# Electronic Supplementary Material (ESI) for Journal of Materials Chemistry # This journal is © The Royal Society of Chemistry 2011 data_global _journal_name_full J.Mater.Chem. _journal_coden_cambridge 1145 _journal_coden_ASTM ? _journal_coeditor_code ? _journal_coeditor_name ? _journal_coeditor_notes ; ? ; #============================================================================== # 2. PROCESSING SUMMARY (IUCr Office Use Only) _journal_data_validation_number ? _journal_date_accepted ? _journal_date_from_coeditor ? _journal_date_printers_final ? _journal_date_printers_first ? _journal_date_proofs_in ? _journal_date_proofs_out ? _journal_date_recd_electronic ? _journal_date_to_coeditor ? _journal_issue ? _journal_page_first ? _journal_page_last ? _journal_paper_category ? _journal_suppl_publ_number ? _journal_suppl_publ_pages ? _journal_techeditor_code ? _journal_techeditor_notes ; ? ; _journal_volume ? _journal_year ? loop_ _publ_author_name _publ_author_footnote _publ_author_address 'Deyin Wang' ; ? ; ; ? ; 'Yun-Chen Wu' '' '' 'Teng-Ming Chen' '' '' _publ_contact_author_address # Address of author for correspondence ; ? ; _publ_contact_author_email tmchen@mail.nctu.edu.tw _publ_contact_author_fax ? _publ_contact_author_phone ? #============================================================================= # this information describes the project, paper etc. for the CIF # # Acta Cryst. Section C papers and editorial correspondence is generated # # from the information in this section # # # # (from) CIF submission form for Rietveld refinements (Acta Cryst. C) # # Version 14 December 1998 # #============================================================================= # 1. SUBMISSION DETAILS _publ_contact_author_name 'Deyin Wang' # Name of author for correspondence _publ_contact_letter ; ? ; _publ_requested_category ? # Acta C: one of CI/CM/CO/FI/FM/FO _publ_requested_coeditor_name ? #============================================================================== # 3. TITLE AND AUTHOR LIST _publ_section_title ; ? ; data_BHS_publ _database_code_depnum_ccdc_archive 'CCDC 843445' #TrackingRef '- BaHfSi3O9.cif' _pd_block_id 2011-06-27T22:16|BHS|D.Y.Wang|D8 _audit_creation_method 'from EXP file using GSAS2CIF' _audit_creation_date 2011-06-27T22:16 _audit_author_name D.Y.Wang _audit_update_record ; 2011-06-27T22:16 Initial CIF as created by GSAS2CIF ; _publ_section_title_footnote ; ? ; #============================================================================== # 4. TEXT _publ_section_synopsis ; ? ; _publ_section_abstract ; ? ; _publ_section_comment ; ? ; _publ_section_exptl_prep # Details of the preparation of the sample(s) # should be given here. ; ? ; _publ_section_exptl_refinement ; ? ; _publ_section_references ; ? ; _publ_section_figure_captions ; ? ; _publ_section_acknowledgements ; ? ; #============================================================================= # 5. OVERALL REFINEMENT & COMPUTING DETAILS _refine_special_details ; ? ; _pd_proc_ls_special_details ; ? ; # The following items are used to identify the programs used. _computing_molecular_graphics ? _computing_publication_material ? _refine_ls_weighting_scheme ? _refine_ls_weighting_details ? _refine_ls_hydrogen_treatment ? _refine_ls_extinction_method ? _refine_ls_extinction_coef ? _refine_ls_number_constraints ? _refine_ls_restrained_S_all ? _refine_ls_restrained_S_obs ? #============================================================================== # 6. SAMPLE PREPARATION DATA # (In the unusual case where multiple samples are used in a single # Rietveld study, this information should be moved into the phase # blocks) # The following three fields describe the preparation of the material. # The cooling rate is in K/min. The pressure at which the sample was # prepared is in kPa. The temperature of preparation is in K. _pd_prep_cool_rate ? _pd_prep_pressure ? _pd_prep_temperature ? _pd_char_colour ? # use ICDD colour descriptions _refine_ls_shift/su_max 0.06 _refine_ls_shift/su_mean 0.01 _computing_structure_refinement GSAS _refine_ls_number_parameters 16 _refine_ls_goodness_of_fit_all 2.12 _refine_ls_number_restraints 0 _refine_ls_matrix_type full #============================================================================== # 7. CHEMICAL, STRUCTURAL AND CRYSTAL DATA _pd_char_particle_morphology ? _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_melting_point ? _chemical_compound_source ? # for minerals and # natural products _symmetry_space_group_name_Hall ? _exptl_crystal_F_000 ? _exptl_crystal_density_diffrn ? _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _cell_measurement_temperature ? _cell_special_details ; ? ; _geom_special_details ? # The following item identifies the program(s) used (if appropriate). _computing_structure_solution ? #============================================================================== # 8. Phase information from GSAS _pd_phase_name 'from D:/BHS/BaZrSi3O9.cif' _cell_length_a 6.77318(8) _cell_length_b 6.77318 _cell_length_c 10.00456(20) _cell_angle_alpha 90.0 _cell_angle_beta 90.0 _cell_angle_gamma 120.0 _cell_volume 397.479(7) _symmetry_cell_setting hexagonal _symmetry_space_group_name_H-M 'P -6 c 2' loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 +x,+y,+z 2 y-x,-x,-z+1/2 3 -y,x-y,+z 4 +x,+y,-z+1/2 5 y-x,-x,+z 6 -y,x-y,-z+1/2 7 y-x,+y,+z+1/2 8 +x,x-y,-z 9 -y,-x,+z+1/2 10 y-x,+y,-z 11 +x,x-y,+z+1/2 12 -y,-x,-z # ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_thermal_displace_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity Ba Ba 0.66667 0.33333 0.0 1.0 Uiso 0.0150(14) 2 Hf Hf 0.33333 0.66667 0.0 1.0 Uiso 0.0108(9) 2 Si Si 0.04979 0.27375 0.25 1.0 Uiso 0.0059(17) 6 O O1 0.25194 0.17981 0.25 1.0 Uiso 0.023(5) 6 O O2 0.07434 0.42128 0.12342 1.0 Uiso 0.0096(26) 12 # If you change Z, be sure to change all 3 of the following _chemical_formula_sum 'Ba Hf O9 Si3' _chemical_formula_weight 544.07 _cell_formula_units_Z 2 # MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_publ_flag ? ? ? ? ? ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle_publ_flag ? ? ? ? ? ? ? ? # Powder diffraction data for histogram 1 #============================================================================== # 9. INSTRUMENT CHARACTERIZATION _exptl_special_details ; ? ; # if regions of the data are excluded, the reason(s) are supplied here: _pd_proc_info_excluded_regions ; ? ; # The following item is used to identify the equipment used to record # the powder pattern when the diffractogram was measured at a laboratory # other than the authors' home institution, e.g. when neutron or synchrotron # radiation is used. _pd_instr_location ; ? ; _pd_calibration_special_details # description of the method used # to calibrate the instrument ; ? ; _diffrn_ambient_temperature ? _diffrn_source ? _diffrn_source_target ? _diffrn_source_type ? _diffrn_measurement_device_type ? _diffrn_detector ? _diffrn_detector_type ? # make or model of detector _pd_meas_scan_method ? # options are 'step', 'cont', # 'tof', 'fixed' or # 'disp' (= dispersive) _pd_meas_special_details ; ? ; # The following two items identify the program(s) used (if appropriate). _computing_data_collection ? _computing_data_reduction ? # Describe any processing performed on the data, prior to refinement. # For example: a manual Lp correction or a precomputed absorption correction _pd_proc_info_data_reduction ? # The following item is used for angular dispersive measurements only. _diffrn_radiation_monochromator ? # The following items are used to define the size of the instrument. # Not all distances are appropriate for all instrument types. _pd_instr_dist_src/mono ? _pd_instr_dist_mono/spec ? _pd_instr_dist_src/spec ? _pd_instr_dist_spec/anal ? _pd_instr_dist_anal/detc ? _pd_instr_dist_spec/detc ? # 10. Specimen size and mounting information # The next three fields give the specimen dimensions in mm. The equatorial # plane contains the incident and diffracted beam. _pd_spec_size_axial ? # perpendicular to # equatorial plane _pd_spec_size_equat ? # parallel to # scattering vector # in transmission _pd_spec_size_thick ? # parallel to # scattering vector # in reflection _pd_spec_mounting # This field should be # used to give details of the # container. ; ? ; _pd_spec_mount_mode ? # options are 'reflection' # or 'transmission' _pd_spec_shape ? # options are 'cylinder' # 'flat_sheet' or 'irregular' loop_ _atom_type_symbol _atom_type_number_in_cell _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source Ba 2.0 0.000 0.000 20.3361 3.21600 19.2970 0.27560 10.8880 20.2073 2.69590 167.202 2.77310 International_Tables_Vol_C Hf 2.0 0.000 0.000 29.1440 1.83262 15.1726 9.59990 14.7586 0.27512 4.30013 72.0290 8.58154 International_Tables_Vol_C Si 6.0 0.000 0.000 6.29150 2.43860 3.03530 32.3337 1.98910 0.67850 1.54100 81.6937 1.14070 International_Tables_Vol_C O 18.0 0.000 0.000 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700 32.9089 0.25080 International_Tables_Vol_C _diffrn_radiation_probe x-ray _diffrn_radiation_polarisn_ratio 0.7 loop_ _diffrn_radiation_wavelength _diffrn_radiation_wavelength_wt _diffrn_radiation_type _diffrn_radiation_wavelength_id 1.540500 1.000 K\a~1~ 1 1.544300 0.508 K\a~2~ 2 _pd_proc_ls_prof_R_factor 0.0779 _pd_proc_ls_prof_wR_factor 0.1185 _pd_proc_ls_prof_wR_expected 0.0560 _refine_ls_R_Fsqd_factor 0.08928 _pd_proc_ls_background_function ; GSAS Background function number 1 with 6 terms. Shifted Chebyshev function of 1st kind 1: 184.514 2: -26.0141 3: 17.1603 4: 4.24306 5: -2.86347 6: 0.188043 ; _exptl_absorpt_process_details ; GSAS Absorption/surface roughness correction: function number 0 No correction is applied. ; _exptl_absorpt_correction_T_min 1.00000 _exptl_absorpt_correction_T_max 1.00000 # Extinction correction _gsas_exptl_extinct_corr_T_min 1.00000 _gsas_exptl_extinct_corr_T_max 1.00000 _pd_proc_ls_profile_function ; CW Profile function number 2 with 18 terms Profile coefficients for Simpson's rule integration of pseudovoigt function C.J. Howard (1982). J. Appl. Cryst.,15,615-620. P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83. #1(GU) = 3.396 #2(GV) = -4.185 #3(GW) = 31.331 #4(LX) = 1.141 #5(LY) = 10.203 #6(trns) = 1.840 #7(asym) = -1.0484 #8(shft) = -0.4330 #9(GP) = 0.792 #10(stec)= 2.95 #11(ptec)= -0.25 #12(sfec)= 0.00 #13(L11) = 0.015 #14(L22) = 0.013 #15(L33) = 0.006 #16(L12) = 0.009 #17(L13) = -0.004 #18(L23) = 0.004 Peak tails are ignored where the intensity is below 0.0100 times the peak Aniso. broadening axis 0.0 0.0 1.0 ; _pd_proc_ls_peak_cutoff 0.01000 _pd_proc_info_datetime 2011-06-27T22:16:52 _pd_calc_method 'Rietveld Refinement' #---- raw/calc data loop ----- _pd_meas_2theta_range_min 10.0 _pd_meas_2theta_range_max 119.719 _pd_meas_2theta_range_inc 0.0167 _pd_proc_2theta_range_min 10.0 _pd_proc_2theta_range_max 119.719 _pd_proc_2theta_range_inc 0.0167 loop_ _pd_meas_counts_total _pd_proc_ls_weight _pd_proc_intensity_bkg_calc _pd_calc_intensity_total 226.0 0.00442 220.39383 220.39526 251.0 0.00398 220.39200 220.39343 238.0 0.00420 220.39015 220.39157 257.0 0.00389 220.38828 220.38966 259.0 0.00386 220.38637 220.38777 244.0 0.00410 220.38445 220.38582 249.0 0.00402 220.38246 220.38385 231.0 0.00433 220.38046 220.38185 239.0 0.00418 220.37845 220.37984 238.0 0.00420 220.37639 220.37778 242.0 0.00413 220.37433 220.37569 226.0 0.00442 220.37221 220.37358 245.0 0.00408 220.37010 220.37144 266.0 0.00376 220.36794 220.36931 244.0 0.00410 220.36575 220.36710 238.0 0.00420 220.36354 220.36488 264.0 0.00379 220.36130 220.36263 249.0 0.00402 220.35902 220.36037 227.0 0.00441 220.35674 220.35806 239.0 0.00418 220.35443 220.35573 261.0 0.00383 220.35208 220.35339 251.0 0.00398 220.34970 220.35101 252.0 0.00397 220.34729 220.34859 261.0 0.00383 220.34486 220.34613 236.0 0.00424 220.34239 220.34369 229.0 0.00437 220.33990 220.34119 233.0 0.00429 220.33739 220.33868 227.0 0.00441 220.33485 220.33614 265.0 0.00377 220.33228 220.33356 234.0 0.00427 220.32968 220.33096 226.0 0.00442 220.32707 220.32832 266.0 0.00376 220.32442 220.32570 218.0 0.00459 220.32176 220.32300 206.0 0.00485 220.31903 220.32030 250.0 0.00400 220.31631 220.31755 266.0 0.00376 220.31357 220.31479 200.0 0.00500 220.31078 220.31201 253.0 0.00395 220.30797 220.30920 249.0 0.00402 220.30511 220.30637 222.0 0.00450 220.30228 220.30348 249.0 0.00402 220.29936 220.30057 246.0 0.00407 220.29643 220.29765 232.0 0.00431 220.29349 220.29469 253.0 0.00395 220.29051 220.29173 237.0 0.00422 220.28752 220.28871 220.0 0.00455 220.28450 220.28569 232.0 0.00431 220.28143 220.28262 229.0 0.00437 220.27837 220.27954 226.0 0.00442 220.27527 220.27643 215.0 0.00465 220.27213 220.27328 209.0 0.00478 220.26895 220.27014 243.0 0.00412 220.26579 220.26697 246.0 0.00407 220.26257 220.26375 239.0 0.00418 220.25934 220.26047 204.0 0.00490 220.25607 220.25720 235.0 0.00426 220.25278 220.25391 234.0 0.00427 220.24944 220.25058 249.0 0.00402 220.24608 220.24725 233.0 0.00429 220.24272 220.24387 255.0 0.00392 220.23932 220.24045 238.0 0.00420 220.23592 220.23700 238.0 0.00420 220.23244 220.23355 235.0 0.00426 220.22896 220.23007 236.0 0.00424 220.22546 220.22659 201.0 0.00498 220.22194 220.22305 247.0 0.00405 220.21838 220.21947 232.0 0.00431 220.21481 220.21588 224.0 0.00446 220.21120 220.21228 209.0 0.00478 220.20755 220.20862 250.0 0.00400 220.20389 220.20497 208.0 0.00481 220.20020 220.20126 235.0 0.00426 220.19650 220.19757 236.0 0.00424 220.19273 220.19380 227.0 0.00441 220.18896 220.19002 224.0 0.00446 220.18518 220.18623 221.0 0.00452 220.18135 220.18242 228.0 0.00439 220.17752 220.17856 226.0 0.00442 220.17363 220.17470 224.0 0.00446 220.16975 220.17078 233.0 0.00429 220.16582 220.16685 217.0 0.00461 220.16187 220.16290 232.0 0.00431 220.15788 220.15892 230.0 0.00435 220.15388 220.15491 215.0 0.00465 220.14987 220.15089 232.0 0.00431 220.14581 220.14682 239.0 0.00418 220.14174 220.14275 245.0 0.00408 220.13762 220.13863 226.0 0.00442 220.13350 220.13448 235.0 0.00426 220.12932 220.13033 232.0 0.00431 220.12515 220.12613 217.0 0.00461 220.12094 220.12193 226.0 0.00442 220.11668 220.11768 254.0 0.00394 220.11244 220.11343 224.0 0.00446 220.10814 220.10915 232.0 0.00431 220.10384 220.10480 225.0 0.00444 220.09952 220.10048 232.0 0.00431 220.09514 220.09612 249.0 0.00402 220.09074 220.09171 226.0 0.00442 220.08633 220.08730 245.0 0.00408 220.08191 220.08284 232.0 0.00431 220.07744 220.07838 210.0 0.00476 220.07294 220.07388 210.0 0.00476 220.06842 220.06937 232.0 0.00431 220.06389 220.06480 232.0 0.00431 220.05930 220.06024 219.0 0.00457 220.05473 220.05565 227.0 0.00441 220.05011 220.05103 226.0 0.00442 220.04547 220.04639 220.0 0.00455 220.04079 220.04170 227.0 0.00441 220.03607 220.03700 212.0 0.00472 220.03139 220.03227 217.0 0.00461 220.02661 220.02753 223.0 0.00448 220.02185 220.02275 190.0 0.00526 220.01704 220.01796 210.0 0.00476 220.01224 220.01314 232.0 0.00431 220.00739 220.00827 232.0 0.00431 220.00253 220.00339 202.0 0.00495 219.99763 219.99850 228.0 0.00439 219.99271 219.99356 225.0 0.00444 219.98776 219.98862 222.0 0.00450 219.98277 219.98364 223.0 0.00448 219.97778 219.97862 212.0 0.00472 219.97275 219.97360 234.0 0.00427 219.96770 219.96858 204.0 0.00490 219.96263 219.96349 226.0 0.00442 219.95753 219.95839 234.0 0.00427 219.95241 219.95326 207.0 0.00483 219.94725 219.94812 226.0 0.00442 219.94209 219.94292 235.0 0.00426 219.93690 219.93773 223.0 0.00448 219.93167 219.93251 233.0 0.00429 219.92642 219.92725 244.0 0.00410 219.92114 219.92198 205.0 0.00488 219.91586 219.91667 209.0 0.00478 219.91054 219.91135 226.0 0.00442 219.90520 219.90599 242.0 0.00413 219.89981 219.90062 207.0 0.00483 219.89441 219.89522 251.0 0.00398 219.88898 219.88980 242.0 0.00413 219.88354 219.88435 217.0 0.00461 219.87807 219.87886 234.0 0.00427 219.87257 219.87337 195.0 0.00513 219.86707 219.86784 199.0 0.00503 219.86151 219.86230 215.0 0.00465 219.85596 219.85674 218.0 0.00459 219.85036 219.85114 220.0 0.00455 219.84473 219.84552 192.0 0.00521 219.83910 219.83986 238.0 0.00420 219.83344 219.83420 219.0 0.00457 219.82774 219.82849 221.0 0.00452 219.82202 219.82278 192.0 0.00521 219.81628 219.81703 228.0 0.00439 219.81050 219.81125 236.0 0.00424 219.80470 219.80547 229.0 0.00437 219.79890 219.79965 222.0 0.00450 219.79306 219.79381 223.0 0.00448 219.78719 219.78793 222.0 0.00450 219.78133 219.78204 234.0 0.00427 219.77541 219.77614 233.0 0.00429 219.76947 219.77017 223.0 0.00448 219.76350 219.76422 219.0 0.00457 219.75752 219.75824 218.0 0.00459 219.75151 219.75223 226.0 0.00442 219.74548 219.74620 219.0 0.00457 219.73943 219.74014 235.0 0.00426 219.73335 219.73404 217.0 0.00461 219.72723 219.72794 213.0 0.00469 219.72112 219.72180 224.0 0.00446 219.71495 219.71565 234.0 0.00427 219.70877 219.70946 204.0 0.00490 219.70256 219.70325 238.0 0.00420 219.69633 219.69704 224.0 0.00446 219.69009 219.69078 203.0 0.00493 219.68384 219.68451 233.0 0.00429 219.67752 219.67821 222.0 0.00450 219.67120 219.67188 234.0 0.00427 219.66486 219.66554 215.0 0.00465 219.65848 219.65915 220.0 0.00455 219.65210 219.65276 245.0 0.00408 219.64568 219.64636 221.0 0.00452 219.63925 219.63988 204.0 0.00490 219.63278 219.63344 198.0 0.00505 219.62630 219.62694 230.0 0.00435 219.61977 219.62041 224.0 0.00446 219.61324 219.61388 204.0 0.00490 219.60667 219.60733 224.0 0.00446 219.60008 219.60072 203.0 0.00493 219.59348 219.59412 224.0 0.00446 219.58685 219.58749 204.0 0.00490 219.58020 219.58083 249.0 0.00402 219.57352 219.57414 227.0 0.00441 219.56682 219.56744 195.0 0.00513 219.56009 219.56071 212.0 0.00472 219.55334 219.55399 196.0 0.00510 219.54659 219.54718 215.0 0.00465 219.53978 219.54039 226.0 0.00442 219.53296 219.53358 218.0 0.00459 219.52614 219.52672 203.0 0.00493 219.51926 219.51985 238.0 0.00420 219.51237 219.51297 227.0 0.00441 219.50545 219.50604 213.0 0.00469 219.49850 219.49911 217.0 0.00461 219.49155 219.49214 224.0 0.00446 219.48457 219.48515 200.0 0.00500 219.47757 219.47815 244.0 0.00410 219.47052 219.47113 255.0 0.00392 219.46347 219.46407 232.0 0.00431 219.45641 219.45697 209.0 0.00478 219.44931 219.44987 216.0 0.00463 219.44218 219.44273 208.0 0.00481 219.43504 219.43561 216.0 0.00463 219.42786 219.42844 222.0 0.00450 219.42068 219.42123 221.0 0.00452 219.41347 219.41402 220.0 0.00455 219.40623 219.40675 218.0 0.00459 219.39896 219.39951 221.0 0.00452 219.39168 219.39223 234.0 0.00427 219.38438 219.38490 211.0 0.00474 219.37703 219.37758 211.0 0.00474 219.36967 219.37022 226.0 0.00442 219.36229 219.36284 207.0 0.00483 219.35492 219.35544 239.0 0.00418 219.34747 219.34802 239.0 0.00418 219.34004 219.34056 213.0 0.00469 219.33255 219.33310 197.0 0.00508 219.32507 219.32561 212.0 0.00472 219.31758 219.31808 215.0 0.00465 219.31003 219.31053 199.0 0.00503 219.30246 219.30298 230.0 0.00435 219.29488 219.29539 217.0 0.00461 219.28729 219.28780 208.0 0.00481 219.27965 219.28015 212.0 0.00472 219.27202 219.27251 247.0 0.00405 219.26433 219.26483 196.0 0.00510 219.25662 219.25713 199.0 0.00503 219.24889 219.24942 204.0 0.00490 219.24115 219.24167 199.0 0.00503 219.23340 219.23392 209.0 0.00478 219.22562 219.22612 211.0 0.00474 219.21779 219.21829 206.0 0.00485 219.20998 219.21045 230.0 0.00435 219.20212 219.20261 213.0 0.00469 219.19424 219.19472 195.0 0.00513 219.18636 219.18683 232.0 0.00431 219.17844 219.17891 207.0 0.00483 219.17049 219.17094 258.0 0.00388 219.16252 219.16296 229.0 0.00437 219.15454 219.15500 202.0 0.00495 219.14651 219.14697 221.0 0.00452 219.13850 219.13895 222.0 0.00450 219.13040 219.13089 200.0 0.00500 219.12233 219.12282 234.0 0.00427 219.11423 219.11469 218.0 0.00459 219.10611 219.10657 217.0 0.00461 219.09796 219.09840 238.0 0.00420 219.08980 219.09026 207.0 0.00483 219.08160 219.08208 226.0 0.00442 219.07339 219.07385 218.0 0.00459 219.06517 219.06561 206.0 0.00485 219.05692 219.05734 221.0 0.00452 219.04861 219.04907 225.0 0.00444 219.04034 219.04076 226.0 0.00442 219.03201 219.03244 251.0 0.00398 219.02367 219.02409 212.0 0.00472 219.01532 219.01572 207.0 0.00483 219.00693 219.00732 223.0 0.00448 218.99849 218.99892 238.0 0.00420 218.99005 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220.60690 230.0 0.00435 173.35349 221.96733 221.0 0.00452 173.36578 222.46544 221.0 0.00452 173.37810 222.05800 195.0 0.00513 173.39040 219.25610 213.0 0.00469 173.40269 217.39482 215.0 0.00465 173.41499 215.07666 209.0 0.00478 173.42729 212.49739 195.0 0.00513 173.43961 209.82204 211.0 0.00474 173.45193 207.18068 209.0 0.00478 173.46423 204.67346 203.0 0.00493 173.47655 202.67195 204.0 0.00490 173.48885 200.65016 185.0 0.00541 173.50114 198.93529 197.0 0.00508 173.51346 197.55103 194.0 0.00515 173.52576 196.50841 198.0 0.00505 173.53809 195.80827 197.0 0.00508 173.55038 195.44475 169.0 0.00592 173.56271 195.40443 199.0 0.00503 173.57501 195.66898 192.0 0.00521 173.58731 196.21375 202.0 0.00495 173.59962 197.00606 200.0 0.00500 173.61194 198.00194 209.0 0.00478 173.62425 199.14148 185.0 0.00541 173.63655 200.34479 203.0 0.00493 173.64888 201.51038 215.0 0.00465 173.66119 202.52100 186.0 0.00538 173.67351 203.26033 206.0 0.00485 173.68582 203.63867 215.0 0.00465 173.69814 203.61880 204.0 0.00490 173.71045 202.43794 185.0 0.00541 173.72278 201.78090 206.0 0.00485 173.73509 200.95500 202.0 0.00495 173.74742 200.08263 187.0 0.00535 173.75974 199.27220 229.0 0.00437 173.77205 198.61021 206.0 0.00485 173.78436 198.16101 234.0 0.00427 173.79668 197.97058 195.0 0.00513 173.80899 198.07071 198.0 0.00505 173.82130 198.48248 209.0 0.00478 173.83363 199.21846 183.0 0.00546 173.84595 200.28407 200.0 0.00500 173.85825 201.67439 195.0 0.00513 173.87061 203.37639 212.0 0.00472 173.88289 205.36301 204.0 0.00490 173.89522 207.58910 212.0 0.00472 173.90756 209.98636 198.0 0.00505 173.91986 212.46019 207.0 0.00483 173.93217 214.89293 226.0 0.00442 173.94450 217.15903 232.0 0.00431 173.95682 219.15318 243.0 0.00412 173.96916 220.82535 242.0 0.00413 173.98146 222.20697 261.0 0.00383 173.99377 223.41385 265.0 0.00377 174.00610 224.62282 234.0 0.00427 174.01843 226.03532 260.0 0.00385 174.03075 227.83772 226.0 0.00442 174.04308 230.18242 221.0 0.00452 174.05537 233.17159 241.0 0.00415 174.06772 236.85106 238.0 0.00420 174.08005 241.20294 239.0 0.00418 174.09235 246.13338 280.0 0.00357 174.10466 251.48442 266.0 0.00376 174.11697 256.89670 259.0 0.00386 174.12932 261.91379 273.0 0.00366 174.14163 266.16211 278.0 0.00360 174.15398 269.05811 289.0 0.003460 174.16628 270.20212 272.0 0.00368 174.17859 269.44449 295.0 0.003390 174.19093 266.92773 314.0 0.003185 174.20325 263.03220 279.0 0.00358 174.21556 258.24866 305.0 0.003279 174.22789 253.04924 252.0 0.00397 174.24020 247.80638 282.0 0.00355 174.25253 242.76678 282.0 0.00355 174.26485 238.06313 241.0 0.00415 174.27719 233.74556 253.0 0.00395 174.28951 229.81943 232.0 0.00431 174.30182 226.28040 230.0 0.00435 174.31415 223.13847 208.0 0.00481 174.32648 220.42432 200.0 0.00500 174.33881 218.18861 218.0 0.00459 174.35112 216.47865 203.0 0.00493 174.36343 215.33176 194.0 0.00515 174.37575 214.76649 199.0 0.00503 174.38808 214.48088 223.0 0.00448 174.40042 215.04974 208.0 0.00481 174.41270 216.11298 209.0 0.00478 174.42503 217.58238 206.0 0.00485 174.43738 219.32744 236.0 0.00424 174.44969 221.18130 214.0 0.00467 174.46202 222.84419 223.0 0.00448 174.47433 224.12227 256.0 0.00391 174.48666 224.71136 209.0 0.00478 174.49898 224.40871 241.0 0.00415 174.51131 223.13905 238.0 0.00420 174.52364 220.97627 219.0 0.00457 174.53592 218.11293 208.0 0.00481 174.54826 214.79666 246.0 0.00407 174.56058 211.26871 215.0 0.00465 174.57291 207.72643 226.0 0.00442 174.58524 204.31142 216.0 0.00463 174.59755 201.11467 220.0 0.00455 174.60985 198.18796 201.0 0.00498 174.62215 195.55446 169.0 0.00592 174.63449 193.21674 175.0 0.00571 174.64682 191.16820 192.0 0.00521 174.65913 189.38957 187.0 0.00535 174.67143 187.85747 183.0 0.00546 174.68378 186.54596 189.0 0.00529 174.69609 185.42792 194.0 0.00515 174.70840 184.32256 184.0 0.00543 174.72072 183.51724 195.0 0.00513 174.73303 182.83130 181.0 0.00552 174.74535 182.24487 173.0 0.00578 174.75768 181.74106 169.0 0.00592 174.76997 181.69359 175.0 0.00571 174.78229 181.32431 159.0 0.00629 174.79460 181.00276 193.0 0.00518 174.80693 180.72166 183.0 0.00546 174.81921 180.47516 192.0 0.00521 174.83154 180.25893 184.0 0.00543 174.84386 180.06972 178.0 0.00562 174.85619 179.90514 182.0 0.00549 174.86850 179.76363 184.0 0.00543 174.88080 179.64421 161.0 0.00621 174.89310 179.54665 177.0 0.00565 174.90543 179.47107 190.0 0.00526 174.91774 179.41823 190.0 0.00526 174.93002 179.38925 181.0 0.00552 174.94234 179.38568 187.0 0.00535 174.95468 179.40929 192.0 0.00521 174.96698 179.46202 175.0 0.00571 174.97928 179.54584 165.0 0.00606 174.99159 179.43044 147.0 0.00680 175.00388 179.58650 159.0 0.00629 175.01620 179.77693 180.0 0.00556 175.02849 180.00095 187.0 0.00535 175.04082 180.25601 172.0 0.00581 175.05310 180.53674 188.0 0.00532 175.06543 180.83400 184.0 0.00543 175.07776 181.13388 150.0 0.00667 175.09006 181.41618 186.0 0.00538 175.10236 181.65643 175.0 0.00571 175.11465 181.82834 162.0 0.00617 175.12695 182.11389 181.0 0.00552 175.13927 182.09894 187.0 0.00535 175.15157 181.98630 183.0 0.00546 175.16388 181.79303 198.0 0.00505 175.17616 181.54425 175.0 0.00571 175.18845 180.69398 179.0 0.00559 175.20074 180.42349 172.0 0.00581 175.21306 180.16417 166.0 0.00602 175.22533 179.92825 192.0 0.00521 175.23764 179.72380 190.0 0.00526 175.24995 179.55537 171.0 0.00585 175.26222 179.42590 181.0 0.00552 175.27454 179.33646 177.0 0.00565 175.28682 179.28726 181.0 0.00552 175.29910 179.27805 166.0 0.00602 175.31140 179.18658 172.0 0.00581 175.32372 179.25792 168.0 0.00595 175.33601 179.36655 172.0 0.00581 175.34828 179.51134 179.0 0.00559 175.36057 179.69089 167.0 0.00599 175.37288 179.90346 191.0 0.00524 175.38516 180.14679 175.0 0.00571 175.39745 180.41695 181.0 0.00552 175.40973 180.70888 164.0 0.00610 175.42203 181.01495 181.0 0.00552 175.43433 181.32545 173.0 0.00578 175.44659 181.62927 168.0 0.00595 175.45888 181.91603 183.0 0.00546 175.47115 182.17969 183.0 0.00546 175.48343 182.42142 179.0 0.00559 175.49573 182.65111 172.0 0.00581 175.50801 182.88591 175.0 0.00571 175.52029 182.85393 181.0 0.00552 175.53258 183.17303 167.0 0.00599 175.54486 183.56635 174.0 0.00575 175.55713 184.05817 181.0 0.00552 175.56941 184.67235 181.0 0.00552 175.58167 185.43460 171.0 0.00585 175.59395 186.37190 186.0 0.00538 175.60623 189.80099 193.0 0.00518 175.61850 191.22981 211.0 0.00474 175.63077 192.92235 192.0 0.00521 175.64304 194.90623 198.0 0.00505 175.65530 197.20560 197.0 0.00508 175.66759 199.83833 198.0 0.00505 175.67986 202.81247 220.0 0.00455 175.69214 206.12338 209.0 0.00478 175.70439 209.73848 187.0 0.00535 175.71666 213.59921 201.0 0.00498 175.72893 217.60101 246.0 0.00407 175.74121 221.58203 235.0 0.00426 175.75345 225.31572 233.0 0.00429 175.76570 228.51942 251.0 0.00398 175.77798 230.89026 244.0 0.00410 175.79022 232.16937 262.0 0.00382 175.80249 232.21584 244.0 0.00410 175.81474 231.05351 219.0 0.00457 175.82703 228.86383 260.0 0.00385 175.83926 225.92809 240.0 0.00417 175.85153 222.55374 228.0 0.00439 175.86380 219.01419 207.0 0.00483 175.87604 215.52939 209.0 0.00478 175.88831 212.25035 230.0 0.00435 175.90056 209.27716 200.0 0.00500 175.91280 206.67041 203.0 0.00493 175.92503 204.46333 221.0 0.00452 175.93729 202.67053 215.0 0.00465 175.94954 202.45158 201.0 0.00498 175.96179 201.51454 205.0 0.00488 175.97401 200.97897 195.0 0.00513 175.98628 200.83098 214.0 0.00467 175.99850 201.05443 198.0 0.00505 176.01076 201.63068 183.0 0.00546 176.02298 202.53838 180.0 0.00556 176.03523 203.75180 192.0 0.00521 176.04749 205.23764 202.0 0.00495 176.05971 206.95038 220.0 0.00455 176.07195 208.82632 206.0 0.00485 176.08418 210.77664 189.0 0.00529 176.09642 212.68298 203.0 0.00493 176.10863 214.40038 202.0 0.00495 176.12086 215.77278 208.0 0.00481 176.13310 216.66344 204.0 0.00490 176.14532 216.96082 226.0 0.00442 176.15755 216.72612 231.0 0.00433 176.16978 216.02240 195.0 0.00513 176.18202 214.96021 216.0 0.00463 176.19423 213.70720 205.0 0.00488 176.20645 212.40631 215.0 0.00465 176.21867 211.42577 210.0 0.00476 176.23091 211.11673 198.0 0.00505 176.24312 210.26883 209.0 0.00478 176.25534 209.66957 209.0 0.00478 176.26755 209.34456 187.0 0.00535 176.27975 209.31183 183.0 0.00546 176.29199 209.58607 176.0 0.00568 176.30420 210.18277 199.0 0.00503 176.31641 211.11908 205.0 0.00488 176.32860 212.41895 175.0 0.00571 176.34082 214.11404 162.0 0.00617 176.35304 216.24658 187.0 0.00535 176.36522 218.87061 204.0 0.00490 176.37744 222.05385 205.0 0.00488 176.38962 225.87831 203.0 0.00493 176.40182 230.43990 192.0 0.00521 176.41403 235.84737 211.0 0.00474 176.42622 242.21986 222.0 0.00450 176.43845 249.68291 239.0 0.00418 176.45062 258.36307 227.0 0.00441 176.46281 268.38068 264.0 0.00379 176.47502 279.84793 229.0 0.00437 176.48721 292.81317 258.0 0.00388 176.49940 307.34686 307.0 0.003257 176.51161 323.39899 283.0 0.00353 176.52379 340.84293 323.0 0.003096 176.53596 359.38870 314.0 0.003185 176.54814 378.56946 368.0 0.002717 176.56035 397.66003 381.0 0.002625 176.57251 415.65167 402.0 0.002488 176.58469 431.81061 441.0 0.002268 176.59686 443.72919 483.0 0.002070 176.60904 450.70251 449.0 0.002227 176.62122 451.96259 459.0 0.002179 176.63339 447.44720 485.0 0.002062 176.64557 437.80441 473.0 0.002114 176.65775 424.20367 459.0 0.002179 176.66992 408.02927 456.0 0.002193 176.68205 390.60336 419.0 0.002387 176.69423 373.02097 397.0 0.002519 176.70642 356.09833 368.0 0.002717 176.71858 340.39563 351.0 0.002849 176.73073 326.27011 331.0 0.003021 176.74287 313.93127 306.0 0.003268 176.75504 303.48691 309.0 0.003236 176.76720 294.97644 295.0 0.003390 176.77936 288.39108 298.0 0.003356 176.79150 283.70337 261.0 0.00383 176.80365 280.45947 291.0 0.003436 176.81581 279.39111 267.0 0.00375 176.82794 280.01480 272.0 0.00368 176.84009 282.24036 261.0 0.00383 176.85225 285.96127 300.0 0.003333 176.86440 291.04480 287.0 0.003484 176.87653 297.31662 278.0 0.00360 176.88867 304.53775 295.0 0.003390 176.90080 312.37784 287.0 0.003484 176.91295 320.39291 295.0 0.003390 176.92506 327.99689 335.0 0.002985 176.93721 334.51703 335.0 0.002985 176.94934 339.25894 369.0 0.002710 176.96146 341.64932 360.0 0.002778 176.97360 341.38519 356.0 0.002809 176.98572 338.52722 349.0 0.002865 176.99783 333.48355 357.0 0.002801 177.00996 326.90952 334.0 0.002994 177.02208 319.49445 341.0 0.002933 177.03421 311.92102 339.0 0.002950 177.04631 304.73700 311.0 0.003215 177.05844 298.35101 318.0 0.003145 177.07054 293.04602 283.0 0.00353 177.08266 289.00061 292.0 0.003425 177.09477 286.32077 285.0 0.00351 177.10687 285.04141 246.0 0.00407 177.11900 285.14587 291.0 0.003436 177.13106 286.56430 279.0 0.00358 177.14320 288.96387 289.0 0.003460 177.15527 292.55893 283.0 0.00353 177.16736 296.85754 313.0 0.003195 177.17946 301.47879 311.0 0.003215 177.19156 305.94202 324.0 0.003086 177.20364 309.68982 269.0 0.00372 177.21577 312.15067 287.0 0.003484 177.22784 312.83307 314.0 . . . _pd_meas_number_of_points 6571 _pd_proc_number_of_points 6571 loop_ _refln_index_h _refln_index_k _refln_index_l _pd_refln_wavelength_id _refln_observed_status _refln_F_squared_meas _refln_F_squared_calc _refln_phase_calc _refln_d_spacing _gsas_i100_meas 1 0 0 1 o 11368.590 11700.544 149.39 5.86574 39.71 1 0 0 2 o 11213.223 11700.544 149.39 5.86574 19.74 0 0 2 1 o 14527.039 14883.566 0.00 5.00228 11.78 0 0 2 2 o 14117.232 14883.566 0.00 5.00228 5.74 1 0 2 1 o 23549.662 23769.422 169.98 3.80618 75.77 1 0 2 2 o 24049.760 23769.422 169.98 3.80618 39.20 1 1 0 1 o 26839.568 27348.047 0.00 3.38659 31.63 1 1 0 2 o 27477.246 27348.047 0.00 3.38659 16.44 1 1 1 1 o 5821.197 3473.527 -180.00 3.20779 14.77 1 1 1 2 o 6235.816 3473.527 -180.00 3.20779 7.99 2 0 0 1 o 14234.793 14702.912 -177.34 2.93287 13.30 2 0 0 2 o 14936.970 14702.912 -177.34 2.93287 7.09 1 1 2 1 o 58713.05 55537.26 0.00 2.80435 100.00 1 1 2 2 o 58459.89 55537.26 0.00 2.80435 50.31 2 0 2 1 o 6032.516 6032.238 -153.95 2.53007 7.13 2 0 2 2 o 6110.405 6032.238 -153.95 2.53007 3.66 0 0 4 1 o 44713.67 50925.32 0.00 2.50114 9.82 0 0 4 2 o 43142.66 50925.32 0.00 2.50114 4.77 1 1 3 1 o 8.056 81.984 -180.00 2.37618 0.00 1 1 3 2 o 8.056 81.984 -180.00 2.37618 0.00 1 0 4 1 o 2373.206 3370.639 166.11 2.30072 1.96 1 0 4 2 o 2081.155 3370.639 166.11 2.30072 0.81 2 1 0 1 o 13499.719 13396.000 174.77 2.21704 13.93 2 1 0 2 o 14163.143 13396.000 174.77 2.21704 7.42 2 1 1 1 o 1235.067 1236.886 -92.56 2.16453 2.78 2 1 1 2 o 975.894 1236.886 -92.56 2.16453 1.12 2 1 2 1 o 5125.282 5570.802 159.45 2.02689 7.49 2 1 2 2 o 5265.125 5570.802 159.45 2.02689 3.92 1 1 4 1 o 34893.188 33603.309 0.00 2.01192 28.52 1 1 4 2 o 36020.84 33603.309 0.00 2.01192 14.95 3 0 0 1 o 41358.85 42548.68 1.09 1.95525 16.13 3 0 0 2 o 38952.59 42548.68 1.09 1.95525 7.62 2 0 4 1 o 18071.369 18350.842 -166.14 1.90309 13.48 2 0 4 2 o 18242.248 18350.842 -166.14 1.90309 6.88 2 1 3 1 o 661.742 1013.577 -14.30 1.84627 1.11 2 1 3 2 o 1079.466 1013.577 -14.30 1.84627 0.89 3 0 2 1 o 31297.580 30513.234 -0.04 1.82108 20.62 3 0 2 2 o 32038.598 30513.234 -0.04 1.82108 10.71 1 1 5 1 o -0.051 0.974 0.00 1.72270 0.00 1 1 5 2 o -0.051 0.974 0.00 1.72270 0.00 2 2 0 1 o 24525.275 24208.617 0.00 1.69329 6.83 2 2 0 2 o 26407.545 24208.617 0.00 1.69329 3.76 2 2 1 1 o 50.191 47.905 0.00 1.66955 0.03 0 0 6 1 o 9723.608 9730.759 0.00 1.66743 0.78 2 2 1 2 o 48.956 47.905 0.00 1.66955 0.02 0 0 6 2 o 10294.250 9730.759 0.00 1.66743 0.43 2 1 4 1 o 15338.484 13916.192 158.79 1.65908 16.89 2 1 4 2 o 15403.236 13916.192 158.79 1.65908 8.58 3 1 0 1 o 8666.443 7885.691 -148.36 1.62686 4.25 3 1 0 2 o 8340.241 7885.691 -148.36 1.62686 2.05 3 1 1 1 o 989.063 1003.868 -88.75 1.60577 1.21 2 2 2 1 o 26990.389 27748.088 0.00 1.60389 13.52 1 0 6 1 o 11476.101 11790.726 167.64 1.60388 5.84 3 1 1 2 o 979.684 1003.868 -88.75 1.60577 0.61 2 2 2 2 o 27839.709 27748.088 0.00 1.60389 7.08 1 0 6 2 o 11873.680 11790.726 167.64 1.60388 3.07 3 1 2 1 o 9775.736 9893.122 -168.97 1.54710 9.19 3 1 2 2 o 10009.742 9893.122 -168.97 1.54710 4.78 3 0 4 1 o 23990.896 22805.920 -0.64 1.54042 11.06 3 0 4 2 o 26120.158 22805.920 -0.64 1.54042 6.16 2 2 3 1 o 565.250 15.148 -180.00 1.50982 0.29 2 2 3 2 o 224.531 15.148 -180.00 1.50982 0.06 1 1 6 1 o 33592.094 31612.287 0.00 1.49593 14.98 1 1 6 2 o 31801.176 31612.287 0.00 1.49593 7.12 2 1 5 1 o 603.370 739.306 171.40 1.48541 0.64 2 1 5 2 o 738.775 739.306 171.40 1.48541 0.39 4 0 0 1 o 9179.892 7413.061 139.60 1.46644 1.83 4 0 0 2 o 8486.405 7413.061 139.60 1.46644 0.84 3 1 3 1 o 1433.368 1191.595 106.44 1.46216 1.43 3 1 3 2 o 1290.408 1191.595 106.44 1.46216 0.66 2 0 6 1 o 5193.430 4386.576 -148.57 1.44954 1.94 2 0 6 2 o 5530.394 4386.576 -148.57 1.44954 1.06 4 0 2 1 o 14052.251 12378.720 165.10 1.40721 5.64 4 0 2 2 o 13358.798 12378.720 165.10 1.40721 2.69 2 2 4 1 o 27347.219 26379.863 0.00 1.40218 10.53 2 2 4 2 o 25319.328 26379.863 0.00 1.40218 4.87 3 1 4 1 o 2782.391 3189.255 -157.91 1.36375 1.64 3 1 4 2 o 2838.945 3189.255 -157.91 1.36375 0.86 3 2 0 1 o 4115.141 4010.853 174.53 1.34569 1.42 3 2 0 2 o 3696.325 4010.853 174.53 1.34569 0.63 2 1 6 1 o 3882.142 3690.951 158.72 1.33260 2.41 3 2 1 1 o 186.358 171.222 -27.65 1.33368 0.16 2 1 6 2 o 3853.840 3690.951 158.72 1.33260 1.21 3 2 1 2 o 179.714 171.222 -27.65 1.33368 0.08 1 1 7 1 o 1803.506 1325.973 0.00 1.31676 0.74 1 1 7 2 o 1306.627 1325.973 0.00 1.31676 0.27 3 2 2 1 o 6431.108 6505.288 154.64 1.29949 3.99 3 2 2 2 o 6359.841 6505.288 154.64 1.29949 1.99 2 2 5 1 o 11.722 9.005 0.00 1.29257 0.00 2 2 5 2 o 10.021 9.005 0.00 1.29257 0.00 4 1 0 1 o 25203.703 26825.617 -3.20 1.28001 8.16 4 1 0 2 o 23463.020 26825.617 -3.20 1.28001 3.80 3 0 6 1 o 17766.789 18538.621 -1.40 1.26873 5.47 4 1 1 1 o 1044.939 1077.712 -80.07 1.26966 0.81 3 0 6 2 o 18272.865 18538.621 -1.40 1.26873 2.86 4 0 4 1 o 706.408 708.904 -166.55 1.26504 0.25 4 1 1 2 o 1033.205 1077.712 -80.07 1.26966 0.41 3 1 5 1 o 1026.590 904.627 -74.59 1.26229 0.78 4 0 4 2 o 811.433 708.904 -166.55 1.26504 0.14 3 1 5 2 o 1203.103 904.627 -74.59 1.26229 0.46 0 0 8 1 o 47109.51 50547.73 0.00 1.25057 2.57 3 2 3 1 o 1506.556 1686.536 122.74 1.24792 1.14 0 0 8 2 o 45825.21 50547.73 0.00 1.25057 1.26 3 2 3 2 o 1601.543 1686.536 122.74 1.24792 0.61 4 1 2 1 o 16429.850 16165.047 2.86 1.24006 9.74 4 1 2 2 o 16300.203 16165.047 2.86 1.24006 4.88 1 0 8 1 o 5181.819 4266.187 148.53 1.22308 1.43 1 0 8 2 o 5104.520 4266.187 148.53 1.22308 0.71 2 1 7 1 o 1061.683 489.240 69.99 1.20125 0.73 2 1 7 2 o 593.384 489.240 69.99 1.20125 0.21 4 1 3 1 o 491.374 575.616 103.36 1.19501 0.35 4 1 3 2 o 565.914 575.616 103.36 1.19501 0.20 2 2 6 1 o 18641.506 18267.885 0.00 1.18809 5.25 2 2 6 2 o 17972.180 18267.885 0.00 1.18809 2.55 3 2 4 1 o 5690.479 5788.572 165.18 1.18506 3.11 3 2 4 2 o 5567.401 5788.572 165.18 1.18506 1.54 5 0 0 1 o 4267.092 4460.596 -166.10 1.17315 0.56 1 1 8 1 o 11010.994 11445.981 0.00 1.17314 2.86 5 0 0 2 o 4162.935 4460.596 -166.10 1.17315 0.27 1 1 8 2 o 10718.330 11445.981 0.00 1.17314 1.40 3 1 6 1 o 6419.675 6428.724 -167.98 1.16444 3.52 3 1 6 2 o 6799.813 6428.724 -167.98 1.16444 1.91 2 0 8 1 o 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