Synthesis, spectroscopic properties and molecular structure of the paramagnetic complex [(η5-3,5-di-tert-butyl-1,2,4-triphosphacyclopentadienyl)(η5-2,4,5-tri-tert-butyl-1,3-diphosphacyclopentadienyl)]vanadium(II)

F. Geoffrey N. Cloke; Kevin R. Flower; Peter B. Hitchcock; John F. Nixon

doi:10.1039/C39950001659

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Synthesis, spectroscopic properties and molecular structure of the paramagnetic complex [(η⁵-3,5-di-tert-butyl-1,2,4-triphosphacyclopentadienyl)(η⁵-2,4,5-tri-tert-butyl-1,3-diphosphacyclopentadienyl)]vanadium(II)

F. Geoffrey N. Cloke, Kevin R. Flower, Peter B. Hitchcock and John F. Nixon

Abstract

Cocondensation of vanadium vapour with the phosphaalkyne Bu^tCP affords the paramagnetic complex [V(η⁵-P₃C₂Bu^t₂)(η⁵-P₂C₃Bu^t₃)], whose molecular structure is determined by a single crystal X-ray diffraction study.

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DOI: https://doi.org/10.1039/C39950001659
Article type: Paper

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J. Chem. Soc., Chem. Commun., 1995, 1659-1660

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Synthesis, spectroscopic properties and molecular structure of the paramagnetic complex [(η⁵-3,5-di-tert-butyl-1,2,4-triphosphacyclopentadienyl)(η⁵-2,4,5-tri-tert-butyl-1,3-diphosphacyclopentadienyl)]vanadium(II)

F. G. N. Cloke, K. R. Flower, P. B. Hitchcock and J. F. Nixon, J. Chem. Soc., Chem. Commun., 1995, 1659 DOI: 10.1039/C39950001659

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Journal of the Chemical Society, Chemical Communications

Synthesis, spectroscopic properties and molecular structure of the paramagnetic complex [(η⁵-3,5-di-tert-butyl-1,2,4-triphosphacyclopentadienyl)(η⁵-2,4,5-tri-tert-butyl-1,3-diphosphacyclopentadienyl)]vanadium(II)

Abstract

Article information

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Synthesis, spectroscopic properties and molecular structure of the paramagnetic complex [(η⁵-3,5-di-tert-butyl-1,2,4-triphosphacyclopentadienyl)(η⁵-2,4,5-tri-tert-butyl-1,3-diphosphacyclopentadienyl)]vanadium(II)

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