# Supplementary Material (ESI) for New Journal of Chemistry # This journal is © The Royal Society of Chemistry and # The Centre National de la Recherche Scientifique, 2008 ############################################################################## ### CIF submission form for results of Rietveld refinements (IUCr journals)### ### Version 10 February 2005 ### ############################################################################## # This is an electronic "form" for submitting the results of a Rietveld # refinement of a model against powder diffraction data to an # IUCr journal as a Crystallographic Information File (CIF). Full details # of the CIF format are given in the paper "The Crystallographic Information # File (CIF): a New Standard Archive File for Crystallography" by S. R. Hall, # F. H. Allen and I. D. Brown [Acta Cryst. (1991), A47, 655-685]. # # The current version of the powder CIF dictionary, which contains definitions # of the terms staring _pd_, may be obtained from # http://www.iucr.org/iucr-top/cif/pd/index.html. Other terms are defined in # the core CIF dictionary at http://www.iucr.org/iucr-top/cif/core/index.html. # # Note that all fields should be numeric or character type EXCEPT those which # are flagged as 'text' - free-form text of any length may be included in # these latter fields provided the text block begins and ends with a semicolon # as the first character of a new line. Note also that the query marks # '?' are significant as placeholders, and should not be deleted where a data # item is not given, UNLESS the accompanying data name is also deleted. # Lines should not exceed 80 characters in length. The comments following # a hash symbol '#' may be deleted if wished. #============================================================================= data_global _publ_requested_journal "New Journal of Chemistry" #============================================================================== # 1. SUBMISSION DETAILS _publ_contact_author_name "Joel Bernstein" _publ_contact_author_address # Address of author for correspondence ; Ben Gurion University of the Negev ; _publ_contact_author_email yoel@bgu.ac.il _publ_contact_author_phone ? _publ_contact_author_fax ? loop_ _publ_author_name _publ_author_address 'Inna Barzky' ; Ben Gurion University of the Negev ; 'Joel Bernstein' ; Ben Gurion University of the Negev ; 'Peter W. Stephens' ; Department of Physics and Astronomy, Stony Brook University, Stony Brook, New York 11794 ; 'Kevin H. Stone' ; Department of Physics and Astronomy, Stony Brook University, Stony Brook, New York 11794 ; _publ_contact_letter ; ? ; #============================================================================== # 3. TITLE AND AUTHOR LIST _publ_section_title ; The study of polymorphic system of 2-chloro-4nitrobenzoic acid ; _publ_section_title_footnote ; ? ; #============================================================================== # 5. CHEMICAL DATA _chemical_name_systematic ; ??? ; _chemical_name_common '2-chloro-4-nitrobenzoic acid' _chemical_formula_moiety 'C7 O4 N Cl H4' _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_formula_sum ? _chemical_formula_weight 201.562 _chemical_melting_point ? _chemical_compound_source ? # for minerals and # natural products loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source _atom_type_scat_length_neutron # include if applicable ? ? ? ? ? ? #============================================================================== # 6. POWDER SPECIMEN AND CRYSTAL DATA _space_group_crystal_system Monoclinic _space_group_name_H-M_alt P21/c _space_group_name_Hall P21/c loop_ _symmetry_equiv_pos_as_xyz '-x, -y, -z' '-x, y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' 'x, y, z' _cell_length_a 10.5323(3) _cell_length_b 6.0752(3) _cell_length_c 13.5080(3) _cell_angle_alpha 90 _cell_angle_beta 107.565(2) _cell_angle_gamma 90 _cell_volume 824.02(5) _cell_formula_units_Z 4 # The next three fields give the specimen dimensions in mm. The equatorial # plane contains the incident and diffracted beam. _pd_spec_size_axial 8 # perpendicular to # equatorial plane _pd_spec_size_equat 1.5 # parallel to # scattering vector # in transmission _pd_spec_size_thick ? # parallel to # scattering vector # in reflection # The next five fields are character fields that describe the specimen. _pd_spec_mounting # This field should be # used to give details of the # container. ; capillary ; _pd_spec_mount_mode transmission # options are 'reflection' # or 'transmission' _pd_spec_shape cylinder # options are 'cylinder' # 'flat_sheet' or 'irregular' _pd_char_particle_morphology ? _pd_char_colour ? # use ICDD colour descriptions # The following three fields describe the preparation of the specimen. # The cooling rate is in K/min. The pressure at which the sample was # prepared is in kPa. The temperature of preparation is in K. _pd_prep_cool_rate ? _pd_prep_pressure ? _pd_prep_temperature ? # The next four fields are normally only needed for transmission experiments. _exptl_absorpt_coefficient_mu ? _exptl_absorpt_correction_type none # include if applicable _exptl_absorpt_process_details ? # include if applicable _exptl_absorpt_correction_T_min ? # include if applicable _exptl_absorpt_correction_T_max ? # include if applicable #============================================================================== # 7. EXPERIMENTAL DATA _exptl_special_details ; ? ; # The following item is used to identify the equipment used to record # the powder pattern when the diffractogram was measured at a laboratory # other than the authors' home institution, e.g. when neutron or synchrotron # radiation is used. _pd_instr_location ; X16C, National Synchrotron Light Source, Brookhaven National Laboratory ; _pd_calibration_special_details # description of the method used # to calibrate the instrument ; NIST standard reference material 1976(sintered plate of Al2O3). 7 reflections were used to calibrate wavelength and detector zero. ; _diffrn_ambient_temperature 356 _diffrn_source synchrotron _diffrn_source_target ? _diffrn_source_type ? _diffrn_radiation_type ? _diffrn_measurement_device_type 'Huber diffractometer' _diffrn_detector 'NaI scintillation counter' _diffrn_detector_type ? # make or model of detector _pd_meas_scan_method step # options are 'step', 'cont', # 'tof', 'fixed' or # 'disp' (= dispersive) _pd_meas_special_details ; ? ; # The following six items are used for angular dispersive measurements only. _diffrn_radiation_wavelength 0.69865 _diffrn_radiation_monochromator 'double Si(111)' # The following four items give details of the measured (not processed) # powder pattern. Angles are in degrees. _pd_meas_number_of_points 5800 _pd_meas_2theta_range_min 1 _pd_meas_2theta_range_max 30 _pd_meas_2theta_range_inc 0.005 # The following three items are used for time-of-flight measurements only. _pd_instr_dist_src/spec ? _pd_instr_dist_spec/detc ? _pd_meas_2theta_fixed ? #============================================================================== # 8. REFINEMENT DATA # Use the next field to give any special details about the fitting of the # powder pattern. _pd_proc_ls_special_details ; Strain broadening was treated anisotropically using the model of Stephens, P. W., Journal of Applied Crystallography, Vol. 32, page 281 ; # The next three items are given as text. _pd_proc_ls_profile_function ; Simple_Axial_Model(8.47973) function with Rp=9999,Rs=300 in TOPAS-Academic ; _pd_proc_ls_background_function ; Chebyshev polynomial with 5 coeffecients and a psuedo-Voight function at an angle of 2.31 degrees and a width of 1.79 degrees. ; _pd_proc_ls_pref_orient_corr ; none ; _pd_proc_ls_prof_R_factor ? _pd_proc_ls_prof_wR_factor 11.760 _pd_proc_ls_prof_wR_expected ? _refine_ls_R_I_factor ? _refine_ls_R_Fsqd_factor ? _refine_ls_R_factor_all ? _refine_special_details ; The molecule was treated as a rigid body. All aromatic bond lengths were refined as a single parameter, with a value of 1.375(3) Angstroms. Other bond lengths refined were the C-COOH distance (refined to a value of 1.507(7) Angstroms), C-Cl distance (refined to a value of 1.748(6) Angstroms), C-N distance (refined to a value of 1.518(6) Angstroms), C-O distance and N-O distance, both of which were refined as a single parameter (with values of 1.215(6) and 1.184(6) Angstroms respectively). The Hydrogen atoms were tethered to their respective atoms at a distance of 0.9 angstroms. The torsions around C-COOH and C-NO2 bonds were also refined (to values of 99.3(3) and 16.1(5) degrees respectively). ; _refine_ls_matrix_type ? _refine_ls_weighting_scheme sigma # options are 'sigma'(based on measured su's) # or 'calc' (calculated weights) _refine_ls_weighting_details 1/(sigma*sigma) _refine_ls_hydrogen_treatment ? _refine_ls_extinction_method ? _refine_ls_extinction_coef ? _refine_ls_number_parameters 41 _refine_ls_number_restraints ? _refine_ls_number_constraints ? # The following item is the same as CHI, the square root of 'CHI squared' _refine_ls_goodness_of_fit_all 2.701 _refine_ls_restrained_S_all ? _refine_ls_shift/su_max 0.0001 _refine_ls_shift/su_mean ? # The following four items apply to angular dispersive measurements. # 2theta minimum, maximum and increment (in degrees) are for the # intensities used in the refinement. _pd_proc_2theta_range_min 1 _pd_proc_2theta_range_max 30 _pd_proc_2theta_range_inc 0.005 _pd_proc_wavelength 0.69865 _pd_block_diffractogram_id 2c4n-acid_83C_profile # The id used for the block containing # the powder pattern profile (section 11) # Give appropriate details in the next two text fields. _pd_proc_info_excluded_regions ? _pd_proc_info_data_reduction ? # The following items are used to identify the programs used. _computing_data_collection EPICS _computing_cell_refinement "TOPAS Academic" _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement "TOPAS Academic" _computing_molecular_graphics ? _computing_publication_material ? # 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_label _atom_site_type_symbol _atom_site_symmetry_multiplicity _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_B_iso_or_equiv Cl1 Cl 4 0.8862014 0.149223 0.2734701 1 7.778768 N1 N 4 0.564959 0.8219857 0.1824732 1 7.778768 C1 C 4 0.8053007 0.3526703 0.08624755 1 7.778768 O4 O 4 0.4849359 0.921426 0.1173712 1 7.778768 C3 C 4 0.720146 0.4989312 0.2170322 1 7.778768 C2 C 4 0.797579 0.3477279 0.1860303 1 7.778768 C4 C 4 0.6504348 0.6550771 0.1482512 1 7.778768 O1 O 4 0.835319 0.02782025 0.003223224 1 7.778768 C7 C 4 0.8901745 0.186937 0.05226659 1 7.778768 C6 C 4 0.7355894 0.5088161 0.01746661 1 7.778768 C5 C 4 0.6581565 0.6600195 0.04846845 1 7.778768 O3 O 4 0.5823855 0.8447779 0.2726369 1 7.778768 O2 O 4 1.009276 0.2206017 0.075588 1 7.778768 H1 H 4 0.7406439 0.5120513 -0.04784914 1 7.778768 H2 H 4 0.612525 0.7622293 0.00344586 1 7.778768 H3 H 4 0.7150916 0.495696 0.2823479 1 7.778768 H4 H 4 1.068389 0.1138328 0.0542309 1 7.778768 #============================================================================== # Additional structures (sections 5-10 and associated data_? identifiers) # may be added at this point. #============================================================================== # The following lines are used to test the character set of files sent by # network email or other means. They are not part of the CIF data set. # abcdefghijklmnopqrstuvwxyzABCDEFGHIJKLMNOPQRSTUVWXYZ0123456789 # !@#$%^&*()_+{}:"~<>?|\-=[];'`,./ #============================================================================== # 11. POWDER PROFILE # Each refinement must be accompanied by a listing of the powder profile # in CIF format. Each listing should be sent as a separate file consisting # of one data block containing a single powder profile. The _pd_block_id # is used to associate each refinement with its corresponding powder profile # since it must match the field _pd_block_diffractogram_id in section 8. data_profile _pd_block_id 2c4n-acid_83C_profile loop_ # _pd_proc_point_id _pd_proc_2theta_corrected # one of # _pd_proc_energy_incident # these # _pd_proc_d_spacing # three _pd_proc_intensity_net _pd_calc_intensity_net _pd_proc_ls_weight 1.000 1285 1334 0.021552 1.005 1292 1327 0.021505 1.010 1171 1320 0.022573 1.015 1244 1313 0.021834 1.020 1267 1306 0.021645 1.025 1254 1300 0.021834 1.030 1166 1293 0.022573 1.035 1219 1287 0.022075 1.040 1147 1280 0.022727 1.045 1140 1274 0.022779 1.050 1276 1268 0.021645 1.055 1251 1262 0.021786 1.060 1188 1256 0.022321 1.065 1188 1250 0.022321 1.070 1128 1244 0.022936 1.075 1214 1238 0.022124 1.080 1243 1232 0.021834 1.085 1195 1227 0.022272 1.090 1262 1221 0.021692 1.095 1145 1216 0.022727 1.100 1210 1210 0.022124 1.105 1234 1205 0.021930 1.110 1206 1199 0.022173 1.115 1177 1194 0.022422 1.120 1132 1189 0.022831 1.125 1194 1184 0.022321 1.130 1174 1179 0.022472 1.135 1083 1174 0.023419 1.140 1155 1169 0.022727 1.145 1136 1164 0.022831 1.150 1162 1159 0.022676 1.155 1208 1154 0.022124 1.160 1185 1150 0.022371 1.165 1118 1145 0.023041 1.170 1206 1141 0.022173 1.175 1158 1136 0.022624 1.180 1208 1132 0.022222 1.185 1101 1127 0.023256 1.190 1108 1123 0.023095 1.195 1103 1119 0.023202 1.200 1116 1114 0.023041 1.205 1087 1110 0.023419 1.210 1100 1106 0.023310 1.215 1147 1102 0.022779 1.220 1104 1098 0.023148 1.225 1136 1094 0.022883 1.230 1069 1090 0.023529 1.235 1125 1086 0.022936 1.240 1058 1082 0.023641 1.245 1124 1079 0.023041 1.250 1054 1075 0.023697 1.255 1057 1071 0.023753 1.260 1070 1068 0.023529 1.265 1162 1064 0.022573 1.270 1101 1061 0.023256 1.275 1047 1057 0.023810 1.280 1120 1054 0.022989 1.285 1126 1050 0.022936 1.290 1046 1047 0.023810 1.295 1046 1044 0.023810 1.300 1075 1041 0.023529 1.305 1101 1037 0.023202 1.310 1058 1034 0.023641 1.315 1070 1031 0.023529 1.320 1035 1028 0.023981 1.325 1048 1025 0.023753 1.330 980 1022 0.024570 1.335 1059 1019 0.023697 1.340 1044 1016 0.023923 1.345 1006 1013 0.024213 1.350 1056 1011 0.023697 1.355 1049 1008 0.023810 1.360 1058 1005 0.023641 1.365 1027 1002 0.024038 1.370 1059 1000 0.023697 1.375 1009 997 0.024272 1.380 1050 995 0.023866 1.385 1039 992 0.023923 1.390 992 990 0.024510 1.395 1025 987 0.024155 1.400 985 985 0.024570 1.405 1022 982 0.024155 1.410 965 980 0.024876 1.415 967 978 0.024752 1.420 992 975 0.024390 1.425 1072 973 0.023529 1.430 1010 971 0.024155 1.435 960 969 0.024876 1.440 982 967 0.024570 1.445 926 965 0.025253 1.450 957 963 0.024876 1.455 1027 960 0.023981 1.460 981 958 0.024631 1.465 983 957 0.024510 1.470 1005 955 0.024331 1.475 944 953 0.025000 1.480 1061 951 0.023641 1.485 940 949 0.025126 1.490 1035 947 0.023923 1.495 911 946 0.025575 1.500 908 944 0.025641 1.505 964 942 0.024876 1.510 947 940 0.025000 1.515 982 939 0.024570 1.520 1076 937 0.023474 1.525 917 936 0.025445 1.530 901 934 0.025641 1.535 937 933 0.025189 1.540 1074 931 0.023474 1.545 949 930 0.025063 1.550 961 928 0.024814 1.555 979 927 0.024631 1.560 998 925 0.024450 1.565 979 924 0.024570 1.570 891 923 0.025707 1.575 895 922 0.025707 1.580 985 920 0.024570 1.585 923 919 0.025381 1.590 896 918 0.025773 1.595 929 917 0.025253 1.600 894 916 0.025840 1.605 945 914 0.025063 1.610 946 913 0.025063 1.615 974 912 0.024752 1.620 929 911 0.025316 1.625 904 910 0.025575 1.630 962 909 0.024814 1.635 914 908 0.025445 1.640 932 907 0.025253 1.645 958 906 0.024876 1.650 1000 906 0.024272 1.655 853 905 0.026316 1.660 889 904 0.025773 1.665 953 903 0.024938 1.670 897 902 0.025641 1.675 941 901 0.025189 1.680 936 901 0.025189 1.685 872 900 0.026110 1.690 968 899 0.024691 1.695 953 898 0.025000 1.700 933 898 0.025189 1.705 912 897 0.025445 1.710 867 897 0.026110 1.715 865 896 0.026110 1.720 889 895 0.025907 1.725 905 895 0.025575 1.730 907 894 0.025575 1.735 865 894 0.026178 1.740 904 893 0.025641 1.745 899 893 0.025641 1.750 921 892 0.025316 1.755 903 892 0.025641 1.760 870 891 0.026110 1.765 897 891 0.025773 1.770 898 890 0.025707 1.775 876 890 0.026042 1.780 874 890 0.026110 1.785 867 889 0.026110 1.790 927 889 0.025316 1.795 861 888 0.026316 1.800 858 888 0.026316 1.805 923 888 0.025316 1.810 908 888 0.025510 1.815 840 887 0.026455 1.820 855 887 0.026316 1.825 922 887 0.025253 1.830 827 886 0.026810 1.835 864 886 0.026110 1.840 851 886 0.026385 1.845 779 886 0.027624 1.850 773 886 0.027624 1.855 866 885 0.026042 1.860 878 885 0.025907 1.865 905 885 0.025575 1.870 907 885 0.025510 1.875 886 885 0.025840 1.880 858 885 0.026385 1.885 905 884 0.025510 1.890 902 884 0.025641 1.895 905 884 0.025575 1.900 878 884 0.025974 1.905 931 884 0.025189 1.910 812 884 0.026954 1.915 875 884 0.025974 1.920 877 884 0.025974 1.925 831 884 0.026667 1.930 832 883 0.026596 1.935 850 883 0.026385 1.940 929 883 0.025189 1.945 836 883 0.026596 1.950 895 883 0.025707 1.955 845 883 0.026525 1.960 883 883 0.025974 1.965 838 883 0.026596 1.970 843 883 0.026385 1.975 836 883 0.026525 1.980 874 883 0.026042 1.985 850 883 0.026385 1.990 769 882 0.027701 1.995 850 882 0.026316 2.000 845 882 0.026525 2.005 815 882 0.026954 2.010 798 882 0.027174 2.015 846 882 0.026385 2.020 840 882 0.026525 2.025 819 882 0.026882 2.030 859 882 0.026247 2.035 852 882 0.026316 2.040 832 881 0.026596 2.045 774 881 0.027624 2.050 800 881 0.027248 2.055 843 881 0.026385 2.060 809 881 0.026954 2.065 852 881 0.026316 2.070 790 881 0.027397 2.075 893 880 0.025773 2.080 802 880 0.027027 2.085 851 880 0.026316 2.090 837 880 0.026525 2.095 834 880 0.026667 2.100 869 879 0.026042 2.105 802 879 0.027174 2.110 854 879 0.026247 2.115 815 879 0.026882 2.120 922 878 0.025381 2.125 833 878 0.026596 2.130 773 878 0.027624 2.135 863 877 0.026247 2.140 851 877 0.026385 2.145 784 877 0.027397 2.150 839 876 0.026455 2.155 872 876 0.026110 2.160 795 876 0.027248 2.165 832 875 0.026596 2.170 888 875 0.025840 2.175 826 874 0.026810 2.180 819 874 0.026882 2.185 858 873 0.026247 2.190 827 873 0.026738 2.195 853 872 0.026385 2.200 839 872 0.026525 2.205 836 871 0.026667 2.210 878 871 0.025974 2.215 824 870 0.026738 2.220 861 870 0.026247 2.225 819 869 0.026954 2.230 848 868 0.026455 2.235 855 868 0.026316 2.240 794 867 0.027322 2.245 838 866 0.026596 2.250 829 865 0.026738 2.255 858 865 0.026247 2.260 821 864 0.026810 2.265 890 863 0.025707 2.270 902 862 0.025641 2.275 828 861 0.026738 2.280 875 861 0.026042 2.285 877 860 0.025840 2.290 853 859 0.026247 2.295 892 858 0.025707 2.300 835 857 0.026667 2.305 884 856 0.025773 2.310 877 855 0.025974 2.315 865 854 0.026110 2.320 843 853 0.026455 2.325 862 852 0.026178 2.330 827 851 0.026810 2.335 857 850 0.026316 2.340 914 848 0.025445 2.345 867 847 0.026110 2.350 862 846 0.026178 2.355 867 845 0.026110 2.360 885 844 0.025840 2.365 871 842 0.026042 2.370 849 841 0.026455 2.375 824 840 0.026738 2.380 898 839 0.025707 2.385 888 837 0.025773 2.390 884 836 0.025840 2.395 932 835 0.025126 2.400 829 833 0.026596 2.405 920 832 0.025381 2.410 827 830 0.026810 2.415 879 829 0.025840 2.420 923 827 0.025253 2.425 944 826 0.024938 2.430 854 824 0.026247 2.435 883 823 0.025840 2.440 946 821 0.024876 2.445 917 820 0.025445 2.450 949 818 0.024938 2.455 842 816 0.026455 2.460 934 815 0.025063 2.465 944 813 0.024938 2.470 924 811 0.025253 2.475 915 810 0.025381 2.480 869 808 0.026178 2.485 945 806 0.025000 2.490 913 804 0.025445 2.495 867 803 0.025974 2.500 893 801 0.025707 2.505 868 799 0.026110 2.510 922 797 0.025316 2.515 880 795 0.025907 2.520 871 793 0.026110 2.525 866 791 0.026042 2.530 891 790 0.025707 2.535 841 788 0.026455 2.540 809 786 0.027027 2.545 818 784 0.026738 2.550 859 782 0.026178 2.555 815 780 0.026882 2.560 766 778 0.027778 2.565 883 776 0.025907 2.570 866 774 0.026042 2.575 792 772 0.027322 2.580 793 770 0.027248 2.585 788 768 0.027397 2.590 848 766 0.026316 2.595 836 764 0.026596 2.600 778 761 0.027473 2.605 809 759 0.027027 2.610 861 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362 0.039062 9.945 426 368 0.036364 9.950 410 377 0.037037 9.955 469 389 0.034602 9.960 433 398 0.035971 9.965 412 405 0.037037 9.970 448 413 0.035461 9.975 496 422 0.033670 9.980 506 432 0.033333 9.985 430 442 0.036232 9.990 508 454 0.033333 9.995 474 466 0.034483 10.000 497 480 0.046083 10.005 534 495 0.044444 10.010 531 511 0.044643 10.015 529 529 0.044643 10.020 554 549 0.043668 10.025 603 572 0.042017 10.030 572 597 0.043103 10.035 624 626 0.041152 10.040 670 659 0.039841 10.045 684 697 0.039370 10.050 774 742 0.037037 10.055 793 795 0.036630 10.060 841 858 0.035461 10.065 971 931 0.033003 10.070 1121 1006 0.030675 10.075 1347 1057 0.028090 10.080 1512 1039 0.026525 10.085 1250 935 0.029070 10.090 731 797 0.038168 10.095 610 686 0.041667 10.100 472 615 0.047393 10.105 491 572 0.046512 10.110 457 546 0.048077 10.115 459 531 0.048077 10.120 442 523 0.048780 10.125 456 519 0.048309 10.130 486 519 0.046729 10.135 480 522 0.046948 10.140 479 526 0.046948 10.145 497 533 0.046083 10.150 489 541 0.046512 10.155 459 552 0.048077 10.160 500 564 0.046083 10.165 489 578 0.046512 10.170 502 595 0.045872 10.175 531 615 0.044643 10.180 578 638 0.042735 10.185 557 665 0.043668 10.190 666 697 0.039841 10.195 747 736 0.037594 10.200 878 785 0.034843 10.205 955 846 0.033333 10.210 1086 927 0.031153 10.215 1220 1035 0.029412 10.220 1402 1175 0.027473 10.225 1568 1349 0.025974 10.230 1699 1555 0.025000 10.235 1780 1789 0.024390 10.240 1958 2049 0.023256 10.245 2107 2334 0.022422 10.250 2514 2646 0.020534 10.255 2841 2988 0.019305 10.260 3119 3363 0.018450 10.265 3983 3777 0.016287 10.270 3843 4233 0.016639 10.275 3973 4740 0.016340 10.280 4365 5307 0.015552 10.285 4753 5944 0.014903 10.290 5393 6667 0.014006 10.295 5964 7493 0.013316 10.300 6874 8449 0.012422 10.305 8526 9566 0.011136 10.310 9886 10886 0.010373 10.315 11290 12458 0.009662 10.320 14447 14332 0.008554 10.325 19220 16497 0.007424 10.330 24006 18715 0.006636 10.335 23976 20168 0.006649 10.340 18998 19456 0.007457 10.345 14438 16091 0.008532 10.350 10358 11731 0.010121 10.355 7895 8185 0.011561 10.360 5857 5835 0.013441 10.365 4410 4345 0.015456 10.370 3420 3376 0.017606 10.375 2812 2720 0.019342 10.380 2230 2259 0.021786 10.385 1972 1923 0.023095 10.390 1679 1671 0.025126 10.395 1503 1477 0.026525 10.400 1274 1325 0.028818 10.405 1178 1204 0.029940 10.410 1093 1106 0.031153 10.415 1005 1026 0.032468 10.420 959 960 0.033223 10.425 819 905 0.035971 10.430 834 858 0.035587 10.435 831 819 0.035587 10.440 707 786 0.038760 10.445 697 758 0.038911 10.450 693 735 0.039062 10.455 666 715 0.039841 10.460 661 699 0.040000 10.465 677 687 0.039526 10.470 655 677 0.040161 10.475 666 671 0.039841 10.480 619 668 0.041322 10.485 636 669 0.040650 10.490 674 674 0.039526 10.495 683 685 0.039370 10.500 680 704 0.039526 10.505 726 733 0.038168 10.510 751 773 0.037453 10.515 825 823 0.035714 10.520 794 882 0.036496 10.525 925 950 0.033784 10.530 1055 1026 0.031646 10.535 1308 1110 0.028409 10.540 1656 1204 0.025253 10.545 1689 1308 0.024938 10.550 1736 1423 0.024691 10.555 1623 1552 0.025510 10.560 1816 1695 0.024096 10.565 1796 1857 0.024213 10.570 2057 2040 0.022624 10.575 2100 2248 0.022422 10.580 2324 2488 0.021322 10.585 2482 2766 0.020619 10.590 2883 3093 0.019120 10.595 3218 3481 0.018116 10.600 3633 3944 0.017036 10.605 4033 4494 0.016181 10.610 4820 5121 0.014837 10.615 5834 5731 0.013423 10.620 6801 6036 0.012469 10.625 5886 5614 0.013405 10.630 4208 4481 0.015823 10.635 3081 3292 0.018553 10.640 2223 2443 0.021834 10.645 1905 1912 0.023529 10.650 1532 1587 0.026247 10.655 1380 1386 0.027701 10.660 1318 1263 0.028329 10.665 1261 1191 0.028986 10.670 1208 1154 0.029586 10.675 1302 1141 0.028490 10.680 1243 1148 0.029155 10.685 1316 1173 0.028249 10.690 1354 1212 0.027933 10.695 1438 1265 0.027100 10.700 1461 1333 0.026882 10.705 1557 1417 0.026042 10.710 1681 1518 0.025063 10.715 1830 1639 0.023981 10.720 1985 1785 0.023095 10.725 2147 1959 0.022173 10.730 2393 2174 0.020964 10.735 2557 2427 0.020325 10.740 2682 2729 0.019881 10.745 2867 3036 0.019194 10.750 2984 3231 0.018762 10.755 3157 3118 0.018282 10.760 2918 2637 0.019048 10.765 2481 2024 0.020661 10.770 1878 1525 0.023641 10.775 1497 1193 0.026525 10.780 1021 980 0.032154 10.785 894 841 0.034364 10.790 708 746 0.038760 10.795 638 679 0.040650 10.800 580 629 0.042553 10.805 598 592 0.042017 10.810 540 564 0.044248 10.815 551 541 0.043668 10.820 527 523 0.044843 10.825 521 509 0.045045 10.830 530 497 0.044643 10.835 524 487 0.044843 10.840 467 479 0.047393 10.845 506 472 0.045662 10.850 479 466 0.046948 10.855 509 462 0.045455 10.860 487 458 0.046512 10.865 477 455 0.046948 10.870 483 452 0.046729 10.875 490 450 0.046512 10.880 496 449 0.046083 10.885 507 448 0.045662 10.890 501 447 0.045872 10.895 498 447 0.046083 10.900 482 448 0.046729 10.905 481 448 0.046948 10.910 484 449 0.046729 10.915 497 451 0.045872 10.920 492 453 0.046296 10.925 531 455 0.044444 10.930 473 458 0.047170 10.935 535 461 0.044248 10.940 498 465 0.045872 10.945 527 469 0.044643 10.950 596 474 0.042194 10.955 537 480 0.044248 10.960 561 487 0.043290 10.965 603 494 0.041667 10.970 623 503 0.041152 10.975 600 513 0.042017 10.980 614 524 0.041494 10.985 627 538 0.040984 10.990 668 554 0.039683 10.995 691 573 0.039062 11.000 716 595 0.038462 11.005 760 621 0.037313 11.010 806 652 0.036232 11.015 860 690 0.035088 11.020 918 732 0.033784 11.025 1027 783 0.032051 11.030 1094 840 0.031056 11.035 1115 904 0.030864 11.040 1196 975 0.029762 11.045 1231 1053 0.029326 11.050 1335 1139 0.028169 11.055 1316 1234 0.028329 11.060 1391 1338 0.027548 11.065 1458 1453 0.026954 11.070 1534 1579 0.026178 11.075 1618 1719 0.025510 11.080 1846 1873 0.023866 11.085 2004 2042 0.022883 11.090 2106 2228 0.022321 11.095 2143 2429 0.022124 11.100 2400 2642 0.020964 11.105 2393 2857 0.020964 11.110 2574 3056 0.020202 11.115 2750 3207 0.019569 11.120 2911 3267 0.018975 11.125 2935 3197 0.018975 11.130 3015 2988 0.018692 11.135 2902 2674 0.019048 11.140 2720 2320 0.019685 11.145 2487 1984 0.020576 11.150 2013 1696 0.022831 11.155 1595 1461 0.025641 11.160 1247 1277 0.029070 11.165 1080 1132 0.031153 11.170 874 1018 0.034722 11.175 818 927 0.035842 11.180 740 855 0.037736 11.185 627 797 0.040984 11.190 601 750 0.041841 11.195 603 711 0.041667 11.200 520 679 0.045045 11.205 572 652 0.042918 11.210 535 630 0.044444 11.215 523 611 0.044843 11.220 465 596 0.047619 11.225 470 583 0.047170 11.230 476 572 0.046948 11.235 503 564 0.045662 11.240 481 557 0.046729 11.245 483 551 0.046729 11.250 481 547 0.046729 11.255 462 545 0.047847 11.260 485 543 0.046512 11.265 476 543 0.046948 11.270 510 544 0.045455 11.275 457 546 0.048077 11.280 475 550 0.046948 11.285 499 554 0.045872 11.290 491 561 0.046296 11.295 473 569 0.047170 11.300 473 579 0.047170 11.305 514 591 0.045249 11.310 525 606 0.044643 11.315 540 623 0.044248 11.320 568 643 0.042918 11.325 599 666 0.041841 11.330 602 693 0.041841 11.335 656 724 0.040161 11.340 689 759 0.039062 11.345 689 799 0.039062 11.350 752 846 0.037313 11.355 821 899 0.035714 11.360 887 960 0.034483 11.365 938 1031 0.033557 11.370 925 1111 0.033670 11.375 1037 1201 0.031746 11.380 1198 1303 0.029674 11.385 1333 1416 0.028090 11.390 1343 1540 0.028011 11.395 1578 1676 0.025840 11.400 1709 1820 0.024752 11.405 1835 1967 0.023923 11.410 2155 2110 0.022124 11.415 2287 2238 0.021459 11.420 2392 2346 0.020964 11.425 2485 2440 0.020576 11.430 2380 2537 0.021008 11.435 2538 2652 0.020325 11.440 2618 2792 0.020080 11.445 2911 2954 0.019011 11.450 3265 3126 0.017921 11.455 3226 3287 0.018083 11.460 3472 3410 0.017391 11.465 3454 3455 0.017422 11.470 3309 3390 0.017794 11.475 3128 3206 0.018315 11.480 2743 2927 0.019531 11.485 2572 2603 0.020243 11.490 2395 2284 0.020921 11.495 2145 1998 0.022173 11.500 1946 1756 0.023202 11.505 1708 1556 0.024814 11.510 1507 1392 0.026385 11.515 1372 1258 0.027701 11.520 1258 1146 0.028818 11.525 1245 1053 0.029070 11.530 1106 975 0.030769 11.535 997 910 0.032468 11.540 972 854 0.032895 11.545 919 806 0.033898 11.550 857 765 0.035088 11.555 814 730 0.035971 11.560 778 700 0.036765 11.565 763 674 0.037175 11.570 747 652 0.037594 11.575 676 634 0.039526 11.580 637 618 0.040650 11.585 725 606 0.038168 11.590 641 598 0.040486 11.595 663 593 0.039841 11.600 672 591 0.039526 11.605 707 591 0.038610 11.610 642 595 0.040486 11.615 642 600 0.040486 11.620 646 608 0.040323 11.625 622 619 0.041152 11.630 633 633 0.040816 11.635 689 649 0.039062 11.640 660 669 0.039841 11.645 692 692 0.038911 11.650 721 720 0.038168 11.655 764 754 0.037175 11.660 814 793 0.035971 11.665 823 841 0.035842 11.670 864 898 0.034965 11.675 904 967 0.034014 11.680 929 1048 0.033557 11.685 946 1137 0.033223 11.690 927 1213 0.033670 11.695 950 1230 0.033223 11.700 912 1141 0.033898 11.705 861 972 0.034965 11.710 789 808 0.036496 11.715 731 692 0.037736 11.720 687 617 0.039062 11.725 699 568 0.038760 11.730 613 536 0.041322 11.735 596 513 0.042017 11.740 548 497 0.043668 11.745 570 485 0.042918 11.750 549 477 0.043860 11.755 520 472 0.044843 11.760 579 468 0.042553 11.765 528 466 0.044643 11.770 556 466 0.043478 11.775 502 466 0.045662 11.780 546 468 0.043860 11.785 529 471 0.044643 11.790 537 474 0.044248 11.795 555 479 0.043478 11.800 543 485 0.043860 11.805 536 491 0.044248 11.810 531 500 0.044444 11.815 517 509 0.045045 11.820 561 520 0.043103 11.825 530 534 0.044444 11.830 638 550 0.040650 11.835 595 568 0.042017 11.840 659 590 0.039841 11.845 690 614 0.039062 11.850 744 636 0.037594 11.855 737 646 0.037736 11.860 741 633 0.037594 11.865 620 601 0.041152 11.870 557 571 0.043290 11.875 526 551 0.044643 11.880 524 541 0.044643 11.885 534 536 0.044248 11.890 515 537 0.045045 11.895 554 540 0.043668 11.900 537 544 0.044248 11.905 562 550 0.043290 11.910 503 555 0.045662 11.915 559 562 0.043290 11.920 521 568 0.044843 11.925 557 574 0.043290 11.930 570 579 0.042918 11.935 529 583 0.044444 11.940 542 586 0.043860 11.945 527 587 0.044643 11.950 549 587 0.043668 11.955 556 586 0.043478 11.960 543 583 0.044053 11.965 471 578 0.047170 11.970 531 571 0.044444 11.975 540 563 0.044053 11.980 543 555 0.043860 11.985 503 545 0.045662 11.990 518 535 0.045045 11.995 546 525 0.043860 12.000 498 515 0.045662 12.005 480 505 0.046729 12.010 513 496 0.045249 12.015 507 487 0.045455 12.020 469 479 0.047170 12.025 505 471 0.045662 12.030 501 464 0.045872 12.035 450 458 0.048309 12.040 477 452 0.046729 12.045 477 446 0.046948 12.050 477 442 0.046729 12.055 475 437 0.046948 12.060 452 433 0.048077 12.065 447 429 0.048544 12.070 427 425 0.049505 12.075 474 422 0.046948 12.080 450 419 0.048309 12.085 456 417 0.047847 12.090 420 415 0.050000 12.095 460 413 0.047619 12.100 421 411 0.049751 12.105 451 410 0.048077 12.110 462 409 0.047619 12.115 468 410 0.047170 12.120 468 410 0.047393 12.125 464 412 0.047393 12.130 426 414 0.049505 12.135 445 416 0.048544 12.140 470 419 0.047170 12.145 466 422 0.047393 12.150 487 426 0.046296 12.155 449 431 0.048309 12.160 431 437 0.049261 12.165 476 444 0.046948 12.170 427 452 0.049505 12.175 495 461 0.045872 12.180 456 473 0.047847 12.185 490 485 0.046296 12.190 495 500 0.045872 12.195 501 518 0.045662 12.200 514 537 0.045045 12.205 507 554 0.045455 12.210 492 558 0.046083 12.215 516 540 0.045045 12.220 540 505 0.044053 12.225 502 471 0.045662 12.230 509 447 0.045249 12.235 472 432 0.046948 12.240 459 422 0.047619 12.245 473 416 0.046948 12.250 449 411 0.048309 12.255 458 409 0.047619 12.260 487 407 0.046296 12.265 424 406 0.049505 12.270 446 406 0.048309 12.275 452 406 0.048077 12.280 479 406 0.046729 12.285 407 407 0.050761 12.290 448 409 0.048309 12.295 445 411 0.048309 12.300 410 414 0.050505 12.305 463 418 0.047393 12.310 446 423 0.048309 12.315 439 428 0.048780 12.320 526 436 0.044643 12.325 525 445 0.044643 12.330 553 456 0.043478 12.335 522 471 0.044643 12.340 550 490 0.043478 12.345 593 512 0.042017 12.350 614 539 0.041152 12.355 668 569 0.039526 12.360 664 603 0.039683 12.365 722 642 0.038023 12.370 752 684 0.037313 12.375 758 732 0.037175 12.380 828 786 0.035587 12.385 1027 847 0.031847 12.390 1066 916 0.031348 12.395 1163 994 0.030030 12.400 1243 1085 0.028986 12.405 1399 1189 0.027322 12.410 1587 1311 0.025641 12.415 1781 1450 0.024213 12.420 2014 1605 0.022831 12.425 2149 1761 0.022075 12.430 2186 1880 0.021882 12.435 1989 1895 0.022883 12.440 1690 1752 0.024876 12.445 1563 1490 0.025840 12.450 1326 1219 0.028011 12.455 1180 1007 0.029674 12.460 1040 860 0.031746 12.465 976 762 0.032680 12.470 855 698 0.034965 12.475 870 657 0.034722 12.480 800 633 0.036101 12.485 870 623 0.034602 12.490 817 626 0.035714 12.495 851 639 0.035088 12.500 924 662 0.033557 12.505 1005 693 0.032258 12.510 958 731 0.033003 12.515 994 777 0.032362 12.520 1066 831 0.031250 12.525 1189 893 0.029674 12.530 1267 964 0.028653 12.535 1517 1046 0.026247 12.540 1633 1140 0.025253 12.545 1645 1250 0.025189 12.550 1734 1379 0.024570 12.555 1894 1530 0.023474 12.560 1985 1710 0.022936 12.565 2088 1923 0.022321 12.570 2174 2171 0.021978 12.575 2444 2439 0.020661 12.580 2730 2666 0.019569 12.585 2973 2721 0.018762 12.590 2963 2475 0.018762 12.595 2470 1995 0.020576 12.600 1788 1522 0.024155 12.605 1166 1183 0.029940 12.610 846 961 0.035088 12.615 687 815 0.038911 12.620 568 716 0.042735 12.625 517 647 0.044843 12.630 469 597 0.047170 12.635 492 560 0.046083 12.640 450 532 0.048077 12.645 439 510 0.048780 12.650 479 492 0.046729 12.655 468 478 0.047170 12.660 478 466 0.046729 12.665 464 456 0.047619 12.670 441 448 0.048544 12.675 440 441 0.048780 12.680 448 435 0.048309 12.685 481 430 0.046512 12.690 454 426 0.047847 12.695 432 422 0.049261 12.700 484 419 0.046296 12.705 438 416 0.048780 12.710 500 413 0.045662 12.715 463 411 0.047393 12.720 486 409 0.046296 12.725 461 407 0.047619 12.730 483 406 0.046512 12.735 455 405 0.047847 12.740 438 403 0.048780 12.745 441 402 0.048544 12.750 454 401 0.047847 12.755 425 401 0.049505 12.760 464 400 0.047393 12.765 447 399 0.048309 12.770 448 399 0.048077 12.775 472 399 0.046948 12.780 463 398 0.047393 12.785 470 398 0.047170 12.790 422 398 0.049505 12.795 445 398 0.048544 12.800 469 398 0.047170 12.805 422 398 0.049751 12.810 478 398 0.046729 12.815 438 399 0.048780 12.820 422 399 0.049751 12.825 456 399 0.047847 12.830 501 400 0.045455 12.835 416 400 0.050000 12.840 484 401 0.046512 12.845 459 401 0.047619 12.850 434 402 0.049020 12.855 468 403 0.047170 12.860 463 404 0.047393 12.865 429 405 0.049261 12.870 459 406 0.047619 12.875 487 407 0.046296 12.880 427 409 0.049505 12.885 448 411 0.048077 12.890 483 413 0.046296 12.895 445 415 0.048309 12.900 465 419 0.047170 12.905 501 422 0.045455 12.910 465 426 0.047393 12.915 472 430 0.046948 12.920 488 434 0.046083 12.925 489 440 0.046083 12.930 485 446 0.046296 12.935 493 453 0.046083 12.940 468 460 0.047170 12.945 502 469 0.045455 12.950 488 478 0.046083 12.955 481 489 0.046512 12.960 479 501 0.046512 12.965 489 514 0.046083 12.970 458 530 0.047619 12.975 470 549 0.046948 12.980 529 570 0.044444 12.985 522 591 0.044643 12.990 520 606 0.044843 12.995 499 605 0.045662 13.000 493 586 0.045872 13.005 496 560 0.045662 13.010 538 541 0.044053 13.015 494 530 0.045872 13.020 561 526 0.043103 13.025 520 527 0.044643 13.030 554 532 0.043290 13.035 529 540 0.044444 13.040 532 550 0.044248 13.045 556 562 0.043290 13.050 521 577 0.044643 13.055 620 596 0.040984 13.060 618 617 0.040984 13.065 640 643 0.040323 13.070 705 674 0.038462 13.075 738 712 0.037594 13.080 803 758 0.035971 13.085 805 816 0.035842 13.090 881 887 0.034247 13.095 913 973 0.033784 13.100 1038 1076 0.031646 13.105 1138 1195 0.030211 13.110 1226 1331 0.029070 13.115 1335 1485 0.027855 13.120 1557 1658 0.025840 13.125 1734 1852 0.024450 13.130 2031 2070 0.022624 13.135 2271 2315 0.021413 13.140 2615 2592 0.019920 13.145 3022 2905 0.018519 13.150 3397 3259 0.017452 13.155 3817 3660 0.016529 13.160 4490 4109 0.015221 13.165 4975 4597 0.014472 13.170 5813 5093 0.013387 13.175 6155 5522 0.012987 13.180 6231 5752 0.012903 13.185 5537 5635 0.013699 13.190 4878 5127 0.014599 13.195 4249 4369 0.015625 13.200 3632 3589 0.016892 13.205 2966 2935 0.018692 13.210 2691 2442 0.019646 13.215 2370 2087 0.020964 13.220 2142 1834 0.021978 13.225 1981 1654 0.022883 13.230 1785 1527 0.024096 13.235 1544 1434 0.025974 13.240 1487 1365 0.026455 13.245 1403 1308 0.027248 13.250 1276 1253 0.028490 13.255 1238 1195 0.028902 13.260 1035 1128 0.031646 13.265 1046 1055 0.031546 13.270 1006 980 0.032051 13.275 955 909 0.032895 13.280 861 844 0.034722 13.285 891 789 0.034130 13.290 822 742 0.035461 13.295 805 702 0.035971 13.300 707 669 0.038314 13.305 720 641 0.037879 13.310 681 618 0.039062 13.315 698 598 0.038462 13.320 651 581 0.040000 13.325 662 566 0.039683 13.330 637 554 0.040486 13.335 611 543 0.041152 13.340 606 534 0.041494 13.345 557 526 0.043103 13.350 579 519 0.042373 13.355 536 514 0.044053 13.360 507 509 0.045249 13.365 594 505 0.041667 13.370 559 501 0.043103 13.375 530 498 0.044248 13.380 540 496 0.043860 13.385 541 495 0.043668 13.390 562 494 0.042918 13.395 590 494 0.041841 13.400 569 495 0.042735 13.405 526 496 0.044444 13.410 573 498 0.042553 13.415 533 500 0.044248 13.420 599 504 0.041667 13.425 611 508 0.041322 13.430 613 512 0.041152 13.435 607 514 0.041322 13.440 610 516 0.041322 13.445 581 518 0.042194 13.450 571 522 0.042553 13.455 592 529 0.041841 13.460 638 539 0.040323 13.465 658 551 0.039683 13.470 654 566 0.039841 13.475 665 585 0.039526 13.480 740 609 0.037453 13.485 753 637 0.037037 13.490 799 671 0.035971 13.495 875 711 0.034364 13.500 885 756 0.034247 13.505 920 807 0.033557 13.510 975 865 0.032573 13.515 1052 930 0.031348 13.520 1075 1003 0.030960 13.525 1327 1084 0.027933 13.530 1302 1175 0.028169 13.535 1596 1278 0.025510 13.540 1629 1392 0.025189 13.545 1817 1517 0.023866 13.550 2038 1652 0.022523 13.555 2121 1790 0.022173 13.560 2258 1914 0.021459 13.565 2289 1998 0.021277 13.570 2188 2007 0.021739 13.575 2135 1917 0.022026 13.580 1925 1742 0.023148 13.585 1723 1528 0.024510 13.590 1496 1324 0.026316 13.595 1217 1153 0.029240 13.600 1065 1021 0.031153 13.605 873 920 0.034483 13.610 802 845 0.035971 13.615 747 788 0.037175 13.620 697 745 0.038462 13.625 659 713 0.039526 13.630 670 688 0.039370 13.635 606 670 0.041322 13.640 660 656 0.039526 13.645 667 645 0.039370 13.650 667 638 0.039370 13.655 669 633 0.039370 13.660 648 630 0.040000 13.665 673 628 0.039216 13.670 672 627 0.039216 13.675 693 627 0.038610 13.680 728 629 0.037594 13.685 709 632 0.038168 13.690 699 636 0.038462 13.695 774 643 0.036496 13.700 763 650 0.036765 13.705 755 660 0.037037 13.710 801 671 0.035842 13.715 809 684 0.035714 13.720 798 698 0.036101 13.725 858 715 0.034722 13.730 887 734 0.034130 13.735 886 754 0.034247 13.740 922 777 0.033445 13.745 969 801 0.032680 13.750 996 827 0.032154 13.755 1043 856 0.031447 13.760 1068 886 0.031250 13.765 1150 917 0.030030 13.770 1101 951 0.030581 13.775 1158 985 0.029940 13.780 1249 1023 0.028818 13.785 1241 1063 0.028902 13.790 1337 1105 0.027778 13.795 1296 1147 0.028249 13.800 1290 1191 0.028409 13.805 1392 1236 0.027322 13.810 1426 1281 0.027027 13.815 1360 1326 0.027624 13.820 1485 1370 0.026385 13.825 1503 1410 0.026247 13.830 1512 1446 0.026247 13.835 1608 1475 0.025381 13.840 1550 1496 0.025773 13.845 1560 1506 0.025707 13.850 1545 1504 0.025907 13.855 1578 1490 0.025641 13.860 1558 1464 0.025773 13.865 1570 1428 0.025707 13.870 1576 1382 0.025641 13.875 1564 1329 0.025707 13.880 1526 1272 0.025974 13.885 1455 1214 0.026596 13.890 1412 1155 0.027027 13.895 1379 1098 0.027322 13.900 1230 1045 0.029070 13.905 1103 994 0.030581 13.910 1074 948 0.030960 13.915 979 906 0.032468 13.920 973 868 0.032573 13.925 833 834 0.035211 13.930 827 803 0.035461 13.935 795 776 0.035971 13.940 818 752 0.035461 13.945 726 731 0.037736 13.950 651 713 0.039841 13.955 666 697 0.039526 13.960 656 684 0.039683 13.965 650 673 0.039841 13.970 632 664 0.040486 13.975 599 659 0.041667 13.980 639 656 0.040161 13.985 607 656 0.041322 13.990 683 661 0.038911 13.995 628 670 0.040650 14.000 706 686 0.038314 14.005 701 707 0.038462 14.010 696 734 0.038610 14.015 721 766 0.037879 14.020 694 804 0.038760 14.025 804 849 0.035842 14.030 774 901 0.036496 14.035 810 961 0.035587 14.040 884 1031 0.034130 14.045 863 1113 0.034602 14.050 1017 1210 0.031847 14.055 1088 1324 0.030769 14.060 1293 1460 0.028329 14.065 1421 1618 0.027027 14.070 1606 1796 0.025381 14.075 1977 1965 0.022883 14.080 2313 2058 0.021142 14.085 2349 1987 0.021008 14.090 1819 1751 0.023866 14.095 1270 1480 0.028571 14.100 1168 1276 0.029851 14.105 1041 1151 0.031447 14.110 1057 1086 0.031250 14.115 1088 1063 0.030769 14.120 1130 1070 0.030211 14.125 1135 1101 0.030211 14.130 1226 1155 0.029070 14.135 1361 1230 0.027548 14.140 1462 1322 0.026525 14.145 1527 1430 0.025974 14.150 1554 1549 0.025840 14.155 1683 1674 0.024814 14.160 1851 1799 0.023641 14.165 1870 1917 0.023474 14.170 2034 2028 0.022573 14.175 2112 2136 0.022173 14.180 2189 2256 0.021739 14.185 2249 2406 0.021413 14.190 2326 2600 0.021053 14.195 2386 2850 0.020833 14.200 2525 3153 0.020284 14.205 2519 3481 0.020284 14.210 2545 3740 0.020161 14.215 2581 3755 0.020040 14.220 2563 3388 0.020080 14.225 2467 2749 0.020492 14.230 2376 2127 0.020833 14.235 2105 1670 0.022124 14.240 1805 1365 0.023866 14.245 1509 1163 0.026110 14.250 1307 1027 0.028090 14.255 1100 932 0.030581 14.260 919 865 0.033557 14.265 878 818 0.034364 14.270 811 785 0.035714 14.275 785 762 0.036364 14.280 715 749 0.038023 14.285 727 743 0.037736 14.290 716 744 0.038023 14.295 700 750 0.038462 14.300 731 762 0.037594 14.305 691 779 0.038610 14.310 699 801 0.038462 14.315 695 828 0.038462 14.320 761 861 0.036765 14.325 790 898 0.036232 14.330 800 942 0.035971 14.335 872 991 0.034483 14.340 860 1047 0.034722 14.345 948 1111 0.033003 14.350 956 1181 0.032895 14.355 1010 1258 0.032051 14.360 1105 1334 0.030581 14.365 1081 1397 0.030960 14.370 1141 1427 0.030120 14.375 1210 1417 0.029240 14.380 1184 1384 0.029499 14.385 1108 1353 0.030488 14.390 1153 1329 0.029940 14.395 1222 1313 0.029070 14.400 1267 1301 0.028490 14.405 1245 1296 0.028818 14.410 1331 1297 0.027855 14.415 1279 1307 0.028409 14.420 1359 1323 0.027624 14.425 1368 1333 0.027473 14.430 1351 1307 0.027701 14.435 1298 1218 0.028169 14.440 1098 1080 0.030675 14.445 868 945 0.034483 14.450 736 841 0.037453 14.455 609 766 0.041152 14.460 622 712 0.040816 14.465 563 672 0.042735 14.470 589 642 0.041841 14.475 539 618 0.043668 14.480 554 599 0.043103 14.485 520 583 0.044643 14.490 512 571 0.044843 14.495 530 561 0.044053 14.500 512 553 0.044843 14.505 521 547 0.044643 14.510 480 542 0.046296 14.515 489 539 0.045872 14.520 483 536 0.046296 14.525 537 535 0.043860 14.530 473 535 0.046729 14.535 470 535 0.046729 14.540 529 536 0.044248 14.545 513 537 0.044843 14.550 535 539 0.043860 14.555 518 540 0.044643 14.560 554 541 0.043103 14.565 491 541 0.045872 14.570 491 541 0.045872 14.575 526 539 0.044248 14.580 515 537 0.044643 14.585 563 533 0.042735 14.590 528 528 0.044248 14.595 545 522 0.043478 14.600 507 516 0.045045 14.605 549 508 0.043290 14.610 535 501 0.043860 14.615 510 493 0.045045 14.620 480 485 0.046296 14.625 508 478 0.045045 14.630 451 471 0.047847 14.635 431 465 0.048780 14.640 469 458 0.046948 14.645 471 453 0.046729 14.650 458 448 0.047619 14.655 404 442 0.050505 14.660 426 438 0.049261 14.665 470 435 0.046729 14.670 401 432 0.050761 14.675 408 430 0.050251 14.680 364 427 0.053191 14.685 384 425 0.051813 14.690 405 424 0.050505 14.695 400 423 0.050761 14.700 407 422 0.050251 14.705 421 421 0.049505 14.710 444 420 0.048077 14.715 421 420 0.049505 14.720 442 420 0.048309 14.725 407 420 0.050251 14.730 416 420 0.049751 14.735 430 421 0.049020 14.740 416 422 0.049751 14.745 392 423 0.051282 14.750 413 424 0.049751 14.755 422 425 0.049505 14.760 416 426 0.049751 14.765 465 427 0.047170 14.770 379 428 0.052083 14.775 432 429 0.048780 14.780 430 429 0.048780 14.785 437 429 0.048544 14.790 442 429 0.048309 14.795 439 428 0.048544 14.800 416 427 0.049751 14.805 421 425 0.049505 14.810 378 423 0.052083 14.815 395 421 0.051020 14.820 427 418 0.049020 14.825 441 416 0.048309 14.830 403 413 0.050505 14.835 389 410 0.051546 14.840 375 408 0.052356 14.845 437 406 0.048544 14.850 418 403 0.049505 14.855 358 401 0.053763 14.860 419 400 0.049505 14.865 370 398 0.052632 14.870 371 396 0.052632 14.875 391 395 0.051282 14.880 385 394 0.051546 14.885 402 393 0.050761 14.890 394 392 0.051020 14.895 375 391 0.052356 14.900 346 390 0.054348 14.905 378 389 0.052083 14.910 391 389 0.051282 14.915 405 388 0.050251 14.920 368 388 0.052910 14.925 384 387 0.051813 14.930 408 387 0.050251 14.935 396 387 0.051020 14.940 346 386 0.054645 14.945 361 386 0.053191 14.950 367 386 0.052910 14.955 365 386 0.053191 14.960 373 386 0.052632 14.965 380 386 0.052083 14.970 412 386 0.050000 14.975 377 386 0.052356 14.980 395 386 0.051020 14.985 357 386 0.053476 14.990 376 386 0.052356 14.995 409 386 0.050251 15.000 386 386 0.051546 15.005 365 386 0.053191 15.010 343 386 0.054645 15.015 375 387 0.052356 15.020 397 387 0.050761 15.025 363 387 0.053191 15.030 404 388 0.050505 15.035 357 388 0.053476 15.040 355 389 0.053763 15.045 374 389 0.052356 15.050 391 390 0.051282 15.055 366 391 0.052910 15.060 393 392 0.051020 15.065 335 393 0.055249 15.070 379 393 0.052083 15.075 419 395 0.049505 15.080 382 396 0.051813 15.085 401 397 0.050505 15.090 383 398 0.051813 15.095 381 400 0.051813 15.100 381 402 0.051813 15.105 379 403 0.051813 15.110 412 406 0.050000 15.115 382 408 0.051813 15.120 393 410 0.051020 15.125 389 413 0.051282 15.130 430 417 0.048780 15.135 392 420 0.051282 15.140 396 424 0.050761 15.145 415 429 0.049505 15.150 403 434 0.050505 15.155 452 440 0.047619 15.160 447 447 0.047847 15.165 409 455 0.050000 15.170 418 464 0.049505 15.175 485 474 0.046083 15.180 398 485 0.050761 15.185 486 498 0.045872 15.190 458 512 0.047170 15.195 461 528 0.047170 15.200 512 545 0.044643 15.205 548 564 0.043290 15.210 522 585 0.044248 15.215 571 606 0.042373 15.220 639 629 0.040000 15.225 639 652 0.040000 15.230 616 674 0.040650 15.235 697 695 0.038314 15.240 670 714 0.039062 15.245 653 728 0.039526 15.250 655 738 0.039526 15.255 717 744 0.037736 15.260 696 746 0.038314 15.265 685 745 0.038610 15.270 714 741 0.037879 15.275 704 735 0.038023 15.280 751 726 0.037037 15.285 701 713 0.038168 15.290 685 698 0.038610 15.295 656 680 0.039526 15.300 648 660 0.039683 15.305 643 640 0.039841 15.310 667 622 0.039216 15.315 591 606 0.041667 15.320 676 594 0.038911 15.325 700 584 0.038168 15.330 671 579 0.039062 15.335 685 578 0.038610 15.340 682 581 0.038760 15.345 732 588 0.037313 15.350 759 600 0.036765 15.355 747 617 0.037037 15.360 728 637 0.037594 15.365 780 663 0.036232 15.370 856 693 0.034602 15.375 866 728 0.034483 15.380 833 769 0.035088 15.385 962 815 0.032680 15.390 955 866 0.032787 15.395 972 922 0.032468 15.400 1099 981 0.030488 15.405 1055 1040 0.031250 15.410 1125 1093 0.030211 15.415 1174 1129 0.029499 15.420 1204 1139 0.029155 15.425 1110 1115 0.030395 15.430 1151 1062 0.029851 15.435 1124 991 0.030211 15.440 1155 919 0.029762 15.445 1076 855 0.030864 15.450 1047 804 0.031250 15.455 962 764 0.032573 15.460 881 733 0.034014 15.465 827 707 0.035211 15.470 764 683 0.036630 15.475 667 659 0.039216 15.480 684 633 0.038610 15.485 660 605 0.039370 15.490 607 579 0.040984 15.495 631 554 0.040323 15.500 579 533 0.042017 15.505 566 514 0.042553 15.510 528 500 0.043860 15.515 492 488 0.045662 15.520 484 478 0.046083 15.525 524 470 0.044053 15.530 495 465 0.045455 15.535 500 461 0.045249 15.540 490 458 0.045662 15.545 493 457 0.045455 15.550 522 458 0.044248 15.555 506 460 0.044843 15.560 517 464 0.044444 15.565 509 470 0.044843 15.570 539 479 0.043668 15.575 544 489 0.043290 15.580 556 500 0.042918 15.585 572 514 0.042194 15.590 565 530 0.042553 15.595 652 548 0.039683 15.600 630 569 0.040323 15.605 675 592 0.038911 15.610 706 618 0.038023 15.615 704 649 0.038023 15.620 763 682 0.036496 15.625 682 718 0.038760 15.630 750 747 0.036900 15.635 670 756 0.039062 15.640 648 727 0.039841 15.645 572 668 0.042194 15.650 541 605 0.043478 15.655 524 557 0.044248 15.660 479 526 0.046083 15.665 521 505 0.044248 15.670 439 492 0.048077 15.675 456 483 0.047393 15.680 414 478 0.049751 15.685 435 474 0.048544 15.690 405 471 0.050251 15.695 397 468 0.050761 15.700 420 465 0.049261 15.705 385 461 0.051546 15.710 392 456 0.051020 15.715 376 451 0.052083 15.720 352 445 0.053763 15.725 340 438 0.054645 15.730 405 432 0.050251 15.735 362 427 0.053191 15.740 379 421 0.052083 15.745 379 416 0.052083 15.750 367 412 0.052632 15.755 330 409 0.055866 15.760 357 406 0.053476 15.765 351 403 0.054054 15.770 351 401 0.053763 15.775 396 399 0.050761 15.780 365 397 0.052910 15.785 344 396 0.054348 15.790 361 395 0.053191 15.795 344 395 0.054645 15.800 367 395 0.052910 15.805 330 395 0.055556 15.810 381 396 0.051813 15.815 397 397 0.050761 15.820 382 399 0.051813 15.825 373 401 0.052356 15.830 385 404 0.051546 15.835 375 407 0.052083 15.840 367 411 0.052632 15.845 419 415 0.049261 15.850 371 421 0.052356 15.855 390 427 0.051020 15.860 368 435 0.052632 15.865 426 443 0.049020 15.870 416 449 0.049505 15.875 452 451 0.047619 15.880 432 445 0.048544 15.885 425 433 0.049020 15.890 400 421 0.050505 15.895 402 413 0.050251 15.900 424 407 0.049020 15.905 402 403 0.050505 15.910 371 401 0.052356 15.915 381 400 0.051813 15.920 346 399 0.054348 15.925 372 398 0.052356 15.930 427 398 0.049020 15.935 376 398 0.052083 15.940 363 398 0.052910 15.945 370 398 0.052632 15.950 391 398 0.051020 15.955 385 398 0.051546 15.960 357 397 0.053476 15.965 380 397 0.051813 15.970 388 397 0.051282 15.975 365 396 0.052910 15.980 374 395 0.052083 15.985 406 394 0.050251 15.990 390 394 0.051282 15.995 363 393 0.052910 16.000 374 391 0.052083 16.005 373 390 0.052356 16.010 372 389 0.052356 16.015 394 388 0.051020 16.020 361 387 0.053191 16.025 351 386 0.053763 16.030 375 385 0.052083 16.035 346 384 0.054348 16.040 355 383 0.053476 16.045 349 382 0.054054 16.050 360 381 0.053191 16.055 383 381 0.051546 16.060 401 380 0.050251 16.065 357 379 0.053476 16.070 351 379 0.053763 16.075 357 378 0.053476 16.080 375 378 0.052083 16.085 367 378 0.052632 16.090 361 377 0.053191 16.095 359 377 0.053191 16.100 339 377 0.054645 16.105 373 377 0.052083 16.110 379 377 0.051813 16.115 366 378 0.052910 16.120 330 378 0.055556 16.125 367 379 0.052632 16.130 401 380 0.050505 16.135 381 380 0.051546 16.140 377 382 0.052083 16.145 377 383 0.052083 16.150 410 384 0.049751 16.155 425 386 0.049020 16.160 412 388 0.049751 16.165 409 390 0.050000 16.170 421 392 0.049261 16.175 368 395 0.052632 16.180 423 398 0.049020 16.185 476 402 0.046296 16.190 426 406 0.048780 16.195 395 411 0.050761 16.200 399 415 0.050505 16.205 442 418 0.048077 16.210 452 416 0.047619 16.215 436 409 0.048309 16.220 433 400 0.048544 16.225 369 392 0.052632 16.230 404 387 0.050000 16.235 410 383 0.050000 16.240 357 381 0.053476 16.245 360 380 0.053191 16.250 372 379 0.052356 16.255 367 378 0.052632 16.260 382 377 0.051813 16.265 352 375 0.053763 16.270 337 374 0.054945 16.275 320 372 0.056497 16.280 335 371 0.055249 16.285 316 370 0.056818 16.290 312 369 0.057143 16.295 350 369 0.054054 16.300 308 368 0.057471 16.305 344 368 0.054348 16.310 326 368 0.055866 16.315 358 367 0.053191 16.320 305 367 0.057803 16.325 311 367 0.057143 16.330 359 367 0.053191 16.335 322 367 0.056180 16.340 341 367 0.054645 16.345 319 367 0.056497 16.350 370 367 0.052356 16.355 308 367 0.057471 16.360 392 367 0.051020 16.365 342 367 0.054645 16.370 333 367 0.055249 16.375 344 367 0.054348 16.380 323 367 0.056180 16.385 305 367 0.057803 16.390 349 367 0.054054 16.395 323 368 0.056180 16.400 343 368 0.054348 16.405 351 368 0.053763 16.410 349 368 0.054054 16.415 364 369 0.052910 16.420 351 369 0.053763 16.425 352 369 0.053763 16.430 372 370 0.052083 16.435 330 371 0.055556 16.440 352 371 0.053763 16.445 355 372 0.053476 16.450 336 373 0.054945 16.455 350 374 0.053763 16.460 335 375 0.055249 16.465 359 376 0.053191 16.470 370 377 0.052356 16.475 355 378 0.053476 16.480 370 380 0.052356 16.485 365 383 0.052632 16.490 370 385 0.052356 16.495 367 389 0.052632 16.500 388 394 0.051282 16.505 399 400 0.050505 16.510 388 407 0.051020 16.515 394 416 0.050761 16.520 396 427 0.050761 16.525 430 439 0.048780 16.530 437 453 0.048077 16.535 483 469 0.045872 16.540 431 488 0.048780 16.545 449 510 0.047619 16.550 438 536 0.048077 16.555 481 567 0.045872 16.560 477 600 0.046296 16.565 498 634 0.045249 16.570 487 658 0.045662 16.575 492 658 0.045455 16.580 486 627 0.045662 16.585 505 576 0.044843 16.590 481 527 0.046083 16.595 473 492 0.046296 16.600 409 469 0.049751 16.605 440 455 0.048077 16.610 417 447 0.049261 16.615 434 443 0.048544 16.620 414 443 0.049505 16.625 418 444 0.049261 16.630 432 448 0.048544 16.635 398 454 0.050505 16.640 384 462 0.051282 16.645 415 472 0.049505 16.650 421 482 0.049020 16.655 466 490 0.046729 16.660 465 494 0.046729 16.665 481 492 0.045872 16.670 461 487 0.046948 16.675 459 484 0.046948 16.680 448 485 0.047619 16.685 501 490 0.045045 16.690 522 497 0.044053 16.695 546 505 0.043103 16.700 487 516 0.045662 16.705 530 527 0.043860 16.710 544 538 0.043103 16.715 517 550 0.044444 16.720 555 560 0.042735 16.725 549 570 0.043103 16.730 593 576 0.041322 16.735 589 580 0.041494 16.740 629 580 0.040161 16.745 574 576 0.042017 16.750 571 568 0.042194 16.755 603 557 0.040984 16.760 639 544 0.039841 16.765 607 529 0.040984 16.770 541 515 0.043290 16.775 562 501 0.042373 16.780 570 489 0.042194 16.785 531 477 0.043668 16.790 539 467 0.043478 16.795 491 458 0.045455 16.800 493 451 0.045455 16.805 486 445 0.045662 16.810 469 440 0.046512 16.815 407 437 0.050000 16.820 440 434 0.048077 16.825 439 433 0.048077 16.830 430 433 0.048544 16.835 454 434 0.047170 16.840 451 438 0.047393 16.845 430 444 0.048544 16.850 454 452 0.047170 16.855 435 462 0.048309 16.860 492 475 0.045455 16.865 493 491 0.045455 16.870 480 509 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