Two chain gallium fluorodiphosphates: synthesis, structure solution, and their transient presence during the hydrothermal crystallisation of a microporous gallium fluorophosphate

Franck Millange; Richard I. Walton; Nathalie Guillou; Thierry Loiseau; Dermot O’Hare; Gérard Férey

doi:10.1039/B201178F

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Two chain gallium fluorodiphosphates: synthesis, structure solution, and their transient presence during the hydrothermal crystallisation of a microporous gallium fluorophosphate†

Franck Millange,*^a Richard I. Walton,^b Nathalie Guillou,^a Thierry Loiseau,^a Dermot O’Hare^c and Gérard Férey^a

Author affiliations

* Corresponding authors

^a Institut Lavoisier, UMR CNRS 8637, Université de Versailles Saint-Quentin-en-Yvelines, 45 Avenue des Etats-Unis, 78035, Versailles cedex, France
E-mail: millange@chimie.uvsq.fr

^b School of Chemistry, University of Exeter, Stocker Road, Exeter, Devon, UK

^c Inorganic Chemistry Laboratory, University of Oxford, South Parks Road, Oxford, UK

Abstract

Two novel gallium fluorodiphosphates have been isolated and their structures solved ab initio from powder X-ray diffraction data; the materials readily interconvert under hydrothermal conditions, and are metastable with respect to an open-framework zeolitic gallium fluorophosphate, during the synthesis of which they are present as transient intermediates.

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Supplementary files

crystal data, atomic coordinates and metrical data for 1 and 2 DOC (49K)

Article information

DOI: https://doi.org/10.1039/B201178F
Article type: Communication
Submitted: 01 Feb 2002
Accepted: 07 Mar 2002
First published: 18 Mar 2002

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Chem. Commun., 2002, 826-827

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Two chain gallium fluorodiphosphates: synthesis, structure solution, and their transient presence during the hydrothermal crystallisation of a microporous gallium fluorophosphate

F. Millange, R. I. Walton, N. Guillou, T. Loiseau, D. O’Hare and G. Férey, Chem. Commun., 2002, 826 DOI: 10.1039/B201178F

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Chemical Communications

Two chain gallium fluorodiphosphates: synthesis, structure solution, and their transient presence during the hydrothermal crystallisation of a microporous gallium fluorophosphate†

Abstract

Supplementary files

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Two chain gallium fluorodiphosphates: synthesis, structure solution, and their transient presence during the hydrothermal crystallisation of a microporous gallium fluorophosphate

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