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data_zhmj0718
_audit_creation_method SHELXL-2013
_chemical_name_systematic
;
?
;
_chemical_name_common ?
_chemical_melting_point ?
_chemical_formula_moiety ?
_chemical_formula_sum 'C35 H32 N2 O2 S'
_chemical_formula_weight 544.68
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_space_group_crystal_system monoclinic
_space_group_IT_number 14
_space_group_name_H-M_alt 'P 21/c'
_space_group_name_Hall '-P 2ybc'
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
_cell_length_a 10.1191(6)
_cell_length_b 9.9999(7)
_cell_length_c 30.7760(14)
_cell_angle_alpha 90
_cell_angle_beta 96.077(5)
_cell_angle_gamma 90
_cell_volume 3096.7(3)
_cell_formula_units_Z 4
_cell_measurement_temperature 293(2)
_cell_measurement_reflns_used ?
_cell_measurement_theta_min ?
_cell_measurement_theta_max ?
_exptl_crystal_description ?
_exptl_crystal_colour ?
_exptl_crystal_density_meas ?
_exptl_crystal_density_method ?
_exptl_crystal_density_diffrn 1.168
_exptl_crystal_F_000 1152
_exptl_transmission_factor_min ?
_exptl_transmission_factor_max ?
_exptl_crystal_size_max ?
_exptl_crystal_size_mid ?
_exptl_crystal_size_min ?
_exptl_absorpt_coefficient_mu 0.137
_shelx_estimated_absorpt_T_min ?
_shelx_estimated_absorpt_T_max ?
_exptl_absorpt_correction_type ?
_exptl_absorpt_correction_T_min ?
_exptl_absorpt_correction_T_max ?
_exptl_absorpt_process_details ?
_exptl_special_details
;
?
;
_diffrn_ambient_temperature 293(2)
_diffrn_radiation_wavelength 0.71073
_diffrn_radiation_type MoK\a
_diffrn_source ?
_diffrn_measurement_device_type ?
_diffrn_measurement_method ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number 14276
_diffrn_reflns_av_unetI/netI 0.1150
_diffrn_reflns_av_R_equivalents 0.0635
_diffrn_reflns_limit_h_min -10
_diffrn_reflns_limit_h_max 12
_diffrn_reflns_limit_k_min -6
_diffrn_reflns_limit_k_max 12
_diffrn_reflns_limit_l_min -37
_diffrn_reflns_limit_l_max 37
_diffrn_reflns_theta_min 2.996
_diffrn_reflns_theta_max 26.022
_diffrn_reflns_theta_full 25.242
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measured_fraction_theta_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_point_group_measured_fraction_full 0.998
_reflns_number_total 6095
_reflns_number_gt 2503
_reflns_threshold_expression 'I > 2\s(I)'
_reflns_Friedel_coverage 0.000
_reflns_Friedel_fraction_max .
_reflns_Friedel_fraction_full .
_reflns_special_details
;
Reflections were merged by SHELXL according to the crystal
class for the calculation of statistics and refinement.
_reflns_Friedel_fraction is defined as the number of unique
Friedel pairs measured divided by the number that would be
possible theoretically, ignoring centric projections and
systematic absences.
;
_computing_data_collection ?
_computing_cell_refinement ?
_computing_data_reduction ?
_computing_structure_solution ?
_computing_structure_refinement 'SHELXL-2013 (Sheldrick, 2013)'
_computing_molecular_graphics ?
_computing_publication_material ?
_refine_special_details
;
?
;
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type full
_refine_ls_weighting_scheme calc
_refine_ls_weighting_details
;
w=1/[\s^2^(Fo^2^)+(0.1880P)^2^]
where P=(Fo^2^+2Fc^2^)/3
;
_atom_sites_solution_primary ?
_atom_sites_solution_secondary ?
_atom_sites_solution_hydrogens geom
_refine_ls_hydrogen_treatment constr
_refine_ls_extinction_method none
_refine_ls_extinction_coef .
_refine_ls_number_reflns 6095
_refine_ls_number_parameters 363
_refine_ls_number_restraints 96
_refine_ls_R_factor_all 0.1936
_refine_ls_R_factor_gt 0.1021
_refine_ls_wR_factor_ref 0.3641
_refine_ls_wR_factor_gt 0.2845
_refine_ls_goodness_of_fit_ref 0.984
_refine_ls_restrained_S_all 1.000
_refine_ls_shift/su_max 0.000
_refine_ls_shift/su_mean 0.000
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
S1 S 0.53908(17) -0.02997(15) 0.40691(5) 0.0742(6) Uani 1 1 d . . . . .
O1 O 0.6064(4) -0.0599(4) 0.44873(12) 0.0880(13) Uani 1 1 d . . . . .
O2 O 0.5968(5) -0.0661(5) 0.36809(13) 0.0996(15) Uani 1 1 d . . . . .
N1 N 0.5176(4) 0.1291(4) 0.40559(12) 0.0582(11) Uani 1 1 d . . . . .
C1 C 0.4492(5) 0.1919(5) 0.36578(14) 0.0552(12) Uani 1 1 d . . . . .
H1A H 0.3960 0.1270 0.3482 0.066 Uiso 1 1 calc R U . . .
H1B H 0.5125 0.2322 0.3481 0.066 Uiso 1 1 calc R U . . .
C2 C 0.3634(4) 0.2957(5) 0.38353(14) 0.0490(11) Uani 1 1 d . . . . .
C3 C 0.3834(4) 0.3014(5) 0.42772(14) 0.0521(12) Uani 1 1 d . . . . .
C4 C 0.4824(5) 0.1994(6) 0.44519(15) 0.0682(15) Uani 1 1 d . . . . .
H4A H 0.5599 0.2416 0.4607 0.082 Uiso 1 1 calc R U . . .
H4B H 0.4439 0.1381 0.4648 0.082 Uiso 1 1 calc R U . . .
C5 C 0.3180(5) 0.3866(5) 0.45622(15) 0.0590(13) Uani 1 1 d . . . . .
H5 H 0.2574 0.4490 0.4436 0.071 Uiso 1 1 calc R U . . .
C6 C 0.3386(5) 0.3820(6) 0.49969(16) 0.0684(15) Uani 1 1 d . . . . .
H6 H 0.3985 0.3184 0.5119 0.082 Uiso 1 1 calc R U . . .
C7 C 0.2755(6) 0.4682(6) 0.52994(16) 0.0662(15) Uani 1 1 d . . . . .
C8 C 0.3206(7) 0.4656(7) 0.57436(18) 0.090(2) Uani 1 1 d . . . . .
H8 H 0.3921 0.4109 0.5839 0.109 Uiso 1 1 calc R U . . .
C9 C 0.2628(8) 0.5412(10) 0.6044(2) 0.111(3) Uani 1 1 d . . . . .
H9 H 0.2918 0.5335 0.6340 0.133 Uiso 1 1 calc R U . . .
C10 C 0.1635(9) 0.6271(8) 0.5909(3) 0.109(3) Uani 1 1 d . . . . .
H10 H 0.1302 0.6852 0.6107 0.130 Uiso 1 1 calc R U . . .
C11 C 0.1111(10) 0.6278(9) 0.5467(3) 0.146(4) Uani 1 1 d . . . . .
H11 H 0.0367 0.6790 0.5375 0.176 Uiso 1 1 calc R U . . .
C12 C 0.1712(9) 0.5518(8) 0.5173(2) 0.122(3) Uani 1 1 d . . . . .
H12 H 0.1401 0.5572 0.4878 0.147 Uiso 1 1 calc R U . . .
C13 C 0.2719(4) 0.3807(5) 0.35380(13) 0.0487(11) Uani 1 1 d . . . . .
H13 H 0.2468 0.4569 0.3712 0.058 Uiso 1 1 calc R U . . .
C14 C 0.3444(5) 0.4375(5) 0.31741(16) 0.0566(13) Uani 1 1 d . . . . .
C15 C 0.4263(6) 0.5495(6) 0.3268(2) 0.0791(17) Uani 1 1 d . . . . .
H15 H 0.4344 0.5854 0.3549 0.095 Uiso 1 1 calc R U . . .
C16 C 0.4941(7) 0.6064(7) 0.2956(3) 0.108(3) Uani 1 1 d . . . . .
H16 H 0.5501 0.6787 0.3027 0.130 Uiso 1 1 calc R U . . .
C17 C 0.4795(8) 0.5573(9) 0.2538(3) 0.106(3) Uani 1 1 d . . . . .
H17 H 0.5238 0.5983 0.2324 0.127 Uiso 1 1 calc R U . . .
C18 C 0.4008(8) 0.4487(9) 0.2432(2) 0.095(2) Uani 1 1 d . . . . .
H18 H 0.3924 0.4159 0.2148 0.114 Uiso 1 1 calc R U . . .
C19 C 0.3318(5) 0.3860(6) 0.27520(16) 0.0680(15) Uani 1 1 d . . . . .
H19 H 0.2789 0.3114 0.2682 0.082 Uiso 1 1 calc R U . . .
C20 C 0.1453(5) 0.3089(5) 0.33787(14) 0.0556(12) Uani 1 1 d . . . . .
C21 C 0.1058(5) 0.1851(6) 0.35083(17) 0.0652(14) Uani 1 1 d . U . . .
H21 H 0.1565 0.1288 0.3700 0.078 Uiso 1 1 calc R U . . .
N22 N -0.0210(5) 0.1559(6) 0.33109(16) 0.0787(14) Uani 1 1 d . U . . .
C23 C -0.0629(5) 0.2650(7) 0.30538(18) 0.0716(16) Uani 1 1 d . U . . .
C24 C -0.2000(7) 0.3958(10) 0.2587(2) 0.106(2) Uani 1 1 d . U . . .
H24 H -0.2791 0.4094 0.2410 0.128 Uiso 1 1 calc R U . . .
C25 C -0.1851(6) 0.2810(9) 0.2796(2) 0.092(2) Uani 1 1 d . U . . .
H25 H -0.2507 0.2154 0.2775 0.110 Uiso 1 1 calc R U . . .
C26 C -0.1071(8) 0.4977(9) 0.2610(2) 0.099(2) Uani 1 1 d . U . . .
H26 H -0.1256 0.5772 0.2459 0.119 Uiso 1 1 calc R U . . .
C27 C 0.0120(6) 0.4803(7) 0.28561(17) 0.0754(16) Uani 1 1 d . U . . .
H27 H 0.0765 0.5468 0.2871 0.090 Uiso 1 1 calc R U . . .
C28 C 0.0352(5) 0.3607(6) 0.30859(15) 0.0596(13) Uani 1 1 d . U . . .
C29 C -0.0969(8) 0.0331(9) 0.3350(3) 0.125(3) Uani 1 1 d . U . . .
H29A H -0.1690 0.0502 0.3522 0.187 Uiso 1 1 calc R U . . .
H29B H -0.0400 -0.0345 0.3490 0.187 Uiso 1 1 calc R U . . .
H29C H -0.1317 0.0030 0.3065 0.187 Uiso 1 1 calc R U . . .
C30 C 0.3871(7) -0.1032(6) 0.40314(19) 0.0798(17) Uani 1 1 d . U . . .
C31 C 0.3228(8) -0.1215(10) 0.4399(3) 0.123(3) Uani 1 1 d . U . . .
H31 H 0.3592 -0.0892 0.4669 0.148 Uiso 1 1 calc R U . . .
C32 C 0.2022(10) -0.1893(10) 0.4359(3) 0.138(3) Uani 1 1 d . U . . .
H32 H 0.1626 -0.2102 0.4609 0.165 Uiso 1 1 calc R U . . .
C33 C 0.1390(8) -0.2269(8) 0.3950(3) 0.116(3) Uani 1 1 d . U . . .
C34 C 0.2047(9) -0.2026(8) 0.3605(3) 0.113(2) Uani 1 1 d . U . . .
H34 H 0.1665 -0.2289 0.3330 0.136 Uiso 1 1 calc R U . . .
C35 C 0.3228(8) -0.1422(7) 0.3637(3) 0.100(2) Uani 1 1 d . U . . .
H35 H 0.3629 -0.1259 0.3384 0.121 Uiso 1 1 calc R U . . .
C36 C 0.0047(11) -0.2987(11) 0.3932(4) 0.176(4) Uani 1 1 d . U . . .
H36A H -0.0462 -0.2803 0.3657 0.265 Uiso 1 1 calc R U . . .
H36B H -0.0429 -0.2675 0.4166 0.265 Uiso 1 1 calc R U . . .
H36C H 0.0191 -0.3933 0.3961 0.265 Uiso 1 1 calc R U . . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
S1 0.0947(12) 0.0654(10) 0.0615(9) 0.0108(7) 0.0040(7) 0.0201(8)
O1 0.101(3) 0.085(3) 0.074(3) 0.027(2) -0.010(2) 0.026(2)
O2 0.123(4) 0.099(4) 0.080(3) -0.002(3) 0.022(2) 0.040(3)
N1 0.066(3) 0.063(3) 0.044(2) 0.008(2) 0.0011(18) 0.010(2)
C1 0.061(3) 0.057(3) 0.047(3) -0.001(2) 0.004(2) 0.006(2)
C2 0.049(3) 0.053(3) 0.044(2) 0.009(2) -0.0035(19) -0.005(2)
C3 0.056(3) 0.053(3) 0.046(3) -0.001(2) 0.000(2) -0.006(2)
C4 0.079(4) 0.073(4) 0.049(3) 0.002(3) -0.009(2) 0.014(3)
C5 0.071(3) 0.056(3) 0.050(3) 0.001(2) 0.002(2) 0.005(3)
C6 0.083(4) 0.072(4) 0.049(3) -0.003(3) 0.001(2) 0.003(3)
C7 0.083(4) 0.072(4) 0.045(3) -0.001(3) 0.008(2) -0.003(3)
C8 0.092(4) 0.118(6) 0.058(3) -0.021(4) -0.007(3) 0.017(4)
C9 0.121(6) 0.153(8) 0.058(4) -0.028(5) 0.007(4) -0.016(6)
C10 0.145(7) 0.104(6) 0.083(5) -0.020(5) 0.037(5) -0.002(6)
C11 0.213(10) 0.132(8) 0.101(6) 0.020(6) 0.048(6) 0.082(7)
C12 0.170(8) 0.144(8) 0.053(4) -0.004(4) 0.017(4) 0.065(6)
C13 0.052(3) 0.048(3) 0.044(2) -0.002(2) -0.0014(19) 0.000(2)
C14 0.049(3) 0.060(3) 0.060(3) 0.013(3) -0.001(2) 0.010(2)
C15 0.077(4) 0.070(4) 0.088(4) 0.017(3) -0.002(3) -0.007(3)
C16 0.096(5) 0.075(5) 0.155(8) 0.043(5) 0.022(5) -0.014(4)
C17 0.084(5) 0.103(7) 0.138(7) 0.061(6) 0.042(5) 0.029(5)
C18 0.105(5) 0.114(6) 0.071(4) 0.024(4) 0.032(4) 0.051(5)
C19 0.071(3) 0.077(4) 0.058(3) 0.009(3) 0.013(2) 0.018(3)
C20 0.054(3) 0.067(3) 0.045(3) 0.001(2) 0.003(2) 0.005(3)
C21 0.059(3) 0.066(4) 0.069(3) 0.003(3) 0.004(2) -0.008(3)
N22 0.063(3) 0.083(4) 0.090(3) -0.012(3) 0.005(2) -0.016(3)
C23 0.052(3) 0.093(4) 0.070(3) -0.015(3) 0.002(2) 0.002(3)
C24 0.074(4) 0.143(7) 0.098(5) -0.019(5) -0.007(4) 0.015(5)
C25 0.068(4) 0.118(5) 0.086(4) -0.017(4) -0.006(3) 0.002(4)
C26 0.098(5) 0.117(5) 0.078(4) 0.010(4) -0.009(3) 0.035(4)
C27 0.070(4) 0.084(4) 0.069(3) 0.006(3) -0.007(3) 0.027(3)
C28 0.052(3) 0.075(4) 0.050(3) -0.005(3) 0.001(2) 0.004(3)
C29 0.095(5) 0.115(6) 0.163(7) 0.007(5) 0.011(5) -0.056(5)
C30 0.106(4) 0.066(4) 0.065(3) 0.015(3) -0.002(3) 0.006(3)
C31 0.120(5) 0.155(7) 0.092(5) 0.037(4) -0.002(4) -0.040(5)
C32 0.154(7) 0.148(7) 0.112(5) 0.036(5) 0.016(5) -0.043(6)
C33 0.117(5) 0.102(5) 0.128(6) 0.015(5) 0.007(5) -0.027(4)
C34 0.136(6) 0.086(5) 0.117(5) 0.011(4) 0.010(5) -0.012(5)
C35 0.113(5) 0.075(4) 0.112(5) -0.012(4) 0.011(4) -0.015(4)
C36 0.182(9) 0.146(8) 0.195(9) 0.038(7) -0.005(7) -0.078(8)
_geom_special_details
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
S1 O1 1.423(4) . ?
S1 O2 1.431(4) . ?
S1 N1 1.605(4) . ?
S1 C30 1.696(7) . ?
N1 C1 1.482(6) . ?
N1 C4 1.483(6) . ?
C1 C2 1.493(7) . ?
C1 H1A 0.9700 . ?
C1 H1B 0.9700 . ?
C2 C3 1.355(6) . ?
C2 C13 1.496(6) . ?
C3 C5 1.434(6) . ?
C3 C4 1.489(7) . ?
C4 H4A 0.9700 . ?
C4 H4B 0.9700 . ?
C5 C6 1.333(6) . ?
C5 H5 0.9300 . ?
C6 C7 1.464(7) . ?
C6 H6 0.9300 . ?
C7 C12 1.370(9) . ?
C7 C8 1.395(7) . ?
C8 C9 1.372(9) . ?
C8 H8 0.9300 . ?
C9 C10 1.353(10) . ?
C9 H9 0.9300 . ?
C10 C11 1.405(10) . ?
C10 H10 0.9300 . ?
C11 C12 1.372(10) . ?
C11 H11 0.9300 . ?
C12 H12 0.9300 . ?
C13 C20 1.505(7) . ?
C13 C14 1.513(6) . ?
C13 H13 0.9800 . ?
C14 C19 1.391(7) . ?
C14 C15 1.405(8) . ?
C15 C16 1.362(9) . ?
C15 H15 0.9300 . ?
C16 C17 1.371(11) . ?
C16 H16 0.9300 . ?
C17 C18 1.366(11) . ?
C17 H17 0.9300 . ?
C18 C19 1.412(8) . ?
C18 H18 0.9300 . ?
C19 H19 0.9300 . ?
C20 C21 1.373(7) . ?
C20 C28 1.452(7) . ?
C21 N22 1.391(7) . ?
C21 H21 0.9300 . ?
N22 C23 1.387(8) . ?
N22 C29 1.460(8) . ?
C23 C28 1.375(8) . ?
C23 C25 1.406(8) . ?
C24 C25 1.317(10) . ?
C24 C26 1.382(11) . ?
C24 H24 0.9300 . ?
C25 H25 0.9300 . ?
C26 C27 1.366(9) . ?
C26 H26 0.9300 . ?
C27 C28 1.396(8) . ?
C27 H27 0.9300 . ?
C29 H29A 0.9600 . ?
C29 H29B 0.9600 . ?
C29 H29C 0.9600 . ?
C30 C35 1.371(8) . ?
C30 C31 1.377(9) . ?
C31 C32 1.389(11) . ?
C31 H31 0.9300 . ?
C32 C33 1.401(11) . ?
C32 H32 0.9300 . ?
C33 C34 1.334(10) . ?
C33 C36 1.533(12) . ?
C34 C35 1.333(10) . ?
C34 H34 0.9300 . ?
C35 H35 0.9300 . ?
C36 H36A 0.9600 . ?
C36 H36B 0.9600 . ?
C36 H36C 0.9600 . ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 S1 O2 120.3(3) . . ?
O1 S1 N1 106.3(2) . . ?
O2 S1 N1 107.2(2) . . ?
O1 S1 C30 108.3(3) . . ?
O2 S1 C30 106.3(3) . . ?
N1 S1 C30 107.9(3) . . ?
C1 N1 C4 110.2(4) . . ?
C1 N1 S1 119.4(3) . . ?
C4 N1 S1 119.5(3) . . ?
N1 C1 C2 103.4(3) . . ?
N1 C1 H1A 111.1 . . ?
C2 C1 H1A 111.1 . . ?
N1 C1 H1B 111.1 . . ?
C2 C1 H1B 111.1 . . ?
H1A C1 H1B 109.1 . . ?
C3 C2 C1 111.5(4) . . ?
C3 C2 C13 127.4(4) . . ?
C1 C2 C13 121.2(4) . . ?
C2 C3 C5 127.5(5) . . ?
C2 C3 C4 110.9(4) . . ?
C5 C3 C4 121.5(4) . . ?
N1 C4 C3 103.8(4) . . ?
N1 C4 H4A 111.0 . . ?
C3 C4 H4A 111.0 . . ?
N1 C4 H4B 111.0 . . ?
C3 C4 H4B 111.0 . . ?
H4A C4 H4B 109.0 . . ?
C6 C5 C3 124.0(5) . . ?
C6 C5 H5 118.0 . . ?
C3 C5 H5 118.0 . . ?
C5 C6 C7 125.8(5) . . ?
C5 C6 H6 117.1 . . ?
C7 C6 H6 117.1 . . ?
C12 C7 C8 116.8(5) . . ?
C12 C7 C6 123.6(5) . . ?
C8 C7 C6 119.5(6) . . ?
C9 C8 C7 122.1(7) . . ?
C9 C8 H8 119.0 . . ?
C7 C8 H8 119.0 . . ?
C10 C9 C8 119.9(7) . . ?
C10 C9 H9 120.0 . . ?
C8 C9 H9 120.0 . . ?
C9 C10 C11 119.4(7) . . ?
C9 C10 H10 120.3 . . ?
C11 C10 H10 120.3 . . ?
C12 C11 C10 119.1(8) . . ?
C12 C11 H11 120.4 . . ?
C10 C11 H11 120.4 . . ?
C7 C12 C11 122.2(7) . . ?
C7 C12 H12 118.9 . . ?
C11 C12 H12 118.9 . . ?
C2 C13 C20 112.2(4) . . ?
C2 C13 C14 110.4(4) . . ?
C20 C13 C14 113.6(4) . . ?
C2 C13 H13 106.7 . . ?
C20 C13 H13 106.7 . . ?
C14 C13 H13 106.7 . . ?
C19 C14 C15 118.8(5) . . ?
C19 C14 C13 123.3(5) . . ?
C15 C14 C13 117.9(5) . . ?
C16 C15 C14 121.2(7) . . ?
C16 C15 H15 119.4 . . ?
C14 C15 H15 119.4 . . ?
C15 C16 C17 120.0(7) . . ?
C15 C16 H16 120.0 . . ?
C17 C16 H16 120.0 . . ?
C18 C17 C16 120.7(7) . . ?
C18 C17 H17 119.7 . . ?
C16 C17 H17 119.7 . . ?
C17 C18 C19 120.4(7) . . ?
C17 C18 H18 119.8 . . ?
C19 C18 H18 119.8 . . ?
C14 C19 C18 118.9(6) . . ?
C14 C19 H19 120.6 . . ?
C18 C19 H19 120.6 . . ?
C21 C20 C28 105.9(5) . . ?
C21 C20 C13 126.8(5) . . ?
C28 C20 C13 127.1(5) . . ?
C20 C21 N22 110.2(5) . . ?
C20 C21 H21 124.9 . . ?
N22 C21 H21 124.9 . . ?
C23 N22 C21 107.3(5) . . ?
C23 N22 C29 125.2(6) . . ?
C21 N22 C29 127.5(6) . . ?
C28 C23 N22 109.4(5) . . ?
C28 C23 C25 123.1(7) . . ?
N22 C23 C25 127.5(6) . . ?
C25 C24 C26 125.2(7) . . ?
C25 C24 H24 117.4 . . ?
C26 C24 H24 117.4 . . ?
C24 C25 C23 115.0(7) . . ?
C24 C25 H25 122.5 . . ?
C23 C25 H25 122.5 . . ?
C27 C26 C24 119.3(8) . . ?
C27 C26 H26 120.3 . . ?
C24 C26 H26 120.3 . . ?
C26 C27 C28 118.8(7) . . ?
C26 C27 H27 120.6 . . ?
C28 C27 H27 120.6 . . ?
C23 C28 C27 118.6(5) . . ?
C23 C28 C20 107.3(5) . . ?
C27 C28 C20 134.1(5) . . ?
N22 C29 H29A 109.5 . . ?
N22 C29 H29B 109.5 . . ?
H29A C29 H29B 109.5 . . ?
N22 C29 H29C 109.5 . . ?
H29A C29 H29C 109.5 . . ?
H29B C29 H29C 109.5 . . ?
C35 C30 C31 118.0(7) . . ?
C35 C30 S1 121.6(5) . . ?
C31 C30 S1 120.4(5) . . ?
C30 C31 C32 118.6(8) . . ?
C30 C31 H31 120.7 . . ?
C32 C31 H31 120.7 . . ?
C31 C32 C33 121.7(8) . . ?
C31 C32 H32 119.2 . . ?
C33 C32 H32 119.2 . . ?
C34 C33 C32 116.5(8) . . ?
C34 C33 C36 124.8(9) . . ?
C32 C33 C36 118.6(9) . . ?
C35 C34 C33 122.9(9) . . ?
C35 C34 H34 118.6 . . ?
C33 C34 H34 118.6 . . ?
C34 C35 C30 122.1(8) . . ?
C34 C35 H35 119.0 . . ?
C30 C35 H35 119.0 . . ?
C33 C36 H36A 109.5 . . ?
C33 C36 H36B 109.5 . . ?
H36A C36 H36B 109.5 . . ?
C33 C36 H36C 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
O1 S1 N1 C1 -179.9(3) . . . . ?
O2 S1 N1 C1 50.3(4) . . . . ?
C30 S1 N1 C1 -63.8(4) . . . . ?
O1 S1 N1 C4 -39.0(4) . . . . ?
O2 S1 N1 C4 -168.8(4) . . . . ?
C30 S1 N1 C4 77.0(4) . . . . ?
C4 N1 C1 C2 -4.3(5) . . . . ?
S1 N1 C1 C2 139.9(3) . . . . ?
N1 C1 C2 C3 3.6(5) . . . . ?
N1 C1 C2 C13 -177.7(4) . . . . ?
C1 C2 C3 C5 -178.9(5) . . . . ?
C13 C2 C3 C5 2.5(8) . . . . ?
C1 C2 C3 C4 -1.6(6) . . . . ?
C13 C2 C3 C4 179.8(5) . . . . ?
C1 N1 C4 C3 3.5(6) . . . . ?
S1 N1 C4 C3 -140.7(4) . . . . ?
C2 C3 C4 N1 -1.2(6) . . . . ?
C5 C3 C4 N1 176.3(4) . . . . ?
C2 C3 C5 C6 176.7(5) . . . . ?
C4 C3 C5 C6 -0.4(8) . . . . ?
C3 C5 C6 C7 179.1(5) . . . . ?
C5 C6 C7 C12 10.4(10) . . . . ?
C5 C6 C7 C8 -170.7(6) . . . . ?
C12 C7 C8 C9 0.9(11) . . . . ?
C6 C7 C8 C9 -178.1(6) . . . . ?
C7 C8 C9 C10 -3.7(12) . . . . ?
C8 C9 C10 C11 6.6(13) . . . . ?
C9 C10 C11 C12 -7.0(14) . . . . ?
C8 C7 C12 C11 -1.4(12) . . . . ?
C6 C7 C12 C11 177.6(8) . . . . ?
C10 C11 C12 C7 4.4(15) . . . . ?
C3 C2 C13 C20 -101.6(5) . . . . ?
C1 C2 C13 C20 79.9(5) . . . . ?
C3 C2 C13 C14 130.5(5) . . . . ?
C1 C2 C13 C14 -48.0(6) . . . . ?
C2 C13 C14 C19 101.7(5) . . . . ?
C20 C13 C14 C19 -25.4(7) . . . . ?
C2 C13 C14 C15 -79.6(6) . . . . ?
C20 C13 C14 C15 153.3(5) . . . . ?
C19 C14 C15 C16 -0.8(9) . . . . ?
C13 C14 C15 C16 -179.6(5) . . . . ?
C14 C15 C16 C17 2.2(10) . . . . ?
C15 C16 C17 C18 -2.0(11) . . . . ?
C16 C17 C18 C19 0.6(11) . . . . ?
C15 C14 C19 C18 -0.6(7) . . . . ?
C13 C14 C19 C18 178.1(5) . . . . ?
C17 C18 C19 C14 0.7(9) . . . . ?
C2 C13 C20 C21 6.0(7) . . . . ?
C14 C13 C20 C21 132.1(5) . . . . ?
C2 C13 C20 C28 -179.7(4) . . . . ?
C14 C13 C20 C28 -53.5(6) . . . . ?
C28 C20 C21 N22 0.7(6) . . . . ?
C13 C20 C21 N22 176.0(4) . . . . ?
C20 C21 N22 C23 -0.6(6) . . . . ?
C20 C21 N22 C29 177.8(6) . . . . ?
C21 N22 C23 C28 0.3(6) . . . . ?
C29 N22 C23 C28 -178.2(6) . . . . ?
C21 N22 C23 C25 -179.5(5) . . . . ?
C29 N22 C23 C25 2.0(10) . . . . ?
C26 C24 C25 C23 -0.9(11) . . . . ?
C28 C23 C25 C24 -0.5(9) . . . . ?
N22 C23 C25 C24 179.3(6) . . . . ?
C25 C24 C26 C27 1.8(11) . . . . ?
C24 C26 C27 C28 -1.4(9) . . . . ?
N22 C23 C28 C27 -179.0(4) . . . . ?
C25 C23 C28 C27 0.8(8) . . . . ?
N22 C23 C28 C20 0.2(6) . . . . ?
C25 C23 C28 C20 180.0(5) . . . . ?
C26 C27 C28 C23 0.2(8) . . . . ?
C26 C27 C28 C20 -178.7(5) . . . . ?
C21 C20 C28 C23 -0.6(5) . . . . ?
C13 C20 C28 C23 -175.8(4) . . . . ?
C21 C20 C28 C27 178.4(5) . . . . ?
C13 C20 C28 C27 3.2(9) . . . . ?
O1 S1 C30 C35 -151.9(5) . . . . ?
O2 S1 C30 C35 -21.3(6) . . . . ?
N1 S1 C30 C35 93.4(6) . . . . ?
O1 S1 C30 C31 30.1(7) . . . . ?
O2 S1 C30 C31 160.7(6) . . . . ?
N1 S1 C30 C31 -84.6(6) . . . . ?
C35 C30 C31 C32 5.9(12) . . . . ?
S1 C30 C31 C32 -176.1(7) . . . . ?
C30 C31 C32 C33 -6.6(15) . . . . ?
C31 C32 C33 C34 4.5(15) . . . . ?
C31 C32 C33 C36 -178.7(10) . . . . ?
C32 C33 C34 C35 -1.9(13) . . . . ?
C36 C33 C34 C35 -178.5(9) . . . . ?
C33 C34 C35 C30 1.6(13) . . . . ?
C31 C30 C35 C34 -3.5(11) . . . . ?
S1 C30 C35 C34 178.5(6) . . . . ?
_refine_diff_density_max 1.029
_refine_diff_density_min -0.421
_refine_diff_density_rms 0.080
_shelxl_version_number 2013-2
_shelx_res_file
;
TITL CF solution in P21/c
CELL 0.71073 10.119137 9.999902 30.775959 90 96.0768 90
ZERR 4 0.000636 0.000655 0.001438 0 0.0048 0
LATT 1
SYMM -X,0.5+Y,0.5-Z
SFAC C H N O S
UNIT 140 128 8 8 4
ISOR 0.01 0.02 C31 C33 C32 C34 C35 C30 C36
ISOR 0.01 0.02 C21 N22 C29 C23 C25 C24 C26 C27 C28
L.S. 10
PLAN 25
BOND $H
HTAB
CONF
fmap 2
ACTA
SHEL 999 0.81
REM D:/olex2_zhmj0718/zhmj0718.hkl
WGHT 0.188000
FVAR 2.69963
S1 5 0.539080 -0.029972 0.406906 11.00000 0.09472 0.06543 =
0.06148 0.01082 0.00403 0.02011
O1 4 0.606383 -0.059858 0.448734 11.00000 0.10092 0.08494 =
0.07402 0.02688 -0.01023 0.02589
O2 4 0.596764 -0.066116 0.368087 11.00000 0.12260 0.09893 =
0.07988 -0.00164 0.02239 0.04009
N1 3 0.517649 0.129105 0.405587 11.00000 0.06639 0.06295 =
0.04414 0.00800 0.00109 0.00970
C1 1 0.449161 0.191946 0.365780 11.00000 0.06128 0.05663 =
0.04727 -0.00099 0.00429 0.00638
AFIX 23
H1A 2 0.396023 0.127028 0.348226 11.00000 -1.20000
H1B 2 0.512479 0.232231 0.348147 11.00000 -1.20000
AFIX 0
C2 1 0.363436 0.295741 0.383529 11.00000 0.04877 0.05264 =
0.04366 0.00882 -0.00354 -0.00483
C3 1 0.383399 0.301413 0.427719 11.00000 0.05603 0.05255 =
0.04645 -0.00068 -0.00039 -0.00600
C4 1 0.482386 0.199448 0.445189 11.00000 0.07876 0.07341 =
0.04912 0.00188 -0.00893 0.01425
AFIX 23
H4A 2 0.559872 0.241561 0.460706 11.00000 -1.20000
H4B 2 0.443893 0.138122 0.464776 11.00000 -1.20000
AFIX 0
C5 1 0.317965 0.386646 0.456221 11.00000 0.07068 0.05559 =
0.04983 0.00119 0.00187 0.00536
AFIX 43
H5 2 0.257400 0.448985 0.443589 11.00000 -1.20000
AFIX 0
C6 1 0.338597 0.382023 0.499688 11.00000 0.08347 0.07203 =
0.04852 -0.00295 0.00077 0.00311
AFIX 43
H6 2 0.398451 0.318370 0.511892 11.00000 -1.20000
AFIX 0
C7 1 0.275481 0.468171 0.529944 11.00000 0.08254 0.07168 =
0.04480 -0.00091 0.00849 -0.00259
C8 1 0.320561 0.465594 0.574360 11.00000 0.09205 0.11836 =
0.05784 -0.02113 -0.00680 0.01672
AFIX 43
H8 2 0.392074 0.410860 0.583932 11.00000 -1.20000
AFIX 0
C9 1 0.262764 0.541230 0.604374 11.00000 0.12111 0.15332 =
0.05751 -0.02823 0.00707 -0.01596
AFIX 43
H9 2 0.291794 0.533509 0.633964 11.00000 -1.20000
AFIX 0
C10 1 0.163475 0.627078 0.590879 11.00000 0.14463 0.10373 =
0.08315 -0.02037 0.03715 -0.00157
AFIX 43
H10 2 0.130163 0.685156 0.610657 11.00000 -1.20000
AFIX 0
C11 1 0.111099 0.627753 0.546723 11.00000 0.21347 0.13165 =
0.10067 0.01994 0.04794 0.08196
AFIX 43
H11 2 0.036680 0.679049 0.537550 11.00000 -1.20000
AFIX 0
C12 1 0.171181 0.551763 0.517330 11.00000 0.17023 0.14407 =
0.05344 -0.00364 0.01717 0.06541
AFIX 43
H12 2 0.140058 0.557175 0.487847 11.00000 -1.20000
AFIX 0
C13 1 0.271934 0.380732 0.353804 11.00000 0.05220 0.04820 =
0.04418 -0.00155 -0.00135 0.00019
AFIX 13
H13 2 0.246761 0.456889 0.371201 11.00000 -1.20000
AFIX 0
C14 1 0.344418 0.437507 0.317406 11.00000 0.04916 0.05955 =
0.05955 0.01289 -0.00149 0.00986
C15 1 0.426333 0.549507 0.326825 11.00000 0.07708 0.07032 =
0.08758 0.01733 -0.00202 -0.00697
AFIX 43
H15 2 0.434443 0.585391 0.354860 11.00000 -1.20000
AFIX 0
C16 1 0.494054 0.606438 0.295632 11.00000 0.09594 0.07460 =
0.15537 0.04342 0.02189 -0.01427
AFIX 43
H16 2 0.550143 0.678660 0.302698 11.00000 -1.20000
AFIX 0
C17 1 0.479547 0.557276 0.253802 11.00000 0.08373 0.10290 =
0.13757 0.06056 0.04240 0.02882
AFIX 43
H17 2 0.523823 0.598285 0.232407 11.00000 -1.20000
AFIX 0
C18 1 0.400757 0.448724 0.243238 11.00000 0.10478 0.11404 =
0.07139 0.02418 0.03177 0.05092
AFIX 43
H18 2 0.392449 0.415921 0.214804 11.00000 -1.20000
AFIX 0
C19 1 0.331828 0.385969 0.275202 11.00000 0.07052 0.07684 =
0.05793 0.00850 0.01319 0.01802
AFIX 43
H19 2 0.278902 0.311430 0.268153 11.00000 -1.20000
AFIX 0
C20 1 0.145309 0.308899 0.337872 11.00000 0.05442 0.06709 =
0.04470 0.00082 0.00279 0.00461
C21 1 0.105822 0.185091 0.350832 11.00000 0.05949 0.06631 =
0.06902 0.00310 0.00377 -0.00802
AFIX 43
H21 2 0.156532 0.128833 0.370036 11.00000 -1.20000
AFIX 0
N22 3 -0.021006 0.155935 0.331091 11.00000 0.06266 0.08325 =
0.08965 -0.01218 0.00540 -0.01646
C23 1 -0.062923 0.264974 0.305384 11.00000 0.05177 0.09254 =
0.06959 -0.01472 0.00223 0.00159
C24 1 -0.199956 0.395805 0.258694 11.00000 0.07380 0.14337 =
0.09811 -0.01906 -0.00714 0.01475
AFIX 43
H24 2 -0.279138 0.409437 0.240994 11.00000 -1.20000
AFIX 0
C25 1 -0.185142 0.281002 0.279603 11.00000 0.06833 0.11846 =
0.08566 -0.01710 -0.00643 0.00164
AFIX 43
H25 2 -0.250652 0.215400 0.277477 11.00000 -1.20000
AFIX 0
C26 1 -0.107124 0.497651 0.260973 11.00000 0.09833 0.11707 =
0.07800 0.01048 -0.00883 0.03459
AFIX 43
H26 2 -0.125609 0.577189 0.245883 11.00000 -1.20000
AFIX 0
C27 1 0.012032 0.480277 0.285615 11.00000 0.06974 0.08384 =
0.06944 0.00567 -0.00740 0.02650
AFIX 43
H27 2 0.076534 0.546839 0.287062 11.00000 -1.20000
AFIX 0
C28 1 0.035180 0.360699 0.308592 11.00000 0.05235 0.07546 =
0.05002 -0.00498 0.00122 0.00428
C29 1 -0.096917 0.033127 0.335041 11.00000 0.09549 0.11466 =
0.16286 0.00669 0.01122 -0.05607
AFIX 137
H29A 2 -0.168951 0.050169 0.352223 11.00000 -1.50000
H29B 2 -0.039957 -0.034484 0.349006 11.00000 -1.50000
H29C 2 -0.131743 0.002969 0.306492 11.00000 -1.50000
AFIX 0
C30 1 0.387107 -0.103245 0.403137 11.00000 0.10607 0.06629 =
0.06465 0.01472 -0.00211 0.00555
C31 1 0.322762 -0.121531 0.439928 11.00000 0.11999 0.15497 =
0.09167 0.03731 -0.00152 -0.03956
AFIX 43
H31 2 0.359201 -0.089234 0.466908 11.00000 -1.20000
AFIX 0
C32 1 0.202244 -0.189263 0.435877 11.00000 0.15354 0.14770 =
0.11213 0.03563 0.01645 -0.04264
AFIX 43
H32 2 0.162559 -0.210164 0.460929 11.00000 -1.20000
AFIX 0
C33 1 0.138961 -0.226885 0.395025 11.00000 0.11747 0.10192 =
0.12796 0.01459 0.00727 -0.02664
C34 1 0.204712 -0.202566 0.360515 11.00000 0.13609 0.08575 =
0.11694 0.01097 0.01033 -0.01156
AFIX 43
H34 2 0.166498 -0.228883 0.333033 11.00000 -1.20000
AFIX 0
C35 1 0.322829 -0.142176 0.363696 11.00000 0.11321 0.07549 =
0.11235 -0.01225 0.01058 -0.01460
AFIX 43
H35 2 0.362881 -0.125946 0.338371 11.00000 -1.20000
AFIX 0
C36 1 0.004700 -0.298712 0.393180 11.00000 0.18223 0.14645 =
0.19531 0.03762 -0.00482 -0.07837
AFIX 137
H36A 2 -0.046153 -0.280333 0.365702 11.00000 -1.50000
H36B 2 -0.042942 -0.267479 0.416570 11.00000 -1.50000
H36C 2 0.019091 -0.393319 0.396113 11.00000 -1.50000
AFIX 0
HKLF 4
REM CF solution in P21/c
REM R1 = 0.1021 for 2503 Fo > 4sig(Fo) and 0.1936 for all 6095 data
REM 363 parameters refined using 96 restraints
END
WGHT 0.1880 0.0000
REM Instructions for potential hydrogen bonds
REM No hydrogen bonds found for HTAB generation
REM Highest difference peak 1.029, deepest hole -0.421, 1-sigma level 0.080
Q1 1 -0.0634 -0.0299 0.4863 11.00000 0.05 1.03
Q2 1 0.0891 -0.1800 0.4207 11.00000 0.05 0.38
Q3 1 0.5070 -0.1228 0.4406 11.00000 0.05 0.25
Q4 1 0.5104 -0.1151 0.3677 11.00000 0.05 0.24
Q5 1 0.1346 -0.1119 0.4536 11.00000 0.05 0.22
Q6 1 -0.0822 0.0306 0.3472 11.00000 0.05 0.22
Q7 1 -0.0547 -0.2195 0.4220 11.00000 0.05 0.21
Q8 1 0.3670 0.2571 0.3969 11.00000 0.05 0.20
Q9 1 0.6033 -0.0531 0.3580 11.00000 0.05 0.19
Q10 1 0.5617 0.1171 0.4080 11.00000 0.05 0.19
Q11 1 0.4307 0.0705 0.3999 11.00000 0.05 0.19
Q12 1 -0.1909 0.4415 0.2507 11.00000 0.05 0.19
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12 1 4 221.274 242.022 5
12 -1 5 207.652 161.357 5
12 1 5 574.116 400.063 5
12 -1 6 143.365 206.840 5
12 1 6 43.5867 84.0873 5
12 -1 7-313.398 280.333 5
12 1 7 183.031 233.312 5
12 -1 8 76.2649 111.604 5
12 1 8 131.079 202.326 5
12 -1 9 20.1840 127.083 5
12 1 9-134.080 213.271 5
12 -1 10 175.614 259.530 5
12 1 10 144.427 164.035 5
12 -2 -18 29.8573 171.777 4
12 -2 -17 242.215 309.116 4
12 -2 -16-58.8028 119.992 4
12 -2 -15 12.7177 31.6473 4
12 -2 -14-229.344 234.515 4
12 2 -14-6.38599 134.792 4
12 -2 -13 232.504 236.917 4
12 2 -13 129.773 259.435 4
12 -2 -12 173.697 223.514 4
12 2 -12 105.346 218.866 4
12 -2 -11-365.710 292.234 4
12 2 -11-79.6009 197.418 4
12 -2 -10 91.2196 135.448 4
12 2 -10 17.3016 96.0992 4
12 -2 -9-15.3433 59.3240 4
12 2 -9 308.043 292.256 4
12 -2 -8 74.5784 165.149 4
12 -2 -7 259.719 286.024 4
12 -2 -6-40.1717 47.5479 4
12 2 -6 91.9598 208.162 5
12 2 -5 56.9496 77.0401 5
12 -2 -5 19.5586 144.686 4
12 2 -4-327.257 257.606 5
12 -2 -4 202.095 257.633 4
12 2 -3 49.4703 141.415 5
12 -2 -3 35.6086 82.5573 4
12 2 -2 162.686 204.096 5
12 -2 -2 82.1230 128.698 4
12 -2 -1-1.06475 152.622 5
12 2 -1-280.218 251.948 5
12 -2 -1 189.917 213.955 4
12 -2 0 226.308 235.711 5
12 2 0 23.9306 164.976 5
12 -2 1 51.3257 68.7899 5
12 2 1-67.9380 177.047 5
12 -2 2 140.950 150.626 5
12 2 2-140.705 270.896 5
12 -2 3-23.8860 129.462 5
12 2 3 90.6048 152.414 5
12 -2 4 50.1631 139.576 5
12 2 4 96.9426 155.892 5
12 -2 5-25.0745 34.1810 5
12 2 5 80.8944 193.447 5
12 -2 6 190.214 293.273 5
12 2 6 140.395 101.369 5
12 -2 7 366.207 333.899 5
12 2 7 69.7065 121.911 5
12 -2 8 52.7448 107.574 5
12 2 8-31.7685 89.8767 5
12 -2 9 86.9099 191.595 5
12 2 9 417.107 340.815 5
12 -2 10 89.2751 119.756 5
12 -3 -18 124.799 231.736 4
12 -3 -17-91.1122 149.120 4
12 -3 -16-39.0784 96.8022 4
12 -3 -15 709.587 442.546 4
12 -3 -14 11.8889 131.098 4
12 -3 -13-146.474 182.930 4
12 -3 -12 383.502 325.900 4
12 3 -12 339.510 314.239 4
12 -3 -11 244.370 274.776 4
12 3 -11-328.054 280.497 4
12 -3 -10-44.0086 99.1357 4
12 3 -10 226.063 345.041 4
12 -3 -9 67.8015 90.7941 4
12 -3 -8-141.345 228.012 4
12 -3 -7 46.5500 90.6422 4
12 3 -7 170.619 207.218 5
12 -3 -6 28.4774 100.209 4
12 3 -6-24.4375 159.105 5
12 -3 -5 77.4974 75.6106 4
12 3 -5 283.915 306.367 5
12 -3 -4-168.694 188.535 4
12 3 -4 89.7859 159.814 5
12 -3 -3-56.8746 154.168 4
12 3 -3 133.868 209.440 5
12 -3 -2 24.3366 60.1136 4
12 3 -2 208.088 256.441 5
12 -3 -1-43.3913 65.2188 4
12 3 -1 62.0811 68.0200 5
12 -3 0 108.340 193.167 4
12 -3 0-83.5658 111.754 5
12 3 1-3.54340 110.024 5
12 -3 1 30.7374 90.6914 5
12 3 2 95.7483 154.731 5
12 -3 2 5.68553 88.0233 5
12 3 3-2.33579 43.2215 5
12 -3 3-69.1265 123.877 5
12 3 4-130.810 163.058 5
12 -3 4 0.29912 64.9819 5
12 3 5-455.498 346.487 5
12 -3 5 62.2445 246.513 5
12 3 6 143.180 214.828 5
12 -3 6-59.6984 119.504 5
12 3 7 254.232 300.075 5
12 -3 7-60.5105 121.774 5
12 -3 8-139.759 187.280 5
12 -3 9 13.8365 137.799 5
12 -4 -17-191.331 212.759 4
12 -4 -16 19.0267 37.8192 4
12 -4 -15 121.481 195.661 4
12 -4 -14-169.865 196.256 4
12 -4 -13-201.734 211.968 4
12 -4 -12-97.1068 145.789 4
12 -4 -11 227.723 217.012 4
12 -4 -10 155.229 201.235 4
12 -4 -9 27.3560 33.1936 4
12 -4 -8 209.595 283.600 4
12 4 -8 188.762 205.215 5
12 4 -7 268.594 262.837 5
12 4 -6-247.404 237.860 5
12 4 -5 28.4607 121.757 5
12 4 -4 345.429 305.082 5
12 4 -3 109.389 168.910 5
12 4 -2-112.657 131.609 5
12 4 -1-248.753 275.470 5
12 4 0 146.883 225.730 5
12 4 1 9.07180 33.4433 5
12 4 2 160.814 259.381 5
12 4 3 187.024 252.103 5
12 4 4 560.969 420.199 5
12 4 5-81.3028 195.886 5
12 5 -9 278.509 276.978 5
12 5 -8 34.6589 109.531 5
12 5 -7 97.7049 71.3486 5
12 5 -6-146.383 156.252 5
12 5 -5-95.3855 32.2602 5
12 5 -4 84.0289 197.046 5
12 5 -3 196.982 267.411 5
12 5 -2 66.7243 66.0761 5
12 5 -1-152.760 199.808 5
12 5 0 304.834 394.025 5
12 5 1 265.014 269.178 5
12 6 -8 81.0497 168.108 5
12 6 -7-77.1781 140.834 5
12 6 -6-131.290 184.884 5
12 6 -5-155.960 202.652 5
13 0 -7 76.7158 180.002 4
13 0 -6 272.137 300.197 4
13 0 -5-140.981 192.386 4
13 0 -4-116.001 174.381 4
13 0 -1 87.2184 31.0605 5
13 0 0-306.585 272.861 5
13 0 1 176.559 254.750 5
13 0 2-220.277 236.732 5
13 0 3 152.892 252.329 5
13 0 4 168.764 276.034 5
13 0 5 44.7417 65.4632 5
13 -1 -9 60.2107 187.309 4
13 -1 -8-74.9766 139.767 4
13 -1 -7-138.999 188.911 4
13 -1 -6 38.0401 127.212 4
13 -1 -5 33.8444 189.791 4
13 -1 -4 421.142 393.128 4
13 -1 -3 377.316 328.983 4
13 1 -2 212.665 276.183 5
13 -1 -2-168.787 205.709 4
13 1 -1 54.0496 57.4633 5
13 -1 0 146.556 212.124 5
13 1 0 254.457 248.748 5
13 -1 1 66.1611 34.8936 5
13 1 1-0.33209 83.9103 5
13 -1 2-27.8614 82.8007 5
13 1 2-226.366 241.481 5
13 -1 3 46.0691 57.7757 5
13 1 3-263.109 262.985 5
13 -1 4 66.4341 93.8951 5
13 1 4-223.016 244.808 5
13 -1 5-135.719 188.716 5
13 -2 -10-136.738 186.853 4
13 -2 -9 0.33428 31.9236 4
13 -2 -8 145.825 226.761 4
13 -2 -7 23.3806 76.4908 4
13 -2 -6 38.5200 195.080 4
13 -2 -5-29.3552 84.8193 4
13 -2 -4 47.8960 141.629 4
13 2 -3 204.594 239.676 5
13 -2 -3 234.228 272.370 4
13 2 -2-65.6173 215.413 5
13 -2 -2 286.739 303.926 4
13 2 -1 290.004 247.889 5
13 -2 -1-335.241 282.495 4
13 2 0-134.709 185.674 5
13 -2 0 110.349 143.468 4
13 2 1 20.5880 126.918 5
13 -2 1 176.216 177.406 4
13 -2 2 132.281 205.253 5
13 2 2 298.197 330.533 5
13 -2 3 189.536 273.183 5
13 2 3-0.35555 53.6965 5
13 -2 4 76.6806 267.190 5
13 -2 5 102.697 132.955 5
13 -3 -11 13.9853 125.411 4
13 -3 -10 6.79520 26.7367 4
13 -3 -9 71.7015 73.0252 4
13 -3 -8 18.4547 70.6502 4
13 -3 -7-0.31553 247.611 4
13 -3 -6 161.453 239.397 4
13 -3 -5-35.5218 91.6063 4
13 3 -4 142.779 186.627 5
13 3 -3 99.6174 219.925 5
13 3 -2-42.3662 104.421 5
13 3 -1-309.064 284.403 5
13 3 0 305.615 235.639 5
13 4 -3 143.925 229.735 5
0 0 0 0.00 0.00 0
TITL zhmj0718 in P2(1)/c
REM P2(1)/c (#14 in standard setting)
CELL 0.71073 10.119137 9.999902 30.775959 90.0000 96.0768 90.0000
ZERR 14.00 0.000636 0.000655 0.001438 0.0000 0.0048 0.0000
LATT 1
SYMM -x, y+1/2,-z+1/2
SFAC C H N O
UNIT 154.00 140.00 14.00 14.00
TREF
HKLF 4
END
;
_shelx_hkl_checksum 90033
_database_code_depnum_ccdc_archive 'CCDC 969442'
#######################################################################
#
# Cambridge Crystallographic Data Centre
# CCDC
#
#######################################################################
#
# This CIF contains data from an original supplementary publication
# deposited with the CCDC, and may include chemical, crystal,
# experimental, refinement, atomic coordinates,
# anisotropic displacement parameters and molecular geometry data,
# as required by the journal to which it was submitted.
#
# This CIF is provided on the understanding that it is used for bona
# fide research purposes only. It may contain copyright material
# of the CCDC or of third parties, and may not be copied or further
# disseminated in any form, whether machine-readable or not,
# except for the purpose of generating routine backup copies
# on your local computer system.
#
# For further information on the CCDC, data deposition and
# data retrieval see:
# www.ccdc.cam.ac.uk
#
# Bona fide researchers may freely download Mercury and enCIFer
# from this site to visualise CIF-encoded structures and
# to carry out CIF format checking respectively.
#
data_zhmj0718
_audit_creation_date 2013-07-19
_audit_creation_method
;
Olex2 1.2
(compiled Apr 23 2013 17:54:37, GUI svn.r4466)
;
_chemical_name_common ?
_chemical_name_systematic
;
?
;
_chemical_formula_moiety 'C35 H32 N2 O2 S'
_chemical_formula_sum 'C35 H32 N2 O2 S'
_chemical_formula_weight 544.68
_chemical_melting_point ?
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
_space_group_crystal_system monoclinic
_space_group_IT_number 14
_space_group_name_H-M_alt 'P 1 21/c 1'
_space_group_name_Hall '-P 2ybc'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
_cell_length_a 10.1191(6)
_cell_length_b 9.9999(7)
_cell_length_c 30.7760(14)
_cell_angle_alpha 90
_cell_angle_beta 96.077(5)
_cell_angle_gamma 90
_cell_volume 3096.7(3)
_cell_formula_units_Z 4
_cell_measurement_reflns_used 2449
_cell_measurement_temperature 295(2)
_cell_measurement_theta_max 20.6170
_cell_measurement_theta_min 3.2430
_exptl_absorpt_coefficient_mu 0.137
_exptl_absorpt_correction_T_max 1.00000
_exptl_absorpt_correction_T_min 0.97912
_exptl_absorpt_correction_type multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb 1 2013,16:14:44)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour 'clear light colourless'
_exptl_crystal_density_diffrn 1.168
_exptl_crystal_density_meas ?
_exptl_crystal_density_method ?
_exptl_crystal_description block
_exptl_crystal_F_000 1152
_exptl_crystal_size_max 0.24
_exptl_crystal_size_mid 0.22
_exptl_crystal_size_min 0.08
_exptl_special_details
;
?
;
_exptl_transmission_factor_max ?
_exptl_transmission_factor_min ?
_diffrn_reflns_av_R_equivalents 0.0635
_diffrn_reflns_av_unetI/netI 0.1150
_diffrn_reflns_Laue_measured_fraction_full 0.998
_diffrn_reflns_Laue_measured_fraction_max 0.998
_diffrn_reflns_limit_h_max 12
_diffrn_reflns_limit_h_min -10
_diffrn_reflns_limit_k_max 12
_diffrn_reflns_limit_k_min -6
_diffrn_reflns_limit_l_max 37
_diffrn_reflns_limit_l_min -37
_diffrn_reflns_number 14276
_diffrn_reflns_point_group_measured_fraction_full 0.998
_diffrn_reflns_point_group_measured_fraction_max 0.998
_diffrn_reflns_theta_full 25.242
_diffrn_reflns_theta_max 26.022
_diffrn_reflns_theta_min 2.996
_diffrn_ambient_temperature 295(2)
_diffrn_detector_area_resol_mean 16.0733
_diffrn_measured_fraction_theta_full 0.9969
_diffrn_measured_fraction_theta_max 0.8902
_diffrn_measurement_details
;
#__ type_ start__ end____ width___ exp.time_
1 omega -8.00 22.00 1.0000 40.0000
omega____ theta____ kappa____ phi______ frames
- -19.2137 -99.0000 120.0000 30
#__ type_ start__ end____ width___ exp.time_
2 omega -20.00 5.00 1.0000 40.0000
omega____ theta____ kappa____ phi______ frames
- -19.2137 -99.0000 -90.0000 25
#__ type_ start__ end____ width___ exp.time_
3 omega 36.00 104.00 1.0000 40.0000
omega____ theta____ kappa____ phi______ frames
- 22.6512 178.0000 90.0000 68
#__ type_ start__ end____ width___ exp.time_
4 omega 63.00 103.00 1.0000 40.0000
omega____ theta____ kappa____ phi______ frames
- 22.6512 178.0000 -180.0000 40
#__ type_ start__ end____ width___ exp.time_
5 omega -32.00 97.00 1.0000 40.0000
omega____ theta____ kappa____ phi______ frames
- 22.6512 0.0000 -30.0000 129
;
_diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, Eos'
_diffrn_measurement_method '\w scans'
_diffrn_orient_matrix_UB_11 -0.0192351000
_diffrn_orient_matrix_UB_12 0.0596236000
_diffrn_orient_matrix_UB_13 -0.0114487000
_diffrn_orient_matrix_UB_21 0.0582437000
_diffrn_orient_matrix_UB_22 0.0321392000
_diffrn_orient_matrix_UB_23 0.0097336000
_diffrn_orient_matrix_UB_31 0.0347617000
_diffrn_orient_matrix_UB_32 -0.0209116000
_diffrn_orient_matrix_UB_33 -0.0176591000
_diffrn_radiation_monochromator mirror
_diffrn_radiation_type 'Mo K\a'
_diffrn_radiation_wavelength 0.7107
_diffrn_source 'SuperNova (Mo) X-ray Source'
_reflns_Friedel_coverage 0.000
_reflns_Friedel_fraction_full .
_reflns_Friedel_fraction_max .
_reflns_number_gt 2503
_reflns_number_total 6095
_reflns_odcompleteness_completeness 99.69
_reflns_odcompleteness_iscentric 1
_reflns_odcompleteness_theta 26.32
_reflns_special_details
;
Reflections were merged by SHELXL according to the crystal
class for the calculation of statistics and refinement.
_reflns_Friedel_fraction is defined as the number of unique
Friedel pairs measured divided by the number that would be
possible theoretically, ignoring centric projections and
systematic absences.
;
_reflns_threshold_expression 'I > 2\s(I)'
_computing_cell_refinement
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb 1 2013,16:14:44)
;
_computing_data_collection
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb 1 2013,16:14:44)
;
_computing_data_reduction
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.28 (release 01-02-2013 CrysAlis171 .NET)
(compiled Feb 1 2013,16:14:44)
;
_computing_molecular_graphics
;
O. V. Dolomanov, L. J. Bourhis, R. J. Gildea, J. A. K. Howard and H. Puschmann,
OLEX2: a complete structure solution, refinement and analysis program.
J. Appl. Cryst. (2009). 42, 339-341.
;
_computing_publication_material
;
O. V. Dolomanov, L. J. Bourhis, R. J. Gildea, J. A. K. Howard and H. Puschmann,
OLEX2: a complete structure solution, refinement and analysis program.
J. Appl. Cryst. (2009). 42, 339-341.
;
_computing_structure_refinement
;
SHELXL, G.M. Sheldrick, Acta Cryst.
(2008). A64, 112-122
;
_computing_structure_solution 'SUPERFLIP, J. Appl. Cryst. (2007) 40, 786-790'
_refine_diff_density_max 1.029
_refine_diff_density_min -0.421
_refine_diff_density_rms 0.080
_refine_ls_extinction_coef .
_refine_ls_extinction_method none
_refine_ls_goodness_of_fit_ref 0.984
_refine_ls_hydrogen_treatment constr
_refine_ls_matrix_type full
_refine_ls_number_parameters 363
_refine_ls_number_reflns 6095
_refine_ls_number_restraints 96
_refine_ls_R_factor_all 0.1936
_refine_ls_R_factor_gt 0.1021
_refine_ls_restrained_S_all 1.000
_refine_ls_shift/su_max 0.000
_refine_ls_shift/su_mean 0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
;
w=1/[\s^2^(Fo^2^)+(0.1880P)^2^]
where P=(Fo^2^+2Fc^2^)/3
;
_refine_ls_weighting_scheme calc
_refine_ls_wR_factor_gt 0.2845
_refine_ls_wR_factor_ref 0.3641
_refine_special_details
;
?
;
_olex2_refinement_description
;
1. Fixed Uiso
At 1.2 times of:
All C(H) groups, All C(H,H) groups
At 1.5 times of:
All C(H,H,H) groups
2. Uiso/Uaniso restraints and constraints
Uanis(C31) \\sim Ueq, Uanis(C33) \\sim Ueq, Uanis(C32) \\sim Ueq, Uanis(C34) \\sim Ueq, Uanis(C35) \\sim Ueq, Uanis(C30) \\sim Ueq, Uanis(C36) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
Uanis(C21) \\sim Ueq, Uanis(N22) \\sim Ueq, Uanis(C29) \\sim Ueq, Uanis(C23) \\sim Ueq, Uanis(C25) \\sim Ueq, Uanis(C24) \\sim Ueq, Uanis(C26) \\sim Ueq, Uanis(C27) \\sim Ueq, Uanis(C28) \\sim Ueq: with sigma of 0.01 and sigma for terminal atoms of 0.02
3.a Ternary CH refined with riding coordinates:
C13(H13)
3.b Secondary CH2 refined with riding coordinates:
C1(H1A,H1B), C4(H4A,H4B)
3.c Aromatic/amide H refined with riding coordinates:
C5(H5), C6(H6), C8(H8), C9(H9), C10(H10), C11(H11), C12(H12), C15(H15),
C16(H16), C17(H17), C18(H18), C19(H19), C21(H21), C24(H24), C25(H25), C26(H26),
C27(H27), C31(H31), C32(H32), C34(H34), C35(H35)
3.d Idealised Me refined as rotating group:
C29(H29A,H29B,H29C), C36(H36A,H36B,H36C)
;
_atom_sites_solution_hydrogens geom
_atom_sites_solution_primary iterative
_atom_sites_solution_secondary ?
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
S1 S 0.53908(17) -0.02997(15) 0.40691(5) 0.0742(6) Uani 1 1 d . . . . .
O1 O 0.6064(4) -0.0599(4) 0.44873(12) 0.0880(13) Uani 1 1 d . . . . .
O2 O 0.5968(5) -0.0661(5) 0.36809(13) 0.0996(15) Uani 1 1 d . . . . .
N1 N 0.5176(4) 0.1291(4) 0.40559(12) 0.0582(11) Uani 1 1 d . . . . .
C1 C 0.4492(5) 0.1919(5) 0.36578(14) 0.0552(12) Uani 1 1 d . . . . .
H1A H 0.3960 0.1270 0.3482 0.066 Uiso 1 1 calc R U . . .
H1B H 0.5125 0.2322 0.3481 0.066 Uiso 1 1 calc R U . . .
C2 C 0.3634(4) 0.2957(5) 0.38353(14) 0.0490(11) Uani 1 1 d . . . . .
C3 C 0.3834(4) 0.3014(5) 0.42772(14) 0.0521(12) Uani 1 1 d . . . . .
C4 C 0.4824(5) 0.1994(6) 0.44519(15) 0.0682(15) Uani 1 1 d . . . . .
H4A H 0.5599 0.2416 0.4607 0.082 Uiso 1 1 calc R U . . .
H4B H 0.4439 0.1381 0.4648 0.082 Uiso 1 1 calc R U . . .
C5 C 0.3180(5) 0.3866(5) 0.45622(15) 0.0590(13) Uani 1 1 d . . . . .
H5 H 0.2574 0.4490 0.4436 0.071 Uiso 1 1 calc R U . . .
C6 C 0.3386(5) 0.3820(6) 0.49969(16) 0.0684(15) Uani 1 1 d . . . . .
H6 H 0.3985 0.3184 0.5119 0.082 Uiso 1 1 calc R U . . .
C7 C 0.2755(6) 0.4682(6) 0.52994(16) 0.0662(15) Uani 1 1 d . . . . .
C8 C 0.3206(7) 0.4656(7) 0.57436(18) 0.090(2) Uani 1 1 d . . . . .
H8 H 0.3921 0.4109 0.5839 0.109 Uiso 1 1 calc R U . . .
C9 C 0.2628(8) 0.5412(10) 0.6044(2) 0.111(3) Uani 1 1 d . . . . .
H9 H 0.2918 0.5335 0.6340 0.133 Uiso 1 1 calc R U . . .
C10 C 0.1635(9) 0.6271(8) 0.5909(3) 0.109(3) Uani 1 1 d . . . . .
H10 H 0.1302 0.6852 0.6107 0.130 Uiso 1 1 calc R U . . .
C11 C 0.1111(10) 0.6278(9) 0.5467(3) 0.146(4) Uani 1 1 d . . . . .
H11 H 0.0367 0.6790 0.5375 0.176 Uiso 1 1 calc R U . . .
C12 C 0.1712(9) 0.5518(8) 0.5173(2) 0.122(3) Uani 1 1 d . . . . .
H12 H 0.1401 0.5572 0.4878 0.147 Uiso 1 1 calc R U . . .
C13 C 0.2719(4) 0.3807(5) 0.35380(13) 0.0487(11) Uani 1 1 d . . . . .
H13 H 0.2468 0.4569 0.3712 0.058 Uiso 1 1 calc R U . . .
C14 C 0.3444(5) 0.4375(5) 0.31741(16) 0.0566(13) Uani 1 1 d . . . . .
C15 C 0.4263(6) 0.5495(6) 0.3268(2) 0.0791(17) Uani 1 1 d . . . . .
H15 H 0.4344 0.5854 0.3549 0.095 Uiso 1 1 calc R U . . .
C16 C 0.4941(7) 0.6064(7) 0.2956(3) 0.108(3) Uani 1 1 d . . . . .
H16 H 0.5501 0.6787 0.3027 0.130 Uiso 1 1 calc R U . . .
C17 C 0.4795(8) 0.5573(9) 0.2538(3) 0.106(3) Uani 1 1 d . . . . .
H17 H 0.5238 0.5983 0.2324 0.127 Uiso 1 1 calc R U . . .
C18 C 0.4008(8) 0.4487(9) 0.2432(2) 0.095(2) Uani 1 1 d . . . . .
H18 H 0.3924 0.4159 0.2148 0.114 Uiso 1 1 calc R U . . .
C19 C 0.3318(5) 0.3860(6) 0.27520(16) 0.0680(15) Uani 1 1 d . . . . .
H19 H 0.2789 0.3114 0.2682 0.082 Uiso 1 1 calc R U . . .
C20 C 0.1453(5) 0.3089(5) 0.33787(14) 0.0556(12) Uani 1 1 d . . . . .
C21 C 0.1058(5) 0.1851(6) 0.35083(17) 0.0652(14) Uani 1 1 d . U . . .
H21 H 0.1565 0.1288 0.3700 0.078 Uiso 1 1 calc R U . . .
N22 N -0.0210(5) 0.1559(6) 0.33109(16) 0.0787(14) Uani 1 1 d . U . . .
C23 C -0.0629(5) 0.2650(7) 0.30538(18) 0.0716(16) Uani 1 1 d . U . . .
C24 C -0.2000(7) 0.3958(10) 0.2587(2) 0.106(2) Uani 1 1 d . U . . .
H24 H -0.2791 0.4094 0.2410 0.128 Uiso 1 1 calc R U . . .
C25 C -0.1851(6) 0.2810(9) 0.2796(2) 0.092(2) Uani 1 1 d . U . . .
H25 H -0.2507 0.2154 0.2775 0.110 Uiso 1 1 calc R U . . .
C26 C -0.1071(8) 0.4977(9) 0.2610(2) 0.099(2) Uani 1 1 d . U . . .
H26 H -0.1256 0.5772 0.2459 0.119 Uiso 1 1 calc R U . . .
C27 C 0.0120(6) 0.4803(7) 0.28561(17) 0.0754(16) Uani 1 1 d . U . . .
H27 H 0.0765 0.5468 0.2871 0.090 Uiso 1 1 calc R U . . .
C28 C 0.0352(5) 0.3607(6) 0.30859(15) 0.0596(13) Uani 1 1 d . U . . .
C29 C -0.0969(8) 0.0331(9) 0.3350(3) 0.125(3) Uani 1 1 d . U . . .
H29A H -0.1690 0.0502 0.3522 0.187 Uiso 1 1 calc R U . . .
H29B H -0.0400 -0.0345 0.3490 0.187 Uiso 1 1 calc R U . . .
H29C H -0.1317 0.0030 0.3065 0.187 Uiso 1 1 calc R U . . .
C30 C 0.3871(7) -0.1032(6) 0.40314(19) 0.0798(17) Uani 1 1 d . U . . .
C31 C 0.3228(8) -0.1215(10) 0.4399(3) 0.123(3) Uani 1 1 d . U . . .
H31 H 0.3592 -0.0892 0.4669 0.148 Uiso 1 1 calc R U . . .
C32 C 0.2022(10) -0.1893(10) 0.4359(3) 0.138(3) Uani 1 1 d . U . . .
H32 H 0.1626 -0.2102 0.4609 0.165 Uiso 1 1 calc R U . . .
C33 C 0.1390(8) -0.2269(8) 0.3950(3) 0.116(3) Uani 1 1 d . U . . .
C34 C 0.2047(9) -0.2026(8) 0.3605(3) 0.113(2) Uani 1 1 d . U . . .
H34 H 0.1665 -0.2289 0.3330 0.136 Uiso 1 1 calc R U . . .
C35 C 0.3228(8) -0.1422(7) 0.3637(3) 0.100(2) Uani 1 1 d . U . . .
H35 H 0.3629 -0.1259 0.3384 0.121 Uiso 1 1 calc R U . . .
C36 C 0.0047(11) -0.2987(11) 0.3932(4) 0.176(4) Uani 1 1 d . U . . .
H36A H -0.0462 -0.2803 0.3657 0.265 Uiso 1 1 calc R U . . .
H36B H -0.0429 -0.2675 0.4166 0.265 Uiso 1 1 calc R U . . .
H36C H 0.0191 -0.3933 0.3961 0.265 Uiso 1 1 calc R U . . .
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
S1 0.0947(12) 0.0654(10) 0.0615(9) 0.0108(7) 0.0040(7) 0.0201(8)
O1 0.101(3) 0.085(3) 0.074(3) 0.027(2) -0.010(2) 0.026(2)
O2 0.123(4) 0.099(4) 0.080(3) -0.002(3) 0.022(2) 0.040(3)
N1 0.066(3) 0.063(3) 0.044(2) 0.008(2) 0.0011(18) 0.010(2)
C1 0.061(3) 0.057(3) 0.047(3) -0.001(2) 0.004(2) 0.006(2)
C2 0.049(3) 0.053(3) 0.044(2) 0.009(2) -0.0035(19) -0.005(2)
C3 0.056(3) 0.053(3) 0.046(3) -0.001(2) 0.000(2) -0.006(2)
C4 0.079(4) 0.073(4) 0.049(3) 0.002(3) -0.009(2) 0.014(3)
C5 0.071(3) 0.056(3) 0.050(3) 0.001(2) 0.002(2) 0.005(3)
C6 0.083(4) 0.072(4) 0.049(3) -0.003(3) 0.001(2) 0.003(3)
C7 0.083(4) 0.072(4) 0.045(3) -0.001(3) 0.008(2) -0.003(3)
C8 0.092(4) 0.118(6) 0.058(3) -0.021(4) -0.007(3) 0.017(4)
C9 0.121(6) 0.153(8) 0.058(4) -0.028(5) 0.007(4) -0.016(6)
C10 0.145(7) 0.104(6) 0.083(5) -0.020(5) 0.037(5) -0.002(6)
C11 0.213(10) 0.132(8) 0.101(6) 0.020(6) 0.048(6) 0.082(7)
C12 0.170(8) 0.144(8) 0.053(4) -0.004(4) 0.017(4) 0.065(6)
C13 0.052(3) 0.048(3) 0.044(2) -0.002(2) -0.0014(19) 0.000(2)
C14 0.049(3) 0.060(3) 0.060(3) 0.013(3) -0.001(2) 0.010(2)
C15 0.077(4) 0.070(4) 0.088(4) 0.017(3) -0.002(3) -0.007(3)
C16 0.096(5) 0.075(5) 0.155(8) 0.043(5) 0.022(5) -0.014(4)
C17 0.084(5) 0.103(7) 0.138(7) 0.061(6) 0.042(5) 0.029(5)
C18 0.105(5) 0.114(6) 0.071(4) 0.024(4) 0.032(4) 0.051(5)
C19 0.071(3) 0.077(4) 0.058(3) 0.009(3) 0.013(2) 0.018(3)
C20 0.054(3) 0.067(3) 0.045(3) 0.001(2) 0.003(2) 0.005(3)
C21 0.059(3) 0.066(4) 0.069(3) 0.003(3) 0.004(2) -0.008(3)
N22 0.063(3) 0.083(4) 0.090(3) -0.012(3) 0.005(2) -0.016(3)
C23 0.052(3) 0.093(4) 0.070(3) -0.015(3) 0.002(2) 0.002(3)
C24 0.074(4) 0.143(7) 0.098(5) -0.019(5) -0.007(4) 0.015(5)
C25 0.068(4) 0.118(5) 0.086(4) -0.017(4) -0.006(3) 0.002(4)
C26 0.098(5) 0.117(5) 0.078(4) 0.010(4) -0.009(3) 0.035(4)
C27 0.070(4) 0.084(4) 0.069(3) 0.006(3) -0.007(3) 0.027(3)
C28 0.052(3) 0.075(4) 0.050(3) -0.005(3) 0.001(2) 0.004(3)
C29 0.095(5) 0.115(6) 0.163(7) 0.007(5) 0.011(5) -0.056(5)
C30 0.106(4) 0.066(4) 0.065(3) 0.015(3) -0.002(3) 0.006(3)
C31 0.120(5) 0.155(7) 0.092(5) 0.037(4) -0.002(4) -0.040(5)
C32 0.154(7) 0.148(7) 0.112(5) 0.036(5) 0.016(5) -0.043(6)
C33 0.117(5) 0.102(5) 0.128(6) 0.015(5) 0.007(5) -0.027(4)
C34 0.136(6) 0.086(5) 0.117(5) 0.011(4) 0.010(5) -0.012(5)
C35 0.113(5) 0.075(4) 0.112(5) -0.012(4) 0.011(4) -0.015(4)
C36 0.182(9) 0.146(8) 0.195(9) 0.038(7) -0.005(7) -0.078(8)
_geom_special_details
;
All esds (except the esd in the dihedral angle between two l.s. planes)
are estimated using the full covariance matrix. The cell esds are taken
into account individually in the estimation of esds in distances, angles
and torsion angles; correlations between esds in cell parameters are only
used when they are defined by crystal symmetry. An approximate (isotropic)
treatment of cell esds is used for estimating esds involving l.s. planes.
;
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
S1 O1 1.423(4) . ?
S1 O2 1.431(4) . ?
S1 N1 1.605(4) . ?
S1 C30 1.696(7) . ?
N1 C1 1.482(6) . ?
N1 C4 1.483(6) . ?
C1 H1A 0.9700 . ?
C1 H1B 0.9700 . ?
C1 C2 1.493(7) . ?
C2 C3 1.355(6) . ?
C2 C13 1.496(6) . ?
C3 C4 1.489(7) . ?
C3 C5 1.434(6) . ?
C4 H4A 0.9700 . ?
C4 H4B 0.9700 . ?
C5 H5 0.9300 . ?
C5 C6 1.333(6) . ?
C6 H6 0.9300 . ?
C6 C7 1.464(7) . ?
C7 C8 1.395(7) . ?
C7 C12 1.370(9) . ?
C8 H8 0.9300 . ?
C8 C9 1.372(9) . ?
C9 H9 0.9300 . ?
C9 C10 1.353(10) . ?
C10 H10 0.9300 . ?
C10 C11 1.405(10) . ?
C11 H11 0.9300 . ?
C11 C12 1.372(10) . ?
C12 H12 0.9300 . ?
C13 H13 0.9800 . ?
C13 C14 1.513(6) . ?
C13 C20 1.505(7) . ?
C14 C15 1.405(8) . ?
C14 C19 1.391(7) . ?
C15 H15 0.9300 . ?
C15 C16 1.362(9) . ?
C16 H16 0.9300 . ?
C16 C17 1.371(11) . ?
C17 H17 0.9300 . ?
C17 C18 1.366(11) . ?
C18 H18 0.9300 . ?
C18 C19 1.412(8) . ?
C19 H19 0.9300 . ?
C20 C21 1.373(7) . ?
C20 C28 1.452(7) . ?
C21 H21 0.9300 . ?
C21 N22 1.391(7) . ?
N22 C23 1.387(8) . ?
N22 C29 1.460(8) . ?
C23 C25 1.406(8) . ?
C23 C28 1.375(8) . ?
C24 H24 0.9300 . ?
C24 C25 1.317(10) . ?
C24 C26 1.382(11) . ?
C25 H25 0.9300 . ?
C26 H26 0.9300 . ?
C26 C27 1.366(9) . ?
C27 H27 0.9300 . ?
C27 C28 1.396(8) . ?
C29 H29A 0.9600 . ?
C29 H29B 0.9600 . ?
C29 H29C 0.9600 . ?
C30 C31 1.377(9) . ?
C30 C35 1.371(8) . ?
C31 H31 0.9300 . ?
C31 C32 1.389(11) . ?
C32 H32 0.9300 . ?
C32 C33 1.401(11) . ?
C33 C34 1.334(10) . ?
C33 C36 1.533(12) . ?
C34 H34 0.9300 . ?
C34 C35 1.333(10) . ?
C35 H35 0.9300 . ?
C36 H36A 0.9600 . ?
C36 H36B 0.9600 . ?
C36 H36C 0.9600 . ?
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 S1 O2 120.3(3) . . ?
O1 S1 N1 106.3(2) . . ?
O1 S1 C30 108.3(3) . . ?
O2 S1 N1 107.2(2) . . ?
O2 S1 C30 106.3(3) . . ?
N1 S1 C30 107.9(3) . . ?
C1 N1 S1 119.4(3) . . ?
C1 N1 C4 110.2(4) . . ?
C4 N1 S1 119.5(3) . . ?
N1 C1 H1A 111.1 . . ?
N1 C1 H1B 111.1 . . ?
N1 C1 C2 103.4(3) . . ?
H1A C1 H1B 109.1 . . ?
C2 C1 H1A 111.1 . . ?
C2 C1 H1B 111.1 . . ?
C1 C2 C13 121.2(4) . . ?
C3 C2 C1 111.5(4) . . ?
C3 C2 C13 127.4(4) . . ?
C2 C3 C4 110.9(4) . . ?
C2 C3 C5 127.5(5) . . ?
C5 C3 C4 121.5(4) . . ?
N1 C4 C3 103.8(4) . . ?
N1 C4 H4A 111.0 . . ?
N1 C4 H4B 111.0 . . ?
C3 C4 H4A 111.0 . . ?
C3 C4 H4B 111.0 . . ?
H4A C4 H4B 109.0 . . ?
C3 C5 H5 118.0 . . ?
C6 C5 C3 124.0(5) . . ?
C6 C5 H5 118.0 . . ?
C5 C6 H6 117.1 . . ?
C5 C6 C7 125.8(5) . . ?
C7 C6 H6 117.1 . . ?
C8 C7 C6 119.5(6) . . ?
C12 C7 C6 123.6(5) . . ?
C12 C7 C8 116.8(5) . . ?
C7 C8 H8 119.0 . . ?
C9 C8 C7 122.1(7) . . ?
C9 C8 H8 119.0 . . ?
C8 C9 H9 120.0 . . ?
C10 C9 C8 119.9(7) . . ?
C10 C9 H9 120.0 . . ?
C9 C10 H10 120.3 . . ?
C9 C10 C11 119.4(7) . . ?
C11 C10 H10 120.3 . . ?
C10 C11 H11 120.4 . . ?
C12 C11 C10 119.1(8) . . ?
C12 C11 H11 120.4 . . ?
C7 C12 C11 122.2(7) . . ?
C7 C12 H12 118.9 . . ?
C11 C12 H12 118.9 . . ?
C2 C13 H13 106.7 . . ?
C2 C13 C14 110.4(4) . . ?
C2 C13 C20 112.2(4) . . ?
C14 C13 H13 106.7 . . ?
C20 C13 H13 106.7 . . ?
C20 C13 C14 113.6(4) . . ?
C15 C14 C13 117.9(5) . . ?
C19 C14 C13 123.3(5) . . ?
C19 C14 C15 118.8(5) . . ?
C14 C15 H15 119.4 . . ?
C16 C15 C14 121.2(7) . . ?
C16 C15 H15 119.4 . . ?
C15 C16 H16 120.0 . . ?
C15 C16 C17 120.0(7) . . ?
C17 C16 H16 120.0 . . ?
C16 C17 H17 119.7 . . ?
C18 C17 C16 120.7(7) . . ?
C18 C17 H17 119.7 . . ?
C17 C18 H18 119.8 . . ?
C17 C18 C19 120.4(7) . . ?
C19 C18 H18 119.8 . . ?
C14 C19 C18 118.9(6) . . ?
C14 C19 H19 120.6 . . ?
C18 C19 H19 120.6 . . ?
C21 C20 C13 126.8(5) . . ?
C21 C20 C28 105.9(5) . . ?
C28 C20 C13 127.1(5) . . ?
C20 C21 H21 124.9 . . ?
C20 C21 N22 110.2(5) . . ?
N22 C21 H21 124.9 . . ?
C21 N22 C29 127.5(6) . . ?
C23 N22 C21 107.3(5) . . ?
C23 N22 C29 125.2(6) . . ?
N22 C23 C25 127.5(6) . . ?
C28 C23 N22 109.4(5) . . ?
C28 C23 C25 123.1(7) . . ?
C25 C24 H24 117.4 . . ?
C25 C24 C26 125.2(7) . . ?
C26 C24 H24 117.4 . . ?
C23 C25 H25 122.5 . . ?
C24 C25 C23 115.0(7) . . ?
C24 C25 H25 122.5 . . ?
C24 C26 H26 120.3 . . ?
C27 C26 C24 119.3(8) . . ?
C27 C26 H26 120.3 . . ?
C26 C27 H27 120.6 . . ?
C26 C27 C28 118.8(7) . . ?
C28 C27 H27 120.6 . . ?
C23 C28 C20 107.3(5) . . ?
C23 C28 C27 118.6(5) . . ?
C27 C28 C20 134.1(5) . . ?
N22 C29 H29A 109.5 . . ?
N22 C29 H29B 109.5 . . ?
N22 C29 H29C 109.5 . . ?
H29A C29 H29B 109.5 . . ?
H29A C29 H29C 109.5 . . ?
H29B C29 H29C 109.5 . . ?
C31 C30 S1 120.4(5) . . ?
C35 C30 S1 121.6(5) . . ?
C35 C30 C31 118.0(7) . . ?
C30 C31 H31 120.7 . . ?
C30 C31 C32 118.6(8) . . ?
C32 C31 H31 120.7 . . ?
C31 C32 H32 119.2 . . ?
C31 C32 C33 121.7(8) . . ?
C33 C32 H32 119.2 . . ?
C32 C33 C36 118.6(9) . . ?
C34 C33 C32 116.5(8) . . ?
C34 C33 C36 124.8(9) . . ?
C33 C34 H34 118.6 . . ?
C35 C34 C33 122.9(9) . . ?
C35 C34 H34 118.6 . . ?
C30 C35 H35 119.0 . . ?
C34 C35 C30 122.1(8) . . ?
C34 C35 H35 119.0 . . ?
C33 C36 H36A 109.5 . . ?
C33 C36 H36B 109.5 . . ?
C33 C36 H36C 109.5 . . ?
H36A C36 H36B 109.5 . . ?
H36A C36 H36C 109.5 . . ?
H36B C36 H36C 109.5 . . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
S1 N1 C1 C2 139.9(3) . . . . ?
S1 N1 C4 C3 -140.7(4) . . . . ?
S1 C30 C31 C32 -176.1(7) . . . . ?
S1 C30 C35 C34 178.5(6) . . . . ?
O1 S1 N1 C1 -179.9(3) . . . . ?
O1 S1 N1 C4 -39.0(4) . . . . ?
O1 S1 C30 C31 30.1(7) . . . . ?
O1 S1 C30 C35 -151.9(5) . . . . ?
O2 S1 N1 C1 50.3(4) . . . . ?
O2 S1 N1 C4 -168.8(4) . . . . ?
O2 S1 C30 C31 160.7(6) . . . . ?
O2 S1 C30 C35 -21.3(6) . . . . ?
N1 S1 C30 C31 -84.6(6) . . . . ?
N1 S1 C30 C35 93.4(6) . . . . ?
N1 C1 C2 C3 3.6(5) . . . . ?
N1 C1 C2 C13 -177.7(4) . . . . ?
C1 N1 C4 C3 3.5(6) . . . . ?
C1 C2 C3 C4 -1.6(6) . . . . ?
C1 C2 C3 C5 -178.9(5) . . . . ?
C1 C2 C13 C14 -48.0(6) . . . . ?
C1 C2 C13 C20 79.9(5) . . . . ?
C2 C3 C4 N1 -1.2(6) . . . . ?
C2 C3 C5 C6 176.7(5) . . . . ?
C2 C13 C14 C15 -79.6(6) . . . . ?
C2 C13 C14 C19 101.7(5) . . . . ?
C2 C13 C20 C21 6.0(7) . . . . ?
C2 C13 C20 C28 -179.7(4) . . . . ?
C3 C2 C13 C14 130.5(5) . . . . ?
C3 C2 C13 C20 -101.6(5) . . . . ?
C3 C5 C6 C7 179.1(5) . . . . ?
C4 N1 C1 C2 -4.3(5) . . . . ?
C4 C3 C5 C6 -0.4(8) . . . . ?
C5 C3 C4 N1 176.3(4) . . . . ?
C5 C6 C7 C8 -170.7(6) . . . . ?
C5 C6 C7 C12 10.4(10) . . . . ?
C6 C7 C8 C9 -178.1(6) . . . . ?
C6 C7 C12 C11 177.6(8) . . . . ?
C7 C8 C9 C10 -3.7(12) . . . . ?
C8 C7 C12 C11 -1.4(12) . . . . ?
C8 C9 C10 C11 6.6(13) . . . . ?
C9 C10 C11 C12 -7.0(14) . . . . ?
C10 C11 C12 C7 4.4(15) . . . . ?
C12 C7 C8 C9 0.9(11) . . . . ?
C13 C2 C3 C4 179.8(5) . . . . ?
C13 C2 C3 C5 2.5(8) . . . . ?
C13 C14 C15 C16 -179.6(5) . . . . ?
C13 C14 C19 C18 178.1(5) . . . . ?
C13 C20 C21 N22 176.0(4) . . . . ?
C13 C20 C28 C23 -175.8(4) . . . . ?
C13 C20 C28 C27 3.2(9) . . . . ?
C14 C13 C20 C21 132.1(5) . . . . ?
C14 C13 C20 C28 -53.5(6) . . . . ?
C14 C15 C16 C17 2.2(10) . . . . ?
C15 C14 C19 C18 -0.6(7) . . . . ?
C15 C16 C17 C18 -2.0(11) . . . . ?
C16 C17 C18 C19 0.6(11) . . . . ?
C17 C18 C19 C14 0.7(9) . . . . ?
C19 C14 C15 C16 -0.8(9) . . . . ?
C20 C13 C14 C15 153.3(5) . . . . ?
C20 C13 C14 C19 -25.4(7) . . . . ?
C20 C21 N22 C23 -0.6(6) . . . . ?
C20 C21 N22 C29 177.8(6) . . . . ?
C21 C20 C28 C23 -0.6(5) . . . . ?
C21 C20 C28 C27 178.4(5) . . . . ?
C21 N22 C23 C25 -179.5(5) . . . . ?
C21 N22 C23 C28 0.3(6) . . . . ?
N22 C23 C25 C24 179.3(6) . . . . ?
N22 C23 C28 C20 0.2(6) . . . . ?
N22 C23 C28 C27 -179.0(4) . . . . ?
C24 C26 C27 C28 -1.4(9) . . . . ?
C25 C23 C28 C20 180.0(5) . . . . ?
C25 C23 C28 C27 0.8(8) . . . . ?
C25 C24 C26 C27 1.8(11) . . . . ?
C26 C24 C25 C23 -0.9(11) . . . . ?
C26 C27 C28 C20 -178.7(5) . . . . ?
C26 C27 C28 C23 0.2(8) . . . . ?
C28 C20 C21 N22 0.7(6) . . . . ?
C28 C23 C25 C24 -0.5(9) . . . . ?
C29 N22 C23 C25 2.0(10) . . . . ?
C29 N22 C23 C28 -178.2(6) . . . . ?
C30 S1 N1 C1 -63.8(4) . . . . ?
C30 S1 N1 C4 77.0(4) . . . . ?
C30 C31 C32 C33 -6.6(15) . . . . ?
C31 C30 C35 C34 -3.5(11) . . . . ?
C31 C32 C33 C34 4.5(15) . . . . ?
C31 C32 C33 C36 -178.7(10) . . . . ?
C32 C33 C34 C35 -1.9(13) . . . . ?
C33 C34 C35 C30 1.6(13) . . . . ?
C35 C30 C31 C32 5.9(12) . . . . ?
C36 C33 C34 C35 -178.5(9) . . . . ?
_shelx_estimated_absorpt_T_max ?
_shelx_estimated_absorpt_T_min ?
_shelx_hkl_checksum 90033
_shelx_hkl_file
;
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12 0 -2 332.594 285.058 5
12 0 -1-38.5078 122.521 5
12 0 0-16.5632 82.6905 5
12 0 1-3.21380 76.5319 5
12 0 2 339.171 324.252 5
12 0 3-172.732 200.863 5
12 0 4 152.179 233.492 5
12 0 5-41.2921 66.1569 5
12 0 6 250.437 205.854 5
12 0 7 350.091 294.055 5
12 0 8-532.914 373.475 5
12 0 9 93.2726 249.530 5
12 0 10 46.3592 246.303 5
12 -1 -17 76.1234 146.719 4
12 -1 -16-41.9857 135.429 4
12 1 -16-12.2989 76.4526 4
12 -1 -15 186.004 231.528 4
12 1 -15 192.124 303.022 4
12 -1 -14-98.6236 199.231 4
12 1 -14 125.433 157.789 4
12 -1 -13 90.7767 81.5026 4
12 1 -13 0.68325 153.418 4
12 -1 -12-26.2061 119.111 4
12 1 -12 122.885 108.924 4
12 -1 -11 111.921 186.320 4
12 1 -11-297.787 274.542 4
12 -1 -10 95.1582 188.507 4
12 1 -10 177.731 247.716 4
12 -1 -9 370.254 309.735 4
12 1 -9 603.778 423.631 4
12 -1 -8 161.954 233.525 4
12 1 -8 289.462 354.049 4
12 -1 -7 48.1775 28.8179 4
12 1 -7 249.281 304.170 4
12 -1 -6 64.2765 103.819 4
12 1 -5 199.695 175.699 5
12 -1 -5-24.0619 97.4473 4
12 1 -4-9.39220 57.3590 5
12 -1 -4 61.3079 156.737 4
12 -1 -3 94.3351 127.237 5
12 1 -3-28.8028 52.4541 5
12 -1 -3-12.4102 52.8952 4
12 -1 -2-118.704 156.997 5
12 1 -2 122.017 178.019 5
12 -1 -1-33.6564 49.5173 5
12 1 -1 16.2968 50.5442 5
12 -1 0-186.273 172.272 5
12 1 0-203.254 266.470 5
12 -1 1-178.522 197.757 5
12 1 1-15.4810 116.269 5
12 -1 2-197.592 210.592 5
12 1 2-180.574 202.543 5
12 -1 3-297.017 261.297 5
12 1 3-87.2139 143.697 5
12 -1 4-232.133 233.736 5
12 1 4 221.274 242.022 5
12 -1 5 207.652 161.357 5
12 1 5 574.116 400.063 5
12 -1 6 143.365 206.840 5
12 1 6 43.5867 84.0873 5
12 -1 7-313.398 280.333 5
12 1 7 183.031 233.312 5
12 -1 8 76.2649 111.604 5
12 1 8 131.079 202.326 5
12 -1 9 20.1840 127.083 5
12 1 9-134.080 213.271 5
12 -1 10 175.614 259.530 5
12 1 10 144.427 164.035 5
12 -2 -18 29.8573 171.777 4
12 -2 -17 242.215 309.116 4
12 -2 -16-58.8028 119.992 4
12 -2 -15 12.7177 31.6473 4
12 -2 -14-229.344 234.515 4
12 2 -14-6.38599 134.792 4
12 -2 -13 232.504 236.917 4
12 2 -13 129.773 259.435 4
12 -2 -12 173.697 223.514 4
12 2 -12 105.346 218.866 4
12 -2 -11-365.710 292.234 4
12 2 -11-79.6009 197.418 4
12 -2 -10 91.2196 135.448 4
12 2 -10 17.3016 96.0992 4
12 -2 -9-15.3433 59.3240 4
12 2 -9 308.043 292.256 4
12 -2 -8 74.5784 165.149 4
12 -2 -7 259.719 286.024 4
12 -2 -6-40.1717 47.5479 4
12 2 -6 91.9598 208.162 5
12 2 -5 56.9496 77.0401 5
12 -2 -5 19.5586 144.686 4
12 2 -4-327.257 257.606 5
12 -2 -4 202.095 257.633 4
12 2 -3 49.4703 141.415 5
12 -2 -3 35.6086 82.5573 4
12 2 -2 162.686 204.096 5
12 -2 -2 82.1230 128.698 4
12 -2 -1-1.06475 152.622 5
12 2 -1-280.218 251.948 5
12 -2 -1 189.917 213.955 4
12 -2 0 226.308 235.711 5
12 2 0 23.9306 164.976 5
12 -2 1 51.3257 68.7899 5
12 2 1-67.9380 177.047 5
12 -2 2 140.950 150.626 5
12 2 2-140.705 270.896 5
12 -2 3-23.8860 129.462 5
12 2 3 90.6048 152.414 5
12 -2 4 50.1631 139.576 5
12 2 4 96.9426 155.892 5
12 -2 5-25.0745 34.1810 5
12 2 5 80.8944 193.447 5
12 -2 6 190.214 293.273 5
12 2 6 140.395 101.369 5
12 -2 7 366.207 333.899 5
12 2 7 69.7065 121.911 5
12 -2 8 52.7448 107.574 5
12 2 8-31.7685 89.8767 5
12 -2 9 86.9099 191.595 5
12 2 9 417.107 340.815 5
12 -2 10 89.2751 119.756 5
12 -3 -18 124.799 231.736 4
12 -3 -17-91.1122 149.120 4
12 -3 -16-39.0784 96.8022 4
12 -3 -15 709.587 442.546 4
12 -3 -14 11.8889 131.098 4
12 -3 -13-146.474 182.930 4
12 -3 -12 383.502 325.900 4
12 3 -12 339.510 314.239 4
12 -3 -11 244.370 274.776 4
12 3 -11-328.054 280.497 4
12 -3 -10-44.0086 99.1357 4
12 3 -10 226.063 345.041 4
12 -3 -9 67.8015 90.7941 4
12 -3 -8-141.345 228.012 4
12 -3 -7 46.5500 90.6422 4
12 3 -7 170.619 207.218 5
12 -3 -6 28.4774 100.209 4
12 3 -6-24.4375 159.105 5
12 -3 -5 77.4974 75.6106 4
12 3 -5 283.915 306.367 5
12 -3 -4-168.694 188.535 4
12 3 -4 89.7859 159.814 5
12 -3 -3-56.8746 154.168 4
12 3 -3 133.868 209.440 5
12 -3 -2 24.3366 60.1136 4
12 3 -2 208.088 256.441 5
12 -3 -1-43.3913 65.2188 4
12 3 -1 62.0811 68.0200 5
12 -3 0 108.340 193.167 4
12 -3 0-83.5658 111.754 5
12 3 1-3.54340 110.024 5
12 -3 1 30.7374 90.6914 5
12 3 2 95.7483 154.731 5
12 -3 2 5.68553 88.0233 5
12 3 3-2.33579 43.2215 5
12 -3 3-69.1265 123.877 5
12 3 4-130.810 163.058 5
12 -3 4 0.29912 64.9819 5
12 3 5-455.498 346.487 5
12 -3 5 62.2445 246.513 5
12 3 6 143.180 214.828 5
12 -3 6-59.6984 119.504 5
12 3 7 254.232 300.075 5
12 -3 7-60.5105 121.774 5
12 -3 8-139.759 187.280 5
12 -3 9 13.8365 137.799 5
12 -4 -17-191.331 212.759 4
12 -4 -16 19.0267 37.8192 4
12 -4 -15 121.481 195.661 4
12 -4 -14-169.865 196.256 4
12 -4 -13-201.734 211.968 4
12 -4 -12-97.1068 145.789 4
12 -4 -11 227.723 217.012 4
12 -4 -10 155.229 201.235 4
12 -4 -9 27.3560 33.1936 4
12 -4 -8 209.595 283.600 4
12 4 -8 188.762 205.215 5
12 4 -7 268.594 262.837 5
12 4 -6-247.404 237.860 5
12 4 -5 28.4607 121.757 5
12 4 -4 345.429 305.082 5
12 4 -3 109.389 168.910 5
12 4 -2-112.657 131.609 5
12 4 -1-248.753 275.470 5
12 4 0 146.883 225.730 5
12 4 1 9.07180 33.4433 5
12 4 2 160.814 259.381 5
12 4 3 187.024 252.103 5
12 4 4 560.969 420.199 5
12 4 5-81.3028 195.886 5
12 5 -9 278.509 276.978 5
12 5 -8 34.6589 109.531 5
12 5 -7 97.7049 71.3486 5
12 5 -6-146.383 156.252 5
12 5 -5-95.3855 32.2602 5
12 5 -4 84.0289 197.046 5
12 5 -3 196.982 267.411 5
12 5 -2 66.7243 66.0761 5
12 5 -1-152.760 199.808 5
12 5 0 304.834 394.025 5
12 5 1 265.014 269.178 5
12 6 -8 81.0497 168.108 5
12 6 -7-77.1781 140.834 5
12 6 -6-131.290 184.884 5
12 6 -5-155.960 202.652 5
13 0 -7 76.7158 180.002 4
13 0 -6 272.137 300.197 4
13 0 -5-140.981 192.386 4
13 0 -4-116.001 174.381 4
13 0 -1 87.2184 31.0605 5
13 0 0-306.585 272.861 5
13 0 1 176.559 254.750 5
13 0 2-220.277 236.732 5
13 0 3 152.892 252.329 5
13 0 4 168.764 276.034 5
13 0 5 44.7417 65.4632 5
13 -1 -9 60.2107 187.309 4
13 -1 -8-74.9766 139.767 4
13 -1 -7-138.999 188.911 4
13 -1 -6 38.0401 127.212 4
13 -1 -5 33.8444 189.791 4
13 -1 -4 421.142 393.128 4
13 -1 -3 377.316 328.983 4
13 1 -2 212.665 276.183 5
13 -1 -2-168.787 205.709 4
13 1 -1 54.0496 57.4633 5
13 -1 0 146.556 212.124 5
13 1 0 254.457 248.748 5
13 -1 1 66.1611 34.8936 5
13 1 1-0.33209 83.9103 5
13 -1 2-27.8614 82.8007 5
13 1 2-226.366 241.481 5
13 -1 3 46.0691 57.7757 5
13 1 3-263.109 262.985 5
13 -1 4 66.4341 93.8951 5
13 1 4-223.016 244.808 5
13 -1 5-135.719 188.716 5
13 -2 -10-136.738 186.853 4
13 -2 -9 0.33428 31.9236 4
13 -2 -8 145.825 226.761 4
13 -2 -7 23.3806 76.4908 4
13 -2 -6 38.5200 195.080 4
13 -2 -5-29.3552 84.8193 4
13 -2 -4 47.8960 141.629 4
13 2 -3 204.594 239.676 5
13 -2 -3 234.228 272.370 4
13 2 -2-65.6173 215.413 5
13 -2 -2 286.739 303.926 4
13 2 -1 290.004 247.889 5
13 -2 -1-335.241 282.495 4
13 2 0-134.709 185.674 5
13 -2 0 110.349 143.468 4
13 2 1 20.5880 126.918 5
13 -2 1 176.216 177.406 4
13 -2 2 132.281 205.253 5
13 2 2 298.197 330.533 5
13 -2 3 189.536 273.183 5
13 2 3-0.35555 53.6965 5
13 -2 4 76.6806 267.190 5
13 -2 5 102.697 132.955 5
13 -3 -11 13.9853 125.411 4
13 -3 -10 6.79520 26.7367 4
13 -3 -9 71.7015 73.0252 4
13 -3 -8 18.4547 70.6502 4
13 -3 -7-0.31553 247.611 4
13 -3 -6 161.453 239.397 4
13 -3 -5-35.5218 91.6063 4
13 3 -4 142.779 186.627 5
13 3 -3 99.6174 219.925 5
13 3 -2-42.3662 104.421 5
13 3 -1-309.064 284.403 5
13 3 0 305.615 235.639 5
13 4 -3 143.925 229.735 5
0 0 0 0.00 0.00 0
TITL zhmj0718 in P2(1)/c
REM P2(1)/c (#14 in standard setting)
CELL 0.71073 10.119137 9.999902 30.775959 90.0000 96.0768 90.0000
ZERR 14.00 0.000636 0.000655 0.001438 0.0000 0.0048 0.0000
LATT 1
SYMM -x, y+1/2,-z+1/2
SFAC C H N O
UNIT 154.00 140.00 14.00 14.00
TREF
HKLF 4
END
;
_shelx_res_checksum 11670
_shelx_res_file
;
TITL CF solution in P21/c
CELL 0.71073 10.119137 9.999902 30.775959 90 96.0768 90
ZERR 4 0.000636 0.000655 0.001438 0 0.0048 0
LATT 1
SYMM -X,0.5+Y,0.5-Z
SFAC C H N O S
UNIT 140 128 8 8 4
ISOR 0.01 0.02 C31 C33 C32 C34 C35 C30 C36
ISOR 0.01 0.02 C21 N22 C29 C23 C25 C24 C26 C27 C28
L.S. 10
PLAN 25
BOND $H
HTAB
CONF
fmap 2
ACTA
SHEL 999 0.81
REM D:/olex2_zhmj0718/zhmj0718.hkl
WGHT 0.188000
FVAR 2.69963
S1 5 0.539080 -0.029972 0.406906 11.00000 0.09472 0.06543 =
0.06148 0.01082 0.00403 0.02011
O1 4 0.606383 -0.059858 0.448734 11.00000 0.10092 0.08494 =
0.07402 0.02688 -0.01023 0.02589
O2 4 0.596764 -0.066116 0.368087 11.00000 0.12260 0.09893 =
0.07988 -0.00164 0.02239 0.04009
N1 3 0.517649 0.129105 0.405587 11.00000 0.06639 0.06295 =
0.04414 0.00800 0.00109 0.00970
C1 1 0.449161 0.191946 0.365780 11.00000 0.06128 0.05663 =
0.04727 -0.00099 0.00429 0.00638
AFIX 23
H1A 2 0.396023 0.127028 0.348226 11.00000 -1.20000
H1B 2 0.512479 0.232231 0.348147 11.00000 -1.20000
AFIX 0
C2 1 0.363436 0.295741 0.383529 11.00000 0.04877 0.05264 =
0.04366 0.00882 -0.00354 -0.00483
C3 1 0.383399 0.301413 0.427719 11.00000 0.05603 0.05255 =
0.04645 -0.00068 -0.00039 -0.00600
C4 1 0.482386 0.199448 0.445189 11.00000 0.07876 0.07341 =
0.04912 0.00188 -0.00893 0.01425
AFIX 23
H4A 2 0.559872 0.241561 0.460706 11.00000 -1.20000
H4B 2 0.443893 0.138122 0.464776 11.00000 -1.20000
AFIX 0
C5 1 0.317965 0.386646 0.456221 11.00000 0.07068 0.05559 =
0.04983 0.00119 0.00187 0.00536
AFIX 43
H5 2 0.257400 0.448985 0.443589 11.00000 -1.20000
AFIX 0
C6 1 0.338597 0.382023 0.499688 11.00000 0.08347 0.07203 =
0.04852 -0.00295 0.00077 0.00311
AFIX 43
H6 2 0.398451 0.318370 0.511892 11.00000 -1.20000
AFIX 0
C7 1 0.275481 0.468171 0.529944 11.00000 0.08254 0.07168 =
0.04480 -0.00091 0.00849 -0.00259
C8 1 0.320561 0.465594 0.574360 11.00000 0.09205 0.11836 =
0.05784 -0.02113 -0.00680 0.01672
AFIX 43
H8 2 0.392074 0.410860 0.583932 11.00000 -1.20000
AFIX 0
C9 1 0.262764 0.541230 0.604374 11.00000 0.12111 0.15332 =
0.05751 -0.02823 0.00707 -0.01596
AFIX 43
H9 2 0.291794 0.533509 0.633964 11.00000 -1.20000
AFIX 0
C10 1 0.163475 0.627078 0.590879 11.00000 0.14463 0.10373 =
0.08315 -0.02037 0.03715 -0.00157
AFIX 43
H10 2 0.130163 0.685156 0.610657 11.00000 -1.20000
AFIX 0
C11 1 0.111099 0.627753 0.546723 11.00000 0.21347 0.13165 =
0.10067 0.01994 0.04794 0.08196
AFIX 43
H11 2 0.036680 0.679049 0.537550 11.00000 -1.20000
AFIX 0
C12 1 0.171181 0.551763 0.517330 11.00000 0.17023 0.14407 =
0.05344 -0.00364 0.01717 0.06541
AFIX 43
H12 2 0.140058 0.557175 0.487847 11.00000 -1.20000
AFIX 0
C13 1 0.271934 0.380732 0.353804 11.00000 0.05220 0.04820 =
0.04418 -0.00155 -0.00135 0.00019
AFIX 13
H13 2 0.246761 0.456889 0.371201 11.00000 -1.20000
AFIX 0
C14 1 0.344418 0.437507 0.317406 11.00000 0.04916 0.05955 =
0.05955 0.01289 -0.00149 0.00986
C15 1 0.426333 0.549507 0.326825 11.00000 0.07708 0.07032 =
0.08758 0.01733 -0.00202 -0.00697
AFIX 43
H15 2 0.434443 0.585391 0.354860 11.00000 -1.20000
AFIX 0
C16 1 0.494054 0.606438 0.295632 11.00000 0.09594 0.07460 =
0.15537 0.04342 0.02189 -0.01427
AFIX 43
H16 2 0.550143 0.678660 0.302698 11.00000 -1.20000
AFIX 0
C17 1 0.479547 0.557276 0.253802 11.00000 0.08373 0.10290 =
0.13757 0.06056 0.04240 0.02882
AFIX 43
H17 2 0.523823 0.598285 0.232407 11.00000 -1.20000
AFIX 0
C18 1 0.400757 0.448724 0.243238 11.00000 0.10478 0.11404 =
0.07139 0.02418 0.03177 0.05092
AFIX 43
H18 2 0.392449 0.415921 0.214804 11.00000 -1.20000
AFIX 0
C19 1 0.331828 0.385969 0.275202 11.00000 0.07052 0.07684 =
0.05793 0.00850 0.01319 0.01802
AFIX 43
H19 2 0.278902 0.311430 0.268153 11.00000 -1.20000
AFIX 0
C20 1 0.145309 0.308899 0.337872 11.00000 0.05442 0.06709 =
0.04470 0.00082 0.00279 0.00461
C21 1 0.105822 0.185091 0.350832 11.00000 0.05949 0.06631 =
0.06902 0.00310 0.00377 -0.00802
AFIX 43
H21 2 0.156532 0.128833 0.370036 11.00000 -1.20000
AFIX 0
N22 3 -0.021006 0.155935 0.331091 11.00000 0.06266 0.08325 =
0.08965 -0.01218 0.00540 -0.01646
C23 1 -0.062923 0.264974 0.305384 11.00000 0.05177 0.09254 =
0.06959 -0.01472 0.00223 0.00159
C24 1 -0.199956 0.395805 0.258694 11.00000 0.07380 0.14337 =
0.09811 -0.01906 -0.00714 0.01475
AFIX 43
H24 2 -0.279138 0.409437 0.240994 11.00000 -1.20000
AFIX 0
C25 1 -0.185142 0.281002 0.279603 11.00000 0.06833 0.11846 =
0.08566 -0.01710 -0.00643 0.00164
AFIX 43
H25 2 -0.250652 0.215400 0.277477 11.00000 -1.20000
AFIX 0
C26 1 -0.107124 0.497651 0.260973 11.00000 0.09833 0.11707 =
0.07800 0.01048 -0.00883 0.03459
AFIX 43
H26 2 -0.125609 0.577189 0.245883 11.00000 -1.20000
AFIX 0
C27 1 0.012032 0.480277 0.285615 11.00000 0.06974 0.08384 =
0.06944 0.00567 -0.00740 0.02650
AFIX 43
H27 2 0.076534 0.546839 0.287062 11.00000 -1.20000
AFIX 0
C28 1 0.035180 0.360699 0.308592 11.00000 0.05235 0.07546 =
0.05002 -0.00498 0.00122 0.00428
C29 1 -0.096917 0.033127 0.335041 11.00000 0.09549 0.11466 =
0.16286 0.00669 0.01122 -0.05607
AFIX 137
H29A 2 -0.168951 0.050169 0.352223 11.00000 -1.50000
H29B 2 -0.039957 -0.034484 0.349006 11.00000 -1.50000
H29C 2 -0.131743 0.002969 0.306492 11.00000 -1.50000
AFIX 0
C30 1 0.387107 -0.103245 0.403137 11.00000 0.10607 0.06629 =
0.06465 0.01472 -0.00211 0.00555
C31 1 0.322762 -0.121531 0.439928 11.00000 0.11999 0.15497 =
0.09167 0.03731 -0.00152 -0.03956
AFIX 43
H31 2 0.359201 -0.089234 0.466908 11.00000 -1.20000
AFIX 0
C32 1 0.202244 -0.189263 0.435877 11.00000 0.15354 0.14770 =
0.11213 0.03563 0.01645 -0.04264
AFIX 43
H32 2 0.162559 -0.210164 0.460929 11.00000 -1.20000
AFIX 0
C33 1 0.138961 -0.226885 0.395025 11.00000 0.11747 0.10192 =
0.12796 0.01459 0.00727 -0.02664
C34 1 0.204712 -0.202566 0.360515 11.00000 0.13609 0.08575 =
0.11694 0.01097 0.01033 -0.01156
AFIX 43
H34 2 0.166498 -0.228883 0.333033 11.00000 -1.20000
AFIX 0
C35 1 0.322829 -0.142176 0.363696 11.00000 0.11321 0.07549 =
0.11235 -0.01225 0.01058 -0.01460
AFIX 43
H35 2 0.362881 -0.125946 0.338371 11.00000 -1.20000
AFIX 0
C36 1 0.004700 -0.298712 0.393180 11.00000 0.18223 0.14645 =
0.19531 0.03762 -0.00482 -0.07837
AFIX 137
H36A 2 -0.046153 -0.280333 0.365702 11.00000 -1.50000
H36B 2 -0.042942 -0.267479 0.416570 11.00000 -1.50000
H36C 2 0.019091 -0.393319 0.396113 11.00000 -1.50000
AFIX 0
HKLF 4
REM CF solution in P21/c
REM R1 = 0.1021 for 2503 Fo > 4sig(Fo) and 0.1936 for all 6095 data
REM 363 parameters refined using 96 restraints
END
WGHT 0.1880 0.0000
REM Instructions for potential hydrogen bonds
REM No hydrogen bonds found for HTAB generation
REM Highest difference peak 1.029, deepest hole -0.421, 1-sigma level 0.080
Q1 1 -0.0634 -0.0299 0.4863 11.00000 0.05 1.03
Q2 1 0.0891 -0.1800 0.4207 11.00000 0.05 0.38
Q3 1 0.5070 -0.1228 0.4406 11.00000 0.05 0.25
Q4 1 0.5104 -0.1151 0.3677 11.00000 0.05 0.24
Q5 1 0.1346 -0.1119 0.4536 11.00000 0.05 0.22
Q6 1 -0.0822 0.0306 0.3472 11.00000 0.05 0.22
Q7 1 -0.0547 -0.2195 0.4220 11.00000 0.05 0.21
Q8 1 0.3670 0.2571 0.3969 11.00000 0.05 0.20
Q9 1 0.6033 -0.0531 0.3580 11.00000 0.05 0.19
Q10 1 0.5617 0.1171 0.4080 11.00000 0.05 0.19
Q11 1 0.4307 0.0705 0.3999 11.00000 0.05 0.19
Q12 1 -0.1909 0.4415 0.2507 11.00000 0.05 0.19
Q13 1 -0.0773 0.5640 0.2632 11.00000 0.05 0.17
Q14 1 0.1549 -0.2561 0.3963 11.00000 0.05 0.17
Q15 1 0.4229 0.4824 0.5099 11.00000 0.05 0.16
Q16 1 0.2912 0.4687 0.5432 11.00000 0.05 0.16
Q17 1 0.4022 -0.1404 0.4028 11.00000 0.05 0.16
Q18 1 0.3471 -0.1667 0.4406 11.00000 0.05 0.16
Q19 1 0.2967 0.5919 0.5304 11.00000 0.05 0.16
Q20 1 -0.1832 0.2100 0.2950 11.00000 0.05 0.16
Q21 1 0.5591 -0.2083 0.4091 11.00000 0.05 0.16
Q22 1 0.2804 -0.1397 0.3925 11.00000 0.05 0.16
Q23 1 -0.2808 0.5039 0.2161 11.00000 0.05 0.16
Q24 1 0.0953 0.4942 0.4905 11.00000 0.05 0.15
Q25 1 -0.0658 -0.2859 0.3528 11.00000 0.05 0.15
;
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelxl_version_number 2013-2
_database_code_depnum_ccdc_archive 'CCDC 969443'