# Electronic Supplementary Material (ESI) for Journal of Materials Chemistry C
# This journal is © The Royal Society of Chemistry 2014

#######################################################################
#
#                 Cambridge Crystallographic Data Centre
#                                CCDC 
# 
#######################################################################
# 
#  This CIF contains data from an original supplementary publication
#  deposited with the CCDC, and may include chemical, crystal,
#  experimental, refinement, atomic coordinates,
#  anisotropic displacement parameters and molecular geometry data,
#  as required by the journal to which it was submitted.
#
#  This CIF is provided on the understanding that it is used for bona
#  fide research purposes only. It may contain copyright material
#  of the CCDC or of third parties, and may not be copied or further
#  disseminated in any form, whether machine-readable or not,
#  except for the purpose of generating routine backup copies
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#  data retrieval see:
#                         www.ccdc.cam.ac.uk
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#  Bona fide researchers may freely download Mercury and enCIFer
#  from this site to visualise CIF-encoded structures and 
#  to carry out CIF format checking respectively.
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data_f

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C26 H14'
_chemical_formula_weight         326.37

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   P2(1)/n

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'

_cell_length_a                   16.2914(19)
_cell_length_b                   5.1448(6)
_cell_length_c                   19.056(2)
_cell_angle_alpha                90.00
_cell_angle_beta                 97.021(6)
_cell_angle_gamma                90.00
_cell_volume                     1585.2(3)
_cell_formula_units_Z            4
_cell_measurement_temperature    296(2)
_cell_measurement_reflns_used    ?
_cell_measurement_theta_min      ?
_cell_measurement_theta_max      ?

_exptl_crystal_description       needle
_exptl_crystal_colour            red
_exptl_crystal_size_max          0.4
_exptl_crystal_size_mid          0.04
_exptl_crystal_size_min          0.04
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    1.368
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             680
_exptl_absorpt_coefficient_mu    0.592
_exptl_absorpt_correction_type   'multi scan'
_exptl_absorpt_correction_T_min  0.788
_exptl_absorpt_correction_T_max  1
_exptl_absorpt_process_details   Sadabs

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      296(2)
_diffrn_radiation_wavelength     1.54178
_diffrn_radiation_type           CuK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'Omega scan'
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            5139
_diffrn_reflns_av_R_equivalents  0.0463
_diffrn_reflns_av_sigmaI/netI    0.0443
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_k_min       -5
_diffrn_reflns_limit_k_max       5
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_theta_min         3.37
_diffrn_reflns_theta_max         57.96
_reflns_number_total             1952
_reflns_number_gt                1679
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_special_details          
; 
 Refinement of F^2^ against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F^2^, conventional R-factors R are based 
 on F, with F set to zero for negative F^2^. The threshold expression of 
 F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F^2^ are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[\s^2^(Fo^2^)+(0.0600P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     SHELXL
_refine_ls_extinction_coef       0.0014(6)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^
_refine_ls_number_reflns         1952
_refine_ls_number_parameters     236
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0665
_refine_ls_R_factor_gt           0.0595
_refine_ls_wR_factor_ref         0.1829
_refine_ls_wR_factor_gt          0.1786
_refine_ls_goodness_of_fit_ref   2.085
_refine_ls_restrained_S_all      2.085
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.94126(16) 0.8431(5) 0.53109(14) 0.0491(7) Uani 1 1 d . . .
C2 C 0.98869(16) 1.0417(5) 0.56776(13) 0.0478(7) Uani 1 1 d . . .
C3 C 1.04760(15) 1.2019(5) 0.53972(14) 0.0482(7) Uani 1 1 d . . .
C4 C 1.08771(18) 1.3926(5) 0.58778(15) 0.0575(8) Uani 1 1 d . . .
H4 H 1.1260 1.5066 0.5723 0.069 Uiso 1 1 calc R . .
C5 C 1.07000(19) 1.4064(6) 0.65503(17) 0.0617(8) Uani 1 1 d . . .
H5 H 1.0975 1.5293 0.6851 0.074 Uiso 1 1 calc R . .
C6 C 1.01143(17) 1.2420(5) 0.68194(15) 0.0595(8) Uani 1 1 d . . .
H6 H 1.0009 1.2570 0.7287 0.071 Uiso 1 1 calc R . .
C7 C 0.97070(17) 1.0614(5) 0.63822(14) 0.0515(7) Uani 1 1 d . . .
C8 C 0.90696(17) 0.8645(5) 0.64655(15) 0.0524(7) Uani 1 1 d . . .
C9 C 0.86696(19) 0.8018(6) 0.70337(16) 0.0633(9) Uani 1 1 d . . .
H9 H 0.8783 0.8912 0.7459 0.076 Uiso 1 1 calc R . .
C10 C 0.8092(2) 0.6024(6) 0.69636(18) 0.0680(9) Uani 1 1 d . . .
H10 H 0.7816 0.5588 0.7346 0.082 Uiso 1 1 calc R . .
C11 C 0.79223(19) 0.4689(6) 0.63428(18) 0.0689(9) Uani 1 1 d . . .
H11 H 0.7538 0.3344 0.6311 0.083 Uiso 1 1 calc R . .
C12 C 0.83183(18) 0.5317(5) 0.57539(16) 0.0620(8) Uani 1 1 d . . .
H12 H 0.8199 0.4414 0.5331 0.074 Uiso 1 1 calc R . .
C13 C 0.88922(16) 0.7317(5) 0.58158(15) 0.0528(7) Uani 1 1 d . . .
C14 C 0.55699(18) 0.4640(5) 0.44933(14) 0.0575(8) Uani 1 1 d . . .
C15 C 0.62391(18) 0.3638(5) 0.41112(15) 0.0551(8) Uani 1 1 d . . .
C16 C 0.6493(2) 0.4345(5) 0.34620(18) 0.0710(10) Uani 1 1 d . . .
H16 H 0.6231 0.5678 0.3191 0.085 Uiso 1 1 calc R . .
C17 C 0.7165(2) 0.2962(6) 0.32293(17) 0.0735(9) Uani 1 1 d . . .
H17 H 0.7349 0.3373 0.2800 0.088 Uiso 1 1 calc R . .
C18 C 0.7539(2) 0.1026(6) 0.36414(17) 0.0712(9) Uani 1 1 d . . .
H18 H 0.7982 0.0150 0.3486 0.085 Uiso 1 1 calc R . .
C19 C 0.7290(2) 0.0324(6) 0.42702(17) 0.0717(10) Uani 1 1 d . . .
H19 H 0.7556 -0.1013 0.4537 0.086 Uiso 1 1 calc R . .
C20 C 0.66429(19) 0.1622(5) 0.45015(16) 0.0609(8) Uani 1 1 d . . .
C21 C 0.62311(18) 0.1285(5) 0.51503(15) 0.0588(8) Uani 1 1 d . . .
C22 C 0.6333(2) -0.0345(6) 0.57110(17) 0.0683(10) Uani 1 1 d . . .
H22 H 0.6746 -0.1602 0.5745 0.082 Uiso 1 1 calc R . .
C23 C 0.57973(19) -0.0116(6) 0.62533(16) 0.0673(9) Uani 1 1 d . . .
H23 H 0.5878 -0.1231 0.6640 0.081 Uiso 1 1 calc R . .
C24 C 0.51850(19) 0.1641(5) 0.62249(16) 0.0655(9) Uani 1 1 d . . .
H24 H 0.4849 0.1706 0.6586 0.079 Uiso 1 1 calc R . .
C25 C 0.50429(18) 0.3436(5) 0.56370(14) 0.0550(8) Uani 1 1 d . . .
C26 C 0.55827(16) 0.3167(5) 0.51166(15) 0.0525(8) Uani 1 1 d . . .

loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
C1 0.0468(16) 0.0458(14) 0.0535(16) 0.0016(14) 0.0010(13) 0.0038(12)
C2 0.0497(16) 0.0447(14) 0.0481(16) 0.0001(13) 0.0021(12) 0.0059(11)
C3 0.0456(16) 0.0420(14) 0.0554(17) -0.0017(13) -0.0006(13) 0.0034(11)
C4 0.0588(19) 0.0529(16) 0.0592(18) -0.0043(15) 0.0005(14) -0.0012(13)
C5 0.0587(19) 0.0598(17) 0.0644(19) -0.0143(15) -0.0017(15) -0.0008(13)
C6 0.064(2) 0.0621(17) 0.0517(16) -0.0065(15) 0.0035(14) 0.0079(14)
C7 0.0514(17) 0.0509(15) 0.0516(16) 0.0003(14) 0.0043(13) 0.0082(12)
C8 0.0506(18) 0.0520(15) 0.0543(17) 0.0036(14) 0.0060(13) 0.0086(12)
C9 0.066(2) 0.0652(18) 0.0595(18) 0.0036(16) 0.0108(16) 0.0093(15)
C10 0.064(2) 0.0724(19) 0.070(2) 0.0117(18) 0.0186(16) 0.0024(16)
C11 0.059(2) 0.0628(18) 0.085(2) 0.0135(18) 0.0069(17) -0.0057(14)
C12 0.061(2) 0.0607(17) 0.0633(19) 0.0025(16) 0.0028(15) 0.0001(14)
C13 0.0480(16) 0.0515(15) 0.0583(17) 0.0065(14) 0.0047(13) 0.0058(12)
C14 0.0622(19) 0.0531(16) 0.0554(18) -0.0081(15) -0.0006(14) -0.0091(14)
C15 0.0581(18) 0.0524(16) 0.0534(17) -0.0079(14) 0.0009(14) -0.0049(13)
C16 0.078(2) 0.0553(17) 0.075(2) 0.0005(17) -0.0111(18) -0.0019(15)
C17 0.077(2) 0.078(2) 0.066(2) -0.0027(18) 0.0132(18) -0.0034(18)
C18 0.068(2) 0.074(2) 0.071(2) -0.0076(19) 0.0097(17) 0.0093(16)
C19 0.076(2) 0.0650(19) 0.071(2) -0.0039(18) -0.0015(18) 0.0068(17)
C20 0.064(2) 0.0549(16) 0.0599(18) -0.0046(15) -0.0079(15) -0.0043(14)
C21 0.068(2) 0.0483(15) 0.0565(18) -0.0017(15) -0.0080(15) -0.0008(13)
C22 0.077(2) 0.0560(18) 0.066(2) 0.0067(16) -0.0138(17) 0.0014(14)
C23 0.078(2) 0.0612(17) 0.0596(19) 0.0098(16) -0.0048(17) -0.0001(16)
C24 0.074(2) 0.0577(17) 0.0619(18) 0.0003(16) -0.0035(16) -0.0006(14)
C25 0.068(2) 0.0452(15) 0.0481(16) 0.0031(14) -0.0071(14) -0.0086(13)
C26 0.0542(18) 0.0416(14) 0.0581(17) -0.0033(14) -0.0074(14) -0.0009(12)

_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C3 1.403(4) 3_776 ?
C1 C2 1.413(3) . ?
C1 C13 1.474(4) . ?
C2 C7 1.413(4) . ?
C2 C3 1.418(4) . ?
C3 C1 1.403(4) 3_776 ?
C3 C4 1.443(4) . ?
C4 C5 1.349(4) . ?
C4 H4 0.9300 . ?
C5 C6 1.417(4) . ?
C5 H5 0.9300 . ?
C6 C7 1.365(4) . ?
C6 H6 0.9300 . ?
C7 C8 1.473(4) . ?
C8 C9 1.369(4) . ?
C8 C13 1.412(4) . ?
C9 C10 1.387(4) . ?
C9 H9 0.9300 . ?
C10 C11 1.367(4) . ?
C10 H10 0.9300 . ?
C11 C12 1.399(4) . ?
C11 H11 0.9300 . ?
C12 C13 1.386(4) . ?
C12 H12 0.9300 . ?
C14 C25 1.406(4) 3_666 ?
C14 C26 1.407(4) . ?
C14 C15 1.476(4) . ?
C15 C20 1.393(4) . ?
C15 C16 1.400(4) . ?
C16 C17 1.422(5) . ?
C16 H16 0.9300 . ?
C17 C18 1.365(4) . ?
C17 H17 0.9300 . ?
C18 C19 1.360(4) . ?
C18 H18 0.9300 . ?
C19 C20 1.366(4) . ?
C19 H19 0.9300 . ?
C20 C21 1.487(4) . ?
C21 C22 1.353(4) . ?
C21 C26 1.429(4) . ?
C22 C23 1.437(4) . ?
C22 H22 0.9300 . ?
C23 C24 1.342(4) . ?
C23 H23 0.9300 . ?
C24 C25 1.449(4) . ?
C24 H24 0.9300 . ?
C25 C14 1.406(4) 3_666 ?
C25 C26 1.410(4) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C3 C1 C2 117.9(2) 3_776 . ?
C3 C1 C13 135.7(2) 3_776 . ?
C2 C1 C13 106.4(2) . . ?
C1 C2 C7 110.9(3) . . ?
C1 C2 C3 126.0(2) . . ?
C7 C2 C3 123.0(2) . . ?
C1 C3 C2 116.1(2) 3_776 . ?
C1 C3 C4 128.4(3) 3_776 . ?
C2 C3 C4 115.5(2) . . ?
C5 C4 C3 120.4(3) . . ?
C5 C4 H4 119.8 . . ?
C3 C4 H4 119.8 . . ?
C4 C5 C6 122.9(3) . . ?
C4 C5 H5 118.5 . . ?
C6 C5 H5 118.5 . . ?
C7 C6 C5 119.0(3) . . ?
C7 C6 H6 120.5 . . ?
C5 C6 H6 120.5 . . ?
C6 C7 C2 119.1(3) . . ?
C6 C7 C8 134.3(3) . . ?
C2 C7 C8 106.5(2) . . ?
C9 C8 C13 120.9(3) . . ?
C9 C8 C7 131.1(3) . . ?
C13 C8 C7 108.0(3) . . ?
C8 C9 C10 118.7(3) . . ?
C8 C9 H9 120.6 . . ?
C10 C9 H9 120.6 . . ?
C11 C10 C9 121.2(3) . . ?
C11 C10 H10 119.4 . . ?
C9 C10 H10 119.4 . . ?
C10 C11 C12 120.9(3) . . ?
C10 C11 H11 119.5 . . ?
C12 C11 H11 119.5 . . ?
C13 C12 C11 118.4(3) . . ?
C13 C12 H12 120.8 . . ?
C11 C12 H12 120.8 . . ?
C12 C13 C8 119.8(3) . . ?
C12 C13 C1 132.0(3) . . ?
C8 C13 C1 108.2(2) . . ?
C25 C14 C26 117.7(3) 3_666 . ?
C25 C14 C15 135.2(3) 3_666 . ?
C26 C14 C15 107.0(2) . . ?
C20 C15 C16 119.6(3) . . ?
C20 C15 C14 109.0(3) . . ?
C16 C15 C14 131.4(3) . . ?
C15 C16 C17 117.9(3) . . ?
C15 C16 H16 121.1 . . ?
C17 C16 H16 121.0 . . ?
C18 C17 C16 119.5(3) . . ?
C18 C17 H17 120.3 . . ?
C16 C17 H17 120.3 . . ?
C19 C18 C17 122.8(3) . . ?
C19 C18 H18 118.6 . . ?
C17 C18 H18 118.6 . . ?
C18 C19 C20 118.6(3) . . ?
C18 C19 H19 120.7 . . ?
C20 C19 H19 120.7 . . ?
C19 C20 C15 121.6(3) . . ?
C19 C20 C21 131.0(3) . . ?
C15 C20 C21 107.4(3) . . ?
C22 C21 C26 118.3(3) . . ?
C22 C21 C20 134.8(3) . . ?
C26 C21 C20 106.9(2) . . ?
C21 C22 C23 119.4(3) . . ?
C21 C22 H22 120.3 . . ?
C23 C22 H22 120.3 . . ?
C24 C23 C22 122.7(3) . . ?
C24 C23 H23 118.7 . . ?
C22 C23 H23 118.7 . . ?
C23 C24 C25 120.5(3) . . ?
C23 C24 H24 119.7 . . ?
C25 C24 H24 119.7 . . ?
C14 C25 C26 115.8(2) 3_666 . ?
C14 C25 C24 128.9(3) 3_666 . ?
C26 C25 C24 115.3(3) . . ?
C14 C26 C25 126.5(2) . . ?
C14 C26 C21 109.7(3) . . ?
C25 C26 C21 123.8(3) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C3 C1 C2 C7 -179.6(2) 3_776 . . . ?
C13 C1 C2 C7 0.6(3) . . . . ?
C3 C1 C2 C3 -0.3(4) 3_776 . . . ?
C13 C1 C2 C3 180.0(2) . . . . ?
C1 C2 C3 C1 0.3(4) . . . 3_776 ?
C7 C2 C3 C1 179.6(2) . . . 3_776 ?
C1 C2 C3 C4 179.6(2) . . . . ?
C7 C2 C3 C4 -1.1(3) . . . . ?
C1 C3 C4 C5 -179.2(3) 3_776 . . . ?
C2 C3 C4 C5 1.6(4) . . . . ?
C3 C4 C5 C6 -1.0(4) . . . . ?
C4 C5 C6 C7 -0.1(4) . . . . ?
C5 C6 C7 C2 0.6(4) . . . . ?
C5 C6 C7 C8 -179.2(3) . . . . ?
C1 C2 C7 C6 179.4(2) . . . . ?
C3 C2 C7 C6 0.0(4) . . . . ?
C1 C2 C7 C8 -0.7(3) . . . . ?
C3 C2 C7 C8 179.9(2) . . . . ?
C6 C7 C8 C9 0.6(5) . . . . ?
C2 C7 C8 C9 -179.2(3) . . . . ?
C6 C7 C8 C13 -179.6(3) . . . . ?
C2 C7 C8 C13 0.5(3) . . . . ?
C13 C8 C9 C10 0.9(4) . . . . ?
C7 C8 C9 C10 -179.4(3) . . . . ?
C8 C9 C10 C11 0.2(4) . . . . ?
C9 C10 C11 C12 -0.9(5) . . . . ?
C10 C11 C12 C13 0.4(4) . . . . ?
C11 C12 C13 C8 0.7(4) . . . . ?
C11 C12 C13 C1 179.4(3) . . . . ?
C9 C8 C13 C12 -1.3(4) . . . . ?
C7 C8 C13 C12 178.9(2) . . . . ?
C9 C8 C13 C1 179.6(2) . . . . ?
C7 C8 C13 C1 -0.2(3) . . . . ?
C3 C1 C13 C12 1.2(5) 3_776 . . . ?
C2 C1 C13 C12 -179.1(3) . . . . ?
C3 C1 C13 C8 -179.9(3) 3_776 . . . ?
C2 C1 C13 C8 -0.2(3) . . . . ?
C25 C14 C15 C20 -178.3(3) 3_666 . . . ?
C26 C14 C15 C20 -0.3(3) . . . . ?
C25 C14 C15 C16 0.6(5) 3_666 . . . ?
C26 C14 C15 C16 178.6(3) . . . . ?
C20 C15 C16 C17 -0.4(4) . . . . ?
C14 C15 C16 C17 -179.2(3) . . . . ?
C15 C16 C17 C18 -0.3(4) . . . . ?
C16 C17 C18 C19 0.7(5) . . . . ?
C17 C18 C19 C20 -0.4(5) . . . . ?
C18 C19 C20 C15 -0.3(4) . . . . ?
C18 C19 C20 C21 179.2(3) . . . . ?
C16 C15 C20 C19 0.7(4) . . . . ?
C14 C15 C20 C19 179.8(3) . . . . ?
C16 C15 C20 C21 -178.9(2) . . . . ?
C14 C15 C20 C21 0.2(3) . . . . ?
C19 C20 C21 C22 -0.8(5) . . . . ?
C15 C20 C21 C22 178.7(3) . . . . ?
C19 C20 C21 C26 -179.5(3) . . . . ?
C15 C20 C21 C26 0.0(3) . . . . ?
C26 C21 C22 C23 -0.7(4) . . . . ?
C20 C21 C22 C23 -179.2(3) . . . . ?
C21 C22 C23 C24 0.9(4) . . . . ?
C22 C23 C24 C25 -0.7(4) . . . . ?
C23 C24 C25 C14 178.6(3) . . . 3_666 ?
C23 C24 C25 C26 0.3(4) . . . . ?
C25 C14 C26 C25 -0.7(4) 3_666 . . . ?
C15 C14 C26 C25 -179.1(2) . . . . ?
C25 C14 C26 C21 178.7(2) 3_666 . . . ?
C15 C14 C26 C21 0.3(3) . . . . ?
C14 C25 C26 C14 0.7(4) 3_666 . . . ?
C24 C25 C26 C14 179.2(2) . . . . ?
C14 C25 C26 C21 -178.7(2) 3_666 . . . ?
C24 C25 C26 C21 -0.1(4) . . . . ?
C22 C21 C26 C14 -179.1(2) . . . . ?
C20 C21 C26 C14 -0.2(3) . . . . ?
C22 C21 C26 C25 0.3(4) . . . . ?
C20 C21 C26 C25 179.3(2) . . . . ?

_diffrn_measured_fraction_theta_max 0.884
_diffrn_reflns_theta_full        57.96
_diffrn_measured_fraction_theta_full 0.884
_refine_diff_density_max         0.357
_refine_diff_density_min         -0.162
_refine_diff_density_rms         0.048
_database_code_depnum_ccdc_archive 'CCDC 969284'