# Electronic Supplementary Material (ESI) for Journal of Materials Chemistry C.
# This journal is © The Royal Society of Chemistry 2015

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_a
_database_code_depnum_ccdc_archive 'CCDC 1021114'
_audit_update_record             
;
2014-08-26 deposited with the CCDC.
2015-01-20 downloaded from the CCDC.
;

_audit_creation_method           SHELXL-2013
_chemical_name_systematic        
;
 ?
;
_chemical_name_common            ?
_chemical_melting_point          ?
_chemical_formula_moiety         'C52 B6 Co F3 N7 O2'
_chemical_formula_sum            'C52 B6 Co F3 N7 O2'
_chemical_formula_weight         935.38

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_space_group_crystal_system      monoclinic
_space_group_IT_number           13
_space_group_name_H-M_alt        'P 2/n'
_space_group_name_Hall           '-P 2yac'

_shelx_space_group_comment       
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;

loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y, -z+1/2'
'-x, -y, -z'
'x-1/2, -y, z-1/2'

_cell_length_a                   17.1066(13)
_cell_length_b                   9.3515(7)
_cell_length_c                   21.8195(16)
_cell_angle_alpha                90
_cell_angle_beta                 107.6370(10)
_cell_angle_gamma                90
_cell_volume                     3326.4(4)
_cell_formula_units_Z            4
_cell_measurement_temperature    296(2)
_cell_measurement_reflns_used    ?
_cell_measurement_theta_min      ?
_cell_measurement_theta_max      ?

_exptl_crystal_description       needle-like
_exptl_crystal_colour            'dark brown'
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    ?
_exptl_crystal_density_diffrn    1.868
_exptl_crystal_F_000             1844
_exptl_transmission_factor_min   ?
_exptl_transmission_factor_max   ?
_exptl_crystal_size_max          ?
_exptl_crystal_size_mid          ?
_exptl_crystal_size_min          ?
_exptl_absorpt_coefficient_mu    0.602
_shelx_estimated_absorpt_T_min   ?
_shelx_estimated_absorpt_T_max   ?
_exptl_absorpt_correction_type   ?
_exptl_absorpt_correction_T_min  ?
_exptl_absorpt_correction_T_max  ?
_exptl_absorpt_process_details   ?

_exptl_special_details           
;
 ?
;

_diffrn_ambient_temperature      296(2)
_diffrn_radiation_wavelength     0.71073
_diffrn_radiation_type           MoK\a
_diffrn_source                   ?
_diffrn_measurement_device_type  ?
_diffrn_measurement_method       ?
_diffrn_detector_area_resol_mean ?
_diffrn_reflns_number            44547
_diffrn_reflns_av_unetI/netI     0.0512
_diffrn_reflns_av_R_equivalents  0.0670
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_theta_min         1.333
_diffrn_reflns_theta_max         28.384
_diffrn_reflns_theta_full        25.242
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measured_fraction_theta_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.997
_diffrn_reflns_point_group_measured_fraction_full 1.000
_reflns_number_total             8316
_reflns_number_gt                5836
_reflns_threshold_expression     'I > 2σ(I)'
_reflns_Friedel_coverage         0.000
_reflns_Friedel_fraction_max     .
_reflns_Friedel_fraction_full    .

_reflns_special_details          
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;

_computing_data_collection       ?
_computing_cell_refinement       ?
_computing_data_reduction        ?
_computing_structure_solution    ?
_computing_structure_refinement  'SHELXL-2013 (Sheldrick, 2013)'
_computing_molecular_graphics    ?
_computing_publication_material  ?

_refine_special_details          
;
 ?
;
_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
;
 w=1/[σ²(Fo²)+(0.1000P)²]
 where P=(Fo²+2Fc²)/3
;
_atom_sites_solution_primary     ?
_atom_sites_solution_secondary   ?
_atom_sites_solution_hydrogens   .
_refine_ls_hydrogen_treatment    undef
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       .
_refine_ls_number_reflns         8316
_refine_ls_number_parameters     640
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.3321
_refine_ls_R_factor_gt           0.2929
_refine_ls_wR_factor_ref         0.6942
_refine_ls_wR_factor_gt          0.6757
_refine_ls_goodness_of_fit_ref   5.398
_refine_ls_restrained_S_all      5.398
_refine_ls_shift/su_max          3.179
_refine_ls_shift/su_mean         0.424

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Co1 Co 0.78532(15) 0.7358(2) 0.79559(11) 0.0239(8) Uani 1 1 d . . . . .
F1 F 0.7757(10) 0.6251(16) 0.8396(7) 0.076(4) Uani 1 1 d . . . . .
F2 F 1.0430(11) 0.8838(18) 1.0218(8) 0.100(5) Uani 1 1 d . . . . .
F3 F 1.1173(14) 0.7288(18) 0.9928(9) 0.096(6) Uani 1 1 d . . . . .
O1S O 1.2274(17) 0.766(3) 1.1968(13) 0.123(10) Uani 1 1 d . . . . .
O1 O 0.7092(16) 1.067(3) 0.6380(10) 0.092(7) Uani 1 1 d . . . . .
N1 N 0.8364(10) 0.6256(16) 0.9179(9) 0.045(4) Uani 1 1 d . . . . .
N2 N 0.9130(9) 0.8133(16) 0.8972(8) 0.032(4) Uani 1 1 d . . . . .
N3 N 0.8661(12) 0.9132(19) 0.7832(11) 0.067(6) Uani 1 1 d . . . . .
N4 N 0.8089(8) 0.9042(14) 0.7135(5) 0.020(3) Uani 1 1 d . . . . .
N5 N 0.6623(8) 0.5588(13) 0.7489(5) 0.018(3) Uani 1 1 d . . . . .
N6 N 0.9094(14) 0.951(3) 0.5836(10) 0.061(6) Uani 1 1 d . . . . .
N7 N 0.8308(13) 1.0552(19) 0.0831(9) 0.048(4) Uani 1 1 d . . . . .
C1 C 0.7091(13) 0.537(2) 0.8149(10) 0.051(5) Uani 1 1 d . . . . .
C2 C 0.8925(16) 0.707(3) 0.9173(11) 0.054(6) Uani 1 1 d . . . . .
C3 C 0.8961(11) 0.6006(19) 0.9885(7) 0.032(4) Uani 1 1 d . . . . .
C4 C 1.050(2) 0.650(3) 1.0560(14) 0.068(8) Uani 1 1 d . . . . .
C5 C 1.1061(13) 0.793(3) 1.0485(9) 0.042(5) Uani 1 1 d . . . . .
C6 C 0.8544(18) 1.064(3) -0.0430(14) 0.076(8) Uani 1 1 d . . . . .
C7 C 0.9766(11) 0.809(2) 0.9676(7) 0.029(4) Uani 1 1 d . . . . .
C8 C 0.9253(12) 0.918(2) 0.8570(9) 0.035(4) Uani 1 1 d . . . . .
C9 C 0.8870(13) 1.007(2) 0.7540(11) 0.045(5) Uani 1 1 d . . . . .
C10 C 0.5950(9) 0.4616(17) 0.7174(8) 0.022(3) Uani 1 1 d . . . . .
C11 C 0.5147(11) 0.5473(19) 0.6863(9) 0.029(4) Uani 1 1 d . . . . .
C12 C 0.4476(13) 0.449(2) 0.6501(10) 0.040(5) Uani 1 1 d . . . . .
C13 C 0.5173(13) 0.449(2) 0.7361(10) 0.042(5) Uani 1 1 d . . . . .
C14 C 0.4441(13) 0.537(2) 0.7007(10) 0.042(5) Uani 1 1 d . . . . .
C15 C 0.3716(14) 0.447(3) 0.6576(10) 0.048(5) Uani 1 1 d . . . . .
C16 C 0.2999(13) 0.543(2) 0.6159(10) 0.042(5) Uani 1 1 d . . . . .
C17 C 0.2363(13) 0.538(2) 0.5272(9) 0.038(5) Uani 1 1 d . . . . .
C18 C 0.1647(13) 0.454(2) 0.4788(9) 0.036(4) Uani 1 1 d . . . . .
C19 C 0.0963(12) 0.550(2) 0.4384(9) 0.033(4) Uani 1 1 d . . . . .
C20 C 0.0272(13) 0.464(2) 0.3903(10) 0.041(5) Uani 1 1 d . . . . .
C21 C 0.0288(16) 0.548(3) 0.4374(11) 0.050(5) Uani 1 1 d . . . . .
C22 C 0.0965(14) 0.457(2) 0.4815(10) 0.045(5) Uani 1 1 d . . . . .
C23 C 0.1660(16) 0.548(3) 0.5245(11) 0.049(6) Uani 1 1 d . . . . .
C24 C 0.2328(13) 0.455(2) 0.5711(11) 0.041(5) Uani 1 1 d . . . . .
C25 C 0.3019(13) 0.451(2) 0.5681(9) 0.038(4) Uani 1 1 d . . . . .
C26 C 0.3733(13) 0.540(2) 0.6095(9) 0.041(5) Uani 1 1 d . . . . .
C27 C -0.0426(14) 0.552(3) 0.3490(9) 0.047(5) Uani 1 1 d . . . . .
C28 C -0.1153(15) 0.459(3) 0.3111(12) 0.060(6) Uani 1 1 d . . . . .
C29 C -0.1131(13) 0.551(3) 0.3584(10) 0.046(5) Uani 1 1 d . . . . .
C30 C -0.0439(14) 0.470(3) 0.3977(11) 0.051(6) Uani 1 1 d . . . . .
C31 C 0.5887(15) 0.545(3) 0.7760(11) 0.056(6) Uani 1 1 d . . . . .
C32 C 0.8131(14) 1.004(2) 0.6621(10) 0.038(5) Uani 1 1 d . . . . .
C33 C 0.9020(12) 0.930(2) 0.6992(9) 0.034(4) Uani 1 1 d . . . . .
C34 C 0.9072(14) 1.032(2) 0.6405(11) 0.048(5) Uani 1 1 d . . . . .
C35 C 0.8298(14) 1.022(2) 0.5502(9) 0.042(5) Uani 1 1 d . . . . .
C36 C 0.8399(14) 0.948(2) 0.4926(10) 0.042(5) Uani 1 1 d . . . . .
C37 C 0.9137(15) 0.965(3) 0.4678(10) 0.049(6) Uani 1 1 d . . . . .
C38 C 0.838(2) 1.035(3) 0.4357(15) 0.067(8) Uani 1 1 d . . . . .
C39 C 0.9119(12) 1.047(2) 0.5266(9) 0.033(4) Uani 1 1 d . . . . .
C40 C 0.8263(16) 0.922(3) 0.6018(11) 0.054(6) Uani 1 1 d . . . . .
C41 C 0.8373(16) 0.951(3) 0.3774(12) 0.053(6) Uani 1 1 d . . . . .
C42 C 0.8444(16) 1.058(3) 0.3189(11) 0.052(6) Uani 1 1 d . . . . .
C43 C 0.8417(17) 0.972(3) 0.2633(11) 0.058(6) Uani 1 1 d . . . . .
C44 C 0.8371(15) 0.967(2) 0.1411(10) 0.043(5) Uani 1 1 d . . . . .
C45 C 0.8289(14) 0.968(2) 0.0236(11) 0.043(5) Uani 1 1 d . . . . .
C46 C 0.8391(14) 1.061(2) 0.2009(10) 0.047(5) Uani 1 1 d . . . . .
C47 C 0.9128(14) 1.051(2) 0.4121(9) 0.045(5) Uani 1 1 d . . . . .
C48 C 0.8525(11) 0.824(2) 0.8227(9) 0.038(5) Uani 1 1 d . . . . .
C49 C 1.2075(18) 0.725(2) 1.0952(11) 0.054(6) Uani 1 1 d . . . . .
C50 C 1.1510(17) 0.756(3) 1.1090(13) 0.068(7) Uani 1 1 d . . . . .
C51 C 1.1000(16) 0.830(3) 1.1283(13) 0.079(9) Uani 1 1 d . . . . .
C52 C 0.7722(13) 0.538(2) 0.8949(10) 0.037(5) Uani 1 1 d . . . . .
B1 B 0.9643(13) 0.698(2) 1.0119(10) 0.031(4) Uani 1 1 d . . . . .
B2 B 0.9068(18) 0.969(3) 0.2347(13) 0.047(6) Uani 1 1 d . . . . .
B3 B 0.900(2) 1.051(3) 0.1745(15) 0.057(7) Uani 1 1 d . . . . .
B4 B 0.898(2) 0.961(3) 0.1163(13) 0.059(7) Uani 1 1 d . . . . .
B5 B 0.9101(17) 1.054(3) 0.2955(12) 0.042(6) Uani 1 1 d . . . . .
B6 B 0.9106(16) 0.964(3) 0.3492(11) 0.040(6) Uani 1 1 d . . . . .


_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Co1 C48 1.393(19) . ?
Co1 F1 1.454(15) . ?
Co1 Co1 1.990(5) 2_656 ?
Co1 N4 2.219(13) 2_656 ?
Co1 N5 2.239(13) 2_656 ?
Co1 N3 2.228(18) . ?
Co1 C1 2.38(2) . ?
F1 C1 1.38(3) . ?
F1 C52 1.47(3) . ?
F1 N1 1.71(2) . ?
F2 C5 1.36(3) . ?
F2 C7 1.54(2) . ?
F2 C6 1.74(3) 3_776 ?
F3 C5 1.42(3) . ?
O1 C32 1.79(3) . ?
N1 C2 1.23(3) . ?
N1 C52 1.34(3) . ?
N1 C3 1.59(2) . ?
N2 C2 1.18(3) . ?
N2 C8 1.37(2) . ?
N2 C7 1.59(2) . ?
N2 C48 1.64(2) . ?
N3 C9 1.20(3) . ?
N3 C48 1.27(3) . ?
N3 N4 1.54(3) . ?
N3 C8 1.62(3) . ?
N4 C32 1.48(2) . ?
N4 C9 1.67(2) . ?
N4 C33 1.73(2) . ?
N4 Co1 2.219(13) 2_656 ?
N5 C1 1.43(2) . ?
N5 C10 1.464(19) . ?
N5 C31 1.55(3) . ?
N5 Co1 2.239(13) 2_656 ?
N6 C34 1.46(3) . ?
N6 C35 1.49(3) . ?
N6 C39 1.55(3) . ?
N6 C40 1.61(3) . ?
N7 B4 1.45(4) . ?
N7 C44 1.48(3) . ?
N7 C45 1.53(3) . ?
N7 B3 1.99(4) . ?
C1 C52 1.75(3) . ?
C1 C31 1.98(3) . ?
C2 C7 1.80(3) . ?
C2 C3 1.83(3) . ?
C2 B1 2.06(3) . ?
C3 B1 1.45(3) . ?
C4 B1 1.55(4) . ?
C4 C5 1.68(4) . ?
C4 C50 2.03(4) . ?
C5 C50 1.36(3) . ?
C5 C6 1.52(4) 3_776 ?
C5 C51 1.81(4) . ?
C5 C49 1.84(3) . ?
C6 C5 1.52(4) 3_776 ?
C6 F2 1.74(3) 3_776 ?
C6 C45 1.87(4) . ?
C7 B1 1.48(3) . ?
C8 C48 1.52(3) . ?
C9 C33 1.48(3) . ?
C9 C32 2.02(3) . ?
C10 C13 1.51(3) . ?
C10 C31 1.53(3) . ?
C10 C11 1.56(2) . ?
C11 C14 1.34(3) . ?
C11 C13 1.41(3) . ?
C11 C12 1.50(3) . ?
C11 C31 1.98(3) . ?
C12 C15 1.36(3) . ?
C12 C14 1.39(3) . ?
C12 C26 1.56(3) . ?
C12 C13 1.89(3) . ?
C13 C14 1.50(3) . ?
C13 C31 1.55(3) . ?
C14 C15 1.56(3) . ?
C14 C26 1.99(3) . ?
C15 C26 1.37(3) . ?
C15 C16 1.57(3) . ?
C15 C25 1.96(3) . ?
C16 C26 1.31(3) . ?
C16 C25 1.36(3) . ?
C16 C24 1.50(3) . ?
C16 C17 1.91(3) . ?
C17 C23 1.19(3) . ?
C17 C24 1.25(3) . ?
C17 C25 1.45(3) . ?
C17 C18 1.56(3) . ?
C18 C22 1.19(3) . ?
C18 C23 1.32(3) . ?
C18 C19 1.52(3) . ?
C18 C24 2.00(3) . ?
C19 C21 1.15(3) . ?
C19 C22 1.28(3) . ?
C19 C20 1.55(3) . ?
C19 C23 1.90(3) . ?
C20 C30 1.28(3) . ?
C20 C21 1.29(3) . ?
C20 C27 1.51(3) . ?
C20 C22 1.99(3) . ?
C21 C30 1.47(3) . ?
C21 C22 1.52(3) . ?
C21 C27 1.95(3) . ?
C22 C23 1.53(3) . ?
C23 C24 1.55(3) . ?
C24 C25 1.20(3) . ?
C25 C26 1.53(3) . ?
C27 C29 1.28(3) . ?
C27 C30 1.32(3) . ?
C27 C28 1.54(3) . ?
C28 C29 1.33(4) . ?
C28 C30 1.92(3) . ?
C29 C30 1.44(3) . ?
C32 C40 1.59(3) . ?
C32 C33 1.64(3) . ?
C32 C34 1.83(3) . ?
C33 C34 1.62(3) . ?
C34 C40 1.72(3) . ?
C34 C35 2.02(3) . ?
C35 C40 1.48(3) . ?
C35 C36 1.49(3) . ?
C35 C39 1.65(3) . ?
C36 C38 1.48(3) . ?
C36 C37 1.52(3) . ?
C36 C39 1.54(3) . ?
C37 C38 1.43(4) . ?
C37 C47 1.45(3) . ?
C37 C39 1.50(3) . ?
C37 C41 2.01(3) . ?
C38 C41 1.49(4) . ?
C38 C47 1.52(4) . ?
C38 C39 2.00(4) . ?
C41 B6 1.56(4) . ?
C41 C47 1.59(3) . ?
C41 C42 1.66(3) . ?
C42 B5 1.37(4) . ?
C42 B6 1.43(3) . ?
C42 C43 1.45(3) . ?
C42 C47 2.02(3) . ?
C43 B5 1.40(4) . ?
C43 B2 1.43(4) . ?
C43 C46 1.58(3) . ?
C43 B6 1.89(3) . ?
C44 B4 1.30(4) . ?
C44 B3 1.35(4) . ?
C44 C46 1.56(3) . ?
C44 B2 2.03(4) . ?
C45 B4 2.01(3) . ?
C46 B3 1.34(4) . ?
C46 B2 1.45(3) . ?
C46 B5 2.05(3) . ?
C47 B6 1.59(3) . ?
C49 C50 1.13(4) . ?
C50 C51 1.28(4) . ?
B2 B3 1.49(4) . ?
B2 B5 1.53(4) . ?
B3 B4 1.51(4) . ?
B5 B6 1.44(3) . ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C48 Co1 F1 112.6(11) . . ?
C48 Co1 Co1 126.7(9) . 2_656 ?
F1 Co1 Co1 120.3(6) . 2_656 ?
C48 Co1 N4 95.8(10) . 2_656 ?
F1 Co1 N4 109.9(7) . 2_656 ?
Co1 Co1 N4 72.9(3) 2_656 2_656 ?
C48 Co1 N5 103.6(9) . 2_656 ?
F1 Co1 N5 84.3(7) . 2_656 ?
Co1 Co1 N5 76.6(3) 2_656 2_656 ?
N4 Co1 N5 149.4(4) 2_656 2_656 ?
C48 Co1 N3 31.6(10) . . ?
F1 Co1 N3 143.9(9) . . ?
Co1 Co1 N3 95.2(6) 2_656 . ?
N4 Co1 N3 85.5(6) 2_656 . ?
N5 Co1 N3 98.8(6) 2_656 . ?
C48 Co1 C1 144.4(11) . . ?
F1 Co1 C1 31.8(8) . . ?
Co1 Co1 C1 88.7(6) 2_656 . ?
N4 Co1 C1 98.6(5) 2_656 . ?
N5 Co1 C1 79.1(5) 2_656 . ?
N3 Co1 C1 175.1(8) . . ?
Co1 F1 C1 114.5(12) . . ?
Co1 F1 C52 167.2(14) . . ?
C1 F1 C52 75.8(14) . . ?
Co1 F1 N1 120.1(12) . . ?
C1 F1 N1 124.9(14) . . ?
C52 F1 N1 49.0(11) . . ?
C5 F2 C7 110.5(16) . . ?
C5 F2 C6 57.0(14) . 3_776 ?
C7 F2 C6 141.3(17) . 3_776 ?
C2 N1 C52 158(2) . . ?
C2 N1 C3 80.0(17) . . ?
C52 N1 C3 119.2(16) . . ?
C2 N1 F1 103.4(17) . . ?
C52 N1 F1 56.2(13) . . ?
C3 N1 F1 170.9(14) . . ?
C2 N2 C8 163(2) . . ?
C2 N2 C7 79.3(16) . . ?
C8 N2 C7 116.1(15) . . ?
C2 N2 C48 104.5(18) . . ?
C8 N2 C48 59.9(13) . . ?
C7 N2 C48 175.7(15) . . ?
C9 N3 C48 170(2) . . ?
C9 N3 N4 73.7(17) . . ?
C48 N3 N4 116.2(16) . . ?
C9 N3 C8 108.0(19) . . ?
C48 N3 C8 62.2(15) . . ?
N4 N3 C8 178.3(17) . . ?
C9 N3 Co1 155(2) . . ?
C48 N3 Co1 35.0(9) . . ?
N4 N3 Co1 81.2(9) . . ?
C8 N3 Co1 97.2(13) . . ?
N3 N4 C32 123.5(14) . . ?
N3 N4 C9 43.8(11) . . ?
C32 N4 C9 79.7(13) . . ?
N3 N4 C33 80.0(11) . . ?
C32 N4 C33 61.0(12) . . ?
C9 N4 C33 51.7(10) . . ?
N3 N4 Co1 110.8(9) . 2_656 ?
C32 N4 Co1 125.6(11) . 2_656 ?
C9 N4 Co1 154.4(10) . 2_656 ?
C33 N4 Co1 140.1(10) . 2_656 ?
C1 N5 C10 120.1(14) . . ?
C1 N5 C31 82.9(12) . . ?
C10 N5 C31 60.9(12) . . ?
C1 N5 Co1 111.5(11) . 2_656 ?
C10 N5 Co1 128.0(9) . 2_656 ?
C31 N5 Co1 135.0(12) . 2_656 ?
C34 N6 C35 86.0(18) . . ?
C34 N6 C39 113.3(19) . . ?
C35 N6 C39 65.8(14) . . ?
C34 N6 C40 67.9(15) . . ?
C35 N6 C40 56.8(15) . . ?
C39 N6 C40 122.5(18) . . ?
B4 N7 C44 52.8(17) . . ?
B4 N7 C45 84.8(17) . . ?
C44 N7 C45 113.8(17) . . ?
B4 N7 B3 49.2(15) . . ?
C44 N7 B3 42.8(13) . . ?
C45 N7 B3 134.0(18) . . ?
N5 C1 F1 116.7(15) . . ?
N5 C1 C52 170.5(18) . . ?
F1 C1 C52 54.4(13) . . ?
N5 C1 C31 51.1(11) . . ?
F1 C1 C31 140.8(15) . . ?
C52 C1 C31 132.4(14) . . ?
N5 C1 Co1 83.0(9) . . ?
F1 C1 Co1 33.7(8) . . ?
C52 C1 Co1 87.9(13) . . ?
C31 C1 Co1 116.7(11) . . ?
N2 C2 N1 148(2) . . ?
N2 C2 C7 60.5(15) . . ?
N1 C2 C7 144(2) . . ?
N2 C2 C3 147(2) . . ?
N1 C2 C3 58.6(15) . . ?
C7 C2 C3 87.5(13) . . ?
N2 C2 B1 104.7(19) . . ?
N1 C2 B1 101.3(19) . . ?
C7 C2 B1 44.4(10) . . ?
C3 C2 B1 43.2(10) . . ?
B1 C3 N1 117.5(16) . . ?
B1 C3 C2 76.8(14) . . ?
N1 C3 C2 41.4(10) . . ?
B1 C4 C5 99.7(18) . . ?
B1 C4 C50 133.9(19) . . ?
C5 C4 C50 41.6(11) . . ?
F2 C5 C50 136(2) . . ?
F2 C5 F3 101.0(16) . . ?
C50 C5 F3 123(2) . . ?
F2 C5 C6 74.3(17) . 3_776 ?
C50 C5 C6 100(2) . 3_776 ?
F3 C5 C6 97.1(19) . 3_776 ?
F2 C5 C4 97.7(18) . . ?
C50 C5 C4 82.8(19) . . ?
F3 C5 C4 88.9(17) . . ?
C6 C5 C4 171(2) 3_776 . ?
F2 C5 C51 91.3(16) . . ?
C50 C5 C51 45.0(16) . . ?
F3 C5 C51 165(2) . . ?
C6 C5 C51 93.6(18) 3_776 . ?
C4 C5 C51 81.8(17) . . ?
F2 C5 C49 161.4(19) . . ?
C50 C5 C49 37.9(14) . . ?
F3 C5 C49 88.8(16) . . ?
C6 C5 C49 88.9(16) 3_776 . ?
C4 C5 C49 98.3(17) . . ?
C51 C5 C49 81.6(13) . . ?
C5 C6 F2 48.7(12) 3_776 3_776 ?
C5 C6 C45 135(2) 3_776 . ?
F2 C6 C45 112.4(17) 3_776 . ?
B1 C7 F2 91.9(13) . . ?
B1 C7 N2 117.2(16) . . ?
F2 C7 N2 149.5(16) . . ?
B1 C7 C2 77.3(15) . . ?
F2 C7 C2 168.3(16) . . ?
N2 C7 C2 40.2(10) . . ?
N2 C8 C48 68.9(14) . . ?
N2 C8 N3 116.2(17) . . ?
C48 C8 N3 47.5(12) . . ?
N3 C9 C33 102.9(18) . . ?
N3 C9 N4 62.5(15) . . ?
C33 C9 N4 66.3(12) . . ?
N3 C9 C32 108.6(18) . . ?
C33 C9 C32 53.3(12) . . ?
N4 C9 C32 46.1(9) . . ?
N5 C10 C13 123.5(15) . . ?
N5 C10 C31 62.3(13) . . ?
C13 C10 C31 61.4(14) . . ?
N5 C10 C11 110.4(13) . . ?
C13 C10 C11 54.9(12) . . ?
C31 C10 C11 80.0(13) . . ?
C14 C11 C13 66.1(15) . . ?
C14 C11 C12 58.6(14) . . ?
C13 C11 C12 81.2(15) . . ?
C14 C11 C10 126.9(18) . . ?
C13 C11 C10 60.8(13) . . ?
C12 C11 C10 110.4(15) . . ?
C14 C11 C31 96.8(16) . . ?
C13 C11 C31 51.0(13) . . ?
C12 C11 C31 132.2(17) . . ?
C10 C11 C31 49.3(11) . . ?
C15 C12 C14 69.0(15) . . ?
C15 C12 C11 123.7(18) . . ?
C14 C12 C11 55.2(13) . . ?
C15 C12 C26 55.4(15) . . ?
C14 C12 C26 84.5(16) . . ?
C11 C12 C26 109.1(16) . . ?
C15 C12 C13 102.7(17) . . ?
C14 C12 C13 51.7(13) . . ?
C11 C12 C13 47.5(12) . . ?
C26 C12 C13 136.2(17) . . ?
C11 C13 C14 54.7(13) . . ?
C11 C13 C10 64.3(13) . . ?
C14 C13 C10 119.0(17) . . ?
C11 C13 C31 83.9(16) . . ?
C14 C13 C31 111.4(19) . . ?
C10 C13 C31 59.9(14) . . ?
C11 C13 C12 51.3(11) . . ?
C14 C13 C12 46.7(12) . . ?
C10 C13 C12 94.3(14) . . ?
C31 C13 C12 135.2(18) . . ?
C11 C14 C12 66.3(15) . . ?
C11 C14 C13 59.3(14) . . ?
C12 C14 C13 81.5(16) . . ?
C11 C14 C15 120.3(19) . . ?
C12 C14 C15 54.5(14) . . ?
C13 C14 C15 113.6(19) . . ?
C11 C14 C26 94.8(16) . . ?
C12 C14 C26 51.4(13) . . ?
C13 C14 C26 132.8(17) . . ?
C15 C14 C26 43.3(12) . . ?
C12 C15 C26 69.8(17) . . ?
C12 C15 C14 56.6(14) . . ?
C26 C15 C14 85.4(17) . . ?
C12 C15 C16 122(2) . . ?
C26 C15 C16 52.2(14) . . ?
C14 C15 C16 112.3(19) . . ?
C12 C15 C25 101.3(17) . . ?
C26 C15 C25 51.2(12) . . ?
C14 C15 C25 136.5(18) . . ?
C16 C15 C25 43.7(11) . . ?
C26 C16 C25 70.0(16) . . ?
C26 C16 C24 119.3(18) . . ?
C25 C16 C24 49.3(14) . . ?
C26 C16 C15 56.1(15) . . ?
C25 C16 C15 83.5(16) . . ?
C24 C16 C15 111.9(18) . . ?
C26 C16 C17 99.4(16) . . ?
C25 C16 C17 49.3(13) . . ?
C24 C16 C17 40.7(12) . . ?
C15 C16 C17 132.8(16) . . ?
C23 C17 C24 79(2) . . ?
C23 C17 C25 131(2) . . ?
C24 C17 C25 52.2(15) . . ?
C23 C17 C18 55.4(16) . . ?
C24 C17 C18 89.7(18) . . ?
C25 C17 C18 115.7(18) . . ?
C23 C17 C16 107.7(19) . . ?
C24 C17 C16 51.9(14) . . ?
C25 C17 C16 45.2(11) . . ?
C18 C17 C16 141.6(17) . . ?
C22 C18 C23 74.9(19) . . ?
C22 C18 C19 54.6(16) . . ?
C23 C18 C19 83.1(17) . . ?
C22 C18 C17 122(2) . . ?
C23 C18 C17 47.7(15) . . ?
C19 C18 C17 113.7(17) . . ?
C22 C18 C24 103.4(17) . . ?
C23 C18 C24 50.7(14) . . ?
C19 C18 C24 133.8(16) . . ?
C17 C18 C24 38.7(11) . . ?
C21 C19 C22 77.4(19) . . ?
C21 C19 C20 54.7(17) . . ?
C22 C19 C20 88.8(17) . . ?
C21 C19 C18 126(2) . . ?
C22 C19 C18 49.1(14) . . ?
C20 C19 C18 112.4(16) . . ?
C21 C19 C23 110.3(19) . . ?
C22 C19 C23 53.4(14) . . ?
C20 C19 C23 142.2(17) . . ?
C18 C19 C23 43.9(11) . . ?
C30 C20 C21 70(2) . . ?
C30 C20 C27 55.8(17) . . ?
C21 C20 C27 88.0(18) . . ?
C30 C20 C19 117(2) . . ?
C21 C20 C19 46.6(15) . . ?
C27 C20 C19 115.1(18) . . ?
C30 C20 C22 100.2(18) . . ?
C21 C20 C22 50.0(14) . . ?
C27 C20 C22 137.9(18) . . ?
C19 C20 C22 40.1(11) . . ?
C19 C21 C20 78.7(19) . . ?
C19 C21 C30 133(2) . . ?
C20 C21 C30 54.6(17) . . ?
C19 C21 C22 55.1(16) . . ?
C20 C21 C22 89.6(18) . . ?
C30 C21 C22 116(2) . . ?
C19 C21 C27 110(2) . . ?
C20 C21 C27 50.7(15) . . ?
C30 C21 C27 42.6(13) . . ?
C22 C21 C27 140.2(19) . . ?
C18 C22 C19 76.4(19) . . ?
C18 C22 C21 124(2) . . ?
C19 C22 C21 47.4(14) . . ?
C18 C22 C23 56.6(16) . . ?
C19 C22 C23 84.4(18) . . ?
C21 C22 C23 112(2) . . ?
C18 C22 C20 104.4(19) . . ?
C19 C22 C20 51.2(13) . . ?
C21 C22 C20 40.4(12) . . ?
C23 C22 C20 135.6(19) . . ?
C17 C23 C18 76.8(19) . . ?
C17 C23 C22 125(2) . . ?
C18 C23 C22 48.5(15) . . ?
C17 C23 C24 52.3(16) . . ?
C18 C23 C24 87.9(18) . . ?
C22 C23 C24 111.9(19) . . ?
C17 C23 C19 111.9(19) . . ?
C18 C23 C19 53.0(13) . . ?
C22 C23 C19 42.1(12) . . ?
C24 C23 C19 140.8(18) . . ?
C25 C24 C17 72.7(18) . . ?
C25 C24 C16 59.1(15) . . ?
C17 C24 C16 87.4(18) . . ?
C25 C24 C23 122(2) . . ?
C17 C24 C23 48.9(15) . . ?
C16 C24 C23 112.7(18) . . ?
C25 C24 C18 103.2(18) . . ?
C17 C24 C18 51.6(14) . . ?
C16 C24 C18 138.9(18) . . ?
C23 C24 C18 41.4(11) . . ?
C24 C25 C16 71.6(17) . . ?
C24 C25 C17 55.1(16) . . ?
C16 C25 C17 85.5(17) . . ?
C24 C25 C26 125(2) . . ?
C16 C25 C26 53.3(14) . . ?
C17 C25 C26 112.6(17) . . ?
C24 C25 C15 104.9(18) . . ?
C16 C25 C15 52.8(13) . . ?
C17 C25 C15 138.2(17) . . ?
C26 C25 C15 44.2(11) . . ?
C16 C26 C15 71.7(17) . . ?
C16 C26 C25 56.7(15) . . ?
C15 C26 C25 84.6(16) . . ?
C16 C26 C12 126(2) . . ?
C15 C26 C12 54.8(14) . . ?
C25 C26 C12 113.9(17) . . ?
C16 C26 C14 102.0(17) . . ?
C15 C26 C14 51.3(12) . . ?
C25 C26 C14 135.9(17) . . ?
C12 C26 C14 44.2(11) . . ?
C29 C27 C30 67.4(18) . . ?
C29 C27 C20 121(2) . . ?
C30 C27 C20 53.2(15) . . ?
C29 C27 C28 55.4(17) . . ?
C30 C27 C28 84.0(19) . . ?
C20 C27 C28 112(2) . . ?
C29 C27 C21 100.3(18) . . ?
C30 C27 C21 49.2(14) . . ?
C20 C27 C21 41.4(11) . . ?
C28 C27 C21 133(2) . . ?
C29 C28 C27 52.5(16) . . ?
C29 C28 C30 48.7(15) . . ?
C27 C28 C30 43.1(13) . . ?
C27 C29 C28 72.1(19) . . ?
C27 C29 C30 57.4(16) . . ?
C28 C29 C30 87(2) . . ?
C20 C30 C27 71.0(19) . . ?
C20 C30 C29 126(2) . . ?
C27 C30 C29 55.2(16) . . ?
C20 C30 C21 55.3(16) . . ?
C27 C30 C21 88.3(19) . . ?
C29 C30 C21 119(2) . . ?
C20 C30 C28 102.6(19) . . ?
C27 C30 C28 53.0(14) . . ?
C29 C30 C28 43.9(14) . . ?
C21 C30 C28 141(2) . . ?
C10 C31 N5 56.8(11) . . ?
C10 C31 C13 58.7(13) . . ?
N5 C31 C13 115.3(18) . . ?
C10 C31 C1 90.7(14) . . ?
N5 C31 C1 46.1(9) . . ?
C13 C31 C1 139.5(19) . . ?
C10 C31 C11 50.6(10) . . ?
N5 C31 C11 88.4(13) . . ?
C13 C31 C11 45.1(11) . . ?
C1 C31 C11 134.0(16) . . ?
N4 C32 C40 112.0(17) . . ?
N4 C32 C33 67.0(12) . . ?
C40 C32 C33 82.2(16) . . ?
N4 C32 O1 99.0(15) . . ?
C40 C32 O1 106.9(16) . . ?
C33 C32 O1 165.8(16) . . ?
N4 C32 C34 122.3(17) . . ?
C40 C32 C34 59.9(14) . . ?
C33 C32 C34 55.3(12) . . ?
O1 C32 C34 138.7(15) . . ?
N4 C32 C9 54.2(10) . . ?
C40 C32 C9 128.5(18) . . ?
C33 C32 C9 46.3(10) . . ?
O1 C32 C9 123.6(15) . . ?
C34 C32 C9 85.4(14) . . ?
C9 C33 C34 114.7(17) . . ?
C9 C33 C32 80.4(15) . . ?
C34 C33 C32 68.1(13) . . ?
C9 C33 N4 61.9(11) . . ?
C34 C33 N4 120.0(15) . . ?
C32 C33 N4 51.9(10) . . ?
N6 C34 C33 112.9(18) . . ?
N6 C34 C40 60.0(14) . . ?
C33 C34 C40 79.1(14) . . ?
N6 C34 C32 113.4(17) . . ?
C33 C34 C32 56.6(12) . . ?
C40 C34 C32 53.3(12) . . ?
N6 C34 C35 47.6(12) . . ?
C33 C34 C35 124.7(16) . . ?
C40 C34 C35 45.7(11) . . ?
C32 C34 C35 82.9(13) . . ?
C40 C35 N6 65.6(15) . . ?
C40 C35 C36 113.0(18) . . ?
N6 C35 C36 83.3(16) . . ?
C40 C35 C39 124.2(18) . . ?
N6 C35 C39 58.7(13) . . ?
C36 C35 C39 58.4(13) . . ?
C40 C35 C34 56.6(13) . . ?
N6 C35 C34 46.4(12) . . ?
C36 C35 C34 129.5(17) . . ?
C39 C35 C34 86.0(13) . . ?
C38 C36 C35 118.1(19) . . ?
C38 C36 C37 56.8(16) . . ?
C35 C36 C37 124.6(19) . . ?
C38 C36 C39 83.2(18) . . ?
C35 C36 C39 66.0(14) . . ?
C37 C36 C39 58.6(14) . . ?
C38 C37 C47 63.8(17) . . ?
C38 C37 C39 86.3(19) . . ?
C47 C37 C39 116(2) . . ?
C38 C37 C36 60.0(17) . . ?
C47 C37 C36 124(2) . . ?
C39 C37 C36 61.2(14) . . ?
C38 C37 C41 47.7(15) . . ?
C47 C37 C41 51.4(13) . . ?
C39 C37 C41 134.0(19) . . ?
C36 C37 C41 88.8(17) . . ?
C37 C38 C36 63.2(18) . . ?
C37 C38 C41 87(2) . . ?
C36 C38 C41 115(2) . . ?
C37 C38 C47 58.9(17) . . ?
C36 C38 C47 122(2) . . ?
C41 C38 C47 63.5(17) . . ?
C37 C38 C39 48.4(15) . . ?
C36 C38 C39 49.7(14) . . ?
C41 C38 C39 135(2) . . ?
C47 C38 C39 89.4(19) . . ?
C37 C39 C36 60.2(14) . . ?
C37 C39 N6 113.8(17) . . ?
C36 C39 N6 79.9(14) . . ?
C37 C39 C35 115.8(17) . . ?
C36 C39 C35 55.6(13) . . ?
N6 C39 C35 55.5(12) . . ?
C37 C39 C38 45.4(13) . . ?
C36 C39 C38 47.1(12) . . ?
N6 C39 C38 127.0(17) . . ?
C35 C39 C38 87.8(14) . . ?
C35 C40 N6 57.6(15) . . ?
C35 C40 C32 112.1(19) . . ?
N6 C40 C32 118.8(19) . . ?
C35 C40 C34 77.7(17) . . ?
N6 C40 C34 52.0(14) . . ?
C32 C40 C34 66.8(14) . . ?
C38 C41 B6 120(2) . . ?
C38 C41 C47 59.1(17) . . ?
B6 C41 C47 60.5(16) . . ?
C38 C41 C42 111(2) . . ?
B6 C41 C42 52.7(15) . . ?
C47 C41 C42 76.8(16) . . ?
C38 C41 C37 45.1(15) . . ?
B6 C41 C37 91.2(17) . . ?
C47 C41 C37 45.7(12) . . ?
C42 C41 C37 122.5(18) . . ?
B5 C42 B6 62.0(19) . . ?
B5 C42 C43 59.4(18) . . ?
B6 C42 C43 82(2) . . ?
B5 C42 C41 122(2) . . ?
B6 C42 C41 60.2(16) . . ?
C43 C42 C41 108.5(19) . . ?
B5 C42 C47 94.9(19) . . ?
B6 C42 C47 51.4(14) . . ?
C43 C42 C47 133(2) . . ?
C41 C42 C47 50.0(12) . . ?
B5 C43 B2 66(2) . . ?
B5 C43 C42 57.5(18) . . ?
B2 C43 C42 123(2) . . ?
B5 C43 C46 86.9(19) . . ?
B2 C43 C46 57.3(16) . . ?
C42 C43 C46 114(2) . . ?
B5 C43 B6 49.3(15) . . ?
B2 C43 B6 96(2) . . ?
C42 C43 B6 48.6(14) . . ?
C46 C43 B6 136(2) . . ?
B4 C44 B3 69(2) . . ?
B4 C44 N7 62.3(17) . . ?
B3 C44 N7 88.9(19) . . ?
B4 C44 C46 124(2) . . ?
B3 C44 C46 54.1(18) . . ?
N7 C44 C46 112.2(17) . . ?
B4 C44 B2 97(2) . . ?
B3 C44 B2 47.5(17) . . ?
N7 C44 B2 136.3(18) . . ?
C46 C44 B2 45.5(12) . . ?
N7 C45 C6 116.7(16) . . ?
N7 C45 B4 46.0(13) . . ?
C6 C45 B4 126.4(18) . . ?
B3 C46 B2 65(2) . . ?
B3 C46 C44 54.7(19) . . ?
B2 C46 C44 84.4(18) . . ?
B3 C46 C43 121(2) . . ?
B2 C46 C43 56.0(17) . . ?
C44 C46 C43 114.2(18) . . ?
B3 C46 B5 97(2) . . ?
B2 C46 B5 48.2(15) . . ?
C44 C46 B5 132.6(18) . . ?
C43 C46 B5 42.7(13) . . ?
C37 C47 C38 57.4(17) . . ?
C37 C47 C41 82.9(18) . . ?
C38 C47 C41 57.3(17) . . ?
C37 C47 B6 116(2) . . ?
C38 C47 B6 116(2) . . ?
C41 C47 B6 58.9(16) . . ?
C37 C47 C42 136.1(19) . . ?
C38 C47 C42 93.2(18) . . ?
C41 C47 C42 53.2(12) . . ?
B6 C47 C42 44.9(12) . . ?
N3 C48 Co1 113.4(16) . . ?
N3 C48 C8 70.3(16) . . ?
Co1 C48 C8 176.0(18) . . ?
N3 C48 N2 121.4(18) . . ?
Co1 C48 N2 125.1(17) . . ?
C8 C48 N2 51.2(10) . . ?
C50 C49 C5 47.2(17) . . ?
C49 C50 C51 161(3) . . ?
C49 C50 C5 95(2) . . ?
C51 C50 C5 87(2) . . ?
C49 C50 C4 112(3) . . ?
C51 C50 C4 84.4(19) . . ?
C5 C50 C4 55.6(16) . . ?
C50 C51 C5 48.4(16) . . ?
N1 C52 F1 74.8(15) . . ?
N1 C52 C1 124.5(18) . . ?
F1 C52 C1 49.7(11) . . ?
C3 B1 C7 118.3(17) . . ?
C3 B1 C4 123(2) . . ?
C7 B1 C4 108.4(18) . . ?
C3 B1 C2 60.0(13) . . ?
C7 B1 C2 58.4(12) . . ?
C4 B1 C2 142.8(18) . . ?
C43 B2 C46 66.6(19) . . ?
C43 B2 B3 121(2) . . ?
C46 B2 B3 54.0(17) . . ?
C43 B2 B5 56.0(17) . . ?
C46 B2 B5 87(2) . . ?
B3 B2 B5 118(2) . . ?
C43 B2 C44 98(2) . . ?
C46 B2 C44 50.1(14) . . ?
B3 B2 C44 41.7(16) . . ?
B5 B2 C44 137(2) . . ?
C46 B3 C44 71(2) . . ?
C46 B3 B2 61.4(19) . . ?
C44 B3 B2 91(2) . . ?
C46 B3 B4 125(3) . . ?
C44 B3 B4 54(2) . . ?
B2 B3 B4 115(3) . . ?
C46 B3 N7 97(2) . . ?
C44 B3 N7 48.3(14) . . ?
B2 B3 N7 139(3) . . ?
B4 B3 N7 46.6(15) . . ?
C44 B4 N7 65(2) . . ?
C44 B4 B3 57(2) . . ?
N7 B4 B3 84(2) . . ?
C44 B4 C45 97(2) . . ?
N7 B4 C45 49.3(12) . . ?
B3 B4 C45 133(2) . . ?
C42 B5 C43 63.1(19) . . ?
C42 B5 B6 61.1(17) . . ?
C43 B5 B6 83(2) . . ?
C42 B5 B2 121(2) . . ?
C43 B5 B2 58.3(18) . . ?
B6 B5 B2 113(2) . . ?
C42 B5 C46 94.2(19) . . ?
C43 B5 C46 50.4(14) . . ?
B6 B5 C46 134(2) . . ?
B2 B5 C46 45.0(14) . . ?
C42 B6 B5 56.9(17) . . ?
C42 B6 C41 67.1(17) . . ?
B5 B6 C41 124(2) . . ?
C42 B6 C47 83.7(17) . . ?
B5 B6 C47 113(2) . . ?
C41 B6 C47 60.6(15) . . ?
C42 B6 C43 49.3(15) . . ?
B5 B6 C43 47.2(15) . . ?
C41 B6 C43 93.5(18) . . ?
C47 B6 C43 132.9(19) . . ?

loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C48 Co1 F1 C1 179.0(14) . . . . ?
Co1 Co1 F1 C1 -7.7(15) 2_656 . . . ?
N4 Co1 F1 C1 73.6(13) 2_656 . . . ?
N5 Co1 F1 C1 -78.6(12) 2_656 . . . ?
N3 Co1 F1 C1 -175.7(11) . . . . ?
C48 Co1 F1 C52 37(7) . . . . ?
Co1 Co1 F1 C52 -150(6) 2_656 . . . ?
N4 Co1 F1 C52 -69(7) 2_656 . . . ?
N5 Co1 F1 C52 139(7) 2_656 . . . ?
N3 Co1 F1 C52 42(7) . . . . ?
C1 Co1 F1 C52 -142(7) . . . . ?
C48 Co1 F1 N1 6.8(17) . . . . ?
Co1 Co1 F1 N1 -179.9(9) 2_656 . . . ?
N4 Co1 F1 N1 -98.6(12) 2_656 . . . ?
N5 Co1 F1 N1 109.3(12) 2_656 . . . ?
N3 Co1 F1 N1 12(2) . . . . ?
C1 Co1 F1 N1 -172(2) . . . . ?
Co1 F1 N1 C2 -16(2) . . . . ?
C1 F1 N1 C2 172.7(19) . . . . ?
C52 F1 N1 C2 173(2) . . . . ?
Co1 F1 N1 C52 171.5(17) . . . . ?
C1 F1 N1 C52 0.2(18) . . . . ?
C9 N3 N4 C32 -1(2) . . . . ?
C48 N3 N4 C32 176.7(18) . . . . ?
Co1 N3 N4 C32 175.6(15) . . . . ?
C48 N3 N4 C9 178(2) . . . . ?
Co1 N3 N4 C9 177.0(15) . . . . ?
C9 N3 N4 C33 43.6(14) . . . . ?
C48 N3 N4 C33 -138.3(18) . . . . ?
Co1 N3 N4 C33 -139.4(9) . . . . ?
C9 N3 N4 Co1 -176.4(14) . . . 2_656 ?
C48 N3 N4 Co1 2(2) . . . 2_656 ?
Co1 N3 N4 Co1 0.6(8) . . . 2_656 ?
C10 N5 C1 F1 174.7(14) . . . . ?
C31 N5 C1 F1 -135.1(17) . . . . ?
Co1 N5 C1 F1 0.6(17) 2_656 . . . ?
C10 N5 C1 C31 -50.2(15) . . . . ?
Co1 N5 C1 C31 135.8(14) 2_656 . . . ?
C10 N5 C1 Co1 176.9(12) . . . . ?
C31 N5 C1 Co1 -132.9(12) . . . . ?
Co1 N5 C1 Co1 2.9(8) 2_656 . . . ?
Co1 F1 C1 N5 4(2) . . . . ?
C52 F1 C1 N5 176.0(17) . . . . ?
N1 F1 C1 N5 175.8(13) . . . . ?
Co1 F1 C1 C52 -171.9(16) . . . . ?
N1 F1 C1 C52 -0.2(14) . . . . ?
Co1 F1 C1 C31 -56(3) . . . . ?
C52 F1 C1 C31 116(2) . . . . ?
N1 F1 C1 C31 116(2) . . . . ?
C52 F1 C1 Co1 171.9(16) . . . . ?
N1 F1 C1 Co1 172(2) . . . . ?
C8 N2 C2 N1 -54(10) . . . . ?
C7 N2 C2 N1 147(5) . . . . ?
C48 N2 C2 N1 -35(5) . . . . ?
C8 N2 C2 C7 158(7) . . . . ?
C48 N2 C2 C7 177.9(15) . . . . ?
C8 N2 C2 C3 176(4) . . . . ?
C7 N2 C2 C3 18(4) . . . . ?
C48 N2 C2 C3 -164(3) . . . . ?
C8 N2 C2 B1 163(6) . . . . ?
C7 N2 C2 B1 4.8(14) . . . . ?
C48 N2 C2 B1 -177.3(13) . . . . ?
C52 N1 C2 N2 56(9) . . . . ?
C3 N1 C2 N2 -150(5) . . . . ?
F1 N1 C2 N2 38(5) . . . . ?
C52 N1 C2 C7 -177(4) . . . . ?
C3 N1 C2 C7 -23(3) . . . . ?
F1 N1 C2 C7 166(3) . . . . ?
C52 N1 C2 C3 -154(6) . . . . ?
F1 N1 C2 C3 -171.4(14) . . . . ?
C52 N1 C2 B1 -161(5) . . . . ?
C3 N1 C2 B1 -7.2(13) . . . . ?
F1 N1 C2 B1 -178.5(12) . . . . ?
C2 N1 C3 B1 11(2) . . . . ?
C52 N1 C3 B1 -179.2(18) . . . . ?
C52 N1 C3 C2 169(2) . . . . ?
N2 C2 C3 B1 -19(4) . . . . ?
N1 C2 C3 B1 -169.7(19) . . . . ?
C7 C2 C3 B1 -3.1(13) . . . . ?
N2 C2 C3 N1 151(5) . . . . ?
C7 C2 C3 N1 167(2) . . . . ?
B1 C2 C3 N1 169.7(19) . . . . ?
C7 F2 C5 C50 -134(3) . . . . ?
C6 F2 C5 C50 88(3) 3_776 . . . ?
C7 F2 C5 F3 44(2) . . . . ?
C6 F2 C5 F3 -94(2) 3_776 . . . ?
C7 F2 C5 C6 138.6(18) . . . 3_776 ?
C7 F2 C5 C4 -46.1(19) . . . . ?
C6 F2 C5 C4 175(2) 3_776 . . . ?
C7 F2 C5 C51 -128.0(17) . . . . ?
C6 F2 C5 C51 93.4(18) 3_776 . . . ?
C7 F2 C5 C49 165(5) . . . . ?
C6 F2 C5 C49 26(6) 3_776 . . . ?
B1 C4 C5 F2 14.4(19) . . . . ?
C50 C4 C5 F2 -136(2) . . . . ?
B1 C4 C5 C50 150(2) . . . . ?
B1 C4 C5 F3 -86.5(19) . . . . ?
C50 C4 C5 F3 123(2) . . . . ?
B1 C4 C5 C51 104.7(17) . . . . ?
C50 C4 C5 C51 -45.4(16) . . . . ?
B1 C4 C5 C49 -175.2(16) . . . . ?
C50 C4 C5 C49 34.7(15) . . . . ?
C5 F2 C7 B1 59.1(19) . . . . ?
C6 F2 C7 B1 122(2) 3_776 . . . ?
C5 F2 C7 N2 -137(3) . . . . ?
C6 F2 C7 N2 -75(4) 3_776 . . . ?
C5 F2 C7 C2 81(8) . . . . ?
C6 F2 C7 C2 143(7) 3_776 . . . ?
C2 N2 C7 B1 -7(2) . . . . ?
C8 N2 C7 B1 179.4(16) . . . . ?
C2 N2 C7 F2 -169(3) . . . . ?
C8 N2 C7 F2 18(4) . . . . ?
C8 N2 C7 C2 -173(2) . . . . ?
N2 C2 C7 B1 173(2) . . . . ?
N1 C2 C7 B1 23(4) . . . . ?
C3 C2 C7 B1 3.0(13) . . . . ?
N2 C2 C7 F2 151(8) . . . . ?
N1 C2 C7 F2 0(11) . . . . ?
C3 C2 C7 F2 -19(8) . . . . ?
B1 C2 C7 F2 -22(8) . . . . ?
N1 C2 C7 N2 -151(4) . . . . ?
C3 C2 C7 N2 -170(2) . . . . ?
B1 C2 C7 N2 -173(2) . . . . ?
C2 N2 C8 C48 22(7) . . . . ?
C7 N2 C8 C48 178.2(16) . . . . ?
C2 N2 C8 N3 18(8) . . . . ?
C7 N2 C8 N3 174.2(14) . . . . ?
C48 N2 C8 N3 -3.9(14) . . . . ?
C9 N3 C8 N2 -177.0(17) . . . . ?
C48 N3 C8 N2 5.0(18) . . . . ?
Co1 N3 C8 N2 5.8(17) . . . . ?
C9 N3 C8 C48 178(2) . . . . ?
Co1 N3 C8 C48 0.8(12) . . . . ?
C48 N3 C9 C33 136(12) . . . . ?
N4 N3 C9 C33 -54.3(15) . . . . ?
C8 N3 C9 C33 125.4(16) . . . . ?
Co1 N3 C9 C33 -61(4) . . . . ?
C48 N3 C9 N4 -170(13) . . . . ?
C8 N3 C9 N4 179.7(16) . . . . ?
Co1 N3 C9 N4 -7(4) . . . . ?
C48 N3 C9 C32 -169(12) . . . . ?
N4 N3 C9 C32 0.9(14) . . . . ?
C8 N3 C9 C32 -179.4(14) . . . . ?
Co1 N3 C9 C32 -6(5) . . . . ?
C32 N4 C9 N3 178.8(18) . . . . ?
C33 N4 C9 N3 -120.1(18) . . . . ?
Co1 N4 C9 N3 8(3) 2_656 . . . ?
N3 N4 C9 C33 120.1(18) . . . . ?
C32 N4 C9 C33 -61.1(13) . . . . ?
Co1 N4 C9 C33 128(2) 2_656 . . . ?
N3 N4 C9 C32 -178.8(18) . . . . ?
C33 N4 C9 C32 61.1(13) . . . . ?
Co1 N4 C9 C32 -171(3) 2_656 . . . ?
C1 N5 C10 C13 66(2) . . . . ?
C31 N5 C10 C13 5.5(18) . . . . ?
Co1 N5 C10 C13 -120.7(16) 2_656 . . . ?
C1 N5 C10 C31 60.8(16) . . . . ?
Co1 N5 C10 C31 -126.2(15) 2_656 . . . ?
C1 N5 C10 C11 126.9(15) . . . . ?
C31 N5 C10 C11 66.2(15) . . . . ?
Co1 N5 C10 C11 -60.1(16) 2_656 . . . ?
N5 C10 C11 C14 -119(2) . . . . ?
C13 C10 C11 C14 -1(2) . . . . ?
C31 C10 C11 C14 -63(2) . . . . ?
N5 C10 C11 C13 -117.3(17) . . . . ?
C31 C10 C11 C13 -62.0(15) . . . . ?
N5 C10 C11 C12 176.0(14) . . . . ?
C13 C10 C11 C12 -66.7(17) . . . . ?
C31 C10 C11 C12 -128.7(18) . . . . ?
N5 C10 C11 C31 -55.3(14) . . . . ?
C13 C10 C11 C31 62.0(15) . . . . ?
C14 C11 C12 C15 8(2) . . . . ?
C13 C11 C12 C15 75(2) . . . . ?
C10 C11 C12 C15 130(2) . . . . ?
C31 C11 C12 C15 77(3) . . . . ?
C13 C11 C12 C14 67.3(16) . . . . ?
C10 C11 C12 C14 121.6(19) . . . . ?
C31 C11 C12 C14 69(2) . . . . ?
C14 C11 C12 C26 68.6(18) . . . . ?
C13 C11 C12 C26 135.9(18) . . . . ?
C10 C11 C12 C26 -169.8(15) . . . . ?
C31 C11 C12 C26 137.1(19) . . . . ?
C14 C11 C12 C13 -67.3(16) . . . . ?
C10 C11 C12 C13 54.2(14) . . . . ?
C31 C11 C12 C13 1.2(18) . . . . ?
C12 C11 C13 C14 -59.4(14) . . . . ?
C10 C11 C13 C14 -178.8(17) . . . . ?
C31 C11 C13 C14 121.7(18) . . . . ?
C14 C11 C13 C10 178.8(17) . . . . ?
C12 C11 C13 C10 119.4(15) . . . . ?
C31 C11 C13 C10 -59.5(13) . . . . ?
C14 C11 C13 C31 -121.7(18) . . . . ?
C12 C11 C13 C31 178.8(17) . . . . ?
C10 C11 C13 C31 59.5(13) . . . . ?
C14 C11 C13 C12 59.4(14) . . . . ?
C10 C11 C13 C12 -119.4(15) . . . . ?
C31 C11 C13 C12 -178.8(17) . . . . ?
N5 C10 C13 C11 92.6(17) . . . . ?
C31 C10 C13 C11 98.2(16) . . . . ?
N5 C10 C13 C14 94(2) . . . . ?
C31 C10 C13 C14 99(2) . . . . ?
C11 C10 C13 C14 1.1(16) . . . . ?
N5 C10 C13 C31 -5.5(18) . . . . ?
C11 C10 C13 C31 -98.2(16) . . . . ?
N5 C10 C13 C12 135.6(15) . . . . ?
C31 C10 C13 C12 141.2(18) . . . . ?
C11 C10 C13 C12 43.0(12) . . . . ?
C15 C12 C13 C11 -124(2) . . . . ?
C14 C12 C13 C11 -74.7(17) . . . . ?
C26 C12 C13 C11 -72(3) . . . . ?
C15 C12 C13 C14 -49.8(19) . . . . ?
C11 C12 C13 C14 74.7(17) . . . . ?
C26 C12 C13 C14 3(2) . . . . ?
C15 C12 C13 C10 -176.4(17) . . . . ?
C14 C12 C13 C10 -126.7(19) . . . . ?
C11 C12 C13 C10 -52.0(14) . . . . ?
C26 C12 C13 C10 -124(2) . . . . ?
C15 C12 C13 C31 -126(3) . . . . ?
C14 C12 C13 C31 -76(3) . . . . ?
C11 C12 C13 C31 -2(2) . . . . ?
C26 C12 C13 C31 -73(4) . . . . ?
C13 C11 C14 C12 -94.2(16) . . . . ?
C10 C11 C14 C12 -93(2) . . . . ?
C31 C11 C14 C12 -136.0(16) . . . . ?
C12 C11 C14 C13 94.2(16) . . . . ?
C10 C11 C14 C13 1.3(19) . . . . ?
C31 C11 C14 C13 -41.7(14) . . . . ?
C13 C11 C14 C15 -101(2) . . . . ?
C12 C11 C14 C15 -6.7(19) . . . . ?
C10 C11 C14 C15 -100(2) . . . . ?
C31 C11 C14 C15 -142.7(19) . . . . ?
C13 C11 C14 C26 -138.1(16) . . . . ?
C12 C11 C14 C26 -43.9(13) . . . . ?
C10 C11 C14 C26 -136.8(17) . . . . ?
C31 C11 C14 C26 -179.9(13) . . . . ?
C15 C12 C14 C11 -173(2) . . . . ?
C26 C12 C14 C11 -117.9(17) . . . . ?
C13 C12 C14 C11 60.1(14) . . . . ?
C15 C12 C14 C13 127.1(19) . . . . ?
C11 C12 C14 C13 -60.1(14) . . . . ?
C26 C12 C14 C13 -177.9(17) . . . . ?
C11 C12 C14 C15 173(2) . . . . ?
C26 C12 C14 C15 55.0(15) . . . . ?
C13 C12 C14 C15 -127.1(19) . . . . ?
C15 C12 C14 C26 -55.0(15) . . . . ?
C11 C12 C14 C26 117.9(17) . . . . ?
C13 C12 C14 C26 177.9(17) . . . . ?
C10 C13 C14 C11 -1.2(18) . . . . ?
C31 C13 C14 C11 65.3(19) . . . . ?
C12 C13 C14 C11 -67.4(15) . . . . ?
C11 C13 C14 C12 67.4(15) . . . . ?
C10 C13 C14 C12 66(2) . . . . ?
C31 C13 C14 C12 132.6(19) . . . . ?
C11 C13 C14 C15 112(2) . . . . ?
C10 C13 C14 C15 111(2) . . . . ?
C31 C13 C14 C15 177.7(18) . . . . ?
C12 C13 C14 C15 45.1(16) . . . . ?
C11 C13 C14 C26 65(2) . . . . ?
C10 C13 C14 C26 64(3) . . . . ?
C31 C13 C14 C26 130(2) . . . . ?
C12 C13 C14 C26 -2.2(18) . . . . ?
C14 C12 C15 C26 98.0(17) . . . . ?
C11 C12 C15 C26 91(2) . . . . ?
C13 C12 C15 C26 138.0(17) . . . . ?
C11 C12 C15 C14 -7(2) . . . . ?
C26 C12 C15 C14 -98.0(17) . . . . ?
C13 C12 C15 C14 40.0(15) . . . . ?
C14 C12 C15 C16 97(2) . . . . ?
C11 C12 C15 C16 90(3) . . . . ?
C26 C12 C15 C16 -0.9(18) . . . . ?
C13 C12 C15 C16 137.1(19) . . . . ?
C14 C12 C15 C25 139.0(18) . . . . ?
C11 C12 C15 C25 131.9(19) . . . . ?
C26 C12 C15 C25 41.0(13) . . . . ?
C13 C12 C15 C25 179.0(13) . . . . ?
C11 C14 C15 C12 8(2) . . . . ?
C13 C14 C15 C12 -59(2) . . . . ?
C26 C14 C15 C12 68.8(17) . . . . ?
C11 C14 C15 C26 -61(2) . . . . ?
C12 C14 C15 C26 -68.8(17) . . . . ?
C13 C14 C15 C26 -128(2) . . . . ?
C11 C14 C15 C16 -107(2) . . . . ?
C12 C14 C15 C16 -115(2) . . . . ?
C13 C14 C15 C16 -174.0(17) . . . . ?
C26 C14 C15 C16 -45.8(16) . . . . ?
C11 C14 C15 C25 -62(3) . . . . ?
C12 C14 C15 C25 -69(3) . . . . ?
C13 C14 C15 C25 -129(2) . . . . ?
C26 C14 C15 C25 -0.4(19) . . . . ?
C12 C15 C16 C26 1(2) . . . . ?
C14 C15 C16 C26 65(2) . . . . ?
C25 C15 C16 C26 -70.3(16) . . . . ?
C12 C15 C16 C25 71(2) . . . . ?
C26 C15 C16 C25 70.3(16) . . . . ?
C14 C15 C16 C25 134.9(19) . . . . ?
C12 C15 C16 C24 113(2) . . . . ?
C26 C15 C16 C24 111(2) . . . . ?
C14 C15 C16 C24 176.0(17) . . . . ?
C25 C15 C16 C24 41.1(15) . . . . ?
C12 C15 C16 C17 70(3) . . . . ?
C26 C15 C16 C17 69(2) . . . . ?
C14 C15 C16 C17 134(2) . . . . ?
C25 C15 C16 C17 -1.1(18) . . . . ?
C23 C17 C18 C22 -7(3) . . . . ?
C24 C17 C18 C22 69(3) . . . . ?
C25 C17 C18 C22 116(2) . . . . ?
C16 C17 C18 C22 67(4) . . . . ?
C24 C17 C18 C23 76(2) . . . . ?
C25 C17 C18 C23 123(2) . . . . ?
C16 C17 C18 C23 74(3) . . . . ?
C23 C17 C18 C19 55(2) . . . . ?
C24 C17 C18 C19 131.3(19) . . . . ?
C25 C17 C18 C19 178.3(17) . . . . ?
C16 C17 C18 C19 129(2) . . . . ?
C23 C17 C18 C24 -76(2) . . . . ?
C25 C17 C18 C24 47.0(16) . . . . ?
C16 C17 C18 C24 -2(2) . . . . ?
C22 C18 C19 C21 -5(3) . . . . ?
C23 C18 C19 C21 -82(3) . . . . ?
C17 C18 C19 C21 -119(3) . . . . ?
C24 C18 C19 C21 -79(3) . . . . ?
C23 C18 C19 C22 -76(2) . . . . ?
C17 C18 C19 C22 -114(2) . . . . ?
C24 C18 C19 C22 -73(2) . . . . ?
C22 C18 C19 C20 -67(2) . . . . ?
C23 C18 C19 C20 -143.5(19) . . . . ?
C17 C18 C19 C20 179.0(17) . . . . ?
C24 C18 C19 C20 -140(2) . . . . ?
C22 C18 C19 C23 76(2) . . . . ?
C17 C18 C19 C23 -37.6(16) . . . . ?
C24 C18 C19 C23 3.0(18) . . . . ?
C21 C19 C20 C30 -2(2) . . . . ?
C22 C19 C20 C30 73(2) . . . . ?
C18 C19 C20 C30 117(2) . . . . ?
C23 C19 C20 C30 75(3) . . . . ?
C22 C19 C20 C21 75(2) . . . . ?
C18 C19 C20 C21 120(2) . . . . ?
C23 C19 C20 C21 77(3) . . . . ?
C21 C19 C20 C27 60(2) . . . . ?
C22 C19 C20 C27 136(2) . . . . ?
C18 C19 C20 C27 179.8(18) . . . . ?
C23 C19 C20 C27 138(2) . . . . ?
C21 C19 C20 C22 -75(2) . . . . ?
C18 C19 C20 C22 44.1(15) . . . . ?
C23 C19 C20 C22 2(2) . . . . ?
C22 C19 C21 C20 -97.5(18) . . . . ?
C18 C19 C21 C20 -93(2) . . . . ?
C23 C19 C21 C20 -140.3(18) . . . . ?
C22 C19 C21 C30 -95(3) . . . . ?
C20 C19 C21 C30 3(3) . . . . ?
C18 C19 C21 C30 -91(3) . . . . ?
C23 C19 C21 C30 -138(3) . . . . ?
C20 C19 C21 C22 97.5(18) . . . . ?
C18 C19 C21 C22 4(2) . . . . ?
C23 C19 C21 C22 -42.8(16) . . . . ?
C22 C19 C21 C27 -138(2) . . . . ?
C20 C19 C21 C27 -40.4(16) . . . . ?
C18 C19 C21 C27 -134(2) . . . . ?
C23 C19 C21 C27 179.3(15) . . . . ?
C30 C20 C21 C19 178(2) . . . . ?
C27 C20 C21 C19 -128.1(19) . . . . ?
C22 C20 C21 C19 54.4(16) . . . . ?
C27 C20 C21 C30 54.1(17) . . . . ?
C19 C20 C21 C30 -178(2) . . . . ?
C22 C20 C21 C30 -123(2) . . . . ?
C30 C20 C21 C22 123(2) . . . . ?
C27 C20 C21 C22 177.4(19) . . . . ?
C19 C20 C21 C22 -54.4(16) . . . . ?
C30 C20 C21 C27 -54.1(17) . . . . ?
C19 C20 C21 C27 128.1(19) . . . . ?
C22 C20 C21 C27 -177.4(19) . . . . ?
C23 C18 C22 C19 92.3(18) . . . . ?
C17 C18 C22 C19 98(2) . . . . ?
C24 C18 C22 C19 134.7(16) . . . . ?
C23 C18 C22 C21 96(3) . . . . ?
C19 C18 C22 C21 4(2) . . . . ?
C17 C18 C22 C21 102(3) . . . . ?
C24 C18 C22 C21 139(2) . . . . ?
C19 C18 C22 C23 -92.3(18) . . . . ?
C17 C18 C22 C23 5(2) . . . . ?
C24 C18 C22 C23 42.4(15) . . . . ?
C23 C18 C22 C20 135.6(18) . . . . ?
C19 C18 C22 C20 43.3(14) . . . . ?
C17 C18 C22 C20 140.9(18) . . . . ?
C24 C18 C22 C20 177.9(13) . . . . ?
C21 C19 C22 C18 176(2) . . . . ?
C20 C19 C22 C18 121.6(18) . . . . ?
C23 C19 C22 C18 -57.0(16) . . . . ?
C20 C19 C22 C21 -54.0(17) . . . . ?
C18 C19 C22 C21 -176(2) . . . . ?
C23 C19 C22 C21 127(2) . . . . ?
C21 C19 C22 C23 -127(2) . . . . ?
C20 C19 C22 C23 178.5(17) . . . . ?
C18 C19 C22 C23 57.0(16) . . . . ?
C21 C19 C22 C20 54.0(16) . . . . ?
C18 C19 C22 C20 -121.6(18) . . . . ?
C23 C19 C22 C20 -178.5(17) . . . . ?
C19 C21 C22 C18 -5(3) . . . . ?
C20 C21 C22 C18 71(3) . . . . ?
C30 C21 C22 C18 121(3) . . . . ?
C27 C21 C22 C18 74(4) . . . . ?
C20 C21 C22 C19 76(2) . . . . ?
C30 C21 C22 C19 126(3) . . . . ?
C27 C21 C22 C19 80(3) . . . . ?
C19 C21 C22 C23 59(2) . . . . ?
C20 C21 C22 C23 135(2) . . . . ?
C30 C21 C22 C23 -175(2) . . . . ?
C27 C21 C22 C23 138(3) . . . . ?
C19 C21 C22 C20 -76(2) . . . . ?
C30 C21 C22 C20 49.5(19) . . . . ?
C27 C21 C22 C20 3(2) . . . . ?
C24 C17 C23 C18 -97.6(18) . . . . ?
C25 C17 C23 C18 -96(3) . . . . ?
C16 C17 C23 C18 -141.1(18) . . . . ?
C24 C17 C23 C22 -92(3) . . . . ?
C25 C17 C23 C22 -90(3) . . . . ?
C18 C17 C23 C22 6(2) . . . . ?
C16 C17 C23 C22 -136(2) . . . . ?
C25 C17 C23 C24 2(2) . . . . ?
C18 C17 C23 C24 97.6(18) . . . . ?
C16 C17 C23 C24 -43.5(15) . . . . ?
C24 C17 C23 C19 -138(2) . . . . ?
C25 C17 C23 C19 -136(2) . . . . ?
C18 C17 C23 C19 -40.5(15) . . . . ?
C16 C17 C23 C19 178.4(14) . . . . ?
C22 C18 C23 C17 174(2) . . . . ?
C19 C18 C23 C17 -131.1(19) . . . . ?
C24 C18 C23 C17 51.8(16) . . . . ?
C19 C18 C23 C22 55.1(15) . . . . ?
C17 C18 C23 C22 -174(2) . . . . ?
C24 C18 C23 C22 -122(2) . . . . ?
C22 C18 C23 C24 122(2) . . . . ?
C19 C18 C23 C24 177.2(17) . . . . ?
C17 C18 C23 C24 -51.8(16) . . . . ?
C22 C18 C23 C19 -55.1(15) . . . . ?
C17 C18 C23 C19 131.1(19) . . . . ?
C24 C18 C23 C19 -177.2(17) . . . . ?
C18 C22 C23 C17 -7(3) . . . . ?
C19 C22 C23 C17 -85(3) . . . . ?
C21 C22 C23 C17 -124(3) . . . . ?
C20 C22 C23 C17 -83(4) . . . . ?
C19 C22 C23 C18 -77.3(19) . . . . ?
C21 C22 C23 C18 -117(2) . . . . ?
C20 C22 C23 C18 -76(3) . . . . ?
C18 C22 C23 C24 -66(2) . . . . ?
C19 C22 C23 C24 -143(2) . . . . ?
C21 C22 C23 C24 177.7(19) . . . . ?
C20 C22 C23 C24 -141(2) . . . . ?
C18 C22 C23 C19 77.3(19) . . . . ?
C21 C22 C23 C19 -39.2(16) . . . . ?
C20 C22 C23 C19 1.6(19) . . . . ?
C21 C19 C23 C17 174(2) . . . . ?
C22 C19 C23 C17 118(3) . . . . ?
C20 C19 C23 C17 116(3) . . . . ?
C18 C19 C23 C17 52(2) . . . . ?
C21 C19 C23 C18 122(2) . . . . ?
C22 C19 C23 C18 66.1(19) . . . . ?
C20 C19 C23 C18 64(3) . . . . ?
C21 C19 C23 C22 56(2) . . . . ?
C20 C19 C23 C22 -2(3) . . . . ?
C18 C19 C23 C22 -66.1(19) . . . . ?
C21 C19 C23 C24 117(3) . . . . ?
C22 C19 C23 C24 62(3) . . . . ?
C20 C19 C23 C24 59(4) . . . . ?
C18 C19 C23 C24 -4(3) . . . . ?
C23 C17 C24 C25 178(2) . . . . ?
C18 C17 C24 C25 123.5(18) . . . . ?
C16 C17 C24 C25 -58.4(15) . . . . ?
C23 C17 C24 C16 -123.5(19) . . . . ?
C25 C17 C24 C16 58.4(15) . . . . ?
C18 C17 C24 C16 -178.2(16) . . . . ?
C25 C17 C24 C23 -178(2) . . . . ?
C18 C17 C24 C23 -54.7(16) . . . . ?
C16 C17 C24 C23 123.5(19) . . . . ?
C23 C17 C24 C18 54.7(16) . . . . ?
C25 C17 C24 C18 -123.5(18) . . . . ?
C16 C17 C24 C18 178.2(16) . . . . ?
C26 C16 C24 C25 3(2) . . . . ?
C15 C16 C24 C25 -59.5(19) . . . . ?
C17 C16 C24 C25 71.4(18) . . . . ?
C26 C16 C24 C17 -69(2) . . . . ?
C25 C16 C24 C17 -71.4(18) . . . . ?
C15 C16 C24 C17 -130.9(19) . . . . ?
C26 C16 C24 C23 -112(2) . . . . ?
C25 C16 C24 C23 -114(2) . . . . ?
C15 C16 C24 C23 -173.9(18) . . . . ?
C17 C16 C24 C23 -43.0(17) . . . . ?
C26 C16 C24 C18 -71(3) . . . . ?
C25 C16 C24 C18 -74(3) . . . . ?
C15 C16 C24 C18 -133(2) . . . . ?
C17 C16 C24 C18 -2.2(19) . . . . ?
C17 C23 C24 C25 -2(2) . . . . ?
C18 C23 C24 C25 73(3) . . . . ?
C22 C23 C24 C25 116(2) . . . . ?
C19 C23 C24 C25 76(4) . . . . ?
C18 C23 C24 C17 75(2) . . . . ?
C22 C23 C24 C17 118(2) . . . . ?
C19 C23 C24 C17 79(3) . . . . ?
C17 C23 C24 C16 65(2) . . . . ?
C18 C23 C24 C16 140(2) . . . . ?
C22 C23 C24 C16 -177.4(18) . . . . ?
C19 C23 C24 C16 143(3) . . . . ?
C17 C23 C24 C18 -75(2) . . . . ?
C22 C23 C24 C18 43.1(16) . . . . ?
C19 C23 C24 C18 4(2) . . . . ?
C17 C24 C25 C16 97.5(17) . . . . ?
C23 C24 C25 C16 99(2) . . . . ?
C18 C24 C25 C16 139.7(17) . . . . ?
C16 C24 C25 C17 -97.5(17) . . . . ?
C23 C24 C25 C17 1.6(19) . . . . ?
C18 C24 C25 C17 42.1(14) . . . . ?
C17 C24 C25 C26 95(2) . . . . ?
C16 C24 C25 C26 -3(2) . . . . ?
C23 C24 C25 C26 97(3) . . . . ?
C18 C24 C25 C26 137.1(18) . . . . ?
C17 C24 C25 C15 139.0(18) . . . . ?
C16 C24 C25 C15 41.5(15) . . . . ?
C23 C24 C25 C15 140.7(19) . . . . ?
C18 C24 C25 C15 -178.8(13) . . . . ?
C26 C16 C25 C24 -177(2) . . . . ?
C15 C16 C25 C24 126.4(19) . . . . ?
C17 C16 C25 C24 -54.6(16) . . . . ?
C26 C16 C25 C17 -122.7(18) . . . . ?
C24 C16 C25 C17 54.6(16) . . . . ?
C15 C16 C25 C17 -178.9(17) . . . . ?
C24 C16 C25 C26 177(2) . . . . ?
C15 C16 C25 C26 -56.2(14) . . . . ?
C17 C16 C25 C26 122.7(18) . . . . ?
C26 C16 C25 C15 56.2(14) . . . . ?
C24 C16 C25 C15 -126.4(19) . . . . ?
C17 C16 C25 C15 178.9(17) . . . . ?
C23 C17 C25 C24 -2(3) . . . . ?
C18 C17 C25 C24 -68(2) . . . . ?
C16 C17 C25 C24 70.7(18) . . . . ?
C23 C17 C25 C16 -73(3) . . . . ?
C24 C17 C25 C16 -70.7(18) . . . . ?
C18 C17 C25 C16 -138.4(19) . . . . ?
C23 C17 C25 C26 -120(3) . . . . ?
C24 C17 C25 C26 -118(2) . . . . ?
C18 C17 C25 C26 174.7(17) . . . . ?
C16 C17 C25 C26 -46.9(16) . . . . ?
C23 C17 C25 C15 -74(4) . . . . ?
C24 C17 C25 C15 -72(3) . . . . ?
C18 C17 C25 C15 -140(2) . . . . ?
C16 C17 C25 C15 -1(2) . . . . ?
C25 C16 C26 C15 -95.7(16) . . . . ?
C24 C16 C26 C15 -98(2) . . . . ?
C17 C16 C26 C15 -136.0(17) . . . . ?
C24 C16 C26 C25 -2.3(18) . . . . ?
C15 C16 C26 C25 95.7(16) . . . . ?
C17 C16 C26 C25 -40.3(13) . . . . ?
C25 C16 C26 C12 -97(2) . . . . ?
C24 C16 C26 C12 -99(3) . . . . ?
C15 C16 C26 C12 -1(2) . . . . ?
C17 C16 C26 C12 -137.0(19) . . . . ?
C25 C16 C26 C14 -137.7(17) . . . . ?
C24 C16 C26 C14 -140.0(18) . . . . ?
C15 C16 C26 C14 -42.0(14) . . . . ?
C17 C16 C26 C14 -178.0(13) . . . . ?
C12 C15 C26 C16 -179(2) . . . . ?
C14 C15 C26 C16 -123.0(18) . . . . ?
C25 C15 C26 C16 56.6(15) . . . . ?
C12 C15 C26 C25 124.3(17) . . . . ?
C14 C15 C26 C25 -179.7(17) . . . . ?
C16 C15 C26 C25 -56.6(15) . . . . ?
C14 C15 C26 C12 56.0(14) . . . . ?
C16 C15 C26 C12 179(2) . . . . ?
C25 C15 C26 C12 -124.3(17) . . . . ?
C12 C15 C26 C14 -56.0(14) . . . . ?
C16 C15 C26 C14 123.0(18) . . . . ?
C25 C15 C26 C14 179.7(17) . . . . ?
C24 C25 C26 C16 3(2) . . . . ?
C17 C25 C26 C16 65(2) . . . . ?
C15 C25 C26 C16 -71.6(18) . . . . ?
C24 C25 C26 C15 75(3) . . . . ?
C16 C25 C26 C15 71.6(18) . . . . ?
C17 C25 C26 C15 137(2) . . . . ?
C24 C25 C26 C12 122(2) . . . . ?
C16 C25 C26 C12 119(2) . . . . ?
C17 C25 C26 C12 -175.6(17) . . . . ?
C15 C25 C26 C12 47.5(16) . . . . ?
C24 C25 C26 C14 74(3) . . . . ?
C16 C25 C26 C14 71(2) . . . . ?
C17 C25 C26 C14 137(2) . . . . ?
C15 C25 C26 C14 -0.4(19) . . . . ?
C15 C12 C26 C16 1(2) . . . . ?
C14 C12 C26 C16 -67(2) . . . . ?
C11 C12 C26 C16 -117(2) . . . . ?
C13 C12 C26 C16 -69(3) . . . . ?
C14 C12 C26 C15 -68.2(17) . . . . ?
C11 C12 C26 C15 -118(2) . . . . ?
C13 C12 C26 C15 -71(2) . . . . ?
C15 C12 C26 C25 -64(2) . . . . ?
C14 C12 C26 C25 -132.2(19) . . . . ?
C11 C12 C26 C25 177.6(16) . . . . ?
C13 C12 C26 C25 -135(2) . . . . ?
C15 C12 C26 C14 68.2(17) . . . . ?
C11 C12 C26 C14 -50.2(15) . . . . ?
C13 C12 C26 C14 -2.3(19) . . . . ?
C30 C20 C27 C29 -2(2) . . . . ?
C21 C20 C27 C29 -69(3) . . . . ?
C19 C20 C27 C29 -108(3) . . . . ?
C22 C20 C27 C29 -66(4) . . . . ?
C21 C20 C27 C30 -67(2) . . . . ?
C19 C20 C27 C30 -106(2) . . . . ?
C22 C20 C27 C30 -64(3) . . . . ?
C30 C20 C27 C28 -64(2) . . . . ?
C21 C20 C27 C28 -131(2) . . . . ?
C19 C20 C27 C28 -170.1(19) . . . . ?
C22 C20 C27 C28 -128(2) . . . . ?
C30 C20 C27 C21 67(2) . . . . ?
C19 C20 C27 C21 -39.2(17) . . . . ?
C22 C20 C27 C21 3(2) . . . . ?
C30 C27 C28 C29 67(2) . . . . ?
C20 C27 C28 C29 113(2) . . . . ?
C21 C27 C28 C29 70(3) . . . . ?
C29 C27 C28 C30 -67(2) . . . . ?
C20 C27 C28 C30 46.2(18) . . . . ?
C21 C27 C28 C30 3(2) . . . . ?
C30 C27 C29 C28 -99(2) . . . . ?
C20 C27 C29 C28 -97(2) . . . . ?
C21 C27 C29 C28 -135.8(19) . . . . ?
C20 C27 C29 C30 2(2) . . . . ?
C28 C27 C29 C30 99(2) . . . . ?
C21 C27 C29 C30 -37.3(16) . . . . ?
C30 C28 C29 C27 56.5(16) . . . . ?
C27 C28 C29 C30 -56.5(16) . . . . ?
C21 C20 C30 C27 101.5(19) . . . . ?
C19 C20 C30 C27 103(2) . . . . ?
C22 C20 C30 C27 142.1(18) . . . . ?
C21 C20 C30 C29 103(3) . . . . ?
C27 C20 C30 C29 2(2) . . . . ?
C19 C20 C30 C29 105(3) . . . . ?
C22 C20 C30 C29 144(2) . . . . ?
C27 C20 C30 C21 -101.5(19) . . . . ?
C19 C20 C30 C21 1.9(18) . . . . ?
C22 C20 C30 C21 40.6(15) . . . . ?
C21 C20 C30 C28 145(2) . . . . ?
C27 C20 C30 C28 43.1(16) . . . . ?
C19 C20 C30 C28 146.5(18) . . . . ?
C22 C20 C30 C28 -174.8(15) . . . . ?
C29 C27 C30 C20 178(2) . . . . ?
C28 C27 C30 C20 123(2) . . . . ?
C21 C27 C30 C20 -53.6(15) . . . . ?
C20 C27 C30 C29 -178(2) . . . . ?
C28 C27 C30 C29 -55.0(17) . . . . ?
C21 C27 C30 C29 128(2) . . . . ?
C29 C27 C30 C21 -128(2) . . . . ?
C20 C27 C30 C21 53.6(15) . . . . ?
C28 C27 C30 C21 177(2) . . . . ?
C29 C27 C30 C28 55.0(17) . . . . ?
C20 C27 C30 C28 -123(2) . . . . ?
C21 C27 C30 C28 -177(2) . . . . ?
C27 C29 C30 C20 -2(3) . . . . ?
C28 C29 C30 C20 68(3) . . . . ?
C28 C29 C30 C27 70(2) . . . . ?
C27 C29 C30 C21 64(2) . . . . ?
C28 C29 C30 C21 135(2) . . . . ?
C27 C29 C30 C28 -70(2) . . . . ?
C19 C21 C30 C20 -3(3) . . . . ?
C22 C21 C30 C20 -69(2) . . . . ?
C27 C21 C30 C20 68(2) . . . . ?
C19 C21 C30 C27 -71(3) . . . . ?
C20 C21 C30 C27 -68(2) . . . . ?
C22 C21 C30 C27 -137(2) . . . . ?
C19 C21 C30 C29 -119(3) . . . . ?
C20 C21 C30 C29 -116(3) . . . . ?
C22 C21 C30 C29 175(2) . . . . ?
C27 C21 C30 C29 -48(2) . . . . ?
C19 C21 C30 C28 -67(5) . . . . ?
C20 C21 C30 C28 -64(3) . . . . ?
C22 C21 C30 C28 -133(3) . . . . ?
C27 C21 C30 C28 4(3) . . . . ?
C13 C10 C31 N5 -174.8(17) . . . . ?
C11 C10 C31 N5 -119.5(13) . . . . ?
N5 C10 C31 C13 174.8(17) . . . . ?
C11 C10 C31 C13 55.3(13) . . . . ?
N5 C10 C31 C1 -33.2(10) . . . . ?
C13 C10 C31 C1 152.0(17) . . . . ?
C11 C10 C31 C1 -152.7(14) . . . . ?
N5 C10 C31 C11 119.5(13) . . . . ?
C13 C10 C31 C11 -55.3(13) . . . . ?
C1 N5 C31 C10 -130.5(14) . . . . ?
Co1 N5 C31 C10 116.1(15) 2_656 . . . ?
C1 N5 C31 C13 -135(2) . . . . ?
C10 N5 C31 C13 -4.9(16) . . . . ?
Co1 N5 C31 C13 111(2) 2_656 . . . ?
C10 N5 C31 C1 130.5(14) . . . . ?
Co1 N5 C31 C1 -113.5(15) 2_656 . . . ?
C1 N5 C31 C11 -172.8(14) . . . . ?
C10 N5 C31 C11 -42.3(10) . . . . ?
Co1 N5 C31 C11 73.8(17) 2_656 . . . ?
C11 C13 C31 C10 -63.8(13) . . . . ?
C14 C13 C31 C10 -112.0(19) . . . . ?
C12 C13 C31 C10 -63(2) . . . . ?
C11 C13 C31 N5 -59.0(19) . . . . ?
C14 C13 C31 N5 -107(2) . . . . ?
C10 C13 C31 N5 4.8(16) . . . . ?
C12 C13 C31 N5 -58(3) . . . . ?
C11 C13 C31 C1 -110(3) . . . . ?
C14 C13 C31 C1 -158(2) . . . . ?
C10 C13 C31 C1 -46(2) . . . . ?
C12 C13 C31 C1 -109(3) . . . . ?
C14 C13 C31 C11 -48.2(15) . . . . ?
C10 C13 C31 C11 63.8(13) . . . . ?
C12 C13 C31 C11 1.3(19) . . . . ?
N3 N4 C32 C40 123.5(18) . . . . ?
C9 N4 C32 C40 122.5(19) . . . . ?
C33 N4 C32 C40 70.7(17) . . . . ?
Co1 N4 C32 C40 -62(2) 2_656 . . . ?
N3 N4 C32 C33 52.8(17) . . . . ?
C9 N4 C32 C33 51.8(12) . . . . ?
Co1 N4 C32 C33 -133.0(13) 2_656 . . . ?
N3 N4 C32 O1 -124.1(16) . . . . ?
C9 N4 C32 O1 -125.1(15) . . . . ?
C33 N4 C32 O1 -176.9(17) . . . . ?
Co1 N4 C32 O1 50.1(17) 2_656 . . . ?
N3 N4 C32 C34 56(2) . . . . ?
C9 N4 C32 C34 55.1(18) . . . . ?
C33 N4 C32 C34 3.3(15) . . . . ?
Co1 N4 C32 C34 -129.7(15) 2_656 . . . ?
N3 N4 C32 C9 1.0(15) . . . . ?
C33 N4 C32 C9 -51.8(11) . . . . ?
Co1 N4 C32 C9 175.3(14) 2_656 . . . ?
N3 C9 C33 C34 164.1(19) . . . . ?
N4 C9 C33 C34 112.2(17) . . . . ?
C32 C9 C33 C34 60.4(16) . . . . ?
N3 C9 C33 C32 104(2) . . . . ?
N4 C9 C33 C32 51.8(11) . . . . ?
N3 C9 C33 N4 51.9(16) . . . . ?
C32 C9 C33 N4 -51.8(11) . . . . ?
N4 C32 C33 C9 -61.8(12) . . . . ?
C40 C32 C33 C9 -179.7(17) . . . . ?
O1 C32 C33 C9 -49(7) . . . . ?
C34 C32 C33 C9 121.6(16) . . . . ?
N4 C32 C33 C34 176.6(16) . . . . ?
C40 C32 C33 C34 58.7(14) . . . . ?
O1 C32 C33 C34 -171(7) . . . . ?
C9 C32 C33 C34 -121.6(16) . . . . ?
C40 C32 C33 N4 -117.9(16) . . . . ?
O1 C32 C33 N4 12(7) . . . . ?
C34 C32 C33 N4 -176.6(16) . . . . ?
C9 C32 C33 N4 61.8(12) . . . . ?
N3 N4 C33 C9 -37.4(13) . . . . ?
C32 N4 C33 C9 100.2(16) . . . . ?
Co1 N4 C33 C9 -147.9(16) 2_656 . . . ?
N3 N4 C33 C34 -141.2(17) . . . . ?
C32 N4 C33 C34 -3.6(17) . . . . ?
C9 N4 C33 C34 -104(2) . . . . ?
Co1 N4 C33 C34 108.3(18) 2_656 . . . ?
N3 N4 C33 C32 -137.6(15) . . . . ?
C9 N4 C33 C32 -100.2(16) . . . . ?
Co1 N4 C33 C32 112.0(16) 2_656 . . . ?
C35 N6 C34 C33 116.9(19) . . . . ?
C39 N6 C34 C33 178.3(16) . . . . ?
C40 N6 C34 C33 61.2(18) . . . . ?
C35 N6 C34 C40 55.6(15) . . . . ?
C39 N6 C34 C40 117(2) . . . . ?
C35 N6 C34 C32 54.8(19) . . . . ?
C39 N6 C34 C32 116.3(19) . . . . ?
C40 N6 C34 C32 -0.8(17) . . . . ?
C39 N6 C34 C35 61.5(17) . . . . ?
C40 N6 C34 C35 -55.6(15) . . . . ?
C9 C33 C34 N6 -171.2(18) . . . . ?
C32 C33 C34 N6 -103.7(19) . . . . ?
N4 C33 C34 N6 -101(2) . . . . ?
C9 C33 C34 C40 -120.5(19) . . . . ?
C32 C33 C34 C40 -53.0(13) . . . . ?
N4 C33 C34 C40 -49.9(17) . . . . ?
C9 C33 C34 C32 -67.5(17) . . . . ?
N4 C33 C34 C32 3.1(14) . . . . ?
C9 C33 C34 C35 -118(2) . . . . ?
C32 C33 C34 C35 -50.4(19) . . . . ?
N4 C33 C34 C35 -47(2) . . . . ?
N4 C32 C34 N6 99(2) . . . . ?
C40 C32 C34 N6 0.8(19) . . . . ?
C33 C32 C34 N6 103(2) . . . . ?
O1 C32 C34 N6 -80(3) . . . . ?
C9 C32 C34 N6 141.1(18) . . . . ?
N4 C32 C34 C33 -3.7(17) . . . . ?
C40 C32 C34 C33 -102.1(17) . . . . ?
O1 C32 C34 C33 177(3) . . . . ?
C9 C32 C34 C33 38.2(12) . . . . ?
N4 C32 C34 C40 98(2) . . . . ?
C33 C32 C34 C40 102.1(17) . . . . ?
O1 C32 C34 C40 -81(3) . . . . ?
C9 C32 C34 C40 140.2(16) . . . . ?
N4 C32 C34 C35 136.7(18) . . . . ?
C40 C32 C34 C35 38.3(13) . . . . ?
C33 C32 C34 C35 140.4(15) . . . . ?
O1 C32 C34 C35 -43(3) . . . . ?
C9 C32 C34 C35 178.5(12) . . . . ?
C34 N6 C35 C40 -66.2(15) . . . . ?
C39 N6 C35 C40 176.0(18) . . . . ?
C34 N6 C35 C36 174.8(17) . . . . ?
C39 N6 C35 C36 57.0(13) . . . . ?
C40 N6 C35 C36 -119.1(18) . . . . ?
C34 N6 C35 C39 117.8(17) . . . . ?
C40 N6 C35 C39 -176.0(18) . . . . ?
C39 N6 C35 C34 -117.8(17) . . . . ?
C40 N6 C35 C34 66.2(15) . . . . ?
C40 C35 C36 C38 176(2) . . . . ?
N6 C35 C36 C38 -125(2) . . . . ?
C39 C35 C36 C38 -67(2) . . . . ?
C34 C35 C36 C38 -120(2) . . . . ?
C40 C35 C36 C37 -117(2) . . . . ?
N6 C35 C36 C37 -57(2) . . . . ?
C39 C35 C36 C37 0.0(18) . . . . ?
C34 C35 C36 C37 -52(3) . . . . ?
C40 C35 C36 C39 -117(2) . . . . ?
N6 C35 C36 C39 -57.2(14) . . . . ?
C34 C35 C36 C39 -52(2) . . . . ?
C35 C36 C37 C38 -103(2) . . . . ?
C39 C36 C37 C38 -103(2) . . . . ?
C38 C36 C37 C47 0(2) . . . . ?
C35 C36 C37 C47 -103(3) . . . . ?
C39 C36 C37 C47 -103(3) . . . . ?
C38 C36 C37 C39 103(2) . . . . ?
C35 C36 C37 C39 0.0(19) . . . . ?
C38 C36 C37 C41 -40.2(17) . . . . ?
C35 C36 C37 C41 -143.6(19) . . . . ?
C39 C36 C37 C41 -143.6(17) . . . . ?
C47 C37 C38 C36 180(2) . . . . ?
C39 C37 C38 C36 -58.7(15) . . . . ?
C41 C37 C38 C36 119(2) . . . . ?
C47 C37 C38 C41 60.6(17) . . . . ?
C39 C37 C38 C41 -178.1(19) . . . . ?
C36 C37 C38 C41 -119(2) . . . . ?
C39 C37 C38 C47 121.4(19) . . . . ?
C36 C37 C38 C47 -180(2) . . . . ?
C41 C37 C38 C47 -60.6(17) . . . . ?
C47 C37 C38 C39 -121.4(19) . . . . ?
C36 C37 C38 C39 58.7(15) . . . . ?
C41 C37 C38 C39 178.1(19) . . . . ?
C35 C36 C38 C37 115(2) . . . . ?
C39 C36 C38 C37 56.8(17) . . . . ?
C35 C36 C38 C41 -172(2) . . . . ?
C37 C36 C38 C41 73(2) . . . . ?
C39 C36 C38 C41 130(3) . . . . ?
C35 C36 C38 C47 115(3) . . . . ?
C37 C36 C38 C47 0(2) . . . . ?
C39 C36 C38 C47 57(3) . . . . ?
C35 C36 C38 C39 58.1(19) . . . . ?
C37 C36 C38 C39 -56.8(17) . . . . ?
C38 C37 C39 C36 57.6(18) . . . . ?
C47 C37 C39 C36 116(2) . . . . ?
C41 C37 C39 C36 56(2) . . . . ?
C38 C37 C39 N6 119(2) . . . . ?
C47 C37 C39 N6 177.6(18) . . . . ?
C36 C37 C39 N6 61.7(17) . . . . ?
C41 C37 C39 N6 117(2) . . . . ?
C38 C37 C39 C35 58(2) . . . . ?
C47 C37 C39 C35 116(2) . . . . ?
C36 C37 C39 C35 0.0(16) . . . . ?
C41 C37 C39 C35 56(3) . . . . ?
C47 C37 C39 C38 58(2) . . . . ?
C36 C37 C39 C38 -57.6(18) . . . . ?
C41 C37 C39 C38 -2(2) . . . . ?
C38 C36 C39 C37 -55.1(16) . . . . ?
C35 C36 C39 C37 -180.0(17) . . . . ?
C38 C36 C39 N6 179.8(18) . . . . ?
C35 C36 C39 N6 54.9(13) . . . . ?
C37 C36 C39 N6 -125.1(17) . . . . ?
C38 C36 C39 C35 124.9(18) . . . . ?
C37 C36 C39 C35 180.0(17) . . . . ?
C35 C36 C39 C38 -124.9(18) . . . . ?
C37 C36 C39 C38 55.1(16) . . . . ?
C34 N6 C39 C37 -179.8(18) . . . . ?
C35 N6 C39 C37 -105.8(19) . . . . ?
C40 N6 C39 C37 -102(2) . . . . ?
C34 N6 C39 C36 -128.9(19) . . . . ?
C35 N6 C39 C36 -55.0(14) . . . . ?
C40 N6 C39 C36 -51(2) . . . . ?
C34 N6 C39 C35 -73.9(19) . . . . ?
C40 N6 C39 C35 3.9(18) . . . . ?
C34 N6 C39 C38 -129(2) . . . . ?
C35 N6 C39 C38 -55(2) . . . . ?
C40 N6 C39 C38 -51(3) . . . . ?
C40 C35 C39 C37 98(2) . . . . ?
N6 C35 C39 C37 102(2) . . . . ?
C36 C35 C39 C37 0.0(17) . . . . ?
C34 C35 C39 C37 142.3(17) . . . . ?
C40 C35 C39 C36 98(2) . . . . ?
N6 C35 C39 C36 102.3(17) . . . . ?
C34 C35 C39 C36 142.2(15) . . . . ?
C40 C35 C39 N6 -4(2) . . . . ?
C36 C35 C39 N6 -102.3(17) . . . . ?
C34 C35 C39 N6 40.0(13) . . . . ?
C40 C35 C39 C38 135(2) . . . . ?
N6 C35 C39 C38 139.2(17) . . . . ?
C36 C35 C39 C38 36.9(13) . . . . ?
C34 C35 C39 C38 179.2(13) . . . . ?
C36 C35 C40 N6 70.6(19) . . . . ?
C39 C35 C40 N6 4.1(19) . . . . ?
C34 C35 C40 N6 -52.6(15) . . . . ?
N6 C35 C40 C32 111(2) . . . . ?
C36 C35 C40 C32 -178.5(18) . . . . ?
C39 C35 C40 C32 115(2) . . . . ?
C34 C35 C40 C32 58.4(17) . . . . ?
N6 C35 C40 C34 52.6(15) . . . . ?
C36 C35 C40 C34 123(2) . . . . ?
C39 C35 C40 C34 57(2) . . . . ?
C34 N6 C40 C35 100.1(18) . . . . ?
C39 N6 C40 C35 -4(2) . . . . ?
C34 N6 C40 C32 1(2) . . . . ?
C35 N6 C40 C32 -99(2) . . . . ?
C39 N6 C40 C32 -103(2) . . . . ?
C35 N6 C40 C34 -100.1(18) . . . . ?
C39 N6 C40 C34 -104(2) . . . . ?
N4 C32 C40 C35 179.5(18) . . . . ?
C33 C32 C40 C35 -119(2) . . . . ?
O1 C32 C40 C35 72(2) . . . . ?
C34 C32 C40 C35 -64.9(19) . . . . ?
C9 C32 C40 C35 -119(2) . . . . ?
N4 C32 C40 N6 -116(2) . . . . ?
C33 C32 C40 N6 -55(2) . . . . ?
O1 C32 C40 N6 136(2) . . . . ?
C34 C32 C40 N6 -0.8(18) . . . . ?
C9 C32 C40 N6 -55(3) . . . . ?
N4 C32 C40 C34 -115.6(19) . . . . ?
C33 C32 C40 C34 -54.3(13) . . . . ?
O1 C32 C40 C34 137.0(17) . . . . ?
C9 C32 C40 C34 -55(2) . . . . ?
N6 C34 C40 C35 -58.3(15) . . . . ?
C33 C34 C40 C35 177.0(17) . . . . ?
C32 C34 C40 C35 120.8(18) . . . . ?
C33 C34 C40 N6 -124.7(18) . . . . ?
C32 C34 C40 N6 179(2) . . . . ?
C35 C34 C40 N6 58.3(15) . . . . ?
N6 C34 C40 C32 -179(2) . . . . ?
C33 C34 C40 C32 56.2(13) . . . . ?
C35 C34 C40 C32 -120.8(18) . . . . ?
C37 C38 C41 B6 -58(3) . . . . ?
C36 C38 C41 B6 -117(3) . . . . ?
C47 C38 C41 B6 -1(2) . . . . ?
C39 C38 C41 B6 -60(4) . . . . ?
C37 C38 C41 C47 -56.4(18) . . . . ?
C36 C38 C41 C47 -115(3) . . . . ?
C39 C38 C41 C47 -58(3) . . . . ?
C37 C38 C41 C42 -116(2) . . . . ?
C36 C38 C41 C42 -175(2) . . . . ?
C47 C38 C41 C42 -59(2) . . . . ?
C39 C38 C41 C42 -118(3) . . . . ?
C36 C38 C41 C37 -59(2) . . . . ?
C47 C38 C41 C37 56.4(18) . . . . ?
C39 C38 C41 C37 -2(2) . . . . ?
C38 C41 C42 B5 116(3) . . . . ?
B6 C41 C42 B5 4(2) . . . . ?
C47 C41 C42 B5 67(3) . . . . ?
C37 C41 C42 B5 67(3) . . . . ?
C38 C41 C42 B6 112(2) . . . . ?
C47 C41 C42 B6 62.8(18) . . . . ?
C37 C41 C42 B6 63(2) . . . . ?
C38 C41 C42 C43 -179(2) . . . . ?
B6 C41 C42 C43 69(2) . . . . ?
C47 C41 C42 C43 132(2) . . . . ?
C37 C41 C42 C43 132(2) . . . . ?
C38 C41 C42 C47 49(2) . . . . ?
B6 C41 C42 C47 -62.8(18) . . . . ?
C37 C41 C42 C47 0.2(16) . . . . ?
B6 C42 C43 B5 -62(2) . . . . ?
C41 C42 C43 B5 -117(2) . . . . ?
C47 C42 C43 B5 -65(3) . . . . ?
B5 C42 C43 B2 -3(3) . . . . ?
B6 C42 C43 B2 -65(3) . . . . ?
C41 C42 C43 B2 -120(3) . . . . ?
C47 C42 C43 B2 -68(4) . . . . ?
B5 C42 C43 C46 -69(2) . . . . ?
B6 C42 C43 C46 -131(2) . . . . ?
C41 C42 C43 C46 174.2(19) . . . . ?
C47 C42 C43 C46 -134(2) . . . . ?
B5 C42 C43 B6 62(2) . . . . ?
C41 C42 C43 B6 -54.8(18) . . . . ?
C47 C42 C43 B6 -3(2) . . . . ?
C45 N7 C44 B4 63(2) . . . . ?
B3 N7 C44 B4 -67(2) . . . . ?
B4 N7 C44 B3 67(2) . . . . ?
C45 N7 C44 B3 130(2) . . . . ?
B4 N7 C44 C46 117(2) . . . . ?
C45 N7 C44 C46 179.9(18) . . . . ?
B3 N7 C44 C46 50.1(19) . . . . ?
B4 N7 C44 B2 69(3) . . . . ?
C45 N7 C44 B2 132(2) . . . . ?
B3 N7 C44 B2 2(2) . . . . ?
B4 N7 C45 C6 -116(2) . . . . ?
C44 N7 C45 C6 -161.1(18) . . . . ?
B3 N7 C45 C6 -115(2) . . . . ?
C44 N7 C45 B4 -45.2(18) . . . . ?
B3 N7 C45 B4 1(2) . . . . ?
C5 C6 C45 N7 15(4) 3_776 . . . ?
F2 C6 C45 N7 68(2) 3_776 . . . ?
C5 C6 C45 B4 -39(4) 3_776 . . . ?
F2 C6 C45 B4 15(3) 3_776 . . . ?
B4 C44 C46 B3 -1(3) . . . . ?
N7 C44 C46 B3 -71(2) . . . . ?
B2 C44 C46 B3 63(2) . . . . ?
B4 C44 C46 B2 -63(3) . . . . ?
B3 C44 C46 B2 -63(2) . . . . ?
N7 C44 C46 B2 -134(2) . . . . ?
B4 C44 C46 C43 -112(3) . . . . ?
B3 C44 C46 C43 -111(3) . . . . ?
N7 C44 C46 C43 177.4(19) . . . . ?
B2 C44 C46 C43 -49(2) . . . . ?
B4 C44 C46 B5 -65(3) . . . . ?
B3 C44 C46 B5 -64(3) . . . . ?
N7 C44 C46 B5 -136(2) . . . . ?
B2 C44 C46 B5 -2(2) . . . . ?
B5 C43 C46 B3 65(3) . . . . ?
B2 C43 C46 B3 2(3) . . . . ?
C42 C43 C46 B3 117(3) . . . . ?
B6 C43 C46 B3 62(4) . . . . ?
B5 C43 C46 B2 63(2) . . . . ?
C42 C43 C46 B2 115(3) . . . . ?
B6 C43 C46 B2 60(3) . . . . ?
B5 C43 C46 C44 127(2) . . . . ?
B2 C43 C46 C44 64(2) . . . . ?
C42 C43 C46 C44 179(2) . . . . ?
B6 C43 C46 C44 124(3) . . . . ?
B2 C43 C46 B5 -63(2) . . . . ?
C42 C43 C46 B5 52(2) . . . . ?
B6 C43 C46 B5 -3(2) . . . . ?
C39 C37 C47 C38 -71(2) . . . . ?
C36 C37 C47 C38 0(2) . . . . ?
C41 C37 C47 C38 55.5(19) . . . . ?
C38 C37 C47 C41 -55.5(19) . . . . ?
C39 C37 C47 C41 -127(2) . . . . ?
C36 C37 C47 C41 -55(2) . . . . ?
C38 C37 C47 B6 -106(2) . . . . ?
C39 C37 C47 B6 -177.3(19) . . . . ?
C36 C37 C47 B6 -106(3) . . . . ?
C41 C37 C47 B6 -50.4(18) . . . . ?
C38 C37 C47 C42 -55(3) . . . . ?
C39 C37 C47 C42 -127(2) . . . . ?
C36 C37 C47 C42 -55(4) . . . . ?
C41 C37 C47 C42 0(2) . . . . ?
C36 C38 C47 C37 0(2) . . . . ?
C41 C38 C47 C37 -104(2) . . . . ?
C39 C38 C47 C37 39.6(15) . . . . ?
C37 C38 C47 C41 104(2) . . . . ?
C36 C38 C47 C41 104(3) . . . . ?
C39 C38 C47 C41 143.3(19) . . . . ?
C37 C38 C47 B6 105(2) . . . . ?
C36 C38 C47 B6 105(3) . . . . ?
C41 C38 C47 B6 1(2) . . . . ?
C39 C38 C47 B6 144.7(18) . . . . ?
C37 C38 C47 C42 145.2(19) . . . . ?
C36 C38 C47 C42 145(2) . . . . ?
C41 C38 C47 C42 41.5(15) . . . . ?
C39 C38 C47 C42 -175.2(14) . . . . ?
C38 C41 C47 C37 55.6(18) . . . . ?
B6 C41 C47 C37 -126(2) . . . . ?
C42 C41 C47 C37 179.8(18) . . . . ?
B6 C41 C47 C38 179(2) . . . . ?
C42 C41 C47 C38 124(2) . . . . ?
C37 C41 C47 C38 -55.6(18) . . . . ?
C38 C41 C47 B6 -179(2) . . . . ?
C42 C41 C47 B6 -54.4(15) . . . . ?
C37 C41 C47 B6 126(2) . . . . ?
C38 C41 C47 C42 -124(2) . . . . ?
B6 C41 C47 C42 54.4(15) . . . . ?
C37 C41 C47 C42 -179.8(18) . . . . ?
C9 N3 C48 Co1 168(12) . . . . ?
N4 N3 C48 Co1 -2(2) . . . . ?
C8 N3 C48 Co1 179(2) . . . . ?
C9 N3 C48 C8 -11(13) . . . . ?
N4 N3 C48 C8 179.6(17) . . . . ?
Co1 N3 C48 C8 -179(2) . . . . ?
C9 N3 C48 N2 -15(14) . . . . ?
N4 N3 C48 N2 175.2(14) . . . . ?
C8 N3 C48 N2 -4.4(16) . . . . ?
Co1 N3 C48 N2 177(3) . . . . ?
F1 Co1 C48 N3 174.1(15) . . . . ?
Co1 Co1 C48 N3 1(2) 2_656 . . . ?
N4 Co1 C48 N3 -71.6(17) 2_656 . . . ?
N5 Co1 C48 N3 84.6(17) 2_656 . . . ?
C1 Co1 C48 N3 174.9(11) . . . . ?
F1 Co1 C48 N2 -3(2) . . . . ?
Co1 Co1 C48 N2 -175.6(11) 2_656 . . . ?
N4 Co1 C48 N2 111.5(17) 2_656 . . . ?
N5 Co1 C48 N2 -92.3(17) 2_656 . . . ?
N3 Co1 C48 N2 -177(3) . . . . ?
C1 Co1 C48 N2 -2(3) . . . . ?
N2 C8 C48 N3 -175.2(17) . . . . ?
N3 C8 C48 N2 175.2(17) . . . . ?
C2 N2 C48 N3 -168(2) . . . . ?
C8 N2 C48 N3 5.3(19) . . . . ?
C2 N2 C48 Co1 8(3) . . . . ?
C8 N2 C48 Co1 -178(2) . . . . ?
C2 N2 C48 C8 -174(2) . . . . ?
F2 C5 C49 C50 82(6) . . . . ?
F3 C5 C49 C50 -156(3) . . . . ?
C6 C5 C49 C50 107(3) 3_776 . . . ?
C4 C5 C49 C50 -67(3) . . . . ?
C51 C5 C49 C50 13(2) . . . . ?
C5 C49 C50 C51 -93(8) . . . . ?
C5 C49 C50 C4 54.7(19) . . . . ?
F2 C5 C50 C49 -153(3) . . . . ?
F3 C5 C50 C49 29(3) . . . . ?
C6 C5 C50 C49 -76(3) 3_776 . . . ?
C4 C5 C50 C49 113(2) . . . . ?
C51 C5 C50 C49 -161(3) . . . . ?
F2 C5 C50 C51 8(4) . . . . ?
F3 C5 C50 C51 -170(3) . . . . ?
C6 C5 C50 C51 85(2) 3_776 . . . ?
C4 C5 C50 C51 -86(2) . . . . ?
C49 C5 C50 C51 161(3) . . . . ?
F2 C5 C50 C4 94(3) . . . . ?
F3 C5 C50 C4 -84(2) . . . . ?
C6 C5 C50 C4 171(2) 3_776 . . . ?
C51 C5 C50 C4 86(2) . . . . ?
C49 C5 C50 C4 -113(2) . . . . ?
C49 C50 C51 C5 95(8) . . . . ?
C4 C50 C51 C5 -55.7(16) . . . . ?
F2 C5 C51 C50 -174(3) . . . . ?
F3 C5 C51 C50 37(8) . . . . ?
C6 C5 C51 C50 -100(2) 3_776 . . . ?
C4 C5 C51 C50 88(2) . . . . ?
C49 C5 C51 C50 -11.7(19) . . . . ?
C2 N1 C52 F1 -20(6) . . . . ?
C3 N1 C52 F1 -170.8(15) . . . . ?
C2 N1 C52 C1 -20(6) . . . . ?
C3 N1 C52 C1 -171.0(15) . . . . ?
F1 N1 C52 C1 -0.2(14) . . . . ?
Co1 F1 C52 N1 -35(7) . . . . ?
C1 F1 C52 N1 -179.8(16) . . . . ?
Co1 F1 C52 C1 145(7) . . . . ?
N1 F1 C52 C1 179.8(16) . . . . ?
F1 C1 C52 N1 0.2(18) . . . . ?
C31 C1 C52 N1 -129(2) . . . . ?
Co1 C1 C52 N1 -4(2) . . . . ?
C31 C1 C52 F1 -130(2) . . . . ?
Co1 C1 C52 F1 -4.5(9) . . . . ?
N1 C3 B1 C7 -3(2) . . . . ?
C2 C3 B1 C7 4.2(18) . . . . ?
N1 C3 B1 C4 -143.9(19) . . . . ?
C2 C3 B1 C4 -136(2) . . . . ?
N1 C3 B1 C2 -7.7(14) . . . . ?
F2 C7 B1 C3 171.3(17) . . . . ?
N2 C7 B1 C3 1(3) . . . . ?
C2 C7 B1 C3 -4.3(18) . . . . ?
F2 C7 B1 C4 -43(2) . . . . ?
N2 C7 B1 C4 146.1(17) . . . . ?
C2 C7 B1 C4 141.3(19) . . . . ?
F2 C7 B1 C2 175.6(16) . . . . ?
N2 C7 B1 C2 4.9(14) . . . . ?
C5 C4 B1 C3 164.7(17) . . . . ?
C50 C4 B1 C3 -168(2) . . . . ?
C5 C4 B1 C7 21(2) . . . . ?
C50 C4 B1 C7 48(3) . . . . ?
C5 C4 B1 C2 83(3) . . . . ?
C50 C4 B1 C2 110(3) . . . . ?
B5 C43 B2 C46 -103(2) . . . . ?
C42 C43 B2 C46 -100(3) . . . . ?
B6 C43 B2 C46 -143(2) . . . . ?
B5 C43 B2 B3 -105(3) . . . . ?
C42 C43 B2 B3 -102(3) . . . . ?
C46 C43 B2 B3 -2(2) . . . . ?
B6 C43 B2 B3 -145(3) . . . . ?
C42 C43 B2 B5 3(2) . . . . ?
C46 C43 B2 B5 103(2) . . . . ?
B6 C43 B2 B5 -40.3(16) . . . . ?
B5 C43 B2 C44 -142(2) . . . . ?
C42 C43 B2 C44 -140(2) . . . . ?
C46 C43 B2 C44 -39.8(14) . . . . ?
B6 C43 B2 C44 177.3(16) . . . . ?
B3 C46 B2 C43 -178(3) . . . . ?
C44 C46 B2 C43 -124(2) . . . . ?
B5 C46 B2 C43 54.2(17) . . . . ?
C44 C46 B2 B3 53.5(19) . . . . ?
C43 C46 B2 B3 178(3) . . . . ?
B5 C46 B2 B3 -128(3) . . . . ?
B3 C46 B2 B5 128(3) . . . . ?
C44 C46 B2 B5 -178.4(19) . . . . ?
C43 C46 B2 B5 -54.2(17) . . . . ?
B3 C46 B2 C44 -53.5(19) . . . . ?
C43 C46 B2 C44 124.3(19) . . . . ?
B5 C46 B2 C44 178.4(19) . . . . ?
B2 C46 B3 C44 102(2) . . . . ?
C43 C46 B3 C44 100(2) . . . . ?
B5 C46 B3 C44 138.0(18) . . . . ?
C44 C46 B3 B2 -102(2) . . . . ?
C43 C46 B3 B2 -2(3) . . . . ?
B5 C46 B3 B2 36.3(18) . . . . ?
B2 C46 B3 B4 102(3) . . . . ?
C44 C46 B3 B4 1(2) . . . . ?
C43 C46 B3 B4 100(3) . . . . ?
B5 C46 B3 B4 139(3) . . . . ?
B2 C46 B3 N7 143(2) . . . . ?
C44 C46 B3 N7 41.3(14) . . . . ?
C43 C46 B3 N7 141(2) . . . . ?
B5 C46 B3 N7 179.3(15) . . . . ?
B4 C44 B3 C46 179(2) . . . . ?
N7 C44 B3 C46 118.7(19) . . . . ?
B2 C44 B3 C46 -59.3(18) . . . . ?
B4 C44 B3 B2 -121(2) . . . . ?
N7 C44 B3 B2 178(2) . . . . ?
C46 C44 B3 B2 59.3(18) . . . . ?
N7 C44 B3 B4 -60.7(18) . . . . ?
C46 C44 B3 B4 -179(2) . . . . ?
B2 C44 B3 B4 121(2) . . . . ?
B4 C44 B3 N7 60.7(18) . . . . ?
C46 C44 B3 N7 -118.7(19) . . . . ?
B2 C44 B3 N7 -178(2) . . . . ?
C43 B2 B3 C46 2(3) . . . . ?
B5 B2 B3 C46 -63(3) . . . . ?
C44 B2 B3 C46 68(2) . . . . ?
C43 B2 B3 C44 -66(3) . . . . ?
C46 B2 B3 C44 -68(2) . . . . ?
B5 B2 B3 C44 -131(3) . . . . ?
C43 B2 B3 B4 -115(3) . . . . ?
C46 B2 B3 B4 -118(3) . . . . ?
B5 B2 B3 B4 180(2) . . . . ?
C44 B2 B3 B4 -50(2) . . . . ?
C43 B2 B3 N7 -63(4) . . . . ?
C46 B2 B3 N7 -66(3) . . . . ?
B5 B2 B3 N7 -128(3) . . . . ?
C44 B2 B3 N7 2(2) . . . . ?
B3 C44 B4 N7 -100(2) . . . . ?
C46 C44 B4 N7 -99(2) . . . . ?
B2 C44 B4 N7 -139.4(17) . . . . ?
N7 C44 B4 B3 100(2) . . . . ?
C46 C44 B4 B3 1(2) . . . . ?
B2 C44 B4 B3 -39.4(17) . . . . ?
B3 C44 B4 C45 -138(2) . . . . ?
N7 C44 B4 C45 -38.5(13) . . . . ?
C46 C44 B4 C45 -138(2) . . . . ?
B2 C44 B4 C45 -177.8(15) . . . . ?
C45 N7 B4 C44 -125.4(19) . . . . ?
B3 N7 B4 C44 55.8(19) . . . . ?
C44 N7 B4 B3 -55.8(19) . . . . ?
C45 N7 B4 B3 179(2) . . . . ?
C44 N7 B4 C45 125.4(19) . . . . ?
B3 N7 B4 C45 -179(2) . . . . ?
C46 B3 B4 C44 -1(3) . . . . ?
B2 B3 B4 C44 71(3) . . . . ?
N7 B3 B4 C44 -64(2) . . . . ?
C46 B3 B4 N7 63(3) . . . . ?
C44 B3 B4 N7 64(2) . . . . ?
B2 B3 B4 N7 135(3) . . . . ?
C46 B3 B4 C45 64(4) . . . . ?
C44 B3 B4 C45 65(3) . . . . ?
B2 B3 B4 C45 136(3) . . . . ?
N7 B3 B4 C45 1(2) . . . . ?
B6 C42 B5 C43 98(2) . . . . ?
C41 C42 B5 C43 94(3) . . . . ?
C47 C42 B5 C43 138.7(19) . . . . ?
C43 C42 B5 B6 -98(2) . . . . ?
C41 C42 B5 B6 -4(2) . . . . ?
C47 C42 B5 B6 41.0(16) . . . . ?
B6 C42 B5 B2 101(3) . . . . ?
C43 C42 B5 B2 3(2) . . . . ?
C41 C42 B5 B2 97(3) . . . . ?
C47 C42 B5 B2 142(2) . . . . ?
B6 C42 B5 C46 139(2) . . . . ?
C43 C42 B5 C46 41.1(15) . . . . ?
C41 C42 B5 C46 135(2) . . . . ?
C47 C42 B5 C46 179.8(14) . . . . ?
B2 C43 B5 C42 177(2) . . . . ?
C46 C43 B5 C42 122(2) . . . . ?
B6 C43 B5 C42 -60.9(17) . . . . ?
B2 C43 B5 B6 -122(2) . . . . ?
C42 C43 B5 B6 60.9(17) . . . . ?
C46 C43 B5 B6 -177(2) . . . . ?
C42 C43 B5 B2 -177(2) . . . . ?
C46 C43 B5 B2 -55.4(16) . . . . ?
B6 C43 B5 B2 122(2) . . . . ?
B2 C43 B5 C46 55.4(16) . . . . ?
C42 C43 B5 C46 -122(2) . . . . ?
B6 C43 B5 C46 177(2) . . . . ?
C43 B2 B5 C42 -3(2) . . . . ?
C46 B2 B5 C42 61(3) . . . . ?
B3 B2 B5 C42 107(3) . . . . ?
C44 B2 B5 C42 59(4) . . . . ?
C46 B2 B5 C43 64(2) . . . . ?
B3 B2 B5 C43 110(3) . . . . ?
C44 B2 B5 C43 62(3) . . . . ?
C43 B2 B5 B6 66(2) . . . . ?
C46 B2 B5 B6 130(2) . . . . ?
B3 B2 B5 B6 176(2) . . . . ?
C44 B2 B5 B6 128(3) . . . . ?
C43 B2 B5 C46 -64(2) . . . . ?
B3 B2 B5 C46 46(2) . . . . ?
C44 B2 B5 C46 -2(2) . . . . ?
C43 C42 B6 B5 59.4(18) . . . . ?
C41 C42 B6 B5 176(2) . . . . ?
C47 C42 B6 B5 -123(2) . . . . ?
B5 C42 B6 C41 -176(2) . . . . ?
C43 C42 B6 C41 -116.7(19) . . . . ?
C47 C42 B6 C41 60.7(15) . . . . ?
B5 C42 B6 C47 123(2) . . . . ?
C43 C42 B6 C47 -177.3(19) . . . . ?
C41 C42 B6 C47 -60.7(15) . . . . ?
B5 C42 B6 C43 -59.4(18) . . . . ?
C41 C42 B6 C43 116.7(19) . . . . ?
C47 C42 B6 C43 177.3(19) . . . . ?
C43 B5 B6 C42 -63(2) . . . . ?
B2 B5 B6 C42 -114(3) . . . . ?
C46 B5 B6 C42 -66(3) . . . . ?
C42 B5 B6 C41 4(3) . . . . ?
C43 B5 B6 C41 -59(3) . . . . ?
B2 B5 B6 C41 -110(3) . . . . ?
C46 B5 B6 C41 -61(4) . . . . ?
C42 B5 B6 C47 -65(2) . . . . ?
C43 B5 B6 C47 -128(2) . . . . ?
B2 B5 B6 C47 -179(2) . . . . ?
C46 B5 B6 C47 -131(3) . . . . ?
C42 B5 B6 C43 63(2) . . . . ?
B2 B5 B6 C43 -51(2) . . . . ?
C46 B5 B6 C43 -3(2) . . . . ?
C38 C41 B6 C42 -94(3) . . . . ?
C47 C41 B6 C42 -95.8(18) . . . . ?
C37 C41 B6 C42 -131.3(18) . . . . ?
C38 C41 B6 B5 -98(3) . . . . ?
C47 C41 B6 B5 -100(3) . . . . ?
C42 C41 B6 B5 -4(2) . . . . ?
C37 C41 B6 B5 -135(2) . . . . ?
C38 C41 B6 C47 1(2) . . . . ?
C42 C41 B6 C47 95.8(18) . . . . ?
C37 C41 B6 C47 -35.5(13) . . . . ?
C38 C41 B6 C43 -137(2) . . . . ?
C47 C41 B6 C43 -138.6(19) . . . . ?
C42 C41 B6 C43 -42.7(15) . . . . ?
C37 C41 B6 C43 -174.0(16) . . . . ?
C37 C47 B6 C42 130(2) . . . . ?
C38 C47 B6 C42 66(2) . . . . ?
C41 C47 B6 C42 67.2(18) . . . . ?
C37 C47 B6 B5 -180(2) . . . . ?
C38 C47 B6 B5 116(3) . . . . ?
C41 C47 B6 B5 117(2) . . . . ?
C42 C47 B6 B5 49.7(19) . . . . ?
C37 C47 B6 C41 63(2) . . . . ?
C38 C47 B6 C41 -1(2) . . . . ?
C42 C47 B6 C41 -67.2(18) . . . . ?
C37 C47 B6 C43 128(3) . . . . ?
C38 C47 B6 C43 63(3) . . . . ?
C41 C47 B6 C43 64(3) . . . . ?
C42 C47 B6 C43 -3(2) . . . . ?
B5 C43 B6 C42 79(2) . . . . ?
B2 C43 B6 C42 130(2) . . . . ?
C46 C43 B6 C42 83(3) . . . . ?
B2 C43 B6 B5 51(2) . . . . ?
C42 C43 B6 B5 -79(2) . . . . ?
C46 C43 B6 B5 4(3) . . . . ?
B5 C43 B6 C41 135(2) . . . . ?
B2 C43 B6 C41 -174(2) . . . . ?
C42 C43 B6 C41 55.6(19) . . . . ?
C46 C43 B6 C41 139(3) . . . . ?
B5 C43 B6 C47 83(3) . . . . ?
B2 C43 B6 C47 134(3) . . . . ?
C42 C43 B6 C47 4(3) . . . . ?
C46 C43 B6 C47 87(4) . . . . ?

_refine_diff_density_max         3.386
_refine_diff_density_min         -6.904
_refine_diff_density_rms         0.500

_shelxl_version_number           2013-2


_atom_sites_special_details      
;
The structure was solved using Patterson Methods, followed by a Tangent Expansion (ShelXS). RE = 0.4, Nqual =   0, Ralpha = 0.265
;
_exptl_crystal_recrystallization_method 
'Re-crystallisation from solvent: methanol'
