Issue 7, 2009
From the journal:

CrystEngComm

The key role of accurate lattice parameters in revealing subtle structural differences—a case study in the system [Ln(phen/phen-d8)2(NO3)3]†

Franz Werner,*a   Kentaro Tada,a   Ayumi Ishii,a   Masaki Takatab  and  Miki Hasegawa*ac  

* Corresponding authors

a Aoyama-Gakuin University, College of Science and Engineering, Department of Chemistry and Biological Science, 5-10-1 Fuchinobe, Sagamihara, Kanagawa, Japan
E-mail: fwerner@mail.zserv.tuwien.ac.at, hasemiki@chem.aoyama.ac.jp
Fax: +81-(0)42-759-6493
Tel: +81-(0)42-759-6220

b RIKEN/SPring-8, 1-1-1 Kouto, Sayo-cho, Sayo-gun, Hyogo, Japan

c Institute of Molecular Science, Okazaki, Aichi, Japan

Abstract

In the model system [Ln(phen/phen-d8)2(NO3)3] (Ln = Eu3+, Tb3+) the assignment of a new modification, based on the unit cell volumes, demonstrates the superior angular accuracy of synchrotron powder diffraction and the value of the lattice parameters refined thereof.

Graphical abstract: The key role of accurate lattice parameters in revealing subtle structural differences—a case study in the system [Ln(phen/phen-d8)2(NO3)3]

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Article information

DOI
https://doi.org/10.1039/B904694C
Article type
Communication
Submitted
06 Mar 2009
Accepted
17 Mar 2009
First published
06 Apr 2009

CrystEngComm, 2009,11, 1197-1200

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The key role of accurate lattice parameters in revealing subtle structural differences—a case study in the system [Ln(phen/phen-d8)2(NO3)3]

F. Werner, K. Tada, A. Ishii, M. Takata and M. Hasegawa, CrystEngComm, 2009, 11, 1197 DOI: 10.1039/B904694C

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