 125.7(4) . . ? C24 C25 C30 126.0(3) . . ? C21 C25 Cr3 71.6(2) . . ? C24 C25 Cr3 70.5(2) . . ? C30 C25 Cr3 126.6(3) . . ? C21 C26 H26A 109.5 . . ? C21 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C21 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C22 C27 H27A 109.5 . . ? C22 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? C22 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? C23 C28 H28A 109.5 . . ? C23 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C23 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C24 C29 H29A 109.5 . . ? C24 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C24 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C25 C30 H30A 109.5 . . ? C25 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? C25 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C24 Cr3 C23 37.98(13) . . ? C24 Cr3 C25 38.14(14) . . ? C23 Cr3 C25 63.38(14) . . ? C24 Cr3 C22 63.30(14) . . ? C23 Cr3 C22 37.69(14) . . ? C25 Cr3 C22 63.05(15) . . ? C24 Cr3 C21 63.44(14) . . ? C23 Cr3 C21 63.25(14) . . ? C25 Cr3 C21 37.62(14) . . ? C22 Cr3 C21 37.77(14) . . ? C24 Cr3 P6 148.58(11) . . ? C23 Cr3 P6 155.12(10) . . ? C25 Cr3 P6 111.64(11) . . ? C22 Cr3 P6 117.49(11) . . ? C21 Cr3 P6 97.41(11) . . ? C24 Cr3 P10 110.49(10) . . ? C23 Cr3 P10 147.53(10) . . ? C25 Cr3 P10 96.11(10) . . ? C22 Cr3 P10 154.20(11) . . ? C21 Cr3 P10 116.43(11) . . ? P6 Cr3 P10 53.63(4) . . ? C24 Cr3 P8 115.52(11) . . ? C23 Cr3 P8 95.84(11) . . ? C25 Cr3 P8 153.64(11) . . ? C22 Cr3 P8 111.13(11) . . ? C21 Cr3 P8 148.10(11) . . ? P6 Cr3 P8 94.00(4) . . ? P10 Cr3 P8 94.26(4) . . ? C24 Cr3 P9 95.50(10) . . ? C23 Cr3 P9 110.49(10) . . ? C25 Cr3 P9 116.15(10) . . ? C22 Cr3 P9 147.34(11) . . ? C21 Cr3 P9 153.76(11) . . ? P6 Cr3 P9 93.71(4) . . ? P10 Cr3 P9 53.93(4) . . ? P8 Cr3 P9 53.53(4) . . ? C24 Cr3 P7 155.12(11) . . ? C23 Cr3 P7 117.29(10) . . ? C25 Cr3 P7 149.43(10) . . ? C22 Cr3 P7 98.16(11) . . ? C21 Cr3 P7 112.89(11) . . ? P6 Cr3 P7 53.47(4) . . ? P10 Cr3 P7 93.33(4) . . ? P8 Cr3 P7 53.27(4) . . ? P9 Cr3 P7 92.81(4) . . ? P10 P6 P7 108.10(5) . . ? P10 P6 Cr3 63.20(4) . . ? P7 P6 Cr3 63.88(4) . . ? P10 P6 Cr4 62.97(4) . . ? P7 P6 Cr4 62.98(4) . . ? Cr3 P6 Cr4 79.92(4) . . ? P8 P7 P6 108.26(5) . . ? P8 P7 Cr4 63.90(4) . . ? P6 P7 Cr4 63.60(4) . . ? P8 P7 Cr3 62.91(4) . . ? P6 P7 Cr3 62.65(4) . . ? Cr4 P7 Cr3 79.66(3) . . ? P7 P8 P9 107.79(5) . . ? P7 P8 Cr3 63.82(4) . . ? P9 P8 Cr3 63.37(4) . . ? P7 P8 Cr4 62.90(4) . . ? P9 P8 Cr4 62.28(4) . . ? Cr3 P8 Cr4 79.62(4) . . ? P8 P9 P10 108.08(5) . . ? P8 P9 Cr4 64.19(4) . . ? P10 P9 Cr4 63.31(4) . . ? P8 P9 Cr3 63.10(4) . . ? P10 P9 Cr3 62.75(4) . . ? Cr4 P9 Cr3 80.32(4) . . ? P6 P10 P9 107.72(5) . . ? P6 P10 Cr3 63.17(4) . . ? P9 P10 Cr3 63.32(4) . . ? P6 P10 Cr4 63.73(4) . . ? P9 P10 Cr4 62.54(4) . . ? Cr3 P10 Cr4 80.23(4) . . ? C31 Cr4 C32 38.35(14) . . ? C31 Cr4 C35 37.81(13) . . ? C32 Cr4 C35 63.65(14) . . ? C31 Cr4 C33 63.48(14) . . ? C32 Cr4 C33 37.96(14) . . ? C35 Cr4 C33 63.18(13) . . ? C31 Cr4 C34 63.23(14) . . ? C32 Cr4 C34 63.21(14) . . ? C35 Cr4 C34 37.89(14) . . ? C33 Cr4 C34 37.37(13) . . ? C31 Cr4 P9 140.14(11) . . ? C32 Cr4 P9 160.48(10) . . ? C35 Cr4 P9 105.72(10) . . ? C33 Cr4 P9 123.27(10) . . ? C34 Cr4 P9 98.11(11) . . ? C31 Cr4 P10 104.83(11) . . ? C32 Cr4 P10 139.85(11) . . ? C35 Cr4 P10 97.15(10) . . ? C33 Cr4 P10 159.63(10) . . ? C34 Cr4 P10 123.25(10) . . ? P9 Cr4 P10 54.15(4) . . ? C31 Cr4 P7 123.30(10) . . ? C32 Cr4 P7 97.82(10) . . ? C35 Cr4 P7 160.43(10) . . ? C33 Cr4 P7 106.72(10) . . ? C34 Cr4 P7 141.02(11) . . ? P9 Cr4 P7 93.83(4) . . ? P10 Cr4 P7 93.64(4) . . ? C31 Cr4 P6 97.44(10) . . ? C32 Cr4 P6 105.78(10) . . ? C35 Cr4 P6 122.84(10) . . ? C33 Cr4 P6 140.83(10) . . ? C34 Cr4 P6 159.85(11) . . ? P9 Cr4 P6 93.74(4) . . ? P10 Cr4 P6 53.30(4) . . ? P7 Cr4 P6 53.42(4) . . ? C31 Cr4 P8 161.60(11) . . ? C32 Cr4 P8 123.88(11) . . ? C35 Cr4 P8 141.60(10) . . ? C33 Cr4 P8 99.16(10) . . ? C34 Cr4 P8 107.29(11) . . ? P9 Cr4 P8 53.53(4) . . ? P10 Cr4 P8 93.54(4) . . ? P7 Cr4 P8 53.20(4) . . ? P6 Cr4 P8 92.86(4) . . ? C35 C31 C32 108.3(3) . . ? C35 C31 C36 126.0(3) . . ? C32 C31 C36 125.7(3) . . ? C35 C31 Cr4 71.8(2) . . ? C32 C31 Cr4 71.1(2) . . ? C36 C31 Cr4 124.8(3) . . ? C33 C32 C31 107.3(3) . . ? C33 C32 C37 126.9(3) . . ? C31 C32 C37 125.8(3) . . ? C33 C32 Cr4 71.5(2) . . ? C31 C32 Cr4 70.5(2) . . ? C37 C32 Cr4 125.3(3) . . ? C34 C33 C32 108.4(3) . . ? C34 C33 C38 124.5(3) . . ? C32 C33 C38 127.1(3) . . ? C34 C33 Cr4 71.5(2) . . ? C32 C33 Cr4 70.5(2) . . ? C38 C33 Cr4 125.6(3) . . ? C33 C34 C35 108.4(3) . . ? C33 C34 C39 125.9(4) . . ? C35 C34 C39 125.7(3) . . ? C33 C34 Cr4 71.1(2) . . ? C35 C34 Cr4 70.7(2) . . ? C39 C34 Cr4 126.9(3) . . ? C31 C35 C34 107.7(3) . . ? C31 C35 C40 126.2(3) . . ? C34 C35 C40 126.0(3) . . ? C31 C35 Cr4 70.4(2) . . ? C34 C35 Cr4 71.4(2) . . ? C40 C35 Cr4 126.0(3) . . ? C31 C36 H36A 109.5 . . ? C31 C36 H36B 109.5 . . ? H36A C36 H36B 109.5 . . ? C31 C36 H36C 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C32 C37 H37A 109.5 . . ? C32 C37 H37B 109.5 . . ? H37A C37 H37B 109.5 . . ? C32 C37 H37C 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? C33 C38 H38A 109.5 . . ? C33 C38 H38B 109.5 . . ? H38A C38 H38B 109.5 . . ? C33 C38 H38C 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? C34 C39 H39A 109.5 . . ? C34 C39 H39B 109.5 . . ? H39A C39 H39B 109.5 . . ? C34 C39 H39C 109.5 . . ? H39A C39 H39C 109.5 . . ? H39B C39 H39C 109.5 . . ? C35 C40 H40A 109.5 . . ? C35 C40 H40B 109.5 . . ? H40A C40 H40B 109.5 . . ? C35 C40 H40C 109.5 . . ? H40A C40 H40C 109.5 . . ? H40B C40 H40C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 C1 C2 C3 -0.2(4) . . . . ? C6 C1 C2 C3 177.0(3) . . . . ? Cr1 C1 C2 C3 -62.3(2) . . . . ? C5 C1 C2 C7 -176.4(3) . . . . ? C6 C1 C2 C7 0.8(6) . . . . ? Cr1 C1 C2 C7 121.5(4) . . . . ? C5 C1 C2 Cr1 62.1(2) . . . . ? C6 C1 C2 Cr1 -120.7(4) . . . . ? C1 C2 C3 C4 0.2(4) . . . . ? C7 C2 C3 C4 176.3(3) . . . . ? Cr1 C2 C3 C4 -62.3(2) . . . . ? C1 C2 C3 C8 -177.6(3) . . . . ? C7 C2 C3 C8 -1.5(6) . . . . ? Cr1 C2 C3 C8 119.8(4) . . . . ? C1 C2 C3 Cr1 62.5(2) . . . . ? C7 C2 C3 Cr1 -121.4(4) . . . . ? C2 C3 C4 C5 -0.2(4) . . . . ? C8 C3 C4 C5 177.8(3) . . . . ? Cr1 C3 C4 C5 -62.1(2) . . . . ? C2 C3 C4 C9 -177.2(3) . . . . ? C8 C3 C4 C9 0.7(6) . . . . ? Cr1 C3 C4 C9 120.8(4) . . . . ? C2 C3 C4 Cr1 62.0(2) . . . . ? C8 C3 C4 Cr1 -120.1(4) . . . . ? C3 C4 C5 C1 0.0(4) . . . . ? C9 C4 C5 C1 177.1(3) . . . . ? Cr1 C4 C5 C1 -61.4(2) . . . . ? C3 C4 C5 C10 -174.6(3) . . . . ? C9 C4 C5 C10 2.4(6) . . . . ? Cr1 C4 C5 C10 123.9(4) . . . . ? C3 C4 C5 Cr1 61.5(2) . . . . ? C9 C4 C5 Cr1 -121.5(4) . . . . ? C2 C1 C5 C4 0.1(4) . . . . ? C6 C1 C5 C4 -177.2(3) . . . . ? Cr1 C1 C5 C4 61.7(2) . . . . ? C2 C1 C5 C10 174.9(3) . . . . ? C6 C1 C5 C10 -2.4(6) . . . . ? Cr1 C1 C5 C10 -123.5(3) . . . . ? C2 C1 C5 Cr1 -61.6(2) . . . . ? C6 C1 C5 Cr1 121.1(4) . . . . ? C4 C3 Cr1 C2 118.0(3) . . . . ? C8 C3 Cr1 C2 -122.2(4) . . . . ? C2 C3 Cr1 C1 -38.0(2) . . . . ? C4 C3 Cr1 C1 80.1(2) . . . . ? C8 C3 Cr1 C1 -160.2(3) . . . . ? C2 C3 Cr1 C4 -118.0(3) . . . . ? C8 C3 Cr1 C4 119.8(4) . . . . ? C2 C3 Cr1 C5 -80.6(2) . . . . ? C4 C3 Cr1 C5 37.4(2) . . . . ? C8 C3 Cr1 C5 157.2(4) . . . . ? C2 C3 Cr1 P5 -150.27(17) . . . . ? C4 C3 Cr1 P5 -32.3(3) . . . . ? C8 C3 Cr1 P5 87.5(3) . . . . ? C2 C3 Cr1 P3 101.49(19) . . . . ? C4 C3 Cr1 P3 -140.5(2) . . . . ? C8 C3 Cr1 P3 -20.7(3) . . . . ? C2 C3 Cr1 P1 -30.9(4) . . . . ? C4 C3 Cr1 P1 87.1(3) . . . . ? C8 C3 Cr1 P1 -153.1(2) . . . . ? C2 C3 Cr1 P4 157.74(18) . . . . ? C4 C3 Cr1 P4 -84.2(2) . . . . ? C8 C3 Cr1 P4 35.5(3) . . . . ? C2 C3 Cr1 P2 49.4(2) . . . . ? C4 C3 Cr1 P2 167.46(17) . . . . ? C8 C3 Cr1 P2 -72.8(3) . . . . ? C2 C3 Cr1 Cr2 120.8(2) . . . . ? C4 C3 Cr1 Cr2 -121.2(2) . . . . ? C8 C3 Cr1 Cr2 -1.4(4) . . . . ? C1 C2 Cr1 C3 -116.9(3) . . . . ? C7 C2 Cr1 C3 122.8(4) . . . . ? C3 C2 Cr1 C1 116.9(3) . . . . ? C7 C2 Cr1 C1 -120.3(4) . . . . ? C3 C2 Cr1 C4 37.3(2) . . . . ? C1 C2 Cr1 C4 -79.6(2) . . . . ? C7 C2 Cr1 C4 160.1(4) . . . . ? C3 C2 Cr1 C5 79.4(2) . . . . ? C1 C2 Cr1 C5 -37.5(2) . . . . ? C7 C2 Cr1 C5 -157.8(4) . . . . ? C3 C2 Cr1 P5 84.6(4) . . . . ? C1 C2 Cr1 P5 -32.4(4) . . . . ? C7 C2 Cr1 P5 -152.7(3) . . . . ? C3 C2 Cr1 P3 -84.49(19) . . . . ? C1 C2 Cr1 P3 158.59(18) . . . . ? C7 C2 Cr1 P3 38.3(3) . . . . ? C3 C2 Cr1 P1 167.58(17) . . . . ? C1 C2 Cr1 P1 50.7(2) . . . . ? C7 C2 Cr1 P1 -69.7(3) . . . . ? C3 C2 Cr1 P4 -32.0(3) . . . . ? C1 C2 Cr1 P4 -148.96(17) . . . . ? C7 C2 Cr1 P4 90.7(3) . . . . ? C3 C2 Cr1 P2 -140.39(19) . . . . ? C1 C2 Cr1 P2 102.69(19) . . . . ? C7 C2 Cr1 P2 -17.6(3) . . . . ? C3 C2 Cr1 Cr2 -120.4(2) . . . . ? C1 C2 Cr1 Cr2 122.7(2) . . . . ? C7 C2 Cr1 Cr2 2.4(4) . . . . ? C2 C1 Cr1 C3 37.7(2) . . . . ? C5 C1 Cr1 C3 -79.7(2) . . . . ? C6 C1 Cr1 C3 159.5(4) . . . . ? C5 C1 Cr1 C2 -117.4(3) . . . . ? C6 C1 Cr1 C2 121.8(4) . . . . ? C2 C1 Cr1 C4 80.4(2) . . . . ? C5 C1 Cr1 C4 -36.9(2) . . . . ? C6 C1 Cr1 C4 -157.8(4) . . . . ? C2 C1 Cr1 C5 117.4(3) . . . . ? C6 C1 Cr1 C5 -120.8(4) . . . . ? C2 C1 Cr1 P5 167.14(17) . . . . ? C5 C1 Cr1 P5 49.8(2) . . . . ? C6 C1 Cr1 P5 -71.1(3) . . . . ? C2 C1 Cr1 P3 -31.0(3) . . . . ? C5 C1 Cr1 P3 -148.38(18) . . . . ? C6 C1 Cr1 P3 90.8(3) . . . . ? C2 C1 Cr1 P1 -139.83(19) . . . . ? C5 C1 Cr1 P1 102.8(2) . . . . ? C6 C1 Cr1 P1 -18.0(3) . . . . ? C2 C1 Cr1 P4 84.8(3) . . . . ? C5 C1 Cr1 P4 -32.6(4) . . . . ? C6 C1 Cr1 P4 -153.5(2) . . . . ? C2 C1 Cr1 P2 -83.6(2) . . . . ? C5 C1 Cr1 P2 158.98(19) . . . . ? C6 C1 Cr1 P2 38.1(3) . . . . ? C2 C1 Cr1 Cr2 -120.4(2) . . . . ? C5 C1 Cr1 Cr2 122.2(2) . . . . ? C6 C1 Cr1 Cr2 1.4(4) . . . . ? C5 C4 Cr1 C3 117.1(3) . . . . ? C9 C4 Cr1 C3 -121.2(4) . . . . ? C5 C4 Cr1 C2 80.0(2) . . . . ? C3 C4 Cr1 C2 -37.1(2) . . . . ? C9 C4 Cr1 C2 -158.4(4) . . . . ? C5 C4 Cr1 C1 37.3(2) . . . . ? C3 C4 Cr1 C1 -79.8(2) . . . . ? C9 C4 Cr1 C1 159.0(4) . . . . ? C3 C4 Cr1 C5 -117.1(3) . . . . ? C9 C4 Cr1 C5 121.7(4) . . . . ? C5 C4 Cr1 P5 -85.1(2) . . . . ? C3 C4 Cr1 P5 157.9(2) . . . . ? C9 C4 Cr1 P5 36.6(3) . . . . ? C5 C4 Cr1 P3 166.49(17) . . . . ? C3 C4 Cr1 P3 49.4(2) . . . . ? C9 C4 Cr1 P3 -71.8(3) . . . . ? C5 C4 Cr1 P1 -32.5(3) . . . . ? C3 C4 Cr1 P1 -149.57(19) . . . . ? C9 C4 Cr1 P1 89.2(3) . . . . ? C5 C4 Cr1 P4 -141.14(19) . . . . ? C3 C4 Cr1 P4 101.8(2) . . . . ? C9 C4 Cr1 P4 -19.5(3) . . . . ? C5 C4 Cr1 P2 86.3(3) . . . . ? C3 C4 Cr1 P2 -30.8(4) . . . . ? C9 C4 Cr1 P2 -152.0(2) . . . . ? C5 C4 Cr1 Cr2 -122.4(2) . . . . ? C3 C4 Cr1 Cr2 120.5(2) . . . . ? C9 C4 Cr1 Cr2 -0.7(4) . . . . ? C4 C5 Cr1 C3 -37.9(2) . . . . ? C1 C5 Cr1 C3 80.1(2) . . . . ? C10 C5 Cr1 C3 -160.5(4) . . . . ? C4 C5 Cr1 C2 -80.4(2) . . . . ? C1 C5 Cr1 C2 37.7(2) . . . . ? C10 C5 Cr1 C2 157.0(4) . . . . ? C4 C5 Cr1 C1 -118.1(3) . . . . ? C10 C5 Cr1 C1 119.4(4) . . . . ? C1 C5 Cr1 C4 118.1(3) . . . . ? C10 C5 Cr1 C4 -122.6(4) . . . . ? C4 C5 Cr1 P5 101.38(19) . . . . ? C1 C5 Cr1 P5 -140.5(2) . . . . ? C10 C5 Cr1 P5 -21.2(3) . . . . ? C4 C5 Cr1 P3 -32.2(4) . . . . ? C1 C5 Cr1 P3 85.8(3) . . . . ? C10 C5 Cr1 P3 -154.8(2) . . . . ? C4 C5 Cr1 P1 157.83(18) . . . . ? C1 C5 Cr1 P1 -84.1(2) . . . . ? C10 C5 Cr1 P1 35.3(3) . . . . ? C4 C5 Cr1 P4 48.4(2) . . . . ? C1 C5 Cr1 P4 166.48(17) . . . . ? C10 C5 Cr1 P4 -74.2(3) . . . . ? C4 C5 Cr1 P2 -148.87(17) . . . . ? C1 C5 Cr1 P2 -30.8(3) . . . . ? C10 C5 Cr1 P2 88.6(3) . . . . ? C4 C5 Cr1 Cr2 119.9(2) . . . . ? C1 C5 Cr1 Cr2 -122.0(2) . . . . ? C10 C5 Cr1 Cr2 -2.6(5) . . . . ? C3 Cr1 P1 P2 94.1(3) . . . . ? C2 Cr1 P1 P2 71.89(12) . . . . ? C1 Cr1 P1 P2 100.48(10) . . . . ? C4 Cr1 P1 P2 157.89(14) . . . . ? C5 Cr1 P1 P2 138.32(11) . . . . ? P5 Cr1 P1 P2 -132.46(6) . . . . ? P3 Cr1 P1 P2 -37.98(5) . . . . ? P4 Cr1 P1 P2 -94.39(5) . . . . ? Cr2 Cr1 P1 P2 -66.38(4) . . . . ? C3 Cr1 P1 P5 -133.4(3) . . . . ? C2 Cr1 P1 P5 -155.65(12) . . . . ? C1 Cr1 P1 P5 -127.05(10) . . . . ? C4 Cr1 P1 P5 -69.65(14) . . . . ? C5 Cr1 P1 P5 -89.22(11) . . . . ? P3 Cr1 P1 P5 94.48(5) . . . . ? P4 Cr1 P1 P5 38.07(5) . . . . ? P2 Cr1 P1 P5 132.46(6) . . . . ? Cr2 Cr1 P1 P5 66.08(4) . . . . ? C3 Cr1 P1 Cr2 160.5(3) . . . . ? C2 Cr1 P1 Cr2 138.26(12) . . . . ? C1 Cr1 P1 Cr2 166.86(10) . . . . ? C4 Cr1 P1 Cr2 -135.74(14) . . . . ? C5 Cr1 P1 Cr2 -155.30(10) . . . . ? P5 Cr1 P1 Cr2 -66.08(4) . . . . ? P3 Cr1 P1 Cr2 28.40(4) . . . . ? P4 Cr1 P1 Cr2 -28.01(4) . . . . ? P2 Cr1 P1 Cr2 66.38(4) . . . . ? P5 P1 P2 P3 0.28(7) . . . . ? Cr2 P1 P2 P3 -43.17(5) . . . . ? Cr1 P1 P2 P3 43.45(5) . . . . ? P5 P1 P2 Cr1 -43.16(5) . . . . ? Cr2 P1 P2 Cr1 -86.62(4) . . . . ? P5 P1 P2 Cr2 43.46(5) . . . . ? Cr1 P1 P2 Cr2 86.62(4) . . . . ? C3 Cr1 P2 P3 72.25(13) . . . . ? C2 Cr1 P2 P3 100.06(10) . . . . ? C1 Cr1 P2 P3 137.95(11) . . . . ? C4 Cr1 P2 P3 94.4(3) . . . . ? C5 Cr1 P2 P3 156.67(15) . . . . ? P5 Cr1 P2 P3 -94.15(5) . . . . ? P1 Cr1 P2 P3 -132.25(6) . . . . ? P4 Cr1 P2 P3 -37.83(5) . . . . ? Cr2 Cr1 P2 P3 -66.10(4) . . . . ? C3 Cr1 P2 P1 -155.50(13) . . . . ? C2 Cr1 P2 P1 -127.69(11) . . . . ? C1 Cr1 P2 P1 -89.80(11) . . . . ? C4 Cr1 P2 P1 -133.4(3) . . . . ? C5 Cr1 P2 P1 -71.08(15) . . . . ? P5 Cr1 P2 P1 38.10(5) . . . . ? P3 Cr1 P2 P1 132.25(6) . . . . ? P4 Cr1 P2 P1 94.41(5) . . . . ? Cr2 Cr1 P2 P1 66.15(4) . . . . ? C3 Cr1 P2 Cr2 138.35(13) . . . . ? C2 Cr1 P2 Cr2 166.17(10) . . . . ? C1 Cr1 P2 Cr2 -155.95(10) . . . . ? C4 Cr1 P2 Cr2 160.5(3) . . . . ? C5 Cr1 P2 Cr2 -137.23(14) . . . . ? P5 Cr1 P2 Cr2 -28.05(4) . . . . ? P3 Cr1 P2 Cr2 66.10(4) . . . . ? P1 Cr1 P2 Cr2 -66.15(4) . . . . ? P4 Cr1 P2 Cr2 28.27(4) . . . . ? P1 P2 P3 P4 -0.29(7) . . . . ? Cr1 P2 P3 P4 43.16(5) . . . . ? Cr2 P2 P3 P4 -43.48(5) . . . . ? P1 P2 P3 Cr2 43.20(5) . . . . ? Cr1 P2 P3 Cr2 86.64(4) . . . . ? P1 P2 P3 Cr1 -43.45(5) . . . . ? Cr2 P2 P3 Cr1 -86.64(4) . . . . ? C3 Cr1 P3 P2 -126.96(11) . . . . ? C2 Cr1 P3 P2 -89.27(11) . . . . ? C1 Cr1 P3 P2 -70.42(15) . . . . ? C4 Cr1 P3 P2 -154.92(12) . . . . ? C5 Cr1 P3 P2 -132.0(3) . . . . ? P5 Cr1 P3 P2 94.51(5) . . . . ? P1 Cr1 P3 P2 38.05(5) . . . . ? P4 Cr1 P3 P2 132.79(5) . . . . ? Cr2 Cr1 P3 P2 66.48(4) . . . . ? C3 Cr1 P3 P4 100.25(11) . . . . ? C2 Cr1 P3 P4 137.94(11) . . . . ? C1 Cr1 P3 P4 156.79(14) . . . . ? C4 Cr1 P3 P4 72.29(12) . . . . ? C5 Cr1 P3 P4 95.2(3) . . . . ? P5 Cr1 P3 P4 -38.28(5) . . . . ? P1 Cr1 P3 P4 -94.74(5) . . . . ? P2 Cr1 P3 P4 -132.79(5) . . . . ? Cr2 Cr1 P3 P4 -66.31(4) . . . . ? C3 Cr1 P3 Cr2 166.56(10) . . . . ? C2 Cr1 P3 Cr2 -155.75(10) . . . . ? C1 Cr1 P3 Cr2 -136.90(14) . . . . ? C4 Cr1 P3 Cr2 138.60(11) . . . . ? C5 Cr1 P3 Cr2 161.5(3) . . . . ? P5 Cr1 P3 Cr2 28.03(4) . . . . ? P1 Cr1 P3 Cr2 -28.43(4) . . . . ? P4 Cr1 P3 Cr2 66.31(4) . . . . ? P2 Cr1 P3 Cr2 -66.48(4) . . . . ? P2 P3 P4 P5 0.18(7) . . . . ? Cr2 P3 P4 P5 -43.39(5) . . . . ? Cr1 P3 P4 P5 43.46(5) . . . . ? P2 P3 P4 Cr1 -43.28(5) . . . . ? Cr2 P3 P4 Cr1 -86.85(4) . . . . ? P2 P3 P4 Cr2 43.56(5) . . . . ? Cr1 P3 P4 Cr2 86.85(4) . . . . ? C3 Cr1 P4 P5 138.81(10) . . . . ? C2 Cr1 P4 P5 158.15(14) . . . . ? C1 Cr1 P4 P5 97.1(3) . . . . ? C4 Cr1 P4 P5 100.91(10) . . . . ? C5 Cr1 P4 P5 73.76(12) . . . . ? P3 Cr1 P4 P5 -132.04(6) . . . . ? P1 Cr1 P4 P5 -38.17(5) . . . . ? P2 Cr1 P4 P5 -94.39(5) . . . . ? Cr2 Cr1 P4 P5 -66.13(4) . . . . ? C3 Cr1 P4 P3 -89.15(10) . . . . ? C2 Cr1 P4 P3 -69.81(14) . . . . ? C1 Cr1 P4 P3 -130.9(3) . . . . ? C4 Cr1 P4 P3 -127.05(10) . . . . ? C5 Cr1 P4 P3 -154.20(12) . . . . ? P5 Cr1 P4 P3 132.04(6) . . . . ? P1 Cr1 P4 P3 93.87(5) . . . . ? P2 Cr1 P4 P3 37.65(5) . . . . ? Cr2 Cr1 P4 P3 65.91(4) . . . . ? C3 Cr1 P4 Cr2 -155.06(10) . . . . ? C2 Cr1 P4 Cr2 -135.72(14) . . . . ? C1 Cr1 P4 Cr2 163.2(3) . . . . ? C4 Cr1 P4 Cr2 167.04(10) . . . . ? C5 Cr1 P4 Cr2 139.89(12) . . . . ? P5 Cr1 P4 Cr2 66.13(4) . . . . ? P3 Cr1 P4 Cr2 -65.91(4) . . . . ? P1 Cr1 P4 Cr2 27.96(4) . . . . ? P2 Cr1 P4 Cr2 -28.26(4) . . . . ? P3 P4 P5 P1 0.00(8) . . . . ? Cr1 P4 P5 P1 43.47(5) . . . . ? Cr2 P4 P5 P1 -43.29(5) . . . . ? P3 P4 P5 Cr1 -43.47(5) . . . . ? Cr2 P4 P5 Cr1 -86.76(4) . . . . ? P3 P4 P5 Cr2 43.29(5) . . . . ? Cr1 P4 P5 Cr2 86.76(4) . . . . ? P2 P1 P5 P4 -0.17(8) . . . . ? Cr2 P1 P5 P4 43.42(5) . . . . ? Cr1 P1 P5 P4 -43.52(5) . . . . ? P2 P1 P5 Cr1 43.35(5) . . . . ? Cr2 P1 P5 Cr1 86.94(4) . . . . ? P2 P1 P5 Cr2 -43.60(5) . . . . ? Cr1 P1 P5 Cr2 -86.94(4) . . . . ? C3 Cr1 P5 P4 -69.06(15) . . . . ? C2 Cr1 P5 P4 -130.8(3) . . . . ? C1 Cr1 P5 P4 -154.26(12) . . . . ? C4 Cr1 P5 P4 -88.66(10) . . . . ? C5 Cr1 P5 P4 -126.18(11) . . . . ? P3 Cr1 P5 P4 38.35(5) . . . . ? P1 Cr1 P5 P4 132.37(5) . . . . ? P2 Cr1 P5 P4 94.42(5) . . . . ? Cr2 Cr1 P5 P4 66.33(4) . . . . ? C3 Cr1 P5 P1 158.58(15) . . . . ? C2 Cr1 P5 P1 96.8(3) . . . . ? C1 Cr1 P5 P1 73.38(12) . . . . ? C4 Cr1 P5 P1 138.98(10) . . . . ? C5 Cr1 P5 P1 101.45(11) . . . . ? P3 Cr1 P5 P1 -94.02(5) . . . . ? P4 Cr1 P5 P1 -132.37(5) . . . . ? P2 Cr1 P5 P1 -37.95(5) . . . . ? Cr2 Cr1 P5 P1 -66.04(4) . . . . ? C3 Cr1 P5 Cr2 -135.39(15) . . . . ? C2 Cr1 P5 Cr2 162.8(3) . . . . ? C1 Cr1 P5 Cr2 139.41(12) . . . . ? C4 Cr1 P5 Cr2 -154.99(10) . . . . ? C5 Cr1 P5 Cr2 167.49(10) . . . . ? P3 Cr1 P5 Cr2 -27.98(4) . . . . ? P1 Cr1 P5 Cr2 66.04(4) . . . . ? P4 Cr1 P5 Cr2 -66.33(4) . . . . ? P2 Cr1 P5 Cr2 28.09(4) . . . . ? P2 P3 Cr2 C12 86.92(12) . . . . ? P4 P3 Cr2 C12 -140.57(12) . . . . ? Cr1 P3 Cr2 C12 153.31(11) . . . . ? P2 P3 Cr2 C11 70.84(17) . . . . ? P4 P3 Cr2 C11 -156.65(16) . . . . ? Cr1 P3 Cr2 C11 137.22(16) . . . . ? P2 P3 Cr2 C14 154.05(12) . . . . ? P4 P3 Cr2 C14 -73.44(12) . . . . ? Cr1 P3 Cr2 C14 -139.57(12) . . . . ? P2 P3 Cr2 C15 141.7(3) . . . . ? P4 P3 Cr2 C15 -85.8(3) . . . . ? Cr1 P3 Cr2 C15 -151.9(3) . . . . ? P2 P3 Cr2 C13 124.29(10) . . . . ? P4 P3 Cr2 C13 -103.20(10) . . . . ? Cr1 P3 Cr2 C13 -169.33(10) . . . . ? P2 P3 Cr2 P5 -94.37(5) . . . . ? P4 P3 Cr2 P5 38.14(5) . . . . ? Cr1 P3 Cr2 P5 -27.98(4) . . . . ? P2 P3 Cr2 P1 -37.91(5) . . . . ? P4 P3 Cr2 P1 94.60(5) . . . . ? Cr1 P3 Cr2 P1 28.48(4) . . . . ? P2 P3 Cr2 P4 -132.51(5) . . . . ? Cr1 P3 Cr2 P4 -66.12(4) . . . . ? P4 P3 Cr2 P2 132.51(5) . . . . ? Cr1 P3 Cr2 P2 66.39(4) . . . . ? P2 P3 Cr2 Cr1 -66.39(4) . . . . ? P4 P3 Cr2 Cr1 66.12(4) . . . . ? P4 P5 Cr2 C12 138.6(3) . . . . ? P1 P5 Cr2 C12 -88.9(3) . . . . ? Cr1 P5 Cr2 C12 -155.1(3) . . . . ? P4 P5 Cr2 C11 152.61(12) . . . . ? P1 P5 Cr2 C11 -74.90(12) . . . . ? Cr1 P5 Cr2 C11 -141.10(12) . . . . ? P4 P5 Cr2 C14 86.35(11) . . . . ? P1 P5 Cr2 C14 -141.15(11) . . . . ? Cr1 P5 Cr2 C14 152.65(10) . . . . ? P4 P5 Cr2 C15 123.28(10) . . . . ? P1 P5 Cr2 C15 -104.23(10) . . . . ? Cr1 P5 Cr2 C15 -170.42(10) . . . . ? P4 P5 Cr2 C13 70.50(16) . . . . ? P1 P5 Cr2 C13 -157.00(16) . . . . ? Cr1 P5 Cr2 C13 136.80(16) . . . . ? P4 P5 Cr2 P3 -38.27(5) . . . . ? P1 P5 Cr2 P3 94.23(5) . . . . ? Cr1 P5 Cr2 P3 28.03(4) . . . . ? P4 P5 Cr2 P1 -132.49(5) . . . . ? Cr1 P5 Cr2 P1 -66.20(4) . . . . ? P1 P5 Cr2 P4 132.49(5) . . . . ? Cr1 P5 Cr2 P4 66.30(4) . . . . ? P4 P5 Cr2 P2 -94.37(5) . . . . ? P1 P5 Cr2 P2 38.13(5) . . . . ? Cr1 P5 Cr2 P2 -28.07(4) . . . . ? P4 P5 Cr2 Cr1 -66.30(4) . . . . ? P1 P5 Cr2 Cr1 66.20(4) . . . . ? P2 P1 Cr2 C12 -74.95(12) . . . . ? P5 P1 Cr2 C12 152.84(12) . . . . ? Cr1 P1 Cr2 C12 -141.26(12) . . . . ? P2 P1 Cr2 C11 -104.76(10) . . . . ? P5 P1 Cr2 C11 123.03(10) . . . . ? Cr1 P1 Cr2 C11 -171.06(10) . . . . ? P2 P1 Cr2 C14 -158.06(16) . . . . ? P5 P1 Cr2 C14 69.73(16) . . . . ? Cr1 P1 Cr2 C14 135.63(16) . . . . ? P2 P1 Cr2 C15 -142.00(10) . . . . ? P5 P1 Cr2 C15 85.78(10) . . . . ? Cr1 P1 Cr2 C15 151.69(10) . . . . ? P2 P1 Cr2 C13 -89.7(3) . . . . ? P5 P1 Cr2 C13 138.1(3) . . . . ? Cr1 P1 Cr2 C13 -156.0(3) . . . . ? P2 P1 Cr2 P3 37.85(5) . . . . ? P5 P1 Cr2 P3 -94.36(5) . . . . ? Cr1 P1 Cr2 P3 -28.46(4) . . . . ? P2 P1 Cr2 P5 132.21(5) . . . . ? Cr1 P1 Cr2 P5 65.90(4) . . . . ? P2 P1 Cr2 P4 94.28(5) . . . . ? P5 P1 Cr2 P4 -37.93(5) . . . . ? Cr1 P1 Cr2 P4 27.97(4) . . . . ? P5 P1 Cr2 P2 -132.21(5) . . . . ? Cr1 P1 Cr2 P2 -66.31(4) . . . . ? P2 P1 Cr2 Cr1 66.31(4) . . . . ? P5 P1 Cr2 Cr1 -65.90(4) . . . . ? P5 P4 Cr2 C12 -156.31(17) . . . . ? P3 P4 Cr2 C12 71.53(17) . . . . ? Cr1 P4 Cr2 C12 137.63(16) . . . . ? P5 P4 Cr2 C11 -87.3(3) . . . . ? P3 P4 Cr2 C11 140.5(3) . . . . ? Cr1 P4 Cr2 C11 -153.4(3) . . . . ? P5 P4 Cr2 C14 -103.56(10) . . . . ? P3 P4 Cr2 C14 124.28(10) . . . . ? Cr1 P4 Cr2 C14 -169.62(10) . . . . ? P5 P4 Cr2 C15 -73.74(12) . . . . ? P3 P4 Cr2 C15 154.10(12) . . . . ? Cr1 P4 Cr2 C15 -139.80(11) . . . . ? P5 P4 Cr2 C13 -140.35(10) . . . . ? P3 P4 Cr2 C13 87.49(10) . . . . ? Cr1 P4 Cr2 C13 153.59(10) . . . . ? P5 P4 Cr2 P3 132.16(6) . . . . ? Cr1 P4 Cr2 P3 66.10(4) . . . . ? P3 P4 Cr2 P5 -132.16(6) . . . . ? Cr1 P4 Cr2 P5 -66.06(4) . . . . ? P5 P4 Cr2 P1 38.07(5) . . . . ? P3 P4 Cr2 P1 -94.09(5) . . . . ? Cr1 P4 Cr2 P1 -27.99(4) . . . . ? P5 P4 Cr2 P2 94.31(5) . . . . ? P3 P4 Cr2 P2 -37.86(5) . . . . ? Cr1 P4 Cr2 P2 28.25(4) . . . . ? P5 P4 Cr2 Cr1 66.06(4) . . . . ? P3 P4 Cr2 Cr1 -66.10(4) . . . . ? P3 P2 Cr2 C12 -104.13(11) . . . . ? P1 P2 Cr2 C12 123.37(11) . . . . ? Cr1 P2 Cr2 C12 -170.38(11) . . . . ? P3 P2 Cr2 C11 -141.31(11) . . . . ? P1 P2 Cr2 C11 86.19(11) . . . . ? Cr1 P2 Cr2 C11 152.44(10) . . . . ? P3 P2 Cr2 C14 -87.6(3) . . . . ? P1 P2 Cr2 C14 139.9(3) . . . . ? Cr1 P2 Cr2 C14 -153.9(3) . . . . ? P3 P2 Cr2 C15 -158.34(15) . . . . ? P1 P2 Cr2 C15 69.17(16) . . . . ? Cr1 P2 Cr2 C15 135.42(15) . . . . ? P3 P2 Cr2 C13 -74.20(12) . . . . ? P1 P2 Cr2 C13 153.31(12) . . . . ? Cr1 P2 Cr2 C13 -140.45(12) . . . . ? P1 P2 Cr2 P3 -132.49(5) . . . . ? Cr1 P2 Cr2 P3 -66.25(4) . . . . ? P3 P2 Cr2 P5 94.23(5) . . . . ? P1 P2 Cr2 P5 -38.26(5) . . . . ? Cr1 P2 Cr2 P5 27.99(4) . . . . ? P3 P2 Cr2 P1 132.49(5) . . . . ? Cr1 P2 Cr2 P1 66.25(4) . . . . ? P3 P2 Cr2 P4 38.03(5) . . . . ? P1 P2 Cr2 P4 -94.47(5) . . . . ? Cr1 P2 Cr2 P4 -28.22(4) . . . . ? P3 P2 Cr2 Cr1 66.25(4) . . . . ? P1 P2 Cr2 Cr1 -66.25(4) . . . . ? C3 Cr1 Cr2 C12 -78.2(3) . . . . ? C2 Cr1 Cr2 C12 -7.3(3) . . . . ? C1 Cr1 Cr2 C12 65.2(3) . . . . ? C4 Cr1 Cr2 C12 -149.7(3) . . . . ? C5 Cr1 Cr2 C12 138.7(3) . . . . ? P5 Cr1 Cr2 C12 162.1(2) . . . . ? P3 Cr1 Cr2 C12 -53.7(2) . . . . ? P1 Cr1 Cr2 C12 89.8(2) . . . . ? P4 Cr1 Cr2 C12 -125.9(2) . . . . ? P2 Cr1 Cr2 C12 18.0(2) . . . . ? C3 Cr1 Cr2 C11 -151.5(3) . . . . ? C2 Cr1 Cr2 C11 -80.6(3) . . . . ? C1 Cr1 Cr2 C11 -8.1(3) . . . . ? C4 Cr1 Cr2 C11 137.1(2) . . . . ? C5 Cr1 Cr2 C11 65.4(3) . . . . ? P5 Cr1 Cr2 C11 88.85(18) . . . . ? P3 Cr1 Cr2 C11 -127.01(18) . . . . ? P1 Cr1 Cr2 C11 16.55(18) . . . . ? P4 Cr1 Cr2 C11 160.80(18) . . . . ? P2 Cr1 Cr2 C11 -55.29(18) . . . . ? C3 Cr1 Cr2 C14 66.5(3) . . . . ? C2 Cr1 Cr2 C14 137.4(3) . . . . ? C1 Cr1 Cr2 C14 -150.1(2) . . . . ? C4 Cr1 Cr2 C14 -4.9(3) . . . . ? C5 Cr1 Cr2 C14 -76.6(3) . . . . ? P5 Cr1 Cr2 C14 -53.16(18) . . . . ? P3 Cr1 Cr2 C14 90.99(18) . . . . ? P1 Cr1 Cr2 C14 -125.46(18) . . . . ? P4 Cr1 Cr2 C14 18.79(18) . . . . ? P2 Cr1 Cr2 C14 162.70(18) . . . . ? C3 Cr1 Cr2 C15 136.9(2) . . . . ? C2 Cr1 Cr2 C15 -152.3(3) . . . . ? C1 Cr1 Cr2 C15 -79.7(3) . . . . ? C4 Cr1 Cr2 C15 65.4(3) . . . . ? C5 Cr1 Cr2 C15 -6.2(3) . . . . ? P5 Cr1 Cr2 C15 17.21(18) . . . . ? P3 Cr1 Cr2 C15 161.36(18) . . . . ? P1 Cr1 Cr2 C15 -55.09(18) . . . . ? P4 Cr1 Cr2 C15 89.16(18) . . . . ? P2 Cr1 Cr2 C15 -126.93(18) . . . . ? C3 Cr1 Cr2 C13 -4.7(3) . . . . ? C2 Cr1 Cr2 C13 66.2(3) . . . . ? C1 Cr1 Cr2 C13 138.7(2) . . . . ? C4 Cr1 Cr2 C13 -76.1(3) . . . . ? C5 Cr1 Cr2 C13 -147.8(3) . . . . ? P5 Cr1 Cr2 C13 -124.36(19) . . . . ? P3 Cr1 Cr2 C13 19.79(18) . . . . ? P1 Cr1 Cr2 C13 163.34(19) . . . . ? P4 Cr1 Cr2 C13 -52.41(18) . . . . ? P2 Cr1 Cr2 C13 91.50(18) . . . . ? C3 Cr1 Cr2 P3 -24.48(18) . . . . ? C2 Cr1 Cr2 P3 46.37(19) . . . . ? C1 Cr1 Cr2 P3 118.95(18) . . . . ? C4 Cr1 Cr2 P3 -95.93(18) . . . . ? C5 Cr1 Cr2 P3 -167.61(19) . . . . ? P5 Cr1 Cr2 P3 -144.14(6) . . . . ? P1 Cr1 Cr2 P3 143.56(6) . . . . ? P4 Cr1 Cr2 P3 -72.19(5) . . . . ? P2 Cr1 Cr2 P3 71.71(5) . . . . ? C3 Cr1 Cr2 P5 119.67(18) . . . . ? C2 Cr1 Cr2 P5 -169.48(19) . . . . ? C1 Cr1 Cr2 P5 -96.91(18) . . . . ? C4 Cr1 Cr2 P5 48.21(18) . . . . ? C5 Cr1 Cr2 P5 -23.46(19) . . . . ? P3 Cr1 Cr2 P5 144.14(6) . . . . ? P1 Cr1 Cr2 P5 -72.30(5) . . . . ? P4 Cr1 Cr2 P5 71.95(5) . . . . ? P2 Cr1 Cr2 P5 -144.14(6) . . . . ? C3 Cr1 Cr2 P1 -168.04(18) . . . . ? C2 Cr1 Cr2 P1 -97.18(19) . . . . ? C1 Cr1 Cr2 P1 -24.61(18) . . . . ? C4 Cr1 Cr2 P1 120.51(18) . . . . ? C5 Cr1 Cr2 P1 48.84(19) . . . . ? P5 Cr1 Cr2 P1 72.30(5) . . . . ? P3 Cr1 Cr2 P1 -143.56(6) . . . . ? P4 Cr1 Cr2 P1 144.25(5) . . . . ? P2 Cr1 Cr2 P1 -71.84(5) . . . . ? C3 Cr1 Cr2 P4 47.71(18) . . . . ? C2 Cr1 Cr2 P4 118.57(19) . . . . ? C1 Cr1 Cr2 P4 -168.86(18) . . . . ? C4 Cr1 Cr2 P4 -23.74(18) . . . . ? C5 Cr1 Cr2 P4 -95.41(19) . . . . ? P5 Cr1 Cr2 P4 -71.95(5) . . . . ? P3 Cr1 Cr2 P4 72.19(5) . . . . ? P1 Cr1 Cr2 P4 -144.25(5) . . . . ? P2 Cr1 Cr2 P4 143.91(5) . . . . ? C3 Cr1 Cr2 P2 -96.19(18) . . . . ? C2 Cr1 Cr2 P2 -25.34(19) . . . . ? C1 Cr1 Cr2 P2 47.23(18) . . . . ? C4 Cr1 Cr2 P2 -167.65(18) . . . . ? C5 Cr1 Cr2 P2 120.68(19) . . . . ? P5 Cr1 Cr2 P2 144.14(6) . . . . ? P3 Cr1 Cr2 P2 -71.71(5) . . . . ? P1 Cr1 Cr2 P2 71.84(5) . . . . ? P4 Cr1 Cr2 P2 -143.91(5) . . . . ? C14 Cr2 C11 C12 -80.3(2) . . . . ? C15 Cr2 C11 C12 -118.0(3) . . . . ? C13 Cr2 C11 C12 -38.0(2) . . . . ? P3 Cr2 C11 C12 26.0(3) . . . . ? P5 Cr2 C11 C12 -171.03(19) . . . . ? P1 Cr2 C11 C12 135.6(2) . . . . ? P4 Cr2 C11 C12 -98.6(3) . . . . ? P2 Cr2 C11 C12 79.8(2) . . . . ? Cr1 Cr2 C11 C12 122.4(2) . . . . ? C12 Cr2 C11 C15 118.0(3) . . . . ? C14 Cr2 C11 C15 37.7(2) . . . . ? C13 Cr2 C11 C15 80.0(2) . . . . ? P3 Cr2 C11 C15 144.01(18) . . . . ? P5 Cr2 C11 C15 -53.0(2) . . . . ? P1 Cr2 C11 C15 -106.4(2) . . . . ? P4 Cr2 C11 C15 19.4(4) . . . . ? P2 Cr2 C11 C15 -162.20(19) . . . . ? Cr1 Cr2 C11 C15 -119.5(2) . . . . ? C12 Cr2 C11 C16 -119.4(4) . . . . ? C14 Cr2 C11 C16 160.4(4) . . . . ? C15 Cr2 C11 C16 122.6(4) . . . . ? C13 Cr2 C11 C16 -157.3(4) . . . . ? P3 Cr2 C11 C16 -93.4(3) . . . . ? P5 Cr2 C11 C16 69.6(3) . . . . ? P1 Cr2 C11 C16 16.2(3) . . . . ? P4 Cr2 C11 C16 142.1(3) . . . . ? P2 Cr2 C11 C16 -39.6(3) . . . . ? Cr1 Cr2 C11 C16 3.1(4) . . . . ? C15 C11 C12 C13 0.6(4) . . . . ? C16 C11 C12 C13 -175.6(3) . . . . ? Cr2 C11 C12 C13 62.5(3) . . . . ? C15 C11 C12 C17 176.2(4) . . . . ? C16 C11 C12 C17 0.0(6) . . . . ? Cr2 C11 C12 C17 -121.9(4) . . . . ? C15 C11 C12 Cr2 -61.9(3) . . . . ? C16 C11 C12 Cr2 121.9(4) . . . . ? C14 Cr2 C12 C11 79.6(2) . . . . ? C15 Cr2 C12 C11 37.2(2) . . . . ? C13 Cr2 C12 C11 116.7(3) . . . . ? P3 Cr2 C12 C11 -163.2(2) . . . . ? P5 Cr2 C12 C11 20.1(4) . . . . ? P1 Cr2 C12 C11 -54.1(2) . . . . ? P4 Cr2 C12 C11 142.51(19) . . . . ? P2 Cr2 C12 C11 -107.3(2) . . . . ? Cr1 Cr2 C12 C11 -121.6(2) . . . . ? C11 Cr2 C12 C13 -116.7(3) . . . . ? C14 Cr2 C12 C13 -37.2(2) . . . . ? C15 Cr2 C12 C13 -79.5(2) . . . . ? P3 Cr2 C12 C13 80.1(2) . . . . ? P5 Cr2 C12 C13 -96.6(3) . . . . ? P1 Cr2 C12 C13 -170.82(18) . . . . ? P4 Cr2 C12 C13 25.8(3) . . . . ? P2 Cr2 C12 C13 135.9(2) . . . . ? Cr1 Cr2 C12 C13 121.6(2) . . . . ? C11 Cr2 C12 C17 122.3(4) . . . . ? C14 Cr2 C12 C17 -158.1(4) . . . . ? C15 Cr2 C12 C17 159.5(4) . . . . ? C13 Cr2 C12 C17 -121.0(4) . . . . ? P3 Cr2 C12 C17 -40.9(4) . . . . ? P5 Cr2 C12 C17 142.4(3) . . . . ? P1 Cr2 C12 C17 68.2(4) . . . . ? P4 Cr2 C12 C17 -95.2(4) . . . . ? P2 Cr2 C12 C17 15.0(3) . . . . ? Cr1 Cr2 C12 C17 0.7(5) . . . . ? C11 C12 C13 C14 -0.7(4) . . . . ? C17 C12 C13 C14 -176.3(3) . . . . ? Cr2 C12 C13 C14 61.8(3) . . . . ? C11 C12 C13 C18 175.3(3) . . . . ? C17 C12 C13 C18 -0.3(6) . . . . ? Cr2 C12 C13 C18 -122.2(4) . . . . ? C11 C12 C13 Cr2 -62.5(2) . . . . ? C17 C12 C13 Cr2 121.9(4) . . . . ? C12 Cr2 C13 C14 -117.6(3) . . . . ? C11 Cr2 C13 C14 -79.8(2) . . . . ? C15 Cr2 C13 C14 -37.2(2) . . . . ? P3 Cr2 C13 C14 135.4(2) . . . . ? P5 Cr2 C13 C14 25.9(3) . . . . ? P1 Cr2 C13 C14 -96.7(3) . . . . ? P4 Cr2 C13 C14 79.2(2) . . . . ? P2 Cr2 C13 C14 -171.73(18) . . . . ? Cr1 Cr2 C13 C14 119.7(2) . . . . ? C11 Cr2 C13 C12 37.8(2) . . . . ? C14 Cr2 C13 C12 117.6(3) . . . . ? C15 Cr2 C13 C12 80.4(2) . . . . ? P3 Cr2 C13 C12 -106.9(2) . . . . ? P5 Cr2 C13 C12 143.52(19) . . . . ? P1 Cr2 C13 C12 20.9(4) . . . . ? P4 Cr2 C13 C12 -163.13(19) . . . . ? P2 Cr2 C13 C12 -54.1(2) . . . . ? Cr1 Cr2 C13 C12 -122.6(2) . . . . ? C12 Cr2 C13 C18 120.8(4) . . . . ? C11 Cr2 C13 C18 158.7(4) . . . . ? C14 Cr2 C13 C18 -121.5(4) . . . . ? C15 Cr2 C13 C18 -158.7(4) . . . . ? P3 Cr2 C13 C18 13.9(3) . . . . ? P5 Cr2 C13 C18 -95.6(3) . . . . ? P1 Cr2 C13 C18 141.8(3) . . . . ? P4 Cr2 C13 C18 -42.3(3) . . . . ? P2 Cr2 C13 C18 66.8(3) . . . . ? Cr1 Cr2 C13 C18 -1.8(4) . . . . ? C12 C13 C14 C15 0.4(4) . . . . ? C18 C13 C14 C15 -175.5(3) . . . . ? Cr2 C13 C14 C15 62.1(3) . . . . ? C12 C13 C14 C19 177.4(3) . . . . ? C18 C13 C14 C19 1.4(6) . . . . ? Cr2 C13 C14 C19 -121.0(4) . . . . ? C12 C13 C14 Cr2 -61.6(3) . . . . ? C18 C13 C14 Cr2 122.4(4) . . . . ? C12 Cr2 C14 C13 37.6(2) . . . . ? C11 Cr2 C14 C13 80.1(2) . . . . ? C15 Cr2 C14 C13 118.0(3) . . . . ? P3 Cr2 C14 C13 -54.4(2) . . . . ? P5 Cr2 C14 C13 -162.8(2) . . . . ? P1 Cr2 C14 C13 144.04(19) . . . . ? P4 Cr2 C14 C13 -107.1(2) . . . . ? P2 Cr2 C14 C13 19.1(4) . . . . ? Cr1 Cr2 C14 C13 -122.0(2) . . . . ? C12 Cr2 C14 C15 -80.4(2) . . . . ? C11 Cr2 C14 C15 -37.9(2) . . . . ? C13 Cr2 C14 C15 -118.0(3) . . . . ? P3 Cr2 C14 C15 -172.35(17) . . . . ? P5 Cr2 C14 C15 79.2(2) . . . . ? P1 Cr2 C14 C15 26.1(3) . . . . ? P4 Cr2 C14 C15 134.92(19) . . . . ? P2 Cr2 C14 C15 -98.9(3) . . . . ? Cr1 Cr2 C14 C15 120.0(2) . . . . ? C12 Cr2 C14 C19 159.4(4) . . . . ? C11 Cr2 C14 C19 -158.1(4) . . . . ? C15 Cr2 C14 C19 -120.2(4) . . . . ? C13 Cr2 C14 C19 121.8(4) . . . . ? P3 Cr2 C14 C19 67.4(3) . . . . ? P5 Cr2 C14 C19 -41.0(3) . . . . ? P1 Cr2 C14 C19 -94.1(3) . . . . ? P4 Cr2 C14 C19 14.7(3) . . . . ? P2 Cr2 C14 C19 140.9(3) . . . . ? Cr1 Cr2 C14 C19 -0.2(4) . . . . ? C13 C14 C15 C11 0.0(4) . . . . ? C19 C14 C15 C11 -177.1(3) . . . . ? Cr2 C14 C15 C11 62.1(2) . . . . ? C13 C14 C15 C20 177.2(3) . . . . ? C19 C14 C15 C20 0.2(6) . . . . ? Cr2 C14 C15 C20 -120.6(4) . . . . ? C13 C14 C15 Cr2 -62.1(2) . . . . ? C19 C14 C15 Cr2 120.8(4) . . . . ? C12 C11 C15 C14 -0.4(4) . . . . ? C16 C11 C15 C14 175.7(3) . . . . ? Cr2 C11 C15 C14 -62.1(2) . . . . ? C12 C11 C15 C20 -177.6(3) . . . . ? C16 C11 C15 C20 -1.5(6) . . . . ? Cr2 C11 C15 C20 120.6(4) . . . . ? C12 C11 C15 Cr2 61.8(3) . . . . ? C16 C11 C15 Cr2 -122.2(4) . . . . ? C12 Cr2 C15 C14 79.7(2) . . . . ? C11 Cr2 C15 C14 116.9(3) . . . . ? C13 Cr2 C15 C14 37.1(2) . . . . ? P3 Cr2 C15 C14 17.5(4) . . . . ? P5 Cr2 C15 C14 -107.0(2) . . . . ? P1 Cr2 C15 C14 -162.88(19) . . . . ? P4 Cr2 C15 C14 -54.4(2) . . . . ? P2 Cr2 C15 C14 144.37(18) . . . . ? Cr1 Cr2 C15 C14 -120.6(2) . . . . ? C12 Cr2 C15 C11 -37.2(2) . . . . ? C14 Cr2 C15 C11 -116.9(3) . . . . ? C13 Cr2 C15 C11 -79.8(2) . . . . ? P3 Cr2 C15 C11 -99.3(3) . . . . ? P5 Cr2 C15 C11 136.2(2) . . . . ? P1 Cr2 C15 C11 80.3(2) . . . . ? P4 Cr2 C15 C11 -171.22(18) . . . . ? P2 Cr2 C15 C11 27.5(3) . . . . ? Cr1 Cr2 C15 C11 122.5(2) . . . . ? C12 Cr2 C15 C20 -159.2(4) . . . . ? C11 Cr2 C15 C20 -122.0(4) . . . . ? C14 Cr2 C15 C20 121.1(4) . . . . ? C13 Cr2 C15 C20 158.2(4) . . . . ? P3 Cr2 C15 C20 138.6(3) . . . . ? P5 Cr2 C15 C20 14.1(3) . . . . ? P1 Cr2 C15 C20 -41.8(3) . . . . ? P4 Cr2 C15 C20 66.7(3) . . . . ? P2 Cr2 C15 C20 -94.5(3) . . . . ? Cr1 Cr2 C15 C20 0.5(4) . . . . ? C25 C21 C22 C23 -0.1(5) . . . . ? C26 C21 C22 C23 175.7(4) . . . . ? Cr3 C21 C22 C23 -61.6(3) . . . . ? C25 C21 C22 C27 -175.8(4) . . . . ? C26 C21 C22 C27 0.0(7) . . . . ? Cr3 C21 C22 C27 122.7(4) . . . . ? C25 C21 C22 Cr3 61.5(3) . . . . ? C26 C21 C22 Cr3 -122.8(4) . . . . ? C21 C22 C23 C24 0.3(5) . . . . ? C27 C22 C23 C24 176.0(4) . . . . ? Cr3 C22 C23 C24 -61.7(3) . . . . ? C21 C22 C23 C28 -175.9(4) . . . . ? C27 C22 C23 C28 -0.1(7) . . . . ? Cr3 C22 C23 C28 122.2(4) . . . . ? C21 C22 C23 Cr3 61.9(3) . . . . ? C27 C22 C23 Cr3 -122.3(4) . . . . ? C22 C23 C24 C25 -0.3(4) . . . . ? C28 C23 C24 C25 175.8(4) . . . . ? Cr3 C23 C24 C25 -62.4(3) . . . . ? C22 C23 C24 C29 -175.3(4) . . . . ? C28 C23 C24 C29 0.8(6) . . . . ? Cr3 C23 C24 C29 122.6(4) . . . . ? C22 C23 C24 Cr3 62.1(3) . . . . ? C28 C23 C24 Cr3 -121.8(4) . . . . ? C22 C21 C25 C24 -0.1(5) . . . . ? C26 C21 C25 C24 -176.0(4) . . . . ? Cr3 C21 C25 C24 61.4(3) . . . . ? C22 C21 C25 C30 176.2(4) . . . . ? C26 C21 C25 C30 0.3(7) . . . . ? Cr3 C21 C25 C30 -122.3(4) . . . . ? C22 C21 C25 Cr3 -61.5(3) . . . . ? C26 C21 C25 Cr3 122.6(4) . . . . ? C23 C24 C25 C21 0.3(4) . . . . ? C29 C24 C25 C21 175.2(4) . . . . ? Cr3 C24 C25 C21 -62.1(3) . . . . ? C23 C24 C25 C30 -176.0(4) . . . . ? C29 C24 C25 C30 -1.1(6) . . . . ? Cr3 C24 C25 C30 121.6(4) . . . . ? C23 C24 C25 Cr3 62.4(3) . . . . ? C29 C24 C25 Cr3 -122.7(4) . . . . ? C25 C24 Cr3 C23 116.9(3) . . . . ? C29 C24 Cr3 C23 -120.7(4) . . . . ? C23 C24 Cr3 C25 -116.9(3) . . . . ? C29 C24 Cr3 C25 122.4(4) . . . . ? C23 C24 Cr3 C22 -37.3(2) . . . . ? C25 C24 Cr3 C22 79.6(2) . . . . ? C29 C24 Cr3 C22 -158.0(4) . . . . ? C23 C24 Cr3 C21 -79.8(2) . . . . ? C25 C24 Cr3 C21 37.1(2) . . . . ? C29 C24 Cr3 C21 159.5(4) . . . . ? C23 C24 Cr3 P6 -137.0(2) . . . . ? C25 C24 Cr3 P6 -20.1(3) . . . . ? C29 C24 Cr3 P6 102.3(4) . . . . ? C23 C24 Cr3 P10 170.08(19) . . . . ? C25 C24 Cr3 P10 -73.0(2) . . . . ? C29 C24 Cr3 P10 49.4(4) . . . . ? C23 C24 Cr3 P8 64.6(2) . . . . ? C25 C24 Cr3 P8 -178.48(18) . . . . ? C29 C24 Cr3 P8 -56.1(4) . . . . ? C23 C24 Cr3 P9 116.6(2) . . . . ? C25 C24 Cr3 P9 -126.48(19) . . . . ? C29 C24 Cr3 P9 -4.1(3) . . . . ? C23 C24 Cr3 P7 7.7(4) . . . . ? C25 C24 Cr3 P7 124.6(3) . . . . ? C29 C24 Cr3 P7 -113.0(3) . . . . ? C22 C23 Cr3 C24 -117.6(3) . . . . ? C28 C23 Cr3 C24 121.4(4) . . . . ? C22 C23 Cr3 C25 -79.6(2) . . . . ? C24 C23 Cr3 C25 38.0(2) . . . . ? C28 C23 Cr3 C25 159.5(4) . . . . ? C24 C23 Cr3 C22 117.6(3) . . . . ? C28 C23 Cr3 C22 -120.9(4) . . . . ? C22 C23 Cr3 C21 -37.3(2) . . . . ? C24 C23 Cr3 C21 80.3(2) . . . . ? C28 C23 Cr3 C21 -158.2(4) . . . . ? C22 C23 Cr3 P6 4.6(4) . . . . ? C24 C23 Cr3 P6 122.3(3) . . . . ? C28 C23 Cr3 P6 -116.3(3) . . . . ? C22 C23 Cr3 P10 -135.1(2) . . . . ? C24 C23 Cr3 P10 -17.5(3) . . . . ? C28 C23 Cr3 P10 103.9(3) . . . . ? C22 C23 Cr3 P8 117.4(2) . . . . ? C24 C23 Cr3 P8 -125.0(2) . . . . ? C28 C23 Cr3 P8 -3.5(3) . . . . ? C22 C23 Cr3 P9 170.6(2) . . . . ? C24 C23 Cr3 P9 -71.8(2) . . . . ? C28 C23 Cr3 P9 49.6(3) . . . . ? C22 C23 Cr3 P7 66.0(2) . . . . ? C24 C23 Cr3 P7 -176.37(18) . . . . ? C28 C23 Cr3 P7 -54.9(3) . . . . ? C21 C25 Cr3 C24 117.8(3) . . . . ? C30 C25 Cr3 C24 -121.0(4) . . . . ? C21 C25 Cr3 C23 80.0(2) . . . . ? C24 C25 Cr3 C23 -37.9(2) . . . . ? C30 C25 Cr3 C23 -158.8(4) . . . . ? C21 C25 Cr3 C22 37.5(2) . . . . ? C24 C25 Cr3 C22 -80.3(2) . . . . ? C30 C25 Cr3 C22 158.8(4) . . . . ? C24 C25 Cr3 C21 -117.8(3) . . . . ? C30 C25 Cr3 C21 121.2(4) . . . . ? C21 C25 Cr3 P6 -73.3(2) . . . . ? C24 C25 Cr3 P6 168.89(18) . . . . ? C30 C25 Cr3 P6 47.9(3) . . . . ? C21 C25 Cr3 P10 -126.5(2) . . . . ? C24 C25 Cr3 P10 115.70(19) . . . . ? C30 C25 Cr3 P10 -5.3(3) . . . . ? C21 C25 Cr3 P8 120.9(3) . . . . ? C24 C25 Cr3 P8 3.1(4) . . . . ? C30 C25 Cr3 P8 -117.9(3) . . . . ? C21 C25 Cr3 P9 -179.09(19) . . . . ? C24 C25 Cr3 P9 63.1(2) . . . . ? C30 C25 Cr3 P9 -57.9(3) . . . . ? C21 C25 Cr3 P7 -19.3(3) . . . . ? C24 C25 Cr3 P7 -137.1(2) . . . . ? C30 C25 Cr3 P7 102.0(3) . . . . ? C23 C22 Cr3 C24 37.6(2) . . . . ? C21 C22 Cr3 C24 -80.3(2) . . . . ? C27 C22 Cr3 C24 157.4(4) . . . . ? C21 C22 Cr3 C23 -117.9(3) . . . . ? C27 C22 Cr3 C23 119.8(4) . . . . ? C23 C22 Cr3 C25 80.6(2) . . . . ? C21 C22 Cr3 C25 -37.4(2) . . . . ? C27 C22 Cr3 C25 -159.6(4) . . . . ? C23 C22 Cr3 C21 117.9(3) . . . . ? C27 C22 Cr3 C21 -122.3(4) . . . . ? C23 C22 Cr3 P6 -177.80(19) . . . . ? C21 C22 Cr3 P6 64.3(2) . . . . ? C27 C22 Cr3 P6 -58.0(4) . . . . ? C23 C22 Cr3 P10 119.6(3) . . . . ? C21 C22 Cr3 P10 1.6(4) . . . . ? C27 C22 Cr3 P10 -120.6(3) . . . . ? C23 C22 Cr3 P8 -71.2(2) . . . . ? C21 C22 Cr3 P8 170.8(2) . . . . ? C27 C22 Cr3 P8 48.6(4) . . . . ? C23 C22 Cr3 P9 -16.5(3) . . . . ? C21 C22 Cr3 P9 -134.5(2) . . . . ? C27 C22 Cr3 P9 103.3(3) . . . . ? C23 C22 Cr3 P7 -124.9(2) . . . . ? C21 C22 Cr3 P7 117.2(2) . . . . ? C27 C22 Cr3 P7 -5.1(3) . . . . ? C25 C21 Cr3 C24 -37.6(2) . . . . ? C22 C21 Cr3 C24 79.9(2) . . . . ? C26 C21 Cr3 C24 -157.9(4) . . . . ? C25 C21 Cr3 C23 -80.3(2) . . . . ? C22 C21 Cr3 C23 37.2(2) . . . . ? C26 C21 Cr3 C23 159.4(4) . . . . ? C22 C21 Cr3 C25 117.6(3) . . . . ? C26 C21 Cr3 C25 -120.3(4) . . . . ? C25 C21 Cr3 C22 -117.6(3) . . . . ? C26 C21 Cr3 C22 122.2(4) . . . . ? C25 C21 Cr3 P6 116.1(2) . . . . ? C22 C21 Cr3 P6 -126.3(2) . . . . ? C26 C21 Cr3 P6 -4.1(3) . . . . ? C25 C21 Cr3 P10 63.2(2) . . . . ? C22 C21 Cr3 P10 -179.21(19) . . . . ? C26 C21 Cr3 P10 -57.0(3) . . . . ? C25 C21 Cr3 P8 -133.9(2) . . . . ? C22 C21 Cr3 P8 -16.3(3) . . . . ? C26 C21 Cr3 P8 105.9(3) . . . . ? C25 C21 Cr3 P9 1.8(4) . . . . ? C22 C21 Cr3 P9 119.4(3) . . . . ? C26 C21 Cr3 P9 -118.4(3) . . . . ? C25 C21 Cr3 P7 169.51(19) . . . . ? C22 C21 Cr3 P7 -72.9(2) . . . . ? C26 C21 Cr3 P7 49.2(4) . . . . ? C24 Cr3 P6 P10 -68.18(19) . . . . ? C23 Cr3 P6 P10 -154.5(3) . . . . ? C25 Cr3 P6 P10 -81.37(11) . . . . ? C22 Cr3 P6 P10 -151.31(13) . . . . ? C21 Cr3 P6 P10 -117.50(11) . . . . ? P8 Cr3 P6 P10 92.36(4) . . . . ? P9 Cr3 P6 P10 38.69(4) . . . . ? P7 Cr3 P6 P10 129.44(5) . . . . ? C24 Cr3 P6 P7 162.38(19) . . . . ? C23 Cr3 P6 P7 76.1(3) . . . . ? C25 Cr3 P6 P7 149.19(11) . . . . ? C22 Cr3 P6 P7 79.25(13) . . . . ? C21 Cr3 P6 P7 113.06(11) . . . . ? P10 Cr3 P6 P7 -129.44(5) . . . . ? P8 Cr3 P6 P7 -37.08(4) . . . . ? P9 Cr3 P6 P7 -90.75(4) . . . . ? C24 Cr3 P6 Cr4 -132.88(19) . . . . ? C23 Cr3 P6 Cr4 140.8(2) . . . . ? C25 Cr3 P6 Cr4 -146.07(11) . . . . ? C22 Cr3 P6 Cr4 144.00(12) . . . . ? C21 Cr3 P6 Cr4 177.81(11) . . . . ? P10 Cr3 P6 Cr4 -64.70(4) . . . . ? P8 Cr3 P6 Cr4 27.66(4) . . . . ? P9 Cr3 P6 Cr4 -26.01(4) . . . . ? P7 Cr3 P6 Cr4 64.74(4) . . . . ? P10 P6 P7 P8 -1.77(7) . . . . ? Cr3 P6 P7 P8 44.71(5) . . . . ? Cr4 P6 P7 P8 -47.07(5) . . . . ? P10 P6 P7 Cr4 45.30(5) . . . . ? Cr3 P6 P7 Cr4 91.79(3) . . . . ? P10 P6 P7 Cr3 -46.49(5) . . . . ? Cr4 P6 P7 Cr3 -91.79(3) . . . . ? C24 Cr3 P7 P8 70.7(3) . . . . ? C23 Cr3 P7 P8 75.98(12) . . . . ? C25 Cr3 P7 P8 159.2(2) . . . . ? C22 Cr3 P7 P8 110.33(11) . . . . ? C21 Cr3 P7 P8 146.59(12) . . . . ? P6 Cr3 P7 P8 -131.37(5) . . . . ? P10 Cr3 P7 P8 -92.84(4) . . . . ? P9 Cr3 P7 P8 -38.83(4) . . . . ? C24 Cr3 P7 P6 -158.0(2) . . . . ? C23 Cr3 P7 P6 -152.65(12) . . . . ? C25 Cr3 P7 P6 -69.4(2) . . . . ? C22 Cr3 P7 P6 -118.31(11) . . . . ? C21 Cr3 P7 P6 -82.04(12) . . . . ? P10 Cr3 P7 P6 38.53(4) . . . . ? P8 Cr3 P7 P6 131.37(5) . . . . ? P9 Cr3 P7 P6 92.54(4) . . . . ? C24 Cr3 P7 Cr4 136.5(2) . . . . ? C23 Cr3 P7 Cr4 141.84(12) . . . . ? C25 Cr3 P7 Cr4 -134.9(2) . . . . ? C22 Cr3 P7 Cr4 176.18(11) . . . . ? C21 Cr3 P7 Cr4 -147.55(12) . . . . ? P6 Cr3 P7 Cr4 -65.51(4) . . . . ? P10 Cr3 P7 Cr4 -26.98(4) . . . . ? P8 Cr3 P7 Cr4 65.85(4) . . . . ? P9 Cr3 P7 Cr4 27.03(4) . . . . ? P6 P7 P8 P9 2.39(7) . . . . ? Cr4 P7 P8 P9 -44.52(5) . . . . ? Cr3 P7 P8 P9 46.97(5) . . . . ? P6 P7 P8 Cr3 -44.58(5) . . . . ? Cr4 P7 P8 Cr3 -91.50(3) . . . . ? P6 P7 P8 Cr4 46.92(5) . . . . ? Cr3 P7 P8 Cr4 91.50(3) . . . . ? C24 Cr3 P8 P7 -153.90(11) . . . . ? C23 Cr3 P8 P7 -119.92(10) . . . . ? C25 Cr3 P8 P7 -156.0(2) . . . . ? C22 Cr3 P8 P7 -84.34(12) . . . . ? C21 Cr3 P8 P7 -73.7(2) . . . . ? P6 Cr3 P8 P7 37.19(4) . . . . ? P10 Cr3 P8 P7 90.98(4) . . . . ? P9 Cr3 P8 P7 128.86(5) . . . . ? C24 Cr3 P8 P9 77.24(11) . . . . ? C23 Cr3 P8 P9 111.22(10) . . . . ? C25 Cr3 P8 P9 75.1(2) . . . . ? C22 Cr3 P8 P9 146.80(12) . . . . ? C21 Cr3 P8 P9 157.4(2) . . . . ? P6 Cr3 P8 P9 -91.67(4) . . . . ? P10 Cr3 P8 P9 -37.88(4) . . . . ? P7 Cr3 P8 P9 -128.86(5) . . . . ? C24 Cr3 P8 Cr4 141.31(11) . . . . ? C23 Cr3 P8 Cr4 175.29(10) . . . . ? C25 Cr3 P8 Cr4 139.2(2) . . . . ? C22 Cr3 P8 Cr4 -149.13(11) . . . . ? C21 Cr3 P8 Cr4 -138.5(2) . . . . ? P6 Cr3 P8 Cr4 -27.59(4) . . . . ? P10 Cr3 P8 Cr4 26.19(4) . . . . ? P9 Cr3 P8 Cr4 64.08(4) . . . . ? P7 Cr3 P8 Cr4 -64.78(4) . . . . ? P7 P8 P9 P10 -2.10(7) . . . . ? Cr3 P8 P9 P10 45.11(5) . . . . ? Cr4 P8 P9 P10 -46.94(5) . . . . ? P7 P8 P9 Cr4 44.84(5) . . . . ? Cr3 P8 P9 Cr4 92.06(3) . . . . ? P7 P8 P9 Cr3 -47.21(5) . . . . ? Cr4 P8 P9 Cr3 -92.06(3) . . . . ? C24 Cr3 P9 P8 -117.85(11) . . . . ? C23 Cr3 P9 P8 -81.89(11) . . . . ? C25 Cr3 P9 P8 -151.44(12) . . . . ? C22 Cr3 P9 P8 -71.2(2) . . . . ? C21 Cr3 P9 P8 -152.7(2) . . . . ? P6 Cr3 P9 P8 92.23(5) . . . . ? P10 Cr3 P9 P8 130.75(5) . . . . ? P7 Cr3 P9 P8 38.67(4) . . . . ? C24 Cr3 P9 P10 111.40(11) . . . . ? C23 Cr3 P9 P10 147.37(11) . . . . ? C25 Cr3 P9 P10 77.82(12) . . . . ? C22 Cr3 P9 P10 158.1(2) . . . . ? C21 Cr3 P9 P10 76.6(3) . . . . ? P6 Cr3 P9 P10 -38.52(4) . . . . ? P8 Cr3 P9 P10 -130.75(5) . . . . ? P7 Cr3 P9 P10 -92.07(4) . . . . ? C24 Cr3 P9 Cr4 176.27(11) . . . . ? C23 Cr3 P9 Cr4 -147.76(11) . . . . ? C25 Cr3 P9 Cr4 142.69(12) . . . . ? C22 Cr3 P9 Cr4 -137.1(2) . . . . ? C21 Cr3 P9 Cr4 141.4(2) . . . . ? P6 Cr3 P9 Cr4 26.35(4) . . . . ? P10 Cr3 P9 Cr4 64.87(4) . . . . ? P8 Cr3 P9 Cr4 -65.88(4) . . . . ? P7 Cr3 P9 Cr4 -27.20(4) . . . . ? P7 P6 P10 P9 0.47(7) . . . . ? Cr3 P6 P10 P9 -46.38(5) . . . . ? Cr4 P6 P10 P9 45.78(5) . . . . ? P7 P6 P10 Cr3 46.85(5) . . . . ? Cr4 P6 P10 Cr3 92.16(4) . . . . ? P7 P6 P10 Cr4 -45.31(5) . . . . ? Cr3 P6 P10 Cr4 -92.16(4) . . . . ? P8 P9 P10 P6 1.01(7) . . . . ? Cr4 P9 P10 P6 -46.40(5) . . . . ? Cr3 P9 P10 P6 46.30(5) . . . . ? P8 P9 P10 Cr3 -45.29(5) . . . . ? Cr4 P9 P10 Cr3 -92.70(3) . . . . ? P8 P9 P10 Cr4 47.41(5) . . . . ? Cr3 P9 P10 Cr4 92.70(3) . . . . ? C24 Cr3 P10 P6 148.89(12) . . . . ? C23 Cr3 P10 P6 160.3(2) . . . . ? C25 Cr3 P10 P6 112.45(11) . . . . ? C22 Cr3 P10 P6 78.1(3) . . . . ? C21 Cr3 P10 P6 79.21(12) . . . . ? P8 Cr3 P10 P6 -91.83(4) . . . . ? P9 Cr3 P10 P6 -129.49(5) . . . . ? P7 Cr3 P10 P6 -38.44(4) . . . . ? C24 Cr3 P10 P9 -81.62(12) . . . . ? C23 Cr3 P10 P9 -70.2(2) . . . . ? C25 Cr3 P10 P9 -118.07(11) . . . . ? C22 Cr3 P10 P9 -152.4(3) . . . . ? C21 Cr3 P10 P9 -151.30(12) . . . . ? P6 Cr3 P10 P9 129.49(5) . . . . ? P8 Cr3 P10 P9 37.66(4) . . . . ? P7 Cr3 P10 P9 91.05(4) . . . . ? C24 Cr3 P10 Cr4 -145.70(11) . . . . ? C23 Cr3 P10 Cr4 -134.3(2) . . . . ? C25 Cr3 P10 Cr4 177.85(10) . . . . ? C22 Cr3 P10 Cr4 143.5(2) . . . . ? C21 Cr3 P10 Cr4 144.62(12) . . . . ? P6 Cr3 P10 Cr4 65.41(4) . . . . ? P8 Cr3 P10 Cr4 -26.42(4) . . . . ? P9 Cr3 P10 Cr4 -64.08(4) . . . . ? P7 Cr3 P10 Cr4 26.97(4) . . . . ? P8 P9 Cr4 C31 162.90(16) . . . . ? P10 P9 Cr4 C31 -68.12(16) . . . . ? Cr3 P9 Cr4 C31 -132.40(16) . . . . ? P8 P9 Cr4 C32 89.4(3) . . . . ? P10 P9 Cr4 C32 -141.6(3) . . . . ? Cr3 P9 Cr4 C32 154.1(3) . . . . ? P8 P9 Cr4 C35 143.54(11) . . . . ? P10 P9 Cr4 C35 -87.49(11) . . . . ? Cr3 P9 Cr4 C35 -151.76(10) . . . . ? P8 P9 Cr4 C33 75.62(12) . . . . ? P10 P9 Cr4 C33 -155.40(12) . . . . ? Cr3 P9 Cr4 C33 140.32(12) . . . . ? P8 P9 Cr4 C34 105.55(11) . . . . ? P10 P9 Cr4 C34 -125.48(11) . . . . ? Cr3 P9 Cr4 C34 170.25(11) . . . . ? P8 P9 Cr4 P10 -128.97(5) . . . . ? Cr3 P9 Cr4 P10 -64.27(4) . . . . ? P8 P9 Cr4 P7 -37.25(4) . . . . ? P10 P9 Cr4 P7 91.72(4) . . . . ? Cr3 P9 Cr4 P7 27.45(4) . . . . ? P8 P9 Cr4 P6 -90.80(4) . . . . ? P10 P9 Cr4 P6 38.18(4) . . . . ? Cr3 P9 Cr4 P6 -26.10(4) . . . . ? P10 P9 Cr4 P8 128.97(5) . . . . ? Cr3 P9 Cr4 P8 64.70(4) . . . . ? P6 P10 Cr4 C31 -88.26(11) . . . . ? P9 P10 Cr4 C31 142.03(11) . . . . ? Cr3 P10 Cr4 C31 -153.06(11) . . . . ? P6 P10 Cr4 C32 -69.06(16) . . . . ? P9 P10 Cr4 C32 161.23(16) . . . . ? Cr3 P10 Cr4 C32 -133.86(15) . . . . ? P6 P10 Cr4 C35 -126.03(11) . . . . ? P9 P10 Cr4 C35 104.26(11) . . . . ? Cr3 P10 Cr4 C35 169.17(10) . . . . ? P6 P10 Cr4 C33 -140.4(3) . . . . ? P9 P10 Cr4 C33 89.9(3) . . . . ? Cr3 P10 Cr4 C33 154.8(3) . . . . ? P6 P10 Cr4 C34 -155.70(13) . . . . ? P9 P10 Cr4 C34 74.59(13) . . . . ? Cr3 P10 Cr4 C34 139.50(13) . . . . ? P6 P10 Cr4 P9 129.71(5) . . . . ? Cr3 P10 Cr4 P9 64.91(4) . . . . ? P6 P10 Cr4 P7 37.61(4) . . . . ? P9 P10 Cr4 P7 -92.10(4) . . . . ? Cr3 P10 Cr4 P7 -27.19(4) . . . . ? P9 P10 Cr4 P6 -129.71(5) . . . . ? Cr3 P10 Cr4 P6 -64.80(4) . . . . ? P6 P10 Cr4 P8 90.93(4) . . . . ? P9 P10 Cr4 P8 -38.78(4) . . . . ? Cr3 P10 Cr4 P8 26.13(4) . . . . ? P8 P7 Cr4 C31 -157.88(13) . . . . ? P6 P7 Cr4 C31 72.86(13) . . . . ? Cr3 P7 Cr4 C31 137.34(12) . . . . ? P8 P7 Cr4 C32 -126.86(11) . . . . ? P6 P7 Cr4 C32 103.89(11) . . . . ? Cr3 P7 Cr4 C32 168.36(11) . . . . ? P8 P7 Cr4 C35 -144.8(3) . . . . ? P6 P7 Cr4 C35 85.9(3) . . . . ? Cr3 P7 Cr4 C35 150.4(3) . . . . ? P8 P7 Cr4 C33 -89.02(11) . . . . ? P6 P7 Cr4 C33 141.73(11) . . . . ? Cr3 P7 Cr4 C33 -153.79(11) . . . . ? P8 P7 Cr4 C34 -70.46(18) . . . . ? P6 P7 Cr4 C34 160.28(18) . . . . ? Cr3 P7 Cr4 C34 -135.24(17) . . . . ? P8 P7 Cr4 P9 37.44(4) . . . . ? P6 P7 Cr4 P9 -91.82(5) . . . . ? Cr3 P7 Cr4 P9 -27.34(4) . . . . ? P8 P7 Cr4 P10 91.71(4) . . . . ? P6 P7 Cr4 P10 -37.54(4) . . . . ? Cr3 P7 Cr4 P10 26.93(4) . . . . ? P8 P7 Cr4 P6 129.25(5) . . . . ? Cr3 P7 Cr4 P6 64.48(4) . . . . ? P6 P7 Cr4 P8 -129.25(5) . . . . ? Cr3 P7 Cr4 P8 -64.78(4) . . . . ? P10 P6 Cr4 C31 102.99(11) . . . . ? P7 P6 Cr4 C31 -126.35(11) . . . . ? Cr3 P6 Cr4 C31 167.94(11) . . . . ? P10 P6 Cr4 C32 141.26(11) . . . . ? P7 P6 Cr4 C32 -88.07(11) . . . . ? Cr3 P6 Cr4 C32 -153.79(11) . . . . ? P10 P6 Cr4 C35 72.76(12) . . . . ? P7 P6 Cr4 C35 -156.57(12) . . . . ? Cr3 P6 Cr4 C35 137.71(12) . . . . ? P10 P6 Cr4 C33 159.44(17) . . . . ? P7 P6 Cr4 C33 -69.89(17) . . . . ? Cr3 P6 Cr4 C33 -135.61(16) . . . . ? P10 P6 Cr4 C34 87.4(3) . . . . ? P7 P6 Cr4 C34 -142.0(3) . . . . ? Cr3 P6 Cr4 C34 152.3(3) . . . . ? P10 P6 Cr4 P9 -38.67(4) . . . . ? P7 P6 Cr4 P9 92.00(5) . . . . ? Cr3 P6 Cr4 P9 26.28(4) . . . . ? P7 P6 Cr4 P10 130.67(5) . . . . ? Cr3 P6 Cr4 P10 64.95(4) . . . . ? P10 P6 Cr4 P7 -130.67(5) . . . . ? Cr3 P6 Cr4 P7 -65.72(4) . . . . ? P10 P6 Cr4 P8 -92.29(5) . . . . ? P7 P6 Cr4 P8 38.38(4) . . . . ? Cr3 P6 Cr4 P8 -27.34(4) . . . . ? P7 P8 Cr4 C31 85.6(3) . . . . ? P9 P8 Cr4 C31 -143.3(3) . . . . ? Cr3 P8 Cr4 C31 151.4(3) . . . . ? P7 P8 Cr4 C32 72.69(12) . . . . ? P9 P8 Cr4 C32 -156.26(12) . . . . ? Cr3 P8 Cr4 C32 138.48(12) . . . . ? P7 P8 Cr4 C35 161.91(16) . . . . ? P9 P8 Cr4 C35 -67.05(16) . . . . ? Cr3 P8 Cr4 C35 -132.30(16) . . . . ? P7 P8 Cr4 C33 104.08(10) . . . . ? P9 P8 Cr4 C33 -124.88(10) . . . . ? Cr3 P8 Cr4 C33 169.87(10) . . . . ? P7 P8 Cr4 C34 141.62(11) . . . . ? P9 P8 Cr4 C34 -87.34(11) . . . . ? Cr3 P8 Cr4 C34 -152.59(11) . . . . ? P7 P8 Cr4 P9 -131.04(5) . . . . ? Cr3 P8 Cr4 P9 -65.26(4) . . . . ? P7 P8 Cr4 P10 -91.89(4) . . . . ? P9 P8 Cr4 P10 39.15(4) . . . . ? Cr3 P8 Cr4 P10 -26.11(4) . . . . ? P9 P8 Cr4 P7 131.04(5) . . . . ? Cr3 P8 Cr4 P7 65.79(4) . . . . ? P7 P8 Cr4 P6 -38.50(4) . . . . ? P9 P8 Cr4 P6 92.54(4) . . . . ? Cr3 P8 Cr4 P6 27.28(4) . . . . ? C32 Cr4 C31 C35 117.5(3) . . . . ? C33 Cr4 C31 C35 79.7(2) . . . . ? C34 Cr4 C31 C35 37.7(2) . . . . ? P9 Cr4 C31 C35 -31.4(3) . . . . ? P10 Cr4 C31 C35 -82.5(2) . . . . ? P7 Cr4 C31 C35 172.92(17) . . . . ? P6 Cr4 C31 C35 -136.4(2) . . . . ? P8 Cr4 C31 C35 100.1(4) . . . . ? C35 Cr4 C31 C32 -117.5(3) . . . . ? C33 Cr4 C31 C32 -37.9(2) . . . . ? C34 Cr4 C31 C32 -79.9(2) . . . . ? P9 Cr4 C31 C32 -148.90(18) . . . . ? P10 Cr4 C31 C32 160.01(19) . . . . ? P7 Cr4 C31 C32 55.4(2) . . . . ? P6 Cr4 C31 C32 106.1(2) . . . . ? P8 Cr4 C31 C32 -17.4(5) . . . . ? C32 Cr4 C31 C36 -120.9(4) . . . . ? C35 Cr4 C31 C36 121.6(4) . . . . ? C33 Cr4 C31 C36 -158.7(4) . . . . ? C34 Cr4 C31 C36 159.3(4) . . . . ? P9 Cr4 C31 C36 90.2(3) . . . . ? P10 Cr4 C31 C36 39.2(3) . . . . ? P7 Cr4 C31 C36 -65.5(3) . . . . ? P6 Cr4 C31 C36 -14.8(3) . . . . ? P8 Cr4 C31 C36 -138.3(3) . . . . ? C35 C31 C32 C33 -0.1(4) . . . . ? C36 C31 C32 C33 -177.7(4) . . . . ? Cr4 C31 C32 C33 62.5(3) . . . . ? C35 C31 C32 C37 177.4(4) . . . . ? C36 C31 C32 C37 -0.2(6) . . . . ? Cr4 C31 C32 C37 -120.1(4) . . . . ? C35 C31 C32 Cr4 -62.5(3) . . . . ? C36 C31 C32 Cr4 119.8(4) . . . . ? C31 Cr4 C32 C33 -116.8(3) . . . . ? C35 Cr4 C32 C33 -79.4(2) . . . . ? C34 Cr4 C32 C33 -36.8(2) . . . . ? P9 Cr4 C32 C33 -18.9(4) . . . . ? P10 Cr4 C32 C33 -147.59(18) . . . . ? P7 Cr4 C32 C33 107.2(2) . . . . ? P6 Cr4 C32 C33 161.32(19) . . . . ? P8 Cr4 C32 C33 56.7(2) . . . . ? C35 Cr4 C32 C31 37.3(2) . . . . ? C33 Cr4 C32 C31 116.8(3) . . . . ? C34 Cr4 C32 C31 79.9(2) . . . . ? P9 Cr4 C32 C31 97.9(4) . . . . ? P10 Cr4 C32 C31 -30.8(3) . . . . ? P7 Cr4 C32 C31 -136.02(19) . . . . ? P6 Cr4 C32 C31 -81.9(2) . . . . ? P8 Cr4 C32 C31 173.47(17) . . . . ? C31 Cr4 C32 C37 120.7(4) . . . . ? C35 Cr4 C32 C37 158.0(4) . . . . ? C33 Cr4 C32 C37 -122.5(4) . . . . ? C34 Cr4 C32 C37 -159.4(4) . . . . ? P9 Cr4 C32 C37 -141.4(3) . . . . ? P10 Cr4 C32 C37 89.9(3) . . . . ? P7 Cr4 C32 C37 -15.3(3) . . . . ? P6 Cr4 C32 C37 38.8(3) . . . . ? P8 Cr4 C32 C37 -65.8(3) . . . . ? C31 C32 C33 C34 0.0(4) . . . . ? C37 C32 C33 C34 -177.4(4) . . . . ? Cr4 C32 C33 C34 61.9(3) . . . . ? C31 C32 C33 C38 177.7(4) . . . . ? C37 C32 C33 C38 0.3(7) . . . . ? Cr4 C32 C33 C38 -120.4(4) . . . . ? C31 C32 C33 Cr4 -61.8(3) . . . . ? C37 C32 C33 Cr4 120.7(4) . . . . ? C31 Cr4 C33 C34 -79.9(2) . . . . ? C32 Cr4 C33 C34 -118.1(3) . . . . ? C35 Cr4 C33 C34 -37.3(2) . . . . ? P9 Cr4 C33 C34 54.5(3) . . . . ? P10 Cr4 C33 C34 -21.3(4) . . . . ? P7 Cr4 C33 C34 160.7(2) . . . . ? P6 Cr4 C33 C34 -147.3(2) . . . . ? P8 Cr4 C33 C34 106.6(2) . . . . ? C31 Cr4 C33 C32 38.3(2) . . . . ? C35 Cr4 C33 C32 80.8(2) . . . . ? C34 Cr4 C33 C32 118.1(3) . . . . ? P9 Cr4 C33 C32 172.57(18) . . . . ? P10 Cr4 C33 C32 96.8(3) . . . . ? P7 Cr4 C33 C32 -81.1(2) . . . . ? P6 Cr4 C33 C32 -29.2(3) . . . . ? P8 Cr4 C33 C32 -135.3(2) . . . . ? C31 Cr4 C33 C38 160.5(4) . . . . ? C32 Cr4 C33 C38 122.2(4) . . . . ? C35 Cr4 C33 C38 -157.0(4) . . . . ? C34 Cr4 C33 C38 -119.7(4) . . . . ? P9 Cr4 C33 C38 -65.2(3) . . . . ? P10 Cr4 C33 C38 -141.0(3) . . . . ? P7 Cr4 C33 C38 41.1(3) . . . . ? P6 Cr4 C33 C38 93.0(3) . . . . ? P8 Cr4 C33 C38 -13.1(3) . . . . ? C32 C33 C34 C35 0.0(5) . . . . ? C38 C33 C34 C35 -177.8(4) . . . . ? Cr4 C33 C34 C35 61.2(3) . . . . ? C32 C33 C34 C39 176.4(4) . . . . ? C38 C33 C34 C39 -1.3(7) . . . . ? Cr4 C33 C34 C39 -122.3(4) . . . . ? C32 C33 C34 Cr4 -61.2(3) . . . . ? C38 C33 C34 Cr4 121.0(4) . . . . ? C31 Cr4 C34 C33 80.6(2) . . . . ? C32 Cr4 C34 C33 37.4(2) . . . . ? C35 Cr4 C34 C33 118.2(3) . . . . ? P9 Cr4 C34 C33 -136.6(2) . . . . ? P10 Cr4 C34 C33 171.29(18) . . . . ? P7 Cr4 C34 C33 -30.1(3) . . . . ? P6 Cr4 C34 C33 98.0(3) . . . . ? P8 Cr4 C34 C33 -82.4(2) . . . . ? C31 Cr4 C34 C35 -37.6(2) . . . . ? C32 Cr4 C34 C35 -80.7(2) . . . . ? C33 Cr4 C34 C35 -118.2(3) . . . . ? P9 Cr4 C34 C35 105.2(2) . . . . ? P10 Cr4 C34 C35 53.1(2) . . . . ? P7 Cr4 C34 C35 -148.31(18) . . . . ? P6 Cr4 C34 C35 -20.2(4) . . . . ? P8 Cr4 C34 C35 159.46(19) . . . . ? C31 Cr4 C34 C39 -158.2(4) . . . . ? C32 Cr4 C34 C39 158.6(4) . . . . ? C35 Cr4 C34 C39 -120.7(4) . . . . ? C33 Cr4 C34 C39 121.1(4) . . . . ? P9 Cr4 C34 C39 -15.4(3) . . . . ? P10 Cr4 C34 C39 -67.6(4) . . . . ? P7 Cr4 C34 C39 91.0(3) . . . . ? P6 Cr4 C34 C39 -140.8(3) . . . . ? P8 Cr4 C34 C39 38.8(3) . . . . ? C32 C31 C35 C34 0.1(4) . . . . ? C36 C31 C35 C34 177.7(4) . . . . ? Cr4 C31 C35 C34 -62.0(3) . . . . ? C32 C31 C35 C40 -177.1(4) . . . . ? C36 C31 C35 C40 0.6(6) . . . . ? Cr4 C31 C35 C40 120.8(4) . . . . ? C32 C31 C35 Cr4 62.1(3) . . . . ? C36 C31 C35 Cr4 -120.3(4) . . . . ? C33 C34 C35 C31 -0.1(5) . . . . ? C39 C34 C35 C31 -176.5(4) . . . . ? Cr4 C34 C35 C31 61.4(3) . . . . ? C33 C34 C35 C40 177.1(4) . . . . ? C39 C34 C35 C40 0.7(7) . . . . ? Cr4 C34 C35 C40 -121.4(4) . . . . ? C33 C34 C35 Cr4 -61.5(3) . . . . ? C39 C34 C35 Cr4 122.1(4) . . . . ? C32 Cr4 C35 C31 -37.9(2) . . . . ? C33 Cr4 C35 C31 -80.5(2) . . . . ? C34 Cr4 C35 C31 -117.4(3) . . . . ? P9 Cr4 C35 C31 159.72(19) . . . . ? P10 Cr4 C35 C31 105.0(2) . . . . ? P7 Cr4 C35 C31 -17.9(4) . . . . ? P6 Cr4 C35 C31 54.5(2) . . . . ? P8 Cr4 C35 C31 -149.99(18) . . . . ? C31 Cr4 C35 C34 117.4(3) . . . . ? C32 Cr4 C35 C34 79.5(2) . . . . ? C33 Cr4 C35 C34 36.8(2) . . . . ? P9 Cr4 C35 C34 -82.9(2) . . . . ? P10 Cr4 C35 C34 -137.6(2) . . . . ? P7 Cr4 C35 C34 99.4(3) . . . . ? P6 Cr4 C35 C34 171.87(18) . . . . ? P8 Cr4 C35 C34 -32.6(3) . . . . ? C31 Cr4 C35 C40 -121.1(4) . . . . ? C32 Cr4 C35 C40 -159.0(4) . . . . ? C33 Cr4 C35 C40 158.3(4) . . . . ? C34 Cr4 C35 C40 121.5(4) . . . . ? P9 Cr4 C35 C40 38.6(3) . . . . ? P10 Cr4 C35 C40 -16.1(3) . . . . ? P7 Cr4 C35 C40 -139.1(3) . . . . ? P6 Cr4 C35 C40 -66.6(3) . . . . ? P8 Cr4 C35 C40 88.9(3) . . . . ? _diffrn_measured_fraction_theta_max 0.906 _diffrn_reflns_theta_full 30.57 _diffrn_measured_fraction_theta_full 0.906 _refine_diff_density_max 3.992 _refine_diff_density_min -2.913 _refine_diff_density_rms 0.209 #===END data_025k _database_code_depnum_ccdc_archive 'CCDC 618761' _audit_creation_method SHELXL-97 _chemical_name_systematic ; \m~2~-\h^5^,\h^5^-cyclopentaphosphole)-bis ((\h^5^-pentamethyl-cyclopentadienyl)-chromium) hexafluoroantimonate ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H30 Cr2 F6 P5 Sb' _chemical_formula_weight 765.04 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M I2/a loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' _cell_length_a 22.845(8) _cell_length_b 21.263(7) _cell_length_c 22.907(8) _cell_angle_alpha 90.000 _cell_angle_beta 101.04(2) _cell_angle_gamma 90.000 _cell_volume 10921(6) _cell_formula_units_Z 16 _cell_measurement_temperature 25(1) _cell_measurement_reflns_used 24 _cell_measurement_theta_min 12.15 _cell_measurement_theta_max 15.36 _exptl_crystal_description 'irregular prism' _exptl_crystal_colour 'dark green' _exptl_crystal_size_max 0.54 _exptl_crystal_size_mid 0.48 _exptl_crystal_size_min 0.34 _exptl_crystal_density_meas 'not measured' _exptl_crystal_density_diffrn 1.861 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 6048 _exptl_absorpt_coefficient_mu 2.108 _exptl_absorpt_correction_type integration _exptl_absorpt_correction_T_min 0.385 _exptl_absorpt_correction_T_max 0.539 _exptl_absorpt_process_details 'XPREP in SHELXTL' _exptl_special_details ; ? ; _diffrn_ambient_temperature 25(1) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Fddd 4-circle diffractometer' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number 4 _diffrn_standards_interval_count 146 _diffrn_standards_interval_time ? _diffrn_standards_decay_% 0 _diffrn_reflns_number 12278 _diffrn_reflns_av_R_equivalents 0.0282 _diffrn_reflns_av_sigmaI/netI 0.0178 _diffrn_reflns_limit_h_min -27 _diffrn_reflns_limit_h_max 26 _diffrn_reflns_limit_k_min -1 _diffrn_reflns_limit_k_max 25 _diffrn_reflns_limit_l_min -1 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_theta_min 1.15 _diffrn_reflns_theta_max 25.00 _reflns_number_total 9623 _reflns_number_gt 9466 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'MAD (Allibon, 1996)' _computing_cell_refinement 'MAD (Allibon, 1996)' _computing_data_reduction 'COLL5N (Lehmann & Wilson, 1987)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'SHELXTL V6.12(Bruker, 2001)' _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0772P)^2^+77.7438P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 9623 _refine_ls_number_parameters 614 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0431 _refine_ls_R_factor_gt 0.0424 _refine_ls_wR_factor_ref 0.1135 _refine_ls_wR_factor_gt 0.1124 _refine_ls_goodness_of_fit_ref 1.035 _refine_ls_restrained_S_all 1.035 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _diffrn_measured_fraction_theta_max 0.998 _diffrn_reflns_theta_full 25.00 _diffrn_measured_fraction_theta_full 0.998 _refine_diff_density_max 1.710 _refine_diff_density_min -1.590 _refine_diff_density_rms 0.245 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb1 Sb 0.138710(17) 0.868720(18) 0.383837(17) 0.01756(10) Uani 1 1 d . . . F1 F 0.09743(15) 0.80761(17) 0.33204(16) 0.0249(8) Uani 1 1 d . . . F2 F 0.09062(16) 0.93185(16) 0.34105(16) 0.0246(7) Uani 1 1 d . . . F3 F 0.08335(15) 0.86014(17) 0.43458(16) 0.0239(7) Uani 1 1 d . . . F4 F 0.18498(14) 0.80476(16) 0.42705(15) 0.0224(7) Uani 1 1 d . . . F5 F 0.19501(16) 0.87684(16) 0.33422(17) 0.0241(8) Uani 1 1 d . . . F6 F 0.17996(15) 0.93051(16) 0.43435(15) 0.0233(7) Uani 1 1 d . . . Sb2 Sb 0.136316(17) 0.127311(18) 0.117144(18) 0.01728(10) Uani 1 1 d . . . F7 F 0.12341(17) 0.05047(18) 0.15211(17) 0.0334(9) Uani 1 1 d . . . F8 F 0.07133(15) 0.16343(18) 0.14344(16) 0.0278(8) Uani 1 1 d . . . F9 F 0.08549(15) 0.10177(18) 0.04624(15) 0.0263(8) Uani 1 1 d . . . F10 F 0.20194(15) 0.09352(18) 0.08941(16) 0.0268(8) Uani 1 1 d . . . F11 F 0.18725(15) 0.15293(17) 0.18759(15) 0.0249(7) Uani 1 1 d . . . F12 F 0.15011(16) 0.20429(18) 0.08144(17) 0.0298(8) Uani 1 1 d . . . C1 C -0.1129(2) 0.3107(3) 0.4475(3) 0.0181(11) Uani 1 1 d . . . C2 C -0.1420(2) 0.2685(3) 0.4031(3) 0.0182(11) Uani 1 1 d . . . C3 C -0.1411(2) 0.2956(3) 0.3461(3) 0.0194(12) Uani 1 1 d . . . C4 C -0.1115(2) 0.3555(3) 0.3552(3) 0.0179(11) Uani 1 1 d . . . C5 C -0.0944(2) 0.3647(3) 0.4177(3) 0.0183(12) Uani 1 1 d . . . C6 C -0.1060(3) 0.3033(3) 0.5134(3) 0.0224(12) Uani 1 1 d . . . H6A H -0.1400 0.3229 0.5267 0.034 Uiso 1 1 calc R . . H6B H -0.0690 0.3237 0.5331 0.034 Uiso 1 1 calc R . . H6C H -0.1045 0.2585 0.5235 0.034 Uiso 1 1 calc R . . C7 C -0.1708(2) 0.2075(3) 0.4146(3) 0.0196(11) Uani 1 1 d . . . H7A H -0.2124 0.2152 0.4178 0.029 Uiso 1 1 calc R . . H7B H -0.1493 0.1891 0.4518 0.029 Uiso 1 1 calc R . . H7C H -0.1696 0.1784 0.3816 0.029 Uiso 1 1 calc R . . C8 C -0.1678(3) 0.2687(3) 0.2866(3) 0.0221(12) Uani 1 1 d . . . H8A H -0.2059 0.2896 0.2713 0.033 Uiso 1 1 calc R . . H8B H -0.1744 0.2235 0.2905 0.033 Uiso 1 1 calc R . . H8C H -0.1406 0.2755 0.2589 0.033 Uiso 1 1 calc R . . C9 C -0.1039(3) 0.4012(3) 0.3076(3) 0.0208(12) Uani 1 1 d . . . H9A H -0.1361 0.4322 0.3026 0.031 Uiso 1 1 calc R . . H9B H -0.1051 0.3786 0.2701 0.031 Uiso 1 1 calc R . . H9C H -0.0654 0.4226 0.3189 0.031 Uiso 1 1 calc R . . C10 C -0.0672(3) 0.4233(3) 0.4488(3) 0.0184(11) Uani 1 1 d . . . H10A H -0.0937 0.4402 0.4739 0.028 Uiso 1 1 calc R . . H10B H -0.0617 0.4548 0.4191 0.028 Uiso 1 1 calc R . . H10C H -0.0285 0.4130 0.4735 0.028 Uiso 1 1 calc R . . Cr1 Cr -0.04858(4) 0.27961(4) 0.39253(4) 0.01603(19) Uani 1 1 d . . . P1 P 0.03494(7) 0.26901(8) 0.47196(7) 0.0258(3) Uani 1 1 d . . . P2 P -0.01395(7) 0.18214(8) 0.43771(8) 0.0247(3) Uani 1 1 d . . . P3 P -0.03324(7) 0.18709(8) 0.33903(8) 0.0235(3) Uani 1 1 d . . . P4 P 0.00310(7) 0.27721(8) 0.31152(7) 0.0238(3) Uani 1 1 d . . . P5 P 0.04523(7) 0.32772(8) 0.39403(8) 0.0247(3) Uani 1 1 d . . . Cr2 Cr 0.06324(4) 0.21798(4) 0.38895(4) 0.01614(19) Uani 1 1 d . . . C11 C 0.1466(2) 0.1773(3) 0.4400(3) 0.0164(11) Uani 1 1 d . . . C12 C 0.1158(2) 0.1300(3) 0.4009(3) 0.0170(11) Uani 1 1 d . . . C13 C 0.1127(2) 0.1521(3) 0.3412(3) 0.0193(12) Uani 1 1 d . . . C14 C 0.1403(2) 0.2121(3) 0.3437(3) 0.0183(12) Uani 1 1 d . . . C15 C 0.1616(2) 0.2280(3) 0.4049(3) 0.0171(11) Uani 1 1 d . . . C16 C 0.1627(3) 0.1709(3) 0.5061(3) 0.0217(12) Uani 1 1 d . . . H16A H 0.2003 0.1477 0.5168 0.033 Uiso 1 1 calc R . . H16B H 0.1310 0.1482 0.5205 0.033 Uiso 1 1 calc R . . H16C H 0.1674 0.2128 0.5242 0.033 Uiso 1 1 calc R . . C17 C 0.0954(3) 0.0670(3) 0.4189(3) 0.0219(12) Uani 1 1 d . . . H17A H 0.1273 0.0361 0.4195 0.033 Uiso 1 1 calc R . . H17B H 0.0600 0.0538 0.3903 0.033 Uiso 1 1 calc R . . H17C H 0.0856 0.0701 0.4586 0.033 Uiso 1 1 calc R . . C18 C 0.0884(3) 0.1155(3) 0.2856(3) 0.0219(12) Uani 1 1 d . . . H18A H 0.1206 0.0911 0.2738 0.033 Uiso 1 1 calc R . . H18B H 0.0717 0.1446 0.2536 0.033 Uiso 1 1 calc R . . H18C H 0.0571 0.0869 0.2933 0.033 Uiso 1 1 calc R . . C19 C 0.1494(3) 0.2502(3) 0.2917(3) 0.0211(12) Uani 1 1 d . . . H19A H 0.1914 0.2482 0.2881 0.032 Uiso 1 1 calc R . . H19B H 0.1383 0.2940 0.2974 0.032 Uiso 1 1 calc R . . H19C H 0.1244 0.2335 0.2555 0.032 Uiso 1 1 calc R . . C20 C 0.1955(3) 0.2862(3) 0.4272(3) 0.0216(12) Uani 1 1 d . . . H20A H 0.2384 0.2783 0.4314 0.032 Uiso 1 1 calc R . . H20B H 0.1865 0.2979 0.4659 0.032 Uiso 1 1 calc R . . H20C H 0.1839 0.3206 0.3988 0.032 Uiso 1 1 calc R . . C21 C 0.1077(3) 0.3849(3) 0.1332(3) 0.0188(12) Uani 1 1 d . . . C22 C 0.1714(3) 0.3821(3) 0.1462(3) 0.0172(12) Uani 1 1 d . . . C23 C 0.1934(3) 0.4384(3) 0.1245(3) 0.0207(12) Uani 1 1 d . . . C24 C 0.1445(3) 0.4762(3) 0.0977(3) 0.0201(12) Uani 1 1 d . . . C25 C 0.0913(3) 0.4432(3) 0.1031(3) 0.0199(12) Uani 1 1 d . . . C26 C 0.0650(3) 0.3350(3) 0.1441(3) 0.0223(12) Uani 1 1 d . . . H26A H 0.0564 0.3070 0.1096 0.033 Uiso 1 1 calc R . . H26B H 0.0279 0.3546 0.1505 0.033 Uiso 1 1 calc R . . H26C H 0.0827 0.3107 0.1794 0.033 Uiso 1 1 calc R . . C27 C 0.2083(3) 0.3275(3) 0.1727(3) 0.0218(12) Uani 1 1 d . . . H27A H 0.2264 0.3072 0.1421 0.033 Uiso 1 1 calc R . . H27B H 0.1829 0.2972 0.1883 0.033 Uiso 1 1 calc R . . H27C H 0.2397 0.3422 0.2051 0.033 Uiso 1 1 calc R . . C28 C 0.2585(3) 0.4518(3) 0.1247(3) 0.0245(13) Uani 1 1 d . . . H28A H 0.2688 0.4364 0.0876 0.037 Uiso 1 1 calc R . . H28B H 0.2833 0.4304 0.1585 0.037 Uiso 1 1 calc R . . H28C H 0.2656 0.4972 0.1280 0.037 Uiso 1 1 calc R . . C29 C 0.1485(3) 0.5375(3) 0.0657(3) 0.0228(12) Uani 1 1 d . . . H29A H 0.1489 0.5292 0.0237 0.034 Uiso 1 1 calc R . . H29B H 0.1852 0.5595 0.0838 0.034 Uiso 1 1 calc R . . H29C H 0.1140 0.5638 0.0688 0.034 Uiso 1 1 calc R . . C30 C 0.0288(3) 0.4643(3) 0.0786(3) 0.0216(12) Uani 1 1 d . . . H30A H 0.0147 0.4443 0.0400 0.032 Uiso 1 1 calc R . . H30B H 0.0280 0.5101 0.0738 0.032 Uiso 1 1 calc R . . H30C H 0.0027 0.4522 0.1062 0.032 Uiso 1 1 calc R . . Cr3 Cr 0.14313(4) 0.46403(4) 0.19309(4) 0.0180(2) Uani 1 1 d . . . P6 P 0.08599(7) 0.44289(7) 0.27000(7) 0.0206(3) Uani 1 1 d . . . P7 P 0.18294(7) 0.42916(7) 0.29518(7) 0.0197(3) Uani 1 1 d . . . P8 P 0.22715(7) 0.50915(7) 0.26137(7) 0.0210(3) Uani 1 1 d . . . P9 P 0.15753(7) 0.57470(7) 0.21830(7) 0.0204(3) Uani 1 1 d . . . P10 P 0.06986(7) 0.53292(7) 0.22276(7) 0.0198(3) Uani 1 1 d . . . Cr4 Cr 0.14543(4) 0.53278(4) 0.31324(4) 0.0179(2) Uani 1 1 d . . . C31 C 0.0962(3) 0.5523(3) 0.3846(3) 0.0186(12) Uani 1 1 d . . . C32 C 0.1522(3) 0.5239(3) 0.4100(3) 0.0180(11) Uani 1 1 d . . . C33 C 0.1983(3) 0.5653(3) 0.3991(3) 0.0194(12) Uani 1 1 d . . . C34 C 0.1709(3) 0.6183(3) 0.3671(3) 0.0194(12) Uani 1 1 d . . . C35 C 0.1075(3) 0.6101(3) 0.3584(3) 0.0183(11) Uani 1 1 d . . . C36 C 0.0358(3) 0.5263(3) 0.3871(3) 0.0218(12) Uani 1 1 d . . . H36A H 0.0210 0.5454 0.4204 0.033 Uiso 1 1 calc R . . H36B H 0.0386 0.4806 0.3927 0.033 Uiso 1 1 calc R . . H36C H 0.0082 0.5358 0.3498 0.033 Uiso 1 1 calc R . . C37 C 0.1610(3) 0.4633(3) 0.4441(3) 0.0213(12) Uani 1 1 d . . . H37A H 0.1539 0.4702 0.4844 0.032 Uiso 1 1 calc R . . H37B H 0.2019 0.4483 0.4460 0.032 Uiso 1 1 calc R . . H37C H 0.1328 0.4318 0.4240 0.032 Uiso 1 1 calc R . . C38 C 0.2645(2) 0.5567(3) 0.4196(3) 0.0221(12) Uani 1 1 d . . . H38A H 0.2775 0.5789 0.4573 0.033 Uiso 1 1 calc R . . H38B H 0.2855 0.5737 0.3896 0.033 Uiso 1 1 calc R . . H38C H 0.2736 0.5118 0.4252 0.033 Uiso 1 1 calc R . . C39 C 0.2032(3) 0.6751(3) 0.3503(3) 0.0224(12) Uani 1 1 d . . . H39A H 0.2116 0.7040 0.3842 0.034 Uiso 1 1 calc R . . H39B H 0.1782 0.6963 0.3165 0.034 Uiso 1 1 calc R . . H39C H 0.2407 0.6619 0.3393 0.034 Uiso 1 1 calc R . . C40 C 0.0622(3) 0.6574(3) 0.3294(3) 0.0226(12) Uani 1 1 d . . . H40A H 0.0515 0.6852 0.3599 0.034 Uiso 1 1 calc R . . H40B H 0.0265 0.6354 0.3088 0.034 Uiso 1 1 calc R . . H40C H 0.0791 0.6824 0.3008 0.034 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.0136(2) 0.01963(18) 0.0191(2) -0.00085(15) 0.00212(14) 0.00017(14) F1 0.0217(17) 0.0262(18) 0.0252(18) -0.0087(15) 0.0006(14) -0.0035(14) F2 0.0257(18) 0.0235(17) 0.0228(18) 0.0037(14) 0.0001(14) 0.0097(15) F3 0.0195(17) 0.0276(17) 0.0264(18) 0.0010(15) 0.0089(14) 0.0031(14) F4 0.0151(16) 0.0247(17) 0.0268(18) 0.0092(15) 0.0029(14) 0.0066(14) F5 0.0188(17) 0.030(2) 0.0255(19) -0.0028(14) 0.0107(15) -0.0012(14) F6 0.0242(18) 0.0228(17) 0.0224(18) -0.0063(14) 0.0031(14) -0.0057(14) Sb2 0.0125(2) 0.01957(18) 0.0192(2) -0.00066(14) 0.00158(13) -0.00018(14) F7 0.036(2) 0.031(2) 0.032(2) 0.0045(16) 0.0029(17) -0.0033(17) F8 0.0179(17) 0.038(2) 0.0285(19) -0.0036(16) 0.0078(14) 0.0060(15) F9 0.0214(18) 0.0318(19) 0.0236(18) -0.0049(16) -0.0011(14) -0.0029(15) F10 0.0175(17) 0.035(2) 0.0279(19) -0.0071(16) 0.0036(14) 0.0068(15) F11 0.0210(17) 0.0298(19) 0.0222(17) -0.0056(14) 0.0000(14) 0.0004(14) F12 0.0248(19) 0.032(2) 0.030(2) 0.0044(16) 0.0009(16) -0.0029(15) C1 0.013(3) 0.021(3) 0.019(3) 0.000(2) 0.002(2) 0.002(2) C2 0.012(3) 0.019(3) 0.022(3) 0.000(2) 0.001(2) 0.003(2) C3 0.006(2) 0.028(3) 0.023(3) -0.003(2) -0.002(2) 0.001(2) C4 0.008(2) 0.022(3) 0.023(3) 0.002(2) 0.001(2) 0.002(2) C5 0.009(2) 0.025(3) 0.022(3) 0.000(2) 0.006(2) 0.006(2) C6 0.021(3) 0.026(3) 0.020(3) 0.001(2) 0.005(2) 0.002(2) C7 0.013(3) 0.023(3) 0.022(3) -0.001(2) 0.001(2) -0.003(2) C8 0.019(3) 0.023(3) 0.022(3) -0.005(2) -0.002(2) -0.003(2) C9 0.014(3) 0.028(3) 0.019(3) 0.001(2) 0.001(2) 0.000(2) C10 0.016(3) 0.020(3) 0.018(3) -0.001(2) 0.001(2) -0.001(2) Cr1 0.0103(4) 0.0186(4) 0.0184(5) -0.0006(3) 0.0011(3) -0.0007(3) P1 0.0176(7) 0.0366(9) 0.0214(8) -0.0057(7) -0.0006(6) 0.0060(6) P2 0.0182(7) 0.0279(8) 0.0291(8) 0.0054(7) 0.0068(6) 0.0033(6) P3 0.0138(7) 0.0248(8) 0.0301(8) -0.0080(6) -0.0006(6) 0.0003(6) P4 0.0181(7) 0.0316(8) 0.0217(8) 0.0034(6) 0.0042(6) 0.0047(6) P5 0.0139(7) 0.0219(8) 0.0380(9) -0.0034(7) 0.0041(6) -0.0018(6) Cr2 0.0103(4) 0.0188(4) 0.0184(5) -0.0006(3) 0.0003(3) 0.0002(3) C11 0.008(2) 0.023(3) 0.018(3) 0.003(2) 0.004(2) 0.005(2) C12 0.010(3) 0.016(3) 0.023(3) 0.000(2) -0.001(2) 0.003(2) C13 0.012(3) 0.019(3) 0.026(3) 0.005(2) 0.003(2) 0.004(2) C14 0.008(2) 0.025(3) 0.020(3) -0.002(2) 0.000(2) 0.003(2) C15 0.012(3) 0.019(3) 0.019(3) 0.002(2) 0.000(2) 0.003(2) C16 0.020(3) 0.028(3) 0.015(3) 0.001(2) -0.002(2) 0.001(2) C17 0.018(3) 0.017(3) 0.031(3) -0.001(2) 0.008(2) -0.003(2) C18 0.014(3) 0.029(3) 0.022(3) -0.005(2) 0.001(2) 0.000(2) C19 0.017(3) 0.025(3) 0.021(3) 0.004(2) 0.002(2) 0.003(2) C20 0.016(3) 0.025(3) 0.023(3) -0.001(2) 0.000(2) 0.001(2) C21 0.012(3) 0.021(3) 0.022(3) 0.001(2) 0.000(2) 0.001(2) C22 0.013(3) 0.023(3) 0.015(3) -0.003(2) 0.003(2) 0.000(2) C23 0.019(3) 0.023(3) 0.021(3) -0.002(2) 0.006(2) -0.001(2) C24 0.014(3) 0.027(3) 0.020(3) 0.005(2) 0.005(2) 0.000(2) C25 0.017(3) 0.022(3) 0.021(3) -0.002(2) 0.002(2) 0.001(2) C26 0.013(3) 0.025(3) 0.028(3) 0.000(2) 0.000(2) -0.004(2) C27 0.017(3) 0.022(3) 0.024(3) 0.001(2) -0.001(2) -0.001(2) C28 0.015(3) 0.031(3) 0.030(3) 0.000(3) 0.009(2) -0.001(2) C29 0.025(3) 0.019(3) 0.025(3) 0.000(2) 0.006(2) 0.000(2) C30 0.019(3) 0.028(3) 0.017(3) 0.003(2) 0.001(2) 0.002(2) Cr3 0.0113(4) 0.0207(5) 0.0214(5) 0.0036(4) 0.0014(4) 0.0018(3) P6 0.0177(7) 0.0244(8) 0.0196(7) -0.0030(6) 0.0036(6) -0.0038(6) P7 0.0189(7) 0.0210(7) 0.0182(7) 0.0008(6) 0.0010(6) 0.0014(6) P8 0.0148(7) 0.0265(8) 0.0212(7) -0.0027(6) 0.0025(6) -0.0014(6) P9 0.0222(7) 0.0201(7) 0.0185(7) 0.0009(6) 0.0031(6) -0.0006(6) P10 0.0155(7) 0.0229(8) 0.0195(7) -0.0018(6) -0.0005(6) 0.0032(6) Cr4 0.0114(4) 0.0205(5) 0.0208(5) 0.0024(4) 0.0002(4) 0.0001(3) C31 0.015(3) 0.020(3) 0.020(3) 0.000(2) 0.002(2) 0.000(2) C32 0.018(3) 0.019(3) 0.016(3) -0.002(2) 0.000(2) -0.004(2) C33 0.015(3) 0.025(3) 0.018(3) -0.004(2) 0.004(2) -0.006(2) C34 0.015(3) 0.022(3) 0.020(3) 0.001(2) 0.002(2) -0.003(2) C35 0.013(3) 0.024(3) 0.017(3) -0.003(2) 0.002(2) -0.003(2) C36 0.018(3) 0.023(3) 0.024(3) 0.003(2) 0.004(2) 0.001(2) C37 0.017(3) 0.021(3) 0.024(3) 0.002(2) -0.001(2) 0.002(2) C38 0.013(3) 0.026(3) 0.024(3) 0.001(2) -0.003(2) 0.002(2) C39 0.020(3) 0.020(3) 0.027(3) 0.002(2) 0.003(2) -0.001(2) C40 0.020(3) 0.026(3) 0.021(3) -0.001(2) 0.004(2) 0.006(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb1 F6 1.880(3) . ? Sb1 F5 1.880(3) . ? Sb1 F4 1.883(3) . ? Sb1 F3 1.883(3) . ? Sb1 F2 1.886(3) . ? Sb1 F1 1.886(3) . ? Sb2 F7 1.868(4) . ? Sb2 F8 1.871(3) . ? Sb2 F10 1.879(3) . ? Sb2 F11 1.880(3) . ? Sb2 F12 1.883(4) . ? Sb2 F9 1.886(3) . ? C1 C2 1.423(8) . ? C1 C5 1.440(8) . ? C1 C6 1.495(8) . ? C1 Cr1 2.212(6) . ? C2 C3 1.431(9) . ? C2 C7 1.499(8) . ? C2 Cr1 2.207(6) . ? C3 C4 1.438(8) . ? C3 C8 1.497(8) . ? C3 Cr1 2.202(5) . ? C4 C5 1.423(8) . ? C4 C9 1.495(8) . ? C4 Cr1 2.220(6) . ? C5 C10 1.509(8) . ? C5 Cr1 2.222(6) . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? Cr1 P5 2.3690(19) . ? Cr1 P3 2.3789(19) . ? Cr1 P1 2.3815(19) . ? Cr1 P2 2.383(2) . ? Cr1 P4 2.3833(19) . ? Cr1 Cr2 2.8861(16) . ? P1 P2 2.222(3) . ? P1 P5 2.227(3) . ? P1 Cr2 2.3834(19) . ? P2 P3 2.221(3) . ? P2 Cr2 2.3859(19) . ? P3 P4 2.227(2) . ? P3 Cr2 2.3730(19) . ? P4 P5 2.226(3) . ? P4 Cr2 2.3845(19) . ? P5 Cr2 2.376(2) . ? Cr2 C12 2.211(6) . ? Cr2 C14 2.211(6) . ? Cr2 C11 2.212(6) . ? Cr2 C15 2.216(6) . ? Cr2 C13 2.216(6) . ? C11 C15 1.425(8) . ? C11 C12 1.438(8) . ? C11 C16 1.493(8) . ? C12 C13 1.434(8) . ? C12 C17 1.502(8) . ? C13 C14 1.420(8) . ? C13 C18 1.504(8) . ? C14 C15 1.433(8) . ? C14 C19 1.487(8) . ? C15 C20 1.498(8) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 C22 1.430(8) . ? C21 C25 1.433(8) . ? C21 C26 1.495(8) . ? C21 Cr3 2.223(6) . ? C22 C23 1.423(8) . ? C22 C27 1.494(8) . ? C22 Cr3 2.207(6) . ? C23 C24 1.416(8) . ? C23 C28 1.514(8) . ? C23 Cr3 2.185(6) . ? C24 C25 1.429(8) . ? C24 C29 1.506(8) . ? C24 Cr3 2.207(6) . ? C25 C30 1.500(8) . ? C25 Cr3 2.215(6) . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C27 H27C 0.9800 . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? Cr3 P10 2.4177(18) . ? Cr3 P6 2.4271(19) . ? Cr3 P8 2.4292(19) . ? Cr3 P9 2.4304(19) . ? Cr3 P7 2.4558(19) . ? P6 P10 2.195(2) . ? P6 P7 2.199(2) . ? P6 Cr4 2.4420(19) . ? P7 P8 2.194(2) . ? P7 Cr4 2.4281(19) . ? P8 P9 2.201(2) . ? P8 Cr4 2.4493(19) . ? P9 P10 2.211(2) . ? P9 Cr4 2.4148(19) . ? P10 Cr4 2.4302(19) . ? Cr4 C31 2.194(6) . ? Cr4 C32 2.201(6) . ? Cr4 C35 2.207(6) . ? Cr4 C34 2.210(6) . ? Cr4 C33 2.211(6) . ? C31 C35 1.412(8) . ? C31 C32 1.435(8) . ? C31 C36 1.498(8) . ? C32 C33 1.430(8) . ? C32 C37 1.499(8) . ? C33 C34 1.422(9) . ? C33 C38 1.507(8) . ? C34 C35 1.434(8) . ? C34 C39 1.503(8) . ? C35 C40 1.502(8) . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C39 H39A 0.9800 . ? C39 H39B 0.9800 . ? C39 H39C 0.9800 . ? C40 H40A 0.9800 . ? C40 H40B 0.9800 . ? C40 H40C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F6 Sb1 F5 89.29(16) . . ? F6 Sb1 F4 90.95(15) . . ? F5 Sb1 F4 90.22(15) . . ? F6 Sb1 F3 90.25(16) . . ? F5 Sb1 F3 179.03(15) . . ? F4 Sb1 F3 88.93(15) . . ? F6 Sb1 F2 89.76(15) . . ? F5 Sb1 F2 91.05(16) . . ? F4 Sb1 F2 178.55(16) . . ? F3 Sb1 F2 89.80(16) . . ? F6 Sb1 F1 179.02(16) . . ? F5 Sb1 F1 90.02(16) . . ? F4 Sb1 F1 89.76(16) . . ? F3 Sb1 F1 90.44(16) . . ? F2 Sb1 F1 89.55(15) . . ? F7 Sb2 F8 91.20(17) . . ? F7 Sb2 F10 90.70(17) . . ? F8 Sb2 F10 178.10(17) . . ? F7 Sb2 F11 90.45(17) . . ? F8 Sb2 F11 90.20(16) . . ? F10 Sb2 F11 89.91(15) . . ? F7 Sb2 F12 179.25(18) . . ? F8 Sb2 F12 89.55(17) . . ? F10 Sb2 F12 88.56(16) . . ? F11 Sb2 F12 89.62(16) . . ? F7 Sb2 F9 89.76(17) . . ? F8 Sb2 F9 89.99(16) . . ? F10 Sb2 F9 89.89(16) . . ? F11 Sb2 F9 179.71(18) . . ? F12 Sb2 F9 90.16(16) . . ? C2 C1 C5 107.7(5) . . ? C2 C1 C6 126.9(5) . . ? C5 C1 C6 125.3(5) . . ? C2 C1 Cr1 71.0(3) . . ? C5 C1 Cr1 71.4(3) . . ? C6 C1 Cr1 126.1(4) . . ? C1 C2 C3 108.1(5) . . ? C1 C2 C7 125.5(5) . . ? C3 C2 C7 126.3(5) . . ? C1 C2 Cr1 71.4(3) . . ? C3 C2 Cr1 70.9(3) . . ? C7 C2 Cr1 125.3(4) . . ? C2 C3 C4 108.3(5) . . ? C2 C3 C8 127.1(5) . . ? C4 C3 C8 124.6(6) . . ? C2 C3 Cr1 71.2(3) . . ? C4 C3 Cr1 71.7(3) . . ? C8 C3 Cr1 124.6(4) . . ? C5 C4 C3 107.3(5) . . ? C5 C4 C9 126.6(5) . . ? C3 C4 C9 125.9(5) . . ? C5 C4 Cr1 71.4(3) . . ? C3 C4 Cr1 70.3(3) . . ? C9 C4 Cr1 126.6(4) . . ? C4 C5 C1 108.6(5) . . ? C4 C5 C10 126.6(5) . . ? C1 C5 C10 124.5(5) . . ? C4 C5 Cr1 71.3(3) . . ? C1 C5 Cr1 70.7(3) . . ? C10 C5 Cr1 128.5(4) . . ? C1 C6 H6A 109.5 . . ? C1 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C1 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C3 Cr1 C2 37.9(2) . . ? C3 Cr1 C1 63.1(2) . . ? C2 Cr1 C1 37.6(2) . . ? C3 Cr1 C4 38.0(2) . . ? C2 Cr1 C4 63.4(2) . . ? C1 Cr1 C4 63.3(2) . . ? C3 Cr1 C5 62.8(2) . . ? C2 Cr1 C5 62.9(2) . . ? C1 Cr1 C5 37.9(2) . . ? C4 Cr1 C5 37.4(2) . . ? C3 Cr1 P5 136.21(17) . . ? C2 Cr1 P5 159.41(16) . . ? C1 Cr1 P5 124.10(16) . . ? C4 Cr1 P5 102.04(15) . . ? C5 Cr1 P5 96.59(16) . . ? C3 Cr1 P3 95.81(17) . . ? C2 Cr1 P3 102.06(16) . . ? C1 Cr1 P3 136.06(16) . . ? C4 Cr1 P3 123.44(16) . . ? C5 Cr1 P3 158.52(16) . . ? P5 Cr1 P3 98.19(7) . . ? C3 Cr1 P1 159.67(17) . . ? C2 Cr1 P1 123.81(17) . . ? C1 Cr1 P1 96.66(16) . . ? C4 Cr1 P1 136.69(16) . . ? C5 Cr1 P1 103.16(16) . . ? P5 Cr1 P1 55.92(7) . . ? P3 Cr1 P1 98.03(7) . . ? C3 Cr1 P2 123.50(17) . . ? C2 Cr1 P2 96.14(16) . . ? C1 Cr1 P2 102.38(16) . . ? C4 Cr1 P2 159.38(15) . . ? C5 Cr1 P2 136.85(17) . . ? P5 Cr1 P2 98.34(7) . . ? P3 Cr1 P2 55.61(7) . . ? P1 Cr1 P2 55.61(7) . . ? C3 Cr1 P4 101.53(17) . . ? C2 Cr1 P4 135.81(17) . . ? C1 Cr1 P4 158.75(16) . . ? C4 Cr1 P4 95.53(15) . . ? C5 Cr1 P4 123.23(17) . . ? P5 Cr1 P4 55.86(6) . . ? P3 Cr1 P4 55.75(6) . . ? P1 Cr1 P4 98.56(7) . . ? P2 Cr1 P4 98.44(7) . . ? C3 Cr1 Cr2 145.99(16) . . ? C2 Cr1 Cr2 146.58(15) . . ? C1 Cr1 Cr2 147.17(16) . . ? C4 Cr1 Cr2 146.11(15) . . ? C5 Cr1 Cr2 147.26(16) . . ? P5 Cr1 Cr2 52.65(5) . . ? P3 Cr1 Cr2 52.51(5) . . ? P1 Cr1 Cr2 52.75(5) . . ? P2 Cr1 Cr2 52.80(5) . . ? P4 Cr1 Cr2 52.77(5) . . ? P2 P1 P5 107.82(9) . . ? P2 P1 Cr1 62.23(7) . . ? P5 P1 Cr1 61.76(6) . . ? P2 P1 Cr2 62.28(7) . . ? P5 P1 Cr2 61.93(7) . . ? Cr1 P1 Cr2 74.56(6) . . ? P3 P2 P1 107.95(9) . . ? P3 P2 Cr1 62.11(7) . . ? P1 P2 Cr1 62.17(7) . . ? P3 P2 Cr2 61.88(6) . . ? P1 P2 Cr2 62.17(7) . . ? Cr1 P2 Cr2 74.49(6) . . ? P2 P3 P4 108.47(9) . . ? P2 P3 Cr2 62.47(6) . . ? P4 P3 Cr2 62.35(6) . . ? P2 P3 Cr1 62.29(7) . . ? P4 P3 Cr1 62.22(7) . . ? Cr2 P3 Cr1 74.80(6) . . ? P5 P4 P3 107.39(9) . . ? P5 P4 Cr1 61.74(7) . . ? P3 P4 Cr1 62.02(6) . . ? P5 P4 Cr2 61.93(7) . . ? P3 P4 Cr2 61.83(7) . . ? Cr1 P4 Cr2 74.50(6) . . ? P4 P5 P1 108.37(9) . . ? P4 P5 Cr1 62.39(6) . . ? P1 P5 Cr1 62.33(6) . . ? P4 P5 Cr2 62.31(7) . . ? P1 P5 Cr2 62.27(7) . . ? Cr1 P5 Cr2 74.92(6) . . ? C12 Cr2 C14 63.1(2) . . ? C12 Cr2 C11 37.9(2) . . ? C14 Cr2 C11 62.8(2) . . ? C12 Cr2 C15 63.3(2) . . ? C14 Cr2 C15 37.8(2) . . ? C11 Cr2 C15 37.5(2) . . ? C12 Cr2 C13 37.8(2) . . ? C14 Cr2 C13 37.4(2) . . ? C11 Cr2 C13 62.9(2) . . ? C15 Cr2 C13 63.0(2) . . ? C12 Cr2 P3 104.93(16) . . ? C14 Cr2 P3 120.53(16) . . ? C11 Cr2 P3 140.60(17) . . ? C15 Cr2 P3 157.61(16) . . ? C13 Cr2 P3 95.82(16) . . ? C12 Cr2 P5 156.87(16) . . ? C14 Cr2 P5 103.84(16) . . ? C11 Cr2 P5 119.88(16) . . ? C15 Cr2 P5 94.43(15) . . ? C13 Cr2 P5 138.98(16) . . ? P3 Cr2 P5 98.15(7) . . ? C12 Cr2 P1 120.70(17) . . ? C14 Cr2 P1 139.60(16) . . ? C11 Cr2 P1 95.40(16) . . ? C15 Cr2 P1 104.24(16) . . ? C13 Cr2 P1 157.45(16) . . ? P3 Cr2 P1 98.14(7) . . ? P5 Cr2 P1 55.80(7) . . ? C12 Cr2 P4 139.49(17) . . ? C14 Cr2 P4 94.48(16) . . ? C11 Cr2 P4 156.22(16) . . ? C15 Cr2 P4 119.57(16) . . ? C13 Cr2 P4 104.01(16) . . ? P3 Cr2 P4 55.81(6) . . ? P5 Cr2 P4 55.76(7) . . ? P1 Cr2 P4 98.48(7) . . ? C12 Cr2 P2 96.02(16) . . ? C14 Cr2 P2 158.09(17) . . ? C11 Cr2 P2 105.45(16) . . ? C15 Cr2 P2 140.38(16) . . ? C13 Cr2 P2 121.45(16) . . ? P3 Cr2 P2 55.64(7) . . ? P5 Cr2 P2 98.07(7) . . ? P1 Cr2 P2 55.55(7) . . ? P4 Cr2 P2 98.32(7) . . ? C12 Cr2 Cr1 147.49(16) . . ? C14 Cr2 Cr1 145.85(16) . . ? C11 Cr2 Cr1 147.15(15) . . ? C15 Cr2 Cr1 145.75(15) . . ? C13 Cr2 Cr1 147.03(16) . . ? P3 Cr2 Cr1 52.69(5) . . ? P5 Cr2 Cr1 52.43(5) . . ? P1 Cr2 Cr1 52.69(5) . . ? P4 Cr2 Cr1 52.73(5) . . ? P2 Cr2 Cr1 52.71(5) . . ? C15 C11 C12 108.6(5) . . ? C15 C11 C16 126.9(5) . . ? C12 C11 C16 124.4(5) . . ? C15 C11 Cr2 71.4(3) . . ? C12 C11 Cr2 71.0(3) . . ? C16 C11 Cr2 126.2(4) . . ? C13 C12 C11 107.1(5) . . ? C13 C12 C17 126.3(5) . . ? C11 C12 C17 126.3(5) . . ? C13 C12 Cr2 71.3(3) . . ? C11 C12 Cr2 71.1(3) . . ? C17 C12 Cr2 126.8(4) . . ? C14 C13 C12 108.3(5) . . ? C14 C13 C18 126.1(5) . . ? C12 C13 C18 125.4(5) . . ? C14 C13 Cr2 71.1(3) . . ? C12 C13 Cr2 70.9(3) . . ? C18 C13 Cr2 127.2(4) . . ? C13 C14 C15 108.4(5) . . ? C13 C14 C19 125.9(5) . . ? C15 C14 C19 125.6(5) . . ? C13 C14 Cr2 71.5(3) . . ? C15 C14 Cr2 71.3(3) . . ? C19 C14 Cr2 126.2(4) . . ? C11 C15 C14 107.5(5) . . ? C11 C15 C20 126.7(5) . . ? C14 C15 C20 125.7(5) . . ? C11 C15 Cr2 71.1(3) . . ? C14 C15 Cr2 70.9(3) . . ? C20 C15 Cr2 125.3(4) . . ? C11 C16 H16A 109.5 . . ? C11 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C11 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C22 C21 C25 107.3(5) . . ? C22 C21 C26 127.4(5) . . ? C25 C21 C26 125.2(5) . . ? C22 C21 Cr3 70.6(3) . . ? C25 C21 Cr3 70.9(3) . . ? C26 C21 Cr3 127.3(4) . . ? C23 C22 C21 107.8(5) . . ? C23 C22 C27 126.0(5) . . ? C21 C22 C27 126.0(5) . . ? C23 C22 Cr3 70.3(3) . . ? C21 C22 Cr3 71.8(3) . . ? C27 C22 Cr3 127.6(4) . . ? C24 C23 C22 109.1(5) . . ? C24 C23 C28 125.9(5) . . ? C22 C23 C28 124.7(5) . . ? C24 C23 Cr3 72.0(3) . . ? C22 C23 Cr3 71.9(3) . . ? C28 C23 Cr3 127.1(4) . . ? C23 C24 C25 107.2(5) . . ? C23 C24 C29 125.9(5) . . ? C25 C24 C29 126.7(5) . . ? C23 C24 Cr3 70.4(3) . . ? C25 C24 Cr3 71.5(3) . . ? C29 C24 Cr3 126.6(4) . . ? C24 C25 C21 108.5(5) . . ? C24 C25 C30 125.9(5) . . ? C21 C25 C30 125.5(5) . . ? C24 C25 Cr3 70.8(3) . . ? C21 C25 Cr3 71.5(3) . . ? C30 C25 Cr3 126.1(4) . . ? C21 C26 H26A 109.5 . . ? C21 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C21 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C22 C27 H27A 109.5 . . ? C22 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? C22 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? C23 C28 H28A 109.5 . . ? C23 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C23 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C24 C29 H29A 109.5 . . ? C24 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C24 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C25 C30 H30A 109.5 . . ? C25 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? C25 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C23 Cr3 C24 37.6(2) . . ? C23 Cr3 C22 37.8(2) . . ? C24 Cr3 C22 63.2(2) . . ? C23 Cr3 C25 62.7(2) . . ? C24 Cr3 C25 37.7(2) . . ? C22 Cr3 C25 62.9(2) . . ? C23 Cr3 C21 63.0(2) . . ? C24 Cr3 C21 63.3(2) . . ? C22 Cr3 C21 37.7(2) . . ? C25 Cr3 C21 37.7(2) . . ? C23 Cr3 P10 147.21(17) . . ? C24 Cr3 P10 110.45(16) . . ? C22 Cr3 P10 153.91(16) . . ? C25 Cr3 P10 96.15(16) . . ? C21 Cr3 P10 116.27(16) . . ? C23 Cr3 P6 154.89(17) . . ? C24 Cr3 P6 148.48(16) . . ? C22 Cr3 P6 117.12(16) . . ? C25 Cr3 P6 111.88(16) . . ? C21 Cr3 P6 97.21(16) . . ? P10 Cr3 P6 53.88(6) . . ? C23 Cr3 P8 95.87(17) . . ? C24 Cr3 P8 115.56(16) . . ? C22 Cr3 P8 110.85(16) . . ? C25 Cr3 P8 153.26(17) . . ? C21 Cr3 P8 147.72(16) . . ? P10 Cr3 P8 94.82(7) . . ? P6 Cr3 P8 94.26(7) . . ? C23 Cr3 P9 110.27(17) . . ? C24 Cr3 P9 95.42(16) . . ? C22 Cr3 P9 147.20(16) . . ? C25 Cr3 P9 115.98(17) . . ? C21 Cr3 P9 153.64(16) . . ? P10 Cr3 P9 54.27(6) . . ? P6 Cr3 P9 94.24(6) . . ? P8 Cr3 P9 53.87(6) . . ? C23 Cr3 P7 117.36(17) . . ? C24 Cr3 P7 154.87(16) . . ? C22 Cr3 P7 97.81(16) . . ? C25 Cr3 P7 149.32(17) . . ? C21 Cr3 P7 112.58(16) . . ? P10 Cr3 P7 93.75(6) . . ? P6 Cr3 P7 53.52(6) . . ? P8 Cr3 P7 53.36(6) . . ? P9 Cr3 P7 93.30(6) . . ? P10 P6 P7 108.10(9) . . ? P10 P6 Cr3 62.84(6) . . ? P7 P6 Cr3 63.91(6) . . ? P10 P6 Cr4 62.95(6) . . ? P7 P6 Cr4 62.84(6) . . ? Cr3 P6 Cr4 79.33(6) . . ? P8 P7 P6 108.25(9) . . ? P8 P7 Cr4 63.77(6) . . ? P6 P7 Cr4 63.48(6) . . ? P8 P7 Cr3 62.70(6) . . ? P6 P7 Cr3 62.57(6) . . ? Cr4 P7 Cr3 79.04(6) . . ? P7 P8 P9 107.90(9) . . ? P7 P8 Cr3 63.94(6) . . ? P9 P8 Cr3 63.09(6) . . ? P7 P8 Cr4 62.78(6) . . ? P9 P8 Cr4 62.30(6) . . ? Cr3 P8 Cr4 79.15(6) . . ? P8 P9 P10 107.93(9) . . ? P8 P9 Cr4 63.90(6) . . ? P10 P9 Cr4 63.20(6) . . ? P8 P9 Cr3 63.04(6) . . ? P10 P9 Cr3 62.57(6) . . ? Cr4 P9 Cr3 79.80(6) . . ? P6 P10 P9 107.77(8) . . ? P6 P10 Cr3 63.28(6) . . ? P9 P10 Cr3 63.16(6) . . ? P6 P10 Cr4 63.50(6) . . ? P9 P10 Cr4 62.49(6) . . ? Cr3 P10 Cr4 79.75(6) . . ? C31 Cr4 C32 38.1(2) . . ? C31 Cr4 C35 37.4(2) . . ? C32 Cr4 C35 63.3(2) . . ? C31 Cr4 C34 63.0(2) . . ? C32 Cr4 C34 63.2(2) . . ? C35 Cr4 C34 37.9(2) . . ? C31 Cr4 C33 63.2(2) . . ? C32 Cr4 C33 37.8(2) . . ? C35 Cr4 C33 63.1(2) . . ? C34 Cr4 C33 37.5(2) . . ? C31 Cr4 P9 139.85(16) . . ? C32 Cr4 P9 160.20(16) . . ? C35 Cr4 P9 105.69(17) . . ? C34 Cr4 P9 97.81(17) . . ? C33 Cr4 P9 123.25(16) . . ? C31 Cr4 P7 123.16(16) . . ? C32 Cr4 P7 97.72(16) . . ? C35 Cr4 P7 159.91(17) . . ? C34 Cr4 P7 141.03(17) . . ? C33 Cr4 P7 106.53(17) . . ? P9 Cr4 P7 94.39(6) . . ? C31 Cr4 P10 104.66(16) . . ? C32 Cr4 P10 139.54(16) . . ? C35 Cr4 P10 96.92(16) . . ? C34 Cr4 P10 122.86(17) . . ? C33 Cr4 P10 159.31(17) . . ? P9 Cr4 P10 54.31(6) . . ? P7 Cr4 P10 94.13(6) . . ? C31 Cr4 P6 97.23(16) . . ? C32 Cr4 P6 105.53(15) . . ? C35 Cr4 P6 122.38(16) . . ? C34 Cr4 P6 159.39(17) . . ? C33 Cr4 P6 140.49(17) . . ? P9 Cr4 P6 94.26(6) . . ? P7 Cr4 P6 53.68(6) . . ? P10 Cr4 P6 53.55(6) . . ? C31 Cr4 P8 161.34(16) . . ? C32 Cr4 P8 123.89(16) . . ? C35 Cr4 P8 141.70(16) . . ? C34 Cr4 P8 107.23(17) . . ? C33 Cr4 P8 99.12(16) . . ? P9 Cr4 P8 53.81(6) . . ? P7 Cr4 P8 53.45(6) . . ? P10 Cr4 P8 93.98(7) . . ? P6 Cr4 P8 93.38(6) . . ? C35 C31 C32 108.5(5) . . ? C35 C31 C36 125.6(5) . . ? C32 C31 C36 125.8(5) . . ? C35 C31 Cr4 71.8(3) . . ? C32 C31 Cr4 71.2(3) . . ? C36 C31 Cr4 124.5(4) . . ? C33 C32 C31 107.3(5) . . ? C33 C32 C37 126.2(5) . . ? C31 C32 C37 126.4(5) . . ? C33 C32 Cr4 71.5(3) . . ? C31 C32 Cr4 70.7(3) . . ? C37 C32 Cr4 125.1(4) . . ? C34 C33 C32 108.2(5) . . ? C34 C33 C38 125.0(5) . . ? C32 C33 C38 126.8(6) . . ? C34 C33 Cr4 71.2(3) . . ? C32 C33 Cr4 70.7(3) . . ? C38 C33 Cr4 125.7(4) . . ? C33 C34 C35 108.0(5) . . ? C33 C34 C39 125.4(5) . . ? C35 C34 C39 126.4(5) . . ? C33 C34 Cr4 71.3(3) . . ? C35 C34 Cr4 71.0(3) . . ? C39 C34 Cr4 127.4(4) . . ? C31 C35 C34 107.9(5) . . ? C31 C35 C40 127.1(5) . . ? C34 C35 C40 124.9(5) . . ? C31 C35 Cr4 70.8(3) . . ? C34 C35 Cr4 71.2(3) . . ? C40 C35 Cr4 126.2(4) . . ? C31 C36 H36A 109.5 . . ? C31 C36 H36B 109.5 . . ? H36A C36 H36B 109.5 . . ? C31 C36 H36C 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C32 C37 H37A 109.5 . . ? C32 C37 H37B 109.5 . . ? H37A C37 H37B 109.5 . . ? C32 C37 H37C 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? C33 C38 H38A 109.5 . . ? C33 C38 H38B 109.5 . . ? H38A C38 H38B 109.5 . . ? C33 C38 H38C 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? C34 C39 H39A 109.5 . . ? C34 C39 H39B 109.5 . . ? H39A C39 H39B 109.5 . . ? C34 C39 H39C 109.5 . . ? H39A C39 H39C 109.5 . . ? H39B C39 H39C 109.5 . . ? C35 C40 H40A 109.5 . . ? C35 C40 H40B 109.5 . . ? H40A C40 H40B 109.5 . . ? C35 C40 H40C 109.5 . . ? H40A C40 H40C 109.5 . . ? H40B C40 H40C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 C1 C2 C3 0.7(6) . . . . ? C6 C1 C2 C3 176.8(5) . . . . ? Cr1 C1 C2 C3 -61.7(4) . . . . ? C5 C1 C2 C7 -177.0(5) . . . . ? C6 C1 C2 C7 -0.8(9) . . . . ? Cr1 C1 C2 C7 120.6(5) . . . . ? C5 C1 C2 Cr1 62.4(4) . . . . ? C6 C1 C2 Cr1 -121.4(6) . . . . ? C1 C2 C3 C4 -0.5(6) . . . . ? C7 C2 C3 C4 177.2(5) . . . . ? Cr1 C2 C3 C4 -62.5(4) . . . . ? C1 C2 C3 C8 -178.3(5) . . . . ? C7 C2 C3 C8 -0.6(9) . . . . ? Cr1 C2 C3 C8 119.6(6) . . . . ? C1 C2 C3 Cr1 62.1(4) . . . . ? C7 C2 C3 Cr1 -120.3(6) . . . . ? C2 C3 C4 C5 0.1(6) . . . . ? C8 C3 C4 C5 178.0(5) . . . . ? Cr1 C3 C4 C5 -62.2(4) . . . . ? C2 C3 C4 C9 -176.3(5) . . . . ? C8 C3 C4 C9 1.6(9) . . . . ? Cr1 C3 C4 C9 121.5(5) . . . . ? C2 C3 C4 Cr1 62.2(4) . . . . ? C8 C3 C4 Cr1 -119.9(6) . . . . ? C3 C4 C5 C1 0.3(6) . . . . ? C9 C4 C5 C1 176.7(5) . . . . ? Cr1 C4 C5 C1 -61.2(4) . . . . ? C3 C4 C5 C10 -174.0(5) . . . . ? C9 C4 C5 C10 2.4(9) . . . . ? Cr1 C4 C5 C10 124.5(6) . . . . ? C3 C4 C5 Cr1 61.5(4) . . . . ? C9 C4 C5 Cr1 -122.2(6) . . . . ? C2 C1 C5 C4 -0.6(6) . . . . ? C6 C1 C5 C4 -176.9(5) . . . . ? Cr1 C1 C5 C4 61.5(4) . . . . ? C2 C1 C5 C10 173.8(5) . . . . ? C6 C1 C5 C10 -2.4(9) . . . . ? Cr1 C1 C5 C10 -124.0(5) . . . . ? C2 C1 C5 Cr1 -62.1(4) . . . . ? C6 C1 C5 Cr1 121.6(6) . . . . ? C4 C3 Cr1 C2 117.4(5) . . . . ? C8 C3 Cr1 C2 -122.6(7) . . . . ? C2 C3 Cr1 C1 -37.3(3) . . . . ? C4 C3 Cr1 C1 80.2(4) . . . . ? C8 C3 Cr1 C1 -159.9(6) . . . . ? C2 C3 Cr1 C4 -117.4(5) . . . . ? C8 C3 Cr1 C4 120.0(7) . . . . ? C2 C3 Cr1 C5 -80.0(4) . . . . ? C4 C3 Cr1 C5 37.4(3) . . . . ? C8 C3 Cr1 C5 157.4(6) . . . . ? C2 C3 Cr1 P5 -149.6(3) . . . . ? C4 C3 Cr1 P5 -32.1(4) . . . . ? C8 C3 Cr1 P5 87.8(5) . . . . ? C2 C3 Cr1 P3 102.2(3) . . . . ? C4 C3 Cr1 P3 -140.4(3) . . . . ? C8 C3 Cr1 P3 -20.4(5) . . . . ? C2 C3 Cr1 P1 -30.6(7) . . . . ? C4 C3 Cr1 P1 86.9(6) . . . . ? C8 C3 Cr1 P1 -153.2(4) . . . . ? C2 C3 Cr1 P2 50.0(4) . . . . ? C4 C3 Cr1 P2 167.5(3) . . . . ? C8 C3 Cr1 P2 -72.6(5) . . . . ? C2 C3 Cr1 P4 158.4(3) . . . . ? C4 C3 Cr1 P4 -84.2(3) . . . . ? C8 C3 Cr1 P4 35.8(5) . . . . ? C2 C3 Cr1 Cr2 121.7(3) . . . . ? C4 C3 Cr1 Cr2 -120.9(3) . . . . ? C8 C3 Cr1 Cr2 -0.9(7) . . . . ? C1 C2 Cr1 C3 -117.7(5) . . . . ? C7 C2 Cr1 C3 121.5(6) . . . . ? C3 C2 Cr1 C1 117.7(5) . . . . ? C7 C2 Cr1 C1 -120.9(6) . . . . ? C1 C2 Cr1 C4 -80.0(4) . . . . ? C3 C2 Cr1 C4 37.6(3) . . . . ? C7 C2 Cr1 C4 159.1(6) . . . . ? C1 C2 Cr1 C5 -37.9(3) . . . . ? C3 C2 Cr1 C5 79.7(4) . . . . ? C7 C2 Cr1 C5 -158.8(6) . . . . ? C1 C2 Cr1 P5 -32.2(7) . . . . ? C3 C2 Cr1 P5 85.5(6) . . . . ? C7 C2 Cr1 P5 -153.0(4) . . . . ? C1 C2 Cr1 P3 158.4(3) . . . . ? C3 C2 Cr1 P3 -83.9(3) . . . . ? C7 C2 Cr1 P3 37.6(5) . . . . ? C1 C2 Cr1 P1 50.1(4) . . . . ? C3 C2 Cr1 P1 167.7(3) . . . . ? C7 C2 Cr1 P1 -70.8(5) . . . . ? C1 C2 Cr1 P2 102.4(3) . . . . ? C3 C2 Cr1 P2 -140.0(3) . . . . ? C7 C2 Cr1 P2 -18.5(5) . . . . ? C1 C2 Cr1 P4 -148.8(3) . . . . ? C3 C2 Cr1 P4 -31.2(4) . . . . ? C7 C2 Cr1 P4 90.3(5) . . . . ? C1 C2 Cr1 Cr2 122.1(3) . . . . ? C3 C2 Cr1 Cr2 -120.2(3) . . . . ? C7 C2 Cr1 Cr2 1.3(7) . . . . ? C2 C1 Cr1 C3 37.6(3) . . . . ? C5 C1 Cr1 C3 -79.5(4) . . . . ? C6 C1 Cr1 C3 159.9(6) . . . . ? C5 C1 Cr1 C2 -117.0(5) . . . . ? C6 C1 Cr1 C2 122.3(7) . . . . ? C2 C1 Cr1 C4 80.3(4) . . . . ? C5 C1 Cr1 C4 -36.7(3) . . . . ? C6 C1 Cr1 C4 -157.4(6) . . . . ? C2 C1 Cr1 C5 117.0(5) . . . . ? C6 C1 Cr1 C5 -120.7(6) . . . . ? C2 C1 Cr1 P5 166.9(3) . . . . ? C5 C1 Cr1 P5 49.9(4) . . . . ? C6 C1 Cr1 P5 -70.7(5) . . . . ? C2 C1 Cr1 P3 -31.2(4) . . . . ? C5 C1 Cr1 P3 -148.2(3) . . . . ? C6 C1 Cr1 P3 91.1(5) . . . . ? C2 C1 Cr1 P1 -140.1(3) . . . . ? C5 C1 Cr1 P1 102.9(3) . . . . ? C6 C1 Cr1 P1 -17.8(5) . . . . ? C2 C1 Cr1 P2 -83.9(3) . . . . ? C5 C1 Cr1 P2 159.1(3) . . . . ? C6 C1 Cr1 P2 38.4(5) . . . . ? C2 C1 Cr1 P4 84.3(5) . . . . ? C5 C1 Cr1 P4 -32.7(6) . . . . ? C6 C1 Cr1 P4 -153.3(4) . . . . ? C2 C1 Cr1 Cr2 -120.7(3) . . . . ? C5 C1 Cr1 Cr2 122.3(3) . . . . ? C6 C1 Cr1 Cr2 1.7(7) . . . . ? C5 C4 Cr1 C3 117.0(5) . . . . ? C9 C4 Cr1 C3 -120.7(7) . . . . ? C5 C4 Cr1 C2 79.5(4) . . . . ? C3 C4 Cr1 C2 -37.6(3) . . . . ? C9 C4 Cr1 C2 -158.2(6) . . . . ? C5 C4 Cr1 C1 37.2(3) . . . . ? C3 C4 Cr1 C1 -79.8(4) . . . . ? C9 C4 Cr1 C1 159.5(6) . . . . ? C3 C4 Cr1 C5 -117.0(5) . . . . ? C9 C4 Cr1 C5 122.3(6) . . . . ? C5 C4 Cr1 P5 -85.1(3) . . . . ? C3 C4 Cr1 P5 157.9(3) . . . . ? C9 C4 Cr1 P5 37.2(5) . . . . ? C5 C4 Cr1 P3 166.6(3) . . . . ? C3 C4 Cr1 P3 49.5(4) . . . . ? C9 C4 Cr1 P3 -71.2(5) . . . . ? C5 C4 Cr1 P1 -32.6(4) . . . . ? C3 C4 Cr1 P1 -149.6(3) . . . . ? C9 C4 Cr1 P1 89.7(5) . . . . ? C5 C4 Cr1 P2 86.2(6) . . . . ? C3 C4 Cr1 P2 -30.9(7) . . . . ? C9 C4 Cr1 P2 -151.6(4) . . . . ? C5 C4 Cr1 P4 -141.3(3) . . . . ? C3 C4 Cr1 P4 101.7(3) . . . . ? C9 C4 Cr1 P4 -19.0(5) . . . . ? C5 C4 Cr1 Cr2 -122.4(3) . . . . ? C3 C4 Cr1 Cr2 120.6(3) . . . . ? C9 C4 Cr1 Cr2 -0.1(7) . . . . ? C4 C5 Cr1 C3 -38.0(3) . . . . ? C1 C5 Cr1 C3 80.4(4) . . . . ? C10 C5 Cr1 C3 -160.4(6) . . . . ? C4 C5 Cr1 C2 -80.8(4) . . . . ? C1 C5 Cr1 C2 37.6(3) . . . . ? C10 C5 Cr1 C2 156.8(6) . . . . ? C4 C5 Cr1 C1 -118.4(5) . . . . ? C10 C5 Cr1 C1 119.2(7) . . . . ? C1 C5 Cr1 C4 118.4(5) . . . . ? C10 C5 Cr1 C4 -122.4(7) . . . . ? C4 C5 Cr1 P5 101.2(3) . . . . ? C1 C5 Cr1 P5 -140.4(3) . . . . ? C10 C5 Cr1 P5 -21.1(5) . . . . ? C4 C5 Cr1 P3 -32.0(6) . . . . ? C1 C5 Cr1 P3 86.4(5) . . . . ? C10 C5 Cr1 P3 -154.4(4) . . . . ? C4 C5 Cr1 P1 157.7(3) . . . . ? C1 C5 Cr1 P1 -83.9(3) . . . . ? C10 C5 Cr1 P1 35.3(5) . . . . ? C4 C5 Cr1 P2 -149.1(3) . . . . ? C1 C5 Cr1 P2 -30.7(4) . . . . ? C10 C5 Cr1 P2 88.5(5) . . . . ? C4 C5 Cr1 P4 48.1(4) . . . . ? C1 C5 Cr1 P4 166.5(3) . . . . ? C10 C5 Cr1 P4 -74.3(5) . . . . ? C4 C5 Cr1 Cr2 119.5(3) . . . . ? C1 C5 Cr1 Cr2 -122.1(3) . . . . ? C10 C5 Cr1 Cr2 -2.9(7) . . . . ? C3 Cr1 P1 P2 94.5(5) . . . . ? C2 Cr1 P1 P2 72.39(19) . . . . ? C1 Cr1 P1 P2 100.46(17) . . . . ? C4 Cr1 P1 P2 158.0(2) . . . . ? C5 Cr1 P1 P2 138.42(17) . . . . ? P5 Cr1 P1 P2 -132.49(9) . . . . ? P3 Cr1 P1 P2 -38.01(7) . . . . ? P4 Cr1 P1 P2 -94.41(8) . . . . ? Cr2 Cr1 P1 P2 -66.43(6) . . . . ? C3 Cr1 P1 P5 -133.0(5) . . . . ? C2 Cr1 P1 P5 -155.12(19) . . . . ? C1 Cr1 P1 P5 -127.04(17) . . . . ? C4 Cr1 P1 P5 -69.5(2) . . . . ? C5 Cr1 P1 P5 -89.09(17) . . . . ? P3 Cr1 P1 P5 94.48(8) . . . . ? P2 Cr1 P1 P5 132.49(9) . . . . ? P4 Cr1 P1 P5 38.09(7) . . . . ? Cr2 Cr1 P1 P5 66.06(7) . . . . ? C3 Cr1 P1 Cr2 160.9(5) . . . . ? C2 Cr1 P1 Cr2 138.82(18) . . . . ? C1 Cr1 P1 Cr2 166.89(16) . . . . ? C4 Cr1 P1 Cr2 -135.5(2) . . . . ? C5 Cr1 P1 Cr2 -155.15(16) . . . . ? P5 Cr1 P1 Cr2 -66.06(7) . . . . ? P3 Cr1 P1 Cr2 28.42(6) . . . . ? P2 Cr1 P1 Cr2 66.43(6) . . . . ? P4 Cr1 P1 Cr2 -27.97(6) . . . . ? P5 P1 P2 P3 0.33(11) . . . . ? Cr1 P1 P2 P3 43.35(7) . . . . ? Cr2 P1 P2 P3 -43.02(7) . . . . ? P5 P1 P2 Cr1 -43.02(7) . . . . ? Cr2 P1 P2 Cr1 -86.37(6) . . . . ? P5 P1 P2 Cr2 43.35(7) . . . . ? Cr1 P1 P2 Cr2 86.37(6) . . . . ? C3 Cr1 P2 P3 72.2(2) . . . . ? C2 Cr1 P2 P3 100.44(17) . . . . ? C1 Cr1 P2 P3 138.00(17) . . . . ? C4 Cr1 P2 P3 94.4(5) . . . . ? C5 Cr1 P2 P3 156.7(2) . . . . ? P5 Cr1 P2 P3 -94.24(8) . . . . ? P1 Cr1 P2 P3 -132.36(8) . . . . ? P4 Cr1 P2 P3 -37.72(7) . . . . ? Cr2 Cr1 P2 P3 -66.02(6) . . . . ? C3 Cr1 P2 P1 -155.5(2) . . . . ? C2 Cr1 P2 P1 -127.21(17) . . . . ? C1 Cr1 P2 P1 -89.64(17) . . . . ? C4 Cr1 P2 P1 -133.2(5) . . . . ? C5 Cr1 P2 P1 -70.9(2) . . . . ? P5 Cr1 P2 P1 38.11(7) . . . . ? P3 Cr1 P2 P1 132.36(8) . . . . ? P4 Cr1 P2 P1 94.64(8) . . . . ? Cr2 Cr1 P2 P1 66.34(7) . . . . ? C3 Cr1 P2 Cr2 138.2(2) . . . . ? C2 Cr1 P2 Cr2 166.45(16) . . . . ? C1 Cr1 P2 Cr2 -155.98(16) . . . . ? C4 Cr1 P2 Cr2 160.4(5) . . . . ? C5 Cr1 P2 Cr2 -137.3(2) . . . . ? P5 Cr1 P2 Cr2 -28.23(7) . . . . ? P3 Cr1 P2 Cr2 66.02(6) . . . . ? P1 Cr1 P2 Cr2 -66.34(7) . . . . ? P4 Cr1 P2 Cr2 28.30(6) . . . . ? P1 P2 P3 P4 -0.31(11) . . . . ? Cr1 P2 P3 P4 43.08(7) . . . . ? Cr2 P2 P3 P4 -43.47(7) . . . . ? P1 P2 P3 Cr2 43.16(7) . . . . ? Cr1 P2 P3 Cr2 86.55(6) . . . . ? P1 P2 P3 Cr1 -43.38(7) . . . . ? Cr2 P2 P3 Cr1 -86.55(6) . . . . ? C3 Cr1 P3 P2 -127.06(17) . . . . ? C2 Cr1 P3 P2 -89.21(17) . . . . ? C1 Cr1 P3 P2 -70.4(2) . . . . ? C4 Cr1 P3 P2 -155.12(18) . . . . ? C5 Cr1 P3 P2 -132.5(4) . . . . ? P5 Cr1 P3 P2 94.54(8) . . . . ? P1 Cr1 P3 P2 38.01(7) . . . . ? P4 Cr1 P3 P2 132.93(8) . . . . ? Cr2 Cr1 P3 P2 66.53(6) . . . . ? C3 Cr1 P3 P4 100.00(17) . . . . ? C2 Cr1 P3 P4 137.86(17) . . . . ? C1 Cr1 P3 P4 156.7(2) . . . . ? C4 Cr1 P3 P4 71.95(18) . . . . ? C5 Cr1 P3 P4 94.6(5) . . . . ? P5 Cr1 P3 P4 -38.39(7) . . . . ? P1 Cr1 P3 P4 -94.92(8) . . . . ? P2 Cr1 P3 P4 -132.93(8) . . . . ? Cr2 Cr1 P3 P4 -66.40(6) . . . . ? C3 Cr1 P3 Cr2 166.41(17) . . . . ? C2 Cr1 P3 Cr2 -155.74(16) . . . . ? C1 Cr1 P3 Cr2 -136.9(2) . . . . ? C4 Cr1 P3 Cr2 138.35(18) . . . . ? C5 Cr1 P3 Cr2 161.0(4) . . . . ? P5 Cr1 P3 Cr2 28.01(7) . . . . ? P1 Cr1 P3 Cr2 -28.52(7) . . . . ? P2 Cr1 P3 Cr2 -66.53(6) . . . . ? P4 Cr1 P3 Cr2 66.40(6) . . . . ? P2 P3 P4 P5 0.17(11) . . . . ? Cr2 P3 P4 P5 -43.36(7) . . . . ? Cr1 P3 P4 P5 43.27(7) . . . . ? P2 P3 P4 Cr1 -43.11(7) . . . . ? Cr2 P3 P4 Cr1 -86.64(6) . . . . ? P2 P3 P4 Cr2 43.53(7) . . . . ? Cr1 P3 P4 Cr2 86.64(6) . . . . ? C3 Cr1 P4 P5 138.75(18) . . . . ? C2 Cr1 P4 P5 157.7(2) . . . . ? C1 Cr1 P4 P5 97.2(4) . . . . ? C4 Cr1 P4 P5 100.81(16) . . . . ? C5 Cr1 P4 P5 73.8(2) . . . . ? P3 Cr1 P4 P5 -132.04(9) . . . . ? P1 Cr1 P4 P5 -38.12(8) . . . . ? P2 Cr1 P4 P5 -94.40(8) . . . . ? Cr2 Cr1 P4 P5 -66.09(7) . . . . ? C3 Cr1 P4 P3 -89.21(18) . . . . ? C2 Cr1 P4 P3 -70.3(2) . . . . ? C1 Cr1 P4 P3 -130.8(4) . . . . ? C4 Cr1 P4 P3 -127.15(16) . . . . ? C5 Cr1 P4 P3 -154.1(2) . . . . ? P5 Cr1 P4 P3 132.04(9) . . . . ? P1 Cr1 P4 P3 93.92(8) . . . . ? P2 Cr1 P4 P3 37.65(7) . . . . ? Cr2 Cr1 P4 P3 65.96(6) . . . . ? C3 Cr1 P4 Cr2 -155.17(17) . . . . ? C2 Cr1 P4 Cr2 -136.2(2) . . . . ? C1 Cr1 P4 Cr2 163.3(4) . . . . ? C4 Cr1 P4 Cr2 166.90(16) . . . . ? C5 Cr1 P4 Cr2 139.92(19) . . . . ? P5 Cr1 P4 Cr2 66.09(7) . . . . ? P3 Cr1 P4 Cr2 -65.96(6) . . . . ? P1 Cr1 P4 Cr2 27.97(6) . . . . ? P2 Cr1 P4 Cr2 -28.31(6) . . . . ? P3 P4 P5 P1 0.04(11) . . . . ? Cr1 P4 P5 P1 43.45(7) . . . . ? Cr2 P4 P5 P1 -43.27(7) . . . . ? P3 P4 P5 Cr1 -43.41(7) . . . . ? Cr2 P4 P5 Cr1 -86.73(6) . . . . ? P3 P4 P5 Cr2 43.31(7) . . . . ? Cr1 P4 P5 Cr2 86.73(6) . . . . ? P2 P1 P5 P4 -0.23(11) . . . . ? Cr1 P1 P5 P4 -43.48(7) . . . . ? Cr2 P1 P5 P4 43.30(8) . . . . ? P2 P1 P5 Cr1 43.26(7) . . . . ? Cr2 P1 P5 Cr1 86.78(6) . . . . ? P2 P1 P5 Cr2 -43.53(7) . . . . ? Cr1 P1 P5 Cr2 -86.78(6) . . . . ? C3 Cr1 P5 P4 -69.0(2) . . . . ? C2 Cr1 P5 P4 -131.2(5) . . . . ? C1 Cr1 P5 P4 -154.26(19) . . . . ? C4 Cr1 P5 P4 -88.54(17) . . . . ? C5 Cr1 P5 P4 -126.03(17) . . . . ? P3 Cr1 P5 P4 38.33(7) . . . . ? P1 Cr1 P5 P4 132.52(9) . . . . ? P2 Cr1 P5 P4 94.58(8) . . . . ? Cr2 Cr1 P5 P4 66.29(6) . . . . ? C3 Cr1 P5 P1 158.5(2) . . . . ? C2 Cr1 P5 P1 96.3(5) . . . . ? C1 Cr1 P5 P1 73.2(2) . . . . ? C4 Cr1 P5 P1 138.94(17) . . . . ? C5 Cr1 P5 P1 101.45(17) . . . . ? P3 Cr1 P5 P1 -94.19(8) . . . . ? P2 Cr1 P5 P1 -37.95(7) . . . . ? P4 Cr1 P5 P1 -132.52(9) . . . . ? Cr2 Cr1 P5 P1 -66.24(7) . . . . ? C3 Cr1 P5 Cr2 -135.3(2) . . . . ? C2 Cr1 P5 Cr2 162.5(5) . . . . ? C1 Cr1 P5 Cr2 139.45(19) . . . . ? C4 Cr1 P5 Cr2 -154.82(16) . . . . ? C5 Cr1 P5 Cr2 167.69(16) . . . . ? P3 Cr1 P5 Cr2 -27.95(7) . . . . ? P1 Cr1 P5 Cr2 66.24(7) . . . . ? P2 Cr1 P5 Cr2 28.29(7) . . . . ? P4 Cr1 P5 Cr2 -66.29(6) . . . . ? P2 P3 Cr2 C12 87.08(18) . . . . ? P4 P3 Cr2 C12 -140.36(18) . . . . ? Cr1 P3 Cr2 C12 153.39(17) . . . . ? P2 P3 Cr2 C14 154.36(19) . . . . ? P4 P3 Cr2 C14 -73.08(19) . . . . ? Cr1 P3 Cr2 C14 -139.33(19) . . . . ? P2 P3 Cr2 C11 71.1(2) . . . . ? P4 P3 Cr2 C11 -156.3(2) . . . . ? Cr1 P3 Cr2 C11 137.4(2) . . . . ? P2 P3 Cr2 C15 142.2(4) . . . . ? P4 P3 Cr2 C15 -85.2(4) . . . . ? Cr1 P3 Cr2 C15 -151.5(4) . . . . ? P2 P3 Cr2 C13 124.44(16) . . . . ? P4 P3 Cr2 C13 -103.00(16) . . . . ? Cr1 P3 Cr2 C13 -169.25(16) . . . . ? P2 P3 Cr2 P5 -94.23(8) . . . . ? P4 P3 Cr2 P5 38.33(8) . . . . ? Cr1 P3 Cr2 P5 -27.92(7) . . . . ? P2 P3 Cr2 P1 -37.81(8) . . . . ? P4 P3 Cr2 P1 94.75(8) . . . . ? Cr1 P3 Cr2 P1 28.50(7) . . . . ? P2 P3 Cr2 P4 -132.55(8) . . . . ? Cr1 P3 Cr2 P4 -66.24(7) . . . . ? P4 P3 Cr2 P2 132.55(8) . . . . ? Cr1 P3 Cr2 P2 66.31(6) . . . . ? P2 P3 Cr2 Cr1 -66.31(6) . . . . ? P4 P3 Cr2 Cr1 66.24(7) . . . . ? P4 P5 Cr2 C12 138.4(4) . . . . ? P1 P5 Cr2 C12 -88.9(4) . . . . ? Cr1 P5 Cr2 C12 -155.2(4) . . . . ? P4 P5 Cr2 C14 85.97(16) . . . . ? P1 P5 Cr2 C14 -141.34(16) . . . . ? Cr1 P5 Cr2 C14 152.35(16) . . . . ? P4 P5 Cr2 C11 152.32(18) . . . . ? P1 P5 Cr2 C11 -74.98(18) . . . . ? Cr1 P5 Cr2 C11 -141.29(17) . . . . ? P4 P5 Cr2 C15 123.09(16) . . . . ? P1 P5 Cr2 C15 -104.22(16) . . . . ? Cr1 P5 Cr2 C15 -170.53(16) . . . . ? P4 P5 Cr2 C13 70.4(3) . . . . ? P1 P5 Cr2 C13 -156.9(2) . . . . ? Cr1 P5 Cr2 C13 136.7(2) . . . . ? P4 P5 Cr2 P3 -38.36(7) . . . . ? P1 P5 Cr2 P3 94.34(8) . . . . ? Cr1 P5 Cr2 P3 28.03(7) . . . . ? P4 P5 Cr2 P1 -132.69(8) . . . . ? Cr1 P5 Cr2 P1 -66.31(6) . . . . ? P1 P5 Cr2 P4 132.69(8) . . . . ? Cr1 P5 Cr2 P4 66.38(6) . . . . ? P4 P5 Cr2 P2 -94.61(8) . . . . ? P1 P5 Cr2 P2 38.08(7) . . . . ? Cr1 P5 Cr2 P2 -28.23(7) . . . . ? P4 P5 Cr2 Cr1 -66.38(6) . . . . ? P1 P5 Cr2 Cr1 66.31(6) . . . . ? P2 P1 Cr2 C12 -74.96(19) . . . . ? P5 P1 Cr2 C12 152.83(19) . . . . ? Cr1 P1 Cr2 C12 -141.32(18) . . . . ? P2 P1 Cr2 C14 -158.4(2) . . . . ? P5 P1 Cr2 C14 69.4(3) . . . . ? Cr1 P1 Cr2 C14 135.2(2) . . . . ? P2 P1 Cr2 C11 -105.05(16) . . . . ? P5 P1 Cr2 C11 122.73(16) . . . . ? Cr1 P1 Cr2 C11 -171.41(16) . . . . ? P2 P1 Cr2 C15 -142.15(16) . . . . ? P5 P1 Cr2 C15 85.64(16) . . . . ? Cr1 P1 Cr2 C15 151.49(16) . . . . ? P2 P1 Cr2 C13 -89.9(4) . . . . ? P5 P1 Cr2 C13 137.9(4) . . . . ? Cr1 P1 Cr2 C13 -156.2(4) . . . . ? P2 P1 Cr2 P3 37.86(7) . . . . ? P5 P1 Cr2 P3 -94.36(8) . . . . ? Cr1 P1 Cr2 P3 -28.51(7) . . . . ? P2 P1 Cr2 P5 132.22(8) . . . . ? Cr1 P1 Cr2 P5 65.85(6) . . . . ? P2 P1 Cr2 P4 94.31(8) . . . . ? P5 P1 Cr2 P4 -37.90(7) . . . . ? Cr1 P1 Cr2 P4 27.95(6) . . . . ? P5 P1 Cr2 P2 -132.22(8) . . . . ? Cr1 P1 Cr2 P2 -66.36(7) . . . . ? P2 P1 Cr2 Cr1 66.36(7) . . . . ? P5 P1 Cr2 Cr1 -65.85(6) . . . . ? P5 P4 Cr2 C12 -156.3(2) . . . . ? P3 P4 Cr2 C12 71.6(2) . . . . ? Cr1 P4 Cr2 C12 137.8(2) . . . . ? P5 P4 Cr2 C14 -103.70(16) . . . . ? P3 P4 Cr2 C14 124.25(17) . . . . ? Cr1 P4 Cr2 C14 -169.56(16) . . . . ? P5 P4 Cr2 C11 -87.1(4) . . . . ? P3 P4 Cr2 C11 140.8(4) . . . . ? Cr1 P4 Cr2 C11 -153.0(4) . . . . ? P5 P4 Cr2 C15 -73.82(18) . . . . ? P3 P4 Cr2 C15 154.13(18) . . . . ? Cr1 P4 Cr2 C15 -139.68(18) . . . . ? P5 P4 Cr2 C13 -140.42(17) . . . . ? P3 P4 Cr2 C13 87.53(17) . . . . ? Cr1 P4 Cr2 C13 153.72(16) . . . . ? P5 P4 Cr2 P3 132.05(9) . . . . ? Cr1 P4 Cr2 P3 66.19(6) . . . . ? P3 P4 Cr2 P5 -132.05(9) . . . . ? Cr1 P4 Cr2 P5 -65.86(6) . . . . ? P5 P4 Cr2 P1 37.93(7) . . . . ? P3 P4 Cr2 P1 -94.12(8) . . . . ? Cr1 P4 Cr2 P1 -27.94(6) . . . . ? P5 P4 Cr2 P2 94.13(8) . . . . ? P3 P4 Cr2 P2 -37.92(7) . . . . ? Cr1 P4 Cr2 P2 28.26(6) . . . . ? P5 P4 Cr2 Cr1 65.86(6) . . . . ? P3 P4 Cr2 Cr1 -66.19(6) . . . . ? P3 P2 Cr2 C12 -103.99(17) . . . . ? P1 P2 Cr2 C12 123.39(17) . . . . ? Cr1 P2 Cr2 C12 -170.28(16) . . . . ? P3 P2 Cr2 C14 -87.1(4) . . . . ? P1 P2 Cr2 C14 140.3(4) . . . . ? Cr1 P2 Cr2 C14 -153.4(4) . . . . ? P3 P2 Cr2 C11 -141.46(17) . . . . ? P1 P2 Cr2 C11 85.92(17) . . . . ? Cr1 P2 Cr2 C11 152.25(17) . . . . ? P3 P2 Cr2 C15 -158.5(2) . . . . ? P1 P2 Cr2 C15 68.9(2) . . . . ? Cr1 P2 Cr2 C15 135.2(2) . . . . ? P3 P2 Cr2 C13 -74.10(19) . . . . ? P1 P2 Cr2 C13 153.29(19) . . . . ? Cr1 P2 Cr2 C13 -140.38(19) . . . . ? P1 P2 Cr2 P3 -132.62(9) . . . . ? Cr1 P2 Cr2 P3 -66.28(6) . . . . ? P3 P2 Cr2 P5 94.40(8) . . . . ? P1 P2 Cr2 P5 -38.22(7) . . . . ? Cr1 P2 Cr2 P5 28.11(6) . . . . ? P3 P2 Cr2 P1 132.62(9) . . . . ? Cr1 P2 Cr2 P1 66.33(7) . . . . ? P3 P2 Cr2 P4 38.01(7) . . . . ? P1 P2 Cr2 P4 -94.60(8) . . . . ? Cr1 P2 Cr2 P4 -28.27(6) . . . . ? P3 P2 Cr2 Cr1 66.28(6) . . . . ? P1 P2 Cr2 Cr1 -66.33(7) . . . . ? C3 Cr1 Cr2 C12 -78.3(4) . . . . ? C2 Cr1 Cr2 C12 -6.8(4) . . . . ? C1 Cr1 Cr2 C12 65.4(4) . . . . ? C4 Cr1 Cr2 C12 -149.6(4) . . . . ? C5 Cr1 Cr2 C12 139.1(4) . . . . ? P5 Cr1 Cr2 C12 162.1(3) . . . . ? P3 Cr1 Cr2 C12 -53.6(3) . . . . ? P1 Cr1 Cr2 C12 89.9(3) . . . . ? P2 Cr1 Cr2 C12 18.2(3) . . . . ? P4 Cr1 Cr2 C12 -125.7(3) . . . . ? C3 Cr1 Cr2 C14 66.1(4) . . . . ? C2 Cr1 Cr2 C14 137.7(4) . . . . ? C1 Cr1 Cr2 C14 -150.1(4) . . . . ? C4 Cr1 Cr2 C14 -5.1(4) . . . . ? C5 Cr1 Cr2 C14 -76.4(4) . . . . ? P5 Cr1 Cr2 C14 -53.4(3) . . . . ? P3 Cr1 Cr2 C14 90.8(3) . . . . ? P1 Cr1 Cr2 C14 -125.6(3) . . . . ? P2 Cr1 Cr2 C14 162.7(3) . . . . ? P4 Cr1 Cr2 C14 18.8(3) . . . . ? C3 Cr1 Cr2 C11 -152.4(4) . . . . ? C2 Cr1 Cr2 C11 -80.8(4) . . . . ? C1 Cr1 Cr2 C11 -8.6(4) . . . . ? C4 Cr1 Cr2 C11 136.4(4) . . . . ? C5 Cr1 Cr2 C11 65.1(4) . . . . ? P5 Cr1 Cr2 C11 88.1(3) . . . . ? P3 Cr1 Cr2 C11 -127.7(3) . . . . ? P1 Cr1 Cr2 C11 15.9(3) . . . . ? P2 Cr1 Cr2 C11 -55.8(3) . . . . ? P4 Cr1 Cr2 C11 160.3(3) . . . . ? C3 Cr1 Cr2 C15 136.4(4) . . . . ? C2 Cr1 Cr2 C15 -152.0(4) . . . . ? C1 Cr1 Cr2 C15 -79.8(4) . . . . ? C4 Cr1 Cr2 C15 65.2(4) . . . . ? C5 Cr1 Cr2 C15 -6.1(4) . . . . ? P5 Cr1 Cr2 C15 16.9(3) . . . . ? P3 Cr1 Cr2 C15 161.2(3) . . . . ? P1 Cr1 Cr2 C15 -55.3(3) . . . . ? P2 Cr1 Cr2 C15 -127.0(3) . . . . ? P4 Cr1 Cr2 C15 89.1(3) . . . . ? C3 Cr1 Cr2 C13 -4.8(4) . . . . ? C2 Cr1 Cr2 C13 66.8(4) . . . . ? C1 Cr1 Cr2 C13 139.0(4) . . . . ? C4 Cr1 Cr2 C13 -76.0(4) . . . . ? C5 Cr1 Cr2 C13 -147.3(4) . . . . ? P5 Cr1 Cr2 C13 -124.3(3) . . . . ? P3 Cr1 Cr2 C13 19.9(3) . . . . ? P1 Cr1 Cr2 C13 163.5(3) . . . . ? P2 Cr1 Cr2 C13 91.8(3) . . . . ? P4 Cr1 Cr2 C13 -52.1(3) . . . . ? C3 Cr1 Cr2 P3 -24.7(3) . . . . ? C2 Cr1 Cr2 P3 46.8(3) . . . . ? C1 Cr1 Cr2 P3 119.0(3) . . . . ? C4 Cr1 Cr2 P3 -95.9(3) . . . . ? C5 Cr1 Cr2 P3 -167.3(3) . . . . ? P5 Cr1 Cr2 P3 -144.21(9) . . . . ? P1 Cr1 Cr2 P3 143.56(9) . . . . ? P2 Cr1 Cr2 P3 71.85(8) . . . . ? P4 Cr1 Cr2 P3 -72.07(8) . . . . ? C3 Cr1 Cr2 P5 119.5(3) . . . . ? C2 Cr1 Cr2 P5 -168.9(3) . . . . ? C1 Cr1 Cr2 P5 -96.8(3) . . . . ? C4 Cr1 Cr2 P5 48.3(3) . . . . ? C5 Cr1 Cr2 P5 -23.1(3) . . . . ? P3 Cr1 Cr2 P5 144.21(9) . . . . ? P1 Cr1 Cr2 P5 -72.22(8) . . . . ? P2 Cr1 Cr2 P5 -143.94(9) . . . . ? P4 Cr1 Cr2 P5 72.14(8) . . . . ? C3 Cr1 Cr2 P1 -168.3(3) . . . . ? C2 Cr1 Cr2 P1 -96.7(3) . . . . ? C1 Cr1 Cr2 P1 -24.5(3) . . . . ? C4 Cr1 Cr2 P1 120.5(3) . . . . ? C5 Cr1 Cr2 P1 49.2(3) . . . . ? P5 Cr1 Cr2 P1 72.22(8) . . . . ? P3 Cr1 Cr2 P1 -143.56(9) . . . . ? P2 Cr1 Cr2 P1 -71.72(8) . . . . ? P4 Cr1 Cr2 P1 144.37(8) . . . . ? C3 Cr1 Cr2 P4 47.4(3) . . . . ? C2 Cr1 Cr2 P4 118.9(3) . . . . ? C1 Cr1 Cr2 P4 -168.9(3) . . . . ? C4 Cr1 Cr2 P4 -23.9(3) . . . . ? C5 Cr1 Cr2 P4 -95.2(3) . . . . ? P5 Cr1 Cr2 P4 -72.14(8) . . . . ? P3 Cr1 Cr2 P4 72.07(8) . . . . ? P1 Cr1 Cr2 P4 -144.37(8) . . . . ? P2 Cr1 Cr2 P4 143.92(8) . . . . ? C3 Cr1 Cr2 P2 -96.6(3) . . . . ? C2 Cr1 Cr2 P2 -25.0(3) . . . . ? C1 Cr1 Cr2 P2 47.2(3) . . . . ? C4 Cr1 Cr2 P2 -167.8(3) . . . . ? C5 Cr1 Cr2 P2 120.9(3) . . . . ? P5 Cr1 Cr2 P2 143.94(9) . . . . ? P3 Cr1 Cr2 P2 -71.85(8) . . . . ? P1 Cr1 Cr2 P2 71.72(8) . . . . ? P4 Cr1 Cr2 P2 -143.92(8) . . . . ? C12 Cr2 C11 C15 118.1(5) . . . . ? C14 Cr2 C11 C15 37.8(3) . . . . ? C13 Cr2 C11 C15 80.1(4) . . . . ? P3 Cr2 C11 C15 143.8(3) . . . . ? P5 Cr2 C11 C15 -53.0(4) . . . . ? P1 Cr2 C11 C15 -106.4(3) . . . . ? P4 Cr2 C11 C15 19.2(6) . . . . ? P2 Cr2 C11 C15 -162.1(3) . . . . ? Cr1 Cr2 C11 C15 -119.0(3) . . . . ? C14 Cr2 C11 C12 -80.3(4) . . . . ? C15 Cr2 C11 C12 -118.1(5) . . . . ? C13 Cr2 C11 C12 -38.1(3) . . . . ? P3 Cr2 C11 C12 25.6(4) . . . . ? P5 Cr2 C11 C12 -171.2(3) . . . . ? P1 Cr2 C11 C12 135.5(3) . . . . ? P4 Cr2 C11 C12 -99.0(5) . . . . ? P2 Cr2 C11 C12 79.8(3) . . . . ? Cr1 Cr2 C11 C12 122.8(3) . . . . ? C12 Cr2 C11 C16 -119.3(6) . . . . ? C14 Cr2 C11 C16 160.4(6) . . . . ? C15 Cr2 C11 C16 122.6(7) . . . . ? C13 Cr2 C11 C16 -157.3(6) . . . . ? P3 Cr2 C11 C16 -93.6(5) . . . . ? P5 Cr2 C11 C16 69.6(5) . . . . ? P1 Cr2 C11 C16 16.2(5) . . . . ? P4 Cr2 C11 C16 141.8(4) . . . . ? P2 Cr2 C11 C16 -39.5(5) . . . . ? Cr1 Cr2 C11 C16 3.6(7) . . . . ? C15 C11 C12 C13 0.7(6) . . . . ? C16 C11 C12 C13 -176.0(5) . . . . ? Cr2 C11 C12 C13 62.6(4) . . . . ? C15 C11 C12 C17 175.9(5) . . . . ? C16 C11 C12 C17 -0.8(9) . . . . ? Cr2 C11 C12 C17 -122.2(6) . . . . ? C15 C11 C12 Cr2 -61.9(4) . . . . ? C16 C11 C12 Cr2 121.4(5) . . . . ? C14 Cr2 C12 C13 -37.0(3) . . . . ? C11 Cr2 C12 C13 -116.4(5) . . . . ? C15 Cr2 C12 C13 -79.5(4) . . . . ? P3 Cr2 C12 C13 80.1(3) . . . . ? P5 Cr2 C12 C13 -96.6(5) . . . . ? P1 Cr2 C12 C13 -170.7(3) . . . . ? P4 Cr2 C12 C13 25.7(4) . . . . ? P2 Cr2 C12 C13 136.1(3) . . . . ? Cr1 Cr2 C12 C13 121.6(3) . . . . ? C14 Cr2 C12 C11 79.5(3) . . . . ? C15 Cr2 C12 C11 37.0(3) . . . . ? C13 Cr2 C12 C11 116.4(5) . . . . ? P3 Cr2 C12 C11 -163.5(3) . . . . ? P5 Cr2 C12 C11 19.8(6) . . . . ? P1 Cr2 C12 C11 -54.3(4) . . . . ? P4 Cr2 C12 C11 142.2(3) . . . . ? P2 Cr2 C12 C11 -107.5(3) . . . . ? Cr1 Cr2 C12 C11 -122.0(3) . . . . ? C14 Cr2 C12 C17 -158.8(6) . . . . ? C11 Cr2 C12 C17 121.7(7) . . . . ? C15 Cr2 C12 C17 158.7(6) . . . . ? C13 Cr2 C12 C17 -121.9(7) . . . . ? P3 Cr2 C12 C17 -41.8(5) . . . . ? P5 Cr2 C12 C17 141.5(4) . . . . ? P1 Cr2 C12 C17 67.4(5) . . . . ? P4 Cr2 C12 C17 -96.1(5) . . . . ? P2 Cr2 C12 C17 14.2(5) . . . . ? Cr1 Cr2 C12 C17 -0.3(7) . . . . ? C11 C12 C13 C14 -0.8(6) . . . . ? C17 C12 C13 C14 -176.1(5) . . . . ? Cr2 C12 C13 C14 61.6(4) . . . . ? C11 C12 C13 C18 175.0(5) . . . . ? C17 C12 C13 C18 -0.2(9) . . . . ? Cr2 C12 C13 C18 -122.6(5) . . . . ? C11 C12 C13 Cr2 -62.4(4) . . . . ? C17 C12 C13 Cr2 122.4(6) . . . . ? C12 Cr2 C13 C14 -118.1(5) . . . . ? C11 Cr2 C13 C14 -79.9(4) . . . . ? C15 Cr2 C13 C14 -37.5(3) . . . . ? P3 Cr2 C13 C14 135.0(3) . . . . ? P5 Cr2 C13 C14 25.5(4) . . . . ? P1 Cr2 C13 C14 -96.9(5) . . . . ? P4 Cr2 C13 C14 78.8(3) . . . . ? P2 Cr2 C13 C14 -172.0(3) . . . . ? Cr1 Cr2 C13 C14 119.2(3) . . . . ? C14 Cr2 C13 C12 118.1(5) . . . . ? C11 Cr2 C13 C12 38.2(3) . . . . ? C15 Cr2 C13 C12 80.6(4) . . . . ? P3 Cr2 C13 C12 -106.9(3) . . . . ? P5 Cr2 C13 C12 143.5(3) . . . . ? P1 Cr2 C13 C12 21.2(6) . . . . ? P4 Cr2 C13 C12 -163.1(3) . . . . ? P2 Cr2 C13 C12 -54.0(4) . . . . ? Cr1 Cr2 C13 C12 -122.8(3) . . . . ? C12 Cr2 C13 C18 120.5(6) . . . . ? C14 Cr2 C13 C18 -121.4(7) . . . . ? C11 Cr2 C13 C18 158.7(6) . . . . ? C15 Cr2 C13 C18 -158.9(6) . . . . ? P3 Cr2 C13 C18 13.6(5) . . . . ? P5 Cr2 C13 C18 -96.0(5) . . . . ? P1 Cr2 C13 C18 141.7(4) . . . . ? P4 Cr2 C13 C18 -42.6(5) . . . . ? P2 Cr2 C13 C18 66.5(5) . . . . ? Cr1 Cr2 C13 C18 -2.3(7) . . . . ? C12 C13 C14 C15 0.6(6) . . . . ? C18 C13 C14 C15 -175.2(5) . . . . ? Cr2 C13 C14 C15 62.1(4) . . . . ? C12 C13 C14 C19 176.8(5) . . . . ? C18 C13 C14 C19 1.0(9) . . . . ? Cr2 C13 C14 C19 -121.7(5) . . . . ? C12 C13 C14 Cr2 -61.5(4) . . . . ? C18 C13 C14 Cr2 122.7(6) . . . . ? C12 Cr2 C14 C13 37.3(3) . . . . ? C11 Cr2 C14 C13 80.1(4) . . . . ? C15 Cr2 C14 C13 117.7(5) . . . . ? P3 Cr2 C14 C13 -54.7(4) . . . . ? P5 Cr2 C14 C13 -163.1(3) . . . . ? P1 Cr2 C14 C13 144.0(3) . . . . ? P4 Cr2 C14 C13 -107.3(3) . . . . ? P2 Cr2 C14 C13 18.4(6) . . . . ? Cr1 Cr2 C14 C13 -122.2(3) . . . . ? C12 Cr2 C14 C15 -80.4(4) . . . . ? C11 Cr2 C14 C15 -37.6(3) . . . . ? C13 Cr2 C14 C15 -117.7(5) . . . . ? P3 Cr2 C14 C15 -172.5(3) . . . . ? P5 Cr2 C14 C15 79.2(3) . . . . ? P1 Cr2 C14 C15 26.3(4) . . . . ? P4 Cr2 C14 C15 135.0(3) . . . . ? P2 Cr2 C14 C15 -99.3(5) . . . . ? Cr1 Cr2 C14 C15 120.1(3) . . . . ? C12 Cr2 C14 C19 158.7(6) . . . . ? C11 Cr2 C14 C19 -158.5(6) . . . . ? C15 Cr2 C14 C19 -120.9(6) . . . . ? C13 Cr2 C14 C19 121.4(6) . . . . ? P3 Cr2 C14 C19 66.6(5) . . . . ? P5 Cr2 C14 C19 -41.7(5) . . . . ? P1 Cr2 C14 C19 -94.6(5) . . . . ? P4 Cr2 C14 C19 14.1(5) . . . . ? P2 Cr2 C14 C19 139.8(4) . . . . ? Cr1 Cr2 C14 C19 -0.8(7) . . . . ? C12 C11 C15 C14 -0.3(6) . . . . ? C16 C11 C15 C14 176.3(5) . . . . ? Cr2 C11 C15 C14 -61.9(4) . . . . ? C12 C11 C15 C20 -178.0(5) . . . . ? C16 C11 C15 C20 -1.4(9) . . . . ? Cr2 C11 C15 C20 120.4(6) . . . . ? C12 C11 C15 Cr2 61.6(4) . . . . ? C16 C11 C15 Cr2 -121.8(6) . . . . ? C13 C14 C15 C11 -0.2(6) . . . . ? C19 C14 C15 C11 -176.4(5) . . . . ? Cr2 C14 C15 C11 62.0(4) . . . . ? C13 C14 C15 C20 177.5(5) . . . . ? C19 C14 C15 C20 1.3(9) . . . . ? Cr2 C14 C15 C20 -120.3(5) . . . . ? C13 C14 C15 Cr2 -62.2(4) . . . . ? C19 C14 C15 Cr2 121.6(6) . . . . ? C12 Cr2 C15 C11 -37.4(3) . . . . ? C14 Cr2 C15 C11 -117.1(5) . . . . ? C13 Cr2 C15 C11 -79.9(4) . . . . ? P3 Cr2 C15 C11 -99.8(5) . . . . ? P5 Cr2 C15 C11 136.0(3) . . . . ? P1 Cr2 C15 C11 80.2(3) . . . . ? P4 Cr2 C15 C11 -171.2(3) . . . . ? P2 Cr2 C15 C11 27.7(4) . . . . ? Cr1 Cr2 C15 C11 122.6(3) . . . . ? C12 Cr2 C15 C14 79.7(4) . . . . ? C11 Cr2 C15 C14 117.1(5) . . . . ? C13 Cr2 C15 C14 37.1(3) . . . . ? P3 Cr2 C15 C14 17.2(6) . . . . ? P5 Cr2 C15 C14 -107.0(3) . . . . ? P1 Cr2 C15 C14 -162.8(3) . . . . ? P4 Cr2 C15 C14 -54.2(4) . . . . ? P2 Cr2 C15 C14 144.7(3) . . . . ? Cr1 Cr2 C15 C14 -120.3(3) . . . . ? C12 Cr2 C15 C20 -159.5(6) . . . . ? C14 Cr2 C15 C20 120.8(6) . . . . ? C11 Cr2 C15 C20 -122.1(6) . . . . ? C13 Cr2 C15 C20 158.0(6) . . . . ? P3 Cr2 C15 C20 138.0(4) . . . . ? P5 Cr2 C15 C20 13.9(5) . . . . ? P1 Cr2 C15 C20 -42.0(5) . . . . ? P4 Cr2 C15 C20 66.6(5) . . . . ? P2 Cr2 C15 C20 -94.5(5) . . . . ? Cr1 Cr2 C15 C20 0.5(7) . . . . ? C25 C21 C22 C23 0.3(7) . . . . ? C26 C21 C22 C23 176.0(6) . . . . ? Cr3 C21 C22 C23 -61.4(4) . . . . ? C25 C21 C22 C27 -174.6(6) . . . . ? C26 C21 C22 C27 1.1(10) . . . . ? Cr3 C21 C22 C27 123.7(6) . . . . ? C25 C21 C22 Cr3 61.7(4) . . . . ? C26 C21 C22 Cr3 -122.6(6) . . . . ? C21 C22 C23 C24 -0.4(7) . . . . ? C27 C22 C23 C24 174.4(6) . . . . ? Cr3 C22 C23 C24 -62.8(4) . . . . ? C21 C22 C23 C28 -174.6(6) . . . . ? C27 C22 C23 C28 0.3(10) . . . . ? Cr3 C22 C23 C28 123.0(6) . . . . ? C21 C22 C23 Cr3 62.4(4) . . . . ? C27 C22 C23 Cr3 -122.8(6) . . . . ? C22 C23 C24 C25 0.4(7) . . . . ? C28 C23 C24 C25 174.5(6) . . . . ? Cr3 C23 C24 C25 -62.4(4) . . . . ? C22 C23 C24 C29 -175.6(6) . . . . ? C28 C23 C24 C29 -1.6(10) . . . . ? Cr3 C23 C24 C29 121.6(6) . . . . ? C22 C23 C24 Cr3 62.8(4) . . . . ? C28 C23 C24 Cr3 -123.2(6) . . . . ? C23 C24 C25 C21 -0.2(7) . . . . ? C29 C24 C25 C21 175.8(6) . . . . ? Cr3 C24 C25 C21 -61.9(4) . . . . ? C23 C24 C25 C30 -177.1(6) . . . . ? C29 C24 C25 C30 -1.1(10) . . . . ? Cr3 C24 C25 C30 121.2(6) . . . . ? C23 C24 C25 Cr3 61.6(4) . . . . ? C29 C24 C25 Cr3 -122.4(6) . . . . ? C22 C21 C25 C24 -0.1(7) . . . . ? C26 C21 C25 C24 -175.9(6) . . . . ? Cr3 C21 C25 C24 61.5(4) . . . . ? C22 C21 C25 C30 176.9(5) . . . . ? C26 C21 C25 C30 1.1(10) . . . . ? Cr3 C21 C25 C30 -121.6(6) . . . . ? C22 C21 C25 Cr3 -61.5(4) . . . . ? C26 C21 C25 Cr3 122.7(6) . . . . ? C22 C23 Cr3 C24 -117.9(5) . . . . ? C28 C23 Cr3 C24 121.9(7) . . . . ? C24 C23 Cr3 C22 117.9(5) . . . . ? C28 C23 Cr3 C22 -120.2(7) . . . . ? C24 C23 Cr3 C25 37.9(3) . . . . ? C22 C23 Cr3 C25 -80.0(4) . . . . ? C28 C23 Cr3 C25 159.7(6) . . . . ? C24 C23 Cr3 C21 80.4(4) . . . . ? C22 C23 Cr3 C21 -37.5(3) . . . . ? C28 C23 Cr3 C21 -157.7(6) . . . . ? C24 C23 Cr3 P10 -16.9(5) . . . . ? C22 C23 Cr3 P10 -134.8(3) . . . . ? C28 C23 Cr3 P10 105.0(5) . . . . ? C24 C23 Cr3 P6 121.5(4) . . . . ? C22 C23 Cr3 P6 3.5(6) . . . . ? C28 C23 Cr3 P6 -116.7(5) . . . . ? C24 C23 Cr3 P8 -125.3(3) . . . . ? C22 C23 Cr3 P8 116.8(3) . . . . ? C28 C23 Cr3 P8 -3.4(5) . . . . ? C24 C23 Cr3 P9 -71.7(3) . . . . ? C22 C23 Cr3 P9 170.4(3) . . . . ? C28 C23 Cr3 P9 50.2(6) . . . . ? C24 C23 Cr3 P7 -176.8(3) . . . . ? C22 C23 Cr3 P7 65.3(4) . . . . ? C28 C23 Cr3 P7 -54.9(6) . . . . ? C25 C24 Cr3 C23 116.8(5) . . . . ? C29 C24 Cr3 C23 -120.7(7) . . . . ? C23 C24 Cr3 C22 -37.3(3) . . . . ? C25 C24 Cr3 C22 79.5(4) . . . . ? C29 C24 Cr3 C22 -158.1(6) . . . . ? C23 C24 Cr3 C25 -116.8(5) . . . . ? C29 C24 Cr3 C25 122.5(7) . . . . ? C23 C24 Cr3 C21 -79.7(4) . . . . ? C25 C24 Cr3 C21 37.1(3) . . . . ? C29 C24 Cr3 C21 159.6(6) . . . . ? C23 C24 Cr3 P10 170.3(3) . . . . ? C25 C24 Cr3 P10 -72.8(3) . . . . ? C29 C24 Cr3 P10 49.6(5) . . . . ? C23 C24 Cr3 P6 -136.2(3) . . . . ? C25 C24 Cr3 P6 -19.3(5) . . . . ? C29 C24 Cr3 P6 103.1(5) . . . . ? C23 C24 Cr3 P8 64.2(4) . . . . ? C25 C24 Cr3 P8 -178.9(3) . . . . ? C29 C24 Cr3 P8 -56.5(5) . . . . ? C23 C24 Cr3 P9 116.5(3) . . . . ? C25 C24 Cr3 P9 -126.6(3) . . . . ? C29 C24 Cr3 P9 -4.2(5) . . . . ? C23 C24 Cr3 P7 6.8(6) . . . . ? C25 C24 Cr3 P7 123.6(4) . . . . ? C29 C24 Cr3 P7 -113.9(5) . . . . ? C21 C22 Cr3 C23 -117.4(5) . . . . ? C27 C22 Cr3 C23 120.7(6) . . . . ? C23 C22 Cr3 C24 37.2(3) . . . . ? C21 C22 Cr3 C24 -80.2(4) . . . . ? C27 C22 Cr3 C24 157.9(6) . . . . ? C23 C22 Cr3 C25 79.7(4) . . . . ? C21 C22 Cr3 C25 -37.7(3) . . . . ? C27 C22 Cr3 C25 -159.6(6) . . . . ? C23 C22 Cr3 C21 117.4(5) . . . . ? C27 C22 Cr3 C21 -121.9(7) . . . . ? C23 C22 Cr3 P10 119.1(4) . . . . ? C21 C22 Cr3 P10 1.7(6) . . . . ? C27 C22 Cr3 P10 -120.2(5) . . . . ? C23 C22 Cr3 P6 -178.3(3) . . . . ? C21 C22 Cr3 P6 64.3(4) . . . . ? C27 C22 Cr3 P6 -57.6(5) . . . . ? C23 C22 Cr3 P8 -71.8(3) . . . . ? C21 C22 Cr3 P8 170.9(3) . . . . ? C27 C22 Cr3 P8 49.0(5) . . . . ? C23 C22 Cr3 P9 -16.8(5) . . . . ? C21 C22 Cr3 P9 -134.2(3) . . . . ? C27 C22 Cr3 P9 103.9(5) . . . . ? C23 C22 Cr3 P7 -125.5(3) . . . . ? C21 C22 Cr3 P7 117.2(3) . . . . ? C27 C22 Cr3 P7 -4.7(5) . . . . ? C24 C25 Cr3 C23 -37.8(3) . . . . ? C21 C25 Cr3 C23 80.4(4) . . . . ? C30 C25 Cr3 C23 -158.8(6) . . . . ? C21 C25 Cr3 C24 118.1(5) . . . . ? C30 C25 Cr3 C24 -121.0(7) . . . . ? C24 C25 Cr3 C22 -80.5(4) . . . . ? C21 C25 Cr3 C22 37.6(3) . . . . ? C30 C25 Cr3 C22 158.5(6) . . . . ? C24 C25 Cr3 C21 -118.1(5) . . . . ? C30 C25 Cr3 C21 120.9(7) . . . . ? C24 C25 Cr3 P10 115.8(3) . . . . ? C21 C25 Cr3 P10 -126.1(3) . . . . ? C30 C25 Cr3 P10 -5.2(5) . . . . ? C24 C25 Cr3 P6 169.2(3) . . . . ? C21 C25 Cr3 P6 -72.6(3) . . . . ? C30 C25 Cr3 P6 48.3(5) . . . . ? C24 C25 Cr3 P8 2.1(6) . . . . ? C21 C25 Cr3 P8 120.3(4) . . . . ? C30 C25 Cr3 P8 -118.9(5) . . . . ? C24 C25 Cr3 P9 62.7(4) . . . . ? C21 C25 Cr3 P9 -179.1(3) . . . . ? C30 C25 Cr3 P9 -58.3(5) . . . . ? C24 C25 Cr3 P7 -136.1(3) . . . . ? C21 C25 Cr3 P7 -18.0(5) . . . . ? C30 C25 Cr3 P7 102.9(5) . . . . ? C22 C21 Cr3 C23 37.6(3) . . . . ? C25 C21 Cr3 C23 -79.5(4) . . . . ? C26 C21 Cr3 C23 160.3(6) . . . . ? C22 C21 Cr3 C24 80.0(4) . . . . ? C25 C21 Cr3 C24 -37.2(3) . . . . ? C26 C21 Cr3 C24 -157.3(6) . . . . ? C25 C21 Cr3 C22 -117.2(5) . . . . ? C26 C21 Cr3 C22 122.7(7) . . . . ? C22 C21 Cr3 C25 117.2(5) . . . . ? C26 C21 Cr3 C25 -120.1(6) . . . . ? C22 C21 Cr3 P10 -179.2(3) . . . . ? C25 C21 Cr3 P10 63.7(4) . . . . ? C26 C21 Cr3 P10 -56.5(5) . . . . ? C22 C21 Cr3 P6 -126.0(3) . . . . ? C25 C21 Cr3 P6 116.8(3) . . . . ? C26 C21 Cr3 P6 -3.3(5) . . . . ? C22 C21 Cr3 P8 -16.1(5) . . . . ? C25 C21 Cr3 P8 -133.3(3) . . . . ? C26 C21 Cr3 P8 106.6(5) . . . . ? C22 C21 Cr3 P9 118.9(4) . . . . ? C25 C21 Cr3 P9 1.7(6) . . . . ? C26 C21 Cr3 P9 -118.4(5) . . . . ? C22 C21 Cr3 P7 -72.6(3) . . . . ? C25 C21 Cr3 P7 170.2(3) . . . . ? C26 C21 Cr3 P7 50.0(5) . . . . ? C23 Cr3 P6 P10 -153.5(4) . . . . ? C24 Cr3 P6 P10 -68.8(3) . . . . ? C22 Cr3 P6 P10 -151.10(18) . . . . ? C25 Cr3 P6 P10 -81.37(18) . . . . ? C21 Cr3 P6 P10 -117.38(16) . . . . ? P8 Cr3 P6 P10 92.86(7) . . . . ? P9 Cr3 P6 P10 38.83(7) . . . . ? P7 Cr3 P6 P10 129.80(8) . . . . ? C23 Cr3 P6 P7 76.7(4) . . . . ? C24 Cr3 P6 P7 161.4(3) . . . . ? C22 Cr3 P6 P7 79.11(18) . . . . ? C25 Cr3 P6 P7 148.83(18) . . . . ? C21 Cr3 P6 P7 112.82(16) . . . . ? P10 Cr3 P6 P7 -129.80(8) . . . . ? P8 Cr3 P6 P7 -36.94(7) . . . . ? P9 Cr3 P6 P7 -90.97(7) . . . . ? C23 Cr3 P6 Cr4 141.5(4) . . . . ? C24 Cr3 P6 Cr4 -133.7(3) . . . . ? C22 Cr3 P6 Cr4 143.96(18) . . . . ? C25 Cr3 P6 Cr4 -146.32(17) . . . . ? C21 Cr3 P6 Cr4 177.67(16) . . . . ? P10 Cr3 P6 Cr4 -64.95(6) . . . . ? P8 Cr3 P6 Cr4 27.91(6) . . . . ? P9 Cr3 P6 Cr4 -26.11(6) . . . . ? P7 Cr3 P6 Cr4 64.85(6) . . . . ? P10 P6 P7 P8 -1.66(11) . . . . ? Cr3 P6 P7 P8 44.33(7) . . . . ? Cr4 P6 P7 P8 -46.79(7) . . . . ? P10 P6 P7 Cr4 45.13(7) . . . . ? Cr3 P6 P7 Cr4 91.12(6) . . . . ? P10 P6 P7 Cr3 -45.99(7) . . . . ? Cr4 P6 P7 Cr3 -91.12(6) . . . . ? C23 Cr3 P7 P8 76.03(19) . . . . ? C24 Cr3 P7 P8 71.4(4) . . . . ? C22 Cr3 P7 P8 110.22(16) . . . . ? C25 Cr3 P7 P8 158.1(3) . . . . ? C21 Cr3 P7 P8 146.28(18) . . . . ? P10 Cr3 P7 P8 -93.22(7) . . . . ? P6 Cr3 P7 P8 -131.68(8) . . . . ? P9 Cr3 P7 P8 -38.84(7) . . . . ? C23 Cr3 P7 P6 -152.29(19) . . . . ? C24 Cr3 P7 P6 -156.9(4) . . . . ? C22 Cr3 P7 P6 -118.10(16) . . . . ? C25 Cr3 P7 P6 -70.3(3) . . . . ? C21 Cr3 P7 P6 -82.04(18) . . . . ? P10 Cr3 P7 P6 38.46(7) . . . . ? P8 Cr3 P7 P6 131.68(8) . . . . ? P9 Cr3 P7 P6 92.84(7) . . . . ? C23 Cr3 P7 Cr4 142.03(18) . . . . ? C24 Cr3 P7 Cr4 137.4(4) . . . . ? C22 Cr3 P7 Cr4 176.23(16) . . . . ? C25 Cr3 P7 Cr4 -135.9(3) . . . . ? C21 Cr3 P7 Cr4 -147.72(17) . . . . ? P10 Cr3 P7 Cr4 -27.22(6) . . . . ? P6 Cr3 P7 Cr4 -65.68(6) . . . . ? P8 Cr3 P7 Cr4 66.00(6) . . . . ? P9 Cr3 P7 Cr4 27.16(6) . . . . ? P6 P7 P8 P9 2.32(11) . . . . ? Cr4 P7 P8 P9 -44.32(7) . . . . ? Cr3 P7 P8 P9 46.59(7) . . . . ? P6 P7 P8 Cr3 -44.27(7) . . . . ? Cr4 P7 P8 Cr3 -90.91(6) . . . . ? P6 P7 P8 Cr4 46.64(7) . . . . ? Cr3 P7 P8 Cr4 90.91(6) . . . . ? C23 Cr3 P8 P7 -119.96(17) . . . . ? C24 Cr3 P8 P7 -153.50(18) . . . . ? C22 Cr3 P8 P7 -84.14(18) . . . . ? C25 Cr3 P8 P7 -154.9(4) . . . . ? C21 Cr3 P8 P7 -73.7(3) . . . . ? P10 Cr3 P8 P7 91.09(7) . . . . ? P6 Cr3 P8 P7 37.03(7) . . . . ? P9 Cr3 P8 P7 129.18(8) . . . . ? C23 Cr3 P8 P9 110.86(17) . . . . ? C24 Cr3 P8 P9 77.32(18) . . . . ? C22 Cr3 P8 P9 146.68(17) . . . . ? C25 Cr3 P8 P9 75.9(4) . . . . ? C21 Cr3 P8 P9 157.1(3) . . . . ? P10 Cr3 P8 P9 -38.09(7) . . . . ? P6 Cr3 P8 P9 -92.15(7) . . . . ? P7 Cr3 P8 P9 -129.18(8) . . . . ? C23 Cr3 P8 Cr4 175.17(17) . . . . ? C24 Cr3 P8 Cr4 141.63(18) . . . . ? C22 Cr3 P8 Cr4 -149.01(17) . . . . ? C25 Cr3 P8 Cr4 140.2(4) . . . . ? C21 Cr3 P8 Cr4 -138.5(3) . . . . ? P10 Cr3 P8 Cr4 26.22(6) . . . . ? P6 Cr3 P8 Cr4 -27.84(6) . . . . ? P9 Cr3 P8 Cr4 64.31(6) . . . . ? P7 Cr3 P8 Cr4 -64.87(6) . . . . ? P7 P8 P9 P10 -2.10(11) . . . . ? Cr3 P8 P9 P10 44.94(7) . . . . ? Cr4 P8 P9 P10 -46.66(7) . . . . ? P7 P8 P9 Cr4 44.57(7) . . . . ? Cr3 P8 P9 Cr4 91.60(6) . . . . ? P7 P8 P9 Cr3 -47.04(7) . . . . ? Cr4 P8 P9 Cr3 -91.60(6) . . . . ? C23 Cr3 P9 P8 -82.26(18) . . . . ? C24 Cr3 P9 P8 -117.86(16) . . . . ? C22 Cr3 P9 P8 -71.4(3) . . . . ? C25 Cr3 P9 P8 -150.96(18) . . . . ? C21 Cr3 P9 P8 -152.1(4) . . . . ? P10 Cr3 P9 P8 130.78(8) . . . . ? P6 Cr3 P9 P8 92.18(7) . . . . ? P7 Cr3 P9 P8 38.54(7) . . . . ? C23 Cr3 P9 P10 146.96(18) . . . . ? C24 Cr3 P9 P10 111.35(16) . . . . ? C22 Cr3 P9 P10 157.8(3) . . . . ? C25 Cr3 P9 P10 78.25(18) . . . . ? C21 Cr3 P9 P10 77.1(4) . . . . ? P6 Cr3 P9 P10 -38.60(7) . . . . ? P8 Cr3 P9 P10 -130.78(8) . . . . ? P7 Cr3 P9 P10 -92.24(7) . . . . ? C23 Cr3 P9 Cr4 -148.05(18) . . . . ? C24 Cr3 P9 Cr4 176.35(16) . . . . ? C22 Cr3 P9 Cr4 -137.2(3) . . . . ? C25 Cr3 P9 Cr4 143.25(18) . . . . ? C21 Cr3 P9 Cr4 142.1(4) . . . . ? P10 Cr3 P9 Cr4 64.99(6) . . . . ? P6 Cr3 P9 Cr4 26.39(6) . . . . ? P8 Cr3 P9 Cr4 -65.79(6) . . . . ? P7 Cr3 P9 Cr4 -27.25(6) . . . . ? P7 P6 P10 P9 0.35(11) . . . . ? Cr3 P6 P10 P9 -46.20(7) . . . . ? Cr4 P6 P10 P9 45.43(7) . . . . ? P7 P6 P10 Cr3 46.55(7) . . . . ? Cr4 P6 P10 Cr3 91.62(6) . . . . ? P7 P6 P10 Cr4 -45.08(7) . . . . ? Cr3 P6 P10 Cr4 -91.62(6) . . . . ? P8 P9 P10 P6 1.08(11) . . . . ? Cr4 P9 P10 P6 -45.95(7) . . . . ? Cr3 P9 P10 P6 46.26(7) . . . . ? P8 P9 P10 Cr3 -45.18(7) . . . . ? Cr4 P9 P10 Cr3 -92.21(6) . . . . ? P8 P9 P10 Cr4 47.03(7) . . . . ? Cr3 P9 P10 Cr4 92.21(6) . . . . ? C23 Cr3 P10 P6 159.6(3) . . . . ? C24 Cr3 P10 P6 148.66(18) . . . . ? C22 Cr3 P10 P6 78.1(4) . . . . ? C25 Cr3 P10 P6 112.66(17) . . . . ? C21 Cr3 P10 P6 79.23(19) . . . . ? P8 Cr3 P10 P6 -91.77(7) . . . . ? P9 Cr3 P10 P6 -129.62(8) . . . . ? P7 Cr3 P10 P6 -38.25(7) . . . . ? C23 Cr3 P10 P9 -70.8(3) . . . . ? C24 Cr3 P10 P9 -81.72(18) . . . . ? C22 Cr3 P10 P9 -152.3(4) . . . . ? C25 Cr3 P10 P9 -117.72(17) . . . . ? C21 Cr3 P10 P9 -151.15(18) . . . . ? P6 Cr3 P10 P9 129.62(8) . . . . ? P8 Cr3 P10 P9 37.86(7) . . . . ? P7 Cr3 P10 P9 91.37(7) . . . . ? C23 Cr3 P10 Cr4 -135.1(3) . . . . ? C24 Cr3 P10 Cr4 -145.97(17) . . . . ? C22 Cr3 P10 Cr4 143.4(4) . . . . ? C25 Cr3 P10 Cr4 178.04(17) . . . . ? C21 Cr3 P10 Cr4 144.61(18) . . . . ? P6 Cr3 P10 Cr4 65.38(6) . . . . ? P8 Cr3 P10 Cr4 -26.39(6) . . . . ? P9 Cr3 P10 Cr4 -64.25(6) . . . . ? P7 Cr3 P10 Cr4 27.12(6) . . . . ? P8 P9 Cr4 C31 162.4(2) . . . . ? P10 P9 Cr4 C31 -68.4(3) . . . . ? Cr3 P9 Cr4 C31 -132.7(2) . . . . ? P8 P9 Cr4 C32 90.4(5) . . . . ? P10 P9 Cr4 C32 -140.4(5) . . . . ? Cr3 P9 Cr4 C32 155.3(5) . . . . ? P8 P9 Cr4 C35 143.57(17) . . . . ? P10 P9 Cr4 C35 -87.26(17) . . . . ? Cr3 P9 Cr4 C35 -151.58(16) . . . . ? P8 P9 Cr4 C34 105.67(17) . . . . ? P10 P9 Cr4 C34 -125.16(17) . . . . ? Cr3 P9 Cr4 C34 170.53(16) . . . . ? P8 P9 Cr4 C33 75.8(2) . . . . ? P10 P9 Cr4 C33 -155.0(2) . . . . ? Cr3 P9 Cr4 C33 140.68(19) . . . . ? P8 P9 Cr4 P7 -37.23(7) . . . . ? P10 P9 Cr4 P7 91.94(7) . . . . ? Cr3 P9 Cr4 P7 27.63(6) . . . . ? P8 P9 Cr4 P10 -129.17(8) . . . . ? Cr3 P9 Cr4 P10 -64.31(6) . . . . ? P8 P9 Cr4 P6 -91.08(7) . . . . ? P10 P9 Cr4 P6 38.10(7) . . . . ? Cr3 P9 Cr4 P6 -26.22(6) . . . . ? P10 P9 Cr4 P8 129.17(8) . . . . ? Cr3 P9 Cr4 P8 64.86(6) . . . . ? P8 P7 Cr4 C31 -157.59(19) . . . . ? P6 P7 Cr4 C31 72.91(19) . . . . ? Cr3 P7 Cr4 C31 137.59(19) . . . . ? P8 P7 Cr4 C32 -126.87(16) . . . . ? P6 P7 Cr4 C32 103.63(16) . . . . ? Cr3 P7 Cr4 C32 168.31(16) . . . . ? P8 P7 Cr4 C35 -144.8(5) . . . . ? P6 P7 Cr4 C35 85.7(5) . . . . ? Cr3 P7 Cr4 C35 150.4(5) . . . . ? P8 P7 Cr4 C34 -70.7(3) . . . . ? P6 P7 Cr4 C34 159.8(3) . . . . ? Cr3 P7 Cr4 C34 -135.5(3) . . . . ? P8 P7 Cr4 C33 -89.18(17) . . . . ? P6 P7 Cr4 C33 141.32(17) . . . . ? Cr3 P7 Cr4 C33 -154.00(16) . . . . ? P8 P7 Cr4 P9 37.43(7) . . . . ? P6 P7 Cr4 P9 -92.07(7) . . . . ? Cr3 P7 Cr4 P9 -27.39(6) . . . . ? P8 P7 Cr4 P10 91.90(7) . . . . ? P6 P7 Cr4 P10 -37.60(7) . . . . ? Cr3 P7 Cr4 P10 27.08(6) . . . . ? P8 P7 Cr4 P6 129.50(8) . . . . ? Cr3 P7 Cr4 P6 64.67(6) . . . . ? P6 P7 Cr4 P8 -129.50(8) . . . . ? Cr3 P7 Cr4 P8 -64.82(6) . . . . ? P6 P10 Cr4 C31 -88.19(17) . . . . ? P9 P10 Cr4 C31 141.70(17) . . . . ? Cr3 P10 Cr4 C31 -153.33(17) . . . . ? P6 P10 Cr4 C32 -69.3(2) . . . . ? P9 P10 Cr4 C32 160.6(2) . . . . ? Cr3 P10 Cr4 C32 -134.5(2) . . . . ? P6 P10 Cr4 C35 -125.53(17) . . . . ? P9 P10 Cr4 C35 104.37(17) . . . . ? Cr3 P10 Cr4 C35 169.34(16) . . . . ? P6 P10 Cr4 C34 -155.3(2) . . . . ? P9 P10 Cr4 C34 74.6(2) . . . . ? Cr3 P10 Cr4 C34 139.60(19) . . . . ? P6 P10 Cr4 C33 -139.4(4) . . . . ? P9 P10 Cr4 C33 90.5(5) . . . . ? Cr3 P10 Cr4 C33 155.5(4) . . . . ? P6 P10 Cr4 P9 130.10(8) . . . . ? Cr3 P10 Cr4 P9 64.97(6) . . . . ? P6 P10 Cr4 P7 37.67(7) . . . . ? P9 P10 Cr4 P7 -92.44(7) . . . . ? Cr3 P10 Cr4 P7 -27.47(6) . . . . ? P9 P10 Cr4 P6 -130.10(8) . . . . ? Cr3 P10 Cr4 P6 -65.14(6) . . . . ? P6 P10 Cr4 P8 91.26(7) . . . . ? P9 P10 Cr4 P8 -38.84(7) . . . . ? Cr3 P10 Cr4 P8 26.12(6) . . . . ? P10 P6 Cr4 C31 102.92(17) . . . . ? P7 P6 Cr4 C31 -126.23(17) . . . . ? Cr3 P6 Cr4 C31 167.74(16) . . . . ? P10 P6 Cr4 C32 140.94(17) . . . . ? P7 P6 Cr4 C32 -88.21(17) . . . . ? Cr3 P6 Cr4 C32 -154.23(17) . . . . ? P10 P6 Cr4 C35 73.1(2) . . . . ? P7 P6 Cr4 C35 -156.1(2) . . . . ? Cr3 P6 Cr4 C35 137.90(19) . . . . ? P10 P6 Cr4 C34 87.3(5) . . . . ? P7 P6 Cr4 C34 -141.9(5) . . . . ? Cr3 P6 Cr4 C34 152.1(5) . . . . ? P10 P6 Cr4 C33 158.8(3) . . . . ? P7 P6 Cr4 C33 -70.3(3) . . . . ? Cr3 P6 Cr4 C33 -136.4(2) . . . . ? P10 P6 Cr4 P9 -38.53(7) . . . . ? P7 P6 Cr4 P9 92.32(7) . . . . ? Cr3 P6 Cr4 P9 26.30(6) . . . . ? P10 P6 Cr4 P7 -130.85(8) . . . . ? Cr3 P6 Cr4 P7 -66.02(6) . . . . ? P7 P6 Cr4 P10 130.85(8) . . . . ? Cr3 P6 Cr4 P10 64.83(6) . . . . ? P10 P6 Cr4 P8 -92.46(7) . . . . ? P7 P6 Cr4 P8 38.39(7) . . . . ? Cr3 P6 Cr4 P8 -27.63(6) . . . . ? P7 P8 Cr4 C31 86.2(5) . . . . ? P9 P8 Cr4 C31 -142.5(5) . . . . ? Cr3 P8 Cr4 C31 152.3(5) . . . . ? P7 P8 Cr4 C32 72.75(19) . . . . ? P9 P8 Cr4 C32 -155.92(19) . . . . ? Cr3 P8 Cr4 C32 138.90(18) . . . . ? P7 P8 Cr4 C35 161.4(3) . . . . ? P9 P8 Cr4 C35 -67.3(3) . . . . ? Cr3 P8 Cr4 C35 -132.5(3) . . . . ? P7 P8 Cr4 C34 141.58(18) . . . . ? P9 P8 Cr4 C34 -87.10(18) . . . . ? Cr3 P8 Cr4 C34 -152.28(17) . . . . ? P7 P8 Cr4 C33 103.87(17) . . . . ? P9 P8 Cr4 C33 -124.80(17) . . . . ? Cr3 P8 Cr4 C33 170.02(17) . . . . ? P7 P8 Cr4 P9 -131.33(8) . . . . ? Cr3 P8 Cr4 P9 -65.18(6) . . . . ? P9 P8 Cr4 P7 131.33(8) . . . . ? Cr3 P8 Cr4 P7 66.15(6) . . . . ? P7 P8 Cr4 P10 -92.19(7) . . . . ? P9 P8 Cr4 P10 39.14(7) . . . . ? Cr3 P8 Cr4 P10 -26.05(6) . . . . ? P7 P8 Cr4 P6 -38.52(7) . . . . ? P9 P8 Cr4 P6 92.81(7) . . . . ? Cr3 P8 Cr4 P6 27.63(6) . . . . ? C32 Cr4 C31 C35 117.7(5) . . . . ? C34 Cr4 C31 C35 37.6(3) . . . . ? C33 Cr4 C31 C35 79.9(4) . . . . ? P9 Cr4 C31 C35 -30.8(4) . . . . ? P7 Cr4 C31 C35 172.8(3) . . . . ? P10 Cr4 C31 C35 -82.1(3) . . . . ? P6 Cr4 C31 C35 -136.3(3) . . . . ? P8 Cr4 C31 C35 99.6(6) . . . . ? C35 Cr4 C31 C32 -117.7(5) . . . . ? C34 Cr4 C31 C32 -80.1(4) . . . . ? C33 Cr4 C31 C32 -37.8(3) . . . . ? P9 Cr4 C31 C32 -148.6(3) . . . . ? P7 Cr4 C31 C32 55.1(4) . . . . ? P10 Cr4 C31 C32 160.1(3) . . . . ? P6 Cr4 C31 C32 106.0(3) . . . . ? P8 Cr4 C31 C32 -18.2(7) . . . . ? C32 Cr4 C31 C36 -121.0(6) . . . . ? C35 Cr4 C31 C36 121.2(6) . . . . ? C34 Cr4 C31 C36 158.8(6) . . . . ? C33 Cr4 C31 C36 -158.9(6) . . . . ? P9 Cr4 C31 C36 90.4(5) . . . . ? P7 Cr4 C31 C36 -66.0(5) . . . . ? P10 Cr4 C31 C36 39.1(5) . . . . ? P6 Cr4 C31 C36 -15.1(5) . . . . ? P8 Cr4 C31 C36 -139.2(4) . . . . ? C35 C31 C32 C33 0.0(7) . . . . ? C36 C31 C32 C33 -178.1(5) . . . . ? Cr4 C31 C32 C33 62.5(4) . . . . ? C35 C31 C32 C37 177.7(5) . . . . ? C36 C31 C32 C37 -0.4(9) . . . . ? Cr4 C31 C32 C37 -119.9(6) . . . . ? C35 C31 C32 Cr4 -62.5(4) . . . . ? C36 C31 C32 Cr4 119.4(6) . . . . ? C31 Cr4 C32 C33 -116.8(5) . . . . ? C35 Cr4 C32 C33 -79.7(4) . . . . ? C34 Cr4 C32 C33 -37.1(3) . . . . ? P9 Cr4 C32 C33 -20.1(7) . . . . ? P7 Cr4 C32 C33 107.1(3) . . . . ? P10 Cr4 C32 C33 -147.2(3) . . . . ? P6 Cr4 C32 C33 161.4(3) . . . . ? P8 Cr4 C32 C33 56.3(4) . . . . ? C35 Cr4 C32 C31 37.0(3) . . . . ? C34 Cr4 C32 C31 79.7(4) . . . . ? C33 Cr4 C32 C31 116.8(5) . . . . ? P9 Cr4 C32 C31 96.6(5) . . . . ? P7 Cr4 C32 C31 -136.2(3) . . . . ? P10 Cr4 C32 C31 -30.4(4) . . . . ? P6 Cr4 C32 C31 -81.8(3) . . . . ? P8 Cr4 C32 C31 173.1(3) . . . . ? C31 Cr4 C32 C37 121.4(6) . . . . ? C35 Cr4 C32 C37 158.5(6) . . . . ? C34 Cr4 C32 C37 -158.9(6) . . . . ? C33 Cr4 C32 C37 -121.8(7) . . . . ? P9 Cr4 C32 C37 -141.9(4) . . . . ? P7 Cr4 C32 C37 -14.7(5) . . . . ? P10 Cr4 C32 C37 91.0(5) . . . . ? P6 Cr4 C32 C37 39.6(5) . . . . ? P8 Cr4 C32 C37 -65.5(5) . . . . ? C31 C32 C33 C34 -0.3(7) . . . . ? C37 C32 C33 C34 -177.9(5) . . . . ? Cr4 C32 C33 C34 61.7(4) . . . . ? C31 C32 C33 C38 177.3(6) . . . . ? C37 C32 C33 C38 -0.3(10) . . . . ? Cr4 C32 C33 C38 -120.7(6) . . . . ? C31 C32 C33 Cr4 -62.0(4) . . . . ? C37 C32 C33 Cr4 120.4(6) . . . . ? C31 Cr4 C33 C34 -79.8(4) . . . . ? C32 Cr4 C33 C34 -117.9(5) . . . . ? C35 Cr4 C33 C34 -37.6(3) . . . . ? P9 Cr4 C33 C34 54.1(4) . . . . ? P7 Cr4 C33 C34 160.9(3) . . . . ? P10 Cr4 C33 C34 -22.1(6) . . . . ? P6 Cr4 C33 C34 -146.8(3) . . . . ? P8 Cr4 C33 C34 106.5(3) . . . . ? C31 Cr4 C33 C32 38.1(3) . . . . ? C35 Cr4 C33 C32 80.3(4) . . . . ? C34 Cr4 C33 C32 117.9(5) . . . . ? P9 Cr4 C33 C32 172.0(3) . . . . ? P7 Cr4 C33 C32 -81.2(3) . . . . ? P10 Cr4 C33 C32 95.8(5) . . . . ? P6 Cr4 C33 C32 -28.8(5) . . . . ? P8 Cr4 C33 C32 -135.6(3) . . . . ? C31 Cr4 C33 C38 160.1(6) . . . . ? C32 Cr4 C33 C38 122.0(7) . . . . ? C35 Cr4 C33 C38 -157.7(6) . . . . ? C34 Cr4 C33 C38 -120.1(6) . . . . ? P9 Cr4 C33 C38 -66.0(5) . . . . ? P7 Cr4 C33 C38 40.8(5) . . . . ? P10 Cr4 C33 C38 -142.2(4) . . . . ? P6 Cr4 C33 C38 93.1(5) . . . . ? P8 Cr4 C33 C38 -13.6(5) . . . . ? C32 C33 C34 C35 0.4(7) . . . . ? C38 C33 C34 C35 -177.2(5) . . . . ? Cr4 C33 C34 C35 61.8(4) . . . . ? C32 C33 C34 C39 175.6(6) . . . . ? C38 C33 C34 C39 -2.1(10) . . . . ? Cr4 C33 C34 C39 -123.1(6) . . . . ? C32 C33 C34 Cr4 -61.4(4) . . . . ? C38 C33 C34 Cr4 121.0(6) . . . . ? C31 Cr4 C34 C33 80.4(4) . . . . ? C32 Cr4 C34 C33 37.4(3) . . . . ? C35 Cr4 C34 C33 117.5(5) . . . . ? P9 Cr4 C34 C33 -136.9(3) . . . . ? P7 Cr4 C34 C33 -29.9(5) . . . . ? P10 Cr4 C34 C33 170.9(3) . . . . ? P6 Cr4 C34 C33 97.8(5) . . . . ? P8 Cr4 C34 C33 -82.5(3) . . . . ? C31 Cr4 C34 C35 -37.2(3) . . . . ? C32 Cr4 C34 C35 -80.2(4) . . . . ? C33 Cr4 C34 C35 -117.5(5) . . . . ? P9 Cr4 C34 C35 105.6(3) . . . . ? P7 Cr4 C34 C35 -147.4(3) . . . . ? P10 Cr4 C34 C35 53.3(4) . . . . ? P6 Cr4 C34 C35 -19.7(7) . . . . ? P8 Cr4 C34 C35 160.0(3) . . . . ? C31 Cr4 C34 C39 -159.0(6) . . . . ? C32 Cr4 C34 C39 158.1(6) . . . . ? C35 Cr4 C34 C39 -121.8(7) . . . . ? C33 Cr4 C34 C39 120.7(7) . . . . ? P9 Cr4 C34 C39 -16.2(5) . . . . ? P7 Cr4 C34 C39 90.8(5) . . . . ? P10 Cr4 C34 C39 -68.4(5) . . . . ? P6 Cr4 C34 C39 -141.5(4) . . . . ? P8 Cr4 C34 C39 38.2(5) . . . . ? C32 C31 C35 C34 0.2(7) . . . . ? C36 C31 C35 C34 178.3(6) . . . . ? Cr4 C31 C35 C34 -61.8(4) . . . . ? C32 C31 C35 C40 -176.6(5) . . . . ? C36 C31 C35 C40 1.5(10) . . . . ? Cr4 C31 C35 C40 121.3(6) . . . . ? C32 C31 C35 Cr4 62.1(4) . . . . ? C36 C31 C35 Cr4 -119.8(6) . . . . ? C33 C34 C35 C31 -0.4(7) . . . . ? C39 C34 C35 C31 -175.5(6) . . . . ? Cr4 C34 C35 C31 61.6(4) . . . . ? C33 C34 C35 C40 176.5(5) . . . . ? C39 C34 C35 C40 1.5(10) . . . . ? Cr4 C34 C35 C40 -121.5(6) . . . . ? C33 C34 C35 Cr4 -62.0(4) . . . . ? C39 C34 C35 Cr4 122.9(6) . . . . ? C32 Cr4 C35 C31 -37.7(3) . . . . ? C34 Cr4 C35 C31 -117.6(5) . . . . ? C33 Cr4 C35 C31 -80.3(4) . . . . ? P9 Cr4 C35 C31 159.9(3) . . . . ? P7 Cr4 C35 C31 -17.7(7) . . . . ? P10 Cr4 C35 C31 105.1(3) . . . . ? P6 Cr4 C35 C31 54.3(4) . . . . ? P8 Cr4 C35 C31 -149.4(3) . . . . ? C31 Cr4 C35 C34 117.6(5) . . . . ? C32 Cr4 C35 C34 79.9(4) . . . . ? C33 Cr4 C35 C34 37.3(3) . . . . ? P9 Cr4 C35 C34 -82.5(3) . . . . ? P7 Cr4 C35 C34 99.9(5) . . . . ? P10 Cr4 C35 C34 -137.3(3) . . . . ? P6 Cr4 C35 C34 171.9(3) . . . . ? P8 Cr4 C35 C34 -31.8(5) . . . . ? C31 Cr4 C35 C40 -122.4(7) . . . . ? C32 Cr4 C35 C40 -160.1(6) . . . . ? C34 Cr4 C35 C40 120.0(7) . . . . ? C33 Cr4 C35 C40 157.3(6) . . . . ? P9 Cr4 C35 C40 37.5(5) . . . . ? P7 Cr4 C35 C40 -140.2(4) . . . . ? P10 Cr4 C35 C40 -17.3(5) . . . . ? P6 Cr4 C35 C40 -68.1(5) . . . . ? P8 Cr4 C35 C40 88.2(5) . . . . ? #===END data_012k _database_code_depnum_ccdc_archive 'CCDC 618762' _audit_creation_method SHELXL-97 _chemical_name_systematic ; \m~2~-\h^5^,\h^5^-cyclopentaphosphole)-bis ((\h^5^-pentamethyl-cyclopentadienyl)-chromium) hexafluoroantimonate ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'C20 H30 Cr2 F6 P5 Sb' _chemical_formula_weight 765.04 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M I2/a loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' _cell_length_a 22.797(14) _cell_length_b 21.216(12) _cell_length_c 22.754(13) _cell_angle_alpha 90.00 _cell_angle_beta 100.51(3) _cell_angle_gamma 90.00 _cell_volume 10821(11) _cell_formula_units_Z 16 _cell_measurement_temperature 12(1) _cell_measurement_reflns_used 24 _cell_measurement_theta_min 12.05 _cell_measurement_theta_max 15.27 _exptl_crystal_description 'irregular prism' _exptl_crystal_colour 'dark green' _exptl_crystal_size_max 0.54 _exptl_crystal_size_mid 0.48 _exptl_crystal_size_min 0.34 _exptl_crystal_density_meas 'not measured' _exptl_crystal_density_diffrn 1.878 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 6048 _exptl_absorpt_coefficient_mu 2.127 _exptl_absorpt_correction_type integration _exptl_absorpt_correction_T_min 0.381 _exptl_absorpt_correction_T_max 0.537 _exptl_absorpt_process_details 'XPREP in SHELXTL' _exptl_special_details ; ? ; _diffrn_ambient_temperature 12(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Fddd 4-circle diffractometer' _diffrn_measurement_method '\w scans' _diffrn_detector_area_resol_mean ? _diffrn_standards_number 4 _diffrn_standards_interval_count 146 _diffrn_standards_interval_time ? _diffrn_standards_decay_% 0 _diffrn_reflns_number 11361 _diffrn_reflns_av_R_equivalents 0.0207 _diffrn_reflns_av_sigmaI/netI 0.0169 _diffrn_reflns_limit_h_min -27 _diffrn_reflns_limit_h_max 26 _diffrn_reflns_limit_k_min -1 _diffrn_reflns_limit_k_max 25 _diffrn_reflns_limit_l_min -1 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_theta_min 1.16 _diffrn_reflns_theta_max 25.01 _reflns_number_total 9546 _reflns_number_gt 9473 _reflns_threshold_expression >2sigma(I) _computing_data_collection 'MAD (Allibon, 1996)' _computing_cell_refinement 'MAD (Allibon, 1996)' _computing_data_reduction 'COLL5N (Lehmann & Wilson, 1987)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics 'SHELXTL V6.12(Bruker, 2001)' _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0489P)^2^+97.3674P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_number_reflns 9546 _refine_ls_number_parameters 614 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0384 _refine_ls_R_factor_gt 0.0381 _refine_ls_wR_factor_ref 0.0992 _refine_ls_wR_factor_gt 0.0988 _refine_ls_goodness_of_fit_ref 1.131 _refine_ls_restrained_S_all 1.131 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _diffrn_measured_fraction_theta_max 0.999 _diffrn_reflns_theta_full 25.01 _diffrn_measured_fraction_theta_full 0.999 _refine_diff_density_max 1.727 _refine_diff_density_min -0.899 _refine_diff_density_rms 0.317 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb1 Sb 0.138775(16) 0.870281(18) 0.382860(17) 0.01366(9) Uani 1 1 d . . . F1 F 0.09484(15) 0.81155(16) 0.33009(16) 0.0217(7) Uani 1 1 d . . . F2 F 0.09276(15) 0.93616(15) 0.34189(15) 0.0205(7) Uani 1 1 d . . . F3 F 0.08374(15) 0.86282(17) 0.43482(16) 0.0205(7) Uani 1 1 d . . . F4 F 0.18328(14) 0.80387(15) 0.42380(15) 0.0184(7) Uani 1 1 d . . . F5 F 0.19461(16) 0.87750(15) 0.33175(17) 0.0209(8) Uani 1 1 d . . . F6 F 0.18285(15) 0.92945(16) 0.43488(15) 0.0206(7) Uani 1 1 d . . . Sb2 Sb 0.133224(17) 0.126428(18) 0.118373(19) 0.01420(9) Uani 1 1 d . . . F7 F 0.12028(17) 0.04607(17) 0.14725(18) 0.0313(9) Uani 1 1 d . . . F8 F 0.06832(15) 0.15905(18) 0.14774(17) 0.0278(8) Uani 1 1 d . . . F9 F 0.08278(15) 0.10670(17) 0.04518(16) 0.0242(8) Uani 1 1 d . . . F10 F 0.19903(14) 0.09641(17) 0.08786(16) 0.0228(7) Uani 1 1 d . . . F11 F 0.18372(15) 0.14593(18) 0.19139(15) 0.0240(8) Uani 1 1 d . . . F12 F 0.14706(16) 0.20680(17) 0.08930(18) 0.0287(8) Uani 1 1 d . . . C1 C -0.1102(2) 0.3112(3) 0.4505(3) 0.0149(11) Uani 1 1 d . . . C2 C -0.1407(2) 0.2685(3) 0.4055(3) 0.0167(12) Uani 1 1 d . . . C3 C -0.1376(2) 0.2946(3) 0.3482(3) 0.0152(12) Uani 1 1 d . . . C4 C -0.1061(3) 0.3533(2) 0.3568(3) 0.0152(11) Uani 1 1 d . . . C5 C -0.0903(2) 0.3632(3) 0.4200(3) 0.0142(11) Uani 1 1 d . . . C6 C -0.1058(3) 0.3053(3) 0.5171(3) 0.0174(12) Uani 1 1 d . . . H6A H -0.1414 0.3236 0.5288 0.026 Uiso 1 1 calc R . . H6B H -0.0702 0.3277 0.5375 0.026 Uiso 1 1 calc R . . H6C H -0.1027 0.2607 0.5284 0.026 Uiso 1 1 calc R . . C7 C -0.1721(3) 0.2094(3) 0.4182(3) 0.0178(12) Uani 1 1 d . . . H7A H -0.2135 0.2193 0.4210 0.027 Uiso 1 1 calc R . . H7B H -0.1519 0.1912 0.4561 0.027 Uiso 1 1 calc R . . H7C H -0.1716 0.1790 0.3859 0.027 Uiso 1 1 calc R . . C8 C -0.1638(3) 0.2671(3) 0.2885(3) 0.0178(12) Uani 1 1 d . . . H8A H -0.2022 0.2874 0.2733 0.027 Uiso 1 1 calc R . . H8B H -0.1698 0.2217 0.2927 0.027 Uiso 1 1 calc R . . H8C H -0.1365 0.2744 0.2605 0.027 Uiso 1 1 calc R . . C9 C -0.0964(3) 0.3977(3) 0.3084(3) 0.0188(12) Uani 1 1 d . . . H9A H -0.1302 0.4268 0.2993 0.028 Uiso 1 1 calc R . . H9B H -0.0928 0.3737 0.2724 0.028 Uiso 1 1 calc R . . H9C H -0.0597 0.4218 0.3217 0.028 Uiso 1 1 calc R . . C10 C -0.0617(3) 0.4217(3) 0.4502(3) 0.0193(12) Uani 1 1 d . . . H10A H -0.0876 0.4396 0.4759 0.029 Uiso 1 1 calc R . . H10B H -0.0559 0.4527 0.4199 0.029 Uiso 1 1 calc R . . H10C H -0.0230 0.4108 0.4746 0.029 Uiso 1 1 calc R . . Cr1 Cr -0.04590(4) 0.27549(4) 0.39711(4) 0.01390(19) Uani 1 1 d . . . P1 P 0.03278(7) 0.25969(8) 0.48118(8) 0.0233(3) Uani 1 1 d . . . P2 P -0.01531(7) 0.17551(8) 0.44684(8) 0.0231(3) Uani 1 1 d . . . P3 P -0.03435(7) 0.17618(9) 0.35017(8) 0.0267(4) Uani 1 1 d . . . P4 P 0.00143(7) 0.26588(9) 0.31570(8) 0.0262(4) Uani 1 1 d . . . P5 P 0.04603(7) 0.32199(7) 0.40309(8) 0.0216(3) Uani 1 1 d . . . Cr2 Cr 0.06189(4) 0.21513(4) 0.39442(4) 0.01367(19) Uani 1 1 d . . . C11 C 0.1467(2) 0.1777(3) 0.4439(3) 0.0153(11) Uani 1 1 d . . . C12 C 0.1173(2) 0.1283(3) 0.4069(3) 0.0143(12) Uani 1 1 d . . . C13 C 0.1118(2) 0.1480(3) 0.3466(3) 0.0165(12) Uani 1 1 d . . . C14 C 0.1374(2) 0.2091(3) 0.3460(3) 0.0162(12) Uani 1 1 d . . . C15 C 0.1596(2) 0.2275(3) 0.4065(3) 0.0154(11) Uani 1 1 d . . . C16 C 0.1651(2) 0.1731(3) 0.5104(3) 0.0179(12) Uani 1 1 d . . . H16A H 0.2024 0.1493 0.5202 0.027 Uiso 1 1 calc R . . H16B H 0.1338 0.1514 0.5271 0.027 Uiso 1 1 calc R . . H16C H 0.1709 0.2155 0.5276 0.027 Uiso 1 1 calc R . . C17 C 0.0997(3) 0.0653(3) 0.4284(3) 0.0201(12) Uani 1 1 d . . . H17A H 0.1347 0.0377 0.4361 0.030 Uiso 1 1 calc R . . H17B H 0.0690 0.0462 0.3978 0.030 Uiso 1 1 calc R . . H17C H 0.0840 0.0709 0.4654 0.030 Uiso 1 1 calc R . . C18 C 0.0871(3) 0.1092(3) 0.2918(3) 0.0216(13) Uani 1 1 d . . . H18A H 0.1198 0.0872 0.2779 0.032 Uiso 1 1 calc R . . H18B H 0.0669 0.1370 0.2600 0.032 Uiso 1 1 calc R . . H18C H 0.0586 0.0783 0.3019 0.032 Uiso 1 1 calc R . . C19 C 0.1445(3) 0.2454(3) 0.2913(3) 0.0191(12) Uani 1 1 d . . . H19A H 0.1849 0.2392 0.2833 0.029 Uiso 1 1 calc R . . H19B H 0.1380 0.2904 0.2978 0.029 Uiso 1 1 calc R . . H19C H 0.1153 0.2306 0.2571 0.029 Uiso 1 1 calc R . . C20 C 0.1936(2) 0.2866(3) 0.4262(3) 0.0169(12) Uani 1 1 d . . . H20A H 0.2364 0.2789 0.4289 0.025 Uiso 1 1 calc R . . H20B H 0.1858 0.2994 0.4654 0.025 Uiso 1 1 calc R . . H20C H 0.1808 0.3202 0.3971 0.025 Uiso 1 1 calc R . . C21 C 0.1077(3) 0.3898(3) 0.1387(3) 0.0173(12) Uani 1 1 d . . . C22 C 0.1716(3) 0.3847(3) 0.1510(3) 0.0148(12) Uani 1 1 d . . . C23 C 0.1944(2) 0.4403(3) 0.1295(3) 0.0145(11) Uani 1 1 d . . . C24 C 0.1471(3) 0.4805(3) 0.1046(3) 0.0171(11) Uani 1 1 d . . . C25 C 0.0933(3) 0.4493(3) 0.1101(3) 0.0171(12) Uani 1 1 d . . . C26 C 0.0637(3) 0.3403(3) 0.1487(3) 0.0182(12) Uani 1 1 d . . . H26A H 0.0558 0.3122 0.1140 0.027 Uiso 1 1 calc R . . H26B H 0.0264 0.3605 0.1543 0.027 Uiso 1 1 calc R . . H26C H 0.0801 0.3158 0.1845 0.027 Uiso 1 1 calc R . . C27 C 0.2065(2) 0.3280(3) 0.1760(3) 0.0157(11) Uani 1 1 d . . . H27A H 0.2267 0.3098 0.1455 0.024 Uiso 1 1 calc R . . H27B H 0.1795 0.2967 0.1882 0.024 Uiso 1 1 calc R . . H27C H 0.2363 0.3405 0.2108 0.024 Uiso 1 1 calc R . . C28 C 0.2595(3) 0.4511(3) 0.1294(3) 0.0206(13) Uani 1 1 d . . . H28A H 0.2694 0.4353 0.0919 0.031 Uiso 1 1 calc R . . H28B H 0.2834 0.4287 0.1631 0.031 Uiso 1 1 calc R . . H28C H 0.2682 0.4963 0.1330 0.031 Uiso 1 1 calc R . . C29 C 0.1530(3) 0.5412(3) 0.0717(3) 0.0176(12) Uani 1 1 d . . . H29A H 0.1539 0.5319 0.0296 0.026 Uiso 1 1 calc R . . H29B H 0.1900 0.5626 0.0898 0.026 Uiso 1 1 calc R . . H29C H 0.1188 0.5685 0.0741 0.026 Uiso 1 1 calc R . . C30 C 0.0307(3) 0.4719(3) 0.0846(3) 0.0192(12) Uani 1 1 d . . . H30A H 0.0170 0.4520 0.0456 0.029 Uiso 1 1 calc R . . H30B H 0.0310 0.5178 0.0798 0.029 Uiso 1 1 calc R . . H30C H 0.0038 0.4605 0.1119 0.029 Uiso 1 1 calc R . . Cr3 Cr 0.14509(4) 0.46766(4) 0.20036(4) 0.01374(19) Uani 1 1 d . . . P6 P 0.09321(7) 0.43542(8) 0.27777(7) 0.0228(3) Uani 1 1 d . . . P7 P 0.18903(7) 0.42574(7) 0.29915(7) 0.0188(3) Uani 1 1 d . . . P8 P 0.23257(6) 0.50533(7) 0.26522(7) 0.0175(3) Uani 1 1 d . . . P9 P 0.16243(7) 0.57381(7) 0.21989(7) 0.0173(3) Uani 1 1 d . . . P10 P 0.06919(7) 0.52637(8) 0.22817(7) 0.0214(3) Uani 1 1 d . . . Cr4 Cr 0.14744(4) 0.53015(4) 0.30904(4) 0.01317(19) Uani 1 1 d . . . C31 C 0.0966(3) 0.5531(3) 0.3804(3) 0.0161(11) Uani 1 1 d . . . C32 C 0.1522(2) 0.5240(3) 0.4071(2) 0.0142(11) Uani 1 1 d . . . C33 C 0.1992(2) 0.5638(3) 0.3954(3) 0.0148(11) Uani 1 1 d . . . C34 C 0.1734(3) 0.6166(3) 0.3621(3) 0.0170(12) Uani 1 1 d . . . C35 C 0.1095(2) 0.6104(3) 0.3531(3) 0.0165(11) Uani 1 1 d . . . C36 C 0.0353(2) 0.5292(3) 0.3835(3) 0.0177(12) Uani 1 1 d . . . H36A H 0.0225 0.5465 0.4191 0.027 Uiso 1 1 calc R . . H36B H 0.0360 0.4831 0.3858 0.027 Uiso 1 1 calc R . . H36C H 0.0074 0.5426 0.3477 0.027 Uiso 1 1 calc R . . C37 C 0.1586(3) 0.4645(3) 0.4432(3) 0.0187(12) Uani 1 1 d . . . H37A H 0.1522 0.4737 0.4838 0.028 Uiso 1 1 calc R . . H37B H 0.1988 0.4474 0.4450 0.028 Uiso 1 1 calc R . . H37C H 0.1291 0.4336 0.4245 0.028 Uiso 1 1 calc R . . C38 C 0.2646(2) 0.5550(3) 0.4181(3) 0.0173(12) Uani 1 1 d . . . H38A H 0.2760 0.5768 0.4565 0.026 Uiso 1 1 calc R . . H38B H 0.2873 0.5725 0.3892 0.026 Uiso 1 1 calc R . . H38C H 0.2734 0.5099 0.4235 0.026 Uiso 1 1 calc R . . C39 C 0.2070(2) 0.6724(3) 0.3458(3) 0.0166(12) Uani 1 1 d . . . H39A H 0.2139 0.7021 0.3794 0.025 Uiso 1 1 calc R . . H39B H 0.1837 0.6932 0.3107 0.025 Uiso 1 1 calc R . . H39C H 0.2453 0.6586 0.3367 0.025 Uiso 1 1 calc R . . C40 C 0.0658(3) 0.6585(3) 0.3229(3) 0.0201(12) Uani 1 1 d . . . H40A H 0.0625 0.6930 0.3508 0.030 Uiso 1 1 calc R . . H40B H 0.0266 0.6387 0.3105 0.030 Uiso 1 1 calc R . . H40C H 0.0797 0.6752 0.2877 0.030 Uiso 1 1 calc R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.01055(18) 0.01375(17) 0.0165(2) -0.00069(15) 0.00201(13) 0.00038(14) F1 0.0181(17) 0.0234(18) 0.0224(18) -0.0047(14) 0.0007(14) -0.0056(14) F2 0.0225(18) 0.0162(16) 0.0214(18) 0.0035(14) 0.0003(13) 0.0104(14) F3 0.0129(16) 0.0269(18) 0.0226(18) 0.0001(15) 0.0058(14) 0.0009(14) F4 0.0127(15) 0.0154(16) 0.0275(19) 0.0046(14) 0.0044(13) 0.0035(13) F5 0.0170(17) 0.0222(19) 0.025(2) 0.0007(14) 0.0075(15) -0.0012(13) F6 0.0195(17) 0.0208(17) 0.0207(18) -0.0060(14) 0.0013(13) -0.0059(14) Sb2 0.0098(2) 0.01411(17) 0.0179(2) -0.00058(14) 0.00045(13) 0.00010(13) F7 0.028(2) 0.0216(18) 0.042(2) 0.0118(17) -0.0003(17) -0.0039(16) F8 0.0166(17) 0.036(2) 0.031(2) -0.0062(17) 0.0036(15) 0.0070(15) F9 0.0184(17) 0.0281(19) 0.0231(19) -0.0098(15) -0.0046(14) -0.0010(15) F10 0.0136(16) 0.0285(19) 0.0264(19) -0.0055(15) 0.0043(14) 0.0046(14) F11 0.0159(17) 0.036(2) 0.0180(18) -0.0076(15) -0.0026(14) 0.0034(15) F12 0.0259(19) 0.0234(18) 0.035(2) 0.0075(16) 0.0012(16) -0.0022(15) C1 0.013(3) 0.013(3) 0.018(3) -0.003(2) 0.004(2) 0.002(2) C2 0.007(2) 0.019(3) 0.025(3) 0.001(2) 0.003(2) 0.001(2) C3 0.004(2) 0.018(3) 0.023(3) 0.001(2) 0.001(2) 0.002(2) C4 0.012(3) 0.008(2) 0.024(3) 0.002(2) 0.000(2) 0.002(2) C5 0.011(3) 0.015(3) 0.017(3) 0.001(2) 0.004(2) 0.001(2) C6 0.018(3) 0.017(3) 0.016(3) -0.003(2) 0.001(2) -0.002(2) C7 0.013(3) 0.018(3) 0.023(3) -0.002(2) 0.004(2) -0.006(2) C8 0.017(3) 0.012(3) 0.023(3) -0.002(2) -0.002(2) -0.001(2) C9 0.018(3) 0.013(3) 0.025(3) -0.002(2) 0.003(2) 0.000(2) C10 0.017(3) 0.018(3) 0.022(3) -0.001(2) 0.002(2) 0.000(2) Cr1 0.0091(4) 0.0146(4) 0.0180(5) -0.0023(4) 0.0023(3) -0.0016(3) P1 0.0144(7) 0.0308(9) 0.0231(8) -0.0076(7) -0.0006(6) 0.0040(6) P2 0.0151(7) 0.0233(8) 0.0314(9) -0.0015(7) 0.0053(6) 0.0012(6) P3 0.0135(7) 0.0310(9) 0.0338(9) -0.0170(7) -0.0005(6) 0.0015(6) P4 0.0150(7) 0.0418(10) 0.0213(8) 0.0011(7) 0.0019(6) 0.0094(7) P5 0.0117(7) 0.0186(7) 0.0337(9) -0.0033(7) 0.0025(6) -0.0010(6) Cr2 0.0075(4) 0.0141(4) 0.0183(5) -0.0010(4) -0.0005(3) 0.0006(3) C11 0.008(2) 0.018(3) 0.019(3) 0.003(2) 0.001(2) 0.006(2) C12 0.009(3) 0.016(3) 0.018(3) 0.000(2) 0.002(2) 0.005(2) C13 0.006(2) 0.021(3) 0.023(3) -0.002(2) 0.002(2) 0.006(2) C14 0.005(2) 0.018(3) 0.025(3) -0.004(2) 0.000(2) 0.008(2) C15 0.004(2) 0.020(3) 0.021(3) 0.000(2) 0.002(2) 0.003(2) C16 0.015(3) 0.024(3) 0.014(3) 0.001(2) -0.001(2) 0.007(2) C17 0.018(3) 0.015(3) 0.029(3) 0.003(2) 0.008(2) -0.001(2) C18 0.015(3) 0.021(3) 0.028(3) -0.004(3) 0.000(2) 0.004(2) C19 0.019(3) 0.022(3) 0.015(3) 0.002(2) -0.001(2) 0.001(2) C20 0.012(3) 0.016(3) 0.021(3) -0.001(2) 0.000(2) 0.007(2) C21 0.012(3) 0.020(3) 0.019(3) -0.004(2) 0.001(2) -0.003(2) C22 0.010(3) 0.018(3) 0.016(3) -0.005(2) 0.001(2) -0.001(2) C23 0.009(3) 0.017(3) 0.016(3) -0.006(2) -0.001(2) 0.001(2) C24 0.016(3) 0.017(3) 0.019(3) 0.000(2) 0.004(2) 0.002(2) C25 0.016(3) 0.019(3) 0.017(3) -0.001(2) 0.002(2) 0.004(2) C26 0.014(3) 0.019(3) 0.020(3) 0.003(2) 0.000(2) 0.001(2) C27 0.012(3) 0.019(3) 0.015(3) -0.002(2) -0.003(2) 0.002(2) C28 0.011(3) 0.028(3) 0.024(3) 0.000(3) 0.005(2) -0.001(2) C29 0.018(3) 0.018(3) 0.018(3) -0.001(2) 0.006(2) 0.000(2) C30 0.011(3) 0.028(3) 0.018(3) 0.002(2) 0.002(2) 0.001(2) Cr3 0.0088(4) 0.0139(4) 0.0180(5) 0.0010(4) 0.0011(3) 0.0014(3) P6 0.0215(8) 0.0263(8) 0.0230(8) -0.0097(7) 0.0099(6) -0.0098(6) P7 0.0201(7) 0.0167(7) 0.0197(8) -0.0010(6) 0.0034(6) 0.0014(6) P8 0.0134(7) 0.0203(7) 0.0187(8) -0.0024(6) 0.0025(6) -0.0019(6) P9 0.0190(7) 0.0156(7) 0.0172(7) -0.0006(6) 0.0032(6) -0.0002(6) P10 0.0118(7) 0.0300(9) 0.0210(8) -0.0078(7) -0.0012(6) 0.0059(6) Cr4 0.0090(4) 0.0138(4) 0.0158(5) -0.0001(3) 0.0000(3) -0.0001(3) C31 0.013(3) 0.013(3) 0.020(3) -0.003(2) -0.003(2) 0.000(2) C32 0.013(3) 0.017(3) 0.013(3) 0.000(2) 0.001(2) -0.003(2) C33 0.012(3) 0.019(3) 0.013(3) -0.001(2) 0.000(2) -0.004(2) C34 0.014(3) 0.020(3) 0.017(3) -0.004(2) 0.001(2) -0.001(2) C35 0.011(3) 0.018(3) 0.020(3) -0.003(2) 0.001(2) -0.001(2) C36 0.011(3) 0.020(3) 0.021(3) 0.002(2) 0.003(2) -0.004(2) C37 0.017(3) 0.025(3) 0.014(3) -0.001(2) 0.000(2) -0.002(2) C38 0.014(3) 0.020(3) 0.017(3) 0.000(2) 0.001(2) -0.002(2) C39 0.010(3) 0.020(3) 0.018(3) 0.002(2) -0.003(2) -0.003(2) C40 0.020(3) 0.021(3) 0.018(3) 0.002(2) 0.000(2) 0.000(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb1 F5 1.881(4) . ? Sb1 F4 1.881(3) . ? Sb1 F3 1.881(3) . ? Sb1 F6 1.885(3) . ? Sb1 F1 1.886(3) . ? Sb1 F2 1.888(3) . ? Sb2 F8 1.864(4) . ? Sb2 F7 1.870(4) . ? Sb2 F10 1.876(3) . ? Sb2 F12 1.876(4) . ? Sb2 F11 1.887(3) . ? Sb2 F9 1.890(3) . ? C1 C5 1.421(8) . ? C1 C2 1.446(8) . ? C1 C6 1.507(8) . ? C1 Cr1 2.201(6) . ? C2 C3 1.430(9) . ? C2 C7 1.499(8) . ? C2 Cr1 2.208(6) . ? C3 C4 1.434(8) . ? C3 C8 1.498(8) . ? C3 Cr1 2.218(6) . ? C4 C5 1.432(8) . ? C4 C9 1.497(8) . ? C4 Cr1 2.235(6) . ? C5 C10 1.509(8) . ? C5 Cr1 2.224(6) . ? C6 H6A 0.9800 . ? C6 H6B 0.9800 . ? C6 H6C 0.9800 . ? C7 H7A 0.9800 . ? C7 H7B 0.9800 . ? C7 H7C 0.9800 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? Cr1 P5 2.298(2) . ? Cr1 P4 2.317(2) . ? Cr1 P1 2.395(2) . ? Cr1 P3 2.398(2) . ? Cr1 P2 2.445(2) . ? Cr1 Cr2 2.7816(19) . ? P1 P2 2.166(3) . ? P1 P5 2.278(3) . ? P1 Cr2 2.389(2) . ? P2 P3 2.163(3) . ? P2 Cr2 2.448(2) . ? P3 P4 2.266(3) . ? P3 Cr2 2.389(2) . ? P4 Cr2 2.317(2) . ? P4 P5 2.381(3) . ? P5 Cr2 2.310(2) . ? Cr2 C11 2.201(6) . ? Cr2 C14 2.210(6) . ? Cr2 C15 2.210(6) . ? Cr2 C12 2.222(5) . ? Cr2 C13 2.228(6) . ? C11 C15 1.422(8) . ? C11 C12 1.434(8) . ? C11 C16 1.498(8) . ? C12 C13 1.418(8) . ? C12 C17 1.503(8) . ? C13 C14 1.422(8) . ? C13 C18 1.514(8) . ? C14 C15 1.432(8) . ? C14 C19 1.497(8) . ? C15 C20 1.499(8) . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 C25 1.430(9) . ? C21 C22 1.435(8) . ? C21 C26 1.499(8) . ? C21 Cr3 2.232(6) . ? C22 C23 1.412(8) . ? C22 C27 1.496(8) . ? C22 Cr3 2.230(6) . ? C23 C24 1.409(8) . ? C23 C28 1.503(8) . ? C23 Cr3 2.205(6) . ? C24 C25 1.419(8) . ? C24 C29 1.508(8) . ? C24 Cr3 2.204(6) . ? C25 C30 1.516(8) . ? C25 Cr3 2.209(6) . ? C26 H26A 0.9800 . ? C26 H26B 0.9800 . ? C26 H26C 0.9800 . ? C27 H27A 0.9800 . ? C27 H27B 0.9800 . ? C27 H27C 0.9800 . ? C28 H28A 0.9800 . ? C28 H28B 0.9800 . ? C28 H28C 0.9800 . ? C29 H29A 0.9800 . ? C29 H29B 0.9800 . ? C29 H29C 0.9800 . ? C30 H30A 0.9800 . ? C30 H30B 0.9800 . ? C30 H30C 0.9800 . ? Cr3 P10 2.312(2) . ? Cr3 P9 2.316(2) . ? Cr3 P8 2.392(2) . ? Cr3 P6 2.394(2) . ? Cr3 P7 2.455(2) . ? Cr3 Cr4 2.7977(18) . ? P6 P7 2.159(3) . ? P6 P10 2.252(3) . ? P6 Cr4 2.399(2) . ? P7 P8 2.171(2) . ? P7 Cr4 2.436(2) . ? P8 P9 2.265(2) . ? P8 Cr4 2.397(2) . ? P9 Cr4 2.311(2) . ? P9 P10 2.390(3) . ? P10 Cr4 2.319(2) . ? Cr4 C31 2.215(6) . ? Cr4 C34 2.216(6) . ? Cr4 C33 2.217(6) . ? Cr4 C32 2.218(6) . ? Cr4 C35 2.230(6) . ? C31 C35 1.422(8) . ? C31 C32 1.440(8) . ? C31 C36 1.498(8) . ? C32 C33 1.430(8) . ? C32 C37 1.498(8) . ? C33 C34 1.417(8) . ? C33 C38 1.498(8) . ? C34 C35 1.439(8) . ? C34 C39 1.493(8) . ? C35 C40 1.502(8) . ? C36 H36A 0.9800 . ? C36 H36B 0.9800 . ? C36 H36C 0.9800 . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C39 H39A 0.9800 . ? C39 H39B 0.9800 . ? C39 H39C 0.9800 . ? C40 H40A 0.9800 . ? C40 H40B 0.9800 . ? C40 H40C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F5 Sb1 F4 90.14(15) . . ? F5 Sb1 F3 179.25(14) . . ? F4 Sb1 F3 89.26(15) . . ? F5 Sb1 F6 89.47(16) . . ? F4 Sb1 F6 90.59(15) . . ? F3 Sb1 F6 90.09(16) . . ? F5 Sb1 F1 90.05(16) . . ? F4 Sb1 F1 89.79(16) . . ? F3 Sb1 F1 90.40(16) . . ? F6 Sb1 F1 179.39(16) . . ? F5 Sb1 F2 90.70(16) . . ? F4 Sb1 F2 178.93(15) . . ? F3 Sb1 F2 89.91(16) . . ? F6 Sb1 F2 90.09(15) . . ? F1 Sb1 F2 89.55(15) . . ? F8 Sb2 F7 91.50(18) . . ? F8 Sb2 F10 178.01(17) . . ? F7 Sb2 F10 90.50(17) . . ? F8 Sb2 F12 89.11(17) . . ? F7 Sb2 F12 179.37(17) . . ? F10 Sb2 F12 88.90(16) . . ? F8 Sb2 F11 89.98(16) . . ? F7 Sb2 F11 90.04(17) . . ? F10 Sb2 F11 89.98(15) . . ? F12 Sb2 F11 89.79(17) . . ? F8 Sb2 F9 90.16(16) . . ? F7 Sb2 F9 89.89(17) . . ? F10 Sb2 F9 89.88(16) . . ? F12 Sb2 F9 90.28(17) . . ? F11 Sb2 F9 179.84(18) . . ? C5 C1 C2 107.2(5) . . ? C5 C1 C6 126.0(5) . . ? C2 C1 C6 126.6(5) . . ? C5 C1 Cr1 72.1(3) . . ? C2 C1 Cr1 71.1(3) . . ? C6 C1 Cr1 126.7(4) . . ? C3 C2 C1 107.8(5) . . ? C3 C2 C7 127.2(5) . . ? C1 C2 C7 124.9(5) . . ? C3 C2 Cr1 71.5(3) . . ? C1 C2 Cr1 70.6(3) . . ? C7 C2 Cr1 125.7(4) . . ? C2 C3 C4 108.6(5) . . ? C2 C3 C8 126.8(5) . . ? C4 C3 C8 124.6(5) . . ? C2 C3 Cr1 70.8(3) . . ? C4 C3 Cr1 71.8(3) . . ? C8 C3 Cr1 124.6(4) . . ? C5 C4 C3 107.0(5) . . ? C5 C4 C9 127.1(5) . . ? C3 C4 C9 125.8(6) . . ? C5 C4 Cr1 70.9(3) . . ? C3 C4 Cr1 70.6(3) . . ? C9 C4 Cr1 127.2(4) . . ? C1 C5 C4 109.4(5) . . ? C1 C5 C10 124.5(5) . . ? C4 C5 C10 126.0(5) . . ? C1 C5 Cr1 70.4(3) . . ? C4 C5 Cr1 71.7(3) . . ? C10 C5 Cr1 128.2(4) . . ? C1 C6 H6A 109.5 . . ? C1 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C1 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C1 Cr1 C2 38.3(2) . . ? C1 Cr1 C3 63.4(2) . . ? C2 Cr1 C3 37.7(2) . . ? C1 Cr1 C5 37.5(2) . . ? C2 Cr1 C5 62.8(2) . . ? C3 Cr1 C5 62.5(2) . . ? C1 Cr1 C4 63.3(2) . . ? C2 Cr1 C4 63.1(2) . . ? C3 Cr1 C4 37.6(2) . . ? C5 Cr1 C4 37.5(2) . . ? C1 Cr1 P5 120.77(16) . . ? C2 Cr1 P5 156.92(16) . . ? C3 Cr1 P5 135.81(16) . . ? C5 Cr1 P5 94.35(16) . . ? C4 Cr1 P5 101.11(16) . . ? C1 Cr1 P4 157.74(16) . . ? C2 Cr1 P4 131.99(17) . . ? C3 Cr1 P4 98.54(17) . . ? C5 Cr1 P4 123.97(16) . . ? C4 Cr1 P4 94.47(16) . . ? P5 Cr1 P4 62.12(7) . . ? C1 Cr1 P1 94.86(17) . . ? C2 Cr1 P1 121.56(17) . . ? C3 Cr1 P1 157.80(16) . . ? C5 Cr1 P1 103.68(16) . . ? C4 Cr1 P1 138.22(16) . . ? P5 Cr1 P1 58.04(7) . . ? P4 Cr1 P1 103.65(8) . . ? C1 Cr1 P3 133.32(16) . . ? C2 Cr1 P3 99.67(16) . . ? C3 Cr1 P3 96.12(16) . . ? C5 Cr1 P3 158.52(16) . . ? C4 Cr1 P3 125.14(17) . . ? P5 Cr1 P3 103.33(7) . . ? P4 Cr1 P3 57.42(7) . . ? P1 Cr1 P3 96.07(7) . . ? C1 Cr1 P2 101.87(16) . . ? C2 Cr1 P2 95.88(16) . . ? C3 Cr1 P2 123.60(16) . . ? C5 Cr1 P2 136.13(16) . . ? C4 Cr1 P2 158.91(15) . . ? P5 Cr1 P2 99.49(7) . . ? P4 Cr1 P2 99.12(7) . . ? P1 Cr1 P2 53.14(6) . . ? P3 Cr1 P2 53.04(7) . . ? C1 Cr1 Cr2 148.25(16) . . ? C2 Cr1 Cr2 148.54(16) . . ? C3 Cr1 Cr2 145.91(16) . . ? C5 Cr1 Cr2 146.25(15) . . ? C4 Cr1 Cr2 144.14(15) . . ? P5 Cr1 Cr2 53.06(6) . . ? P4 Cr1 Cr2 53.11(5) . . ? P1 Cr1 Cr2 54.35(6) . . ? P3 Cr1 Cr2 54.31(5) . . ? P2 Cr1 Cr2 55.40(5) . . ? P2 P1 P5 109.12(10) . . ? P2 P1 Cr2 64.80(7) . . ? P5 P1 Cr2 59.26(7) . . ? P2 P1 Cr1 64.61(7) . . ? P5 P1 Cr1 58.83(7) . . ? Cr2 P1 Cr1 71.09(7) . . ? P3 P2 P1 110.85(10) . . ? P3 P2 Cr1 62.37(7) . . ? P1 P2 Cr1 62.25(8) . . ? P3 P2 Cr2 62.03(7) . . ? P1 P2 Cr2 62.03(7) . . ? Cr1 P2 Cr2 69.29(6) . . ? P2 P3 P4 109.84(9) . . ? P2 P3 Cr2 64.85(7) . . ? P4 P3 Cr2 59.63(7) . . ? P2 P3 Cr1 64.59(7) . . ? P4 P3 Cr1 59.48(7) . . ? Cr2 P3 Cr1 71.05(6) . . ? P3 P4 Cr2 62.81(7) . . ? P3 P4 Cr1 63.10(7) . . ? Cr2 P4 Cr1 73.79(7) . . ? P3 P4 P5 104.87(10) . . ? Cr2 P4 P5 58.89(7) . . ? Cr1 P4 P5 58.55(7) . . ? P1 P5 Cr1 63.12(7) . . ? P1 P5 Cr2 62.76(7) . . ? Cr1 P5 Cr2 74.27(6) . . ? P1 P5 P4 105.32(10) . . ? Cr1 P5 P4 59.33(7) . . ? Cr2 P5 P4 59.17(6) . . ? C11 Cr2 C14 62.8(2) . . ? C11 Cr2 C15 37.6(2) . . ? C14 Cr2 C15 37.8(2) . . ? C11 Cr2 C12 37.8(2) . . ? C14 Cr2 C12 62.6(2) . . ? C15 Cr2 C12 63.0(2) . . ? C11 Cr2 C13 62.6(2) . . ? C14 Cr2 C13 37.4(2) . . ? C15 Cr2 C13 62.8(2) . . ? C12 Cr2 C13 37.2(2) . . ? C11 Cr2 P5 116.55(17) . . ? C14 Cr2 P5 104.35(16) . . ? C15 Cr2 P5 92.45(15) . . ? C12 Cr2 P5 153.78(16) . . ? C13 Cr2 P5 140.46(16) . . ? C11 Cr2 P4 155.04(16) . . ? C14 Cr2 P4 92.80(17) . . ? C15 Cr2 P4 118.99(17) . . ? C12 Cr2 P4 136.70(17) . . ? C13 Cr2 P4 101.78(16) . . ? P5 Cr2 P4 61.94(7) . . ? C11 Cr2 P3 138.14(17) . . ? C14 Cr2 P3 120.57(17) . . ? C15 Cr2 P3 157.08(16) . . ? C12 Cr2 P3 102.92(16) . . ? C13 Cr2 P3 94.86(16) . . ? P5 Cr2 P3 103.26(7) . . ? P4 Cr2 P3 57.56(8) . . ? C11 Cr2 P1 94.05(17) . . ? C14 Cr2 P1 142.55(16) . . ? C15 Cr2 P1 106.03(17) . . ? C12 Cr2 P1 117.38(16) . . ? C13 Cr2 P1 154.23(16) . . ? P5 Cr2 P1 57.97(7) . . ? P4 Cr2 P1 103.84(8) . . ? P3 Cr2 P1 96.49(7) . . ? C11 Cr2 P2 105.64(17) . . ? C14 Cr2 P2 156.55(16) . . ? C15 Cr2 P2 141.12(17) . . ? C12 Cr2 P2 95.48(16) . . ? C13 Cr2 P2 119.70(16) . . ? P5 Cr2 P2 99.08(7) . . ? P4 Cr2 P2 99.04(8) . . ? P3 Cr2 P2 53.12(7) . . ? P1 Cr2 P2 53.17(7) . . ? C11 Cr2 Cr1 148.45(16) . . ? C14 Cr2 Cr1 144.00(16) . . ? C15 Cr2 Cr1 144.80(16) . . ? C12 Cr2 Cr1 149.60(15) . . ? C13 Cr2 Cr1 146.86(15) . . ? P5 Cr2 Cr1 52.67(5) . . ? P4 Cr2 Cr1 53.11(6) . . ? P3 Cr2 Cr1 54.64(6) . . ? P1 Cr2 Cr1 54.55(5) . . ? P2 Cr2 Cr1 55.31(6) . . ? C15 C11 C12 108.5(5) . . ? C15 C11 C16 127.2(5) . . ? C12 C11 C16 124.1(5) . . ? C15 C11 Cr2 71.5(3) . . ? C12 C11 Cr2 71.9(3) . . ? C16 C11 Cr2 126.7(4) . . ? C13 C12 C11 107.6(5) . . ? C13 C12 C17 126.6(5) . . ? C11 C12 C17 125.6(5) . . ? C13 C12 Cr2 71.6(3) . . ? C11 C12 Cr2 70.3(3) . . ? C17 C12 Cr2 126.9(4) . . ? C12 C13 C14 108.3(5) . . ? C12 C13 C18 126.2(5) . . ? C14 C13 C18 125.4(5) . . ? C12 C13 Cr2 71.2(3) . . ? C14 C13 Cr2 70.6(3) . . ? C18 C13 Cr2 127.1(4) . . ? C13 C14 C15 108.3(5) . . ? C13 C14 C19 125.7(5) . . ? C15 C14 C19 125.8(5) . . ? C13 C14 Cr2 72.0(3) . . ? C15 C14 Cr2 71.1(3) . . ? C19 C14 Cr2 126.6(4) . . ? C11 C15 C14 107.3(5) . . ? C11 C15 C20 126.5(5) . . ? C14 C15 C20 126.1(5) . . ? C11 C15 Cr2 70.9(3) . . ? C14 C15 Cr2 71.1(3) . . ? C20 C15 Cr2 126.2(4) . . ? C11 C16 H16A 109.5 . . ? C11 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C11 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C25 C21 C22 107.3(5) . . ? C25 C21 C26 125.7(5) . . ? C22 C21 C26 126.9(5) . . ? C25 C21 Cr3 70.3(3) . . ? C22 C21 Cr3 71.2(3) . . ? C26 C21 Cr3 127.8(4) . . ? C23 C22 C21 107.0(5) . . ? C23 C22 C27 126.8(5) . . ? C21 C22 C27 125.9(5) . . ? C23 C22 Cr3 70.5(3) . . ? C21 C22 Cr3 71.3(3) . . ? C27 C22 Cr3 128.1(4) . . ? C24 C23 C22 110.0(5) . . ? C24 C23 C28 126.1(5) . . ? C22 C23 C28 123.7(5) . . ? C24 C23 Cr3 71.3(3) . . ? C22 C23 Cr3 72.4(3) . . ? C28 C23 Cr3 126.6(4) . . ? C23 C24 C25 107.0(5) . . ? C23 C24 C29 125.9(5) . . ? C25 C24 C29 126.7(5) . . ? C23 C24 Cr3 71.4(3) . . ? C25 C24 Cr3 71.4(3) . . ? C29 C24 Cr3 128.1(4) . . ? C24 C25 C21 108.7(5) . . ? C24 C25 C30 126.0(5) . . ? C21 C25 C30 125.1(5) . . ? C24 C25 Cr3 71.0(3) . . ? C21 C25 Cr3 72.1(3) . . ? C30 C25 Cr3 127.3(4) . . ? C21 C26 H26A 109.5 . . ? C21 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C21 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C22 C27 H27A 109.5 . . ? C22 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? C22 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? C23 C28 H28A 109.5 . . ? C23 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C23 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C24 C29 H29A 109.5 . . ? C24 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C24 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C25 C30 H30A 109.5 . . ? C25 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? C25 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C24 Cr3 C23 37.3(2) . . ? C24 Cr3 C25 37.5(2) . . ? C23 Cr3 C25 62.0(2) . . ? C24 Cr3 C22 62.8(2) . . ? C23 Cr3 C22 37.1(2) . . ? C25 Cr3 C22 62.6(2) . . ? C24 Cr3 C21 62.9(2) . . ? C23 Cr3 C21 62.1(2) . . ? C25 Cr3 C21 37.6(2) . . ? C22 Cr3 C21 37.5(2) . . ? C24 Cr3 P10 110.84(16) . . ? C23 Cr3 P10 148.08(16) . . ? C25 Cr3 P10 92.87(16) . . ? C22 Cr3 P10 148.00(16) . . ? C21 Cr3 P10 110.59(16) . . ? C24 Cr3 P9 92.04(16) . . ? C23 Cr3 P9 107.74(16) . . ? C25 Cr3 P9 113.17(16) . . ? C22 Cr3 P9 144.31(16) . . ? C21 Cr3 P9 150.71(17) . . ? P10 Cr3 P9 62.19(7) . . ? C24 Cr3 P8 113.75(17) . . ? C23 Cr3 P8 93.48(15) . . ? C25 Cr3 P8 151.23(17) . . ? C22 Cr3 P8 107.63(16) . . ? C21 Cr3 P8 144.54(17) . . ? P10 Cr3 P8 103.44(7) . . ? P9 Cr3 P8 57.49(6) . . ? C24 Cr3 P6 149.89(17) . . ? C23 Cr3 P6 148.11(16) . . ? C25 Cr3 P6 112.46(17) . . ? C22 Cr3 P6 111.13(17) . . ? C21 Cr3 P6 93.89(16) . . ? P10 Cr3 P6 57.16(7) . . ? P9 Cr3 P6 103.10(7) . . ? P8 Cr3 P6 96.30(8) . . ? C24 Cr3 P7 150.58(16) . . ? C23 Cr3 P7 113.40(16) . . ? C25 Cr3 P7 147.91(17) . . ? C22 Cr3 P7 94.16(17) . . ? C21 Cr3 P7 110.65(17) . . ? P10 Cr3 P7 98.36(7) . . ? P9 Cr3 P7 98.61(7) . . ? P8 Cr3 P7 53.20(6) . . ? P6 Cr3 P7 52.88(7) . . ? C24 Cr3 Cr4 144.53(15) . . ? C23 Cr3 Cr4 147.27(15) . . ? C25 Cr3 Cr4 145.72(16) . . ? C22 Cr3 Cr4 148.87(16) . . ? C21 Cr3 Cr4 148.16(16) . . ? P10 Cr3 Cr4 52.94(5) . . ? P9 Cr3 Cr4 52.73(5) . . ? P8 Cr3 Cr4 54.33(5) . . ? P6 Cr3 Cr4 54.37(5) . . ? P7 Cr3 Cr4 54.79(6) . . ? P7 P6 P10 109.75(9) . . ? P7 P6 Cr3 65.02(7) . . ? P10 P6 Cr3 59.60(6) . . ? P7 P6 Cr4 64.36(7) . . ? P10 P6 Cr4 59.71(7) . . ? Cr3 P6 Cr4 71.44(6) . . ? P6 P7 P8 110.81(9) . . ? P6 P7 Cr4 62.59(6) . . ? P8 P7 Cr4 62.38(7) . . ? P6 P7 Cr3 62.11(7) . . ? P8 P7 Cr3 61.91(7) . . ? Cr4 P7 Cr3 69.78(6) . . ? P7 P8 P9 109.29(9) . . ? P7 P8 Cr3 64.89(7) . . ? P9 P8 Cr3 59.56(7) . . ? P7 P8 Cr4 64.24(7) . . ? P9 P8 Cr4 59.37(7) . . ? Cr3 P8 Cr4 71.50(7) . . ? P8 P9 Cr4 63.15(7) . . ? P8 P9 Cr3 62.94(7) . . ? Cr4 P9 Cr3 74.41(6) . . ? P8 P9 P10 104.95(9) . . ? Cr4 P9 P10 59.07(6) . . ? Cr3 P9 P10 58.83(6) . . ? P6 P10 Cr3 63.25(7) . . ? P6 P10 Cr4 63.29(6) . . ? Cr3 P10 Cr4 74.34(7) . . ? P6 P10 P9 105.19(8) . . ? Cr3 P10 P9 58.98(7) . . ? Cr4 P10 P9 58.77(7) . . ? C31 Cr4 C34 62.7(2) . . ? C31 Cr4 C33 62.9(2) . . ? C34 Cr4 C33 37.3(2) . . ? C31 Cr4 C32 37.9(2) . . ? C34 Cr4 C32 62.7(2) . . ? C33 Cr4 C32 37.6(2) . . ? C31 Cr4 C35 37.3(2) . . ? C34 Cr4 C35 37.8(2) . . ? C33 Cr4 C35 62.8(2) . . ? C32 Cr4 C35 62.9(2) . . ? C31 Cr4 P9 137.43(16) . . ? C34 Cr4 P9 94.54(17) . . ? C33 Cr4 P9 120.53(16) . . ? C32 Cr4 P9 156.75(15) . . ? C35 Cr4 P9 102.71(17) . . ? C31 Cr4 P10 99.19(16) . . ? C34 Cr4 P10 123.44(17) . . ? C33 Cr4 P10 157.26(16) . . ? C32 Cr4 P10 133.26(16) . . ? C35 Cr4 P10 94.46(16) . . ? P9 Cr4 P10 62.16(7) . . ? C31 Cr4 P8 157.70(16) . . ? C34 Cr4 P8 104.65(16) . . ? C33 Cr4 P8 95.65(16) . . ? C32 Cr4 P8 120.74(16) . . ? C35 Cr4 P8 139.90(16) . . ? P9 Cr4 P8 57.48(6) . . ? P10 Cr4 P8 103.09(8) . . ? C31 Cr4 P6 95.23(16) . . ? C34 Cr4 P6 157.95(17) . . ? C33 Cr4 P6 134.05(16) . . ? C32 Cr4 P6 100.16(15) . . ? C35 Cr4 P6 123.52(16) . . ? P9 Cr4 P6 103.08(7) . . ? P10 Cr4 P6 57.00(7) . . ? P8 Cr4 P6 96.04(7) . . ? C31 Cr4 P7 122.14(16) . . ? C34 Cr4 P7 137.17(17) . . ? C33 Cr4 P7 102.81(16) . . ? C32 Cr4 P7 95.20(15) . . ? C35 Cr4 P7 157.77(17) . . ? P9 Cr4 P7 99.27(7) . . ? P10 Cr4 P7 98.70(7) . . ? P8 Cr4 P7 53.38(6) . . ? P6 Cr4 P7 53.05(7) . . ? C31 Cr4 Cr3 145.49(15) . . ? C34 Cr4 Cr3 146.53(16) . . ? C33 Cr4 Cr3 148.98(16) . . ? C32 Cr4 Cr3 148.28(15) . . ? C35 Cr4 Cr3 144.39(15) . . ? P9 Cr4 Cr3 52.87(6) . . ? P10 Cr4 Cr3 52.72(5) . . ? P8 Cr4 Cr3 54.17(5) . . ? P6 Cr4 Cr3 54.20(5) . . ? P7 Cr4 Cr3 55.42(5) . . ? C35 C31 C32 108.4(5) . . ? C35 C31 C36 125.3(5) . . ? C32 C31 C36 126.2(5) . . ? C35 C31 Cr4 71.9(3) . . ? C32 C31 Cr4 71.1(3) . . ? C36 C31 Cr4 125.2(4) . . ? C33 C32 C31 107.5(5) . . ? C33 C32 C37 126.8(5) . . ? C31 C32 C37 125.7(5) . . ? C33 C32 Cr4 71.2(3) . . ? C31 C32 Cr4 71.0(3) . . ? C37 C32 Cr4 125.7(4) . . ? C34 C33 C32 108.3(5) . . ? C34 C33 C38 125.1(5) . . ? C32 C33 C38 126.5(5) . . ? C34 C33 Cr4 71.3(3) . . ? C32 C33 Cr4 71.2(3) . . ? C38 C33 Cr4 127.0(4) . . ? C33 C34 C35 108.5(5) . . ? C33 C34 C39 125.2(5) . . ? C35 C34 C39 126.0(5) . . ? C33 C34 Cr4 71.4(3) . . ? C35 C34 Cr4 71.6(3) . . ? C39 C34 Cr4 128.2(4) . . ? C31 C35 C34 107.5(5) . . ? C31 C35 C40 127.5(5) . . ? C34 C35 C40 125.0(5) . . ? C31 C35 Cr4 70.8(3) . . ? C34 C35 Cr4 70.6(3) . . ? C40 C35 Cr4 126.3(4) . . ? C31 C36 H36A 109.5 . . ? C31 C36 H36B 109.5 . . ? H36A C36 H36B 109.5 . . ? C31 C36 H36C 109.5 . . ? H36A C36 H36C 109.5 . . ? H36B C36 H36C 109.5 . . ? C32 C37 H37A 109.5 . . ? C32 C37 H37B 109.5 . . ? H37A C37 H37B 109.5 . . ? C32 C37 H37C 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? C33 C38 H38A 109.5 . . ? C33 C38 H38B 109.5 . . ? H38A C38 H38B 109.5 . . ? C33 C38 H38C 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? C34 C39 H39A 109.5 . . ? C34 C39 H39B 109.5 . . ? H39A C39 H39B 109.5 . . ? C34 C39 H39C 109.5 . . ? H39A C39 H39C 109.5 . . ? H39B C39 H39C 109.5 . . ? C35 C40 H40A 109.5 . . ? C35 C40 H40B 109.5 . . ? H40A C40 H40B 109.5 . . ? C35 C40 H40C 109.5 . . ? H40A C40 H40C 109.5 . . ? H40B C40 H40C 109.5 . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 C1 C2 C3 1.3(6) . . . . ? C6 C1 C2 C3 175.6(5) . . . . ? Cr1 C1 C2 C3 -62.3(4) . . . . ? C5 C1 C2 C7 -175.9(5) . . . . ? C6 C1 C2 C7 -1.5(9) . . . . ? Cr1 C1 C2 C7 120.6(5) . . . . ? C5 C1 C2 Cr1 63.5(4) . . . . ? C6 C1 C2 Cr1 -122.1(6) . . . . ? C1 C2 C3 C4 -0.6(6) . . . . ? C7 C2 C3 C4 176.5(5) . . . . ? Cr1 C2 C3 C4 -62.3(4) . . . . ? C1 C2 C3 C8 -179.0(5) . . . . ? C7 C2 C3 C8 -1.9(9) . . . . ? Cr1 C2 C3 C8 119.3(6) . . . . ? C1 C2 C3 Cr1 61.7(4) . . . . ? C7 C2 C3 Cr1 -121.3(6) . . . . ? C2 C3 C4 C5 -0.3(6) . . . . ? C8 C3 C4 C5 178.1(5) . . . . ? Cr1 C3 C4 C5 -61.9(4) . . . . ? C2 C3 C4 C9 -176.0(5) . . . . ? C8 C3 C4 C9 2.4(9) . . . . ? Cr1 C3 C4 C9 122.4(6) . . . . ? C2 C3 C4 Cr1 61.6(4) . . . . ? C8 C3 C4 Cr1 -120.0(5) . . . . ? C2 C1 C5 C4 -1.5(6) . . . . ? C6 C1 C5 C4 -175.9(5) . . . . ? Cr1 C1 C5 C4 61.4(4) . . . . ? C2 C1 C5 C10 173.7(5) . . . . ? C6 C1 C5 C10 -0.7(9) . . . . ? Cr1 C1 C5 C10 -123.4(5) . . . . ? C2 C1 C5 Cr1 -62.9(4) . . . . ? C6 C1 C5 Cr1 122.8(6) . . . . ? C3 C4 C5 C1 1.1(6) . . . . ? C9 C4 C5 C1 176.8(5) . . . . ? Cr1 C4 C5 C1 -60.6(4) . . . . ? C3 C4 C5 C10 -174.0(5) . . . . ? C9 C4 C5 C10 1.7(9) . . . . ? Cr1 C4 C5 C10 124.3(6) . . . . ? C3 C4 C5 Cr1 61.7(4) . . . . ? C9 C4 C5 Cr1 -122.6(6) . . . . ? C5 C1 Cr1 C2 -116.0(5) . . . . ? C6 C1 Cr1 C2 122.0(6) . . . . ? C5 C1 Cr1 C3 -78.6(4) . . . . ? C2 C1 Cr1 C3 37.4(3) . . . . ? C6 C1 Cr1 C3 159.4(6) . . . . ? C2 C1 Cr1 C5 116.0(5) . . . . ? C6 C1 Cr1 C5 -122.0(6) . . . . ? C5 C1 Cr1 C4 -36.4(3) . . . . ? C2 C1 Cr1 C4 79.6(4) . . . . ? C6 C1 Cr1 C4 -158.4(6) . . . . ? C5 C1 Cr1 P5 50.8(4) . . . . ? C2 C1 Cr1 P5 166.8(3) . . . . ? C6 C1 Cr1 P5 -71.2(5) . . . . ? C5 C1 Cr1 P4 -40.2(6) . . . . ? C2 C1 Cr1 P4 75.8(5) . . . . ? C6 C1 Cr1 P4 -162.2(3) . . . . ? C5 C1 Cr1 P1 106.2(3) . . . . ? C2 C1 Cr1 P1 -137.7(3) . . . . ? C6 C1 Cr1 P1 -15.7(5) . . . . ? C5 C1 Cr1 P3 -150.7(3) . . . . ? C2 C1 Cr1 P3 -34.7(4) . . . . ? C6 C1 Cr1 P3 87.3(5) . . . . ? C5 C1 Cr1 P2 159.5(3) . . . . ? C2 C1 Cr1 P2 -84.4(3) . . . . ? C6 C1 Cr1 P2 37.6(5) . . . . ? C5 C1 Cr1 Cr2 119.3(3) . . . . ? C2 C1 Cr1 Cr2 -124.7(3) . . . . ? C6 C1 Cr1 Cr2 -2.7(7) . . . . ? C3 C2 Cr1 C1 117.3(5) . . . . ? C7 C2 Cr1 C1 -119.7(7) . . . . ? C1 C2 Cr1 C3 -117.3(5) . . . . ? C7 C2 Cr1 C3 123.0(7) . . . . ? C3 C2 Cr1 C5 79.4(4) . . . . ? C1 C2 Cr1 C5 -37.9(3) . . . . ? C7 C2 Cr1 C5 -157.6(6) . . . . ? C3 C2 Cr1 C4 37.1(3) . . . . ? C1 C2 Cr1 C4 -80.2(4) . . . . ? C7 C2 Cr1 C4 160.2(6) . . . . ? C3 C2 Cr1 P5 87.4(5) . . . . ? C1 C2 Cr1 P5 -29.9(6) . . . . ? C7 C2 Cr1 P5 -149.6(4) . . . . ? C3 C2 Cr1 P4 -33.1(4) . . . . ? C1 C2 Cr1 P4 -150.4(3) . . . . ? C7 C2 Cr1 P4 90.0(5) . . . . ? C3 C2 Cr1 P1 169.2(3) . . . . ? C1 C2 Cr1 P1 51.9(4) . . . . ? C7 C2 Cr1 P1 -67.8(5) . . . . ? C3 C2 Cr1 P3 -87.5(3) . . . . ? C1 C2 Cr1 P3 155.2(3) . . . . ? C7 C2 Cr1 P3 35.5(5) . . . . ? C3 C2 Cr1 P2 -141.0(3) . . . . ? C1 C2 Cr1 P2 101.7(3) . . . . ? C7 C2 Cr1 P2 -17.9(5) . . . . ? C3 C2 Cr1 Cr2 -118.7(4) . . . . ? C1 C2 Cr1 Cr2 124.0(3) . . . . ? C7 C2 Cr1 Cr2 4.3(7) . . . . ? C2 C3 Cr1 C1 -38.0(3) . . . . ? C4 C3 Cr1 C1 80.0(4) . . . . ? C8 C3 Cr1 C1 -160.0(6) . . . . ? C4 C3 Cr1 C2 118.0(5) . . . . ? C8 C3 Cr1 C2 -122.0(6) . . . . ? C2 C3 Cr1 C5 -80.2(4) . . . . ? C4 C3 Cr1 C5 37.8(3) . . . . ? C8 C3 Cr1 C5 157.8(6) . . . . ? C2 C3 Cr1 C4 -118.0(5) . . . . ? C8 C3 Cr1 C4 120.0(6) . . . . ? C2 C3 Cr1 P5 -145.8(3) . . . . ? C4 C3 Cr1 P5 -27.8(4) . . . . ? C8 C3 Cr1 P5 92.2(5) . . . . ? C2 C3 Cr1 P4 155.8(3) . . . . ? C4 C3 Cr1 P4 -86.2(3) . . . . ? C8 C3 Cr1 P4 33.8(5) . . . . ? C2 C3 Cr1 P1 -25.1(6) . . . . ? C4 C3 Cr1 P1 92.9(5) . . . . ? C8 C3 Cr1 P1 -147.0(4) . . . . ? C2 C3 Cr1 P3 97.9(3) . . . . ? C4 C3 Cr1 P3 -144.1(3) . . . . ? C8 C3 Cr1 P3 -24.1(5) . . . . ? C2 C3 Cr1 P2 48.8(4) . . . . ? C4 C3 Cr1 P2 166.8(3) . . . . ? C8 C3 Cr1 P2 -73.2(5) . . . . ? C2 C3 Cr1 Cr2 125.2(3) . . . . ? C4 C3 Cr1 Cr2 -116.8(3) . . . . ? C8 C3 Cr1 Cr2 3.3(7) . . . . ? C4 C5 Cr1 C1 -119.3(5) . . . . ? C10 C5 Cr1 C1 118.9(7) . . . . ? C1 C5 Cr1 C2 38.8(3) . . . . ? C4 C5 Cr1 C2 -80.5(4) . . . . ? C10 C5 Cr1 C2 157.7(6) . . . . ? C1 C5 Cr1 C3 81.4(4) . . . . ? C4 C5 Cr1 C3 -37.9(3) . . . . ? C10 C5 Cr1 C3 -159.6(6) . . . . ? C1 C5 Cr1 C4 119.3(5) . . . . ? C10 C5 Cr1 C4 -121.8(6) . . . . ? C1 C5 Cr1 P5 -138.1(3) . . . . ? C4 C5 Cr1 P5 102.6(3) . . . . ? C10 C5 Cr1 P5 -19.2(5) . . . . ? C1 C5 Cr1 P4 162.8(3) . . . . ? C4 C5 Cr1 P4 43.6(4) . . . . ? C10 C5 Cr1 P4 -78.2(5) . . . . ? C1 C5 Cr1 P1 -80.0(3) . . . . ? C4 C5 Cr1 P1 160.8(3) . . . . ? C10 C5 Cr1 P1 39.0(5) . . . . ? C1 C5 Cr1 P3 76.3(6) . . . . ? C4 C5 Cr1 P3 -42.9(6) . . . . ? C10 C5 Cr1 P3 -164.7(4) . . . . ? C1 C5 Cr1 P2 -29.6(4) . . . . ? C4 C5 Cr1 P2 -148.9(3) . . . . ? C10 C5 Cr1 P2 89.4(5) . . . . ? C1 C5 Cr1 Cr2 -124.3(3) . . . . ? C4 C5 Cr1 Cr2 116.4(3) . . . . ? C10 C5 Cr1 Cr2 -5.3(7) . . . . ? C5 C4 Cr1 C1 36.4(3) . . . . ? C3 C4 Cr1 C1 -80.4(4) . . . . ? C9 C4 Cr1 C1 158.9(6) . . . . ? C5 C4 Cr1 C2 79.5(4) . . . . ? C3 C4 Cr1 C2 -37.3(3) . . . . ? C9 C4 Cr1 C2 -158.0(6) . . . . ? C5 C4 Cr1 C3 116.8(5) . . . . ? C9 C4 Cr1 C3 -120.7(7) . . . . ? C3 C4 Cr1 C5 -116.8(5) . . . . ? C9 C4 Cr1 C5 122.5(7) . . . . ? C5 C4 Cr1 P5 -82.6(3) . . . . ? C3 C4 Cr1 P5 160.6(3) . . . . ? C9 C4 Cr1 P5 39.9(5) . . . . ? C5 C4 Cr1 P4 -145.0(3) . . . . ? C3 C4 Cr1 P4 98.2(3) . . . . ? C9 C4 Cr1 P4 -22.5(5) . . . . ? C5 C4 Cr1 P1 -28.7(4) . . . . ? C3 C4 Cr1 P1 -145.5(3) . . . . ? C9 C4 Cr1 P1 93.8(5) . . . . ? C5 C4 Cr1 P3 162.2(3) . . . . ? C3 C4 Cr1 P3 45.5(4) . . . . ? C9 C4 Cr1 P3 -75.3(5) . . . . ? C5 C4 Cr1 P2 84.8(5) . . . . ? C3 C4 Cr1 P2 -31.9(7) . . . . ? C9 C4 Cr1 P2 -152.7(4) . . . . ? C5 C4 Cr1 Cr2 -121.9(3) . . . . ? C3 C4 Cr1 Cr2 121.3(3) . . . . ? C9 C4 Cr1 Cr2 0.6(7) . . . . ? C1 Cr1 P1 P2 101.20(16) . . . . ? C2 Cr1 P1 P2 71.92(19) . . . . ? C3 Cr1 P1 P2 89.6(4) . . . . ? C5 Cr1 P1 P2 138.14(17) . . . . ? C4 Cr1 P1 P2 155.7(2) . . . . ? P5 Cr1 P1 P2 -135.29(9) . . . . ? P4 Cr1 P1 P2 -91.25(8) . . . . ? P3 Cr1 P1 P2 -33.35(8) . . . . ? Cr2 Cr1 P1 P2 -70.39(7) . . . . ? C1 Cr1 P1 P5 -123.51(16) . . . . ? C2 Cr1 P1 P5 -152.79(19) . . . . ? C3 Cr1 P1 P5 -135.1(4) . . . . ? C5 Cr1 P1 P5 -86.57(17) . . . . ? C4 Cr1 P1 P5 -69.1(2) . . . . ? P4 Cr1 P1 P5 44.04(8) . . . . ? P3 Cr1 P1 P5 101.94(8) . . . . ? P2 Cr1 P1 P5 135.29(9) . . . . ? Cr2 Cr1 P1 P5 64.90(7) . . . . ? C1 Cr1 P1 Cr2 171.59(15) . . . . ? C2 Cr1 P1 Cr2 142.31(19) . . . . ? C3 Cr1 P1 Cr2 160.0(4) . . . . ? C5 Cr1 P1 Cr2 -151.47(16) . . . . ? C4 Cr1 P1 Cr2 -134.0(2) . . . . ? P5 Cr1 P1 Cr2 -64.90(7) . . . . ? P4 Cr1 P1 Cr2 -20.86(7) . . . . ? P3 Cr1 P1 Cr2 37.04(6) . . . . ? P2 Cr1 P1 Cr2 70.39(7) . . . . ? P5 P1 P2 P3 0.85(12) . . . . ? Cr2 P1 P2 P3 -39.60(8) . . . . ? Cr1 P1 P2 P3 40.43(8) . . . . ? P5 P1 P2 Cr1 -39.58(7) . . . . ? Cr2 P1 P2 Cr1 -80.03(7) . . . . ? P5 P1 P2 Cr2 40.46(7) . . . . ? Cr1 P1 P2 Cr2 80.03(7) . . . . ? C1 Cr1 P2 P3 135.99(17) . . . . ? C2 Cr1 P2 P3 97.69(17) . . . . ? C3 Cr1 P2 P3 70.1(2) . . . . ? C5 Cr1 P2 P3 153.9(2) . . . . ? C4 Cr1 P2 P3 92.9(5) . . . . ? P5 Cr1 P2 P3 -99.59(8) . . . . ? P4 Cr1 P2 P3 -36.56(8) . . . . ? P1 Cr1 P2 P3 -136.83(9) . . . . ? Cr2 Cr1 P2 P3 -68.41(7) . . . . ? C1 Cr1 P2 P1 -87.17(17) . . . . ? C2 Cr1 P2 P1 -125.48(17) . . . . ? C3 Cr1 P2 P1 -153.0(2) . . . . ? C5 Cr1 P2 P1 -69.3(2) . . . . ? C4 Cr1 P2 P1 -130.2(5) . . . . ? P5 Cr1 P2 P1 37.24(8) . . . . ? P4 Cr1 P2 P1 100.28(9) . . . . ? P3 Cr1 P2 P1 136.83(9) . . . . ? Cr2 Cr1 P2 P1 68.43(7) . . . . ? C1 Cr1 P2 Cr2 -155.60(16) . . . . ? C2 Cr1 P2 Cr2 166.10(17) . . . . ? C3 Cr1 P2 Cr2 138.55(19) . . . . ? C5 Cr1 P2 Cr2 -137.7(2) . . . . ? C4 Cr1 P2 Cr2 161.3(5) . . . . ? P5 Cr1 P2 Cr2 -31.18(7) . . . . ? P4 Cr1 P2 Cr2 31.85(6) . . . . ? P1 Cr1 P2 Cr2 -68.43(7) . . . . ? P3 Cr1 P2 Cr2 68.41(7) . . . . ? P1 P2 P3 P4 -0.65(12) . . . . ? Cr1 P2 P3 P4 39.73(8) . . . . ? Cr2 P2 P3 P4 -40.25(7) . . . . ? P1 P2 P3 Cr2 39.60(8) . . . . ? Cr1 P2 P3 Cr2 79.98(6) . . . . ? P1 P2 P3 Cr1 -40.38(8) . . . . ? Cr2 P2 P3 Cr1 -79.98(6) . . . . ? C1 Cr1 P3 P2 -69.2(2) . . . . ? C2 Cr1 P3 P2 -90.11(17) . . . . ? C3 Cr1 P3 P2 -128.01(16) . . . . ? C5 Cr1 P3 P2 -123.5(4) . . . . ? C4 Cr1 P3 P2 -153.93(19) . . . . ? P5 Cr1 P3 P2 91.94(8) . . . . ? P4 Cr1 P3 P2 135.74(9) . . . . ? P1 Cr1 P3 P2 33.40(7) . . . . ? Cr2 Cr1 P3 P2 70.46(7) . . . . ? C1 Cr1 P3 P4 155.1(2) . . . . ? C2 Cr1 P3 P4 134.15(17) . . . . ? C3 Cr1 P3 P4 96.24(17) . . . . ? C5 Cr1 P3 P4 100.8(4) . . . . ? C4 Cr1 P3 P4 70.33(19) . . . . ? P5 Cr1 P3 P4 -43.80(8) . . . . ? P1 Cr1 P3 P4 -102.35(9) . . . . ? P2 Cr1 P3 P4 -135.74(9) . . . . ? Cr2 Cr1 P3 P4 -65.28(7) . . . . ? C1 Cr1 P3 Cr2 -139.6(2) . . . . ? C2 Cr1 P3 Cr2 -160.57(17) . . . . ? C3 Cr1 P3 Cr2 161.52(16) . . . . ? C5 Cr1 P3 Cr2 166.0(4) . . . . ? C4 Cr1 P3 Cr2 135.61(19) . . . . ? P5 Cr1 P3 Cr2 21.48(7) . . . . ? P4 Cr1 P3 Cr2 65.28(7) . . . . ? P1 Cr1 P3 Cr2 -37.07(7) . . . . ? P2 Cr1 P3 Cr2 -70.46(7) . . . . ? P2 P3 P4 Cr2 42.68(8) . . . . ? Cr1 P3 P4 Cr2 84.76(7) . . . . ? P2 P3 P4 Cr1 -42.08(8) . . . . ? Cr2 P3 P4 Cr1 -84.76(7) . . . . ? P2 P3 P4 P5 0.19(11) . . . . ? Cr2 P3 P4 P5 -42.49(7) . . . . ? Cr1 P3 P4 P5 42.27(7) . . . . ? C1 Cr1 P4 P3 -126.0(4) . . . . ? C2 Cr1 P4 P3 -72.1(2) . . . . ? C3 Cr1 P4 P3 -91.83(16) . . . . ? C5 Cr1 P4 P3 -154.30(19) . . . . ? C4 Cr1 P4 P3 -129.43(16) . . . . ? P5 Cr1 P4 P3 130.36(8) . . . . ? P1 Cr1 P4 P3 88.50(8) . . . . ? P2 Cr1 P4 P3 34.39(7) . . . . ? Cr2 Cr1 P4 P3 67.29(7) . . . . ? C1 Cr1 P4 Cr2 166.7(4) . . . . ? C2 Cr1 P4 Cr2 -139.4(2) . . . . ? C3 Cr1 P4 Cr2 -159.12(16) . . . . ? C5 Cr1 P4 Cr2 138.41(19) . . . . ? C4 Cr1 P4 Cr2 163.28(16) . . . . ? P5 Cr1 P4 Cr2 63.07(7) . . . . ? P1 Cr1 P4 Cr2 21.21(7) . . . . ? P3 Cr1 P4 Cr2 -67.29(7) . . . . ? P2 Cr1 P4 Cr2 -32.90(6) . . . . ? C1 Cr1 P4 P5 103.6(4) . . . . ? C2 Cr1 P4 P5 157.5(2) . . . . ? C3 Cr1 P4 P5 137.81(17) . . . . ? C5 Cr1 P4 P5 75.34(19) . . . . ? C4 Cr1 P4 P5 100.21(16) . . . . ? P1 Cr1 P4 P5 -41.86(8) . . . . ? P3 Cr1 P4 P5 -130.36(8) . . . . ? P2 Cr1 P4 P5 -95.97(8) . . . . ? Cr2 Cr1 P4 P5 -63.07(7) . . . . ? P2 P1 P5 Cr1 42.27(8) . . . . ? Cr2 P1 P5 Cr1 85.36(6) . . . . ? P2 P1 P5 Cr2 -43.08(8) . . . . ? Cr1 P1 P5 Cr2 -85.36(6) . . . . ? P2 P1 P5 P4 -0.70(11) . . . . ? Cr2 P1 P5 P4 42.39(7) . . . . ? Cr1 P1 P5 P4 -42.97(7) . . . . ? C1 Cr1 P5 P1 75.22(19) . . . . ? C2 Cr1 P5 P1 96.3(4) . . . . ? C3 Cr1 P5 P1 157.5(2) . . . . ? C5 Cr1 P5 P1 103.42(17) . . . . ? C4 Cr1 P5 P1 140.64(17) . . . . ? P4 Cr1 P5 P1 -130.16(9) . . . . ? P3 Cr1 P5 P1 -88.87(9) . . . . ? P2 Cr1 P5 P1 -34.80(7) . . . . ? Cr2 Cr1 P5 P1 -67.02(7) . . . . ? C1 Cr1 P5 Cr2 142.24(18) . . . . ? C2 Cr1 P5 Cr2 163.3(4) . . . . ? C3 Cr1 P5 Cr2 -135.5(2) . . . . ? C5 Cr1 P5 Cr2 170.45(16) . . . . ? C4 Cr1 P5 Cr2 -152.33(17) . . . . ? P4 Cr1 P5 Cr2 -63.13(6) . . . . ? P1 Cr1 P5 Cr2 67.02(7) . . . . ? P3 Cr1 P5 Cr2 -21.84(7) . . . . ? P2 Cr1 P5 Cr2 32.23(7) . . . . ? C1 Cr1 P5 P4 -154.63(19) . . . . ? C2 Cr1 P5 P4 -133.6(4) . . . . ? C3 Cr1 P5 P4 -72.3(2) . . . . ? C5 Cr1 P5 P4 -126.42(16) . . . . ? C4 Cr1 P5 P4 -89.20(17) . . . . ? P1 Cr1 P5 P4 130.16(9) . . . . ? P3 Cr1 P5 P4 41.29(8) . . . . ? P2 Cr1 P5 P4 95.36(8) . . . . ? Cr2 Cr1 P5 P4 63.13(6) . . . . ? P3 P4 P5 P1 0.30(10) . . . . ? Cr2 P4 P5 P1 -44.27(7) . . . . ? Cr1 P4 P5 P1 44.98(7) . . . . ? P3 P4 P5 Cr1 -44.67(7) . . . . ? Cr2 P4 P5 Cr1 -89.25(7) . . . . ? P3 P4 P5 Cr2 44.57(8) . . . . ? Cr1 P4 P5 Cr2 89.25(7) . . . . ? P1 P5 Cr2 C11 -77.32(19) . . . . ? Cr1 P5 Cr2 C11 -144.79(18) . . . . ? P4 P5 Cr2 C11 151.89(18) . . . . ? P1 P5 Cr2 C14 -143.76(17) . . . . ? Cr1 P5 Cr2 C14 148.77(17) . . . . ? P4 P5 Cr2 C14 85.45(17) . . . . ? P1 P5 Cr2 C15 -107.42(17) . . . . ? Cr1 P5 Cr2 C15 -174.88(16) . . . . ? P4 P5 Cr2 C15 121.80(17) . . . . ? P1 P5 Cr2 C12 -87.6(4) . . . . ? Cr1 P5 Cr2 C12 -155.0(4) . . . . ? P4 P5 Cr2 C12 141.6(4) . . . . ? P1 P5 Cr2 C13 -155.6(2) . . . . ? Cr1 P5 Cr2 C13 136.9(2) . . . . ? P4 P5 Cr2 C13 73.6(2) . . . . ? P1 P5 Cr2 P4 130.79(9) . . . . ? Cr1 P5 Cr2 P4 63.32(7) . . . . ? P1 P5 Cr2 P3 89.40(8) . . . . ? Cr1 P5 Cr2 P3 21.93(8) . . . . ? P4 P5 Cr2 P3 -41.39(8) . . . . ? Cr1 P5 Cr2 P1 -67.46(7) . . . . ? P4 P5 Cr2 P1 -130.79(9) . . . . ? P1 P5 Cr2 P2 35.32(7) . . . . ? Cr1 P5 Cr2 P2 -32.14(7) . . . . ? P4 P5 Cr2 P2 -95.46(9) . . . . ? P1 P5 Cr2 Cr1 67.46(7) . . . . ? P4 P5 Cr2 Cr1 -63.32(7) . . . . ? P3 P4 Cr2 C11 136.5(4) . . . . ? Cr1 P4 Cr2 C11 -155.8(4) . . . . ? P5 P4 Cr2 C11 -93.2(4) . . . . ? P3 P4 Cr2 C14 124.90(16) . . . . ? Cr1 P4 Cr2 C14 -167.45(16) . . . . ? P5 P4 Cr2 C14 -104.78(16) . . . . ? P3 P4 Cr2 C15 153.58(19) . . . . ? Cr1 P4 Cr2 C15 -138.78(18) . . . . ? P5 P4 Cr2 C15 -76.11(19) . . . . ? P3 P4 Cr2 C12 73.3(2) . . . . ? Cr1 P4 Cr2 C12 140.9(2) . . . . ? P5 P4 Cr2 C12 -156.4(2) . . . . ? P3 P4 Cr2 C13 88.28(17) . . . . ? Cr1 P4 Cr2 C13 155.92(16) . . . . ? P5 P4 Cr2 C13 -141.41(16) . . . . ? P3 P4 Cr2 P5 -130.31(9) . . . . ? Cr1 P4 Cr2 P5 -62.67(6) . . . . ? Cr1 P4 Cr2 P3 67.64(7) . . . . ? P5 P4 Cr2 P3 130.31(9) . . . . ? P3 P4 Cr2 P1 -88.93(8) . . . . ? Cr1 P4 Cr2 P1 -21.28(7) . . . . ? P5 P4 Cr2 P1 41.39(7) . . . . ? P3 P4 Cr2 P2 -34.79(7) . . . . ? Cr1 P4 Cr2 P2 32.85(7) . . . . ? P5 P4 Cr2 P2 95.52(7) . . . . ? P3 P4 Cr2 Cr1 -67.64(7) . . . . ? P5 P4 Cr2 Cr1 62.67(6) . . . . ? P2 P3 Cr2 C11 70.6(2) . . . . ? P4 P3 Cr2 C11 -154.2(2) . . . . ? Cr1 P3 Cr2 C11 140.7(2) . . . . ? P2 P3 Cr2 C14 152.73(19) . . . . ? P4 P3 Cr2 C14 -72.05(19) . . . . ? Cr1 P3 Cr2 C14 -137.14(18) . . . . ? P2 P3 Cr2 C15 136.4(4) . . . . ? P4 P3 Cr2 C15 -88.4(4) . . . . ? Cr1 P3 Cr2 C15 -153.4(4) . . . . ? P2 P3 Cr2 C12 87.15(17) . . . . ? P4 P3 Cr2 C12 -137.64(17) . . . . ? Cr1 P3 Cr2 C12 157.27(16) . . . . ? P2 P3 Cr2 C13 123.91(17) . . . . ? P4 P3 Cr2 C13 -100.88(17) . . . . ? Cr1 P3 Cr2 C13 -165.97(16) . . . . ? P2 P3 Cr2 P5 -91.48(8) . . . . ? P4 P3 Cr2 P5 43.74(8) . . . . ? Cr1 P3 Cr2 P5 -21.36(7) . . . . ? P2 P3 Cr2 P4 -135.21(9) . . . . ? Cr1 P3 Cr2 P4 -65.09(7) . . . . ? P2 P3 Cr2 P1 -32.91(8) . . . . ? P4 P3 Cr2 P1 102.30(8) . . . . ? Cr1 P3 Cr2 P1 37.21(7) . . . . ? P4 P3 Cr2 P2 135.21(9) . . . . ? Cr1 P3 Cr2 P2 70.12(7) . . . . ? P2 P3 Cr2 Cr1 -70.12(7) . . . . ? P4 P3 Cr2 Cr1 65.09(7) . . . . ? P2 P1 Cr2 C11 -106.53(17) . . . . ? P5 P1 Cr2 C11 118.97(17) . . . . ? Cr1 P1 Cr2 C11 -176.67(16) . . . . ? P2 P1 Cr2 C14 -155.1(3) . . . . ? P5 P1 Cr2 C14 70.4(3) . . . . ? Cr1 P1 Cr2 C14 134.7(3) . . . . ? P2 P1 Cr2 C15 -142.82(17) . . . . ? P5 P1 Cr2 C15 82.69(17) . . . . ? Cr1 P1 Cr2 C15 147.04(16) . . . . ? P2 P1 Cr2 C12 -75.31(19) . . . . ? P5 P1 Cr2 C12 150.19(18) . . . . ? Cr1 P1 Cr2 C12 -145.46(17) . . . . ? P2 P1 Cr2 C13 -82.7(4) . . . . ? P5 P1 Cr2 C13 142.8(4) . . . . ? Cr1 P1 Cr2 C13 -152.8(4) . . . . ? P2 P1 Cr2 P5 134.50(9) . . . . ? Cr1 P1 Cr2 P5 64.36(6) . . . . ? P2 P1 Cr2 P4 91.02(9) . . . . ? P5 P1 Cr2 P4 -43.48(8) . . . . ? Cr1 P1 Cr2 P4 20.87(7) . . . . ? P2 P1 Cr2 P3 32.89(8) . . . . ? P5 P1 Cr2 P3 -101.61(8) . . . . ? Cr1 P1 Cr2 P3 -37.25(7) . . . . ? P5 P1 Cr2 P2 -134.50(9) . . . . ? Cr1 P1 Cr2 P2 -70.14(7) . . . . ? P2 P1 Cr2 Cr1 70.14(7) . . . . ? P5 P1 Cr2 Cr1 -64.36(6) . . . . ? P3 P2 Cr2 C11 -139.19(18) . . . . ? P1 P2 Cr2 C11 83.22(18) . . . . ? Cr1 P2 Cr2 C11 151.95(17) . . . . ? P3 P2 Cr2 C14 -82.4(4) . . . . ? P1 P2 Cr2 C14 140.0(4) . . . . ? Cr1 P2 Cr2 C14 -151.3(4) . . . . ? P3 P2 Cr2 C15 -154.7(3) . . . . ? P1 P2 Cr2 C15 67.7(3) . . . . ? Cr1 P2 Cr2 C15 136.5(2) . . . . ? P3 P2 Cr2 C12 -102.06(17) . . . . ? P1 P2 Cr2 C12 120.35(17) . . . . ? Cr1 P2 Cr2 C12 -170.92(16) . . . . ? P3 P2 Cr2 C13 -72.18(18) . . . . ? P1 P2 Cr2 C13 150.24(18) . . . . ? Cr1 P2 Cr2 C13 -141.04(18) . . . . ? P3 P2 Cr2 P5 99.82(8) . . . . ? P1 P2 Cr2 P5 -37.76(8) . . . . ? Cr1 P2 Cr2 P5 30.96(6) . . . . ? P3 P2 Cr2 P4 37.01(8) . . . . ? P1 P2 Cr2 P4 -100.57(9) . . . . ? Cr1 P2 Cr2 P4 -31.85(7) . . . . ? P1 P2 Cr2 P3 -137.59(9) . . . . ? Cr1 P2 Cr2 P3 -68.86(7) . . . . ? P3 P2 Cr2 P1 137.59(9) . . . . ? Cr1 P2 Cr2 P1 68.72(7) . . . . ? P3 P2 Cr2 Cr1 68.86(7) . . . . ? P1 P2 Cr2 Cr1 -68.72(7) . . . . ? C1 Cr1 Cr2 C11 -9.7(4) . . . . ? C2 Cr1 Cr2 C11 -87.2(4) . . . . ? C3 Cr1 Cr2 C11 -160.3(4) . . . . ? C5 Cr1 Cr2 C11 63.0(4) . . . . ? C4 Cr1 Cr2 C11 131.4(4) . . . . ? P5 Cr1 Cr2 C11 80.3(3) . . . . ? P4 Cr1 Cr2 C11 160.7(3) . . . . ? P1 Cr1 Cr2 C11 6.3(3) . . . . ? P3 Cr1 Cr2 C11 -126.1(3) . . . . ? P2 Cr1 Cr2 C11 -59.9(3) . . . . ? C1 Cr1 Cr2 C14 -148.8(4) . . . . ? C2 Cr1 Cr2 C14 133.7(4) . . . . ? C3 Cr1 Cr2 C14 60.6(4) . . . . ? C5 Cr1 Cr2 C14 -76.0(4) . . . . ? C4 Cr1 Cr2 C14 -7.7(4) . . . . ? P5 Cr1 Cr2 C14 -58.7(3) . . . . ? P4 Cr1 Cr2 C14 21.7(3) . . . . ? P1 Cr1 Cr2 C14 -132.7(3) . . . . ? P3 Cr1 Cr2 C14 94.8(3) . . . . ? P2 Cr1 Cr2 C14 161.0(3) . . . . ? C1 Cr1 Cr2 C15 -81.2(4) . . . . ? C2 Cr1 Cr2 C15 -158.6(4) . . . . ? C3 Cr1 Cr2 C15 128.2(4) . . . . ? C5 Cr1 Cr2 C15 -8.4(4) . . . . ? C4 Cr1 Cr2 C15 60.0(4) . . . . ? P5 Cr1 Cr2 C15 8.9(3) . . . . ? P4 Cr1 Cr2 C15 89.3(3) . . . . ? P1 Cr1 Cr2 C15 -65.1(3) . . . . ? P3 Cr1 Cr2 C15 162.4(3) . . . . ? P2 Cr1 Cr2 C15 -131.4(3) . . . . ? C1 Cr1 Cr2 C12 68.3(4) . . . . ? C2 Cr1 Cr2 C12 -9.2(5) . . . . ? C3 Cr1 Cr2 C12 -82.3(4) . . . . ? C5 Cr1 Cr2 C12 141.0(4) . . . . ? C4 Cr1 Cr2 C12 -150.6(4) . . . . ? P5 Cr1 Cr2 C12 158.4(3) . . . . ? P4 Cr1 Cr2 C12 -121.3(3) . . . . ? P1 Cr1 Cr2 C12 84.4(3) . . . . ? P3 Cr1 Cr2 C12 -48.1(3) . . . . ? P2 Cr1 Cr2 C12 18.1(3) . . . . ? C1 Cr1 Cr2 C13 142.6(4) . . . . ? C2 Cr1 Cr2 C13 65.2(4) . . . . ? C3 Cr1 Cr2 C13 -8.0(4) . . . . ? C5 Cr1 Cr2 C13 -144.6(4) . . . . ? C4 Cr1 Cr2 C13 -76.2(4) . . . . ? P5 Cr1 Cr2 C13 -127.3(3) . . . . ? P4 Cr1 Cr2 C13 -46.9(3) . . . . ? P1 Cr1 Cr2 C13 158.7(3) . . . . ? P3 Cr1 Cr2 C13 26.2(3) . . . . ? P2 Cr1 Cr2 C13 92.4(3) . . . . ? C1 Cr1 Cr2 P5 -90.1(3) . . . . ? C2 Cr1 Cr2 P5 -167.5(3) . . . . ? C3 Cr1 Cr2 P5 119.3(3) . . . . ? C5 Cr1 Cr2 P5 -17.3(3) . . . . ? C4 Cr1 Cr2 P5 51.1(3) . . . . ? P4 Cr1 Cr2 P5 80.37(9) . . . . ? P1 Cr1 Cr2 P5 -74.00(8) . . . . ? P3 Cr1 Cr2 P5 153.53(9) . . . . ? P2 Cr1 Cr2 P5 -140.29(9) . . . . ? C1 Cr1 Cr2 P4 -170.4(3) . . . . ? C2 Cr1 Cr2 P4 112.1(3) . . . . ? C3 Cr1 Cr2 P4 39.0(3) . . . . ? C5 Cr1 Cr2 P4 -97.7(3) . . . . ? C4 Cr1 Cr2 P4 -29.3(3) . . . . ? P5 Cr1 Cr2 P4 -80.37(9) . . . . ? P1 Cr1 Cr2 P4 -154.37(9) . . . . ? P3 Cr1 Cr2 P4 73.16(9) . . . . ? P2 Cr1 Cr2 P4 139.34(9) . . . . ? C1 Cr1 Cr2 P3 116.4(3) . . . . ? C2 Cr1 Cr2 P3 38.9(3) . . . . ? C3 Cr1 Cr2 P3 -34.2(3) . . . . ? C5 Cr1 Cr2 P3 -170.9(3) . . . . ? C4 Cr1 Cr2 P3 -102.5(3) . . . . ? P5 Cr1 Cr2 P3 -153.53(9) . . . . ? P4 Cr1 Cr2 P3 -73.16(9) . . . . ? P1 Cr1 Cr2 P3 132.48(9) . . . . ? P2 Cr1 Cr2 P3 66.18(9) . . . . ? C1 Cr1 Cr2 P1 -16.1(3) . . . . ? C2 Cr1 Cr2 P1 -93.5(3) . . . . ? C3 Cr1 Cr2 P1 -166.7(3) . . . . ? C5 Cr1 Cr2 P1 56.7(3) . . . . ? C4 Cr1 Cr2 P1 125.0(3) . . . . ? P5 Cr1 Cr2 P1 74.00(8) . . . . ? P4 Cr1 Cr2 P1 154.37(9) . . . . ? P3 Cr1 Cr2 P1 -132.48(9) . . . . ? P2 Cr1 Cr2 P1 -66.29(8) . . . . ? C1 Cr1 Cr2 P2 50.2(3) . . . . ? C2 Cr1 Cr2 P2 -27.3(3) . . . . ? C3 Cr1 Cr2 P2 -100.4(3) . . . . ? C5 Cr1 Cr2 P2 123.0(3) . . . . ? C4 Cr1 Cr2 P2 -168.7(3) . . . . ? P5 Cr1 Cr2 P2 140.29(9) . . . . ? P4 Cr1 Cr2 P2 -139.34(9) . . . . ? P1 Cr1 Cr2 P2 66.29(8) . . . . ? P3 Cr1 Cr2 P2 -66.18(9) . . . . ? C14 Cr2 C11 C15 37.9(3) . . . . ? C12 Cr2 C11 C15 117.4(5) . . . . ? C13 Cr2 C11 C15 80.2(4) . . . . ? P5 Cr2 C11 C15 -55.2(4) . . . . ? P4 Cr2 C11 C15 24.9(6) . . . . ? P3 Cr2 C11 C15 144.4(3) . . . . ? P1 Cr2 C11 C15 -111.2(3) . . . . ? P2 Cr2 C11 C15 -164.0(3) . . . . ? Cr1 Cr2 C11 C15 -116.4(4) . . . . ? C14 Cr2 C11 C12 -79.5(4) . . . . ? C15 Cr2 C11 C12 -117.4(5) . . . . ? C13 Cr2 C11 C12 -37.2(3) . . . . ? P5 Cr2 C11 C12 -172.6(3) . . . . ? P4 Cr2 C11 C12 -92.6(5) . . . . ? P3 Cr2 C11 C12 26.9(4) . . . . ? P1 Cr2 C11 C12 131.4(3) . . . . ? P2 Cr2 C11 C12 78.5(3) . . . . ? Cr1 Cr2 C11 C12 126.2(3) . . . . ? C14 Cr2 C11 C16 161.1(6) . . . . ? C15 Cr2 C11 C16 123.1(7) . . . . ? C12 Cr2 C11 C16 -119.5(6) . . . . ? C13 Cr2 C11 C16 -156.7(6) . . . . ? P5 Cr2 C11 C16 67.9(5) . . . . ? P4 Cr2 C11 C16 148.0(4) . . . . ? P3 Cr2 C11 C16 -92.5(5) . . . . ? P1 Cr2 C11 C16 11.9(5) . . . . ? P2 Cr2 C11 C16 -40.9(5) . . . . ? Cr1 Cr2 C11 C16 6.7(7) . . . . ? C15 C11 C12 C13 -0.3(6) . . . . ? C16 C11 C12 C13 -175.2(5) . . . . ? Cr2 C11 C12 C13 62.3(4) . . . . ? C15 C11 C12 C17 175.6(5) . . . . ? C16 C11 C12 C17 0.7(9) . . . . ? Cr2 C11 C12 C17 -121.8(5) . . . . ? C15 C11 C12 Cr2 -62.6(4) . . . . ? C16 C11 C12 Cr2 122.5(5) . . . . ? C11 Cr2 C12 C13 -117.2(5) . . . . ? C14 Cr2 C12 C13 -37.1(3) . . . . ? C15 Cr2 C12 C13 -79.8(4) . . . . ? P5 Cr2 C12 C13 -102.2(4) . . . . ? P4 Cr2 C12 C13 24.8(4) . . . . ? P3 Cr2 C12 C13 80.9(3) . . . . ? P1 Cr2 C12 C13 -174.7(3) . . . . ? P2 Cr2 C12 C13 134.2(3) . . . . ? Cr1 Cr2 C12 C13 119.4(3) . . . . ? C14 Cr2 C12 C11 80.1(4) . . . . ? C15 Cr2 C12 C11 37.4(3) . . . . ? C13 Cr2 C12 C11 117.2(5) . . . . ? P5 Cr2 C12 C11 15.0(6) . . . . ? P4 Cr2 C12 C11 142.1(3) . . . . ? P3 Cr2 C12 C11 -161.9(3) . . . . ? P1 Cr2 C12 C11 -57.5(3) . . . . ? P2 Cr2 C12 C11 -108.5(3) . . . . ? Cr1 Cr2 C12 C11 -123.4(3) . . . . ? C11 Cr2 C12 C17 120.3(7) . . . . ? C14 Cr2 C12 C17 -159.6(6) . . . . ? C15 Cr2 C12 C17 157.7(6) . . . . ? C13 Cr2 C12 C17 -122.5(7) . . . . ? P5 Cr2 C12 C17 135.4(4) . . . . ? P4 Cr2 C12 C17 -97.6(5) . . . . ? P3 Cr2 C12 C17 -41.6(5) . . . . ? P1 Cr2 C12 C17 62.8(5) . . . . ? P2 Cr2 C12 C17 11.8(5) . . . . ? Cr1 Cr2 C12 C17 -3.1(7) . . . . ? C11 C12 C13 C14 -0.3(6) . . . . ? C17 C12 C13 C14 -176.1(5) . . . . ? Cr2 C12 C13 C14 61.2(4) . . . . ? C11 C12 C13 C18 175.8(5) . . . . ? C17 C12 C13 C18 0.0(9) . . . . ? Cr2 C12 C13 C18 -122.7(5) . . . . ? C11 C12 C13 Cr2 -61.4(4) . . . . ? C17 C12 C13 Cr2 122.7(6) . . . . ? C11 Cr2 C13 C12 37.9(3) . . . . ? C14 Cr2 C13 C12 118.1(5) . . . . ? C15 Cr2 C13 C12 80.4(4) . . . . ? P5 Cr2 C13 C12 137.3(3) . . . . ? P4 Cr2 C13 C12 -162.9(3) . . . . ? P3 Cr2 C13 C12 -105.0(3) . . . . ? P1 Cr2 C13 C12 10.9(6) . . . . ? P2 Cr2 C13 C12 -55.2(4) . . . . ? Cr1 Cr2 C13 C12 -126.2(3) . . . . ? C11 Cr2 C13 C14 -80.2(4) . . . . ? C15 Cr2 C13 C14 -37.7(3) . . . . ? C12 Cr2 C13 C14 -118.1(5) . . . . ? P5 Cr2 C13 C14 19.2(4) . . . . ? P4 Cr2 C13 C14 79.0(3) . . . . ? P3 Cr2 C13 C14 136.8(3) . . . . ? P1 Cr2 C13 C14 -107.2(4) . . . . ? P2 Cr2 C13 C14 -173.3(3) . . . . ? Cr1 Cr2 C13 C14 115.6(3) . . . . ? C11 Cr2 C13 C18 159.5(6) . . . . ? C14 Cr2 C13 C18 -120.3(7) . . . . ? C15 Cr2 C13 C18 -158.0(6) . . . . ? C12 Cr2 C13 C18 121.6(7) . . . . ? P5 Cr2 C13 C18 -101.1(5) . . . . ? P4 Cr2 C13 C18 -41.2(5) . . . . ? P3 Cr2 C13 C18 16.6(5) . . . . ? P1 Cr2 C13 C18 132.5(4) . . . . ? P2 Cr2 C13 C18 66.4(5) . . . . ? Cr1 Cr2 C13 C18 -4.6(7) . . . . ? C12 C13 C14 C15 0.7(6) . . . . ? C18 C13 C14 C15 -175.5(5) . . . . ? Cr2 C13 C14 C15 62.2(4) . . . . ? C12 C13 C14 C19 175.8(5) . . . . ? C18 C13 C14 C19 -0.3(9) . . . . ? Cr2 C13 C14 C19 -122.6(5) . . . . ? C12 C13 C14 Cr2 -61.6(4) . . . . ? C18 C13 C14 Cr2 122.3(5) . . . . ? C11 Cr2 C14 C13 79.7(4) . . . . ? C15 Cr2 C14 C13 117.4(5) . . . . ? C12 Cr2 C14 C13 36.9(3) . . . . ? P5 Cr2 C14 C13 -167.5(3) . . . . ? P4 Cr2 C14 C13 -105.8(3) . . . . ? P3 Cr2 C14 C13 -52.3(4) . . . . ? P1 Cr2 C14 C13 136.9(3) . . . . ? P2 Cr2 C14 C13 14.7(6) . . . . ? Cr1 Cr2 C14 C13 -123.0(3) . . . . ? C11 Cr2 C14 C15 -37.7(3) . . . . ? C12 Cr2 C14 C15 -80.5(4) . . . . ? C13 Cr2 C14 C15 -117.4(5) . . . . ? P5 Cr2 C14 C15 75.0(3) . . . . ? P4 Cr2 C14 C15 136.8(3) . . . . ? P3 Cr2 C14 C15 -169.7(3) . . . . ? P1 Cr2 C14 C15 19.5(5) . . . . ? P2 Cr2 C14 C15 -102.7(5) . . . . ? Cr1 Cr2 C14 C15 119.6(3) . . . . ? C11 Cr2 C14 C19 -158.8(6) . . . . ? C15 Cr2 C14 C19 -121.0(6) . . . . ? C12 Cr2 C14 C19 158.4(6) . . . . ? C13 Cr2 C14 C19 121.6(6) . . . . ? P5 Cr2 C14 C19 -46.0(5) . . . . ? P4 Cr2 C14 C19 15.7(5) . . . . ? P3 Cr2 C14 C19 69.2(5) . . . . ? P1 Cr2 C14 C19 -101.5(5) . . . . ? P2 Cr2 C14 C19 136.3(4) . . . . ? Cr1 Cr2 C14 C19 -1.5(7) . . . . ? C12 C11 C15 C14 0.7(6) . . . . ? C16 C11 C15 C14 175.4(5) . . . . ? Cr2 C11 C15 C14 -62.1(4) . . . . ? C12 C11 C15 C20 -175.8(5) . . . . ? C16 C11 C15 C20 -1.1(9) . . . . ? Cr2 C11 C15 C20 121.4(5) . . . . ? C12 C11 C15 Cr2 62.8(4) . . . . ? C16 C11 C15 Cr2 -122.5(6) . . . . ? C13 C14 C15 C11 -0.8(6) . . . . ? C19 C14 C15 C11 -176.0(5) . . . . ? Cr2 C14 C15 C11 62.0(4) . . . . ? C13 C14 C15 C20 175.7(5) . . . . ? C19 C14 C15 C20 0.5(9) . . . . ? Cr2 C14 C15 C20 -121.5(5) . . . . ? C13 C14 C15 Cr2 -62.8(4) . . . . ? C19 C14 C15 Cr2 122.0(5) . . . . ? C14 Cr2 C15 C11 -116.9(5) . . . . ? C12 Cr2 C15 C11 -37.6(3) . . . . ? C13 Cr2 C15 C11 -79.6(4) . . . . ? P5 Cr2 C15 C11 132.7(3) . . . . ? P4 Cr2 C15 C11 -168.3(3) . . . . ? P3 Cr2 C15 C11 -93.6(5) . . . . ? P1 Cr2 C15 C11 75.4(3) . . . . ? P2 Cr2 C15 C11 24.9(5) . . . . ? Cr1 Cr2 C15 C11 125.6(3) . . . . ? C11 Cr2 C15 C14 116.9(5) . . . . ? C12 Cr2 C15 C14 79.2(4) . . . . ? C13 Cr2 C15 C14 37.3(3) . . . . ? P5 Cr2 C15 C14 -110.5(3) . . . . ? P4 Cr2 C15 C14 -51.4(4) . . . . ? P3 Cr2 C15 C14 23.2(6) . . . . ? P1 Cr2 C15 C14 -167.8(3) . . . . ? P2 Cr2 C15 C14 141.8(3) . . . . ? Cr1 Cr2 C15 C14 -117.5(3) . . . . ? C11 Cr2 C15 C20 -121.7(7) . . . . ? C14 Cr2 C15 C20 121.4(6) . . . . ? C12 Cr2 C15 C20 -159.3(6) . . . . ? C13 Cr2 C15 C20 158.7(6) . . . . ? P5 Cr2 C15 C20 11.0(5) . . . . ? P4 Cr2 C15 C20 70.0(5) . . . . ? P3 Cr2 C15 C20 144.7(4) . . . . ? P1 Cr2 C15 C20 -46.3(5) . . . . ? P2 Cr2 C15 C20 -96.8(5) . . . . ? Cr1 Cr2 C15 C20 3.9(7) . . . . ? C25 C21 C22 C23 -0.4(7) . . . . ? C26 C21 C22 C23 174.6(6) . . . . ? Cr3 C21 C22 C23 -61.8(4) . . . . ? C25 C21 C22 C27 -174.6(5) . . . . ? C26 C21 C22 C27 0.4(10) . . . . ? Cr3 C21 C22 C27 124.0(6) . . . . ? C25 C21 C22 Cr3 61.4(4) . . . . ? C26 C21 C22 Cr3 -123.6(6) . . . . ? C21 C22 C23 C24 0.6(7) . . . . ? C27 C22 C23 C24 174.7(5) . . . . ? Cr3 C22 C23 C24 -61.8(4) . . . . ? C21 C22 C23 C28 -174.9(5) . . . . ? C27 C22 C23 C28 -0.8(9) . . . . ? Cr3 C22 C23 C28 122.7(6) . . . . ? C21 C22 C23 Cr3 62.3(4) . . . . ? C27 C22 C23 Cr3 -123.5(6) . . . . ? C22 C23 C24 C25 -0.6(7) . . . . ? C28 C23 C24 C25 174.8(5) . . . . ? Cr3 C23 C24 C25 -63.0(4) . . . . ? C22 C23 C24 C29 -173.5(5) . . . . ? C28 C23 C24 C29 1.9(10) . . . . ? Cr3 C23 C24 C29 124.1(6) . . . . ? C22 C23 C24 Cr3 62.4(4) . . . . ? C28 C23 C24 Cr3 -122.2(6) . . . . ? C23 C24 C25 C21 0.3(7) . . . . ? C29 C24 C25 C21 173.2(6) . . . . ? Cr3 C24 C25 C21 -62.6(4) . . . . ? C23 C24 C25 C30 -174.2(6) . . . . ? C29 C24 C25 C30 -1.3(10) . . . . ? Cr3 C24 C25 C30 122.8(6) . . . . ? C23 C24 C25 Cr3 63.0(4) . . . . ? C29 C24 C25 Cr3 -124.2(6) . . . . ? C22 C21 C25 C24 0.0(7) . . . . ? C26 C21 C25 C24 -175.1(6) . . . . ? Cr3 C21 C25 C24 62.0(4) . . . . ? C22 C21 C25 C30 174.6(5) . . . . ? C26 C21 C25 C30 -0.5(10) . . . . ? Cr3 C21 C25 C30 -123.4(6) . . . . ? C22 C21 C25 Cr3 -62.0(4) . . . . ? C26 C21 C25 Cr3 123.0(6) . . . . ? C25 C24 Cr3 C23 116.0(5) . . . . ? C29 C24 Cr3 C23 -121.5(7) . . . . ? C23 C24 Cr3 C25 -116.0(5) . . . . ? C29 C24 Cr3 C25 122.5(7) . . . . ? C23 C24 Cr3 C22 -36.4(3) . . . . ? C25 C24 Cr3 C22 79.6(4) . . . . ? C29 C24 Cr3 C22 -157.9(6) . . . . ? C23 C24 Cr3 C21 -78.7(4) . . . . ? C25 C24 Cr3 C21 37.3(3) . . . . ? C29 C24 Cr3 C21 159.8(6) . . . . ? C23 C24 Cr3 P10 178.1(3) . . . . ? C25 C24 Cr3 P10 -65.9(3) . . . . ? C29 C24 Cr3 P10 56.6(5) . . . . ? C23 C24 Cr3 P9 117.2(3) . . . . ? C25 C24 Cr3 P9 -126.9(3) . . . . ? C29 C24 Cr3 P9 -4.3(5) . . . . ? C23 C24 Cr3 P8 62.0(3) . . . . ? C25 C24 Cr3 P8 178.0(3) . . . . ? C29 C24 Cr3 P8 -59.5(5) . . . . ? C23 C24 Cr3 P6 -121.9(4) . . . . ? C25 C24 Cr3 P6 -6.0(5) . . . . ? C29 C24 Cr3 P6 116.6(5) . . . . ? C23 C24 Cr3 P7 5.6(5) . . . . ? C25 C24 Cr3 P7 121.5(4) . . . . ? C29 C24 Cr3 P7 -116.0(5) . . . . ? C23 C24 Cr3 Cr4 123.3(3) . . . . ? C25 C24 Cr3 Cr4 -120.7(3) . . . . ? C29 C24 Cr3 Cr4 1.8(7) . . . . ? C22 C23 Cr3 C24 -119.1(5) . . . . ? C28 C23 Cr3 C24 121.6(7) . . . . ? C24 C23 Cr3 C25 38.3(3) . . . . ? C22 C23 Cr3 C25 -80.8(4) . . . . ? C28 C23 Cr3 C25 160.0(6) . . . . ? C24 C23 Cr3 C22 119.1(5) . . . . ? C28 C23 Cr3 C22 -119.3(7) . . . . ? C24 C23 Cr3 C21 81.1(4) . . . . ? C22 C23 Cr3 C21 -38.0(3) . . . . ? C28 C23 Cr3 C21 -157.3(6) . . . . ? C24 C23 Cr3 P10 -3.4(5) . . . . ? C22 C23 Cr3 P10 -122.5(4) . . . . ? C28 C23 Cr3 P10 118.3(5) . . . . ? C24 C23 Cr3 P9 -69.0(3) . . . . ? C22 C23 Cr3 P9 171.9(3) . . . . ? C28 C23 Cr3 P9 52.6(5) . . . . ? C24 C23 Cr3 P8 -125.9(3) . . . . ? C22 C23 Cr3 P8 115.0(3) . . . . ? C28 C23 Cr3 P8 -4.3(5) . . . . ? C24 C23 Cr3 P6 126.3(3) . . . . ? C22 C23 Cr3 P6 7.2(5) . . . . ? C28 C23 Cr3 P6 -112.1(5) . . . . ? C24 C23 Cr3 P7 -177.0(3) . . . . ? C22 C23 Cr3 P7 63.9(3) . . . . ? C28 C23 Cr3 P7 -55.4(5) . . . . ? C24 C23 Cr3 Cr4 -116.3(3) . . . . ? C22 C23 Cr3 Cr4 124.6(3) . . . . ? C28 C23 Cr3 Cr4 5.3(7) . . . . ? C21 C25 Cr3 C24 117.9(5) . . . . ? C30 C25 Cr3 C24 -121.3(7) . . . . ? C24 C25 Cr3 C23 -38.1(3) . . . . ? C21 C25 Cr3 C23 79.8(4) . . . . ? C30 C25 Cr3 C23 -159.3(6) . . . . ? C24 C25 Cr3 C22 -80.2(4) . . . . ? C21 C25 Cr3 C22 37.6(3) . . . . ? C30 C25 Cr3 C22 158.5(6) . . . . ? C24 C25 Cr3 C21 -117.9(5) . . . . ? C30 C25 Cr3 C21 120.9(7) . . . . ? C24 C25 Cr3 P10 121.3(3) . . . . ? C21 C25 Cr3 P10 -120.8(3) . . . . ? C30 C25 Cr3 P10 0.0(5) . . . . ? C24 C25 Cr3 P9 60.4(3) . . . . ? C21 C25 Cr3 P9 178.3(3) . . . . ? C30 C25 Cr3 P9 -60.8(5) . . . . ? C24 C25 Cr3 P8 -3.8(5) . . . . ? C21 C25 Cr3 P8 114.1(4) . . . . ? C30 C25 Cr3 P8 -125.0(5) . . . . ? C24 C25 Cr3 P6 176.8(3) . . . . ? C21 C25 Cr3 P6 -65.4(3) . . . . ? C30 C25 Cr3 P6 55.5(5) . . . . ? C24 C25 Cr3 P7 -128.0(3) . . . . ? C21 C25 Cr3 P7 -10.1(5) . . . . ? C30 C25 Cr3 P7 110.8(5) . . . . ? C24 C25 Cr3 Cr4 117.6(3) . . . . ? C21 C25 Cr3 Cr4 -124.5(3) . . . . ? C30 C25 Cr3 Cr4 -3.6(7) . . . . ? C23 C22 Cr3 C24 36.5(3) . . . . ? C21 C22 Cr3 C24 -80.1(4) . . . . ? C27 C22 Cr3 C24 158.4(6) . . . . ? C21 C22 Cr3 C23 -116.6(5) . . . . ? C27 C22 Cr3 C23 121.9(6) . . . . ? C23 C22 Cr3 C25 78.9(4) . . . . ? C21 C22 Cr3 C25 -37.7(3) . . . . ? C27 C22 Cr3 C25 -159.2(6) . . . . ? C23 C22 Cr3 C21 116.6(5) . . . . ? C27 C22 Cr3 C21 -121.4(7) . . . . ? C23 C22 Cr3 P10 122.7(3) . . . . ? C21 C22 Cr3 P10 6.0(5) . . . . ? C27 C22 Cr3 P10 -115.4(5) . . . . ? C23 C22 Cr3 P9 -13.3(5) . . . . ? C21 C22 Cr3 P9 -129.9(3) . . . . ? C27 C22 Cr3 P9 108.6(5) . . . . ? C23 C22 Cr3 P8 -71.7(3) . . . . ? C21 C22 Cr3 P8 171.7(3) . . . . ? C27 C22 Cr3 P8 50.2(5) . . . . ? C23 C22 Cr3 P6 -175.9(3) . . . . ? C21 C22 Cr3 P6 67.4(4) . . . . ? C27 C22 Cr3 P6 -54.0(5) . . . . ? C23 C22 Cr3 P7 -124.3(3) . . . . ? C21 C22 Cr3 P7 119.1(3) . . . . ? C27 C22 Cr3 P7 -2.4(5) . . . . ? C23 C22 Cr3 Cr4 -120.6(3) . . . . ? C21 C22 Cr3 Cr4 122.8(3) . . . . ? C27 C22 Cr3 Cr4 1.4(7) . . . . ? C25 C21 Cr3 C24 -37.2(3) . . . . ? C22 C21 Cr3 C24 79.8(4) . . . . ? C26 C21 Cr3 C24 -157.7(6) . . . . ? C25 C21 Cr3 C23 -79.4(4) . . . . ? C22 C21 Cr3 C23 37.6(3) . . . . ? C26 C21 Cr3 C23 160.1(6) . . . . ? C22 C21 Cr3 C25 117.0(5) . . . . ? C26 C21 Cr3 C25 -120.4(7) . . . . ? C25 C21 Cr3 C22 -117.0(5) . . . . ? C26 C21 Cr3 C22 122.5(7) . . . . ? C25 C21 Cr3 P10 66.4(3) . . . . ? C22 C21 Cr3 P10 -176.6(3) . . . . ? C26 C21 Cr3 P10 -54.1(6) . . . . ? C25 C21 Cr3 P9 -3.2(5) . . . . ? C22 C21 Cr3 P9 113.8(4) . . . . ? C26 C21 Cr3 P9 -123.7(5) . . . . ? C25 C21 Cr3 P8 -130.8(3) . . . . ? C22 C21 Cr3 P8 -13.7(5) . . . . ? C26 C21 Cr3 P8 108.8(5) . . . . ? C25 C21 Cr3 P6 122.7(3) . . . . ? C22 C21 Cr3 P6 -120.3(3) . . . . ? C26 C21 Cr3 P6 2.2(5) . . . . ? C25 C21 Cr3 P7 174.3(3) . . . . ? C22 C21 Cr3 P7 -68.7(4) . . . . ? C26 C21 Cr3 P7 53.8(5) . . . . ? C25 C21 Cr3 Cr4 118.4(4) . . . . ? C22 C21 Cr3 Cr4 -124.6(3) . . . . ? C26 C21 Cr3 Cr4 -2.0(7) . . . . ? C24 Cr3 P6 P7 150.7(3) . . . . ? C23 Cr3 P6 P7 74.1(3) . . . . ? C25 Cr3 P6 P7 146.81(18) . . . . ? C22 Cr3 P6 P7 78.75(17) . . . . ? C21 Cr3 P6 P7 113.06(17) . . . . ? P10 Cr3 P6 P7 -134.87(8) . . . . ? P9 Cr3 P6 P7 -90.96(8) . . . . ? P8 Cr3 P6 P7 -32.92(7) . . . . ? Cr4 Cr3 P6 P7 -69.69(7) . . . . ? C24 Cr3 P6 P10 -74.4(3) . . . . ? C23 Cr3 P6 P10 -151.0(3) . . . . ? C25 Cr3 P6 P10 -78.32(18) . . . . ? C22 Cr3 P6 P10 -146.37(17) . . . . ? C21 Cr3 P6 P10 -112.06(17) . . . . ? P9 Cr3 P6 P10 43.92(7) . . . . ? P8 Cr3 P6 P10 101.95(8) . . . . ? P7 Cr3 P6 P10 134.87(8) . . . . ? Cr4 Cr3 P6 P10 65.18(7) . . . . ? C24 Cr3 P6 Cr4 -139.6(3) . . . . ? C23 Cr3 P6 Cr4 143.8(3) . . . . ? C25 Cr3 P6 Cr4 -143.50(17) . . . . ? C22 Cr3 P6 Cr4 148.45(17) . . . . ? C21 Cr3 P6 Cr4 -177.24(17) . . . . ? P10 Cr3 P6 Cr4 -65.18(7) . . . . ? P9 Cr3 P6 Cr4 -21.26(6) . . . . ? P8 Cr3 P6 Cr4 36.77(6) . . . . ? P7 Cr3 P6 Cr4 69.69(7) . . . . ? P10 P6 P7 P8 -0.95(12) . . . . ? Cr3 P6 P7 P8 39.55(8) . . . . ? Cr4 P6 P7 P8 -40.90(8) . . . . ? P10 P6 P7 Cr4 39.95(8) . . . . ? Cr3 P6 P7 Cr4 80.45(6) . . . . ? P10 P6 P7 Cr3 -40.50(7) . . . . ? Cr4 P6 P7 Cr3 -80.45(6) . . . . ? C24 Cr3 P7 P6 -150.0(3) . . . . ? C23 Cr3 P7 P6 -146.38(17) . . . . ? C25 Cr3 P7 P6 -72.2(3) . . . . ? C22 Cr3 P7 P6 -113.47(16) . . . . ? C21 Cr3 P7 P6 -78.80(17) . . . . ? P10 Cr3 P7 P6 37.00(8) . . . . ? P9 Cr3 P7 P6 99.96(7) . . . . ? P8 Cr3 P7 P6 137.57(9) . . . . ? Cr4 Cr3 P7 P6 68.89(6) . . . . ? C24 Cr3 P7 P8 72.4(3) . . . . ? C23 Cr3 P7 P8 76.05(18) . . . . ? C25 Cr3 P7 P8 150.2(3) . . . . ? C22 Cr3 P7 P8 108.96(16) . . . . ? C21 Cr3 P7 P8 143.62(17) . . . . ? P10 Cr3 P7 P8 -100.58(8) . . . . ? P9 Cr3 P7 P8 -37.62(7) . . . . ? P6 Cr3 P7 P8 -137.57(9) . . . . ? Cr4 Cr3 P7 P8 -68.69(7) . . . . ? C24 Cr3 P7 Cr4 141.1(3) . . . . ? C23 Cr3 P7 Cr4 144.73(17) . . . . ? C25 Cr3 P7 Cr4 -141.1(3) . . . . ? C22 Cr3 P7 Cr4 177.64(15) . . . . ? C21 Cr3 P7 Cr4 -147.69(17) . . . . ? P10 Cr3 P7 Cr4 -31.89(6) . . . . ? P9 Cr3 P7 Cr4 31.07(6) . . . . ? P8 Cr3 P7 Cr4 68.69(7) . . . . ? P6 Cr3 P7 Cr4 -68.89(6) . . . . ? P6 P7 P8 P9 1.18(12) . . . . ? Cr4 P7 P8 P9 -39.81(7) . . . . ? Cr3 P7 P8 P9 40.82(7) . . . . ? P6 P7 P8 Cr3 -39.63(8) . . . . ? Cr4 P7 P8 Cr3 -80.62(6) . . . . ? P6 P7 P8 Cr4 40.99(8) . . . . ? Cr3 P7 P8 Cr4 80.62(6) . . . . ? C24 Cr3 P8 P7 -149.24(17) . . . . ? C23 Cr3 P8 P7 -116.83(17) . . . . ? C25 Cr3 P8 P7 -146.7(3) . . . . ? C22 Cr3 P8 P7 -81.79(18) . . . . ? C21 Cr3 P8 P7 -73.1(3) . . . . ? P10 Cr3 P8 P7 90.45(8) . . . . ? P9 Cr3 P8 P7 134.31(8) . . . . ? P6 Cr3 P8 P7 32.76(7) . . . . ? Cr4 Cr3 P8 P7 69.56(7) . . . . ? C24 Cr3 P8 P9 76.45(17) . . . . ? C23 Cr3 P8 P9 108.86(16) . . . . ? C25 Cr3 P8 P9 79.0(3) . . . . ? C22 Cr3 P8 P9 143.90(18) . . . . ? C21 Cr3 P8 P9 152.6(3) . . . . ? P10 Cr3 P8 P9 -43.86(8) . . . . ? P6 Cr3 P8 P9 -101.54(7) . . . . ? P7 Cr3 P8 P9 -134.31(8) . . . . ? Cr4 Cr3 P8 P9 -64.75(6) . . . . ? C24 Cr3 P8 Cr4 141.20(17) . . . . ? C23 Cr3 P8 Cr4 173.61(16) . . . . ? C25 Cr3 P8 Cr4 143.7(3) . . . . ? C22 Cr3 P8 Cr4 -151.35(17) . . . . ? C21 Cr3 P8 Cr4 -142.6(3) . . . . ? P10 Cr3 P8 Cr4 20.89(7) . . . . ? P9 Cr3 P8 Cr4 64.75(6) . . . . ? P6 Cr3 P8 Cr4 -36.79(6) . . . . ? P7 Cr3 P8 Cr4 -69.56(7) . . . . ? P7 P8 P9 Cr4 42.07(8) . . . . ? Cr3 P8 P9 Cr4 85.43(6) . . . . ? P7 P8 P9 Cr3 -43.35(8) . . . . ? Cr4 P8 P9 Cr3 -85.43(6) . . . . ? P7 P8 P9 P10 -0.92(11) . . . . ? Cr3 P8 P9 P10 42.44(7) . . . . ? Cr4 P8 P9 P10 -42.99(7) . . . . ? C24 Cr3 P9 P8 -117.07(17) . . . . ? C23 Cr3 P9 P8 -82.63(17) . . . . ? C25 Cr3 P9 P8 -149.08(18) . . . . ? C22 Cr3 P9 P8 -74.2(3) . . . . ? C21 Cr3 P9 P8 -147.0(3) . . . . ? P10 Cr3 P9 P8 130.37(8) . . . . ? P6 Cr3 P9 P8 89.16(8) . . . . ? P7 Cr3 P9 P8 35.42(7) . . . . ? Cr4 Cr3 P9 P8 67.42(7) . . . . ? C24 Cr3 P9 Cr4 175.51(16) . . . . ? C23 Cr3 P9 Cr4 -150.04(16) . . . . ? C25 Cr3 P9 Cr4 143.50(17) . . . . ? C22 Cr3 P9 Cr4 -141.7(3) . . . . ? C21 Cr3 P9 Cr4 145.6(3) . . . . ? P10 Cr3 P9 Cr4 62.95(6) . . . . ? P8 Cr3 P9 Cr4 -67.42(7) . . . . ? P6 Cr3 P9 Cr4 21.74(6) . . . . ? P7 Cr3 P9 Cr4 -32.00(6) . . . . ? C24 Cr3 P9 P10 112.56(17) . . . . ? C23 Cr3 P9 P10 147.01(16) . . . . ? C25 Cr3 P9 P10 80.55(18) . . . . ? C22 Cr3 P9 P10 155.4(3) . . . . ? C21 Cr3 P9 P10 82.7(3) . . . . ? P8 Cr3 P9 P10 -130.37(8) . . . . ? P6 Cr3 P9 P10 -41.21(7) . . . . ? P7 Cr3 P9 P10 -94.95(8) . . . . ? Cr4 Cr3 P9 P10 -62.95(6) . . . . ? P7 P6 P10 Cr3 43.04(8) . . . . ? Cr4 P6 P10 Cr3 85.14(7) . . . . ? P7 P6 P10 Cr4 -42.10(8) . . . . ? Cr3 P6 P10 Cr4 -85.14(7) . . . . ? P7 P6 P10 P9 0.34(11) . . . . ? Cr3 P6 P10 P9 -42.70(7) . . . . ? Cr4 P6 P10 P9 42.43(7) . . . . ? C24 Cr3 P10 P6 148.87(18) . . . . ? C23 Cr3 P10 P6 151.0(3) . . . . ? C25 Cr3 P10 P6 115.03(17) . . . . ? C22 Cr3 P10 P6 77.1(3) . . . . ? C21 Cr3 P10 P6 81.02(19) . . . . ? P9 Cr3 P10 P6 -130.20(8) . . . . ? P8 Cr3 P10 P6 -88.86(8) . . . . ? P7 Cr3 P10 P6 -34.83(7) . . . . ? Cr4 Cr3 P10 P6 -67.57(7) . . . . ? C24 Cr3 P10 Cr4 -143.56(17) . . . . ? C23 Cr3 P10 Cr4 -141.4(3) . . . . ? C25 Cr3 P10 Cr4 -177.40(16) . . . . ? C22 Cr3 P10 Cr4 144.7(3) . . . . ? C21 Cr3 P10 Cr4 148.59(18) . . . . ? P9 Cr3 P10 Cr4 -62.63(6) . . . . ? P8 Cr3 P10 Cr4 -21.28(7) . . . . ? P6 Cr3 P10 Cr4 67.57(7) . . . . ? P7 Cr3 P10 Cr4 32.75(6) . . . . ? C24 Cr3 P10 P9 -80.93(18) . . . . ? C23 Cr3 P10 P9 -78.8(3) . . . . ? C25 Cr3 P10 P9 -114.77(17) . . . . ? C22 Cr3 P10 P9 -152.7(3) . . . . ? C21 Cr3 P10 P9 -148.78(18) . . . . ? P8 Cr3 P10 P9 41.35(7) . . . . ? P6 Cr3 P10 P9 130.20(8) . . . . ? P7 Cr3 P10 P9 95.38(7) . . . . ? Cr4 Cr3 P10 P9 62.63(6) . . . . ? P8 P9 P10 P6 0.35(10) . . . . ? Cr4 P9 P10 P6 -44.82(7) . . . . ? Cr3 P9 P10 P6 44.96(7) . . . . ? P8 P9 P10 Cr3 -44.61(7) . . . . ? Cr4 P9 P10 Cr3 -89.78(6) . . . . ? P8 P9 P10 Cr4 45.17(7) . . . . ? Cr3 P9 P10 Cr4 89.78(6) . . . . ? P8 P9 Cr4 C31 158.1(2) . . . . ? Cr3 P9 Cr4 C31 -134.7(2) . . . . ? P10 P9 Cr4 C31 -72.1(2) . . . . ? P8 P9 Cr4 C34 104.49(17) . . . . ? Cr3 P9 Cr4 C34 171.66(16) . . . . ? P10 P9 Cr4 C34 -125.68(17) . . . . ? P8 P9 Cr4 C33 76.09(19) . . . . ? Cr3 P9 Cr4 C33 143.26(18) . . . . ? P10 P9 Cr4 C33 -154.08(19) . . . . ? P8 P9 Cr4 C32 93.0(4) . . . . ? Cr3 P9 Cr4 C32 160.1(4) . . . . ? P10 P9 Cr4 C32 -137.2(4) . . . . ? P8 P9 Cr4 C35 141.83(16) . . . . ? Cr3 P9 Cr4 C35 -151.00(15) . . . . ? P10 P9 Cr4 C35 -88.34(16) . . . . ? P8 P9 Cr4 P10 -129.83(8) . . . . ? Cr3 P9 Cr4 P10 -62.66(6) . . . . ? Cr3 P9 Cr4 P8 67.17(6) . . . . ? P10 P9 Cr4 P8 129.83(8) . . . . ? P8 P9 Cr4 P6 -88.86(8) . . . . ? Cr3 P9 Cr4 P6 -21.69(6) . . . . ? P10 P9 Cr4 P6 40.97(7) . . . . ? P8 P9 Cr4 P7 -34.83(7) . . . . ? Cr3 P9 Cr4 P7 32.34(6) . . . . ? P10 P9 Cr4 P7 95.00(7) . . . . ? P8 P9 Cr4 Cr3 -67.17(6) . . . . ? P10 P9 Cr4 Cr3 62.66(6) . . . . ? P6 P10 Cr4 C31 -90.28(16) . . . . ? Cr3 P10 Cr4 C31 -157.81(16) . . . . ? P9 P10 Cr4 C31 139.32(16) . . . . ? P6 P10 Cr4 C34 -153.6(2) . . . . ? Cr3 P10 Cr4 C34 138.9(2) . . . . ? P9 P10 Cr4 C34 76.0(2) . . . . ? P6 P10 Cr4 C33 -126.5(4) . . . . ? Cr3 P10 Cr4 C33 165.9(4) . . . . ? P9 P10 Cr4 C33 103.1(4) . . . . ? P6 P10 Cr4 C32 -71.2(2) . . . . ? Cr3 P10 Cr4 C32 -138.7(2) . . . . ? P9 P10 Cr4 C32 158.4(2) . . . . ? P6 P10 Cr4 C35 -127.58(17) . . . . ? Cr3 P10 Cr4 C35 164.90(16) . . . . ? P9 P10 Cr4 C35 102.02(17) . . . . ? P6 P10 Cr4 P9 130.40(7) . . . . ? Cr3 P10 Cr4 P9 62.88(7) . . . . ? P6 P10 Cr4 P8 88.73(7) . . . . ? Cr3 P10 Cr4 P8 21.21(7) . . . . ? P9 P10 Cr4 P8 -41.67(7) . . . . ? Cr3 P10 Cr4 P6 -67.52(7) . . . . ? P9 P10 Cr4 P6 -130.40(7) . . . . ? P6 P10 Cr4 P7 34.46(7) . . . . ? Cr3 P10 Cr4 P7 -33.06(6) . . . . ? P9 P10 Cr4 P7 -95.94(7) . . . . ? P6 P10 Cr4 Cr3 67.52(7) . . . . ? P9 P10 Cr4 Cr3 -62.88(7) . . . . ? P7 P8 Cr4 C31 86.2(4) . . . . ? P9 P8 Cr4 C31 -138.4(4) . . . . ? Cr3 P8 Cr4 C31 156.6(4) . . . . ? P7 P8 Cr4 C34 138.60(18) . . . . ? P9 P8 Cr4 C34 -86.01(18) . . . . ? Cr3 P8 Cr4 C34 -151.00(17) . . . . ? P7 P8 Cr4 C33 101.77(16) . . . . ? P9 P8 Cr4 C33 -122.84(17) . . . . ? Cr3 P8 Cr4 C33 172.16(16) . . . . ? P7 P8 Cr4 C32 71.91(18) . . . . ? P9 P8 Cr4 C32 -152.70(18) . . . . ? Cr3 P8 Cr4 C32 142.31(17) . . . . ? P7 P8 Cr4 C35 155.2(2) . . . . ? P9 P8 Cr4 C35 -69.4(3) . . . . ? Cr3 P8 Cr4 C35 -134.4(2) . . . . ? P7 P8 Cr4 P9 -135.39(8) . . . . ? Cr3 P8 Cr4 P9 -64.99(7) . . . . ? P7 P8 Cr4 P10 -91.19(8) . . . . ? P9 P8 Cr4 P10 44.20(8) . . . . ? Cr3 P8 Cr4 P10 -20.79(7) . . . . ? P7 P8 Cr4 P6 -33.72(7) . . . . ? P9 P8 Cr4 P6 101.68(8) . . . . ? Cr3 P8 Cr4 P6 36.68(6) . . . . ? P9 P8 Cr4 P7 135.39(8) . . . . ? Cr3 P8 Cr4 P7 70.40(6) . . . . ? P7 P8 Cr4 Cr3 -70.40(6) . . . . ? P9 P8 Cr4 Cr3 64.99(7) . . . . ? P7 P6 Cr4 C31 -126.84(16) . . . . ? P10 P6 Cr4 C31 97.57(17) . . . . ? Cr3 P6 Cr4 C31 162.61(16) . . . . ? P7 P6 Cr4 C34 -126.0(5) . . . . ? P10 P6 Cr4 C34 98.5(5) . . . . ? Cr3 P6 Cr4 C34 163.5(4) . . . . ? P7 P6 Cr4 C33 -70.0(2) . . . . ? P10 P6 Cr4 C33 154.4(2) . . . . ? Cr3 P6 Cr4 C33 -140.6(2) . . . . ? P7 P6 Cr4 C32 -88.88(16) . . . . ? P10 P6 Cr4 C32 135.54(16) . . . . ? Cr3 P6 Cr4 C32 -159.43(16) . . . . ? P7 P6 Cr4 C35 -153.0(2) . . . . ? P10 P6 Cr4 C35 71.4(2) . . . . ? Cr3 P6 Cr4 C35 136.43(19) . . . . ? P7 P6 Cr4 P9 91.85(8) . . . . ? P10 P6 Cr4 P9 -43.73(7) . . . . ? Cr3 P6 Cr4 P9 21.30(6) . . . . ? P7 P6 Cr4 P10 135.58(9) . . . . ? Cr3 P6 Cr4 P10 65.03(7) . . . . ? P7 P6 Cr4 P8 33.88(7) . . . . ? P10 P6 Cr4 P8 -101.70(8) . . . . ? Cr3 P6 Cr4 P8 -36.67(6) . . . . ? P10 P6 Cr4 P7 -135.58(9) . . . . ? Cr3 P6 Cr4 P7 -70.55(7) . . . . ? P7 P6 Cr4 Cr3 70.55(7) . . . . ? P10 P6 Cr4 Cr3 -65.03(7) . . . . ? P6 P7 Cr4 C31 70.25(19) . . . . ? P8 P7 Cr4 C31 -153.44(18) . . . . ? Cr3 P7 Cr4 C31 138.50(18) . . . . ? P6 P7 Cr4 C34 153.4(2) . . . . ? P8 P7 Cr4 C34 -70.2(3) . . . . ? Cr3 P7 Cr4 C34 -138.3(2) . . . . ? P6 P7 Cr4 C33 136.15(16) . . . . ? P8 P7 Cr4 C33 -87.53(17) . . . . ? Cr3 P7 Cr4 C33 -155.60(16) . . . . ? P6 P7 Cr4 C32 98.81(16) . . . . ? P8 P7 Cr4 C32 -124.87(16) . . . . ? Cr3 P7 Cr4 C32 167.06(15) . . . . ? P6 P7 Cr4 C35 89.2(4) . . . . ? P8 P7 Cr4 C35 -134.5(4) . . . . ? Cr3 P7 Cr4 C35 157.4(4) . . . . ? P6 P7 Cr4 P9 -99.44(8) . . . . ? P8 P7 Cr4 P9 36.87(7) . . . . ? Cr3 P7 Cr4 P9 -31.20(6) . . . . ? P6 P7 Cr4 P10 -36.43(8) . . . . ? P8 P7 Cr4 P10 99.88(9) . . . . ? Cr3 P7 Cr4 P10 31.82(6) . . . . ? P6 P7 Cr4 P8 -136.31(9) . . . . ? Cr3 P7 Cr4 P8 -68.07(7) . . . . ? P8 P7 Cr4 P6 136.31(9) . . . . ? Cr3 P7 Cr4 P6 68.25(7) . . . . ? P6 P7 Cr4 Cr3 -68.25(7) . . . . ? P8 P7 Cr4 Cr3 68.07(7) . . . . ? C24 Cr3 Cr4 C31 114.2(4) . . . . ? C23 Cr3 Cr4 C31 -176.5(4) . . . . ? C25 Cr3 Cr4 C31 45.8(4) . . . . ? C22 Cr3 Cr4 C31 -102.5(4) . . . . ? C21 Cr3 Cr4 C31 -26.5(4) . . . . ? P10 Cr3 Cr4 C31 41.2(3) . . . . ? P9 Cr3 Cr4 C31 122.0(3) . . . . ? P8 Cr3 Cr4 C31 -164.6(3) . . . . ? P6 Cr3 Cr4 C31 -31.7(3) . . . . ? P7 Cr3 Cr4 C31 -97.9(3) . . . . ? C24 Cr3 Cr4 C34 -22.9(4) . . . . ? C23 Cr3 Cr4 C34 46.4(4) . . . . ? C25 Cr3 Cr4 C34 -91.4(4) . . . . ? C22 Cr3 Cr4 C34 120.4(4) . . . . ? C21 Cr3 Cr4 C34 -163.6(4) . . . . ? P10 Cr3 Cr4 C34 -96.0(3) . . . . ? P9 Cr3 Cr4 C34 -15.2(3) . . . . ? P8 Cr3 Cr4 C34 58.2(3) . . . . ? P6 Cr3 Cr4 C34 -168.8(3) . . . . ? P7 Cr3 Cr4 C34 124.9(3) . . . . ? C24 Cr3 Cr4 C33 -96.5(4) . . . . ? C23 Cr3 Cr4 C33 -27.1(4) . . . . ? C25 Cr3 Cr4 C33 -164.9(4) . . . . ? C22 Cr3 Cr4 C33 46.9(4) . . . . ? C21 Cr3 Cr4 C33 122.9(4) . . . . ? P10 Cr3 Cr4 C33 -169.5(3) . . . . ? P9 Cr3 Cr4 C33 -88.7(3) . . . . ? P8 Cr3 Cr4 C33 -15.3(3) . . . . ? P6 Cr3 Cr4 C33 117.6(3) . . . . ? P7 Cr3 Cr4 C33 51.4(3) . . . . ? C24 Cr3 Cr4 C32 -173.0(4) . . . . ? C23 Cr3 Cr4 C32 -103.6(4) . . . . ? C25 Cr3 Cr4 C32 118.6(4) . . . . ? C22 Cr3 Cr4 C32 -29.6(4) . . . . ? C21 Cr3 Cr4 C32 46.4(4) . . . . ? P10 Cr3 Cr4 C32 114.0(3) . . . . ? P9 Cr3 Cr4 C32 -165.2(3) . . . . ? P8 Cr3 Cr4 C32 -91.8(3) . . . . ? P6 Cr3 Cr4 C32 41.1(3) . . . . ? P7 Cr3 Cr4 C32 -25.1(3) . . . . ? C24 Cr3 Cr4 C35 46.6(4) . . . . ? C23 Cr3 Cr4 C35 115.9(4) . . . . ? C25 Cr3 Cr4 C35 -21.9(4) . . . . ? C22 Cr3 Cr4 C35 -170.1(4) . . . . ? C21 Cr3 Cr4 C35 -94.1(4) . . . . ? P10 Cr3 Cr4 C35 -26.5(3) . . . . ? P9 Cr3 Cr4 C35 54.3(3) . . . . ? P8 Cr3 Cr4 C35 127.8(3) . . . . ? P6 Cr3 Cr4 C35 -99.3(3) . . . . ? P7 Cr3 Cr4 C35 -165.6(3) . . . . ? C24 Cr3 Cr4 P9 -7.8(3) . . . . ? C23 Cr3 Cr4 P9 61.6(3) . . . . ? C25 Cr3 Cr4 P9 -76.2(3) . . . . ? C22 Cr3 Cr4 P9 135.6(3) . . . . ? C21 Cr3 Cr4 P9 -148.4(3) . . . . ? P10 Cr3 Cr4 P9 -80.80(8) . . . . ? P8 Cr3 Cr4 P9 73.44(7) . . . . ? P6 Cr3 Cr4 P9 -153.65(8) . . . . ? P7 Cr3 Cr4 P9 140.12(8) . . . . ? C24 Cr3 Cr4 P10 73.1(3) . . . . ? C23 Cr3 Cr4 P10 142.4(3) . . . . ? C25 Cr3 Cr4 P10 4.6(3) . . . . ? C22 Cr3 Cr4 P10 -143.6(3) . . . . ? C21 Cr3 Cr4 P10 -67.6(3) . . . . ? P9 Cr3 Cr4 P10 80.80(8) . . . . ? P8 Cr3 Cr4 P10 154.24(8) . . . . ? P6 Cr3 Cr4 P10 -72.85(9) . . . . ? P7 Cr3 Cr4 P10 -139.08(8) . . . . ? C24 Cr3 Cr4 P8 -81.2(3) . . . . ? C23 Cr3 Cr4 P8 -11.9(3) . . . . ? C25 Cr3 Cr4 P8 -149.6(3) . . . . ? C22 Cr3 Cr4 P8 62.1(3) . . . . ? C21 Cr3 Cr4 P8 138.1(3) . . . . ? P10 Cr3 Cr4 P8 -154.24(8) . . . . ? P9 Cr3 Cr4 P8 -73.44(7) . . . . ? P6 Cr3 Cr4 P8 132.91(8) . . . . ? P7 Cr3 Cr4 P8 66.67(7) . . . . ? C24 Cr3 Cr4 P6 145.9(3) . . . . ? C23 Cr3 Cr4 P6 -144.8(3) . . . . ? C25 Cr3 Cr4 P6 77.5(3) . . . . ? C22 Cr3 Cr4 P6 -70.8(3) . . . . ? C21 Cr3 Cr4 P6 5.2(3) . . . . ? P10 Cr3 Cr4 P6 72.85(9) . . . . ? P9 Cr3 Cr4 P6 153.65(8) . . . . ? P8 Cr3 Cr4 P6 -132.91(8) . . . . ? P7 Cr3 Cr4 P6 -66.23(8) . . . . ? C24 Cr3 Cr4 P7 -147.9(3) . . . . ? C23 Cr3 Cr4 P7 -78.5(3) . . . . ? C25 Cr3 Cr4 P7 143.7(3) . . . . ? C22 Cr3 Cr4 P7 -4.6(3) . . . . ? C21 Cr3 Cr4 P7 71.5(3) . . . . ? P10 Cr3 Cr4 P7 139.08(8) . . . . ? P9 Cr3 Cr4 P7 -140.12(8) . . . . ? P8 Cr3 Cr4 P7 -66.67(7) . . . . ? P6 Cr3 Cr4 P7 66.23(8) . . . . ? C34 Cr4 C31 C35 37.7(3) . . . . ? C33 Cr4 C31 C35 79.9(4) . . . . ? C32 Cr4 C31 C35 117.5(5) . . . . ? P9 Cr4 C31 C35 -26.8(4) . . . . ? P10 Cr4 C31 C35 -85.3(3) . . . . ? P8 Cr4 C31 C35 97.3(5) . . . . ? P6 Cr4 C31 C35 -142.6(3) . . . . ? P7 Cr4 C31 C35 168.3(3) . . . . ? Cr3 Cr4 C31 C35 -117.3(3) . . . . ? C34 Cr4 C31 C32 -79.8(3) . . . . ? C33 Cr4 C31 C32 -37.7(3) . . . . ? C35 Cr4 C31 C32 -117.5(5) . . . . ? P9 Cr4 C31 C32 -144.3(3) . . . . ? P10 Cr4 C31 C32 157.2(3) . . . . ? P8 Cr4 C31 C32 -20.3(6) . . . . ? P6 Cr4 C31 C32 99.8(3) . . . . ? P7 Cr4 C31 C32 50.8(3) . . . . ? Cr3 Cr4 C31 C32 125.2(3) . . . . ? C34 Cr4 C31 C36 158.7(6) . . . . ? C33 Cr4 C31 C36 -159.2(6) . . . . ? C32 Cr4 C31 C36 -121.6(6) . . . . ? C35 Cr4 C31 C36 120.9(6) . . . . ? P9 Cr4 C31 C36 94.1(5) . . . . ? P10 Cr4 C31 C36 35.7(5) . . . . ? P8 Cr4 C31 C36 -141.8(4) . . . . ? P6 Cr4 C31 C36 -21.7(5) . . . . ? P7 Cr4 C31 C36 -70.8(5) . . . . ? Cr3 Cr4 C31 C36 3.6(7) . . . . ? C35 C31 C32 C33 -0.4(7) . . . . ? C36 C31 C32 C33 -177.4(6) . . . . ? Cr4 C31 C32 C33 62.2(4) . . . . ? C35 C31 C32 C37 176.5(5) . . . . ? C36 C31 C32 C37 -0.5(9) . . . . ? Cr4 C31 C32 C37 -120.8(6) . . . . ? C35 C31 C32 Cr4 -62.6(4) . . . . ? C36 C31 C32 Cr4 120.4(6) . . . . ? C31 Cr4 C32 C33 -116.9(5) . . . . ? C34 Cr4 C32 C33 -37.1(3) . . . . ? C35 Cr4 C32 C33 -79.8(4) . . . . ? P9 Cr4 C32 C33 -24.2(6) . . . . ? P10 Cr4 C32 C33 -148.6(3) . . . . ? P8 Cr4 C32 C33 54.3(4) . . . . ? P6 Cr4 C32 C33 157.6(3) . . . . ? P7 Cr4 C32 C33 104.3(3) . . . . ? Cr3 Cr4 C32 C33 124.8(3) . . . . ? C34 Cr4 C32 C31 79.8(3) . . . . ? C33 Cr4 C32 C31 116.9(5) . . . . ? C35 Cr4 C32 C31 37.1(3) . . . . ? P9 Cr4 C32 C31 92.8(5) . . . . ? P10 Cr4 C32 C31 -31.7(4) . . . . ? P8 Cr4 C32 C31 171.2(3) . . . . ? P6 Cr4 C32 C31 -85.4(3) . . . . ? P7 Cr4 C32 C31 -138.8(3) . . . . ? Cr3 Cr4 C32 C31 -118.3(3) . . . . ? C31 Cr4 C32 C37 120.8(6) . . . . ? C34 Cr4 C32 C37 -159.4(6) . . . . ? C33 Cr4 C32 C37 -122.3(6) . . . . ? C35 Cr4 C32 C37 157.9(5) . . . . ? P9 Cr4 C32 C37 -146.5(4) . . . . ? P10 Cr4 C32 C37 89.1(5) . . . . ? P8 Cr4 C32 C37 -68.0(5) . . . . ? P6 Cr4 C32 C37 35.3(5) . . . . ? P7 Cr4 C32 C37 -18.0(5) . . . . ? Cr3 Cr4 C32 C37 2.5(7) . . . . ? C31 C32 C33 C34 0.0(6) . . . . ? C37 C32 C33 C34 -176.9(5) . . . . ? Cr4 C32 C33 C34 62.0(4) . . . . ? C31 C32 C33 C38 175.4(5) . . . . ? C37 C32 C33 C38 -1.5(10) . . . . ? Cr4 C32 C33 C38 -122.6(6) . . . . ? C31 C32 C33 Cr4 -62.1(4) . . . . ? C37 C32 C33 Cr4 121.0(6) . . . . ? C31 Cr4 C33 C34 -79.7(4) . . . . ? C32 Cr4 C33 C34 -117.7(5) . . . . ? C35 Cr4 C33 C34 -37.6(3) . . . . ? P9 Cr4 C33 C34 51.5(4) . . . . ? P10 Cr4 C33 C34 -38.8(6) . . . . ? P8 Cr4 C33 C34 106.8(3) . . . . ? P6 Cr4 C33 C34 -149.1(3) . . . . ? P7 Cr4 C33 C34 160.5(3) . . . . ? Cr3 Cr4 C33 C34 119.2(4) . . . . ? C31 Cr4 C33 C32 38.0(3) . . . . ? C34 Cr4 C33 C32 117.7(5) . . . . ? C35 Cr4 C33 C32 80.1(4) . . . . ? P9 Cr4 C33 C32 169.2(3) . . . . ? P10 Cr4 C33 C32 78.9(5) . . . . ? P8 Cr4 C33 C32 -135.5(3) . . . . ? P6 Cr4 C33 C32 -31.4(4) . . . . ? P7 Cr4 C33 C32 -81.8(3) . . . . ? Cr3 Cr4 C33 C32 -123.1(3) . . . . ? C31 Cr4 C33 C38 160.0(6) . . . . ? C34 Cr4 C33 C38 -120.3(6) . . . . ? C32 Cr4 C33 C38 122.1(6) . . . . ? C35 Cr4 C33 C38 -157.9(6) . . . . ? P9 Cr4 C33 C38 -68.8(5) . . . . ? P10 Cr4 C33 C38 -159.0(3) . . . . ? P8 Cr4 C33 C38 -13.4(5) . . . . ? P6 Cr4 C33 C38 90.6(5) . . . . ? P7 Cr4 C33 C38 40.2(5) . . . . ? Cr3 Cr4 C33 C38 -1.1(7) . . . . ? C32 C33 C34 C35 0.5(7) . . . . ? C38 C33 C34 C35 -175.0(5) . . . . ? Cr4 C33 C34 C35 62.4(4) . . . . ? C32 C33 C34 C39 173.9(5) . . . . ? C38 C33 C34 C39 -1.6(9) . . . . ? Cr4 C33 C34 C39 -124.2(6) . . . . ? C32 C33 C34 Cr4 -62.0(4) . . . . ? C38 C33 C34 Cr4 122.5(6) . . . . ? C31 Cr4 C34 C33 80.3(4) . . . . ? C32 Cr4 C34 C33 37.5(3) . . . . ? C35 Cr4 C34 C33 117.6(5) . . . . ? P9 Cr4 C34 C33 -137.5(3) . . . . ? P10 Cr4 C34 C33 163.1(3) . . . . ? P8 Cr4 C34 C33 -79.9(3) . . . . ? P6 Cr4 C34 C33 79.3(5) . . . . ? P7 Cr4 C34 C33 -28.6(4) . . . . ? Cr3 Cr4 C34 C33 -125.4(3) . . . . ? C31 Cr4 C34 C35 -37.3(3) . . . . ? C33 Cr4 C34 C35 -117.6(5) . . . . ? C32 Cr4 C34 C35 -80.2(4) . . . . ? P9 Cr4 C34 C35 104.9(3) . . . . ? P10 Cr4 C34 C35 45.5(4) . . . . ? P8 Cr4 C34 C35 162.5(3) . . . . ? P6 Cr4 C34 C35 -38.3(6) . . . . ? P7 Cr4 C34 C35 -146.2(3) . . . . ? Cr3 Cr4 C34 C35 117.0(3) . . . . ? C31 Cr4 C34 C39 -159.1(6) . . . . ? C33 Cr4 C34 C39 120.6(7) . . . . ? C32 Cr4 C34 C39 158.0(6) . . . . ? C35 Cr4 C34 C39 -121.8(7) . . . . ? P9 Cr4 C34 C39 -16.9(5) . . . . ? P10 Cr4 C34 C39 -76.3(5) . . . . ? P8 Cr4 C34 C39 40.7(5) . . . . ? P6 Cr4 C34 C39 -160.1(3) . . . . ? P7 Cr4 C34 C39 92.0(5) . . . . ? Cr3 Cr4 C34 C39 -4.8(7) . . . . ? C32 C31 C35 C34 0.7(7) . . . . ? C36 C31 C35 C34 177.8(5) . . . . ? Cr4 C31 C35 C34 -61.4(4) . . . . ? C32 C31 C35 C40 -176.3(6) . . . . ? C36 C31 C35 C40 0.8(10) . . . . ? Cr4 C31 C35 C40 121.6(6) . . . . ? C32 C31 C35 Cr4 62.2(4) . . . . ? C36 C31 C35 Cr4 -120.8(6) . . . . ? C33 C34 C35 C31 -0.8(7) . . . . ? C39 C34 C35 C31 -174.1(6) . . . . ? Cr4 C34 C35 C31 61.6(4) . . . . ? C33 C34 C35 C40 176.3(5) . . . . ? C39 C34 C35 C40 3.0(10) . . . . ? Cr4 C34 C35 C40 -121.4(6) . . . . ? C33 C34 C35 Cr4 -62.3(4) . . . . ? C39 C34 C35 Cr4 124.4(6) . . . . ? C34 Cr4 C35 C31 -117.4(5) . . . . ? C33 Cr4 C35 C31 -80.2(4) . . . . ? C32 Cr4 C35 C31 -37.7(3) . . . . ? P9 Cr4 C35 C31 161.8(3) . . . . ? P10 Cr4 C35 C31 99.3(3) . . . . ? P8 Cr4 C35 C31 -144.2(3) . . . . ? P6 Cr4 C35 C31 46.4(4) . . . . ? P7 Cr4 C35 C31 -27.0(6) . . . . ? Cr3 Cr4 C35 C31 120.2(3) . . . . ? C31 Cr4 C35 C34 117.4(5) . . . . ? C33 Cr4 C35 C34 37.1(3) . . . . ? C32 Cr4 C35 C34 79.6(4) . . . . ? P9 Cr4 C35 C34 -80.9(3) . . . . ? P10 Cr4 C35 C34 -143.3(3) . . . . ? P8 Cr4 C35 C34 -26.9(5) . . . . ? P6 Cr4 C35 C34 163.8(3) . . . . ? P7 Cr4 C35 C34 90.4(5) . . . . ? Cr3 Cr4 C35 C34 -122.5(3) . . . . ? C31 Cr4 C35 C40 -122.9(6) . . . . ? C34 Cr4 C35 C40 119.7(7) . . . . ? C33 Cr4 C35 C40 156.9(6) . . . . ? C32 Cr4 C35 C40 -160.7(6) . . . . ? P9 Cr4 C35 C40 38.9(5) . . . . ? P10 Cr4 C35 C40 -23.6(5) . . . . ? P8 Cr4 C35 C40 92.9(5) . . . . ? P6 Cr4 C35 C40 -76.5(5) . . . . ? P7 Cr4 C35 C40 -149.9(4) . . . . ? Cr3 Cr4 C35 C40 -2.7(7) . . . . ? #===END