Issue 2, 1977

Preparation of macrocyclic compounds by thermal dimerization of 1,10-phenanthroline derivatives

Abstract

An efficient non-template synthesis of a new macrocycle, a conjugated tautomer of 1,14 : 7,8-diethenotetrapyrido-[2,1,6-cd:2′,1′,6′-gh :2″,1″,6″-jk:2‴,1‴,6‴-na][1,4,8,11]tetra-azacyclotetradecine (3), is described. The thermal behaviour of several disubstituted 1,10-phenanthrolines towards dimerization is studied by use of differential thermal analysis and thermogravimetric analysis, and some spectroscopic properties of the macrocycles produced are described.

Article information

Article type
Paper

J. Chem. Soc., Perkin Trans. 1, 1977, 214-216

Preparation of macrocyclic compounds by thermal dimerization of 1,10-phenanthroline derivatives

S. Ogawa, J. Chem. Soc., Perkin Trans. 1, 1977, 214 DOI: 10.1039/P19770000214

To request permission to reproduce material from this article, please go to the Copyright Clearance Center request page.

If you are an author contributing to an RSC publication, you do not need to request permission provided correct acknowledgement is given.

If you are the author of this article, you do not need to request permission to reproduce figures and diagrams provided correct acknowledgement is given. If you want to reproduce the whole article in a third-party publication (excluding your thesis/dissertation for which permission is not required) please go to the Copyright Clearance Center request page.

Read more about how to correctly acknowledge RSC content.

Spotlight

Advertisements