# Electronic Supplementary Material (ESI) for New Journal of Chemistry
# This journal is © The Royal Society of Chemistry and The Centre National de la Recherche Scientifique 2014

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#
#                 Cambridge Crystallographic Data Centre
#                                CCDC 
# 
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# 
#  This CIF contains data from an original supplementary publication
#  deposited with the CCDC, and may include chemical, crystal,
#  experimental, refinement, atomic coordinates,
#  anisotropic displacement parameters and molecular geometry data,
#  as required by the journal to which it was submitted.
#
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#  fide research purposes only. It may contain copyright material
#  of the CCDC or of third parties, and may not be copied or further
#  disseminated in any form, whether machine-readable or not,
#  except for the purpose of generating routine backup copies
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#  from this site to visualise CIF-encoded structures and 
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data_111

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'Al3 K6 Na3 O24 P6'
_chemical_formula_weight         954.33

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           Monoclinic
_symmetry_space_group_name_H-M   P2(1)/c


loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'

_cell_length_a                   19.9204(16)
_cell_length_b                   9.6139(8)
_cell_length_c                   13.2845(11)
_cell_angle_alpha                90.00
_cell_angle_beta                 98.934(4)
_cell_angle_gamma                90.00
_cell_volume                     2513.3(4)
_cell_formula_units_Z            4
_cell_measurement_temperature    296(2)
_cell_measurement_reflns_used    9922
_cell_measurement_theta_min      2.63
_cell_measurement_theta_max      27.24

_exptl_crystal_description       block
_exptl_crystal_colour            colorless
_exptl_crystal_size_max          0.22
_exptl_crystal_size_mid          0.14
_exptl_crystal_size_min          0.09
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    2.522
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1872
_exptl_absorpt_coefficient_mu    1.683
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_correction_T_min  0.7084
_exptl_absorpt_correction_T_max  0.8605
_exptl_absorpt_process_details   face-indexed

_exptl_special_details           
;
ISOR 0.001 O5A O6A O5B O6B 
omit -1 0 2
omit 2 1 0

PART 1
O5A    1   0.173212   0.409025   0.275940  21.000000   0.023800 = 
           0.046280   0.020160  -0.003720   0.007850   0.002960
O6A    1   0.209465   0.219180   0.173848  31.000000   0.054750 = 
           0.012490   0.046230  -0.002810   0.019550   0.001030
PART 2
O5B    1   0.157105   0.337792   0.249762 -21.000000   0.036200 = 
           0.036120   0.036100   0.000070   0.005780   0.000080
O6B    1   0.208863   0.233330   0.118434 -31.000000   0.031510 = 
           0.030900   0.031170  -0.000130   0.004750   0.000240
PART 0
;

_diffrn_ambient_temperature      296(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       '\f and \w scans'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         0
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            39102
_diffrn_reflns_av_R_equivalents  0.0341
_diffrn_reflns_av_sigmaI/netI    0.0182
_diffrn_reflns_limit_h_min       -23
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_theta_min         1.03
_diffrn_reflns_theta_max         24.99
_reflns_number_total             4430
_reflns_number_gt                3878
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'Bruker APEX2'
_computing_cell_refinement       'Bruker SAINT'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'

_refine_special_details          
; 
 Refinement of F^2^ against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F^2^, conventional R-factors R are based 
 on F, with F set to zero for negative F^2^. The threshold expression of 
 F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F^2^ are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[\s^2^(Fo^2^)+(0.0546P)^2^+7.7629P] where P=(Fo^2^+2Fc^2^)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   ?
_refine_ls_hydrogen_treatment    ?
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         4430
_refine_ls_number_parameters     399
_refine_ls_number_restraints     12
_refine_ls_R_factor_all          0.0431
_refine_ls_R_factor_gt           0.0370
_refine_ls_wR_factor_ref         0.1076
_refine_ls_wR_factor_gt          0.1033
_refine_ls_goodness_of_fit_ref   1.047
_refine_ls_restrained_S_all      1.046
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Na1 Na 0.26906(7) 0.55797(15) 0.35713(11) 0.0240(3) Uani 1 1 d . . .
Na2 Na 0.42086(7) 0.96744(15) 0.18782(11) 0.0230(3) Uani 1 1 d . . .
Na3 Na 0.06685(7) 0.43333(15) 0.31870(11) 0.0231(3) Uani 1 1 d . . .
K1 K 0.05460(5) 0.16634(10) 0.08008(7) 0.0321(2) Uani 1 1 d . . .
K2 K 0.20005(5) 0.18444(9) 0.40232(7) 0.0307(2) Uani 1 1 d . . .
K3 K 0.28702(4) 0.66646(9) 0.08147(7) 0.0301(2) Uani 1 1 d . . .
K4 K 0.44934(5) 0.81613(9) -0.09782(7) 0.0308(2) Uani 1 1 d . . .
K5 K 0.13566(5) 0.81379(10) 0.27746(7) 0.0299(2) Uani 1 1 d . . .
K6 K 0.39566(6) 0.34089(14) 0.24559(9) 0.0534(3) Uani 1 1 d . . .
Al1 Al 0.40312(5) 0.43237(11) -0.04789(8) 0.0161(2) Uani 1 1 d . . .
Al2 Al 0.24234(5) 0.07465(10) 0.11809(8) 0.0163(2) Uani 1 1 d . . .
Al3 Al 0.10240(5) 0.56523(11) 0.05686(8) 0.0148(2) Uani 1 1 d . . .
P1 P 0.03304(4) 0.06753(9) 0.35518(7) 0.0146(2) Uani 1 1 d . . .
P2 P 0.35613(5) 0.15033(10) -0.00432(8) 0.0231(2) Uani 1 1 d . . .
P3 P 0.20751(5) 0.37795(9) 0.18467(7) 0.0160(2) Uani 1 1 d . . .
P4 P 0.45866(5) 0.61859(10) 0.12810(7) 0.0186(2) Uani 1 1 d . . .
P5 P 0.14315(5) 0.86253(10) 0.00763(7) 0.0187(2) Uani 1 1 d . . .
P6 P 0.30381(5) 0.90378(10) 0.30507(7) 0.0200(2) Uani 1 1 d . . .
O1 O -0.04376(13) 0.0437(3) 0.3609(2) 0.0322(7) Uani 1 1 d . . .
O2 O 0.07052(14) -0.0437(3) 0.42915(19) 0.0264(6) Uani 1 1 d . . .
O3 O 0.04320(13) 0.0281(3) 0.24934(19) 0.0253(6) Uani 1 1 d . . .
O4 O 0.05575(15) 0.2106(3) 0.3906(2) 0.0325(7) Uani 1 1 d . . .
O5A O 0.17321(18) 0.4090(5) 0.2759(3) 0.0296(15) Uani 0.880(16) 1 d P A 1
O6A O 0.2095(2) 0.2192(4) 0.1738(6) 0.0366(19) Uani 0.81(2) 1 d P A 1
O5B O 0.1571(16) 0.338(4) 0.250(3) 0.036(9) Uani 0.120(16) 1 d PU A 2
O6B O 0.2089(9) 0.2333(19) 0.118(3) 0.031(6) Uani 0.19(2) 1 d PU . 2
O7 O 0.28140(13) 0.1154(3) 0.0138(2) 0.0318(7) Uani 1 1 d . . .
O8 O 0.37682(16) 0.0431(3) -0.0749(3) 0.0481(9) Uani 1 1 d . . .
O9 O 0.34690(12) 0.2932(3) -0.0605(2) 0.0224(6) Uani 1 1 d . . .
O10 O 0.40293(15) 0.1666(3) 0.0947(2) 0.0440(9) Uani 1 1 d . . .
O11 O 0.16462(14) 0.4383(3) 0.0864(2) 0.0353(7) Uani 1 1 d . . .
O12 O 0.27734(14) 0.4374(3) 0.1963(2) 0.0364(7) Uani 1 1 d . A .
O13 O 0.30316(17) 0.7514(3) 0.2843(2) 0.0415(8) Uani 1 1 d . . .
O14 O 0.13480(14) 0.7322(3) 0.0765(2) 0.0288(6) Uani 1 1 d . A .
O15 O 0.07619(15) 0.9071(3) -0.0485(3) 0.0445(8) Uani 1 1 d . . .
O16 O 0.16901(14) 0.9772(3) 0.0872(2) 0.0318(7) Uani 1 1 d . . .
O17 O 0.25123(14) 0.9558(3) 0.3641(2) 0.0344(7) Uani 1 1 d . . .
O18 O 0.19662(17) 0.8300(3) -0.0549(3) 0.0427(8) Uani 1 1 d . . .
O19 O 0.30033(15) 0.9825(4) 0.2014(2) 0.0479(9) Uani 1 1 d . . .
O20 O 0.37731(13) 0.9442(3) 0.3583(2) 0.0279(6) Uani 1 1 d . . .
O21 O 0.42291(17) 0.7570(3) 0.1212(3) 0.0532(10) Uani 1 1 d . A .
O22 O 0.51858(13) 0.6312(3) 0.0652(2) 0.0255(6) Uani 1 1 d . . .
O23 O 0.48177(15) 0.5629(4) 0.2315(2) 0.0512(10) Uani 1 1 d . . .
O24 O 0.40852(13) 0.5107(3) 0.0701(2) 0.0283(6) Uani 1 1 d . A .

loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Na1 0.0243(8) 0.0233(8) 0.0252(8) -0.0040(6) 0.0064(6) 0.0011(6)
Na2 0.0221(8) 0.0219(7) 0.0252(8) 0.0016(6) 0.0044(6) 0.0016(6)
Na3 0.0238(8) 0.0245(8) 0.0213(8) 0.0009(6) 0.0044(6) 0.0028(6)
K1 0.0294(5) 0.0406(5) 0.0271(5) 0.0090(4) 0.0070(4) -0.0027(4)
K2 0.0319(5) 0.0274(5) 0.0329(5) 0.0000(4) 0.0051(4) 0.0016(4)
K3 0.0232(4) 0.0320(5) 0.0356(5) 0.0036(4) 0.0067(4) 0.0040(4)
K4 0.0310(5) 0.0255(5) 0.0374(5) 0.0053(4) 0.0096(4) 0.0002(4)
K5 0.0312(5) 0.0352(5) 0.0237(5) -0.0029(4) 0.0060(4) 0.0047(4)
K6 0.0522(7) 0.0637(8) 0.0477(7) -0.0151(6) 0.0187(6) -0.0122(6)
Al1 0.0153(5) 0.0170(5) 0.0161(5) -0.0003(4) 0.0032(4) -0.0030(4)
Al2 0.0171(5) 0.0118(5) 0.0188(5) 0.0022(4) -0.0012(4) -0.0019(4)
Al3 0.0125(5) 0.0179(5) 0.0136(5) 0.0008(4) 0.0013(4) -0.0024(4)
P1 0.0136(4) 0.0174(4) 0.0130(4) 0.0005(3) 0.0028(3) -0.0005(3)
P2 0.0174(5) 0.0202(5) 0.0293(5) 0.0099(4) -0.0041(4) -0.0064(4)
P3 0.0174(5) 0.0133(4) 0.0177(5) 0.0008(3) 0.0041(4) 0.0022(3)
P4 0.0164(5) 0.0206(5) 0.0195(5) -0.0057(4) 0.0047(4) -0.0016(4)
P5 0.0212(5) 0.0188(5) 0.0165(5) -0.0024(4) 0.0041(4) -0.0080(4)
P6 0.0212(5) 0.0212(5) 0.0178(5) 0.0034(4) 0.0039(4) -0.0025(4)
O1 0.0162(14) 0.0555(19) 0.0261(15) -0.0120(14) 0.0067(11) -0.0033(13)
O2 0.0361(16) 0.0237(14) 0.0168(13) 0.0005(11) -0.0041(11) 0.0075(12)
O3 0.0262(14) 0.0352(15) 0.0157(13) 0.0000(11) 0.0069(11) 0.0015(12)
O4 0.0428(17) 0.0193(14) 0.0348(17) -0.0019(12) 0.0036(14) -0.0067(12)
O5A 0.0238(19) 0.046(3) 0.0202(19) -0.0037(17) 0.0079(14) 0.0030(17)
O6A 0.055(3) 0.0125(19) 0.046(5) -0.0028(18) 0.020(2) 0.0010(16)
O5B 0.036(9) 0.036(9) 0.036(9) 0.0001(10) 0.0058(18) 0.0001(10)
O6B 0.032(6) 0.031(6) 0.031(6) -0.0001(10) 0.0047(14) 0.0002(10)
O7 0.0236(14) 0.0471(18) 0.0228(14) 0.0136(13) -0.0024(11) -0.0179(13)
O8 0.0342(18) 0.0292(17) 0.081(3) -0.0080(16) 0.0077(17) 0.0051(14)
O9 0.0177(13) 0.0198(13) 0.0277(14) 0.0083(11) -0.0027(11) -0.0035(10)
O10 0.0346(17) 0.0457(19) 0.0435(19) 0.0262(15) -0.0192(14) -0.0221(14)
O11 0.0307(16) 0.057(2) 0.0183(14) 0.0064(13) 0.0038(12) 0.0210(14)
O12 0.0241(15) 0.0396(17) 0.0445(18) -0.0086(14) 0.0023(13) -0.0081(13)
O13 0.059(2) 0.0262(16) 0.0447(19) -0.0129(14) 0.0248(16) -0.0158(14)
O14 0.0383(16) 0.0242(14) 0.0219(14) 0.0027(11) -0.0017(12) -0.0139(12)
O15 0.0312(17) 0.0463(19) 0.049(2) 0.0209(16) -0.0145(15) -0.0104(14)
O16 0.0355(16) 0.0331(16) 0.0290(15) -0.0123(12) 0.0117(13) -0.0197(13)
O17 0.0293(16) 0.0360(16) 0.0417(18) -0.0064(14) 0.0172(14) -0.0051(13)
O18 0.054(2) 0.0338(17) 0.0479(19) -0.0102(15) 0.0321(17) -0.0092(15)
O19 0.0290(17) 0.079(3) 0.0372(18) 0.0379(18) 0.0083(14) 0.0176(16)
O20 0.0240(14) 0.0250(14) 0.0324(16) -0.0093(12) -0.0023(12) 0.0048(11)
O21 0.043(2) 0.0253(16) 0.099(3) -0.0095(18) 0.037(2) 0.0033(14)
O22 0.0209(13) 0.0234(13) 0.0343(15) 0.0012(12) 0.0110(12) -0.0017(11)
O23 0.0274(17) 0.106(3) 0.0187(16) 0.0074(17) -0.0003(13) 0.0086(18)
O24 0.0234(14) 0.0395(16) 0.0235(14) -0.0115(12) 0.0085(11) -0.0097(12)

_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Na1 O13 2.250(3) . ?
Na1 O18 2.266(3) 4_576 ?
Na1 O8 2.401(4) 4_566 ?
Na1 O12 2.459(3) . ?
Na1 O5A 2.494(5) . ?
Na1 O7 2.648(3) 4_566 ?
Na1 P2 3.0683(18) 4_566 ?
Na2 O21 2.211(3) . ?
Na2 O23 2.260(3) 2_655 ?
Na2 O10 2.277(3) 1_565 ?
Na2 O19 2.440(3) . ?
Na2 O20 2.557(3) . ?
Na2 P2 3.2011(17) 1_565 ?
Na3 O5A 2.289(3) . ?
Na3 O15 2.323(3) 4_576 ?
Na3 O5B 2.33(3) . ?
Na3 O4 2.369(3) . ?
Na3 O3 2.416(3) 2 ?
Na3 O1 2.586(3) 2 ?
K1 O3 2.652(3) . ?
K1 O15 2.669(3) 3_565 ?
K1 O4 2.785(3) 4_565 ?
K1 O16 2.906(3) 1_545 ?
K1 O15 3.089(4) 1_545 ?
K1 O6B 3.103(18) . ?
K1 O6A 3.183(5) . ?
K1 O5B 3.25(4) . ?
K1 O11 3.404(3) . ?
K2 O17 2.508(3) 1_545 ?
K2 O5B 2.54(3) . ?
K2 O5A 2.736(4) . ?
K2 O7 2.789(3) 4_566 ?
K2 O4 2.865(3) . ?
K2 O9 2.898(3) 4_566 ?
K2 O11 2.900(3) 4_566 ?
K2 O6B 2.96(3) 4_566 ?
K2 O6A 3.088(9) . ?
K3 O12 2.702(3) . ?
K3 O13 2.786(3) . ?
K3 O21 2.814(3) . ?
K3 O18 2.825(4) . ?
K3 O24 2.870(3) . ?
K3 O14 3.088(3) . ?
K3 O17 3.096(3) 4_575 ?
K3 O11 3.288(3) . ?
K3 O19 3.422(4) . ?
K4 O8 2.660(3) 1_565 ?
K4 O23 2.714(3) 4_575 ?
K4 O20 2.899(3) 4_575 ?
K4 O10 2.941(3) 3_665 ?
K4 O22 2.971(3) . ?
K4 O21 3.089(4) . ?
K4 O13 3.152(4) 4_575 ?
K5 O18 2.740(3) 4_576 ?
K5 O3 2.750(3) 1_565 ?
K5 O17 2.769(3) . ?
K5 O14 2.780(3) . ?
K5 O2 2.904(3) 1_565 ?
K5 O16 3.133(3) . ?
K5 O13 3.377(4) . ?
K6 O12 2.523(3) . ?
K6 O10 2.634(4) . ?
K6 O8 2.711(4) 4_566 ?
K6 O23 2.763(4) . ?
K6 O24 2.890(3) . ?
K6 O9 3.165(3) 4_566 ?
Al1 O22 1.723(3) 3_665 ?
Al1 O24 1.727(3) . ?
Al1 O9 1.736(3) . ?
Al1 O20 1.740(3) 4_575 ?
Al2 O6B 1.665(18) . ?
Al2 O19 1.717(3) 1_545 ?
Al2 O16 1.730(3) 1_545 ?
Al2 O7 1.735(3) . ?
Al2 O6A 1.749(4) . ?
Al3 O2 1.729(3) 4_565 ?
Al3 O1 1.731(3) 2 ?
Al3 O14 1.735(3) . ?
Al3 O11 1.740(3) . ?
P1 O3 1.500(3) . ?
P1 O4 1.500(3) . ?
P1 O1 1.561(3) . ?
P1 O2 1.562(3) . ?
P2 O8 1.494(3) . ?
P2 O10 1.497(3) . ?
P2 O9 1.560(3) . ?
P2 O7 1.581(3) . ?
P3 O5B 1.47(3) . ?
P3 O12 1.490(3) . ?
P3 O5A 1.511(3) . ?
P3 O6A 1.534(3) . ?
P3 O11 1.557(3) . ?
P3 O6B 1.65(2) . ?
P4 O23 1.480(3) . ?
P4 O21 1.506(3) . ?
P4 O24 1.558(3) . ?
P4 O22 1.565(3) . ?
P5 O18 1.482(3) . ?
P5 O15 1.487(3) . ?
P5 O16 1.559(3) . ?
P5 O14 1.576(3) . ?
P6 O17 1.489(3) . ?
P6 O13 1.490(3) . ?
P6 O19 1.563(3) . ?
P6 O20 1.573(3) . ?
O1 Al3 1.731(3) 2_545 ?
O1 Na3 2.586(3) 2_545 ?
O2 Al3 1.729(3) 4_566 ?
O2 K5 2.904(3) 1_545 ?
O3 Na3 2.416(3) 2_545 ?
O3 K5 2.750(3) 1_545 ?
O4 K1 2.785(3) 4_566 ?
O6B K2 2.96(3) 4_565 ?
O7 Na1 2.648(3) 4_565 ?
O7 K2 2.789(3) 4_565 ?
O8 Na1 2.401(4) 4_565 ?
O8 K4 2.660(3) 1_545 ?
O8 K6 2.711(4) 4_565 ?
O9 K2 2.898(3) 4_565 ?
O9 K6 3.165(3) 4_565 ?
O10 Na2 2.277(3) 1_545 ?
O10 K4 2.941(3) 3_665 ?
O11 K2 2.900(3) 4_565 ?
O13 K4 3.152(4) 4_576 ?
O15 Na3 2.323(3) 4_575 ?
O15 K1 2.669(3) 3_565 ?
O15 K1 3.089(4) 1_565 ?
O16 Al2 1.730(3) 1_565 ?
O16 K1 2.906(3) 1_565 ?
O17 K2 2.508(3) 1_565 ?
O17 K3 3.096(3) 4_576 ?
O18 Na1 2.266(3) 4_575 ?
O18 K5 2.740(3) 4_575 ?
O19 Al2 1.717(3) 1_565 ?
O20 Al1 1.740(3) 4_576 ?
O20 K4 2.899(3) 4_576 ?
O22 Al1 1.723(3) 3_665 ?
O23 Na2 2.260(3) 2_645 ?
O23 K4 2.714(3) 4_576 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O13 Na1 O18 95.04(12) . 4_576 ?
O13 Na1 O8 100.61(13) . 4_566 ?
O18 Na1 O8 127.03(14) 4_576 4_566 ?
O13 Na1 O12 87.16(11) . . ?
O18 Na1 O12 143.76(13) 4_576 . ?
O8 Na1 O12 87.68(12) 4_566 . ?
O13 Na1 O5A 123.42(14) . . ?
O18 Na1 O5A 89.42(13) 4_576 . ?
O8 Na1 O5A 120.67(13) 4_566 . ?
O12 Na1 O5A 60.25(10) . . ?
O13 Na1 O7 149.43(13) . 4_566 ?
O18 Na1 O7 83.24(10) 4_576 4_566 ?
O8 Na1 O7 58.76(11) 4_566 4_566 ?
O12 Na1 O7 112.09(11) . 4_566 ?
O5A Na1 O7 87.13(11) . 4_566 ?
O13 Na1 P2 128.11(11) . 4_566 ?
O18 Na1 P2 110.29(10) 4_576 4_566 ?
O8 Na1 P2 28.51(8) 4_566 4_566 ?
O12 Na1 P2 96.07(9) . 4_566 ?
O5A Na1 P2 102.02(10) . 4_566 ?
O7 Na1 P2 31.01(6) 4_566 4_566 ?
O13 Na1 K4 57.03(10) . 4_576 ?
O18 Na1 K4 115.81(10) 4_576 4_576 ?
O8 Na1 K4 44.94(8) 4_566 4_576 ?
O12 Na1 K4 95.68(8) . 4_576 ?
O5A Na1 K4 154.76(10) . 4_576 ?
O7 Na1 K4 96.20(7) 4_566 4_576 ?
P2 Na1 K4 71.14(4) 4_566 4_576 ?
O13 Na1 K3 76.85(9) . 4_576 ?
O18 Na1 K3 44.30(10) 4_576 4_576 ?
O8 Na1 K3 90.96(10) 4_566 4_576 ?
O12 Na1 K3 163.42(9) . 4_576 ?
O5A Na1 K3 133.07(9) . 4_576 ?
O7 Na1 K3 80.97(7) 4_566 4_576 ?
P2 Na1 K3 90.50(4) 4_566 4_576 ?
K4 Na1 K3 72.04(3) 4_576 4_576 ?
O21 Na2 O23 119.58(15) . 2_655 ?
O21 Na2 O10 124.24(15) . 1_565 ?
O23 Na2 O10 88.11(13) 2_655 1_565 ?
O21 Na2 O19 99.40(14) . . ?
O23 Na2 O19 136.29(14) 2_655 . ?
O10 Na2 O19 85.26(12) 1_565 . ?
O21 Na2 O20 107.73(13) . . ?
O23 Na2 O20 89.99(11) 2_655 . ?
O10 Na2 O20 120.55(13) 1_565 . ?
O19 Na2 O20 57.76(10) . . ?
O21 Na2 P2 102.33(12) . 1_565 ?
O23 Na2 P2 111.40(11) 2_655 1_565 ?
O10 Na2 P2 25.21(8) 1_565 1_565 ?
O19 Na2 P2 75.36(8) . 1_565 ?
O20 Na2 P2 127.15(8) . 1_565 ?
O21 Na2 K4 109.35(10) . 3_675 ?
O23 Na2 K4 47.66(9) 2_655 3_675 ?
O10 Na2 K4 53.42(8) 1_565 3_675 ?
O19 Na2 K4 138.03(9) . 3_675 ?
O20 Na2 K4 133.84(8) . 3_675 ?
P2 Na2 K4 69.20(4) 1_565 3_675 ?
O21 Na2 K6 167.59(13) . 1_565 ?
O23 Na2 K6 69.13(11) 2_655 1_565 ?
O10 Na2 K6 44.46(10) 1_565 1_565 ?
O19 Na2 K6 76.22(10) . 1_565 ?
O20 Na2 K6 80.00(7) . 1_565 ?
P2 Na2 K6 65.42(4) 1_565 1_565 ?
K4 Na2 K6 69.13(3) 3_675 1_565 ?
O21 Na2 K6 74.04(10) . 2_655 ?
O23 Na2 K6 45.60(11) 2_655 2_655 ?
O10 Na2 K6 117.19(9) 1_565 2_655 ?
O19 Na2 K6 156.65(9) . 2_655 ?
O20 Na2 K6 102.18(7) . 2_655 ?
P2 Na2 K6 127.70(5) 1_565 2_655 ?
K4 Na2 K6 63.78(3) 3_675 2_655 ?
K6 Na2 K6 114.46(4) 1_565 2_655 ?
O21 Na2 K4 69.20(11) . 4_576 ?
O23 Na2 K4 85.48(11) 2_655 4_576 ?
O10 Na2 K4 166.48(11) 1_565 4_576 ?
O19 Na2 K4 91.17(8) . 4_576 ?
O20 Na2 K4 47.68(6) . 4_576 ?
P2 Na2 K4 163.00(5) 1_565 4_576 ?
K4 Na2 K4 127.07(4) 3_675 4_576 ?
K6 Na2 K4 122.02(4) 1_565 4_576 ?
K6 Na2 K4 65.50(3) 2_655 4_576 ?
O5A Na3 O15 106.73(16) . 4_576 ?
O5A Na3 O5B 20.2(10) . . ?
O15 Na3 O5B 125.7(11) 4_576 . ?
O5A Na3 O4 98.95(15) . . ?
O15 Na3 O4 106.99(13) 4_576 . ?
O5B Na3 O4 85.9(9) . . ?
O5A Na3 O3 140.05(12) . 2 ?
O15 Na3 O3 89.78(11) 4_576 2 ?
O5B Na3 O3 135.4(8) . 2 ?
O4 Na3 O3 110.83(11) . 2 ?
O5A Na3 O1 81.48(11) . 2 ?
O15 Na3 O1 114.31(13) 4_576 2 ?
O5B Na3 O1 80.6(7) . 2 ?
O4 Na3 O1 136.73(12) . 2 ?
O3 Na3 O1 58.61(9) 2 2 ?
O5A Na3 P1 111.77(10) . 2 ?
O15 Na3 P1 104.99(9) 4_576 2 ?
O5B Na3 P1 108.5(7) . 2 ?
O4 Na3 P1 126.13(9) . 2 ?
O3 Na3 P1 28.43(6) 2 2 ?
O1 Na3 P1 30.32(6) 2 2 ?
O5A Na3 P5 85.19(13) . 4_576 ?
O15 Na3 P5 22.03(8) 4_576 4_576 ?
O5B Na3 P5 103.7(11) . 4_576 ?
O4 Na3 P5 106.67(9) . 4_576 ?
O3 Na3 P5 109.77(8) 2 4_576 ?
O1 Na3 P5 116.42(9) 2 4_576 ?
P1 Na3 P5 118.64(5) 2 4_576 ?
O5A Na3 K1 114.26(9) . 4_566 ?
O15 Na3 K1 57.29(10) 4_576 4_566 ?
O5B Na3 K1 116.1(7) . 4_566 ?
O4 Na3 K1 49.80(8) . 4_566 ?
O3 Na3 K1 105.32(8) 2 4_566 ?
O1 Na3 K1 163.26(8) 2 4_566 ?
P1 Na3 K1 133.75(5) 2 4_566 ?
P5 Na3 K1 62.05(3) 4_576 4_566 ?
O5A Na3 K1 146.58(15) . 2 ?
O15 Na3 K1 45.90(8) 4_576 2 ?
O5B Na3 K1 165.9(10) . 2 ?
O4 Na3 K1 107.08(9) . 2 ?
O3 Na3 K1 45.66(7) 2 2 ?
O1 Na3 K1 93.11(8) 2 2 ?
P1 Na3 K1 68.72(4) 2 2 ?
P5 Na3 K1 67.67(3) 4_576 2 ?
K1 Na3 K1 70.66(4) 4_566 2 ?
O5A Na3 K5 141.19(14) . 2_545 ?
O15 Na3 K5 111.81(9) 4_576 2_545 ?
O5B Na3 K5 122.4(11) . 2_545 ?
O4 Na3 K5 74.32(8) . 2_545 ?
O3 Na3 K5 38.40(7) 2 2_545 ?
O1 Na3 K5 78.85(7) 2 2_545 ?
P1 Na3 K5 53.81(3) 2 2_545 ?
P5 Na3 K5 133.58(4) 4_576 2_545 ?
K1 Na3 K5 90.83(4) 4_566 2_545 ?
K1 Na3 K5 67.96(3) 2 2_545 ?
O3 K1 O15 77.92(9) . 3_565 ?
O3 K1 O4 173.32(9) . 4_565 ?
O15 K1 O4 96.61(9) 3_565 4_565 ?
O3 K1 O16 80.14(8) . 1_545 ?
O15 K1 O16 125.53(10) 3_565 1_545 ?
O4 K1 O16 100.31(8) 4_565 1_545 ?
O3 K1 O15 95.86(9) . 1_545 ?
O15 K1 O15 85.17(11) 3_565 1_545 ?
O4 K1 O15 79.72(8) 4_565 1_545 ?
O16 K1 O15 48.50(8) 1_545 1_545 ?
O3 K1 O6B 100.2(6) . . ?
O15 K1 O6B 176.6(4) 3_565 . ?
O4 K1 O6B 85.0(6) 4_565 . ?
O16 K1 O6B 51.2(3) 1_545 . ?
O15 K1 O6B 92.2(4) 1_545 . ?
O3 K1 O6A 87.34(15) . . ?
O15 K1 O6A 165.20(16) 3_565 . ?
O4 K1 O6A 98.19(16) 4_565 . ?
O16 K1 O6A 51.64(8) 1_545 . ?
O15 K1 O6A 97.78(10) 1_545 . ?
O6B K1 O6A 13.6(5) . . ?
O3 K1 O5B 78.1(5) . . ?
O15 K1 O5B 137.5(5) 3_565 . ?
O4 K1 O5B 108.6(5) 4_565 . ?
O16 K1 O5B 83.6(5) 1_545 . ?
O15 K1 O5B 131.8(5) 1_545 . ?
O6B K1 O5B 44.0(7) . . ?
O6A K1 O5B 35.0(5) . . ?
O3 K1 O11 120.23(8) . . ?
O15 K1 O11 144.70(9) 3_565 . ?
O4 K1 O11 66.45(8) 4_565 . ?
O16 K1 O11 88.91(7) 1_545 . ?
O15 K1 O11 119.27(8) 1_545 . ?
O6B K1 O11 38.7(4) . . ?
O6A K1 O11 44.49(10) . . ?
O5B K1 O11 42.2(5) . . ?
O3 K1 P5 86.02(6) . 1_545 ?
O15 K1 P5 104.40(8) 3_565 1_545 ?
O4 K1 P5 91.70(6) 4_565 1_545 ?
O16 K1 P5 24.69(5) 1_545 1_545 ?
O15 K1 P5 23.98(6) 1_545 1_545 ?
O6B K1 P5 72.5(3) . 1_545 ?
O6A K1 P5 75.53(7) . 1_545 ?
O5B K1 P5 108.3(5) . 1_545 ?
O11 K1 P5 106.74(5) . 1_545 ?
O3 K1 Na3 134.66(7) . 4_565 ?
O15 K1 Na3 89.35(8) 3_565 4_565 ?
O4 K1 Na3 40.51(6) 4_565 4_565 ?
O16 K1 Na3 72.46(6) 1_545 4_565 ?
O15 K1 Na3 39.27(6) 1_545 4_565 ?
O6B K1 Na3 90.0(6) . 4_565 ?
O6A K1 Na3 102.15(14) . 4_565 ?
O5B K1 Na3 131.8(5) . 4_565 ?
O11 K1 Na3 95.02(5) . 4_565 ?
P5 K1 Na3 55.06(3) 1_545 4_565 ?
O3 K1 Na3 40.67(6) . 2_545 ?
O15 K1 Na3 38.69(7) 3_565 2_545 ?
O4 K1 Na3 133.11(7) 4_565 2_545 ?
O16 K1 Na3 99.39(6) 1_545 2_545 ?
O15 K1 Na3 82.39(7) 1_545 2_545 ?
O6B K1 Na3 138.8(6) . 2_545 ?
O6A K1 Na3 127.09(14) . 2_545 ?
O5B K1 Na3 115.6(5) . 2_545 ?
O11 K1 Na3 155.61(6) . 2_545 ?
P5 K1 Na3 88.92(3) 1_545 2_545 ?
Na3 K1 Na3 109.34(4) 4_565 2_545 ?
O17 K2 O5B 116.3(9) 1_545 . ?
O17 K2 O5A 127.90(11) 1_545 . ?
O5B K2 O5A 17.2(10) . . ?
O17 K2 O7 119.42(9) 1_545 4_566 ?
O5B K2 O7 96.8(10) . 4_566 ?
O5A K2 O7 79.84(13) . 4_566 ?
O17 K2 O4 120.11(9) 1_545 . ?
O5B K2 O4 72.3(7) . . ?
O5A K2 O4 78.38(9) . . ?
O7 K2 O4 117.63(8) 4_566 . ?
O17 K2 O9 70.62(8) 1_545 4_566 ?
O5B K2 O9 107.4(8) . 4_566 ?
O5A K2 O9 98.15(10) . 4_566 ?
O7 K2 O9 50.98(7) 4_566 4_566 ?
O4 K2 O9 168.60(8) . 4_566 ?
O17 K2 O11 88.50(10) 1_545 4_566 ?
O5B K2 O11 144.3(6) . 4_566 ?
O5A K2 O11 142.06(10) . 4_566 ?
O7 K2 O11 91.73(9) 4_566 4_566 ?
O4 K2 O11 73.03(9) . 4_566 ?
O9 K2 O11 104.95(8) 4_566 4_566 ?
O17 K2 O6B 117.8(3) 1_545 4_566 ?
O5B K2 O6B 125.5(10) . 4_566 ?
O5A K2 O6B 111.2(4) . 4_566 ?
O7 K2 O6B 50.0(3) 4_566 4_566 ?
O4 K2 O6B 86.4(3) . 4_566 ?
O9 K2 O6B 84.8(3) 4_566 4_566 ?
O11 K2 O6B 43.6(3) 4_566 4_566 ?
O17 K2 O6A 78.89(10) 1_545 . ?
O5B K2 O6A 38.6(8) . . ?
O5A K2 O6A 49.27(11) . . ?
O7 K2 O6A 109.18(10) 4_566 . ?
O4 K2 O6A 98.65(10) . . ?
O9 K2 O6A 86.88(10) 4_566 . ?
O11 K2 O6A 158.89(9) 4_566 . ?
O6B K2 O6A 157.2(4) 4_566 . ?
O17 K2 P2 95.83(7) 1_545 4_566 ?
O5B K2 P2 100.8(9) . 4_566 ?
O5A K2 P2 86.45(10) . 4_566 ?
O7 K2 P2 25.58(5) 4_566 4_566 ?
O4 K2 P2 143.02(6) . 4_566 ?
O9 K2 P2 25.66(5) 4_566 4_566 ?
O11 K2 P2 101.70(6) 4_566 4_566 ?
O6B K2 P2 67.9(3) 4_566 4_566 ?
O6A K2 P2 96.41(8) . 4_566 ?
O17 K2 Al2 131.16(8) 1_545 4_566 ?
O5B K2 Al2 105.3(10) . 4_566 ?
O5A K2 Al2 88.89(11) . 4_566 ?
O7 K2 Al2 26.88(6) 4_566 4_566 ?
O4 K2 Al2 95.38(6) . 4_566 ?
O9 K2 Al2 73.60(5) 4_566 4_566 ?
O11 K2 Al2 69.84(6) 4_566 4_566 ?
O6B K2 Al2 26.3(3) 4_566 4_566 ?
O6A K2 Al2 131.00(7) . 4_566 ?
P2 K2 Al2 50.38(3) 4_566 4_566 ?
O17 K2 P6 15.44(6) 1_545 1_545 ?
O5B K2 P6 106.1(8) . 1_545 ?
O5A K2 P6 114.97(8) . 1_545 ?
O7 K2 P6 111.95(6) 4_566 1_545 ?
O4 K2 P6 130.28(6) . 1_545 ?
O9 K2 P6 61.06(5) 4_566 1_545 ?
O11 K2 P6 102.55(7) 4_566 1_545 ?
O6B K2 P6 125.1(3) 4_566 1_545 ?
O6A K2 P6 67.55(7) . 1_545 ?
P2 K2 P6 86.70(3) 4_566 1_545 ?
Al2 K2 P6 130.52(3) 4_566 1_545 ?
O12 K3 O13 72.58(9) . . ?
O12 K3 O21 107.29(10) . . ?
O13 K3 O21 76.39(11) . . ?
O12 K3 O18 136.14(9) . . ?
O13 K3 O18 115.03(10) . . ?
O21 K3 O18 116.54(10) . . ?
O12 K3 O24 74.89(9) . . ?
O13 K3 O24 103.43(9) . . ?
O21 K3 O24 51.45(8) . . ?
O18 K3 O24 135.67(9) . . ?
O12 K3 O14 91.31(8) . . ?
O13 K3 O14 85.76(9) . . ?
O21 K3 O14 148.58(8) . . ?
O18 K3 O14 49.19(8) . . ?
O24 K3 O14 159.89(8) . . ?
O12 K3 O17 100.99(9) . 4_575 ?
O13 K3 O17 171.28(9) . 4_575 ?
O21 K3 O17 111.58(10) . 4_575 ?
O18 K3 O17 65.29(8) . 4_575 ?
O24 K3 O17 80.02(8) . 4_575 ?
O14 K3 O17 88.55(7) . 4_575 ?
O12 K3 O11 47.70(8) . . ?
O13 K3 O11 98.67(8) . . ?
O21 K3 O11 153.81(9) . . ?
O18 K3 O11 89.04(8) . . ?
O24 K3 O11 106.69(8) . . ?
O14 K3 O11 53.71(7) . . ?
O17 K3 O11 72.62(7) 4_575 . ?
O12 K3 O19 117.89(8) . . ?
O13 K3 O19 45.60(8) . . ?
O21 K3 O19 68.61(8) . . ?
O18 K3 O19 78.46(8) . . ?
O24 K3 O19 118.86(8) . . ?
O14 K3 O19 80.39(7) . . ?
O17 K3 O19 139.58(8) 4_575 . ?
O11 K3 O19 125.95(7) . . ?
O12 K3 P6 115.17(7) . 4_575 ?
O13 K3 P6 166.57(7) . 4_575 ?
O21 K3 P6 90.56(8) . 4_575 ?
O18 K3 P6 67.81(6) . 4_575 ?
O24 K3 P6 69.80(6) . 4_575 ?
O14 K3 P6 104.44(6) . 4_575 ?
O17 K3 P6 22.07(5) 4_575 4_575 ?
O11 K3 P6 94.45(5) . 4_575 ?
O19 K3 P6 126.57(6) . 4_575 ?
O12 K3 Na1 164.44(7) . 4_575 ?
O13 K3 Na1 120.98(7) . 4_575 ?
O21 K3 Na1 84.61(9) . 4_575 ?
O18 K3 Na1 34.06(6) . 4_575 ?
O24 K3 Na1 106.71(6) . 4_575 ?
O14 K3 Na1 82.73(6) . 4_575 ?
O17 K3 Na1 64.64(6) 4_575 4_575 ?
O11 K3 Na1 118.72(6) . 4_575 ?
O19 K3 Na1 75.40(6) . 4_575 ?
P6 K3 Na1 53.35(3) 4_575 4_575 ?
O12 K3 K2 67.54(7) . 4_565 ?
O13 K3 K2 137.38(7) . 4_565 ?
O21 K3 K2 129.41(7) . 4_565 ?
O18 K3 K2 85.44(7) . 4_565 ?
O24 K3 K2 80.41(6) . 4_565 ?
O14 K3 K2 80.80(5) . 4_565 ?
O17 K3 K2 34.67(5) 4_575 4_565 ?
O11 K3 K2 42.01(5) . 4_565 ?
O19 K3 K2 160.52(6) . 4_565 ?
P6 K3 K2 54.43(2) 4_575 4_565 ?
Na1 K3 K2 97.23(3) 4_575 4_565 ?
O8 K4 O23 87.03(12) 1_565 4_575 ?
O8 K4 O20 118.07(9) 1_565 4_575 ?
O23 K4 O20 112.11(10) 4_575 4_575 ?
O8 K4 O10 120.79(10) 1_565 3_665 ?
O23 K4 O10 67.68(9) 4_575 3_665 ?
O20 K4 O10 120.97(9) 4_575 3_665 ?
O8 K4 O22 127.32(10) 1_565 . ?
O23 K4 O22 136.19(9) 4_575 . ?
O20 K4 O22 77.84(8) 4_575 . ?
O10 K4 O22 70.93(8) 3_665 . ?
O8 K4 O21 82.41(10) 1_565 . ?
O23 K4 O21 164.42(11) 4_575 . ?
O20 K4 O21 83.07(9) 4_575 . ?
O10 K4 O21 108.27(9) 3_665 . ?
O22 K4 O21 48.01(8) . . ?
O8 K4 O13 75.50(9) 1_565 4_575 ?
O23 K4 O13 89.70(9) 4_575 4_575 ?
O20 K4 O13 48.08(7) 4_575 4_575 ?
O10 K4 O13 149.74(9) 3_665 4_575 ?
O22 K4 O13 121.82(8) . 4_575 ?
O21 K4 O13 98.65(9) . 4_575 ?
O8 K4 P6 95.72(8) 1_565 4_575 ?
O23 K4 P6 103.39(7) 4_575 4_575 ?
O20 K4 P6 24.42(5) 4_575 4_575 ?
O10 K4 P6 140.73(8) 3_665 4_575 ?
O22 K4 P6 99.44(6) . 4_575 ?
O21 K4 P6 89.09(7) . 4_575 ?
O13 K4 P6 23.82(5) 4_575 4_575 ?
O8 K4 Na2 89.71(8) 1_565 3_675 ?
O23 K4 Na2 37.99(7) 4_575 3_675 ?
O20 K4 Na2 141.04(7) 4_575 3_675 ?
O10 K4 Na2 38.44(6) 3_665 3_675 ?
O22 K4 Na2 107.86(6) . 3_675 ?
O21 K4 Na2 130.12(8) . 3_675 ?
O13 K4 Na2 126.85(6) 4_575 3_675 ?
P6 K4 Na2 140.77(4) 4_575 3_675 ?
O8 K4 P4 94.82(9) 1_565 4_575 ?
O23 K4 P4 19.51(8) 4_575 4_575 ?
O20 K4 P4 92.69(6) 4_575 4_575 ?
O10 K4 P4 78.63(7) 3_665 4_575 ?
O22 K4 P4 136.46(6) . 4_575 ?
O21 K4 P4 173.05(7) . 4_575 ?
O13 K4 P4 74.45(6) 4_575 4_575 ?
P6 K4 P4 84.82(3) 4_575 4_575 ?
Na2 K4 P4 55.98(3) 3_675 4_575 ?
O8 K4 Na1 39.61(7) 1_565 4_575 ?
O23 K4 Na1 94.28(8) 4_575 4_575 ?
O20 K4 Na1 79.32(6) 4_575 4_575 ?
O10 K4 Na1 156.29(7) 3_665 4_575 ?
O22 K4 Na1 129.38(6) . 4_575 ?
O21 K4 Na1 84.87(7) . 4_575 ?
O13 K4 Na1 36.78(6) 4_575 4_575 ?
P6 K4 Na1 56.16(3) 4_575 4_575 ?
Na2 K4 Na1 118.16(4) 3_675 4_575 ?
P4 K4 Na1 88.94(3) 4_575 4_575 ?
O8 K4 Na2 129.32(9) 1_565 4_575 ?
O23 K4 Na2 73.59(9) 4_575 4_575 ?
O20 K4 Na2 40.71(6) 4_575 4_575 ?
O10 K4 Na2 94.67(8) 3_665 4_575 ?
O22 K4 Na2 96.42(6) . 4_575 ?
O21 K4 Na2 121.99(7) . 4_575 ?
O13 K4 Na2 58.50(6) 4_575 4_575 ?
P6 K4 Na2 47.49(3) 4_575 4_575 ?
Na2 K4 Na2 100.83(3) 3_675 4_575 ?
P4 K4 Na2 55.32(3) 4_575 4_575 ?
Na1 K4 Na2 94.68(4) 4_575 4_575 ?
O18 K5 O3 133.74(9) 4_576 1_565 ?
O18 K5 O17 71.09(10) 4_576 . ?
O3 K5 O17 100.55(9) 1_565 . ?
O18 K5 O14 125.04(9) 4_576 . ?
O3 K5 O14 100.19(9) 1_565 . ?
O17 K5 O14 114.78(9) . . ?
O18 K5 O2 82.14(8) 4_576 1_565 ?
O3 K5 O2 51.60(7) 1_565 1_565 ?
O17 K5 O2 84.90(8) . 1_565 ?
O14 K5 O2 149.62(9) . 1_565 ?
O18 K5 O16 141.81(9) 4_576 . ?
O3 K5 O16 74.70(8) 1_565 . ?
O17 K5 O16 79.70(8) . . ?
O14 K5 O16 48.51(7) . . ?
O2 K5 O16 119.78(8) 1_565 . ?
O18 K5 O13 64.99(9) 4_576 . ?
O3 K5 O13 140.77(8) 1_565 . ?
O17 K5 O13 47.32(8) . . ?
O14 K5 O13 80.48(8) . . ?
O2 K5 O13 127.66(8) 1_565 . ?
O16 K5 O13 77.20(8) . . ?
O18 K5 P1 108.82(7) 4_576 1_565 ?
O3 K5 P1 24.97(5) 1_565 1_565 ?
O17 K5 P1 91.14(7) . 1_565 ?
O14 K5 P1 124.93(7) . 1_565 ?
O2 K5 P1 26.81(5) 1_565 1_565 ?
O16 K5 P1 95.55(6) . 1_565 ?
O13 K5 P1 138.40(6) . 1_565 ?
O18 K5 P5 24.02(7) 4_576 4_576 ?
O3 K5 P5 114.89(6) 1_565 4_576 ?
O17 K5 P5 87.45(7) . 4_576 ?
O14 K5 P5 134.39(6) . 4_576 ?
O2 K5 P5 65.34(5) 1_565 4_576 ?
O16 K5 P5 165.39(6) . 4_576 ?
O13 K5 P5 89.00(6) . 4_576 ?
P1 K5 P5 91.61(3) 1_565 4_576 ?
O18 K5 K2 92.22(8) 4_576 1_565 ?
O3 K5 K2 63.88(6) 1_565 1_565 ?
O17 K5 K2 37.49(6) . 1_565 ?
O14 K5 K2 126.54(6) . 1_565 ?
O2 K5 K2 56.53(6) 1_565 1_565 ?
O16 K5 K2 78.22(5) . 1_565 ?
O13 K5 K2 84.06(5) . 1_565 ?
P1 K5 K2 54.50(2) 1_565 1_565 ?
P5 K5 K2 95.80(3) 4_576 1_565 ?
O18 K5 Na3 132.00(7) 4_576 2 ?
O3 K5 Na3 33.07(6) 1_565 2 ?
O17 K5 Na3 133.56(7) . 2 ?
O14 K5 Na3 85.57(7) . 2 ?
O2 K5 Na3 64.55(6) 1_565 2 ?
O16 K5 Na3 86.07(6) . 2 ?
O13 K5 Na3 162.82(6) . 2 ?
P1 K5 Na3 46.37(3) 1_565 2 ?
P5 K5 Na3 107.99(3) 4_576 2 ?
K2 K5 Na3 96.42(3) 1_565 2 ?
O18 K5 K1 160.27(8) 4_576 1_565 ?
O3 K5 K1 34.12(5) 1_565 1_565 ?
O17 K5 K1 94.12(7) . 1_565 ?
O14 K5 K1 72.57(6) . 1_565 ?
O2 K5 K1 83.61(5) 1_565 1_565 ?
O16 K5 K1 40.80(6) . 1_565 ?
O13 K5 K1 114.78(6) . 1_565 ?
P1 K5 K1 57.11(2) 1_565 1_565 ?
P5 K5 K1 148.68(3) 4_576 1_565 ?
K2 K5 K1 68.47(2) 1_565 1_565 ?
Na3 K5 K1 50.67(2) 2 1_565 ?
O12 K6 O10 101.30(10) . . ?
O12 K6 O8 79.96(10) . 4_566 ?
O10 K6 O8 164.30(10) . 4_566 ?
O12 K6 O23 105.25(11) . . ?
O10 K6 O23 109.39(10) . . ?
O8 K6 O23 85.06(10) 4_566 . ?
O12 K6 O24 77.23(10) . . ?
O10 K6 O24 73.93(9) . . ?
O8 K6 O24 121.25(10) 4_566 . ?
O23 K6 O24 51.33(8) . . ?
O12 K6 O9 88.21(9) . 4_566 ?
O10 K6 O9 114.86(9) . 4_566 ?
O8 K6 O9 49.45(8) 4_566 4_566 ?
O23 K6 O9 129.94(9) . 4_566 ?
O24 K6 O9 164.47(8) . 4_566 ?
O12 K6 P2 84.24(8) . 4_566 ?
O10 K6 P2 141.05(8) . 4_566 ?
O8 K6 P2 23.27(7) 4_566 4_566 ?
O23 K6 P2 106.06(7) . 4_566 ?
O24 K6 P2 143.69(7) . 4_566 ?
O9 K6 P2 26.22(5) 4_566 4_566 ?
O12 K6 Na2 116.86(8) . 1_545 ?
O10 K6 Na2 37.27(7) . 1_545 ?
O8 K6 Na2 128.31(8) 4_566 1_545 ?
O23 K6 Na2 128.78(9) . 1_545 ?
O24 K6 Na2 110.30(7) . 1_545 ?
O9 K6 Na2 80.98(6) 4_566 1_545 ?
P2 K6 Na2 105.90(4) 4_566 1_545 ?
O12 K6 P4 160.89(8) . 2_645 ?
O10 K6 P4 81.32(7) . 2_645 ?
O8 K6 P4 92.51(8) 4_566 2_645 ?
O23 K6 P4 91.43(8) . 2_645 ?
O24 K6 P4 121.29(7) . 2_645 ?
O9 K6 P4 73.74(5) 4_566 2_645 ?
P2 K6 P4 82.18(3) 4_566 2_645 ?
Na2 K6 P4 55.07(3) 1_545 2_645 ?
O12 K6 Al1 111.93(8) . 4_566 ?
O10 K6 Al1 96.28(7) . 4_566 ?
O8 K6 Al1 69.10(7) 4_566 4_566 ?
O23 K6 Al1 129.08(8) . 4_566 ?
O24 K6 Al1 168.10(7) . 4_566 ?
O9 K6 Al1 27.10(5) 4_566 4_566 ?
P2 K6 Al1 47.48(3) 4_566 4_566 ?
Na2 K6 Al1 59.24(3) 1_545 4_566 ?
P4 K6 Al1 49.07(3) 2_645 4_566 ?
O12 K6 Na2 139.81(8) . 2_645 ?
O10 K6 Na2 102.42(8) . 2_645 ?
O8 K6 Na2 85.61(8) 4_566 2_645 ?
O23 K6 Na2 35.76(7) . 2_645 ?
O24 K6 Na2 78.79(6) . 2_645 ?
O9 K6 Na2 110.15(6) 4_566 2_645 ?
P2 K6 Na2 96.86(4) 4_566 2_645 ?
Na2 K6 Na2 101.54(4) 1_545 2_645 ?
P4 K6 Na2 55.73(3) 2_645 2_645 ?
Al1 K6 Na2 97.16(4) 4_566 2_645 ?
O12 K6 K4 89.73(8) . 4_576 ?
O10 K6 K4 152.64(8) . 4_576 ?
O8 K6 K4 42.06(7) 4_566 4_576 ?
O23 K6 K4 43.26(7) . 4_576 ?
O24 K6 K4 84.42(6) . 4_576 ?
O9 K6 K4 90.20(5) 4_566 4_576 ?
P2 K6 K4 64.35(3) 4_566 4_576 ?
Na2 K6 K4 151.45(5) 1_545 4_576 ?
P4 K6 K4 96.41(3) 2_645 4_576 ?
Al1 K6 K4 102.73(4) 4_566 4_576 ?
Na2 K6 K4 56.12(3) 2_645 4_576 ?
O22 Al1 O24 110.22(14) 3_665 . ?
O22 Al1 O9 107.29(13) 3_665 . ?
O24 Al1 O9 111.85(14) . . ?
O22 Al1 O20 108.62(14) 3_665 4_575 ?
O24 Al1 O20 108.82(15) . 4_575 ?
O9 Al1 O20 109.98(13) . 4_575 ?
O22 Al1 K6 65.90(10) 3_665 4_565 ?
O24 Al1 K6 161.89(11) . 4_565 ?
O9 Al1 K6 56.15(9) . 4_565 ?
O20 Al1 K6 88.85(10) 4_575 4_565 ?
O6B Al2 O19 134.5(10) . 1_545 ?
O6B Al2 O16 100.0(6) . 1_545 ?
O19 Al2 O16 109.39(17) 1_545 1_545 ?
O6B Al2 O7 91.4(11) . . ?
O19 Al2 O7 106.92(15) 1_545 . ?
O16 Al2 O7 113.57(14) 1_545 . ?
O6B Al2 O6A 25.1(10) . . ?
O19 Al2 O6A 113.3(3) 1_545 . ?
O16 Al2 O6A 99.93(17) 1_545 . ?
O7 Al2 O6A 113.7(3) . . ?
O6B Al2 K2 51.8(12) . 4_565 ?
O19 Al2 K2 151.27(11) 1_545 4_565 ?
O16 Al2 K2 94.21(11) 1_545 4_565 ?
O7 Al2 K2 46.61(10) . 4_565 ?
O6A Al2 K2 77.0(3) . 4_565 ?
O2 Al3 O1 115.07(14) 4_565 2 ?
O2 Al3 O14 109.26(13) 4_565 . ?
O1 Al3 O14 106.71(15) 2 . ?
O2 Al3 O11 106.12(14) 4_565 . ?
O1 Al3 O11 107.48(14) 2 . ?
O14 Al3 O11 112.31(16) . . ?
O2 Al3 K2 62.86(10) 4_565 4_565 ?
O1 Al3 K2 134.74(12) 2 4_565 ?
O14 Al3 K2 116.59(11) . 4_565 ?
O11 Al3 K2 44.47(9) . 4_565 ?
O3 P1 O4 116.57(16) . . ?
O3 P1 O1 106.53(15) . . ?
O4 P1 O1 111.69(17) . . ?
O3 P1 O2 107.22(15) . . ?
O4 P1 O2 109.82(16) . . ?
O1 P1 O2 104.19(16) . . ?
O3 P1 Na3 50.07(11) . 2_545 ?
O4 P1 Na3 138.19(12) . 2_545 ?
O1 P1 Na3 56.79(11) . 2_545 ?
O2 P1 Na3 111.98(11) . 2_545 ?
O3 P1 K5 50.73(11) . 1_545 ?
O4 P1 K5 125.41(12) . 1_545 ?
O1 P1 K5 122.87(12) . 1_545 ?
O2 P1 K5 57.00(10) . 1_545 ?
Na3 P1 K5 79.82(4) 2_545 1_545 ?
O8 P2 O10 115.4(2) . . ?
O8 P2 O9 109.31(18) . . ?
O10 P2 O9 109.85(16) . . ?
O8 P2 O7 107.90(18) . . ?
O10 P2 O7 111.14(17) . . ?
O9 P2 O7 102.48(15) . . ?
O8 P2 Na1 50.10(13) . 4_565 ?
O10 P2 Na1 144.26(13) . 4_565 ?
O9 P2 Na1 105.89(11) . 4_565 ?
O7 P2 Na1 59.66(12) . 4_565 ?
O8 P2 Na2 90.29(15) . 1_545 ?
O10 P2 Na2 40.38(12) . 1_545 ?
O9 P2 Na2 150.22(11) . 1_545 ?
O7 P2 Na2 91.94(11) . 1_545 ?
Na1 P2 Na2 103.89(5) 4_565 1_545 ?
O8 P2 K6 45.79(14) . 4_565 ?
O10 P2 K6 128.63(14) . 4_565 ?
O9 P2 K6 63.64(11) . 4_565 ?
O7 P2 K6 120.10(11) . 4_565 ?
Na1 P2 K6 68.85(4) 4_565 4_565 ?
Na2 P2 K6 129.95(5) 1_545 4_565 ?
O8 P2 K2 113.75(14) . 4_565 ?
O10 P2 K2 130.85(16) . 4_565 ?
O9 P2 K2 53.53(10) . 4_565 ?
O7 P2 K2 49.61(11) . 4_565 ?
Na1 P2 K2 72.47(4) 4_565 4_565 ?
Na2 P2 K2 138.50(4) 1_545 4_565 ?
K6 P2 K2 88.38(3) 4_565 4_565 ?
O5B P3 O12 138.6(16) . . ?
O5B P3 O5A 31.5(16) . . ?
O12 P3 O5A 111.9(2) . . ?
O5B P3 O6A 79.9(16) . . ?
O12 P3 O6A 110.8(2) . . ?
O5A P3 O6A 107.0(3) . . ?
O5B P3 O11 104.7(12) . . ?
O12 P3 O11 109.01(18) . . ?
O5A P3 O11 109.96(16) . . ?
O6A P3 O11 108.1(3) . . ?
O5B P3 O6B 99(2) . . ?
O12 P3 O6B 106.7(7) . . ?
O5A P3 O6B 130.0(11) . . ?
O6A P3 O6B 26.8(9) . . ?
O11 P3 O6B 85.4(10) . . ?
O5B P3 K2 128.0(17) . 4_565 ?
O12 P3 K2 93.20(13) . 4_565 ?
O5A P3 K2 151.03(15) . 4_565 ?
O6A P3 K2 75.3(3) . 4_565 ?
O11 P3 K2 45.18(11) . 4_565 ?
O6B P3 K2 48.5(12) . 4_565 ?
O23 P4 O21 116.9(2) . . ?
O23 P4 O24 107.55(19) . . ?
O21 P4 O24 107.30(19) . . ?
O23 P4 O22 111.77(17) . . ?
O21 P4 O22 106.96(17) . . ?
O24 P4 O22 105.73(15) . . ?
O23 P4 K4 37.77(15) . 4_576 ?
O21 P4 K4 79.39(16) . 4_576 ?
O24 P4 K4 118.02(10) . 4_576 ?
O22 P4 K4 131.80(11) . 4_576 ?
O23 P4 K6 71.68(15) . 2_655 ?
O21 P4 K6 81.40(15) . 2_655 ?
O24 P4 K6 169.96(11) . 2_655 ?
O22 P4 K6 66.20(11) . 2_655 ?
K4 P4 K6 67.82(3) 4_576 2_655 ?
O18 P5 O15 116.6(2) . . ?
O18 P5 O16 109.79(17) . . ?
O15 P5 O16 108.21(19) . . ?
O18 P5 O14 107.90(18) . . ?
O15 P5 O14 110.69(17) . . ?
O16 P5 O14 102.83(15) . . ?
O18 P5 Na3 89.19(15) . 4_575 ?
O15 P5 Na3 35.89(12) . 4_575 ?
O16 P5 Na3 99.05(12) . 4_575 ?
O14 P5 Na3 145.34(11) . 4_575 ?
O18 P5 K5 48.80(13) . 4_575 ?
O15 P5 K5 77.71(15) . 4_575 ?
O16 P5 K5 154.87(11) . 4_575 ?
O14 P5 K5 97.41(11) . 4_575 ?
Na3 P5 K5 71.05(3) 4_575 4_575 ?
O18 P5 K1 137.88(13) . 1_565 ?
O15 P5 K1 57.59(15) . 1_565 ?
O16 P5 K1 51.11(12) . 1_565 ?
O14 P5 K1 112.81(12) . 1_565 ?
Na3 P5 K1 62.89(3) 4_575 1_565 ?
K5 P5 K1 132.13(4) 4_575 1_565 ?
O17 P6 O13 116.17(17) . . ?
O17 P6 O19 111.28(18) . . ?
O13 P6 O19 108.4(2) . . ?
O17 P6 O20 111.22(16) . . ?
O13 P6 O20 107.87(18) . . ?
O19 P6 O20 100.78(17) . . ?
O17 P6 K4 126.31(13) . 4_576 ?
O13 P6 K4 58.71(14) . 4_576 ?
O19 P6 K4 120.98(12) . 4_576 ?
O20 P6 K4 49.67(10) . 4_576 ?
O17 P6 K2 26.63(12) . 1_565 ?
O13 P6 K2 141.44(13) . 1_565 ?
O19 P6 K2 90.22(14) . 1_565 ?
O20 P6 K2 101.06(10) . 1_565 ?
K4 P6 K2 138.06(3) 4_576 1_565 ?
O17 P6 K3 51.38(13) . 4_576 ?
O13 P6 K3 90.25(13) . 4_576 ?
O19 P6 K3 159.88(15) . 4_576 ?
O20 P6 K3 79.93(11) . 4_576 ?
K4 P6 K3 74.95(3) 4_576 4_576 ?
K2 P6 K3 70.05(3) 1_565 4_576 ?
P1 O1 Al3 140.89(18) . 2_545 ?
P1 O1 Na3 92.89(12) . 2_545 ?
Al3 O1 Na3 126.19(14) 2_545 2_545 ?
P1 O2 Al3 140.02(17) . 4_566 ?
P1 O2 K5 96.19(12) . 1_545 ?
Al3 O2 K5 119.26(13) 4_566 1_545 ?
P1 O3 Na3 101.50(13) . 2_545 ?
P1 O3 K1 135.24(16) . . ?
Na3 O3 K1 93.67(9) 2_545 . ?
P1 O3 K5 104.29(13) . 1_545 ?
Na3 O3 K5 108.53(11) 2_545 1_545 ?
K1 O3 K5 110.30(9) . 1_545 ?
P1 O4 Na3 138.15(18) . . ?
P1 O4 K1 128.92(16) . 4_566 ?
Na3 O4 K1 89.69(9) . 4_566 ?
P1 O4 K2 100.83(14) . . ?
Na3 O4 K2 86.88(10) . . ?
K1 O4 K2 97.87(9) 4_566 . ?
P3 O5A Na3 140.4(2) . . ?
P3 O5A Na1 92.83(19) . . ?
Na3 O5A Na1 120.7(2) . . ?
P3 O5A K2 105.5(2) . . ?
Na3 O5A K2 91.63(13) . . ?
Na1 O5A K2 97.13(12) . . ?
P3 O6A Al2 147.9(4) . . ?
P3 O6A K2 90.5(3) . . ?
Al2 O6A K2 114.5(3) . . ?
P3 O6A K1 99.1(2) . . ?
Al2 O6A K1 96.4(2) . . ?
K2 O6A K1 99.45(16) . . ?
P3 O5B Na3 140(2) . . ?
P3 O5B K2 116.3(15) . . ?
Na3 O5B K2 95.7(10) . . ?
P3 O5B K1 97.9(18) . . ?
Na3 O5B K1 91.9(11) . . ?
K2 O5B K1 110.9(14) . . ?
P3 O6B Al2 144.5(18) . . ?
P3 O6B K2 106.8(12) . 4_565 ?
Al2 O6B K2 101.9(13) . 4_565 ?
P3 O6B K1 99.5(8) . . ?
Al2 O6B K1 101.3(8) . . ?
K2 O6B K1 89.3(7) 4_565 . ?
P2 O7 Al2 136.01(17) . . ?
P2 O7 Na1 89.33(14) . 4_565 ?
Al2 O7 Na1 119.13(14) . 4_565 ?
P2 O7 K2 104.81(13) . 4_565 ?
Al2 O7 K2 106.51(14) . 4_565 ?
Na1 O7 K2 92.36(9) 4_565 4_565 ?
P2 O8 Na1 101.39(16) . 4_565 ?
P2 O8 K4 147.7(2) . 1_545 ?
Na1 O8 K4 95.44(11) 4_565 1_545 ?
P2 O8 K6 110.94(17) . 4_565 ?
Na1 O8 K6 94.21(13) 4_565 4_565 ?
K4 O8 K6 94.88(12) 1_545 4_565 ?
P2 O9 Al1 127.29(16) . . ?
P2 O9 K2 100.82(12) . 4_565 ?
Al1 O9 K2 125.32(12) . 4_565 ?
P2 O9 K6 90.15(12) . 4_565 ?
Al1 O9 K6 96.75(11) . 4_565 ?
K2 O9 K6 108.71(8) 4_565 4_565 ?
P2 O10 Na2 114.41(17) . 1_545 ?
P2 O10 K6 129.4(2) . . ?
Na2 O10 K6 98.27(12) 1_545 . ?
P2 O10 K4 120.23(19) . 3_665 ?
Na2 O10 K4 88.15(11) 1_545 3_665 ?
K6 O10 K4 97.25(9) . 3_665 ?
P3 O11 Al3 136.84(19) . . ?
P3 O11 K2 112.44(14) . 4_565 ?
Al3 O11 K2 110.67(12) . 4_565 ?
P3 O11 K3 87.32(13) . . ?
Al3 O11 K3 91.84(13) . . ?
K2 O11 K3 88.64(8) 4_565 . ?
P3 O11 K1 90.11(14) . . ?
Al3 O11 K1 95.72(12) . . ?
K2 O11 K1 84.64(8) 4_565 . ?
K3 O11 K1 171.28(10) . . ?
P3 O12 Na1 94.77(15) . . ?
P3 O12 K6 134.85(18) . . ?
Na1 O12 K6 97.68(11) . . ?
P3 O12 K3 113.69(16) . . ?
Na1 O12 K3 97.29(11) . . ?
K6 O12 K3 107.49(11) . . ?
P6 O13 Na1 136.70(19) . . ?
P6 O13 K3 117.61(18) . . ?
Na1 O13 K3 100.15(11) . . ?
P6 O13 K4 97.47(16) . 4_576 ?
Na1 O13 K4 86.18(12) . 4_576 ?
K3 O13 K4 112.26(10) . 4_576 ?
P6 O13 K5 79.09(14) . . ?
Na1 O13 K5 78.19(10) . . ?
K3 O13 K5 93.48(10) . . ?
K4 O13 K5 151.95(11) 4_576 . ?
P5 O14 Al3 135.96(18) . . ?
P5 O14 K5 110.36(13) . . ?
Al3 O14 K5 110.63(12) . . ?
P5 O14 K3 89.04(12) . . ?
Al3 O14 K3 98.92(12) . . ?
K5 O14 K3 100.24(8) . . ?
P5 O15 Na3 122.08(18) . 4_575 ?
P5 O15 K1 141.30(18) . 3_565 ?
Na3 O15 K1 95.40(11) 4_575 3_565 ?
P5 O15 K1 98.43(16) . 1_565 ?
Na3 O15 K1 83.44(11) 4_575 1_565 ?
K1 O15 K1 94.83(11) 3_565 1_565 ?
P5 O16 Al2 136.18(18) . 1_565 ?
P5 O16 K1 104.20(14) . 1_565 ?
Al2 O16 K1 107.35(13) 1_565 1_565 ?
P5 O16 K5 95.93(12) . . ?
Al2 O16 K5 110.94(13) 1_565 . ?
K1 O16 K5 94.40(8) 1_565 . ?
P6 O17 K2 137.93(17) . 1_565 ?
P6 O17 K5 102.87(14) . . ?
K2 O17 K5 100.28(10) 1_565 . ?
P6 O17 K3 106.55(15) . 4_576 ?
K2 O17 K3 100.72(10) 1_565 4_576 ?
K5 O17 K3 104.87(9) . 4_576 ?
P5 O18 Na1 139.43(19) . 4_575 ?
P5 O18 K5 107.19(17) . 4_575 ?
Na1 O18 K5 93.31(11) 4_575 4_575 ?
P5 O18 K3 101.56(17) . . ?
Na1 O18 K3 101.64(13) 4_575 . ?
K5 O18 K3 113.47(11) 4_575 . ?
P6 O19 Al2 138.7(2) . 1_565 ?
P6 O19 Na2 97.30(14) . . ?
Al2 O19 Na2 123.65(15) 1_565 . ?
P6 O19 K3 88.29(16) . . ?
Al2 O19 K3 99.34(16) 1_565 . ?
Na2 O19 K3 85.35(11) . . ?
P6 O20 Al1 129.91(17) . 4_576 ?
P6 O20 Na2 92.52(13) . . ?
Al1 O20 Na2 118.15(14) 4_576 . ?
P6 O20 K4 105.90(13) . 4_576 ?
Al1 O20 K4 111.26(12) 4_576 4_576 ?
Na2 O20 K4 91.61(9) . 4_576 ?
P4 O21 Na2 145.3(3) . . ?
P4 O21 K3 99.79(15) . . ?
Na2 O21 K3 106.33(12) . . ?
P4 O21 K4 94.12(16) . . ?
Na2 O21 K4 103.02(13) . . ?
K3 O21 K4 100.37(13) . . ?
P4 O22 Al1 145.58(19) . 3_665 ?
P4 O22 K4 97.44(12) . . ?
Al1 O22 K4 116.26(12) 3_665 . ?
P4 O23 Na2 135.04(19) . 2_645 ?
P4 O23 K4 122.7(2) . 4_576 ?
Na2 O23 K4 94.36(11) 2_645 4_576 ?
P4 O23 K6 103.62(17) . . ?
Na2 O23 K6 98.64(15) 2_645 . ?
K4 O23 K6 92.50(10) 4_576 . ?
P4 O24 Al1 133.15(17) . . ?
P4 O24 K3 96.19(13) . . ?
Al1 O24 K3 109.95(13) . . ?
P4 O24 K6 96.16(13) . . ?
Al1 O24 K6 119.00(14) . . ?
K3 O24 K6 94.08(8) . . ?

_diffrn_measured_fraction_theta_max 1.000
_diffrn_reflns_theta_full        24.99
_diffrn_measured_fraction_theta_full 1.000
_refine_diff_density_max         0.817
_refine_diff_density_min         -1.495
_refine_diff_density_rms         0.104
_database_code_depnum_ccdc_archive 'CCDC 969011'