# Electronic Supplementary Material (ESI) for Journal of Materials Chemistry C.
# This journal is © The Royal Society of Chemistry 2015

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_q1
_database_code_depnum_ccdc_archive 'CCDC 966679'
_audit_update_record             
;
2013-10-16 deposited with the CCDC.
2015-01-21 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        
; 
 ? 
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         ?
_chemical_formula_sum            'C34 H26 F8 N2 O4 Pt2'
_chemical_formula_weight         1068.75

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           Triclinic
_symmetry_space_group_name_H-M   'P-1   '

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   11.7020(6)
_cell_length_b                   12.4402(7)
_cell_length_c                   12.7534(7)
_cell_angle_alpha                89.883(3)
_cell_angle_beta                 82.150(3)
_cell_angle_gamma                65.050(3)
_cell_volume                     1664.35(16)
_cell_formula_units_Z            2
_cell_measurement_temperature    296(2)
_cell_measurement_reflns_used    6084
_cell_measurement_theta_min      2.35
_cell_measurement_theta_max      27.42

_exptl_crystal_description       cuboid
_exptl_crystal_colour            yellow
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.15
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    2.133
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1008
_exptl_absorpt_coefficient_mu    8.482
_exptl_absorpt_correction_type   'multi scan'
_exptl_absorpt_correction_T_min  0.3674
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_process_details   'SADABS (Sheldrick, 1996)'

_exptl_special_details           
; 
 ? 
;

_diffrn_ambient_temperature      296(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            11633
_diffrn_reflns_av_R_equivalents  0.0323
_diffrn_reflns_av_sigmaI/netI    0.0461
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_l_min       -8
_diffrn_reflns_limit_l_max       15
_diffrn_reflns_theta_min         1.61
_diffrn_reflns_theta_max         25.00
_reflns_number_total             5814
_reflns_number_gt                4954
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'Bruker SMART'
_computing_cell_refinement       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'

_refine_special_details          
; 
 Refinement of F² against ALL reflections.  The weighted R-factor wR and 
 goodness of fit S are based on F², conventional R-factors R are based 
 on F, with F set to zero for negative F². The threshold expression of 
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is 
 not relevant to the choice of reflections for refinement.  R-factors based 
 on F² are statistically about twice as large as those based on F, and R- 
 factors based on ALL data will be even larger. 
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[σ²(Fo²)+(0.0508P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   geom
_refine_ls_hydrogen_treatment    constr
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         5814
_refine_ls_number_parameters     451
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0410
_refine_ls_R_factor_gt           0.0342
_refine_ls_wR_factor_ref         0.0913
_refine_ls_wR_factor_gt          0.0885
_refine_ls_goodness_of_fit_ref   1.059
_refine_ls_restrained_S_all      1.059
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.52239(2) 0.91637(2) 1.129160(17) 0.04068(10) Uani 1 1 d . . .
Pt2 Pt 0.54530(2) 0.57127(2) 0.618712(17) 0.04156(10) Uani 1 1 d . . .
N1 N 0.4064(5) 0.6746(4) 0.5399(4) 0.0431(12) Uani 1 1 d . . .
O4 O 0.3987(4) 1.0159(4) 1.2517(3) 0.0512(10) Uani 1 1 d . . .
O2 O 0.6978(4) 0.4698(4) 0.6844(3) 0.0515(11) Uani 1 1 d . . .
C23 C 0.4367(7) 0.8234(5) 0.9690(5) 0.0489(16) Uani 1 1 d . . .
O1 O 0.4214(4) 0.5466(4) 0.7394(3) 0.0514(11) Uani 1 1 d . . .
C22 C 0.5728(7) 0.7811(5) 0.9321(4) 0.0458(15) Uani 1 1 d . . .
C24 C 0.3930(6) 0.8912(5) 1.0638(5) 0.0438(14) Uani 1 1 d . . .
C5 C 0.4454(6) 0.7177(5) 0.4491(4) 0.0434(15) Uani 1 1 d . . .
C7 C 0.6518(6) 0.6029(5) 0.4993(4) 0.0444(15) Uani 1 1 d . . .
C6 C 0.5811(7) 0.6782(5) 0.4266(5) 0.0482(15) Uani 1 1 d . . .
C8 C 0.7839(7) 0.5609(6) 0.4817(5) 0.0517(16) Uani 1 1 d . . .
H8A H 0.8331 0.5118 0.5290 0.062 Uiso 1 1 calc R . .
C12 C 0.4585(7) 0.4814(6) 0.8157(5) 0.0504(16) Uani 1 1 d . . .
C1 C 0.2837(7) 0.7012(5) 0.5698(5) 0.0491(15) Uani 1 1 d . . .
H1A H 0.2595 0.6707 0.6312 0.059 Uiso 1 1 calc R . .
C14 C 0.6941(7) 0.4164(6) 0.7705(5) 0.0553(17) Uani 1 1 d . . .
C13 C 0.5853(7) 0.4203(6) 0.8329(5) 0.0563(18) Uani 1 1 d . . .
H13A H 0.5981 0.3773 0.8933 0.068 Uiso 1 1 calc R . .
C18 C 0.7581(7) 0.7799(6) 0.9837(5) 0.0530(16) Uani 1 1 d . . .
H18A H 0.7968 0.8047 1.0315 0.064 Uiso 1 1 calc R . .
C31 C 0.6620(7) 0.9908(6) 1.2701(5) 0.0502(16) Uani 1 1 d . . .
C30 C 0.5470(8) 1.0528(7) 1.3395(6) 0.0602(19) Uani 1 1 d . . .
H30A H 0.5522 1.0929 1.3988 0.072 Uiso 1 1 calc R . .
C29 C 0.4276(7) 1.0610(6) 1.3296(5) 0.0517(17) Uani 1 1 d . . .
C19 C 0.8321(7) 0.7083(7) 0.8960(6) 0.0635(19) Uani 1 1 d . . .
C25 C 0.2637(7) 0.9331(7) 1.1046(6) 0.0609(19) Uani 1 1 d . . .
H25A H 0.2301 0.9796 1.1679 0.073 Uiso 1 1 calc R . .
C4 C 0.3525(8) 0.7908(7) 0.3910(6) 0.061(2) Uani 1 1 d . . .
H4A H 0.3773 0.8208 0.3295 0.073 Uiso 1 1 calc R . .
C2 C 0.1911(7) 0.7729(6) 0.5122(5) 0.0570(17) Uani 1 1 d . . .
C3 C 0.2273(7) 0.8194(7) 0.4215(6) 0.0604(19) Uani 1 1 d . . .
H3A H 0.1665 0.8693 0.3823 0.072 Uiso 1 1 calc R . .
C28 C 0.3544(9) 0.7957(7) 0.9116(6) 0.060(2) Uani 1 1 d . . .
H28A H 0.3858 0.7503 0.8476 0.073 Uiso 1 1 calc R . .
C21 C 0.6451(8) 0.7111(7) 0.8427(6) 0.061(2) Uani 1 1 d . . .
H21A H 0.6053 0.6895 0.7937 0.073 Uiso 1 1 calc R . .
C11 C 0.6401(7) 0.7100(6) 0.3385(5) 0.0512(17) Uani 1 1 d . . .
H11A H 0.5921 0.7586 0.2903 0.061 Uiso 1 1 calc R . .
C26 C 0.1870(7) 0.9034(7) 1.0479(6) 0.0636(19) Uani 1 1 d . . .
C27 C 0.2284(9) 0.8380(8) 0.9538(7) 0.073(2) Uani 1 1 d . . .
H27A H 0.1719 0.8223 0.9188 0.088 Uiso 1 1 calc R . .
C20 C 0.7736(9) 0.6730(7) 0.8247(6) 0.068(2) Uani 1 1 d . . .
H20A H 0.8218 0.6237 0.7651 0.082 Uiso 1 1 calc R . .
C10 C 0.7715(9) 0.6687(7) 0.3230(6) 0.067(2) Uani 1 1 d . . .
H10A H 0.8129 0.6915 0.2658 0.080 Uiso 1 1 calc R . .
F4 F 0.9693(4) 0.5506(5) 0.3765(3) 0.0837(13) Uani 1 1 d . . .
F1 F 0.0320(6) 0.7203(6) 0.5919(6) 0.141(3) Uani 1 1 d . . .
F2 F 0.0016(7) 0.8882(7) 0.6171(9) 0.199(5) Uani 1 1 d . . .
C17 C 0.0557(8) 0.8023(8) 0.5489(8) 0.077(2) Uani 1 1 d . . .
F3 F -0.0127(7) 0.8333(12) 0.4750(6) 0.233(6) Uani 1 1 d . . .
N2 N 0.6340(5) 0.8146(4) 1.0021(4) 0.0426(12) Uani 1 1 d . . .
C15 C 0.3550(8) 0.4735(8) 0.8934(6) 0.071(2) Uani 1 1 d . . .
H15A H 0.2740 0.5194 0.8712 0.106 Uiso 1 1 calc R . .
H15B H 0.3562 0.5040 0.9622 0.106 Uiso 1 1 calc R . .
H15C H 0.3683 0.3921 0.8969 0.106 Uiso 1 1 calc R . .
C16 C 0.8217(8) 0.3476(7) 0.8036(6) 0.078(2) Uani 1 1 d . . .
H16A H 0.8867 0.3530 0.7520 0.117 Uiso 1 1 calc R . .
H16B H 0.8366 0.2659 0.8088 0.117 Uiso 1 1 calc R . .
H16C H 0.8237 0.3798 0.8714 0.117 Uiso 1 1 calc R . .
C9 C 0.8397(7) 0.5930(6) 0.3940(5) 0.0601(18) Uani 1 1 d . . .
F8 F 0.0605(5) 0.9427(5) 1.0916(4) 0.0955(15) Uani 1 1 d . . .
F5 F 1.0174(6) 0.6645(10) 0.9682(6) 0.181(4) Uani 1 1 d . . .
C34 C 0.9716(10) 0.6644(14) 0.8858(9) 0.111(4) Uani 1 1 d . . .
F6 F 1.0342(7) 0.5708(12) 0.8366(13) 0.289(9) Uani 1 1 d . . .
F7 F 1.0113(9) 0.7282(17) 0.8308(12) 0.295(10) Uani 1 1 d . . .
O3 O 0.6735(4) 0.9318(4) 1.1863(3) 0.0491(10) Uani 1 1 d . . .
C33 C 0.7816(7) 0.9892(8) 1.2988(6) 0.074(2) Uani 1 1 d . . .
H33A H 0.8517 0.9438 1.2448 0.111 Uiso 1 1 calc R . .
H33B H 0.7967 0.9538 1.3654 0.111 Uiso 1 1 calc R . .
H33C H 0.7737 1.0691 1.3046 0.111 Uiso 1 1 calc R . .
C32 C 0.3139(8) 1.1294(8) 1.4119(6) 0.078(3) Uani 1 1 d . . .
H32A H 0.2397 1.1252 1.3920 0.117 Uiso 1 1 calc R . .
H32B H 0.3007 1.2110 1.4170 0.117 Uiso 1 1 calc R . .
H32C H 0.3289 1.0959 1.4794 0.117 Uiso 1 1 calc R . .


_geom_special_details            
; 
 All esds (except the esd in the dihedral angle between two l.s. planes) 
 are estimated using the full covariance matrix.  The cell esds are taken 
 into account individually in the estimation of esds in distances, angles 
 and torsion angles; correlations between esds in cell parameters are only 
 used when they are defined by crystal symmetry.  An approximate (isotropic) 
 treatment of cell esds is used for estimating esds involving l.s. planes. 
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C24 1.957(6) . ?
Pt1 N2 1.992(5) . ?
Pt1 O4 1.987(4) . ?
Pt1 O3 2.082(4) . ?
Pt2 C7 1.980(6) . ?
Pt2 O2 1.996(4) . ?
Pt2 N1 1.995(5) . ?
Pt2 O1 2.080(4) . ?
N1 C1 1.329(8) . ?
N1 C5 1.377(7) . ?
O4 C29 1.292(8) . ?
O2 C14 1.287(7) . ?
C23 C24 1.381(9) . ?
C23 C28 1.435(9) . ?
C23 C22 1.457(9) . ?
O1 C12 1.269(7) . ?
C22 C21 1.377(10) . ?
C22 N2 1.382(7) . ?
C24 C25 1.397(10) . ?
C5 C4 1.393(9) . ?
C5 C6 1.437(9) . ?
C7 C8 1.391(9) . ?
C7 C6 1.406(8) . ?
C6 C11 1.382(9) . ?
C8 C9 1.363(9) . ?
C8 H8A 0.9300 . ?
C12 C13 1.402(10) . ?
C12 C15 1.493(10) . ?
C1 C2 1.382(9) . ?
C1 H1A 0.9300 . ?
C14 C13 1.388(10) . ?
C14 C16 1.495(10) . ?
C13 H13A 0.9300 . ?
C18 N2 1.315(8) . ?
C18 C19 1.373(9) . ?
C18 H18A 0.9300 . ?
C31 O3 1.256(7) . ?
C31 C30 1.411(10) . ?
C31 C33 1.487(9) . ?
C30 C29 1.381(10) . ?
C30 H30A 0.9300 . ?
C29 C32 1.504(10) . ?
C19 C20 1.384(10) . ?
C19 C34 1.473(12) . ?
C25 C26 1.387(10) . ?
C25 H25A 0.9300 . ?
C4 C3 1.353(11) . ?
C4 H4A 0.9300 . ?
C2 C3 1.386(10) . ?
C2 C17 1.474(11) . ?
C3 H3A 0.9300 . ?
C28 C27 1.368(12) . ?
C28 H28A 0.9300 . ?
C21 C20 1.358(11) . ?
C21 H21A 0.9300 . ?
C11 C10 1.385(11) . ?
C11 H11A 0.9300 . ?
C26 F8 1.381(8) . ?
C26 C27 1.360(11) . ?
C27 H27A 0.9300 . ?
C20 H20A 0.9300 . ?
C10 C9 1.380(10) . ?
C10 H10A 0.9300 . ?
F4 C9 1.365(8) . ?
F1 C17 1.270(10) . ?
F2 C17 1.258(11) . ?
C17 F3 1.275(10) . ?
C15 H15A 0.9600 . ?
C15 H15B 0.9600 . ?
C15 H15C 0.9600 . ?
C16 H16A 0.9600 . ?
C16 H16B 0.9600 . ?
C16 H16C 0.9600 . ?
F5 C34 1.243(12) . ?
C34 F6 1.202(13) . ?
C34 F7 1.247(17) . ?
C33 H33A 0.9600 . ?
C33 H33B 0.9600 . ?
C33 H33C 0.9600 . ?
C32 H32A 0.9600 . ?
C32 H32B 0.9600 . ?
C32 H32C 0.9600 . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C24 Pt1 N2 81.2(2) . . ?
C24 Pt1 O4 93.8(2) . . ?
N2 Pt1 O4 175.03(19) . . ?
C24 Pt1 O3 174.2(2) . . ?
N2 Pt1 O3 93.00(18) . . ?
O4 Pt1 O3 91.96(17) . . ?
C7 Pt2 O2 92.0(2) . . ?
C7 Pt2 N1 81.6(2) . . ?
O2 Pt2 N1 173.60(19) . . ?
C7 Pt2 O1 175.7(2) . . ?
O2 Pt2 O1 92.26(17) . . ?
N1 Pt2 O1 94.13(19) . . ?
C1 N1 C5 120.5(5) . . ?
C1 N1 Pt2 124.0(4) . . ?
C5 N1 Pt2 115.5(4) . . ?
C29 O4 Pt1 125.0(4) . . ?
C14 O2 Pt2 124.7(5) . . ?
C24 C23 C28 122.4(7) . . ?
C24 C23 C22 115.1(5) . . ?
C28 C23 C22 122.4(6) . . ?
C12 O1 Pt2 123.5(4) . . ?
C21 C22 N2 118.2(7) . . ?
C21 C22 C23 129.3(6) . . ?
N2 C22 C23 112.4(5) . . ?
C23 C24 C25 118.0(6) . . ?
C23 C24 Pt1 115.5(5) . . ?
C25 C24 Pt1 126.5(5) . . ?
N1 C5 C4 118.1(6) . . ?
N1 C5 C6 113.5(5) . . ?
C4 C5 C6 128.4(6) . . ?
C8 C7 C6 118.6(6) . . ?
C8 C7 Pt2 127.7(4) . . ?
C6 C7 Pt2 113.6(5) . . ?
C11 C6 C7 121.4(6) . . ?
C11 C6 C5 122.9(6) . . ?
C7 C6 C5 115.7(6) . . ?
C9 C8 C7 118.8(6) . . ?
C9 C8 H8A 120.6 . . ?
C7 C8 H8A 120.6 . . ?
O1 C12 C13 125.6(6) . . ?
O1 C12 C15 115.4(7) . . ?
C13 C12 C15 119.0(6) . . ?
N1 C1 C2 121.8(6) . . ?
N1 C1 H1A 119.1 . . ?
C2 C1 H1A 119.1 . . ?
O2 C14 C13 126.2(6) . . ?
O2 C14 C16 114.1(7) . . ?
C13 C14 C16 119.7(6) . . ?
C12 C13 C14 127.7(6) . . ?
C12 C13 H13A 116.1 . . ?
C14 C13 H13A 116.1 . . ?
N2 C18 C19 121.9(6) . . ?
N2 C18 H18A 119.1 . . ?
C19 C18 H18A 119.1 . . ?
O3 C31 C30 125.3(6) . . ?
O3 C31 C33 116.0(6) . . ?
C30 C31 C33 118.6(6) . . ?
C29 C30 C31 127.6(6) . . ?
C29 C30 H30A 116.2 . . ?
C31 C30 H30A 116.2 . . ?
O4 C29 C30 126.1(6) . . ?
O4 C29 C32 112.7(7) . . ?
C30 C29 C32 121.2(6) . . ?
C18 C19 C20 118.7(7) . . ?
C18 C19 C34 118.6(7) . . ?
C20 C19 C34 122.5(8) . . ?
C26 C25 C24 118.1(7) . . ?
C26 C25 H25A 120.9 . . ?
C24 C25 H25A 120.9 . . ?
C3 C4 C5 121.7(7) . . ?
C3 C4 H4A 119.1 . . ?
C5 C4 H4A 119.1 . . ?
C1 C2 C3 119.0(7) . . ?
C1 C2 C17 120.2(7) . . ?
C3 C2 C17 120.7(7) . . ?
C4 C3 C2 118.9(7) . . ?
C4 C3 H3A 120.6 . . ?
C2 C3 H3A 120.6 . . ?
C27 C28 C23 118.0(7) . . ?
C27 C28 H28A 121.0 . . ?
C23 C28 H28A 121.0 . . ?
C22 C21 C20 121.1(7) . . ?
C22 C21 H21A 119.4 . . ?
C20 C21 H21A 119.4 . . ?
C10 C11 C6 119.2(6) . . ?
C10 C11 H11A 120.4 . . ?
C6 C11 H11A 120.4 . . ?
F8 C26 C27 118.5(7) . . ?
F8 C26 C25 117.0(7) . . ?
C27 C26 C25 124.5(8) . . ?
C26 C27 C28 118.9(7) . . ?
C26 C27 H27A 120.5 . . ?
C28 C27 H27A 120.5 . . ?
C21 C20 C19 119.3(7) . . ?
C21 C20 H20A 120.4 . . ?
C19 C20 H20A 120.4 . . ?
C11 C10 C9 118.6(7) . . ?
C11 C10 H10A 120.7 . . ?
C9 C10 H10A 120.7 . . ?
F2 C17 F3 103.7(10) . . ?
F2 C17 F1 103.5(9) . . ?
F3 C17 F1 104.7(9) . . ?
F2 C17 C2 114.3(8) . . ?
F3 C17 C2 113.2(8) . . ?
F1 C17 C2 116.2(7) . . ?
C18 N2 C22 120.8(6) . . ?
C18 N2 Pt1 123.5(4) . . ?
C22 N2 Pt1 115.7(4) . . ?
C12 C15 H15A 109.5 . . ?
C12 C15 H15B 109.5 . . ?
H15A C15 H15B 109.5 . . ?
C12 C15 H15C 109.5 . . ?
H15A C15 H15C 109.5 . . ?
H15B C15 H15C 109.5 . . ?
C14 C16 H16A 109.5 . . ?
C14 C16 H16B 109.5 . . ?
H16A C16 H16B 109.5 . . ?
C14 C16 H16C 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
F4 C9 C8 118.6(6) . . ?
F4 C9 C10 118.2(7) . . ?
C8 C9 C10 123.3(7) . . ?
F6 C34 F5 108.5(14) . . ?
F6 C34 F7 99.1(11) . . ?
F5 C34 F7 100.9(14) . . ?
F6 C34 C19 116.5(11) . . ?
F5 C34 C19 117.2(8) . . ?
F7 C34 C19 112.1(13) . . ?
C31 O3 Pt1 124.0(4) . . ?
C31 C33 H33A 109.5 . . ?
C31 C33 H33B 109.5 . . ?
H33A C33 H33B 109.5 . . ?
C31 C33 H33C 109.5 . . ?
H33A C33 H33C 109.5 . . ?
H33B C33 H33C 109.5 . . ?
C29 C32 H32A 109.5 . . ?
C29 C32 H32B 109.5 . . ?
H32A C32 H32B 109.5 . . ?
C29 C32 H32C 109.5 . . ?
H32A C32 H32C 109.5 . . ?
H32B C32 H32C 109.5 . . ?

_diffrn_measured_fraction_theta_max 0.992
_diffrn_reflns_theta_full        25.00
_diffrn_measured_fraction_theta_full 0.992
_refine_diff_density_max         2.223
_refine_diff_density_min         -0.844
_refine_diff_density_rms         0.153
